9214_HollySpringsCDLF_OakviewElementaryVIReport_DIN26680_20160725

3500 Gateway Centre Blvd. Suite 200, Morrisville, NC 27560 p | 919.755.5011 f | 919.755.1414

July 25, 2016
File No. 20160086.001A| RAL16R41635

Jaclynne Drummond Via e-mail: [e-mail]
Compliance Hydrogeologist
Division of Waste Management - Solid Waste Section
NC Department of Environmental Quality
Asheville Regional Office
2090 US Highway 70
Swannanoa, NC 28778

Reference: Limited Vapor Intrusion Assessment
Wake County Public Schools System
Oakview Elementary School Site
Holly Springs New Hill Road
Holly Springs, NC

Dear Ms. Drummond:

Kleinfelder has completed a Limited Vapor Intrusion Assessment of the referenced Site and is
submitting this report for your review. We understand that as the agency staff member responsible
for the oversight of the adjacent closed landfill, Holly Springs C&D Landfill 9214-CDLF-1993, that
you are the appropriate person to receive this report.

Should you have questions or require additional information regarding this project, please do not
hesitate to contact me.

Sincerely,
KLEINFELDER, INC.
Firm License No. F-1312

Michael A. Sussman, PE
Principal Engineer

Enclosure

3500 Gateway Centre Blvd. Suite 200, Morrisville, NC 27560 p | 919.755.5011 f | 919.755.1414

June 10, 2016
File No. 20160086.001A| RAL16R41635

Mr. Micheal Lynch
Senior Project Manager
Wake County Public School System
1429 Rock Quarry Road | Suite 116
Raleigh, NC 27610

Reference: Limited Vapor Intrusion Assessment
Wake County Public Schools System
Oakview Elementary School Site
Holly Springs New Hill Road
Holly Springs, NC

Dear Mr. Lynch:

Kleinfelder has completed the Limited Vapor Intrusion Assessment of the referenced Site.

Kleinfelder appreciates the opportunity to be of service to you. Should you have questions or
require additional information regarding this project, please do not hesitate to contact the
undersigned.

Sincerely,
KLEINFELDER, INC.
Firm License No. F-1312

Michael A. Sussman, PE
Principal Engineer

Michael J. Burns, PG
Environmental Program Manager

MAS/MJB:cas
Enclosure

LIMITED VAPOR INTRUSION ASSESSMENT
WAKE COUNTY PUBLIC SCHOOLS SYSTEM
OAKVIEW ELEMENTARY SCHOOL SITE
HOLLY SPRINGS NEW HILL ROAD
HOLLY SPRINGS, NC

KLEINFELDER PROJECT NO. 20160086.001A

JUNE 10, 2016

Copyright 2016 Kleinfelder
All Rights Reserved

ONLY THE CLIENT OR ITS DESIGNATED REPRESENTATIVES MAY USE THIS DOCUMENT AND ONLY FOR THE SPECIFIC
PROJECT FOR WHICH THIS REPORT WAS PREPARED.

20160086.001A | RAL16R41635 Page i June 10, 2016
© 2016 Kleinfelder

A Report Prepared for:

Mr. Micheal Lynch
Senior Project Manager
Wake County Public School System
1429 Rock Quarry Road | Suite 116
Raleigh, North Carolina 27610

LIMITED VAPOR INTRUSION ASSESSMENT
WAKE COUNTY PUBLIC SCHOOLS SYSTEM
OAKVIEW ELEMENTARY SCHOOL SITE
HOLLY SPRINGS NEW HILL ROAD
HOLLY SPRINGS, NC

Prepared by:

Michael A. Sussman, PE
Principal Engineer

Reviewed by:

Michael J. Burns, PG
Environmental Program Manager

KLEINFELDER
3500 Gateway Centre Blvd. Suite 200
Morrisville, NC 27560

P | 919.755.5011
F | 919.755.1414

June 10, 2016
20160086.001A

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© 2016 Kleinfelder
TABLE OF CONTENTS

EXECUTIVE SUMMARY ........................................................................................................... 1
1 GENERAL INFORMATION ............................................................................................ 3
1.1 SITE INFORMATION .......................................................................................... 3
1.2 SITE HISTORY ................................................................................................... 3
2 SITE GEOLOGY AND HYDROGEOLOGY ..................................................................... 4
3 LIMITED VAPOR INTRUSION ASSESSMENT .............................................................. 5
3.1 VAPOR PROBE INSTALLATION ........................................................................ 5
3.2 SOIL VAPOR SAMPLING ................................................................................... 6
3.2.1 Vapor sampling apparatus ....................................................................... 6
3.2.2 Sampling apparatus leak detection .......................................................... 6
3.2.3 Vapor Probe Purging ............................................................................... 7
3.2.4 Vapor Probe Monitoring ........................................................................... 7
3.2.5 Vapor Probe Sampling ............................................................................ 8
3.3 Sub-Slab Vapor Point Installation ................................................................... 8
3.4 SUB-SLAB VAPOR SAMPLING .................................................................... 9
3.4.1 Vapor Sampling Apparatus ................................................................... 9
3.4.2 Sampling Apparatus Leak Detection ...................................................... 9
3.4.3 Vapor Probe Purging ....................................................................... 10
3.4.4 Vapor Probe Monitoring ................................................................... 10
3.4.5 Vapor Probe Sampling........................................................................ 11
3.5 SOIL AND GROUNDWATER SAMPLING POINT INSTALLATION ...................11
3.5.1 Drilling .............................................................................................. 11
3.5.2 Field Screening of Soil ..................................................................... 12
3.5.3 Field Screening of Groundwater ........................................................ 12
3.6 SOIL AND GROUNDWATER SAMPLING .........................................................12
3.6.1 Soil Sampling .................................................................................. 12
3.6.2 Groundwater Grab Sampling ............................................................... 13
4 RESULTS ............................................................................................................ 14
4.1 DATA STANDARDS ................................................................................... 14
4.2 SAMPLE RESULTS ................................................................................... 16
4.2.1 Soil Vapor Sampling Results ............................................................ 16
4.2.2 Sub-Slab Vapor Sampling Results..........................................................17
4.2.3 Soil and Groundwater Sampling Results ............................................ 18
5 CONCLUSIONS ................................................................................................... 19
6 LIMITATIONS ....................................................................................................... 20
REFERENCES .........................................................................................................................21

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FIGURES

Figure 1 Site Location Map
Figure 2 Soil Gas Fixed Gas Sample Results Map
Figure 3 Soil Gas VOC Sample Results Map
Figure 4 Soil Gas Isotopic Analysis Results
Figure 5 Indoor Vapor Sampling Point Location Map
Figure 6 Soil and Groundwater Sampling Locations

APPENDICES

Appendix A Data Tables
Appendix B Laboratory Data
Appendix C Sample Probe Construction Records
Appendix D Field Data
Appendix E Building Construction Details
Appendix F Sub-Slab Vapor Sampling NCDEQ Approval

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EXECUTIVE SUMMARY

This report has been prepared to present the investigation activities undertaken to evaluate soil
vapor concerns at Wake County Public Schools E-43 (Oakview Elementary) School Site located
in Holly Springs, NC.

Soil vapors were encountered during the routine installation of the underground sewer line in a
deep trench (30 feet below grade) at the Site giving rise to worker safety concerns and concerns
over potential for vapor intrusion. The vapors were encountered approximately 350 feet from the
new school building footprint. The Site is adjacent to a closed landfill.

Soil vapor sampling was performed in January and February 2016, including areas near the sewer
line, the adjacent landfill and the school building footprint. In the soil vapor samples: hydrogen
sulfide was not detected; methane was detected at concentrations exceeding the lower explosive
limit in samples collected within 200 feet of the building footprint; and volatile organic compounds
were detected widely across the Site at concentrations above the North Carolina residential soil
gas screening levels and in one case above the commercial soil gas screening level. Isotopic
analysis indicates the methane is most likely from near surface decomposition of organic material
rather than from a natural gas source.

No pressure differential was observed between the atmospheric pressure and the probe pressure
indicating there is not currently a pressure gradient that would drive vapors into the building.
Based on the building construction, the commercial soil gas screening levels (SGSLs) may be
most appropriate for this structure; however, the North Carolina Department of Environmental
Quality (NCDEQ) guidance indicates that due to the use of the structure as a school the residential
standard should apply.

The NCDEQ DWM guidance states, “When sample results exceed the screening levels, additional
evaluation, assessment or mitigation are warranted. However, if any individual sampling result
exceeds the screening level that does not mean VI [vapor intrusion] will pose an unacceptable
health risk. Sample results can be expected to be variable spatially and temporally, and the DWM
screening levels are very conservative and assume a long period of exposure at that level.”

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To further evaluate the potential for vapor intrusion risk at the Site. Sub-slab vapor sampling was
performed on April 6, 2016, which included nine sampling locations in the school building footprint.
Volatile organic compounds were detected under the building slab; however, the concentrations
did not exceed North Carolina residential sub-slab gas screening levels or commercial sub-slab
gas screening levels. Methane concentrations were not detected above the action level or lower
explosive limit.

Soil sampling was performed in March 2016, which included ten soil grab samples located
throughout the Site and five soil composite samples of the stockpiles at the multi-purpose field.
Volatile organic compounds were detected across the Site from the soil grab samples; however,
the concentrations did not exceed the NCDEQ’s Soil-to-Groundwater MSCCs and the NCDEQ’s
RSCLs. Volatile organic compounds were detected in two of the stockpile samples exceeded the
NCDEQ’s Soil-to-Groundwater Maximum Soil Contamination Concentrations and the NCDEQ’s
Residential Maximum Contaminant Concentrations. The concentrations detected were methylene
chloride, a common laboratory contaminant. It is Kleinfelder’s opinion that the methylene chloride
detected is a laboratory artifact and not representative of actual Site conditions.

Three of the soil sampling locations were converted to temporary monitoring wells to facilitate the
collection of groundwater samples in areas with the highest soil gas concentrations. Groundwater
sampling was conducted in May 2016. The groundwater results did not indicate volatile organic
compounds that exceed the NCDEQ, 15A NCAC 02L Groundwater Standards.

In summary, soil vapor sampling around the site detected methane and volatile organic
compounds at concentrations above screening levels. Subsequent sub-slab vapor sampling
under the building footprint detected volatile organic compounds and methane; however, the
concentrations did not exceed the screening levels. The NCDEQ DWM guidance on the matter
states that “DWM prefers the collection of sub-slab over near slab soil gas samples,” and
furthermore states that, “if soil gas concentrations do not exceed the SGSLs, typically no further
investigation is necessary….” Kleinfelder is requesting that based on the results to date, the DWM
make a determination that further investigation or remedial action is not required at this time.

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1 GENERAL INFORMATION

1.1 SITE INFORMATION
The Site is located at on Holly Springs New Hill Road in Holly Springs, North Carolina (Figure 1).
The Site consists of one tax parcel (Wake County Parcel Identification Number 0639958908)
which has an area of 23.11 acres (hereafter referred to as the “property” or “Site”) and is currently
owned by Wake County Public School System (WCPSS).

1.2 SITE HISTORY
Wake County Public Schools, is currently constructing Oakview Elementary School on the subject
property. The parcel is adjacent to the closed Holly Springs Landfill 9214-CDLF-1993.

A Phase I ESA completed by Mid-Atlantic Associates (MAA May 9, 2014) stated that the property
consisted of wooded and cleared land with residential structures and that the subject Site appears
to have been wooded and agricultural land back to at least 1959. The Phase I ESA identified one
Recognized Environmental Condition (REC) at the property: the presence of a closed construction
and debris landfill adjacent to the northeast.

Soil vapors were encountered during the installation of an underground sewer line near the
northern boundary of the Site. Based on discussions with Site personnel, there were no elevated
concentrations of vapors noted during the sewer line excavation until rock blasting was performed.
The area where the rock blasting was performed is about 200 feet from the adjacent closed
landfill. An evaluation was performed of the air in excavations at the Site on September 8 and
17, 2015 and included measuring organic vapor concentrations using a photoionization detector
(PID), oxygen, carbon dioxide (CO2), carbon monoxide (CO), flammable vapors (as percent lower
explosive limit (% LEL) calibrated on methane), hydrogen sulfide, and methane. Air screening
indicated the presence of subsurface CO between 82 to 171 parts per million (ppm), hydrogen
sulfide between 0 to 2.2 ppm, methane between 0 to 8% LEL, and depleted oxygen across the
test pits. Later sampling completed in January and February 2016 determined that the elevated
concentrations of CO, hydrogen sulfide, and methane observed in the excavations during the
September 2015 sampling appeared to have been transient and were not still present.

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2 SITE GEOLOGY AND HYDROGEOLOGY

According to the Geologic Map of North Carolina (Brown, 1985), the Site is located in the Triassic
Basin of the Piedmont physiographic province, just to the west of the Raleigh Belt. The regional
geology consists of Triassic age consolidated sediments of the Sanford Formation. During
subsurface assessment activities, a Kleinfelder licensed geologist noted that the soil appeared to
be related to the weathering of arkosic sandstone and mudstone. Surface remnants observed
after the blasting activities in the northeast portion of the Site appeared to indicate the presence
of arkosic conglomerate. Competent bedrock was encountered onsite from 10 to 30 feet below
ground surface (bgs).

The United States Geological Survey (USGS) Green Level Quadrangle Topographic Map
indicates the direction of groundwater flow to be either to the west-northwest or north-northeast
based on the location onsite. Groundwater levels appear to be highly variable based on rainfall
with recent groundwater levels of between 5 and 15 feet bgs.

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3 LIMITED VAPOR INTRUSION ASSESSMENT

3.1 VAPOR PROBE INSTALLATION
Soil vapor sampling probes were installed in general accordance with the North Carolina
Department of Environmental Quality (NCDEQ) Division of Waste Management (DWM), “Vapor
Intrusion Guidance (April 2014)” and the NCDEQ Inactive Hazardous Sites Branch (IHSB),
“Supplemental Guidelines for the Evaluation of Structural Vapor Intrusion Potential for Site
Assessments and Remedial Actions. (March 2014)”. These are collectively called the NCDEQ
Guidance in the rest of this report. Kleinfelder generally followed this guidance although the
current Site is not within the regulatory oversight of the DWM or IHSB.

For unimproved property located within 500 feet of the waste footprint of a landfill, the IHSB
guidance suggests soil gas samples should be collected at depths between five and ten feet bgs
and if subsurface vapor pathways exist, soil gas samples should be collected at various intervals
between five feet bgs and the depth of the base of the landfill waste.

To evaluate the potential for vapor intrusion from the landfill (initially presumed source) into the
utility trench and to the proposed school building, Kleinfelder installed soil vapor sample probes
at 16 locations at the Site (see Figures 2 and 3). Kleinfelder attempted to install probes at the
depth of the base of the landfill waste (approximately 70 feet bgs); however, seasonally elevated
groundwater was encountered at a depth of approximately 10 to 15 feet bgs. This limited the
installation of vapor sampling probes to the 5 to 10 feet bgs interval.

On January 18-19 and February 2-3, 2016, soil vapor sampling probes were installed to
approximately 5 or 10 feet bgs by Quantex Drilling and Probing. The sample probes were installed
using a Geoprobe® DPT rig equipped with 2-inch diameter stainless steel Macro-core® rods. The
Macro-core® rods were decontaminated prior to being brought to the Site. Three soil vapor
sampling probes (SV-13, SV-15, and SV-16) were installed to approximately 5 feet bgs using a
hand auger due to limited access.

The soil vapor probes were constructed as follows. Once the soil boring was completed, sand
was be placed in the bottom of the boring and a stainless steel sample probe connected to Teflon
tubing with Swageloks compression fittings was installed. The boring was then backfilled with

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approximately one foot of sand, followed with approximately one half foot of dry bentonite, and
capped with Type I/II Portland cement seal to the ground surface. All backfill and seal materials
were placed with a tremie to reduce bridging. The location of vapor probes is shown on Figures
2 and 3. Copies of the sample probe construction records are included as Appendix C.

3.2 SOIL VAPOR SAMPLING
Soil vapor sampling methods, including shut-in tests, tracer gas testing, vapor purging, and soil
vapor sample collection, were performed consistent with the NCDEQ Guidance. Field data sheets
documenting the activities are provided in Appendix D.

3.2.1 Vapor sampling apparatus
To collect samples, the vapor probe tubing was connected to a sampling manifold which included
two pressure gauges, a flow controller and a series of valves which allows the vapor probe to be
purged, monitored, and sampled without allowing ambient air to enter the connections or requiring
disturbing the shroud used for leak testing, see photos in Appendix D. Samples were collected in
laboratory evacuated one-liter Summa canisters. The summa canisters and sampling manifolds
were pre-cleaned and batch certified as clean, and provided by Eurofins Air Toxics Inc. The flow
regulator on the canister was set at 0.2 liters per minute (L/Min) by the laboratory.

3.2.2 Sampling apparatus leak detection

Prior to mobilization, a shut-in test was performed on the sampling apparatus (canister and
manifold) to check for leaks in the fittings of each sample train. The shut-in test consisted of
assembling the Summa canister, flow controller, and sampling manifold, and then sealing the
“probe” connection point of the manifold with a brass cap and ensuring the purge valve of the
manifold was closed. The canister valve was then opened exposing the sampling train to the
canister vacuum. The canister vacuum gauge was observed for at least one minute. If there was
a noticeably loss of vacuum, the sampling train (canister and manifold) failed the shut-in test and
was not used.

Consistent with the NCDEQ Guidance, during purging and sampling of each soil vapor probe, a
tracer gas test was performed to evaluate and validate sample integrity. A plastic shroud was
placed over the entire sampling train and the soil vapor probe tubing connection at ground surface.

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A laboratory grade helium tracer gas was introduced into the shroud. The concentration of helium
under the shroud was measured with a Dielectric Model MGD-2002 Helium Detector. The helium
concentration under the shroud was maintained at a minimum of 10 percent during the purging
and sampling. At the conclusion of the purging, a sample of the purged soil vapor was collected
in a Tedlar bag and screened for percentage of helium. If the screened sample contained less
than 5% of the helium concentration within the shroud, then the sample flow train integrity was
considered adequate and within an acceptable range. If the screened sample contained more
than five percent of the helium concentration within the shroud then the equipment was inspected,
adjusted, and purged again.

The final samples were also analyzed for helium concentration by the laboratory to verify the
integrity of the sample. The helium tracer gas concentrations in the SV-10 sample were measured
by the laboratory above 5% of the concentration within the shroud during sampling, this indicates
that there was a vapor connection between the surface and the soil vapor probe and therefore
the data from this point is of limited value. Concentrations of helium in the remaining samples
were below 5% of the helium concentration in the shroud for each of those points indicating a
competent seal was achieved between the surface and the soil vapor probe.

3.2.3 Vapor Probe Purging
Prior to monitoring or sampling each soil vapor probe an SKC pump calibrated to 200 ml/minute
was connected to the tubing or manifold to purge the probe and tubing. The vapor probe and
tubing were purged by removing three volumes of air (see calculations in Appendix D).

3.2.4 Vapor Probe Monitoring
At least 24 hours after probe construction, each vapor probe was purged. After purging was
completed, vapor concentrations of LEL, CO, CO2, methane, and hydrogen sulfide were
measured using a calibrated GEM 2000+ portable field instrument. The instrument was either
attached directly to the probe tubing or the sample was collected through the purge pump and
into a Tedlar bag which was screened using the instrument. The pressure differential between
the ambient air and the probe was measured by connecting the GEM 2000+ directly to the probe
tubing.

The sample probes were allowed to equilibrate for at least an additional 24 hours before the

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probes were again purged, monitored, and then sampled.

3.2.5 Vapor Probe Sampling
After the second purge and monitoring as described above, the probes were sampled. This
second purging, monitoring and sampling occurred on January 21, 2016 and February 9-10, 2016.
After purging and monitoring was completed, the purge valve was closed and the manifold valve
connected to the one-liter Summa canister was opened and Summa canister filled at the rate of
at 0.2 L/M.in. Canister vacuum readings were recorded before and after the sample collection.
The soil vapor samples were submitted under chain of custody to Eurofins Air Toxics Inc. (a
NELAC accredited laboratory) for volatile organic compounds (VOCs) by Method TO-15 analysis
and ASTM D-1946 analysis for fixed gases, including methane and helium.

Two additional soil vapor samples were collected from SV-7 and SV-8 on February 10, 2016, for
carbon and hydrogen isotopic analysis. Samples were collected in accordance with Pace
Analytical Energy Services, LLC procedure F-PAE-Q-031-rev.00. After the purging, monitoring
and collection of the TO-15 and ASTM D-1946 samples described above, a Teflon septum was
fitted to the purge end of the vapor collection manifold. The purge valve was opened and a new
plastic syringe fitted with a stop cock and needle was used to withdraw a sample through the
Teflon septum. Once the sample was pulled into the syringe and before the needle was removed
from the sample port, the syringe stop cock was closed. When the needle was inserted into the
septum on the collection vial, the stopcock was opened and the sample injected into the vial.
These samples were collected in 22 milliliter glass vials, with aluminum caps and Teflon septum.

The two samples collected on February 10, 2016, were submitted to Pace Analytical Energy
Services, LLC (a NELAC accredited laboratory) for isotopic analyses.

3.3 Sub-Slab Vapor Point Installation
The sub-slab vapor sampling point construction method used was not included in the NCDEQ
Guidance; however, NCDEQ approved the vapor point construction method as an alternative.
NCDEQ approval is included in Appendix F. This vapor point construction has been previously
accepted by NCDEQ under the Dry-Cleaning Solvent Cleanup Act Program. The vapor point
construction method uses a Vapor PinTM, a stainless steel barbed fitting with a silicone sheath
that creates a seal with the concrete and a metal cap. This method allows for the installation of

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the sampling point to proceed much quicker and allows the 2-inch diameter cap to be flush with
the slab.

Kleinfelder followed the sampling method detailed in the NCDEQ Guidance. To evaluate the
potential for vapor intrusion from the landfill (initially presumed source) into the school building
footprint, Kleinfelder installed sub-slab vapor sample points at nine locations at the Site (see
Figure 5).

On April 4, 2016, sub-slab vapor sampling points were installed. The sampling points were
installed by Quantex Drilling and Kleinfelder. To install the sampling point, a 1.5 to 1.75 inch hole
was drilled through the concrete slab and into the fill beneath. The concrete slab was
approximately 4 to 6.5 inches thick. The Vapor PinTM was hammered into the hole and fitted with
silicone cap and metal cover. The sub-slab vapor sampling points are shown on Figure 5.

3.4 SUB-SLAB VAPOR SAMPLING
Sub-slab vapor sampling methods, including shut-in tests, tracer gas testing, vapor purging, and
sub-slab vapor sample collection, were performed consistent with the NCDEQ Guidance. Field
data sheets documenting the activities are provided in Appendix D.

