6004_DukeMcGuireLF1_July2016_2ndSemiAnnual_DIN26823_20161005

McGuire Nuclear Station – Landfill #1
(Unlined) Permit No. 6004
Semiannual Groundwater
Monitoring Report
July 2016 Sampling Event

October 4, 2016

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
July 2016 Sampling Event
CONTENTS

ii

Contents
Page
Report Verification ......................................................................................................................... i
Contents ........................................................................................................................................ ii
Section 1 - Background ................................................................................................................. 1
Section 2 - Methods ...................................................................................................................... 3
2.1 Sampling and Analysis Methods .................................................................................... 3
2.2 Statement of Work .......................................................................................................... 4
Section 3 - Results ........................................................................................................................ 5
3.1 Site Groundwater Flow ................................................................................................... 5
3.2 Analytical Results ........................................................................................................... 5

FIGURES
1. Site Location Map
2. Sample Locations
3. Generalized Groundwater Surface Contours
TABLES
1. Well Construction Information
2. Groundwater Flow Velocities
3. Field Data Parameters
4. Groundwater Field and Analytical Results
5. Field and Analytical Results that Equal or Exceed 15A NCAC 2L Groundwater Quality
Standards
6. Surface Water Field and Analytical Results
7. Field and Analytical Results that Equal or Exceed 15A NCAC 2B Surface Water Quality
Standards
8. Radiological Analytical Results
APPENDICES
A. Field Sampling Forms
B. Laboratory Report and Chain-of-Custody Forms
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
July 2016 Sampling Event
SECTION 1 - BACKGROUND

1

Section 1 - Background
The McGuire Nuclear Station Landfill #1 (Unlined)1 is located at the Duke Energy Carolinas,
LLC (Duke Energy) McGuire Nuclear Station in Mecklenburg County, North Carolina. The
landfill is closed and no longer accepts waste. The landfill and nearby area are depicted on
Figure 1. The approximate limit of waste is shown on Figure 2.
The landfill is located south of NC Highway 73, east of the Catawba River, and to the west of
Cashion Road. Cashion Road runs along a topographic divide with topography sloping away
from Cashion Road to the northwest and to the southeast. Surface water to the northwest of
Cashion Road drains towards the Catawba River. There are two surface water drainage
features adjacent to the landfill. The surface water drainage feature located to the north of the
landfill contains an unnamed perennial stream that drains to the northwest towards another
perennial unnamed stream that flows to the Catawba River. The surface water drainage feature
located to the south and west of the landfill also drains to an unnamed stream that flows to the
Catawba River.
As described in the Sampling and Analysis Plan2 (SAP), the monitoring system at the landfill
consists of the following:
Monitoring Wells: MW-1
MW-1D
MW-2A
MW-2D
MW-3
MW-3D
MW-4
MW-4D
MW-11
MW-11D
MW-12
MW-12D
MW-4R
MW-4DR

Surface Water Sample Location: SW-1

The monitoring wells and the surface water sample location are shown on Figure 2. The wells
were installed as well pairs with one shallow well and one deeper well adjacent to each other.
The well with the “D” designation is the deeper well in each well pair. The shallow wells are
1 In response to the North Carolina Division of Public Health, Radiation Protection Section, November 17,
2006, letter to Duke Energy, LLC, Duke Energy offered to indicate the McGuire Nuclear Station Landfill
#1 as (Unlined) in reports.
2 McGuire Nuclear Station Landfill #1, Permit Number 60-04, Ground-Water Monitoring Program
Sampling and Analysis Plan (SAP), September 14, 1996, Revised, November 24, 1997, March 9, 2001.

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
July 2016 Sampling Event
SECTION 1 - BACKGROUND

2

screened to intercept the water table. The deep wells are constructed so that the bottom of the
screen is located in residual material just above auger refusal. Monitoring wells MW-1 and
MW-1D are located upgradient of the landfill.
Monitoring wells MW-4R and MW-4DR are not included in the SAP. These wells were installed
in December 2013 as replacement wells for MW-4 and MW-4D, respectively. Monitoring wells
MW-4 and MW-4D are approximately 15 feet outside of the waste boundary. The replacement
wells were installed in the vicinity of MW-4 and MW-4D and are located near the review
boundary. Table 1 presents well construction information for the landfill monitoring wells.
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
July 2016 Sampling Event
SECTION 2 - METHODS

3

Section 2 - Methods
2.1 Sampling and Analysis Methods
The collection of samples and documentation of sampling was performed by Duke Energy
personnel (Field Certification #5193) according to the North Carolina Solid Waste Management
Guidelines. Copies of the field sampling forms are included in Appendix A. The parameters and
constituents reported were selected by Duke Energy and the North Carolina Department of
Environmental Quality (NCDEQ) Division of Solid Waste and were analyzed by TestAmerica
Laboratories, Inc. (North Carolina Laboratory Certification #387) and the Duke Energy Analytical
Laboratory (North Carolina Laboratory Certification #248).
The groundwater and surface water samples were analyzed for the following constituents in
accordance with the SAP:
 Barium, chromium, and silver using Solid Waste (SW)-8463 Method 6010D
 Arsenic, cadmium, lead, and selenium using SW-846 Method 6020B
 Mercury using SW-846 Method 7470A
 Sulfate using SW-846 Method 9056A
 Volatile organic compounds (VOCs) using SW-846 Method 8260B
Surface water sample SW-1 was field-filtered and analyzed for the dissolved fraction of the
following constituents:
 Barium, chromium, and silver using SW-846 Method 6010D
 Arsenic, cadmium, and lead using SW-846 Method 6020B
In addition, the following analyses were performed in accordance with the requirements of the
Radioactive Materials License No. 060-0379-7 issued by the North Carolina Department of
Health and Human Services Radiation Protection Section:
 Gross alpha radioactivity using EPA Method 900
 Gross beta radioactivity using EPA Method 900
 Tritium using EPA Method 906.0 Modified
 Gamma radioactivity for select isotopes

 3 EPA Hazardous Waste Test Methods (SW-846); available online at https://www.epa.gov/hw-sw846
(Accessed August 30, 2016)
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
July 2016 Sampling Event
SECTION 2 - METHODS

4

1 EPA Hazardous Waste Test Methods (SW-846); available online at https://www.epa.gov/hw-sw846
(Accessed August 30, 2016)
2.2 Statement of Work
HDR completed the following tasks:
 Received field sampling information provided by Duke Energy (performed by Duke
Energy personnel) for monitoring wells MW-1, MW-1D, MW-2A, MW-2D, MW-3, MW-3D,
MW-4, MW-4R, MW-4D, MW-4DR, MW-11, MW-11D, MW-12, and MW-12D. Data was
also received for surface water sample location SW-1. The samples were collected on
July 13, 2016, and HDR received the data on August 26, 2016. The field sampling forms
are included in Appendix A.
 Reviewed the laboratory analytical results for the samples. The Electronic Data
Deliverable (EDD) provided by Duke Energy was adapted to conform to the format
requirements of the NCDEQ EDD template. HDR added an italicized J data qualifier (J)
to indicate a measured concentration that is equal to or greater than the laboratory’s
method reporting limit (MRL) but is less than the Solid Waste Section Limit4 (SWSL). A
copy of the original EDD is retained in HDR’s files.
 Developed a generalized groundwater surface contour map using map data and
groundwater elevation data supplied by Duke Energy. Calculated groundwater flow
velocities based on groundwater surface contours.
 Prepared and submitted this Semiannual Groundwater Monitoring Report to Duke
Energy.
4 The Solid Waste Section Limit (SWSL) is defined by NCDEQ as the lowest amount of analyte in a
sample that can be quantitatively determined with suitable precision and accuracy. The SWSL is the
concentration below which reported results must be qualified as estimated. NCDEQ Division of Waste
Management Memorandum dated February 23, 2007.
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
July 2016 Sampling Event
SECTION 3 - RESULTS

5

Section 3 - Results
3.1 Site Groundwater Flow
Generalized groundwater surface contours and groundwater flow direction arrows for the site
are shown on Figure 3. These contours were developed using groundwater elevations
measured at the shallow wells on the date of sampling. Calculated flow velocities are presented
in Table 2.
Groundwater flow in the area of the landfill is generally from the southeast near MW-1/MW-1D
and Cashion Road, toward the northwest, toward MW-3/MW-3D, MW-4/MW-4D, and
MW-4R/MW-4DR.
3.2 Analytical Results
A summary of the field data is presented in Table 3.
The field and analytical results of groundwater samples collected from the monitoring wells are
summarized in Table 4. The analytical results for these samples are compared to the
groundwater standards found in Title 15A NCAC 02L .0202 (g) (2L Standards). Concentrations
with values that attain or exceed the 2L Standards are noted on Table 4 by bold font. A
summary of the field and analytical results that attain or exceed the 2L Standards and a
preliminary analysis of the cause and significance of the exceedances are presented in Table 5.
Surface water sample location SW-1 is located on an unnamed stream. The unnamed stream is
a tributary to the Catawba River which is classified by the NCDEQ Division of Water Quality as
Class WS-IV water at its confluence with the unnamed stream. As a result, the field and
analytical results from this location are compared to Title 15A, North Carolina Administrative
Code (NCAC), Subchapter 2B Standards (2B Standards) for Class WS-IV water. The field and
analytical results of surface water sampling are summarized in Table 6. Concentrations with
values that attain or exceed the 2B Standards are noted on Table 6 by bold font. A summary of
the field and analytical results that attain or exceed the 2B Standards and a preliminary analysis
of the cause and significance of the exceedances are presented in Table 7.
The minimum detection limit (MDL) was greater than the respective 2L Standard for the
following constituents:
 1,2,3-Trichloropropane
 1,2-Dibromo-3-chloropropane
 1,2-Dibromoethane (EDB)
 Vinyl chloride

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
July 2016 Sampling Event
SECTION 3 - RESULTS

6

The MDL was greater than the respective 2B Standard for the following constituents:
 Mercury
 Silver, dissolved
The MDLs for the listed constituents were all below their corresponding SWSLs as required by
the February 23, 2007, NCDEQ memo5. With the exception of the dissolved silver concentration
at SW-1 these constituents were not detected above the MDL in the analyzed samples and are
not considered to exceed their respective 2L or 2B Standards.
Analytical results with values that equal or are greater than the SWSLs are noted in Table 4 by
gray cells.
The results of the radiological analysis are presented in Table 8. A copy of this report has been
submitted to the North Carolina Department of Health and Human Services Radiation Protection
Section for reference. HDR did not evaluate this data.
Select samples were diluted, as is normal laboratory practice, to bring samples within the
calibrated range of the analysis. Specifics regarding the samples that were diluted, including the
dilution amount, are reported in the EDD. The laboratory reports and chain-of-custody forms can
be found in Appendix B.

5 The Solid Waste Section Limit (SWSL) is defined by NCDEQ as the lowest amount of analyte in a
sample that can be quantitatively determined with suitable precision and accuracy. The SWSL is the
concentration below which reported results must be qualified as estimated. NCDEQ Division of Waste
Management Memorandum dated February 23, 2007.

Figures

Tables

Ta
b
l
e

1

-

W
e
l
l

C
o
n
s
t
r
u
c
t
i
o
n

I
n
f
o
r
m
a
t
i
o
n
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
La
t
i
t
u
d
e

L
o
n
g
i
t
u
d
e
MW
-
1

7
/
1
8
/
1
9
8
9

3
5
.
4
1
1
4
5
5
7

-
8
0
.
9
4
7
6
0
7
8

7
3
0
.
2
3

7
2
9
.
5
8

0
.
6
5

7
0
1
.
8
0

2
8
.
4
3

6
8
.
5
5

5
8
.
5
5

5
8
.
5
5
-
6
8
.
5
5

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
1
D

7
/
2
0
/
1
9
8
9

3
5
.
4
1
1
4
7
3
7

-
8
0
.
9
4
7
6
0
4
7

7
3
0
.
6
1

7
2
9
.
7
5

0
.
8
6

7
0
1
.
3
0

2
9
.
3
1

8
8
.
2
2

7
8
.
2
2

7
8
.
2
2
-
8
8
.
2
2

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
2
A

7
/
2
1
/
1
9
8
9

3
5
.
4
1
3
0
6
3
9

-
8
0
.
9
4
9
0
5
1
7

7
3
9
.
6
7

7
3
6
.
9
6

2
.
7
1

6
8
8
.
4
1

5
1
.
2
6

7
7
.
5
7

6
7
.
5
7

6
7
.
5
7
-
7
7
.
5
7

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
2
D

7
/
2
0
/
1
9
8
9

3
5
.
4
1
3
0
8
0
8

-
8
0
.
9
4
9
0
9
2
0

7
4
0
.
7
7

7
3
7
.
4
1

3
.
3
6

6
8
7
.
4
6

5
3
.
3
1

1
0
8
.
8
2

9
8
.
8
2

9
8
.
8
2
-
1
0
8
.
8
2

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
3

7
/
1
0
/
1
9
8
9

3
5
.
4
1
4
0
7
0
5

-
8
0
.
9
5
0
4
8
6
8

7
2
8
.
4
3

7
2
4
.
9
8

3
.
4
5

6
7
1
.
5
8

5
6
.
8
5

7
3
.
6
4

6
3
.
6
4

6
3
.
6
4
-
7
3
.
6
4

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
3
D

7
/
1
0
/
1
9
8
9

3
5
.
4
1
4
0
6
8
1

-
8
0
.
9
5
0
5
0
3
8

7
2
8
.
3
9

7
2
4
.
9
8

3
.
4
1

6
7
1
.
5
8

5
6
.
8
1

9
0
.
1
9

8
0
.
1
9

8
0
.
1
9
-
9
0
.
1
9

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
4

7
/
6
/
1
9
8
9

3
5
.
4
1
3
4
8
8
9

-
8
0
.
9
5
1
1
5
3
3

7
4
1
.
1
3

7
3
8
.
4
0

2
.
7
3

6
7
7
.
1
0

6
4
.
0
3

7
4
.
1
5

6
4
.
1
5

6
4
.
1
5
-
7
4
.
1
5

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
4
D

7
/
6
/
1
9
8
9

3
5
.
4
1
3
4
7
9
1

-
8
0
.
9
5
1
1
6
6
5

7
4
0
.
5
8

7
3
8
.
2
5

2
.
3
3

6
7
6
.
1
4

6
4
.
4
4

1
0
2
.
2
4

9
2
.
2
4

9
2
.
2
4
-
1
0
2
.
2
4

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
1
1

1
2
/
1
5
/
2
0
0
4

3
5
.
4
1
1
3
8
2
9

-
8
0
.
9
5
0
4
9
7
9

7
2
2
.
6
0

7
2
0
.
1
0

2
.
5
0

6
9
2
.
2
6

3
0
.
3
4

3
8
.
4
5

2
3
.
4
5

2
3
.
4
5
-
3
8
.
4
5

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
1
1
D

1
2
/
1
5
/
2
0
0
4

3
5
.
4
1
1
3
8
8
5

-
8
0
.
9
5
0
4
7
2
5

7
2
3
.
1
4

7
2
0
.
8
4

2
.
3
0

6
9
1
.
9
4

3
1
.
2
0

1
0
1
.
5
5

9
1
.
5
5

9
1
.
5
5
-
1
0
1
.
5
5

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
1
2

1
2
/
1
5
/
2
0
0
4

3
5
.
4
1
1
0
0
4
7

-
8
0
.
9
4
9
1
7
2
3

7
2
4
.
8
1

7
2
2
.
2
1

2
.
6
0

6
9
9
.
6
0

2
5
.
2
1

2
9
.
4
9

1
4
.
4
9

1
4
.
4
9
-
2
9
.
4
9

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
1
2
D

1
2
/
1
5
/
2
0
0
4

3
5
.
4
1
1
0
1
4
7

-
8
0
.
9
4
9
2
0
9
3

7
2
4
.
7
7

7
2
2
.
2
1

2
.
5
6

6
9
8
.
6
7

2
6
.
1
0

6
8
.
4
2

5
8
.
4
2

5
8
.
4
2
-
6
8
.
4
2

P
W
R

2

P
V
C
MW
-
4
R

1
2
/
4
/
2
0
1
3

3
5
.
4
1
3
4
1
2
3

-
8
0
.
9
5
1
6
1
0
5

7
1
3
.
8
7

7
1
1
.
1
5

2
.
7
2

6
7
5
.
5
1

3
8
.
3
6

4
5
.
7
3

3
0
.
7
2

3
0
.
7
2
-
4
5
.
7
3

S
a
p
r
o
l
i
t
e

2

P
V
C
MW
-
4
D
R

1
2
/
4
/
2
0
1
3

3
5
.
4
1
3
3
9
6
9

-
8
0
.
9
5
1
6
2
0
5

7
1
3
.
7
5

7
1
1
.
1
5

2
.
6
0

6
7
4
.
9
8

3
8
.
7
7

9
0
.
4
0

7
5
.
2
0

7
5
.
2
0
-
9
0
.
4
0

S
a
p
r
o
l
i
t
e

2

P
V
C
No
t
e
s
:
1
.

T
O
C

i
n
d
i
c
a
t
e
s

t
o
p

o
f

c
a
s
i
n
g
.
2
.

f
t
.

i
n
d
i
c
a
t
e
s

f
e
e
t
.
3
.

i
n
.

i
n
d
i
c
a
t
e
s

i
n
c
h
e
s

n
o
m
i
n
a
l

d
i
a
m
e
t
e
r
.
4
.

P
V
C

i
n
d
i
c
a
t
e
s

p
o
l
y
v
i
n
y
l

c
h
l
o
r
i
d
e
.
5
.

P
W
R

i
n
d
i
c
a
t
e
s

p
a
r
t
i
a
l
l
y

w
e
a
t
h
e
r
e
d

r
o
c
k
.
6
.

H
o
r
i
z
o
n
t
a
l

d
a
t
u
m

N
A
D
8
3
.
7
.

V
e
r
t
i
c
a
l

d
a
t
u
m

i
s

N
A
V
D

8
8
.
8
.

D
e
p
t
h

t
o

g
r
o
u
n
d
w
a
t
e
r

g
a
u
g
e
d

o
n

J
u
l
y

1
3
,

2
0
1
6
.
9
.

I
n
f
o
r
m
a
t
i
o
n

p
r
o
v
i
d
e
d

b
y

D
u
k
e

E
n
e
r
g
y
.
10
.

T
o
t
a
l

w
e
l
l

d
e
p
t
h
s

f
r
o
m

2
0
1
5

w
e
l
l

d
e
p
t
h

c
o
n
f
i
r
m
a
t
i
o
n
.
11
.

T
o
p

o
f

C
a
s
i
n
g

a
n
d

G
r
o
u
n
d

S
u
r
f
a
c
e

E
l
e
v
e
t
i
o
n
s

f
r
o
m

J
a
n
u
a
r
y

2
0
1
5

r
e
-
s
u
r
v
e
y

b
y

P
r
o
v
i
d
e
n
c
e

L
a
n
d

G
r
o
u
p
.
Co
o
r
d
i
n
a
t
e
s
We
l
l

I
D
We
l
l

In
s
t
a
l
l
a
t
i
o
n

Da
t
e
W
e
l
l

T
O
C

Ele
v
a
t
i
o
n

(
f
t
.
)
Gr
o
u
n
d

S
u
r
f
a
c
e

Ele
v
a
t
i
o
n
(f
t
.
)
Sc
r
e
e
n
e
d

I
n
t
e
r
v
a
l

be
l
o
w

T
O
C
(f
t
.
)
Casing TypeWell Diameter (in.)Geology of Screened Interval
We
l
l

S
t
i
c
k
-
u
p

He
i
g
h
t

A
b
o
v
e

Gr
o
u
n
d

S
u
r
f
a
c
e
(f
t
.
)
Gr
o
u
n
d
w
a
t
e
r

Ele
v
a
t
i
o
n
(ft
.
)
De
p
t
h

t
o

W
a
t
e
r

be
l
o
w

T
O
C
(ft
.
)
To
t
a
l

W
e
l
l

De
p
t
h

b
e
l
o
w

TO
C
(f
t
.
)
De
p
t
h

t
o

T
o
p

o
f

Sc
r
e
e
n

f
r
o
m

T
O
C
(f
t
.
)
Page  1  of  1
Ta
b
l
e

2

-

G
r
o
u
n
d
w
a
t
e
r

F
l
o
w

V
e
l
o
c
i
t
i
e
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
We
l
l

I
D

U
p
g
r
a
d
i
e
n
t

Gr
o
u
n
d
w
a
t
e
r

Co
n
t
o
u
r

El
e
v
a
t
i
o
n
(f
t
)
D
o
w
n
g
r
a
d
i
e
n
t

Gr
o
u
n
d
w
a
t
e
r

Co
n
t
o
u
r

E
l
e
v
a
t
i
o
n
(f
t
)
Li
n
e
a
r

Di
s
t
a
n
c
e

Be
t
w
e
e
n

Co
n
t
o
u
r
s

th
r
o
u
g
h

W
e
l
l
(f
t
)
Hy
d
r
a
u
l
i
c

Gr
a
d
i
e
n
t

(f
t
/
f
t
)
Hy
d
r
a
u
l
i
c

Co
n
d
u
c
t
i
v
i
t
y

(f
t
/
d
a
y
)
Ef
f
e
c
t
i
v
e

Po
r
o
s
i
t
y

(%
/
1
0
0
)
Groundwater Velocity (ft/day)
MW
-
1

7
0
1
.
8
0

7
0
0

4
9

0
.
0
4

0
.
4
1

0
.
2
5
9

0
.
0
6
MW
-
2
A

6
9
0

6
8
8

1
0
4

0
.
0
2

0
.
4
1

0
.
2
5
9

0
.
0
3
MW
-
3

6
7
2

6
7
0

7
2

0
.
0
3

0
.
4
1

0
.
2
5
9

0
.
0
4
MW
-
4

6
7
8

6
7
6

9
7

0
.
0
2

0
.
4
1

0
.
2
5
9

0
.
0
3
MW
-
1
1

6
9
4

6
9
2

9
8

0
.
0
2

0
.
4
1

0
.
2
5
9

0
.
0
3
MW
-
1
2

7
0
0

6
9
8

1
0
3

0
.
0
2

0
.
4
1

0
.
2
5
9

0
.
0
3
MW
-
4
R

6
7
6

6
7
5
.
5
1

6
9

0
.
0
1

0
.
4
1

0
.
2
5
9

0
.
0
1
No
t
e
s
:
1
.

L
i
n
e
a
r

d
i
s
t
a
n
c
e

m
e
a
s
u
r
e
d

t
h
r
o
u
g
h

m
o
n
i
t
o
r
i
n
g

w
e
l
l
s

i
s

g
e
n
e
r
a
l
l
y

p
e
r
p
e
n
d
i
c
u
l
a
r

t
o

g
r
o
u
n
d
w
a
t
e
r

c
o
n
t
o
u
r
s
.
2
.

A
t

m
o
n
i
t
o
r
i
n
g

w
e
l
l

l
o
c
a
t
i
o
n
s

w
h
e
r
e

d
o
w
n
g
r
a
d
i
e
n
t

c
o
n
t
o
u
r
s

a
r
e

n
o
t

p
r
e
s
e
n
t
,

t
h
e

g
r
o
u
n
d
w
a
t
e
r

e
l
e
v
a
t
i
o
n

a
t

t
h
e

m
o
n
i
t
o
r
i
n
g

w
e
l
l

i
s

u
s
e
d

a
s

t
h
e

d
o
w
n
g
r
a
d
i
e
n
t

g
r
o
u
n
d
w
a
t
e
r

e
l
e
v
a
t
i
o
n
.
3
.

A
t

m
o
n
i
t
o
r
i
n
g

w
e
l
l

l
o
c
a
t
i
o
n
s

w
h
e
r
e

u
p
g
r
a
d
i
e
n
t

c
o
n
t
o
u
r
s

a
r
e

n
o
t

p
r
e
s
e
n
t
,

t
h
e

g
r
o
u
n
d
w
a
t
e
r

e
l
e
v
a
t
i
o
n

a
t

t
h
e

m
o
n
i
t
o
r
i
n
g

w
e
l
l

i
s

u
s
e
d

a
s

t
h
e

u
p
g
r
a
d
i
e
n
t

g
r
o
u
n
d
w
a
t
e
r

e
l
e
v
a
t
i
o
n
.
4
.

M
o
n
i
t
o
r
i
n
g

w
e
l
l
s

a
r
e

n
o
t

l
i
s
t
e
d

w
h
e
r
e

i
n
s
u
f
f
i
c
i
e
n
t

g
r
o
u
n
d
w
a
t
e
r

c
o
n
t
o
u
r

i
n
f
o
r
m
a
t
i
o
n

i
s

a
v
a
i
l
a
b
l
e

t
o

c
a
l
c
u
l
a
t
e

v
e
l
o
c
i
t
y
.
5
.

H
y
d
r
a
u
l
i
c

g
r
a
d
i
e
n
t
s

a
n
d

g
r
o
u
n
d
w
a
t
e
r

v
e
l
o
c
i
t
i
e
s

a
r
e

a
p
p
r
o
x
i
m
a
t
e
.
6
.

H
y
d
r
a
u
l
i
c

c
o
n
d
u
c
t
i
v
i
t
y

p
r
e
s
e
n
t
e
d

i
s

t
h
e

g
e
o
m
e
t
r
i
c

m
e
a
n

o
f

t
h
e

c
o
n
d
u
c
t
i
v
i
t
y

d
a
t
a

f
o
r

t
h
e

a
l
l
u
v
i
u
m
/
s
o
i
l
/
s
a
p
r
o
l
i
t
e

a
n
d

P
W
R

h
y
d
r
o
s
t
r
a
t
i
g
r
a
p
h
i
c

l
a
y
e
r

i
n

t
h
e

H
D
R

C
o
n
d
u
c
t
i
v
i
t
y

D
a
t
a
b
a
s
e

(
u
n
p
u
b
l
i
s
h
e
d

d
a
t
a

f
r
o
m

P
i
e
d
m
o
n
t

C
a
r
o
l
i
n
a

s
i
t
e
s

w
i
t
h

f
o
l
i
a
t
e
d
/
l
ay
e
r
e
d

b
e
d
r
o
c
k
)
.
7
.

E
f
f
e
c
t
i
v
e

p
o
r
o
s
i
t
y

p
r
e
s
e
n
t
e
d

i
s

t
h
e

m
e
a
n

v
a
l
u
e

o
f

t
h
e

a
l
l
u
v
i
u
m
/
s
o
i
l
/
s
a
p
r
o
l
i
t
e

a
n
d

P
W
R

h
y
d
r
o
s
t
r
a
t
i
g
r
a
p
h
i
c

l
a
y
e
r

e
s
t
i
m
a
t
e
d

f
r
o
m

s
o
i
l

t
e
s
t
i
n
g

u
s
i
n
g

F
e
t
t
e
r
/
B
e
a
r

D
i
a
g
r
a
m
s
.

8
.

H
y
d
r
a
u
l
i
c

g
r
a
d
i
e
n
t

a
n
d

g
r
o
u
n
d
w
a
t
e
r

v
e
l
o
c
i
t
i
e
s

a
r
e

b
a
s
e
d

o
n

J
u
l
y

1
3
,

2
0
1
6

m
e
a
s
u
r
e
d

w
a
t
e
r

e
l
e
v
a
t
i
o
n
s
.
Page 1 of 1
Ta
b
l
e

3

-

F
i
e
l
d

D
a
t
a

P
a
r
a
m
e
t
e
r
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
DA
T
E
SA
M
P
L
E

I
D
WE
L
L
DE
P
T
H
(f
e
e
t
)
DE
P
T
H

T
O
WA
T
E
R
(f
e
e
t
)
WA
T
E
R
EL
E
V
.
(f
e
e
t
)

A
P
P
E
A
R
A
N
C
E
OD
O
R
PU
R
G
E
ME
T
H
O
D

PU
M
P

R
A
T
E
(m
L
/
m
i
n
)
WE
L
L
VO
L
U
M
E
(g
a
l
)
EV
A
C
VO
L
U
M
E
(g
a
l
)
EV
A
C
(y
e
s
/
n
o
)
TE
M
P
(d
e
g

C
)
SP
E
C
I
F
I
C
CO
N
D
U
C
T
A
N
C
E
(µ
Լ /c
m
)
pH
(S
U
)
TURBIDITY (NTU)ORP (mV-NHE)DO (mg/L)
7/
1
3
/
2
0
1
6

M
W
-
1

6
8
.
5
5

2
8
.
4
3

7
0
1
.
8
0

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

6
.
5
4

2
0
.
2
5

N
O

1
6
.
5
5

1
1
0

6
.
2

4
.
4

2
6
5

0
.
3
5
7/
1
3
/
2
0
1
6

M
W
-
1
D

8
8
.
2
2

2
9
.
3
1

7
0
1
.
3
0

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

9
.
6
1

2
9
.
2
5

N
O

1
6
.
3
6

9
9

6
.
2

3
.
4

2
6
7

0
.
1
2
7/
1
3
/
2
0
1
6

M
W
-
2
A

7
7
.
5
7

5
1
.
2
6

6
8
8
.
4
1

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

4
.
2
9

1
3
.
5
0

N
O

1
7
.
4
7

9
8

6
.
5

2
.
2

4
9
6

5
.
8
2
7/
1
3
/
2
0
1
6

M
W
-
2
D

1
0
8
.
8
2

5
3
.
3
1

6
8
7
.
4
6

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

9
.
0
5

1
9
.
2
5

N
O

1
7
.
0
5

6
0

6
.
9

3
.
0

4
8
9

9
.
5
4
7/
1
3
/
2
0
1
6

M
W
-
3

7
3
.
6
4

5
6
.
8
5

6
7
1
.
5
8

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

2
.
7
4

8
.
5
0

N
O

1
5
.
7
4

7
8

6
.
4

1
.
8

4
1
9

5
.
8
7
7/
1
3
/
2
0
1
6

M
W
-
3
D

9
0
.
1
9

5
6
.
8
1

6
7
1
.
5
8

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

5
.
4
4

1
6
.
5
0

N
O

1
5
.
7
4

1
1
6

6
.
7

2
.
2

3
7
4

2
.
3
3
7/
1
3
/
2
0
1
6

M
W
-
4

7
4
.
1
5

6
4
.
0
3

6
7
7
.
1
0

N
o
r
m
a
l

N
o
n
e

E
O
P

N
/
A

1
.
6
5

0
.
5
5

N
/
A

1
6
.
2
1

1
3
4

5
.
7

1
.
1

3
1
4

0
.
4
4
7/
1
3
/
2
0
1
6

M
W
-
4
D

1
0
2
.
2
4

6
4
.
4
4

6
7
6
.
1
4

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

6
.
1
7

2
5
.
0
0

N
O

1
6
.
0
3

1
7
5

6
.
6

2
.
8

1
8
4

0
.
0
0
7/
1
3
/
2
0
1
6

M
W
-
1
1

3
8
.
4
5

3
0
.
3
4

6
9
2
.
2
6

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

1
.
3
2

4
.
5
0

N
O

1
6
.
2
6

2
0

5
.
0

1
7
.
1

4
5
4

1
.
3
3
7/
1
3
/
2
0
1
6

M
W
-
1
1
D

1
0
1
.
5
5

3
1
.
2
0

6
9
1
.
9
4

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

1
1
.
4
7

2
8
.
5
0

N
O

1
5
.
2
7

2
9

5
.
7

3
.
8

5
4
9

6
.
8
1
7/
1
3
/
2
0
1
6

M
W
-
1
2

2
9
.
4
9

2
5
.
2
1

6
9
9
.
6
0

N
o
r
m
a
l

N
o
n
e

E
O
P

N
/
A

0
.
7
0

0
.
3
0

N
/
A

1
5
.
8
3

2
3

4
.
9

1
5
.
3

5
8
0

3
.
4
4
7/
1
3
/
2
0
1
6

M
W
-
1
2
D

6
8
.
4
2

2
6
.
1
0

6
9
8
.
6
7

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

6
.
9
0

1
5
.
5
0

N
O

1
5
.
0
9

8
0

6
.
3

4
.
9

5
3
8

7
.
7
4
7/
1
3
/
2
0
1
6

S
W
-
1

N
/
A

N
/
A

N
/
A

N
o
r
m
a
l

N
o
n
e
N/
A
N/
A

N
/
A

N
/
A

N
/
A

2
3
.
6
9

1
2
2

7
.
3

1
9
.
9

1
8
6

7
.
1
9
7/
1
3
/
2
0
1
6

M
W
-
4
R

4
5
.
7
3

3
8
.
3
6

6
7
5
.
5
1

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

1
.
2
0

4
.
0
0

N
O

1
5
.
8
0

1
0
3

6
.
1

6
.
2

3
4
3

6
.
3
7
7/
1
3
/
2
0
1
6

M
W
-
4
D
R

9
0
.
4
0

3
8
.
7
7

6
7
4
.
9
8

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

8
.
4
2

2
5
.
5
0

N
O

1
5
.
4
7

1
3
1

6
.
9

4
.
3

3
5
2

4
.
7
3
No
t
e
s
:
1
.

