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HomeMy WebLinkAboutUniversity Ford_Phase II_20160808 August 8, 2016 Mr. Peter McGrath Jr. Moore & Van Allen PLLC 100 North Tryon Street, Suite 4700 Charlotte, North Carolina 28202-4003 Subject: Report of Limited Phase II Environmental Site Assessment University Ford/Kia, 601Willard Street and 600 Julian Car Street Durham, North Carolina ASE Project No. 1272C Dear Mr. McGrath: Atlantic Shores Environmental Services, Ltd. (ASE) is pleased to provide you with the results of our Limited Phase II Environmental Site Assessment (ESA) for the referenced property. Our services were provided in general accordance with ASE Proposal No. 916-P, dated June 20, 2016. Included in this report is a description of the field activities, the results obtained, and our conclusions and recommendations. The activities and evaluative approaches used in this assessment are consistent with those normally employed in assessment and remediation projects of this type. Our evaluation of site conditions has been based on our understanding of the project information, limited sampling locations and the data obtained during our field activities. ASE appreciates the opportunity to provide our environmental consulting services to you on this project. If there are questions regarding this report, or a need for further information, please contact us at 910-371- 5980. Sincerely, ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. Cheryl J, Moody, REM Elliot Swain Principal Scientist Staff Scientist Attachments: Report Environmental Services, Ltd. LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT 601 WILLARD STREET AND 600 JULIAN CARR STREET DURHAM, NORTH CAROLINA ASE PROJECT NO. 1272C FOR MOORE & VAN ALLEN PLLC AUGUST 8, 2016 Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C i TABLE OF CONTENTS 1.0 BACKGROUND .............................................................................................. 1 2.0 FIELD ACTIVITIES ........................................................................................ 1 2.1 Ground Penetrating Radar Survey (GPR) 1 2.2 Environmental Sampling 1 2.3 Geotechnical Services 5 3.0 RESULTS ......................................................................................................... 5 3.1 Ground Penetrating Radar Survey (GPR) 5 3.2 Environmental Sampling 6 3.2.1 Soil 6 3.2.2 Groundwater 6 3.3 Geotechnical Services 7 4.0 CONCLUSIONS .............................................................................................. 7 5.0 RECOMMENDATIONS ................................................................................. 7 Appendices Appendix 1 - Figures Appendix 2 - Tables Appendix 3 - Soil Boring Logs/Well construction Records Appendix 4 - Laboratory Data Sheets Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C 1 1.0 BACKGROUND ASE performed a Phase I Environmental Site Assessment of the site dated May 26, 2016. As documented and qualified by this report, the assessment revealed the following evidence of on site recognized environmental conditions in connection with the property: • Potential former on site USTs; • Current and former RCRA status and exterior historic hazardous waste storage; • Potential presence of approximately 69 below grade hydraulic lifts. However, recent investigations suggest that there is likely 27 interior below grade hydraulic lifts total, with one (1) below grade hydraulic lift outside of the parts department. • Exterior waste oil AST staining; • Compressor blow down staining (two locations). • Off site concerns. The following evidence of offsite recognized environmental conditions or controlled recognized environmental conditions were identified in connection with the property: • The site has a land use restriction in conjunction with a former on site 1,000-gallon gasoline UST. • Durham Transit Station, W. Pettigrew St. This release is considered an off site controlled recognized environmental condition. 2.0 FIELD ACTIVITIES Field activities for this limited Phase II environmental Site Assessment included the following: 2.1 Ground Penetrating Radar Survey (GPR) • A ground penetrating radar survey (GPR) was conducted on the site to attempt to identify the location of the former USTs, if additional USTs are present, to attempt to locate the discharge location of the garage trench drain and to attempt to identify if an oil and water separator is associated with the maintenance and repair building. 2.2 Environmental Sampling • Twelve (12) soil borings were advanced on the site on June 23, 24, 27, 28, and 29, 2016 using CME45 and BK51 track-mounted drill rigs. Four (4) soil borings were advanced onsite on July 17, 2016 and July 24, 2016 using a Geoprobe model 7822DT. See Figure 2 for the approximate boring locations. CME45 and BK51 soil borings were advanced using hollow stem auger techniques. The CME45 drill rig is a trailer-mounted skid rig pulled behind a Ford F350 pickup truck. The BK51 is a track- mounted drill rig. During project boring activities, the CME45 and BK51 rigs utilized two and one quarter (2 ¼) inch hollow stem augers and four and one quarter (4 ¼) hollow stem augers to bore Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C 2 down to refusal depths. Bridger Drilling Enterprises, Inc., dba Carolina Drilling and Parrot Wolff Drilling were contracted for the drilling operations during this project. A Geoprobe model 7822DT was utilized for interior sampling using hollow stem augers and air hammer drilling techniques. Soil sampling was conducted down to 15 feet or refusal whichever was more shallow. Rock was encountered between 10 and 25 feet in these borings. Geotechnical soil samples were collected in conjunction with the environmental samples using two-foot split spoon samplers. The split spoons were driven down to a depth of 15 feet or refusal for the geotechnical sampling. The drillers logged the blow counts and collected the geotechnical samples. • Soil samples were collected and placed into plastic zip-lock bags to be screened with a photoionization detector (PID). • Following soil PID screening, soil samples were collected and screened for laboratory analysis as listed in Table 2. After being filled, the sample containers were labeled with the project name and number, the time and date of sample collection, the analyses to be performed, and the absence or presence of preservative. The filled sample containers were placed into an ice filled cooler to maintain the samples at approximately 4° Celsius. Sixteen (16) soil samples were submitted for volatile organic compound (VOC) analysis, semi-volatile organic compound (SVOC) analysis by EPA methods 8260 and 8270, respectively and for RCRA 8 metals by method 6010 ICP metals and 7471 Mercury. Four of the samples were also laboratory analyzed fro the presence of PCBs. • Permanent groundwater monitoring wells were installed in 14 of the 16 soil boring locations using hollow stem auger techniques. The wells were developed and purged before sampling. The groundwater samples were collected using a 36-inch plastic environmental bailer, monofilament nylon string and new disposable nitrile gloves. After being filled, the sample containers were labeled with the project name and number, the time and date of sample collection, the analyses to be performed, and the absence or presence of preservative. The filled sample containers were placed into an ice filled cooler to maintain the samples at approximately 4° Celsius. The groundwater samples were laboratory analyzed for VOC and SVOC by EPA methods 8260 and 8270 and for RCRA 8 metals by method 6010 ICP metals and 7471 Mercury. • The samples were given to a Pace Analytical Laboratory currier under chain of custody, where they were then driven to the Huntersville, North Carolina Pace Analytical Laboratory, for analysis. • Purge water and soil cutting from the borings/wells were collected on site in labeled 55-gallon drums. These drums remain on the site and await proper disposal. Boring logs, listing the soils observed and responses from the PID have been attached to this report. The following borings were advanced at the site: Boring B-1 (MW-1)– This boring was advanced approximately 50 feet north of the shipping and receiving area of the maintenance and repair building. The GPR survey identified a 15-foot by 10-foot anomaly in this area. This anomaly could have been a former UST location. This boring was advanced to approximately 25.5 feet below grade. Visual or olfactory impacts or indications of backfill were not apparent in the observed soils. One composite soil sample was taken from 2.5 feet to 6 feet below grade. This boring was completed as a monitoring well (MW-1) with an approximate depth of 25.3 feet. Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C 3 Boring B-2 (MW-2) – This boring was advanced along the north exterior side of the maintenance and repair building approximately five (5) feet west of the an air compressor (with apparent staining), a 1,750- gallon new oil AST and a 500-gallon transmission fluid AST. This boring was advanced to approximately 15 feet below grade. Visual or olfactory impacts were not apparent in the observed soils. One composite soil sample was taken from 1 to 2.5 feet below grade. This boring was completed as a monitoring well (MW-2) with an approximate depth of 14.9 feet. Boring B-3 (MW-3) – This boring was advanced on the southeast corner of the maintenance and repair shop, hydrologically down gradient from the former below grade hydraulic lifts located in the maintenance and repair building. This boring was advanced to approximately 20 feet below grade. Visual or olfactory impacts were not apparent in the observed soils. One composite soil sample was taken from 1 to 2.5 feet below grade. This boring was completed as a monitoring well (MW-3) with an approximate depth of 19.6 feet. Boring B-4 (MW-4) – This boring was advanced on the southern portion of the site within the inventory parking lot approximately 55 feet southwest of the University Ford showroom. The placement of this boring serves as a down gradient boring. This boring was advanced to approximately 22 feet below grade. Visual or olfactory impacts were not apparent in the observed soils. One composite soil sample was taken from 1 to 2.5 feet below grade. This boring was completed as a monitoring well (MW-3) with an approximate depth of 20.5 feet. Boring B-5 (MW-5) – This boring was advanced on the western portion of the site approximately 50 feet west of the University Kia building. The placement of this boring serves as a downgradient boring. This boring was advanced to approximately 21 feet below grade. Visual and olfactory impacts were not apparent in the observed soils. One composite soil sample was taken from 4 to 6 feet below grade. This boring was completed as a monitoring well (MW-5) with an approximate depth of 21.0 feet. Boring B6 (MW-6) – This boring was advanced south of the maintenance and repair building. The GPR identified an approximate 15-foot by 10-foot area that could have been a former UST in this area. This boring was advanced to approximately 20 feet below grade. Fill material and debris were observed from one to five feet below grade. Visual or olfactory impacts were not apparent in the observed soils. One composite soil sample was taken from 3.5 to 7 feet below grade. This boring was completed as a monitoring well (MW-6) with an approximate depth of 19.7 feet. Boring B7 (MW-7) – This boring was advanced inside of the maintenance and repair building, approximately two feet southwest of the trench drain outflow pipe. This boring was advanced to approximately 18 feet below grade and serves as a down gradient sampling location. Visual and olfactory impacts were not apparent in the observed soils. One composite soil sample was taken from 2 to 4 feet below grade. This boring was completed as a monitoring well (MW-7) with an approximate depth of 18 feet. Boring B8 (MW-8) – This boring was advanced approximately four (4) feet south of the University Ford maintenance and repair building waste oil AST. This boring was advanced approximately 15 feet below grade. Olfactory impacts were not apparent in the observed soils. However, oil staining was observed on the asphalt. One composite soil sample was taken from 4 to 6 feet below grade. This boring was completed as a monitoring well (MW-8) with an approximate depth of 14 feet. Boring B9 (MW-9) – This boring was advanced on the north side of the maintenance and repair building within the fifth bay from the east of the building. This boring was advanced approximately two feet south Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C 4 of a former below grade hydraulic lift. The boring was advanced to approximately 18.5 feet below grade. Visual and olfactory impacts were not apparent in the observed soils. One composite soil sample was taken from 2 to 4 feet below grade. This boring was completed as a monitoring well (MW-9) with an approximate depth of 18.5 feet. Due to slow recharge, the volume available for sampling from this well was limited. VOC and SVOC samples were not collected. This monitoring well was only sampled for RCRA 8 metals. Boring B10 (MW-10) – This boring was advanced on the southeast portion of the auto body building in south of the paint booth portion of the building. The placement of this boring serves as a down gradient boring for the body shop. This boring was advanced approximately 14 feet below grade. Visual and olfactory impacts were not apparent in the observed soils. One composite sample was taken from 3.5 to 5 feet below grade. This boring was completed as a monitoring well (MW-10) with an approximate depth of 14 feet. Boring B11 (MW-11) – This boring was advanced in the south side of the auto body shop within the seventh bay from the east end of the auto body building. The boring was advanced approximately 1 foot south of a former below grade hydraulic lift for this bay. The boring was advanced to approximately 21.5 feet below grade. Water was present in this boring from just under the concrete to approximately 10 feet (rock surface). The unconsolidated soils above 10 feet were saturated. According to University Ford personnel, previous coring activities in this area to install equipment ruptured a water line. ASE believes that the observed water is a result of this former water loss. Visual and olfactory impacts were observed within the top 6 feet of soil. The odor observed appeared to smell slightly similar to antifreeze. Visually the soils appeared to be greasy. One composite sample was taken from 0 to 4 feet below grade. This boring was completed as a monitoring well (MW-11) with an approximate depth of 21.5 feet. This monitoring well was not sampled due to the absence of groundwater at the time of sampling. Boring B12 – This boring was advanced north of the maintenance and repair building centrally along the building. The GPR survey identified a 20-foot by 10-foot area that may have been a former UST location. This boring was advanced to approximately 10 feet below grade. Visual and olfactory impacts were not apparent in the observed soils. One composite sample was taken from 1 to 2.5 feet below grade. This boring was not completed as a monitoring well. Boring B13 (MW-13) – This boring was advanced within the detailing shop in the auto body building. The boring was advanced southeast of a former below grade hydraulic lift. This boring was advanced to approximately 20 feet below grade. Visual and olfactory impacts were not apparent in the observed soils. One composite sample was taken from 0 to 2 feet below grade. This boring was completed as a monitoring well (MW-13) with a total depth of 19.3 feet. Boring B14 (MW-14) – This boring was advanced along the north exterior side of the paint and auto body building between the compressor and former hazardous waste storage area. This boring was advanced to approximately 21 feet below grade. Visual and olfactory impacts were not apparent in the observed soils. One composite sample was taken from 2.5 to 3.5 feet below grade. This boring was completed as a monitoring well (MW-14) with an approximate depth of 20.7 feet. Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C 5 Boring B15 (MW-15) – This boring was advanced approximately 5 feet west of the southwest portion of the maintenance and repair building. ASE observed stained pavement in this area that appears to originate from the interior waste oil storage area. This boring was advanced to approximately 20 feet below grade. Visual and olfactory impacts were observed in the sampled soils. One composite sample was taken from 3.5 to 6.5 feet below grade. This boring was completed as a monitoring well (MW-15) with an approximate depth of 18.7 feet. Boring B16 – This boring was advanced approximately 10 feet north of the University Kia showroom building. The GPR survey of the area, suggests that this area could be a former UST location. This boring was advanced to approximately 7.5 feet below grade. Visual and olfactory impacts were not apparent in the observed soils. One composite sample was taken from 1 to 2.5 feet below grade. This boring was not completed as a monitoring well. 2.3 Geotechnical Services Four (4) additional soil borings were advanced on the site on June 29, 2016 using BK51 track-mounted drill rig. Geotechnical soil samples were collected using two-foot split spoon samplers. The split spoons were driven down to a depth of 15 feet or refusal for the geotechnical sampling. The drillers logged the blow counts and collected the geotechnical samples. Boring Falcon B17 – This boring was advanced on the northern portion of the site. ASE did not collect soil samples from this boring. However, soils collected for geotechnical purposes were screened in the field using a PID. Neither visual, olfactory nor positive PID readings suggesting impacts were observed from this boring. This boring was advanced to approximately 6 feet below grade. Boring Falcon B18 – This boring was advanced on the northeastern portion of the site. ASE did not collect soil samples from this boring. However, soils collected for geotechnical purposes were screened in the field using a PID. Neither visual, olfactory nor positive PID readings suggesting impacts were observed from this boring. This boring was advanced to approximately 3.5 feet below grade. Boring Falcon B19 – This boring was advanced on the northwestern portion of the site. ASE did not collect soil samples from this boring. However, soils collected for geotechnical purposes were screened in the field using a PID. Neither visual, olfactory nor positive PID readings suggesting impacts were observed from this boring. This boring was to advanced approximately 17 feet below grade. Boring Falcon B20 – This boring was advanced on the southern portion of the site. ASE did not collect soil samples from this boring. However, soils collected for geotechnical purposes were screened in the field using a PID. Neither visual, olfactory nor positive PID readings suggesting impacts were observed from this boring. This boring was advanced to approximately 17.5 feet below grade. 3.0 RESULTS 3.1 Ground Penetrating Radar Survey (GPR) Geo Solutions completed a geophysical survey of the site utilizing two types of non-invasive geophysical surveys: Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C 6 1. A GEM2 Multifrequency electromagnetic profiler (EM) was utilized to survey throughout accessible areas of the site to locate potential buried features. 2. A Model 3000 GSSI ground-penetrating radar (GPR) equipped with a 400 MHz antenna was utilized to survey around the onsite buildings and over the targets identified in the EM survey. As part of this survey, a plumber was engaged to attempt to identify the discharge location of the trench drain located in the repair garage. The drain has reportedly not drained for many years. ASE contracted Noble Oil to clean out the trench drain prior to attempting to clear the apparent blockage in the discharge pipe. The trench drain was drained and pressure washed. According to Noble Oil, 576 gallons of wastewater and 220 gallons of non-hazardous solid waster were removed and disposed of. The plumber was able to trace the discharge line within the building approximately 40 feet from the drain but attempts to follow the line further were not successful. However, it appears that the plumber was successful in clearing the line. The plumber indicated that water now appears to drain from the trench drain. GPR was used to attempt to pick up the discharge line at the location the plumber stopped. However, due to the presence of significant rebar in the concrete floor, the pipe was not located. The ultimate discharge location of this trench drain is still undetermined. The GPR survey identified four areas on the site that could suggest the possible location of former USTs as discussed in section 2.0. Refer to Figures 2 and 3 for the findings of the GPR survey. Borings B-1, B-6, B-12 and B-16 were placed to evaluate these areas. Indications of former tanks at the locations of these anomalies were not identified during the boring activities. 3.2 Environmental Sampling 3.2.1 Soil Target VOCs and SVOCs were not identified in the soil samples submitted to the laboratory above State criteria with the exception of the presence of poly aromatic hydrocarbons (PAHs) in soil sample B-5. Benzo(a)anthracecne, benzo(b)fluoranthene, and benzo(a)pyrene were identified above Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals; residential and/or protection of groundwater standards. It should be noted that trace concentrations of chlorinated solvents and their breakdown products were identified in the soil samples collected from B-8, B-10, B-13, B-15 and B-16. Target metals were not identified in the soil samples submitted to the laboratory above State criteria with the exception of the presence of arsenic. Arsenic was identified in all soil samples (with the exception of B-6) above the Preliminary Soil Remediation Goals residential and/or protection of groundwater standards. A summary of soil data is presented in Tables 1 and 2. Copies of the lab data sheets have also been attached to this report. 3.2.2 Groundwater Target analyte concentrations above the 2L drinking water standards were not identified in the groundwater samples with the exception of the following: • MW-1 – Chromium Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C 7 • MW-2 – Chromium • MW-3 – Chromium • MW-6 – Arsenic, Barium, Chromium and Lead. • MW-14 – Chromium • MW-15 – Naphthalene, Chromium However, it should be noted that trace amounts of perchloroethene and trichloroethene were identified in MW-1 and MW-15, respectively. It also should be noted that samples MW-2, MW-3, MW-6, and MW-15 were relatively turbid samples. A summary of the water data is presented in Table 3. Copies of the lab data sheets have also been attached to this report. 3.3 Geotechnical Services Falcon Engineering was contracted to conduct and engineering evaluation of the site soils. The results of these services have been provided in a separate report issued by Falcon Engineering. 4.0 CONCLUSIONS Based on the field observations and laboratory data collected during this investigation, some impacts to the site have been identified. Soil samples across the site exhibit elevated arsenic concentrations above the Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals residential and/or protection of groundwater standards. In addition, benzo(a)anthracecne, benzo(b)fluoranthene, and benzo(a)pyrene, were identified in the soil above residential and/or protection of groundwater standards in B-5. It should be noted that trace concentrations of chlorinated solvents and their breakdown products were identified in the soil samples collected from B-8, B-10, B-13, B-15 and B-16. Chromium concentrations above 2L standards were identified in 10 of the 13 sampled monitoring wells. Arsenic, barium and lead were also identified above 2L standards in MW-6. Naphthalene was identified above 2L standards in B15. B15 is located adjacent to the waste oil AST. It should be noted that trace amounts of perchloroethene and trichloroethene were identified in MW-1 and MW-15, respectively. These are shallow wells (25.3 feet and 18.7 feet deep respectively.) MW-1 is located directly downgradient of the body shop mixing room and MW-15 is adjacent to the waste storage area at the repair facility. It should be noted that of the 13 groundwater samples, elevated turbidity was observed in samples taken from MW-2, MW-3, MW-6 and MW-15. Due to the elevated turbidity in these samples, erroneously high metal concentrations are possible. The identified impacts to the site trigger a NCDEQ reporting requirement for the owner. 5.0 RECOMMENDATIONS ASE recommends submitting this report to the North Carolina Department of Environmental Quality (NCDEQ) Brownfield Program for evaluation under the pending Brownfield Agreement. Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C FIGURES FIGURE 1: SITE LOCATION MAP N Approximate Scale: Contour Interval = 10 ft. Source: USGS Southwest Durham, North Carolina Quadrangle, 1987. ASE Project No. 1272C August 2016 SITE 0 900 ft. Phase II Environmental Site Assessment 601 Willard and 600 Julian Carr Street Durham, Durham County, North Carolina feet meters 1000 400 FIGURE 2: Boring Locations N Approximate Scale: Not to Scale Source: Google Earth 2013 Aerial Photograph ASE Project No. 1272C August 2016 Phase II Environmental Site Assessment 601 Willard and 600 Julian Carr Street Durham, Durham County, North Carolina Key: - Existing monitoring wells - ASE Boring locations B1 B4 B3 B5 B6 B2 B7 B8 B9 B12 B13 B11 B14 B10 B15 B16 Falcon B18 Falcon B17 Falcon B19 Falcon B20 - Geotechnical borings Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C TABLES Boring B-1 B-2 B-3 B-4 B-5 Depth 2.5-6.0 1-2.5'1-2.5'2.5-3.5'4-6' Date 06/24/16 06/28/16 06/29/16 06/23/16 06/27/16 Arsenic 1.2 2.5 3.2J 1.2 3.2 0.68 5.8 Barium 126 106 152 119 111 3,000 580 Cadmium <0.043 <0.043 <0.043 <0.043 0.14 14.2 3.0 Chromium 19.4 11.7 39.5 32.2 16.7 24,000 360,000 Lead 8.6 7.5 26.6 4.1 99.6 400 270 Selenium 1.2 0.50J <0.043 1.1 1.7 78 2.1 Mercury .00035J 0.00041J <0.00011 0.0016J 0.05 2.2 1 Boring B-6 B-7 B-8 B-9 B-10 Depth 3.5-7'2-4'4-6'2-4'3.5-5' Date 06/29/16 07/17/16 06/27/16 07/17/16 06/28/16 Arsenic 0.55J 1.7 3.1J 1.8 1.5 0.68 5.8 Barium 27.1 53.9 227.0 71.5 158 3,000 580 Cadmium <0.043 <0.043 <0.043 <0.043 <0.043 14.2 3.0 Chromium 5.5 12.4 25.0 19.3 13.0 24,000 360,000 Lead 6.6 13.2 11.1 6.2 8.1 400 270 Selenium <0.75 0.99 <4.9 0.79 0.58J 78 2.1 Mercury <0.00011 0.0087 .0023J 0.00028J <0.0054 2.2 1 Boring B-11 B-12 B-13 B-14 B-15 B-16 Depth 0-4'1-2.5'0-2'2.5-3.5-3.5-6.5'1-2.5' Date 07/24/16 06/29/16 07/24/16 06/24/16 6/27/16 6/28/16 Arsenic 6.70 2.10 6.30 1.60 1.40 4.6J 0.68 5.8 Barium 76.70 89.90 176.00 78.30 42.4 148.0 3,000 580 Cadmium <0.043 <0.043 <0.043 <0.043 <0.043 <0.043 3.0 3.0 Chromium 10.60 12.40 30.40 12.70 8.1 21.0 24,000 360,000 Lead 6.80 1.90 12.00 9.90 19.5 21.2 400 270 Selenium <0.043 0.59J <0.043 1.20 0.92 <0.043 78 2.1 Mercury .0018J <0.0055 .0010J 0.00041J 0.047 0.011 2.2 1 * - April 2016 Bold = exceedance of Residential Criteria (Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals) Results are in mg/kg J values represent estimated concentration above adjusted method detection limit and below the adjusted reporting limit. PSRG (Res)* (mg/kg) PSRG (GW)* (mg/kg) Shading =exceedance of Protection of GW criteria Table 2 -Metal Soil Sample Analytical Results 600 Julian Carr Street, Durhan, NC PSRG (Res)* (mg/kg) PSRG (GW)* (mg/kg) PSRG (Res)* (mg/kg) PSRG (GW)* (mg/kg) Boring B-1 B-2 B-3 B-4 B-5 B-6 B-7 B-8 Depth 2.5-6'1-2.5'1-2.5'1-2.5'4-6'3.5-7'2-4'4-6' Date 06/24/16 06/28/16 06/29/16 06/23/16 06/27/16 06/29/16 07/17/16 06/27/16 Acetone <11.7 12.6J <11.7 19.2J <11.7 62.0J 28.1J 72.4J 1.22E+07 1.0E+04 2-Butanone (MEK)<3.4 <3.4 <3.4 <3.4 <3.4 13.0J <3.4 <3.4 5.40E+06 1.6E+04 cis-1,2-Dichloroethene <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 NE NE Methyl-Tert-Butyl-Ether (MBTE)<1.8 <1.8 <1.8 <1.8 <1.8 <1.8 20.90 <1.8 4.7E+04 850.0 Methylene Chloride <3.5 <3.5 <3.5 <3.5 <3.5 <3.5 <3.5 2.9J 5.7E+04 2.3E+05 Naphthalene <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 2.7J 3.8E+03 210 Ethylbenzene <2.1 <2.1 <2.1 <2.1 <2.1 <2.1 <2.1 2.7J 5.8E+03 8.1E+03 Toluene <2.1 <2.1 <2.1 <2.1 <2.1 <2.1 <2.1 <2.1 8.19E+05 5.5E+03 Trichloroethene <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 NE NE1,2,4-Trimethylbenzene <2.3 <2.3 <2.3 <2.3 <2.3 <2.3 <2.3 5.7 1.16E+04 670.0m&p-Xylene <4.2 <4.2 <4.2 <4.2 <4.2 <4.2 <4.2 <4.2 1.16E+05 6.0E+03 Benzo(a)anthracene <72.6 <72.6 <72.6 <72.6 281J <72.6 <72.6 <72.6 160.00 180.00 Benzo(b)fluoranthene <67.9 <67.9 <67.9 <67.9 342J <67.9 <67.9 <67.9 160.00 600.00 Benzo(k)fluoranthene <77.4 <77.4 <77.4 <77.4 127J <77.4 <77.4 <77.4 1.60E+03 5.9E+03 Benzo(a)pyrene <75.0 <75.0 <75.0 <75.0 250J <75.0 <75.0 <75.0 16.00 59.00 Benzo(g,h,i)perylene <100 <100 <100 <100 158J <100 <100 <100 NE 7.8E+06 Chrysene <52.4 <52.4 <52.4 <52.4 272J <52.4 <52.4 <52.4 1.6E+04 NEFluoranthene<57.2 <57.2 <57.2 <57.2 683 <57.2 94.2J <57.2 4.80E+05 3.3E+05Indeno(1,2,3-cd)pyrene <81.0 <81.0 <81.0 <81.0 143J <81.0 <81.0 <81.0 160 2.0E+03Phenanthrene<65.5 <65.5 <65.5 <65.5 393J <65.5 <65.5 <65.5 NE 6.8E+04 Pyrene <66.7 <66.7 <66.7 <66.7 464 <66.7 70.9J <66.7 3.6E+04 2.2E+05 1-Methylnaphthalene <102 <102 <102 <102 <102 <102 <102 <102 1.8E+04 55 2-Methylnaphthalene <84.6 <84.6 <84.6 <84.6 <84.6 <84.6 <84.6 <84.6 4.8E+04 160 Boring B-9 B-10 B-11 B-12 B-13 B-14 B-15 B-16Depth2-4'3.5-5'0-4'1-2.5'0-2'2.5-3.5 3.5-6.5'1-2.5' Date 07/17/16 06/28/16 07/24/16 06/29/16 07/24/16 06/24/16 6/27/16 6/28/16 Acetone 61.4J 27.7J 39.1J 20.1J <11.7 19.7J 23.6J 30.5J 1.22E+07 1.0E+04 2-Butanone (MEK)<3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 5.40E+06 1.6E+04 cis-1,2-Dichloroethene <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 1.4J <1.6 NE NE Methyl-Tert-Butyl-Ether (MBTE)2.9J <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 4.7E+04 850.0Methylene Chloride <3.5 6.5J <3.5 <3.5 7.2J <3.5 <3.5 3.7J 5.7E+04 2.3E+05Naphthalene<1.4 <1.4 1.1J <1.4 <1.4 <1.4 1.2J <1.4 3.8E+03 210Ethylbenzene<2.1 <2.1 <2.1 <2.1 <2.1 <2.1 <2.1 <2.1 5.8E+03 8.1E+03Toluene<2.1 <2.1 3.8J <2.1 <2.1 <2.1 <2.1 <2.1 8.19E+05 5.5E+03 Trichloroethene <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 2.8J <2.5 NE NE 1,2,4-Trimethylbenzene <2.3 <2.3 2.0J <2.3 <2.3 <2.3 <2.3 <2.3 1.16E+04 670.0 m&p-Xylene <4.2 <4.2 3.9J <4.2 <4.2 <4.2 <4.2 <4.2 1.16E+05 6.0E+03 Benzo(a)anthracene <72.6 <72.6 <72.6 <72.6 <72.6 <72.6 78.8J <72.6 160.00 180.00 Benzo(b)fluoranthene <67.9 <67.9 <67.9 <67.9 <67.9 <67.9 98.3J <67.9 160.00 600.00Benzo(k)fluoranthene <77.4 <77.4 <77.4 <77.4 <77.4 <77.4 <77.4 <77.4 1,600.00 5,900.00Benzo(a)pyrene <75.0 <75.0 <75.0 <75.0 <75.0 <75.0 <75.0 <75.0 16.00 5.90Benzo(g,h,i)perylene <100 <100 <100 <100 <100 <100 <100 <100 NE 7.8E+06 Chrysene <52.4 <52.4 <52.4 <52.4 <52.4 <52.4 77.3J <52.4 1.6E+04 NE Fluoranthene <57.2 <57.2 <57.2 <57.2 <57.2 <57.2 215J <57.2 480 330 Indeno(1,2,3-cd)pyrene <81.0 <81.0 <81.0 <81.0 <81.0 <81.0 <81.0 <81.0 160 2.0E+03 Phenanthrene <65.5 <65.5 <65.5 <65.5 <65.5 <65.5 147J <65.5 NE 6.8E+04 Pyrene <66.7 <66.7 <66.7 <66.7 <66.7 <66.7 132J <66.7 3.6E+04 2.2E+05 1-Methylnaphthalene <102 <102 <102 <102 <102 <102 <102 <102 1.8E+04 55 2-Methylnaphthalene <84.6 <84.6 <84.6 <84.6 <84.6 <84.6 122J <84.6 4.8E+04 160 * - April 2016 Bold = exceedance of Residential Criteria (Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals) NE = Not Established J values represent estimated concentratino above adjusted method detection limit and below the adjusted reporting limit. PSRG (Res)* (µg/Kg) PSRG (GW)* (µg/Kg) 8260 (ug/kg) 8270 (ug/kg) Shading =exceedance of Protection of GW criteria 8270 (ug/kg) Table 1 -VOC/SVOC Soil Sample Analytical Results600 Julian Carr Street, Durhan, NC PSRG (Res)* (µg/Kg) PSRG (GW)* (µg/Kg) 8260 (ug/kg) MW-1 MW-2 MW-3 MW-4 MW-5 2L Date Sampled 07/11/16 07/11/16 07/11/16 07/11/16 07/11/16 µg/L Acetone <10.0 <10.0 <10.0 <10.0 27.1 6,000 cis-1,2-Dichloroethene <0.19 <0.19 <0.19 <0.19 <0.19 70 Tetrachloroethene 0.54J <0.46 <0.46 <0.46 <0.46 0.7 Diisopropyl ether <0.12 <0.12 <0.12 <0.12 <0.12 70 Ethylbenzene <0.30 <0.30 <0.30 <0.30 <0.30 600 Trichloroethene <0.47 <0.47 <0.47 <0.47 <0.47 3Xylene (total)<0.66 <0.66 <0.66 <0.66 <0.66 500m&p-Xylene <0.66 <0.66 <0.66 <0.66 <0.66 500o-Xylene <0.23 <0.23 <0.23 <0.23 <0.23 NE4-Methyl-2-pentanone (MIBK)<0.33 <0.33 <0.33 <0.33 <0.33 NEMethyl-Tert-Butyl-Ether <0.21 <0.21 0.22J <0.21 <0.21 20Naphthalene<0.24 <0.24 <0.24 <0.24 0.7J 6p-Isopropyltoluene <0.31 <0.31 <0.31 <0.31 10.3 NE 1-Methylnaphthalene <0.32 <0.32 <0.32 <0.32 <0.32 NE2-Methylnaphthalene <0.28 <0.28 <0.28 <0.28 <0.28 30Acenaphthene<0.25 <0.25 <0.25 <0.25 1.8J NE Phenanthrene <0.22 <0.22 <0.22 <0.22 1.1J 200 Arsenic <5.0 <5.0 <5.0 <5.0 <5.0 10 Barium 328 266 356 131 337 700 Chromium 33.4 33.6 39.1 <2.5 3.2J 10 Lead 7.7 8.4 10.9 <2.5 4.1J 15 Mercury <0.1 <0.1 <0.1 <0.1 <0.1 1 MW-6 MW-7 MW-8 MW-9 MW-10 2L Date Sampled 07/11/16 07/25/16 07/11/16 07/25/16 07/11/16 µg/L Acetone <10.0 <10.0 <10.0 Not Analyzed 11.4J 6,000 cis-1,2-Dichloroethene <0.19 <0.19 <0.19 Not Analyzed <0.19 70 Tetrachloroethene <0.46 <0.46 <0.46 Not Analyzed <0.46 0.7 Diisopropyl ether <0.12 <0.12 <0.12 Not Analyzed <0.12 70 Ethylbenzene <0.30 <0.30 <0.30 Not Analyzed <0.30 600 Trichloroethene <0.47 <0.47 <0.47 Not Analyzed <0.47 3 Xylene (total)<0.66 <0.66 <0.66 Not Analyzed <0.66 500 m&p-Xylene <0.66 <0.66 <0.66 Not Analyzed <0.66 500 o-Xylene <0.23 <0.23 <0.23 Not Analyzed <0.23 NE 4-Methyl-2-pentanone (MIBK)<0.33 <0.33 0.86J Not Analyzed <0.33 NE Methyl-Tert-Butyl-Ether <0.21 12.8 5.8 Not Analyzed <0.21 20 Naphthalene <0.24 <0.24 <0.24 Not Analyzed <0.24 6 p-Isopropyltoluene <0.31 <0.31 <0.31 Not Analyzed <0.31 25* 1-Methylnaphthalene <0.32 <0.32 <0.32 Not Analyzed <0.32 NE 2-Methylnaphthalene <0.28 <0.28 <0.28 Not Analyzed <0.28 30Acenapthene<0.25 <0.25 <0.25 Not Analyzed <0.25 NEPhenanthrene<0.22 <0.22 <0.22 Not Analyzed <0.22 200 Arsenic 36.5 <5.0 <5.0 <5.0 <5.0 10 Barium 1190 226 83.9 271 182 700 Chromium 180 <2.5 <2.5 9.6 9.1 10 Lead 382 <2.5 <2.5 <2.5 3.4J 15 Mercury 0.4 <0.1 <0.1 <0.1 <0.1 1 MW-11 MW-12 MW-13 MW-14 MW-15 2LDate Sampled Not Sampled Not installed 07/25/16 07/11/16 07/11/16 µg/L Acetone NA NA <10.0 <10.0 <10.0 6,000cis-1,2-Dichloroethene NA NA <0.19 <0.19 2.6 70TetrachloroetheneNANA<0.46 <0.46 <0.46 3.0Diisopropyl ether NA NA <0.12 <0.12 0.21J 70EthylbenzeneNANA<0.30 <0.30 0.34J 600TrichloroetheneNANA<0.47 <0.47 1.6 3Xylene (total)NA NA <0.23 <0.23 3.0 500 m&p-Xylene NA NA <0.66 <0.66 1.1J 500 o-Xylene NA NA <0.23 <0.23 3.0 NE 4-Methyl-2-pentanone (MIBK)NA NA <0.33 <0.33 1.8J NE Methyl-Tert-Butyl-Ether NA NA <0.21 <0.21 0.47J 20 Naphthalene NA NA <0.24 <0.24 7.1 6 p-Isopropyltoluene NA NA <0.31 <0.31 1.5 NE 1-Methylnaphthalene NA NA <0.32 <0.32 10.1 NE2-Methylnaphthalene NA NA <0.28 <0.28 2.9J 30AcenaptheneNANA<0.25 <0.25 <0.25 NEPhenanthreneNANA<0.22 <0.22 <0.22 200 Arsenic NA NA <5.0 <5.0 <5.0 10 Barium NA NA 191 255 189 700 Chromium NA NA <2.5 21.1 15.4 10 Lead NA NA <2.5 6.1 14.7 15 Mercury NA NA <0.1 <0.1 <0.1 1 2L = NCAC Title 15A Subchapeter 2L 4/13 Interim Maximum Allowable Concentration (IMAC)Bold data represent guidance criteria excedance. NE - Not EstablishedJ values represent estimated concentration above adjusted method detection limit and below the adjusted reporting limit. 8270 (µg/L) Metals(mg/L) 8260 (µg/L) 8270 (µg/L) Metals(mg/L) Table 3 - Groundwater Sample Analytical Results 600 Julian Carr Street, Durham North Carolina 8260 (µg/L) 8270 (µg/L) Metals(mg/L) 8260 (µg/L) Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C SOIL BORING LOGS/WELL LOGS ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451 910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B1 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -- 18 Brownish Red silty clay with light gray streaking 0.4 -- 18 Light gray silty clay 0.5 -3 - -- -5 - -12 Brownish red silt with weathered rock 0.0 - -- 12 Brownish red silt with weathered rock 0.0 -8 - -18 Brownish red silt with weathered rock 0.0 - -10 - -- -- -13 - -- -15 - -- -17 - -- -- -20 - -- -- -- -- -25 Bottom of boring - NOTES: Finished as permanent well 06/24/16 06/24/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe RoadLeland, NC 28451 910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B2 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -18 Dark brown silty clay with rocks 0.7 - -- -3 - 6 Dark brown silty clay with rock 0.5 -- -5 - -18 Brownish green silty clay 0.5 - -- -8 - -18 Brownish green weathered rock 1.0 - -10 - -- -- -13 - 18 Brownish green weathered rock 0.2 -- -15 Bottom of boring - -- -17 - -- -- -20 - -- -- -- -- -25 - NOTES: Finished as permanent well 06/28/16 06/28/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B3 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -18 Brownish red silt 1.0 - -- -3 - 18 Brownish red silt 2.2 -- -5 - -18 Brownish gray sand 1.8 - -- -8 - -18 Gray with orange mottle with rock 1.5 - -10 - -- -- -13 - 18 Brownish red silt with weathered rock 1.5 -- -15 - -- -17 - -- -- -20 Bottom of boring - -- -- -- -- -25 - NOTES: Finished as permanent well 06/29/16 06/29/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451 910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B4 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -18 Brownish red silty clay 0.0 - -- -3 - 18 Brownish red clay 0.0 -- -5 - -18 Brownish red silty clay 0.0 - -- -8 - -18 Brownish orange clay with gray streaking 0.0 - -10 - -- -- -13 - 18 Brownish red silt with weathered rock 0.0 -- -15 - -18 Brownish red silt with rock 0.0 - -17 - -- -- -20 18 Light brown silt with weathered rock 0.0 - -- -- -- -- -25 Bottom of boring - NOTES: Finished as permanent well 06/23/16 06/23/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451 910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B5 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -18 Brick and sand fill with clay 0.4 - -- -3 - 18 Brick and sand fill with clay 0.9 -1.9 - -5 - -18 Brownish clay 0.4 - -- -8 - -18 Dark brown clay 1.6 - -10 - -- -- -13 - 18 Light and dark brown clay 1.6 -- -15 - -- -17 Weathered rock and stone 0.2 - -- -- -20 Bottom of boring - -- -- -- -- -25 - NOTES: Finished as permanent well 06/27/16 06/27/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451 910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B6 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -12 Brownish red clay with orange streak 0.1 - -- -3 - 6 Fill material (brick and wood)5.0 -- -5 - -18 Brown sandy clay 0.0 - -- -8 - -18 Gray clay with yellow streaking 0.0 - -10 - -- -- -13 - 18 Brownish red silt with rock 2.0 -- -15 - -- -17 - -- -Bottom of boring - -20 - -- -- -- -- -25 - NOTES: Finished as permanent well 06/29/16 06/29/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451 910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B7 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS: Hollow Stem Auger and Air Hammer DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -- -24 Brown silty clay 0.0 - -3 - -24 Brown silty clay 0.0 - -5 - -24 Brick and asphalt observed 1.0 - -- -8 4 Weathered sand stone 0.0 - -- -10 Air hammer to 18 0.0 - -- -- -13 - -- -15 - -- -17 - -Bottom of boring - -- -20 - -- -- -- -- -25 - NOTES: Finished as permanent well 07/17/16 07/17/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451 910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B8 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -Grayish green silty clay 2.4 - 1.5 -Olive to red mottled silty clay - -3 - Olive to red mottled silty clay -- -5 - -Brownish red clay with mica and gravel 1.7 - -- Dark Brownish red clay -8 - -- -10 - -- -- -13 - -- -15 Bottom of boring - -- -17 - -- -- -20 - -- -- -- -- -25 - NOTES: Finished as permanent well 06/27/16 06/27/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451 910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B9 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS: Hollow Stem Auger/Air Hammer DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -Concrete - -12 Brown Silty Clay 0.0 - -3 - -18 Brown Silt with trace clay and green layers 0.9 - -5 - -20 Brown Silt with trace clay and green layers 1.2 - -- -8 20 Brown Silt with trace clay and green layers. Begin Air 0.6 - Hammer to 18.5. -- -10 - -- -- -13 - -- -15 - -- -17 - -- Bottom of boring -- -20 - -- -- -- -- -25 - NOTES: Finished as permanent well 07/17/16 07/17/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B10 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -18 Brown sandy silt with gravel and trace of clay 0.4 - -- -3 - 18 Brownish red silt 0.5 -- -5 - -18 Brownish red silt with weathered rock with gravel 0.3 - -- -8 - -18 Brownish green weathered rock 0.5 - -10 - -- -- -13 - 18 Rock with silt 1.5 -Bottom of boring - -15 - -- -17 - -- -- -20 - -- -- -- -- -25 - NOTES: Finished as permanent well 06/28/16 06/28/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451 910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B11 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS: Hollow Stem Auger/Air Hammer DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -- -4 Dark brown silty clay 3.5 - -3 - -4 Dark brown silty clay 1.1 - -5 - -24 Dark brown silty clay 2.2 - -- -8 24 Dark brown silty clay rock at 8. Begin air hammer 0.4 - -- -10 - -- -- -13 - -- -15 - -- -17 - -- -- -20 - -Bottom of boring - -- -- -- -25 - NOTES: Finished as permanent well 07/24/16 07/24/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B12 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -18 Grayish brown loam 0.5 - -- -3 - 18 brownish orange clayey loam 0.5 -- -5 - -18 Brownish red silt 0.5 - -- -8 - -18 brownish red silt with pebbles 0.0 - -10 Bottom of boring - -- -- -13 - -- -15 - -- -17 - -- -- -20 - -- -- -- -- -25 - NOTES: Not finished as well 6/29/2016 6/29/2016 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451 910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B13 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS: Hollow Stem Auger/Air Hammer DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -- -24 Dark brown silty clay 0.0 - -3 - -24 Brownish red silty clay 0.0 - -5 - -24 Brownish red silty clay 0.0 - -- -8 24 Brownish red silt 0.0 - -- -10 24 Brown silt 0.0 - -- -24 Dark brown silt 0.0 - -13 - -- -15 - -- -17 - -- -- -20 - -- -- -- -- -25 Bottom of boring - NOTES: Finished as permanent well 07/24/16 07/24/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B14 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -18 gravel with dark gray clayey sand 0.0 - -- -3 - 18 Brownish red silty clay with light gray streaking 2.0 -- -5 - -18 Brownish red silt 0.0 - -- -8 - -5 Brownish red silt with weathered rock 0.0 - -10 - -- -- -13 - -- -15 - -- -17 - -- -- -20 - - Bottom of boring - -- -- -- -25 - NOTES: Finished as permanent well 06/24/16 06/24/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B15 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -18 Grayish green silty clay *note odor observed 7.4 - -- -3 - 4 Dark brown silty sand 10.3 -- -5 - -18 Brown silty clay *note odor observed 8.9 - -- -8 - -18 Light brown silty clay with rock 7.5 - -10 - -- -- -13 - -- -15 - -- -17 - -- -- -20 Bottom of boring - -- -- -- -- -25 - NOTES: Finished as permanent well 06/27/16 06/27/16 ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD. 154 Backhoe Road Leland, NC 28451910-371-5980 VISUAL CLASSIFICATION OF SOILS PROJECT NUMBER:1272C PROJECT NAME:University Ford Phase II ESA BORING NUMBER:B16 COORDINATES NA ELEVATION:NA GWL: NA GEOLOGIST/ENGINEER:C. Moody DATE STARTED: DRILLING METHODS:Hollow Stem Auger DATE COMPLETED:PAGE 1 0F 1 SAMPLE PENATRAT. RECOVERY DESCRIPTION USCS REMARKS DEPTH BLOWS (IN)SYMBOL Hnu Readings (FT) PER FT.