3.4.1 Vapor Sampling Apparatus
To collect samples, the Vapor PinTM was connected to a sampling manifold which included two
pressure gauges, a flow controller and a series of valves which allows the Vapor Pin to be purged,
monitored, and sampled without allowing ambient air to enter the connections or requiring
disturbing the shroud used for leak testing, see photos in Appendix D. Samples were collected in
laboratory evacuated one-liter Summa canisters. The summa canisters and sampling manifolds
were pre-cleaned and individually certified as clean, and provided by Eurofins Air Toxics Inc. The
flow regulator on the canisters were set at 0.2 L/Min by the laboratory.

3.4.2 Sampling Apparatus Leak Detection
Prior to mobilization, a shut-in test was performed on the sampling apparatus (canister and
manifold) to check for leaks in the fittings of each sample train. The shut-in test consisted of
assembling the Summa canister, flow controller, and sampling manifold, and then sealing the
“probe” connection point of the manifold with a brass cap and ensuring the purge valve of the

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manifold was closed. The canister valve was then opened exposing the sampling train to the
canister vacuum. The canister vacuum gauge was observed for at least one minute. If there was
a noticeably loss of vacuum, the sampling train (canister and manifold) failed the shut-in test and
was not used.

Consistent with the NCDEQ Guidance, during purging and sampling of each sub-slab vapor point,
a tracer gas test was performed to evaluate and validate sample integrity. A plastic shroud was
placed over the entire sampling train and the sub-slab vapor probe tubing connection at ground
surface. A laboratory grade helium tracer gas was introduced into the shroud. The concentration
of helium under the shroud was measured with a Dielectric Model MGD-2002 Helium Detector.
The helium concentration under the shroud was maintained at a minimum of 10 percent (%) during
the purging and sampling. At the conclusion of the purging, a sample of the purged sub-slab vapor
was collected in a Tedlar bag and screened for percentage of helium. If the screened sample
contained less than 5% of the helium concentration within the shroud, then the sample flow train
integrity was considered adequate and within an acceptable range. If the screened sample
contained more than 5% of the helium concentration within the shroud then the equipment was
inspected, adjusted, and purged again.

The final samples were also analyzed for helium concentration by the laboratory to verify the
integrity of the sample. Concentrations of helium in the samples were below 5% of the helium
concentration in the shroud indicating a competent seal was achieved between the surface and
the sub-slab vapor probe.

3.4.3 Vapor Probe Purging
Prior to monitoring or sampling each sub-slab vapor probe an SKC pump calibrated to 200
ml/minute was connected to the tubing or manifold to purge the probe and tubing. The vapor
probe and tubing were purged by removing three volumes of air (see calculations in Appendix D).

3.4.4 Vapor Probe Monitoring
At least 24 hours after probe construction, each vapor probe was purged. After purging was
completed, vapor concentrations of LEL, CO, CO2, methane, and hydrogen sulfide were
measured using a calibrated GEM 2000+ portable field instrument. The instrument was either
attached directly to the probe tubing or the sample was collected through the purge pump and

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into a Tedlar bag which was screened using the instrument. The pressure differential between
the ambient air and the probe was measured by connecting the GEM 2000+ directly to the probe
tubing.

The sample probes were allowed to equilibrate for at least an additional 24 hours before the
probes were again purged, monitored, and then sampled.

3.4.5 Vapor Probe Sampling

After the second purge and monitoring as described above, the probes were sampled. This
second purging, monitoring and sampling occurred on April 6, 2016. After purging and monitoring
was completed, the purge valve was closed and the manifold valve connected to the one-liter
Summa canister was opened and Summa canister filled at the rate of at 0.2 L/M.in. Canister
vacuum readings were recorded before and after the sample collection. The sub-slab vapor
samples were submitted under chain of custody to Eurofins Air Toxics Inc. (a NELAC accredited
laboratory) for TO-15 analysis (VOCs) and ASTM D-1946 (fixed gases, including methane and
helium) analysis.

3.5 SOIL AND GROUNDWATER SAMPLING POINT INSTALLATION
Soil and groundwater sampling methods were performed consistent with the NCDEQ Guidance.
Field notes documenting the activities are provided in Appendix D.

3.5.1 Drilling
Soil borings were advanced using a direct-push drill rig with soil samples screened with a FID.
Soil borings DP-1, DP-2, DP-4, DP-5, DP-6, DP-7 and DP-9 were advanced to 5 feet bgs. The
grade was 2 feet higher than the final grade at DP-1, DP-2 and DP-4, and the grade was
approximate to the final grade at DP-5, DP-6, DP-7 and DP-9. Soil boring DP-9 was advanced
within the building footprint which will be a future play area. A temporary monitoring well was not
installed in this area due to the potential of being damaged or destroyed by future construction
activities.

Soil borings DP-3, DP-8 and DP-10 were installed at former vapor points SV-8, SV-13 and
SV-14, and the soil borings were advanced to probe refusal. The temporary monitoring wells were

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installed in the borings and consisted of 10 feet length of 1 inch diameter slotted PVC screen
threaded to solid 1 inch diameter PVC riser. The well risers extended 1 foot above the ground
surface. A sand pack was placed from the bottom of the boring to 1 to 2 feet above the well
screen, and then 1 to 2 feet of bentonite was placed above the sand pack. After completion, the
wells were purged at least five well volumes of groundwater using a peristaltic pump or pumped
dry three times. The equipment was decontaminated between each soil boring. The soil boring
logs are provided in Appendix C. The sample locations are provided on Figure 6.

3.5.2 Field Screening of Soil
Soil samples collected from the borings and stockpiled soil were screened using a Flame
Ionization Detector (FID) to identify VOC contamination. Since the FID calibration gas was
methane, elevated readings appear to be related to methane in the subsurface and not petroleum-
related impact. Field screening observations and results are reported in Appendix D.

3.5.3 Field Screening of Groundwater
The temporary monitoring wells were screened by removing the well cap and inserting the
measuring probe into the well. TMW-1 and TMW-2 were sealed 24 hours prior to measurements;
however, TMW-3 was not screened because the well cap was not properly sealed. The temporary
monitoring wells were screened for percent methane, percent carbon dioxide, percent oxygen,
and concentration of carbon monoxide and concentration of hydrogen sulfide reported in ppm.
The well screening data is provided in the field notes provided in Appendix C.

3.6 SOIL AND GROUNDWATER SAMPLING
3.6.1 Soil Sampling
Soil grab sample depths are indicated on the soil laboratory results Table 3 in Appendix A. Soil
composite sampling of stockpiles varied in depth. Soil grab samples and soil composite samples
were collected and analyzed for VOCs by USEPA Method 8260. The soil sampling locations are
provided on Figure 6.

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© 2016 Kleinfelder
3.6.2 Groundwater Grab Sampling
During drilling of the bores, collection of groundwater grab samples was attempted where
groundwater was encountered at the three temporary monitoring well locations TMW1/DP-3,
TMW2/DP-8 and TMW3/DP-10. Groundwater retrieved from each temporary monitoring well
location was transferred to laboratory supplied bottles. Groundwater samples were collected and
analyzed for VOCs by USEPA Method 8260. Groundwater laboratory results are in Table 4 in
Appendix A.

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© 2016 Kleinfelder
4 RESULTS

4.1 DATA STANDARDS
VOC
Results of the TO-15 (VOC) analysis were compared to the Sub-Slab and Exterior SGSL as
published by the NCDEQ Division of Waste Management (DWM) (September 2015).

The DWM publishes two sets of SGSLs, one for residential properties and one for commercial
properties. The DWM states in its guidance:

“The target soil gas concentration corresponding to a chemical’s target indoor air
concentration is calculated by dividing the target indoor air concentration by an appropriate
attenuation factor. The attenuation factor represents the factor by which subsurface vapor
concentrations migrating into indoor air spaces are reduced due to diffusive, advective, and/or
other attenuating mechanisms.

For the calculation of SGSLs, DWM uses the IASL associated with a target cancer risk of
1E-05 or a hazard quotient of 0.2 and an attenuation factor (α) of 0.03 for residential exposure
and 0.01 for non-residential exposure.

Many industrial and commercial buildings have HVAC systems that increase air exchange
rates and are typically constructed with thicker, more competent slabs than in residential
settings. Increased air exchange rates result in a greater attenuation of contaminants in indoor
air, and thicker, more competent slabs may provide an additional barrier to vapor intrusion. It
is reasonable to assume a greater attenuation in non-residential settings, therefore; DWM
uses a higher attenuation factor for non-residential SGSLs.”

However, the guidance further states:

“It is DWM policy that day care facilities, schools and any other similar structures where
children (under 18) are the primary occupants are evaluated as residential use due to the
potentially sensitive nature of the exposed population.”

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© 2016 Kleinfelder
The onsite construction management firm, Balfour Beatty, reported that the school building is
constructed with an approximately 4 inch thick concrete slab, underlain by a plastic moisture vapor
barrier, a porous fill layer made of two layers of stone: 4 inches of #57 stone directly below the
moisture vapor barrier and another 4 inches of ABC below that. The moisture vapor barrier was
reported to be a Stego Wrap Vapor Barrier which is a 15 mil thick polyolefin vapor barrier. The
vapor barrier edges were reported to be taped with Stego Tape per the specifications. (See
Appendix E).

Based on this construction the commercial SGSLs may be the most appropriate for this structure;
however, the guidance quoted above indicates that due to the use of the structure as a school
the residential standard should apply. For comparison purposes the data collected from this
assessment is compared to both the residential and the commercial SGSLs.

The DWM guidance states, “When sample results exceed the screening levels, additional
evaluation, assessment or mitigation are warranted. However, if any individual sampling result
exceeds the screening level, that does not mean VI [vapor intrusion] will pose an unacceptable
health risk. Sample results can be expected to be variable spatially and temporally, and the DWM
screening levels are very conservative and assume a long period of exposure at that level.”

Methane
Methane is an asphyxiant and is combustible and potentially explosive when it is present at
concentrations in excess of 53,000 parts per million by volume (ppmv) in the presence of ambient
concentrations of oxygen. This concentration is referred to as the Lower Explosive Limit (LEL). In
order to provide some margin of safety, a concentration of approximately 10% of the LEL or 5,000
ppmv in ambient air is commonly utilized as an “action level” above which mitigation measures
may be considered. Kleinfelder compared methane concentrations to the California EPA advisory
on methane assessment at school sites (DTSC 2005), which is generally accepted as being
protective of human health. Per this guidance a potential problematic accumulation of methane
within a structure could be caused under the following conditions:
• Sub surface methane concentration in excess of 53,000 ppmv and sufficient
volume to produce elevated gas levels on the interior of the structure; and
• An elevated sub surface gas pressure (e.g. greater than 0.1 psi) sufficient to
induce flow into the building.

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© 2016 Kleinfelder
Isotopic Analysis
The ratios of the stable isotopes of carbon (12C and 13C) and hydrogen (1H and 2H) within methane
gas varies depending on the process by which the methane was produced. The two principal
methods of methane production are biological reduction of organic matter by microbes at shallow
depths (biogenic production) and non-biological thermal decomposition of deeply buried organic
matter (thermogenic production). Biogenic production can occur by fermentation of organic matter
and dissociation of acetate or through the reduction of carbon dioxide. Biogenic methane is
typically associated with shallow buried organic material such as trace organics is soil, yard waste,
animal waste or landfill material. Thermogenic methane is typically associated with petroleum and
natural gas reserves. Each process has a unique isotopic fingerprint (Hackley et. al., 1996; Kaplan
et. al., 1997) that is commonly used to evaluate the general source of methane found at sites.
This is done by plotting the isotopic signature of samples collected at a site on a graph of
established isotopic relationships for each methane production process.

Soil and Groundwater
Results of soil and groundwater VOC analysis were compared to the Groundwater Screening
Level (GWSL) for vapor intrusion as published by the NCDEQ DWM (September 2015). As
described above, the DWM publishes two sets of GWSLs, one for residential properties and one
for commercial properties. For comparison purposes the data collected from this assessment is
compared to both.

Results of soil VOC analysis were also compared to the NCDEQ’s Soil-to-Water Maximum Soil
Contamination Concentrations (MSCCs) and the NCDEQ’s Residential MSCCs.

Results of groundwater VOC analysis were also compared to NCDEQ Groundwater Quality
Standards, 15A NCAC 02L .0202 (2L Standard).

4.2 SAMPLE RESULTS
4.2.1 Soil Vapor Sampling Results
VOC
Results of VOC analysis identified 23 VOCs present in the soil vapor at concentrations above the
laboratory reporting limits. Of these, 6 VOCs were present above the residential SGSLs (benzene,
ethyl benzene, m,p-xylene, 1,2,4-trimethylbenzene, 1,3 butadiene, and chloroform). Only one of

20160086.001A| RAL16R41635 Page 17 June 10, 2016
© 2016 Kleinfelder
the identified VOCs (chloroform) was observed at concentrations that exceeded the non-
residential SGSLs, and that occurred in only one sample location (SV-8).

Results are presented on Figure 3, and in Table 1 in Appendix A. A laboratory data package is
presented in Appendix B.

Methane
Methane was detected at concentrations above the laboratory reporting limits in seven sample
locations. Of those, only three locations (SV-1, SV-7, and SV-8) contained methane at
concentrations above the 0.5% action level. Results are presented on Figure 2 and in Table 2 in
Appendix A. A laboratory data package is presented in Appendix B.

Pressure
Subsurface pressure was assessed with the field instrument by measuring the pressure in the
pressure in the sampling probes with respect to atmospheric pressure. No pressure differential
was observed between the atmospheric pressure and the subsurface probe.

Isotopic Analysis
The stable isotope ratios of carbon and hydrogen were plotted against isotopic ratios from past
research (Hackley et. al., 1996) in Figure 4 the isotopic signatures of the methane samples
collected at the Site are generally similar to that of biogenic gas production Discussions with the
laboratory indicted that the fact that the data plots more to the right on the graph is expected as
the plots were developed approximately 20 years ago. Results are presented in Figure 4 and in
Table 3 in Appendix A. A laboratory data package is presented in Appendix B.

4.2.2 Sub-Slab Vapor Sampling Results
VOC
Results of VOC analysis identified 19 VOCs present in the sub-slab vapor at concentrations above
the laboratory reporting limits. The VOCs present do not exceed the residential SGSLs or non-
residential SGSLs.

Results are presented on Figure 3, and in Table 1a in Appendix A. A laboratory data package is
presented in Appendix B.

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© 2016 Kleinfelder
Methane
Methane was detected at concentrations above the laboratory reporting limits in three sample
locations. The methane concentrations present do not exceed the 0.5% action level or the 5%
LEL. Results are presented on Figure 2 and in Table 2b in Appendix A. A laboratory data package
is presented in Appendix B.

Pressure
Sub-slab pressure was assessed with the field instrument by measuring the pressure in the
sampling point with respect to atmospheric pressure. No pressure differential was observed
between the atmospheric pressure and the sub slab.

4.2.3 Soil and Groundwater Sampling Results
VOC
VOC concentrations from soil grab samples detected four VOCs above the laboratory reporting
limits. The VOCs present do not exceed the NCDEQ’s Soil-to-Water or the Residential MSCCs.
Stockpile composite VOC sample concentrations were detected above the laboratory reporting
limits for seven VOCs. The VOCs present do not exceed the NCDEQ’s Soil-to-Water or the
Residential MSCCs except for two sample locations. Methylene chloride concentrations
exceeded NCDEQ’s Soil-to-Water MSCC at sample locations SC-2 and SC-3. Methylene chloride
is a common laboratory contaminant and is not considered to represent Site conditions. Results
are presented in Table 3 in Appendix A and the laboratory data package is presented in
Appendix B.

Results of VOC analysis identified six VOCs present in the groundwater at concentrations above
the laboratory reporting limits. The VOCs present do not exceed the NCDEQ, 15A NCAC 02L
Groundwater Standards. Results are presented in Table 4 in Appendix A and the laboratory data
package is presented in Appendix B.

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© 2016 Kleinfelder
5 CONCLUSIONS

Based on the investigation Kleinfelder offers the following conclusions:
• VOCs are present in the soil vapor at wide spread locations across the site and
the adjoining property. The VOCs are present in the soil gas outside of the building
footprint above the residential SGSLs (benzene, ethyl benzene, m,p-xylene, 1,2,4-
trimethylbenzene, 1,3 butadiene, and chloroform) and in one location above the
non-residential SGSLs (chloroform). However, sub-slab vapor sampling shows
that the VOC concentrations directly beneath the building footprint did not exceed
the residential or non-residential SGSLs.
• Methane concentrations were detected above the 0.5% action level in soil vapor
samples collected from three locations, SV-1, SV-7, and SV-8. Methane
generation is most likely from recent near surface decomposition. Methane
concentrations directly beneath the building footprint were not detected above the
0.5% action level or the 5% LEL.
• No pressure differential was observed between the atmospheric pressure and the
probe pressure indicating there is not an existing gradient that would drive vapors
into the building.
• VOCs are present in the soil at various locations across the Site. VOCs are present
in the soil above the Soil-to-Water MSCC (methylene chloride) at two stockpile
sampling locations. The methylene chloride detected is considered to be a
laboratory artifact and is, in Kleinfelder’s opinion, not representative of actual Site
conditions. VOCs are present in the groundwater at all three temporary monitoring
well sampling locations. The VOC concentrations did not exceed the NCDEQ 15A
NCAC 02L Groundwater Standards.
In summary, soil vapor sampling around the site detected methane and volatile organic
compounds at concentrations above screening levels. Subsequent sub-slab vapor sampling
under the building footprint detected volatile organic compounds and methane; however, the
concentrations did not exceed the screening levels. The NCDEQ DWM guidance on the matter
states that “DWM prefers the collection of sub-slab over near slab soil gas samples,” and
furthermore states that, “if soil gas concentrations do not exceed the SGSLs, typically no further
investigation is necessary….” Kleinfelder is requesting that based on the results to date, the DWM
make a determination that further investigation or remedial action is not required at this time.

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© 2016 Kleinfelder
6 LIMITATIONS

Kleinfelder’s work was performed in a manner consistent with that level of care and skill ordinarily
exercised by other members of its profession practicing in the same locality, under similar
conditions, and at the date the services are provided. Kleinfelder’s conclusions, opinions, and
recommendations are based on a limited number of observations and data. It is possible that
conditions could vary between or beyond the data evaluated.

Kleinfelder makes no guarantee or warranty, express or implied, regarding the services,
communication (oral or written), report, opinion, or instrument of service provided.

Kleinfelder offers various levels of investigative and engineering services to suit the varying needs
of different clients. Although risk can never be eliminated, more detailed and extensive studies
will yield more information, which may help understand and manage the level of risk involved.
Since detailed study and analysis involves greater expense, Kleinfelder‘s clients participate in
determining levels of service that provide adequate information for their purposes at acceptable
levels of risk. More extensive studies could be performed to reduce these uncertainties.

The information included on graphic representations in the report has been compiled from a
variety of sources and is subject to change without notice. Kleinfelder makes no representations
or warranties, express or implied, as to accuracy, completeness, timeliness, or rights to the use
of such information. These documents are not intended for use as a land survey product, nor are
they designed or intended as a construction design document. The use or misuse of the
information contained on these graphic representations is at the sole risk of the party using or
misusing the information.

20160086.001A| RAL16R41635 Page 21 June 10, 2016
© 2016 Kleinfelder
REFERENCES

“Advisory on Methane Assessment and Common Remedies at School Sites” June 2005
California Environmental Protection Agency Department of Toxic Substances Control

“Division of Waste Management Non-Residential Vapor Intrusion Screening Concentrations”,
September 2015, North Carolina Department of Environmental Quality Division of Waste
Management

“Division of Waste Management Residential Vapor Intrusion Screening Concentrations”,
September 2015, North Carolina Department of Environmental Quality Division of Waste
Management

Geologic Map of North Carolina, 1985, Department of Natural Resources and Community
Development, Division of Land Resources.

Hackley, et al, 1996, “Environmental Isotope Characteristics of Landfill Leachates and Gases"
Ground Water, Vol 35, No 5, 827-836

Kaplan, I.R. et. al., 1997, “Forensic Environmental Geochemistry: Differentiation of fuel types,
their sources and release times.” Organic Geochemistry, 27,289-317

“Phase I Environmental Site Assessment Report, Proposed E-43 School Site”, May 2014,
Mid-Atlantic Associates

“Procedure F-PAE-Q-031-rev.00” Feb 2015, Pace Analytical Energy Services, LLC

“Supplemental Guidelines for the Evaluation of Structural Vapor Intrusion Potential for Site
Assessments and Remedial Actions” March 2014, North Carolina Department of Environmental
Quality Inactive Hazardous Sites Branch

“Vapor Intrusion Guidance,” April 2014, North Carolina Department of Environmental Quality
Division of Waste Management

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.
FIGURE
20
1
6
0
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6
.
0
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1
A
3/
2
5
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2
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6
NL MA
S
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:

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Is
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SV ‐7 SV ‐8
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s
(C
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.
DW
D

W
R
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F
.
REF.
REF.
FEC
FEC
FEC
FEC
F
E
C
F
E
C
F
E
C
F
E
C
F
E
C
FEC
FEC
FEC
F
E
C
F
E
C
REF.
REF.
S
S
SS
S
S
F
F
F
F
S
S
F
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F
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F
F
F
F
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HREXCR
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:
FILE NAME:
16-0302--E43 Elem-SoilnGWSampleLoc.dwg
DRAWN BY:
CHECKED BY:
DRAWN:
PROJECT NO.
www.kleinfelder.com
The information included on this graphic representation has been compiled from a variety of
sources and is subject to change without notice. Kleinfelder makes no representations or
warranties, express or implied, as to accuracy, completeness, timeliness, or rights to the use ofsuch information. This document is not intended for use as a land survey product nor is it
designed or intended as a construction design document. The use or misuse of the information
contained on this graphic representation is at the sole risk of the party using or misusing the
information.
MT
.