P
u
r
g
e

M
e
t
h
o
d
s
;

L
F
=
L
o
w

F
l
o
w
,

C
P
=
C
o
n
v
e
n
t
i
o
n
a
l

P
u
r
g
e

(
3
-
5

w
e
l
l

v
o
l
u
m
e
s
)
,

N
P
=
N
o

P
u
r
g
e

(
H
y
d
r
a
S
l
e
e
v
e
)
,

E
O
P
=
E
q
u
i
p
m
e
n
t

O
n
l
y

P
u
r
g
e
.

P
u
m
p

r
a
t
e

a
p
p
l
i
c
a
b
l
e

t
o

L
F

p
u
r
g
i
n
g

o
n
l
y
.
2
.

F
i
e
l
d

s
a
m
p
l
i
n
g

p
e
r
f
o
r
m
e
d

b
y

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C

p
e
r
s
o
n
n
e
l
.
3
.

E
V
A
C

i
n
d
i
c
a
t
e
s

w
h
e
t
h
e
r

t
h
e

w
a
t
e
r

l
e
v
e
l

i
n

t
h
e

w
e
l
l

w
a
s

d
r
a
w
n

d
o
w
n

t
o

t
h
e

l
e
v
e
l

o
f

t
h
e

p
u
m
p

d
u
r
i
n
g

p
u
r
g
i
n
g
.
4
.

µ
Լ /c
m

i
n
d
i
c
a
t
e
s

m
i
c
r
o

m
h
o
s

p
e
r

c
e
n
t
i
m
e
t
e
r
.
5
.

S
U

i
n
d
i
c
a
t
e
s

S
t
a
n
d
a
r
d

U
n
i
t
s
.
6
.

N
T
U

i
n
d
i
c
a
t
e
s

N
e
p
h
e
l
o
m
e
t
r
i
c

T
u
r
b
i
d
i
t
y

U
n
i
t
s
.
7
.

m
V
-
N
H
E

i
n
d
i
c
a
t
e
s

m
i
l
l
i
v
o
l
t
s
-
N
o
r
m
a
l

H
y
d
r
o
g
e
n

E
l
e
c
t
r
o
d
e
.
8
.

m
g
/
L

i
n
d
i
c
a
t
e
s

m
i
l
l
i
g
r
a
m
s

p
e
r

l
i
t
e
r
.
9
.

N
/
A

i
n
d
i
c
a
t
e
s

n
o
t

a
p
p
l
i
c
a
b
l
e
.
10
.

I
n
f
o
r
m
a
t
i
o
n

p
r
o
v
i
d
e
d

b
y

T
i
m

H
u
n
s
u
c
k
e
r

o
f

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C

o
n

A
u
g
u
s
t

2
6
,

2
0
1
6
.
Page 1 of 1
Ta
b
l
e

4

-

G
r
o
u
n
d
w
a
t
e
r

F
i
e
l
d

a
n
d

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
Fie
l
d

p
H

3
2
0

S
U

5
1
9
3
-

N
E

6
.
5
-
8
.
5

6
.
5
-
8
.
5
*
Sp
e
c
i
f
i
c

C
o
n
d
u
c
t
a
n
c
e

3
2
3

µ
Լ /cm

5
1
9
3
-N
E

N
E

N
E
Te
m
p
e
r
a
t
u
r
e

3
2
5

°
C

5
1
9
3
-N
E

N
E

N
E
To
p

o
f

C
a
s
i
n
g
32
8

f
e
e
t

-
-N
E

N
E

N
E
De
p
t
h

t
o

W
a
t
e
r

3
1
8

f
e
e
t

-
-N
E

N
E

N
E
Wa
t
e
r

E
l
e
v
a
t
i
o
n

4
2
7

f
e
e
t

-
-N
E

N
E

N
E
We
l
l

D
e
p
t
h

4
1
1

f
e
e
t

-
-N
E

N
E

N
E
Ar
s
e
n
i
c

1
4
µg/
L
24
8

0
.
2
0
6
J
0.2
1
9
J
0.1
8
3
J
0.
0
8
5

J

0
.
1
2
1
J
0.
0
7
8

1
0

1
0

1
0
Ba
r
i
u
m

1
5
µg/
L
24
8

2
1
8

1
0
0

3
0
.
2
J'
14
.
1
J'
39
.
5
J'
0.1

1
0
0

7
0
0

2
,
0
0
0
Ca
d
m
i
u
m

3
4
µg/
L
24
8

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

1

2

5
Ch
r
o
m
i
u
m

5
1
µg/
L
24
8

0
.
5
1
3
J
0.
5

U

0
.
5

U

0
.
5

U

0
.
5

U

0
.
5

1
0

1
0

1
0
0
Le
a
d

1
3
1
µg/
L
24
8

0
.
0
6
5

U

0
.
0
6
5

U

0
.
3
9
5
J
0.0
6
8
5

J

1
.
2
4
J'
0.
0
6
5

1
0

1
5

1
5
Me
r
c
u
r
y

1
3
2
µg/
L
24
8

0
.
0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4

0
.
2

1

2
Se
l
e
n
i
u
m

1
8
3
µg/
L
24
8

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

1
0

2
0

5
0
Si
l
v
e
r

1
8
4
µg/
L
24
8

0
.
7

U

0
.
7

U

0
.
7

U

0
.
7

U

0
.
7

U

0
.
7

1
0

2
0

1
0
0
*
Su
l
f
a
t
e

3
1
5
µg/
L
24
8

3
4
1
J'
34
7
J'
64
4
J'
34
2
J'
53
0
J'
18

2
5
0
,
0
0
0

2
5
0
,
0
0
0

2
5
0
,
0
0
0
*
cis
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e

7
8
µg/
L

3
8
7

0
.
2
1

U

0
.
2
1

U

0
.
2
1

U

0
.
2
1

U

0
.
2
1

U

0
.
2
1

5

7
0

7
0
Dic
h
l
o
r
o
m
e
t
h
a
n
e

1
4
0
µg/
L

3
8
7
1U

1
U

1
U

1
U

1
U
11

5

5
Te
t
r
a
c
h
l
o
r
o
e
t
h
y
l
e
n
e

1
9
2
µg/
L

3
8
7
0.1
4

U

0
.
1
4

U

0
.
1
4

U

0
.
1
4

U

0
.
1
4

U
0.
1
4

1

0
.
7

5
Tr
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e

2
0
1
µg/
L

3
8
7
0.2

U

0
.
2

U

0
.
2

U

0
.
2

U

0
.
2

U
0.2

1

3

5
Xy
l
e
n
e

(
t
o
t
a
l
)

3
4
6

µ
g
/
L

3
8
7
0.5
8

U

0
.
5
8

U

0
.
5
8

U

0
.
5
8

U

0
.
5
8

U
0.
5
8

5

5
0
0

1
0
,
0
0
0
No
t
e
s
:

1
.

C
o
n
c
e
n
t
r
a
t
i
o
n
s

p
r
e
s
e
n
t
e
d

i
n

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r

(
µ
g
/
L
)
.

2
.

S
U

i
n
d
i
c
a
t
e
s

S
t
a
n
d
a
r
d

U
n
i
t
s
.

3
.

µ
Լ /c
m

i
n
d
i
c
a
t
e
s

m
i
c
r
o
m
h
o
s

p
e
r

c
e
n
t
i
m
e
t
e
r
.

4
.

S
W
S

I
D

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

I
d
e
n
t
i
f
i
c
a
t
i
o
n

N
u
m
b
e
r
.

5
.

M
D
L

i
s

t
h
e

l
a
b
o
r
a
t
o
r
y

m
e
t
h
o
d

d
e
t
e
c
t
i
o
n

l
i
m
i
t
.

T
h
e

M
D
L

v
a
l
u
e
s

p
r
e
s
e
n
t
e
d

a
r
e

f
o
r

s
a
m
p
l
e
s

n
o
t

d
i
l
u
t
e
d

b
y

t
h
e

l
a
b
o
r
a
t
o
r
y

d
u
r
i
ng

a
n
a
l
y
s
i
s
.

6
.

S
W
S
L

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

L
i
m
i
t
.

N
C
D
E
Q

d
e
f
i
n
e
s

t
h
e

S
W
S
L

a
s

t
h
e

l
o
w
e
s
t

a
m
o
u
n
t

o
f

a
n
a
l
y
t
e

i
n

a

s
a
m
p
l
e

t
h
a
t

c
a
n

b
e

q
u
a
n
tit
a
t
i
v
e
l
y

d
e
t
e
r
m
i
n
e
d

w
i
t
h

s
u
i
t
a
b
l
e

p
r
e
c
i
s
i
o
n

a
n
d

a
c
c
u
r
a
c
y
.

7
.

1
5
A

N
C
A
C

2
L

S
t
a
n
d
a
r
d

r
e
f
e
r
s

t
o

C
l
a
s
s

G
A

S
t
a
n
d
a
r
d
s

a
s

f
o
u
n
d

i
n

1
5
A

N
C
A
C

0
2
L

.
0
2
0
2

G
r
o
u
n
d
w
a
t
e
r

Q
u
a
l
i
t
y

S
t
a
n
d
a
r
d
s
,

l
a
s
t

a
m
e
n
de
d

o
n

A
p
r
i
l

1
,

2
0
1
3
.

8
.

M
C
L

i
s

t
h
e

F
e
d
e
r
a
l

M
a
x
i
m
u
m

C
o
n
t
a
m
i
n
a
n
t

L
e
v
e
l

a
s

f
o
u
n
d

i
n

4
0

C
F
R
,

S
u
b
p
a
r
t

G
,

§
1
4
1
.
6
2
.

9
.

*

C
o
n
c
e
n
t
r
a
t
i
o
n

l
i
s
t
e
d

i
s

a

s
e
c
o
n
d
a
r
y

m
a
x
i
m
u
m

c
o
n
t
a
m
i
n
a
n
t

l
e
v
e
l

(
S
M
C
L
)
.

S
M
C
L
s

a
r
e

e
s
t
a
b
l
i
s
h
e
d

b
y

E
P
A

i
n

t
h
e

N
a
t
i
o
n
a
l

S
e
c
o
nd
a
r
y

D
r
i
n
k
i
n
g

W
a
t
e
r

R
e
g
u
l
a
t
i
o
n
s

a
s

f
o
u
n
d

i
n

4
0

C
F
R

§
1
4
3
.
3
.
10
.

N
E

i
n
d
i
c
a
t
e
s

n
o
t

e
s
t
a
b
l
i
s
h
e
d
.

N
A

i
n
d
i
c
a
t
e
s

n
o
t

a
n
a
l
y
z
e
d
.

N
S

i
n
d
i
c
a
t
e
s

n
o

s
a
m
p
l
e

w
a
s

c
o
l
l
e
c
t
e
d
.

B
l
a
n
k

c
e
l
l
s

i
n
d
i
c
a
t
e

t
h
a
t

th
e
r
e

i
s

n
o

i
n
f
o
r
m
a
t
i
o
n

r
e
l
e
v
a
n
t

t
o

t
h
e

r
e
s
p
e
c
t
i
v
e

r
o
w
.
11
.

G
r
a
y
e
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

v
a
l
u
e
s

t
h
a
t

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

S
W
S
L
.
12
.

B
o
l
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

v
a
l
u
e
s

t
h
a
t

a
t
t
a
i
n

o
r

e
x
c
e
e
d

t
h
e

1
5
A

N
C
A
C

2
L

S
t
a
n
d
a
r
d
.
13
.

Q
u
a
l
i
f
i
e
r
s

i
n

n
o
n
-
i
t
a
l
i
c
i
z
e
d

t
e
x
t

a
r
e

l
a
b
o
r
a
t
o
r
y

d
a
t
a

q
u
a
l
i
f
i
e
r
s

o
r

"
f
l
a
g
s
"
.

"
U
"

i
s

u
s
e
d

t
o

i
d
e
n
t
i
f
y

r
e
s
u
l
t
s

n
o
t

d
e
t
e
c
t
e
d

a
t c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

t
h
e

l
a
b
o
r
a
t
o
r
y
'
s

M
D
L
.

"
J
"

i
s

u
s
e
d

t
o

i
d
e
n
t
i
f
y

e
s
t
i
m
a
t
e
d

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

M
D
L

b
u
t

a
r
e

l
e
s
s

t
h
a
n

t
h
e

l
a
b
o
r
a
t
o
r
y's

m
e
t
h
o
d

r
e
p
o
r
t
i
n
g

l
i
m
i
t

(
M
R
L
)
.

A
n

i
t
a
l
i
c
i
z
e
d

J'-fl
a
g

i
s

a

d
a
t
a

q
u
a
l
i
f
i
e
r
,

a
d
d
e
d

b
y

H
D
R

t
o

i
n
d
i
c
a
t
e

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

l
a
b
o
r
a
t
o
r
y
'
s

M
R
L

b
u
t

a
r
e
le
s
s

t
h
a
n

t
h
e

S
W
S
L
.

14
.

C
o
n
s
t
i
t
u
e
n
t
s

l
i
s
t
e
d

b
e
l
o
w

t
h
e

b
o
l
d

l
i
n
e

a
r
e

E
P
A

M
e
t
h
o
d

8
2
6
0

v
o
l
a
t
i
l
e

o
r
g
a
n
i
c

c
o
m
p
o
u
n
d
s

(
V
O
C
s
)

m
e
a
s
u
r
e
d

a
t

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
ic
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e
i
r

M
D
L

i
n

o
n
e

o
r

m
o
r
e

s
a
m
p
l
e
s
.

R
e
s
u
l
t
s

f
o
r

a
l
l

o
t
h
e
r

S
W
-
8
4
6

M
e
t
h
o
d

8
2
6
0

c
o
n
s
t
i
t
u
e
n
t
s

w
e
r
e

l
e
s
s

t
h
a
n

t
h
e
i
r

M
D
L
s
.
15
.

A
n
a
l
y
t
i
c
a
l

r
e
s
u
l
t
s

o
b
t
a
i
n
e
d

f
r
o
m

E
l
e
c
t
r
o
n
i
c

D
a
t
a

D
e
l
i
v
e
r
a
b
l
e

(
E
D
D
)

p
r
o
v
i
d
e
d

b
y

T
i
m

H
u
n
s
u
c
k
e
r

o
f

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s

o
n

A
u
gu
s
t

2
6
,

2
0
1
6
.
28
.
4
3
70
1
.
8
0
68
.
5
5
53
.
3
1
51
.
2
6
68
8
.
4
1
77
.
5
7
88
.
2
2
70
1
.
3
0
29
.
3
1
60
0
4

M
W
-
2
D

6
0
0
4

M
W
-
3
Mo
n
i
t
o
r
i
n
g

W
e
l
l
s
MD
L
16
.
3
6
996.2
6.
2
11
0
16
.
5
5

1
7
.
0
5
606.9
6.
5 98
17
.
4
7
73
0
.
6
1
73
0
.
2
3

7
3
9
.
6
7

7
2
8
.
4
3
La
b
o
r
a
t
o
r
y

C
e
r
t
i
f
i
c
a
t
e

C
o
d
e
s
:
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s

F
i
e
l
d

#
5
1
9
3
Du
k
e

E
n
e
r
g
y

A
n
a
l
y
t
i
c
a
l

L
a
b
o
r
a
t
o
r
y

#
2
4
8
Te
s
t
A
m
e
r
i
c
a

L
a
b
o
r
a
t
o
r
i
e
s
,

I
n
c
.

#
3
8
7
Federal MCL
15
A

N
C
A
C

2
L

St
a
n
d
a
r
d
SW
S
L
Sa
m
p
l
e

D
a
t
e
:

J
u
l
y

1
3
,

2
0
1
6

Fie
l
d

S
a
m
p
l
i
n
g

p
e
r
f
o
r
m
e
d

b
y

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C

Pa
r
a
m
e
t
e
r

S
W
S

I
D

U
n
i
t
s
Ce
r
t
i
f
i
c
a
t
e
Co
d
e

6
0
0
4

M
W
-
1

6
0
0
4

M
W
-
1
D

6
0
0
4

M
W
-
2
A
73
.
6
4
10
8
.
8
2
68
7
.
4
6
6.4 78
15
.
7
4
56
.
8
5
67
1
.
5
8
74
0
.
7
7
Page 1 of 3
Ta
b
l
e

4

-

G
r
o
u
n
d
w
a
t
e
r

F
i
e
l
d

a
n
d

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
Fi
e
l
d

p
H

3
2
0

S
U

5
1
9
3
-
NE

6
.
5
-
8
.
5

6
.
5
-
8
.
5
*
Sp
e
c
i
f
i
c

C
o
n
d
u
c
t
a
n
c
e

3
2
3

µ
Լ /c
m

5
1
9
3
-
NE

N
E

N
E
Te
m
p
e
r
a
t
u
r
e

3
2
5

°
C

5
1
9
3
-
NE

N
E

N
E
To
p

o
f

C
a
s
i
n
g

3
2
8

f
e
e
t

-
-N
E

N
E

N
E
De
p
t
h

t
o

W
a
t
e
r

3
1
8

f
e
e
t

-
-N
E

N
E

N
E
Wa
t
e
r

E
l
e
v
a
t
i
o
n

4
2
7

f
e
e
t

-
-N
E

N
E

N
E
We
l
l

D
e
p
t
h

4
1
1

f
e
e
t

-
-N
E

N
E

N
E
Ar
s
e
n
i
c

1
4
µg/
L

2
4
8
0.1
1
1
J
0.0
8
9
7
J
0.1
4
2
J
0.2
1
2

J

0
.
0
8
7
6
J
0.0
7
8
10

1
0

1
0
Ba
r
i
u
m

1
5
µg/
L

2
4
8
27
J '
70
.
5
J '
11
.
6
J '
49
.
6
J '
13
.
8
J '
0.
1
10
0

7
0
0

2
,
0
0
0
Ca
d
m
i
u
m

3
4
µg/
L

2
4
8
0.1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1
125
Ch
r
o
m
i
u
m

5
1
µg/
L

2
4
8
0.5

U

0
.
6
5
5
J
0.5

U

0
.
5

U

0
.
5

U

0
.
5
10

1
0

1
0
0
Le
a
d

1
3
1
µg/
L

2
4
8
0.0
6
5

U

0
.
0
6
5

U

0
.
1
1
7
J
0.0
6
5

U

0
.
0
6
5

U

0
.
0
6
5
10

1
5

1
5
Me
r
c
u
r
y

1
3
2
µg/
L

2
4
8
0.0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4
0.
2

1

2
Se
l
e
n
i
u
m

1
8
3
µg/
L

2
4
8
0.0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2
10

2
0

5
0
Sil
v
e
r

1
8
4
µg/
L

2
4
8
0.7

U

0
.
7

U

0
.
7

U

0
.
7

U

0
.
7

U

0
.
7
10

2
0

1
0
0
*
Su
l
f
a
t
e

3
1
5
µg/
L

2
4
8
94
0
J '
98
5
J '
35
7
J '
27
4
J '
12
4
0
J '
18
25
0
,
0
0
0

2
5
0
,
0
0
0

2
5
0
,
0
0
0
*
ci
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e

7
8
µg/
L

3
8
7

0
.
9
5
9

J

1
.
2
8
J'
0.
2
1

U

1
4
.
1

0
.
2
1

U

0
.
2
1

5

7
0

7
0
Dic
h
l
o
r
o
m
e
t
h
a
n
e

1
4
0
µg/
L

3
8
7
1U

1
U

1
U
6.8
3
1U
11

5

5
Te
t
r
a
c
h
l
o
r
o
e
t
h
y
l
e
n
e

1
9
2
µg/
L

3
8
7
0.3
7
6
J
2.
2
4
0.4
8
1
J
1.4
8
0.
2
6
2
J
0.
1
4

1

0
.
7

5
Tr
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e

2
0
1
µg/
L

3
8
7
0.6
2
7
J
0.
6
2
2
J
0.2

U
4.1
1
0.
2

U
0.
2

1

3

5
Xy
l
e
n
e

(
t
o
t
a
l
)

3
4
6

µ
g
/
L

3
8
7
5.1
9

0
.
5
8

U

0
.
5
8

U

5
1
.
7

0
.
5
8

U
0.
5
8

5

5
0
0

1
0
,
0
0
0
No
t
e
s
:

1
.

C
o
n
c
e
n
t
r
a
t
i
o
n
s

p
r
e
s
e
n
t
e
d

i
n

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r

(
µ
g
/
L
)
.

2
.

S
U

i
n
d
i
c
a
t
e
s

S
t
a
n
d
a
r
d

U
n
i
t
s
.

3
.

µ
Լ /c
m

i
n
d
i
c
a
t
e
s

m
i
c
r
o
m
h
o
s

p
e
r

c
e
n
t
i
m
e
t
e
r
.

4
.

S
W
S

I
D

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

I
d
e
n
t
i
f
i
c
a
t
i
o
n

N
u
m
b
e
r
.

5
.

M
D
L

i
s

t
h
e

l
a
b
o
r
a
t
o
r
y

m
e
t
h
o
d

d
e
t
e
c
t
i
o
n

l
i
m
i
t
.

T
h
e

M
D
L

v
a
l
u
e
s

p
r
e
s
e
n
t
e
d

a
r
e

f
o
r

s
a
m
p
l
e
s

n
o
t

d
i
l
u
t
e
d

b
y

t
h
e

l
a
b
o
r
a
t
o
r
y

d
u
r
i
ng

a
n
a
l
y
s
i
s
.

6
.

S
W
S
L

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

L
i
m
i
t
.

N
C
D
E
Q

d
e
f
i
n
e
s

t
h
e

S
W
S
L

a
s

t
h
e

l
o
w
e
s
t

a
m
o
u
n
t

o
f

a
n
a
l
y
t
e

i
n

a

s
a
m
p
l
e

t
h
a
t

c
a
n

b
e

q
u
a
n
ti
t
a
t
i
v
e
l
y

d
e
t
e
r
m
i
n
e
d

w
i
t
h

s
u
i
t
a
b
l
e

p
r
e
c
i
s
i
o
n

a
n
d

a
c
c
u
r
a
c
y
.

7
.

1
5
A

N
C
A
C

2
L

S
t
a
n
d
a
r
d

r
e
f
e
r
s

t
o

C
l
a
s
s

G
A

S
t
a
n
d
a
r
d
s

a
s

f
o
u
n
d

i
n

1
5
A

N
C
A
C

0
2
L

.
0
2
0
2

G
r
o
u
n
d
w
a
t
e
r

Q
u
a
l
i
t
y

S
t
a
n
d
a
r
d
s
,

l
a
s
t

a
m
e
n
de
d

o
n

A
p
r
i
l

1
,

2
0
1
3
.

8
.

M
C
L

i
s

t
h
e

F
e
d
e
r
a
l

M
a
x
i
m
u
m

C
o
n
t
a
m
i
n
a
n
t

L
e
v
e
l

a
s

f
o
u
n
d

i
n

4
0

C
F
R
,

S
u
b
p
a
r
t

G
,

§
1
4
1
.
6
2
.

9
.

*

C
o
n
c
e
n
t
r
a
t
i
o
n

l
i
s
t
e
d

i
s

a

s
e
c
o
n
d
a
r
y

m
a
x
i
m
u
m

c
o
n
t
a
m
i
n
a
n
t

l
e
v
e
l

(
S
M
C
L
)
.

S
M
C
L
s

a
r
e

e
s
t
a
b
l
i
s
h
e
d

b
y

E
P
A

i
n

t
h
e

N
a
t
i
o
n
a
l

S
e
c
o
nd
a
r
y

D
r
i
n
k
i
n
g

W
a
t
e
r

R
e
g
u
l
a
t
i
o
n
s

a
s

f
o
u
n
d

i
n

4
0

C
F
R

§
1
4
3
.
3
.
10
.

N
E

i
n
d
i
c
a
t
e
s

n
o
t

e
s
t
a
b
l
i
s
h
e
d
.

N
A

i
n
d
i
c
a
t
e
s

n
o
t

a
n
a
l
y
z
e
d
.

N
S

i
n
d
i
c
a
t
e
s

n
o

s
a
m
p
l
e

w
a
s

c
o
l
l
e
c
t
e
d
.

B
l
a
n
k

c
e
l
l
s

i
n
d
i
c
a
t
e

t
h
a
t

th
e
r
e

i
s

n
o

i
n
f
o
r
m
a
t
i
o
n

r
e
l
e
v
a
n
t

t
o

t
h
e

r
e
s
p
e
c
t
i
v
e

r
o
w
.
11
.

G
r
a
y
e
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

v
a
l
u
e
s

t
h
a
t

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

S
W
S
L
.
12
.

B
o
l
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

v
a
l
u
e
s

t
h
a
t

a
t
t
a
i
n

o
r

e
x
c
e
e
d

t
h
e

1
5
A

N
C
A
C

2
L

S
t
a
n
d
a
r
d
.
13
.

Q
u
a
l
i
f
i
e
r
s

i
n

n
o
n
-
i
t
a
l
i
c
i
z
e
d

t
e
x
t

a
r
e

l
a
b
o
r
a
t
o
r
y

d
a
t
a

q
u
a
l
i
f
i
e
r
s

o
r

"
f
l
a
g
s
"
.

"
U
"

i
s

u
s
e
d

t
o

i
d
e
n
t
i
f
y

r
e
s
u
l
t
s

n
o
t

d
e
t
e
c
t
e
d

a
t c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

t
h
e

l
a
b
o
r
a
t
o
r
y
'
s

M
D
L
.

"
J
"

i
s

u
s
e
d

t
o

i
d
e
n
t
i
f
y

e
s
t
i
m
a
t
e
d

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

M
D
L

b
u
t

a
r
e

l
e
s
s

t
h
a
n

t
h
e

l
a
b
o
r
a
t
o
r
y's

m
e
t
h
o
d

r
e
p
o
r
t
i
n
g

l
i
m
i
t

(
M
R
L
)
.

A
n

i
t
a
l
i
c
i
z
e
d

J'
-fl
a
g

i
s

a

d
a
t
a

q
u
a
l
i
f
i
e
r
,

a
d
d
e
d

b
y

H
D
R

t
o

i
n
d
i
c
a
t
e

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

l
a
b
o
r
a
t
o
r
y
'
s

M
R
L

b
u
t

a
r
e
le
s
s

t
h
a
n

t
h
e

S
W
S
L
.

14
.

C
o
n
s
t
i
t
u
e
n
t
s

l
i
s
t
e
d

b
e
l
o
w

t
h
e

b
o
l
d

l
i
n
e

a
r
e

E
P
A

M
e
t
h
o
d

8
2
6
0

v
o
l
a
t
i
l
e

o
r
g
a
n
i
c

c
o
m
p
o
u
n
d
s

(
V
O
C
s
)

m
e
a
s
u
r
e
d

a
t

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
ic
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e
i
r

M
D
L

i
n

o
n
e

o
r

m
o
r
e

s
a
m
p
l
e
s
.

R
e
s
u
l
t
s

f
o
r

a
l
l

o
t
h
e
r

S
W
-
8
4
6

M
e
t
h
o
d

8
2
6
0

c
o
n
s
t
i
t
u
e
n
t
s

w
e
r
e

l
e
s
s

t
h
a
n

t
h
e
i
r

M
D
L
s
.
15
.

A
n
a
l
y
t
i
c
a
l

r
e
s
u
l
t
s

o
b
t
a
i
n
e
d

f
r
o
m

E
l
e
c
t
r
o
n
i
c

D
a
t
a

D
e
l
i
v
e
r
a
b
l
e

(
E
D
D
)

p
r
o
v
i
d
e
d

b
y

T
i
m

H
u
n
s
u
c
k
e
r

o
f

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s

o
n

A
u
gu
s
t

2
6
,

2
0
1
6
.
67
4
.
9
8
90
.
4
0
6.9
13
1
15
.
4
7
71
3
.
7
5
38
.
7
7
64
.
0
3
67
7
.
1
0
74
.
1
5
90
.
1
9
67
1
.
5
8
56
.
8
1
67
5
.
5
1
45
.
7
3

1
0
2
.
2
4
67
6
.
1
4
64
.
4
4
38
.
3
6
Sa
m
p
l
e

D
a
t
e
:

J
u
l
y

1
3
,

2
0
1
6

Fi
e
l
d

S
a
m
p
l
i
n
g

p
e
r
f
o
r
m
e
d

b
y

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C

Laboratory Certificate Codes:
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s

F
i
e
l
d

#
5
1
9
3
Du
k
e

E
n
e
r
g
y

A
n
a
l
y
t
i
c
a
l

L
a
b
o
r
a
t
o
r
y

#
2
4
8
Te
s
t
A
m
e
r
i
c
a

L
a
b
o
r
a
t
o
r
i
e
s
,

I
n
c
.