(ppm) -18 Grayish green silty clay 1.3 - -- -3 - 18 Light brownish gray sandy clay with fill 0.5 -- -5 - -18 Light brownish gray sandy clay with fill 0.4 - -- 5 Light brown silty clay with rock. Bottom of boring -8 - -7.5 - -10 - -- -- -13 - -- -15 - -- -17 - -- -- -20 - -- -- -- -- -25 - NOTES: Not finished as well 06/28/16 06/28/16 WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: WELL CONSTRUCTION RECORD This form can be used for single or multiple wells Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is (are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed. For Internal Use ONLY: Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C LABORATORY DATA AND CHAIN OF CUSTODY #=CL# July 26, 2016 LIMS USE: FR - ELLIOT SWAIN LIMS OBJECT ID: 92303397 92303397 Project: Pace Project No.: RE: Elliot SwainAtlantic Shore Environmental154 Backhoe RdLeland, NC 28451 UNIVERSITY FORD 1272C Dear Elliot Swain: Enclosed are the analytical results for sample(s) received by the laboratory on June 28, 2016. The results relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Report revised 7/26 to show MDL/J-flags If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell taylor.ezell@pacelabs.com Project Manager Enclosures cc:Cheryl Moody, Atlantic Shore Environmental REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 44 #=CP# CERTIFICATIONS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 44 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Lab ID Sample ID Matrix Date Collected Date Received 92303397001 B-5 (4-6)Solid 06/27/16 09:10 06/28/16 16:15 92303397002 B-8 (4-6)Solid 06/27/16 12:30 06/28/16 16:15 92303397003 B-15 (3.5-6.5)Solid 06/27/16 15:40 06/28/16 16:15 92303397004 B-16 (1-2.5)Solid 06/28/16 08:15 06/28/16 16:15 92303397005 B-2 (1-2.5)Solid 06/28/16 11:40 06/28/16 16:15 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 44 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92303397001 B-5 (4-6)EPA 6010 7 PASI-AJMW EPA 7471 1 PASI-AWAB EPA 8270 74 PASI-CBPJ EPA 8260 70 PASI-CDLK ASTM D2974-87 1 PASI-CKDF 92303397002 B-8 (4-6)EPA 6010 7 PASI-AJMW EPA 7471 1 PASI-AWAB EPA 8270 74 PASI-CBPJ EPA 8260 70 PASI-CDLK ASTM D2974-87 1 PASI-CKDF 92303397003 B-15 (3.5-6.5)EPA 6010 7 PASI-AJMW EPA 7471 1 PASI-AWAB EPA 8270 74 PASI-CBPJ EPA 8260 70 PASI-CDLK ASTM D2974-87 1 PASI-CKDF 92303397004 B-16 (1-2.5)EPA 6010 7 PASI-AJMW EPA 7471 1 PASI-AWAB EPA 8270 74 PASI-CBPJ EPA 8260 70 PASI-CDLK ASTM D2974-87 1 PASI-CKDF 92303397005 B-2 (1-2.5)EPA 6010 7 PASI-AJMW EPA 7471 1 PASI-AWAB EPA 8270 74 PASI-CBPJ EPA 8260 70 PASI-CDLK ASTM D2974-87 1 PASI-CKDF REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-5 (4-6)Lab ID: 92303397001 Collected: 06/27/16 09:10 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP Arsenic 3.2 mg/kg 07/06/16 16:53 7440-38-207/01/16 23:551.1 0.56 1 Barium 111 mg/kg 07/06/16 16:53 7440-39-307/01/16 23:550.56 0.28 1 Cadmium 0.14 mg/kg 07/06/16 16:53 7440-43-907/01/16 23:550.11 0.056 1 Chromium 16.7 mg/kg 07/06/16 16:53 7440-47-307/01/16 23:550.56 0.28 1 Lead 99.6 mg/kg 07/06/16 16:53 7439-92-107/01/16 23:550.56 0.28 1 Selenium 1.7 mg/kg 07/06/16 16:53 7782-49-207/01/16 23:551.1 0.56 1 Silver ND mg/kg 07/06/16 16:53 7440-22-407/01/16 23:550.56 0.28 1 Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury Mercury 0.050 mg/kg 07/12/16 10:34 7439-97-6 M107/08/16 05:150.0033 0.000067 1 Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave Acenaphthene ND ug/kg 07/08/16 13:56 83-32-906/30/16 14:23418 96.3 1 Acenaphthylene ND ug/kg 07/08/16 13:56 208-96-806/30/16 14:23418 98.9 1 Aniline ND ug/kg 07/08/16 13:56 62-53-306/30/16 14:23418 113 1 Anthracene ND ug/kg 07/08/16 13:56 120-12-706/30/16 14:23418 93.8 1 Benzo(a)anthracene 281J ug/kg 07/08/16 13:56 56-55-306/30/16 14:23418 77.3 1 Benzo(a)pyrene 250J ug/kg 07/08/16 13:56 50-32-806/30/16 14:23418 79.9 1 Benzo(b)fluoranthene 342J ug/kg 07/08/16 13:56 205-99-206/30/16 14:23418 72.2 1 Benzo(g,h,i)perylene 158J ug/kg 07/08/16 13:56 191-24-206/30/16 14:23418 106 1 Benzo(k)fluoranthene 127J ug/kg 07/08/16 13:56 207-08-906/30/16 14:23418 82.4 1 Benzoic Acid ND ug/kg 07/08/16 13:56 65-85-006/30/16 14:232090 76.1 1 Benzyl alcohol ND ug/kg 07/08/16 13:56 100-51-606/30/16 14:23837 83.7 1 4-Bromophenylphenyl ether ND ug/kg 07/08/16 13:56 101-55-306/30/16 14:23418 76.1 1 Butylbenzylphthalate ND ug/kg 07/08/16 13:56 85-68-706/30/16 14:23418 88.7 1 4-Chloro-3-methylphenol ND ug/kg 07/08/16 13:56 59-50-706/30/16 14:23837 86.2 1 4-Chloroaniline ND ug/kg 07/08/16 13:56 106-47-806/30/16 14:232090 117 1 bis(2-Chloroethoxy)methane ND ug/kg 07/08/16 13:56 111-91-106/30/16 14:23418 97.6 1 bis(2-Chloroethyl) ether ND ug/kg 07/08/16 13:56 111-44-406/30/16 14:23418 106 1 2-Chloronaphthalene ND ug/kg 07/08/16 13:56 91-58-706/30/16 14:23418 82.4 1 2-Chlorophenol ND ug/kg 07/08/16 13:56 95-57-806/30/16 14:23418 114 1 4-Chlorophenylphenyl ether ND ug/kg 07/08/16 13:56 7005-72-306/30/16 14:23418 86.2 1 Chrysene 272J ug/kg 07/08/16 13:56 218-01-906/30/16 14:23418 55.8 1 Dibenz(a,h)anthracene ND ug/kg 07/08/16 13:56 53-70-306/30/16 14:23418 88.7 1 Dibenzofuran ND ug/kg 07/08/16 13:56 132-64-906/30/16 14:23418 68.4 1 1,2-Dichlorobenzene ND ug/kg 07/08/16 13:56 95-50-106/30/16 14:23418 112 1 1,3-Dichlorobenzene ND ug/kg 07/08/16 13:56 541-73-106/30/16 14:23418 95.1 1 1,4-Dichlorobenzene ND ug/kg 07/08/16 13:56 106-46-706/30/16 14:23418 118 1 3,3'-Dichlorobenzidine ND ug/kg 07/08/16 13:56 91-94-106/30/16 14:232090 91.3 1 2,4-Dichlorophenol ND ug/kg 07/08/16 13:56 120-83-206/30/16 14:23418 91.3 1 Diethylphthalate ND ug/kg 07/08/16 13:56 84-66-206/30/16 14:23418 64.6 1 2,4-Dimethylphenol ND ug/kg 07/08/16 13:56 105-67-906/30/16 14:23418 165 1 Dimethylphthalate ND ug/kg 07/08/16 13:56 131-11-306/30/16 14:23418 84.9 1 Di-n-butylphthalate ND ug/kg 07/08/16 13:56 84-74-206/30/16 14:23418 68.4 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/08/16 13:56 534-52-106/30/16 14:23837 83.7 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-5 (4-6)Lab ID: 92303397001 Collected: 06/27/16 09:10 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave 2,4-Dinitrophenol ND ug/kg 07/08/16 13:56 51-28-506/30/16 14:232090 68.4 1 2,4-Dinitrotoluene ND ug/kg 07/08/16 13:56 121-14-206/30/16 14:23418 78.6 1 2,6-Dinitrotoluene ND ug/kg 07/08/16 13:56 606-20-206/30/16 14:23418 87.5 1 Di-n-octylphthalate ND ug/kg 07/08/16 13:56 117-84-006/30/16 14:23418 87.5 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/08/16 13:56 117-81-706/30/16 14:23418 114 1 Fluoranthene 683 ug/kg 07/08/16 13:56 206-44-006/30/16 14:23418 60.8 1 Fluorene ND ug/kg 07/08/16 13:56 86-73-706/30/16 14:23418 86.2 1 Hexachloro-1,3-butadiene ND ug/kg 07/08/16 13:56 87-68-306/30/16 14:23418 72.2 1 Hexachlorobenzene ND ug/kg 07/08/16 13:56 118-74-106/30/16 14:23418 53.2 1 Hexachlorocyclopentadiene ND ug/kg 07/08/16 13:56 77-47-406/30/16 14:23418 77.3 1 Hexachloroethane ND ug/kg 07/08/16 13:56 67-72-106/30/16 14:23418 110 1 Indeno(1,2,3-cd)pyrene 143J ug/kg 07/08/16 13:56 193-39-506/30/16 14:23418 86.2 1 Isophorone ND ug/kg 07/08/16 13:56 78-59-106/30/16 14:23418 93.8 1 1-Methylnaphthalene ND ug/kg 07/08/16 13:56 90-12-006/30/16 14:23418 109 1 2-Methylnaphthalene ND ug/kg 07/08/16 13:56 91-57-606/30/16 14:23418 90.0 1 2-Methylphenol(o-Cresol)ND ug/kg 07/08/16 13:56 95-48-706/30/16 14:23418 127 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/08/16 13:5606/30/16 14:23418 165 1 Naphthalene ND ug/kg 07/08/16 13:56 91-20-306/30/16 14:23418 103 1 2-Nitroaniline ND ug/kg 07/08/16 13:56 88-74-406/30/16 14:232090 129 1 3-Nitroaniline ND ug/kg 07/08/16 13:56 99-09-206/30/16 14:232090 114 1 4-Nitroaniline ND ug/kg 07/08/16 13:56 100-01-606/30/16 14:23837 118 1 Nitrobenzene ND ug/kg 07/08/16 13:56 98-95-306/30/16 14:23418 114 1 2-Nitrophenol ND ug/kg 07/08/16 13:56 88-75-506/30/16 14:23418 101 1 4-Nitrophenol ND ug/kg 07/08/16 13:56 100-02-706/30/16 14:232090 74.8 1 N-Nitrosodimethylamine ND ug/kg 07/08/16 13:56 62-75-906/30/16 14:23418 136 1 N-Nitroso-di-n-propylamine ND ug/kg 07/08/16 13:56 621-64-706/30/16 14:23418 79.9 1 N-Nitrosodiphenylamine ND ug/kg 07/08/16 13:56 86-30-606/30/16 14:23418 124 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/08/16 13:56 108-60-106/30/16 14:23418 112 1 Pentachlorophenol ND ug/kg 07/08/16 13:56 87-86-506/30/16 14:232090 76.1 1 Phenanthrene 393J ug/kg 07/08/16 13:56 85-01-806/30/16 14:23418 69.7 1 Phenol ND ug/kg 07/08/16 13:5606/30/16 14:23418 125 1 Pyrene 464 ug/kg 07/08/16 13:56 129-00-006/30/16 14:23418 71.0 1 1,2,4-Trichlorobenzene ND ug/kg 07/08/16 13:56 120-82-106/30/16 14:23418 81.1 1 2,4,5-Trichlorophenol ND ug/kg 07/08/16 13:56 95-95-406/30/16 14:23418 129 1 2,4,6-Trichlorophenol ND ug/kg 07/08/16 13:56 88-06-206/30/16 14:23418 92.5 1 Surrogates Nitrobenzene-d5 (S)56 %07/08/16 13:56 4165-60-006/30/16 14:2323-110 1 2-Fluorobiphenyl (S)55 %07/08/16 13:56 321-60-806/30/16 14:2330-110 1 Terphenyl-d14 (S)73 %07/08/16 13:56 1718-51-006/30/16 14:2328-110 1 Phenol-d6 (S)64 %07/08/16 13:56 13127-88-306/30/16 14:2322-110 1 2-Fluorophenol (S)62 %07/08/16 13:56 367-12-406/30/16 14:2313-110 1 2,4,6-Tribromophenol (S)70 %07/08/16 13:56 118-79-606/30/16 14:2327-110 1 Analytical Method: EPA 82608260/5035A Volatile Organics Acetone 158 ug/kg 07/07/16 21:34 67-64-1113 11.3 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-5 (4-6)Lab ID: 92303397001 Collected: 06/27/16 09:10 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260/5035A Volatile Organics Benzene ND ug/kg 07/07/16 21:34 71-43-25.6 1.8 1 Bromobenzene ND ug/kg 07/07/16 21:34 108-86-15.6 2.3 1 Bromochloromethane ND ug/kg 07/07/16 21:34 74-97-55.6 1.9 1 Bromodichloromethane ND ug/kg 07/07/16 21:34 75-27-45.6 2.1 1 Bromoform ND ug/kg 07/07/16 21:34 75-25-25.6 2.6 1 Bromomethane ND ug/kg 07/07/16 21:34 74-83-911.3 2.8 1 2-Butanone (MEK)ND ug/kg 07/07/16 21:34 78-93-3113 3.3 1 n-Butylbenzene ND ug/kg 07/07/16 21:34 104-51-85.6 2.0 1 sec-Butylbenzene ND ug/kg 07/07/16 21:34 135-98-85.6 1.8 1 tert-Butylbenzene ND ug/kg 07/07/16 21:34 98-06-65.6 2.3 1 Carbon tetrachloride ND ug/kg 07/07/16 21:34 56-23-55.6 2.9 1 Chlorobenzene ND ug/kg 07/07/16 21:34 108-90-75.6 2.1 1 Chloroethane ND ug/kg 07/07/16 21:34 75-00-311.3 2.7 1 Chloroform ND ug/kg 07/07/16 21:34 67-66-35.6 1.8 1 Chloromethane ND ug/kg 07/07/16 21:34 74-87-311.3 2.7 1 2-Chlorotoluene ND ug/kg 07/07/16 21:34 95-49-85.6 1.9 1 4-Chlorotoluene ND ug/kg 07/07/16 21:34 106-43-45.6 2.0 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/07/16 21:34 96-12-85.6 4.1 1 Dibromochloromethane ND ug/kg 07/07/16 21:34 124-48-15.6 2.0 1 1,2-Dibromoethane (EDB)ND ug/kg 07/07/16 21:34 106-93-45.6 2.0 1 Dibromomethane ND ug/kg 07/07/16 21:34 74-95-35.6 2.8 1 1,2-Dichlorobenzene ND ug/kg 07/07/16 21:34 95-50-15.6 2.1 1 1,3-Dichlorobenzene ND ug/kg 07/07/16 21:34 541-73-15.6 2.3 1 1,4-Dichlorobenzene ND ug/kg 07/07/16 21:34 106-46-75.6 1.9 1 Dichlorodifluoromethane ND ug/kg 07/07/16 21:34 75-71-811.3 4.1 1 1,1-Dichloroethane ND ug/kg 07/07/16 21:34 75-34-35.6 1.7 1 1,2-Dichloroethane ND ug/kg 07/07/16 21:34 107-06-25.6 2.5 1 1,1-Dichloroethene ND ug/kg 07/07/16 21:34 75-35-45.6 2.0 1 cis-1,2-Dichloroethene ND ug/kg 07/07/16 21:34 156-59-25.6 1.6 1 trans-1,2-Dichloroethene ND ug/kg 07/07/16 21:34 156-60-55.6 2.1 1 1,2-Dichloropropane ND ug/kg 07/07/16 21:34 78-87-55.6 1.9 1 1,3-Dichloropropane ND ug/kg 07/07/16 21:34 142-28-95.6 2.1 1 2,2-Dichloropropane ND ug/kg 07/07/16 21:34 594-20-75.6 1.9 1 1,1-Dichloropropene ND ug/kg 07/07/16 21:34 563-58-65.6 1.7 1 cis-1,3-Dichloropropene ND ug/kg 07/07/16 21:34 10061-01-55.6 2.0 1 trans-1,3-Dichloropropene ND ug/kg 07/07/16 21:34 10061-02-65.6 1.7 1 Diisopropyl ether ND ug/kg 07/07/16 21:34 108-20-35.6 1.9 1 Ethylbenzene ND ug/kg 07/07/16 21:34 100-41-45.6 2.0 1 Hexachloro-1,3-butadiene ND ug/kg 07/07/16 21:34 87-68-35.6 2.3 1 2-Hexanone ND ug/kg 07/07/16 21:34 591-78-656.3 4.4 1 Isopropylbenzene (Cumene)ND ug/kg 07/07/16 21:34 98-82-85.6 2.1 1 p-Isopropyltoluene ND ug/kg 07/07/16 21:34 99-87-65.6 1.9 1 Methylene Chloride ND ug/kg 07/07/16 21:34 75-09-222.5 3.4 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/07/16 21:34 108-10-156.3 4.2 1 Methyl-tert-butyl ether ND ug/kg 07/07/16 21:34 1634-04-45.6 1.7 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-5 (4-6)Lab ID: 92303397001 Collected: 06/27/16 09:10 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260/5035A Volatile Organics Naphthalene ND ug/kg 07/07/16 21:34 91-20-35.6 1.4 1 n-Propylbenzene ND ug/kg 07/07/16 21:34 103-65-15.6 1.9 1 Styrene ND ug/kg 07/07/16 21:34 100-42-55.6 2.0 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/07/16 21:34 630-20-65.6 2.4 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/07/16 21:34 79-34-55.6 2.1 1 Tetrachloroethene ND ug/kg 07/07/16 21:34 127-18-45.6 1.9 1 Toluene ND ug/kg 07/07/16 21:34 108-88-35.6 2.0 1 1,2,3-Trichlorobenzene ND ug/kg 07/07/16 21:34 87-61-65.6 2.5 1 1,2,4-Trichlorobenzene ND ug/kg 07/07/16 21:34 120-82-15.6 1.8 1 1,1,1-Trichloroethane ND ug/kg 07/07/16 21:34 71-55-65.6 2.0 1 1,1,2-Trichloroethane ND ug/kg 07/07/16 21:34 79-00-55.6 2.4 1 Trichloroethene ND ug/kg 07/07/16 21:34 79-01-65.6 2.4 1 Trichlorofluoromethane ND ug/kg 07/07/16 21:34 75-69-45.6 2.5 1 1,2,3-Trichloropropane ND ug/kg 07/07/16 21:34 96-18-45.6 1.8 1 1,2,4-Trimethylbenzene ND ug/kg 07/07/16 21:34 95-63-65.6 2.3 1 1,3,5-Trimethylbenzene ND ug/kg 07/07/16 21:34 108-67-85.6 2.0 1 Vinyl acetate ND ug/kg 07/07/16 21:34 108-05-456.3 9.9 1 Vinyl chloride ND ug/kg 07/07/16 21:34 75-01-411.3 2.0 1 Xylene (Total)ND ug/kg 07/07/16 21:34 1330-20-711.3 4.1 1 m&p-Xylene ND ug/kg 07/07/16 21:34 179601-23-111.3 4.1 1 o-Xylene ND ug/kg 07/07/16 21:34 95-47-65.6 2.1 1 Surrogates Toluene-d8 (S)104 %07/07/16 21:34 2037-26-570-130 1 4-Bromofluorobenzene (S)98 %07/07/16 21:34 460-00-470-130 1 1,2-Dichloroethane-d4 (S)90 %07/07/16 21:34 17060-07-070-132 1 Analytical Method: ASTM D2974-87Percent Moisture Percent Moisture 21.1 %06/30/16 13:590.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-8 (4-6)Lab ID: 92303397002 Collected: 06/27/16 12:30 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP Arsenic 3.1J mg/kg 07/07/16 14:46 7440-38-2 D307/01/16 23:554.9 2.5 5 Barium 227 mg/kg 07/07/16 14:46 7440-39-307/01/16 23:552.5 1.2 5 Cadmium ND mg/kg 07/07/16 14:46 7440-43-9 D307/01/16 23:550.49 0.25 5 Chromium 25.0 mg/kg 07/07/16 14:46 7440-47-307/01/16 23:552.5 1.2 5 Lead 11.1 mg/kg 07/07/16 14:46 7439-92-107/01/16 23:552.5 1.2 5 Selenium ND mg/kg 07/07/16 14:46 7782-49-2 D307/01/16 23:554.9 2.5 5 Silver ND mg/kg 07/07/16 14:46 7440-22-4 D307/01/16 23:552.5 1.2 5 Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury Mercury 0.0023J mg/kg 07/12/16 10:42 7439-97-607/08/16 05:150.0047 0.000093 1 Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave Acenaphthene ND ug/kg 07/07/16 17:37 83-32-906/30/16 14:233910 900 10 Acenaphthylene ND ug/kg 07/07/16 17:37 208-96-806/30/16 14:233910 923 10 Aniline ND ug/kg 07/07/16 17:37 62-53-306/30/16 14:233910 1050 10 Anthracene ND ug/kg 07/07/16 17:37 120-12-706/30/16 14:233910 876 10 Benzo(a)anthracene ND ug/kg 07/07/16 17:37 56-55-306/30/16 14:233910 722 10 Benzo(a)pyrene ND ug/kg 07/07/16 17:37 50-32-806/30/16 14:233910 746 10 Benzo(b)fluoranthene ND ug/kg 07/07/16 17:37 205-99-206/30/16 14:233910 675 10 Benzo(g,h,i)perylene ND ug/kg 07/07/16 17:37 191-24-206/30/16 14:233910 994 10 Benzo(k)fluoranthene ND ug/kg 07/07/16 17:37 207-08-906/30/16 14:233910 769 10 Benzoic Acid ND ug/kg 07/07/16 17:37 65-85-006/30/16 14:2319500 710 10 Benzyl alcohol ND ug/kg 07/07/16 17:37 100-51-606/30/16 14:237810 781 10 4-Bromophenylphenyl ether ND ug/kg 07/07/16 17:37 101-55-306/30/16 14:233910 710 10 Butylbenzylphthalate ND ug/kg 07/07/16 17:37 85-68-706/30/16 14:233910 829 10 4-Chloro-3-methylphenol ND ug/kg 07/07/16 17:37 59-50-706/30/16 14:237810 805 10 4-Chloroaniline ND ug/kg 07/07/16 17:37 106-47-806/30/16 14:2319500 1090 10 bis(2-Chloroethoxy)methane ND ug/kg 07/07/16 17:37 111-91-106/30/16 14:233910 912 10 bis(2-Chloroethyl) ether ND ug/kg 07/07/16 17:37 111-44-406/30/16 14:233910 994 10 2-Chloronaphthalene ND ug/kg 07/07/16 17:37 91-58-706/30/16 14:233910 769 10 2-Chlorophenol ND ug/kg 07/07/16 17:37 95-57-806/30/16 14:233910 1070 10 4-Chlorophenylphenyl ether ND ug/kg 07/07/16 17:37 7005-72-306/30/16 14:233910 805 10 Chrysene ND ug/kg 07/07/16 17:37 218-01-906/30/16 14:233910 521 10 Dibenz(a,h)anthracene ND ug/kg 07/07/16 17:37 53-70-306/30/16 14:233910 829 10 Dibenzofuran ND ug/kg 07/07/16 17:37 132-64-906/30/16 14:233910 639 10 1,2-Dichlorobenzene ND ug/kg 07/07/16 17:37 95-50-106/30/16 14:233910 1040 10 1,3-Dichlorobenzene ND ug/kg 07/07/16 17:37 541-73-106/30/16 14:233910 888 10 1,4-Dichlorobenzene ND ug/kg 07/07/16 17:37 106-46-706/30/16 14:233910 1100 10 3,3'-Dichlorobenzidine ND ug/kg 07/07/16 17:37 91-94-106/30/16 14:2319500 852 10 2,4-Dichlorophenol ND ug/kg 07/07/16 17:37 120-83-206/30/16 14:233910 852 10 Diethylphthalate ND ug/kg 07/07/16 17:37 84-66-206/30/16 14:233910 604 10 2,4-Dimethylphenol ND ug/kg 07/07/16 17:37 105-67-906/30/16 14:233910 1540 10 Dimethylphthalate ND ug/kg 07/07/16 17:37 131-11-306/30/16 14:233910 793 10 Di-n-butylphthalate ND ug/kg 07/07/16 17:37 84-74-206/30/16 14:233910 639 10 4,6-Dinitro-2-methylphenol ND ug/kg 07/07/16 17:37 534-52-106/30/16 14:237810 781 10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-8 (4-6)Lab ID: 92303397002 Collected: 06/27/16 12:30 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave 2,4-Dinitrophenol ND ug/kg 07/07/16 17:37 51-28-506/30/16 14:2319500 639 10 2,4-Dinitrotoluene ND ug/kg 07/07/16 17:37 121-14-206/30/16 14:233910 734 10 2,6-Dinitrotoluene ND ug/kg 07/07/16 17:37 606-20-206/30/16 14:233910 817 10 Di-n-octylphthalate ND ug/kg 07/07/16 17:37 117-84-006/30/16 14:233910 817 10 bis(2-Ethylhexyl)phthalate ND ug/kg 07/07/16 17:37 117-81-706/30/16 14:233910 1070 10 Fluoranthene ND ug/kg 07/07/16 17:37 206-44-006/30/16 14:233910 568 10 Fluorene ND ug/kg 07/07/16 17:37 86-73-706/30/16 14:233910 805 10 Hexachloro-1,3-butadiene ND ug/kg 07/07/16 17:37 87-68-306/30/16 14:233910 675 10 Hexachlorobenzene ND ug/kg 07/07/16 17:37 118-74-106/30/16 14:233910 497 10 Hexachlorocyclopentadiene ND ug/kg 07/07/16 17:37 77-47-406/30/16 14:233910 722 10 Hexachloroethane ND ug/kg 07/07/16 17:37 67-72-106/30/16 14:233910 1030 10 Indeno(1,2,3-cd)pyrene ND ug/kg 07/07/16 17:37 193-39-506/30/16 14:233910 805 10 Isophorone ND ug/kg 07/07/16 17:37 78-59-106/30/16 14:233910 876 10 1-Methylnaphthalene ND ug/kg 07/07/16 17:37 90-12-006/30/16 14:233910 1020 10 2-Methylnaphthalene ND ug/kg 07/07/16 17:37 91-57-606/30/16 14:233910 840 10 2-Methylphenol(o-Cresol)ND ug/kg 07/07/16 17:37 95-48-706/30/16 14:233910 1180 10 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/07/16 17:3706/30/16 14:233910 1540 10 Naphthalene ND ug/kg 07/07/16 17:37 91-20-306/30/16 14:233910 959 10 2-Nitroaniline ND ug/kg 07/07/16 17:37 88-74-406/30/16 14:2319500 1210 10 3-Nitroaniline ND ug/kg 07/07/16 17:37 99-09-206/30/16 14:2319500 1070 10 4-Nitroaniline ND ug/kg 07/07/16 17:37 100-01-606/30/16 14:237810 1100 10 Nitrobenzene ND ug/kg 07/07/16 17:37 98-95-306/30/16 14:233910 1070 10 2-Nitrophenol ND ug/kg 07/07/16 17:37 88-75-506/30/16 14:233910 947 10 4-Nitrophenol ND ug/kg 07/07/16 17:37 100-02-706/30/16 14:2319500 698 10 N-Nitrosodimethylamine ND ug/kg 07/07/16 17:37 62-75-906/30/16 14:233910 1270 10 N-Nitroso-di-n-propylamine ND ug/kg 07/07/16 17:37 621-64-706/30/16 14:233910 746 10 N-Nitrosodiphenylamine ND ug/kg 07/07/16 17:37 86-30-606/30/16 14:233910 1160 10 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/07/16 17:37 108-60-106/30/16 14:233910 1040 10 Pentachlorophenol ND ug/kg 07/07/16 17:37 87-86-506/30/16 14:2319500 710 10 Phenanthrene ND ug/kg 07/07/16 17:37 85-01-806/30/16 14:233910 651 10 Phenol ND ug/kg 07/07/16 17:3706/30/16 14:233910 1170 10 Pyrene ND ug/kg 07/07/16 17:37 129-00-006/30/16 14:233910 663 10 1,2,4-Trichlorobenzene ND ug/kg 07/07/16 17:37 120-82-106/30/16 14:233910 758 10 2,4,5-Trichlorophenol ND ug/kg 07/07/16 17:37 95-95-406/30/16 14:233910 1210 10 2,4,6-Trichlorophenol ND ug/kg 07/07/16 17:37 88-06-206/30/16 14:233910 864 10 Surrogates Nitrobenzene-d5 (S)0 %07/07/16 17:37 4165-60-0 D3,S406/30/16 14:2323-110 10 2-Fluorobiphenyl (S)0 %07/07/16 17:37 321-60-8 S406/30/16 14:2330-110 10 Terphenyl-d14 (S)0 %07/07/16 17:37 1718-51-0 S406/30/16 14:2328-110 10 Phenol-d6 (S)0 %07/07/16 17:37 13127-88-3 S406/30/16 14:2322-110 10 2-Fluorophenol (S)0 %07/07/16 17:37 367-12-4 S406/30/16 14:2313-110 10 2,4,6-Tribromophenol (S)0 %07/07/16 17:37 118-79-6 S406/30/16 14:2327-110 10 Analytical Method: EPA 82608260/5035A Volatile Organics Acetone 72.4J ug/kg 07/07/16 21:54 67-64-192.2 9.2 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-8 (4-6)Lab ID: 92303397002 Collected: 06/27/16 12:30 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260/5035A Volatile Organics Benzene ND ug/kg 07/07/16 21:54 71-43-24.6 1.5 1 Bromobenzene ND ug/kg 07/07/16 21:54 108-86-14.6 1.8 1 Bromochloromethane ND ug/kg 07/07/16 21:54 74-97-54.6 1.6 1 Bromodichloromethane ND ug/kg 07/07/16 21:54 75-27-44.6 1.8 1 Bromoform ND ug/kg 07/07/16 21:54 75-25-24.6 2.1 1 Bromomethane ND ug/kg 07/07/16 21:54 74-83-99.2 2.3 1 2-Butanone (MEK)ND ug/kg 07/07/16 21:54 78-93-392.2 2.7 1 n-Butylbenzene ND ug/kg 07/07/16 21:54 104-51-84.6 1.7 1 sec-Butylbenzene ND ug/kg 07/07/16 21:54 135-98-84.6 1.5 1 tert-Butylbenzene ND ug/kg 07/07/16 21:54 98-06-64.6 1.8 1 Carbon tetrachloride ND ug/kg 07/07/16 21:54 56-23-54.6 2.4 1 Chlorobenzene ND ug/kg 07/07/16 21:54 108-90-74.6 1.8 1 Chloroethane ND ug/kg 07/07/16 21:54 75-00-39.2 2.2 1 Chloroform ND ug/kg 07/07/16 21:54 67-66-34.6 1.5 1 Chloromethane ND ug/kg 07/07/16 21:54 74-87-39.2 2.2 1 2-Chlorotoluene ND ug/kg 07/07/16 21:54 95-49-84.6 1.6 1 4-Chlorotoluene ND ug/kg 07/07/16 21:54 106-43-44.6 1.7 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/07/16 21:54 96-12-84.6 3.3 1 Dibromochloromethane ND ug/kg 07/07/16 21:54 124-48-14.6 1.7 1 1,2-Dibromoethane (EDB)ND ug/kg 07/07/16 21:54 106-93-44.6 1.7 1 Dibromomethane ND ug/kg 07/07/16 21:54 74-95-34.6 2.3 1 1,2-Dichlorobenzene ND ug/kg 07/07/16 21:54 95-50-14.6 1.8 1 1,3-Dichlorobenzene ND ug/kg 07/07/16 21:54 541-73-14.6 1.8 1 1,4-Dichlorobenzene ND ug/kg 07/07/16 21:54 106-46-74.6 1.6 1 Dichlorodifluoromethane ND ug/kg 07/07/16 21:54 75-71-89.2 3.3 1 1,1-Dichloroethane ND ug/kg 07/07/16 21:54 75-34-34.6 1.4 1 1,2-Dichloroethane ND ug/kg 07/07/16 21:54 107-06-24.6 2.0 1 1,1-Dichloroethene ND ug/kg 07/07/16 21:54 75-35-44.6 1.7 1 cis-1,2-Dichloroethene ND ug/kg 07/07/16 21:54 156-59-24.6 1.3 1 trans-1,2-Dichloroethene ND ug/kg 07/07/16 21:54 156-60-54.6 1.8 1 1,2-Dichloropropane ND ug/kg 07/07/16 21:54 78-87-54.6 1.6 1 1,3-Dichloropropane ND ug/kg 07/07/16 21:54 142-28-94.6 1.8 1 2,2-Dichloropropane ND ug/kg 07/07/16 21:54 594-20-74.6 1.6 1 1,1-Dichloropropene ND ug/kg 07/07/16 21:54 563-58-64.6 1.4 1 cis-1,3-Dichloropropene ND ug/kg 07/07/16 21:54 10061-01-54.6 1.7 1 trans-1,3-Dichloropropene ND ug/kg 07/07/16 21:54 10061-02-64.6 1.4 1 Diisopropyl ether ND ug/kg 07/07/16 21:54 108-20-34.6 1.6 1 Ethylbenzene 2.7J ug/kg 07/07/16 21:54 100-41-44.6 1.7 1 Hexachloro-1,3-butadiene ND ug/kg 07/07/16 21:54 87-68-34.6 1.8 1 2-Hexanone ND ug/kg 07/07/16 21:54 591-78-646.1 3.6 1 Isopropylbenzene (Cumene)ND ug/kg 07/07/16 21:54 98-82-84.6 1.8 1 p-Isopropyltoluene ND ug/kg 07/07/16 21:54 99-87-64.6 1.6 1 Methylene Chloride 2.9J ug/kg 07/07/16 21:54 75-09-218.4 2.8 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/07/16 21:54 108-10-146.1 3.4 1 Methyl-tert-butyl ether ND ug/kg 07/07/16 21:54 1634-04-44.6 1.4 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-8 (4-6)Lab ID: 92303397002 Collected: 06/27/16 12:30 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260/5035A Volatile Organics Naphthalene 2.7J ug/kg 07/07/16 21:54 91-20-34.6 1.1 1 n-Propylbenzene ND ug/kg 07/07/16 21:54 103-65-14.6 1.6 1 Styrene ND ug/kg 07/07/16 21:54 100-42-54.6 1.7 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/07/16 21:54 630-20-64.6 1.9 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/07/16 21:54 79-34-54.6 1.8 1 Tetrachloroethene ND ug/kg 07/07/16 21:54 127-18-44.6 1.6 1 Toluene ND ug/kg 07/07/16 21:54 108-88-34.6 1.7 1 1,2,3-Trichlorobenzene ND ug/kg 07/07/16 21:54 87-61-64.6 2.0 1 1,2,4-Trichlorobenzene ND ug/kg 07/07/16 21:54 120-82-14.6 1.5 1 1,1,1-Trichloroethane ND ug/kg 07/07/16 21:54 71-55-64.6 1.7 1 1,1,2-Trichloroethane ND ug/kg 07/07/16 21:54 79-00-54.6 1.9 1 Trichloroethene ND ug/kg 07/07/16 21:54 79-01-64.6 1.9 1 Trichlorofluoromethane ND ug/kg 07/07/16 21:54 75-69-44.6 2.0 1 1,2,3-Trichloropropane ND ug/kg 07/07/16 21:54 96-18-44.6 1.5 1 1,2,4-Trimethylbenzene 5.7 ug/kg 07/07/16 21:54 95-63-64.6 1.8 1 1,3,5-Trimethylbenzene ND ug/kg 07/07/16 21:54 108-67-84.6 1.7 1 Vinyl acetate ND ug/kg 07/07/16 21:54 108-05-446.1 8.1 1 Vinyl chloride ND ug/kg 07/07/16 21:54 75-01-49.2 1.7 1 Xylene (Total)ND ug/kg 07/07/16 21:54 1330-20-79.2 3.3 1 m&p-Xylene ND ug/kg 07/07/16 21:54 179601-23-19.2 3.3 1 o-Xylene ND ug/kg 07/07/16 21:54 95-47-64.6 1.8 1 Surrogates Toluene-d8 (S)104 %07/07/16 21:54 2037-26-570-130 1 4-Bromofluorobenzene (S)98 %07/07/16 21:54 460-00-470-130 1 1,2-Dichloroethane-d4 (S)96 %07/07/16 21:54 17060-07-070-132 1 Analytical Method: ASTM D2974-87Percent Moisture Percent Moisture 15.5 %06/30/16 14:000.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-15 (3.5-6.5)Lab ID: 92303397003 Collected: 06/27/16 15:40 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP Arsenic 1.4 mg/kg 07/06/16 16:59 7440-38-207/01/16 23:550.71 0.36 1 Barium 42.4 mg/kg 07/06/16 16:59 7440-39-307/01/16 23:550.36 0.18 1 Cadmium ND mg/kg 07/06/16 16:59 7440-43-907/01/16 23:550.071 0.036 1 Chromium 8.1 mg/kg 07/06/16 16:59 7440-47-307/01/16 23:550.36 0.18 1 Lead 19.5 mg/kg 07/06/16 16:59 7439-92-107/01/16 23:550.36 0.18 1 Selenium 0.92 mg/kg 07/06/16 16:59 7782-49-207/01/16 23:550.71 0.36 1 Silver ND mg/kg 07/06/16 16:59 7440-22-407/01/16 23:550.36 0.18 1 Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury Mercury 0.047 mg/kg 07/12/16 10:51 7439-97-607/08/16 05:150.0026 0.000051 1 Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave Acenaphthene ND ug/kg 07/08/16 14:30 83-32-906/30/16 14:23396 91.1 1 Acenaphthylene ND ug/kg 07/08/16 14:30 208-96-806/30/16 14:23396 93.5 1 Aniline ND ug/kg 07/08/16 14:30 62-53-306/30/16 14:23396 107 1 Anthracene ND ug/kg 07/08/16 14:30 120-12-706/30/16 14:23396 88.7 1 Benzo(a)anthracene 78.8J ug/kg 07/08/16 14:30 56-55-306/30/16 14:23396 73.1 1 Benzo(a)pyrene ND ug/kg 07/08/16 14:30 50-32-806/30/16 14:23396 75.5 1 Benzo(b)fluoranthene 98.3J ug/kg 07/08/16 14:30 205-99-206/30/16 14:23396 68.3 1 Benzo(g,h,i)perylene ND ug/kg 07/08/16 14:30 191-24-206/30/16 14:23396 101 1 Benzo(k)fluoranthene ND ug/kg 07/08/16 14:30 207-08-906/30/16 14:23396 77.9 1 Benzoic Acid ND ug/kg 07/08/16 14:30 65-85-006/30/16 14:231980 71.9 1 Benzyl alcohol ND ug/kg 07/08/16 14:30 100-51-606/30/16 14:23791 79.1 1 4-Bromophenylphenyl ether ND ug/kg 07/08/16 14:30 101-55-306/30/16 14:23396 71.9 1 Butylbenzylphthalate ND ug/kg 07/08/16 14:30 85-68-706/30/16 14:23396 83.9 1 4-Chloro-3-methylphenol ND ug/kg 07/08/16 14:30 59-50-706/30/16 14:23791 81.5 1 4-Chloroaniline ND ug/kg 07/08/16 14:30 106-47-806/30/16 14:231980 110 1 bis(2-Chloroethoxy)methane ND ug/kg 07/08/16 14:30 111-91-106/30/16 14:23396 92.3 1 bis(2-Chloroethyl) ether ND ug/kg 07/08/16 14:30 111-44-406/30/16 14:23396 101 1 2-Chloronaphthalene ND ug/kg 07/08/16 14:30 91-58-706/30/16 14:23396 77.9 1 2-Chlorophenol ND ug/kg 07/08/16 14:30 95-57-806/30/16 14:23396 108 1 4-Chlorophenylphenyl ether ND ug/kg 07/08/16 14:30 7005-72-306/30/16 14:23396 81.5 1 Chrysene 77.3J ug/kg 07/08/16 14:30 218-01-906/30/16 14:23396 52.7 1 Dibenz(a,h)anthracene ND ug/kg 07/08/16 14:30 53-70-306/30/16 14:23396 83.9 1 Dibenzofuran ND ug/kg 07/08/16 14:30 132-64-906/30/16 14:23396 64.7 1 1,2-Dichlorobenzene ND ug/kg 07/08/16 14:30 95-50-106/30/16 14:23396 105 1 1,3-Dichlorobenzene ND ug/kg 07/08/16 14:30 541-73-106/30/16 14:23396 89.9 1 1,4-Dichlorobenzene ND ug/kg 07/08/16 14:30 106-46-706/30/16 14:23396 111 1 3,3'-Dichlorobenzidine ND ug/kg 07/08/16 14:30 91-94-106/30/16 14:231980 86.3 1 2,4-Dichlorophenol ND ug/kg 07/08/16 14:30 120-83-206/30/16 14:23396 86.3 1 Diethylphthalate ND ug/kg 07/08/16 14:30 84-66-206/30/16 14:23396 61.1 1 2,4-Dimethylphenol ND ug/kg 07/08/16 14:30 105-67-906/30/16 14:23396 156 1 Dimethylphthalate ND ug/kg 07/08/16 14:30 131-11-306/30/16 14:23396 80.3 1 Di-n-butylphthalate ND ug/kg 07/08/16 14:30 84-74-206/30/16 14:23396 64.7 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/08/16 14:30 534-52-106/30/16 14:23791 79.1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-15 (3.5-6.5)Lab ID: 92303397003 Collected: 06/27/16 15:40 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave 2,4-Dinitrophenol ND ug/kg 07/08/16 14:30 51-28-506/30/16 14:231980 64.7 1 2,4-Dinitrotoluene ND ug/kg 07/08/16 14:30 121-14-206/30/16 14:23396 74.3 1 2,6-Dinitrotoluene ND ug/kg 07/08/16 14:30 606-20-206/30/16 14:23396 82.7 1 Di-n-octylphthalate ND ug/kg 07/08/16 14:30 117-84-006/30/16 14:23396 82.7 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/08/16 14:30 117-81-706/30/16 14:23396 108 1 Fluoranthene 215J ug/kg 07/08/16 14:30 206-44-006/30/16 14:23396 57.5 1 Fluorene ND ug/kg 07/08/16 14:30 86-73-706/30/16 14:23396 81.5 1 Hexachloro-1,3-butadiene ND ug/kg 07/08/16 14:30 87-68-306/30/16 14:23396 68.3 1 Hexachlorobenzene ND ug/kg 07/08/16 14:30 118-74-106/30/16 14:23396 50.3 1 Hexachlorocyclopentadiene ND ug/kg 07/08/16 14:30 77-47-406/30/16 14:23396 73.1 1 Hexachloroethane ND ug/kg 07/08/16 14:30 67-72-106/30/16 14:23396 104 1 Indeno(1,2,3-cd)pyrene ND ug/kg 07/08/16 14:30 193-39-506/30/16 14:23396 81.5 1 Isophorone ND ug/kg 07/08/16 14:30 78-59-106/30/16 14:23396 88.7 1 1-Methylnaphthalene ND ug/kg 07/08/16 14:30 90-12-006/30/16 14:23396 103 1 2-Methylnaphthalene 122J ug/kg 07/08/16 14:30 91-57-606/30/16 14:23396 85.1 1 2-Methylphenol(o-Cresol)ND ug/kg 07/08/16 14:30 95-48-706/30/16 14:23396 120 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/08/16 14:3006/30/16 14:23396 156 1 Naphthalene ND ug/kg 07/08/16 14:30 91-20-306/30/16 14:23396 97.1 1 2-Nitroaniline ND ug/kg 07/08/16 14:30 88-74-406/30/16 14:231980 122 1 3-Nitroaniline ND ug/kg 07/08/16 14:30 99-09-206/30/16 14:231980 108 1 4-Nitroaniline ND ug/kg 07/08/16 14:30 100-01-606/30/16 14:23791 111 1 Nitrobenzene ND ug/kg 07/08/16 14:30 98-95-306/30/16 14:23396 108 1 2-Nitrophenol ND ug/kg 07/08/16 14:30 88-75-506/30/16 14:23396 95.9 1 4-Nitrophenol ND ug/kg 07/08/16 14:30 100-02-706/30/16 14:231980 70.7 1 N-Nitrosodimethylamine ND ug/kg 07/08/16 14:30 62-75-906/30/16 14:23396 128 1 N-Nitroso-di-n-propylamine ND ug/kg 07/08/16 14:30 621-64-706/30/16 14:23396 75.5 1 N-Nitrosodiphenylamine ND ug/kg 07/08/16 14:30 86-30-606/30/16 14:23396 117 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/08/16 14:30 108-60-106/30/16 14:23396 105 1 Pentachlorophenol ND ug/kg 07/08/16 14:30 87-86-506/30/16 14:231980 71.9 1 Phenanthrene 147J ug/kg 07/08/16 14:30 85-01-806/30/16 14:23396 65.9 1 Phenol ND ug/kg 07/08/16 14:3006/30/16 14:23396 119 1 Pyrene 132J ug/kg 07/08/16 14:30 129-00-006/30/16 14:23396 67.1 1 1,2,4-Trichlorobenzene ND ug/kg 07/08/16 14:30 120-82-106/30/16 14:23396 76.7 1 2,4,5-Trichlorophenol ND ug/kg 07/08/16 14:30 95-95-406/30/16 14:23396 122 1 2,4,6-Trichlorophenol ND ug/kg 07/08/16 14:30 88-06-206/30/16 14:23396 87.5 1 Surrogates Nitrobenzene-d5 (S)54 %07/08/16 14:30 4165-60-006/30/16 14:2323-110 1 2-Fluorobiphenyl (S)49 %07/08/16 14:30 321-60-806/30/16 14:2330-110 1 Terphenyl-d14 (S)67 %07/08/16 14:30 1718-51-006/30/16 14:2328-110 1 Phenol-d6 (S)59 %07/08/16 14:30 13127-88-306/30/16 14:2322-110 1 2-Fluorophenol (S)56 %07/08/16 14:30 367-12-406/30/16 14:2313-110 1 2,4,6-Tribromophenol (S)69 %07/08/16 14:30 118-79-606/30/16 14:2327-110 1 Analytical Method: EPA 82608260/5035A Volatile Organics Acetone 23.6J ug/kg 07/07/16 22:14 67-64-196.2 9.6 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-15 (3.5-6.5)Lab ID: 92303397003 Collected: 06/27/16 15:40 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260/5035A Volatile Organics Benzene ND ug/kg 07/07/16 22:14 71-43-24.8 1.5 1 Bromobenzene ND ug/kg 07/07/16 22:14 108-86-14.8 1.9 1 Bromochloromethane ND ug/kg 07/07/16 22:14 74-97-54.8 1.6 1 Bromodichloromethane ND ug/kg 07/07/16 22:14 75-27-44.8 1.8 1 Bromoform ND ug/kg 07/07/16 22:14 75-25-24.8 2.2 1 Bromomethane ND ug/kg 07/07/16 22:14 74-83-99.6 2.4 1 2-Butanone (MEK)ND ug/kg 07/07/16 22:14 78-93-396.2 2.8 1 n-Butylbenzene ND ug/kg 07/07/16 22:14 104-51-84.8 1.7 1 sec-Butylbenzene ND ug/kg 07/07/16 22:14 135-98-84.8 1.5 1 tert-Butylbenzene ND ug/kg 07/07/16 22:14 98-06-64.8 1.9 1 Carbon tetrachloride ND ug/kg 07/07/16 22:14 56-23-54.8 2.5 1 Chlorobenzene ND ug/kg 07/07/16 22:14 108-90-74.8 1.8 1 Chloroethane ND ug/kg 07/07/16 22:14 75-00-39.6 2.3 1 Chloroform ND ug/kg 07/07/16 22:14 67-66-34.8 1.5 1 Chloromethane ND ug/kg 07/07/16 22:14 74-87-39.6 2.3 1 2-Chlorotoluene ND ug/kg 07/07/16 22:14 95-49-84.8 1.6 1 4-Chlorotoluene ND ug/kg 07/07/16 22:14 106-43-44.8 1.7 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/07/16 22:14 96-12-84.8 3.5 1 Dibromochloromethane ND ug/kg 07/07/16 22:14 124-48-14.8 1.7 1 1,2-Dibromoethane (EDB)ND ug/kg 07/07/16 22:14 106-93-44.8 1.7 1 Dibromomethane ND ug/kg 07/07/16 22:14 74-95-34.8 2.4 1 1,2-Dichlorobenzene ND ug/kg 07/07/16 22:14 95-50-14.8 1.8 1 1,3-Dichlorobenzene ND ug/kg 07/07/16 22:14 541-73-14.8 1.9 1 1,4-Dichlorobenzene ND ug/kg 07/07/16 22:14 106-46-74.8 1.6 1 Dichlorodifluoromethane ND ug/kg 07/07/16 22:14 75-71-89.6 3.5 1 1,1-Dichloroethane ND ug/kg 07/07/16 22:14 75-34-34.8 1.4 1 1,2-Dichloroethane ND ug/kg 07/07/16 22:14 107-06-24.8 2.1 1 1,1-Dichloroethene ND ug/kg 07/07/16 22:14 75-35-44.8 1.7 1 cis-1,2-Dichloroethene 1.4J ug/kg 07/07/16 22:14 156-59-24.8 1.3 1 trans-1,2-Dichloroethene ND ug/kg 07/07/16 22:14 156-60-54.8 1.8 1 1,2-Dichloropropane ND ug/kg 07/07/16 22:14 78-87-54.8 1.6 1 1,3-Dichloropropane ND ug/kg 07/07/16 22:14 142-28-94.8 1.8 1 2,2-Dichloropropane ND ug/kg 07/07/16 22:14 594-20-74.8 1.6 1 1,1-Dichloropropene ND ug/kg 07/07/16 22:14 563-58-64.8 1.4 1 cis-1,3-Dichloropropene ND ug/kg 07/07/16 22:14 10061-01-54.8 1.7 1 trans-1,3-Dichloropropene ND ug/kg 07/07/16 22:14 10061-02-64.8 1.4 1 Diisopropyl ether ND ug/kg 07/07/16 22:14 108-20-34.8 1.6 1 Ethylbenzene ND ug/kg 07/07/16 22:14 100-41-44.8 1.7 1 Hexachloro-1,3-butadiene ND ug/kg 07/07/16 22:14 87-68-34.8 1.9 1 2-Hexanone ND ug/kg 07/07/16 22:14 591-78-648.1 3.8 1 Isopropylbenzene (Cumene)ND ug/kg 07/07/16 22:14 98-82-84.8 1.8 1 p-Isopropyltoluene ND ug/kg 07/07/16 22:14 99-87-64.8 1.6 1 Methylene Chloride ND ug/kg 07/07/16 22:14 75-09-219.2 2.9 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/07/16 22:14 108-10-148.1 3.6 1 Methyl-tert-butyl ether ND ug/kg 07/07/16 22:14 1634-04-44.8 1.4 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-15 (3.5-6.5)Lab ID: 92303397003 Collected: 06/27/16 15:40 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260/5035A Volatile Organics Naphthalene 1.2J ug/kg 07/07/16 22:14 91-20-34.8 1.2 1 n-Propylbenzene ND ug/kg 07/07/16 22:14 103-65-14.8 1.6 1 Styrene ND ug/kg 07/07/16 22:14 100-42-54.8 1.7 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/07/16 22:14 630-20-64.8 2.0 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/07/16 22:14 79-34-54.8 1.8 1 Tetrachloroethene ND ug/kg 07/07/16 22:14 127-18-44.8 1.6 1 Toluene ND ug/kg 07/07/16 22:14 108-88-34.8 1.7 1 1,2,3-Trichlorobenzene ND ug/kg 07/07/16 22:14 87-61-64.8 2.1 1 1,2,4-Trichlorobenzene ND ug/kg 07/07/16 22:14 120-82-14.8 1.5 1 1,1,1-Trichloroethane ND ug/kg 07/07/16 22:14 71-55-64.8 1.7 1 1,1,2-Trichloroethane ND ug/kg 07/07/16 22:14 79-00-54.8 2.0 1 Trichloroethene 2.8J ug/kg 07/07/16 22:14 79-01-64.8 2.0 1 Trichlorofluoromethane ND ug/kg 07/07/16 22:14 75-69-44.8 2.1 1 1,2,3-Trichloropropane ND ug/kg 07/07/16 22:14 96-18-44.8 1.5 1 1,2,4-Trimethylbenzene ND ug/kg 07/07/16 22:14 95-63-64.8 1.9 1 1,3,5-Trimethylbenzene ND ug/kg 07/07/16 22:14 108-67-84.8 1.7 1 Vinyl acetate ND ug/kg 07/07/16 22:14 108-05-448.1 8.5 1 Vinyl chloride ND ug/kg 07/07/16 22:14 75-01-49.6 1.7 1 Xylene (Total)ND ug/kg 07/07/16 22:14 1330-20-79.6 3.5 1 m&p-Xylene ND ug/kg 07/07/16 22:14 179601-23-19.6 3.5 1 o-Xylene ND ug/kg 07/07/16 22:14 95-47-64.8 1.8 1 Surrogates Toluene-d8 (S)109 %07/07/16 22:14 2037-26-570-130 1 4-Bromofluorobenzene (S)98 %07/07/16 22:14 460-00-470-130 1 1,2-Dichloroethane-d4 (S)80 %07/07/16 22:14 17060-07-070-132 1 Analytical Method: ASTM D2974-87Percent Moisture Percent Moisture 16.6 %06/30/16 14:000.