D
O
R
A
,

F
L
E-43 ELEMENTARY SCHOOL
11500 HOLLY SPRINGS NEW HILL ROAD
HOLLY SPRINGS, NORTH CAROLINA
FIGURE
6CLB
MAS
6/08/2016
20160086.001A
SOIL AND GROUNDWATER
SAMPLE LOCATIONS
0100 10025
APPROXIMATE SCALE (feet)
REFERENCE: CLH DESIGN, PA.
LEGEND
SAMPLE LOCATIONS

APPENDIX A
DATA TABLES

TA
B
L
E

1
:

S
u
m
m
a
r
y

o
f

V
O
C

S
a
m
p
l
i
n
g

R
e
s
u
l
t
s
Pa
r
a
m
e
t
e
r
Sa
m
p
l
e

I
D
SV
2
SV
4

(
D
u
p
)

S
V
5

S
V
6
Sa
m
p
l
e

D
a
t
e

1
/
2
1
/
2
0
1
6

2
/
9
/
2
0
1
6

1
/
2
1
/
2
0
1
6

1
/
2
1
/
2
0
1
6

2
/
1
0
/
2
0
1
6

1
/
2
1
/
2
0
1
6

2
/
1
0
/
2
0
1
6

1
/
2
1
/
2
0
1
6

1
/
2
1
/
2
0
1
6

1
/
2
1
/
2
0
1
6

1
/
2
1
/
2
0
1
6

2
/
1
0
/
2
0
1
6
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
16
0
ND
44

2
1
0
ND
39
0
NS
52
0
NS
23
0
ND

N
D
48
.
7
613
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
79
ND
71

1
0
0
ND
18
0
NS
24
0
NS
10
0
ND

N
D
NE
NE
2,
2
,
4
-
T
r
i
m
e
t
h
y
l
p
e
n
t
a
n
e
14
0

1
4

8
5
0

3
2
0
0

6
5
0

2
6
0
NS
23
0
NS
16
0
ND

N
D
NE
NE
4-
E
t
h
y
l
t
o
l
u
e
n
e
37
0
ND
10
0

3
2
0
ND
58
0
NS
71
0
NS
35
0
ND

N
D
NE
NE
Be
n
z
e
n
e
17
0
ND
85

3
6
0
ND
16
0
NS
17
0
NS
13
0
ND

N
D
12
0
1570
Cu
m
e
n
e
29
ND
ND

N
D

N
D
38
NS
43
NS
20
ND

N
D
27
8
0
0
35000
Eth
y
l

B
e
n
z
e
n
e
13
0
0
38
12
0

1
2
0
ND
48
0
NS
58
0
NS
30
0
ND

N
D
37
4
4910
He
p
t
a
n
e
11
0
0
ND
21
0
0

6
4
0
0

1
7
0

2
1
0
0
NS
19
0
0
NS
13
0
0
ND

N
D
NE
NE
He
x
a
n
e
26
0
ND
22
0
0

8
8
0
0

5
6
0

7
8
0
NS
68
0
NS
79
0

4
3

4
8
NE
NE
m,
p
-
X
y
l
e
n
e
19
0
0
ND
43
0

1
4
0
0

7
2

2
4
0
0
NS
29
0
0
NS
13
0
0

1
9
ND
69
5
8760
o-
X
y
l
e
n
e
36
0
ND
67

2
5
0
ND
42
0
NS
53
0
NS
24
0

4
.
8
ND
69
5
8760
Pr
o
p
y
l
b
e
n
z
e
n
e
10
0
ND
ND
92
ND
14
0
NS
18
0
NS
89
ND

N
D
69
5
0
87600
To
l
u
e
n
e
18
0
0
12
47
0

1
8
0
0

8
8

1
7
0
0
NS
19
0
0
NS
11
0
0

1
3
ND
34
8
0
0
438000
1,
3

B
u
t
a
d
i
e
n
e
ND
ND
29

6
6
ND

N
D

N
S

N
D
NS
18
ND

N
D
13
.
9
175
Eth
a
n
o
l
ND
ND
74
ND

N
D

N
D

N
S

N
D
NS

N
D
12
ND
NE
NE
Ac
e
t
o
n
e
ND
ND
ND

N
D

N
D

N
D

N
S

N
D
NS

N
D
17
0
ND
21
6
0
0
0
2720000
Br
o
m
o
d
i
c
h
l
o
r
o
m
e
t
h
a
n
e

N
D
ND
ND

N
D

N
D

N
D

N
S

N
D
NS

N
D

N
D

N
D
25
.
3
331
Ch
l
o
r
o
f
o
r
m
ND
ND
ND

N
D

N
D

N
D

N
S

N
D
NS

N
D

N
D
6.
2
40
.
7
533
2-
P
r
o
p
a
n
o
l
ND

N
D

N
D

N
D
12
0
ND

N
S

N
D
NS

N
D

N
D

N
D
NE
NE
2-
B
u
t
a
n
o
n
e

(
M
E
K
)
ND

N
D

N
D

N
D
89
ND

N
S

N
D
NS

N
D

N
D

N
D
34
8
0
0
438000
Sty
r
e
n
e
ND

N
D

N
D
ND
ND
ND

N
S

N
D
NS

N
D

N
D

N
D
69
5
0
77600
Ca
r
b
o
n

D
i
s
u
l
f
i
d
e
ND

N
D

N
D
ND
ND
ND

N
S

N
D
NS

N
D

N
D

N
D
48
7
0
61300
Te
t
r
a
h
y
d
r
o
f
u
r
a
n
ND
ND
ND
ND
ND
ND

N
S

N
D
NS

N
D

N
D

N
D
13
9
0
0
175000
No
t
e
s
1)

-

A
l
l

u
n
i
t
s

a
r
e

i
n

u
g
/
m
3
4)

-

B
o
l
d
e
d

V
a
l
u
e
s

i
n
d
i
c
a
t
e

d
e
t
e
c
t
i
o
n
s

a
b
o
v
e

t
h
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
s

7
)

-

N
E

=

S
t
a
n
d
a
r
d

N
o
t

E
s
t
a
b
l
i
s
h
e
d
2)

-

N
D

=

N
o
t

d
e
t
e
c
t
e
d

a
b
o
v
e

l
a
b
o
r
a
t
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y

r
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p
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n
g

l
i
m
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t
s

5
)

-

S
h
a
d
e
d

V
a
l
u
e
s

i
n
d
i
c
a
t
e

d
e
t
e
c
t
i
o
n
s

a
b
o
v
e

t
h
e

r
e
s
i
d
e
n
t
i
a
l

S
G
S
L

8
)

-
*

=

H
e
l
i
u
m

D
e
t
e
c
t
e
d

a
b
o
v
e

1
0
%
3)

-

N
S

=

N
o
t

S
a
m
p
l
e
d

d
u
e

t
o

w
a
t
e
r

i
n

v
a
p
o
r

p
o
i
n
t
6)

-

S
h
a
d
e
d

a
n
d

c
r
o
s
s

h
a
t
c
h
e
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

d
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e
c
t
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s

a
b
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v
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t
h
e

n
o
n
-
r
e
s
i
d
e
n
t
i
a
l

S
G
S
L
TO

1
5

V
O
C
s
Non-Residential Sub Slab and Exterior Soil Gas Screening Levels (ug/m3)
SV
1
Re
s
i
d
e
n
t
i
a
l

S
u
b

S
l
a
b

a
n
d

Ex
t
e
r
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r

S
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G
a
s

S
c
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n
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n
g

Le
v
e
l
s

(
u
g
/
m
3
)
SV
3
SV
4
SV
7
TA
B
L
E

1
:

S
u
m
m
a
r
y

o
f

V
O
C

S
a
m
p
l
i
n
g

R
e
s
u
l
t
s
Pa
r
a
m
e
t
e
r
Sa
m
p
l
e

I
D
SV
9

S
V
1
0
*

S
V
1
1

S
V
1
2

S
V
1
3

S
V
1
4

S
V
1
5

S
V
1
6
Sa
m
p
l
e

D
a
t
e

1
/
2
1
/
2
0
1
6

2
/
1
0
/
2
0
1
6
2/
9
/
2
0
1
6

2
/
9
/
2
0
1
6
2/
9
/
2
0
1
6

2
/
9
/
2
0
1
6
2/9
/
2
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1
6

2
/
9
/
2
0
1
6
2/
9
/
2
0
1
6
2/
9
/
2
0
1
6
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e

N
D

N
D
62
ND

N
S

N
S
34
0

1
9
0
NS

N
D
61
3
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e

N
D

N
D

N
D

N
D

N
S

N
S
24
0

9
3
NS

N
D
NE
2,
2
,
4
-
T
r
i
m
e
t
h
y
l
p
e
n
t
a
n
e
5
ND

N
D

N
D

N
S

N
S
14
0

3
8
NS
57
NE
4-
E
t
h
y
l
t
o
l
u
e
n
e
6
ND
50
ND

N
S

N
S
42
0

2
4
0
NS

N
D
NE
Be
n
z
e
n
e
5.
7
ND

N
D

N
D

N
S

N
S
27

1
8
NS

N
D
15
7
0
Cu
m
e
n
e

N
D

N
D

N
D

N
D

N
S

N
S
32

1
7
NS

N
D
35
0
0
0
Eth
y
l

B
e
n
z
e
n
e
15

N
D
51
ND

N
S

N
S
20
0

1
6
0
NS

N
D
49
1
0
He
p
t
a
n
e
18
0

6
5
ND

N
D

N
S

N
S
32

2
0
0
NS
18
0
NE
He
x
a
n
e
12
0

1
3
0
ND

N
D

N
S

N
S
16
0

2
9
NS
93
NE
m,
p
-
X
y
l
e
n
e
30
ND
32
0
ND

N
S

N
S
13
0
0

9
0
0
NS
93
87
6
0
o-
X
y
l
e
n
e
5.
2
ND
94
ND

N
S

N
S
26
0

1
8
0
NS

N
D
87
6
0
Pr
o
p
y
l
b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
S

N
S
74
61
NS

N
D
87
6
0
0
To
l
u
e
n
e
32

1
0

2
2
0

7
.
9
NS

N
S
46
0

3
0
0
NS
14
0
43
8
0
0
0
1,
3

B
u
t
a
d
i
n
e
ND

N
D

N
D

N
D

N
S

N
S
75
ND
NS

N
D
17
5
Eth
a
n
o
l
ND

N
D

N
D

N
D

N
S

N
S

N
D

N
D
NS

N
D
NE
Ac
e
t
o
n
e
46
ND

N
D

N
D

N
S

N
S

N
D

N
D
NS

N
D
27
2
0
0
0
0
Br
o
m
o
d
i
c
h
l
o
r
o
m
e
t
h
a
n
e
11

6
2
ND

N
D

N
S

N
S

N
D

N
D
NS

N
D
33
1
Ch
l
o
r
o
f
o
r
m
11
0
0

3
0
0
0
ND

N
D

N
S

N
S

N
D
28
NS

N
D
53
3
2-
P
r
o
p
a
n
o
l
ND

N
D

N
D

N
D

N
S

N
S

N
D

N
D
NS

N
D
NE
2-
B
u
t
a
n
o
n
e

(
M
E
K
)
ND

N
D

N
D

N
D

N
S

N
S

N
D

N
D
NS
12
0
43
8
0
0
0
Sty
r
e
n
e
ND

N
D
43
ND

N
S

N
S
25
28
NS

N
D
77
6
0
0
Ca
r
b
o
n

D
i
s
u
l
f
i
d
e
ND

N
D

N
D
ND

N
S

N
S
58
ND
NS

N
D
61
3
0
0
Te
t
r
a
h
y
d
r
o
f
u
r
a
n
ND
ND
ND
ND

N
S

N
S
ND
ND
NS
48
17
5
0
0
0
No
t
e
s
1)

-

A
l
l

u
n
i
t
s

a
r
e

i
n

u
g
/
m
3
4)

-

B
o
l
d
e
d

V
a
l
u
e
s

i
n
d
i
c
a
t
e

d
e
t
e
c
t
i
o
n
s

a
b
o
v
e

t
h
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
s

7
)

-

N
E

=

S
t
a
n
d
a
r
d

N
o
t

E
s
t
a
b
l
i
s
h
e
d
2)

-

N
D

=

N
o
t

d
e
t
e
c
t
e
d

a
b
o
v
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
s

5
)

-

S
h
a
d
e
d

V
a
l
u
e
s

i
n
d
i
c
a
t
e

d
e
t
e
c
t
i
o
n
s

a
b
o
v
e

t
h
e

r
e
s
i
d
e
n
t
i
a
l

S
G
S
L

8
)

-
*

=

H
e
l
i
u
m

D
e
t
e
c
t
e
d

a
b
o
v
e

1
0
%
3)

-

N
S

=

N
o
t

S
a
m
p
l
e
d

d
u
e

t
o

w
a
t
e
r

i
n

v
a
p
o
r

p
o
i
n
t
6)

-

S
h
a
d
e
d

a
n
d

c
r
o
s
s

h
a
t
c
h
e
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

d
e
t
e
c
t
i
o
n
s

a
b
o
v
e

t
h
e

n
o
n
-
r
e
s
i
d
e
n
t
i
a
l

S
G
S
L
No
n
-
R
e
s
i
d
e
n
t
i
a
l

S
u
b

S
l
a
b

an
d

E
x
t
e
r
i
o
r

S
o
i
l

G
a
s

Sc
r
e
e
n
i
n
g

L
e
v
e
l
s

(
u
g
/
m
3
)
TO

1
5

V
O
C
s
NE
SV
8
NE
Re
s
i
d
e
n
t
i
a
l

S
u
b

S
l
a
b

a
n
d

Ex
t
e
r
i
o
r

S
o
i
l

G
a
s

Sc
r
e
e
n
i
n
g

L
e
v
e
l
s

(u
g
/
m
3
)
48
.
7
NE
21
6
0
0
0
12
0
27
8
0
0
37
4
NE NE
69
5
69
5
69
5
0
34
8
0
0
13
.
9
NE
13
9
0
0
25
.
3
40
.
7
NE
34
8
0
0
69
5
0
48
7
0
TA
B
L
E

1
a
:

S
u
m
m
a
r
y

o
f

s
u
b
s
l
a
b

v
a
p
o
r

s
a
m
p
l
i
n
g

r
e
s
u
l
t
s
Pa
r
a
m
e
t
e
r
Sa
m
p
l
e

I
D
IV
P
1

I
V
P
2

I
V
P
4

I
V
P
5

I
V
P
6

I
V
P
7

I
V
P
8

I
V
P
9
Sa
m
p
l
e

D
a
t
e
4/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
6.
8

3
6
ND
11

2
9
ND

N
D

N
D
48
.
7
613
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e

N
D
17
ND

N
D
12
ND

N
D

N
D
NE
NE
2,
2
,
4
-
T
r
i
m
e
t
h
y
l
p
e
n
t
a
n
e

N
D
30
0

5
.
7

3
7

2
0
0

7
.
4
ND

N
D
NE
NE
4-
E
t
h
y
l
t
o
l
u
e
n
e
7.
6
48
ND
12

3
7
ND

N
D
6
NE
NE
Be
n
z
e
n
e
ND
26
ND

N
D
18
ND

N
D

N
D
12
0
1570
Et
h
y
l

B
e
n
z
e
n
e
ND
77
ND
11

5
0
ND

N
D

N
D
37
4
4910
He
p
t
a
n
e
ND
90
ND
11
ND

N
D

N
D

N
D
NE
NE
He
x
a
n
e
4.
5
52
ND
6.
8

3
3
ND

N
D

N
D
NE
NE
m,
p
-
X
y
l
e
n
e
15
24
0
7.
9

4
1

1
6
0

1
1

1
2

1
0
69
5
8760
o-
X
y
l
e
n
e
6.
9
81
ND
15

6
1
ND
6
ND
69
5
8760
Pr
o
p
y
l
b
e
n
z
e
n
e
ND
11
ND

N
D
8.
4
ND

N
D

N
D
69
5
0
8760
To
l
u
e
n
e
5.
2
43
0
12

5
4

2
8
0

1
5

6
.
5

4
.
9
34
8
0
0
438000
1,
3

B
u
t
a
d
i
e
n
e
ND

N
D

N
D

N
D

N
D

N
D

N
D

N
D
13
.
9
175
Et
h
a
n
o
l
76
46
64

3
2
0

8
6

1
4
0

2
2
0

1
2
0
NE
NE
Ac
e
t
o
n
e
12
0
77
90

2
5
0

1
0
0

1
5
0

7
4
0

2
3
0
21
6
0
0
0
2720000
Ch
l
o
r
o
f
o
r
m
ND

N
D

N
D

N
D

N
D

N
D

N
D

N
D
40
.
7
533
2-
P
r
o
p
a
n
o
l
ND
33
ND
18

2
6
12

1
2
ND
NE
NE
2-
B
u
t
a
n
o
n
e

(
M
E
K
)
ND

N
D

N
D

N
D

N
D
ND
30
ND
34
8
0
0
438000
Cy
c
l
o
h
e
x
a
n
e
17

5
5
ND
7.
3
33
ND

N
D

N
D
41
7
0
0
526000
4-
M
e
t
h
y
l
-
2
-
p
e
n
t
a
n
o
n
e
ND

N
D

N
D
8.
1
ND
ND
23

8
.
5
20
9
0
0
263000
Te
t
r
a
h
y
d
r
o
f
u
r
a
n
3.
8
ND

N
D
3.
5
ND
5

1
1

4
.
3
13
9
0
0
175000
No
t
e
s
1)

-

A
l
l

u
n
i
t
s

a
r
e

i
n

u
g
/
m
3
4)

-

B
o
l
d
e
d

V
a
l
u
e
s

i
n
d
i
c
a
t
e

d
e
t
e
c
t
i
o
n
s

a
b
o
v
e

t
h
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
s
2)

-

N
D

=

N
o
t

d
e
t
e
c
t
e
d

a
b
o
v
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
s

5
)

-

S
h
a
d
e
d

V
a
l
u
e
s

i
n
d
i
c
a
t
e

d
e
t
e
c
t
i
o
n
s

a
b
o
v
e

t
h
e

r
e
s
i
d
e
n
t
i
a
l

S
G
S
L
3)

-

N
S

=

N
o
t

S
a
m
p
l
e
d

6)

-

S
h
a
d
e
d

a
n
d

c
r
o
s
s

h
a
t
c
h
e
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

d
e
t
e
c
t
i
o
n
s

a
b
o
v
e

t
h
e

n
o
n
-
r
e
s
i
d
e
n
t
i
a
l

S
G
S
L
TO

1
5

V
O
C
s
Re
s
i
d
e
n
t
i
a
l

S
u
b

S
l
a
b

a
n
d

Ex
t
e
r
i
o
r

S
o
i
l

G
a
s

Sc
r
e
e
n
i
n
g

L
e
v
e
l
s

(
u
g
/
m
3
)
Non-Residential Sub Slab and Exterior Soil Gas Screening Levels (ug/m3)
TA
B
L
E

2
:

S
u
m
m
a
r
y

o
f

F
i
x
e
d

G
a
s

S
a
m
p
l
i
n
g

R
e
s
u
l
t
s
Pa
r
a
m
e
t
e
r
Sa
m
p
l
e

I
D
SV
2
SV
4

(
D
u
p
)

S
V
-
5

S
V
6
Sa
m
p
l
e

D
a
t
e

1
/
2
1
/
2
0
1
6

2
/
9
/
2
0
1
6

1
/
2
1
/
2
0
1
6

1
/
2
1
/
2
0
1
6

2
/
1
0
/
2
0
1
6

1
/
2
1
/
2
0
1
6

2
/
1
0
/
2
0
1
6

1
/
2
1
/
2
0
1
6

2
/
1
0
/
2
0
1
6

1
/
2
1
/
2
0
1
6
Ox
y
g
e
n
9.
8

7
.
2

1
3

1
9

1
2

1
9

N
S

2
0

N
S

2
0
Nit
r
o
g
e
n
82

8
1

8
6

7
9

8
8

8
0

N
S

7
9

N
S

7
9
Ca
r
b
o
n

M
o
n
o
x
i
d
e
ND

N
D

N
D

N
D

N
D

N
D

N
S

N
D

N
S

N
D
Ca
r
b
o
n

D
i
o
x
i
d
e
7.
2

1
1

0
.
5
4

1
.
5

0
.
3
7

0
.
9
9

N
S

0
.
8
9

N
S

1
.
1
He
l
i
u
m
ND

N
D

N
D

N
D

N
D

N
D

N
S

0
.
3
8

N
S

N
D
Me
t
h
a
n
e
1.
2

0
.
9
6
ND

0
.
0
0
0
5
7

N
D

N
D

N
S

N
D

N
S

0
.
0
0
4
1
1)

-

A
l
l

u
n
i
t
s

a
r
e

i
n

%
2)

-

N
D

=

N
o
t

d
e
t
e
c
t
e
d

a
b
o
v
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
s
3)

-

N
S

=

N
o
t

S
a
m
p
l
e
d

d
u
e

t
o

w
a
t
e
r

i
n

v
a
p
o
r

p
o
i
n
t
4)

-
*

=

H
e
l
i
u
m

D
e
t
e
c
t
e
d

a
b
o
v
e

1
0
%
5)

L
E
L

d
a
t
a

f
r
o
m

G
a
s

D
a
t
a

B
o
o
k
,

7
t
h

e
d
i
t
i
o
n
,

c
o
p
y
r
i
g
h
t

2
0
0
1

b
y

M
a
t
h
e
s
o
n

G
a
s

P
r
o
d
u
c
t
s
.
AS
T
M
D

1
9
4
6

+

H
e
SV
1
SV
3
SV
4
Ac
t
i
o
n

L
e
v
e
l

a
n
d

L
E
L
Ac
t
i
o
n

L
e
v
e
l

=

0
.
5
%

a
n
d

L
E
L

=

5
%
TA
B
L
E

2
:

S
u
m
m
a
r
y

o
f

F
i
x
e
d

G
a
s

S
a
m
p
l
i
n
g

R
e
s
u
l
t
s
Pa
r
a
m
e
t
e
r
Sa
m
p
l
e

I
D
SV
9

S
V
1
0
*

S
V
1
1

S
V
1
2

S
V
1
3

S
V
1
4

S
V
1
5

S
V
1
6
Sa
m
p
l
e

D
a
t
e

1
/
2
1
/
2
0
1
6

2
/
1
0
/
2
0
1
6

1
/
2
1
/
2
0
1
6

2
/
1
0
/
2
0
1
6
2/
9
/
2
0
1
6

2
/
9
/
2
0
1
6
2/
9
/
2
0
1
6

2
/
9
/
2
0
1
6
2/
9
/
2
0
1
6

2
/
9
/
2
0
1
6
2/
9
/
2
0
1
6
2/
9
/
2
0
1
6
Ox
y
g
e
n
6.
5

3
.
8

1
.
7

3
.
3

9
.
6

1
3

N
S

N
S

1
7

2
.
6

N
S

9
.
9
Nit
r
o
g
e
n
78

7
9

7
0

7
0

9
0

4
9

N
S

N
S

8
2

9
2

N
S

9
0
Ca
r
b
o
n

M
o
n
o
x
i
d
e
ND

N
D

N
D

N
D

N
D

N
D

N
S

N
S

N
D

N
D

N
S

N
D
Ca
r
b
o
n

D
i
o
x
i
d
e
6.
8

8
.
1

1
8

1
7

0
.
3
3

N
D

N
S

N
S

0
.
7
1

5
.
6

N
S

N
D
He
l
i
u
m
ND

N
D

N
D

N
D

N
D

3
8

N
S

N
S

N
D

N
D

N
S

N
D
Me
t
h
a
n
e
8.
2

9
.
4

9
.
9

9
.
4
ND

N
D

N
S

N
S

0
.
0
0
0
7
4

0
.
0
0
0
5
5

N
S

N
D
No
t
e
s
1)

-

A
l
l

u
n
i
t
s

a
r
e

i
n

%
2)

-

N
D

=

N
o
t

d
e
t
e
c
t
e
d

a
b
o
v
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
s
3)

-

N
S

=

N
o
t

S
a
m
p
l
e
d

d
u
e

t
o

w
a
t
e
r

i
n

v
a
p
o
r

p
o
i
n
t
4)