#
3
8
7
Pa
r
a
m
e
t
e
r

S
W
S

I
D

U
n
i
t
s
Ce
r
t
i
f
i
c
a
t
e
Co
d
e
SW
S
L
Federal MCL
60
0
4

M
W
-
3
D

6
0
0
4

M
W
-
4

6
0
0
4

M
W
-
4
R

6
0
0
4

M
W
-
4
D

6
0
0
4

M
W
-
4
D
R
Mo
n
i
t
o
r
i
n
g

W
e
l
l
s
15A NCAC 2L Standard
MD
L
72
8
.
3
9

7
1
3
.
8
7
74
1
.
1
3

7
4
0
.
5
8
6.1
10
3
15
.
8
0

1
6
.
0
3
17
5
6.6
5.7
13
4
16
.
2
1
15
.
7
4
11
6
6.7
Page 2 of 3
Ta
b
l
e

4

-

G
r
o
u
n
d
w
a
t
e
r

F
i
e
l
d

a
n
d

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
Fie
l
d

p
H

3
2
0

S
U

5
1
9
3
-

N
E

6
.
5
-
8
.
5

6
.
5
-
8
.
5
*
Sp
e
c
i
f
i
c

C
o
n
d
u
c
t
a
n
c
e

3
2
3

µ
Լ /cm

5
1
9
3
-N
E

N
E

N
E
Te
m
p
e
r
a
t
u
r
e

3
2
5

°
C

5
1
9
3
-N
E

N
E

N
E
To
p

o
f

C
a
s
i
n
g
32
8

f
e
e
t

-
-N
E

N
E

N
E
De
p
t
h

t
o

W
a
t
e
r
31
8

f
e
e
t

-
-N
E

N
E

N
E
Wa
t
e
r

E
l
e
v
a
t
i
o
n

4
2
7

f
e
e
t

-
-N
E

N
E

N
E
We
l
l

D
e
p
t
h

4
1
1

f
e
e
t

-
-N
E

N
E

N
E
Ar
s
e
n
i
c

1
4
µg/
L
24
8

0
.
1
6
9
J
0.0
7
8

U

0
.
2
7
9
J
0.
0
7
8

U

0
.
0
7
8

U

0
.
0
7
8

1
0

1
0

1
0
Ba
r
i
u
m

1
5
µg/
L
24
8

9
.
6
4
J '
12
J '
16
J '
9
J '
0.1

U

0
.
1

1
0
0

7
0
0

2
,
0
0
0
Ca
d
m
i
u
m

3
4
µg/
L
24
8

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

1

2

5
Ch
r
o
m
i
u
m

5
1
µg/
L
24
8

0
.
5

U

0
.
5

U

0
.
7
6
4
J
0.
5

U

0
.
5

U

0
.
5

1
0

1
0

1
0
0
Le
a
d

1
3
1
µg/
L
24
8

0
.
2
5
3
J
0.0
6
5

U

0
.
6
2
J
0.
0
6
5

U

0
.
0
6
5

U

0
.
0
6
5

1
0

1
5

1
5
Me
r
c
u
r
y

1
3
2
µg/
L
24
8

0
.
0
4
4
J
0.0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4

U

0
.
0
3
3
4

0
.
2

1

2
Se
l
e
n
i
u
m

1
8
3
µg/
L
24
8

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

1
0

2
0

5
0
Sil
v
e
r

1
8
4
µg/
L
24
8

0
.
7

U

0
.
7

U

0
.
7

U

0
.
7

U

0
.
7

U

0
.
7

1
0

2
0

1
0
0
*
Su
l
f
a
t
e

3
1
5
µg/
L
24
8

2
7
9
J '
72
4
J '
29
7
J '
83
.
7
J
18

U

1
8

2
5
0
,
0
0
0

2
5
0
,
0
0
0

2
5
0
,
0
0
0
*
cis
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e

7
8
µg/
L

3
8
7

0
.
2
1

U

0
.
2
1

U

0
.
2
1

U

0
.
2
1

U

0
.
2
1

U

0
.
2
1

U

0
.
2
1

5

7
0

7
0
Dic
h
l
o
r
o
m
e
t
h
a
n
e

1
4
0
µg/
L

3
8
7
1U

1
U

1
U

1
U

1
U

1
U
11

5

5
Te
t
r
a
c
h
l
o
r
o
e
t
h
y
l
e
n
e

1
9
2
µg/
L

3
8
7
0.1
4

U

0
.
1
4

U

0
.
1
4

U

0
.
1
4

U

0
.
1
4

U

0
.
1
4

U
0.
1
4

1

0
.
7

5
Tr
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e

2
0
1
µg/
L

3
8
7
0.
2

U

0
.
2

U

0
.
2

U

0
.
2

U

0
.
2

U

0
.
2

U
0.
2

1

3

5
Xy
l
e
n
e

(
t
o
t
a
l
)

3
4
6

µ
g
/
L

3
8
7
0.5
8

U

0
.
5
8

U

0
.
5
8

U

0
.
5
8

U

0
.
5
8

U

0
.
5
8

U
0.
5
8

5

5
0
0

1
0
,
0
0
0
No
t
e
s
:

1
.

C
o
n
c
e
n
t
r
a
t
i
o
n
s

p
r
e
s
e
n
t
e
d

i
n

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r

(
µ
g
/
L
)
.

2
.

S
U

i
n
d
i
c
a
t
e
s

S
t
a
n
d
a
r
d

U
n
i
t
s
.

3
.

µ
Լ /c
m

i
n
d
i
c
a
t
e
s

m
i
c
r
o
m
h
o
s

p
e
r

c
e
n
t
i
m
e
t
e
r
.

4
.

S
W
S

I
D

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

I
d
e
n
t
i
f
i
c
a
t
i
o
n

N
u
m
b
e
r
.

5
.

M
D
L

i
s

t
h
e

l
a
b
o
r
a
t
o
r
y

m
e
t
h
o
d

d
e
t
e
c
t
i
o
n

l
i
m
i
t
.

T
h
e

M
D
L

v
a
l
u
e
s

p
r
e
s
e
n
t
e
d

a
r
e

f
o
r

s
a
m
p
l
e
s

n
o
t

d
i
l
u
t
e
d

b
y

t
h
e

l
a
b
o
r
a
t
o
r
y

d
u
r
i
ng

a
n
a
l
y
s
i
s
.

6
.

S
W
S
L

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

L
i
m
i
t
.

N
C
D
E
Q

d
e
f
i
n
e
s

t
h
e

S
W
S
L

a
s

t
h
e

l
o
w
e
s
t

a
m
o
u
n
t

o
f

a
n
a
l
y
t
e

i
n

a

s
a
m
p
l
e

t
h
a
t

c
a
n

b
e

q
u
a
n
ti
t
a
t
i
v
e
l
y

d
e
t
e
r
m
i
n
e
d

w
i
t
h

s
u
i
t
a
b
l
e

p
r
e
c
i
s
i
o
n

a
n
d

a
c
c
u
r
a
c
y
.

7
.

1
5
A

N
C
A
C

2
L

S
t
a
n
d
a
r
d

r
e
f
e
r
s

t
o

C
l
a
s
s

G
A

S
t
a
n
d
a
r
d
s

a
s

f
o
u
n
d

i
n

1
5
A

N
C
A
C

0
2
L

.
0
2
0
2

G
r
o
u
n
d
w
a
t
e
r

Q
u
a
l
i
t
y

S
t
a
n
d
a
r
d
s
,

l
a
s
t

a
m
e
n
de
d

o
n

A
p
r
i
l

1
,

2
0
1
3
.

8
.

M
C
L

i
s

t
h
e

F
e
d
e
r
a
l

M
a
x
i
m
u
m

C
o
n
t
a
m
i
n
a
n
t

L
e
v
e
l

a
s

f
o
u
n
d

i
n

4
0

C
F
R
,

S
u
b
p
a
r
t

G
,

§
1
4
1
.
6
2
.

9
.

*

C
o
n
c
e
n
t
r
a
t
i
o
n

l
i
s
t
e
d

i
s

a

s
e
c
o
n
d
a
r
y

m
a
x
i
m
u
m

c
o
n
t
a
m
i
n
a
n
t

l
e
v
e
l

(
S
M
C
L
)
.

S
M
C
L
s

a
r
e

e
s
t
a
b
l
i
s
h
e
d

b
y

E
P
A

i
n

t
h
e

N
a
t
i
o
n
a
l

S
e
c
o
nd
a
r
y

D
r
i
n
k
i
n
g

W
a
t
e
r

R
e
g
u
l
a
t
i
o
n
s

a
s

f
o
u
n
d

i
n

4
0

C
F
R

§
1
4
3
.
3
.
10
.

N
E

i
n
d
i
c
a
t
e
s

n
o
t

e
s
t
a
b
l
i
s
h
e
d
.

N
A

i
n
d
i
c
a
t
e
s

n
o
t

a
n
a
l
y
z
e
d
.

N
S

i
n
d
i
c
a
t
e
s

n
o

s
a
m
p
l
e

w
a
s

c
o
l
l
e
c
t
e
d
.

B
l
a
n
k

c
e
l
l
s

i
n
d
i
c
a
t
e

t
h
a
t

th
e
r
e

i
s

n
o

i
n
f
o
r
m
a
t
i
o
n

r
e
l
e
v
a
n
t

t
o

t
h
e

r
e
s
p
e
c
t
i
v
e

r
o
w
.
11
.

G
r
a
y
e
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

v
a
l
u
e
s

t
h
a
t

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

S
W
S
L
.
12
.

B
o
l
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

v
a
l
u
e
s

t
h
a
t

a
t
t
a
i
n

o
r

e
x
c
e
e
d

t
h
e

1
5
A

N
C
A
C

2
L

S
t
a
n
d
a
r
d
.
13
.

Q
u
a
l
i
f
i
e
r
s

i
n

n
o
n
-
i
t
a
l
i
c
i
z
e
d

t
e
x
t

a
r
e

l
a
b
o
r
a
t
o
r
y

d
a
t
a

q
u
a
l
i
f
i
e
r
s

o
r

"
f
l
a
g
s
"
.

"
U
"

i
s

u
s
e
d

t
o

i
d
e
n
t
i
f
y

r
e
s
u
l
t
s

n
o
t

d
e
t
e
c
t
e
d

a
t c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

t
h
e

l
a
b
o
r
a
t
o
r
y
'
s

M
D
L
.

"
J
"

i
s

u
s
e
d

t
o

i
d
e
n
t
i
f
y

e
s
t
i
m
a
t
e
d

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

M
D
L

b
u
t

a
r
e

l
e
s
s

t
h
a
n

t
h
e

l
a
b
o
r
a
t
o
r
y's

m
e
t
h
o
d

r
e
p
o
r
t
i
n
g

l
i
m
i
t

(
M
R
L
)
.

A
n

i
t
a
l
i
c
i
z
e
d

J'
-fl
a
g

i
s

a

d
a
t
a

q
u
a
l
i
f
i
e
r
,

a
d
d
e
d

b
y

H
D
R

t
o

i
n
d
i
c
a
t
e

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

l
a
b
o
r
a
t
o
r
y
'
s

M
R
L

b
u
t

a
r
e
le
s
s

t
h
a
n

t
h
e

S
W
S
L
.

14
.

C
o
n
s
t
i
t
u
e
n
t
s

l
i
s
t
e
d

b
e
l
o
w

t
h
e

b
o
l
d

l
i
n
e

a
r
e

E
P
A

M
e
t
h
o
d

8
2
6
0

v
o
l
a
t
i
l
e

o
r
g
a
n
i
c

c
o
m
p
o
u
n
d
s

(
V
O
C
s
)

m
e
a
s
u
r
e
d

a
t

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
ic
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e
i
r

M
D
L

i
n

o
n
e

o
r

m
o
r
e

s
a
m
p
l
e
s
.

R
e
s
u
l
t
s

f
o
r

a
l
l

o
t
h
e
r

S
W
-
8
4
6

M
e
t
h
o
d

8
2
6
0

c
o
n
s
t
i
t
u
e
n
t
s

w
e
r
e

l
e
s
s

t
h
a
n

t
h
e
i
r

M
D
L
s
.
15
.

A
n
a
l
y
t
i
c
a
l

r
e
s
u
l
t
s

o
b
t
a
i
n
e
d

f
r
o
m

E
l
e
c
t
r
o
n
i
c

D
a
t
a

D
e
l
i
v
e
r
a
b
l
e

(
E
D
D
)

p
r
o
v
i
d
e
d

b
y

T
i
m

H
u
n
s
u
c
k
e
r

o
f

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s

o
n

A
u
gu
s
t

2
6
,

2
0
1
6
.
10
1
.
5
5
69
1
.
9
4
31
.
2
0
30
.
3
4
69
2
.
2
6
38
.
4
5
26
.
1
0
69
8
.
6
7
68
.
4
2
25
.
2
1
69
9
.
6
0
29
.
4
9
--
-
6.3 80
---
----
Laboratory Certificate Codes:Duke Energy Carolinas Field #5193
Du
k
e

E
n
e
r
g
y

A
n
a
l
y
t
i
c
a
l

L
a
b
o
r
a
t
o
r
y

#
2
4
8
TestAmerica Laboratories, Inc. #387 Federal MCL
Sa
m
p
l
e

D
a
t
e
:

J
u
l
y

1
3
,

2
0
1
6

Fi
e
l
d

S
a
m
p
l
i
n
g

p
e
r
f
o
r
m
e
d

b
y

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C

15A NCAC 2L Standard
Pa
r
a
m
e
t
e
r

S
W
S

I
D

U
n
i
t
s
Ce
r
t
i
f
i
c
a
t
e
Co
d
e
SW
S
L
60
0
4

M
W
-
1
2

6
0
0
4

M
W
-
1
2
D
Tr
i
p
Bla
n
k
Fie
l
d
Bla
n
k
60
0
4

M
W
-
1
1
D
60
0
4

M
W
-
1
1
MD
L
Mo
n
i
t
o
r
i
n
g

W
e
l
l
s
72
4
.
7
7
72
4
.
8
1
72
2
.
6
0

7
2
3
.
1
4
15
.
0
9
15
.
8
3
15
.
2
7
5.7
5.0

4
.
9
23
29
20
16
.
2
6
----
NANANANANANANANANA
Page 3 of 3
Ta
b
l
e

5

-

F
i
e
l
d

a
n
d

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s

t
h
a
t

E
q
u
a
l

o
r

E
x
c
e
e
d
15
A

N
C
A
C

2
L

G
r
o
u
n
d
w
a
t
e
r

Q
u
a
l
i
t
y

S
t
a
n
d
a
r
d
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
Pa
r
a
m
e
t
e
r

S
a
m
p
l
e

I
D

R
e
s
u
l
t

U
n
i
t
s
15
A

N
C
A
C
2L

S
t
a
n
d
a
r
d
Hi
s
t
o
r
i
c
a
l

C
o
n
c
e
n
t
r
a
t
i
o
n
s

C
a
u
s
e

a
n
d

S
i
g
n
i
f
i
c
a
n
c
e
MW
-
1

6
.
2

5
.
9

-

7
.
0

p
H

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

a
t

M
W
-
1
.
MW
-
1
D

6
.
2

5
.
9

-

7
.
0

p
H

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

a
t

M
W
-
1
D
.
MW
-
2
A

6
.
5

5
.
7

-

7
.
4

p
H

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

a
t

M
W
-
2
A
.
MW
-
3

6
.
4

5
.
7

-

7
.
5

p
H

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

a
t

M
W
-
3
.
MW
-
4

5
.
7

5
.
3

-

8
.
1

p
H

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

a
t

M
W
-
4
.
MW
-
4
R

6
.
1

5
.
9

-

6
.
3

p
H

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

a
t

M
W
-
4
R
.

T
h
i
s

i
s

t
h
e

s
i
x
t
h

s
a
m
p
l
i
n
g

e
v
e
n
t

a
t

m
o
n
i
t
o
r
i
n
g

w
e
l
l

M
W
-
4
R
.
MW
-
1
1

5
.
0

4
.
3

-

5
.
3

p
H

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

a
t

M
W
-
1
1
.
MW
-
1
1
D

5
.
7

5
.
3

-

6
.
2

p
H

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

a
t

M
W
-
1
1
D
.
MW
-
1
2

4
.
9

4
.
7

-

5
.
6

p
H

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

a
t

M
W
-
1
2
.
MW
-
1
2
D

6
.
3

6
.
1

-

7
.
4

p
H

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

a
t

M
W
-
1
2
D
.
Di
c
h
l
o
r
o
m
e
t
h
a
n
e

M
W
-
4
D

6
.
8
3

µ
g
/
L

5

0
.
5
3

-

7
.
5
Dic
h
l
o
r
o
m
e
t
h
a
n
e

c
o
n
c
e
n
t
r
a
t
i
o
n

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

i
n

M
W
-
4
D
.

M
W
-
4
D

i
s

l
o
c
a
t
e
d

a
p
p
r
o
x
i
m
a
t
e
l
y

15

f
e
e
t

o
u
t
s
i
d
e

t
h
e

w
a
s
t
e

b
o
u
n
d
a
r
y

a
n
d

a
p
p
r
o
x
i
m
a
t
e
l
y

1
1
0

f
e
e
t

w
i
t
h
i
n

t
h
e

l
a
n
d
f
i
l
l

r
e
v
i
e
w

b
o
u
n
d
a
r
y
.

MW
-
4

2
.
2
4

0
.
8
8

-

2
.
3
Te
t
r
a
c
h
l
o
r
o
e
t
h
y
l
e
n
e

c
o
n
c
e
n
t
r
a
t
i
o
n

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

i
n

M
W
-
4
.

M
W
-
4

i
s

l
o
c
a
t
e
d

a
p
p
r
o
x
i
m
a
t
e
l
y

15

f
e
e
t

o
u
t
s
i
d
e

t
h
e

w
a
s
t
e

b
o
u
n
d
a
r
y

a
n
d

a
p
p
r
o
x
i
m
a
t
e
l
y

1
1
0

f
e
e
t

w
i
t
h
i
n

t
h
e

l
a
n
d
f
i
l
l

r
e
v
i
e
w

b
o
u
n
d
a
r
y
.

MW
-
4
D

1
.
4
8

0
.
5
2

-

1
.
7
3
Te
t
r
a
c
h
l
o
r
o
e
t
h
y
l
e
n
e

c
o
n
c
e
n
t
r
a
t
i
o
n

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

i
n

M
W
-
4
D
.

M
W
-
4
D

i
s

l
o
c
a
t
e
d

ap
p
r
o
x
i
m
a
t
e
l
y

1
5

f
e
e
t

o
u
t
s
i
d
e

t
h
e

w
a
s
t
e

b
o
u
n
d
a
r
y

a
n
d

a
p
p
r
o
x
i
m
a
t
e
l
y

1
1
0

f
e
e
t

w
i
t
h
i
n

t
h
e

l
a
n
d
f
i
l
l

r
e
v
i
e
w

b
o
u
n
d
a
r
y
.

Tr
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e

M
W
-
4
D

4
.
1
1

µ
g
/
L

3

0
.
5
8

-

5
.
2
Tr
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e

c
o
n
c
e
n
t
r
a
t
i
o
n

i
s

c
o
n
s
i
s
t
e
n
t

w
i
t
h

h
i
s
t
o
r
i
c
a
l

r
e
a
d
i
n
g
s

i
n

M
W
-
4
D
.

M
W
-
4
D

i
s

l
o
c
a
t
e
d

a
p
p
r
o
x
i
m
a
t
e
l
y

15

f
e
e
t

o
u
t
s
i
d
e

t
h
e

w
a
s
t
e

b
o
u
n
d
a
r
y

a
n
d

a
p
p
r
o
x
i
m
a
t
e
l
y

1
1
0

f
e
e
t

w
i
t
h
i
n

t
h
e

l
a
n
d
f
i
l
l

r
e
v
i
e
w

b
o
u
n
d
a
r
y
.
No
t
e
s
:
1
.

1
5
A

N
C
A
C

2
L

S
t
a
n
d
a
r
d

r
e
f
e
r
s

t
o

C
l
a
s
s

G
A

S
t
a
n
d
a
r
d
s

a
s

f
o
u
n
d

i
n

1
5
A

N
C
A
C

0
2
L

.
0
2
0
2

G
r
o
u
n
d
w
a
t
e
r

Q
u
a
l
i
t
y

S
t
a
n
d
a
r
d
s
,

l
a
s
t

a
m
e
n
de
d

o
n

A
p
r
i
l

1
,

2
0
1
3
.

2
.

µ
g
/
L

i
n
d
i
c
a
t
e
s

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r
.
3
.

S
U

i
n
d
i
c
a
t
e
s

S
t
a
n
d
a
r
d

U
n
i
t
s
.
4
.

H
i
s
t
o
r
i
c
a
l

c
o
n
c
e
n
t
r
a
t
i
o
n
s

b
a
s
e
d

o
n

d
a
t
a

i
n

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C

a
n
a
l
y
t
i
c
a
l

r
e
s
u
l
t
s

d
a
t
a
b
a
s
e
.
5
.

A
n
a
l
y
t
i
c
a
l

r
e
s
u
l
t
s

o
b
t
a
i
n
e
d

f
r
o
m

E
l
e
c
t
r
o
n
i
c

D
a
t
a

D
e
l
i
v
e
r
a
b
l
e

(
E
D
D
)

p
r
o
v
i
d
e
d

b
y

T
i
m

H
u
n
s
u
c
k
e
r

o
f

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
o
n

A
u
g
u
s
t

2
6
,

2
0
1
6
.
Sa
m
p
l
e

D
a
t
e
:

J
u
l
y

1
3
,

2
0
1
6
Fie
l
d

s
a
m
p
l
i
n
g

p
e
r
f
o
r
m
e
d

b
y

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
pH

S
U

6
.
5

-

8
.
5
0.7
Te
t
r
a
c
h
l
o
r
o
e
t
h
y
l
e
n
e

µ
g
/
L
Page 1 of 1
Ta
b
l
e

6

-

S
u
r
f
a
c
e

W
a
t
e
r

F
i
e
l
d

a
n
d

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
Fi
e
l
d

p
H

3
2
0

S
U

5
1
9
3

-

N
E

6
.
0
-
9
.
0

6
.
5
-
8
.
5
*
Sp
e
c
i
f
i
c

C
o
n
d
u
c
t
a
n
c
e

3
2
3

µ
Լ /c
m

5
1
9
3

-

N
E

N
E

N
E
Te
m
p
e
r
a
t
u
r
e

3
2
5

°
C

5
1
9
3

-

N
E

N
E

N
E
Ar
s
e
n
i
c
14
µg/
L
24
8

0
.
3
7
1

J

0
.
0
7
8

1
0
10

1
0
Ar
s
e
n
i
c
,

d
i
s
s
o
l
v
e
d
14
µg/
L
24
8

0
.
1
7
7

J

0
.
0
7
8

1
0
15
0

N
E
Ba
r
i
u
m
15
µg/
L
24
8

3
3
.
7
J'
0.1

1
0
0
NE

2
,
0
0
0
Ba
r
i
u
m
,

d
i
s
s
o
l
v
e
d
15
µg/
L
24
8

3
1
.
6
J'
0.1

1
0
0
NE

N
E
Ca
d
m
i
u
m
34
µg/
L
24
8

0
.
1
0
1

U

0
.
1
0
1

1
NE

5
Ca
d
m
i
u
m
,

d
i
s
s
o
l
v
e
d

(
h
)
34
µg/
L
24
8

0
.
1
0
1

U

0
.
1
0
1

1
0.1
5

N
E
Ch
r
o
m
i
u
m
51
µg/
L
24
8

0
.
5

U

0
.
5

1
0
NE

1
0
0
Ch
r
o
m
i
u
m
,

d
i
s
s
o
l
v
e
d

†
51
µg/
L
24
8

0
.
5

U

0
.
5

1
0
11

N
E
Le
a
d
13
1
µg/
L
24
8

0
.
1
6
7

J

0
.
0
6
5

1
0
NE

1
5
Le
a
d
,

d
i
s
s
o
l
v
e
d

(
h
)
13
1
µg/
L
24
8

0
.
0
6
5

U

0
.
0
6
5

1
0
0.5
4

N
E
Me
r
c
u
r
y

1
3
2
µg/
L
24
8

0
.
0
3
3
4

U

0
.
0
3
3
4

0
.
2

0
.
0
1
2

2
Se
l
e
n
i
u
m

1
8
3
µg/
L
24
8

0
.
0
9
2

U

0
.
0
9
2

1
0

5

5
0
Sil
v
e
r

1
8
4
µg/
L
24
8

0
.
7

U

0
.
7

1
0
NE

1
0
0
*
Sil
v
e
r
,

d
i
s
s
o
l
v
e
d

1
8
4
µg/
L
24
8

0
.
8
7

J

1
8

1
0
0.0
6

N
E
Su
l
f
a
t
e

3
1
5
µg/
L
24
8

1
,
2
1
0
J'
18

2
5
0
,
0
0
0
NE

2
5
0
,
0
0
0
*
EP
A

8
2
6
0
B

(
V
O
C
s
)
No
t
e
s
:
1
.

C
o
n
c
e
n
t
r
a
t
i
o
n
s

p
r
e
s
e
n
t
e
d

i
n

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r

(
µ
g
/
L
)
.
2
.

S
U

i
n
d
i
c
a
t
e
s

S
t
a
n
d
a
r
d

U
n
i
t
s
.
3
.

µ
Լ /c
m

i
n
d
i
c
a
t
e
s

m
i
c
r
o
m
h
o
s

p
e
r

c
e
n
t
i
m
e
t
e
r
.
4
.

S
W
S

I
D

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

I
d
e
n
t
i
f
i
c
a
t
i
o
n

N
u
m
b
e
r
.
5
.

M
D
L

i
s

t
h
e

l
a
b
o
r
a
t
o
r
y

m
e
t
h
o
d

d
e
t
e
c
t
i
o
n

l
i
m
i
t
.

T
h
e

M
D
L

v
a
l
u
e
s

p
r
e
s
e
n
t
e
d

a
r
e

f
o
r

s
a
m
p
l
e
s

n
o
t

d
i
l
u
t
e
d

b
y

t
h
e

l
a
b
o
r
a
t
o
r
y

d
u
r
i
ng

a
n
a
l
y
s
i
s
.

6
.

S
W
S
L

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

L
i
m
i
t
.

N
C
D
E
Q

d
e
f
i
n
e
s

t
h
e

S
W
S
L

a
s

t
h
e

l
o
w
e
s
t

a
m
o
u
n
t

o
f

a
n
a
l
y
t
e

i
n

a

s
a
m
p
l
e

t
h
a
t

c
a
n

b
e

q
u
a
nt
i
t
a
t
i
v
e
l
y

d
e
t
e
r
m
i
n
e
d

w
i
t
h

s
u
i
t
a
b
l
e

p
r
e
c
i
s
i
o
n

a
n
d

a
c
c
u
r
a
c
y
.

7
.

1
5
A

N
C
A
C

2
B

S
t
a
n
d
a
r
d

i
s

f
r
o
m

"
N
o
r
t
h

C
a
r
o
l
i
n
a

A
d
m
i
n
i
s
t
r
a
t
i
v
e

C
o
d
e
,

T
i
t
l
e

1
5
A
:

D
e
p
a
r
m
e
n
t

o
f

E
n
v
i
r
o
n
m
e
n
t
a
l

Q
u
a
l
i
t
y
,

S
u
b
c
h
a
p
t
e
r
2
B

-

S
u
r
f
a
c
e

W
a
t
e
r

a
n
d

W
e
t
l
a
n
d

S
t
a
n
d
a
r
d
s
,
"

(
l
a
s
t

a
m
e
n
d
e
d

o
n

J
a
n
u
a
r
y

1
,

2
0
1
5
)

f
o
r

C
l
a
s
s

W
S
-
I
V

w
a
t
e
r
s
.
8
.

M
C
L

i
s

t
h
e

F
e
d
e
r
a
l

M
a
x
i
m
u
m

C
o
n
t
a
m
i
n
a
n
t

L
e
v
e
l

a
s

f
o
u
n
d

i
n

4
0

C
F
R
,

S
u
b
p
a
r
t

G
,

§
1
4
1
.
6
2
.
9
.

*

C
o
n
c
e
n
t
r
a
t
i
o
n

l
i
s
t
e
d

i
s

a

s
e
c
o
n
d
a
r
y

m
a
x
i
m
u
m

c
o
n
t
a
m
i
n
a
n
t

l
e
v
e
l

(
S
M
C
L
)
.

S
M
C
L
s

a
r
e

e
s
t
a
b
l
i
s
h
e
d

b
y

E
P
A

i
n

t
h
e

N
a
t
i
o
n
a
l

S
e
c
o
nd
a
r
y

D
r
i
n
k
i
n
g

W
a
t
e
r

R
e
g
u
l
a
t
i
o
n
s

a
s

f
o
u
n
d

i
n

4
0

C
F
R

§
1
4
3
.
3
.
10
.

N
E

i
n
d
i
c
a
t
e
s

n
o
t

e
s
t
a
b
l
i
s
h
e
d
.

11
.

G
r
a
y
e
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

v
a
l
u
e
s

t
h
a
t

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

S
W
S
L
.
12
.

B
o
l
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

v
a
l
u
e
s

t
h
a
t

a
t
t
a
i
n

o
r

e
x
c
e
e
d

t
h
e

1
5
A

N
C
A
C

2
B

S
t
a
n
d
a
r
d
.
13
.

Q
u
a
l
i
f
i
e
r
s

i
n

n
o
n
-
i
t
a
l
i
c
i
z
e
d

t
e
x
t

a
r
e

l
a
b
o
r
a
t
o
r
y

d
a
t
a

q
u
a
l
i
f
i
e
r
s

o
r

"
f
l
a
g
s
"
.

"
U
"

i
s

u
s
e
d

t
o

i
d
e
n
t
i
f
y

r
e
s
u
l
t
s

n
o
t

d
e
t
e
c
t
e
d

a
t c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

t
h
e

l
a
b
o
r
a
t
o
r
y
'
s

M
D
L
.

"
J
"

i
s

u
s
e
d

t
o

i
d
e
n
t
i
f
y

e
s
t
i
m
a
t
e
d

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

M
D
L

b
u
t

a
r
e

l
e
s
s

t
h
a
n

t
h
e

l
a
b
o
r
a
t
o
r
y's

m
e
t
h
o
d

r
e
p
o
r
t
i
n
g

l
i
m
i
t

(
M
R
L
)
.

A
n

i
t
a
l
i
c
i
z
e
d

J'
-f
l
a
g

i
s

a

d
a
t
a

q
u
a
l
i
f
i
e
r
,

a
d
d
e
d

b
y

H
D
R

t
o

i
n
d
i
c
a
t
e

c
o
n
c
e
n
t
r
a
t
i
o
n
s

w
h
i
c
h

e
q
u
a
l

o
r

a
r
e

g
r
e
a
t
e
r

t
h
a
n

t
h
e

l
a
b
o
r
a
t
o
r
y
'
s

M
R
L

b
u
t

a
r
e
l
e
s
s

t
h
a
n

t
h
e

S
W
S
L
.

14
.

†

S
t
a
n
d
a
r
d

l
i
s
t
e
d

i
s

m
o
s
t

s
t
r
i
n
g
e
n
t

o
f

C
r
(
I
I
I
)

a
n
d

C
r
(
V
I
)
.
15
.

(
h
)

S
t
a
n
d
a
r
d

i
s

h
a
r
d
n
e
s
s

d
e
p
e
n
d
e
n
t
;

s
t
a
n
d
a
r
d

i
s

d
i
s
p
l
a
y
e
d

a
s
s
u
m
i
n
g

a

h
a
r
d
n
e
s
s

o
f

≤ 2
5

m
g
/
L
.
16
.

R
e
s
u
l
t
s

f
o
r

a
l
l

S
W
-
8
4
6

M
e
t
h
o
d

8
2
6
0

c
o
n
s
t
i
t
u
e
n
t
s

w
e
r
e

l
e
s
s

t
h
a
n

t
h
e
i
r

M
D
L
s
.
17
.

A
n
a
l
y
t
i
c
a
l

r
e
s
u
l
t
s

o
b
t
a
i
n
e
d

f
r
o
m

E
l
e
c
t
r
o
n
i
c

D
a
t
a

D
e
l
i
v
e
r
a
b
l
e

(
E
D
D
)

p
r
o
v
i
d
e
d

b
y

T
i
m

H
u
n
s
u
c
k
e
r

o
f

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s

o
n

A
u
gu
s
t

2
6
,

2
0
1
6
.
SE
E

N
O
T
E

1
6
15
A

N
C
A
C

2
B

St
a
n
d
a
r
d
F
e
d
e
r
a
l
MC
L
MD
L
23
.
6
9
12
2
7.
3
La
b
o
r
a
t
o
r
y

C
e
r
t
i
f
i
c
a
t
e

C
o
d
e
s
:
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s

F
i
e
l
d

#
5
1
9
3
Du
k
e

E
n
e
r
g
y

A
n
a
l
y
t
i
c
a
l

L
a
b
o
r
a
t
o
r
y

#
2
4
8
Te
s
t
A
m
e
r
i
c
a

L
a
b
o
r
a
t
o
r
i
e
s
,

I
n
c
.