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-16 (1-2.5)Lab ID: 92303397004 Collected: 06/28/16 08:15 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP Arsenic 4.6J mg/kg 07/07/16 14:49 7440-38-2 D307/01/16 23:555.0 2.5 5 Barium 148 mg/kg 07/07/16 14:49 7440-39-307/01/16 23:552.5 1.3 5 Cadmium ND mg/kg 07/07/16 14:49 7440-43-9 D307/01/16 23:550.50 0.25 5 Chromium 21.0 mg/kg 07/07/16 14:49 7440-47-307/01/16 23:552.5 1.3 5 Lead 21.2 mg/kg 07/07/16 14:49 7439-92-107/01/16 23:552.5 1.3 5 Selenium ND mg/kg 07/07/16 14:49 7782-49-2 D307/01/16 23:555.0 2.5 5 Silver ND mg/kg 07/07/16 14:49 7440-22-4 D307/01/16 23:552.5 1.3 5 Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury Mercury 0.011 mg/kg 07/12/16 10:53 7439-97-607/08/16 05:150.0040 0.000080 1 Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave Acenaphthene ND ug/kg 07/08/16 10:38 83-32-906/30/16 14:23413 95.1 1 Acenaphthylene ND ug/kg 07/08/16 10:38 208-96-806/30/16 14:23413 97.6 1 Aniline ND ug/kg 07/08/16 10:38 62-53-306/30/16 14:23413 111 1 Anthracene ND ug/kg 07/08/16 10:38 120-12-706/30/16 14:23413 92.6 1 Benzo(a)anthracene ND ug/kg 07/08/16 10:38 56-55-306/30/16 14:23413 76.4 1 Benzo(a)pyrene ND ug/kg 07/08/16 10:38 50-32-806/30/16 14:23413 78.9 1 Benzo(b)fluoranthene ND ug/kg 07/08/16 10:38 205-99-206/30/16 14:23413 71.3 1 Benzo(g,h,i)perylene ND ug/kg 07/08/16 10:38 191-24-206/30/16 14:23413 105 1 Benzo(k)fluoranthene ND ug/kg 07/08/16 10:38 207-08-906/30/16 14:23413 81.4 1 Benzoic Acid ND ug/kg 07/08/16 10:38 65-85-006/30/16 14:232070 75.1 1 Benzyl alcohol ND ug/kg 07/08/16 10:38 100-51-606/30/16 14:23826 82.6 1 4-Bromophenylphenyl ether ND ug/kg 07/08/16 10:38 101-55-306/30/16 14:23413 75.1 1 Butylbenzylphthalate ND ug/kg 07/08/16 10:38 85-68-706/30/16 14:23413 87.6 1 4-Chloro-3-methylphenol ND ug/kg 07/08/16 10:38 59-50-706/30/16 14:23826 85.1 1 4-Chloroaniline ND ug/kg 07/08/16 10:38 106-47-806/30/16 14:232070 115 1 bis(2-Chloroethoxy)methane ND ug/kg 07/08/16 10:38 111-91-106/30/16 14:23413 96.4 1 bis(2-Chloroethyl) ether ND ug/kg 07/08/16 10:38 111-44-406/30/16 14:23413 105 1 2-Chloronaphthalene ND ug/kg 07/08/16 10:38 91-58-706/30/16 14:23413 81.4 1 2-Chlorophenol ND ug/kg 07/08/16 10:38 95-57-806/30/16 14:23413 113 1 4-Chlorophenylphenyl ether ND ug/kg 07/08/16 10:38 7005-72-306/30/16 14:23413 85.1 1 Chrysene ND ug/kg 07/08/16 10:38 218-01-906/30/16 14:23413 55.1 1 Dibenz(a,h)anthracene ND ug/kg 07/08/16 10:38 53-70-306/30/16 14:23413 87.6 1 Dibenzofuran ND ug/kg 07/08/16 10:38 132-64-906/30/16 14:23413 67.6 1 1,2-Dichlorobenzene ND ug/kg 07/08/16 10:38 95-50-106/30/16 14:23413 110 1 1,3-Dichlorobenzene ND ug/kg 07/08/16 10:38 541-73-106/30/16 14:23413 93.9 1 1,4-Dichlorobenzene ND ug/kg 07/08/16 10:38 106-46-706/30/16 14:23413 116 1 3,3'-Dichlorobenzidine ND ug/kg 07/08/16 10:38 91-94-106/30/16 14:232070 90.1 1 2,4-Dichlorophenol ND ug/kg 07/08/16 10:38 120-83-206/30/16 14:23413 90.1 1 Diethylphthalate ND ug/kg 07/08/16 10:38 84-66-206/30/16 14:23413 63.8 1 2,4-Dimethylphenol ND ug/kg 07/08/16 10:38 105-67-906/30/16 14:23413 163 1 Dimethylphthalate ND ug/kg 07/08/16 10:38 131-11-306/30/16 14:23413 83.9 1 Di-n-butylphthalate ND ug/kg 07/08/16 10:38 84-74-206/30/16 14:23413 67.6 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/08/16 10:38 534-52-106/30/16 14:23826 82.6 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-16 (1-2.5)Lab ID: 92303397004 Collected: 06/28/16 08:15 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave 2,4-Dinitrophenol ND ug/kg 07/08/16 10:38 51-28-506/30/16 14:232070 67.6 1 2,4-Dinitrotoluene ND ug/kg 07/08/16 10:38 121-14-206/30/16 14:23413 77.6 1 2,6-Dinitrotoluene ND ug/kg 07/08/16 10:38 606-20-206/30/16 14:23413 86.4 1 Di-n-octylphthalate ND ug/kg 07/08/16 10:38 117-84-006/30/16 14:23413 86.4 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/08/16 10:38 117-81-706/30/16 14:23413 113 1 Fluoranthene ND ug/kg 07/08/16 10:38 206-44-006/30/16 14:23413 60.1 1 Fluorene ND ug/kg 07/08/16 10:38 86-73-706/30/16 14:23413 85.1 1 Hexachloro-1,3-butadiene ND ug/kg 07/08/16 10:38 87-68-306/30/16 14:23413 71.3 1 Hexachlorobenzene ND ug/kg 07/08/16 10:38 118-74-106/30/16 14:23413 52.6 1 Hexachlorocyclopentadiene ND ug/kg 07/08/16 10:38 77-47-406/30/16 14:23413 76.4 1 Hexachloroethane ND ug/kg 07/08/16 10:38 67-72-106/30/16 14:23413 109 1 Indeno(1,2,3-cd)pyrene ND ug/kg 07/08/16 10:38 193-39-506/30/16 14:23413 85.1 1 Isophorone ND ug/kg 07/08/16 10:38 78-59-106/30/16 14:23413 92.6 1 1-Methylnaphthalene ND ug/kg 07/08/16 10:38 90-12-006/30/16 14:23413 108 1 2-Methylnaphthalene ND ug/kg 07/08/16 10:38 91-57-606/30/16 14:23413 88.9 1 2-Methylphenol(o-Cresol)ND ug/kg 07/08/16 10:38 95-48-706/30/16 14:23413 125 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/08/16 10:3806/30/16 14:23413 163 1 Naphthalene ND ug/kg 07/08/16 10:38 91-20-306/30/16 14:23413 101 1 2-Nitroaniline ND ug/kg 07/08/16 10:38 88-74-406/30/16 14:232070 128 1 3-Nitroaniline ND ug/kg 07/08/16 10:38 99-09-206/30/16 14:232070 113 1 4-Nitroaniline ND ug/kg 07/08/16 10:38 100-01-606/30/16 14:23826 116 1 Nitrobenzene ND ug/kg 07/08/16 10:38 98-95-306/30/16 14:23413 113 1 2-Nitrophenol ND ug/kg 07/08/16 10:38 88-75-506/30/16 14:23413 100 1 4-Nitrophenol ND ug/kg 07/08/16 10:38 100-02-706/30/16 14:232070 73.8 1 N-Nitrosodimethylamine ND ug/kg 07/08/16 10:38 62-75-906/30/16 14:23413 134 1 N-Nitroso-di-n-propylamine ND ug/kg 07/08/16 10:38 621-64-706/30/16 14:23413 78.9 1 N-Nitrosodiphenylamine ND ug/kg 07/08/16 10:38 86-30-606/30/16 14:23413 123 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/08/16 10:38 108-60-106/30/16 14:23413 110 1 Pentachlorophenol ND ug/kg 07/08/16 10:38 87-86-506/30/16 14:232070 75.1 1 Phenanthrene ND ug/kg 07/08/16 10:38 85-01-806/30/16 14:23413 68.8 1 Phenol ND ug/kg 07/08/16 10:3806/30/16 14:23413 124 1 Pyrene ND ug/kg 07/08/16 10:38 129-00-006/30/16 14:23413 70.1 1 1,2,4-Trichlorobenzene ND ug/kg 07/08/16 10:38 120-82-106/30/16 14:23413 80.1 1 2,4,5-Trichlorophenol ND ug/kg 07/08/16 10:38 95-95-406/30/16 14:23413 128 1 2,4,6-Trichlorophenol ND ug/kg 07/08/16 10:38 88-06-206/30/16 14:23413 91.4 1 Surrogates Nitrobenzene-d5 (S)67 %07/08/16 10:38 4165-60-006/30/16 14:2323-110 1 2-Fluorobiphenyl (S)66 %07/08/16 10:38 321-60-806/30/16 14:2330-110 1 Terphenyl-d14 (S)72 %07/08/16 10:38 1718-51-006/30/16 14:2328-110 1 Phenol-d6 (S)78 %07/08/16 10:38 13127-88-306/30/16 14:2322-110 1 2-Fluorophenol (S)70 %07/08/16 10:38 367-12-406/30/16 14:2313-110 1 2,4,6-Tribromophenol (S)78 %07/08/16 10:38 118-79-606/30/16 14:2327-110 1 Analytical Method: EPA 82608260/5035A Volatile Organics Acetone 30.5J ug/kg 07/07/16 22:34 67-64-197.2 9.7 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-16 (1-2.5)Lab ID: 92303397004 Collected: 06/28/16 08:15 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260/5035A Volatile Organics Benzene ND ug/kg 07/07/16 22:34 71-43-24.9 1.6 1 Bromobenzene ND ug/kg 07/07/16 22:34 108-86-14.9 1.9 1 Bromochloromethane ND ug/kg 07/07/16 22:34 74-97-54.9 1.7 1 Bromodichloromethane ND ug/kg 07/07/16 22:34 75-27-44.9 1.8 1 Bromoform ND ug/kg 07/07/16 22:34 75-25-24.9 2.2 1 Bromomethane ND ug/kg 07/07/16 22:34 74-83-99.7 2.4 1 2-Butanone (MEK)ND ug/kg 07/07/16 22:34 78-93-397.2 2.8 1 n-Butylbenzene ND ug/kg 07/07/16 22:34 104-51-84.9 1.7 1 sec-Butylbenzene ND ug/kg 07/07/16 22:34 135-98-84.9 1.6 1 tert-Butylbenzene ND ug/kg 07/07/16 22:34 98-06-64.9 1.9 1 Carbon tetrachloride ND ug/kg 07/07/16 22:34 56-23-54.9 2.5 1 Chlorobenzene ND ug/kg 07/07/16 22:34 108-90-74.9 1.8 1 Chloroethane ND ug/kg 07/07/16 22:34 75-00-39.7 2.3 1 Chloroform ND ug/kg 07/07/16 22:34 67-66-34.9 1.6 1 Chloromethane ND ug/kg 07/07/16 22:34 74-87-39.7 2.3 1 2-Chlorotoluene ND ug/kg 07/07/16 22:34 95-49-84.9 1.7 1 4-Chlorotoluene ND ug/kg 07/07/16 22:34 106-43-44.9 1.7 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/07/16 22:34 96-12-84.9 3.5 1 Dibromochloromethane ND ug/kg 07/07/16 22:34 124-48-14.9 1.7 1 1,2-Dibromoethane (EDB)ND ug/kg 07/07/16 22:34 106-93-44.9 1.7 1 Dibromomethane ND ug/kg 07/07/16 22:34 74-95-34.9 2.4 1 1,2-Dichlorobenzene ND ug/kg 07/07/16 22:34 95-50-14.9 1.8 1 1,3-Dichlorobenzene ND ug/kg 07/07/16 22:34 541-73-14.9 1.9 1 1,4-Dichlorobenzene ND ug/kg 07/07/16 22:34 106-46-74.9 1.7 1 Dichlorodifluoromethane ND ug/kg 07/07/16 22:34 75-71-89.7 3.5 1 1,1-Dichloroethane ND ug/kg 07/07/16 22:34 75-34-34.9 1.5 1 1,2-Dichloroethane ND ug/kg 07/07/16 22:34 107-06-24.9 2.1 1 1,1-Dichloroethene ND ug/kg 07/07/16 22:34 75-35-44.9 1.7 1 cis-1,2-Dichloroethene ND ug/kg 07/07/16 22:34 156-59-24.9 1.4 1 trans-1,2-Dichloroethene ND ug/kg 07/07/16 22:34 156-60-54.9 1.8 1 1,2-Dichloropropane ND ug/kg 07/07/16 22:34 78-87-54.9 1.7 1 1,3-Dichloropropane ND ug/kg 07/07/16 22:34 142-28-94.9 1.8 1 2,2-Dichloropropane ND ug/kg 07/07/16 22:34 594-20-74.9 1.7 1 1,1-Dichloropropene ND ug/kg 07/07/16 22:34 563-58-64.9 1.5 1 cis-1,3-Dichloropropene ND ug/kg 07/07/16 22:34 10061-01-54.9 1.7 1 trans-1,3-Dichloropropene ND ug/kg 07/07/16 22:34 10061-02-64.9 1.5 1 Diisopropyl ether ND ug/kg 07/07/16 22:34 108-20-34.9 1.7 1 Ethylbenzene ND ug/kg 07/07/16 22:34 100-41-44.9 1.7 1 Hexachloro-1,3-butadiene ND ug/kg 07/07/16 22:34 87-68-34.9 1.9 1 2-Hexanone ND ug/kg 07/07/16 22:34 591-78-648.6 3.8 1 Isopropylbenzene (Cumene)ND ug/kg 07/07/16 22:34 98-82-84.9 1.8 1 p-Isopropyltoluene ND ug/kg 07/07/16 22:34 99-87-64.9 1.7 1 Methylene Chloride 3.7J ug/kg 07/07/16 22:34 75-09-219.4 2.9 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/07/16 22:34 108-10-148.6 3.6 1 Methyl-tert-butyl ether ND ug/kg 07/07/16 22:34 1634-04-44.9 1.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-16 (1-2.5)Lab ID: 92303397004 Collected: 06/28/16 08:15 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260/5035A Volatile Organics Naphthalene ND ug/kg 07/07/16 22:34 91-20-34.9 1.2 1 n-Propylbenzene ND ug/kg 07/07/16 22:34 103-65-14.9 1.7 1 Styrene ND ug/kg 07/07/16 22:34 100-42-54.9 1.7 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/07/16 22:34 630-20-64.9 2.0 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/07/16 22:34 79-34-54.9 1.8 1 Tetrachloroethene ND ug/kg 07/07/16 22:34 127-18-44.9 1.7 1 Toluene ND ug/kg 07/07/16 22:34 108-88-34.9 1.7 1 1,2,3-Trichlorobenzene ND ug/kg 07/07/16 22:34 87-61-64.9 2.1 1 1,2,4-Trichlorobenzene ND ug/kg 07/07/16 22:34 120-82-14.9 1.6 1 1,1,1-Trichloroethane ND ug/kg 07/07/16 22:34 71-55-64.9 1.7 1 1,1,2-Trichloroethane ND ug/kg 07/07/16 22:34 79-00-54.9 2.0 1 Trichloroethene ND ug/kg 07/07/16 22:34 79-01-64.9 2.0 1 Trichlorofluoromethane ND ug/kg 07/07/16 22:34 75-69-44.9 2.1 1 1,2,3-Trichloropropane ND ug/kg 07/07/16 22:34 96-18-44.9 1.6 1 1,2,4-Trimethylbenzene ND ug/kg 07/07/16 22:34 95-63-64.9 1.9 1 1,3,5-Trimethylbenzene ND ug/kg 07/07/16 22:34 108-67-84.9 1.7 1 Vinyl acetate ND ug/kg 07/07/16 22:34 108-05-448.6 8.6 1 Vinyl chloride ND ug/kg 07/07/16 22:34 75-01-49.7 1.7 1 Xylene (Total)ND ug/kg 07/07/16 22:34 1330-20-79.7 3.5 1 m&p-Xylene ND ug/kg 07/07/16 22:34 179601-23-19.7 3.5 1 o-Xylene ND ug/kg 07/07/16 22:34 95-47-64.9 1.8 1 Surrogates Toluene-d8 (S)102 %07/07/16 22:34 2037-26-570-130 1 4-Bromofluorobenzene (S)95 %07/07/16 22:34 460-00-470-130 1 1,2-Dichloroethane-d4 (S)85 %07/07/16 22:34 17060-07-070-132 1 Analytical Method: ASTM D2974-87Percent Moisture Percent Moisture 20.1 %06/30/16 14:000.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-2 (1-2.5)Lab ID: 92303397005 Collected: 06/28/16 11:40 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP Arsenic 2.5 mg/kg 07/06/16 17:15 7440-38-207/01/16 23:550.81 0.41 1 Barium 106 mg/kg 07/06/16 17:15 7440-39-307/01/16 23:550.41 0.20 1 Cadmium ND mg/kg 07/06/16 17:15 7440-43-907/01/16 23:550.081 0.041 1 Chromium 11.7 mg/kg 07/06/16 17:15 7440-47-307/01/16 23:550.41 0.20 1 Lead 7.5 mg/kg 07/06/16 17:15 7439-92-107/01/16 23:550.41 0.20 1 Selenium 0.50J mg/kg 07/06/16 17:15 7782-49-207/01/16 23:550.81 0.41 1 Silver ND mg/kg 07/06/16 17:15 7440-22-407/01/16 23:550.41 0.20 1 Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury Mercury 0.00041J mg/kg 07/12/16 10:56 7439-97-607/08/16 05:150.0022 0.000044 1 Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave Acenaphthene ND ug/kg 07/06/16 20:25 83-32-906/30/16 14:23376 86.6 1 Acenaphthylene ND ug/kg 07/06/16 20:25 208-96-806/30/16 14:23376 88.9 1 Aniline ND ug/kg 07/06/16 20:25 62-53-306/30/16 14:23376 101 1 Anthracene ND ug/kg 07/06/16 20:25 120-12-706/30/16 14:23376 84.3 1 Benzo(a)anthracene ND ug/kg 07/06/16 20:25 56-55-306/30/16 14:23376 69.5 1 Benzo(a)pyrene ND ug/kg 07/06/16 20:25 50-32-806/30/16 14:23376 71.8 1 Benzo(b)fluoranthene ND ug/kg 07/06/16 20:25 205-99-206/30/16 14:23376 65.0 1 Benzo(g,h,i)perylene ND ug/kg 07/06/16 20:25 191-24-206/30/16 14:23376 95.7 1 Benzo(k)fluoranthene ND ug/kg 07/06/16 20:25 207-08-906/30/16 14:23376 74.1 1 Benzoic Acid ND ug/kg 07/06/16 20:25 65-85-006/30/16 14:231880 68.4 1 Benzyl alcohol ND ug/kg 07/06/16 20:25 100-51-606/30/16 14:23752 75.2 1 4-Bromophenylphenyl ether ND ug/kg 07/06/16 20:25 101-55-306/30/16 14:23376 68.4 1 Butylbenzylphthalate ND ug/kg 07/06/16 20:25 85-68-706/30/16 14:23376 79.8 1 4-Chloro-3-methylphenol ND ug/kg 07/06/16 20:25 59-50-706/30/16 14:23752 77.5 1 4-Chloroaniline ND ug/kg 07/06/16 20:25 106-47-806/30/16 14:231880 105 1 bis(2-Chloroethoxy)methane ND ug/kg 07/06/16 20:25 111-91-106/30/16 14:23376 87.8 1 bis(2-Chloroethyl) ether ND ug/kg 07/06/16 20:25 111-44-406/30/16 14:23376 95.7 1 2-Chloronaphthalene ND ug/kg 07/06/16 20:25 91-58-706/30/16 14:23376 74.1 1 2-Chlorophenol ND ug/kg 07/06/16 20:25 95-57-806/30/16 14:23376 103 1 4-Chlorophenylphenyl ether ND ug/kg 07/06/16 20:25 7005-72-306/30/16 14:23376 77.5 1 Chrysene ND ug/kg 07/06/16 20:25 218-01-906/30/16 14:23376 50.1 1 Dibenz(a,h)anthracene ND ug/kg 07/06/16 20:25 53-70-306/30/16 14:23376 79.8 1 Dibenzofuran ND ug/kg 07/06/16 20:25 132-64-906/30/16 14:23376 61.5 1 1,2-Dichlorobenzene ND ug/kg 07/06/16 20:25 95-50-106/30/16 14:23376 100 1 1,3-Dichlorobenzene ND ug/kg 07/06/16 20:25 541-73-106/30/16 14:23376 85.5 1 1,4-Dichlorobenzene ND ug/kg 07/06/16 20:25 106-46-706/30/16 14:23376 106 1 3,3'-Dichlorobenzidine ND ug/kg 07/06/16 20:25 91-94-106/30/16 14:231880 82.1 1 2,4-Dichlorophenol ND ug/kg 07/06/16 20:25 120-83-206/30/16 14:23376 82.1 1 Diethylphthalate ND ug/kg 07/06/16 20:25 84-66-206/30/16 14:23376 58.1 1 2,4-Dimethylphenol ND ug/kg 07/06/16 20:25 105-67-906/30/16 14:23376 148 1 Dimethylphthalate ND ug/kg 07/06/16 20:25 131-11-306/30/16 14:23376 76.4 1 Di-n-butylphthalate ND ug/kg 07/06/16 20:25 84-74-206/30/16 14:23376 61.5 1 4,6-Dinitro-2-methylphenol ND ug/kg 07/06/16 20:25 534-52-106/30/16 14:23752 75.2 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-2 (1-2.5)Lab ID: 92303397005 Collected: 06/28/16 11:40 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave 2,4-Dinitrophenol ND ug/kg 07/06/16 20:25 51-28-506/30/16 14:231880 61.5 1 2,4-Dinitrotoluene ND ug/kg 07/06/16 20:25 121-14-206/30/16 14:23376 70.7 1 2,6-Dinitrotoluene ND ug/kg 07/06/16 20:25 606-20-206/30/16 14:23376 78.6 1 Di-n-octylphthalate ND ug/kg 07/06/16 20:25 117-84-006/30/16 14:23376 78.6 1 bis(2-Ethylhexyl)phthalate ND ug/kg 07/06/16 20:25 117-81-706/30/16 14:23376 103 1 Fluoranthene ND ug/kg 07/06/16 20:25 206-44-006/30/16 14:23376 54.7 1 Fluorene ND ug/kg 07/06/16 20:25 86-73-706/30/16 14:23376 77.5 1 Hexachloro-1,3-butadiene ND ug/kg 07/06/16 20:25 87-68-306/30/16 14:23376 65.0 1 Hexachlorobenzene ND ug/kg 07/06/16 20:25 118-74-106/30/16 14:23376 47.9 1 Hexachlorocyclopentadiene ND ug/kg 07/06/16 20:25 77-47-406/30/16 14:23376 69.5 1 Hexachloroethane ND ug/kg 07/06/16 20:25 67-72-106/30/16 14:23376 99.2 1 Indeno(1,2,3-cd)pyrene ND ug/kg 07/06/16 20:25 193-39-506/30/16 14:23376 77.5 1 Isophorone ND ug/kg 07/06/16 20:25 78-59-106/30/16 14:23376 84.3 1 1-Methylnaphthalene ND ug/kg 07/06/16 20:25 90-12-006/30/16 14:23376 98.0 1 2-Methylnaphthalene ND ug/kg 07/06/16 20:25 91-57-606/30/16 14:23376 80.9 1 2-Methylphenol(o-Cresol)ND ug/kg 07/06/16 20:25 95-48-706/30/16 14:23376 114 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 07/06/16 20:2506/30/16 14:23376 148 1 Naphthalene ND ug/kg 07/06/16 20:25 91-20-306/30/16 14:23376 92.3 1 2-Nitroaniline ND ug/kg 07/06/16 20:25 88-74-406/30/16 14:231880 116 1 3-Nitroaniline ND ug/kg 07/06/16 20:25 99-09-206/30/16 14:231880 103 1 4-Nitroaniline ND ug/kg 07/06/16 20:25 100-01-606/30/16 14:23752 106 1 Nitrobenzene ND ug/kg 07/06/16 20:25 98-95-306/30/16 14:23376 103 1 2-Nitrophenol ND ug/kg 07/06/16 20:25 88-75-506/30/16 14:23376 91.2 1 4-Nitrophenol ND ug/kg 07/06/16 20:25 100-02-706/30/16 14:231880 67.2 1 N-Nitrosodimethylamine ND ug/kg 07/06/16 20:25 62-75-906/30/16 14:23376 122 1 N-Nitroso-di-n-propylamine ND ug/kg 07/06/16 20:25 621-64-706/30/16 14:23376 71.8 1 N-Nitrosodiphenylamine ND ug/kg 07/06/16 20:25 86-30-606/30/16 14:23376 112 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 07/06/16 20:25 108-60-106/30/16 14:23376 100 1 Pentachlorophenol ND ug/kg 07/06/16 20:25 87-86-506/30/16 14:231880 68.4 1 Phenanthrene ND ug/kg 07/06/16 20:25 85-01-806/30/16 14:23376 62.7 1 Phenol ND ug/kg 07/06/16 20:2506/30/16 14:23376 113 1 Pyrene ND ug/kg 07/06/16 20:25 129-00-006/30/16 14:23376 63.8 1 1,2,4-Trichlorobenzene ND ug/kg 07/06/16 20:25 120-82-106/30/16 14:23376 72.9 1 2,4,5-Trichlorophenol ND ug/kg 07/06/16 20:25 95-95-406/30/16 14:23376 116 1 2,4,6-Trichlorophenol ND ug/kg 07/06/16 20:25 88-06-206/30/16 14:23376 83.2 1 Surrogates Nitrobenzene-d5 (S)36 %07/06/16 20:25 4165-60-006/30/16 14:2323-110 1 2-Fluorobiphenyl (S)40 %07/06/16 20:25 321-60-806/30/16 14:2330-110 1 Terphenyl-d14 (S)86 %07/06/16 20:25 1718-51-006/30/16 14:2328-110 1 Phenol-d6 (S)35 %07/06/16 20:25 13127-88-306/30/16 14:2322-110 1 2-Fluorophenol (S)39 %07/06/16 20:25 367-12-406/30/16 14:2313-110 1 2,4,6-Tribromophenol (S)56 %07/06/16 20:25 118-79-606/30/16 14:2327-110 1 Analytical Method: EPA 82608260/5035A Volatile Organics Acetone 12.6J ug/kg 07/07/16 22:54 67-64-180.2 8.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-2 (1-2.5)Lab ID: 92303397005 Collected: 06/28/16 11:40 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260/5035A Volatile Organics Benzene ND ug/kg 07/07/16 22:54 71-43-24.0 1.3 1 Bromobenzene ND ug/kg 07/07/16 22:54 108-86-14.0 1.6 1 Bromochloromethane ND ug/kg 07/07/16 22:54 74-97-54.0 1.4 1 Bromodichloromethane ND ug/kg 07/07/16 22:54 75-27-44.0 1.5 1 Bromoform ND ug/kg 07/07/16 22:54 75-25-24.0 1.8 1 Bromomethane ND ug/kg 07/07/16 22:54 74-83-98.0 2.0 1 2-Butanone (MEK)ND ug/kg 07/07/16 22:54 78-93-380.2 2.3 1 n-Butylbenzene ND ug/kg 07/07/16 22:54 104-51-84.0 1.4 1 sec-Butylbenzene ND ug/kg 07/07/16 22:54 135-98-84.0 1.3 1 tert-Butylbenzene ND ug/kg 07/07/16 22:54 98-06-64.0 1.6 1 Carbon tetrachloride ND ug/kg 07/07/16 22:54 56-23-54.0 2.1 1 Chlorobenzene ND ug/kg 07/07/16 22:54 108-90-74.0 1.5 1 Chloroethane ND ug/kg 07/07/16 22:54 75-00-38.0 1.9 1 Chloroform ND ug/kg 07/07/16 22:54 67-66-34.0 1.3 1 Chloromethane ND ug/kg 07/07/16 22:54 74-87-38.0 1.9 1 2-Chlorotoluene ND ug/kg 07/07/16 22:54 95-49-84.0 1.4 1 4-Chlorotoluene ND ug/kg 07/07/16 22:54 106-43-44.0 1.4 1 1,2-Dibromo-3-chloropropane ND ug/kg 07/07/16 22:54 96-12-84.0 2.9 1 Dibromochloromethane ND ug/kg 07/07/16 22:54 124-48-14.0 1.4 1 1,2-Dibromoethane (EDB)ND ug/kg 07/07/16 22:54 106-93-44.0 1.4 1 Dibromomethane ND ug/kg 07/07/16 22:54 74-95-34.0 2.0 1 1,2-Dichlorobenzene ND ug/kg 07/07/16 22:54 95-50-14.0 1.5 1 1,3-Dichlorobenzene ND ug/kg 07/07/16 22:54 541-73-14.0 1.6 1 1,4-Dichlorobenzene ND ug/kg 07/07/16 22:54 106-46-74.0 1.4 1 Dichlorodifluoromethane ND ug/kg 07/07/16 22:54 75-71-88.0 2.9 1 1,1-Dichloroethane ND ug/kg 07/07/16 22:54 75-34-34.0 1.2 1 1,2-Dichloroethane ND ug/kg 07/07/16 22:54 107-06-24.0 1.8 1 1,1-Dichloroethene ND ug/kg 07/07/16 22:54 75-35-44.0 1.4 1 cis-1,2-Dichloroethene ND ug/kg 07/07/16 22:54 156-59-24.0 1.1 1 trans-1,2-Dichloroethene ND ug/kg 07/07/16 22:54 156-60-54.0 1.5 1 1,2-Dichloropropane ND ug/kg 07/07/16 22:54 78-87-54.0 1.4 1 1,3-Dichloropropane ND ug/kg 07/07/16 22:54 142-28-94.0 1.5 1 2,2-Dichloropropane ND ug/kg 07/07/16 22:54 594-20-74.0 1.4 1 1,1-Dichloropropene ND ug/kg 07/07/16 22:54 563-58-64.0 1.2 1 cis-1,3-Dichloropropene ND ug/kg 07/07/16 22:54 10061-01-54.0 1.4 1 trans-1,3-Dichloropropene ND ug/kg 07/07/16 22:54 10061-02-64.0 1.2 1 Diisopropyl ether ND ug/kg 07/07/16 22:54 108-20-34.0 1.4 1 Ethylbenzene ND ug/kg 07/07/16 22:54 100-41-44.0 1.4 1 Hexachloro-1,3-butadiene ND ug/kg 07/07/16 22:54 87-68-34.0 1.6 1 2-Hexanone ND ug/kg 07/07/16 22:54 591-78-640.1 3.1 1 Isopropylbenzene (Cumene)ND ug/kg 07/07/16 22:54 98-82-84.0 1.5 1 p-Isopropyltoluene ND ug/kg 07/07/16 22:54 99-87-64.0 1.4 1 Methylene Chloride ND ug/kg 07/07/16 22:54 75-09-216.0 2.4 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 07/07/16 22:54 108-10-140.1 3.0 1 Methyl-tert-butyl ether ND ug/kg 07/07/16 22:54 1634-04-44.0 1.2 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Sample: B-2 (1-2.5)Lab ID: 92303397005 Collected: 06/28/16 11:40 Received: 06/28/16 16:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260/5035A Volatile Organics Naphthalene ND ug/kg 07/07/16 22:54 91-20-34.0 0.96 1 n-Propylbenzene ND ug/kg 07/07/16 22:54 103-65-14.0 1.4 1 Styrene ND ug/kg 07/07/16 22:54 100-42-54.0 1.4 1 1,1,1,2-Tetrachloroethane ND ug/kg 07/07/16 22:54 630-20-64.0 1.7 1 1,1,2,2-Tetrachloroethane ND ug/kg 07/07/16 22:54 79-34-54.0 1.5 1 Tetrachloroethene ND ug/kg 07/07/16 22:54 127-18-44.0 1.4 1 Toluene ND ug/kg 07/07/16 22:54 108-88-34.0 1.4 1 1,2,3-Trichlorobenzene ND ug/kg 07/07/16 22:54 87-61-64.0 1.8 1 1,2,4-Trichlorobenzene ND ug/kg 07/07/16 22:54 120-82-14.0 1.3 1 1,1,1-Trichloroethane ND ug/kg 07/07/16 22:54 71-55-64.0 1.4 1 1,1,2-Trichloroethane ND ug/kg 07/07/16 22:54 79-00-54.0 1.7 1 Trichloroethene ND ug/kg 07/07/16 22:54 79-01-64.0 1.7 1 Trichlorofluoromethane ND ug/kg 07/07/16 22:54 75-69-44.0 1.8 1 1,2,3-Trichloropropane ND ug/kg 07/07/16 22:54 96-18-44.0 1.3 1 1,2,4-Trimethylbenzene ND ug/kg 07/07/16 22:54 95-63-64.0 1.6 1 1,3,5-Trimethylbenzene ND ug/kg 07/07/16 22:54 108-67-84.0 1.4 1 Vinyl acetate ND ug/kg 07/07/16 22:54 108-05-440.1 7.1 1 Vinyl chloride ND ug/kg 07/07/16 22:54 75-01-48.0 1.4 1 Xylene (Total)ND ug/kg 07/07/16 22:54 1330-20-78.0 2.9 1 m&p-Xylene ND ug/kg 07/07/16 22:54 179601-23-18.0 2.9 1 o-Xylene ND ug/kg 07/07/16 22:54 95-47-64.0 1.5 1 Surrogates Toluene-d8 (S)104 %07/07/16 22:54 2037-26-570-130 1 4-Bromofluorobenzene (S)100 %07/07/16 22:54 460-00-470-130 1 1,2-Dichloroethane-d4 (S)85 %07/07/16 22:54 17060-07-070-132 1 Analytical Method: ASTM D2974-87Percent Moisture Percent Moisture 12.3 %06/30/16 14:000.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 320368 EPA 7471 EPA 7471 7471 Mercury Associated Lab Samples: 92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1775321 Associated Lab Samples:92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Matrix: Solid AnalyzedMDL Mercury mg/kg ND 0.0050 07/12/16 10:300.00010 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1775322LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/kg 0.087.083 104 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1775323MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92303397001 1775324 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury mg/kg M1.061 70 75-12566 3 20.060.050 0.093 0.090 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 319694 EPA 3050 EPA 6010 6010 MET Associated Lab Samples: 92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1771833 Associated Lab Samples:92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Matrix: Solid AnalyzedMDL Arsenic mg/kg ND 1.0 07/07/16 14:430.50 Barium mg/kg ND 0.50 07/07/16 14:430.25 Cadmium mg/kg ND 0.10 07/07/16 14:430.050 Chromium mg/kg ND 0.50 07/07/16 14:430.25 Lead mg/kg ND 0.50 07/07/16 14:430.25 Selenium mg/kg ND 1.0 07/07/16 14:430.50 Silver mg/kg ND 0.50 07/07/16 14:430.25 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1771834LABORATORY CONTROL SAMPLE: LCSSpike Arsenic mg/kg 52.650 105 80-120 Barium mg/kg 51.950 104 80-120 Cadmium mg/kg 53.650 107 80-120 Chromium mg/kg 54.050 108 80-120 Lead mg/kg 53.250 106 80-120 Selenium mg/kg 53.550 107 80-120 Silver mg/kg 27.425 110 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1771835MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92302870005 1771836 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic mg/kg M160.2 66 75-12578 19 2072.242.8 82.3 99.1 Barium mg/kg M160.2 110 75-12566 12 2072.2102 168 150 Cadmium mg/kg 60.2 103 75-12599 14 2072.20.29 62.1 71.5 Chromium mg/kg 60.2 99 75-125100 17 2072.27.9 67.5 79.8 Lead mg/kg M160.2 -488 75-125-279 14 2072.2919 626 718 Selenium mg/kg 60.2 95 75-12593 15 2072.24.4 61.5 71.8 Silver mg/kg 30 100 75-12596 14 2036.11.1 31.1 35.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 320259 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples: 92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1774626 Associated Lab Samples:92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Matrix: Solid AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/kg ND 5.5 07/07/16 13:582.3 1,1,1-Trichloroethane ug/kg ND 5.5 07/07/16 13:582.0 1,1,2,2-Tetrachloroethane ug/kg ND 5.5 07/07/16 13:582.1 1,1,2-Trichloroethane ug/kg ND 5.5 07/07/16 13:582.3 1,1-Dichloroethane ug/kg ND 5.5 07/07/16 13:581.6 1,1-Dichloroethene ug/kg ND 5.5 07/07/16 13:582.0 1,1-Dichloropropene ug/kg ND 5.5 07/07/16 13:581.6 1,2,3-Trichlorobenzene ug/kg ND 5.5 07/07/16 13:582.4 1,2,3-Trichloropropane ug/kg ND 5.5 07/07/16 13:581.8 1,2,4-Trichlorobenzene ug/kg ND 5.5 07/07/16 13:581.8 1,2,4-Trimethylbenzene ug/kg ND 5.5 07/07/16 13:582.2 1,2-Dibromo-3-chloropropane ug/kg ND 5.5 07/07/16 13:583.9 1,2-Dibromoethane (EDB)ug/kg ND 5.5 07/07/16 13:582.0 1,2-Dichlorobenzene ug/kg ND 5.5 07/07/16 13:582.1 1,2-Dichloroethane ug/kg ND 5.5 07/07/16 13:582.4 1,2-Dichloropropane ug/kg ND 5.5 07/07/16 13:581.9 1,3,5-Trimethylbenzene ug/kg ND 5.5 07/07/16 13:582.0 1,3-Dichlorobenzene ug/kg ND 5.5 07/07/16 13:582.2 1,3-Dichloropropane ug/kg ND 5.5 07/07/16 13:582.1 1,4-Dichlorobenzene ug/kg ND 5.5 07/07/16 13:581.9 2,2-Dichloropropane ug/kg ND 5.5 07/07/16 13:581.9 2-Butanone (MEK)ug/kg ND 110 07/07/16 13:583.2 2-Chlorotoluene ug/kg ND 5.5 07/07/16 13:581.9 2-Hexanone ug/kg ND 54.8 07/07/16 13:584.3 4-Chlorotoluene ug/kg ND 5.5 07/07/16 13:582.0 4-Methyl-2-pentanone (MIBK)ug/kg ND 54.8 07/07/16 13:584.1 Acetone ug/kg ND 110 07/07/16 13:5811.0 Benzene ug/kg ND 5.5 07/07/16 13:581.8 Bromobenzene ug/kg ND 5.5 07/07/16 13:582.2 Bromochloromethane ug/kg ND 5.5 07/07/16 13:581.9 Bromodichloromethane ug/kg ND 5.5 07/07/16 13:582.1 Bromoform ug/kg ND 5.5 07/07/16 13:582.5 Bromomethane ug/kg ND 11.0 07/07/16 13:582.7 Carbon tetrachloride ug/kg ND 5.5 07/07/16 13:582.9 Chlorobenzene ug/kg ND 5.5 07/07/16 13:582.1 Chloroethane ug/kg ND 11.0 07/07/16 13:582.6 Chloroform ug/kg ND 5.5 07/07/16 13:581.8 Chloromethane ug/kg ND 11.0 07/07/16 13:582.6 cis-1,2-Dichloroethene ug/kg ND 5.5 07/07/16 13:581.5 cis-1,3-Dichloropropene ug/kg ND 5.5 07/07/16 13:582.0 Dibromochloromethane ug/kg ND 5.5 07/07/16 13:582.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1774626 Associated Lab Samples:92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Matrix: Solid AnalyzedMDL Dibromomethane ug/kg ND 5.5 07/07/16 13:582.7 Dichlorodifluoromethane ug/kg ND 11.0 07/07/16 13:583.9 Diisopropyl ether ug/kg ND 5.5 07/07/16 13:581.9 Ethylbenzene ug/kg ND 5.5 07/07/16 13:582.0 Hexachloro-1,3-butadiene ug/kg ND 5.5 07/07/16 13:582.2 Isopropylbenzene (Cumene)ug/kg ND 5.5 07/07/16 13:582.1 m&p-Xylene ug/kg ND 11.0 07/07/16 13:583.9 Methyl-tert-butyl ether ug/kg ND 5.5 07/07/16 13:581.6 Methylene Chloride ug/kg ND 21.9 07/07/16 13:583.3 n-Butylbenzene ug/kg ND 5.5 07/07/16 13:582.0 n-Propylbenzene ug/kg ND 5.5 07/07/16 13:581.9 Naphthalene ug/kg ND 5.5 07/07/16 13:581.3 o-Xylene ug/kg ND 5.5 07/07/16 13:582.1 p-Isopropyltoluene ug/kg ND 5.5 07/07/16 13:581.9 sec-Butylbenzene ug/kg ND 5.5 07/07/16 13:581.8 Styrene ug/kg ND 5.5 07/07/16 13:582.0 tert-Butylbenzene ug/kg ND 5.5 07/07/16 13:582.2 Tetrachloroethene ug/kg ND 5.5 07/07/16 13:581.9 Toluene ug/kg ND 5.5 07/07/16 13:582.0 trans-1,2-Dichloroethene ug/kg ND 5.5 07/07/16 13:582.1 trans-1,3-Dichloropropene ug/kg ND 5.5 07/07/16 13:581.6 Trichloroethene ug/kg ND 5.5 07/07/16 13:582.3 Trichlorofluoromethane ug/kg ND 5.5 07/07/16 13:582.4 Vinyl acetate ug/kg ND 54.8 07/07/16 13:589.6 Vinyl chloride ug/kg ND 11.0 07/07/16 13:582.0 Xylene (Total)ug/kg ND 11.0 07/07/16 13:583.9 1,2-Dichloroethane-d4 (S)%84 70-132 07/07/16 13:58 4-Bromofluorobenzene (S)%101 70-130 07/07/16 13:58 Toluene-d8 (S)%104 70-130 07/07/16 13:58 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1774627LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 48.552.6 92 74-137 1,1,1-Trichloroethane ug/kg 46.352.6 88 67-140 1,1,2,2-Tetrachloroethane ug/kg 47.152.6 90 72-141 1,1,2-Trichloroethane ug/kg 45.652.6 87 78-138 1,1-Dichloroethane ug/kg 46.452.6 88 69-134 1,1-Dichloroethene ug/kg 50.452.6 96 67-138 1,1-Dichloropropene ug/kg 46.052.6 87 69-139 1,2,3-Trichlorobenzene ug/kg 46.552.6 88 70-146 1,2,3-Trichloropropane ug/kg 49.652.6 94 69-144 1,2,4-Trichlorobenzene ug/kg 49.952.6 95 68-148 1,2,4-Trimethylbenzene ug/kg 52.152.6 99 74-137 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1774627LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromo-3-chloropropane ug/kg 45.052.6 85 65-140 1,2-Dibromoethane (EDB)ug/kg 51.552.6 98 77-135 1,2-Dichlorobenzene ug/kg 51.752.6 98 77-141 1,2-Dichloroethane ug/kg 43.452.6 82 65-137 1,2-Dichloropropane ug/kg 47.352.6 90 72-136 1,3,5-Trimethylbenzene ug/kg 52.252.6 99 76-133 1,3-Dichlorobenzene ug/kg 51.952.6 99 74-138 1,3-Dichloropropane ug/kg 46.252.6 88 71-139 1,4-Dichlorobenzene ug/kg 50.852.6 96 76-138 2,2-Dichloropropane ug/kg 48.052.6 91 68-137 2-Butanone (MEK)ug/kg 93.4J105 89 58-147 2-Chlorotoluene ug/kg 52.952.6 101 73-139 2-Hexanone ug/kg 98.8105 94 62-145 4-Chlorotoluene ug/kg 51.452.6 98 76-141 4-Methyl-2-pentanone (MIBK)ug/kg 95.3105 91 64-149 Acetone ug/kg 83.9J105 80 53-153 Benzene ug/kg 52.252.6 99 73-135 Bromobenzene ug/kg 50.452.6 96 75-133 Bromochloromethane ug/kg 45.752.6 87 73-134 Bromodichloromethane ug/kg 49.352.6 94 71-135 Bromoform ug/kg 44.552.6 85 66-141 Bromomethane ug/kg 48.352.6 92 53-160 Carbon tetrachloride ug/kg 52.952.6 100 60-145 Chlorobenzene ug/kg 51.952.6 99 78-130 Chloroethane ug/kg 45.252.6 86 64-149 Chloroform ug/kg 46.352.6 88 70-134 Chloromethane ug/kg 42.452.6 80 52-150 cis-1,2-Dichloroethene ug/kg 47.052.6 89 70-133 cis-1,3-Dichloropropene ug/kg 48.552.6 92 68-134 Dibromochloromethane ug/kg 47.552.6 90 71-138 Dibromomethane ug/kg 47.752.6 91 74-130 Dichlorodifluoromethane ug/kg 47.052.6 89 40-160 Diisopropyl ether ug/kg 44.952.6 85 69-141 Ethylbenzene ug/kg 52.652.6 100 75-133 Hexachloro-1,3-butadiene ug/kg 54.852.6 104 68-143 Isopropylbenzene (Cumene)ug/kg 51.852.6 98 76-143 m&p-Xylene ug/kg 104105 99 75-136 Methyl-tert-butyl ether ug/kg 43.452.6 83 68-144 Methylene Chloride ug/kg 43.352.6 82 45-154 n-Butylbenzene ug/kg 53.652.6 102 72-137 n-Propylbenzene ug/kg 51.152.6 97 76-136 Naphthalene ug/kg 45.452.6 86 68-151 o-Xylene ug/kg 50.452.6 96 76-141 p-Isopropyltoluene ug/kg 52.052.6 99 76-140 sec-Butylbenzene ug/kg 51.152.6 97 79-139 Styrene ug/kg 52.552.6 100 79-137 tert-Butylbenzene ug/kg 45.052.6 86 74-143 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1774627LABORATORY CONTROL SAMPLE: LCSSpike Tetrachloroethene ug/kg 48.852.6 93 71-138 Toluene ug/kg 50.352.6 96 74-131 trans-1,2-Dichloroethene ug/kg 47.952.6 91 67-135 trans-1,3-Dichloropropene ug/kg 46.852.6 89 65-146 Trichloroethene ug/kg 49.352.6 94 67-135 Trichlorofluoromethane ug/kg 49.552.6 94 59-144 Vinyl acetate ug/kg 90.1 F310586 40-160 Vinyl chloride ug/kg 45.252.6 86 56-141 Xylene (Total)ug/kg 155158 98 76-137 1,2-Dichloroethane-d4 (S)%86 70-132 4-Bromofluorobenzene (S)%104 70-130 Toluene-d8 (S)%97 70-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1775561MATRIX SPIKE SAMPLE: MSSpike Result 92303600004 1,1,1,2-Tetrachloroethane ug/kg 20.920.5 102 70-130ND 1,1,1-Trichloroethane ug/kg 20.820.5 102 70-130ND 1,1,2,2-Tetrachloroethane ug/kg 22.920.5 112 70-130ND 1,1,2-Trichloroethane ug/kg 22.720.5 111 70-130ND 1,1-Dichloroethane ug/kg 22.020.5 107 70-130ND 1,1-Dichloroethene ug/kg 22.220.5 108 49-180ND 1,1-Dichloropropene ug/kg 20.120.5 98 70-130ND 1,2,3-Trichlorobenzene ug/kg 18.720.5 91 70-130ND 1,2,3-Trichloropropane ug/kg 23.620.5 115 70-130ND 1,2,4-Trichlorobenzene ug/kg 17.120.5 83 70-130ND 1,2,4-Trimethylbenzene ug/kg 18.920.5 92 70-130ND 1,2-Dibromo-3-chloropropane ug/kg 21.820.5 107 70-130ND 1,2-Dibromoethane (EDB)ug/kg 24.820.5 121 70-130ND 1,2-Dichlorobenzene ug/kg 21.920.5 107 70-130ND 1,2-Dichloroethane ug/kg 22.920.5 112 70-130ND 1,2-Dichloropropane ug/kg 22.320.5 109 70-130ND 1,3,5-Trimethylbenzene ug/kg 19.120.5 93 70-130ND 1,3-Dichlorobenzene ug/kg 20.820.5 101 70-130ND 1,3-Dichloropropane ug/kg 22.720.5 111 70-130ND 1,4-Dichlorobenzene ug/kg 20.820.5 102 70-130ND 2,2-Dichloropropane ug/kg 21.820.5 106 70-130ND 2-Butanone (MEK)ug/kg 43.6J41 107 70-130ND 2-Chlorotoluene ug/kg 21.420.5 104 70-130ND 2-Hexanone ug/kg 49.3J41 120 70-130ND 4-Chlorotoluene ug/kg 20.920.5 102 70-130ND 4-Methyl-2-pentanone (MIBK)ug/kg 50.0J41 122 70-130ND Acetone ug/kg 54.4J M14169 70-130ND Benzene ug/kg 31.420.5 135 50-166ND Bromobenzene ug/kg 22.120.5 108 70-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 30 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1775561MATRIX SPIKE SAMPLE: MSSpike Result 92303600004 Bromochloromethane ug/kg 21.920.5 107 70-130ND Bromodichloromethane ug/kg 22.420.5 109 70-130ND Bromoform ug/kg 20.820.5 102 70-130ND Bromomethane ug/kg 24.020.5 117 70-130ND Carbon tetrachloride ug/kg 22.120.5 108 70-130ND Chlorobenzene ug/kg 21.820.5 107 43-169ND Chloroethane ug/kg 23.220.5 113 70-130ND Chloroform ug/kg 22.020.5 108 70-130ND Chloromethane ug/kg 21.820.5 107 70-130ND cis-1,2-Dichloroethene ug/kg 22.020.5 108 70-130ND cis-1,3-Dichloropropene ug/kg 22.020.5 107 70-130ND Dibromochloromethane ug/kg 21.920.5 107 70-130ND Dibromomethane ug/kg 23.420.5 114 70-130ND Dichlorodifluoromethane ug/kg 20.920.5 102 70-130ND Diisopropyl ether ug/kg 21.820.5 107 70-130ND Ethylbenzene ug/kg 21.920.5 107 70-130ND Hexachloro-1,3-butadiene ug/kg 18.020.5 88 70-130ND Isopropylbenzene (Cumene)ug/kg 21.720.5 106 70-130ND m&p-Xylene ug/kg 44.541 109 70-130ND Methyl-tert-butyl ether ug/kg 23.220.5 113 70-130ND Methylene Chloride ug/kg 34.820.5 88 70-130ND n-Butylbenzene ug/kg 18.220.5 89 70-130ND n-Propylbenzene ug/kg 19.820.5 96 70-130ND Naphthalene ug/kg 19.420.5 95 70-130ND o-Xylene ug/kg 22.320.5 109 70-130ND p-Isopropyltoluene ug/kg 19.520.5 95 70-130ND sec-Butylbenzene ug/kg 19.520.5 95 70-130ND Styrene ug/kg 23.320.5 114 70-130ND tert-Butylbenzene ug/kg 18.320.5 89 70-130ND Tetrachloroethene ug/kg 18.720.5 91 70-130ND Toluene ug/kg 21.220.5 104 52-163ND trans-1,2-Dichloroethene ug/kg 22.320.5 109 70-130ND trans-1,3-Dichloropropene ug/kg 21.820.5 107 70-130ND Trichloroethene ug/kg 21.120.5 103 49-167ND Trichlorofluoromethane ug/kg 21.720.5 106 70-130ND Vinyl acetate ug/kg 43.5J41 106 70-130ND Vinyl chloride ug/kg 19.620.5 96 70-130ND 1,2-Dichloroethane-d4 (S)%104 70-132 4-Bromofluorobenzene (S)%108 70-130 Toluene-d8 (S)%97 70-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92303397001 1775560SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/kg ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 31 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92303397001 1775560SAMPLE DUPLICATE: 1,1,1-Trichloroethane ug/kg ND 30ND 1,1,2,2-Tetrachloroethane ug/kg ND 30ND 1,1,2-Trichloroethane ug/kg ND 30ND 1,1-Dichloroethane ug/kg ND 30ND 1,1-Dichloroethene ug/kg ND 30ND 1,1-Dichloropropene ug/kg ND 30ND 1,2,3-Trichlorobenzene ug/kg ND 30ND 1,2,3-Trichloropropane ug/kg ND 30ND 1,2,4-Trichlorobenzene ug/kg ND 30ND 1,2,4-Trimethylbenzene ug/kg ND 30ND 1,2-Dibromo-3-chloropropane ug/kg ND 30ND 1,2-Dibromoethane (EDB)ug/kg ND 30ND 1,2-Dichlorobenzene ug/kg ND 30ND 1,2-Dichloroethane ug/kg ND 30ND 1,2-Dichloropropane ug/kg ND 30ND 1,3,5-Trimethylbenzene ug/kg ND 30ND 1,3-Dichlorobenzene ug/kg ND 30ND 1,3-Dichloropropane ug/kg ND 30ND 1,4-Dichlorobenzene ug/kg ND 30ND 2,2-Dichloropropane ug/kg ND 30ND 2-Butanone (MEK)ug/kg ND 30ND 2-Chlorotoluene ug/kg ND 30ND 2-Hexanone ug/kg ND 30ND 4-Chlorotoluene ug/kg ND 30ND 4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND Acetone ug/kg 129 21 30158 Benzene ug/kg ND 30ND Bromobenzene ug/kg ND 30ND Bromochloromethane ug/kg ND 30ND Bromodichloromethane ug/kg ND 30ND Bromoform ug/kg ND 30ND Bromomethane ug/kg ND 30ND Carbon tetrachloride ug/kg ND 30ND Chlorobenzene ug/kg ND 30ND Chloroethane ug/kg ND 30ND Chloroform ug/kg ND 30ND Chloromethane ug/kg ND 30ND cis-1,2-Dichloroethene ug/kg ND 30ND cis-1,3-Dichloropropene ug/kg ND 30ND Dibromochloromethane ug/kg ND 30ND Dibromomethane ug/kg ND 30ND Dichlorodifluoromethane ug/kg ND 30ND Diisopropyl ether ug/kg ND 30ND Ethylbenzene ug/kg ND 30ND Hexachloro-1,3-butadiene ug/kg ND 30ND Isopropylbenzene (Cumene)ug/kg ND 30ND m&p-Xylene ug/kg ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 32 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92303397001 1775560SAMPLE DUPLICATE: Methyl-tert-butyl ether ug/kg ND 30ND Methylene Chloride ug/kg ND 30ND n-Butylbenzene ug/kg ND 30ND n-Propylbenzene ug/kg ND 30ND Naphthalene ug/kg ND 30ND o-Xylene ug/kg ND 30ND p-Isopropyltoluene ug/kg ND 30ND sec-Butylbenzene ug/kg ND 30ND Styrene ug/kg ND 30ND tert-Butylbenzene ug/kg ND 30ND Tetrachloroethene ug/kg ND 30ND Toluene ug/kg ND 30ND trans-1,2-Dichloroethene ug/kg ND 30ND trans-1,3-Dichloropropene ug/kg ND 30ND Trichloroethene ug/kg ND 30ND Trichlorofluoromethane ug/kg ND 30ND Vinyl acetate ug/kg ND 30ND Vinyl chloride ug/kg ND 30ND Xylene (Total)ug/kg ND 30ND 1,2-Dichloroethane-d4 (S)%85 990 4-Bromofluorobenzene (S)%93 998 Toluene-d8 (S)%114 5104 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 33 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 319471 EPA 3546 EPA 8270 8270 Solid MSSV Microwave Associated Lab Samples: 92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1770338 Associated Lab Samples:92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Matrix: Solid AnalyzedMDL 1,2,4-Trichlorobenzene ug/kg ND 330 07/05/16 14:1964.0 1,2-Dichlorobenzene ug/kg ND 330 07/05/16 14:1988.0 1,3-Dichlorobenzene ug/kg ND 330 07/05/16 14:1975.0 1,4-Dichlorobenzene ug/kg ND 330 07/05/16 14:1993.0 1-Methylnaphthalene ug/kg ND 330 07/05/16 14:1986.0 2,2'-Oxybis(1-chloropropane)ug/kg ND 330 07/05/16 14:1988.0 2,4,5-Trichlorophenol ug/kg ND 330 07/05/16 14:19102 2,4,6-Trichlorophenol ug/kg ND 330 07/05/16 14:1973.0 2,4-Dichlorophenol ug/kg ND 330 07/05/16 14:1972.0 2,4-Dimethylphenol ug/kg ND 330 07/05/16 14:19130 2,4-Dinitrophenol ug/kg ND 1650 07/05/16 14:1954.0 2,4-Dinitrotoluene ug/kg ND 330 07/05/16 14:1962.0 2,6-Dinitrotoluene ug/kg ND 330 07/05/16 14:1969.0 2-Chloronaphthalene ug/kg ND 330 07/05/16 14:1965.0 2-Chlorophenol ug/kg ND 330 07/05/16 14:1990.0 2-Methylnaphthalene ug/kg ND 330 07/05/16 14:1971.0 2-Methylphenol(o-Cresol)ug/kg ND 330 07/05/16 14:19100 2-Nitroaniline ug/kg ND 1650 07/05/16 14:19102 2-Nitrophenol ug/kg ND 330 07/05/16 14:1980.0 3&4-Methylphenol(m&p Cresol)ug/kg ND 330 07/05/16 14:19130 3,3'-Dichlorobenzidine ug/kg ND 1650 07/05/16 14:1972.0 3-Nitroaniline ug/kg ND 1650 07/05/16 14:1990.0 4,6-Dinitro-2-methylphenol ug/kg ND 660 07/05/16 14:1966.0 4-Bromophenylphenyl ether ug/kg ND 330 07/05/16 14:1960.0 4-Chloro-3-methylphenol ug/kg ND 660 07/05/16 14:1968.0 4-Chloroaniline ug/kg ND 1650 07/05/16 14:1992.0 4-Chlorophenylphenyl ether ug/kg ND 330 07/05/16 14:1968.0 4-Nitroaniline ug/kg ND 660 07/05/16 14:1993.0 4-Nitrophenol ug/kg ND 1650 07/05/16 14:1959.0 Acenaphthene ug/kg ND 330 07/05/16 14:1976.0 Acenaphthylene ug/kg ND 330 07/05/16 14:1978.0 Aniline ug/kg ND 330 07/05/16 14:1989.0 Anthracene ug/kg ND 330 07/05/16 14:1974.0 Benzo(a)anthracene ug/kg ND 330 07/05/16 14:1961.0 Benzo(a)pyrene ug/kg ND 330 07/05/16 14:1963.0 Benzo(b)fluoranthene ug/kg ND 330 07/05/16 14:1957.0 Benzo(g,h,i)perylene ug/kg ND 330 07/05/16 14:1984.0 Benzo(k)fluoranthene ug/kg ND 330 07/05/16 14:1965.0 Benzoic Acid ug/kg ND 1650 07/05/16 14:1960.0 Benzyl alcohol ug/kg ND 660 07/05/16 14:1966.0 bis(2-Chloroethoxy)methane ug/kg ND 330 07/05/16 14:1977.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 34 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1770338 Associated Lab Samples:92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Matrix: Solid AnalyzedMDL bis(2-Chloroethyl) ether ug/kg ND 330 07/05/16 14:1984.0 bis(2-Ethylhexyl)phthalate ug/kg ND 330 07/05/16 14:1990.0 Butylbenzylphthalate ug/kg ND 330 07/05/16 14:1970.0 Chrysene ug/kg ND 330 07/05/16 14:1944.0 Di-n-butylphthalate ug/kg ND 330 07/05/16 14:1954.0 Di-n-octylphthalate ug/kg ND 330 07/05/16 14:1969.0 Dibenz(a,h)anthracene ug/kg ND 330 07/05/16 14:1970.0 Dibenzofuran ug/kg ND 330 07/05/16 14:1954.0 Diethylphthalate ug/kg ND 330 07/05/16 14:1951.0 Dimethylphthalate ug/kg ND 330 07/05/16 14:1967.0 Fluoranthene ug/kg ND 330 07/05/16 14:1948.0 Fluorene ug/kg ND 330 07/05/16 14:1968.0 Hexachloro-1,3-butadiene ug/kg ND 330 07/05/16 14:1957.0 Hexachlorobenzene ug/kg ND 330 07/05/16 14:1942.0 Hexachlorocyclopentadiene ug/kg ND 330 07/05/16 14:1961.0 Hexachloroethane ug/kg ND 330 07/05/16 14:1987.0 Indeno(1,2,3-cd)pyrene ug/kg ND 330 07/05/16 14:1968.0 Isophorone ug/kg ND 330 07/05/16 14:1974.0 N-Nitroso-di-n-propylamine ug/kg ND 330 07/05/16 14:1963.0 N-Nitrosodimethylamine ug/kg ND 330 07/05/16 14:19107 N-Nitrosodiphenylamine ug/kg ND 330 07/05/16 14:1998.0 Naphthalene ug/kg ND 330 07/05/16 14:1981.0 Nitrobenzene ug/kg ND 330 07/05/16 14:1990.0 Pentachlorophenol ug/kg ND 1650 07/05/16 14:1960.0 Phenanthrene ug/kg ND 330 07/05/16 14:1955.0 Phenol ug/kg ND 330 07/05/16 14:1999.0 Pyrene ug/kg ND 330 07/05/16 14:1956.0 2,4,6-Tribromophenol (S)%81 27-110 07/05/16 14:19 2-Fluorobiphenyl (S)%81 30-110 07/05/16 14:19 2-Fluorophenol (S)%75 13-110 07/05/16 14:19 Nitrobenzene-d5 (S)%73 23-110 07/05/16 14:19 Phenol-d6 (S)%78 22-110 07/05/16 14:19 Terphenyl-d14 (S)%105 28-110 07/05/16 14:19 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1770339LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/kg 14101670 84 36-120 1,2-Dichlorobenzene ug/kg 12801670 77 41-120 1,3-Dichlorobenzene ug/kg 13201670 79 66-120 1,4-Dichlorobenzene ug/kg 13201670 79 42-120 1-Methylnaphthalene ug/kg 14701670 88 40-120 2,2'-Oxybis(1-chloropropane)ug/kg 12701670 76 17-120 2,4,5-Trichlorophenol ug/kg 13501670 81 37-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 35 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1770339LABORATORY CONTROL SAMPLE: LCSSpike 2,4,6-Trichlorophenol ug/kg 13901670 84 40-120 2,4-Dichlorophenol ug/kg 14101670 85 33-120 2,4-Dimethylphenol ug/kg 14001670 84 36-120 2,4-Dinitrophenol ug/kg 35408330 42 22-121 2,4-Dinitrotoluene ug/kg 14301670 86 60-120 2,6-Dinitrotoluene ug/kg 14401670 87 54-120 2-Chloronaphthalene ug/kg 13101670 78 41-120 2-Chlorophenol ug/kg 13301670 80 39-120 2-Methylnaphthalene ug/kg 14301670 86 26-120 2-Methylphenol(o-Cresol)ug/kg 13101670 78 41-120 2-Nitroaniline ug/kg 26303330 79 45-120 2-Nitrophenol ug/kg 14201670 85 35-120 3&4-Methylphenol(m&p Cresol)ug/kg 12601670 76 35-120 3,3'-Dichlorobenzidine ug/kg 25203330 76 16-125 3-Nitroaniline ug/kg 25003330 75 45-120 4,6-Dinitro-2-methylphenol ug/kg 20403330 61 46-120 4-Bromophenylphenyl ether ug/kg 14801670 89 36-120 4-Chloro-3-methylphenol ug/kg 28403330 85 37-120 4-Chloroaniline ug/kg 25803330 77 35-120 4-Chlorophenylphenyl ether ug/kg 14701670 88 30-120 4-Nitroaniline ug/kg 25703330 77 48-120 4-Nitrophenol ug/kg 59208330 71 43-120 Acenaphthene ug/kg 13801670 83 46-120 Acenaphthylene ug/kg 13601670 81 46-120 Aniline ug/kg 11501670 69 33-120 Anthracene ug/kg 14301670 86 63-120 Benzo(a)anthracene ug/kg 14001670 84 61-120 Benzo(a)pyrene ug/kg 15301670 92 59-120 Benzo(b)fluoranthene ug/kg 15201670 91 55-120 Benzo(g,h,i)perylene ug/kg 12201670 73 57-120 Benzo(k)fluoranthene ug/kg 16501670 99 56-120 Benzoic Acid ug/kg 53308330 64 13-120 Benzyl alcohol ug/kg 27303330 82 34-120 bis(2-Chloroethoxy)methane ug/kg 14001670 84 21-120 bis(2-Chloroethyl) ether ug/kg 13801670 83 25-120 bis(2-Ethylhexyl)phthalate ug/kg 12101670 73 56-123 Butylbenzylphthalate ug/kg 12901670 78 57-120 Chrysene ug/kg 14101670 85 64-120 Di-n-butylphthalate ug/kg 14401670 86 58-120 Di-n-octylphthalate ug/kg 11101670 67 47-121 Dibenz(a,h)anthracene ug/kg 13301670 80 56-120 Dibenzofuran ug/kg 14401670 87 43-120 Diethylphthalate ug/kg 14201670 85 55-120 Dimethylphthalate ug/kg 14201670 85 54-120 Fluoranthene ug/kg 14301670 86 61-120 Fluorene ug/kg 14401670 86 51-120 Hexachloro-1,3-butadiene ug/kg 14201670 85 22-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 36 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1770339LABORATORY CONTROL SAMPLE: LCSSpike Hexachlorobenzene ug/kg 14001670 84 53-120 Hexachlorocyclopentadiene ug/kg 10801670 65 18-150 Hexachloroethane ug/kg 12701670 76 39-120 Indeno(1,2,3-cd)pyrene ug/kg 12901670 77 58-120 Isophorone ug/kg 13301670 80 38-120 N-Nitroso-di-n-propylamine ug/kg 11401670 69 30-120 N-Nitrosodimethylamine ug/kg 9941670 60 32-120 N-Nitrosodiphenylamine ug/kg 13101670 79 50-120 Naphthalene ug/kg 13801670 83 38-120 Nitrobenzene ug/kg 13601670 82 37-120 Pentachlorophenol ug/kg 23803330 71 10-120 Phenanthrene ug/kg 14101670 85 62-120 Phenol ug/kg 13101670 79 37-120 Pyrene ug/kg 13901670 83 63-120 2,4,6-Tribromophenol (S)%92 27-110 2-Fluorobiphenyl (S)%80 30-110 2-Fluorophenol (S)%80 13-110 Nitrobenzene-d5 (S)%78 23-110 Phenol-d6 (S)%81 22-110 Terphenyl-d14 (S)%86 28-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1770340MATRIX SPIKE SAMPLE: MSSpike Result 92302696003 1,2,4-Trichlorobenzene ug/kg 12701830 70 18-119ND 1,2-Dichlorobenzene ug/kg 12101830 66 50-110ND 1,3-Dichlorobenzene ug/kg 12501830 68 27-110ND 1,4-Dichlorobenzene ug/kg 12201830 67 28-110ND 1-Methylnaphthalene ug/kg 14201830 78 24-116ND 2,2'-Oxybis(1-chloropropane)ug/kg 11801830 64 50-150ND 2,4,5-Trichlorophenol ug/kg 14401830 79 28-110ND 2,4,6-Trichlorophenol ug/kg 14201830 77 17-117ND 2,4-Dichlorophenol ug/kg 13501830 74 21-128ND 2,4-Dimethylphenol ug/kg 12701830 69 10-120ND 2,4-Dinitrophenol ug/kg 43909140 48 10-107ND 2,4-Dinitrotoluene ug/kg 14801830 81 36-109ND 2,6-Dinitrotoluene ug/kg 14601830 80 32-110ND 2-Chloronaphthalene ug/kg 12701830 70 30-107ND 2-Chlorophenol ug/kg 12701830 69 14-106ND 2-Methylnaphthalene ug/kg 13401830 73 10-135ND 2-Methylphenol(o-Cresol)ug/kg 12001830 66 10-124ND 2-Nitroaniline ug/kg 26803660 73 26-116ND 2-Nitrophenol ug/kg 13301830 73 28-103ND 3&4-Methylphenol(m&p Cresol)ug/kg 12001830 66 10-109ND 3,3'-Dichlorobenzidine ug/kg 22503660 61 10-150ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 37 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1770340MATRIX SPIKE SAMPLE: MSSpike Result 92302696003 3-Nitroaniline ug/kg 25503660 70 22-110ND 4,6-Dinitro-2-methylphenol ug/kg 22903660 63 13-121ND 4-Bromophenylphenyl ether ug/kg 14501830 79 31-109ND 4-Chloro-3-methylphenol ug/kg 29003660 79 13-128ND 4-Chloroaniline ug/kg 22803660 62 18-102ND 4-Chlorophenylphenyl ether ug/kg 15001830 82 29-112ND 4-Nitroaniline ug/kg 26903660 74 16-111ND 4-Nitrophenol ug/kg 64409140 70 14-135ND Acenaphthene ug/kg 13401830 73 26-114ND Acenaphthylene ug/kg 13601830 74 32-108ND Aniline ug/kg 7771830 42 10-107ND Anthracene ug/kg 13901830 76 32-111ND Benzo(a)anthracene ug/kg 14401830 76 25-117ND Benzo(a)pyrene ug/kg 14901830 79 25-106ND Benzo(b)fluoranthene ug/kg 15001830 80 24-110ND Benzo(g,h,i)perylene ug/kg 13001830 71 19-112ND Benzo(k)fluoranthene ug/kg 15501830 82 24-114ND Benzoic Acid ug/kg 53609140 59 10-110ND Benzyl alcohol ug/kg 25803660 70 24-106ND bis(2-Chloroethoxy)methane ug/kg 12701830 69 13-119ND bis(2-Chloroethyl) ether ug/kg 13201830 72 10-134ND bis(2-Ethylhexyl)phthalate ug/kg 13801830 73 10-125ND Butylbenzylphthalate ug/kg 14301830 78 18-110ND Chrysene ug/kg 14201830 75 30-110ND Di-n-butylphthalate ug/kg 14701830 81 19-112ND Di-n-octylphthalate ug/kg 13101830 72 17-105ND Dibenz(a,h)anthracene ug/kg 13701830 75 23-111ND Dibenzofuran ug/kg 14601830 80 35-103ND Diethylphthalate ug/kg 14901830 82 27-113ND Dimethylphthalate ug/kg 14601830 80 26-111ND Fluoranthene ug/kg 14501830 79 33-109ND Fluorene ug/kg 14901830 81 32-113ND Hexachloro-1,3-butadiene ug/kg 12701830 70 16-116ND Hexachlorobenzene ug/kg 13401830 73 27-120ND Hexachlorocyclopentadiene ug/kg 9851830 54 10-108ND Hexachloroethane ug/kg 11801830 64 10-117ND Indeno(1,2,3-cd)pyrene ug/kg 13401830 73 10-122ND Isophorone ug/kg 12801830 70 28-114ND N-Nitroso-di-n-propylamine ug/kg 11001830 60 27-113ND N-Nitrosodimethylamine ug/kg 9471830 52 10-109ND N-Nitrosodiphenylamine ug/kg 12601830 69 10-128ND Naphthalene ug/kg 12601830 69 25-110ND Nitrobenzene ug/kg 12501830 68 18-114ND Pentachlorophenol ug/kg 27603660 75 10-122ND Phenanthrene ug/kg 13901830 76 30-114ND Phenol ug/kg 12101830 66 11-102ND Pyrene ug/kg 14101830 77 25-116ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 38 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1770340MATRIX SPIKE SAMPLE: MSSpike Result 92302696003 2,4,6-Tribromophenol (S)%81 27-110 2-Fluorobiphenyl (S)%70 30-110 2-Fluorophenol (S)%66 13-110 Nitrobenzene-d5 (S)%65 23-110 Phenol-d6 (S)%67 22-110 Terphenyl-d14 (S)%80 28-110 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 39 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 319284 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples: 92303397001, 92303397002, 92303397003, 92303397004, 92303397005 Parameter Units Dup Result Max RPD QualifiersRPDResult 92303397001 1769417SAMPLE DUPLICATE: Percent Moisture %22.5 6 2521.