-
*

=

H
e
l
i
u
m

D
e
t
e
c
t
e
d

a
b
o
v
e

1
0
%
5)

L
E
L

d
a
t
a

f
r
o
m

G
a
s

D
a
t
a

B
o
o
k
,

7
t
h

e
d
i
t
i
o
n
,

c
o
p
y
r
i
g
h
t

2
0
0
1

b
y

M
a
t
h
e
s
o
n

G
a
s

P
r
o
d
u
c
t
s
.
Action Level = 0.5% and LEL = 5%
SV
8
Action Level and LEL
AS
T
M

D
1
9
4
6

+

H
e
SV
7
TA
B
L
E

2
b
:

S
u
b
s
l
a
b

p
o
i
n
t
s

-

S
u
m
m
a
r
y

o
f

F
i
x
e
d

G
a
s

S
a
m
p
l
i
n
g

R
e
s
u
l
t
s
Pa
r
a
m
e
t
e
r
Sa
m
p
l
e

I
D
IV
P
1

I
V
P
2

I
V
P
4

I
V
P
5

I
V
P
6

I
V
P
7

I
V
P
8

I
V
P
9
Sa
m
p
l
e

D
a
t
e

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6

4
/
6
/
2
0
1
6
Ox
y
g
e
n
21

2
1

2
1

2
0

2
1

2
1

2
1

2
1
Ni
t
r
o
g
e
n
79

7
8

7
9

8
0

7
9

7
9

7
9

7
9
Ca
r
b
o
n

M
o
n
o
x
i
d
e

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D
Ca
r
b
o
n

D
i
o
x
i
d
e

0
.
2
2

0
.
4
3

0
.
2

0
.
0
8
5

0
.
0
5
1

N
D

N
D

0
.
1
6
He
l
i
u
m
ND

N
D

0
.
1
3

N
D

0
.
2
9

N
D

N
D

N
D
Me
t
h
a
n
e
0.
0
0
0
2
3

N
D

0
.
0
0
0
2
6

0
.
0
0
0
3
2

N
D

N
D

N
D

N
D
1)

-

A
l
l

u
n
i
t
s

a
r
e

i
n

%
2)

-

N
D

=

N
o
t

d
e
t
e
c
t
e
d

a
b
o
v
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
s
3)

-

N
S

=

N
o
t

S
a
m
p
l
e
d

d
u
e

t
o

w
a
t
e
r

i
n

v
a
p
o
r

p
o
i
n
t
4)

-
*

=

H
e
l
i
u
m

D
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APPENDIX B
LABORATORY DATA