#
3
8
7
Sa
m
p
l
e

D
a
t
e
:

J
u
l
y

1
3
,

2
0
1
6

Fi
e
l
d

S
a
m
p
l
i
n
g

p
e
r
f
o
r
m
e
d

b
y

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C

SW
S
L
Pa
r
a
m
e
t
e
r

S
W
S

I
D

U
n
i
t
s
Ce
r
t
i
f
i
c
a
t
e
Co
d
e

S
W
-
1
Page 1 of 1
Ta
b
l
e

8

-

R
a
d
i
o
l
o
g
i
c
a
l

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#

1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
MW
-
1

M
W
-
1
D

M
W
-
2
A

M
W
-
2
D

M
W
-
3

M
W
-
3
D

M
W
-
4

M
W
-
4
R

M
W
-
4
D

M
W
-
4
D
R

M
W
-
1
1

M
W
-
1
1
D

M
W
-
1
2

M
W
-
1
2
D
Alp
h
a

p
C
i
/
L
24
8
<-
0
.
1
1

<
0
.
0
3
6
7

<
-
0
.
0
0
9
4

<
-
0
.
1

<
-
0
.
1

<
0
.
2
1
1

<
0
.
1
0
5

<
-
0
.
1
1

<
-
0
.
0
6
4

<
0
.
1
0
2

<
0
.
2

<
0
.
0
4
4
3

<
0
.
2
3
7

<
0
.
1
9
9

<
-
0
.
2
2
Ba
L
a
-
1
4
0

p
C
i
/
L
24
8
<1
1
.
2

<
8
.
6
7

<
6
.
6
3

<
6
.
7
4

<
6
.
7
4

<
9
.
3

<
5
.
6
7

<
3
.
8
5

<
5
.
9
7

<
5
.
2
5

<
3
.
9
7

<
8
.
3
9

<
7
.
7

<
5
.
0
6

<
7
.
4
9
Be
-
7

p
C
i
/
L
24
8
<4
5
.
4

1
2
.
1

<
4
0

<
4
0
.
2

<
4
0
.
2

<
4
3
.
9

<
4
1
.
3

<
3
0
.
6

<
4
4
.
5

<
3
4
.
9

<
3
8
.
8

<
4
2
.
4

<
4
0
.
2

<
2
1
.
1

<
4
7
Be
t
a

p
C
i
/
L
24
8
1.6
6

2
.
6
5

1
.
7

0
.
9
5
8

0
.
9
5
8

0
.
8
7
2

0
.
6
1
8

0
.
7
4
2

<
0
.
4
0
5

1
.
5
2

<
0
.
0
8
0
8

<
-
0
.
4
9

1
.
2
9

<
0
.
2
3
9

1
.
8
Co
-
5
8

p
C
i
/
L
24
8
<5
.
6

<
6
.
5
7

<
4
.
6
2

<
6
.
6
3

<
6
.
6
3

<
5
.
4
8

<
5
.
7
7

<
4
.
0
4

<
6
.
1
5

<
4
.
3
9

<
3
.
5

<
4
.
8
6

<
3
.
6
5

<
2
.
9
1

<
5
.
2
3
Co
-
6
0

p
C
i
/
L
24
8
<7
.
2
1

<
8
.
5
1

<
5
.
6
6

<
6
.
7

<
6
.
7

<
5
.
9
4

<
5
.
8
3

<
4
.
9
7

<
5
.
3
9

<
5
.
3
6

<
4
.
5
3

<
7
.
4
4

<
6
.
3
8

<
3
.
2
2

<
5
.
2
7
Cs
-
1
3
4

p
C
i
/
L
24
8
<6
.
9
6

<
6
.
3
2

<
5
.
9
3

<
5
.
8
9

<
5
.
8
9

<
6

<
5
.
4
3

<
4
.
5
9

<
6
.
1
3

<
7
.
5
4

<
6
.
8
5

<
6
.
1
8

<
7
.
0
8

<
3
.
0
8

<
5
.
5
2
Cs
-
1
3
7

p
C
i
/
L
24
8
<
5
.
7

<
5
.
6
9

<
5
.
3
4

<
6
.
2
1

<
6
.
2
1

<
7
.
8
6

<
4
.
9
4

<
4
.
9
1

<
4
.
2
5

<
6
.
5
8

<
5
.
6
1

<
5
.
8
1

<
5
.
8
6

<
3
.
2

<
4
.
9
9
Fe
-
5
9

p
C
i
/
L
24
8
<1
0
.
8

<
1
2
.
5

<
8
.
7
8

<
1
1
.
6

<
1
1
.
6

<
1
3
.
2

<
1
1
.
2

<
9
.
0
7

<
8
.
9

<
8
.
3
5

<
1
0
.
9

<
1
1
.
1

<
1
2
.
2

<
5
.
3
1

<
7
.
1
2
H3
G
W

p
C
i
/
L
24
8
<-1
9

<
-
9
.
5

<
3
3
.
7

<
3
6
.
1

<
3
6
.
1

<
-
2
6

<
-
6
8

<
-
5
9

<
-
5
5

<
-
1
8

<
-
3
6

<
7
9
.
2

<
-
7
.
6

<
1
4
.
4

<
-
5
3
I-
1
3
1

p
C
i
/
L
24
8
<6
.
4

<
7
.
1
8

<
5
.
2
1

<
6
.
0
3

<
6
.
0
3

<
5
.
8
5

<
4
.
8

<
4
.
3
9

<
6
.
4
8

<
5
.
5
3

<
5
.
7
6

<
8
.
3
7

<
4
.
3
2

<
4
.
1
3

<
7
.
9
K-4
0

p
C
i
/
L
24
8
<1
0
6

5
2
.
5

7
7
.
5

<
9
5
.
3

<
9
5
.
3

5
7
.
4

<
9
0
.
7

<
8
8
.
3

<
6
8
.
6

<
1
0
7

1
5
2

1
0
6

9
.
7
2

7
0
.
5

5
2
.
3
Mn
-
5
4

p
C
i
/
L
24
8
<6
.
8
6

<
6
.
6
3

<
4
.
8
8

<
4
.
7
2

<
4
.
7
2

<
5
.
9
1

<
6
.
8

<
3
.
7
9

<
6
.
3
6

<
4
.
9
8

<
5
.
7
3

<
4
.
7
6

<
5
.
0
9

<
3
.
1
6

<
4
.
7
1
Nb
-
9
5

p
C
i
/
L
24
8
<7

<
6
.
4
8

<
4
.
4
5

<
6
.
3
9

<
6
.
3
9

<
5
.
8
2

<
6
.
9
3

<
5
.
0
1

<
4
.
7
5

<
5
.
2
4

<
5
.
6
7

<
5
.
1
5

<
6
.
4
5

<
3
.
2

<
5
.
0
2
Zn
-
6
5

p
C
i
/
L
24
8
<1
2
.
8

<
5
.
3

<
1
1
.
1

<
1
4
.
2

<
1
4
.
2

<
1
2
.
3

<
1
1
.
5

<
7
.
8

<
1
0
.
9

<
1
3

<
1
0
.
4

<
1
0
.
4

<
1
1
.
7

<
5
.
0
2

<
1
0
Zr
-
9
5

p
C
i
/
L
24
8
<1
0
.
1

<
1
0
.
9

<
8
.
3
8

<
1
1
.
5

<
1
1
.
5

<
1
0
.
5

<
8
.
6
8

<
7
.
9

<
7
.
7
7

<
7
.
6
3

<
8
.
0
3

<
8
.
9
6

<
1
0
.
3

<
4
.
9

<
8
.
3
7
No
t
e
s
:
1
.

C
o
n
c
e
n
t
r
a
t
i
o
n
s

p
r
e
s
e
n
t
e
d

i
n

p
i
c
o
c
u
r
i
e
s

p
e
r

l
i
t
e
r

(
p
C
i
/
L
)
.
2
.

N
S

i
n
d
i
c
a
t
e
s

n
o

s
a
m
p
l
e

w
a
s

c
o
l
l
e
c
t
e
d
.
3
.

A
n
a
l
y
t
i
c
a
l

r
e
s
u
l
t
s

o
b
t
a
i
n
e
d

f
r
o
m

E
n
R
a
d

L
a
b
o
r
a
t
o
r
y

R
e
p
o
r
t

J
o
b
:

M
N
S
_
9
J
U
N
2
0
1
6
_
A

M
c
G
u
i
r
e

L
a
n
d
f
i
l
l

1

G
r
o
u
n
d
w
a
t
e
r
s

p
r
o
v
i
d
e
d

b
y

T
i
m
H
u
n
s
u
c
k
e
r

o
f

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s

o
n

A
u
g
u
s
t

2
6
,

2
0
1
6
.
Sa
m
p
l
e

D
a
t
e
:

J
u
l
y

1
3
,

2
0
1
6
Fi
e
l
d

S
a
m
p
l
i
n
g

P
e
r
f
o
r
m
e
d

b
y

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
Laboratory Certification Code Duke Energy Analytical Laboratory #248
Pa
r
a
m
e
t
e
r

U
n
i
t
s
Ce
r
t
i
f
i
c
a
t
e
Co
d
e
SW-1
Mo
n
i
t
o
r
i
n
g

W
e
l
l
s
Page 1 of 1

A
Appendix A
Field Sampling Forms

ANALYZER SERIAL #:
WEATHER CONDITIONS:
DATE:TIME:DATE:TIME:
Calibation Instrument Standard Instrument Standard
Standard Value Value Value Value
SS 0.0 ▬▬►0.0 0.0 ▬/▬►0.0
SS 229.0 ▬▬►227 223.0 ▬/▬►227
SS 72.9 ▬/▬►75 73.5 ▬/▬►75
SS ▬/▬►1410 ▬/▬►1410
B (7.00)7.00 ▬▬►7.02 7.26 ▬/▬►7.02
B (4.00)4.20 ▬▬►4.00 4.33 ▬/▬►4.00
B (10.00)10.22 ▬▬►10.06 10.40 ▬/▬►10.04
20.26 20.58
pH Check B (7.00)▬▬►7.13
Time:0.00
425 ▬▬►440 438 ▬/▬►440
N/A ▬/▬►N/A N/A ▬/▬►N/A
Zobell's 20.23 20.40
TEMP (CO)
BP (mmHg)
COND
100 % mg/L 8.91 ▬▬►8.89 8.87 ▬/▬►8.87
After Cal 8.92 100.29 8.85 99.73
LCS 8.87 99.73 8.85 99.73
LCSD 8.88 0.11 8.83 -0.23
SS 53.1 ▬/▬►54.5 53.1 ▬/▬►54.5
NIST N/A ▬/▬►N/A N/A ▬/▬►N/A
KEY:
NOTES:
FIELD SAMPLING CALIBRATION FORM
STUDY:McGUIRE NUCLEAR STATION - LANDFILL 1 GROUNDWATER MONITORING
DATE (s):July 13, 2016 SURFACE UNIT READER:LDC
OTHER EQUIPMENT:TURBIDIMETER NO.2 - 3260-GW Clear, slight breeze, 75 to 85 deg F
COLLECTORS:LDC, PSP SURFACE UNIT SERIAL #:0722
ANALYZER MODEL#:HL4 400504
Calibration Date / Time 13-Jul-16 445 14-Jul-16 415
PROCEDURE #:HYDROLAB 3210.6 VALIDATED BY:
Parameter Calibration Results Calibration Results
CALIBRATION BP (mmHg)744.64 CALIBRATION BP (mmHg)743.16
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
INSTRUMENT ZEROED INSTRUMENT ZEROED
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
CHECK (uS/cm)
SPEC. COND.
(uS/cm)
pH
(units)
CALIBRATION ACCEPTED CALIBRATION FAILED
CALIBRATION ACCEPTED CALIBRATION FAILED
CALIBRATION ACCEPTED CALIBRATION FAILED
Buffer Temp.Buffer Temp.
ORP Temp.ORP Temp.
ORP CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Buffer Temp.
107.1
CALIBRATION PASS CALIBRATION PASS
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
After Cal % SAT After Cal % SAT
TURB
(ntu)CALIBRATION ACCEPTED CALIBRATION ACCEPTED
CALIBRATION PASS CALIBRATION PASS
DO
(mg/L)
20.04 20.05
744.64 743.16
105.9
Temp Cert Device #
TEMP
(deg C)Adjustment Not Available Adjustment Not Available
Tested - OK Replaced ref Electrode KCL
See Notes Replaced Ref. Electrode Tip
INSTRUMENT MAINTENANCE DATE / TIME
Conductance Subsystem pH Subsystem
Cleaned Electrodes Cleaned Electrodes
Tested - OK See Notes Tested - OK See Notes
Dissolved Oxygen Subsystem
Replaced Teflon Membrane Cleaned Electrode
Tested - OK See Notes
Oxidation Reduction Subsystem Temperature Subsystem
Cleaned Electrode Cleaned Electrode
Replaced DO electrolyte See Notes
Field Barometric Pressure
Beginning BP 744.9 (mmHg)Ending BP 745.4
SS = Standard solution AW = Average Winkler ▬/▬►= Not Adjusted To
TSH 7/15/16 - post cal of pH failed. Reviewed field data & and historical pH values for impacted wells. All pH values are similar to hitorical
values. Resample not warranted.
(mmHg)
B = Buffer W = Winkler ▬▬► = Adjusted To N/A = Not Applicable
ANALYZER SERIAL #:
WEATHER CONDITIONS:
DATE:TIME:DATE:TIME:
Calibation Instrument Standard Instrument Standard
Standard Value Value Value Value
SS 0.0 ▬▬►0.0 0.0 ▬/▬►0.0
SS 231.4 ▬▬►227 218.1 ▬/▬►227
SS 72.1 ▬/▬►75 73.5 ▬/▬►75
SS ▬/▬►1410 ▬/▬►1410
B (7.00)7.07 ▬▬►7.02 7.06 ▬/▬►7.02
B (4.00)4.08 ▬▬►4.00 4.03 ▬/▬►4.00
B (10.00)10.11 ▬/▬►10.04 10.11 ▬/▬►10.04
20.54 20.52
pH Check B (7.00)▬▬►7.13
Time:0.00
439 ▬▬►440 437 ▬/▬►440
N/A ▬/▬►N/A N/A ▬/▬►N/A
Zobell's 20.45 20.37
TEMP (CO)
BP (mmHg)
COND
100 % mg/L 8.83 ▬▬►8.89 8.91 ▬/▬►8.87
After Cal 8.90 100.14 8.92 100.53
LCS 8.89 100.03 8.88 100.08
LCSD 8.88 -0.11 8.89 0.11
SS 52.9 ▬/▬►53.5 53.6 ▬/▬►53.5
NIST N/A ▬/▬►N/A N/A ▬/▬►N/A
KEY:
NOTES:
FIELD SAMPLING CALIBRATION FORM
STUDY:McGUIRE NUCLEAR STATION - LANDFILL 1 GROUNDWATER MONITORING
DATE (s):July 13, 2016 SURFACE UNIT READER:PSP
OTHER EQUIPMENT:TURBIDIMETER NO.1 - 3260-GW Clear, slight breeze, 75 to 85 deg F
COLLECTORS:LDC, PSP SURFACE UNIT SERIAL #:0730
ANALYZER MODEL#:HL4 400440
Calibration Date / Time 13-Jul-16 355 14-Jul-16 430
PROCEDURE #:HYDROLAB 3210.6 VALIDATED BY:
Parameter Calibration Results Calibration Results
CALIBRATION BP (mmHg)744.64 CALIBRATION BP (mmHg)743.16
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
INSTRUMENT ZEROED INSTRUMENT ZEROED
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
CHECK (uS/cm)
SPEC. COND.
(uS/cm)
pH
(units)
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Buffer Temp.Buffer Temp.
ORP Temp.ORP Temp.
ORP CALIBRATION ACCEPTED CALIBRATION ACCEPTED
Buffer Temp.
103.4
CALIBRATION PASS CALIBRATION PASS
CALIBRATION ACCEPTED CALIBRATION ACCEPTED
After Cal % SAT After Cal % SAT
TURB
(ntu)CALIBRATION ACCEPTED CALIBRATION ACCEPTED
CALIBRATION PASS CALIBRATION PASS
DO
(mg/L)
20.08 20.06
744.64 743.16
101.7
Temp Cert Device #
TEMP
(deg C)Adjustment Not Available Adjustment Not Available
Tested - OK Replaced ref Electrode KCL
See Notes Replaced Ref. Electrode Tip
INSTRUMENT MAINTENANCE DATE / TIME
Conductance Subsystem pH Subsystem
Cleaned Electrodes Cleaned Electrodes
Tested - OK See Notes Tested - OK See Notes
Dissolved Oxygen Subsystem
Replaced Teflon Membrane Cleaned Electrode
Tested - OK See Notes
Oxidation Reduction Subsystem Temperature Subsystem
Cleaned Electrode Cleaned Electrode
Replaced DO electrolyte See Notes
Field Barometric Pressure
Beginning BP 744.9 (mmHg)Ending BP 745.4
SS = Standard solution AW = Average Winkler ▬/▬►= Not Adjusted To
(mmHg)
B = Buffer W = Winkler ▬▬► = Adjusted To N/A = Not Applicable
58.55 68.55
35 (psi)9 (sec)(sec)
(gal)
6.54 (gal)
@
QC By:
SAMPLING NOTES
QC for rad collected
ADDITIONAL WELL CONDITION NOTES
Good Tag
WELL CONDITION
PROTECTIVE CASING
WELL PAD
WELL TAG
Good Condition
Good Condition
Good ConditionWELL CASING
LDC 0
TOTAL PURGE
VOLUME
20.25
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY
6.75 NO
6.75 NO 16.55 110 6.15
110 6.08 7.1
(recalculates on
current water
level)(deg C)(umho/cm)(SU)(NTU)(mV-NHE)(mg/L)
16.4 285 0.72
SAMPLING EQUIPMENT
TUBING DIAMETER (in)1/2 OD
QED T1200
PURGE COMPLETE TEMP SPECIFIC pH TURBIDITY
WATER ELEVATION (ft msl)701.80
APPEARANCE
DETECTED ODOR None
Normal
WATER LEVEL
AFTER PURGE *
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88
WELL DEPTH (ft TOC)
WELL DIAMETER (in)MIDDLE OF WETTED SCREEN (ft toc)
WELL VOL
SCREEN INTERVAL (ft TOC)TO
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)28.43 WATER COLUMN (ft)40.12
EQUIPMENT INFORMATION
LEVEL METER SERIAL#28650
68.05PUMP INTAKE DEPTH (ft TOC)68.55
TOC ELEV (ft msl)
GS ELEV (ft msl)
730.23
729.58
WELL/LOCATION NAME MW-1
FIELD CREW LDC, PSP
MONITORING WELL INFORMATION
2
N/A
PROCEDURE NO 3175.4DUKE ENERGY
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING
SAMPLING DATE(s)13-Jul-2016
63.55
PURGE METHOD
Conventional
DISCHARGERECHARGEPRESSURE 6
PUMP CONTROLLER SETTINGS
0.1631CONVERSION FACTOR
Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
6.54WELL VOLUME
(gal)
ORP
(ft)(YES/NO)
6.75 NO 16.35 109 6.06
16.48
VOLUME EVACUATION COND.
7/13/2016 1215
Sample preservation verified to pH
(units)< 2.0
DATE TIME
DISSOLVED
OXYGEN
4.4 265 0.35
0.45272
78.22 88.22
42 (psi)8 (sec)(sec)
(gal)
9.61 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-1D
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)730.61 MIDDLE OF WETTED SCREEN (ft toc)83.22
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)88.22 GS ELEV (ft msl)729.75 PUMP INTAKE DEPTH (ft TOC)87.72
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 7
28650 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)29.31 WATER COLUMN (ft)58.91 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)701.30 WELL VOLUME 9.61
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
9.75 NO 16.21 97 6.09 4.9 284
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
0.20
9.75 NO 16.36 99 6.19 3.4 267 0.12
9.75 NO 16.27 98 6.16 3.1 273 0.12
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
29.25 LDC 7/13/2016 1205 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
67.57 77.57
48 (psi)10 (sec)(sec)
(gal)
4.29 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
13.50 LDC 7/13/2016 1345 0
4.50 NO 17.47 98 6.52 2.2 496 5.82
4.50 NO 16.97 98 6.50 2.4 463 5.21
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
4.50 NO 16.74 99 6.57 2.7 422
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
6.04
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)51.26 WATER COLUMN (ft)26.31 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)688.41 WELL VOLUME 4.29
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
28650 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)739.67 MIDDLE OF WETTED SCREEN (ft toc)72.57
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)77.57 GS ELEV (ft msl)736.96 PUMP INTAKE DEPTH (ft TOC)77.07
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-2A
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
98.82 108.82
50 (psi)5 (sec)(sec)
(gal)
9.05 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
19.25 LDC 7/13/2016 1405 0
5.00 NO 17.05 60 6.93 3.0 489 9.54
5.00 NO 17.08 60 6.94 2.7 474 9.54
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
9.25 78.90 NO 17.02 61 7.01 4.0 451
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
11.01 4.88
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)53.31 WATER COLUMN (ft)55.51 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)687.46 WELL VOLUME 9.05
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
28650 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)740.77 MIDDLE OF WETTED SCREEN (ft toc)103.82
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)108.82 GS ELEV (ft msl)737.41 PUMP INTAKE DEPTH (ft TOC)108.32
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-2D
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
63.64 73.64
38 (psi)10 (sec)(sec)
(gal)
2.74 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
8.50 PSP 7/13/2016 1005 0
3.00 NO 15.74 78 6.39 1.8 419 5.87
2.75 NO 15.72 77 6.36 2.3 424 5.56
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
2.75 NO 15.79 74 6.33 3.7 427
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
4.76
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)56.85 WATER COLUMN (ft)16.79 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)671.58 WELL VOLUME 2.74
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)728.43 MIDDLE OF WETTED SCREEN (ft toc)68.64
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)73.64 GS ELEV (ft msl)724.98 PUMP INTAKE DEPTH (ft TOC)73.14
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-3
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
80.19 90.19
48 (psi)14 (sec)(sec)
(gal)
5.44 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
16.50 PSP 7/13/2016 1030 0
5.50 NO 15.74 116 6.71 2.2 374 2.33
5.50 NO 15.73 114 6.75 1.5 373 2.18
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
5.50 NO 15.70 109 6.71 1.4 372
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
2.25
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)56.81 WATER COLUMN (ft)33.38 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)671.58 WELL VOLUME 5.44
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 6
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)728.39 MIDDLE OF WETTED SCREEN (ft toc)85.19
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)90.19 GS ELEV (ft msl)724.98 PUMP INTAKE DEPTH (ft TOC)89.69
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-3D
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
64.15 74.15
45 (psi)45 (sec)(sec)
(gal)
1600 (ml)
495 (ml)
2095 (ml)=0.55 (gal)@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
0
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
SAMPLE COLLECTED BY DATE TIME
Total Purge Volume PSP 7/13/2016 0710
Sample preservation verified to pH
(units)< 2.0
1.1 314 0.44 N/A
Tubing Volume Purged 0.75 gal.EQUIPMENT PURGE ONLY SAMPLE CHLORINE
(mg/l)Pump (Bladder) Volume
64.03 N/A 67.79 16.21 134 5.67
(ft)(ml/min)(ft)(deg C)(umho/cm)(SU)(NTU)(mV-NHE)(mg/L)
WATER LEVEL RATE WATER LEVEL COND.OXYGEN
INITIAL FLOW FINAL TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)64.03 WATER COLUMN (ft)10.12 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)677.10 WELL VOLUME 1.65
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 15
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Equip. Only Purge
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)741.13 MIDDLE OF WETTED SCREEN (ft toc)69.15
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)74.15 GS ELEV (ft msl)738.40 PUMP INTAKE DEPTH (ft TOC)73.65
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-4
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR EQUIPMENT PURGE ONLY SAMPLING
92.24 102.24
60 (psi)10 (sec)(sec)
(gal)
6.17 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
25.00 PSP 7/13/2016 0835 0
6.25 NO 16.03 175 6.61 2.8 184 0.00
6.25 NO 16.00 175 6.53 4.5 183 0.00
6.25 NO 16.00 173 6.44 18.6 187 0.00
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
6.25 NO 16.01 162 6.37 52.6 202
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
0.00
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)64.44 WATER COLUMN (ft)37.80 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)676.14 WELL VOLUME 6.17
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)740.58 MIDDLE OF WETTED SCREEN (ft toc)97.24
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)102.24 GS ELEV (ft msl)738.25 PUMP INTAKE DEPTH (ft TOC)101.74
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-4D
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
28.00 43.00
30 (psi)13 (sec)(sec)
(gal)
1.20 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
4.00 PSP 7/13/2016 1125 0
1.25 NO 15.80 103 6.11 6.2 343 6.37
1.25 NO 15.47 99 6.13 13.9 329 6.76
OXYGEN (recalculates on
current water
level)(mV -NEH)(mg/L)
1.50 NO 15.55 94 6.17 19.8 307
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
7.09
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
1.20
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)38.36 WATER COLUMN (ft)7.37 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)675.51 WELL VOLUME
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 7
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)713.87 MIDDLE OF WETTED SCREEN (ft toc)42.05
SCREEN LENGTH (ft)15.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)45.73 GS ELEV (ft msl)711.15 PUMP INTAKE DEPTH (ft TOC)45.23
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-4R
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
75.40 90.40
60 (psi)10 (sec)(sec)
(gal)
8.42 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
25.50 PSP 7/13/2016 1220 0
8.50 NO 15.47 131 6.86 4.3 352 4.73
8.50 NO 15.48 130 6.84 2.2 347 4.75
OXYGEN (recalculates on
current water
level)(mV -NEH)(mg/L)
8.50 NO 15.49 130 6.88 4.4 339
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
4.80
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
8.42
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)38.77 WATER COLUMN (ft)51.63 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)674.98 WELL VOLUME
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 5
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)713.75 MIDDLE OF WETTED SCREEN (ft toc)82.90
SCREEN LENGTH (ft)15.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)90.40 GS ELEV (ft msl)711.15 PUMP INTAKE DEPTH (ft TOC)89.90
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-4DR
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
23.45 38.45
25 (psi)13 (sec)(sec)
(gal)
1.32 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
4.50 LDC 7/13/2016 0735 0
0.50 NO 16.26 20 5.02 17.1 454 1.33
0.50 NO 16.14 21 5.04 15.7 445 1.01
0.38
0.50 NO 16.00 21 5.11 13.9 443 0.55
1.50 36.11 NO 15.71 21 5.10 5.7 454 0.38
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
1.50 NO 15.06 22 5.16 14.7 495
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
0.23
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)30.34 WATER COLUMN (ft)8.11 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)692.26 WELL VOLUME 1.32
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 7
28650 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)722.60 MIDDLE OF WETTED SCREEN (ft toc)34.40
SCREEN LENGTH (ft)15.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)38.45 GS ELEV (ft msl)720.10 PUMP INTAKE DEPTH (ft TOC)37.95
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-11
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
91.55 101.55
50 (psi)8 (sec)(sec)
(gal)
11.47 (gal)
@
QC By:
SAMPLING NOTES
After initial well volume is removed - WL drops to 65 ft - recalculate well volume and use for subsequent readings.
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
28.50 LDC 7/13/2016 0815 0
8.50 NO 15.27 29 5.70 3.8 549 6.81
8.50 NO 15.27 29 5.63 8.6 511 6.78
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
11.50 51.02 NO 15.29 29 5.58 7.5 484
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
6.69 8.24
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)31.20 WATER COLUMN (ft)70.35 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)691.94 WELL VOLUME 11.47
See note below PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 7
28650 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)723.14 MIDDLE OF WETTED SCREEN (ft toc)96.55
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)101.55 GS ELEV (ft msl)720.84 PUMP INTAKE DEPTH (ft TOC)101.05
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-11D
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
14.49 29.49
18 (psi)14 (sec)(sec)
(gal)
630 (ml)
495 (ml)
1125 (ml)=0.30 (gal)@
QC By:
SAMPLING NOTES
Decided to equipment purge since this well has previously been not sampled when well volume is low and didn’t want to chance evacuating the well. After sampling, the
drawdown seemed stable at 26.43 ft so this well can probably be sampled like the Jan 2016 event (conventional).
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
NA
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
SAMPLE COLLECTED BY DATE TIME
Total Purge Volume LDC 7/13/2016 0910
Sample preservation verified to pH
(units)< 2.0
15.3 580 3.44 N/A
Tubing Volume Removed 0.5 gal.EQUIPMENT PURGE ONLY SAMPLE CHLORINE
(mg/l)Pump (Bladder) Volume
25.21 180 26.43 15.83 23 4.92
(ft)(ml/min)(ft)(deg C)(umho/cm)(SU)(NTU)(mV -NEH)(mg/L)
WATER LEVEL RATE WATER LEVEL COND.OXYGEN
INITIAL FLOW FINAL TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)25.21 WATER COLUMN (ft)4.28 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)699.60 WELL VOLUME 0.70
See notes PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 6
28650 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Equip. Only Purge
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)724.81 MIDDLE OF WETTED SCREEN (ft toc)27.35
SCREEN LENGTH (ft)15.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)29.49 GS ELEV (ft msl)722.21 PUMP INTAKE DEPTH (ft TOC)28.99
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-12
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR EQUIPMENT PURGE ONLY SAMPLING
58.42 68.42
35 (psi)10 (sec)(sec)
(gal)
6.90 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
15.50 LDC 7/13/2016 0955 0
4.25 NO 15.09 80 6.28 4.9 538 7.74
4.25 NO 15.10 79 6.28 6.2 539 7.85
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
7.00 42.83 NO 15.08 79 6.29 7.3 538
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
7.90 4.17
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
6.90
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)26.10 WATER COLUMN (ft)42.32 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)698.67 WELL VOLUME
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
28650 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)724.77 MIDDLE OF WETTED SCREEN (ft toc)63.42
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)68.42 GS ELEV (ft msl)722.21 PUMP INTAKE DEPTH (ft TOC)67.92
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME MW-12D
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
0.00 0.00
N/A (psi)N/A (sec)(sec)
(gal)
(ft)=(in)@
QC By:
SAMPLING NOTES
PROTECTIVE CASING
WELL PAD
WELL CASING
WELL TAG
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
1255
186 7.19
0
N/A
Deployed Water Column In Screen
Above Top Of Hydrasleeve
NO PURGE SAMPLE CHLORINE
(mg/l)Top Weight SAMPLE COLLECTED BY DATE
(NTU)(mV-NHE)(mg/L)
N/A N/A N/A 23.69 122 7.32 19.9
TIME
PSP 7/13/2016
LENGTH DEPTH (top)DEPLOYED COND.OXYGEN
(inches)(ft TOC)(deg C)(umho/cm)(SU)
HYDRASLEEVE DEPLOYED DATE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
DETECTED ODOR None CONVERSION FACTOR
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)N/A WATER COLUMN (ft)Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)WELL VOLUME
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE N/A
N/A SAMPLING EQUIPMENT PERISTALTIC PUMP PURGE METHOD
TUBING DIAMETER (in)3/8 OD No Purge
MONITORING WELL INFORMATION
WELL DIAMETER (in)TOC ELEV (ft msl)N/A MIDDLE OF WETTED SCREEN (ft toc)
SCREEN LENGTH (ft)ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)GS ELEV (ft msl)PUMP INTAKE DEPTH (ft TOC)N/A
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)13-Jul-2016 WELL/LOCATION NAME SW-1
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.4
GROUNDWATER MONITORING DATA SHEET
FOR NO PURGE SAMPLING
PERMIT #
MW-1 MW-1D MW-2 MW-2D MW-3 MW-3D MW-4 MW-4D MW-11 MW-11D MW-12 MW-12D SW-1 MW-4R MW-4PR
YES YES YES YES YES YES YES YES YES YES YES YES YES YES YES
YES YES YES YES YES YES YES YES YES YES YES YES YES YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
NORTH CAROLINA GROUNDWATER SAMPLING SITE CHECKLIST
LOCATION / SITE McGUIRE NUCLEAR STATION - LANDFILL #1 GROUNDWATER MONITORING 60-04 SAMPLE DATE July 13, 2016
SITE CONTACT John Williamson FIELD CREW LDC, PSP
WEATHER Clear, slight breeze, 75 to 85 deg F
WELL LOCK CONDITION
PAGE 1 OF 1
ACCESS TO WELLS
Access cleared into well
Access cleared around well
Tall grass or weeds - needs mowing
Road washing out / muddy / needs grading
Fallen tree blocking access
WELL SECURITY
Well found locked
Well found unlocked
Undermined / washing out
Lock in good condition
Lock rusted, difficult to open / needs replacing
Replaced damaged lock
WELL CASINGS
Casing in good condition
Damaged casing / still functional
Damaged casing / repair required
CONCRETE PADS
Pad in good condition
Minor cracks
Major cracks / broken / repair required
Replaced damaged well cap
Fire ants around concrete pad
WELL PROTECTIVE CASINGS
Casing in good condition
Damaged casing / still functional
Damaged casing / repair required
Broken hinge on protective lid
Wasp nest inside protective casing
Ants inside protective casing
WELL CAPS
Well cap in good conditon
Damaged / needs replacement
Lacks required information - Completion date
FLUSH MOUNT WELLS
Vault in good condition
Water inside vault
Vault bolt holes broken or stripped
Bolts stripped
Vault lid cracked or broken
WELL ID TAGS
Well tag in good condition
Well tag missing
Well tag damaged / illegible
Lacks required information - Driller Reg #
Lacks required information - Total well depth
Lacks required information - Depth to screen
Lacks required information - Non potable tag
NOTE:
WELL DEPTH TO WATER Purge AVG *WELL EVAC SPECIFIC
WELL DEPTH WATER ELEV.Method PMP RATE VOL VOL EVAC TEMP CONDUCTANCE pH TURBIDITY ORP DO
DATE NO.(feet-toc)(feet-toc)(feet)APPEARANCE ODOR (ml/min)(gal)(gal)(yes/no)(deg C)(umho/cm)(units)(NTU)(mV-NHE)(mg/l)
7/13/2016 MW-1 68.55 28.43 701.80 Normal None C N/A 6.54 20.25 NO 16.55 110 6.2 4.4 265 0.35
7/13/2016 MW-1D 88.22 29.31 701.30 Normal None C N/A 9.61 29.25 NO 16.36 99 6.2 3.4 267 0.12
7/13/2016 MW-2A 77.57 51.26 688.41 Normal None C N/A 4.29 13.50 NO 17.47 98 6.5 2.2 496 5.82
7/13/2016 MW-2D 108.82 53.31 687.46 Normal None C N/A 9.05 19.25 NO 17.05 60 6.9 3.0 489 9.54
7/13/2016 MW-3 73.64 56.85 671.58 Normal None C N/A 2.74 8.50 NO 15.74 78 6.4 1.8 419 5.87
7/13/2016 MW-3D 90.19 56.81 671.58 Normal None C N/A 5.44 16.50 NO 15.74 116 6.7 2.2 374 2.33
7/13/2016 MW-4 74.15 64.03 677.10 Normal None EOP N/A 1.65 0.55 N/A 16.21 134 5.7 1.1 314 0.44
7/13/2016 MW-4D 102.24 64.44 676.14 Normal None C N/A 6.17 25.00 NO 16.03 175 6.6 2.8 184 0.00
7/13/2016 MW-11 38.45 30.34 692.26 Normal None C N/A 1.32 4.50 NO 16.26 20 5.0 17.1 454 1.33
7/13/2016 MW-11D 101.55 31.20 691.94 Normal None C N/A 11.47 28.50 NO 15.27 29 5.7 3.8 549 6.81
7/13/2016 MW-12 29.49 25.21 699.60 Normal None EOP N/A 0.70 0.30 N/A 15.83 23 4.9 15.3 580 3.44
7/13/2016 MW-12D 68.42 26.10 698.67 Normal None C N/A 6.90 15.50 NO 15.09 80 6.3 4.9 538 7.74
7/13/2016 SW-1 N/A N/A N/A Normal None NP N/A N/A N/A N/A 23.69 122 7.3 19.9 186 7.19
7/13/2016 MW-4R 45.73 38.36 675.51 Normal None C N/A 1.20 4.00 NO 15.80 103 6.1 6.2 343 6.37
7/13/2016 MW-4DR 90.40 38.77 674.98 Normal None C N/A 8.42 25.50 NO 15.47 131 6.9 4.3 352 4.73
Purge Methods
LF = Low Flow
LF(M) = Low Flow (Mod.)
C = Connventional
NP = No Purge
EOP = Equip. Only Purge
LO = Level Only
* = Applicable to LF & LF(M) Purging Only
McGUIRE NUCLEAR STATION
LANDFILL 1 GROUNDWATER MONITORING
GROUNDWATER MONITORING FIELD DATA
PERMIT #60-04