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 40 of 44 #=QL# QUALIFIERS Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3 The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside thelaboratory's control limits. The result is estimated.F3 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 Surrogate recovery not evaluated against control limits due to sample dilution.S4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 41 of 44 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92303397 UNIVERSITY FORD 1272C Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92303397001 319694 319724B-5 (4-6)EPA 3050 EPA 6010 92303397002 319694 319724B-8 (4-6)EPA 3050 EPA 6010 92303397003 319694 319724B-15 (3.5-6.5)EPA 3050 EPA 6010 92303397004 319694 319724B-16 (1-2.5)EPA 3050 EPA 6010 92303397005 319694 319724B-2 (1-2.5)EPA 3050 EPA 6010 92303397001 320368 320389B-5 (4-6)EPA 7471 EPA 7471 92303397002 320368 320389B-8 (4-6)EPA 7471 EPA 7471 92303397003 320368 320389B-15 (3.5-6.5)EPA 7471 EPA 7471 92303397004 320368 320389B-16 (1-2.5)EPA 7471 EPA 7471 92303397005 320368 320389B-2 (1-2.5)EPA 7471 EPA 7471 92303397001 319471 319872B-5 (4-6)EPA 3546 EPA 8270 92303397002 319471 319872B-8 (4-6)EPA 3546 EPA 8270 92303397003 319471 319872B-15 (3.5-6.5)EPA 3546 EPA 8270 92303397004 319471 319872B-16 (1-2.5)EPA 3546 EPA 8270 92303397005 319471 319872B-2 (1-2.5)EPA 3546 EPA 8270 92303397001 320259B-5 (4-6)EPA 8260 92303397002 320259B-8 (4-6)EPA 8260 92303397003 320259B-15 (3.5-6.5)EPA 8260 92303397004 320259B-16 (1-2.5)EPA 8260 92303397005 320259B-2 (1-2.5)EPA 8260 92303397001 319284B-5 (4-6)ASTM D2974-87 92303397002 319284B-8 (4-6)ASTM D2974-87 92303397003 319284B-15 (3.5-6.5)ASTM D2974-87 92303397004 319284B-16 (1-2.5)ASTM D2974-87 92303397005 319284B-2 (1-2.5)ASTM D2974-87 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/26/2016 04:36 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 42 of 44 Page 43 of 44 Document Name: Document Revised:April 25, 2016 /~eAnalytical~ Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: f ••·•• i F-CHR·CS-003-rev.19 Pace Huntersville Quality Office ; Sample Condition Upon Receipt · Client Name: A-rL C{,(.w(_ s l\_c:f '(-IV) t /VU./l ~~n. \/V\9.A,'-..w 2 of 2 for Internal Use ONLY lJO# : 92303397 Courier: D Commercial 0Fed Ex ($Pace OusPs Oother: __ Project#: Oclient II I Ill 1111111111111111 92303397 Custody Seal Present? Oves ~No Seals Intact? Oves ~No Date/Initials Person Examining Contents: Y 6(1.Sil/.b Packing Material: 0Bubble Wrap T1505 l;K]Bubble Bags 0None 00ther: __ Thermometer: Type of Ice: t;i!lwet 4:' f/(_,,, Correction Factor: o.o•c Cooler Temp Corrected (°C): Temp should be above freezing to 6°C 0Blue 0None O samples on ice, cooling process has begun Biological Tissue Frozen? Oves IRJNo ON/A USDA Regulated Soil ( D N/A, water sample) Did samples originate in a·quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, 0Yes RlNo I Chain of Custody Present? Samples Arrived within Hold Time? Short Hold Time Analysis (<72 hr.)? Rush Turn Around Time Requested? Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers Intact? Samples Field Filtered? Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: S' c1t' J , All containers needing acid/base preservation have been checked? _ _ All containers needing preservation are found to be in compliance with EPA recommendation? (HN03, H2S04, HCl<2; NaOH >9 Sulfide, Na0H>12 Cyanide) Exceptions: VOA, Coliform, TOC, Oil and Grease, DR0/8015 (water) DOC,LLHg Samples checked for dechlorination? Headspace in VOA Vials (>5-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? Pace Trip Blank Lot# (if purchased): CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Project Manager SCURF Review: including Hawaii and Puerto Rico)? 0Yes 1'51JNo Comments/Discrepancy: ~Yes 0No ON/A 1. [5i]Yes 0No ON/A 2. 00Yes ON/A 3. 0 Yes l':g!No ON/A 4. ~Yes 0No ON/A 5. lfJYes 0No ON/A 6. ~Yes 0No ON/A filYes 0No ON/A 7. 0 Yes 0 Yes G]Yes 0Yes 0 Yes 0 Yes 0 Yes 0Yes 0Yes IX)No 11JNo ~No ~No [ii!No [K]No ~No ON/A ON/A ON/A ON/A ON/A ON/A 8. Note if sediment is visible in the dissolved container 9. 0) l.5-S-·1"'wJD .:~02.JCVL..:i7~e-q -3D c.t c.-o £.,,., .. 1 CDc -ct ·\ o 10. HNo pH,2 ~ --• -' L f \'\:l::::i (VO 'J) ,QQ_ c'"'- tta pH<2 (i) (Jg ·-~~ ~~<;;;_r;, l ·-r 4~ Q, ,~ H2S04pH,2 ~ l31r D l' i? "-At· , '1 it) ~) l) O I I.....)(._, I VV'T{;v\..f: l\h:, D~ a.o P.~coc_ N10HpH>l2 NaOH/ZnOAc pH>9 11. ON/A 12. ON/A 13. ON/A Field Data Required? 0Yes 0No Date/Time: ® Date: ---:-(.p-'l=-~=p ___ _ Project Manager SRF Review: @ Date: ___ fo_0_f3_0 _____ _ Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect_Eontainers} •. , . Page 44 of 44 /2 ' ...... ,. 4;..,".i" • /l. \-:-i::.,t.·';;..'.VC1· .-.• •• , fl,ICl"''.10 ~ -),.. Section A Required Client lnfomi.111on S e c t i o n B R e q u i r e d P r o i c c l 1 n r o r m n 1 1 o n C H A I N - O F - C U S T O D Y I A n a l y t i c a l R e q u e s t D o c u m e n t T h e C h a m - o f - C u s t o d y i s a L E G A L D O C U M E N T A l l r e l e v a n t f i e l d s m u s t b e c o m p l e t e d o c c u r a l c l y S e c t i o n C l n v o 1 c o l n f o r m n h o n ! P a g e : f o f / I l Company Atlantic Shores Environmental R e p o r t T o ~ s w _ a _ ! o _ @ a t l a n t i c _ s _ h Q r e s e n v i r o n m e n t a l . c o m A l t c n ! L O n C h e r y l M o o d y Address 154 Backhoe Rd NE Leland. NC 28451 Email To Elliot Swain Phone (910) 371-5980 1Fax Requested Cuc OatcfTAT: 50AY Section O R1.-quirt.-d Ch1·nl !nl0tm,1l!on SAMPLE ID (A·Z.0·91 ·l Sample IDs MUST BE UNIQUE .. ::; w !:: 1 2 3 4 5 6 -7 -8 -9 -10 11 12 ADDITIONAL COMMENTS C o p y T o c m o o d y @ a t a l n t i c s h o r e s e n v i r o n m J ? ~ n t a L ~ o J : ! ! P u r c h a s e O r d e r N o P r o ; c c t N a m e P r o J C C I N u m b e r 1 2 7 2 C C o m p a n y N a m e A t l a n t i c S h o r e s E n v i r o n m e n t a l : A d d r e s s P ; 1 c t • 0 1 m l 1 • R 1 · h • 1 1 • n c ~ P ~ n • P I O J l " ' : I M , m , 1 q l ' f P a c n P , o h l • • I I 1 5 4 B a c k h o e R d N E L e l a n d N C 0 5 2 6 1 6 _ A S E _ S a m p 1 m g E v e n t T a y l o r E z e l l R E G U L A T O R Y A G E N C Y N P D E S U S T S i t o L o c a t i o n S T A T E : G R O U N D W A T E R R C R A N C D R I N K I N G W A T E R O T H E R R e q u e s t e d A n a l y s i s F i l t e r e d ( Y I N ) Valid M o t r l x C o d e s IM.]B_ ! ! . ; ; _ Q Q E tJU11ltll!. < ' . " , W A l [ R O W WAH R v n ll'JA~l £ W I I T f R W W PROD U C T p t,OIL'.. . O l l D S L O>L O l Wlf•(· W P AIH A R OTHE R 0 1 Tl~!.U f : 1 : ; s w 0 0 u x i i : > - < ( : : ; i i : 6 1 - u u a > r ? . " & w ~ w i t 5 : ( I ) S L I G S L I G S L I G S L I G S L I G S L I G S L I G S L I G S L I G S L I G S L I G S L I G C O L L E C T E D D A T E T I M E C A T E i , · R ~ ~ S H E O J , n A F F I L I A T I O N / : : z : : ; : - - ~ T I M E z 0 . : u ~ 5 u > - < ( a . ~ w i t ~ ( I ) ( / ) n : : w z < > - z 0 u " - 0 " ' P r e s e r v a t i v e s T - 0 Q J c : Q J ~ o , . . x i g - r n ~ ~ o o ' 1 . : : > I I I ~ ~ z ; : . . . . " ' . , t - . ! ! l 0 " ' c 2 : - " ' ~ . . . r : : . Q J c : ~ 6 < t O l } " [ E A I T I M E I , , A C C E ~ " ' 9 1 ) B Y I A F F I L I A T I O N ( l ' . ) u a . . 6 / Z f 7 7 1 w . 0 t t I ~ ~ : . P ~ ~ 2 P A - - c . · D A T E I T I M E I ? Z t f · / f . . l , k ' p : : : , " ' . . , , , ~ ~ ~ < ? ~ t ' F f £ t : ' ~ ~ 1 7 ' i - - ~ ~ o ) r i ; , ~ d i 1 ~ w ~ c . S A M P L E R N A M E A N D S I G N A T U R E - / / , , A - I l ) ' / G £ l ~ P R I N T N a m e o f S A M P L E R : 7 . ! . R Z / ' A ' ' / S I G N A T U R E o f S A M P L E R ; / / ~ I 1 M w / o o r r v ) : L z . . . : . _ ; ; ; - - 7 [ , , A . . - , - . , - . , - z ? : . Q J c " § : c i c o 3 0 ~ ' 3 ~ ~ Q J C l : S A M P L E C O N D I T I O N S / r , - / J v , N v - , u c f > - ~ ~ - 1 i > ° " ~ " ~ ~ o ! D ~ Z ~ g c . . 8 ~ 8 ~ 7 ~ [ o . . G E o " " t . n ~ #=CL# August 02, 2016 LIMS USE: FR - ELLIOT SWAIN LIMS OBJECT ID: 92306363 92306363 Project: Pace Project No.: RE: Elliot SwainAtlantic Shore Environmental154 Backhoe RdLeland, NC 28451 UNIVERSITY FORD 1272C Dear Elliot Swain: Enclosed are the analytical results for sample(s) received by the laboratory on July 25, 2016. The results relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Report revised on 8/2/16 to add MDLs. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell taylor.ezell@pacelabs.com Project Manager Enclosures cc:Cheryl Moody, Atlantic Shore Environmental REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 29 #=CP# CERTIFICATIONS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 29 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Lab ID Sample ID Matrix Date Collected Date Received 92306363001 MW-7 Water 07/25/16 09:30 07/25/16 14:20 92306363002 MW-13 Water 07/25/16 13:00 07/25/16 14:20 92306363003 MW-9 Water 07/25/16 10:00 07/25/16 14:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 29 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92306363001 MW-7 EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-AWAB EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92306363002 MW-13 EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-AWAB EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92306363003 MW-9 EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-AWAB REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 29 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Sample: MW-7 Lab ID: 92306363001 Collected: 07/25/16 09:30 Received: 07/25/16 14:20 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/29/16 19:22 7440-38-207/28/16 19:4010.0 5.0 1 Barium 226 ug/L 07/29/16 19:22 7440-39-307/28/16 19:405.0 2.5 1 Cadmium ND ug/L 07/29/16 19:22 7440-43-907/28/16 19:401.0 0.50 1 Chromium ND ug/L 07/29/16 19:22 7440-47-307/28/16 19:405.0 2.5 1 Lead ND ug/L 07/29/16 19:22 7439-92-107/28/16 19:405.0 2.5 1 Selenium ND ug/L 07/29/16 19:22 7782-49-207/28/16 19:4010.0 5.0 1 Silver ND ug/L 07/29/16 19:22 7440-22-407/28/16 19:405.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/28/16 12:46 7439-97-607/28/16 08:400.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/29/16 09:16 83-32-907/27/16 11:2112.5 0.31 1 Acenaphthylene ND ug/L 07/29/16 09:16 208-96-807/27/16 11:2112.5 0.26 1 Aniline ND ug/L 07/29/16 09:16 62-53-307/27/16 11:2112.5 1.6 1 Anthracene ND ug/L 07/29/16 09:16 120-12-707/27/16 11:2112.5 0.18 1 Benzo(a)anthracene ND ug/L 07/29/16 09:16 56-55-307/27/16 11:2112.5 0.41 1 Benzo(a)pyrene ND ug/L 07/29/16 09:16 50-32-807/27/16 11:2112.5 0.38 1 Benzo(b)fluoranthene ND ug/L 07/29/16 09:16 205-99-207/27/16 11:2112.5 0.35 1 Benzo(g,h,i)perylene ND ug/L 07/29/16 09:16 191-24-207/27/16 11:2112.5 0.48 1 Benzo(k)fluoranthene ND ug/L 07/29/16 09:16 207-08-907/27/16 11:2112.5 0.54 1 Benzoic Acid ND ug/L 07/29/16 09:16 65-85-007/27/16 11:2162.5 13.9 1 Benzyl alcohol ND ug/L 07/29/16 09:16 100-51-607/27/16 11:2125.0 4.2 1 4-Bromophenylphenyl ether ND ug/L 07/29/16 09:16 101-55-307/27/16 11:2112.5 1.7 1 Butylbenzylphthalate ND ug/L 07/29/16 09:16 85-68-707/27/16 11:2112.5 0.94 1 4-Chloro-3-methylphenol ND ug/L 07/29/16 09:16 59-50-707/27/16 11:2125.0 5.2 1 4-Chloroaniline ND ug/L 07/29/16 09:16 106-47-807/27/16 11:2125.0 4.2 1 bis(2-Chloroethoxy)methane ND ug/L 07/29/16 09:16 111-91-107/27/16 11:2112.5 2.1 1 bis(2-Chloroethyl) ether ND ug/L 07/29/16 09:16 111-44-407/27/16 11:2112.5 1.8 1 2-Chloronaphthalene ND ug/L 07/29/16 09:16 91-58-707/27/16 11:2112.5 2.8 1 2-Chlorophenol ND ug/L 07/29/16 09:16 95-57-807/27/16 11:2112.5 1.8 1 4-Chlorophenylphenyl ether ND ug/L 07/29/16 09:16 7005-72-307/27/16 11:2112.5 2.6 1 Chrysene ND ug/L 07/29/16 09:16 218-01-907/27/16 11:2112.5 0.26 1 Dibenz(a,h)anthracene ND ug/L 07/29/16 09:16 53-70-307/27/16 11:2112.5 0.69 1 Dibenzofuran ND ug/L 07/29/16 09:16 132-64-907/27/16 11:2112.5 2.2 1 1,2-Dichlorobenzene ND ug/L 07/29/16 09:16 95-50-107/27/16 11:2112.5 1.5 1 1,3-Dichlorobenzene ND ug/L 07/29/16 09:16 541-73-107/27/16 11:2112.5 1.4 1 1,4-Dichlorobenzene ND ug/L 07/29/16 09:16 106-46-707/27/16 11:2112.5 1.5 1 3,3'-Dichlorobenzidine ND ug/L 07/29/16 09:16 91-94-107/27/16 11:2125.0 1.8 1 2,4-Dichlorophenol ND ug/L 07/29/16 09:16 120-83-207/27/16 11:2112.5 2.1 1 Diethylphthalate ND ug/L 07/29/16 09:16 84-66-207/27/16 11:2112.5 1.7 1 2,4-Dimethylphenol ND ug/L 07/29/16 09:16 105-67-907/27/16 11:2112.5 2.7 1 Dimethylphthalate ND ug/L 07/29/16 09:16 131-11-307/27/16 11:2112.5 1.8 1 Di-n-butylphthalate ND ug/L 07/29/16 09:16 84-74-207/27/16 11:2112.5 1.3 1 4,6-Dinitro-2-methylphenol ND ug/L 07/29/16 09:16 534-52-107/27/16 11:2125.0 2.1 1 2,4-Dinitrophenol ND ug/L 07/29/16 09:16 51-28-507/27/16 11:2162.5 8.2 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 29 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Sample: MW-7 Lab ID: 92306363001 Collected: 07/25/16 09:30 Received: 07/25/16 14:20 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/29/16 09:16 121-14-207/27/16 11:2112.5 1.5 1 2,6-Dinitrotoluene ND ug/L 07/29/16 09:16 606-20-207/27/16 11:2112.5 2.1 1 Di-n-octylphthalate ND ug/L 07/29/16 09:16 117-84-007/27/16 11:2112.5 1.1 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/29/16 09:16 117-81-707/27/16 11:217.5 1.1 1 Fluoranthene ND ug/L 07/29/16 09:16 206-44-007/27/16 11:2112.5 0.26 1 Fluorene ND ug/L 07/29/16 09:16 86-73-707/27/16 11:2112.5 0.26 1 Hexachloro-1,3-butadiene ND ug/L 07/29/16 09:16 87-68-307/27/16 11:2112.5 2.3 1 Hexachlorobenzene ND ug/L 07/29/16 09:16 118-74-107/27/16 11:2112.5 1.4 1 Hexachlorocyclopentadiene ND ug/L 07/29/16 09:16 77-47-407/27/16 11:2112.5 2.2 1 Hexachloroethane ND ug/L 07/29/16 09:16 67-72-107/27/16 11:2112.5 1.8 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/29/16 09:16 193-39-507/27/16 11:2112.5 0.36 1 Isophorone ND ug/L 07/29/16 09:16 78-59-107/27/16 11:2112.5 2.2 1 1-Methylnaphthalene ND ug/L 07/29/16 09:16 90-12-007/27/16 11:2112.5 0.40 1 2-Methylnaphthalene ND ug/L 07/29/16 09:16 91-57-607/27/16 11:2112.5 0.35 1 2-Methylphenol(o-Cresol)ND ug/L 07/29/16 09:16 95-48-707/27/16 11:2112.5 2.2 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/29/16 09:1607/27/16 11:2112.5 2.1 1 Naphthalene ND ug/L 07/29/16 09:16 91-20-307/27/16 11:2112.5 0.42 1 2-Nitroaniline ND ug/L 07/29/16 09:16 88-74-407/27/16 11:2162.5 3.5 1 3-Nitroaniline ND ug/L 07/29/16 09:16 99-09-207/27/16 11:2162.5 3.0 1 4-Nitroaniline ND ug/L 07/29/16 09:16 100-01-607/27/16 11:2125.0 3.2 1 Nitrobenzene ND ug/L 07/29/16 09:16 98-95-307/27/16 11:2112.5 2.1 1 2-Nitrophenol ND ug/L 07/29/16 09:16 88-75-507/27/16 11:2112.5 2.1 1 4-Nitrophenol ND ug/L 07/29/16 09:16 100-02-707/27/16 11:2162.5 7.2 1 N-Nitrosodimethylamine ND ug/L 07/29/16 09:16 62-75-907/27/16 11:2112.5 1.6 1 N-Nitroso-di-n-propylamine ND ug/L 07/29/16 09:16 621-64-707/27/16 11:2112.5 2.6 1 N-Nitrosodiphenylamine ND ug/L 07/29/16 09:16 86-30-607/27/16 11:2112.5 1.7 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/29/16 09:16 108-60-107/27/16 11:2112.5 2.0 1 Pentachlorophenol ND ug/L 07/29/16 09:16 87-86-507/27/16 11:2131.2 2.9 1 Phenanthrene ND ug/L 07/29/16 09:16 85-01-807/27/16 11:2112.5 0.28 1 Phenol ND ug/L 07/29/16 09:1607/27/16 11:2112.5 2.1 1 Pyrene ND ug/L 07/29/16 09:16 129-00-007/27/16 11:2112.5 0.24 1 1,2,4-Trichlorobenzene ND ug/L 07/29/16 09:16 120-82-107/27/16 11:2112.5 2.4 1 2,4,5-Trichlorophenol ND ug/L 07/29/16 09:16 95-95-407/27/16 11:2112.5 2.8 1 2,4,6-Trichlorophenol ND ug/L 07/29/16 09:16 88-06-207/27/16 11:2112.5 2.4 1 Surrogates Nitrobenzene-d5 (S)85 %07/29/16 09:16 4165-60-007/27/16 11:2121-110 1 2-Fluorobiphenyl (S)74 %07/29/16 09:16 321-60-807/27/16 11:2127-110 1 Terphenyl-d14 (S)97 %07/29/16 09:16 1718-51-007/27/16 11:2131-107 1 Phenol-d6 (S)43 %07/29/16 09:16 13127-88-307/27/16 11:2110-110 1 2-Fluorophenol (S)54 %07/29/16 09:16 367-12-407/27/16 11:2112-110 1 2,4,6-Tribromophenol (S)88 %07/29/16 09:16 118-79-607/27/16 11:2127-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone ND ug/L 07/28/16 15:40 67-64-125.0 10.0 1 Benzene ND ug/L 07/28/16 15:40 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/28/16 15:40 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 29 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Sample: MW-7 Lab ID: 92306363001 Collected: 07/25/16 09:30 Received: 07/25/16 14:20 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/28/16 15:40 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/28/16 15:40 75-27-41.0 0.18 1 Bromoform ND ug/L 07/28/16 15:40 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/28/16 15:40 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/28/16 15:40 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/28/16 15:40 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/28/16 15:40 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/28/16 15:40 75-00-31.0 0.54 1 Chloroform ND ug/L 07/28/16 15:40 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/28/16 15:40 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/28/16 15:40 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/28/16 15:40 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/28/16 15:40 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/28/16 15:40 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/28/16 15:40 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/28/16 15:40 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/28/16 15:40 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/28/16 15:40 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/28/16 15:40 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/28/16 15:40 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/28/16 15:40 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/28/16 15:40 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/28/16 15:40 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/28/16 15:40 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/28/16 15:40 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/28/16 15:40 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/28/16 15:40 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/28/16 15:40 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/28/16 15:40 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/28/16 15:40 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/28/16 15:40 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/28/16 15:40 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/28/16 15:40 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/28/16 15:40 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/28/16 15:40 591-78-65.0 0.46 1 p-Isopropyltoluene ND ug/L 07/28/16 15:40 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/28/16 15:40 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/16 15:40 108-10-15.0 0.33 1 Methyl-tert-butyl ether 12.8 ug/L 07/28/16 15:40 1634-04-41.0 0.21 1 Naphthalene ND ug/L 07/28/16 15:40 91-20-31.0 0.24 1 Styrene ND ug/L 07/28/16 15:40 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/28/16 15:40 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/28/16 15:40 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/28/16 15:40 127-18-41.0 0.46 1 Toluene ND ug/L 07/28/16 15:40 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/28/16 15:40 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 29 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Sample: MW-7 Lab ID: 92306363001 Collected: 07/25/16 09:30 Received: 07/25/16 14:20 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/28/16 15:40 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/28/16 15:40 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/28/16 15:40 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/28/16 15:40 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/28/16 15:40 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/28/16 15:40 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/28/16 15:40 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/28/16 15:40 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/28/16 15:40 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/28/16 15:40 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/28/16 15:40 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)99 %07/28/16 15:40 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/28/16 15:40 17060-07-070-130 1 Toluene-d8 (S)100 %07/28/16 15:40 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 29 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Sample: MW-13 Lab ID: 92306363002 Collected: 07/25/16 13:00 Received: 07/25/16 14:20 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/29/16 19:41 7440-38-207/28/16 19:4010.0 5.0 1 Barium 191 ug/L 07/29/16 19:41 7440-39-307/28/16 19:405.0 2.5 1 Cadmium ND ug/L 07/29/16 19:41 7440-43-907/28/16 19:401.0 0.50 1 Chromium ND ug/L 07/29/16 19:41 7440-47-307/28/16 19:405.0 2.5 1 Lead ND ug/L 07/29/16 19:41 7439-92-107/28/16 19:405.0 2.5 1 Selenium ND ug/L 07/29/16 19:41 7782-49-207/28/16 19:4010.0 5.0 1 Silver ND ug/L 07/29/16 19:41 7440-22-407/28/16 19:405.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/28/16 12:53 7439-97-607/28/16 08:400.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/29/16 11:43 83-32-907/27/16 11:2110.0 0.25 1 Acenaphthylene ND ug/L 07/29/16 11:43 208-96-807/27/16 11:2110.0 0.21 1 Aniline ND ug/L 07/29/16 11:43 62-53-307/27/16 11:2110.0 1.3 1 Anthracene ND ug/L 07/29/16 11:43 120-12-707/27/16 11:2110.0 0.14 1 Benzo(a)anthracene ND ug/L 07/29/16 11:43 56-55-307/27/16 11:2110.0 0.33 1 Benzo(a)pyrene ND ug/L 07/29/16 11:43 50-32-807/27/16 11:2110.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/29/16 11:43 205-99-207/27/16 11:2110.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/29/16 11:43 191-24-207/27/16 11:2110.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/29/16 11:43 207-08-907/27/16 11:2110.0 0.43 1 Benzoic Acid ND ug/L 07/29/16 11:43 65-85-007/27/16 11:2150.0 11.1 1 Benzyl alcohol ND ug/L 07/29/16 11:43 100-51-607/27/16 11:2120.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/29/16 11:43 101-55-307/27/16 11:2110.0 1.3 1 Butylbenzylphthalate ND ug/L 07/29/16 11:43 85-68-707/27/16 11:2110.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/29/16 11:43 59-50-707/27/16 11:2120.0 4.2 1 4-Chloroaniline ND ug/L 07/29/16 11:43 106-47-807/27/16 11:2120.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/29/16 11:43 111-91-107/27/16 11:2110.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/29/16 11:43 111-44-407/27/16 11:2110.0 1.5 1 2-Chloronaphthalene ND ug/L 07/29/16 11:43 91-58-707/27/16 11:2110.0 2.2 1 2-Chlorophenol ND ug/L 07/29/16 11:43 95-57-807/27/16 11:2110.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/29/16 11:43 7005-72-307/27/16 11:2110.0 2.1 1 Chrysene ND ug/L 07/29/16 11:43 218-01-907/27/16 11:2110.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/29/16 11:43 53-70-307/27/16 11:2110.0 0.55 1 Dibenzofuran ND ug/L 07/29/16 11:43 132-64-907/27/16 11:2110.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/29/16 11:43 95-50-107/27/16 11:2110.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/29/16 11:43 541-73-107/27/16 11:2110.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/29/16 11:43 106-46-707/27/16 11:2110.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/29/16 11:43 91-94-107/27/16 11:2120.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/29/16 11:43 120-83-207/27/16 11:2110.0 1.7 1 Diethylphthalate ND ug/L 07/29/16 11:43 84-66-207/27/16 11:2110.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/29/16 11:43 105-67-907/27/16 11:2110.0 2.2 1 Dimethylphthalate ND ug/L 07/29/16 11:43 131-11-307/27/16 11:2110.0 1.5 1 Di-n-butylphthalate ND ug/L 07/29/16 11:43 84-74-207/27/16 11:2110.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/29/16 11:43 534-52-107/27/16 11:2120.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/29/16 11:43 51-28-507/27/16 11:2150.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 29 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Sample: MW-13 Lab ID: 92306363002 Collected: 07/25/16 13:00 Received: 07/25/16 14:20 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/29/16 11:43 121-14-207/27/16 11:2110.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/29/16 11:43 606-20-207/27/16 11:2110.0 1.7 1 Di-n-octylphthalate ND ug/L 07/29/16 11:43 117-84-007/27/16 11:2110.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/29/16 11:43 117-81-707/27/16 11:216.0 0.85 1 Fluoranthene ND ug/L 07/29/16 11:43 206-44-007/27/16 11:2110.0 0.21 1 Fluorene ND ug/L 07/29/16 11:43 86-73-707/27/16 11:2110.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/29/16 11:43 87-68-307/27/16 11:2110.0 1.8 1 Hexachlorobenzene ND ug/L 07/29/16 11:43 118-74-107/27/16 11:2110.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/29/16 11:43 77-47-407/27/16 11:2110.0 1.8 1 Hexachloroethane ND ug/L 07/29/16 11:43 67-72-107/27/16 11:2110.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/29/16 11:43 193-39-507/27/16 11:2110.0 0.29 1 Isophorone ND ug/L 07/29/16 11:43 78-59-107/27/16 11:2110.0 1.8 1 1-Methylnaphthalene ND ug/L 07/29/16 11:43 90-12-007/27/16 11:2110.0 0.32 1 2-Methylnaphthalene ND ug/L 07/29/16 11:43 91-57-607/27/16 11:2110.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/29/16 11:43 95-48-707/27/16 11:2110.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/29/16 11:4307/27/16 11:2110.0 1.7 1 Naphthalene ND ug/L 07/29/16 11:43 91-20-307/27/16 11:2110.0 0.34 1 2-Nitroaniline ND ug/L 07/29/16 11:43 88-74-407/27/16 11:2150.0 2.8 1 3-Nitroaniline ND ug/L 07/29/16 11:43 99-09-207/27/16 11:2150.0 2.4 1 4-Nitroaniline ND ug/L 07/29/16 11:43 100-01-607/27/16 11:2120.0 2.5 1 Nitrobenzene ND ug/L 07/29/16 11:43 98-95-307/27/16 11:2110.0 1.7 1 2-Nitrophenol ND ug/L 07/29/16 11:43 88-75-507/27/16 11:2110.0 1.7 1 4-Nitrophenol ND ug/L 07/29/16 11:43 100-02-707/27/16 11:2150.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/29/16 11:43 62-75-907/27/16 11:2110.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/29/16 11:43 621-64-707/27/16 11:2110.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/29/16 11:43 86-30-607/27/16 11:2110.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/29/16 11:43 108-60-107/27/16 11:2110.0 1.6 1 Pentachlorophenol ND ug/L 07/29/16 11:43 87-86-507/27/16 11:2125.0 2.3 1 Phenanthrene ND ug/L 07/29/16 11:43 85-01-807/27/16 11:2110.0 0.22 1 Phenol ND ug/L 07/29/16 11:4307/27/16 11:2110.0 1.7 1 Pyrene ND ug/L 07/29/16 11:43 129-00-007/27/16 11:2110.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/29/16 11:43 120-82-107/27/16 11:2110.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/29/16 11:43 95-95-407/27/16 11:2110.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/29/16 11:43 88-06-207/27/16 11:2110.0 1.9 1 Surrogates Nitrobenzene-d5 (S)82 %07/29/16 11:43 4165-60-007/27/16 11:2121-110 1 2-Fluorobiphenyl (S)76 %07/29/16 11:43 321-60-807/27/16 11:2127-110 1 Terphenyl-d14 (S)93 %07/29/16 11:43 1718-51-007/27/16 11:2131-107 1 Phenol-d6 (S)39 %07/29/16 11:43 13127-88-307/27/16 11:2110-110 1 2-Fluorophenol (S)51 %07/29/16 11:43 367-12-407/27/16 11:2112-110 1 2,4,6-Tribromophenol (S)83 %07/29/16 11:43 118-79-607/27/16 11:2127-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone ND ug/L 07/28/16 12:49 67-64-125.0 10.0 1 Benzene ND ug/L 07/28/16 12:49 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/28/16 12:49 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 29 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Sample: MW-13 Lab ID: 92306363002 Collected: 07/25/16 13:00 Received: 07/25/16 14:20 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/28/16 12:49 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/28/16 12:49 75-27-41.0 0.18 1 Bromoform ND ug/L 07/28/16 12:49 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/28/16 12:49 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/28/16 12:49 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/28/16 12:49 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/28/16 12:49 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/28/16 12:49 75-00-31.0 0.54 1 Chloroform ND ug/L 07/28/16 12:49 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/28/16 12:49 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/28/16 12:49 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/28/16 12:49 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/28/16 12:49 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/28/16 12:49 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/28/16 12:49 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/28/16 12:49 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/28/16 12:49 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/28/16 12:49 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/28/16 12:49 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/28/16 12:49 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/28/16 12:49 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/28/16 12:49 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/28/16 12:49 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/28/16 12:49 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/28/16 12:49 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/28/16 12:49 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/28/16 12:49 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/28/16 12:49 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/28/16 12:49 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/28/16 12:49 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/28/16 12:49 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/28/16 12:49 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/28/16 12:49 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/28/16 12:49 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/28/16 12:49 591-78-65.0 0.46 1 p-Isopropyltoluene ND ug/L 07/28/16 12:49 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/28/16 12:49 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/16 12:49 108-10-15.0 0.33 1 Methyl-tert-butyl ether ND ug/L 07/28/16 12:49 1634-04-41.0 0.21 1 Naphthalene ND ug/L 07/28/16 12:49 91-20-31.0 0.24 1 Styrene ND ug/L 07/28/16 12:49 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/28/16 12:49 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/28/16 12:49 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/28/16 12:49 127-18-41.0 0.46 1 Toluene ND ug/L 07/28/16 12:49 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/28/16 12:49 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 29 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Sample: MW-13 Lab ID: 92306363002 Collected: 07/25/16 13:00 Received: 07/25/16 14:20 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/28/16 12:49 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/28/16 12:49 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/28/16 12:49 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/28/16 12:49 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/28/16 12:49 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/28/16 12:49 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/28/16 12:49 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/28/16 12:49 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/28/16 12:49 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/28/16 12:49 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/28/16 12:49 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)99 %07/28/16 12:49 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/28/16 12:49 17060-07-070-130 1 Toluene-d8 (S)99 %07/28/16 12:49 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 29 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Sample: MW-9 Lab ID: 92306363003 Collected: 07/25/16 10:00 Received: 07/25/16 14:20 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/29/16 19:44 7440-38-207/28/16 19:4010.0 5.0 1 Barium 271 ug/L 07/29/16 19:44 7440-39-307/28/16 19:405.0 2.5 1 Cadmium ND ug/L 07/29/16 19:44 7440-43-907/28/16 19:401.0 0.50 1 Chromium 9.6 ug/L 07/29/16 19:44 7440-47-307/28/16 19:405.0 2.5 1 Lead ND ug/L 07/29/16 19:44 7439-92-107/28/16 19:405.0 2.5 1 Selenium ND ug/L 07/29/16 19:44 7782-49-207/28/16 19:4010.0 5.0 1 Silver ND ug/L 07/29/16 19:44 7440-22-407/28/16 19:405.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/28/16 12:56 7439-97-607/28/16 08:400.20 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 322816 EPA 7470 EPA 7470 7470 Mercury Associated Lab Samples: 92306363001, 92306363002, 92306363003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1788620 Associated Lab Samples:92306363001, 92306363002, 92306363003 Matrix: Water AnalyzedMDL Mercury ug/L ND 0.20 07/28/16 12:420.10 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1788621LABORATORY CONTROL SAMPLE: LCSSpike Mercury ug/L 2.62.5 104 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1788622MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92306363001 1788623 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury ug/L 2.5 80 75-12576 6 252.5ND 2.0 1.