1/29/2016
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte NC 28269
Project Name: WCPSS
Project #: 20160086.001A
Dear Mr. Michael Sussman
The following report includes the data for the above referenced project for sample(s)
received on 1/26/2016 at Air Toxics Ltd.
The data and associated QC analyzed by TO-15 are compliant with the project
requirements or laboratory criteria with the exception of the deviations noted in the
attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contactthe Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1601347A
Page 1 of 31
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
WORK ORDER #:1601347A
CLIENT:BILL TO:
PHONE:
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
704-598-1049
704-598-1050
01/26/2016
DATE COMPLETED:01/29/2016
P.O. #
PROJECT #20160086.001A WCPSS
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A SV1 TO-15 4.1 "Hg 14.4 psi
02A SV7 TO-15 2.2 "Hg 14.8 psi
03A SV8 TO-15 0.4 psi 15.1 psi
04A SV6 TO-15 16.1 "Hg 15 psi
05A SV2 TO-15 26.5 "Hg 15 psi
06A SV3 TO-15 16.0 "Hg 15 psi
07A SV4 TO-15 20.5 "Hg 15 psi
08A SV4 Dup TO-15 22.0 "Hg 15 psi
09A Lab Blank TO-15 NA NA
10A CCV TO-15 NA NA
11A LCS TO-15 NA NA
11AA LCSD TO-15 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2014, Expiration date: 10/17/2015.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
[phone] . [phone] . FAX [phone]
01/29/16
Page 2 of 31
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704343-14-7, UT NELAP CA009332014-5, VA NELAP - 460197, WA NELAP - C935
LABORATORY NARRATIVEEPA Method TO-15Kleinfelder Southeast, Inc.Workorder# 1601347A
Eight 1 Liter Summa Canister samples were received on January 26, 2016. The laboratory performed
analysis via EPA Method TO-15 using GC/MS in the full scan mode.
This workorder was independently validated prior to submittal using 'USEPA National Functional
Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based, logic
driven, independent validation engine was employed to assess completeness, evaluate pass/fail of relevant
project quality control requirements and verification of all quantified amounts.
There was a significant difference (greater than 5.0" Hg) between the measured canister receipt vacuum
and that which was reported on the Chain of Custody (COC) for sample SV8. A leak test indicated that
the valve was functioning properly.
Samples SV6, SV2, SV3, SV4 and SV4 Dup were received with significant vacuum remaining in the
canister. The residual canister vacuum resulted in elevated reporting limits.
Receiving Notes
All Quality Control Limit exceedances and affected sample results are noted by flags. Each flag is defined
at the bottom of this Case Narrative and on each Sample Result Summary page.
Dilution was performed on samples SV1 and SV3 due to the presence of high level target species.
Analytical Notes
Eight qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction not
performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. See
data page for project specific U-flag definition.
UJ- Non-detected compound associated with low bias in the CCV
N - The identification is based on presumptive evidence.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 3 of 31
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SV1
Lab ID#: 1601347A-01A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.3 73 8.1 260Hexane
2.3 31 11 1402,2,4-Trimethylpentane
2.3 54 7.3 170Benzene
2.3 270 9.4 1100Heptane
2.3 480 8.6 1800Toluene
2.3 300 9.9 1300Ethyl Benzene
2.3 430 9.9 1900m,p-Xylene
2.3 84 9.9 360o-Xylene
2.3 5.9 11 29Cumene
2.3 21 11 100Propylbenzene
2.3 74 11 3704-Ethyltoluene
2.3 16 11 791,3,5-Trimethylbenzene
2.3 32 11 1601,2,4-Trimethylbenzene
Client Sample ID: SV7
Lab ID#: 1601347A-02A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
4.3 6.1 8.1 12Ethanol
11 73 26 170Acetone
1.1 12 3.8 43Hexane
1.1 3.5 4.1 13Toluene
1.1 4.4 4.7 19m,p-Xylene
1.1 1.1 4.7 4.8o-Xylene
Client Sample ID: SV8
Lab ID#: 1601347A-03A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
9.8 19 23 46Acetone
0.98 34 3.5 120Hexane
0.98 230 4.8 1100Chloroform
0.98 1.1 4.6 5.02,2,4-Trimethylpentane
Page 4 of 31
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SV8
Lab ID#: 1601347A-03A
0.98 1.8 3.1 5.7Benzene
0.98 45 4.0 180Heptane
0.98 1.6 6.6 11Bromodichloromethane
0.98 8.6 3.7 32Toluene
0.98 3.4 4.3 15Ethyl Benzene
0.98 7.0 4.3 30m,p-Xylene
0.98 1.2 4.3 5.2o-Xylene
0.98 1.2 4.8 6.04-Ethyltoluene
Client Sample ID: SV6
Lab ID#: 1601347A-04A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.2 7.9 4.8 181,3-Butadiene
2.2 220 7.7 790Hexane
2.2 34 10 1602,2,4-Trimethylpentane
2.2 41 7.0 130Benzene
2.2 330 8.9 1300Heptane
2.2 290 8.2 1100Toluene
2.2 70 9.5 300Ethyl Benzene
2.2 300 9.5 1300m,p-Xylene
2.2 56 9.5 240o-Xylene
2.2 4.2 11 20Cumene
2.2 18 11 89Propylbenzene
2.2 71 11 3504-Ethyltoluene
2.2 21 11 1001,3,5-Trimethylbenzene
2.2 48 11 2301,2,4-Trimethylbenzene
Client Sample ID: SV2
Lab ID#: 1601347A-05A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
8.6 13 19 291,3-Butadiene
35 39 65 74Ethanol
Page 5 of 31
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SV2
Lab ID#: 1601347A-05A
8.6 610 30 2200Hexane
8.6 180 40 8502,2,4-Trimethylpentane
8.6 27 28 85Benzene
8.6 520 35 2100Heptane
8.6 120 32 470Toluene
8.6 28 38 120Ethyl Benzene
8.6 98 38 430m,p-Xylene
8.6 15 38 67o-Xylene
8.6 20 42 1004-Ethyltoluene
8.6 14 42 711,3,5-Trimethylbenzene
8.6 8.9 42 441,2,4-Trimethylbenzene
Client Sample ID: SV3
Lab ID#: 1601347A-06A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
11 30 24 661,3-Butadiene
11 2500 38 8800Hexane
11 680 50 32002,2,4-Trimethylpentane
11 110 34 360Benzene
11 1600 44 6400Heptane
11 490 41 1800Toluene
11 90 47 390Ethyl Benzene
11 320 47 1400m,p-Xylene
11 58 47 250o-Xylene
11 19 53 92Propylbenzene
11 66 53 3204-Ethyltoluene
11 21 53 1001,3,5-Trimethylbenzene
11 43 53 2101,2,4-Trimethylbenzene
Client Sample ID: SV4
Lab ID#: 1601347A-07A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
Page 6 of 31
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SV4
Lab ID#: 1601347A-07A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
3.2 220 11 780Hexane
3.2 56 15 2602,2,4-Trimethylpentane
3.2 49 10 160Benzene
3.2 520 13 2100Heptane
3.2 460 12 1700Toluene
3.2 110 14 480Ethyl Benzene
3.2 560 14 2400m,p-Xylene
3.2 98 14 420o-Xylene
3.2 7.6 16 38Cumene
3.2 29 16 140Propylbenzene
3.2 120 16 5804-Ethyltoluene
3.2 37 16 1801,3,5-Trimethylbenzene
3.2 80 16 3901,2,4-Trimethylbenzene
Client Sample ID: SV4 Dup
Lab ID#: 1601347A-08A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
3.8 190 13 680Hexane
3.8 49 18 2302,2,4-Trimethylpentane
3.8 53 12 170Benzene
3.8 460 16 1900Heptane
3.8 520 14 1900Toluene
3.8 130 16 580Ethyl Benzene
3.8 660 16 2900m,p-Xylene
3.8 120 16 530o-Xylene
3.8 8.8 19 43Cumene
3.8 36 19 180Propylbenzene
3.8 140 19 7104-Ethyltoluene
3.8 48 19 2401,3,5-Trimethylbenzene
3.8 100 19 5201,2,4-Trimethylbenzene
Page 7 of 31
Client Sample ID: SV1
Lab ID#: 1601347A-01A
EPA METHOD TO-15 GC/MS FULL SCAN
a012817File Name:
Dil. Factor:4.58
Date of Collection: 1/21/16 9:28:00 AM
Date of Analysis: 1/28/16 11:39 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.3 Not Detected 11 Not DetectedFreon 12
2.3 Not Detected 16 Not DetectedFreon 114
23 Not Detected 47 Not DetectedChloromethane
2.3 Not Detected 5.8 Not DetectedVinyl Chloride
2.3 Not Detected 5.1 Not Detected1,3-Butadiene
23 Not Detected 89 Not DetectedBromomethane
9.2 Not Detected 24 Not DetectedChloroethane
2.3 Not Detected 13 Not DetectedFreon 11
9.2 Not Detected 17 Not DetectedEthanol
2.3 Not Detected 18 Not DetectedFreon 113
2.3 Not Detected 9.1 Not Detected1,1-Dichloroethene
23 Not Detected 54 Not DetectedAcetone
9.2 Not Detected 22 Not Detected2-Propanol
9.2 Not Detected 28 Not DetectedCarbon Disulfide
9.2 Not Detected 29 Not Detected3-Chloropropene
23 Not Detected 80 Not DetectedMethylene Chloride
2.3 Not Detected 8.2 Not DetectedMethyl tert-butyl ether
2.3 Not Detected 9.1 Not Detectedtrans-1,2-Dichloroethene
2.3 73 8.1 260Hexane
2.3 Not Detected 9.3 Not Detected1,1-Dichloroethane
9.2 Not Detected 27 Not Detected2-Butanone (Methyl Ethyl Ketone)
2.3 Not Detected 9.1 Not Detectedcis-1,2-Dichloroethene
2.3 Not Detected 6.8 Not DetectedTetrahydrofuran
2.3 Not Detected 11 Not DetectedChloroform
2.3 Not Detected 12 Not Detected1,1,1-Trichloroethane
2.3 Not Detected 7.9 Not DetectedCyclohexane
2.3 Not Detected 14 Not DetectedCarbon Tetrachloride
2.3 31 11 1402,2,4-Trimethylpentane
2.3 54 7.3 170Benzene
2.3 Not Detected 9.3 Not Detected1,2-Dichloroethane
2.3 270 9.4 1100Heptane
2.3 Not Detected 12 Not DetectedTrichloroethene
2.3 Not Detected 10 Not Detected1,2-Dichloropropane
9.2 Not Detected 33 Not Detected1,4-Dioxane
2.3 Not Detected 15 Not DetectedBromodichloromethane
2.3 Not Detected 10 Not Detectedcis-1,3-Dichloropropene
2.3 Not Detected 9.4 Not Detected4-Methyl-2-pentanone
2.3 480 8.6 1800Toluene
2.3 Not Detected 10 Not Detectedtrans-1,3-Dichloropropene
2.3 Not Detected 12 Not Detected1,1,2-Trichloroethane
2.3 Not Detected 16 Not DetectedTetrachloroethene
9.2 Not Detected 38 Not Detected2-Hexanone
Page 8 of 31
Client Sample ID: SV1
Lab ID#: 1601347A-01A
EPA METHOD TO-15 GC/MS FULL SCAN
a012817File Name:
Dil. Factor:4.58
Date of Collection: 1/21/16 9:28:00 AM
Date of Analysis: 1/28/16 11:39 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.3 Not Detected 20 Not DetectedDibromochloromethane
2.3 Not Detected 18 Not Detected1,2-Dibromoethane (EDB)
2.3 Not Detected 10 Not DetectedChlorobenzene
2.3 300 9.9 1300Ethyl Benzene
2.3 430 9.9 1900m,p-Xylene
2.3 84 9.9 360o-Xylene
2.3 Not Detected 9.8 Not DetectedStyrene
2.3 Not Detected 24 Not DetectedBromoform
2.3 5.9 11 29Cumene
2.3 Not Detected 16 Not Detected1,1,2,2-Tetrachloroethane
2.3 21 11 100Propylbenzene
2.3 74 11 3704-Ethyltoluene
2.3 16 11 791,3,5-Trimethylbenzene
2.3 32 11 1601,2,4-Trimethylbenzene
2.3 Not Detected 14 Not Detected1,3-Dichlorobenzene
2.3 Not Detected 14 Not Detected1,4-Dichlorobenzene
2.3 Not Detected 12 Not Detectedalpha-Chlorotoluene
2.3 Not Detected 14 Not Detected1,2-Dichlorobenzene
9.2 Not Detected UJ 68 Not Detected UJ1,2,4-Trichlorobenzene
9.2 Not Detected UJ 98 Not Detected UJHexachlorobutadiene
UJ = Analyte associated with low bias in the CCV and/or LCS.
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
95 70-130Toluene-d8
100 70-1301,2-Dichloroethane-d4
103 70-1304-Bromofluorobenzene
Page 9 of 31
Client Sample ID: SV7
Lab ID#: 1601347A-02A
EPA METHOD TO-15 GC/MS FULL SCAN
a012818File Name:
Dil. Factor:2.16
Date of Collection: 1/21/16 10:10:00 AM
Date of Analysis: 1/29/16 12:17 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 5.3 Not DetectedFreon 12
1.1 Not Detected 7.6 Not DetectedFreon 114
11 Not Detected 22 Not DetectedChloromethane
1.1 Not Detected 2.8 Not DetectedVinyl Chloride
1.1 Not Detected 2.4 Not Detected1,3-Butadiene
11 Not Detected 42 Not DetectedBromomethane
4.3 Not Detected 11 Not DetectedChloroethane
1.1 Not Detected 6.1 Not DetectedFreon 11
4.3 6.1 8.1 12Ethanol
1.1 Not Detected 8.3 Not DetectedFreon 113
1.1 Not Detected 4.3 Not Detected1,1-Dichloroethene
11 73 26 170Acetone
4.3 Not Detected 11 Not Detected2-Propanol
4.3 Not Detected 13 Not DetectedCarbon Disulfide
4.3 Not Detected 14 Not Detected3-Chloropropene
11 Not Detected 38 Not DetectedMethylene Chloride
1.1 Not Detected 3.9 Not DetectedMethyl tert-butyl ether
1.1 Not Detected 4.3 Not Detectedtrans-1,2-Dichloroethene
1.1 12 3.8 43Hexane
1.1 Not Detected 4.4 Not Detected1,1-Dichloroethane
4.3 Not Detected 13 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.1 Not Detected 4.3 Not Detectedcis-1,2-Dichloroethene
1.1 Not Detected 3.2 Not DetectedTetrahydrofuran
1.1 Not Detected 5.3 Not DetectedChloroform
1.1 Not Detected 5.9 Not Detected1,1,1-Trichloroethane
1.1 Not Detected 3.7 Not DetectedCyclohexane
1.1 Not Detected 6.8 Not DetectedCarbon Tetrachloride
1.1 Not Detected 5.0 Not Detected2,2,4-Trimethylpentane
1.1 Not Detected 3.4 Not DetectedBenzene
1.1 Not Detected 4.4 Not Detected1,2-Dichloroethane
1.1 Not Detected 4.4 Not DetectedHeptane
1.1 Not Detected 5.8 Not DetectedTrichloroethene
1.1 Not Detected 5.0 Not Detected1,2-Dichloropropane
4.3 Not Detected 16 Not Detected1,4-Dioxane
1.1 Not Detected 7.2 Not DetectedBromodichloromethane
1.1 Not Detected 4.9 Not Detectedcis-1,3-Dichloropropene
1.1 Not Detected 4.4 Not Detected4-Methyl-2-pentanone
1.1 3.5 4.1 13Toluene
1.1 Not Detected 4.9 Not Detectedtrans-1,3-Dichloropropene
1.1 Not Detected 5.9 Not Detected1,1,2-Trichloroethane
1.1 Not Detected 7.3 Not DetectedTetrachloroethene
4.3 Not Detected 18 Not Detected2-Hexanone
Page 10 of 31
Client Sample ID: SV7
Lab ID#: 1601347A-02A
EPA METHOD TO-15 GC/MS FULL SCAN
a012818File Name:
Dil. Factor:2.16
Date of Collection: 1/21/16 10:10:00 AM
Date of Analysis: 1/29/16 12:17 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 9.2 Not DetectedDibromochloromethane
1.1 Not Detected 8.3 Not Detected1,2-Dibromoethane (EDB)
1.1 Not Detected 5.0 Not DetectedChlorobenzene
1.1 Not Detected 4.7 Not DetectedEthyl Benzene
1.1 4.4 4.7 19m,p-Xylene
1.1 1.1 4.7 4.8o-Xylene
1.1 Not Detected 4.6 Not DetectedStyrene
1.1 Not Detected 11 Not DetectedBromoform
1.1 Not Detected 5.3 Not DetectedCumene
1.1 Not Detected 7.4 Not Detected1,1,2,2-Tetrachloroethane
1.1 Not Detected 5.3 Not DetectedPropylbenzene
1.1 Not Detected 5.3 Not Detected4-Ethyltoluene
1.1 Not Detected 5.3 Not Detected1,3,5-Trimethylbenzene
1.1 Not Detected 5.3 Not Detected1,2,4-Trimethylbenzene
1.1 Not Detected 6.5 Not Detected1,3-Dichlorobenzene
1.1 Not Detected 6.5 Not Detected1,4-Dichlorobenzene
1.1 Not Detected 5.6 Not Detectedalpha-Chlorotoluene
1.1 Not Detected 6.5 Not Detected1,2-Dichlorobenzene
4.3 Not Detected UJ 32 Not Detected UJ1,2,4-Trichlorobenzene
4.3 Not Detected UJ 46 Not Detected UJHexachlorobutadiene
UJ = Analyte associated with low bias in the CCV and/or LCS.
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
97 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
100 70-1304-Bromofluorobenzene
Page 11 of 31
Client Sample ID: SV8
Lab ID#: 1601347A-03A
EPA METHOD TO-15 GC/MS FULL SCAN
a012819File Name:
Dil. Factor:1.97
Date of Collection: 1/21/16 10:46:00 AM
Date of Analysis: 1/29/16 12:43 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.98 Not Detected 4.9 Not DetectedFreon 12
0.98 Not Detected 6.9 Not DetectedFreon 114
9.8 Not Detected 20 Not DetectedChloromethane
0.98 Not Detected 2.5 Not DetectedVinyl Chloride
0.98 Not Detected 2.2 Not Detected1,3-Butadiene
9.8 Not Detected 38 Not DetectedBromomethane
3.9 Not Detected 10 Not DetectedChloroethane
0.98 Not Detected 5.5 Not DetectedFreon 11
3.9 Not Detected 7.4 Not DetectedEthanol
0.98 Not Detected 7.5 Not DetectedFreon 113
0.98 Not Detected 3.9 Not Detected1,1-Dichloroethene
9.8 19 23 46Acetone
3.9 Not Detected 9.7 Not Detected2-Propanol
3.9 Not Detected 12 Not DetectedCarbon Disulfide
3.9 Not Detected 12 Not Detected3-Chloropropene
9.8 Not Detected 34 Not DetectedMethylene Chloride
0.98 Not Detected 3.6 Not DetectedMethyl tert-butyl ether
0.98 Not Detected 3.9 Not Detectedtrans-1,2-Dichloroethene
0.98 34 3.5 120Hexane
0.98 Not Detected 4.0 Not Detected1,1-Dichloroethane
3.9 Not Detected 12 Not Detected2-Butanone (Methyl Ethyl Ketone)
0.98 Not Detected 3.9 Not Detectedcis-1,2-Dichloroethene
0.98 Not Detected 2.9 Not DetectedTetrahydrofuran
0.98 230 4.8 1100Chloroform
0.98 Not Detected 5.4 Not Detected1,1,1-Trichloroethane
0.98 Not Detected 3.4 Not DetectedCyclohexane
0.98 Not Detected 6.2 Not DetectedCarbon Tetrachloride
0.98 1.1 4.6 5.02,2,4-Trimethylpentane
0.98 1.8 3.1 5.7Benzene
0.98 Not Detected 4.0 Not Detected1,2-Dichloroethane
0.98 45 4.0 180Heptane
0.98 Not Detected 5.3 Not DetectedTrichloroethene
0.98 Not Detected 4.6 Not Detected1,2-Dichloropropane
3.9 Not Detected 14 Not Detected1,4-Dioxane
0.98 1.6 6.6 11Bromodichloromethane
0.98 Not Detected 4.5 Not Detectedcis-1,3-Dichloropropene
0.98 Not Detected 4.0 Not Detected4-Methyl-2-pentanone
0.98 8.6 3.7 32Toluene
0.98 Not Detected 4.5 Not Detectedtrans-1,3-Dichloropropene
0.98 Not Detected 5.4 Not Detected1,1,2-Trichloroethane
0.98 Not Detected 6.7 Not DetectedTetrachloroethene
3.9 Not Detected 16 Not Detected2-Hexanone
Page 12 of 31
Client Sample ID: SV8
Lab ID#: 1601347A-03A
EPA METHOD TO-15 GC/MS FULL SCAN
a012819File Name:
Dil. Factor:1.97
Date of Collection: 1/21/16 10:46:00 AM
Date of Analysis: 1/29/16 12:43 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.98 Not Detected 8.4 Not DetectedDibromochloromethane
0.98 Not Detected 7.6 Not Detected1,2-Dibromoethane (EDB)
0.98 Not Detected 4.5 Not DetectedChlorobenzene
0.98 3.4 4.3 15Ethyl Benzene
0.98 7.0 4.3 30m,p-Xylene
0.98 1.2 4.3 5.2o-Xylene
0.98 Not Detected 4.2 Not DetectedStyrene
0.98 Not Detected 10 Not DetectedBromoform
0.98 Not Detected 4.8 Not DetectedCumene
0.98 Not Detected 6.8 Not Detected1,1,2,2-Tetrachloroethane
0.98 Not Detected 4.8 Not DetectedPropylbenzene
0.98 1.2 4.8 6.04-Ethyltoluene
0.98 Not Detected 4.8 Not Detected1,3,5-Trimethylbenzene
0.98 Not Detected 4.8 Not Detected1,2,4-Trimethylbenzene
0.98 Not Detected 5.9 Not Detected1,3-Dichlorobenzene
0.98 Not Detected 5.9 Not Detected1,4-Dichlorobenzene
0.98 Not Detected 5.1 Not Detectedalpha-Chlorotoluene
0.98 Not Detected 5.9 Not Detected1,2-Dichlorobenzene
3.9 Not Detected UJ 29 Not Detected UJ1,2,4-Trichlorobenzene
3.9 Not Detected UJ 42 Not Detected UJHexachlorobutadiene
UJ = Analyte associated with low bias in the CCV and/or LCS.
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
96 70-130Toluene-d8
96 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 13 of 31
Client Sample ID: SV6
Lab ID#: 1601347A-04A
EPA METHOD TO-15 GC/MS FULL SCAN
a012820File Name:
Dil. Factor:4.36
Date of Collection: 1/21/16 11:31:00 AM
Date of Analysis: 1/29/16 01:21 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.2 Not Detected 11 Not DetectedFreon 12
2.2 Not Detected 15 Not DetectedFreon 114
22 Not Detected 45 Not DetectedChloromethane
2.2 Not Detected 5.6 Not DetectedVinyl Chloride
2.2 7.9 4.8 181,3-Butadiene
22 Not Detected 85 Not DetectedBromomethane
8.7 Not Detected 23 Not DetectedChloroethane
2.2 Not Detected 12 Not DetectedFreon 11
8.7 Not Detected 16 Not DetectedEthanol
2.2 Not Detected 17 Not DetectedFreon 113
2.2 Not Detected 8.6 Not Detected1,1-Dichloroethene
22 Not Detected 52 Not DetectedAcetone
8.7 Not Detected 21 Not Detected2-Propanol
8.7 Not Detected 27 Not DetectedCarbon Disulfide
8.7 Not Detected 27 Not Detected3-Chloropropene
22 Not Detected 76 Not DetectedMethylene Chloride
2.2 Not Detected 7.8 Not DetectedMethyl tert-butyl ether
2.2 Not Detected 8.6 Not Detectedtrans-1,2-Dichloroethene
2.2 220 7.7 790Hexane
2.2 Not Detected 8.8 Not Detected1,1-Dichloroethane
8.7 Not Detected 26 Not Detected2-Butanone (Methyl Ethyl Ketone)
2.2 Not Detected 8.6 Not Detectedcis-1,2-Dichloroethene
2.2 Not Detected 6.4 Not DetectedTetrahydrofuran
2.2 Not Detected 11 Not DetectedChloroform
2.2 Not Detected 12 Not Detected1,1,1-Trichloroethane
2.2 Not Detected 7.5 Not DetectedCyclohexane
2.2 Not Detected 14 Not DetectedCarbon Tetrachloride
2.2 34 10 1602,2,4-Trimethylpentane
2.2 41 7.0 130Benzene
2.2 Not Detected 8.8 Not Detected1,2-Dichloroethane
2.2 330 8.9 1300Heptane
2.2 Not Detected 12 Not DetectedTrichloroethene
2.2 Not Detected 10 Not Detected1,2-Dichloropropane
8.7 Not Detected 31 Not Detected1,4-Dioxane
2.2 Not Detected 15 Not DetectedBromodichloromethane
2.2 Not Detected 9.9 Not Detectedcis-1,3-Dichloropropene
2.2 Not Detected 8.9 Not Detected4-Methyl-2-pentanone
2.2 290 8.2 1100Toluene
2.2 Not Detected 9.9 Not Detectedtrans-1,3-Dichloropropene
2.2 Not Detected 12 Not Detected1,1,2-Trichloroethane
2.2 Not Detected 15 Not DetectedTetrachloroethene
8.7 Not Detected 36 Not Detected2-Hexanone
Page 14 of 31
Client Sample ID: SV6
Lab ID#: 1601347A-04A
EPA METHOD TO-15 GC/MS FULL SCAN
a012820File Name:
Dil. Factor:4.36
Date of Collection: 1/21/16 11:31:00 AM
Date of Analysis: 1/29/16 01:21 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.2 Not Detected 18 Not DetectedDibromochloromethane
2.2 Not Detected 17 Not Detected1,2-Dibromoethane (EDB)
2.2 Not Detected 10 Not DetectedChlorobenzene
2.2 70 9.5 300Ethyl Benzene
2.2 300 9.5 1300m,p-Xylene
2.2 56 9.5 240o-Xylene
2.2 Not Detected 9.3 Not DetectedStyrene
2.2 Not Detected 22 Not DetectedBromoform
2.2 4.2 11 20Cumene
2.2 Not Detected 15 Not Detected1,1,2,2-Tetrachloroethane
2.2 18 11 89Propylbenzene
2.2 71 11 3504-Ethyltoluene
2.2 21 11 1001,3,5-Trimethylbenzene
2.2 48 11 2301,2,4-Trimethylbenzene
2.2 Not Detected 13 Not Detected1,3-Dichlorobenzene
2.2 Not Detected 13 Not Detected1,4-Dichlorobenzene
2.2 Not Detected 11 Not Detectedalpha-Chlorotoluene
2.2 Not Detected 13 Not Detected1,2-Dichlorobenzene
8.7 Not Detected UJ 65 Not Detected UJ1,2,4-Trichlorobenzene
8.7 Not Detected UJ 93 Not Detected UJHexachlorobutadiene
UJ = Analyte associated with low bias in the CCV and/or LCS.
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
95 70-130Toluene-d8
100 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 15 of 31
Client Sample ID: SV2
Lab ID#: 1601347A-05A
EPA METHOD TO-15 GC/MS FULL SCAN
a012821File Name:
Dil. Factor:17.3
Date of Collection: 1/21/16 1:00:00 PM
Date of Analysis: 1/29/16 01:47 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
8.6 Not Detected 43 Not DetectedFreon 12
8.6 Not Detected 60 Not DetectedFreon 114
86 Not Detected 180 Not DetectedChloromethane
8.6 Not Detected 22 Not DetectedVinyl Chloride
8.6 13 19 291,3-Butadiene
86 Not Detected 340 Not DetectedBromomethane
35 Not Detected 91 Not DetectedChloroethane
8.6 Not Detected 49 Not DetectedFreon 11
35 39 65 74Ethanol
8.6 Not Detected 66 Not DetectedFreon 113
8.6 Not Detected 34 Not Detected1,1-Dichloroethene
86 Not Detected 200 Not DetectedAcetone
35 Not Detected 85 Not Detected2-Propanol
35 Not Detected 110 Not DetectedCarbon Disulfide