B
Appendix B
Laboratory Report and
Chain-of-Custody Forms

13339 Hagers Ferry RoadHuntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J16070043
Project Name:MCGUIRE - GW LF1
Lab Contact: Anne Pridgeon
Date:8/2/2016
Customer Address:13225 Hagers Ferry Rd
Customer Name(s):TIM HUNSUCKER, CHUCK CAMPBELL
Mail Code: MG01CH
Huntersville, NC 28078-8985
Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Anne Pridgeon) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results) under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of specific methods.
Anne Pridgeon
Page 1 of 82
Reason: I have reviewed this
document.
Date: 2016.08.02 16:42:04
-04'00'
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection Date and Time Collected By Sample Description
2016019943 MCGUIRE 13-Jul-16 5:15 AM PSP TRIP BLANK
2016019944 MCGUIRE 13-Jul-16 12:15 PM LDC MW-1
2016019945 MCGUIRE 13-Jul-16 12:05 PM LDC MW-1D
2016019946 MCGUIRE 13-Jul-16 1:45 PM LDC MW-2A
2016019947 MCGUIRE 13-Jul-16 2:05 PM LDC MW-2D
2016019948 MCGUIRE 13-Jul-16 10:05 AM PSP MW-3
2016019949 MCGUIRE 13-Jul-16 10:30 AM PSP MW-3D
2016019950 MCGUIRE 13-Jul-16 7:10 AM PSP MW-4
2016019951 MCGUIRE 13-Jul-16 8:35 AM PSP MW-4D
2016019952 MCGUIRE 13-Jul-16 7:35 AM LDC MW-11
2016019953 MCGUIRE 13-Jul-16 8:15 AM LDC MW-11D
2016019954 MCGUIRE 13-Jul-16 9:10 AM LDC MW-12
2016019955 MCGUIRE 13-Jul-16 9:55 AM LDC MW-12D
2016019956 MCGUIRE 13-Jul-16 12:55 PM PSP SW-1
2016019957 MCGUIRE 13-Jul-16 11:25 AM PSP MW-4R
2016019958 MCGUIRE 13-Jul-16 12:20 PM PSP MW-4DR
2016019959 MCGUIRE 13-Jul-16 2:20 PM PSP FIELD BLANK
17 Total Samples
Page 2 of 82
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:8/2/2016
Electronic Data Deliverable (EDD) Sent Separatel
Page 3 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019943
Collection Date:13-Jul-16 5:15 AM
Site:TRIP BLANK
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 4 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019944
Collection Date:13-Jul-16 12:15 PM
Site:MW-1
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)53 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 2.1 mg/L EPA 9056A 07/16/2016 10:23 BGN90340.1 1
Sulfate 0.34 mg/L EPA 9056A 07/16/2016 10:23 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 13:29 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.218 mg/L SW 6010D 07/18/2016 16:37 JJMACKE0.005 1
Calcium (Ca)6.99 mg/L SW 6010D 07/18/2016 16:37 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 16:37 JJMACKE0.005 1
Magnesium (Mg)3.16 mg/L SW 6010D 07/18/2016 16:37 JJMACKE0.005 1
Potassium (K)1.11 mg/L SW 6010D 07/18/2016 16:37 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 16:37 JJMACKE0.005 1
Sodium (Na)6.26 mg/L SW 6010D 07/18/2016 16:37 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 14:25 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 14:25 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 14:25 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 14:25 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 5 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019945
Collection Date:13-Jul-16 12:05 PM
Site:MW-1D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)48 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 1.8 mg/L EPA 9056A 07/16/2016 11:15 BGN90340.1 1
Sulfate 0.35 mg/L EPA 9056A 07/16/2016 11:15 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 13:39 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.100 mg/L SW 6010D 07/18/2016 16:49 JJMACKE0.005 1
Calcium (Ca)7.14 mg/L SW 6010D 07/18/2016 16:49 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 16:49 JJMACKE0.005 1
Magnesium (Mg)2.43 mg/L SW 6010D 07/18/2016 16:49 JJMACKE0.005 1
Potassium (K)1.06 mg/L SW 6010D 07/18/2016 16:49 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 16:49 JJMACKE0.005 1
Sodium (Na)6.76 mg/L SW 6010D 07/18/2016 16:49 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 14:31 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 14:31 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 14:31 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 14:31 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 6 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019946
Collection Date:13-Jul-16 1:45 PM
Site:MW-2A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)44 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 1.5 mg/L EPA 9056A 07/16/2016 11:33 BGN90340.1 1
Sulfate 0.64 mg/L EPA 9056A 07/16/2016 11:33 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 13:36 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.030 mg/L SW 6010D 07/18/2016 16:53 JJMACKE0.005 1
Calcium (Ca)10.3 mg/L SW 6010D 07/18/2016 16:53 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 16:53 JJMACKE0.005 1
Magnesium (Mg)2.89 mg/L SW 6010D 07/18/2016 16:53 JJMACKE0.005 1
Potassium (K)0.418 mg/L SW 6010D 07/18/2016 16:53 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 16:53 JJMACKE0.005 1
Sodium (Na)6.76 mg/L SW 6010D 07/18/2016 16:53 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 15:10 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 15:10 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 15:10 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 15:10 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 7 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019947
Collection Date:13-Jul-16 2:05 PM
Site:MW-2D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)25 mg/L
(CaCO3)
SM 2320B 07/18/2016 11:45 GHUTCHI51
INORGANIC IONS BY IC
Chloride 1.3 mg/L EPA 9056A 07/16/2016 11:51 BGN90340.1 1
Sulfate 0.34 mg/L EPA 9056A 07/16/2016 11:51 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 13:41 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.014 mg/L SW 6010D 07/18/2016 16:56 JJMACKE0.005 1
Calcium (Ca)5.17 mg/L SW 6010D 07/18/2016 16:56 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 16:56 JJMACKE0.005 1
Magnesium (Mg)1.48 mg/L SW 6010D 07/18/2016 16:56 JJMACKE0.005 1
Potassium (K)0.334 mg/L SW 6010D 07/18/2016 16:56 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 16:56 JJMACKE0.005 1
Sodium (Na)5.33 mg/L SW 6010D 07/18/2016 16:56 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 15:17 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 15:17 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 15:17 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 15:17 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 8 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019948
Collection Date:13-Jul-16 10:05 AM
Site:MW-3
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)40 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 1.6 mg/L EPA 9056A 07/16/2016 12:09 BGN90340.1 1
Sulfate 0.53 mg/L EPA 9056A 07/16/2016 12:09 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 13:44 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.039 mg/L SW 6010D 07/18/2016 17:00 JJMACKE0.005 1
Calcium (Ca)7.64 mg/L SW 6010D 07/18/2016 17:00 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 17:00 JJMACKE0.005 1
Magnesium (Mg)3.15 mg/L SW 6010D 07/18/2016 17:00 JJMACKE0.005 1
Potassium (K)0.747 mg/L SW 6010D 07/18/2016 17:00 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 17:00 JJMACKE0.005 1
Sodium (Na)4.22 mg/L SW 6010D 07/18/2016 17:00 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 15:23 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 15:23 CWSPEN311
Lead (Pb)1.24 ug/L SW 6020B 07/15/2016 15:23 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 15:23 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 9 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019949
Collection Date:13-Jul-16 10:30 AM
Site:MW-3D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)57 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 1.7 mg/L EPA 9056A 07/16/2016 12:27 BGN90340.1 1
Sulfate 0.94 mg/L EPA 9056A 07/16/2016 12:27 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 13:46 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.027 mg/L SW 6010D 07/18/2016 17:04 JJMACKE0.005 1
Calcium (Ca)12.8 mg/L SW 6010D 07/18/2016 17:04 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 17:04 JJMACKE0.005 1
Magnesium (Mg)4.15 mg/L SW 6010D 07/18/2016 17:04 JJMACKE0.005 1
Potassium (K)0.861 mg/L SW 6010D 07/18/2016 17:04 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 17:04 JJMACKE0.005 1
Sodium (Na)6.16 mg/L SW 6010D 07/18/2016 17:04 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 15:30 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 15:30 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 15:30 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 15:30 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 10 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019950
Collection Date:13-Jul-16 7:10 AM
Site:MW-4
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)75 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 2.6 mg/L EPA 9056A 07/16/2016 12:45 BGN90340.1 1
Sulfate 0.98 mg/L EPA 9056A 07/16/2016 12:45 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 13:48 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.070 mg/L SW 6010D 07/18/2016 17:25 JJMACKE0.005 1
Calcium (Ca)11.9 mg/L SW 6010D 07/18/2016 17:25 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 17:25 JJMACKE0.005 1
Magnesium (Mg)11.7 mg/L SW 6010D 07/18/2016 17:25 JJMACKE0.005 1
Potassium (K)0.569 mg/L SW 6010D 07/18/2016 17:25 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 17:25 JJMACKE0.005 1
Sodium (Na)2.33 mg/L SW 6010D 07/18/2016 17:25 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 15:36 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 15:36 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 15:36 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 15:36 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 11 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019951
Collection Date:13-Jul-16 8:35 AM
Site:MW-4D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)92 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 2.0 mg/L EPA 9056A 07/16/2016 13:03 BGN90340.1 1
Sulfate 0.27 mg/L EPA 9056A 07/16/2016 13:03 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 13:51 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.050 mg/L SW 6010D 07/18/2016 17:35 JJMACKE0.005 1
Calcium (Ca)18.8 mg/L SW 6010D 07/18/2016 17:35 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 17:35 JJMACKE0.005 1
Magnesium (Mg)8.55 mg/L SW 6010D 07/18/2016 17:35 JJMACKE0.005 1
Potassium (K)0.609 mg/L SW 6010D 07/18/2016 17:35 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 17:35 JJMACKE0.005 1
Sodium (Na)4.41 mg/L SW 6010D 07/18/2016 17:35 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 15:43 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 15:43 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 15:43 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 15:43 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 12 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019952
Collection Date:13-Jul-16 7:35 AM
Site:MW-11
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)< 5 mg/L
(CaCO3)
SM 2320B 07/18/2016 11:45 GHUTCHI51
INORGANIC IONS BY IC
Chloride 2.0 mg/L EPA 9056A 07/16/2016 13:21 BGN90340.1 1
Sulfate 0.28 mg/L EPA 9056A 07/16/2016 13:21 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 13:53 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.010 mg/L SW 6010D 07/18/2016 17:38 JJMACKE0.005 1
Calcium (Ca)0.716 mg/L SW 6010D 07/18/2016 17:38 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 17:38 JJMACKE0.005 1
Magnesium (Mg)0.662 mg/L SW 6010D 07/18/2016 17:38 JJMACKE0.005 1
Potassium (K)0.136 mg/L SW 6010D 07/18/2016 17:38 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 17:38 JJMACKE0.005 1
Sodium (Na)1.47 mg/L SW 6010D 07/18/2016 17:38 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 15:49 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 15:49 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 15:49 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 15:49 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 13 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019953
Collection Date:13-Jul-16 8:15 AM
Site:MW-11D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)9.9 mg/L
(CaCO3)
SM 2320B 07/18/2016 11:45 GHUTCHI51
INORGANIC IONS BY IC
Chloride 1.4 mg/L EPA 9056A 07/16/2016 13:38 BGN90340.1 1
Sulfate 0.72 mg/L EPA 9056A 07/16/2016 13:38 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 13:56 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.012 mg/L SW 6010D 07/18/2016 17:42 JJMACKE0.005 1
Calcium (Ca)1.57 mg/L SW 6010D 07/18/2016 17:42 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 17:42 JJMACKE0.005 1
Magnesium (Mg)0.943 mg/L SW 6010D 07/18/2016 17:42 JJMACKE0.005 1
Potassium (K)0.169 mg/L SW 6010D 07/18/2016 17:42 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 17:42 JJMACKE0.005 1
Sodium (Na)3.42 mg/L SW 6010D 07/18/2016 17:42 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 15:56 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 15:56 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 15:56 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 15:56 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 14 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019954
Collection Date:13-Jul-16 9:10 AM
Site:MW-12
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)< 5 mg/L
(CaCO3)
SM 2320B 07/18/2016 11:45 GHUTCHI51
INORGANIC IONS BY IC
Chloride 4.5 mg/L EPA 9056A 07/16/2016 14:50 BGN90340.1 1
Sulfate 0.30 mg/L EPA 9056A 07/16/2016 14:50 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 14:18 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.016 mg/L SW 6010D 07/18/2016 17:46 JJMACKE0.005 1
Calcium (Ca)1.08 mg/L SW 6010D 07/18/2016 17:46 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 17:46 JJMACKE0.005 1
Magnesium (Mg)0.703 mg/L SW 6010D 07/18/2016 17:46 JJMACKE0.005 1
Potassium (K)0.430 mg/L SW 6010D 07/18/2016 17:46 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 17:46 JJMACKE0.005 1
Sodium (Na)1.89 mg/L SW 6010D 07/18/2016 17:46 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 16:02 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 16:02 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 16:02 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 16:02 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 15 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019955
Collection Date:13-Jul-16 9:55 AM
Site:MW-12D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)37 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 3.1 mg/L EPA 9056A 07/16/2016 15:44 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 9056A 07/16/2016 15:44 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 14:08 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.009 mg/L SW 6010D 07/18/2016 17:50 JJMACKE0.005 1
Calcium (Ca)7.81 mg/L SW 6010D 07/18/2016 17:50 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 17:50 JJMACKE0.005 1
Magnesium (Mg)1.20 mg/L SW 6010D 07/18/2016 17:50 JJMACKE0.005 1
Potassium (K)0.300 mg/L SW 6010D 07/18/2016 17:50 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 17:50 JJMACKE0.005 1
Sodium (Na)8.09 mg/L SW 6010D 07/18/2016 17:50 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 16:09 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 16:09 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 16:09 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 16:09 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 16 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019956
Collection Date:13-Jul-16 12:55 PM
Site:SW-1
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)58 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 2.3 mg/L EPA 9056A 07/16/2016 16:02 BGN90340.1 1
Sulfate 1.2 mg/L EPA 9056A 07/16/2016 16:02 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 14:20 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.034 mg/L SW 6010D 07/18/2016 17:54 JJMACKE0.005 1
Calcium (Ca)12.1 mg/L SW 6010D 07/18/2016 17:54 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 17:54 JJMACKE0.005 1
Magnesium (Mg)4.56 mg/L SW 6010D 07/18/2016 17:54 JJMACKE0.005 1
Potassium (K)1.19 mg/L SW 6010D 07/18/2016 17:54 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 17:54 JJMACKE0.005 1
Sodium (Na)5.69 mg/L SW 6010D 07/18/2016 17:54 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 16:35 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 16:35 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 16:35 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 16:35 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 17 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019957
Collection Date:13-Jul-16 11:25 AM
Site:MW-4R
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)53 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 3.5 mg/L EPA 9056A 07/16/2016 16:20 BGN90340.1 1
Sulfate 0.36 mg/L EPA 9056A 07/16/2016 16:20 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 14:15 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.012 mg/L SW 6010D 07/18/2016 17:57 JJMACKE0.005 1
Calcium (Ca)9.15 mg/L SW 6010D 07/18/2016 17:57 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 17:57 JJMACKE0.005 1
Magnesium (Mg)7.80 mg/L SW 6010D 07/18/2016 17:57 JJMACKE0.005 1
Potassium (K)0.280 mg/L SW 6010D 07/18/2016 17:57 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 17:57 JJMACKE0.005 1
Sodium (Na)2.42 mg/L SW 6010D 07/18/2016 17:57 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 16:41 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 16:41 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 16:41 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 16:41 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 18 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019958
Collection Date:13-Jul-16 12:20 PM
Site:MW-4DR
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)67 mg/L
(CaCO3)
SM 2320B 07/15/2016 09:41 CJELLIO201
INORGANIC IONS BY IC
Chloride 1.9 mg/L EPA 9056A 07/16/2016 16:38 BGN90340.1 1
Sulfate 1.2 mg/L EPA 9056A 07/16/2016 16:38 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 14:23 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.014 mg/L SW 6010D 07/18/2016 18:01 JJMACKE0.005 1
Calcium (Ca)14.9 mg/L SW 6010D 07/18/2016 18:01 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 18:01 JJMACKE0.005 1
Magnesium (Mg)4.54 mg/L SW 6010D 07/18/2016 18:01 JJMACKE0.005 1
Potassium (K)0.833 mg/L SW 6010D 07/18/2016 18:01 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 18:01 JJMACKE0.005 1
Sodium (Na)7.01 mg/L SW 6010D 07/18/2016 18:01 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 16:48 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 16:48 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 16:48 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 16:48 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 19 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
2016019959
Collection Date:13-Jul-16 2:20 PM
Site:FIELD BLANK
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)< 5 mg/L
(CaCO3)
SM 2320B 07/18/2016 11:45 GHUTCHI51
INORGANIC IONS BY IC
Chloride < 0.1 mg/L EPA 9056A 07/16/2016 16:55 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 9056A 07/16/2016 16:55 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470A 07/22/2016 14:25 DMFRANC0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)< 0.005 mg/L SW 6010D 07/18/2016 18:05 JJMACKE0.005 1
Calcium (Ca)< 0.01 mg/L SW 6010D 07/18/2016 18:05 JJMACKE0.01 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/18/2016 18:05 JJMACKE0.005 1
Magnesium (Mg)< 0.005 mg/L SW 6010D 07/18/2016 18:05 JJMACKE0.005 1
Potassium (K)< 0.1 mg/L SW 6010D 07/18/2016 18:05 JJMACKE0.1 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/18/2016 18:05 JJMACKE0.005 1
Sodium (Na)0.103 mg/L SW 6010D 07/18/2016 18:05 JJMACKE0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/15/2016 16:54 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/15/2016 16:54 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/15/2016 16:54 CWSPEN311
Selenium (Se)< 1 ug/L SW 6020B 07/15/2016 16:54 CWSPEN311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 20 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
Q16070363 ALK_FIX4.5 ALKALINITY (FIXED END POINT 4.5)
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Duplicate # 1
RPD
Parent Sample: J16070043 -- 2016019944
Alkalinity (mg/L CaCO3)0.907mg/L (CaCO3)-153.3
Final QualifierDilMeasuredUnits:Parameter
Duplicate # 2
RPD
Parent Sample: J16070373 -- 2016021665
Alkalinity (mg/L CaCO3)1.79mg/L (CaCO3)-123.8
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Alkalinity (mg/L CaCO3) 98.8 96.2mg/L (CaCO3)-12080195
Final QualifierDilMeasuredUnits:Parameter
LCS # 2
% Recovery LCL UCLSpike
Alkalinity (mg/L CaCO3) 98.8 97.1mg/L (CaCO3)-12080195.9
Page 21 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
Q16070424 ALK_LL_Fix LOW LEVEL ALKALINITY (FIXED END POINT)
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Duplicate # 1
RPD
Parent Sample: J16070043 -- 2016019947
Alkalinity (mg/L CaCO3) 25.2 2.18mg/L (CaCO3)-125.2
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Alkalinity (mg/L CaCO3) 9.08 9.88 91.9mg/L (CaCO3)-1208019.08
Page 22 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
Q16070380 Dionex INORGANIC IONS BY IC
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Chloride 0.0095 mg/L -10.0095 0.1 < 1/2 RDL
Sulfate 0.0373 mg/L -10.0373 0.1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
Spiked Sample # 1
Chloride 2.14 mg/L -12.14 0.1
Sulfate 0.341 mg/L -10.341 0.1
Final QualifierDilMeasuredUnits:Parameter
Spiked Sample # 2
Chloride 4.48 mg/L -14.48 0.1
Sulfate 0.297 mg/L -10.297 0.1
Final QualifierDilMeasuredUnits:Parameter
IS # 1
% Recovery LCL UCLSpike
Chloride 6.81 5 93.5mg/L -1208016.81
Sulfate 5.38 5 101mg/L -1208015.38
Final QualifierDilMeasuredUnits:Parameter
ISD # 1
RPD% Recovery LCL UCLSpike
Chloride 6.53 5 87.8 6.22mg/L -1208016.53
Sulfate 5.16 5 96.4 4.33mg/L -1208015.16
Final QualifierDilMeasuredUnits:Parameter
IS # 2
% Recovery LCL UCLSpike
Chloride 9.32 5 96.7mg/L -1208019.32
Sulfate 5.43 5 103mg/L -1208015.43
Final QualifierDilMeasuredUnits:Parameter
ISD # 2
RPD% Recovery LCL UCLSpike
Chloride 9.33 5 96.9 0.266mg/L -1208019.33
Sulfate 5.42 5 102 0.316mg/L -1208015.42
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Chloride 5.11 5 102mg/L -1208015.11
Sulfate 5.17 5 103mg/L -1208015.17
Page 23 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
Q16070588 HG 7470 MERCURY (COLD VAPOR) IN WATER
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Mercury (Hg) 0.023 ug/L -10.023 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
Blank # 2
RDL Relative Concentration
Mercury (Hg) 0.021 ug/L -10.021 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
Spiked Sample # 1
Mercury (Hg) 0.0325 ug/L -1003.25 0.05
Final QualifierDilMeasuredUnits:Parameter
IS # 1
% Recovery LCL UCLSpike
Mercury (Hg) 0.989 100 95.6ug/L -1257510098.9
Final QualifierDilMeasuredUnits:Parameter
ISD # 1
RPD% Recovery LCL UCLSpike
Mercury (Hg) 1.01 100 98 2.39ug/L -12575100101
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Mercury (Hg) 2.01 2 101ug/L -1158512.01
Final QualifierDilMeasuredUnits:Parameter
LCS # 2
% Recovery LCL UCLSpike
Mercury (Hg) 1.96 2 98.2ug/L -1158511.96
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16070043 -- 2016019944
Mercury (Hg) 1.01 1 98.8ug/L -1257511.01
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16070043 -- 2016019944
Mercury (Hg) 1.02 1 99.8 1.01ug/L -1257511.02
Final QualifierDilMeasuredUnits:Parameter
MS # 2
% Recovery LCL UCLSpike
Parent Sample: J16070043 -- 2016019955
Mercury (Hg) 1.01 1 97.9ug/L -1257511.01
Final QualifierDilMeasuredUnits:Parameter
MSD # 2
RPD% Recovery LCL UCLSpike
Parent Sample: J16070043 -- 2016019955
Mercury (Hg) 0.997 1 97 0.924ug/L -1257510.997
Page 24 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
Q16070347 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Barium (Ba) 0.000263 mg/L -10.000263 0.005 < 1/2 RDL
Calcium (Ca) 0.00184 mg/L -10.00184 0.01 < 1/2 RDL
Chromium (Cr) -0.000563 mg/L -1-0.000563 0.005 < 1/2 RDL
Magnesium (Mg) 0.000302 mg/L -10.000302 0.005 < 1/2 RDL
Potassium (K) 0.00382 mg/L -10.00382 0.1 < 1/2 RDL
Silver (Ag) -0.000141 mg/L -1-0.000141 0.005 < 1/2 RDL
Sodium (Na) -0.00758 mg/L -1-0.00758 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Barium (Ba) 5.11 5 102mg/L -1208015.11
Calcium (Ca) 4.92 5 98.5mg/L -1208014.92
Chromium (Cr) 4.95 5 98.9mg/L -1208014.95
Magnesium (Mg) 5.15 5 103mg/L -1208015.15
Potassium (K) 5.04 5 101mg/L -1208015.04
Silver (Ag) 0.525 0.5 105mg/L -1208010.525
Sodium (Na) 5.1 5 102mg/L -1208015.1
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16070043 -- 2016019944
Barium (Ba) 5.3 5 102mg/L -1257515.3
Calcium (Ca) 12.1 5 103mg/L -12575112.1
Chromium (Cr) 4.88 5 97.5mg/L -1257514.88
Magnesium (Mg) 8.29 5 103mg/L -1257518.29
Potassium (K) 6.09 5 99.6mg/L -1257516.09
Silver (Ag) 0.511 0.5 102mg/L -1257510.511
Sodium (Na) 11.4 5 102mg/L -12575111.4
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16070043 -- 2016019944
Barium (Ba) 5.29 5 101 0.237mg/L -1257515.29
Calcium (Ca) 12.2 5 103 0.485mg/L -12575112.2
Chromium (Cr) 4.87 5 97.3 0.246mg/L -1257514.87
Magnesium (Mg) 8.31 5 103 0.35mg/L -1257518.31
Potassium (K) 6.07 5 99.2 0.342mg/L -1257516.07
Silver (Ag) 0.51 0.5 102 0.191mg/L -1257510.51
Sodium (Na) 11.4 5 102 0.117mg/L -12575111.4
Page 25 of 82
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070043
Q16070311 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Arsenic (As) 0.0269 ug/L -10.0269 1 < 1/2 RDL
Cadmium (Cd) 0.002 ug/L -10.002 1 < 1/2 RDL
Lead (Pb) 0.0053 ug/L -10.0053 1 < 1/2 RDL
Selenium (Se) -0.109 ug/L -1-0.109 1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Arsenic (As) 53.6 50 107ug/L -12080153.6
Cadmium (Cd) 53.1 50 106ug/L -12080153.1
Lead (Pb) 52.9 50 106ug/L -12080152.9
Selenium (Se) 52 50 104ug/L -12080152
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16060167 -- 2016016246
Arsenic (As) 54.7 50 109ug/L -12575154.7
Cadmium (Cd) 51.7 50 103ug/L -12575151.7
Lead (Pb) 52.5 50 105ug/L -12575152.5
Selenium (Se) 51.9 50 104ug/L -12575151.9
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16060167 -- 2016016246
Arsenic (As) 53.9 50 107 1.37ug/L -12575153.9
Cadmium (Cd) 52.2 50 104 0.848ug/L -12575152.2
Lead (Pb) 53.1 50 106 1.17ug/L -12575153.1
Selenium (Se) 52.6 50 105 1.46ug/L -12575152.6
Page 26 of 82
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel:[phone]
TestAmerica Job ID: 490-107797-1
Client Project/Site: MNS Landfill #1 J16070043
For:
Duke Energy Corporation
13339 Hagers Ferry Road
Huntersville, North Carolina 28078
Attn: Lab Customer
Authorized for release by:
7/28/2016 10:03:26 AM
Shali Brown, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 27 of 82
Table of Contents
Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16070043
TestAmerica Job ID: 490-107797-1
Page 2 of 55 TestAmerica Nashville7/28/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .40
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 28 of 82











!
" #$%&$'
()*+,


 

 

-!.'&/ 0
 #,#+11 #1#+1
2 %0 0
 #,#+21 #1#+1
, %0 0
 #,#+21 #1#+1
 %02 0
 #,#+,1 #1#+1
1 %02 0
 #,#+1 #1#+1
+ %0, 0
 #,#+1 #1#+1
 %0, 0
 #,#+, #1#+1
3 %0 0
 #,#+ #1#+1
 %0 0
 #,#+3,1 #1#+1
 %0 0
 #,#+,1 #1#+1
 %0 0
 #,#+31 #1#+1
2 %02 0
 #,#+ #1#+1
, %02 0
 #,#+11 #1#+1
 $0 0
 #,#+211 #1#+1
1 %0- 0
 #,#+21 #1#+1
+ %0- 0
 #,#+22 #1#+1
 4'.'&/ 0
 #,#+2 #1#+1


&
56
Page 3 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 29 of 82









 
   
!
"#$%&$'()*+ ,



 




 !!"

 #$% #&
' #
()*#+, -./
!'$

-../()
)0(
(
1
)1(.).(

1


(

2(3((

4

1
1..(

01./(13.15(.2.1

1..
)
..(30(

)


..
01
(
(36
(
(0
.


("
(
2.(

4

(3

&.2.2().

(
(
)

(.
3

)
(
)1
(
.(

$7!.

8#8

(

(
(.
.(3
9


.2
21(.()
1..

8#8
0((
.2)
(1.



.
1(13
.

.

&'!
4

)


)
1..
(
4

(
23/
&'!
4


(.

3!


&'!0.



(
(0/)
01.
.1


2).