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 322834 EPA 3010A EPA 6010 6010 MET Associated Lab Samples: 92306363001, 92306363002, 92306363003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1788776 Associated Lab Samples:92306363001, 92306363002, 92306363003 Matrix: Water AnalyzedMDL Arsenic ug/L ND 10.0 07/29/16 19:165.0 Barium ug/L ND 5.0 07/29/16 19:162.5 Cadmium ug/L ND 1.0 07/29/16 19:160.50 Chromium ug/L ND 5.0 07/29/16 19:162.5 Lead ug/L ND 5.0 07/29/16 19:162.5 Selenium ug/L ND 10.0 07/29/16 19:165.0 Silver ug/L ND 5.0 07/29/16 19:162.5 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1788777LABORATORY CONTROL SAMPLE: LCSSpike Arsenic ug/L 462500 92 80-120 Barium ug/L 502500 100 80-120 Cadmium ug/L 487500 97 80-120 Chromium ug/L 490500 98 80-120 Lead ug/L 473500 95 80-120 Selenium ug/L 477500 95 80-120 Silver ug/L 241250 97 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1788778MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92306363001 1788779 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic ug/L 500 94 75-12598 4 20500ND471 489 Barium ug/L 500 100 75-125102 1 20500226724 734 Cadmium ug/L 500 98 75-125100 3 20500ND489 502 Chromium ug/L 500 95 75-12598 3 20500ND479 493 Lead ug/L 500 91 75-12594 3 20500ND457 469 Selenium ug/L 500 96 75-12599 3 20500ND480 494 Silver ug/L 250 96 75-12599 3 20250ND240 247 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 322900 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples: 92306363001, 92306363002 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1789050 Associated Lab Samples:92306363001, 92306363002 Matrix: Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/28/16 11:580.33 1,1,1-Trichloroethane ug/L ND 1.0 07/28/16 11:580.48 1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/28/16 11:580.40 1,1,2-Trichloroethane ug/L ND 1.0 07/28/16 11:580.29 1,1-Dichloroethane ug/L ND 1.0 07/28/16 11:580.32 1,1-Dichloroethene ug/L ND 1.0 07/28/16 11:580.56 1,1-Dichloropropene ug/L ND 1.0 07/28/16 11:580.49 1,2,3-Trichlorobenzene ug/L ND 1.0 07/28/16 11:580.33 1,2,3-Trichloropropane ug/L ND 1.0 07/28/16 11:580.41 1,2,4-Trichlorobenzene ug/L ND 1.0 07/28/16 11:580.35 1,2-Dibromo-3-chloropropane ug/L ND 2.0 07/28/16 11:582.0 1,2-Dibromoethane (EDB)ug/L ND 1.0 07/28/16 11:580.27 1,2-Dichlorobenzene ug/L ND 1.0 07/28/16 11:580.30 1,2-Dichloroethane ug/L ND 1.0 07/28/16 11:580.24 1,2-Dichloropropane ug/L ND 1.0 07/28/16 11:580.27 1,3-Dichlorobenzene ug/L ND 1.0 07/28/16 11:580.24 1,3-Dichloropropane ug/L ND 1.0 07/28/16 11:580.28 1,4-Dichlorobenzene ug/L ND 1.0 07/28/16 11:580.33 2,2-Dichloropropane ug/L ND 1.0 07/28/16 11:580.13 2-Butanone (MEK)ug/L ND 5.0 07/28/16 11:580.96 2-Chlorotoluene ug/L ND 1.0 07/28/16 11:580.35 2-Hexanone ug/L ND 5.0 07/28/16 11:580.46 4-Chlorotoluene ug/L ND 1.0 07/28/16 11:580.31 4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/28/16 11:580.33 Acetone ug/L ND 25.0 07/28/16 11:5810.0 Benzene ug/L ND 1.0 07/28/16 11:580.25 Bromobenzene ug/L ND 1.0 07/28/16 11:580.30 Bromochloromethane ug/L ND 1.0 07/28/16 11:580.17 Bromodichloromethane ug/L ND 1.0 07/28/16 11:580.18 Bromoform ug/L ND 1.0 07/28/16 11:580.26 Bromomethane ug/L ND 2.0 07/28/16 11:580.29 Carbon tetrachloride ug/L ND 1.0 07/28/16 11:580.25 Chlorobenzene ug/L ND 1.0 07/28/16 11:580.23 Chloroethane ug/L ND 1.0 07/28/16 11:580.54 Chloroform ug/L ND 1.0 07/28/16 11:580.14 Chloromethane ug/L ND 1.0 07/28/16 11:580.11 cis-1,2-Dichloroethene ug/L ND 1.0 07/28/16 11:580.19 cis-1,3-Dichloropropene ug/L ND 1.0 07/28/16 11:580.13 Dibromochloromethane ug/L ND 1.0 07/28/16 11:580.21 Dibromomethane ug/L ND 1.0 07/28/16 11:580.21 Dichlorodifluoromethane ug/L ND 1.0 07/28/16 11:580.21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1789050 Associated Lab Samples:92306363001, 92306363002 Matrix: Water AnalyzedMDL Diisopropyl ether ug/L ND 1.0 07/28/16 11:580.12 Ethylbenzene ug/L ND 1.0 07/28/16 11:580.30 Hexachloro-1,3-butadiene ug/L ND 1.0 07/28/16 11:580.71 m&p-Xylene ug/L ND 2.0 07/28/16 11:580.66 Methyl-tert-butyl ether ug/L ND 1.0 07/28/16 11:580.21 Methylene Chloride ug/L ND 2.0 07/28/16 11:580.97 Naphthalene ug/L ND 1.0 07/28/16 11:580.24 o-Xylene ug/L ND 1.0 07/28/16 11:580.23 p-Isopropyltoluene ug/L ND 1.0 07/28/16 11:580.31 Styrene ug/L ND 1.0 07/28/16 11:580.26 Tetrachloroethene ug/L ND 1.0 07/28/16 11:580.46 Toluene ug/L ND 1.0 07/28/16 11:580.26 trans-1,2-Dichloroethene ug/L ND 1.0 07/28/16 11:580.49 trans-1,3-Dichloropropene ug/L ND 1.0 07/28/16 11:580.26 Trichloroethene ug/L ND 1.0 07/28/16 11:580.47 Trichlorofluoromethane ug/L ND 1.0 07/28/16 11:580.20 Vinyl acetate ug/L ND 2.0 07/28/16 11:580.35 Vinyl chloride ug/L ND 1.0 07/28/16 11:580.62 Xylene (Total)ug/L ND 1.0 07/28/16 11:580.66 1,2-Dichloroethane-d4 (S)%101 70-130 07/28/16 11:58 4-Bromofluorobenzene (S)%100 70-130 07/28/16 11:58 Toluene-d8 (S)%100 70-130 07/28/16 11:58 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1789051LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 49.050 98 70-130 1,1,1-Trichloroethane ug/L 49.450 99 70-130 1,1,2,2-Tetrachloroethane ug/L 47.850 96 70-130 1,1,2-Trichloroethane ug/L 49.450 99 70-130 1,1-Dichloroethane ug/L 49.150 98 70-130 1,1-Dichloroethene ug/L 52.850 106 70-132 1,1-Dichloropropene ug/L 51.850 104 70-130 1,2,3-Trichlorobenzene ug/L 50.850 102 70-135 1,2,3-Trichloropropane ug/L 47.250 94 70-130 1,2,4-Trichlorobenzene ug/L 51.450 103 70-134 1,2-Dibromo-3-chloropropane ug/L 51.650 103 70-130 1,2-Dibromoethane (EDB)ug/L 52.250 104 70-130 1,2-Dichlorobenzene ug/L 50.250 100 70-130 1,2-Dichloroethane ug/L 46.550 93 70-130 1,2-Dichloropropane ug/L 48.650 97 70-130 1,3-Dichlorobenzene ug/L 51.450 103 70-130 1,3-Dichloropropane ug/L 47.650 95 70-130 1,4-Dichlorobenzene ug/L 51.250 102 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1789051LABORATORY CONTROL SAMPLE: LCSSpike 2,2-Dichloropropane ug/L 52.750 105 58-145 2-Butanone (MEK)ug/L 93.9100 94 70-145 2-Chlorotoluene ug/L 50.650 101 70-130 2-Hexanone ug/L 97.1100 97 70-144 4-Chlorotoluene ug/L 50.650 101 70-130 4-Methyl-2-pentanone (MIBK)ug/L 96.8100 97 70-140 Acetone ug/L 95.9100 96 50-175 Benzene ug/L 50.650 101 70-130 Bromobenzene ug/L 50.350 101 70-130 Bromochloromethane ug/L 51.550 103 70-130 Bromodichloromethane ug/L 50.050 100 70-130 Bromoform ug/L 49.350 99 70-130 Bromomethane ug/L 35.350 71 54-130 Carbon tetrachloride ug/L 52.750 105 70-132 Chlorobenzene ug/L 51.350 103 70-130 Chloroethane ug/L 53.450 107 64-134 Chloroform ug/L 48.150 96 70-130 Chloromethane ug/L 39.750 79 64-130 cis-1,2-Dichloroethene ug/L 50.150 100 70-131 cis-1,3-Dichloropropene ug/L 51.450 103 70-130 Dibromochloromethane ug/L 50.250 100 70-130 Dibromomethane ug/L 50.150 100 70-131 Dichlorodifluoromethane ug/L 51.250 102 56-130 Diisopropyl ether ug/L 49.150 98 70-130 Ethylbenzene ug/L 49.950 100 70-130 Hexachloro-1,3-butadiene ug/L 50.850 102 70-130 m&p-Xylene ug/L 98.9100 99 70-130 Methyl-tert-butyl ether ug/L 49.750 99 70-130 Methylene Chloride ug/L 49.050 98 63-130 Naphthalene ug/L 50.450 101 70-138 o-Xylene ug/L 49.250 98 70-130 p-Isopropyltoluene ug/L 50.050 100 70-130 Styrene ug/L 52.450 105 70-130 Tetrachloroethene ug/L 48.850 98 70-130 Toluene ug/L 50.250 100 70-130 trans-1,2-Dichloroethene ug/L 52.850 106 70-130 trans-1,3-Dichloropropene ug/L 49.350 99 70-132 Trichloroethene ug/L 50.550 101 70-130 Trichlorofluoromethane ug/L 52.750 105 62-133 Vinyl acetate ug/L 92.0100 92 66-157 Vinyl chloride ug/L 51.550 103 50-150 Xylene (Total)ug/L 148150 99 70-130 1,2-Dichloroethane-d4 (S)%97 70-130 4-Bromofluorobenzene (S)%99 70-130 Toluene-d8 (S)%100 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1789053MATRIX SPIKE SAMPLE: MSSpike Result 92306586001 1,1,1,2-Tetrachloroethane ug/L 21.720 109 70-130ND 1,1,1-Trichloroethane ug/L 22.120 111 70-130ND 1,1,2,2-Tetrachloroethane ug/L 21.020 105 70-130ND 1,1,2-Trichloroethane ug/L 21.220 106 70-130ND 1,1-Dichloroethane ug/L 21.520 107 70-130ND 1,1-Dichloroethene ug/L 22.720 114 70-166ND 1,1-Dichloropropene ug/L 22.220 111 70-130ND 1,2,3-Trichlorobenzene ug/L 22.220 111 70-130ND 1,2,3-Trichloropropane ug/L 20.120 100 70-130ND 1,2,4-Trichlorobenzene ug/L 21.820 109 70-130ND 1,2-Dibromo-3-chloropropane ug/L 20.420 102 70-130ND 1,2-Dibromoethane (EDB)ug/L 22.620 113 70-130ND 1,2-Dichlorobenzene ug/L 21.820 109 70-130ND 1,2-Dichloroethane ug/L 20.520 103 70-130ND 1,2-Dichloropropane ug/L 20.920 104 70-130ND 1,3-Dichlorobenzene ug/L 22.420 112 70-130ND 1,3-Dichloropropane ug/L 20.820 104 70-130ND 1,4-Dichlorobenzene ug/L 22.220 111 70-130ND 2,2-Dichloropropane ug/L 20.620 103 70-130ND 2-Butanone (MEK)ug/L 38.740 97 70-130ND 2-Chlorotoluene ug/L 22.620 113 70-130ND 2-Hexanone ug/L 40.740 102 70-130ND 4-Chlorotoluene ug/L 22.920 114 70-130ND 4-Methyl-2-pentanone (MIBK)ug/L 40.740 102 70-130ND Acetone ug/L 42.640 106 70-130ND Benzene ug/L 21.520 107 70-148ND Bromobenzene ug/L 21.920 109 70-130ND Bromochloromethane ug/L 21.520 107 70-130ND Bromodichloromethane ug/L 22.820 107 70-1301.4 Bromoform ug/L 19.920 99 70-130ND Bromomethane ug/L 6.2 M12031 70-130ND Carbon tetrachloride ug/L 22.520 113 70-130ND Chlorobenzene ug/L 23.020 115 70-146ND Chloroethane ug/L 21.920 110 70-130ND Chloroform ug/L 26.320 103 70-1305.8 Chloromethane ug/L 12.7 M12063 70-130ND cis-1,2-Dichloroethene ug/L 21.920 109 70-130ND cis-1,3-Dichloropropene ug/L 20.920 104 70-130ND Dibromochloromethane ug/L 21.720 109 70-130ND Dibromomethane ug/L 21.120 106 70-130ND Dichlorodifluoromethane ug/L 14.320 71 70-130ND Diisopropyl ether ug/L 21.120 106 70-130ND Ethylbenzene ug/L 22.320 112 70-130ND Hexachloro-1,3-butadiene ug/L 22.120 110 70-130ND m&p-Xylene ug/L 43.840 110 70-130ND Methyl-tert-butyl ether ug/L 23.820 105 70-1302.7 Methylene Chloride ug/L 20.220 101 70-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1789053MATRIX SPIKE SAMPLE: MSSpike Result 92306586001 Naphthalene ug/L 20.720 104 70-130ND o-Xylene ug/L 21.920 109 70-130ND p-Isopropyltoluene ug/L 22.020 110 70-130ND Styrene ug/L 22.920 115 70-130ND Tetrachloroethene ug/L 21.520 107 70-130ND Toluene ug/L 24.420 107 70-1553.0 trans-1,2-Dichloroethene ug/L 23.020 115 70-130ND trans-1,3-Dichloropropene ug/L 19.920 99 70-130ND Trichloroethene ug/L 22.020 110 69-151ND Trichlorofluoromethane ug/L 22.520 113 70-130ND Vinyl acetate ug/L 33.740 84 70-130ND Vinyl chloride ug/L 19.320 97 70-130ND 1,2-Dichloroethane-d4 (S)%98 70-130 4-Bromofluorobenzene (S)%102 70-130 Toluene-d8 (S)%100 70-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92306683004 1789052SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/L ND 30ND 1,1,1-Trichloroethane ug/L ND 30ND 1,1,2,2-Tetrachloroethane ug/L ND 30ND 1,1,2-Trichloroethane ug/L ND 30ND 1,1-Dichloroethane ug/L ND 30ND 1,1-Dichloroethene ug/L ND 30ND 1,1-Dichloropropene ug/L ND 30ND 1,2,3-Trichlorobenzene ug/L ND 30ND 1,2,3-Trichloropropane ug/L ND 30ND 1,2,4-Trichlorobenzene ug/L ND 30ND 1,2-Dibromo-3-chloropropane ug/L ND 30ND 1,2-Dibromoethane (EDB)ug/L ND 30ND 1,2-Dichlorobenzene ug/L ND 30ND 1,2-Dichloroethane ug/L ND 30ND 1,2-Dichloropropane ug/L ND 30ND 1,3-Dichlorobenzene ug/L ND 30ND 1,3-Dichloropropane ug/L ND 30ND 1,4-Dichlorobenzene ug/L ND 30ND 2,2-Dichloropropane ug/L ND 30ND 2-Butanone (MEK)ug/L ND 30ND 2-Chlorotoluene ug/L ND 30ND 2-Hexanone ug/L ND 30ND 4-Chlorotoluene ug/L ND 30ND 4-Methyl-2-pentanone (MIBK)ug/L ND 30ND Acetone ug/L ND 30ND Benzene ug/L ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92306683004 1789052SAMPLE DUPLICATE: Bromobenzene ug/L ND 30ND Bromochloromethane ug/L ND 30ND Bromodichloromethane ug/L ND 30ND Bromoform ug/L ND 30ND Bromomethane ug/L ND 30ND Carbon tetrachloride ug/L ND 30ND Chlorobenzene ug/L ND 30ND Chloroethane ug/L ND 30ND Chloroform ug/L ND 30ND Chloromethane ug/L ND 30ND cis-1,2-Dichloroethene ug/L ND 30ND cis-1,3-Dichloropropene ug/L ND 30ND Dibromochloromethane ug/L ND 30ND Dibromomethane ug/L ND 30ND Dichlorodifluoromethane ug/L ND 30ND Diisopropyl ether ug/L ND 30ND Ethylbenzene ug/L ND 30ND Hexachloro-1,3-butadiene ug/L ND 30ND m&p-Xylene ug/L ND 30ND Methyl-tert-butyl ether ug/L ND 30ND Methylene Chloride ug/L ND 30ND Naphthalene ug/L ND 30ND o-Xylene ug/L ND 30ND p-Isopropyltoluene ug/L ND 30ND Styrene ug/L ND 30ND Tetrachloroethene ug/L ND 30ND Toluene ug/L ND 30ND trans-1,2-Dichloroethene ug/L ND 30ND trans-1,3-Dichloropropene ug/L ND 30ND Trichloroethene ug/L ND 30ND Trichlorofluoromethane ug/L ND 30ND Vinyl acetate ug/L ND 30ND Vinyl chloride ug/L ND 30ND Xylene (Total)ug/L ND 30ND 1,2-Dichloroethane-d4 (S)%100 099 4-Bromofluorobenzene (S)%100 199 Toluene-d8 (S)%99 198 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 322727 EPA 3510 EPA 8270 8270 Water MSSV Associated Lab Samples: 92306363001, 92306363002 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1788005 Associated Lab Samples:92306363001, 92306363002 Matrix: Water AnalyzedMDL 1,2,4-Trichlorobenzene ug/L ND 10.0 07/28/16 12:111.9 1,2-Dichlorobenzene ug/L ND 10.0 07/28/16 12:111.2 1,3-Dichlorobenzene ug/L ND 10.0 07/28/16 12:111.1 1,4-Dichlorobenzene ug/L ND 10.0 07/28/16 12:111.2 1-Methylnaphthalene ug/L ND 10.0 07/28/16 12:110.32 2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 07/28/16 12:111.6 2,4,5-Trichlorophenol ug/L ND 10.0 07/28/16 12:112.2 2,4,6-Trichlorophenol ug/L ND 10.0 07/28/16 12:111.9 2,4-Dichlorophenol ug/L ND 10.0 07/28/16 12:111.7 2,4-Dimethylphenol ug/L ND 10.0 07/28/16 12:112.2 2,4-Dinitrophenol ug/L ND 50.0 07/28/16 12:116.5 2,4-Dinitrotoluene ug/L ND 10.0 07/28/16 12:111.2 2,6-Dinitrotoluene ug/L ND 10.0 07/28/16 12:111.7 2-Chloronaphthalene ug/L ND 10.0 07/28/16 12:112.2 2-Chlorophenol ug/L ND 10.0 07/28/16 12:111.5 2-Methylnaphthalene ug/L ND 10.0 07/28/16 12:110.28 2-Methylphenol(o-Cresol)ug/L ND 10.0 07/28/16 12:111.7 2-Nitroaniline ug/L ND 50.0 07/28/16 12:112.8 2-Nitrophenol ug/L ND 10.0 07/28/16 12:111.7 3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/28/16 12:111.7 3,3'-Dichlorobenzidine ug/L ND 20.0 07/28/16 12:111.4 3-Nitroaniline ug/L ND 50.0 07/28/16 12:112.4 4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/28/16 12:111.7 4-Bromophenylphenyl ether ug/L ND 10.0 07/28/16 12:111.3 4-Chloro-3-methylphenol ug/L ND 20.0 07/28/16 12:114.2 4-Chloroaniline ug/L ND 20.0 07/28/16 12:113.4 4-Chlorophenylphenyl ether ug/L ND 10.0 07/28/16 12:112.1 4-Nitroaniline ug/L ND 20.0 07/28/16 12:112.5 4-Nitrophenol ug/L ND 50.0 07/28/16 12:115.8 Acenaphthene ug/L ND 10.0 07/28/16 12:110.25 Acenaphthylene ug/L ND 10.0 07/28/16 12:110.21 Aniline ug/L ND 10.0 07/28/16 12:111.3 Anthracene ug/L ND 10.0 07/28/16 12:110.14 Benzo(a)anthracene ug/L ND 10.0 07/28/16 12:110.33 Benzo(a)pyrene ug/L ND 10.0 07/28/16 12:110.30 Benzo(b)fluoranthene ug/L ND 10.0 07/28/16 12:110.28 Benzo(g,h,i)perylene ug/L ND 10.0 07/28/16 12:110.38 Benzo(k)fluoranthene ug/L ND 10.0 07/28/16 12:110.43 Benzoic Acid ug/L ND 50.0 07/28/16 12:1111.1 Benzyl alcohol ug/L ND 20.0 07/28/16 12:113.4 bis(2-Chloroethoxy)methane ug/L ND 10.0 07/28/16 12:111.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1788005 Associated Lab Samples:92306363001, 92306363002 Matrix: Water AnalyzedMDL bis(2-Chloroethyl) ether ug/L ND 10.0 07/28/16 12:111.5 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 07/28/16 12:110.85 Butylbenzylphthalate ug/L ND 10.0 07/28/16 12:110.75 Chrysene ug/L ND 10.0 07/28/16 12:110.21 Di-n-butylphthalate ug/L ND 10.0 07/28/16 12:111.1 Di-n-octylphthalate ug/L ND 10.0 07/28/16 12:110.86 Dibenz(a,h)anthracene ug/L ND 10.0 07/28/16 12:110.55 Dibenzofuran ug/L ND 10.0 07/28/16 12:111.8 Diethylphthalate ug/L ND 10.0 07/28/16 12:111.3 Dimethylphthalate ug/L ND 10.0 07/28/16 12:111.5 Fluoranthene ug/L ND 10.0 07/28/16 12:110.21 Fluorene ug/L ND 10.0 07/28/16 12:110.21 Hexachloro-1,3-butadiene ug/L ND 10.0 07/28/16 12:111.8 Hexachlorobenzene ug/L ND 10.0 07/28/16 12:111.1 Hexachlorocyclopentadiene ug/L ND 10.0 07/28/16 12:111.8 Hexachloroethane ug/L ND 10.0 07/28/16 12:111.5 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/28/16 12:110.29 Isophorone ug/L ND 10.0 07/28/16 12:111.8 N-Nitroso-di-n-propylamine ug/L ND 10.0 07/28/16 12:112.1 N-Nitrosodimethylamine ug/L ND 10.0 07/28/16 12:111.3 N-Nitrosodiphenylamine ug/L ND 10.0 07/28/16 12:111.3 Naphthalene ug/L ND 10.0 07/28/16 12:110.34 Nitrobenzene ug/L ND 10.0 07/28/16 12:111.7 Pentachlorophenol ug/L ND 25.0 07/28/16 12:112.3 Phenanthrene ug/L ND 10.0 07/28/16 12:110.22 Phenol ug/L ND 10.0 07/28/16 12:111.7 Pyrene ug/L ND 10.0 07/28/16 12:110.19 2,4,6-Tribromophenol (S)%87 27-110 07/28/16 12:11 2-Fluorobiphenyl (S)%84 27-110 07/28/16 12:11 2-Fluorophenol (S)%48 12-110 07/28/16 12:11 Nitrobenzene-d5 (S)%90 21-110 07/28/16 12:11 Phenol-d6 (S)%34 10-110 07/28/16 12:11 Terphenyl-d14 (S)%104 31-107 07/28/16 12:11 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1788006LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/L 37.850 76 31-120 1,2-Dichlorobenzene ug/L 37.150 74 38-120 1,3-Dichlorobenzene ug/L 36.650 73 30-122 1,4-Dichlorobenzene ug/L 36.250 72 37-120 1-Methylnaphthalene ug/L 45.450 91 34-113 2,2'-Oxybis(1-chloropropane)ug/L 50.150 100 18-120 2,4,5-Trichlorophenol ug/L 46.450 93 43-113 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1788006LABORATORY CONTROL SAMPLE: LCSSpike 2,4,6-Trichlorophenol ug/L 47.850 96 42-120 2,4-Dichlorophenol ug/L 46.050 92 30-120 2,4-Dimethylphenol ug/L 46.750 93 29-111 2,4-Dinitrophenol ug/L 162250 65 19-132 2,4-Dinitrotoluene ug/L 49.450 99 58-128 2,6-Dinitrotoluene ug/L 52.550 105 54-129 2-Chloronaphthalene ug/L 50.550 101 43-117 2-Chlorophenol ug/L 43.450 87 37-120 2-Methylnaphthalene ug/L 45.550 91 33-120 2-Methylphenol(o-Cresol)ug/L 39.850 80 31-120 2-Nitroaniline ug/L 108100 108 48-121 2-Nitrophenol ug/L 46.450 93 25-116 3&4-Methylphenol(m&p Cresol)ug/L 35.150 70 23-120 3,3'-Dichlorobenzidine ug/L 101100 101 10-154 3-Nitroaniline ug/L 102100 102 43-115 4,6-Dinitro-2-methylphenol ug/L 101100 101 44-124 4-Bromophenylphenyl ether ug/L 46.750 93 34-113 4-Chloro-3-methylphenol ug/L 98.5100 98 31-110 4-Chloroaniline ug/L 100100 100 20-120 4-Chlorophenylphenyl ether ug/L 44.550 89 34-116 4-Nitroaniline ug/L 97.6100 98 46-128 4-Nitrophenol ug/L 112250 45 11-120 Acenaphthene ug/L 44.750 89 48-114 Acenaphthylene ug/L 46.350 93 48-112 Aniline ug/L 40.950 82 26-120 Anthracene ug/L 45.850 92 57-118 Benzo(a)anthracene ug/L 47.150 94 56-121 Benzo(a)pyrene ug/L 47.050 94 55-127 Benzo(b)fluoranthene ug/L 48.050 96 53-128 Benzo(g,h,i)perylene ug/L 44.250 88 54-125 Benzo(k)fluoranthene ug/L 47.650 95 51-123 Benzoic Acid ug/L 77.8250 31 10-120 Benzyl alcohol ug/L 99.9100 100 27-120 bis(2-Chloroethoxy)methane ug/L 48.050 96 32-120 bis(2-Chloroethyl) ether ug/L 45.050 90 33-111 bis(2-Ethylhexyl)phthalate ug/L 55.050 110 50-145 Butylbenzylphthalate ug/L 57.150 114 54-138 Chrysene ug/L 45.750 91 58-127 Di-n-butylphthalate ug/L 48.550 97 56-125 Di-n-octylphthalate ug/L 49.250 98 50-134 Dibenz(a,h)anthracene ug/L 43.950 88 53-129 Dibenzofuran ug/L 49.450 99 45-120 Diethylphthalate ug/L 45.450 91 53-120 Dimethylphthalate ug/L 43.550 87 55-116 Fluoranthene ug/L 44.350 89 57-125 Fluorene ug/L 46.450 93 53-118 Hexachloro-1,3-butadiene ug/L 34.250 68 23-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 29 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1788006LABORATORY CONTROL SAMPLE: LCSSpike Hexachlorobenzene ug/L 42.650 85 49-116 Hexachlorocyclopentadiene ug/L 38.550 77 26-158 Hexachloroethane ug/L 35.950 72 30-114 Indeno(1,2,3-cd)pyrene ug/L 44.050 88 55-128 Isophorone ug/L 53.350 107 31-118 N-Nitroso-di-n-propylamine ug/L 59.050 118 32-119 N-Nitrosodimethylamine ug/L 26.850 54 13-120 N-Nitrosodiphenylamine ug/L 49.050 98 43-120 Naphthalene ug/L 41.850 84 32-120 Nitrobenzene ug/L 49.350 99 33-110 Pentachlorophenol ug/L 91.5100 92 10-137 Phenanthrene ug/L 44.350 89 57-117 Phenol ug/L 24.450 49 10-120 Pyrene ug/L 50.750 101 55-122 2,4,6-Tribromophenol (S)%93 27-110 2-Fluorobiphenyl (S)%86 27-110 2-Fluorophenol (S)%54 12-110 Nitrobenzene-d5 (S)%96 21-110 Phenol-d6 (S)%42 10-110 Terphenyl-d14 (S)%103 31-107 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 29 #=QL# QUALIFIERS Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 29 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92306363 UNIVERSITY FORD 1272C Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92306363001 322834 323044MW-7 EPA 3010A EPA 6010 92306363002 322834 323044MW-13 EPA 3010A EPA 6010 92306363003 322834 323044MW-9 EPA 3010A EPA 6010 92306363001 322816 322897MW-7 EPA 7470 EPA 7470 92306363002 322816 322897MW-13 EPA 7470 EPA 7470 92306363003 322816 322897MW-9 EPA 7470 EPA 7470 92306363001 322727 322883MW-7 EPA 3510 EPA 8270 92306363002 322727 322883MW-13 EPA 3510 EPA 8270 92306363001 322900MW-7 EPA 8260 92306363002 322900MW-13 EPA 8260 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:52 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 29 Page 28 of 29 Document Name: Sample Condition Upon Recelpt(SCUR) Document No.: Document Revised:April 25, 2016 Page 1 of 2 Issuing Authority: ;::2ceAnalytical~ l F·CHR·CS-003-rev.19 Pace Huntersville Quality Office · Sample 'conditio~, Upon Client Name: ~:,, _' ,Jt~_c~iPJL_:.,_, .:~_:_!__ Courier: D Commercial Custody Seal Present? Packing Material: Thermometer: 0Fed Ex ~Pace Oves ~No 0Bubble Wrap TlSOS OuPs OusPs Oother: __ Seals Intact? Oves 18:]Bubble Bags 0None Type of Ice: ijJWet Correction Factor: o.o•c Cooler Temp Corrected (°C): -)' .\ · .. c_. Temp should be above freezing to 6°C USDA Regulated Soil ( 0 N/A, water sample) Page 2 of 2 for Internal Use ONL) Project# LJQ#•92306363 II I Ill 1111111111111111 92306363 Oclient _16JNo Date/lnltlals Person Examining Contents: f.-P J/ft:/JJ; Oother: __ 0Blue O None Osamples on ice, cooling process has begun Biological Tissue Frozen? Oves ~No ON/A Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? 0Yes ~No Did samples originate from a foreign source (internationally, Chain of Custody Present? lilYes 0No ON/A Samples Arrived within Hold Time? riJYes 0No ON/A Short Hold Time Analysis (<72 hr.)? Oves l'ilNo ON/A Rush Turn Around Time Requested? O ves ~No ON/A Sufficient Volume? Iii Yes 0No ON/A Correct Containers Used? i,Jves 0No ON/A -Pace Containers Used? liJYes 0No ON/A Containers Intact? !'MYes 0No ON/A Samples Field Filtered? I Iii No O ves ON/A Sample Labels Match COC? ~ 11JYes 0No ON/A -Includes Date/Time/ID/ Analysis Matrix: h 1 /· 5l, All containers needing acid/base preservation have been .cb.e.cked? _________________________ ~'fes---QNo----GJN/A- All containers needing preservation are found to be in compliance with EPA recommendation? (HN03, H2S04, HCl<2; NaOH >9 Sulfide, Na0H>12 Cyanide) Exceptions: VOA, Coliform, TOC, Oil and Grease, DR0/8015 (water) DOC,LLHg Samples checked for dechlorination? Headspace in VOA Vials (>5-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? Pace Trip Blank Lot# (if purchased): CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: ~Yes 0 No ON/A 0 Yes IYINo ON/A l'ilYes 0No ON/A ' Oves l'ilNo ON/A O ves ~No ON/A Oves ~No ON/A including Hawaii and Puerto Rico)? 0 Yes [i!No Comments/Discrepancy: 1. 2. 3. 4. 5. 6. 7. 8. Note if sediment is visible in the dissolved container 9. lQ, HNC3pH<2 ------·----~·--·------··--------·--·-------·-HOpH<2 H2504 pH<2 Na0HpH>12 NaOH/ZnOA< pH>9 11. 12. 13. Field Data Required? O ves 0No Date: 7/zJ Date: __ ___:._7/_1.,-1-7 ___ _ Note: Whenever there Is a discrepancy affecting North Carolina co itance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, Incorrect preservative, out of temp, incorrect containers) Page 29 of 29 ~ Pace AnalyUcal • C H A I N - O F - C U S T O D Y I A n a l y t i c a l R e q u e s t D o c u m e n t T h e C h a i n - o f - C u s t o d y i s a L E G A L D O C U M E N T . A l l r e l e v a n t f i e l d s m u s t b e c o m p l e t e d a c c u r a t e l y . www.pace1aos.com P a g e : o f Section A S e c t i o n B S e c t i o n C Required Client Information: R e q u i r e d P r o j e c t I n f o r m a t i o n : I n v o i c e I n f o r m a t i o n : 2 0 5 6 1 7 9 Company: A5 {; R e p o r t T o : C t J . r y J ) 1 C 7 ] ) , / A t t e n t i o n : C 0 r - v l , l { o c > c l v Address: /S-'--1 13c,c lc\.,,c,t :--~ C o p y T o e . . S . ' ~ j ~ . ~ V ( v U l > - · ' " 1 Z ! ! 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R e f e r e n c e : PhoP://t ,;-le ~c I Fax P r o j e c t N a m e : ( } . 1 l k , • J P a c e P r o j c c l S i t e L o c a t i o n n - V v - ; : · t - , M a n a g e r : ) ) ( _ Requested Due Date/TAT:$"' Jrv (Si6) P r o j e c t N u m b e r : ) ) 1 l l P a c e P r o f i l e # : ' 5 l e S ' S - ' 2 . . . - - S T A T E : R e q u e s t e d A n a l y s i s F i l t e r e d ( Y / N ) - Section O Matrix C o d e s j i i : " z Required Client lnfonnation MATRIX I ~ Q D ~ ; : ! , C O L L E C T E D P r e s e r v a t i v e s > ' 0 0 Drinking Wate r o w i 0 z Waler W T I I 0 0 C O M P O S I T E C O M P O S I T E ; : : Waste Water W W " C a : : , E N O / G R A B 0 z S T A R T w Product p ~ ~ . . . J : , : Soil/Solid S L . , , < . ' . ) 6 C f ) - - . , , I I 0 Q ) SAMPLE ID Oil O L ! ! ! , C l ' . i i i < . ' . ) > - - w c Wipe W P - · ~ w < ( z C l ~ (A-Z. 0-9/ ,-) Air A R 0 w l l . < { " O I - : c Sample IDs MUST BE UNIQUE Tissue T S 0 l l . ; : ! , I - Q ) V > I ~ ~ ~ ( ) 0 ~ w z c : · . ; ; Other O T > - - 0 , t : : ; , . . . r o > < w w 0 Q ) 0 c > , "" a : . . . J . . . J u ( / ) ( ) M " ' ~ c o ~ : : , ::;; l l . l l . L L ~ I 0 : . c Q ) ~ " O I - ; : ! , : : : a . ( / ) 0 - 0 - . c c : · ; ; ; w < ( < ( < ( 0 c N Z ( ) " ' " ' Q ) - < ( ~ Q ) !::: 2 r n D A T E T I M E D A T E T I M E r n " " : : : : > I I I Z z ~ o . . . 0 : : P a c e P r o j e c t N o . / L a b 1 . 0 . 1 .Ill! w-7 v v i b 7 / J , , ? ~ n < ' ~ I L f ~ ~ x 2 !"1 IN ~ I I t ? / 1 « ' ) o v o . ; J h I . / x e u u I f ' 1 ' ) ' 1 , " ' MtA.J·i5 t i v i / J . , f l ~ c - o l 7 ; _ _ ) ~ ' ) ( x x ( 3 4 5 6 7 8 9 10 11 12 ADDITIONAL COMMENTS R E U N Q U t S H E D B Y I A F F I L I A T I O N D A T E T I M E ~ C ~ P T 1 B Y I A F A J t O N F i l l D A T E T I M E S A M P L E C O N D I T I O N S /2Ct2.4 y" tYtl Lf 4-,;r ,,v!W - 1 l / l ~ I - J , v a : " " / A 5 e 7 / ) , ; , 7 ! 1 , l ' i 0 1 ) M ~ a t ~ ~ Q ' l } l O N V \ l f . r f . _ r - , , 0 0 ! C t 1 l i f l . E I V / _ , L / ~ / l l u ; _ 7 k l l c . t ' Y ( 3 7 / . / / ~ ~ ~ h ~ / 0 7 f 7 ~ f ) { h , t _ _ ( Q _ . / H / l - 7 b ? I . / / J { / ' ? 7 - ~ - { y , v Y : · · - ( S A M P L E R N A M E A N D S I G N A T U R E c ' " 1 3 O R I G I N A L p o - , . . a " ' . , , z . , , 0 - E - P R I N T N a m e o f S A M P L E R : j - J / ; ' 6 t ~ M . . - ~ - ~ ~ * ~ ~ " ' z a . " E . ~ E " ' " ' " . , _ 4 - . S - D A T E S i g n e d · 7 / ) c ; / ( ~ " ' u u o . ; ; E S I G N A T U R E o f S A M P L E R : { u . v f w - I - Q ' . " " ' ( M M / D D / Y Y ) : r n r n • 1mpor1an1 Note: By s1gn1ng this form you arc acccp h n g P a c e ' s N E T 3 0 d a y p a y m e n t l c r m s a n d a g r e e i n g 1 0 l a t e c h a r g e s o f 1 . 5 % , p e r m o n 1 h f o r a n y i n \ l o i c c s n o t p a i d w 1 l h 1 n 3 0 d a y s . F - A L L - Q - 0 2 0 r e v . 0 7 . 1 5 - M a y - 2 0 0 7 #=CL# August 02, 2016 LIMS USE: FR - ELLIOT SWAIN LIMS OBJECT ID: 92304618 92304618 Project: Pace Project No.: RE: Elliot SwainAtlantic Shore Environmental154 Backhoe RdLeland, NC 28451 UNIVERSITY FORD 1272C Dear Elliot Swain: Enclosed are the analytical results for sample(s) received by the laboratory on July 11, 2016. The results relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Report revised on 8/2/16 to include MDLs. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell taylor.ezell@pacelabs.com Project Manager Enclosures cc:Cheryl Moody, Atlantic Shore Environmental REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 61 #=CP# CERTIFICATIONS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 61 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Lab ID Sample ID Matrix Date Collected Date Received 92304618001 MW-4 Water 07/11/16 13:30 07/11/16 16:30 92304618002 MW-5 Water 07/11/16 14:15 07/11/16 16:30 92304618003 MW-15 Water 07/11/16 14:30 07/11/16 16:30 92304618004 MW-8 Water 07/11/16 14:00 07/11/16 16:30 92304618005 MW-10 Water 07/11/16 15:30 07/11/16 16:30 92304618006 MW-2 Water 07/11/16 14:30 07/11/16 16:30 92304618007 MW-1 Water 07/11/16 15:10 07/11/16 16:30 92304618008 MW-14 Water 07/11/16 15:35 07/11/16 16:30 92304618009 MW-3 Water 07/11/16 15:40 07/11/16 16:30 92304618010 MW-6 Water 07/11/16 15:35 07/11/16 16:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 61 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92304618001 MW-4 EPA 6010 7 PASI-AJMW EPA 7470 1 PASI-ASER EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92304618002 MW-5 EPA 6010 7 PASI-AJMW EPA 7470 1 PASI-ASER EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92304618003 MW-15 EPA 6010 7 PASI-AJMW EPA 7470 1 PASI-ASER EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92304618004 MW-8 EPA 6010 7 PASI-AJMW EPA 7470 1 PASI-ASER EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92304618005 MW-10 EPA 6010 7 PASI-AJMW EPA 7470 1 PASI-ASER EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92304618006 MW-2 EPA 6010 7 PASI-AJMW EPA 7470 1 PASI-ASER EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92304618007 MW-1 EPA 6010 7 PASI-AJMW EPA 7470 1 PASI-ASER EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92304618008 MW-14 EPA 6010 7 PASI-AJMW EPA 7470 1 PASI-ASER EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92304618009 MW-3 EPA 6010 7 PASI-AJMW EPA 7470 1 PASI-ASER EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB 92304618010 MW-6 EPA 6010 7 PASI-AJMW REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 61 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts EPA 7470 1 PASI-ASER EPA 8270 74 PASI-CBPJ EPA 8260 63 PASI-CNB REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-4 Lab ID: 92304618001 Collected: 07/11/16 13:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/15/16 14:07 7440-38-207/14/16 19:5010.0 5.0 1 Barium 131 ug/L 07/15/16 14:07 7440-39-307/14/16 19:505.0 2.5 1 Cadmium ND ug/L 07/15/16 14:07 7440-43-907/14/16 19:501.0 0.50 1 Chromium ND ug/L 07/15/16 14:07 7440-47-307/14/16 19:505.0 2.5 1 Lead ND ug/L 07/15/16 14:07 7439-92-107/14/16 19:505.0 2.5 1 Selenium ND ug/L 07/15/16 14:07 7782-49-207/14/16 19:5010.0 5.0 1 Silver ND ug/L 07/15/16 14:07 7440-22-407/14/16 19:505.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/16/16 02:52 7439-97-607/15/16 06:350.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/13/16 17:11 83-32-907/12/16 08:0910.0 0.25 1 Acenaphthylene ND ug/L 07/13/16 17:11 208-96-807/12/16 08:0910.0 0.21 1 Aniline ND ug/L 07/13/16 17:11 62-53-307/12/16 08:0910.0 1.3 1 Anthracene ND ug/L 07/13/16 17:11 120-12-707/12/16 08:0910.0 0.14 1 Benzo(a)anthracene ND ug/L 07/13/16 17:11 56-55-307/12/16 08:0910.0 0.33 1 Benzo(a)pyrene ND ug/L 07/13/16 17:11 50-32-807/12/16 08:0910.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/13/16 17:11 205-99-207/12/16 08:0910.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/13/16 17:11 191-24-207/12/16 08:0910.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/13/16 17:11 207-08-907/12/16 08:0910.0 0.43 1 Benzoic Acid ND ug/L 07/13/16 17:11 65-85-007/12/16 08:0950.0 11.1 1 Benzyl alcohol ND ug/L 07/13/16 17:11 100-51-6 L307/12/16 08:0920.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/13/16 17:11 101-55-307/12/16 08:0910.0 1.3 1 Butylbenzylphthalate ND ug/L 07/13/16 17:11 85-68-707/12/16 08:0910.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/13/16 17:11 59-50-7 L307/12/16 08:0920.0 4.2 1 4-Chloroaniline ND ug/L 07/13/16 17:11 106-47-807/12/16 08:0920.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/13/16 17:11 111-91-107/12/16 08:0910.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/13/16 17:11 111-44-407/12/16 08:0910.0 1.5 1 2-Chloronaphthalene ND ug/L 07/13/16 17:11 91-58-707/12/16 08:0910.0 2.2 1 2-Chlorophenol ND ug/L 07/13/16 17:11 95-57-807/12/16 08:0910.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/13/16 17:11 7005-72-307/12/16 08:0910.0 2.1 1 Chrysene ND ug/L 07/13/16 17:11 218-01-907/12/16 08:0910.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/13/16 17:11 53-70-307/12/16 08:0910.0 0.55 1 Dibenzofuran ND ug/L 07/13/16 17:11 132-64-907/12/16 08:0910.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/13/16 17:11 95-50-107/12/16 08:0910.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/13/16 17:11 541-73-107/12/16 08:0910.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/13/16 17:11 106-46-707/12/16 08:0910.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/13/16 17:11 91-94-107/12/16 08:0920.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/13/16 17:11 120-83-207/12/16 08:0910.0 1.7 1 Diethylphthalate ND ug/L 07/13/16 17:11 84-66-207/12/16 08:0910.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/13/16 17:11 105-67-907/12/16 08:0910.0 2.2 1 Dimethylphthalate ND ug/L 07/13/16 17:11 131-11-307/12/16 08:0910.0 1.5 1 Di-n-butylphthalate ND ug/L 07/13/16 17:11 84-74-207/12/16 08:0910.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/13/16 17:11 534-52-107/12/16 08:0920.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/13/16 17:11 51-28-507/12/16 08:0950.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-4 Lab ID: 92304618001 Collected: 07/11/16 13:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/13/16 17:11 121-14-207/12/16 08:0910.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/13/16 17:11 606-20-207/12/16 08:0910.0 1.7 1 Di-n-octylphthalate ND ug/L 07/13/16 17:11 117-84-007/12/16 08:0910.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/13/16 17:11 117-81-707/12/16 08:096.0 0.85 1 Fluoranthene ND ug/L 07/13/16 17:11 206-44-007/12/16 08:0910.0 0.21 1 Fluorene ND ug/L 07/13/16 17:11 86-73-707/12/16 08:0910.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/13/16 17:11 87-68-307/12/16 08:0910.0 1.8 1 Hexachlorobenzene ND ug/L 07/13/16 17:11 118-74-107/12/16 08:0910.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/13/16 17:11 77-47-407/12/16 08:0910.0 1.8 1 Hexachloroethane ND ug/L 07/13/16 17:11 67-72-107/12/16 08:0910.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/13/16 17:11 193-39-507/12/16 08:0910.0 0.29 1 Isophorone ND ug/L 07/13/16 17:11 78-59-107/12/16 08:0910.0 1.8 1 1-Methylnaphthalene ND ug/L 07/13/16 17:11 90-12-007/12/16 08:0910.0 0.32 1 2-Methylnaphthalene ND ug/L 07/13/16 17:11 91-57-607/12/16 08:0910.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/13/16 17:11 95-48-707/12/16 08:0910.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/13/16 17:1107/12/16 08:0910.0 1.7 1 Naphthalene ND ug/L 07/13/16 17:11 91-20-307/12/16 08:0910.0 0.34 1 2-Nitroaniline ND ug/L 07/13/16 17:11 88-74-407/12/16 08:0950.0 2.8 1 3-Nitroaniline ND ug/L 07/13/16 17:11 99-09-207/12/16 08:0950.0 2.4 1 4-Nitroaniline ND ug/L 07/13/16 17:11 100-01-607/12/16 08:0920.0 2.5 1 Nitrobenzene ND ug/L 07/13/16 17:11 98-95-307/12/16 08:0910.0 1.7 1 2-Nitrophenol ND ug/L 07/13/16 17:11 88-75-507/12/16 08:0910.0 1.7 1 4-Nitrophenol ND ug/L 07/13/16 17:11 100-02-707/12/16 08:0950.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/13/16 17:11 62-75-907/12/16 08:0910.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/13/16 17:11 621-64-7 L307/12/16 08:0910.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/13/16 17:11 86-30-607/12/16 08:0910.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/13/16 17:11 108-60-107/12/16 08:0910.0 1.6 1 Pentachlorophenol ND ug/L 07/13/16 17:11 87-86-507/12/16 08:0925.0 2.3 1 Phenanthrene ND ug/L 07/13/16 17:11 85-01-807/12/16 08:0910.0 0.22 1 Phenol ND ug/L 07/13/16 17:1107/12/16 08:0910.0 1.7 1 Pyrene ND ug/L 07/13/16 17:11 129-00-007/12/16 08:0910.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/13/16 17:11 120-82-107/12/16 08:0910.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/13/16 17:11 95-95-407/12/16 08:0910.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/13/16 17:11 88-06-207/12/16 08:0910.0 1.9 1 Surrogates Nitrobenzene-d5 (S)87 %07/13/16 17:11 4165-60-007/12/16 08:0921-110 1 2-Fluorobiphenyl (S)75 %07/13/16 17:11 321-60-807/12/16 08:0927-110 1 Terphenyl-d14 (S)96 %07/13/16 17:11 1718-51-007/12/16 08:0931-107 1 Phenol-d6 (S)39 %07/13/16 17:11 13127-88-307/12/16 08:0910-110 1 2-Fluorophenol (S)51 %07/13/16 17:11 367-12-407/12/16 08:0912-110 1 2,4,6-Tribromophenol (S)95 %07/13/16 17:11 118-79-607/12/16 08:0927-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone ND ug/L 07/14/16 07:06 67-64-125.0 10.0 1 Benzene ND ug/L 07/14/16 07:06 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/14/16 07:06 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-4 Lab ID: 92304618001 Collected: 07/11/16 13:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/14/16 07:06 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/14/16 07:06 75-27-41.0 0.18 1 Bromoform ND ug/L 07/14/16 07:06 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/14/16 07:06 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/14/16 07:06 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/14/16 07:06 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/14/16 07:06 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/14/16 07:06 75-00-31.0 0.54 1 Chloroform ND ug/L 07/14/16 07:06 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/14/16 07:06 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/14/16 07:06 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/14/16 07:06 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 07:06 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/14/16 07:06 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/14/16 07:06 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/14/16 07:06 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/14/16 07:06 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/14/16 07:06 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/14/16 07:06 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/14/16 07:06 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/14/16 07:06 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/14/16 07:06 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/14/16 07:06 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/14/16 07:06 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/14/16 07:06 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/14/16 07:06 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/14/16 07:06 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/14/16 07:06 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/14/16 07:06 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/14/16 07:06 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/14/16 07:06 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/14/16 07:06 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/14/16 07:06 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/14/16 07:06 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/14/16 07:06 591-78-65.0 0.46 1 p-Isopropyltoluene ND ug/L 07/14/16 07:06 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/14/16 07:06 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 07:06 108-10-15.0 0.33 1 Methyl-tert-butyl ether ND ug/L 07/14/16 07:06 1634-04-41.0 0.21 1 Naphthalene ND ug/L 07/14/16 07:06 91-20-31.0 0.24 1 Styrene ND ug/L 07/14/16 07:06 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 07:06 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 07:06 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/14/16 07:06 127-18-41.0 0.46 1 Toluene ND ug/L 07/14/16 07:06 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/14/16 07:06 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-4 Lab ID: 92304618001 Collected: 07/11/16 13:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/14/16 07:06 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/14/16 07:06 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/14/16 07:06 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/14/16 07:06 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/14/16 07:06 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/14/16 07:06 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/14/16 07:06 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/14/16 07:06 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/14/16 07:06 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/14/16 07:06 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/14/16 07:06 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)99 %07/14/16 07:06 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/14/16 07:06 17060-07-070-130 1 Toluene-d8 (S)99 %07/14/16 07:06 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-5 Lab ID: 92304618002 Collected: 07/11/16 14:15 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/15/16 14:25 7440-38-207/14/16 19:5010.0 5.0 1 Barium 337 ug/L 07/15/16 14:25 7440-39-307/14/16 19:505.0 2.5 1 Cadmium ND ug/L 07/15/16 14:25 7440-43-907/14/16 19:501.0 0.50 1 Chromium 3.2J ug/L 07/15/16 14:25 7440-47-307/14/16 19:505.0 2.5 1 Lead 4.1J ug/L 07/15/16 14:25 7439-92-107/14/16 19:505.0 2.5 1 Selenium ND ug/L 07/15/16 14:25 7782-49-207/14/16 19:5010.0 5.0 1 Silver ND ug/L 07/15/16 14:25 7440-22-407/14/16 19:505.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/16/16 02:59 7439-97-607/15/16 06:350.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene 1.8J ug/L 07/13/16 17:46 83-32-907/12/16 08:0910.0 0.25 1 Acenaphthylene ND ug/L 07/13/16 17:46 208-96-807/12/16 08:0910.0 0.21 1 Aniline ND ug/L 07/13/16 17:46 62-53-307/12/16 08:0910.0 1.3 1 Anthracene ND ug/L 07/13/16 17:46 120-12-707/12/16 08:0910.0 0.14 1 Benzo(a)anthracene ND ug/L 07/13/16 17:46 56-55-307/12/16 08:0910.0 0.33 1 Benzo(a)pyrene ND ug/L 07/13/16 17:46 50-32-807/12/16 08:0910.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/13/16 17:46 205-99-207/12/16 08:0910.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/13/16 17:46 191-24-207/12/16 08:0910.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/13/16 17:46 207-08-907/12/16 08:0910.0 0.43 1 Benzoic Acid ND ug/L 07/13/16 17:46 65-85-007/12/16 08:0950.0 11.1 1 Benzyl alcohol ND ug/L 07/13/16 17:46 100-51-6 L307/12/16 08:0920.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/13/16 17:46 101-55-307/12/16 08:0910.0 1.3 1 Butylbenzylphthalate ND ug/L 07/13/16 17:46 85-68-707/12/16 08:0910.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/13/16 17:46 59-50-7 L307/12/16 08:0920.0 4.2 1 4-Chloroaniline ND ug/L 07/13/16 17:46 106-47-807/12/16 08:0920.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/13/16 17:46 111-91-107/12/16 08:0910.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/13/16 17:46 111-44-407/12/16 08:0910.0 1.5 1 2-Chloronaphthalene ND ug/L 07/13/16 17:46 91-58-707/12/16 08:0910.0 2.2 1 2-Chlorophenol ND ug/L 07/13/16 17:46 95-57-807/12/16 08:0910.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/13/16 17:46 7005-72-307/12/16 08:0910.0 2.1 1 Chrysene ND ug/L 07/13/16 17:46 218-01-907/12/16 08:0910.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/13/16 17:46 53-70-307/12/16 08:0910.0 0.55 1 Dibenzofuran ND ug/L 07/13/16 17:46 132-64-907/12/16 08:0910.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/13/16 17:46 95-50-107/12/16 08:0910.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/13/16 17:46 541-73-107/12/16 08:0910.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/13/16 17:46 106-46-707/12/16 08:0910.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/13/16 17:46 91-94-107/12/16 08:0920.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/13/16 17:46 120-83-207/12/16 08:0910.0 1.7 1 Diethylphthalate ND ug/L 07/13/16 17:46 84-66-207/12/16 08:0910.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/13/16 17:46 105-67-907/12/16 08:0910.0 2.2 1 Dimethylphthalate ND ug/L 07/13/16 17:46 131-11-307/12/16 08:0910.0 1.5 1 Di-n-butylphthalate ND ug/L 07/13/16 17:46 84-74-207/12/16 08:0910.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/13/16 17:46 534-52-107/12/16 08:0920.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/13/16 17:46 51-28-507/12/16 08:0950.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-5 Lab ID: 92304618002 Collected: 07/11/16 14:15 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/13/16 17:46 121-14-207/12/16 08:0910.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/13/16 17:46 606-20-207/12/16 08:0910.0 1.7 1 Di-n-octylphthalate ND ug/L 07/13/16 17:46 117-84-007/12/16 08:0910.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/13/16 17:46 117-81-707/12/16 08:096.0 0.85 1 Fluoranthene ND ug/L 07/13/16 17:46 206-44-007/12/16 08:0910.0 0.21 1 Fluorene ND ug/L 07/13/16 17:46 86-73-707/12/16 08:0910.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/13/16 17:46 87-68-307/12/16 08:0910.0 1.8 1 Hexachlorobenzene ND ug/L 07/13/16 17:46 118-74-107/12/16 08:0910.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/13/16 17:46 77-47-407/12/16 08:0910.0 1.8 1 Hexachloroethane ND ug/L 07/13/16 17:46 67-72-107/12/16 08:0910.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/13/16 17:46 193-39-507/12/16 08:0910.0 0.29 1 Isophorone ND ug/L 07/13/16 17:46 78-59-107/12/16 08:0910.0 1.8 1 1-Methylnaphthalene ND ug/L 07/13/16 17:46 90-12-007/12/16 08:0910.0 0.32 1 2-Methylnaphthalene ND ug/L 07/13/16 17:46 91-57-607/12/16 08:0910.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/13/16 17:46 95-48-707/12/16 08:0910.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/13/16 17:4607/12/16 08:0910.0 1.7 1 Naphthalene ND ug/L 07/13/16 17:46 91-20-307/12/16 08:0910.0 0.34 1 2-Nitroaniline ND ug/L 07/13/16 17:46 88-74-407/12/16 08:0950.0 2.8 1 3-Nitroaniline ND ug/L 07/13/16 17:46 99-09-207/12/16 08:0950.0 2.4 1 4-Nitroaniline ND ug/L 07/13/16 17:46 100-01-607/12/16 08:0920.0 2.5 1 Nitrobenzene ND ug/L 07/13/16 17:46 98-95-307/12/16 08:0910.0 1.7 1 2-Nitrophenol ND ug/L 07/13/16 17:46 88-75-507/12/16 08:0910.0 1.7 1 4-Nitrophenol ND ug/L 07/13/16 17:46 100-02-707/12/16 08:0950.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/13/16 17:46 62-75-907/12/16 08:0910.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/13/16 17:46 621-64-7 L307/12/16 08:0910.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/13/16 17:46 86-30-607/12/16 08:0910.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/13/16 17:46 108-60-107/12/16 08:0910.0 1.6 1 Pentachlorophenol ND ug/L 07/13/16 17:46 87-86-507/12/16 08:0925.0 2.3 1 Phenanthrene 1.1J ug/L 07/13/16 17:46 85-01-807/12/16 08:0910.0 0.22 1 Phenol ND ug/L 07/13/16 17:4607/12/16 08:0910.0 1.7 1 Pyrene ND ug/L 07/13/16 17:46 129-00-007/12/16 08:0910.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/13/16 17:46 120-82-107/12/16 08:0910.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/13/16 17:46 95-95-407/12/16 08:0910.