35 Not Detected 110 Not Detected3-Chloropropene
86 Not Detected 300 Not DetectedMethylene Chloride
8.6 Not Detected 31 Not DetectedMethyl tert-butyl ether
8.6 Not Detected 34 Not Detectedtrans-1,2-Dichloroethene
8.6 610 30 2200Hexane
8.6 Not Detected 35 Not Detected1,1-Dichloroethane
35 Not Detected 100 Not Detected2-Butanone (Methyl Ethyl Ketone)
8.6 Not Detected 34 Not Detectedcis-1,2-Dichloroethene
8.6 Not Detected 26 Not DetectedTetrahydrofuran
8.6 Not Detected 42 Not DetectedChloroform
8.6 Not Detected 47 Not Detected1,1,1-Trichloroethane
8.6 Not Detected 30 Not DetectedCyclohexane
8.6 Not Detected 54 Not DetectedCarbon Tetrachloride
8.6 180 40 8502,2,4-Trimethylpentane
8.6 27 28 85Benzene
8.6 Not Detected 35 Not Detected1,2-Dichloroethane
8.6 520 35 2100Heptane
8.6 Not Detected 46 Not DetectedTrichloroethene
8.6 Not Detected 40 Not Detected1,2-Dichloropropane
35 Not Detected 120 Not Detected1,4-Dioxane
8.6 Not Detected 58 Not DetectedBromodichloromethane
8.6 Not Detected 39 Not Detectedcis-1,3-Dichloropropene
8.6 Not Detected 35 Not Detected4-Methyl-2-pentanone
8.6 120 32 470Toluene
8.6 Not Detected 39 Not Detectedtrans-1,3-Dichloropropene
8.6 Not Detected 47 Not Detected1,1,2-Trichloroethane
8.6 Not Detected 59 Not DetectedTetrachloroethene
35 Not Detected 140 Not Detected2-Hexanone
Page 16 of 31
Client Sample ID: SV2
Lab ID#: 1601347A-05A
EPA METHOD TO-15 GC/MS FULL SCAN
a012821File Name:
Dil. Factor:17.3
Date of Collection: 1/21/16 1:00:00 PM
Date of Analysis: 1/29/16 01:47 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
8.6 Not Detected 74 Not DetectedDibromochloromethane
8.6 Not Detected 66 Not Detected1,2-Dibromoethane (EDB)
8.6 Not Detected 40 Not DetectedChlorobenzene
8.6 28 38 120Ethyl Benzene
8.6 98 38 430m,p-Xylene
8.6 15 38 67o-Xylene
8.6 Not Detected 37 Not DetectedStyrene
8.6 Not Detected 89 Not DetectedBromoform
8.6 Not Detected 42 Not DetectedCumene
8.6 Not Detected 59 Not Detected1,1,2,2-Tetrachloroethane
8.6 Not Detected 42 Not DetectedPropylbenzene
8.6 20 42 1004-Ethyltoluene
8.6 14 42 711,3,5-Trimethylbenzene
8.6 8.9 42 441,2,4-Trimethylbenzene
8.6 Not Detected 52 Not Detected1,3-Dichlorobenzene
8.6 Not Detected 52 Not Detected1,4-Dichlorobenzene
8.6 Not Detected 45 Not Detectedalpha-Chlorotoluene
8.6 Not Detected 52 Not Detected1,2-Dichlorobenzene
35 Not Detected UJ 260 Not Detected UJ1,2,4-Trichlorobenzene
35 Not Detected UJ 370 Not Detected UJHexachlorobutadiene
UJ = Analyte associated with low bias in the CCV and/or LCS.
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
96 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 17 of 31
Client Sample ID: SV3
Lab ID#: 1601347A-06A
EPA METHOD TO-15 GC/MS FULL SCAN
a012822File Name:
Dil. Factor:21.6
Date of Collection: 1/21/16 2:26:00 PM
Date of Analysis: 1/29/16 02:23 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
11 Not Detected 53 Not DetectedFreon 12
11 Not Detected 76 Not DetectedFreon 114
110 Not Detected 220 Not DetectedChloromethane
11 Not Detected 28 Not DetectedVinyl Chloride
11 30 24 661,3-Butadiene
110 Not Detected 420 Not DetectedBromomethane
43 Not Detected 110 Not DetectedChloroethane
11 Not Detected 61 Not DetectedFreon 11
43 Not Detected 81 Not DetectedEthanol
11 Not Detected 83 Not DetectedFreon 113
11 Not Detected 43 Not Detected1,1-Dichloroethene
110 Not Detected 260 Not DetectedAcetone
43 Not Detected 110 Not Detected2-Propanol
43 Not Detected 130 Not DetectedCarbon Disulfide
43 Not Detected 140 Not Detected3-Chloropropene
110 Not Detected 380 Not DetectedMethylene Chloride
11 Not Detected 39 Not DetectedMethyl tert-butyl ether
11 Not Detected 43 Not Detectedtrans-1,2-Dichloroethene
11 2500 38 8800Hexane
11 Not Detected 44 Not Detected1,1-Dichloroethane
43 Not Detected 130 Not Detected2-Butanone (Methyl Ethyl Ketone)
11 Not Detected 43 Not Detectedcis-1,2-Dichloroethene
11 Not Detected 32 Not DetectedTetrahydrofuran
11 Not Detected 53 Not DetectedChloroform
11 Not Detected 59 Not Detected1,1,1-Trichloroethane
11 Not Detected 37 Not DetectedCyclohexane
11 Not Detected 68 Not DetectedCarbon Tetrachloride
11 680 50 32002,2,4-Trimethylpentane
11 110 34 360Benzene
11 Not Detected 44 Not Detected1,2-Dichloroethane
11 1600 44 6400Heptane
11 Not Detected 58 Not DetectedTrichloroethene
11 Not Detected 50 Not Detected1,2-Dichloropropane
43 Not Detected 160 Not Detected1,4-Dioxane
11 Not Detected 72 Not DetectedBromodichloromethane
11 Not Detected 49 Not Detectedcis-1,3-Dichloropropene
11 Not Detected 44 Not Detected4-Methyl-2-pentanone
11 490 41 1800Toluene
11 Not Detected 49 Not Detectedtrans-1,3-Dichloropropene
11 Not Detected 59 Not Detected1,1,2-Trichloroethane
11 Not Detected 73 Not DetectedTetrachloroethene
43 Not Detected 180 Not Detected2-Hexanone
Page 18 of 31
Client Sample ID: SV3
Lab ID#: 1601347A-06A
EPA METHOD TO-15 GC/MS FULL SCAN
a012822File Name:
Dil. Factor:21.6
Date of Collection: 1/21/16 2:26:00 PM
Date of Analysis: 1/29/16 02:23 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
11 Not Detected 92 Not DetectedDibromochloromethane
11 Not Detected 83 Not Detected1,2-Dibromoethane (EDB)
11 Not Detected 50 Not DetectedChlorobenzene
11 90 47 390Ethyl Benzene
11 320 47 1400m,p-Xylene
11 58 47 250o-Xylene
11 Not Detected 46 Not DetectedStyrene
11 Not Detected 110 Not DetectedBromoform
11 Not Detected 53 Not DetectedCumene
11 Not Detected 74 Not Detected1,1,2,2-Tetrachloroethane
11 19 53 92Propylbenzene
11 66 53 3204-Ethyltoluene
11 21 53 1001,3,5-Trimethylbenzene
11 43 53 2101,2,4-Trimethylbenzene
11 Not Detected 65 Not Detected1,3-Dichlorobenzene
11 Not Detected 65 Not Detected1,4-Dichlorobenzene
11 Not Detected 56 Not Detectedalpha-Chlorotoluene
11 Not Detected 65 Not Detected1,2-Dichlorobenzene
43 Not Detected UJ 320 Not Detected UJ1,2,4-Trichlorobenzene
43 Not Detected UJ 460 Not Detected UJHexachlorobutadiene
UJ = Analyte associated with low bias in the CCV and/or LCS.
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
94 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 19 of 31
Client Sample ID: SV4
Lab ID#: 1601347A-07A
EPA METHOD TO-15 GC/MS FULL SCAN
a012823File Name:
Dil. Factor:6.38
Date of Collection: 1/21/16 3:37:00 PM
Date of Analysis: 1/29/16 02:49 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
3.2 Not Detected 16 Not DetectedFreon 12
3.2 Not Detected 22 Not DetectedFreon 114
32 Not Detected 66 Not DetectedChloromethane
3.2 Not Detected 8.2 Not DetectedVinyl Chloride
3.2 Not Detected 7.0 Not Detected1,3-Butadiene
32 Not Detected 120 Not DetectedBromomethane
13 Not Detected 34 Not DetectedChloroethane
3.2 Not Detected 18 Not DetectedFreon 11
13 Not Detected 24 Not DetectedEthanol
3.2 Not Detected 24 Not DetectedFreon 113
3.2 Not Detected 13 Not Detected1,1-Dichloroethene
32 Not Detected 76 Not DetectedAcetone
13 Not Detected 31 Not Detected2-Propanol
13 Not Detected 40 Not DetectedCarbon Disulfide
13 Not Detected 40 Not Detected3-Chloropropene
32 Not Detected 110 Not DetectedMethylene Chloride
3.2 Not Detected 12 Not DetectedMethyl tert-butyl ether
3.2 Not Detected 13 Not Detectedtrans-1,2-Dichloroethene
3.2 220 11 780Hexane
3.2 Not Detected 13 Not Detected1,1-Dichloroethane
13 Not Detected 38 Not Detected2-Butanone (Methyl Ethyl Ketone)
3.2 Not Detected 13 Not Detectedcis-1,2-Dichloroethene
3.2 Not Detected 9.4 Not DetectedTetrahydrofuran
3.2 Not Detected 16 Not DetectedChloroform
3.2 Not Detected 17 Not Detected1,1,1-Trichloroethane
3.2 Not Detected 11 Not DetectedCyclohexane
3.2 Not Detected 20 Not DetectedCarbon Tetrachloride
3.2 56 15 2602,2,4-Trimethylpentane
3.2 49 10 160Benzene
3.2 Not Detected 13 Not Detected1,2-Dichloroethane
3.2 520 13 2100Heptane
3.2 Not Detected 17 Not DetectedTrichloroethene
3.2 Not Detected 15 Not Detected1,2-Dichloropropane
13 Not Detected 46 Not Detected1,4-Dioxane
3.2 Not Detected 21 Not DetectedBromodichloromethane
3.2 Not Detected 14 Not Detectedcis-1,3-Dichloropropene
3.2 Not Detected 13 Not Detected4-Methyl-2-pentanone
3.2 460 12 1700Toluene
3.2 Not Detected 14 Not Detectedtrans-1,3-Dichloropropene
3.2 Not Detected 17 Not Detected1,1,2-Trichloroethane
3.2 Not Detected 22 Not DetectedTetrachloroethene
13 Not Detected 52 Not Detected2-Hexanone
Page 20 of 31
Client Sample ID: SV4
Lab ID#: 1601347A-07A
EPA METHOD TO-15 GC/MS FULL SCAN
a012823File Name:
Dil. Factor:6.38
Date of Collection: 1/21/16 3:37:00 PM
Date of Analysis: 1/29/16 02:49 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
3.2 Not Detected 27 Not DetectedDibromochloromethane
3.2 Not Detected 24 Not Detected1,2-Dibromoethane (EDB)
3.2 Not Detected 15 Not DetectedChlorobenzene
3.2 110 14 480Ethyl Benzene
3.2 560 14 2400m,p-Xylene
3.2 98 14 420o-Xylene
3.2 Not Detected 14 Not DetectedStyrene
3.2 Not Detected 33 Not DetectedBromoform
3.2 7.6 16 38Cumene
3.2 Not Detected 22 Not Detected1,1,2,2-Tetrachloroethane
3.2 29 16 140Propylbenzene
3.2 120 16 5804-Ethyltoluene
3.2 37 16 1801,3,5-Trimethylbenzene
3.2 80 16 3901,2,4-Trimethylbenzene
3.2 Not Detected 19 Not Detected1,3-Dichlorobenzene
3.2 Not Detected 19 Not Detected1,4-Dichlorobenzene
3.2 Not Detected 16 Not Detectedalpha-Chlorotoluene
3.2 Not Detected 19 Not Detected1,2-Dichlorobenzene
13 Not Detected UJ 95 Not Detected UJ1,2,4-Trichlorobenzene
13 Not Detected UJ 140 Not Detected UJHexachlorobutadiene
UJ = Analyte associated with low bias in the CCV and/or LCS.
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
96 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
103 70-1304-Bromofluorobenzene
Page 21 of 31
Client Sample ID: SV4 Dup
Lab ID#: 1601347A-08A
EPA METHOD TO-15 GC/MS FULL SCAN
a012824File Name:
Dil. Factor:7.58
Date of Collection: 1/21/16 3:31:00 PM
Date of Analysis: 1/29/16 03:28 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
3.8 Not Detected 19 Not DetectedFreon 12
3.8 Not Detected 26 Not DetectedFreon 114
38 Not Detected 78 Not DetectedChloromethane
3.8 Not Detected 9.7 Not DetectedVinyl Chloride
3.8 Not Detected 8.4 Not Detected1,3-Butadiene
38 Not Detected 150 Not DetectedBromomethane
15 Not Detected 40 Not DetectedChloroethane
3.8 Not Detected 21 Not DetectedFreon 11
15 Not Detected 28 Not DetectedEthanol
3.8 Not Detected 29 Not DetectedFreon 113
3.8 Not Detected 15 Not Detected1,1-Dichloroethene
38 Not Detected 90 Not DetectedAcetone
15 Not Detected 37 Not Detected2-Propanol
15 Not Detected 47 Not DetectedCarbon Disulfide
15 Not Detected 47 Not Detected3-Chloropropene
38 Not Detected 130 Not DetectedMethylene Chloride
3.8 Not Detected 14 Not DetectedMethyl tert-butyl ether
3.8 Not Detected 15 Not Detectedtrans-1,2-Dichloroethene
3.8 190 13 680Hexane
3.8 Not Detected 15 Not Detected1,1-Dichloroethane
15 Not Detected 45 Not Detected2-Butanone (Methyl Ethyl Ketone)
3.8 Not Detected 15 Not Detectedcis-1,2-Dichloroethene
3.8 Not Detected 11 Not DetectedTetrahydrofuran
3.8 Not Detected 18 Not DetectedChloroform
3.8 Not Detected 21 Not Detected1,1,1-Trichloroethane
3.8 Not Detected 13 Not DetectedCyclohexane
3.8 Not Detected 24 Not DetectedCarbon Tetrachloride
3.8 49 18 2302,2,4-Trimethylpentane
3.8 53 12 170Benzene
3.8 Not Detected 15 Not Detected1,2-Dichloroethane
3.8 460 16 1900Heptane
3.8 Not Detected 20 Not DetectedTrichloroethene
3.8 Not Detected 18 Not Detected1,2-Dichloropropane
15 Not Detected 55 Not Detected1,4-Dioxane
3.8 Not Detected 25 Not DetectedBromodichloromethane
3.8 Not Detected 17 Not Detectedcis-1,3-Dichloropropene
3.8 Not Detected 16 Not Detected4-Methyl-2-pentanone
3.8 520 14 1900Toluene
3.8 Not Detected 17 Not Detectedtrans-1,3-Dichloropropene
3.8 Not Detected 21 Not Detected1,1,2-Trichloroethane
3.8 Not Detected 26 Not DetectedTetrachloroethene
15 Not Detected 62 Not Detected2-Hexanone
Page 22 of 31
Client Sample ID: SV4 Dup
Lab ID#: 1601347A-08A
EPA METHOD TO-15 GC/MS FULL SCAN
a012824File Name:
Dil. Factor:7.58
Date of Collection: 1/21/16 3:31:00 PM
Date of Analysis: 1/29/16 03:28 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
3.8 Not Detected 32 Not DetectedDibromochloromethane
3.8 Not Detected 29 Not Detected1,2-Dibromoethane (EDB)
3.8 Not Detected 17 Not DetectedChlorobenzene
3.8 130 16 580Ethyl Benzene
3.8 660 16 2900m,p-Xylene
3.8 120 16 530o-Xylene
3.8 Not Detected 16 Not DetectedStyrene
3.8 Not Detected 39 Not DetectedBromoform
3.8 8.8 19 43Cumene
3.8 Not Detected 26 Not Detected1,1,2,2-Tetrachloroethane
3.8 36 19 180Propylbenzene
3.8 140 19 7104-Ethyltoluene
3.8 48 19 2401,3,5-Trimethylbenzene
3.8 100 19 5201,2,4-Trimethylbenzene
3.8 Not Detected 23 Not Detected1,3-Dichlorobenzene
3.8 Not Detected 23 Not Detected1,4-Dichlorobenzene
3.8 Not Detected 20 Not Detectedalpha-Chlorotoluene
3.8 Not Detected 23 Not Detected1,2-Dichlorobenzene
15 Not Detected UJ 110 Not Detected UJ1,2,4-Trichlorobenzene
15 Not Detected UJ 160 Not Detected UJHexachlorobutadiene
UJ = Analyte associated with low bias in the CCV and/or LCS.
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
95 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 23 of 31
Client Sample ID: Lab Blank
Lab ID#: 1601347A-09A
EPA METHOD TO-15 GC/MS FULL SCAN
a012807File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 04:26 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 2.5 Not DetectedFreon 12
0.50 Not Detected 3.5 Not DetectedFreon 114
5.0 Not Detected 10 Not DetectedChloromethane
0.50 Not Detected 1.3 Not DetectedVinyl Chloride
0.50 Not Detected 1.1 Not Detected1,3-Butadiene
5.0 Not Detected 19 Not DetectedBromomethane
2.0 Not Detected 5.3 Not DetectedChloroethane
0.50 Not Detected 2.8 Not DetectedFreon 11
2.0 Not Detected 3.8 Not DetectedEthanol
0.50 Not Detected 3.8 Not DetectedFreon 113
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethene
5.0 Not Detected 12 Not DetectedAcetone
2.0 Not Detected 4.9 Not Detected2-Propanol
2.0 Not Detected 6.2 Not DetectedCarbon Disulfide
2.0 Not Detected 6.3 Not Detected3-Chloropropene
5.0 Not Detected 17 Not DetectedMethylene Chloride
0.50 Not Detected 1.8 Not DetectedMethyl tert-butyl ether
0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene
0.50 Not Detected 1.8 Not DetectedHexane
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethane
2.0 Not Detected 5.9 Not Detected2-Butanone (Methyl Ethyl Ketone)
0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene
0.50 Not Detected 1.5 Not DetectedTetrahydrofuran
0.50 Not Detected 2.4 Not DetectedChloroform
0.50 Not Detected 2.7 Not Detected1,1,1-Trichloroethane
0.50 Not Detected 1.7 Not DetectedCyclohexane
0.50 Not Detected 3.1 Not DetectedCarbon Tetrachloride
0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane
0.50 Not Detected 1.6 Not DetectedBenzene
0.50 Not Detected 2.0 Not Detected1,2-Dichloroethane
0.50 Not Detected 2.0 Not DetectedHeptane
0.50 Not Detected 2.7 Not DetectedTrichloroethene
0.50 Not Detected 2.3 Not Detected1,2-Dichloropropane
2.0 Not Detected 7.2 Not Detected1,4-Dioxane
0.50 Not Detected 3.4 Not DetectedBromodichloromethane
0.50 Not Detected 2.3 Not Detectedcis-1,3-Dichloropropene
0.50 Not Detected 2.0 Not Detected4-Methyl-2-pentanone
0.50 Not Detected 1.9 Not DetectedToluene
0.50 Not Detected 2.3 Not Detectedtrans-1,3-Dichloropropene
0.50 Not Detected 2.7 Not Detected1,1,2-Trichloroethane
0.50 Not Detected 3.4 Not DetectedTetrachloroethene
2.0 Not Detected 8.2 Not Detected2-Hexanone
Page 24 of 31
Client Sample ID: Lab Blank
Lab ID#: 1601347A-09A
EPA METHOD TO-15 GC/MS FULL SCAN
a012807File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 04:26 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 4.2 Not DetectedDibromochloromethane
0.50 Not Detected 3.8 Not Detected1,2-Dibromoethane (EDB)
0.50 Not Detected 2.3 Not DetectedChlorobenzene
0.50 Not Detected 2.2 Not DetectedEthyl Benzene
0.50 Not Detected 2.2 Not Detectedm,p-Xylene
0.50 Not Detected 2.2 Not Detectedo-Xylene
0.50 Not Detected 2.1 Not DetectedStyrene
0.50 Not Detected 5.2 Not DetectedBromoform
0.50 Not Detected 2.4 Not DetectedCumene
0.50 Not Detected 3.4 Not Detected1,1,2,2-Tetrachloroethane
0.50 Not Detected 2.4 Not DetectedPropylbenzene
0.50 Not Detected 2.4 Not Detected4-Ethyltoluene
0.50 Not Detected 2.4 Not Detected1,3,5-Trimethylbenzene
0.50 Not Detected 2.4 Not Detected1,2,4-Trimethylbenzene
0.50 Not Detected 3.0 Not Detected1,3-Dichlorobenzene
0.50 Not Detected 3.0 Not Detected1,4-Dichlorobenzene
0.50 Not Detected 2.6 Not Detectedalpha-Chlorotoluene
0.50 Not Detected 3.0 Not Detected1,2-Dichlorobenzene
2.0 Not Detected UJ 15 Not Detected UJ1,2,4-Trichlorobenzene
2.0 Not Detected UJ 21 Not Detected UJHexachlorobutadiene
UJ = Analyte associated with low bias in the CCV and/or LCS.
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
96 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 25 of 31
Client Sample ID: CCV
Lab ID#: 1601347A-10A
EPA METHOD TO-15 GC/MS FULL SCAN
a012802File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 12:56 PM
%RecoveryCompound
90Freon 12
90Freon 114
87Chloromethane
96Vinyl Chloride
901,3-Butadiene
95Bromomethane
94Chloroethane
89Freon 11
87Ethanol
88Freon 113
851,1-Dichloroethene
98Acetone
832-Propanol
95Carbon Disulfide
903-Chloropropene
88Methylene Chloride
87Methyl tert-butyl ether
88trans-1,2-Dichloroethene
90Hexane
941,1-Dichloroethane
892-Butanone (Methyl Ethyl Ketone)
85cis-1,2-Dichloroethene
76Tetrahydrofuran
86Chloroform
781,1,1-Trichloroethane
85Cyclohexane
82Carbon Tetrachloride
862,2,4-Trimethylpentane
90Benzene
901,2-Dichloroethane
89Heptane
81Trichloroethene
851,2-Dichloropropane
901,4-Dioxane
87Bromodichloromethane
83cis-1,3-Dichloropropene
764-Methyl-2-pentanone
83Toluene
87trans-1,3-Dichloropropene
901,1,2-Trichloroethane
87Tetrachloroethene
882-Hexanone
Page 26 of 31
Client Sample ID: CCV
Lab ID#: 1601347A-10A
EPA METHOD TO-15 GC/MS FULL SCAN
a012802File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 12:56 PM
%RecoveryCompound
86Dibromochloromethane
871,2-Dibromoethane (EDB)
86Chlorobenzene
86Ethyl Benzene
85m,p-Xylene
85o-Xylene
88Styrene
85Bromoform
84Cumene
891,1,2,2-Tetrachloroethane
84Propylbenzene
834-Ethyltoluene
861,3,5-Trimethylbenzene
841,2,4-Trimethylbenzene
821,3-Dichlorobenzene
821,4-Dichlorobenzene
81alpha-Chlorotoluene
821,2-Dichlorobenzene
69 Q1,2,4-Trichlorobenzene
66 QHexachlorobutadiene
Q = Exceeds Quality Control limits.
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
96 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
103 70-1304-Bromofluorobenzene
Page 27 of 31
Client Sample ID: LCS
Lab ID#: 1601347A-11A
EPA METHOD TO-15 GC/MS FULL SCAN
a012803File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 01:20 PM
Limits%RecoveryCompound
Method
88 70-130Freon 12
92 70-130Freon 114
84 70-130Chloromethane
97 70-130Vinyl Chloride
84 70-1301,3-Butadiene
95 70-130Bromomethane
97 70-130Chloroethane
91 70-130Freon 11
88 70-130Ethanol
86 70-130Freon 113
82 70-1301,1-Dichloroethene
98 70-130Acetone
83 70-1302-Propanol
81 70-130Carbon Disulfide
85 70-1303-Chloropropene
88 70-130Methylene Chloride
85 70-130Methyl tert-butyl ether
90 70-130trans-1,2-Dichloroethene
89 70-130Hexane
94 70-1301,1-Dichloroethane
85 70-1302-Butanone (Methyl Ethyl Ketone)
86 70-130cis-1,2-Dichloroethene
74 70-130Tetrahydrofuran
86 70-130Chloroform
78 70-1301,1,1-Trichloroethane
86 70-130Cyclohexane
81 70-130Carbon Tetrachloride
86 70-1302,2,4-Trimethylpentane
92 70-130Benzene
89 70-1301,2-Dichloroethane
88 70-130Heptane
87 70-130Trichloroethene
86 70-1301,2-Dichloropropane
86 70-1301,4-Dioxane
90 70-130Bromodichloromethane
79 70-130cis-1,3-Dichloropropene
76 70-1304-Methyl-2-pentanone
83 70-130Toluene
84 70-130trans-1,3-Dichloropropene
89 70-1301,1,2-Trichloroethane
86 70-130Tetrachloroethene
83 70-1302-Hexanone
Page 28 of 31
Client Sample ID: LCS
Lab ID#: 1601347A-11A
EPA METHOD TO-15 GC/MS FULL SCAN
a012803File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 01:20 PM
Limits%RecoveryCompound
Method
84 70-130Dibromochloromethane
86 70-1301,2-Dibromoethane (EDB)
84 70-130Chlorobenzene
83 70-130Ethyl Benzene
82 70-130m,p-Xylene
84 70-130o-Xylene
82 70-130Styrene
85 70-130Bromoform
82 70-130Cumene
80 70-1301,1,2,2-Tetrachloroethane
84 70-130Propylbenzene
83 70-1304-Ethyltoluene
82 70-1301,3,5-Trimethylbenzene
82 70-1301,2,4-Trimethylbenzene
82 70-1301,3-Dichlorobenzene
80 70-1301,4-Dichlorobenzene
82 70-130alpha-Chlorotoluene
81 70-1301,2-Dichlorobenzene
80 70-1301,2,4-Trichlorobenzene
77 70-130Hexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
97 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 29 of 31
Client Sample ID: LCSD
Lab ID#: 1601347A-11AA
EPA METHOD TO-15 GC/MS FULL SCAN
a012804File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 01:57 PM
Limits%RecoveryCompound
Method
88 70-130Freon 12
91 70-130Freon 114
82 70-130Chloromethane
96 70-130Vinyl Chloride
85 70-1301,3-Butadiene
94 70-130Bromomethane
98 70-130Chloroethane
90 70-130Freon 11
86 70-130Ethanol
87 70-130Freon 113
84 70-1301,1-Dichloroethene
96 70-130Acetone
82 70-1302-Propanol
83 70-130Carbon Disulfide
86 70-1303-Chloropropene
87 70-130Methylene Chloride
85 70-130Methyl tert-butyl ether
88 70-130trans-1,2-Dichloroethene
88 70-130Hexane
92 70-1301,1-Dichloroethane
87 70-1302-Butanone (Methyl Ethyl Ketone)
86 70-130cis-1,2-Dichloroethene
74 70-130Tetrahydrofuran
85 70-130Chloroform
77 70-1301,1,1-Trichloroethane
86 70-130Cyclohexane
81 70-130Carbon Tetrachloride
87 70-1302,2,4-Trimethylpentane
93 70-130Benzene
90 70-1301,2-Dichloroethane
88 70-130Heptane
88 70-130Trichloroethene
87 70-1301,2-Dichloropropane
85 70-1301,4-Dioxane
90 70-130Bromodichloromethane
78 70-130cis-1,3-Dichloropropene
76 70-1304-Methyl-2-pentanone
84 70-130Toluene
88 70-130trans-1,3-Dichloropropene
88 70-1301,1,2-Trichloroethane
86 70-130Tetrachloroethene
86 70-1302-Hexanone
Page 30 of 31
Client Sample ID: LCSD
Lab ID#: 1601347A-11AA
EPA METHOD TO-15 GC/MS FULL SCAN
a012804File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 01:57 PM
Limits%RecoveryCompound
Method
86 70-130Dibromochloromethane
88 70-1301,2-Dibromoethane (EDB)