3




)
()


(2(

())



(

3
.(1
(



2()
..(
)
(.0
.
1((.
(2(
13
(




(:
2(:
.
1((.
);(2
.
.(.(
3
.



)(((()
.
)
(3
!
(
.1

2( #<#=+>.

2(((0



2((3.


).


1=3
3
"0 0!1

0*(0231
*4
$?!@'&AB  C0%-B  =C0%- B  ,C0%-=B  C0%-= B  <C0
%-,B  +C0%-, B   C0%-B  DC0%- B  C0%-B  C0%- 
B  C0%-=B  =C0%-= B  ,C0$-B  C0%-?B  <C0%- ?
B  +C(6' @'&AB   C1
5()
2

(BE
%$C
(1.!
$-D+%.(D=+@3.1
5( ##=+3
&
4

1
(0.
..(
(2
. )#E
3

&.2Page 4 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 30 of 82












!
" #$%&$'
()*+,



 




 -.
.-'
.

/

.%'
(.
 




0
1
2










3 '((.44

(
.
.
(

(5.



6- ! -
1
7' 

7'/(
&7 


7'/(
-  



8

9(

()) :
7

7


';-;-;& (


;-

;-0

;

((



#




).
 
'  
1
 


% %( 

1
' 
( 
'
% %( 

 


%' %.
( 
'
%' %'18
0:
& &

 
(
& &
( (
.
8
%'
').
5:
!<' !

<


'
< <



-- -
1



-' -
'
-/('8-
(
.:
-! -
1! )) ;


).
1()) 55



7

0 /1
7

8
0:

<

0 /1
<
8
0:


&
.1
Page 5 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 31 of 82












!
" #$%&$'
()*+,
 



!"# ! 
$%&'(')**
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+,, 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+,,  
 &
/ /- #' ##+,, 01 &
/ /. #' ##+,, 0

2

2
 &
/ / #' ##+,, 0

( 2

2
 &
/ /- #' ##+,, 0

)
 &
/ /,. #' ##+,, 0

2
 &
./ -/+ #' ##+,, -0

3%45 &
/ /-- #' ##+,, 

()( &
/ /6 #' ##+,, 


2
( &
/ /6 #' ##+,, 2

1 &
/ /-. #' ##+,, 2

(

2
 &
/ /,+ #' ##+,, 2

2
 &
/ /-, #' ##+,, 2

)
 &
/ /,+ #' ##+,, 2

2
 &
/ /- #' ##+,,  7- 2

2 &
/ / #' ##+,,  7, 2


 &
/ / #' ##+,, 7-

,2



 &
/ /- #' ##+,, 7-

2
305 &
/ /. #' ##+,, 

2
 &
/ / #' ##+,, 7- 2

1 &
/ / #' ##+,, 7 2

1 &
/ /- #' ##+,, 7 2

2
 &
/ /- #' ##+,, 7- 2

2
 &
/ /-. #' ##+,, 7 2

2 &
/ /-. #' ##+,, 7- 2



 &
/ / #' ##+,, 21 &
/ /-6 #' ##+,, -89

 &
/ /. #' ##+,, 
(
2
 &
/ / #' ##+,, %22
( &
/ /6 #' ##+,, %2- 

3%045 &
/ /-6 #' ##+,, $ &
/ /. #' ##+,, 777-

2

2
 &
/ / #' ##+,, 77-7-

2

2
 &
/ / #' ##+,, 

2

2 &
/ / #' ##+,, 

 &
./ /+ #' ##+,, 
7 2

- &
/ /-, #' ##+,, 
7- 2

2 &
/ / #' ##+,, 
7, 2


 &
/ / #' ##+,, 77
 2

2
 &
/ / #' ##+,, 77-
 2

2
 &
/ /- #' ##+,, 
 2

2 &
/ /- #' ##+,, 
 2

)

2
 &
/ /-, #' ##+,, 7-7,
 2



 &
/ / #' ##+,, :

 &
/ /6 #' ##+,, : 2
( &
,/ /.6 #' ##+,, ;7


 &


&
2<
Page 6 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 32 of 82












!
" #$%&$'
()*+,
 



!"# ! 
$%&'(')**
 %+&'*')*

 

    
 





 



   

 
 !"
  #
 
$ "#  
 


&
2<
Page 7 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 33 of 82












!
" #$%&$'
()*+,
 
.

 #
!"# ! 
$%&'(').*
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##++ 
 56 % 57&! !&8 
 9 :!
/ /. #' ##++  
 &
/ /- #' ##++ 01 &
/ /. #' ##++ 0

2

2
 &
/ / #' ##++ 0

( 2

2
 &
/ /- #' ##++ 0

)
 &
/ /,. #' ##++ 0

2
 &
./ -/+ #' ##++ -0

3%45 &
/ /-- #' ##++ 

()( &
/ /6 #' ##++ 


2
( &
/ /6 #' ##++ 2

1 &
/ /-. #' ##++ 2

(

2
 &
/ /,+ #' ##++ 2

2
 &
/ /-, #' ##++ 2

)
 &
/ /,+ #' ##++ 2

2
 &
/ /- #' ##++  7- 2

2 &
/ / #' ##++  7, 2


 &
/ / #' ##++ 7-

,2



 &
/ /- #' ##++ 7-

2
305 &
/ /. #' ##++ 

2
 &
/ / #' ##++ 7- 2

1 &
/ / #' ##++ 7 2

1 &
/ /- #' ##++ 7 2

2
 &
/ /- #' ##++ 7- 2

2
 &
/ /-. #' ##++ 7 2

2 &
/ /-. #' ##++ 7- 2



 &
/ / #' ##++ 21 &
/ /-6 #' ##++ -89

 &
/ /. #' ##++ 
(
2
 &
/ / #' ##++ %22
( &
/ /6 #' ##++ %2- 

3%045 &
/ /-6 #' ##++ $ &
/ /. #' ##++ 777-

2

2
 &
/ / #' ##++ 77-7-

2

2
 &
/ / #' ##++ 

2

2 &
/ / #' ##++ 

 &
./ /+ #' ##++ 
7 2

- &
/ /-, #' ##++ 
7- 2

2 &
/ / #' ##++ 
7, 2


 &
/ / #' ##++ 77
 2

2
 &
/ / #' ##++ 77-
 2

2
 &
/ /- #' ##++ 
 2

2 &
/ /- #' ##++ 
 2

)

2
 &
/ /-, #' ##++ 7-7,
 2



 &
/ / #' ##++ :

 &
/ /6 #' ##++ : 2
( &
,/ /.6 #' ##++ ;7


 &


&
2<
Page 8 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 34 of 82












!
" #$%&$'
()*+,
 
.

 #
!"# ! 
$%&'(').*
 %+&'*')*

 

     





 



   % 
 !"
  % 
$ "#   


&
2<
Page 9 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 35 of 82












!
" #$%&$'
()*+,
 
(

 #
!"# ! 
$%&'(').*
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##++,. 
 56 % 57&! !&8 
 9 :!
/ /. #' ##++,.  
 &
/ /- #' ##++,. 01 &
/ /. #' ##++,. 0

2

2
 &
/ / #' ##++,. 0

( 2

2
 &
/ /- #' ##++,. 0

)
 &
/ /,. #' ##++,. 0

2
 &
./ -/+ #' ##++,. -0

3%45 &
/ /-- #' ##++,. 

()( &
/ /6 #' ##++,. 


2
( &
/ /6 #' ##++,. 2

1 &
/ /-. #' ##++,. 2

(

2
 &
/ /,+ #' ##++,. 2

2
 &
/ /-, #' ##++,. 2

)
 &
/ /,+ #' ##++,. 2

2
 &
/ /- #' ##++,.  7- 2

2 &
/ / #' ##++,.  7, 2


 &
/ / #' ##++,. 7-

,2



 &
/ /- #' ##++,. 7-

2
305 &
/ /. #' ##++,. 

2
 &
/ / #' ##++,. 7- 2

1 &
/ / #' ##++,. 7 2

1 &
/ /- #' ##++,. 7 2

2
 &
/ /- #' ##++,. 7- 2

2
 &
/ /-. #' ##++,. 7 2

2 &
/ /-. #' ##++,. 7- 2



 &
/ / #' ##++,. 21 &
/ /-6 #' ##++,. -89

 &
/ /. #' ##++,. 
(
2
 &
/ / #' ##++,. %22
( &
/ /6 #' ##++,. %2- 

3%045 &
/ /-6 #' ##++,. $ &
/ /. #' ##++,. 777-

2

2
 &
/ / #' ##++,. 77-7-

2

2
 &
/ / #' ##++,. 

2

2 &
/ / #' ##++,. 

 &
./ /+ #' ##++,. 
7 2

- &
/ /-, #' ##++,. 
7- 2

2 &
/ / #' ##++,. 
7, 2


 &
/ / #' ##++,. 77
 2

2
 &
/ / #' ##++,. 77-
 2

2
 &
/ /- #' ##++,. 
 2

2 &
/ /- #' ##++,. 
 2

)

2
 &
/ /-, #' ##++,. 7-7,
 2



 &
/ / #' ##++,. :

 &
/ /6 #' ##++,. : 2
( &
,/ /.6 #' ##++,. ;7


 &


&
2<
Page 10 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 36 of 82












!
" #$%&$'
()*+,
 
(

 #
!"# ! 
$%&'(').*
 %+&'*')*

 

    % 





 



   %% 
 !"
  % 
$ "#  % 


&
2<
Page 11 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 37 of 82












!
" #$%&$'
()*+,
 


 #.
!"# ! 
$%&'(')(*
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+- 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+-  
 &
/ /- #' ##+- 01 &
/ /. #' ##+- 0

2

2
 &
/ / #' ##+- 0

( 2

2
 &
/ /- #' ##+- 0

)
 &
/ /,. #' ##+- 0

2
 &
./ -/+ #' ##+- -0

3%45 &
/ /-- #' ##+- 

()( &
/ /6 #' ##+- 


2
( &
/ /6 #' ##+- 2

1 &
/ /-. #' ##+- 2

(

2
 &
/ /,+ #' ##+- 2

2
 &
/ /-, #' ##+- 2

)
 &
/ /,+ #' ##+- 2

2
 &
/ /- #' ##+-  7- 2

2 &
/ / #' ##+-  7, 2


 &
/ / #' ##+- 7-

,2



 &
/ /- #' ##+- 7-

2
305 &
/ /. #' ##+- 

2
 &
/ / #' ##+- 7- 2

1 &
/ / #' ##+- 7 2

1 &
/ /- #' ##+- 7 2

2
 &
/ /- #' ##+- 7- 2

2
 &
/ /-. #' ##+- 7 2

2 &
/ /-. #' ##+- 7- 2



 &
/ / #' ##+- 21 &
/ /-6 #' ##+- -89

 &
/ /. #' ##+- 
(
2
 &
/ / #' ##+- %22
( &
/ /6 #' ##+- %2- 

3%045 &
/ /-6 #' ##+- $ &
/ /. #' ##+- 777-

2

2
 &
/ / #' ##+- 77-7-

2

2
 &
/ / #' ##+- 

2

2 &
/ / #' ##+- 

 &
./ /+ #' ##+- 
7 2

- &
/ /-, #' ##+- 
7- 2

2 &
/ / #' ##+- 
7, 2


 &
/ / #' ##+- 77
 2

2
 &
/ / #' ##+- 77-
 2

2
 &
/ /- #' ##+- 
 2

2 &
/ /- #' ##+- 
 2

)

2
 &
/ /-, #' ##+- 7-7,
 2



 &
/ / #' ##+- :

 &
/ /6 #' ##+- : 2
( &
,/ /.6 #' ##+- ;7


 &


&
2<
Page 12 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 38 of 82












!
" #$%&$'
()*+,
 


 #.
!"# ! 
$%&'(')(*
 %+&'*')*

 

     





 



   % 
 !"
  % 
$ "#   


&
2<
Page 13 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 39 of 82












!
" #$%&$'
()*+,
 
*

 #.
!"# ! 
$%&'(')*
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+-6 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+-6  
 &
/ /- #' ##+-6 01 &
/ /. #' ##+-6 0

2

2
 &
/ / #' ##+-6 0

( 2

2
 &
/ /- #' ##+-6 0

)
 &
/ /,. #' ##+-6 0

2
 &
./ -/+ #' ##+-6 -0

3%45 &
/ /-- #' ##+-6 

()( &
/ /6 #' ##+-6 


2
( &
/ /6 #' ##+-6 2

1 &
/ /-. #' ##+-6 2

(

2
 &
/ /,+ #' ##+-6 2

2
 &
/ /-, #' ##+-6 2

)
 &
/ /,+ #' ##+-6 2

2
 &
/ /- #' ##+-6  7- 2

2 &
/ / #' ##+-6  7, 2


 &
/ / #' ##+-6 7-

,2



 &
/ /- #' ##+-6 7-

2
305 &
/ /. #' ##+-6 

2
 &
/ / #' ##+-6 7- 2

1 &
/ / #' ##+-6 7 2

1 &
/ /- #' ##+-6 7 2

2
 &
/ /- #' ##+-6 7- 2

2
 &
/ /-. #' ##+-6 7 2

2 &
/ /-. #' ##+-6 7- 2



 &
/ / #' ##+-6 21 &
/ /-6 #' ##+-6 -89

 &
/ /. #' ##+-6 
(
2
 &
/ / #' ##+-6 %22
( &
/ /6 #' ##+-6 %2- 

3%045 &
/ /-6 #' ##+-6 $ &
/ /. #' ##+-6 777-

2

2
 &
/ / #' ##+-6 77-7-

2

2
 &
/ / #' ##+-6 

2

2 &
/ / #' ##+-6 

 &
./ /+ #' ##+-6 
7 2

- &
/ /-, #' ##+-6 
7- 2

2 &
/ / #' ##+-6 
7, 2


 &
/ / #' ##+-6 77
 2

2
 &
/ / #' ##+-6 77-
 2

2
 &
/ /- #' ##+-6 
 2

2 &
/ /- #' ##+-6 
 2

)

2
 &
/ /-, #' ##+-6 7-7,
 2



 &
/ / #' ##+-6 :

 &
/ /6 #' ##+-6 : 2
( &
,/ /.6 #' ##+-6 ;7


 &


&
2<
Page 14 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 40 of 82












!
" #$%&$'
()*+,
 
*

 #.
!"# ! 
$%&'(')*
 %+&'*')*

 

     # 





 



    # 
 !"
   # 
$ "#   # 


&
2<
Page 15 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 41 of 82












!
" #$%&$'
()*+,
 
)

 #(
!"# ! 
$%&'(')*
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+.. 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+..  
 &
/ /- #' ##+.. 01 &
/ /. #' ##+.. 0

2

2
 &
/ / #' ##+.. 0

( 2

2
 &
/ /- #' ##+.. 0

)
 &
/ /,. #' ##+.. 0

2
 &
./ -/+ #' ##+.. -0

3%45 &
/ /-- #' ##+.. 

()( &
/ /6 #' ##+.. 


2
( &
/ /6 #' ##+.. 2

1 &
/ /-. #' ##+.. 2

(

2
 &
/ /,+ #' ##+.. 2

2
 &
/ /-, #' ##+.. 2

)
 &
/ /,+ #' ##+.. 2

2
 &
/ /- #' ##+..  7- 2

2 &
/ / #' ##+..  7, 2


 &
/ / #' ##+.. 7-

,2



 &
/ /- #' ##+.. 7-

2
305 &
/ /. #' ##+.. 

2
 &
/ / #' ##+.. 7- 2

1 &
/ / #' ##+.. 7 2

1 &
/ /- #' ##+.. 7 2

2
 &
/ /- #' ##+.. 7- 2

2
 &
/ /-. #' ##+.. 7 2

2 &
/ /-. #' ##+.. 7- 2



 &
/ / #' ##+.. 21 &
/ /-6 #' ##+.. -89

 &
/ /. #' ##+.. 
(
2
 &
/ / #' ##+.. %22
( &
/ /6 #' ##+.. %2- 

3%045 &
/ /-6 #' ##+.. $ &
/ /. #' ##+.. 777-

2

2
 &
/ / #' ##+.. 77-7-

2

2
 &
/ / #' ##+.. 

2

2 &
/ / #' ##+.. 

 &
./ /+ #' ##+.. 
7 2

- &
/ /-, #' ##+.. 
7- 2

2 &
/ / #' ##+.. 
7, 2


 &
/ / #' ##+.. 77
 2

2
 &
/ / #' ##+.. 77-
 2

2
 &
/ /- #' ##+.. 
 2

2 &
/ /- #' ##+.. 
 2

)

2
 &
/ /-, #' ##+.. 7-7,
 2



 &
/ / #' ##+.. :

 &
/ /6 #' ##+.. : 2
( &
,/ /.6 #' ##+.. ;7


 &


&
2<
Page 16 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 42 of 82












!
" #$%&$'
()*+,
 
)

 #(
!"# ! 
$%&'(')*
 %+&'*')*

 

    %% 





 



   %% 
 !"
  %%% 
$ "#  %% 


&
2<
Page 17 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 43 of 82












!
" #$%&$'
()*+,
 


 #(
!"# ! 
$%&'(')(
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+6- 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+6-  
 &
/ /- #' ##+6- 01 &
/ /. #' ##+6- 0

2

2
 &
/ / #' ##+6- 0

( 2

2
 &
/ /- #' ##+6- 0

)
 &
/ /,. #' ##+6- 0

2
 &
./ -/+ #' ##+6- -0

3%45 &
/ /-- #' ##+6- 

()( &
/ /6 #' ##+6- 


2
( &
/ /6 #' ##+6- 2

1 &
/ /-. #' ##+6- 2

(

2
 &
/ /,+ #' ##+6- 2

2
 &
/ /-, #' ##+6- 2

)
 &
/ /,+ #' ##+6- 2

2
 &
/ /- #' ##+6- %
;.%,$!$, <* =
/ / #' ##+6-  7, 2


 &
/ / #' ##+6- 7-

,2



 &
/ /- #' ##+6- 7-

2
305 &
/ /. #' ##+6- 

2
 &
/ / #' ##+6- 7- 2

1 &
/ / #' ##+6- 7 2

1 &
/ /- #' ##+6- 7 2

2
 &
/ /- #' ##+6- 7- 2

2
 &
/ /-. #' ##+6- 7 2

2 &
/ /-. #' ##+6- 7- 2



 &
/ / #' ##+6- 21 &
/ /-6 #' ##+6- -89

 &
/ /. #' ##+6- 
(
2
 &
/ / #' ##+6- %22
( &
/ /6 #' ##+6- %2- 

3%045 &
/ /-6 #' ##+6- $ &
/ /. #' ##+6- 777-

2

2
 &
/ / #' ##+6- 77-7-

2

2
 &
/ / #' ##+6- ! %,$!$, <() =
/ / #' ##+6- 

 &
./ /+ #' ##+6- 
7 2

- &
/ /-, #' ##+6- 
7- 2

2 &
/ / #' ##+6- 
7, 2


 &
/ / #' ##+6- 77
 2

2
 &
/ / #' ##+6- 77-
 2

2
 &
/ /- #' ##+6- !%,$!$, <). =
/ /- #' ##+6- !%,$!$:$!$
,  <( =
/ /-, #' ##+6- 7-7,
 2



 &
/ / #' ##+6- :

 &
/ /6 #' ##+6- : 2
( &
,/ /.6 #' ##+6- >5
;$  *<


&
2<
Page 18 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 44 of 82












!
" #$%&$'
()*+,
 


 #(
!"# ! 
$%&'(')(
 %+&'*')*

 

  
 #  





 



   %#  
 !"
   #  
$ "#  #  


&
2<
Page 19 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 45 of 82












!
" #$%&$'
()*+,
 
-

 #
!"# ! 
$%&'(')
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+6 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+6  
 &
/ /- #' ##+6 01 &
/ /. #' ##+6 0

2

2
 &
/ / #' ##+6 0

( 2

2
 &
/ /- #' ##+6 0

)
 &
/ /,. #' ##+6 0

2
 &
./ -/+ #' ##+6 -0

3%45 &
/ /-- #' ##+6 

()( &
/ /6 #' ##+6 


2
( &
/ /6 #' ##+6 2

1 &
/ /-. #' ##+6 2

(

2
 &
/ /,+ #' ##+6 2

2
 &
/ /-, #' ##+6 2

)
 &
/ /,+ #' ##+6 2

2
 &
/ /- #' ##+6 %
;.%,$!$, <.-
/ / #' ##+6  7, 2


 &
/ / #' ##+6 7-

,2



 &
/ /- #' ##+6 7-

2
305 &
/ /. #' ##+6 

2
 &
/ / #' ##+6 7- 2

1 &
/ / #' ##+6 7 2

1 &
/ /- #' ##+6 7 2

2
 &
/ /- #' ##+6 7- 2

2
 &
/ /-. #' ##+6 7 2

2 &
/ /-. #' ##+6 7- 2



 &
/ / #' ##+6 21 &
/ /-6 #' ##+6 -89

 &
/ /. #' ##+6 
(
2
 &
/ / #' ##+6 %22
( &
/ /6 #' ##+6 %2- 

3%045 &
/ /-6 #' ##+6 $ &
/ /. #' ##+6 777-

2

2
 &
/ / #' ##+6 77-7-

2

2
 &
/ / #' ##+6 ! %,$!$, .<.
/ / #' ##+6 

 &
./ /+ #' ##+6 
7 2

- &
/ /-, #' ##+6 
7- 2

2 &
/ / #' ##+6 
7, 2


 &
/ / #' ##+6 77
 2

2
 &
/ / #' ##+6 77-
 2

2
 &
/ /- #' ##+6 !%,$!$, <).. =
/ /- #' ##+6 
 2

)

2
 &
/ /-, #' ##+6 7-7,
 2



 &
/ / #' ##+6 :

 &
/ /6 #' ##+6 : 2
( &
,/ /.6 #' ##+6 ;7


 &


&
2<
Page 20 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 46 of 82












!
" #$%&$'
()*+,
 
-

 #
!"# ! 
$%&'(')
 %+&'*')*

 

    #
 





 



   #
 
 !"
  %#
 
$ "#   #
 


&
2<
Page 21 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 47 of 82












!
" #$%&$'
()*+,
 


 #
!"# ! 
$%&'(')-(*
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+, 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+,  
 &
/ /- #' ##+, 7 <*( =
/ /. #' ##+, 0

2

2
 &
/ / #' ##+, 0

( 2

2
 &
/ /- #' ##+, 0

)
 &
/ /,. #' ##+, 0

2
 &
./ -/+ #' ##+, -0

3%45 &
/ /-- #' ##+, 

()( &
/ /6 #' ##+, 


2
( &
/ /6 #' ##+, 2

1 &
/ /-. #' ##+, 2

(

2
 &
/ /,+ #' ##+, 2

2
 &
/ /-, #' ##+, 2

)
 &
/ /,+ #' ##+, 2

2
 &
/ /- #' ##+, %
;.%,$!$, <
/ / #' ##+,  7, 2


 &
/ / #' ##+, 7-

,2



 &
/ /- #' ##+, 7-

2
305 &
/ /. #' ##+, 

2
 &
/ / #' ##+, 7- 2

1 &
/ / #' ##+, 7 2

1 &
/ /- #' ##+, ;%,$!$,  <(( =
/ /- #' ##+, 7- 2

2
 &
/ /-. #' ##+, 7 2

2 &
/ /-. #' ##+, 7- 2



 &
/ / #' ##+, 21 &
/ /-6 #' ##+, -89

 &
/ /. #' ##+, 
(
2
 &
/ / #' ##+,  ,5
,$!& )<-(
/ /6 #' ##+, %2- 

3%045 &
/ /-6 #' ##+, $ &
/ /. #' ##+, 777-

2

2
 &
/ / #' ##+, 77-7-

2

2
 &
/ / #' ##+, ! %,$!$, <-
/ / #' ##+, $ <.-. =
./ /+ #' ##+, 
7 2

- &
/ /-, #' ##+, 
7- 2

2 &
/ / #' ##+, 
7, 2


 &
/ / #' ##+, 77
 2

2
 &
/ / #' ##+, 77-
 2

2
 &
/ /- #' ##+, !%,$!$, <
/ /- #' ##+, 
 2

)

2
 &
/ /-, #' ##+, 7-7,
 2



 &
/ / #' ##+, :

 &
/ /6 #' ##+, /5%,$!& <*( =
,/ /.6 #' ##+, >5
;$  *<


&
2<
Page 22 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 48 of 82












!
" #$%&$'
()*+,
 


 #
!"# ! 
$%&'(')-(*
 %+&'*')*

 

     





 



    
 !"
   
$ "#    


&
2<
Page 23 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 49 of 82












!
" #$%&$'
()*+,
 


 #
!"# ! 
$%&'(')(*
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+ 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+  
 &
/ /- #' ##+ 01 &
/ /. #' ##+ 0

2

2
 &
/ / #' ##+ 0

( 2

2
 &
/ /- #' ##+ 0

)
 &
/ /,. #' ##+ 0

2
 &
./ -/+ #' ##+ -0

3%45 &
/ /-- #' ##+ 

()( &
/ /6 #' ##+ 


2
( &
/ /6 #' ##+ 2

1 &
/ /-. #' ##+ 2

(

2
 &
/ /,+ #' ##+ 2

2
 &
/ /-, #' ##+ 2

)
 &
/ /,+ #' ##+ 2

2
 &
/ /- #' ##+  7- 2

2 &
/ / #' ##+  7, 2


 &
/ / #' ##+ 7-

,2



 &
/ /- #' ##+ 7-

2
305 &
/ /. #' ##+ 

2
 &
/ / #' ##+ 7- 2

1 &
/ / #' ##+ 7 2

1 &
/ /- #' ##+ 7 2

2
 &
/ /- #' ##+ 7- 2

2
 &
/ /-. #' ##+ 7 2

2 &
/ /-. #' ##+ 7- 2



 &
/ / #' ##+ 21 &
/ /-6 #' ##+ -89

 &
/ /. #' ##+ 
(
2
 &
/ / #' ##+ %22
( &
/ /6 #' ##+ %2- 

3%045 &
/ /-6 #' ##+ $ &
/ /. #' ##+ 777-

2

2
 &
/ / #' ##+ 77-7-

2

2
 &
/ / #' ##+ 

2

2 &
/ / #' ##+ 

 &
./ /+ #' ##+ 
7 2

- &
/ /-, #' ##+ 
7- 2

2 &
/ / #' ##+ 
7, 2


 &
/ / #' ##+ 77
 2

2
 &
/ / #' ##+ 77-
 2

2
 &
/ /- #' ##+ 
 2

2 &
/ /- #' ##+ 
 2

)

2
 &
/ /-, #' ##+ 7-7,
 2



 &
/ / #' ##+ :

 &
/ /6 #' ##+ : 2
( &
,/ /.6 #' ##+ ;7


 &


&
2<
Page 24 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 50 of 82












!
" #$%&$'
()*+,
 


 #
!"# ! 
$%&'(')(*
 %+&'*')*

 

    
 





 



   
 
 !"
  %
 
$ "#  
 


&
2<
Page 25 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 51 of 82












!
" #$%&$'
()*+,
 


 #
!"# ! 
$%&'(')-*
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+-+ 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+-+  
 &
/ /- #' ##+-+ 01 &
/ /. #' ##+-+ 0

2

2
 &
/ / #' ##+-+ 0

( 2

2
 &
/ /- #' ##+-+ 0

)
 &
/ /,. #' ##+-+ 0

2
 &
./ -/+ #' ##+-+ -0

3%45 &
/ /-- #' ##+-+ 

()( &
/ /6 #' ##+-+ 


2
( &
/ /6 #' ##+-+ 2

1 &
/ /-. #' ##+-+ 2

(

2
 &
/ /,+ #' ##+-+ 2

2
 &
/ /-, #' ##+-+ 2

)
 &
/ /,+ #' ##+-+ 2

2
 &
/ /- #' ##+-+  7- 2

2 &
/ / #' ##+-+  7, 2


 &
/ / #' ##+-+ 7-

,2



 &
/ /- #' ##+-+ 7-

2
305 &
/ /. #' ##+-+ 

2
 &
/ / #' ##+-+ 7- 2

1 &
/ / #' ##+-+ 7 2

1 &
/ /- #' ##+-+ 7 2

2
 &
/ /- #' ##+-+ 7- 2

2
 &
/ /-. #' ##+-+ 7 2

2 &
/ /-. #' ##+-+ 7- 2



 &
/ / #' ##+-+ 21 &
/ /-6 #' ##+-+ -89

 &
/ /. #' ##+-+ 
(
2
 &
/ / #' ##+-+ %22
( &
/ /6 #' ##+-+ %2- 

3%045 &
/ /-6 #' ##+-+ $ &
/ /. #' ##+-+ 777-

2

2
 &
/ / #' ##+-+ 77-7-

2

2
 &
/ / #' ##+-+ 

2

2 &
/ / #' ##+-+ 

 &
./ /+ #' ##+-+ 
7 2

- &
/ /-, #' ##+-+ 
7- 2

2 &
/ / #' ##+-+ 
7, 2


 &
/ / #' ##+-+ 77
 2

2
 &
/ / #' ##+-+ 77-
 2

2
 &
/ /- #' ##+-+ 
 2

2 &
/ /- #' ##+-+ 
 2

)

2
 &
/ /-, #' ##+-+ 7-7,
 2



 &
/ / #' ##+-+ :

 &
/ /6 #' ##+-+ : 2
( &
,/ /.6 #' ##+-+ ;7


 &


&
2<
Page 26 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 52 of 82












!
" #$%&$'
()*+,
 


 #
!"# ! 
$%&'(')-*
 %+&'*')*

 

      





 



   %  
 !"
    
$ "#     


&
2<
Page 27 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 53 of 82












!
" #$%&$'
()*+,
 
.

 #.
!"# ! 
$%&'(')
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+-,- 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+-,-  
 &
/ /- #' ##+-,- 01 &
/ /. #' ##+-,- 0

2

2
 &
/ / #' ##+-,- 0

( 2

2
 &
/ /- #' ##+-,- 0

)
 &
/ /,. #' ##+-,- 0

2
 &
./ -/+ #' ##+-,- -0

3%45 &
/ /-- #' ##+-,- 

()( &
/ /6 #' ##+-,- 


2
( &
/ /6 #' ##+-,- 2

1 &
/ /-. #' ##+-,- 2

(

2
 &
/ /,+ #' ##+-,- 2

2
 &
/ /-, #' ##+-,- 2

)
 &
/ /,+ #' ##+-,- 2

2
 &
/ /- #' ##+-,-  7- 2

2 &
/ / #' ##+-,-  7, 2


 &
/ / #' ##+-,- 7-

,2



 &
/ /- #' ##+-,- 7-

2
305 &
/ /. #' ##+-,- 

2
 &
/ / #' ##+-,- 7- 2

1 &
/ / #' ##+-,- 7 2

1 &
/ /- #' ##+-,- 7 2

2
 &
/ /- #' ##+-,- 7- 2

2
 &
/ /-. #' ##+-,- 7 2

2 &
/ /-. #' ##+-,- 7- 2



 &
/ / #' ##+-,- 21 &
/ /-6 #' ##+-,- -89

 &
/ /. #' ##+-,- 
(
2
 &
/ / #' ##+-,- %22
( &
/ /6 #' ##+-,- %2- 

3%045 &
/ /-6 #' ##+-,- $ &
/ /. #' ##+-,- 777-

2

2
 &
/ / #' ##+-,- 77-7-

2

2
 &
/ / #' ##+-,- 

2

2 &
/ / #' ##+-,- 

 &
./ /+ #' ##+-,- 
7 2

- &
/ /-, #' ##+-,- 
7- 2

2 &
/ / #' ##+-,- 
7, 2


 &
/ / #' ##+-,- 77
 2

2
 &
/ / #' ##+-,- 77-
 2

2
 &
/ /- #' ##+-,- 
 2

2 &
/ /- #' ##+-,- 
 2

)

2
 &
/ /-, #' ##+-,- 7-7,
 2



 &
/ / #' ##+-,- :

 &
/ /6 #' ##+-,- : 2
( &
,/ /.6 #' ##+-,- ;7


 &


&
2<
Page 28 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 54 of 82












!
" #$%&$'
()*+,
 
.