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/13/16 17:46 88-06-207/12/16 08:0910.0 1.9 1 Surrogates Nitrobenzene-d5 (S)86 %07/13/16 17:46 4165-60-007/12/16 08:0921-110 1 2-Fluorobiphenyl (S)75 %07/13/16 17:46 321-60-807/12/16 08:0927-110 1 Terphenyl-d14 (S)72 %07/13/16 17:46 1718-51-007/12/16 08:0931-107 1 Phenol-d6 (S)36 %07/13/16 17:46 13127-88-307/12/16 08:0910-110 1 2-Fluorophenol (S)50 %07/13/16 17:46 367-12-407/12/16 08:0912-110 1 2,4,6-Tribromophenol (S)90 %07/13/16 17:46 118-79-607/12/16 08:0927-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone 27.1 ug/L 07/14/16 07:24 67-64-125.0 10.0 1 Benzene ND ug/L 07/14/16 07:24 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/14/16 07:24 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-5 Lab ID: 92304618002 Collected: 07/11/16 14:15 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/14/16 07:24 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/14/16 07:24 75-27-41.0 0.18 1 Bromoform ND ug/L 07/14/16 07:24 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/14/16 07:24 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/14/16 07:24 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/14/16 07:24 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/14/16 07:24 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/14/16 07:24 75-00-31.0 0.54 1 Chloroform ND ug/L 07/14/16 07:24 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/14/16 07:24 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/14/16 07:24 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/14/16 07:24 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 07:24 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/14/16 07:24 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/14/16 07:24 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/14/16 07:24 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/14/16 07:24 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/14/16 07:24 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/14/16 07:24 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/14/16 07:24 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/14/16 07:24 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/14/16 07:24 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/14/16 07:24 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/14/16 07:24 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/14/16 07:24 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/14/16 07:24 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/14/16 07:24 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/14/16 07:24 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/14/16 07:24 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/14/16 07:24 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/14/16 07:24 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/14/16 07:24 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/14/16 07:24 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/14/16 07:24 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/14/16 07:24 591-78-65.0 0.46 1 p-Isopropyltoluene 10.3 ug/L 07/14/16 07:24 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/14/16 07:24 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 07:24 108-10-15.0 0.33 1 Methyl-tert-butyl ether ND ug/L 07/14/16 07:24 1634-04-41.0 0.21 1 Naphthalene 0.70J ug/L 07/14/16 07:24 91-20-31.0 0.24 1 Styrene ND ug/L 07/14/16 07:24 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 07:24 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 07:24 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/14/16 07:24 127-18-41.0 0.46 1 Toluene ND ug/L 07/14/16 07:24 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/14/16 07:24 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-5 Lab ID: 92304618002 Collected: 07/11/16 14:15 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/14/16 07:24 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/14/16 07:24 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/14/16 07:24 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/14/16 07:24 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/14/16 07:24 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/14/16 07:24 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/14/16 07:24 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/14/16 07:24 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/14/16 07:24 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/14/16 07:24 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/14/16 07:24 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)99 %07/14/16 07:24 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/14/16 07:24 17060-07-070-130 1 Toluene-d8 (S)100 %07/14/16 07:24 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-15 Lab ID: 92304618003 Collected: 07/11/16 14:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/15/16 14:29 7440-38-207/14/16 19:5010.0 5.0 1 Barium 189 ug/L 07/15/16 14:29 7440-39-307/14/16 19:505.0 2.5 1 Cadmium ND ug/L 07/15/16 14:29 7440-43-907/14/16 19:501.0 0.50 1 Chromium 15.4 ug/L 07/15/16 14:29 7440-47-307/14/16 19:505.0 2.5 1 Lead 14.7 ug/L 07/15/16 14:29 7439-92-107/14/16 19:505.0 2.5 1 Selenium ND ug/L 07/15/16 14:29 7782-49-207/14/16 19:5010.0 5.0 1 Silver ND ug/L 07/15/16 14:29 7440-22-407/14/16 19:505.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/16/16 03:01 7439-97-607/15/16 06:350.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/13/16 18:20 83-32-907/12/16 08:0910.0 0.25 1 Acenaphthylene ND ug/L 07/13/16 18:20 208-96-807/12/16 08:0910.0 0.21 1 Aniline ND ug/L 07/13/16 18:20 62-53-307/12/16 08:0910.0 1.3 1 Anthracene ND ug/L 07/13/16 18:20 120-12-707/12/16 08:0910.0 0.14 1 Benzo(a)anthracene ND ug/L 07/13/16 18:20 56-55-307/12/16 08:0910.0 0.33 1 Benzo(a)pyrene ND ug/L 07/13/16 18:20 50-32-807/12/16 08:0910.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/13/16 18:20 205-99-207/12/16 08:0910.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/13/16 18:20 191-24-207/12/16 08:0910.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/13/16 18:20 207-08-907/12/16 08:0910.0 0.43 1 Benzoic Acid ND ug/L 07/13/16 18:20 65-85-007/12/16 08:0950.0 11.1 1 Benzyl alcohol ND ug/L 07/13/16 18:20 100-51-6 L307/12/16 08:0920.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/13/16 18:20 101-55-307/12/16 08:0910.0 1.3 1 Butylbenzylphthalate ND ug/L 07/13/16 18:20 85-68-707/12/16 08:0910.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/13/16 18:20 59-50-7 L307/12/16 08:0920.0 4.2 1 4-Chloroaniline ND ug/L 07/13/16 18:20 106-47-807/12/16 08:0920.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/13/16 18:20 111-91-107/12/16 08:0910.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/13/16 18:20 111-44-407/12/16 08:0910.0 1.5 1 2-Chloronaphthalene ND ug/L 07/13/16 18:20 91-58-707/12/16 08:0910.0 2.2 1 2-Chlorophenol ND ug/L 07/13/16 18:20 95-57-807/12/16 08:0910.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/13/16 18:20 7005-72-307/12/16 08:0910.0 2.1 1 Chrysene ND ug/L 07/13/16 18:20 218-01-907/12/16 08:0910.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/13/16 18:20 53-70-307/12/16 08:0910.0 0.55 1 Dibenzofuran ND ug/L 07/13/16 18:20 132-64-907/12/16 08:0910.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/13/16 18:20 95-50-107/12/16 08:0910.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/13/16 18:20 541-73-107/12/16 08:0910.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/13/16 18:20 106-46-707/12/16 08:0910.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/13/16 18:20 91-94-107/12/16 08:0920.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/13/16 18:20 120-83-207/12/16 08:0910.0 1.7 1 Diethylphthalate ND ug/L 07/13/16 18:20 84-66-207/12/16 08:0910.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/13/16 18:20 105-67-907/12/16 08:0910.0 2.2 1 Dimethylphthalate ND ug/L 07/13/16 18:20 131-11-307/12/16 08:0910.0 1.5 1 Di-n-butylphthalate ND ug/L 07/13/16 18:20 84-74-207/12/16 08:0910.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/13/16 18:20 534-52-107/12/16 08:0920.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/13/16 18:20 51-28-507/12/16 08:0950.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-15 Lab ID: 92304618003 Collected: 07/11/16 14:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/13/16 18:20 121-14-207/12/16 08:0910.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/13/16 18:20 606-20-207/12/16 08:0910.0 1.7 1 Di-n-octylphthalate ND ug/L 07/13/16 18:20 117-84-007/12/16 08:0910.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/13/16 18:20 117-81-707/12/16 08:096.0 0.85 1 Fluoranthene ND ug/L 07/13/16 18:20 206-44-007/12/16 08:0910.0 0.21 1 Fluorene ND ug/L 07/13/16 18:20 86-73-707/12/16 08:0910.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/13/16 18:20 87-68-307/12/16 08:0910.0 1.8 1 Hexachlorobenzene ND ug/L 07/13/16 18:20 118-74-107/12/16 08:0910.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/13/16 18:20 77-47-407/12/16 08:0910.0 1.8 1 Hexachloroethane ND ug/L 07/13/16 18:20 67-72-107/12/16 08:0910.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/13/16 18:20 193-39-507/12/16 08:0910.0 0.29 1 Isophorone ND ug/L 07/13/16 18:20 78-59-107/12/16 08:0910.0 1.8 1 1-Methylnaphthalene 10.1 ug/L 07/13/16 18:20 90-12-007/12/16 08:0910.0 0.32 1 2-Methylnaphthalene 2.9J ug/L 07/13/16 18:20 91-57-607/12/16 08:0910.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/13/16 18:20 95-48-707/12/16 08:0910.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/13/16 18:2007/12/16 08:0910.0 1.7 1 Naphthalene 2.4J ug/L 07/13/16 18:20 91-20-307/12/16 08:0910.0 0.34 1 2-Nitroaniline ND ug/L 07/13/16 18:20 88-74-407/12/16 08:0950.0 2.8 1 3-Nitroaniline ND ug/L 07/13/16 18:20 99-09-207/12/16 08:0950.0 2.4 1 4-Nitroaniline ND ug/L 07/13/16 18:20 100-01-607/12/16 08:0920.0 2.5 1 Nitrobenzene ND ug/L 07/13/16 18:20 98-95-307/12/16 08:0910.0 1.7 1 2-Nitrophenol ND ug/L 07/13/16 18:20 88-75-507/12/16 08:0910.0 1.7 1 4-Nitrophenol ND ug/L 07/13/16 18:20 100-02-707/12/16 08:0950.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/13/16 18:20 62-75-907/12/16 08:0910.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/13/16 18:20 621-64-7 L307/12/16 08:0910.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/13/16 18:20 86-30-607/12/16 08:0910.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/13/16 18:20 108-60-107/12/16 08:0910.0 1.6 1 Pentachlorophenol ND ug/L 07/13/16 18:20 87-86-507/12/16 08:0925.0 2.3 1 Phenanthrene ND ug/L 07/13/16 18:20 85-01-807/12/16 08:0910.0 0.22 1 Phenol ND ug/L 07/13/16 18:2007/12/16 08:0910.0 1.7 1 Pyrene ND ug/L 07/13/16 18:20 129-00-007/12/16 08:0910.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/13/16 18:20 120-82-107/12/16 08:0910.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/13/16 18:20 95-95-407/12/16 08:0910.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/13/16 18:20 88-06-207/12/16 08:0910.0 1.9 1 Surrogates Nitrobenzene-d5 (S)84 %07/13/16 18:20 4165-60-007/12/16 08:0921-110 1 2-Fluorobiphenyl (S)74 %07/13/16 18:20 321-60-807/12/16 08:0927-110 1 Terphenyl-d14 (S)73 %07/13/16 18:20 1718-51-007/12/16 08:0931-107 1 Phenol-d6 (S)35 %07/13/16 18:20 13127-88-307/12/16 08:0910-110 1 2-Fluorophenol (S)47 %07/13/16 18:20 367-12-407/12/16 08:0912-110 1 2,4,6-Tribromophenol (S)98 %07/13/16 18:20 118-79-607/12/16 08:0927-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone ND ug/L 07/14/16 07:58 67-64-125.0 10.0 1 Benzene ND ug/L 07/14/16 07:58 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/14/16 07:58 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-15 Lab ID: 92304618003 Collected: 07/11/16 14:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/14/16 07:58 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/14/16 07:58 75-27-41.0 0.18 1 Bromoform ND ug/L 07/14/16 07:58 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/14/16 07:58 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/14/16 07:58 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/14/16 07:58 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/14/16 07:58 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/14/16 07:58 75-00-31.0 0.54 1 Chloroform ND ug/L 07/14/16 07:58 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/14/16 07:58 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/14/16 07:58 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/14/16 07:58 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 07:58 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/14/16 07:58 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/14/16 07:58 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/14/16 07:58 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/14/16 07:58 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/14/16 07:58 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/14/16 07:58 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/14/16 07:58 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/14/16 07:58 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/14/16 07:58 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/14/16 07:58 75-35-41.0 0.56 1 cis-1,2-Dichloroethene 2.6 ug/L 07/14/16 07:58 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/14/16 07:58 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/14/16 07:58 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/14/16 07:58 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/14/16 07:58 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/14/16 07:58 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/14/16 07:58 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/14/16 07:58 10061-02-61.0 0.26 1 Diisopropyl ether 0.21J ug/L 07/14/16 07:58 108-20-31.0 0.12 1 Ethylbenzene 0.34J ug/L 07/14/16 07:58 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/14/16 07:58 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/14/16 07:58 591-78-65.0 0.46 1 p-Isopropyltoluene 1.5 ug/L 07/14/16 07:58 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/14/16 07:58 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)1.8J ug/L 07/14/16 07:58 108-10-15.0 0.33 1 Methyl-tert-butyl ether 0.47J ug/L 07/14/16 07:58 1634-04-41.0 0.21 1 Naphthalene 7.1 ug/L 07/14/16 07:58 91-20-31.0 0.24 1 Styrene ND ug/L 07/14/16 07:58 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 07:58 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 07:58 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/14/16 07:58 127-18-41.0 0.46 1 Toluene ND ug/L 07/14/16 07:58 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/14/16 07:58 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-15 Lab ID: 92304618003 Collected: 07/11/16 14:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/14/16 07:58 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/14/16 07:58 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/14/16 07:58 79-00-51.0 0.29 1 Trichloroethene 1.6 ug/L 07/14/16 07:58 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/14/16 07:58 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/14/16 07:58 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/14/16 07:58 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/14/16 07:58 75-01-41.0 0.62 1 Xylene (Total)3.0 ug/L 07/14/16 07:58 1330-20-71.0 0.66 1 m&p-Xylene 1.1J ug/L 07/14/16 07:58 179601-23-12.0 0.66 1 o-Xylene 3.0 ug/L 07/14/16 07:58 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)101 %07/14/16 07:58 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/14/16 07:58 17060-07-070-130 1 Toluene-d8 (S)101 %07/14/16 07:58 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-8 Lab ID: 92304618004 Collected: 07/11/16 14:00 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/15/16 14:33 7440-38-207/14/16 19:5010.0 5.0 1 Barium 83.9 ug/L 07/15/16 14:33 7440-39-307/14/16 19:505.0 2.5 1 Cadmium ND ug/L 07/15/16 14:33 7440-43-907/14/16 19:501.0 0.50 1 Chromium ND ug/L 07/15/16 14:33 7440-47-307/14/16 19:505.0 2.5 1 Lead ND ug/L 07/15/16 14:33 7439-92-107/14/16 19:505.0 2.5 1 Selenium ND ug/L 07/15/16 14:33 7782-49-207/14/16 19:5010.0 5.0 1 Silver ND ug/L 07/15/16 14:33 7440-22-407/14/16 19:505.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/16/16 03:04 7439-97-607/15/16 06:350.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/13/16 18:54 83-32-907/12/16 08:0910.0 0.25 1 Acenaphthylene ND ug/L 07/13/16 18:54 208-96-807/12/16 08:0910.0 0.21 1 Aniline ND ug/L 07/13/16 18:54 62-53-307/12/16 08:0910.0 1.3 1 Anthracene ND ug/L 07/13/16 18:54 120-12-707/12/16 08:0910.0 0.14 1 Benzo(a)anthracene ND ug/L 07/13/16 18:54 56-55-307/12/16 08:0910.0 0.33 1 Benzo(a)pyrene ND ug/L 07/13/16 18:54 50-32-807/12/16 08:0910.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/13/16 18:54 205-99-207/12/16 08:0910.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/13/16 18:54 191-24-207/12/16 08:0910.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/13/16 18:54 207-08-907/12/16 08:0910.0 0.43 1 Benzoic Acid ND ug/L 07/13/16 18:54 65-85-007/12/16 08:0950.0 11.1 1 Benzyl alcohol ND ug/L 07/13/16 18:54 100-51-6 L307/12/16 08:0920.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/13/16 18:54 101-55-307/12/16 08:0910.0 1.3 1 Butylbenzylphthalate ND ug/L 07/13/16 18:54 85-68-707/12/16 08:0910.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/13/16 18:54 59-50-7 L307/12/16 08:0920.0 4.2 1 4-Chloroaniline ND ug/L 07/13/16 18:54 106-47-807/12/16 08:0920.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/13/16 18:54 111-91-107/12/16 08:0910.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/13/16 18:54 111-44-407/12/16 08:0910.0 1.5 1 2-Chloronaphthalene ND ug/L 07/13/16 18:54 91-58-707/12/16 08:0910.0 2.2 1 2-Chlorophenol ND ug/L 07/13/16 18:54 95-57-807/12/16 08:0910.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/13/16 18:54 7005-72-307/12/16 08:0910.0 2.1 1 Chrysene ND ug/L 07/13/16 18:54 218-01-907/12/16 08:0910.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/13/16 18:54 53-70-307/12/16 08:0910.0 0.55 1 Dibenzofuran ND ug/L 07/13/16 18:54 132-64-907/12/16 08:0910.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/13/16 18:54 95-50-107/12/16 08:0910.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/13/16 18:54 541-73-107/12/16 08:0910.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/13/16 18:54 106-46-707/12/16 08:0910.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/13/16 18:54 91-94-107/12/16 08:0920.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/13/16 18:54 120-83-207/12/16 08:0910.0 1.7 1 Diethylphthalate ND ug/L 07/13/16 18:54 84-66-207/12/16 08:0910.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/13/16 18:54 105-67-907/12/16 08:0910.0 2.2 1 Dimethylphthalate ND ug/L 07/13/16 18:54 131-11-307/12/16 08:0910.0 1.5 1 Di-n-butylphthalate ND ug/L 07/13/16 18:54 84-74-207/12/16 08:0910.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/13/16 18:54 534-52-107/12/16 08:0920.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/13/16 18:54 51-28-507/12/16 08:0950.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-8 Lab ID: 92304618004 Collected: 07/11/16 14:00 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/13/16 18:54 121-14-207/12/16 08:0910.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/13/16 18:54 606-20-207/12/16 08:0910.0 1.7 1 Di-n-octylphthalate ND ug/L 07/13/16 18:54 117-84-007/12/16 08:0910.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/13/16 18:54 117-81-707/12/16 08:096.0 0.85 1 Fluoranthene ND ug/L 07/13/16 18:54 206-44-007/12/16 08:0910.0 0.21 1 Fluorene ND ug/L 07/13/16 18:54 86-73-707/12/16 08:0910.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/13/16 18:54 87-68-307/12/16 08:0910.0 1.8 1 Hexachlorobenzene ND ug/L 07/13/16 18:54 118-74-107/12/16 08:0910.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/13/16 18:54 77-47-407/12/16 08:0910.0 1.8 1 Hexachloroethane ND ug/L 07/13/16 18:54 67-72-107/12/16 08:0910.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/13/16 18:54 193-39-507/12/16 08:0910.0 0.29 1 Isophorone ND ug/L 07/13/16 18:54 78-59-107/12/16 08:0910.0 1.8 1 1-Methylnaphthalene ND ug/L 07/13/16 18:54 90-12-007/12/16 08:0910.0 0.32 1 2-Methylnaphthalene ND ug/L 07/13/16 18:54 91-57-607/12/16 08:0910.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/13/16 18:54 95-48-707/12/16 08:0910.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/13/16 18:5407/12/16 08:0910.0 1.7 1 Naphthalene ND ug/L 07/13/16 18:54 91-20-307/12/16 08:0910.0 0.34 1 2-Nitroaniline ND ug/L 07/13/16 18:54 88-74-407/12/16 08:0950.0 2.8 1 3-Nitroaniline ND ug/L 07/13/16 18:54 99-09-207/12/16 08:0950.0 2.4 1 4-Nitroaniline ND ug/L 07/13/16 18:54 100-01-607/12/16 08:0920.0 2.5 1 Nitrobenzene ND ug/L 07/13/16 18:54 98-95-307/12/16 08:0910.0 1.7 1 2-Nitrophenol ND ug/L 07/13/16 18:54 88-75-507/12/16 08:0910.0 1.7 1 4-Nitrophenol ND ug/L 07/13/16 18:54 100-02-707/12/16 08:0950.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/13/16 18:54 62-75-907/12/16 08:0910.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/13/16 18:54 621-64-7 L307/12/16 08:0910.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/13/16 18:54 86-30-607/12/16 08:0910.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/13/16 18:54 108-60-107/12/16 08:0910.0 1.6 1 Pentachlorophenol ND ug/L 07/13/16 18:54 87-86-507/12/16 08:0925.0 2.3 1 Phenanthrene ND ug/L 07/13/16 18:54 85-01-807/12/16 08:0910.0 0.22 1 Phenol ND ug/L 07/13/16 18:5407/12/16 08:0910.0 1.7 1 Pyrene ND ug/L 07/13/16 18:54 129-00-007/12/16 08:0910.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/13/16 18:54 120-82-107/12/16 08:0910.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/13/16 18:54 95-95-407/12/16 08:0910.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/13/16 18:54 88-06-207/12/16 08:0910.0 1.9 1 Surrogates Nitrobenzene-d5 (S)88 %07/13/16 18:54 4165-60-007/12/16 08:0921-110 1 2-Fluorobiphenyl (S)79 %07/13/16 18:54 321-60-807/12/16 08:0927-110 1 Terphenyl-d14 (S)73 %07/13/16 18:54 1718-51-007/12/16 08:0931-107 1 Phenol-d6 (S)36 %07/13/16 18:54 13127-88-307/12/16 08:0910-110 1 2-Fluorophenol (S)48 %07/13/16 18:54 367-12-407/12/16 08:0912-110 1 2,4,6-Tribromophenol (S)95 %07/13/16 18:54 118-79-607/12/16 08:0927-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone ND ug/L 07/14/16 08:15 67-64-125.0 10.0 1 Benzene ND ug/L 07/14/16 08:15 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/14/16 08:15 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-8 Lab ID: 92304618004 Collected: 07/11/16 14:00 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/14/16 08:15 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/14/16 08:15 75-27-41.0 0.18 1 Bromoform ND ug/L 07/14/16 08:15 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/14/16 08:15 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/14/16 08:15 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/14/16 08:15 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/14/16 08:15 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/14/16 08:15 75-00-31.0 0.54 1 Chloroform ND ug/L 07/14/16 08:15 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/14/16 08:15 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/14/16 08:15 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/14/16 08:15 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 08:15 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/14/16 08:15 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/14/16 08:15 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/14/16 08:15 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/14/16 08:15 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/14/16 08:15 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/14/16 08:15 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/14/16 08:15 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/14/16 08:15 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/14/16 08:15 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/14/16 08:15 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/14/16 08:15 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/14/16 08:15 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/14/16 08:15 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/14/16 08:15 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/14/16 08:15 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/14/16 08:15 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/14/16 08:15 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/14/16 08:15 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/14/16 08:15 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/14/16 08:15 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/14/16 08:15 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/14/16 08:15 591-78-65.0 0.46 1 p-Isopropyltoluene ND ug/L 07/14/16 08:15 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/14/16 08:15 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)0.86J ug/L 07/14/16 08:15 108-10-15.0 0.33 1 Methyl-tert-butyl ether 5.8 ug/L 07/14/16 08:15 1634-04-41.0 0.21 1 Naphthalene ND ug/L 07/14/16 08:15 91-20-31.0 0.24 1 Styrene ND ug/L 07/14/16 08:15 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 08:15 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 08:15 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/14/16 08:15 127-18-41.0 0.46 1 Toluene ND ug/L 07/14/16 08:15 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/14/16 08:15 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-8 Lab ID: 92304618004 Collected: 07/11/16 14:00 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/14/16 08:15 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/14/16 08:15 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/14/16 08:15 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/14/16 08:15 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/14/16 08:15 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/14/16 08:15 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/14/16 08:15 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/14/16 08:15 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/14/16 08:15 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/14/16 08:15 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/14/16 08:15 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)98 %07/14/16 08:15 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/14/16 08:15 17060-07-070-130 1 Toluene-d8 (S)99 %07/14/16 08:15 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-10 Lab ID: 92304618005 Collected: 07/11/16 15:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/15/16 14:37 7440-38-207/14/16 19:5010.0 5.0 1 Barium 182 ug/L 07/15/16 14:37 7440-39-307/14/16 19:505.0 2.5 1 Cadmium ND ug/L 07/15/16 14:37 7440-43-907/14/16 19:501.0 0.50 1 Chromium 9.1 ug/L 07/15/16 14:37 7440-47-307/14/16 19:505.0 2.5 1 Lead 3.4J ug/L 07/15/16 14:37 7439-92-107/14/16 19:505.0 2.5 1 Selenium ND ug/L 07/15/16 14:37 7782-49-207/14/16 19:5010.0 5.0 1 Silver ND ug/L 07/15/16 14:37 7440-22-407/14/16 19:505.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/16/16 03:09 7439-97-607/15/16 06:350.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/13/16 19:28 83-32-907/12/16 08:0910.0 0.25 1 Acenaphthylene ND ug/L 07/13/16 19:28 208-96-807/12/16 08:0910.0 0.21 1 Aniline ND ug/L 07/13/16 19:28 62-53-307/12/16 08:0910.0 1.3 1 Anthracene ND ug/L 07/13/16 19:28 120-12-707/12/16 08:0910.0 0.14 1 Benzo(a)anthracene ND ug/L 07/13/16 19:28 56-55-307/12/16 08:0910.0 0.33 1 Benzo(a)pyrene ND ug/L 07/13/16 19:28 50-32-807/12/16 08:0910.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/13/16 19:28 205-99-207/12/16 08:0910.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/13/16 19:28 191-24-207/12/16 08:0910.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/13/16 19:28 207-08-907/12/16 08:0910.0 0.43 1 Benzoic Acid ND ug/L 07/13/16 19:28 65-85-007/12/16 08:0950.0 11.1 1 Benzyl alcohol ND ug/L 07/13/16 19:28 100-51-6 L307/12/16 08:0920.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/13/16 19:28 101-55-307/12/16 08:0910.0 1.3 1 Butylbenzylphthalate ND ug/L 07/13/16 19:28 85-68-707/12/16 08:0910.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/13/16 19:28 59-50-7 L307/12/16 08:0920.0 4.2 1 4-Chloroaniline ND ug/L 07/13/16 19:28 106-47-807/12/16 08:0920.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/13/16 19:28 111-91-107/12/16 08:0910.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/13/16 19:28 111-44-407/12/16 08:0910.0 1.5 1 2-Chloronaphthalene ND ug/L 07/13/16 19:28 91-58-707/12/16 08:0910.0 2.2 1 2-Chlorophenol ND ug/L 07/13/16 19:28 95-57-807/12/16 08:0910.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/13/16 19:28 7005-72-307/12/16 08:0910.0 2.1 1 Chrysene ND ug/L 07/13/16 19:28 218-01-907/12/16 08:0910.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/13/16 19:28 53-70-307/12/16 08:0910.0 0.55 1 Dibenzofuran ND ug/L 07/13/16 19:28 132-64-907/12/16 08:0910.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/13/16 19:28 95-50-107/12/16 08:0910.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/13/16 19:28 541-73-107/12/16 08:0910.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/13/16 19:28 106-46-707/12/16 08:0910.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/13/16 19:28 91-94-107/12/16 08:0920.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/13/16 19:28 120-83-207/12/16 08:0910.0 1.7 1 Diethylphthalate ND ug/L 07/13/16 19:28 84-66-207/12/16 08:0910.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/13/16 19:28 105-67-907/12/16 08:0910.0 2.2 1 Dimethylphthalate ND ug/L 07/13/16 19:28 131-11-307/12/16 08:0910.0 1.5 1 Di-n-butylphthalate ND ug/L 07/13/16 19:28 84-74-207/12/16 08:0910.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/13/16 19:28 534-52-107/12/16 08:0920.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/13/16 19:28 51-28-507/12/16 08:0950.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-10 Lab ID: 92304618005 Collected: 07/11/16 15:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/13/16 19:28 121-14-207/12/16 08:0910.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/13/16 19:28 606-20-207/12/16 08:0910.0 1.7 1 Di-n-octylphthalate ND ug/L 07/13/16 19:28 117-84-007/12/16 08:0910.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/13/16 19:28 117-81-707/12/16 08:096.0 0.85 1 Fluoranthene ND ug/L 07/13/16 19:28 206-44-007/12/16 08:0910.0 0.21 1 Fluorene ND ug/L 07/13/16 19:28 86-73-707/12/16 08:0910.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/13/16 19:28 87-68-307/12/16 08:0910.0 1.8 1 Hexachlorobenzene ND ug/L 07/13/16 19:28 118-74-107/12/16 08:0910.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/13/16 19:28 77-47-407/12/16 08:0910.0 1.8 1 Hexachloroethane ND ug/L 07/13/16 19:28 67-72-107/12/16 08:0910.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/13/16 19:28 193-39-507/12/16 08:0910.0 0.29 1 Isophorone ND ug/L 07/13/16 19:28 78-59-107/12/16 08:0910.0 1.8 1 1-Methylnaphthalene ND ug/L 07/13/16 19:28 90-12-007/12/16 08:0910.0 0.32 1 2-Methylnaphthalene ND ug/L 07/13/16 19:28 91-57-607/12/16 08:0910.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/13/16 19:28 95-48-707/12/16 08:0910.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/13/16 19:2807/12/16 08:0910.0 1.7 1 Naphthalene ND ug/L 07/13/16 19:28 91-20-307/12/16 08:0910.0 0.34 1 2-Nitroaniline ND ug/L 07/13/16 19:28 88-74-407/12/16 08:0950.0 2.8 1 3-Nitroaniline ND ug/L 07/13/16 19:28 99-09-207/12/16 08:0950.0 2.4 1 4-Nitroaniline ND ug/L 07/13/16 19:28 100-01-607/12/16 08:0920.0 2.5 1 Nitrobenzene ND ug/L 07/13/16 19:28 98-95-307/12/16 08:0910.0 1.7 1 2-Nitrophenol ND ug/L 07/13/16 19:28 88-75-507/12/16 08:0910.0 1.7 1 4-Nitrophenol ND ug/L 07/13/16 19:28 100-02-707/12/16 08:0950.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/13/16 19:28 62-75-907/12/16 08:0910.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/13/16 19:28 621-64-7 L307/12/16 08:0910.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/13/16 19:28 86-30-607/12/16 08:0910.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/13/16 19:28 108-60-107/12/16 08:0910.0 1.6 1 Pentachlorophenol ND ug/L 07/13/16 19:28 87-86-507/12/16 08:0925.0 2.3 1 Phenanthrene ND ug/L 07/13/16 19:28 85-01-807/12/16 08:0910.0 0.22 1 Phenol ND ug/L 07/13/16 19:2807/12/16 08:0910.0 1.7 1 Pyrene ND ug/L 07/13/16 19:28 129-00-007/12/16 08:0910.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/13/16 19:28 120-82-107/12/16 08:0910.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/13/16 19:28 95-95-407/12/16 08:0910.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/13/16 19:28 88-06-207/12/16 08:0910.0 1.9 1 Surrogates Nitrobenzene-d5 (S)86 %07/13/16 19:28 4165-60-007/12/16 08:0921-110 1 2-Fluorobiphenyl (S)75 %07/13/16 19:28 321-60-807/12/16 08:0927-110 1 Terphenyl-d14 (S)90 %07/13/16 19:28 1718-51-007/12/16 08:0931-107 1 Phenol-d6 (S)33 %07/13/16 19:28 13127-88-307/12/16 08:0910-110 1 2-Fluorophenol (S)44 %07/13/16 19:28 367-12-407/12/16 08:0912-110 1 2,4,6-Tribromophenol (S)92 %07/13/16 19:28 118-79-607/12/16 08:0927-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone 11.4J ug/L 07/14/16 08:32 67-64-125.0 10.0 1 Benzene ND ug/L 07/14/16 08:32 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/14/16 08:32 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-10 Lab ID: 92304618005 Collected: 07/11/16 15:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/14/16 08:32 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/14/16 08:32 75-27-41.0 0.18 1 Bromoform ND ug/L 07/14/16 08:32 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/14/16 08:32 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/14/16 08:32 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/14/16 08:32 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/14/16 08:32 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/14/16 08:32 75-00-31.0 0.54 1 Chloroform ND ug/L 07/14/16 08:32 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/14/16 08:32 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/14/16 08:32 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/14/16 08:32 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 08:32 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/14/16 08:32 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/14/16 08:32 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/14/16 08:32 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/14/16 08:32 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/14/16 08:32 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/14/16 08:32 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/14/16 08:32 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/14/16 08:32 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/14/16 08:32 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/14/16 08:32 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/14/16 08:32 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/14/16 08:32 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/14/16 08:32 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/14/16 08:32 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/14/16 08:32 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/14/16 08:32 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/14/16 08:32 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/14/16 08:32 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/14/16 08:32 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/14/16 08:32 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/14/16 08:32 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/14/16 08:32 591-78-65.0 0.46 1 p-Isopropyltoluene ND ug/L 07/14/16 08:32 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/14/16 08:32 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 08:32 108-10-15.0 0.33 1 Methyl-tert-butyl ether ND ug/L 07/14/16 08:32 1634-04-41.0 0.21 1 Naphthalene ND ug/L 07/14/16 08:32 91-20-31.0 0.24 1 Styrene ND ug/L 07/14/16 08:32 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 08:32 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 08:32 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/14/16 08:32 127-18-41.0 0.46 1 Toluene ND ug/L 07/14/16 08:32 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/14/16 08:32 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-10 Lab ID: 92304618005 Collected: 07/11/16 15:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/14/16 08:32 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/14/16 08:32 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/14/16 08:32 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/14/16 08:32 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/14/16 08:32 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/14/16 08:32 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/14/16 08:32 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/14/16 08:32 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/14/16 08:32 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/14/16 08:32 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/14/16 08:32 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)100 %07/14/16 08:32 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/14/16 08:32 17060-07-070-130 1 Toluene-d8 (S)99 %07/14/16 08:32 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-2 Lab ID: 92304618006 Collected: 07/11/16 14:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/15/16 14:52 7440-38-207/14/16 19:5010.0 5.0 1 Barium 266 ug/L 07/15/16 14:52 7440-39-307/14/16 19:505.0 2.5 1 Cadmium ND ug/L 07/15/16 14:52 7440-43-907/14/16 19:501.0 0.50 1 Chromium 33.6 ug/L 07/15/16 14:52 7440-47-307/14/16 19:505.0 2.5 1 Lead 8.4 ug/L 07/15/16 14:52 7439-92-107/14/16 19:505.0 2.5 1 Selenium ND ug/L 07/15/16 14:52 7782-49-207/14/16 19:5010.0 5.0 1 Silver ND ug/L 07/15/16 14:52 7440-22-407/14/16 19:505.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/16/16 03:11 7439-97-607/15/16 06:350.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/13/16 20:02 83-32-907/12/16 08:0910.0 0.25 1 Acenaphthylene ND ug/L 07/13/16 20:02 208-96-807/12/16 08:0910.0 0.21 1 Aniline ND ug/L 07/13/16 20:02 62-53-307/12/16 08:0910.0 1.3 1 Anthracene ND ug/L 07/13/16 20:02 120-12-707/12/16 08:0910.0 0.14 1 Benzo(a)anthracene ND ug/L 07/13/16 20:02 56-55-307/12/16 08:0910.0 0.33 1 Benzo(a)pyrene ND ug/L 07/13/16 20:02 50-32-807/12/16 08:0910.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/13/16 20:02 205-99-207/12/16 08:0910.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/13/16 20:02 191-24-207/12/16 08:0910.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/13/16 20:02 207-08-907/12/16 08:0910.0 0.43 1 Benzoic Acid ND ug/L 07/13/16 20:02 65-85-007/12/16 08:0950.0 11.1 1 Benzyl alcohol ND ug/L 07/13/16 20:02 100-51-6 L307/12/16 08:0920.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/13/16 20:02 101-55-307/12/16 08:0910.0 1.3 1 Butylbenzylphthalate ND ug/L 07/13/16 20:02 85-68-707/12/16 08:0910.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/13/16 20:02 59-50-7 L307/12/16 08:0920.0 4.2 1 4-Chloroaniline ND ug/L 07/13/16 20:02 106-47-807/12/16 08:0920.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/13/16 20:02 111-91-107/12/16 08:0910.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/13/16 20:02 111-44-407/12/16 08:0910.0 1.5 1 2-Chloronaphthalene ND ug/L 07/13/16 20:02 91-58-707/12/16 08:0910.0 2.2 1 2-Chlorophenol ND ug/L 07/13/16 20:02 95-57-807/12/16 08:0910.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/13/16 20:02 7005-72-307/12/16 08:0910.0 2.1 1 Chrysene ND ug/L 07/13/16 20:02 218-01-907/12/16 08:0910.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/13/16 20:02 53-70-307/12/16 08:0910.0 0.55 1 Dibenzofuran ND ug/L 07/13/16 20:02 132-64-907/12/16 08:0910.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/13/16 20:02 95-50-107/12/16 08:0910.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/13/16 20:02 541-73-107/12/16 08:0910.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/13/16 20:02 106-46-707/12/16 08:0910.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/13/16 20:02 91-94-107/12/16 08:0920.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/13/16 20:02 120-83-207/12/16 08:0910.0 1.7 1 Diethylphthalate ND ug/L 07/13/16 20:02 84-66-207/12/16 08:0910.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/13/16 20:02 105-67-907/12/16 08:0910.0 2.2 1 Dimethylphthalate ND ug/L 07/13/16 20:02 131-11-307/12/16 08:0910.0 1.5 1 Di-n-butylphthalate ND ug/L 07/13/16 20:02 84-74-207/12/16 08:0910.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/13/16 20:02 534-52-107/12/16 08:0920.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/13/16 20:02 51-28-507/12/16 08:0950.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-2 Lab ID: 92304618006 Collected: 07/11/16 14:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/13/16 20:02 121-14-207/12/16 08:0910.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/13/16 20:02 606-20-207/12/16 08:0910.0 1.7 1 Di-n-octylphthalate ND ug/L 07/13/16 20:02 117-84-007/12/16 08:0910.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/13/16 20:02 117-81-707/12/16 08:096.0 0.85 1 Fluoranthene ND ug/L 07/13/16 20:02 206-44-007/12/16 08:0910.0 0.21 1 Fluorene ND ug/L 07/13/16 20:02 86-73-707/12/16 08:0910.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/13/16 20:02 87-68-307/12/16 08:0910.0 1.8 1 Hexachlorobenzene ND ug/L 07/13/16 20:02 118-74-107/12/16 08:0910.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/13/16 20:02 77-47-407/12/16 08:0910.0 1.8 1 Hexachloroethane ND ug/L 07/13/16 20:02 67-72-107/12/16 08:0910.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/13/16 20:02 193-39-507/12/16 08:0910.0 0.29 1 Isophorone ND ug/L 07/13/16 20:02 78-59-107/12/16 08:0910.0 1.8 1 1-Methylnaphthalene ND ug/L 07/13/16 20:02 90-12-007/12/16 08:0910.0 0.32 1 2-Methylnaphthalene ND ug/L 07/13/16 20:02 91-57-607/12/16 08:0910.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/13/16 20:02 95-48-707/12/16 08:0910.