85 70-130Chlorobenzene
86 70-130Ethyl Benzene
85 70-130m,p-Xylene
86 70-130o-Xylene
84 70-130Styrene
88 70-130Bromoform
84 70-130Cumene
83 70-1301,1,2,2-Tetrachloroethane
86 70-130Propylbenzene
87 70-1304-Ethyltoluene
84 70-1301,3,5-Trimethylbenzene
86 70-1301,2,4-Trimethylbenzene
85 70-1301,3-Dichlorobenzene
85 70-1301,4-Dichlorobenzene
85 70-130alpha-Chlorotoluene
85 70-1301,2-Dichlorobenzene
88 70-1301,2,4-Trichlorobenzene
84 70-130Hexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
96 70-130Toluene-d8
95 70-1301,2-Dichloroethane-d4
103 70-1304-Bromofluorobenzene
Page 31 of 31
1/29/2016
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte NC 28269
Project Name: WCPSS
Project #: 20160086.001A
Dear Mr. Michael Sussman
The following report includes the data for the above referenced project for sample(s)
received on 1/26/2016 at Air Toxics Ltd.
The data and associated QC analyzed by Modified ASTM D-1946 are compliant with
the project requirements or laboratory criteria with the exception of the deviations
noted in the attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contactthe Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1601347B
Page 1 of 18
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
WORK ORDER #:1601347B
CLIENT:BILL TO:
PHONE:
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
704-598-1049
704-598-1050
01/26/2016
DATE COMPLETED:01/29/2016
P.O. #
PROJECT #20160086.001A WCPSS
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A SV1 Modified ASTM D-1946 4.1 "Hg 14.4 psi
02A SV7 Modified ASTM D-1946 2.2 "Hg 14.8 psi
03A SV8 Modified ASTM D-1946 0.4 psi 15.1 psi
04A SV6 Modified ASTM D-1946 16.1 "Hg 15 psi
05A SV2 Modified ASTM D-1946 26.5 "Hg 15 psi
06A SV3 Modified ASTM D-1946 16.0 "Hg 15 psi
07A SV4 Modified ASTM D-1946 20.5 "Hg 15 psi
08A SV4 Dup Modified ASTM D-1946 22.0 "Hg 15 psi
09A Lab Blank Modified ASTM D-1946 NA NA
09B Lab Blank Modified ASTM D-1946 NA NA
10A LCS Modified ASTM D-1946 NA NA
10AA LCSD Modified ASTM D-1946 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2014, Expiration date: 10/17/2015.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
[phone] . [phone] . FAX [phone]
01/29/16
Page 2 of 18
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704343-14-7, UT NELAP CA009332014-5, VA NELAP - 460197, WA NELAP - C935
LABORATORY NARRATIVEModified ASTM D-1946Kleinfelder Southeast, Inc.Workorder# 1601347B
Eight 1 Liter Summa Canister samples were received on January 26, 2016. The laboratory performed
analysis via Modified ASTM Method D-1946 for Methane and fixed gases in air using GC/FID or
GC/TCD. The method involves direct injection of 1.0 mL of sample.
On the analytical column employed for this analysis, Oxygen coelutes with Argon. The corresponding
peak is quantitated as Oxygen.
Since Nitrogen is used to pressurize samples, the reported Nitrogen values are calculated by adding all
the sample components and subtracting from 100%.
Method modifications taken to run these samples are summarized in the table below. Specific project
requirements may over-ride the ATL modifications.
Requirement ATL ModificationsASTM D-1946
Calibration A single point
calibration is
performed using a
reference standard
closely matching the
composition of the
unknown.
A minimum of 5-point calibration curve is performed.
Quantitation is based on average Response Factor.
Reference Standard The composition of any
reference standard
must be known to
within 0.01 mol % for
any component.
The standards used by ATL are blended to a >/= 95%
accuracy.
Sample Injection Volume Components whose
concentrations are in
excess of 5 % should
not be analyzed by
using sample volumes
greater than 0.5 mL.
The sample container is connected directly to a fixed
volume sample loop of 1.0 mL on the GC. Linear range
is defined by the calibration curve. Bags are loaded by
vacuum.
Normalization Normalize the mole
percent values by
multiplying each value
by 100 and dividing by
the sum of the original
values. The sum of the
original values should
not differ from 100%
by more than 1.0%.
Results are not normalized. The sum of the reported
values can differ from 100% by as much as 15%, either
due to analytical variability or an unusual sample matrix.
Precision Precision requirements
established at each
concentration level.
Duplicates should agree within 25% RPD for detections
> 5 X's the RL.
Page 3 of 18
Receiving Notes
There was a significant difference (greater than 5.0" Hg) between the measured canister receipt
vacuum and that which was reported on the Chain of Custody (COC) for sample SV8. A leak test
indicated that the valve was functioning properly.
Samples SV6, SV2, SV3, SV4 and SV4 Dup were received with significant vacuum remaining in the
canister. The residual canister vacuum resulted in elevated reporting limits.
There were no analytical discrepancies.
Analytical Notes
Seven qualifiers may have been used on the data analysis sheets and indicate as follows:
B - Compound present in laboratory blank greater than reporting limit.
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the detection limit.
M - Reported value may be biased due to apparent matrix interferences.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 4 of 18
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
Summary of Detected Compounds
Client Sample ID: SV1
Lab ID#: 1601347B-01A
(%)(%)Compound
AmountRpt. Limit
0.23 9.8Oxygen
0.23 82Nitrogen
0.00023 1.2Methane
0.023 7.2Carbon Dioxide
Client Sample ID: SV7
Lab ID#: 1601347B-02A
(%)(%)Compound
AmountRpt. Limit
0.22 6.5Oxygen
0.22 78Nitrogen
0.00022 8.2Methane
0.022 6.8Carbon Dioxide
Client Sample ID: SV8
Lab ID#: 1601347B-03A
(%)(%)Compound
AmountRpt. Limit
0.20 1.7Oxygen
0.20 70Nitrogen
0.00020 9.9Methane
0.020 18Carbon Dioxide
Client Sample ID: SV6
Lab ID#: 1601347B-04A
(%)(%)Compound
AmountRpt. Limit
0.44 20Oxygen
0.44 79Nitrogen
0.00044 0.0041Methane
0.044 1.1Carbon Dioxide
Page 5 of 18
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
Summary of Detected Compounds
Client Sample ID: SV2
Lab ID#: 1601347B-05A
(%)(%)Compound
AmountRpt. Limit
1.7 13Oxygen
1.7 86Nitrogen
0.17 0.54Carbon Dioxide
Client Sample ID: SV3
Lab ID#: 1601347B-06A
(%)(%)Compound
AmountRpt. Limit
0.43 19Oxygen
0.43 79Nitrogen
0.00043 0.00057Methane
0.043 1.5Carbon Dioxide
Client Sample ID: SV4
Lab ID#: 1601347B-07A
(%)(%)Compound
AmountRpt. Limit
0.64 19Oxygen
0.64 80Nitrogen
0.064 0.99Carbon Dioxide
Client Sample ID: SV4 Dup
Lab ID#: 1601347B-08A
(%)(%)Compound
AmountRpt. Limit
0.76 20Oxygen
0.76 79Nitrogen
0.076 0.89Carbon Dioxide
0.38 0.38Helium
Page 6 of 18
Client Sample ID: SV1
Lab ID#: 1601347B-01A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012812File Name:
Dil. Factor:2.29
Date of Collection: 1/21/16 9:28:00 AM
Date of Analysis: 1/28/16 12:10 PM
(%)(%)Compound
AmountRpt. Limit
0.23 9.8Oxygen
0.23 82Nitrogen
0.023 Not DetectedCarbon Monoxide
0.00023 1.2Methane
0.023 7.2Carbon Dioxide
0.0023 Not DetectedEthane
0.0023 Not DetectedEthene
0.11 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 7 of 18
Client Sample ID: SV7
Lab ID#: 1601347B-02A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012813File Name:
Dil. Factor:2.17
Date of Collection: 1/21/16 10:10:00 AM
Date of Analysis: 1/28/16 12:42 PM
(%)(%)Compound
AmountRpt. Limit
0.22 6.5Oxygen
0.22 78Nitrogen
0.022 Not DetectedCarbon Monoxide
0.00022 8.2Methane
0.022 6.8Carbon Dioxide
0.0022 Not DetectedEthane
0.0022 Not DetectedEthene
0.11 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 8 of 18
Client Sample ID: SV8
Lab ID#: 1601347B-03A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012814File Name:
Dil. Factor:1.97
Date of Collection: 1/21/16 10:46:00 AM
Date of Analysis: 1/28/16 01:35 PM
(%)(%)Compound
AmountRpt. Limit
0.20 1.7Oxygen
0.20 70Nitrogen
0.020 Not DetectedCarbon Monoxide
0.00020 9.9Methane
0.020 18Carbon Dioxide
0.0020 Not DetectedEthane
0.0020 Not DetectedEthene
0.098 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 9 of 18
Client Sample ID: SV6
Lab ID#: 1601347B-04A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012823File Name:
Dil. Factor:4.37
Date of Collection: 1/21/16 11:31:00 AM
Date of Analysis: 1/28/16 07:15 PM
(%)(%)Compound
AmountRpt. Limit
0.44 20Oxygen
0.44 79Nitrogen
0.044 Not DetectedCarbon Monoxide
0.00044 0.0041Methane
0.044 1.1Carbon Dioxide
0.0044 Not DetectedEthane
0.0044 Not DetectedEthene
0.22 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 10 of 18
Client Sample ID: SV2
Lab ID#: 1601347B-05A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012816File Name:
Dil. Factor:17.3
Date of Collection: 1/21/16 1:00:00 PM
Date of Analysis: 1/28/16 02:51 PM
(%)(%)Compound
AmountRpt. Limit
1.7 13Oxygen
1.7 86Nitrogen
0.17 Not DetectedCarbon Monoxide
0.0017 Not DetectedMethane
0.17 0.54Carbon Dioxide
0.017 Not DetectedEthane
0.017 Not DetectedEthene
0.87 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 11 of 18
Client Sample ID: SV3
Lab ID#: 1601347B-06A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012817File Name:
Dil. Factor:4.33
Date of Collection: 1/21/16 2:26:00 PM
Date of Analysis: 1/28/16 03:23 PM
(%)(%)Compound
AmountRpt. Limit
0.43 19Oxygen
0.43 79Nitrogen
0.043 Not DetectedCarbon Monoxide
0.00043 0.00057Methane
0.043 1.5Carbon Dioxide
0.0043 Not DetectedEthane
0.0043 Not DetectedEthene
0.22 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 12 of 18
Client Sample ID: SV4
Lab ID#: 1601347B-07A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012818File Name:
Dil. Factor:6.38
Date of Collection: 1/21/16 3:37:00 PM
Date of Analysis: 1/28/16 04:07 PM
(%)(%)Compound
AmountRpt. Limit
0.64 19Oxygen
0.64 80Nitrogen
0.064 Not DetectedCarbon Monoxide
0.00064 Not DetectedMethane
0.064 0.99Carbon Dioxide
0.0064 Not DetectedEthane
0.0064 Not DetectedEthene
0.32 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 13 of 18
Client Sample ID: SV4 Dup
Lab ID#: 1601347B-08A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012819File Name:
Dil. Factor:7.58
Date of Collection: 1/21/16 3:31:00 PM
Date of Analysis: 1/28/16 05:02 PM
(%)(%)Compound
AmountRpt. Limit
0.76 20Oxygen
0.76 79Nitrogen
0.076 Not DetectedCarbon Monoxide
0.00076 Not DetectedMethane
0.076 0.89Carbon Dioxide
0.0076 Not DetectedEthane
0.0076 Not DetectedEthene
0.38 0.38Helium
Container Type: 1 Liter Summa Canister
Page 14 of 18
Client Sample ID: Lab Blank
Lab ID#: 1601347B-09A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012804File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 08:32 AM
(%)(%)Compound
AmountRpt. Limit
0.10 Not DetectedOxygen
0.10 Not DetectedNitrogen
0.010 Not DetectedCarbon Monoxide
0.00010 Not DetectedMethane
0.010 Not DetectedCarbon Dioxide
0.0010 Not DetectedEthane
0.0010 Not DetectedEthene
Container Type: NA - Not Applicable
Page 15 of 18
Client Sample ID: Lab Blank
Lab ID#: 1601347B-09B
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012805cFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 09:01 AM
(%)(%)Compound
AmountRpt. Limit
0.050 Not DetectedHelium
Container Type: NA - Not Applicable
Page 16 of 18
Client Sample ID: LCS
Lab ID#: 1601347B-10A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012802File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 07:40 AM
Limits%RecoveryCompound
Method
100 85-115Oxygen
93 85-115Nitrogen
95 85-115Carbon Monoxide
99 85-115Methane
98 85-115Carbon Dioxide
99 85-115Ethane
100 85-115Ethene
107 85-115Helium
Container Type: NA - Not Applicable
Page 17 of 18
Client Sample ID: LCSD
Lab ID#: 1601347B-10AA
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10012827File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 1/28/16 09:04 PM
Limits%RecoveryCompound
Method
100 85-115Oxygen
93 85-115Nitrogen
94 85-115Carbon Monoxide
101 85-115Methane
100 85-115Carbon Dioxide
100 85-115Ethane
101 85-115Ethene
104 85-115Helium
Container Type: NA - Not Applicable
Page 18 of 18
2/17/2016
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte NC 28269
Project Name: E43
Project #: 20160086.001A
Dear Mr. Michael Sussman
The following report includes the data for the above referenced project for sample(s)
received on 2/12/2016 at Air Toxics Ltd.
The data and associated QC analyzed by TO-15 are compliant with the project
requirements or laboratory criteria with the exception of the deviations noted in the
attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contactthe Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1602234A
Page 1 of 40
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
WORK ORDER #:1602234A
CLIENT:BILL TO:
PHONE:
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
704-598-1049
704-598-1050
02/12/2016
DATE COMPLETED:02/17/2016
P.O. #
PROJECT #20160086.001A E43
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A SV3 TO-15 25.5 "Hg 15 psi
02A SV10 TO-15 7.0 "Hg 15 psi
03A SV9 TO-15 27.0 "Hg 15 psi
04A SV14 TO-15 6.5 "Hg 15 psi
05A SV13 TO-15 19 "Hg 15 psi
06A SV1 TO-15 16 "Hg 15 psi
07A SV16 TO-15 26.5 "Hg 15 psi
08A SV8 TO-15 7.0 "Hg 15 psi
09A SV7 TO-15 6.0 "Hg 15 psi
10A Lab Blank TO-15 NA NA
10B Lab Blank TO-15 NA NA
11A CCV TO-15 NA NA
11B CCV TO-15 NA NA
12A LCS TO-15 NA NA
12AA LCSD TO-15 NA NA
12B LCS TO-15 NA NA
12BB LCSD TO-15 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2014, Expiration date: 10/17/2015.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
[phone] . [phone] . FAX [phone]
02/17/16
Page 2 of 40
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704343-14-7, UT NELAP CA009332014-5, VA NELAP - 460197, WA NELAP - C935
LABORATORY NARRATIVEEPA Method TO-15Kleinfelder Southeast, Inc.Workorder# 1602234A
Nine 1 Liter Summa Canister samples were received on February 12, 2016. The laboratory performed
analysis via EPA Method TO-15 using GC/MS in the full scan mode.
This workorder was independently validated prior to submittal using 'USEPA National Functional
Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based, logic
driven, independent validation engine was employed to assess completeness, evaluate pass/fail of relevant
project quality control requirements and verification of all quantified amounts.
Samples SV3, SV9, SV13, SV1 and SV16 were received with significant vacuum remaining in the
canister. The residual canister vacuum resulted in elevated reporting limits.
Sample collection date was incomplete on the Chain of Custody for samples SV3, SV10, SV9, SV14,
SV13, SV1, SV16, SV8 and SV7. The year of collection was assumed to be 2016.
Receiving Notes
Dilution was performed on sample SV8 due to the presence of high level target species.
All Quality Control Limit exceedances and affected sample results are noted by flags. Each flag is defined
at the bottom of this Case Narrative and on each Sample Result Summary page. Target compound
non-detects in the samples that are associated with high bias in CCV analyses have not been flagged.
Analytical Notes
Eight qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction not
performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. See
data page for project specific U-flag definition.
UJ- Non-detected compound associated with low bias in the CCV
N - The identification is based on presumptive evidence.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 3 of 40
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SV3
Lab ID#: 1602234A-01A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
27 48 66 1202-Propanol
6.8 160 24 560Hexane
27 30 80 892-Butanone (Methyl Ethyl Ketone)
6.8 140 32 6502,2,4-Trimethylpentane
6.8 40 28 170Heptane
6.8 23 25 88Toluene
6.8 16 29 72m,p-Xylene
Client Sample ID: SV10
Lab ID#: 1602234A-02A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 2.1 5.0 7.9Toluene
Client Sample ID: SV9
Lab ID#: 1602234A-03A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
10 60 38 220Toluene
10 12 44 51Ethyl Benzene
10 74 44 320m,p-Xylene
10 22 44 94o-Xylene
10 10 43 43Styrene
10 10 50 504-Ethyltoluene
10 13 50 621,2,4-Trimethylbenzene
Client Sample ID: SV14
Lab ID#: 1602234A-04A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 8.3 4.5 29Hexane
1.3 5.6 6.3 28Chloroform
Page 4 of 40
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SV14
Lab ID#: 1602234A-04A
1.3 8.2 6.0 382,2,4-Trimethylpentane
1.3 5.5 4.1 18Benzene
1.3 48 5.3 200Heptane
1.3 80 4.9 300Toluene
1.3 37 5.6 160Ethyl Benzene
1.3 210 5.6 900m,p-Xylene
1.3 40 5.6 180o-Xylene
1.3 6.7 5.5 28Styrene
1.3 3.5 6.3 17Cumene
1.3 12 6.3 61Propylbenzene
1.3 49 6.3 2404-Ethyltoluene
1.3 19 6.3 931,3,5-Trimethylbenzene
1.3 38 6.3 1901,2,4-Trimethylbenzene
Client Sample ID: SV13
Lab ID#: 1602234A-05A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.8 34 6.1 751,3-Butadiene
11 18 34 58Carbon Disulfide
2.8 46 9.7 160Hexane
2.8 29 13 1402,2,4-Trimethylpentane
2.8 8.4 8.8 27Benzene
2.8 7.8 11 32Heptane
2.8 120 10 460Toluene
2.8 45 12 200Ethyl Benzene
2.8 300 12 1300m,p-Xylene
2.8 60 12 260o-Xylene
2.8 6.0 12 25Styrene
2.8 6.6 14 32Cumene
2.8 15 14 74Propylbenzene
2.8 86 14 4204-Ethyltoluene
2.8 50 14 2401,3,5-Trimethylbenzene
2.8 68 14 3401,2,4-Trimethylbenzene
Page 5 of 40
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SV1
Lab ID#: 1602234A-06A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.2 3.0 10 142,2,4-Trimethylpentane
2.2 3.1 8.2 12Toluene
2.2 8.6 9.4 38Ethyl Benzene
Client Sample ID: SV16
Lab ID#: 1602234A-07A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
8.6 26 30 93Hexane
35 42 100 1202-Butanone (Methyl Ethyl Ketone)
8.6 16 26 48Tetrahydrofuran
8.6 12 40 572,2,4-Trimethylpentane
8.6 45 35 180Heptane
8.6 36 32 140Toluene
8.6 21 38 93m,p-Xylene
Client Sample ID: SV8
Lab ID#: 1602234A-08A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.6 36 9.3 130Hexane
2.6 610 13 3000Chloroform
2.6 16 11 65Heptane
2.6 9.2 18 62Bromodichloromethane
2.6 2.7 9.9 10Toluene
Client Sample ID: SV7
Lab ID#: 1602234A-09A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 14 4.4 48Hexane
1.3 1.3 6.2 6.2Chloroform
Page 6 of 40
Client Sample ID: SV3
Lab ID#: 1602234A-01A
EPA METHOD TO-15 GC/MS FULL SCAN
p021510File Name:
Dil. Factor:13.5
Date of Collection: 2/10/16 1:20:00 PM
Date of Analysis: 2/15/16 09:46 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
6.8 Not Detected 33 Not DetectedFreon 12
6.8 Not Detected 47 Not DetectedFreon 114
68 Not Detected 140 Not DetectedChloromethane
6.8 Not Detected 17 Not DetectedVinyl Chloride
6.8 Not Detected 15 Not Detected1,3-Butadiene
68 Not Detected 260 Not DetectedBromomethane
27 Not Detected 71 Not DetectedChloroethane
6.8 Not Detected 38 Not DetectedFreon 11
27 Not Detected 51 Not DetectedEthanol
6.8 Not Detected 52 Not DetectedFreon 113
6.8 Not Detected 27 Not Detected1,1-Dichloroethene
68 Not Detected 160 Not DetectedAcetone
27 48 66 1202-Propanol
27 Not Detected 84 Not DetectedCarbon Disulfide
27 Not Detected 84 Not Detected3-Chloropropene
68 Not Detected 230 Not DetectedMethylene Chloride
6.8 Not Detected 24 Not DetectedMethyl tert-butyl ether
6.8 Not Detected 27 Not Detectedtrans-1,2-Dichloroethene
6.8 160 24 560Hexane
6.8 Not Detected 27 Not Detected1,1-Dichloroethane
27 30 80 892-Butanone (Methyl Ethyl Ketone)
6.8 Not Detected 27 Not Detectedcis-1,2-Dichloroethene
6.8 Not Detected 20 Not DetectedTetrahydrofuran
6.8 Not Detected 33 Not DetectedChloroform
6.8 Not Detected 37 Not Detected1,1,1-Trichloroethane
6.8 Not Detected 23 Not DetectedCyclohexane
6.8 Not Detected 42 Not DetectedCarbon Tetrachloride
6.8 140 32 6502,2,4-Trimethylpentane
6.8 Not Detected 22 Not DetectedBenzene
6.8 Not Detected 27 Not Detected1,2-Dichloroethane
6.8 40 28 170Heptane
6.8 Not Detected 36 Not DetectedTrichloroethene
6.8 Not Detected 31 Not Detected1,2-Dichloropropane
27 Not Detected 97 Not Detected1,4-Dioxane
6.8 Not Detected 45 Not DetectedBromodichloromethane
6.8 Not Detected 31 Not Detectedcis-1,3-Dichloropropene
6.8 Not Detected 28 Not Detected4-Methyl-2-pentanone
6.8 23 25 88Toluene
6.8 Not Detected 31 Not Detectedtrans-1,3-Dichloropropene
6.8 Not Detected 37 Not Detected1,1,2-Trichloroethane
6.8 Not Detected 46 Not DetectedTetrachloroethene
27 Not Detected 110 Not Detected2-Hexanone
Page 7 of 40
Client Sample ID: SV3
Lab ID#: 1602234A-01A
EPA METHOD TO-15 GC/MS FULL SCAN
p021510File Name:
Dil. Factor:13.5
Date of Collection: 2/10/16 1:20:00 PM
Date of Analysis: 2/15/16 09:46 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
6.8 Not Detected 58 Not DetectedDibromochloromethane
6.8 Not Detected 52 Not Detected1,2-Dibromoethane (EDB)
6.8 Not Detected 31 Not DetectedChlorobenzene
6.8 Not Detected 29 Not DetectedEthyl Benzene
6.8 16 29 72m,p-Xylene
6.8 Not Detected 29 Not Detectedo-Xylene
6.8 Not Detected 29 Not DetectedStyrene
6.8 Not Detected 70 Not DetectedBromoform
6.8 Not Detected 33 Not DetectedCumene
6.8 Not Detected 46 Not Detected1,1,2,2-Tetrachloroethane
6.8 Not Detected 33 Not DetectedPropylbenzene
6.8 Not Detected 33 Not Detected4-Ethyltoluene
6.8 Not Detected 33 Not Detected1,3,5-Trimethylbenzene
6.8 Not Detected 33 Not Detected1,2,4-Trimethylbenzene
6.8 Not Detected 40 Not Detected1,3-Dichlorobenzene
6.8 Not Detected 40 Not Detected1,4-Dichlorobenzene
6.8 Not Detected 35 Not Detectedalpha-Chlorotoluene
6.8 Not Detected 40 Not Detected1,2-Dichlorobenzene
27 Not Detected 200 Not Detected1,2,4-Trichlorobenzene
27 Not Detected 290 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
92 70-1304-Bromofluorobenzene
Page 8 of 40
Client Sample ID: SV10
Lab ID#: 1602234A-02A
EPA METHOD TO-15 GC/MS FULL SCAN
p021511File Name:
Dil. Factor:2.64
Date of Collection: 2/9/16 10:20:00 AM
Date of Analysis: 2/15/16 10:13 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 6.5 Not DetectedFreon 12
1.3 Not Detected 9.2 Not DetectedFreon 114
13 Not Detected 27 Not DetectedChloromethane
1.3 Not Detected 3.4 Not DetectedVinyl Chloride
1.3 Not Detected 2.9 Not Detected1,3-Butadiene
13 Not Detected 51 Not DetectedBromomethane
5.3 Not Detected 14 Not DetectedChloroethane