 #.
!"# ! 
$%&'(')
 %+&'*')*

 

      





 



   %  
 !"
     
$ "#  
  


&
2<
Page 29 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 55 of 82












!
" #$%&$'
()*+,
 
(

 #.
!"# ! 
$%&'(')**
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+-.6 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+-.6  
 &
/ /- #' ##+-.6 01 &
/ /. #' ##+-.6 0

2

2
 &
/ / #' ##+-.6 0

( 2

2
 &
/ /- #' ##+-.6 0

)
 &
/ /,. #' ##+-.6 0

2
 &
./ -/+ #' ##+-.6 -0

3%45 &
/ /-- #' ##+-.6 

()( &
/ /6 #' ##+-.6 


2
( &
/ /6 #' ##+-.6 2

1 &
/ /-. #' ##+-.6 2

(

2
 &
/ /,+ #' ##+-.6 2

2
 &
/ /-, #' ##+-.6 2

)
 &
/ /,+ #' ##+-.6 2

2
 &
/ /- #' ##+-.6  7- 2

2 &
/ / #' ##+-.6  7, 2


 &
/ / #' ##+-.6 7-

,2



 &
/ /- #' ##+-.6 7-

2
305 &
/ /. #' ##+-.6 

2
 &
/ / #' ##+-.6 7- 2

1 &
/ / #' ##+-.6 7 2

1 &
/ /- #' ##+-.6 7 2

2
 &
/ /- #' ##+-.6 7- 2

2
 &
/ /-. #' ##+-.6 7 2

2 &
/ /-. #' ##+-.6 7- 2



 &
/ / #' ##+-.6 21 &
/ /-6 #' ##+-.6 -89

 &
/ /. #' ##+-.6 
(
2
 &
/ / #' ##+-.6 %22
( &
/ /6 #' ##+-.6 %2- 

3%045 &
/ /-6 #' ##+-.6 $ &
/ /. #' ##+-.6 777-

2

2
 &
/ / #' ##+-.6 77-7-

2

2
 &
/ / #' ##+-.6 

2

2 &
/ / #' ##+-.6 

 &
./ /+ #' ##+-.6 
7 2

- &
/ /-, #' ##+-.6 
7- 2

2 &
/ / #' ##+-.6 
7, 2


 &
/ / #' ##+-.6 77
 2

2
 &
/ / #' ##+-.6 77-
 2

2
 &
/ /- #' ##+-.6 
 2

2 &
/ /- #' ##+-.6 
 2

)

2
 &
/ /-, #' ##+-.6 7-7,
 2



 &
/ / #' ##+-.6 :

 &
/ /6 #' ##+-.6 : 2
( &
,/ /.6 #' ##+-.6 ;7


 &


&
2<
Page 30 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 56 of 82












!
" #$%&$'
()*+,
 
(

 #.
!"# ! 
$%&'(')**
 %+&'*')*

 

     %# 





 



    %# 
 !"
   %# 
$ "#   %# 


&
2<
Page 31 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 57 of 82












!
" #$%&$'
()*+,
 


#
!"# ! 
$%&'(').**
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+--. 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+--.  
 &
/ /- #' ##+--. 01 &
/ /. #' ##+--. 0

2

2
 &
/ / #' ##+--. 0

( 2

2
 &
/ /- #' ##+--. 0

)
 &
/ /,. #' ##+--. 0

2
 &
./ -/+ #' ##+--. -0

3%45 &
/ /-- #' ##+--. 

()( &
/ /6 #' ##+--. 


2
( &
/ /6 #' ##+--. 2

1 &
/ /-. #' ##+--. 2

(

2
 &
/ /,+ #' ##+--. 2

2
 &
/ /-, #' ##+--. 2

)
 &
/ /,+ #' ##+--. 2

2
 &
/ /- #' ##+--.  7- 2

2 &
/ / #' ##+--.  7, 2


 &
/ / #' ##+--. 7-

,2



 &
/ /- #' ##+--. 7-

2
305 &
/ /. #' ##+--. 

2
 &
/ / #' ##+--. 7- 2

1 &
/ / #' ##+--. 7 2

1 &
/ /- #' ##+--. 7 2

2
 &
/ /- #' ##+--. 7- 2

2
 &
/ /-. #' ##+--. 7 2

2 &
/ /-. #' ##+--. 7- 2



 &
/ / #' ##+--. 21 &
/ /-6 #' ##+--. -89

 &
/ /. #' ##+--. 
(
2
 &
/ / #' ##+--. %22
( &
/ /6 #' ##+--. %2- 

3%045 &
/ /-6 #' ##+--. $ &
/ /. #' ##+--. 777-

2

2
 &
/ / #' ##+--. 77-7-

2

2
 &
/ / #' ##+--. 

2

2 &
/ / #' ##+--. 

 &
./ /+ #' ##+--. 
7 2

- &
/ /-, #' ##+--. 
7- 2

2 &
/ / #' ##+--. 
7, 2


 &
/ / #' ##+--. 77
 2

2
 &
/ / #' ##+--. 77-
 2

2
 &
/ /- #' ##+--. 
 2

2 &
/ /- #' ##+--. 
 2

)

2
 &
/ /-, #' ##+--. 7-7,
 2



 &
/ / #' ##+--. :

 &
/ /6 #' ##+--. : 2
( &
,/ /.6 #' ##+--. ;7


 &


&
2<
Page 32 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 58 of 82












!
" #$%&$'
()*+,
 


#
!"# ! 
$%&'(').**
 %+&'*')*

 

      % 





 



   %  % 
 !"
    % 
$ "#    % 


&
2<
Page 33 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 59 of 82












!
" #$%&$'
()*+,
 
*

 #
!"# ! 
$%&'(').*
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+-. 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+-.  
 &
/ /- #' ##+-. 01 &
/ /. #' ##+-. 0

2

2
 &
/ / #' ##+-. 0

( 2

2
 &
/ /- #' ##+-. 0

)
 &
/ /,. #' ##+-. 0

2
 &
./ -/+ #' ##+-. -0

3%45 &
/ /-- #' ##+-. 

()( &
/ /6 #' ##+-. 


2
( &
/ /6 #' ##+-. 2

1 &
/ /-. #' ##+-. 2

(

2
 &
/ /,+ #' ##+-. 2

2
 &
/ /-, #' ##+-. 2

)
 &
/ /,+ #' ##+-. 2

2
 &
/ /- #' ##+-.  7- 2

2 &
/ / #' ##+-.  7, 2


 &
/ / #' ##+-. 7-

,2



 &
/ /- #' ##+-. 7-

2
305 &
/ /. #' ##+-. 

2
 &
/ / #' ##+-. 7- 2

1 &
/ / #' ##+-. 7 2

1 &
/ /- #' ##+-. 7 2

2
 &
/ /- #' ##+-. 7- 2

2
 &
/ /-. #' ##+-. 7 2

2 &
/ /-. #' ##+-. 7- 2



 &
/ / #' ##+-. 21 &
/ /-6 #' ##+-. -89

 &
/ /. #' ##+-. 
(
2
 &
/ / #' ##+-. %22
( &
/ /6 #' ##+-. %2- 

3%045 &
/ /-6 #' ##+-. $ &
/ /. #' ##+-. 777-

2

2
 &
/ / #' ##+-. 77-7-

2

2
 &
/ / #' ##+-. ! %,$!$, <- =
/ / #' ##+-. 

 &
./ /+ #' ##+-. 
7 2

- &
/ /-, #' ##+-. 
7- 2

2 &
/ / #' ##+-. 
7, 2


 &
/ / #' ##+-. 77
 2

2
 &
/ / #' ##+-. 77-
 2

2
 &
/ /- #' ##+-. 
 2

2 &
/ /- #' ##+-. 
 2

)

2
 &
/ /-, #' ##+-. 7-7,
 2



 &
/ / #' ##+-. :

 &
/ /6 #' ##+-. : 2
( &
,/ /.6 #' ##+-. ;7


 &


&
2<
Page 34 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 60 of 82












!
" #$%&$'
()*+,
 
*

 #
!"# ! 
$%&'(').*
 %+&'*')*

 

     % 





 



   % % 
 !"
   % 
$ "#   % 


&
2<
Page 35 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 61 of 82












!
" #$%&$'
()*+,
 
)

 #
!"# ! 
$%&'(')..
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+-- 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+--  
 &
/ /- #' ##+-- 01 &
/ /. #' ##+-- 0

2

2
 &
/ / #' ##+-- 0

( 2

2
 &
/ /- #' ##+-- 0

)
 &
/ /,. #' ##+-- 0

2
 &
./ -/+ #' ##+-- -0

3%45 &
/ /-- #' ##+-- 

()( &
/ /6 #' ##+-- 


2
( &
/ /6 #' ##+-- 2

1 &
/ /-. #' ##+-- 2

(

2
 &
/ /,+ #' ##+-- 2

2
 &
/ /-, #' ##+-- 2

)
 &
/ /,+ #' ##+-- 2

2
 &
/ /- #' ##+--  7- 2

2 &
/ / #' ##+--  7, 2


 &
/ / #' ##+-- 7-

,2



 &
/ /- #' ##+-- 7-

2
305 &
/ /. #' ##+-- 

2
 &
/ / #' ##+-- 7- 2

1 &
/ / #' ##+-- 7 2

1 &
/ /- #' ##+-- 7 2

2
 &
/ /- #' ##+-- 7- 2

2
 &
/ /-. #' ##+-- 7 2

2 &
/ /-. #' ##+-- 7- 2



 &
/ / #' ##+-- 21 &
/ /-6 #' ##+-- -89

 &
/ /. #' ##+-- 
(
2
 &
/ / #' ##+-- %22
( &
/ /6 #' ##+-- %2- 

3%045 &
/ /-6 #' ##+-- $ &
/ /. #' ##+-- 777-

2

2
 &
/ / #' ##+-- 77-7-

2

2
 &
/ / #' ##+-- ! %,$!$, <.). =
/ / #' ##+-- 

 &
./ /+ #' ##+-- 
7 2

- &
/ /-, #' ##+-- 
7- 2

2 &
/ / #' ##+-- 
7, 2


 &
/ / #' ##+-- 77
 2

2
 &
/ / #' ##+-- 77-
 2

2
 &
/ /- #' ##+-- 
 2

2 &
/ /- #' ##+-- 
 2

)

2
 &
/ /-, #' ##+-- 7-7,
 2



 &
/ / #' ##+-- :

 &
/ /6 #' ##+-- : 2
( &
,/ /.6 #' ##+-- ;7


 &


&
2<
Page 36 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 62 of 82












!
" #$%&$'
()*+,
 
)

 #
!"# ! 
$%&'(')..
 %+&'*')*

 

      





 



   %  
 !"
    
$ "#     


&
2<
Page 37 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 63 of 82












!
" #$%&$'
()*+,
 


6?
!"# ! 
$%&'(').
 %+&'*')*
,$&-.)/$ 0!1 %
$
$&
23
' 4
 
 
 & -./ -/++ #' ##+ 
 56 % 57&! !&8 
 9 :!
/ /. #' ##+  
 &
/ /- #' ##+ 01 &
/ /. #' ##+ 0

2

2
 &
/ / #' ##+ 0

( 2

2
 &
/ /- #' ##+ 0

)
 &
/ /,. #' ##+ 0

2
 &
./ -/+ #' ##+ -0

3%45 &
/ /-- #' ##+ 

()( &
/ /6 #' ##+ 


2
( &
/ /6 #' ##+ 2

1 &
/ /-. #' ##+ 2

(

2
 &
/ /,+ #' ##+ 2

2
 &
/ /-, #' ##+ 2

)
 &
/ /,+ #' ##+ 2

2
 &
/ /- #' ##+  7- 2

2 &
/ / #' ##+  7, 2


 &
/ / #' ##+ 7-

,2



 &
/ /- #' ##+ 7-

2
305 &
/ /. #' ##+ 

2
 &
/ / #' ##+ 7- 2

1 &
/ / #' ##+ 7 2

1 &
/ /- #' ##+ 7 2

2
 &
/ /- #' ##+ 7- 2

2
 &
/ /-. #' ##+ 7 2

2 &
/ /-. #' ##+ 7- 2



 &
/ / #' ##+ 21 &
/ /-6 #' ##+ -89

 &
/ /. #' ##+ 
(
2
 &
/ / #' ##+ %22
( &
/ /6 #' ##+ %2- 

3%045 &
/ /-6 #' ##+ $ &
/ /. #' ##+ 777-

2

2
 &
/ / #' ##+ 77-7-

2

2
 &
/ / #' ##+ 

2

2 &
/ / #' ##+ 

 &
./ /+ #' ##+ 
7 2

- &
/ /-, #' ##+ 
7- 2

2 &
/ / #' ##+ 
7, 2


 &
/ / #' ##+ 77
 2

2
 &
/ / #' ##+ 77-
 2

2
 &
/ /- #' ##+ 
 2

2 &
/ /- #' ##+ 
 2

)

2
 &
/ /-, #' ##+ 7-7,
 2



 &
/ / #' ##+ :

 &
/ /6 #' ##+ : 2
( &
,/ /.6 #' ##+ ;7


 &


&
2<
Page 38 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 64 of 82












!
" #$%&$'
()*+,
 


6?
!"# ! 
$%&'(').
 %+&'*')*

 

  %  
 





 



   #
 
 !"
  %
 
$ "#  
 


&
2<
Page 39 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 65 of 82

 









!
" #$%&$'
()*+,


  !"#
 
 $%
&'( $%)*+,-.*"

/0
1 23 2
"45
53
+,-.*

' %'
 
 & -./ -/++ #' ##+, 
 
53
%6537 1  %8


9 
& /./ #' ##+,  

& /-/ #' ##+, 01
& /./ #' ##+, 0

2

2

& // #' ##+, 0

( 2

2

& /-/ #' ##+, 0

)

& /,./ #' ##+, 0

2

& -/+./ #' ##+, -0

3%45
& /--/ #' ##+, 

()(
& /6/ #' ##+, 


2
(
& /6/ #' ##+, 2

1
& /-./ #' ##+, 2

(

2

& /,+/ #' ##+, 2

2

& /-,/ #' ##+, 2

)

& /,+/ #' ##+, 2

2

& /-/ #' ##+,  7- 2

2
& // #' ##+,  7, 2



& // #' ##+, 7-

,2




& /-/ #' ##+, 7-

2
305
& /./ #' ##+, 

2

& // #' ##+, 7- 2

1
& // #' ##+, 7 2

1
& /-/ #' ##+, 7 2

2

& /-/ #' ##+, 7- 2

2

& /-./ #' ##+, 7 2

2
& /-./ #' ##+, 7- 2




& // #' ##+, 21
& /-6/ #' ##+, -89


& /./ #' ##+, 
(
2

& // #' ##+, %22
(
& /6/ #' ##+, %2- 

3%045
& /-6/ #' ##+, $
& /./ #' ##+, 777-

2

2

& // #' ##+, 77-7-

2

2

& // #' ##+, 

2

2
& // #' ##+, 


& /+./ #' ##+, 
7 2

-
& /-,/ #' ##+, 
7- 2

2
& // #' ##+, 
7, 2



& // #' ##+, 77
 2

2

& // #' ##+, 77-
 2

2

& /-/ #' ##+, 
 2

2
& /-/ #' ##+, 
 2

)

2

& /-,/ #' ##+, 7-7,
 2




& // #' ##+, :


& /6/ #' ##+, : 2
(
& /.6,/ #' ##+, ;7





&
2<
Page 40 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 66 of 82

 









!
" #$%&$'
()*+,


  !"# 
 #
 
 $%
&'( $%)*+,-.*"

/0
1 23 2
"45
53
+,-.*

 

  
  







 



  


 
   

  !"
  
  # "$  
 
 $%'(
 '( $%')*+,-.*"+

/0
1 23 2
"45
53
+,-.*
 
 -. -/- #' 6 ,.
53

' '
%8


9  :

&
5 
:
;
'

 
 . 6/ #' + +,,.
01 ./ /, #' 6, ,
0

2

2
 ./ ./- #'  ,
0

( 2

2
 ./ ./, #'  ,
0

)
 ./ .,/ #' + ,
0

2
 ./ /- #' 6- .,.
-0

3%45 -. -,/. #' . ..,


()( ./ /., #' 6, +,.



2
( ./ ,/+ #' 6 
2

1 ./ /, #'  ,
2

(

2
 ./ .,/ #' 6 ,,
2

2
 ./ / #' 6, +,6
2

)
 ./ / #' 6 ,
2

2
 ./ /, #' 6 ,,.
7- 2

2 ./ -/+6 #' 6. ,
7, 2


 ./ .-/- #' . ,,
7-

,2



 ./ ./+ #'  .,6
7-

2
305 ./ ./+ #'  ,


2
 ./ +/ #' - ,
7- 2

1 ./ ../- #'  ,
7 2

1 ./ .,/+ #'  ,
7 2

2
 ./ / #' 6 ,
7- 2

2
 ./ +/, #' - ,
7 2

2 ./ ,/-- #' 6+ ,-
7- 2



 ./ ./, #'  ,
21 ./ 6/ #' 6 ,
-89

 -. ,/, #' - .-

(
2
 ./ /, #' 6 .
%22
( ./ /. #' 6 ,
%2- 

3%045 -. ,/, #' -, +,
$ ./ ./ #'  ,
777-

2

2
 ./ ./, #' , ,
77-7-

2

2
 ./ ./6 #' + +,


2

2 ./ 6/ #' 6 ,


 ./ +/+ #' , ,

7 2

- ./ .+/-+ #' , .

7- 2

2 ./ -/ #' 6 ,


&
2<
Page 41 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 67 of 82

 









!
" #$%&$'
()*+,


  !"# 
 #
 
 $%'(
 '( $%')*+,-.*"+

/0
1 23 2
"45
53
+,-.*

7, 2


 ./ ../ #' - +,-
53

' '
%8


9  :

&
5 
:
;
'

77
 2

2
 ./ -/+ #' 6 ,.
77-
 2

2
 ./ .,/, #' + ,

 2

2 ./ -/6 #' 6+ ,

 2

)

2
 ./ ./6. #' - ..
7-7,
 2



 ./ ./, #' . ,
:

  +/,+ #' + .+
: 2
( ./ /- #' 66 .,
;7


  / #'  ,-

 

  



   


  



   
$ !"
  
# "$  
 
 $%'(
 %'( $%'%)*+,-.*")

/0
1 23 2
"45
53
+,-.*
 
 -. -.-/. #'  ,.  -,
53

'% '%
%8


9  :

&
5 
:
;
'
 '
1%

1%
 
 . +/ #'  +,,. , +
01 ./ /6 #' 6 , - -
0

2

2
 ./ / #'  ,  +
0

( 2

2
 ./ ./-, #'  ,  
0

)
 ./ .-/- #' . ,  
0

2
 ./ -/ #' 6 .,. - 
-0

3%45 -. -,-/- #' , .., - 


()( ./ /6, #' 6 +,.  +



2
( ./ /- #'   , +
2

1 ./ /6 #'  ,  -
2

(

2
 ./ .,/-- #' + ,,  ,
2

2
 ./ ,/+ #' 6+ +,6  .
2

)
 ./ -/- #' 6. ,  
2

2
 ./ -/ #' 6+ ,,. + -
7- 2

2 ./ ,/ #' 6+ ,  .
7, 2


 ./ .,/6 #' 6 ,, , .
7-

,2



 ./ ./ #' . .,6  
7-

2
305 ./ ./ #' 6 ,  ,


2
 ./ ./+ #'  ,  
7- 2

1 ./ ../ #'  ,  -
7 2

1 ./ .,/6 #' 6 ,  -
7 2

2
 ./ -/ #' 6+ , - 
7- 2

2
 ./ ./ #'  , - ,
7 2

2 ./ /+ #' 66 ,- - -
7- 2



 ./ ./6 #' - ,  .
21 ./ /, #'  , - -


&
2<
Page 42 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 68 of 82

 









!
" #$%&$'
()*+,


  !"# 
 #
 
 $%'(
 %'( $%'%)*+,-.*")

/0
1 23 2
"45
53
+,-.*
-89

 -. ,./- #' -- .- - 
53

'% '%
%8


9  :

&
5 
:
;
'
 '
1%

1%

(
2
 ./ ./ #'  . , -
%22
( ./ /.6 #' 6 ,  .
%2- 

3%045 -. ,/ #' - +, - -
$ ./ .-/. #'  ,  -
777-

2

2
 ./ ./. #'  ,  ,
77-7-

2

2
 ./ .+/6+ #'  +, - .


2

2 ./ ./-- #'  , - 


 ./ 6/.- #'  ,  ,

7 2

- ./ ./ #'  . - -

7- 2

2 ./ -/ #' 6+ , - .

7, 2


 ./ ../6 #' - +,-  ,
77
 2

2
 ./ ,/6 #' 6+ ,. , .
77-
 2

2
 ./ .-/ #' + ,  ,

 2

2 ./ ,/ #' 6 , - 

 2

)

2
 ./ /++ #' . ..  --
7-7,
 2



 ./ .+/6, #'  ,  
:

  ,/6 #'  .+ , -
: 2
( ./ ./, #'  ., - .
;7


  / #'  ,- - 

 

  


%
   


  




   
$ !"
  
# "$  
 
 $%0-'( $%)*-..*.

/0
1 23 2
"45
53
+,-.*
 
 & -. -,/, #' + ,.
53

 
%8


9  :

&
5 






9 
:
;
'

 
 & . -/ #' 66 .,.
01 & ./ -/,6 #' 6. ..
0

2

2
 & ./ ./, #'  .,-
0

( 2

2
 & ./ ./,, #'  
0

)
 & ./ ./-- #' - .,.
0

2
 & ./ /-- #' 6 ,.
-0

3%45 & -. -+/ #' 6+ .,


()( & ./ -/- #' 6 ,..



2
( & ./ +/, #' , .+.
2

1 & ./ ./- #'  ,
2

(

2
 & ./ .,/ #' 6 ++
2

2
 & ./ ,/ #' 6 .6 
2

)
 & ./ -/66 #' 6+ ++,6
2

2
 & ./ /- #' 6- .
7- 2

2 & ./ ,/+ #' 6+ +6 ,


&
2<
Page 43 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 69 of 82

 









!
" #$%&$'
()*+,


  !"# 
 #
 
 $%0-'( $%)*-..*.

/0
1 23 2
"45
53
+,-.*
7, 2


 & ./ .,/ #' + ,,
53

 
%8


9  :

&
5 






9 
:
;
'

7-

,2



 & ./ ./- #' , ,6 ,6
7-

2
305 & ./ .-/6 #'  +.,


2
 & ./ /.. #' 6 ,
7- 2

1 & ./ ./6, #'  ,
7 2

1 & ./ ./ #' - ,
7 2

2
 & ./ ,/6 #' 66 +,
7- 2

2
 & ./ -/ #' 6+ +,+
7 2

2 & ./ ./-. #'  ..
7- 2



 & ./ +/- #' - +,
21 & ./ ./+ #'  +.,
-89

 & -. -66/ #' . .

(
2
 & ./ / #' 66 ,.
%22
( & ./ /,. #' 6 +,
%2- 

3%045 & -. -6+/ #' . .
$ & ./ .-/+. #' . ,
777-

2

2
 & ./ ./. #'  ,
77-7-

2

2
 & ./ .,/ #'  .+.


2

2 & ./ /+ #'  .,6


 & ./ /-. #' 6 +,+

7 2

- & ./ ./, #'  ,.

7- 2

2 & ./ -/ #' 6+ .,

7, 2


 & ./ ./ #' 6 +,-
77
 2

2
 & ./ ./- #'  +6 
77-
 2

2
 & ./ ./+. #' , ,

 2

2 & ./ ,/6 #' 6 +,,.

 2

)

2
 & ./ /+ #' 6 .
7-7,
 2



 & ./ .,/, #'  +.,
:

 &  6,/-. #' 6, ,+
: 2
( & ./ ./, #'  ..
;7


 &  /6 #' - +,-

 

  








  


%
   
 !"
  
# "$  
 
 $%0-'( $%)*-..*.%

/0
1 23 2
"45
53
+,-.*
 
 & -. -6/ #'  ,. . -6
53

% %
%8


9  :

&
5 






9 
:
;
'
 '
1%

1%
 
 & . .+/ #' , .,. . -,
01 & ./ +/6 #'  ..  --
0

2

2
 & ./ ./. #' - .,-  -
0

( 2

2
 & ./ ./, #'    +


&
2<
Page 44 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 70 of 82

 









!
" #$%&$'
()*+,


  !"# 
 #
 
 $%0-'( $%)*-..*.%

/0
1 23 2
"45
53
+,-.*
0

)
 & ./ ./+ #' + .,. - -
53

% %
%8


9  :

&
5 






9 
:
;
'
 '
1%

1%
0

2
 & ./ +/.. #' , ,. . 
-0

3%45 & -. -6/, #'  .,  -6


()( & ./ +/+6 #' , ,..  ,



2
( & ./ /. #'  .+.  6
2

1 & ./ ./- #'  ,  .
2

(

2
 & ./ ./, #'  ++  
2

2
 & ./ / #'  .6  - ,
2

)
 & ./ /- #' . ++,6  -
2

2
 & ./ / #'  .  ,
7- 2

2 & ./ /++ #' . +6 ,  -
7, 2


 & ./ ./- #'  ,,  
7-

,2



 & ./ +/ #' - ,6 ,6 . -+
7-

2
305 & ./ ./ #'  +., , -


2
 & ./ ./, #'  , - 
7- 2

1 & ./ ./, #'  , , .
7 2

1 & ./ ./. #' . , - 
7 2

2
 & ./ 6/- #' + +,  -,
7- 2

2
 & ./ /, #'  +,+ . --
7 2

2 & ./ ./6- #' - .. - -
7- 2



 & ./ ./- #'  +,  
21 & ./ ../+ #'  +.,  6
-89

 & -. ,,-/ #' ,, .  -

(
2
 & ./ ./+ #'  ,.  ,
%22
( & ./ ./, #'  +,  --
%2- 

3%045 & -. ,-/, #' , . , -
$ & ./ ./+6 #' . ,  +
777-

2

2
 & ./ ./-6 #' . ,  +
77-7-

2

2
 & ./ +-/- #' - .+. . 


2

2 & ./ ../, #'  .,6  


 & ./ .-/+6 #' . +,+  6

7 2

- & ./ ./ #' 6 ,. + -6

7- 2

2 & ./ 6/- #' + .,  -.

7, 2


 & ./ +/- #' - +,-  6
77
 2

2
 & ./ / #' 6 +6  6 
77-
 2

2
 & ./ ./- #' + ,  6

 2

2 & ./ 6/-. #'  +,,.  

 2

)

2
 & ./ .,/.6 #'  .  ,-
7-7,
 2



 & ./ +/. #' - +., . 
:

 &  ,/6 #'  ,+ - -
: 2
( & ./ ./+ #' - .. - ,
;7


 &  /+ #' - +,-  

 

  








  



   
 !"
  

# "$  


&
2<
Page 45 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 71 of 82



 








!
" #$%&$'
()*+,

 

! "#$% #
 "#$% &#"'"# 
( #
) &#"

-
 ./+0
1!0'&2


#&
-
 ./+0/ %- 


#&
-
 ./+0, %- 


#&
-
 ./+0 %- /


#&
-
 ./+03 %- /


#&
-
 ./+0+ %- ,


#&
-
 ./+0 %- ,


#&
-
 ./+0. %- 


#&
-
 ./+0 %- 


#&
-
 ./+0 %- 


#&
-
 ./+0 %- 


#&
-
 ./+0/ %- /


#&
-
 ./+0, %- /


#&
-
 ./+0 $- 


#&
-
 ./+03 %- 1


#&
-
 ./+0+ %- 1


#&
-
 ./+0 4'0'&2


#&
-
 ./+0%0,3+#+ %5
(0



#&
-
 ./+0'$,3+#, '


$
 


#&
-
 ./+0'$,3+# '


$
 


#&
-
 ./+0/%$ %- 


#&
-
 ./+0/%$ %- 


#&


&
56
Page 46 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 72 of 82









   
!
"#$%&$'()*+ ,






 !!!
"
#$



%!& '& () )



*
%!& )& ( )
 -.+/  ##+,, 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$

 !!!0
"
#$



%!& '& ( 0 )



*
%!& )& ( )
 -.+/  ##++ 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$ 

 !!!'
"
#$



%!& '& ( 0)



*
%!& )& ( )
 -.+/  ##++,1 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$0

 !!!
"
#$



%!& '& ( ')



*
%!& )& ( )
 -.+/  ##+ . 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$0

 !!!)
"
#$



%!& '& ( )



*
%!& )& ( )
 -.+/  ##+ .- 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$'

 !!!(
"
#$



%!& '& ( )



*
%!& )& ( )
 -.+/  ##+ 11 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&

&34
Page 47 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 73 of 82









   
!
"#$%&$'()*+ ,



"$'

 !!!!
"
#$



%!& '& ( '



*
%!& )& ( )
 -.+/  ##+-. 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$

 !!!1
"
#$



%!& '& (! 



*
%!& )& ( )
 -.+/  ##+- 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$

 !!!
"
#$



%!& '& (1')



*
%!& )& ( )
 -.+/  ##+, 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$

 !!! 
"
#$



%!& '& (!')



*
%!& )& ( )
 -.+/  ##+ 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$ 

 !!!
"
#$



%!& '& (1 )



*
%!& )& ( )
 -.+/  ##+.+ 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$ 0

 !!! 0
"
#$



%!& '& ( 



*
%!& )& ( )
 -.+/  ##+.,. 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&

&34
Page 48 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 74 of 82









   
!
"#$%&$'()*+ ,



"$ 0

 !!! '
"
#$



%!& '& ())



*
%!& )& ( )
 -.+/  ##+.1- 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



$

 !!! 
"
#$



%!& '& ( 0))



*
%!& )& ( )
 -.+/  ##+..1 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$

 !!! )
"
#$



%!& '& ( 0)



*
%!& )& ( )
 -.+/  ##+.1 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



"$

 !!! (
"
#$



%!& '& ( 00



*
%!& )& ( )
 -.+/  ##+.. 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&



/2



 !!! !
"
#$



%!& '& ( 0



*
%!& )& ( )
 -.+/  ##+ 0 ,1+  '&$2
+

 
"
%
+

 +,-


%
 +.
%

-


-

/
#&

+
3


,
'&$25
&346.+7


3
46&346&, .6'8+19 .+

&34
Page 49 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 75 of 82










!
" #$%&$'
()*+,




$-.+./+0 1

2
 

(34#%$5
'&$6

$-.+78
%9
(:
;

$
(-
<!9
#9
%9
(8<
9((
<&
;.+(= (
>



'&$67

&
9;</+:
9
;<&
9;<
&,/<
'3+?5/+


&
9;
Page 50 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 76 of 82











   
!
"#$%&$'()*+ ,
  
-
)(.
-

/

    


  !

&
-

011#$12 ,3 $!

4,+

&-5
Page 51 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 77 of 82
Page 52 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 78 of 82
Page 53 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 79 of 82
Page 54 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 80 of 82














 



 
  
 !

" #

 

 !"#$%&"'"!
%()*"

!%%

!%

#

+

'"
&%"
%!%,-
%,%"+
)."
%!%%,-
%,
"+

'"

%%!
'#"
%!


!$'+

%$

"#!"+






%""+






%
"
!!+


/
%
%+


/
%-!
!+


/
%-!
$'
-
+

0%'1!
&%
%
/
2

'

!%"
"%$'"
%
"#!!'
/
+

%

"#!$'3!45"
!%%$'!
3%6

"
%'#%+



%


+

""!)%

#!!+

.

%"
%

%!+

%
"-!+
).7
%
#8
-!+

'
%%
--"#+-

9
%!%%,"+
9
%!
:): %



%
9

;
'!%"'#'!%"

%
(<4)=6+

:
'%"%%

%+

%!
9

%
"%+
). %!