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/13/16 20:0207/12/16 08:0910.0 1.7 1 Naphthalene ND ug/L 07/13/16 20:02 91-20-307/12/16 08:0910.0 0.34 1 2-Nitroaniline ND ug/L 07/13/16 20:02 88-74-407/12/16 08:0950.0 2.8 1 3-Nitroaniline ND ug/L 07/13/16 20:02 99-09-207/12/16 08:0950.0 2.4 1 4-Nitroaniline ND ug/L 07/13/16 20:02 100-01-607/12/16 08:0920.0 2.5 1 Nitrobenzene ND ug/L 07/13/16 20:02 98-95-307/12/16 08:0910.0 1.7 1 2-Nitrophenol ND ug/L 07/13/16 20:02 88-75-507/12/16 08:0910.0 1.7 1 4-Nitrophenol ND ug/L 07/13/16 20:02 100-02-707/12/16 08:0950.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/13/16 20:02 62-75-907/12/16 08:0910.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/13/16 20:02 621-64-7 L307/12/16 08:0910.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/13/16 20:02 86-30-607/12/16 08:0910.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/13/16 20:02 108-60-107/12/16 08:0910.0 1.6 1 Pentachlorophenol ND ug/L 07/13/16 20:02 87-86-507/12/16 08:0925.0 2.3 1 Phenanthrene ND ug/L 07/13/16 20:02 85-01-807/12/16 08:0910.0 0.22 1 Phenol ND ug/L 07/13/16 20:0207/12/16 08:0910.0 1.7 1 Pyrene ND ug/L 07/13/16 20:02 129-00-007/12/16 08:0910.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/13/16 20:02 120-82-107/12/16 08:0910.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/13/16 20:02 95-95-407/12/16 08:0910.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/13/16 20:02 88-06-207/12/16 08:0910.0 1.9 1 Surrogates Nitrobenzene-d5 (S)89 %07/13/16 20:02 4165-60-007/12/16 08:0921-110 1 2-Fluorobiphenyl (S)82 %07/13/16 20:02 321-60-807/12/16 08:0927-110 1 Terphenyl-d14 (S)76 %07/13/16 20:02 1718-51-007/12/16 08:0931-107 1 Phenol-d6 (S)34 %07/13/16 20:02 13127-88-307/12/16 08:0910-110 1 2-Fluorophenol (S)47 %07/13/16 20:02 367-12-407/12/16 08:0912-110 1 2,4,6-Tribromophenol (S)92 %07/13/16 20:02 118-79-607/12/16 08:0927-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone ND ug/L 07/14/16 08:50 67-64-125.0 10.0 1 Benzene ND ug/L 07/14/16 08:50 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/14/16 08:50 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-2 Lab ID: 92304618006 Collected: 07/11/16 14:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/14/16 08:50 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/14/16 08:50 75-27-41.0 0.18 1 Bromoform ND ug/L 07/14/16 08:50 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/14/16 08:50 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/14/16 08:50 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/14/16 08:50 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/14/16 08:50 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/14/16 08:50 75-00-31.0 0.54 1 Chloroform ND ug/L 07/14/16 08:50 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/14/16 08:50 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/14/16 08:50 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/14/16 08:50 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 08:50 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/14/16 08:50 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/14/16 08:50 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/14/16 08:50 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/14/16 08:50 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/14/16 08:50 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/14/16 08:50 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/14/16 08:50 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/14/16 08:50 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/14/16 08:50 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/14/16 08:50 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/14/16 08:50 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/14/16 08:50 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/14/16 08:50 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/14/16 08:50 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/14/16 08:50 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/14/16 08:50 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/14/16 08:50 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/14/16 08:50 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/14/16 08:50 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/14/16 08:50 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/14/16 08:50 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/14/16 08:50 591-78-65.0 0.46 1 p-Isopropyltoluene ND ug/L 07/14/16 08:50 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/14/16 08:50 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 08:50 108-10-15.0 0.33 1 Methyl-tert-butyl ether ND ug/L 07/14/16 08:50 1634-04-41.0 0.21 1 Naphthalene ND ug/L 07/14/16 08:50 91-20-31.0 0.24 1 Styrene ND ug/L 07/14/16 08:50 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 08:50 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 08:50 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/14/16 08:50 127-18-41.0 0.46 1 Toluene ND ug/L 07/14/16 08:50 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/14/16 08:50 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-2 Lab ID: 92304618006 Collected: 07/11/16 14:30 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/14/16 08:50 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/14/16 08:50 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/14/16 08:50 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/14/16 08:50 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/14/16 08:50 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/14/16 08:50 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/14/16 08:50 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/14/16 08:50 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/14/16 08:50 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/14/16 08:50 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/14/16 08:50 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)98 %07/14/16 08:50 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/14/16 08:50 17060-07-070-130 1 Toluene-d8 (S)100 %07/14/16 08:50 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-1 Lab ID: 92304618007 Collected: 07/11/16 15:10 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/15/16 14:56 7440-38-207/14/16 19:5010.0 5.0 1 Barium 328 ug/L 07/15/16 14:56 7440-39-307/14/16 19:505.0 2.5 1 Cadmium ND ug/L 07/15/16 14:56 7440-43-907/14/16 19:501.0 0.50 1 Chromium 33.4 ug/L 07/15/16 14:56 7440-47-307/14/16 19:505.0 2.5 1 Lead 7.7 ug/L 07/15/16 14:56 7439-92-107/14/16 19:505.0 2.5 1 Selenium ND ug/L 07/15/16 14:56 7782-49-207/14/16 19:5010.0 5.0 1 Silver ND ug/L 07/15/16 14:56 7440-22-407/14/16 19:505.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/16/16 03:20 7439-97-607/15/16 06:350.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/13/16 20:36 83-32-907/12/16 08:0910.0 0.25 1 Acenaphthylene ND ug/L 07/13/16 20:36 208-96-807/12/16 08:0910.0 0.21 1 Aniline ND ug/L 07/13/16 20:36 62-53-307/12/16 08:0910.0 1.3 1 Anthracene ND ug/L 07/13/16 20:36 120-12-707/12/16 08:0910.0 0.14 1 Benzo(a)anthracene ND ug/L 07/13/16 20:36 56-55-307/12/16 08:0910.0 0.33 1 Benzo(a)pyrene ND ug/L 07/13/16 20:36 50-32-807/12/16 08:0910.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/13/16 20:36 205-99-207/12/16 08:0910.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/13/16 20:36 191-24-207/12/16 08:0910.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/13/16 20:36 207-08-907/12/16 08:0910.0 0.43 1 Benzoic Acid ND ug/L 07/13/16 20:36 65-85-007/12/16 08:0950.0 11.1 1 Benzyl alcohol ND ug/L 07/13/16 20:36 100-51-6 L307/12/16 08:0920.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/13/16 20:36 101-55-307/12/16 08:0910.0 1.3 1 Butylbenzylphthalate ND ug/L 07/13/16 20:36 85-68-707/12/16 08:0910.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/13/16 20:36 59-50-7 L307/12/16 08:0920.0 4.2 1 4-Chloroaniline ND ug/L 07/13/16 20:36 106-47-807/12/16 08:0920.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/13/16 20:36 111-91-107/12/16 08:0910.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/13/16 20:36 111-44-407/12/16 08:0910.0 1.5 1 2-Chloronaphthalene ND ug/L 07/13/16 20:36 91-58-707/12/16 08:0910.0 2.2 1 2-Chlorophenol ND ug/L 07/13/16 20:36 95-57-807/12/16 08:0910.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/13/16 20:36 7005-72-307/12/16 08:0910.0 2.1 1 Chrysene ND ug/L 07/13/16 20:36 218-01-907/12/16 08:0910.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/13/16 20:36 53-70-307/12/16 08:0910.0 0.55 1 Dibenzofuran ND ug/L 07/13/16 20:36 132-64-907/12/16 08:0910.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/13/16 20:36 95-50-107/12/16 08:0910.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/13/16 20:36 541-73-107/12/16 08:0910.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/13/16 20:36 106-46-707/12/16 08:0910.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/13/16 20:36 91-94-107/12/16 08:0920.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/13/16 20:36 120-83-207/12/16 08:0910.0 1.7 1 Diethylphthalate ND ug/L 07/13/16 20:36 84-66-207/12/16 08:0910.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/13/16 20:36 105-67-907/12/16 08:0910.0 2.2 1 Dimethylphthalate ND ug/L 07/13/16 20:36 131-11-307/12/16 08:0910.0 1.5 1 Di-n-butylphthalate ND ug/L 07/13/16 20:36 84-74-207/12/16 08:0910.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/13/16 20:36 534-52-107/12/16 08:0920.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/13/16 20:36 51-28-507/12/16 08:0950.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 30 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-1 Lab ID: 92304618007 Collected: 07/11/16 15:10 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/13/16 20:36 121-14-207/12/16 08:0910.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/13/16 20:36 606-20-207/12/16 08:0910.0 1.7 1 Di-n-octylphthalate ND ug/L 07/13/16 20:36 117-84-007/12/16 08:0910.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/13/16 20:36 117-81-707/12/16 08:096.0 0.85 1 Fluoranthene ND ug/L 07/13/16 20:36 206-44-007/12/16 08:0910.0 0.21 1 Fluorene ND ug/L 07/13/16 20:36 86-73-707/12/16 08:0910.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/13/16 20:36 87-68-307/12/16 08:0910.0 1.8 1 Hexachlorobenzene ND ug/L 07/13/16 20:36 118-74-107/12/16 08:0910.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/13/16 20:36 77-47-407/12/16 08:0910.0 1.8 1 Hexachloroethane ND ug/L 07/13/16 20:36 67-72-107/12/16 08:0910.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/13/16 20:36 193-39-507/12/16 08:0910.0 0.29 1 Isophorone ND ug/L 07/13/16 20:36 78-59-107/12/16 08:0910.0 1.8 1 1-Methylnaphthalene ND ug/L 07/13/16 20:36 90-12-007/12/16 08:0910.0 0.32 1 2-Methylnaphthalene ND ug/L 07/13/16 20:36 91-57-607/12/16 08:0910.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/13/16 20:36 95-48-707/12/16 08:0910.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/13/16 20:3607/12/16 08:0910.0 1.7 1 Naphthalene ND ug/L 07/13/16 20:36 91-20-307/12/16 08:0910.0 0.34 1 2-Nitroaniline ND ug/L 07/13/16 20:36 88-74-407/12/16 08:0950.0 2.8 1 3-Nitroaniline ND ug/L 07/13/16 20:36 99-09-207/12/16 08:0950.0 2.4 1 4-Nitroaniline ND ug/L 07/13/16 20:36 100-01-607/12/16 08:0920.0 2.5 1 Nitrobenzene ND ug/L 07/13/16 20:36 98-95-307/12/16 08:0910.0 1.7 1 2-Nitrophenol ND ug/L 07/13/16 20:36 88-75-507/12/16 08:0910.0 1.7 1 4-Nitrophenol ND ug/L 07/13/16 20:36 100-02-707/12/16 08:0950.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/13/16 20:36 62-75-907/12/16 08:0910.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/13/16 20:36 621-64-7 L307/12/16 08:0910.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/13/16 20:36 86-30-607/12/16 08:0910.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/13/16 20:36 108-60-107/12/16 08:0910.0 1.6 1 Pentachlorophenol ND ug/L 07/13/16 20:36 87-86-507/12/16 08:0925.0 2.3 1 Phenanthrene ND ug/L 07/13/16 20:36 85-01-807/12/16 08:0910.0 0.22 1 Phenol ND ug/L 07/13/16 20:3607/12/16 08:0910.0 1.7 1 Pyrene ND ug/L 07/13/16 20:36 129-00-007/12/16 08:0910.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/13/16 20:36 120-82-107/12/16 08:0910.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/13/16 20:36 95-95-407/12/16 08:0910.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/13/16 20:36 88-06-207/12/16 08:0910.0 1.9 1 Surrogates Nitrobenzene-d5 (S)90 %07/13/16 20:36 4165-60-007/12/16 08:0921-110 1 2-Fluorobiphenyl (S)80 %07/13/16 20:36 321-60-807/12/16 08:0927-110 1 Terphenyl-d14 (S)91 %07/13/16 20:36 1718-51-007/12/16 08:0931-107 1 Phenol-d6 (S)41 %07/13/16 20:36 13127-88-307/12/16 08:0910-110 1 2-Fluorophenol (S)52 %07/13/16 20:36 367-12-407/12/16 08:0912-110 1 2,4,6-Tribromophenol (S)87 %07/13/16 20:36 118-79-607/12/16 08:0927-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone ND ug/L 07/14/16 09:07 67-64-125.0 10.0 1 Benzene ND ug/L 07/14/16 09:07 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/14/16 09:07 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 31 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-1 Lab ID: 92304618007 Collected: 07/11/16 15:10 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/14/16 09:07 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/14/16 09:07 75-27-41.0 0.18 1 Bromoform ND ug/L 07/14/16 09:07 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/14/16 09:07 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/14/16 09:07 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/14/16 09:07 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/14/16 09:07 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/14/16 09:07 75-00-31.0 0.54 1 Chloroform ND ug/L 07/14/16 09:07 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/14/16 09:07 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/14/16 09:07 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/14/16 09:07 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 09:07 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/14/16 09:07 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/14/16 09:07 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/14/16 09:07 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/14/16 09:07 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/14/16 09:07 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/14/16 09:07 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/14/16 09:07 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/14/16 09:07 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/14/16 09:07 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/14/16 09:07 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/14/16 09:07 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/14/16 09:07 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/14/16 09:07 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/14/16 09:07 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/14/16 09:07 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/14/16 09:07 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/14/16 09:07 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/14/16 09:07 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/14/16 09:07 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/14/16 09:07 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/14/16 09:07 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/14/16 09:07 591-78-65.0 0.46 1 p-Isopropyltoluene ND ug/L 07/14/16 09:07 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/14/16 09:07 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 09:07 108-10-15.0 0.33 1 Methyl-tert-butyl ether ND ug/L 07/14/16 09:07 1634-04-41.0 0.21 1 Naphthalene ND ug/L 07/14/16 09:07 91-20-31.0 0.24 1 Styrene ND ug/L 07/14/16 09:07 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 09:07 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 09:07 79-34-51.0 0.40 1 Tetrachloroethene 0.54J ug/L 07/14/16 09:07 127-18-41.0 0.46 1 Toluene ND ug/L 07/14/16 09:07 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/14/16 09:07 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 32 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-1 Lab ID: 92304618007 Collected: 07/11/16 15:10 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/14/16 09:07 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/14/16 09:07 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/14/16 09:07 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/14/16 09:07 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/14/16 09:07 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/14/16 09:07 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/14/16 09:07 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/14/16 09:07 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/14/16 09:07 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/14/16 09:07 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/14/16 09:07 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)98 %07/14/16 09:07 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/14/16 09:07 17060-07-070-130 1 Toluene-d8 (S)100 %07/14/16 09:07 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 33 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-14 Lab ID: 92304618008 Collected: 07/11/16 15:35 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/15/16 15:00 7440-38-207/14/16 19:5010.0 5.0 1 Barium 255 ug/L 07/15/16 15:00 7440-39-307/14/16 19:505.0 2.5 1 Cadmium ND ug/L 07/15/16 15:00 7440-43-907/14/16 19:501.0 0.50 1 Chromium 21.1 ug/L 07/15/16 15:00 7440-47-307/14/16 19:505.0 2.5 1 Lead 6.1 ug/L 07/15/16 15:00 7439-92-107/14/16 19:505.0 2.5 1 Selenium ND ug/L 07/15/16 15:00 7782-49-207/14/16 19:5010.0 5.0 1 Silver ND ug/L 07/15/16 15:00 7440-22-407/14/16 19:505.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/16/16 03:23 7439-97-607/15/16 06:350.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/13/16 21:09 83-32-907/12/16 08:0910.0 0.25 1 Acenaphthylene ND ug/L 07/13/16 21:09 208-96-807/12/16 08:0910.0 0.21 1 Aniline ND ug/L 07/13/16 21:09 62-53-307/12/16 08:0910.0 1.3 1 Anthracene ND ug/L 07/13/16 21:09 120-12-707/12/16 08:0910.0 0.14 1 Benzo(a)anthracene ND ug/L 07/13/16 21:09 56-55-307/12/16 08:0910.0 0.33 1 Benzo(a)pyrene ND ug/L 07/13/16 21:09 50-32-807/12/16 08:0910.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/13/16 21:09 205-99-207/12/16 08:0910.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/13/16 21:09 191-24-207/12/16 08:0910.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/13/16 21:09 207-08-907/12/16 08:0910.0 0.43 1 Benzoic Acid ND ug/L 07/13/16 21:09 65-85-007/12/16 08:0950.0 11.1 1 Benzyl alcohol ND ug/L 07/13/16 21:09 100-51-6 L307/12/16 08:0920.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/13/16 21:09 101-55-307/12/16 08:0910.0 1.3 1 Butylbenzylphthalate ND ug/L 07/13/16 21:09 85-68-707/12/16 08:0910.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/13/16 21:09 59-50-7 L307/12/16 08:0920.0 4.2 1 4-Chloroaniline ND ug/L 07/13/16 21:09 106-47-807/12/16 08:0920.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/13/16 21:09 111-91-107/12/16 08:0910.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/13/16 21:09 111-44-407/12/16 08:0910.0 1.5 1 2-Chloronaphthalene ND ug/L 07/13/16 21:09 91-58-707/12/16 08:0910.0 2.2 1 2-Chlorophenol ND ug/L 07/13/16 21:09 95-57-807/12/16 08:0910.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/13/16 21:09 7005-72-307/12/16 08:0910.0 2.1 1 Chrysene ND ug/L 07/13/16 21:09 218-01-907/12/16 08:0910.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/13/16 21:09 53-70-307/12/16 08:0910.0 0.55 1 Dibenzofuran ND ug/L 07/13/16 21:09 132-64-907/12/16 08:0910.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/13/16 21:09 95-50-107/12/16 08:0910.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/13/16 21:09 541-73-107/12/16 08:0910.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/13/16 21:09 106-46-707/12/16 08:0910.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/13/16 21:09 91-94-107/12/16 08:0920.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/13/16 21:09 120-83-207/12/16 08:0910.0 1.7 1 Diethylphthalate ND ug/L 07/13/16 21:09 84-66-207/12/16 08:0910.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/13/16 21:09 105-67-907/12/16 08:0910.0 2.2 1 Dimethylphthalate ND ug/L 07/13/16 21:09 131-11-307/12/16 08:0910.0 1.5 1 Di-n-butylphthalate ND ug/L 07/13/16 21:09 84-74-207/12/16 08:0910.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/13/16 21:09 534-52-107/12/16 08:0920.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/13/16 21:09 51-28-507/12/16 08:0950.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 34 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-14 Lab ID: 92304618008 Collected: 07/11/16 15:35 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/13/16 21:09 121-14-207/12/16 08:0910.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/13/16 21:09 606-20-207/12/16 08:0910.0 1.7 1 Di-n-octylphthalate ND ug/L 07/13/16 21:09 117-84-007/12/16 08:0910.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/13/16 21:09 117-81-707/12/16 08:096.0 0.85 1 Fluoranthene ND ug/L 07/13/16 21:09 206-44-007/12/16 08:0910.0 0.21 1 Fluorene ND ug/L 07/13/16 21:09 86-73-707/12/16 08:0910.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/13/16 21:09 87-68-307/12/16 08:0910.0 1.8 1 Hexachlorobenzene ND ug/L 07/13/16 21:09 118-74-107/12/16 08:0910.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/13/16 21:09 77-47-407/12/16 08:0910.0 1.8 1 Hexachloroethane ND ug/L 07/13/16 21:09 67-72-107/12/16 08:0910.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/13/16 21:09 193-39-507/12/16 08:0910.0 0.29 1 Isophorone ND ug/L 07/13/16 21:09 78-59-107/12/16 08:0910.0 1.8 1 1-Methylnaphthalene ND ug/L 07/13/16 21:09 90-12-007/12/16 08:0910.0 0.32 1 2-Methylnaphthalene ND ug/L 07/13/16 21:09 91-57-607/12/16 08:0910.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/13/16 21:09 95-48-707/12/16 08:0910.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/13/16 21:0907/12/16 08:0910.0 1.7 1 Naphthalene ND ug/L 07/13/16 21:09 91-20-307/12/16 08:0910.0 0.34 1 2-Nitroaniline ND ug/L 07/13/16 21:09 88-74-407/12/16 08:0950.0 2.8 1 3-Nitroaniline ND ug/L 07/13/16 21:09 99-09-207/12/16 08:0950.0 2.4 1 4-Nitroaniline ND ug/L 07/13/16 21:09 100-01-607/12/16 08:0920.0 2.5 1 Nitrobenzene ND ug/L 07/13/16 21:09 98-95-307/12/16 08:0910.0 1.7 1 2-Nitrophenol ND ug/L 07/13/16 21:09 88-75-507/12/16 08:0910.0 1.7 1 4-Nitrophenol ND ug/L 07/13/16 21:09 100-02-707/12/16 08:0950.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/13/16 21:09 62-75-907/12/16 08:0910.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/13/16 21:09 621-64-7 L307/12/16 08:0910.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/13/16 21:09 86-30-607/12/16 08:0910.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/13/16 21:09 108-60-107/12/16 08:0910.0 1.6 1 Pentachlorophenol ND ug/L 07/13/16 21:09 87-86-507/12/16 08:0925.0 2.3 1 Phenanthrene ND ug/L 07/13/16 21:09 85-01-807/12/16 08:0910.0 0.22 1 Phenol ND ug/L 07/13/16 21:0907/12/16 08:0910.0 1.7 1 Pyrene ND ug/L 07/13/16 21:09 129-00-007/12/16 08:0910.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/13/16 21:09 120-82-107/12/16 08:0910.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/13/16 21:09 95-95-407/12/16 08:0910.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/13/16 21:09 88-06-207/12/16 08:0910.0 1.9 1 Surrogates Nitrobenzene-d5 (S)93 %07/13/16 21:09 4165-60-007/12/16 08:0921-110 1 2-Fluorobiphenyl (S)90 %07/13/16 21:09 321-60-807/12/16 08:0927-110 1 Terphenyl-d14 (S)100 %07/13/16 21:09 1718-51-007/12/16 08:0931-107 1 Phenol-d6 (S)40 %07/13/16 21:09 13127-88-307/12/16 08:0910-110 1 2-Fluorophenol (S)54 %07/13/16 21:09 367-12-407/12/16 08:0912-110 1 2,4,6-Tribromophenol (S)89 %07/13/16 21:09 118-79-607/12/16 08:0927-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone ND ug/L 07/14/16 09:24 67-64-125.0 10.0 1 Benzene ND ug/L 07/14/16 09:24 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/14/16 09:24 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 35 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-14 Lab ID: 92304618008 Collected: 07/11/16 15:35 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/14/16 09:24 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/14/16 09:24 75-27-41.0 0.18 1 Bromoform ND ug/L 07/14/16 09:24 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/14/16 09:24 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/14/16 09:24 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/14/16 09:24 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/14/16 09:24 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/14/16 09:24 75-00-31.0 0.54 1 Chloroform ND ug/L 07/14/16 09:24 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/14/16 09:24 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/14/16 09:24 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/14/16 09:24 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 09:24 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/14/16 09:24 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/14/16 09:24 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/14/16 09:24 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/14/16 09:24 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/14/16 09:24 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/14/16 09:24 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/14/16 09:24 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/14/16 09:24 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/14/16 09:24 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/14/16 09:24 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/14/16 09:24 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/14/16 09:24 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/14/16 09:24 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/14/16 09:24 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/14/16 09:24 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/14/16 09:24 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/14/16 09:24 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/14/16 09:24 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/14/16 09:24 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/14/16 09:24 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/14/16 09:24 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/14/16 09:24 591-78-65.0 0.46 1 p-Isopropyltoluene ND ug/L 07/14/16 09:24 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/14/16 09:24 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 09:24 108-10-15.0 0.33 1 Methyl-tert-butyl ether ND ug/L 07/14/16 09:24 1634-04-41.0 0.21 1 Naphthalene ND ug/L 07/14/16 09:24 91-20-31.0 0.24 1 Styrene ND ug/L 07/14/16 09:24 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 09:24 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 09:24 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/14/16 09:24 127-18-41.0 0.46 1 Toluene ND ug/L 07/14/16 09:24 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/14/16 09:24 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 36 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-14 Lab ID: 92304618008 Collected: 07/11/16 15:35 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/14/16 09:24 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/14/16 09:24 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/14/16 09:24 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/14/16 09:24 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/14/16 09:24 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/14/16 09:24 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/14/16 09:24 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/14/16 09:24 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/14/16 09:24 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/14/16 09:24 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/14/16 09:24 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)99 %07/14/16 09:24 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/14/16 09:24 17060-07-070-130 1 Toluene-d8 (S)99 %07/14/16 09:24 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 37 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-3 Lab ID: 92304618009 Collected: 07/11/16 15:40 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND ug/L 07/15/16 15:04 7440-38-207/14/16 19:5010.0 5.0 1 Barium 356 ug/L 07/15/16 15:04 7440-39-307/14/16 19:505.0 2.5 1 Cadmium ND ug/L 07/15/16 15:04 7440-43-907/14/16 19:501.0 0.50 1 Chromium 39.1 ug/L 07/15/16 15:04 7440-47-307/14/16 19:505.0 2.5 1 Lead 10.9 ug/L 07/15/16 15:04 7439-92-107/14/16 19:505.0 2.5 1 Selenium ND ug/L 07/15/16 15:04 7782-49-207/14/16 19:5010.0 5.0 1 Silver ND ug/L 07/15/16 15:04 7440-22-407/14/16 19:505.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND ug/L 07/16/16 03:25 7439-97-607/15/16 06:350.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/13/16 21:42 83-32-907/12/16 08:0910.0 0.25 1 Acenaphthylene ND ug/L 07/13/16 21:42 208-96-807/12/16 08:0910.0 0.21 1 Aniline ND ug/L 07/13/16 21:42 62-53-307/12/16 08:0910.0 1.3 1 Anthracene ND ug/L 07/13/16 21:42 120-12-707/12/16 08:0910.0 0.14 1 Benzo(a)anthracene ND ug/L 07/13/16 21:42 56-55-307/12/16 08:0910.0 0.33 1 Benzo(a)pyrene ND ug/L 07/13/16 21:42 50-32-807/12/16 08:0910.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/13/16 21:42 205-99-207/12/16 08:0910.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/13/16 21:42 191-24-207/12/16 08:0910.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/13/16 21:42 207-08-907/12/16 08:0910.0 0.43 1 Benzoic Acid ND ug/L 07/13/16 21:42 65-85-007/12/16 08:0950.0 11.1 1 Benzyl alcohol ND ug/L 07/13/16 21:42 100-51-6 L307/12/16 08:0920.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/13/16 21:42 101-55-307/12/16 08:0910.0 1.3 1 Butylbenzylphthalate ND ug/L 07/13/16 21:42 85-68-707/12/16 08:0910.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/13/16 21:42 59-50-7 L307/12/16 08:0920.0 4.2 1 4-Chloroaniline ND ug/L 07/13/16 21:42 106-47-807/12/16 08:0920.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/13/16 21:42 111-91-107/12/16 08:0910.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/13/16 21:42 111-44-407/12/16 08:0910.0 1.5 1 2-Chloronaphthalene ND ug/L 07/13/16 21:42 91-58-707/12/16 08:0910.0 2.2 1 2-Chlorophenol ND ug/L 07/13/16 21:42 95-57-807/12/16 08:0910.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/13/16 21:42 7005-72-307/12/16 08:0910.0 2.1 1 Chrysene ND ug/L 07/13/16 21:42 218-01-907/12/16 08:0910.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/13/16 21:42 53-70-307/12/16 08:0910.0 0.55 1 Dibenzofuran ND ug/L 07/13/16 21:42 132-64-907/12/16 08:0910.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/13/16 21:42 95-50-107/12/16 08:0910.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/13/16 21:42 541-73-107/12/16 08:0910.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/13/16 21:42 106-46-707/12/16 08:0910.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/13/16 21:42 91-94-107/12/16 08:0920.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/13/16 21:42 120-83-207/12/16 08:0910.0 1.7 1 Diethylphthalate ND ug/L 07/13/16 21:42 84-66-207/12/16 08:0910.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/13/16 21:42 105-67-907/12/16 08:0910.0 2.2 1 Dimethylphthalate ND ug/L 07/13/16 21:42 131-11-307/12/16 08:0910.0 1.5 1 Di-n-butylphthalate ND ug/L 07/13/16 21:42 84-74-207/12/16 08:0910.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/13/16 21:42 534-52-107/12/16 08:0920.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/13/16 21:42 51-28-507/12/16 08:0950.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 38 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-3 Lab ID: 92304618009 Collected: 07/11/16 15:40 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/13/16 21:42 121-14-207/12/16 08:0910.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/13/16 21:42 606-20-207/12/16 08:0910.0 1.7 1 Di-n-octylphthalate ND ug/L 07/13/16 21:42 117-84-007/12/16 08:0910.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/13/16 21:42 117-81-707/12/16 08:096.0 0.85 1 Fluoranthene ND ug/L 07/13/16 21:42 206-44-007/12/16 08:0910.0 0.21 1 Fluorene ND ug/L 07/13/16 21:42 86-73-707/12/16 08:0910.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/13/16 21:42 87-68-307/12/16 08:0910.0 1.8 1 Hexachlorobenzene ND ug/L 07/13/16 21:42 118-74-107/12/16 08:0910.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/13/16 21:42 77-47-407/12/16 08:0910.0 1.8 1 Hexachloroethane ND ug/L 07/13/16 21:42 67-72-107/12/16 08:0910.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/13/16 21:42 193-39-507/12/16 08:0910.0 0.29 1 Isophorone ND ug/L 07/13/16 21:42 78-59-107/12/16 08:0910.0 1.8 1 1-Methylnaphthalene ND ug/L 07/13/16 21:42 90-12-007/12/16 08:0910.0 0.32 1 2-Methylnaphthalene ND ug/L 07/13/16 21:42 91-57-607/12/16 08:0910.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/13/16 21:42 95-48-707/12/16 08:0910.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/13/16 21:4207/12/16 08:0910.0 1.7 1 Naphthalene ND ug/L 07/13/16 21:42 91-20-307/12/16 08:0910.0 0.34 1 2-Nitroaniline ND ug/L 07/13/16 21:42 88-74-407/12/16 08:0950.0 2.8 1 3-Nitroaniline ND ug/L 07/13/16 21:42 99-09-207/12/16 08:0950.0 2.4 1 4-Nitroaniline ND ug/L 07/13/16 21:42 100-01-607/12/16 08:0920.0 2.5 1 Nitrobenzene ND ug/L 07/13/16 21:42 98-95-307/12/16 08:0910.0 1.7 1 2-Nitrophenol ND ug/L 07/13/16 21:42 88-75-507/12/16 08:0910.0 1.7 1 4-Nitrophenol ND ug/L 07/13/16 21:42 100-02-707/12/16 08:0950.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/13/16 21:42 62-75-907/12/16 08:0910.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/13/16 21:42 621-64-7 L307/12/16 08:0910.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/13/16 21:42 86-30-607/12/16 08:0910.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/13/16 21:42 108-60-107/12/16 08:0910.0 1.6 1 Pentachlorophenol ND ug/L 07/13/16 21:42 87-86-507/12/16 08:0925.0 2.3 1 Phenanthrene ND ug/L 07/13/16 21:42 85-01-807/12/16 08:0910.0 0.22 1 Phenol ND ug/L 07/13/16 21:4207/12/16 08:0910.0 1.7 1 Pyrene ND ug/L 07/13/16 21:42 129-00-007/12/16 08:0910.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/13/16 21:42 120-82-107/12/16 08:0910.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/13/16 21:42 95-95-407/12/16 08:0910.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/13/16 21:42 88-06-207/12/16 08:0910.0 1.9 1 Surrogates Nitrobenzene-d5 (S)95 %07/13/16 21:42 4165-60-007/12/16 08:0921-110 1 2-Fluorobiphenyl (S)87 %07/13/16 21:42 321-60-807/12/16 08:0927-110 1 Terphenyl-d14 (S)99 %07/13/16 21:42 1718-51-007/12/16 08:0931-107 1 Phenol-d6 (S)36 %07/13/16 21:42 13127-88-307/12/16 08:0910-110 1 2-Fluorophenol (S)50 %07/13/16 21:42 367-12-407/12/16 08:0912-110 1 2,4,6-Tribromophenol (S)93 %07/13/16 21:42 118-79-607/12/16 08:0927-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone ND ug/L 07/14/16 09:41 67-64-125.0 10.0 1 Benzene ND ug/L 07/14/16 09:41 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/14/16 09:41 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 39 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-3 Lab ID: 92304618009 Collected: 07/11/16 15:40 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/14/16 09:41 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/14/16 09:41 75-27-41.0 0.18 1 Bromoform ND ug/L 07/14/16 09:41 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/14/16 09:41 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/14/16 09:41 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/14/16 09:41 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/14/16 09:41 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/14/16 09:41 75-00-31.0 0.54 1 Chloroform ND ug/L 07/14/16 09:41 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/14/16 09:41 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/14/16 09:41 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/14/16 09:41 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 09:41 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/14/16 09:41 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/14/16 09:41 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/14/16 09:41 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/14/16 09:41 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/14/16 09:41 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/14/16 09:41 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/14/16 09:41 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/14/16 09:41 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/14/16 09:41 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/14/16 09:41 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/14/16 09:41 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/14/16 09:41 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/14/16 09:41 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/14/16 09:41 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/14/16 09:41 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/14/16 09:41 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/14/16 09:41 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/14/16 09:41 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/14/16 09:41 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/14/16 09:41 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/14/16 09:41 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/14/16 09:41 591-78-65.0 0.46 1 p-Isopropyltoluene ND ug/L 07/14/16 09:41 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/14/16 09:41 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 09:41 108-10-15.0 0.33 1 Methyl-tert-butyl ether 0.22J ug/L 07/14/16 09:41 1634-04-41.0 0.21 1 Naphthalene ND ug/L 07/14/16 09:41 91-20-31.0 0.24 1 Styrene ND ug/L 07/14/16 09:41 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 09:41 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 09:41 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/14/16 09:41 127-18-41.0 0.46 1 Toluene ND ug/L 07/14/16 09:41 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/14/16 09:41 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 40 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-3 Lab ID: 92304618009 Collected: 07/11/16 15:40 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/14/16 09:41 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/14/16 09:41 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/14/16 09:41 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/14/16 09:41 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/14/16 09:41 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/14/16 09:41 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/14/16 09:41 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/14/16 09:41 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/14/16 09:41 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/14/16 09:41 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/14/16 09:41 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)99 %07/14/16 09:41 460-00-470-130 1 1,2-Dichloroethane-d4 (S)100 %07/14/16 09:41 17060-07-070-130 1 Toluene-d8 (S)99 %07/14/16 09:41 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 41 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-6 Lab ID: 92304618010 Collected: 07/11/16 15:35 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic 36.5 ug/L 07/15/16 15:08 7440-38-207/14/16 19:5010.0 5.0 1 Barium 1190 ug/L 07/15/16 15:08 7440-39-307/14/16 19:505.0 2.5 1 Cadmium ND ug/L 07/15/16 15:08 7440-43-907/14/16 19:501.0 0.50 1 Chromium 180 ug/L 07/15/16 15:08 7440-47-307/14/16 19:505.0 2.5 1 Lead 382 ug/L 07/15/16 15:08 7439-92-107/14/16 19:505.0 2.5 1 Selenium ND ug/L 07/15/16 15:08 7782-49-207/14/16 19:5010.0 5.0 1 Silver ND ug/L 07/15/16 15:08 7440-22-407/14/16 19:505.0 2.5 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury 0.40 ug/L 07/16/16 03:28 7439-97-607/15/16 06:350.20 0.10 1 Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic Acenaphthene ND ug/L 07/13/16 22:15 83-32-907/12/16 08:0910.0 0.25 1 Acenaphthylene ND ug/L 07/13/16 22:15 208-96-807/12/16 08:0910.0 0.21 1 Aniline ND ug/L 07/13/16 22:15 62-53-307/12/16 08:0910.0 1.3 1 Anthracene ND ug/L 07/13/16 22:15 120-12-707/12/16 08:0910.0 0.14 1 Benzo(a)anthracene ND ug/L 07/13/16 22:15 56-55-307/12/16 08:0910.0 0.33 1 Benzo(a)pyrene ND ug/L 07/13/16 22:15 50-32-807/12/16 08:0910.0 0.30 1 Benzo(b)fluoranthene ND ug/L 07/13/16 22:15 205-99-207/12/16 08:0910.0 0.28 1 Benzo(g,h,i)perylene ND ug/L 07/13/16 22:15 191-24-207/12/16 08:0910.0 0.38 1 Benzo(k)fluoranthene ND ug/L 07/13/16 22:15 207-08-907/12/16 08:0910.0 0.43 1 Benzoic Acid ND ug/L 07/13/16 22:15 65-85-007/12/16 08:0950.0 11.1 1 Benzyl alcohol ND ug/L 07/13/16 22:15 100-51-6 L307/12/16 08:0920.0 3.4 1 4-Bromophenylphenyl ether ND ug/L 07/13/16 22:15 101-55-307/12/16 08:0910.0 1.3 1 Butylbenzylphthalate ND ug/L 07/13/16 22:15 85-68-707/12/16 08:0910.0 0.75 1 4-Chloro-3-methylphenol ND ug/L 07/13/16 22:15 59-50-7 L307/12/16 08:0920.0 4.2 1 4-Chloroaniline ND ug/L 07/13/16 22:15 106-47-807/12/16 08:0920.0 3.4 1 bis(2-Chloroethoxy)methane ND ug/L 07/13/16 22:15 111-91-107/12/16 08:0910.0 1.7 1 bis(2-Chloroethyl) ether ND ug/L 07/13/16 22:15 111-44-407/12/16 08:0910.0 1.5 1 2-Chloronaphthalene ND ug/L 07/13/16 22:15 91-58-707/12/16 08:0910.0 2.2 1 2-Chlorophenol ND ug/L 07/13/16 22:15 95-57-807/12/16 08:0910.0 1.5 1 4-Chlorophenylphenyl ether ND ug/L 07/13/16 22:15 7005-72-307/12/16 08:0910.0 2.1 1 Chrysene ND ug/L 07/13/16 22:15 218-01-907/12/16 08:0910.0 0.21 1 Dibenz(a,h)anthracene ND ug/L 07/13/16 22:15 53-70-307/12/16 08:0910.0 0.55 1 Dibenzofuran ND ug/L 07/13/16 22:15 132-64-907/12/16 08:0910.0 1.8 1 1,2-Dichlorobenzene ND ug/L 07/13/16 22:15 95-50-107/12/16 08:0910.0 1.2 1 1,3-Dichlorobenzene ND ug/L 07/13/16 22:15 541-73-107/12/16 08:0910.0 1.1 1 1,4-Dichlorobenzene ND ug/L 07/13/16 22:15 106-46-707/12/16 08:0910.0 1.2 1 3,3'-Dichlorobenzidine ND ug/L 07/13/16 22:15 91-94-107/12/16 