'

'"!+
" #Page 55 of 55 7/28/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 81 of 82
Page 82 of 82
13339 Hagers Ferry RoadHuntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J16070056
Project Name:MCGUIRE -
Lab Contact: Anne Pridgeon
Date:8/5/2016
Customer Address:13225 Hagers Ferry Rd
Customer Name(s):TIM HUNSUCKER, CHUCK CAMPBELL
Mail Code: MG01CH
Huntersville, NC 28078-8985
Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Anne Pridgeon) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results) under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of specific methods.
Anne Pridgeon
Duke Energy Analytical Lab
Page 1 of 8
Reason: I have reviewed
this document.
Date: 2016.08.05 12:17:24
-04'00'
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection Date and Time Collected By Sample Description
2016019983 MCGUIRE 13-Jul-16 12:55 PM PSP SW-1
1 Total Samples
Duke Energy Analytical Lab
Page 2 of 8
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:Anne Pridgeon Date:7/29/2016
Electronic Data Deliverable (EDD) Sent Separatel
Duke Energy Analytical Lab
Page 3 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070056
2016019983
Collection Date:13-Jul-16 12:55 PM
Site:SW-1
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP
Barium (Ba)0.032 mg/L SW 6010D 07/26/2016 12:44 JJMACKE0.005 1
Chromium (Cr)< 0.005 mg/L SW 6010D 07/26/2016 12:44 JJMACKE0.005 1
Silver (Ag)< 0.005 mg/L SW 6010D 07/26/2016 12:44 JJMACKE0.005 1
DISSOLVED METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020B 07/19/2016 14:34 CWSPEN311
Cadmium (Cd)< 1 ug/L SW 6020B 07/19/2016 14:34 CWSPEN311
Lead (Pb)< 1 ug/L SW 6020B 07/19/2016 14:34 CWSPEN311
Duke Energy Analytical Lab
Page 4 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070056
Q16070711 ICP Dissolved DISSOLVED METALS BY ICP
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Barium (Ba) 0.000136 mg/L -10.000136 0.005 < 1/2 RDL
Chromium (Cr) -0.000611 mg/L -1-0.000611 0.005 < 1/2 RDL
Silver (Ag) 0.000349 mg/L -10.000349 0.005 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Barium (Ba) 0.964 1 96.4mg/L -1158510.964
Chromium (Cr) 1 1 100mg/L -1158511
Silver (Ag) 0.973 1 97.3mg/L -1158510.973
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16070039 -- 2016019936
Barium (Ba) 5.48 5 109mg/L -1307015.48
Chromium (Cr) 5.33 5 107mg/L -1307015.33
Silver (Ag) 4.69 5 93.8mg/L -1307014.69
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16070039 -- 2016019936
Barium (Ba) 5.51 5 110 0.512mg/L -1307015.51
Chromium (Cr) 5.38 5 108 0.99mg/L -1307015.38
Silver (Ag) 4.71 5 94.2 0.425mg/L -1307014.71
Duke Energy Analytical Lab
Page 5 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070056
Q16070476 IMS Dissolved DISSOLVED METALS BY ICP-MS
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Arsenic (As) -0.0037 ug/L -1-0.0037 1 < 1/2 RDL
Cadmium (Cd) 0.0018 ug/L -10.0018 1 < 1/2 RDL
Lead (Pb) 0.0027 ug/L -10.0027 1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
Blank # 2
RDL Relative Concentration
Arsenic (As) -0.011 ug/L -1-0.011 1 < 1/2 RDL
Cadmium (Cd) 0.0047 ug/L -10.0047 1 < 1/2 RDL
Lead (Pb) 0.0152 ug/L -10.0152 1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Arsenic (As) 80.3 80 100ug/L -12080180.3
Cadmium (Cd) 8.12 8 102ug/L -1208018.12
Lead (Pb) 81.9 80 102ug/L -12080181.9
Final QualifierDilMeasuredUnits:Parameter
LCS # 2
% Recovery LCL UCLSpike
Arsenic (As) 82.8 80 103ug/L -12080182.8
Cadmium (Cd) 8.32 8 104ug/L -1208018.32
Lead (Pb) 83.1 80 104ug/L -12080183.1
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16070039 -- 2016019936
Arsenic (As) 49.3 50 98.5ug/L -12575149.3
Cadmium (Cd) 50.8 50 102ug/L -12575150.8
Lead (Pb) 50.4 50 101ug/L -12575150.4
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16070039 -- 2016019936
Arsenic (As) 48.8 50 97.4 1.06ug/L -13070148.8
Cadmium (Cd) 50.3 50 101 0.911ug/L -13070150.3
Lead (Pb) 50.2 50 100 0.326ug/L -13070150.2
Final QualifierDilMeasuredUnits:Parameter
MS # 2
% Recovery LCL UCLSpike
Parent Sample: J16070412 -- 2016021928
Arsenic (As) 53.9 50 108ug/L -12575153.9
Cadmium (Cd) 51.6 50 103ug/L -12575151.6
Lead (Pb) 52.1 50 104ug/L -12575152.1
Final QualifierDilMeasuredUnits:Parameter
MSD # 2
RPD% Recovery LCL UCLSpike
Parent Sample: J16070412 -- 2016021928
Arsenic (As) 54.1 50 108 0.269ug/L -13070154.1
Duke Energy Analytical Lab
Page 6 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16070056
Q16070476 IMS Dissolved DISSOLVED METALS BY ICP-MS
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
MSD # 2
RPD% Recovery LCL UCLSpike
Parent Sample: J16070412 -- 2016021928
Cadmium (Cd) 50.9 50 102 1.37ug/L -13070150.9
Lead (Pb) 51.5 50 103 1.04ug/L -13070151.5
Duke Energy Analytical Lab
Page 7 of 8
Duke Energy Analytical Lab Page 8 of 8
Radiological Data for MCGUIRE
414437Sample #:Station:MCGUIRE
Collection End: 7/13/2016 12:15:00
Collection Start:7/13/2016 12:15:00Location:MW-1_ML1 [ MNS Landfill 1 / MW-1 ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-1.1E-01 0.00E+00 9.59E-01 LLD OK<3
Beta 1.66E+00 7.77E-01 1.22E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <6.86E+00 0.00E+00 6.86E+00 <1000 LLD OK<15
Co-58 <5.60E+00 0.00E+00 5.60E+00 <1000 LLD OK<15
Fe-59 <1.08E+01 0.00E+00 1.08E+01 <400 LLD OK<30
Co-60 <7.21E+00 0.00E+00 7.21E+00 <300 LLD OK<15
Zn-65 <1.28E+01 0.00E+00 1.28E+01 <300 LLD OK<30
Zr-95 <1.01E+01 0.00E+00 1.01E+01 <400 LLD OK<15
Nb-95 <7.00E+00 0.00E+00 7.00E+00 <400 LLD OK<15
I-131 <6.40E+00 0.00E+00 6.40E+00 LLD OK<15
Cs-134 <6.96E+00 0.00E+00 6.96E+00 <30 LLD OK<15
Cs-137 <5.70E+00 0.00E+00 5.70E+00 <50 LLD OK<18
BaLa-140 <1.12E+01 0.00E+00 1.12E+01 <200 LLD OK<15
Be-7 <4.54E+01 0.00E+00 4.54E+01
K-40 <1.06E+02 0.00E+00 1.06E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-1.9E+01 0.00E+00 1.88E+02 <20000 LLD OK<250
414438Sample #:Station:MCGUIRE
Collection End: 7/13/2016 12:05:00
Collection Start:7/13/2016 12:05:00Location:MW-1D_ML1 [ MNS Landfill 1 / MW-1D ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <3.67E-02 0.00E+00 9.65E-01 LLD OK<3
Beta 2.65E+00 8.23E-01 1.22E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <6.63E+00 0.00E+00 6.63E+00 <1000 LLD OK<15
Co-58 <6.57E+00 0.00E+00 6.57E+00 <1000 LLD OK<15
Fe-59 <1.25E+01 0.00E+00 1.25E+01 <400 LLD OK<30
Page 1 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 1 of 13 08.25.2016
Radiological Data for MCGUIRE
414438Sample #:Station:MCGUIRE
Collection End: 7/13/2016 12:05:00
Collection Start:7/13/2016 12:05:00Location:MW-1D_ML1 [ MNS Landfill 1 / MW-1D ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <8.51E+00 0.00E+00 8.51E+00 <300 LLD OK<15
Zn-65 <5.30E+00 0.00E+00 5.30E+00 <300 LLD OK<30
Zr-95 <1.09E+01 0.00E+00 1.09E+01 <400 LLD OK<15
Nb-95 <6.48E+00 0.00E+00 6.48E+00 <400 LLD OK<15
I-131 <7.18E+00 0.00E+00 7.18E+00 LLD OK<15
Cs-134 <6.32E+00 0.00E+00 6.32E+00 <30 LLD OK<15
Cs-137 <5.69E+00 0.00E+00 5.69E+00 <50 LLD OK<18
BaLa-140 <8.67E+00 0.00E+00 8.67E+00 <200 LLD OK<15
Be-7 1.21E+01 2.78E+01 4.53E+01
K-40 5.25E+01 4.21E+01 6.03E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-9.5E+00 0.00E+00 1.86E+02 <20000 LLD OK<250
414439Sample #:Station:MCGUIRE
Collection End: 7/13/2016 13:45:00
Collection Start:7/13/2016 13:45:00Location:MW-2A_ML1 [ MNS Landfill 1 / MW-2A ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-9.4E-03 0.00E+00 9.86E-01 LLD OK<3
Beta 1.70E+00 7.84E-01 1.23E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.88E+00 0.00E+00 4.88E+00 <1000 LLD OK<15
Co-58 <4.62E+00 0.00E+00 4.62E+00 <1000 LLD OK<15
Fe-59 <8.78E+00 0.00E+00 8.78E+00 <400 LLD OK<30
Co-60 <5.66E+00 0.00E+00 5.66E+00 <300 LLD OK<15
Zn-65 <1.11E+01 0.00E+00 1.11E+01 <300 LLD OK<30
Zr-95 <8.38E+00 0.00E+00 8.38E+00 <400 LLD OK<15
Nb-95 <4.45E+00 0.00E+00 4.45E+00 <400 LLD OK<15
I-131 <5.21E+00 0.00E+00 5.21E+00 LLD OK<15
Cs-134 <5.93E+00 0.00E+00 5.93E+00 <30 LLD OK<15
Cs-137 <5.34E+00 0.00E+00 5.34E+00 <50 LLD OK<18
BaLa-140 <6.63E+00 0.00E+00 6.63E+00 <200 LLD OK<15
Page 2 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 2 of 13 08.25.2016
Radiological Data for MCGUIRE
414439Sample #:Station:MCGUIRE
Collection End: 7/13/2016 13:45:00
Collection Start:7/13/2016 13:45:00Location:MW-2A_ML1 [ MNS Landfill 1 / MW-2A ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.00E+01 0.00E+00 4.00E+01
K-40 7.75E+01 5.94E+01 8.89E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <3.37E+01 0.00E+00 1.88E+02 <20000 LLD OK<250
414440Sample #:Station:MCGUIRE
Collection End: 7/13/2016 14:05:00
Collection Start:7/13/2016 14:05:00Location:MW-2D_ML1 [ MNS Landfill 1 / MW-2D ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-1.0E-01 0.00E+00 9.06E-01 LLD OK<3
Beta 9.58E-01 7.35E-01 1.21E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.72E+00 0.00E+00 4.72E+00 <1000 LLD OK<15
Co-58 <6.63E+00 0.00E+00 6.63E+00 <1000 LLD OK<15
Fe-59 <1.16E+01 0.00E+00 1.16E+01 <400 LLD OK<30
Co-60 <6.70E+00 0.00E+00 6.70E+00 <300 LLD OK<15
Zn-65 <1.42E+01 0.00E+00 1.42E+01 <300 LLD OK<30
Zr-95 <1.15E+01 0.00E+00 1.15E+01 <400 LLD OK<15
Nb-95 <6.39E+00 0.00E+00 6.39E+00 <400 LLD OK<15
I-131 <6.03E+00 0.00E+00 6.03E+00 LLD OK<15
Cs-134 <5.89E+00 0.00E+00 5.89E+00 <30 LLD OK<15
Cs-137 <6.21E+00 0.00E+00 6.21E+00 <50 LLD OK<18
BaLa-140 <6.74E+00 0.00E+00 6.74E+00 <200 LLD OK<15
Be-7 <4.02E+01 0.00E+00 4.02E+01
K-40 <9.53E+01 0.00E+00 9.53E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <3.61E+01 0.00E+00 1.88E+02 <20000 LLD OK<250
Page 3 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 3 of 13 08.25.2016
Radiological Data for MCGUIRE
414441Sample #:Station:MCGUIRE
Collection End: 7/13/2016 10:05:00
Collection Start:7/13/2016 10:05:00Location:MW-3_ML1 [ MNS Landfill 1 / MW-3 ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <1.88E-01 0.00E+00 9.15E-01 LLD OK<3
Beta 1.28E+00 7.54E-01 1.21E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.02E+00 0.00E+00 5.02E+00 <1000 LLD OK<15
Co-58 <5.18E+00 0.00E+00 5.18E+00 <1000 LLD OK<15
Fe-59 <9.02E+00 0.00E+00 9.02E+00 <400 LLD OK<30
Co-60 <7.73E+00 0.00E+00 7.73E+00 <300 LLD OK<15
Zn-65 <1.35E+01 0.00E+00 1.35E+01 <300 LLD OK<30
Zr-95 <5.96E+00 0.00E+00 5.96E+00 <400 LLD OK<15
Nb-95 <5.88E+00 0.00E+00 5.88E+00 <400 LLD OK<15
I-131 <5.51E+00 0.00E+00 5.51E+00 LLD OK<15
Cs-134 <7.46E+00 0.00E+00 7.46E+00 <30 LLD OK<15
Cs-137 <5.13E+00 0.00E+00 5.13E+00 <50 LLD OK<18
BaLa-140 <6.83E+00 0.00E+00 6.83E+00 <200 LLD OK<15
Be-7 <3.81E+01 0.00E+00 3.81E+01
K-40 <8.53E+01 0.00E+00 8.53E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <2.66E+01 0.00E+00 1.89E+02 <20000 LLD OK<250
414442Sample #:Station:MCGUIRE
Collection End: 7/13/2016 10:30:00
Collection Start:7/13/2016 10:30:00Location:MW-3D_ML1 [ MNS Landfill 1 / MW-3D ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <2.11E-01 0.00E+00 1.02E+00 LLD OK<3
Beta 8.72E-01 7.51E-01 1.24E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.91E+00 0.00E+00 5.91E+00 <1000 LLD OK<15
Co-58 <5.48E+00 0.00E+00 5.48E+00 <1000 LLD OK<15
Fe-59 <1.32E+01 0.00E+00 1.32E+01 <400 LLD OK<30
Page 4 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 4 of 13 08.25.2016
Radiological Data for MCGUIRE
414442Sample #:Station:MCGUIRE
Collection End: 7/13/2016 10:30:00
Collection Start:7/13/2016 10:30:00Location:MW-3D_ML1 [ MNS Landfill 1 / MW-3D ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <5.94E+00 0.00E+00 5.94E+00 <300 LLD OK<15
Zn-65 <1.23E+01 0.00E+00 1.23E+01 <300 LLD OK<30
Zr-95 <1.05E+01 0.00E+00 1.05E+01 <400 LLD OK<15
Nb-95 <5.82E+00 0.00E+00 5.82E+00 <400 LLD OK<15
I-131 <5.85E+00 0.00E+00 5.85E+00 LLD OK<15
Cs-134 <6.00E+00 0.00E+00 6.00E+00 <30 LLD OK<15
Cs-137 <7.86E+00 0.00E+00 7.86E+00 <50 LLD OK<18
BaLa-140 <9.30E+00 0.00E+00 9.30E+00 <200 LLD OK<15
Be-7 <4.39E+01 0.00E+00 4.39E+01
K-40 5.74E+01 5.29E+01 8.14E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-2.6E+01 0.00E+00 1.87E+02 <20000 LLD OK<250
414444Sample #:Station:MCGUIRE
Collection End: 7/13/2016 07:10:00
Collection Start:7/13/2016 07:10:00Location:MW-4_ML1 [ MNS Landfill 1 / MW-4 ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <1.05E-01 0.00E+00 1.02E+00 LLD OK<3
Beta 6.18E-01 7.39E-01 1.24E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <6.80E+00 0.00E+00 6.80E+00 <1000 LLD OK<15
Co-58 <5.77E+00 0.00E+00 5.77E+00 <1000 LLD OK<15
Fe-59 <1.12E+01 0.00E+00 1.12E+01 <400 LLD OK<30
Co-60 <5.83E+00 0.00E+00 5.83E+00 <300 LLD OK<15
Zn-65 <1.15E+01 0.00E+00 1.15E+01 <300 LLD OK<30
Zr-95 <8.68E+00 0.00E+00 8.68E+00 <400 LLD OK<15
Nb-95 <6.93E+00 0.00E+00 6.93E+00 <400 LLD OK<15
I-131 <4.80E+00 0.00E+00 4.80E+00 LLD OK<15
Cs-134 <5.43E+00 0.00E+00 5.43E+00 <30 LLD OK<15
Cs-137 <4.94E+00 0.00E+00 4.94E+00 <50 LLD OK<18
BaLa-140 <5.67E+00 0.00E+00 5.67E+00 <200 LLD OK<15
Page 5 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 5 of 13 08.25.2016
Radiological Data for MCGUIRE
414444Sample #:Station:MCGUIRE
Collection End: 7/13/2016 07:10:00
Collection Start:7/13/2016 07:10:00Location:MW-4_ML1 [ MNS Landfill 1 / MW-4 ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.13E+01 0.00E+00 4.13E+01
K-40 <9.07E+01 0.00E+00 9.07E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-6.8E+01 0.00E+00 1.90E+02 <20000 LLD OK<250
414445Sample #:Station:MCGUIRE
Collection End: 7/13/2016 11:25:00
Collection Start:7/13/2016 11:25:00Location:MW-4R_ML1 [ MNS Landfill 1 / MW-4R ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-1.1E-01 0.00E+00 9.47E-01 LLD OK<3
Beta 7.42E-01 7.31E-01 1.22E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <3.79E+00 0.00E+00 3.79E+00 <1000 LLD OK<15
Co-58 <4.04E+00 0.00E+00 4.04E+00 <1000 LLD OK<15
Fe-59 <9.07E+00 0.00E+00 9.07E+00 <400 LLD OK<30
Co-60 <4.97E+00 0.00E+00 4.97E+00 <300 LLD OK<15
Zn-65 <7.80E+00 0.00E+00 7.80E+00 <300 LLD OK<30
Zr-95 <7.90E+00 0.00E+00 7.90E+00 <400 LLD OK<15
Nb-95 <5.01E+00 0.00E+00 5.01E+00 <400 LLD OK<15
I-131 <4.39E+00 0.00E+00 4.39E+00 LLD OK<15
Cs-134 <4.59E+00 0.00E+00 4.59E+00 <30 LLD OK<15
Cs-137 <4.91E+00 0.00E+00 4.91E+00 <50 LLD OK<18
BaLa-140 <3.85E+00 0.00E+00 3.85E+00 <200 LLD OK<15
Be-7 <3.06E+01 0.00E+00 3.06E+01
K-40 <8.83E+01 0.00E+00 8.83E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-5.9E+01 0.00E+00 1.91E+02 <20000 LLD OK<250
Page 6 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 6 of 13 08.25.2016
Radiological Data for MCGUIRE
414446Sample #:Station:MCGUIRE
Collection End: 7/13/2016 08:35:00
Collection Start:7/13/2016 08:35:00Location:MW-4D_ML1 [ MNS Landfill 1 / MW-4D ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-6.4E-02 0.00E+00 1.16E+00 LLD OK<3
Beta <4.05E-01 0.00E+00 1.30E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <6.36E+00 0.00E+00 6.36E+00 <1000 LLD OK<15
Co-58 <6.15E+00 0.00E+00 6.15E+00 <1000 LLD OK<15
Fe-59 <8.90E+00 0.00E+00 8.90E+00 <400 LLD OK<30
Co-60 <5.39E+00 0.00E+00 5.39E+00 <300 LLD OK<15
Zn-65 <1.09E+01 0.00E+00 1.09E+01 <300 LLD OK<30
Zr-95 <7.77E+00 0.00E+00 7.77E+00 <400 LLD OK<15
Nb-95 <4.75E+00 0.00E+00 4.75E+00 <400 LLD OK<15
I-131 <6.48E+00 0.00E+00 6.48E+00 LLD OK<15
Cs-134 <6.13E+00 0.00E+00 6.13E+00 <30 LLD OK<15
Cs-137 <4.25E+00 0.00E+00 4.25E+00 <50 LLD OK<18
BaLa-140 <5.97E+00 0.00E+00 5.97E+00 <200 LLD OK<15
Be-7 <4.45E+01 0.00E+00 4.45E+01
K-40 <6.86E+01 0.00E+00 6.86E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-5.5E+01 0.00E+00 1.90E+02 <20000 LLD OK<250
414447Sample #:Station:MCGUIRE
Collection End: 7/13/2016 12:20:00
Collection Start:7/13/2016 12:20:00Location:MW-4DR_ML1 [ MNS Landfill 1 / MW-4DR ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <1.02E-01 0.00E+00 1.04E+00 LLD OK<3
Beta 1.52E+00 7.86E-01 1.24E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.98E+00 0.00E+00 4.98E+00 <1000 LLD OK<15
Co-58 <4.39E+00 0.00E+00 4.39E+00 <1000 LLD OK<15
Fe-59 <8.35E+00 0.00E+00 8.35E+00 <400 LLD OK<30
Page 7 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 7 of 13 08.25.2016
Radiological Data for MCGUIRE
414447Sample #:Station:MCGUIRE
Collection End: 7/13/2016 12:20:00
Collection Start:7/13/2016 12:20:00Location:MW-4DR_ML1 [ MNS Landfill 1 / MW-4DR ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <5.36E+00 0.00E+00 5.36E+00 <300 LLD OK<15
Zn-65 <1.30E+01 0.00E+00 1.30E+01 <300 LLD OK<30
Zr-95 <7.63E+00 0.00E+00 7.63E+00 <400 LLD OK<15
Nb-95 <5.24E+00 0.00E+00 5.23E+00 <400 LLD OK<15
I-131 <5.53E+00 0.00E+00 5.53E+00 LLD OK<15
Cs-134 <7.54E+00 0.00E+00 7.54E+00 <30 LLD OK<15
Cs-137 <6.58E+00 0.00E+00 6.58E+00 <50 LLD OK<18
BaLa-140 <5.25E+00 0.00E+00 5.25E+00 <200 LLD OK<15
Be-7 <3.49E+01 0.00E+00 3.49E+01
K-40 <1.07E+02 0.00E+00 1.07E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-1.8E+01 0.00E+00 1.89E+02 <20000 LLD OK<250
414448Sample #:Station:MCGUIRE
Collection End: 7/13/2016 07:35:00
Collection Start:7/13/2016 07:35:00Location:MW-11_ML1 [ MNS Landfill 1 / MW-11 ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <2.00E-01 0.00E+00 7.54E-01 LLD OK<3
Beta <8.08E-02 0.00E+00 1.18E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.73E+00 0.00E+00 5.73E+00 <1000 LLD OK<15
Co-58 <3.50E+00 0.00E+00 3.50E+00 <1000 LLD OK<15
Fe-59 <1.09E+01 0.00E+00 1.09E+01 <400 LLD OK<30
Co-60 <4.53E+00 0.00E+00 4.53E+00 <300 LLD OK<15
Zn-65 <1.04E+01 0.00E+00 1.04E+01 <300 LLD OK<30
Zr-95 <8.03E+00 0.00E+00 8.03E+00 <400 LLD OK<15
Nb-95 <5.67E+00 0.00E+00 5.67E+00 <400 LLD OK<15
I-131 <5.76E+00 0.00E+00 5.76E+00 LLD OK<15
Cs-134 <6.85E+00 0.00E+00 6.85E+00 <30 LLD OK<15
Cs-137 <5.61E+00 0.00E+00 5.61E+00 <50 LLD OK<18
BaLa-140 <3.97E+00 0.00E+00 3.97E+00 <200 LLD OK<15
Page 8 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 8 of 13 08.25.2016
Radiological Data for MCGUIRE
414448Sample #:Station:MCGUIRE
Collection End: 7/13/2016 07:35:00
Collection Start:7/13/2016 07:35:00Location:MW-11_ML1 [ MNS Landfill 1 / MW-11 ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <3.88E+01 0.00E+00 3.88E+01
K-40 1.52E+02 6.67E+01 7.96E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-3.6E+01 0.00E+00 1.87E+02 <20000 LLD OK<250
414449Sample #:Station:MCGUIRE
Collection End: 7/13/2016 08:15:00
Collection Start:7/13/2016 08:15:00Location:MW-11D_ML1 [ MNS Landfill 1 / MW-11D ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <4.43E-02 0.00E+00 7.86E-01 LLD OK<3
Beta <-4.9E-01 0.00E+00 1.18E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.76E+00 0.00E+00 4.76E+00 <1000 LLD OK<15
Co-58 <4.86E+00 0.00E+00 4.86E+00 <1000 LLD OK<15
Fe-59 <1.11E+01 0.00E+00 1.11E+01 <400 LLD OK<30
Co-60 <7.44E+00 0.00E+00 7.44E+00 <300 LLD OK<15
Zn-65 <1.04E+01 0.00E+00 1.04E+01 <300 LLD OK<30
Zr-95 <8.96E+00 0.00E+00 8.96E+00 <400 LLD OK<15
Nb-95 <5.15E+00 0.00E+00 5.15E+00 <400 LLD OK<15
I-131 <8.37E+00 0.00E+00 8.37E+00 LLD OK<15
Cs-134 <6.18E+00 0.00E+00 6.18E+00 <30 LLD OK<15
Cs-137 <5.81E+00 0.00E+00 5.81E+00 <50 LLD OK<18
BaLa-140 <8.39E+00 0.00E+00 8.39E+00 <200 LLD OK<15
Be-7 <4.24E+01 0.00E+00 4.24E+01
K-40 1.06E+02 5.98E+01 7.83E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <7.92E+01 0.00E+00 1.87E+02 <20000 LLD OK<250
Page 9 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 9 of 13 08.25.2016
Radiological Data for MCGUIRE
414450Sample #:Station:MCGUIRE
Collection End: 7/13/2016 09:10:00
Collection Start:7/13/2016 09:10:00Location:MW-12_ML1 [ MNS Landfill 1 / MW-12 ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <2.37E-01 0.00E+00 7.64E-01 LLD OK<3
Beta 1.29E+00 7.40E-01 1.18E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.09E+00 0.00E+00 5.09E+00 <1000 LLD OK<15
Co-58 <3.65E+00 0.00E+00 3.65E+00 <1000 LLD OK<15
Fe-59 <1.22E+01 0.00E+00 1.22E+01 <400 LLD OK<30
Co-60 <6.38E+00 0.00E+00 6.38E+00 <300 LLD OK<15
Zn-65 <1.17E+01 0.00E+00 1.17E+01 <300 LLD OK<30
Zr-95 <1.03E+01 0.00E+00 1.03E+01 <400 LLD OK<15
Nb-95 <6.45E+00 0.00E+00 6.45E+00 <400 LLD OK<15
I-131 <4.32E+00 0.00E+00 4.32E+00 LLD OK<15
Cs-134 <7.08E+00 0.00E+00 7.08E+00 <30 LLD OK<15
Cs-137 <5.86E+00 0.00E+00 5.86E+00 <50 LLD OK<18
BaLa-140 <7.70E+00 0.00E+00 7.70E+00 <200 LLD OK<15
Be-7 <4.02E+01 0.00E+00 4.02E+01
K-40 9.72E+00 4.89E+01 8.88E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-7.6E+00 0.00E+00 1.96E+02 <20000 LLD OK<250
414451Sample #:Station:MCGUIRE
Collection End: 7/13/2016 09:55:00
Collection Start:7/13/2016 09:55:00Location:MW-12D_ML1 [ MNS Landfill 1 / MW-12D ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <1.99E-01 0.00E+00 9.44E-01 LLD OK<3
Beta <2.39E-01 0.00E+00 1.21E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <3.16E+00 0.00E+00 3.16E+00 <1000 LLD OK<15
Co-58 <2.91E+00 0.00E+00 2.91E+00 <1000 LLD OK<15
Fe-59 <5.31E+00 0.00E+00 5.31E+00 <400 LLD OK<30
Page 10 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 10 of 13 08.25.2016
Radiological Data for MCGUIRE
414451Sample #:Station:MCGUIRE
Collection End: 7/13/2016 09:55:00
Collection Start:7/13/2016 09:55:00Location:MW-12D_ML1 [ MNS Landfill 1 / MW-12D ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <3.22E+00 0.00E+00 3.22E+00 <300 LLD OK<15
Zn-65 <5.02E+00 0.00E+00 5.02E+00 <300 LLD OK<30
Zr-95 <4.90E+00 0.00E+00 4.90E+00 <400 LLD OK<15
Nb-95 <3.20E+00 0.00E+00 3.20E+00 <400 LLD OK<15
I-131 <4.13E+00 0.00E+00 4.13E+00 LLD OK<15
Cs-134 <3.08E+00 0.00E+00 3.08E+00 <30 LLD OK<15
Cs-137 <3.20E+00 0.00E+00 3.20E+00 <50 LLD OK<18
BaLa-140 <5.06E+00 0.00E+00 5.06E+00 <200 LLD OK<15
Be-7 <2.11E+01 0.00E+00 2.11E+01
K-40 7.05E+01 3.14E+01 4.19E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <1.44E+01 0.00E+00 1.87E+02 <20000 LLD OK<250
414452Sample #:Station:MCGUIRE
Collection End: 7/13/2016 12:55:00
Collection Start:7/13/2016 12:55:00Location:SW-1_ML1 [ MNS Landfill 1 / SW-1 ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-2.2E-01 0.00E+00 9.83E-01 LLD OK<3
Beta 1.80E+00 7.86E-01 1.23E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.71E+00 0.00E+00 4.71E+00 <1000 LLD OK<15
Co-58 <5.23E+00 0.00E+00 5.23E+00 <1000 LLD OK<15
Fe-59 <7.12E+00 0.00E+00 7.12E+00 <400 LLD OK<30
Co-60 <5.27E+00 0.00E+00 5.27E+00 <300 LLD OK<15
Zn-65 <1.00E+01 0.00E+00 1.00E+01 <300 LLD OK<30
Zr-95 <8.37E+00 0.00E+00 8.37E+00 <400 LLD OK<15
Nb-95 <5.02E+00 0.00E+00 5.02E+00 <400 LLD OK<15
I-131 <7.90E+00 0.00E+00 7.90E+00 LLD OK<15
Cs-134 <5.52E+00 0.00E+00 5.52E+00 <30 LLD OK<15
Cs-137 <4.99E+00 0.00E+00 4.99E+00 <50 LLD OK<18
BaLa-140 <7.49E+00 0.00E+00 7.49E+00 <200 LLD OK<15
Page 11 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 11 of 13 08.25.2016
Radiological Data for MCGUIRE
414452Sample #:Station:MCGUIRE
Collection End: 7/13/2016 12:55:00
Collection Start:7/13/2016 12:55:00Location:SW-1_ML1 [ MNS Landfill 1 / SW-1 ( LANDFILL ) ]
MNS_9JUN2016_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.70E+01 0.00E+00 4.70E+01
K-40 5.23E+01 4.29E+01 6.25E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA2 Sigma ErrorActivity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-5.3E+01 0.00E+00 1.89E+02 <20000 LLD OK<250
Page 12 of 12Report Generated @ 8/25/2016 12:01:41
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 12 of 13 08.25.2016
EnRad Laboratory Page 13 of 13 08.25.2016