08:0920.0 1.4 1 2,4-Dichlorophenol ND ug/L 07/13/16 22:15 120-83-207/12/16 08:0910.0 1.7 1 Diethylphthalate ND ug/L 07/13/16 22:15 84-66-207/12/16 08:0910.0 1.3 1 2,4-Dimethylphenol ND ug/L 07/13/16 22:15 105-67-907/12/16 08:0910.0 2.2 1 Dimethylphthalate ND ug/L 07/13/16 22:15 131-11-307/12/16 08:0910.0 1.5 1 Di-n-butylphthalate ND ug/L 07/13/16 22:15 84-74-207/12/16 08:0910.0 1.1 1 4,6-Dinitro-2-methylphenol ND ug/L 07/13/16 22:15 534-52-107/12/16 08:0920.0 1.7 1 2,4-Dinitrophenol ND ug/L 07/13/16 22:15 51-28-507/12/16 08:0950.0 6.5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 42 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-6 Lab ID: 92304618010 Collected: 07/11/16 15:35 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic 2,4-Dinitrotoluene ND ug/L 07/13/16 22:15 121-14-207/12/16 08:0910.0 1.2 1 2,6-Dinitrotoluene ND ug/L 07/13/16 22:15 606-20-207/12/16 08:0910.0 1.7 1 Di-n-octylphthalate ND ug/L 07/13/16 22:15 117-84-007/12/16 08:0910.0 0.86 1 bis(2-Ethylhexyl)phthalate ND ug/L 07/13/16 22:15 117-81-707/12/16 08:096.0 0.85 1 Fluoranthene ND ug/L 07/13/16 22:15 206-44-007/12/16 08:0910.0 0.21 1 Fluorene ND ug/L 07/13/16 22:15 86-73-707/12/16 08:0910.0 0.21 1 Hexachloro-1,3-butadiene ND ug/L 07/13/16 22:15 87-68-307/12/16 08:0910.0 1.8 1 Hexachlorobenzene ND ug/L 07/13/16 22:15 118-74-107/12/16 08:0910.0 1.1 1 Hexachlorocyclopentadiene ND ug/L 07/13/16 22:15 77-47-407/12/16 08:0910.0 1.8 1 Hexachloroethane ND ug/L 07/13/16 22:15 67-72-107/12/16 08:0910.0 1.5 1 Indeno(1,2,3-cd)pyrene ND ug/L 07/13/16 22:15 193-39-507/12/16 08:0910.0 0.29 1 Isophorone ND ug/L 07/13/16 22:15 78-59-107/12/16 08:0910.0 1.8 1 1-Methylnaphthalene ND ug/L 07/13/16 22:15 90-12-007/12/16 08:0910.0 0.32 1 2-Methylnaphthalene ND ug/L 07/13/16 22:15 91-57-607/12/16 08:0910.0 0.28 1 2-Methylphenol(o-Cresol)ND ug/L 07/13/16 22:15 95-48-707/12/16 08:0910.0 1.7 1 3&4-Methylphenol(m&p Cresol)ND ug/L 07/13/16 22:1507/12/16 08:0910.0 1.7 1 Naphthalene ND ug/L 07/13/16 22:15 91-20-307/12/16 08:0910.0 0.34 1 2-Nitroaniline ND ug/L 07/13/16 22:15 88-74-407/12/16 08:0950.0 2.8 1 3-Nitroaniline ND ug/L 07/13/16 22:15 99-09-207/12/16 08:0950.0 2.4 1 4-Nitroaniline ND ug/L 07/13/16 22:15 100-01-607/12/16 08:0920.0 2.5 1 Nitrobenzene ND ug/L 07/13/16 22:15 98-95-307/12/16 08:0910.0 1.7 1 2-Nitrophenol ND ug/L 07/13/16 22:15 88-75-507/12/16 08:0910.0 1.7 1 4-Nitrophenol ND ug/L 07/13/16 22:15 100-02-707/12/16 08:0950.0 5.8 1 N-Nitrosodimethylamine ND ug/L 07/13/16 22:15 62-75-907/12/16 08:0910.0 1.3 1 N-Nitroso-di-n-propylamine ND ug/L 07/13/16 22:15 621-64-7 L307/12/16 08:0910.0 2.1 1 N-Nitrosodiphenylamine ND ug/L 07/13/16 22:15 86-30-607/12/16 08:0910.0 1.3 1 2,2'-Oxybis(1-chloropropane)ND ug/L 07/13/16 22:15 108-60-107/12/16 08:0910.0 1.6 1 Pentachlorophenol ND ug/L 07/13/16 22:15 87-86-507/12/16 08:0925.0 2.3 1 Phenanthrene ND ug/L 07/13/16 22:15 85-01-807/12/16 08:0910.0 0.22 1 Phenol ND ug/L 07/13/16 22:1507/12/16 08:0910.0 1.7 1 Pyrene ND ug/L 07/13/16 22:15 129-00-007/12/16 08:0910.0 0.19 1 1,2,4-Trichlorobenzene ND ug/L 07/13/16 22:15 120-82-107/12/16 08:0910.0 1.9 1 2,4,5-Trichlorophenol ND ug/L 07/13/16 22:15 95-95-407/12/16 08:0910.0 2.2 1 2,4,6-Trichlorophenol ND ug/L 07/13/16 22:15 88-06-207/12/16 08:0910.0 1.9 1 Surrogates Nitrobenzene-d5 (S)92 %07/13/16 22:15 4165-60-007/12/16 08:0921-110 1 2-Fluorobiphenyl (S)82 %07/13/16 22:15 321-60-807/12/16 08:0927-110 1 Terphenyl-d14 (S)94 %07/13/16 22:15 1718-51-007/12/16 08:0931-107 1 Phenol-d6 (S)40 %07/13/16 22:15 13127-88-307/12/16 08:0910-110 1 2-Fluorophenol (S)52 %07/13/16 22:15 367-12-407/12/16 08:0912-110 1 2,4,6-Tribromophenol (S)91 %07/13/16 22:15 118-79-607/12/16 08:0927-110 1 Analytical Method: EPA 82608260 MSV Low Level Acetone ND ug/L 07/14/16 09:58 67-64-125.0 10.0 1 Benzene ND ug/L 07/14/16 09:58 71-43-21.0 0.25 1 Bromobenzene ND ug/L 07/14/16 09:58 108-86-11.0 0.30 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 43 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-6 Lab ID: 92304618010 Collected: 07/11/16 15:35 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Bromochloromethane ND ug/L 07/14/16 09:58 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 07/14/16 09:58 75-27-41.0 0.18 1 Bromoform ND ug/L 07/14/16 09:58 75-25-21.0 0.26 1 Bromomethane ND ug/L 07/14/16 09:58 74-83-92.0 0.29 1 2-Butanone (MEK)ND ug/L 07/14/16 09:58 78-93-35.0 0.96 1 Carbon tetrachloride ND ug/L 07/14/16 09:58 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 07/14/16 09:58 108-90-71.0 0.23 1 Chloroethane ND ug/L 07/14/16 09:58 75-00-31.0 0.54 1 Chloroform ND ug/L 07/14/16 09:58 67-66-31.0 0.14 1 Chloromethane ND ug/L 07/14/16 09:58 74-87-31.0 0.11 1 2-Chlorotoluene ND ug/L 07/14/16 09:58 95-49-81.0 0.35 1 4-Chlorotoluene ND ug/L 07/14/16 09:58 106-43-41.0 0.31 1 1,2-Dibromo-3-chloropropane ND ug/L 07/14/16 09:58 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 07/14/16 09:58 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 07/14/16 09:58 106-93-41.0 0.27 1 Dibromomethane ND ug/L 07/14/16 09:58 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 07/14/16 09:58 95-50-11.0 0.30 1 1,3-Dichlorobenzene ND ug/L 07/14/16 09:58 541-73-11.0 0.24 1 1,4-Dichlorobenzene ND ug/L 07/14/16 09:58 106-46-71.0 0.33 1 Dichlorodifluoromethane ND ug/L 07/14/16 09:58 75-71-81.0 0.21 1 1,1-Dichloroethane ND ug/L 07/14/16 09:58 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 07/14/16 09:58 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 07/14/16 09:58 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 07/14/16 09:58 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 07/14/16 09:58 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 07/14/16 09:58 78-87-51.0 0.27 1 1,3-Dichloropropane ND ug/L 07/14/16 09:58 142-28-91.0 0.28 1 2,2-Dichloropropane ND ug/L 07/14/16 09:58 594-20-71.0 0.13 1 1,1-Dichloropropene ND ug/L 07/14/16 09:58 563-58-61.0 0.49 1 cis-1,3-Dichloropropene ND ug/L 07/14/16 09:58 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 07/14/16 09:58 10061-02-61.0 0.26 1 Diisopropyl ether ND ug/L 07/14/16 09:58 108-20-31.0 0.12 1 Ethylbenzene ND ug/L 07/14/16 09:58 100-41-41.0 0.30 1 Hexachloro-1,3-butadiene ND ug/L 07/14/16 09:58 87-68-31.0 0.71 1 2-Hexanone ND ug/L 07/14/16 09:58 591-78-65.0 0.46 1 p-Isopropyltoluene ND ug/L 07/14/16 09:58 99-87-61.0 0.31 1 Methylene Chloride ND ug/L 07/14/16 09:58 75-09-22.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 07/14/16 09:58 108-10-15.0 0.33 1 Methyl-tert-butyl ether ND ug/L 07/14/16 09:58 1634-04-41.0 0.21 1 Naphthalene ND ug/L 07/14/16 09:58 91-20-31.0 0.24 1 Styrene ND ug/L 07/14/16 09:58 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 07/14/16 09:58 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 07/14/16 09:58 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 07/14/16 09:58 127-18-41.0 0.46 1 Toluene ND ug/L 07/14/16 09:58 108-88-31.0 0.26 1 1,2,3-Trichlorobenzene ND ug/L 07/14/16 09:58 87-61-61.0 0.33 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 44 of 61 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Sample: MW-6 Lab ID: 92304618010 Collected: 07/11/16 15:35 Received: 07/11/16 16:30 Matrix: Water Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,2,4-Trichlorobenzene ND ug/L 07/14/16 09:58 120-82-11.0 0.35 1 1,1,1-Trichloroethane ND ug/L 07/14/16 09:58 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 07/14/16 09:58 79-00-51.0 0.29 1 Trichloroethene ND ug/L 07/14/16 09:58 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 07/14/16 09:58 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 07/14/16 09:58 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 07/14/16 09:58 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 07/14/16 09:58 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 07/14/16 09:58 1330-20-71.0 0.66 1 m&p-Xylene ND ug/L 07/14/16 09:58 179601-23-12.0 0.66 1 o-Xylene ND ug/L 07/14/16 09:58 95-47-61.0 0.23 1 Surrogates 4-Bromofluorobenzene (S)98 %07/14/16 09:58 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/14/16 09:58 17060-07-070-130 1 Toluene-d8 (S)99 %07/14/16 09:58 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 45 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 321121 EPA 7470 EPA 7470 7470 Mercury Associated Lab Samples:92304618001, 92304618002, 92304618003, 92304618004, 92304618005, 92304618006, 92304618007,92304618008, 92304618009, 92304618010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1779548 Associated Lab Samples: 92304618001, 92304618002, 92304618003, 92304618004, 92304618005, 92304618006, 92304618007,92304618008, 92304618009, 92304618010 Matrix: Water AnalyzedMDL Mercury ug/L ND 0.20 07/16/16 02:450.10 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1779549LABORATORY CONTROL SAMPLE: LCSSpike Mercury ug/L 2.42.5 98 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1779550MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92304618001 1779551 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury ug/L 2.5 95 75-12594 1 252.5ND 2.4 2.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 46 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 321102 EPA 3010A EPA 6010 6010 MET Associated Lab Samples:92304618001, 92304618002, 92304618003, 92304618004, 92304618005, 92304618006, 92304618007,92304618008, 92304618009, 92304618010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1779500 Associated Lab Samples: 92304618001, 92304618002, 92304618003, 92304618004, 92304618005, 92304618006, 92304618007,92304618008, 92304618009, 92304618010 Matrix: Water AnalyzedMDL Arsenic ug/L ND 10.0 07/15/16 13:565.0 Barium ug/L ND 5.0 07/15/16 13:562.5 Cadmium ug/L ND 1.0 07/15/16 13:560.50 Chromium ug/L ND 5.0 07/15/16 13:562.5 Lead ug/L ND 5.0 07/15/16 13:562.5 Selenium ug/L ND 10.0 07/15/16 13:565.0 Silver ug/L ND 5.0 07/15/16 13:562.5 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1779501LABORATORY CONTROL SAMPLE: LCSSpike Arsenic ug/L 440500 88 80-120 Barium ug/L 456500 91 80-120 Cadmium ug/L 451500 90 80-120 Chromium ug/L 452500 90 80-120 Lead ug/L 450500 90 80-120 Selenium ug/L 444500 89 80-120 Silver ug/L 231250 92 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1779502MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92304618001 1779503 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic ug/L 500 92 75-12595 4 20500ND458 476 Barium ug/L 500 89 75-12593 4 20500131576 598 Cadmium ug/L 500 88 75-12591 4 20500ND440 456 Chromium ug/L 500 89 75-12593 4 20500ND445 465 Lead ug/L 500 87 75-12592 5 20500ND439 460 Selenium ug/L 500 92 75-12596 5 20500ND461 483 Silver ug/L 250 94 75-12598 5 20250ND234 245 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 47 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 321049 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples:92304618001, 92304618002, 92304618003, 92304618004, 92304618005, 92304618006, 92304618007,92304618008, 92304618009, 92304618010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1779157 Associated Lab Samples: 92304618001, 92304618002, 92304618003, 92304618004, 92304618005, 92304618006, 92304618007,92304618008, 92304618009, 92304618010 Matrix: Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/14/16 02:150.33 1,1,1-Trichloroethane ug/L ND 1.0 07/14/16 02:150.48 1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/14/16 02:150.40 1,1,2-Trichloroethane ug/L ND 1.0 07/14/16 02:150.29 1,1-Dichloroethane ug/L ND 1.0 07/14/16 02:150.32 1,1-Dichloroethene ug/L ND 1.0 07/14/16 02:150.56 1,1-Dichloropropene ug/L ND 1.0 07/14/16 02:150.49 1,2,3-Trichlorobenzene ug/L ND 1.0 07/14/16 02:150.33 1,2,3-Trichloropropane ug/L ND 1.0 07/14/16 02:150.41 1,2,4-Trichlorobenzene ug/L ND 1.0 07/14/16 02:150.35 1,2-Dibromo-3-chloropropane ug/L ND 2.0 07/14/16 02:152.0 1,2-Dibromoethane (EDB)ug/L ND 1.0 07/14/16 02:150.27 1,2-Dichlorobenzene ug/L ND 1.0 07/14/16 02:150.30 1,2-Dichloroethane ug/L ND 1.0 07/14/16 02:150.24 1,2-Dichloropropane ug/L ND 1.0 07/14/16 02:150.27 1,3-Dichlorobenzene ug/L ND 1.0 07/14/16 02:150.24 1,3-Dichloropropane ug/L ND 1.0 07/14/16 02:150.28 1,4-Dichlorobenzene ug/L ND 1.0 07/14/16 02:150.33 2,2-Dichloropropane ug/L ND 1.0 07/14/16 02:150.13 2-Butanone (MEK)ug/L ND 5.0 07/14/16 02:150.96 2-Chlorotoluene ug/L ND 1.0 07/14/16 02:150.35 2-Hexanone ug/L ND 5.0 07/14/16 02:150.46 4-Chlorotoluene ug/L ND 1.0 07/14/16 02:150.31 4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/14/16 02:150.33 Acetone ug/L ND 25.0 07/14/16 02:1510.0 Benzene ug/L ND 1.0 07/14/16 02:150.25 Bromobenzene ug/L ND 1.0 07/14/16 02:150.30 Bromochloromethane ug/L ND 1.0 07/14/16 02:150.17 Bromodichloromethane ug/L ND 1.0 07/14/16 02:150.18 Bromoform ug/L ND 1.0 07/14/16 02:150.26 Bromomethane ug/L ND 2.0 07/14/16 02:150.29 Carbon tetrachloride ug/L ND 1.0 07/14/16 02:150.25 Chlorobenzene ug/L ND 1.0 07/14/16 02:150.23 Chloroethane ug/L ND 1.0 07/14/16 02:150.54 Chloroform ug/L ND 1.0 07/14/16 02:150.14 Chloromethane ug/L ND 1.0 07/14/16 02:150.11 cis-1,2-Dichloroethene ug/L ND 1.0 07/14/16 02:150.19 cis-1,3-Dichloropropene ug/L ND 1.0 07/14/16 02:150.13 Dibromochloromethane ug/L ND 1.0 07/14/16 02:150.21 Dibromomethane ug/L ND 1.0 07/14/16 02:150.21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 48 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1779157 Associated Lab Samples: 92304618001, 92304618002, 92304618003, 92304618004, 92304618005, 92304618006, 92304618007,92304618008, 92304618009, 92304618010 Matrix: Water AnalyzedMDL Dichlorodifluoromethane ug/L ND 1.0 07/14/16 02:150.21 Diisopropyl ether ug/L ND 1.0 07/14/16 02:150.12 Ethylbenzene ug/L ND 1.0 07/14/16 02:150.30 Hexachloro-1,3-butadiene ug/L ND 1.0 07/14/16 02:150.71 m&p-Xylene ug/L ND 2.0 07/14/16 02:150.66 Methyl-tert-butyl ether ug/L ND 1.0 07/14/16 02:150.21 Methylene Chloride ug/L ND 2.0 07/14/16 02:150.97 Naphthalene ug/L ND 1.0 07/14/16 02:150.24 o-Xylene ug/L ND 1.0 07/14/16 02:150.23 p-Isopropyltoluene ug/L ND 1.0 07/14/16 02:150.31 Styrene ug/L ND 1.0 07/14/16 02:150.26 Tetrachloroethene ug/L ND 1.0 07/14/16 02:150.46 Toluene ug/L ND 1.0 07/14/16 02:150.26 trans-1,2-Dichloroethene ug/L ND 1.0 07/14/16 02:150.49 trans-1,3-Dichloropropene ug/L ND 1.0 07/14/16 02:150.26 Trichloroethene ug/L ND 1.0 07/14/16 02:150.47 Trichlorofluoromethane ug/L ND 1.0 07/14/16 02:150.20 Vinyl acetate ug/L ND 2.0 07/14/16 02:150.35 Vinyl chloride ug/L ND 1.0 07/14/16 02:150.62 Xylene (Total)ug/L ND 1.0 07/14/16 02:150.66 1,2-Dichloroethane-d4 (S)%100 70-130 07/14/16 02:15 4-Bromofluorobenzene (S)%100 70-130 07/14/16 02:15 Toluene-d8 (S)%99 70-130 07/14/16 02:15 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1779158LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 46.150 92 70-130 1,1,1-Trichloroethane ug/L 44.550 89 70-130 1,1,2,2-Tetrachloroethane ug/L 45.350 91 70-130 1,1,2-Trichloroethane ug/L 45.150 90 70-130 1,1-Dichloroethane ug/L 43.450 87 70-130 1,1-Dichloroethene ug/L 45.650 91 70-132 1,1-Dichloropropene ug/L 42.150 84 70-130 1,2,3-Trichlorobenzene ug/L 48.650 97 70-135 1,2,3-Trichloropropane ug/L 44.950 90 70-130 1,2,4-Trichlorobenzene ug/L 46.950 94 70-134 1,2-Dibromo-3-chloropropane ug/L 49.750 99 70-130 1,2-Dibromoethane (EDB)ug/L 49.250 98 70-130 1,2-Dichlorobenzene ug/L 48.950 98 70-130 1,2-Dichloroethane ug/L 44.750 89 70-130 1,2-Dichloropropane ug/L 44.150 88 70-130 1,3-Dichlorobenzene ug/L 46.450 93 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 49 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1779158LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichloropropane ug/L 44.550 89 70-130 1,4-Dichlorobenzene ug/L 46.050 92 70-130 2,2-Dichloropropane ug/L 40.850 82 58-145 2-Butanone (MEK)ug/L 92.1100 92 70-145 2-Chlorotoluene ug/L 45.650 91 70-130 2-Hexanone ug/L 94.6100 95 70-144 4-Chlorotoluene ug/L 44.350 89 70-130 4-Methyl-2-pentanone (MIBK)ug/L 94.1100 94 70-140 Acetone ug/L 93.5100 94 50-175 Benzene ug/L 44.550 89 70-130 Bromobenzene ug/L 46.050 92 70-130 Bromochloromethane ug/L 47.450 95 70-130 Bromodichloromethane ug/L 46.550 93 70-130 Bromoform ug/L 41.650 83 70-130 Bromomethane ug/L 48.050 96 54-130 Carbon tetrachloride ug/L 44.850 90 70-132 Chlorobenzene ug/L 46.350 93 70-130 Chloroethane ug/L 45.050 90 64-134 Chloroform ug/L 44.350 89 70-130 Chloromethane ug/L 50.050 100 64-130 cis-1,2-Dichloroethene ug/L 44.850 90 70-131 cis-1,3-Dichloropropene ug/L 44.750 89 70-130 Dibromochloromethane ug/L 47.650 95 70-130 Dibromomethane ug/L 47.050 94 70-131 Dichlorodifluoromethane ug/L 48.250 96 56-130 Diisopropyl ether ug/L 45.950 92 70-130 Ethylbenzene ug/L 44.450 89 70-130 Hexachloro-1,3-butadiene ug/L 45.150 90 70-130 m&p-Xylene ug/L 88.1100 88 70-130 Methyl-tert-butyl ether ug/L 46.350 93 70-130 Methylene Chloride ug/L 44.750 89 63-130 Naphthalene ug/L 45.650 91 70-138 o-Xylene ug/L 43.650 87 70-130 p-Isopropyltoluene ug/L 45.350 91 70-130 Styrene ug/L 47.950 96 70-130 Tetrachloroethene ug/L 40.850 82 70-130 Toluene ug/L 44.950 90 70-130 trans-1,2-Dichloroethene ug/L 44.650 89 70-130 trans-1,3-Dichloropropene ug/L 44.850 90 70-132 Trichloroethene ug/L 43.750 87 70-130 Trichlorofluoromethane ug/L 47.750 95 62-133 Vinyl acetate ug/L 87.7100 88 66-157 Vinyl chloride ug/L 45.350 91 50-150 Xylene (Total)ug/L 132150 88 70-130 1,2-Dichloroethane-d4 (S)%100 70-130 4-Bromofluorobenzene (S)%101 70-130 Toluene-d8 (S)%100 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 50 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1779159MATRIX SPIKE SAMPLE: MSSpike Result 92304618001 1,1,1,2-Tetrachloroethane ug/L 20.220 101 70-130ND 1,1,1-Trichloroethane ug/L 20.820 104 70-130ND 1,1,2,2-Tetrachloroethane ug/L 19.420 97 70-130ND 1,1,2-Trichloroethane ug/L 19.420 97 70-130ND 1,1-Dichloroethane ug/L 20.120 100 70-130ND 1,1-Dichloroethene ug/L 21.720 108 70-166ND 1,1-Dichloropropene ug/L 19.520 98 70-130ND 1,2,3-Trichlorobenzene ug/L 20.020 100 70-130ND 1,2,3-Trichloropropane ug/L 18.820 94 70-130ND 1,2,4-Trichlorobenzene ug/L 19.820 99 70-130ND 1,2-Dibromo-3-chloropropane ug/L 20.620 103 70-130ND 1,2-Dibromoethane (EDB)ug/L 20.920 104 70-130ND 1,2-Dichlorobenzene ug/L 21.120 106 70-130ND 1,2-Dichloroethane ug/L 19.620 98 70-130ND 1,2-Dichloropropane ug/L 18.720 94 70-130ND 1,3-Dichlorobenzene ug/L 20.520 102 70-130ND 1,3-Dichloropropane ug/L 19.120 96 70-130ND 1,4-Dichlorobenzene ug/L 20.520 102 70-130ND 2,2-Dichloropropane ug/L 16.820 84 70-130ND 2-Butanone (MEK)ug/L 40.440 101 70-130ND 2-Chlorotoluene ug/L 21.020 105 70-130ND 2-Hexanone ug/L 40.340 101 70-130ND 4-Chlorotoluene ug/L 20.020 100 70-130ND 4-Methyl-2-pentanone (MIBK)ug/L 39.840 99 70-130ND Acetone ug/L 41.940 101 70-130ND Benzene ug/L 20.320 101 70-148ND Bromobenzene ug/L 20.520 102 70-130ND Bromochloromethane ug/L 21.020 105 70-130ND Bromodichloromethane ug/L 19.920 99 70-130ND Bromoform ug/L 18.020 90 70-130ND Bromomethane ug/L 20.220 101 70-130ND Carbon tetrachloride ug/L 21.520 108 70-130ND Chlorobenzene ug/L 20.820 104 70-146ND Chloroethane ug/L 21.920 110 70-130ND Chloroform ug/L 20.320 101 70-130ND Chloromethane ug/L 22.720 114 70-130ND cis-1,2-Dichloroethene ug/L 20.720 104 70-130ND cis-1,3-Dichloropropene ug/L 18.620 93 70-130ND Dibromochloromethane ug/L 19.820 99 70-130ND Dibromomethane ug/L 20.420 102 70-130ND Dichlorodifluoromethane ug/L 21.820 109 70-130ND Diisopropyl ether ug/L 19.420 97 70-130ND Ethylbenzene ug/L 20.220 101 70-130ND Hexachloro-1,3-butadiene ug/L 19.620 98 70-130ND m&p-Xylene ug/L 40.140 100 70-130ND Methyl-tert-butyl ether ug/L 19.120 95 70-130ND Methylene Chloride ug/L 19.020 95 70-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 51 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1779159MATRIX SPIKE SAMPLE: MSSpike Result 92304618001 Naphthalene ug/L 18.820 94 70-130ND o-Xylene ug/L 19.820 99 70-130ND p-Isopropyltoluene ug/L 20.120 101 70-130ND Styrene ug/L 21.220 106 70-130ND Tetrachloroethene ug/L 19.120 95 70-130ND Toluene ug/L 20.420 102 70-155ND trans-1,2-Dichloroethene ug/L 21.320 107 70-130ND trans-1,3-Dichloropropene ug/L 18.020 90 70-130ND Trichloroethene ug/L 19.820 99 69-151ND Trichlorofluoromethane ug/L 23.920 119 70-130ND Vinyl acetate ug/L 29.340 73 70-130ND Vinyl chloride ug/L 22.120 111 70-130ND 1,2-Dichloroethane-d4 (S)%100 70-130 4-Bromofluorobenzene (S)%101 70-130 Toluene-d8 (S)%99 70-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92304618002 1779160SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/L ND 30ND 1,1,1-Trichloroethane ug/L ND 30ND 1,1,2,2-Tetrachloroethane ug/L ND 30ND 1,1,2-Trichloroethane ug/L ND 30ND 1,1-Dichloroethane ug/L ND 30ND 1,1-Dichloroethene ug/L ND 30ND 1,1-Dichloropropene ug/L ND 30ND 1,2,3-Trichlorobenzene ug/L ND 30ND 1,2,3-Trichloropropane ug/L ND 30ND 1,2,4-Trichlorobenzene ug/L ND 30ND 1,2-Dibromo-3-chloropropane ug/L ND 30ND 1,2-Dibromoethane (EDB)ug/L ND 30ND 1,2-Dichlorobenzene ug/L ND 30ND 1,2-Dichloroethane ug/L ND 30ND 1,2-Dichloropropane ug/L ND 30ND 1,3-Dichlorobenzene ug/L ND 30ND 1,3-Dichloropropane ug/L ND 30ND 1,4-Dichlorobenzene ug/L ND 30ND 2,2-Dichloropropane ug/L ND 30ND 2-Butanone (MEK)ug/L ND 30ND 2-Chlorotoluene ug/L ND 30ND 2-Hexanone ug/L ND 30ND 4-Chlorotoluene ug/L ND 30ND 4-Methyl-2-pentanone (MIBK)ug/L ND 30ND Acetone ug/L 29.0 7 3027.1 Benzene ug/L ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 52 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92304618002 1779160SAMPLE DUPLICATE: Bromobenzene ug/L ND 30ND Bromochloromethane ug/L ND 30ND Bromodichloromethane ug/L ND 30ND Bromoform ug/L ND 30ND Bromomethane ug/L ND 30ND Carbon tetrachloride ug/L ND 30ND Chlorobenzene ug/L ND 30ND Chloroethane ug/L ND 30ND Chloroform ug/L ND 30ND Chloromethane ug/L ND 30ND cis-1,2-Dichloroethene ug/L ND 30ND cis-1,3-Dichloropropene ug/L ND 30ND Dibromochloromethane ug/L ND 30ND Dibromomethane ug/L ND 30ND Dichlorodifluoromethane ug/L ND 30ND Diisopropyl ether ug/L ND 30ND Ethylbenzene ug/L ND 30ND Hexachloro-1,3-butadiene ug/L ND 30ND m&p-Xylene ug/L ND 30ND Methyl-tert-butyl ether ug/L ND 30ND Methylene Chloride ug/L ND 30ND Naphthalene ug/L 0.72J 300.70J o-Xylene ug/L ND 30ND p-Isopropyltoluene ug/L 9.9 4 3010.3 Styrene ug/L ND 30ND Tetrachloroethene ug/L ND 30ND Toluene ug/L ND 30ND trans-1,2-Dichloroethene ug/L ND 30ND trans-1,3-Dichloropropene ug/L ND 30ND Trichloroethene ug/L ND 30ND Trichlorofluoromethane ug/L ND 30ND Vinyl acetate ug/L ND 30ND Vinyl chloride ug/L ND 30ND Xylene (Total)ug/L ND 30ND 1,2-Dichloroethane-d4 (S)%102 1101 4-Bromofluorobenzene (S)%99 199 Toluene-d8 (S)%99 1100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 53 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 320942 EPA 3510 EPA 8270 8270 Water MSSV Associated Lab Samples:92304618001, 92304618002, 92304618003, 92304618004, 92304618005, 92304618006, 92304618007,92304618008, 92304618009, 92304618010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1778412 Associated Lab Samples: 92304618001, 92304618002, 92304618003, 92304618004, 92304618005, 92304618006, 92304618007,92304618008, 92304618009, 92304618010 Matrix: Water AnalyzedMDL 1,2,4-Trichlorobenzene ug/L ND 10.0 07/13/16 13:531.9 1,2-Dichlorobenzene ug/L ND 10.0 07/13/16 13:531.2 1,3-Dichlorobenzene ug/L ND 10.0 07/13/16 13:531.1 1,4-Dichlorobenzene ug/L ND 10.0 07/13/16 13:531.2 1-Methylnaphthalene ug/L ND 10.0 07/13/16 13:530.32 2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 07/13/16 13:531.6 2,4,5-Trichlorophenol ug/L ND 10.0 07/13/16 13:532.2 2,4,6-Trichlorophenol ug/L ND 10.0 07/13/16 13:531.9 2,4-Dichlorophenol ug/L ND 10.0 07/13/16 13:531.7 2,4-Dimethylphenol ug/L ND 10.0 07/13/16 13:532.2 2,4-Dinitrophenol ug/L ND 50.0 07/13/16 13:536.5 2,4-Dinitrotoluene ug/L ND 10.0 07/13/16 13:531.2 2,6-Dinitrotoluene ug/L ND 10.0 07/13/16 13:531.7 2-Chloronaphthalene ug/L ND 10.0 07/13/16 13:532.2 2-Chlorophenol ug/L ND 10.0 07/13/16 13:531.5 2-Methylnaphthalene ug/L ND 10.0 07/13/16 13:530.28 2-Methylphenol(o-Cresol)ug/L ND 10.0 07/13/16 13:531.7 2-Nitroaniline ug/L ND 50.0 07/13/16 13:532.8 2-Nitrophenol ug/L ND 10.0 07/13/16 13:531.7 3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/13/16 13:531.7 3,3'-Dichlorobenzidine ug/L ND 20.0 07/13/16 13:531.4 3-Nitroaniline ug/L ND 50.0 07/13/16 13:532.4 4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/13/16 13:531.7 4-Bromophenylphenyl ether ug/L ND 10.0 07/13/16 13:531.3 4-Chloro-3-methylphenol ug/L ND 20.0 07/13/16 13:534.2 4-Chloroaniline ug/L ND 20.0 07/13/16 13:533.4 4-Chlorophenylphenyl ether ug/L ND 10.0 07/13/16 13:532.1 4-Nitroaniline ug/L ND 20.0 07/13/16 13:532.5 4-Nitrophenol ug/L ND 50.0 07/13/16 13:535.8 Acenaphthene ug/L ND 10.0 07/13/16 13:530.25 Acenaphthylene ug/L ND 10.0 07/13/16 13:530.21 Aniline ug/L ND 10.0 07/13/16 13:531.3 Anthracene ug/L ND 10.0 07/13/16 13:530.14 Benzo(a)anthracene ug/L ND 10.0 07/13/16 13:530.33 Benzo(a)pyrene ug/L ND 10.0 07/13/16 13:530.30 Benzo(b)fluoranthene ug/L ND 10.0 07/13/16 13:530.28 Benzo(g,h,i)perylene ug/L ND 10.0 07/13/16 13:530.38 Benzo(k)fluoranthene ug/L ND 10.0 07/13/16 13:530.43 Benzoic Acid ug/L ND 50.0 07/13/16 13:5311.1 Benzyl alcohol ug/L ND 20.0 07/13/16 13:533.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 54 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 1778412 Associated Lab Samples: 92304618001, 92304618002, 92304618003, 92304618004, 92304618005, 92304618006, 92304618007,92304618008, 92304618009, 92304618010 Matrix: Water AnalyzedMDL bis(2-Chloroethoxy)methane ug/L ND 10.0 07/13/16 13:531.7 bis(2-Chloroethyl) ether ug/L ND 10.0 07/13/16 13:531.5 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 07/13/16 13:530.85 Butylbenzylphthalate ug/L ND 10.0 07/13/16 13:530.75 Chrysene ug/L ND 10.0 07/13/16 13:530.21 Di-n-butylphthalate ug/L ND 10.0 07/13/16 13:531.1 Di-n-octylphthalate ug/L ND 10.0 07/13/16 13:530.86 Dibenz(a,h)anthracene ug/L ND 10.0 07/13/16 13:530.55 Dibenzofuran ug/L ND 10.0 07/13/16 13:531.8 Diethylphthalate ug/L ND 10.0 07/13/16 13:531.3 Dimethylphthalate ug/L ND 10.0 07/13/16 13:531.5 Fluoranthene ug/L ND 10.0 07/13/16 13:530.21 Fluorene ug/L ND 10.0 07/13/16 13:530.21 Hexachloro-1,3-butadiene ug/L ND 10.0 07/13/16 13:531.8 Hexachlorobenzene ug/L ND 10.0 07/13/16 13:531.1 Hexachlorocyclopentadiene ug/L ND 10.0 07/13/16 13:531.8 Hexachloroethane ug/L ND 10.0 07/13/16 13:531.5 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/13/16 13:530.29 Isophorone ug/L ND 10.0 07/13/16 13:531.8 N-Nitroso-di-n-propylamine ug/L ND 10.0 07/13/16 13:532.1 N-Nitrosodimethylamine ug/L ND 10.0 07/13/16 13:531.3 N-Nitrosodiphenylamine ug/L ND 10.0 07/13/16 13:531.3 Naphthalene ug/L ND 10.0 07/13/16 13:530.34 Nitrobenzene ug/L ND 10.0 07/13/16 13:531.7 Pentachlorophenol ug/L ND 25.0 07/13/16 13:532.3 Phenanthrene ug/L ND 10.0 07/13/16 13:530.22 Phenol ug/L ND 10.0 07/13/16 13:531.7 Pyrene ug/L ND 10.0 07/13/16 13:530.19 2,4,6-Tribromophenol (S)%88 27-110 07/13/16 13:53 2-Fluorobiphenyl (S)%79 27-110 07/13/16 13:53 2-Fluorophenol (S)%47 12-110 07/13/16 13:53 Nitrobenzene-d5 (S)%88 21-110 07/13/16 13:53 Phenol-d6 (S)%35 10-110 07/13/16 13:53 Terphenyl-d14 (S)%110 31-107 S307/13/16 13:53 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1778413LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/L 31.250 62 31-120 1,2-Dichlorobenzene ug/L 33.750 67 38-120 1,3-Dichlorobenzene ug/L 30.550 61 30-122 1,4-Dichlorobenzene ug/L 31.050 62 37-120 1-Methylnaphthalene ug/L 47.150 94 34-113 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 55 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1778413LABORATORY CONTROL SAMPLE: LCSSpike 2,2'-Oxybis(1-chloropropane)ug/L 56.450 113 18-120 2,4,5-Trichlorophenol ug/L 48.250 96 43-113 2,4,6-Trichlorophenol ug/L 46.750 93 42-120 2,4-Dichlorophenol ug/L 50.550 101 30-120 2,4-Dimethylphenol ug/L 49.150 98 29-111 2,4-Dinitrophenol ug/L 187250 75 19-132 2,4-Dinitrotoluene ug/L 55.150 110 58-128 2,6-Dinitrotoluene ug/L 55.850 112 54-129 2-Chloronaphthalene ug/L 44.150 88 43-117 2-Chlorophenol ug/L 48.350 97 37-120 2-Methylnaphthalene ug/L 46.350 93 33-120 2-Methylphenol(o-Cresol)ug/L 50.450 101 31-120 2-Nitroaniline ug/L 107100 107 48-121 2-Nitrophenol ug/L 45.350 91 25-116 3&4-Methylphenol(m&p Cresol)ug/L 46.950 94 23-120 3,3'-Dichlorobenzidine ug/L 109100 109 10-154 3-Nitroaniline ug/L 106100 106 43-115 4,6-Dinitro-2-methylphenol ug/L 108100 108 44-124 4-Bromophenylphenyl ether ug/L 45.050 90 34-113 4-Chloro-3-methylphenol ug/L 117 L0100117 31-110 4-Chloroaniline ug/L 106100 106 20-120 4-Chlorophenylphenyl ether ug/L 46.750 93 34-116 4-Nitroaniline ug/L 108100 108 46-128 4-Nitrophenol ug/L 130250 52 11-120 Acenaphthene ug/L 43.850 88 48-114 Acenaphthylene ug/L 45.250 90 48-112 Aniline ug/L 45.550 91 26-120 Anthracene ug/L 45.550 91 57-118 Benzo(a)anthracene ug/L 47.350 95 56-121 Benzo(a)pyrene ug/L 46.450 93 55-127 Benzo(b)fluoranthene ug/L 47.250 94 53-128 Benzo(g,h,i)perylene ug/L 47.750 95 54-125 Benzo(k)fluoranthene ug/L 45.050 90 51-123 Benzoic Acid ug/L 107250 43 10-120 Benzyl alcohol ug/L 121 L0100121 27-120 bis(2-Chloroethoxy)methane ug/L 50.250 100 32-120 bis(2-Chloroethyl) ether ug/L 49.350 99 33-111 bis(2-Ethylhexyl)phthalate ug/L 53.950 108 50-145 Butylbenzylphthalate ug/L 55.750 111 54-138 Chrysene ug/L 45.850 92 58-127 Di-n-butylphthalate ug/L 51.450 103 56-125 Di-n-octylphthalate ug/L 50.550 101 50-134 Dibenz(a,h)anthracene ug/L 46.150 92 53-129 Dibenzofuran ug/L 49.150 98 45-120 Diethylphthalate ug/L 49.250 98 53-120 Dimethylphthalate ug/L 48.350 97 55-116 Fluoranthene ug/L 49.050 98 57-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 56 of 61 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1778413LABORATORY CONTROL SAMPLE: LCSSpike Fluorene ug/L 48.050 96 53-118 Hexachloro-1,3-butadiene ug/L 26.150 52 23-120 Hexachlorobenzene ug/L 41.250 82 49-116 Hexachlorocyclopentadiene ug/L 26.750 53 26-158 Hexachloroethane ug/L 29.550 59 30-114 Indeno(1,2,3-cd)pyrene ug/L 46.450 93 55-128 Isophorone ug/L 57.950 116 31-118 N-Nitroso-di-n-propylamine ug/L 76.2 L050152 32-119 N-Nitrosodimethylamine ug/L 23.450 47 13-120 N-Nitrosodiphenylamine ug/L 46.850 94 43-120 Naphthalene ug/L 38.850 78 32-120 Nitrobenzene ug/L 48.250 96 33-110 Pentachlorophenol ug/L 101100 101 10-137 Phenanthrene ug/L 45.050 90 57-117 Phenol ug/L 28.950 58 10-120 Pyrene ug/L 46.350 93 55-122 2,4,6-Tribromophenol (S)%92 27-110 2-Fluorobiphenyl (S)%79 27-110 2-Fluorophenol (S)%54 12-110 Nitrobenzene-d5 (S)%92 21-110 Phenol-d6 (S)%48 10-110 Terphenyl-d14 (S)%97 31-107 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 57 of 61 #=QL# QUALIFIERS Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.L3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples.Results unaffected by high bias.S3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 58 of 61 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92304618 UNIVERSITY FORD 1272C Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92304618001 321102 321285MW-4 EPA 3010A EPA 6010 92304618002 321102 321285MW-5 EPA 3010A EPA 6010 92304618003 321102 321285MW-15 EPA 3010A EPA 6010 92304618004 321102 321285MW-8 EPA 3010A EPA 6010 92304618005 321102 321285MW-10 EPA 3010A EPA 6010 92304618006 321102 321285MW-2 EPA 3010A EPA 6010 92304618007 321102 321285MW-1 EPA 3010A EPA 6010 92304618008 321102 321285MW-14 EPA 3010A EPA 6010 92304618009 321102 321285MW-3 EPA 3010A EPA 6010 92304618010 321102 321285MW-6 EPA 3010A EPA 6010 92304618001 321121 321300MW-4 EPA 7470 EPA 7470 92304618002 321121 321300MW-5 EPA 7470 EPA 7470 92304618003 321121 321300MW-15 EPA 7470 EPA 7470 92304618004 321121 321300MW-8 EPA 7470 EPA 7470 92304618005 321121 321300MW-10 EPA 7470 EPA 7470 92304618006 321121 321300MW-2 EPA 7470 EPA 7470 92304618007 321121 321300MW-1 EPA 7470 EPA 7470 92304618008 321121 321300MW-14 EPA 7470 EPA 7470 92304618009 321121 321300MW-3 EPA 7470 EPA 7470 92304618010 321121 321300MW-6 EPA 7470 EPA 7470 92304618001 320942 321137MW-4 EPA 3510 EPA 8270 92304618002 320942 321137MW-5 EPA 3510 EPA 8270 92304618003 320942 321137MW-15 EPA 3510 EPA 8270 92304618004 320942 321137MW-8 EPA 3510 EPA 8270 92304618005 320942 321137MW-10 EPA 3510 EPA 8270 92304618006 320942 321137MW-2 EPA 3510 EPA 8270 92304618007 320942 321137MW-1 EPA 3510 EPA 8270 92304618008 320942 321137MW-14 EPA 3510 EPA 8270 92304618009 320942 321137MW-3 EPA 3510 EPA 8270 92304618010 320942 321137MW-6 EPA 3510 EPA 8270 92304618001 321049MW-4 EPA 8260 92304618002 321049MW-5 EPA 8260 92304618003 321049MW-15 EPA 8260 92304618004 321049MW-8 EPA 8260 92304618005 321049MW-10 EPA 8260 92304618006 321049MW-2 EPA 8260 92304618007 321049MW-1 EPA 8260 92304618008 321049MW-14 EPA 8260 92304618009 321049MW-3 EPA 8260 92304618010 321049MW-6 EPA 8260 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 08/02/2016 12:44 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 59 of 61 Page 60 of 61 Document Name: Document Revised:April 25, 2016 ~:::ZeAnalytica!" Sample Condition Upon Receipt(SCUR) Page 1 of 2 I····· i ' Sample Condition Upon Receipt Courier: D Commercial Client Name: QFe~x @Pace OuPs Document No.: F·CHR·CS-003-rev.19 Project · OusPs Oclient Oother: __ - Issuing Authority: Pace Huntersville Quality Office Page 2 of 2 for Internal Use ONLY W0#·92304618 1111111111111111111.111 __ 92304618 D~ Seals Intact? tE~ 0No t..w /" Date/Initials Person Examining Contents:'l • \d, -\ l O Custody Seal Present? O ves Packing Material: 0Bubble Wrap []BGbble Bags 0None / Oother: __ Thermometer: TlSOS Type of Ice: ~Wet 0Blue 0 None ~es on ice, cooling process_h~n Correction Factor: o.o·c Cooler Temp Corrected (°C): 3 . ll> Biological Tissue Frozen? Oves 0No '{ZJN/A Temp should be above freezi_!)g-to 6°C USDA Regulated Soil ( [}N7A, water sample) Did samples ~ate· in a quarantine zone within the United States: CA, NY, or SC (check maps)? Oves fil. including Hawaii and Puerto Rico)? 0 Yes Qo Did samples originate from a foreign source (inter~ally, Chain of Custody Present? Samples Arrived within Hold Time? Short Hold Time Analysis (<72 hr.)? Rush Turn Around Time Requested? Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers Intact? Samples Field Filtered? Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: ~!:l\ All containers needing acid/base preservation have been che_cked?_ ------------- All containers needing preservation are found to be in compliance with EPA recommendation? (HN03, H2S04, HCl<2; NaOH >9 Sulfide, NaOH>12 Cyanide) Exceptions: VOA, Coliform, TOC, Oil and Grease, DR0/8015 (water) DOC,LLHg Samples checked for dechlorination? Headspace in VOA Vials (>5-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? Pace Trip Blank Lot # (if purchased}: CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: - ~s Dves O ves O ves g,re; [\4.(s' h°'b'(s"" ~ 0Yes CJ~ D~ mfu O ves n (e; 0Yes Oves Oves Comments/Discrepancy: 0No ON/A 1. n~ ON/A 2 . .Qfifo ON/A 3. iuN{ ON/A 4. 0No ON/A 5. 0No ON/A 6. 0 No ON/A 0No ON/A 7. 0No DN1A 8. Note if sediment is visible in the dissolved container 0No ON/A 9. 10. HNC3 pH<2 QNo [JN/A--. HC pH<2 H2504 pH<2 0No ON/A N1oti pH>l2 0No nNt)'\ NaOH/ZnOAc pH>9 0 No ON/A 11. 0N6 ON/A 12. 0No g ~ 13. 0No G:IN1A Field Data Required? O ves 0No Date/Time: Project Manager SCURF Review: @ Date: ____ 1_(;.../,_3..,_ ____ _ Project Manager SRF Review: :f0 Date: ) f 11; -· Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 61 of 61 ~ Pace Analytical www.pacelabs.com - ~ \ Y ¥ A ~ C H A I N - O F - C U S T O D Y I A n a l y t i c a l R e q u e s t D o c u m e n t T h e C h a i n - o f - C u s t o d y i s a L E G A L D O C U M E N T . A l l r e l e v a n t f i e l d s m u s t b e c o m p l e t e d a c c u r a t e l y . Section A S e c t i o n B S e c t i o n C P a g e : o f Required Client lnformalion: R e q u i r e d P r o j e c t I n f o r m a t i o n : Company: A I) 1 , c:;:. 1 , 1.-, { I R e p o r t T o : ( ' r y / l I I I A l t e n t i o n : - . _ +-lAVlh (. v_""O'"°" i;;..,v.,;,._....,,, I A - < ! / V \ O O c ' [ _ _ . . . , , . . ~ 4 0 I n v o i c e I n f o r m a t i o n : ( , ; , , ~ i _ . i . . . . . J . c . 2 0 5 6 1 7 8 Address: • . f> ..-1 I C o p y T o : 1 \ • 1 c o m p a n y N a m e · ___ /(,__'-l l.)1<(kl-o-'-,'d. ( $ v - J < . < . ' . A @ t , ~ l , , . . . 1 - t ~ ' < _ l i ' ' ) V - £ c , . . . . . . _ . I R E G U L A T O R Y A G E N C Y <'lt,,,J I, l -'\J · A d d r e s s : Email To:(IVll)C<±,/id a 1-l~.., \_. 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P a c e P r o 1 c c t ~ ~ ~ ~ ~ e r : P a c e P r o f i l e # ' S i t e L o c a t i o n S T A T E : J y _ ( . , R e q u e s t e d A n a l y s i s F i l t e r e d ( Y / N ) .. ::;; w !:: 1 2 3 4 5 6 7 8 9 10 11 12 Section O Required Client Information SAMPLE ID (A-Z,0-9/ ,-) Sample IDs MUST BE UNIQUE .,M v-.l-lo /\,{.1,0 -l fa\ \,V ' \ I M.vJ-l~ MIJJ-.!V\.vJ-ADDITIONAL COMMENTS I Matrix C o d e s " ' i i : ' - z MATRIX I C O D E m : : ; : C O L L E C T E D P r e s e N a l i v e s > Drinking Wat e r Water Waste Water Product Soil/Solid Oil Wipe Air Tissue Other ! ) 0 D W ( . ) W T " z 0 j ( . ) W W - 0 r o p ~ £ 2 C O M P O S I T E S T A R T C O M P O S I T E E N D / G R A B ; : : ( . ) w S L m C l m O L . ! ' ! . " C l W P - A R w a w T S 0 a . O T l . ) ~ x w ~ . . . J a . I - : : ; : < ( < ( z e n D A T E T I M E D A T E . . . J . . . J 0 ( / ) ( . ) a : : I - w < ( z a . ~ : : ; : w z I - w 0 . . . J l . ) a . u . : : ; : 0 < ( T I M E I e n . . - 0 Q ) ~ Q ) t " ' ) 0 < I ) . . , . 0 c : : e o M : r : ( / ) ~ J ; ; ; a . < n O - o N - . c c " ' Z U r o r c a > - : : : > : r : : r : : r : z z 2 0 - ~ ~ . . . ~ j , : : , p ' 1 : . l 1 l . . s c : : - ~ ~ ~ - < . ; d - - w T l : , ' X l x 7 1 X r ~ ' 1 ' t l 1 J f ~ ~ I 1 7 l · t 1 1 ' J ~ [ x i ) ( ' . ' ! " ) . _ I x . I · x 1 1 Y . H 3 o - i i . \ ' { } - 0 J 5 a o x _ i x i J s x i ; 3 - i H ~ O i ~ l o " i i ' ) Q i l i J " y ' j ' ) < - i _ l ~ I J , ~ 3 ; J l - ~ ~ ~ ; - 1 I J I J 1 1 1 ~ 1 J f i l I X l i J ' J R E L I N Q U I S H E D B Y I A F F I L I A T I O N ~ ~ Z , / A : 5 c , " l i } w f V i d - f ~ 7 / J J / I ~ I ! b J t ; . I [ ~ V W / f 1 . r - 0 - ~ D A T E I T I M E I i f / A ; C C E P T F J ! _ f , Y I ~ F F I L ~ T I O N 1 1 , , , 1 , , _ ~ l t l P ~ 5 L t : ; : ~ ~ / ~ , h l " . 7 - ) ) . ) - 6 I , z . L J - s . k [ - Q " l , j y \ ' " ) _ _ Q Q C I Q _ l l r ' l ~ Z / A c . b \ S A M P L E R N A M E A N D S I G N A T U R E P R I N T N a m e o f S A M P L E R : t / { ~ o j - ~ ( ; . : r s O R I G I I \ J A L S I G N A T U R E o f S A M P L E R : U ( _ / / t v z : L - D A T E S i g n e d ( M M / D D / Y Y ) : ·1rnporiant Note: By signing lhtS form you arc acccpt m g P a c e ' s N E T 3 0 d a y p a y m e n t t e r m s ~ n d a g r e e i n g t o l a t e c h a r g e s o r 1 . 5 % p e r m o n l h f o r a n y 1 1 w o 1 c c s n o t p a i d w i t h i n 3 0 d a y s . D A T E T I M E 1 L f 1 _ [ { 1 ; f l b W 1 1 / / ) / b ~ J O z ~ Q ) . ! : 0 : c u r n : : : , - 0 · ; : ; ; Q ) 0 : : P a c e P r o j e c t N o . / L a b I . D . S A M P L E C O N D I T I O N S · n ' - l ~ I I r 1 J 1 ~ J 3 ~ _ J ' - I I ~ I ' - - - \ 0 7 / / 1 / / I > ; - ' · ' = a . E ~ c : o - - 0 z ~ E · w ( 1 ) u u < l > - a : : ' " > - 0 " 0 - 0 ( . ) Z i i i " O 3 : : , . , _ u ' " . , U ) F - A L L - Q - 0 2 0 r e v . 0 7 . 1 5 - M a y - 2 0 0 7 u r o c i ~ - > - a . - E r o e n Report of Limited Phase II Environmental Site Assessment August 8, 2016 University Ford/Kia, 601Willard Street and 600 Julian Carr Street Durham, North Carolina ASE Project No. 1272C MATERIAL DISPOSAL MANIFESTS THIS IS NOT AN INVOICE FOR EMERGENCY RESPONSE: Call: CHEMTREC for Spill, Leak, Accident 1-800-424-9300 24 HRS. PER DAY, 7 DAYS PER WEEK .NQ"~· Document No. 13 3 Q 1 Q 1 1-800-662-5364 5617 CLYDE RHYNE DR. SANFORD, NC 27330 EPA ID# NCO 986172476 DATE l-a1...-I ~ GENERATOR CUSTOMER ADDRESS CITY DURHAtvl CONTACT SHERYL MOODY STATE NC SERVICE RECEIPT BILLING CUSTOMER ADDRESS Zl~7701 CITY CONTACT PHONE xt. EPAID# PHONE START-TIME: -STOPTIME: \:lZlu PO# COUNTY Region: NC O PARTS WASHER SERVICE O FILTER BIN SERVICE INDUSTRIAL SERVICES HM US DOT Description MATERIAL Seivlce PROFILE# Quentltv UHd 011 end Wlt•r Mlxtur•, Non-Regulated Met•r111 Oii/Water Mix, Bulk· 52 WIICell Petroleum Contemlneted Solids, not USDOT or RCRA Regulated Sludge, Bulk • 52 '\NlllCall 07trJ) ()JC-J) Cl,!ST ID# Work order I AJD160 1202741 STATE NC TRUCK~Q ZONE O RECOVERY SERVICES ~Rle TOTAL $ Service Charge IS. 52 WIICall L~~) $180.00 SC-2 Minimum Charge IS· 52 VVlllCall ~~ s. ~ d.Ja.... t>\.,.+ fv<' e.. ll we,,. \J. vJ o.frtN'" ~v-+o ?.w. Method of Payment Credit Card I Check I Cash I PO Amount Recd Total Qty: t--~~--~~~~--Subtotal 13 i------------1 c i r c I e one $ Sales Tax NOBLE OIL EPA ID#: NCD9861-72476 Service Charge i-,--------1 TOTAL DUE$ ......_ ______ _. 7~~j~""~ Generator Certification and Indemnification: I, the generator of the materials Identified above, certify that these materials are accuralely and fully characterized, described, classified, packaged, marked and labeled and are in the proper condition for transporl in compliance with applicable Slate, U.S. EPA and U.S. Department of Transportation (DOD regulations. I, the generator, also hereby certify, warrant and represent to Noble Oil Services, Inc., wilh lhe exception ol properly identilied and manifested Toxic Substance and Conlrol Act (TSCA) and Resource Conservation and Recovery Act (RCRA) materials, that (1) the material, described above, contains no quantifiable concentration of polychlorinated biphenyls (PCBs) nor any hazardous waste as defined by RCRA; and (2) accurate laboratory testing for this shipmen! has been provided to Noble Oil Services, Inc. to verify that this shipment contains no quantifiable concentralion of PCBs nor any waste as defined by RCRA. In lhe event that this certification Is inaccurate, I, the generator, will indemnify Noble Oil Services, Inc. and promptly pay for costs directly or indirectly resulting from this inaccurale certification including, but not limited lo, contaminated (including co-mingled) product or inventory, proper storage, shipmen! and disposal, sampling, testing, decontamination, attorneys fees, expert witness fees, penalties, fines and court costs. Oil Screen Test: D Positive O Negative Order Type Order FACILITY COPY/ORIUlhJAL