1.3 Not Detected 7.4 Not DetectedFreon 11
5.3 Not Detected 9.9 Not DetectedEthanol
1.3 Not Detected 10 Not DetectedFreon 113
1.3 Not Detected 5.2 Not Detected1,1-Dichloroethene
13 Not Detected 31 Not DetectedAcetone
5.3 Not Detected 13 Not Detected2-Propanol
5.3 Not Detected 16 Not DetectedCarbon Disulfide
5.3 Not Detected 16 Not Detected3-Chloropropene
13 Not Detected 46 Not DetectedMethylene Chloride
1.3 Not Detected 4.8 Not DetectedMethyl tert-butyl ether
1.3 Not Detected 5.2 Not Detectedtrans-1,2-Dichloroethene
1.3 Not Detected 4.6 Not DetectedHexane
1.3 Not Detected 5.3 Not Detected1,1-Dichloroethane
5.3 Not Detected 16 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.3 Not Detected 5.2 Not Detectedcis-1,2-Dichloroethene
1.3 Not Detected 3.9 Not DetectedTetrahydrofuran
1.3 Not Detected 6.4 Not DetectedChloroform
1.3 Not Detected 7.2 Not Detected1,1,1-Trichloroethane
1.3 Not Detected 4.5 Not DetectedCyclohexane
1.3 Not Detected 8.3 Not DetectedCarbon Tetrachloride
1.3 Not Detected 6.2 Not Detected2,2,4-Trimethylpentane
1.3 Not Detected 4.2 Not DetectedBenzene
1.3 Not Detected 5.3 Not Detected1,2-Dichloroethane
1.3 Not Detected 5.4 Not DetectedHeptane
1.3 Not Detected 7.1 Not DetectedTrichloroethene
1.3 Not Detected 6.1 Not Detected1,2-Dichloropropane
5.3 Not Detected 19 Not Detected1,4-Dioxane
1.3 Not Detected 8.8 Not DetectedBromodichloromethane
1.3 Not Detected 6.0 Not Detectedcis-1,3-Dichloropropene
1.3 Not Detected 5.4 Not Detected4-Methyl-2-pentanone
1.3 2.1 5.0 7.9Toluene
1.3 Not Detected 6.0 Not Detectedtrans-1,3-Dichloropropene
1.3 Not Detected 7.2 Not Detected1,1,2-Trichloroethane
1.3 Not Detected 9.0 Not DetectedTetrachloroethene
5.3 Not Detected 22 Not Detected2-Hexanone
Page 9 of 40
Client Sample ID: SV10
Lab ID#: 1602234A-02A
EPA METHOD TO-15 GC/MS FULL SCAN
p021511File Name:
Dil. Factor:2.64
Date of Collection: 2/9/16 10:20:00 AM
Date of Analysis: 2/15/16 10:13 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 11 Not DetectedDibromochloromethane
1.3 Not Detected 10 Not Detected1,2-Dibromoethane (EDB)
1.3 Not Detected 6.1 Not DetectedChlorobenzene
1.3 Not Detected 5.7 Not DetectedEthyl Benzene
1.3 Not Detected 5.7 Not Detectedm,p-Xylene
1.3 Not Detected 5.7 Not Detectedo-Xylene
1.3 Not Detected 5.6 Not DetectedStyrene
1.3 Not Detected 14 Not DetectedBromoform
1.3 Not Detected 6.5 Not DetectedCumene
1.3 Not Detected 9.1 Not Detected1,1,2,2-Tetrachloroethane
1.3 Not Detected 6.5 Not DetectedPropylbenzene
1.3 Not Detected 6.5 Not Detected4-Ethyltoluene
1.3 Not Detected 6.5 Not Detected1,3,5-Trimethylbenzene
1.3 Not Detected 6.5 Not Detected1,2,4-Trimethylbenzene
1.3 Not Detected 7.9 Not Detected1,3-Dichlorobenzene
1.3 Not Detected 7.9 Not Detected1,4-Dichlorobenzene
1.3 Not Detected 6.8 Not Detectedalpha-Chlorotoluene
1.3 Not Detected 7.9 Not Detected1,2-Dichlorobenzene
5.3 Not Detected 39 Not Detected1,2,4-Trichlorobenzene
5.3 Not Detected 56 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
93 70-1301,2-Dichloroethane-d4
92 70-1304-Bromofluorobenzene
Page 10 of 40
Client Sample ID: SV9
Lab ID#: 1602234A-03A
EPA METHOD TO-15 GC/MS FULL SCAN
p021512File Name:
Dil. Factor:20.2
Date of Collection: 2/9/16 9:28:00 AM
Date of Analysis: 2/15/16 10:39 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
10 Not Detected 50 Not DetectedFreon 12
10 Not Detected 71 Not DetectedFreon 114
100 Not Detected 210 Not DetectedChloromethane
10 Not Detected 26 Not DetectedVinyl Chloride
10 Not Detected 22 Not Detected1,3-Butadiene
100 Not Detected 390 Not DetectedBromomethane
40 Not Detected 110 Not DetectedChloroethane
10 Not Detected 57 Not DetectedFreon 11
40 Not Detected 76 Not DetectedEthanol
10 Not Detected 77 Not DetectedFreon 113
10 Not Detected 40 Not Detected1,1-Dichloroethene
100 Not Detected 240 Not DetectedAcetone
40 Not Detected 99 Not Detected2-Propanol
40 Not Detected 120 Not DetectedCarbon Disulfide
40 Not Detected 130 Not Detected3-Chloropropene
100 Not Detected 350 Not DetectedMethylene Chloride
10 Not Detected 36 Not DetectedMethyl tert-butyl ether
10 Not Detected 40 Not Detectedtrans-1,2-Dichloroethene
10 Not Detected 36 Not DetectedHexane
10 Not Detected 41 Not Detected1,1-Dichloroethane
40 Not Detected 120 Not Detected2-Butanone (Methyl Ethyl Ketone)
10 Not Detected 40 Not Detectedcis-1,2-Dichloroethene
10 Not Detected 30 Not DetectedTetrahydrofuran
10 Not Detected 49 Not DetectedChloroform
10 Not Detected 55 Not Detected1,1,1-Trichloroethane
10 Not Detected 35 Not DetectedCyclohexane
10 Not Detected 64 Not DetectedCarbon Tetrachloride
10 Not Detected 47 Not Detected2,2,4-Trimethylpentane
10 Not Detected 32 Not DetectedBenzene
10 Not Detected 41 Not Detected1,2-Dichloroethane
10 Not Detected 41 Not DetectedHeptane
10 Not Detected 54 Not DetectedTrichloroethene
10 Not Detected 47 Not Detected1,2-Dichloropropane
40 Not Detected 140 Not Detected1,4-Dioxane
10 Not Detected 68 Not DetectedBromodichloromethane
10 Not Detected 46 Not Detectedcis-1,3-Dichloropropene
10 Not Detected 41 Not Detected4-Methyl-2-pentanone
10 60 38 220Toluene
10 Not Detected 46 Not Detectedtrans-1,3-Dichloropropene
10 Not Detected 55 Not Detected1,1,2-Trichloroethane
10 Not Detected 68 Not DetectedTetrachloroethene
40 Not Detected 160 Not Detected2-Hexanone
Page 11 of 40
Client Sample ID: SV9
Lab ID#: 1602234A-03A
EPA METHOD TO-15 GC/MS FULL SCAN
p021512File Name:
Dil. Factor:20.2
Date of Collection: 2/9/16 9:28:00 AM
Date of Analysis: 2/15/16 10:39 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
10 Not Detected 86 Not DetectedDibromochloromethane
10 Not Detected 78 Not Detected1,2-Dibromoethane (EDB)
10 Not Detected 46 Not DetectedChlorobenzene
10 12 44 51Ethyl Benzene
10 74 44 320m,p-Xylene
10 22 44 94o-Xylene
10 10 43 43Styrene
10 Not Detected 100 Not DetectedBromoform
10 Not Detected 50 Not DetectedCumene
10 Not Detected 69 Not Detected1,1,2,2-Tetrachloroethane
10 Not Detected 50 Not DetectedPropylbenzene
10 10 50 504-Ethyltoluene
10 Not Detected 50 Not Detected1,3,5-Trimethylbenzene
10 13 50 621,2,4-Trimethylbenzene
10 Not Detected 61 Not Detected1,3-Dichlorobenzene
10 Not Detected 61 Not Detected1,4-Dichlorobenzene
10 Not Detected 52 Not Detectedalpha-Chlorotoluene
10 Not Detected 61 Not Detected1,2-Dichlorobenzene
40 Not Detected 300 Not Detected1,2,4-Trichlorobenzene
40 Not Detected 430 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
97 70-130Toluene-d8
99 70-1301,2-Dichloroethane-d4
94 70-1304-Bromofluorobenzene
Page 12 of 40
Client Sample ID: SV14
Lab ID#: 1602234A-04A
EPA METHOD TO-15 GC/MS FULL SCAN
p021513File Name:
Dil. Factor:2.58
Date of Collection: 2/9/16 12:30:00 PM
Date of Analysis: 2/15/16 11:05 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 6.4 Not DetectedFreon 12
1.3 Not Detected 9.0 Not DetectedFreon 114
13 Not Detected 27 Not DetectedChloromethane
1.3 Not Detected 3.3 Not DetectedVinyl Chloride
1.3 Not Detected 2.8 Not Detected1,3-Butadiene
13 Not Detected 50 Not DetectedBromomethane
5.2 Not Detected 14 Not DetectedChloroethane
1.3 Not Detected 7.2 Not DetectedFreon 11
5.2 Not Detected 9.7 Not DetectedEthanol
1.3 Not Detected 9.9 Not DetectedFreon 113
1.3 Not Detected 5.1 Not Detected1,1-Dichloroethene
13 Not Detected 31 Not DetectedAcetone
5.2 Not Detected 13 Not Detected2-Propanol
5.2 Not Detected 16 Not DetectedCarbon Disulfide
5.2 Not Detected 16 Not Detected3-Chloropropene
13 Not Detected 45 Not DetectedMethylene Chloride
1.3 Not Detected 4.6 Not DetectedMethyl tert-butyl ether
1.3 Not Detected 5.1 Not Detectedtrans-1,2-Dichloroethene
1.3 8.3 4.5 29Hexane
1.3 Not Detected 5.2 Not Detected1,1-Dichloroethane
5.2 Not Detected 15 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.3 Not Detected 5.1 Not Detectedcis-1,2-Dichloroethene
1.3 Not Detected 3.8 Not DetectedTetrahydrofuran
1.3 5.6 6.3 28Chloroform
1.3 Not Detected 7.0 Not Detected1,1,1-Trichloroethane
1.3 Not Detected 4.4 Not DetectedCyclohexane
1.3 Not Detected 8.1 Not DetectedCarbon Tetrachloride
1.3 8.2 6.0 382,2,4-Trimethylpentane
1.3 5.5 4.1 18Benzene
1.3 Not Detected 5.2 Not Detected1,2-Dichloroethane
1.3 48 5.3 200Heptane
1.3 Not Detected 6.9 Not DetectedTrichloroethene
1.3 Not Detected 6.0 Not Detected1,2-Dichloropropane
5.2 Not Detected 18 Not Detected1,4-Dioxane
1.3 Not Detected 8.6 Not DetectedBromodichloromethane
1.3 Not Detected 5.8 Not Detectedcis-1,3-Dichloropropene
1.3 Not Detected 5.3 Not Detected4-Methyl-2-pentanone
1.3 80 4.9 300Toluene
1.3 Not Detected 5.8 Not Detectedtrans-1,3-Dichloropropene
1.3 Not Detected 7.0 Not Detected1,1,2-Trichloroethane
1.3 Not Detected 8.8 Not DetectedTetrachloroethene
5.2 Not Detected 21 Not Detected2-Hexanone
Page 13 of 40
Client Sample ID: SV14
Lab ID#: 1602234A-04A
EPA METHOD TO-15 GC/MS FULL SCAN
p021513File Name:
Dil. Factor:2.58
Date of Collection: 2/9/16 12:30:00 PM
Date of Analysis: 2/15/16 11:05 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 11 Not DetectedDibromochloromethane
1.3 Not Detected 9.9 Not Detected1,2-Dibromoethane (EDB)
1.3 Not Detected 5.9 Not DetectedChlorobenzene
1.3 37 5.6 160Ethyl Benzene
1.3 210 5.6 900m,p-Xylene
1.3 40 5.6 180o-Xylene
1.3 6.7 5.5 28Styrene
1.3 Not Detected 13 Not DetectedBromoform
1.3 3.5 6.3 17Cumene
1.3 Not Detected 8.8 Not Detected1,1,2,2-Tetrachloroethane
1.3 12 6.3 61Propylbenzene
1.3 49 6.3 2404-Ethyltoluene
1.3 19 6.3 931,3,5-Trimethylbenzene
1.3 38 6.3 1901,2,4-Trimethylbenzene
1.3 Not Detected 7.8 Not Detected1,3-Dichlorobenzene
1.3 Not Detected 7.8 Not Detected1,4-Dichlorobenzene
1.3 Not Detected 6.7 Not Detectedalpha-Chlorotoluene
1.3 Not Detected 7.8 Not Detected1,2-Dichlorobenzene
5.2 Not Detected 38 Not Detected1,2,4-Trichlorobenzene
5.2 Not Detected 55 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
97 70-130Toluene-d8
95 70-1301,2-Dichloroethane-d4
95 70-1304-Bromofluorobenzene
Page 14 of 40
Client Sample ID: SV13
Lab ID#: 1602234A-05A
EPA METHOD TO-15 GC/MS FULL SCAN
p021514File Name:
Dil. Factor:5.51
Date of Collection: 2/9/16 2:20:00 PM
Date of Analysis: 2/15/16 11:31 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.8 Not Detected 14 Not DetectedFreon 12
2.8 Not Detected 19 Not DetectedFreon 114
28 Not Detected 57 Not DetectedChloromethane
2.8 Not Detected 7.0 Not DetectedVinyl Chloride
2.8 34 6.1 751,3-Butadiene
28 Not Detected 110 Not DetectedBromomethane
11 Not Detected 29 Not DetectedChloroethane
2.8 Not Detected 15 Not DetectedFreon 11
11 Not Detected 21 Not DetectedEthanol
2.8 Not Detected 21 Not DetectedFreon 113
2.8 Not Detected 11 Not Detected1,1-Dichloroethene
28 Not Detected 65 Not DetectedAcetone
11 Not Detected 27 Not Detected2-Propanol
11 18 34 58Carbon Disulfide
11 Not Detected 34 Not Detected3-Chloropropene
28 Not Detected 96 Not DetectedMethylene Chloride
2.8 Not Detected 9.9 Not DetectedMethyl tert-butyl ether
2.8 Not Detected 11 Not Detectedtrans-1,2-Dichloroethene
2.8 46 9.7 160Hexane
2.8 Not Detected 11 Not Detected1,1-Dichloroethane
11 Not Detected 32 Not Detected2-Butanone (Methyl Ethyl Ketone)
2.8 Not Detected 11 Not Detectedcis-1,2-Dichloroethene
2.8 Not Detected 8.1 Not DetectedTetrahydrofuran
2.8 Not Detected 13 Not DetectedChloroform
2.8 Not Detected 15 Not Detected1,1,1-Trichloroethane
2.8 Not Detected 9.5 Not DetectedCyclohexane
2.8 Not Detected 17 Not DetectedCarbon Tetrachloride
2.8 29 13 1402,2,4-Trimethylpentane
2.8 8.4 8.8 27Benzene
2.8 Not Detected 11 Not Detected1,2-Dichloroethane
2.8 7.8 11 32Heptane
2.8 Not Detected 15 Not DetectedTrichloroethene
2.8 Not Detected 13 Not Detected1,2-Dichloropropane
11 Not Detected 40 Not Detected1,4-Dioxane
2.8 Not Detected 18 Not DetectedBromodichloromethane
2.8 Not Detected 12 Not Detectedcis-1,3-Dichloropropene
2.8 Not Detected 11 Not Detected4-Methyl-2-pentanone
2.8 120 10 460Toluene
2.8 Not Detected 12 Not Detectedtrans-1,3-Dichloropropene
2.8 Not Detected 15 Not Detected1,1,2-Trichloroethane
2.8 Not Detected 19 Not DetectedTetrachloroethene
11 Not Detected 45 Not Detected2-Hexanone
Page 15 of 40
Client Sample ID: SV13
Lab ID#: 1602234A-05A
EPA METHOD TO-15 GC/MS FULL SCAN
p021514File Name:
Dil. Factor:5.51
Date of Collection: 2/9/16 2:20:00 PM
Date of Analysis: 2/15/16 11:31 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.8 Not Detected 23 Not DetectedDibromochloromethane
2.8 Not Detected 21 Not Detected1,2-Dibromoethane (EDB)
2.8 Not Detected 13 Not DetectedChlorobenzene
2.8 45 12 200Ethyl Benzene
2.8 300 12 1300m,p-Xylene
2.8 60 12 260o-Xylene
2.8 6.0 12 25Styrene
2.8 Not Detected 28 Not DetectedBromoform
2.8 6.6 14 32Cumene
2.8 Not Detected 19 Not Detected1,1,2,2-Tetrachloroethane
2.8 15 14 74Propylbenzene
2.8 86 14 4204-Ethyltoluene
2.8 50 14 2401,3,5-Trimethylbenzene
2.8 68 14 3401,2,4-Trimethylbenzene
2.8 Not Detected 16 Not Detected1,3-Dichlorobenzene
2.8 Not Detected 16 Not Detected1,4-Dichlorobenzene
2.8 Not Detected 14 Not Detectedalpha-Chlorotoluene
2.8 Not Detected 16 Not Detected1,2-Dichlorobenzene
11 Not Detected 82 Not Detected1,2,4-Trichlorobenzene
11 Not Detected 120 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
94 70-1304-Bromofluorobenzene
Page 16 of 40
Client Sample ID: SV1
Lab ID#: 1602234A-06A
EPA METHOD TO-15 GC/MS FULL SCAN
p021515File Name:
Dil. Factor:4.33
Date of Collection: 2/9/16 3:18:00 PM
Date of Analysis: 2/15/16 11:57 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.2 Not Detected 11 Not DetectedFreon 12
2.2 Not Detected 15 Not DetectedFreon 114
22 Not Detected 45 Not DetectedChloromethane
2.2 Not Detected 5.5 Not DetectedVinyl Chloride
2.2 Not Detected 4.8 Not Detected1,3-Butadiene
22 Not Detected 84 Not DetectedBromomethane
8.7 Not Detected 23 Not DetectedChloroethane
2.2 Not Detected 12 Not DetectedFreon 11
8.7 Not Detected 16 Not DetectedEthanol
2.2 Not Detected 16 Not DetectedFreon 113
2.2 Not Detected 8.6 Not Detected1,1-Dichloroethene
22 Not Detected 51 Not DetectedAcetone
8.7 Not Detected 21 Not Detected2-Propanol
8.7 Not Detected 27 Not DetectedCarbon Disulfide
8.7 Not Detected 27 Not Detected3-Chloropropene
22 Not Detected 75 Not DetectedMethylene Chloride
2.2 Not Detected 7.8 Not DetectedMethyl tert-butyl ether
2.2 Not Detected 8.6 Not Detectedtrans-1,2-Dichloroethene
2.2 Not Detected 7.6 Not DetectedHexane
2.2 Not Detected 8.8 Not Detected1,1-Dichloroethane
8.7 Not Detected 26 Not Detected2-Butanone (Methyl Ethyl Ketone)
2.2 Not Detected 8.6 Not Detectedcis-1,2-Dichloroethene
2.2 Not Detected 6.4 Not DetectedTetrahydrofuran
2.2 Not Detected 10 Not DetectedChloroform
2.2 Not Detected 12 Not Detected1,1,1-Trichloroethane
2.2 Not Detected 7.4 Not DetectedCyclohexane
2.2 Not Detected 14 Not DetectedCarbon Tetrachloride
2.2 3.0 10 142,2,4-Trimethylpentane
2.2 Not Detected 6.9 Not DetectedBenzene
2.2 Not Detected 8.8 Not Detected1,2-Dichloroethane
2.2 Not Detected 8.9 Not DetectedHeptane
2.2 Not Detected 12 Not DetectedTrichloroethene
2.2 Not Detected 10 Not Detected1,2-Dichloropropane
8.7 Not Detected 31 Not Detected1,4-Dioxane
2.2 Not Detected 14 Not DetectedBromodichloromethane
2.2 Not Detected 9.8 Not Detectedcis-1,3-Dichloropropene
2.2 Not Detected 8.9 Not Detected4-Methyl-2-pentanone
2.2 3.1 8.2 12Toluene
2.2 Not Detected 9.8 Not Detectedtrans-1,3-Dichloropropene
2.2 Not Detected 12 Not Detected1,1,2-Trichloroethane
2.2 Not Detected 15 Not DetectedTetrachloroethene
8.7 Not Detected 35 Not Detected2-Hexanone
Page 17 of 40
Client Sample ID: SV1
Lab ID#: 1602234A-06A
EPA METHOD TO-15 GC/MS FULL SCAN
p021515File Name:
Dil. Factor:4.33
Date of Collection: 2/9/16 3:18:00 PM
Date of Analysis: 2/15/16 11:57 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.2 Not Detected 18 Not DetectedDibromochloromethane
2.2 Not Detected 17 Not Detected1,2-Dibromoethane (EDB)
2.2 Not Detected 10 Not DetectedChlorobenzene
2.2 8.6 9.4 38Ethyl Benzene
2.2 Not Detected 9.4 Not Detectedm,p-Xylene
2.2 Not Detected 9.4 Not Detectedo-Xylene
2.2 Not Detected 9.2 Not DetectedStyrene
2.2 Not Detected 22 Not DetectedBromoform
2.2 Not Detected 11 Not DetectedCumene
2.2 Not Detected 15 Not Detected1,1,2,2-Tetrachloroethane
2.2 Not Detected 11 Not DetectedPropylbenzene
2.2 Not Detected 11 Not Detected4-Ethyltoluene
2.2 Not Detected 11 Not Detected1,3,5-Trimethylbenzene
2.2 Not Detected 11 Not Detected1,2,4-Trimethylbenzene
2.2 Not Detected 13 Not Detected1,3-Dichlorobenzene
2.2 Not Detected 13 Not Detected1,4-Dichlorobenzene
2.2 Not Detected 11 Not Detectedalpha-Chlorotoluene
2.2 Not Detected 13 Not Detected1,2-Dichlorobenzene
8.7 Not Detected 64 Not Detected1,2,4-Trichlorobenzene
8.7 Not Detected 92 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
97 70-130Toluene-d8
96 70-1301,2-Dichloroethane-d4
94 70-1304-Bromofluorobenzene
Page 18 of 40
Client Sample ID: SV16
Lab ID#: 1602234A-07A
EPA METHOD TO-15 GC/MS FULL SCAN
p021516File Name:
Dil. Factor:17.3
Date of Collection: 2/9/16 1:20:00 PM
Date of Analysis: 2/16/16 12:24 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
8.6 Not Detected 43 Not DetectedFreon 12
8.6 Not Detected 60 Not DetectedFreon 114
86 Not Detected 180 Not DetectedChloromethane
8.6 Not Detected 22 Not DetectedVinyl Chloride
8.6 Not Detected 19 Not Detected1,3-Butadiene
86 Not Detected 340 Not DetectedBromomethane
35 Not Detected 91 Not DetectedChloroethane
8.6 Not Detected 49 Not DetectedFreon 11
35 Not Detected 65 Not DetectedEthanol
8.6 Not Detected 66 Not DetectedFreon 113
8.6 Not Detected 34 Not Detected1,1-Dichloroethene
86 Not Detected 200 Not DetectedAcetone
35 Not Detected 85 Not Detected2-Propanol
35 Not Detected 110 Not DetectedCarbon Disulfide
35 Not Detected 110 Not Detected3-Chloropropene
86 Not Detected 300 Not DetectedMethylene Chloride
8.6 Not Detected 31 Not DetectedMethyl tert-butyl ether
8.6 Not Detected 34 Not Detectedtrans-1,2-Dichloroethene
8.6 26 30 93Hexane
8.6 Not Detected 35 Not Detected1,1-Dichloroethane
35 42 100 1202-Butanone (Methyl Ethyl Ketone)
8.6 Not Detected 34 Not Detectedcis-1,2-Dichloroethene
8.6 16 26 48Tetrahydrofuran
8.6 Not Detected 42 Not DetectedChloroform
8.6 Not Detected 47 Not Detected1,1,1-Trichloroethane
8.6 Not Detected 30 Not DetectedCyclohexane
8.6 Not Detected 54 Not DetectedCarbon Tetrachloride
8.6 12 40 572,2,4-Trimethylpentane
8.6 Not Detected 28 Not DetectedBenzene
8.6 Not Detected 35 Not Detected1,2-Dichloroethane
8.6 45 35 180Heptane
8.6 Not Detected 46 Not DetectedTrichloroethene
8.6 Not Detected 40 Not Detected1,2-Dichloropropane
35 Not Detected 120 Not Detected1,4-Dioxane
8.6 Not Detected 58 Not DetectedBromodichloromethane
8.6 Not Detected 39 Not Detectedcis-1,3-Dichloropropene
8.6 Not Detected 35 Not Detected4-Methyl-2-pentanone
8.6 36 32 140Toluene
8.6 Not Detected 39 Not Detectedtrans-1,3-Dichloropropene
8.6 Not Detected 47 Not Detected1,1,2-Trichloroethane
8.6 Not Detected 59 Not DetectedTetrachloroethene
35 Not Detected 140 Not Detected2-Hexanone
Page 19 of 40
Client Sample ID: SV16
Lab ID#: 1602234A-07A
EPA METHOD TO-15 GC/MS FULL SCAN
p021516File Name:
Dil. Factor:17.3
Date of Collection: 2/9/16 1:20:00 PM
Date of Analysis: 2/16/16 12:24 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
8.6 Not Detected 74 Not DetectedDibromochloromethane
8.6 Not Detected 66 Not Detected1,2-Dibromoethane (EDB)
8.6 Not Detected 40 Not DetectedChlorobenzene
8.6 Not Detected 38 Not DetectedEthyl Benzene
8.6 21 38 93m,p-Xylene
8.6 Not Detected 38 Not Detectedo-Xylene
8.6 Not Detected 37 Not DetectedStyrene
8.6 Not Detected 89 Not DetectedBromoform
8.6 Not Detected 42 Not DetectedCumene
8.6 Not Detected 59 Not Detected1,1,2,2-Tetrachloroethane
8.6 Not Detected 42 Not DetectedPropylbenzene
8.6 Not Detected 42 Not Detected4-Ethyltoluene
8.6 Not Detected 42 Not Detected1,3,5-Trimethylbenzene
8.6 Not Detected 42 Not Detected1,2,4-Trimethylbenzene
8.6 Not Detected 52 Not Detected1,3-Dichlorobenzene
8.6 Not Detected 52 Not Detected1,4-Dichlorobenzene
8.6 Not Detected 45 Not Detectedalpha-Chlorotoluene
8.6 Not Detected 52 Not Detected1,2-Dichlorobenzene
35 Not Detected 260 Not Detected1,2,4-Trichlorobenzene
35 Not Detected 370 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
94 70-1304-Bromofluorobenzene
Page 20 of 40
Client Sample ID: SV8
Lab ID#: 1602234A-08A
EPA METHOD TO-15 GC/MS FULL SCAN
3021607File Name:
Dil. Factor:5.27
Date of Collection: 2/10/16 9:20:00 AM
Date of Analysis: 2/16/16 01:20 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.6 Not Detected 13 Not DetectedFreon 12
2.6 Not Detected 18 Not DetectedFreon 114
26 Not Detected 54 Not DetectedChloromethane
2.6 Not Detected 6.7 Not DetectedVinyl Chloride
2.6 Not Detected 5.8 Not Detected1,3-Butadiene
26 Not Detected 100 Not DetectedBromomethane
10 Not Detected 28 Not DetectedChloroethane
2.6 Not Detected 15 Not DetectedFreon 11
10 Not Detected 20 Not DetectedEthanol
2.6 Not Detected 20 Not DetectedFreon 113
2.6 Not Detected 10 Not Detected1,1-Dichloroethene
26 Not Detected 62 Not DetectedAcetone
10 Not Detected 26 Not Detected2-Propanol
10 Not Detected 33 Not DetectedCarbon Disulfide
10 Not Detected 33 Not Detected3-Chloropropene
26 Not Detected 92 Not DetectedMethylene Chloride
2.6 Not Detected 9.5 Not DetectedMethyl tert-butyl ether
2.6 Not Detected 10 Not Detectedtrans-1,2-Dichloroethene
2.6 36 9.3 130Hexane
2.6 Not Detected 11 Not Detected1,1-Dichloroethane
10 Not Detected 31 Not Detected2-Butanone (Methyl Ethyl Ketone)
2.6 Not Detected 10 Not Detectedcis-1,2-Dichloroethene
2.6 Not Detected 7.8 Not DetectedTetrahydrofuran
2.6 610 13 3000Chloroform
2.6 Not Detected 14 Not Detected1,1,1-Trichloroethane
2.6 Not Detected 9.1 Not DetectedCyclohexane
2.6 Not Detected 16 Not DetectedCarbon Tetrachloride
2.6 Not Detected 12 Not Detected2,2,4-Trimethylpentane
2.6 Not Detected 8.4 Not DetectedBenzene
2.6 Not Detected 11 Not Detected1,2-Dichloroethane
2.6 16 11 65Heptane
2.6 Not Detected 14 Not DetectedTrichloroethene
2.6 Not Detected 12 Not Detected1,2-Dichloropropane
10 Not Detected 38 Not Detected1,4-Dioxane
2.6 9.2 18 62Bromodichloromethane
2.6 Not Detected 12 Not Detectedcis-1,3-Dichloropropene
2.6 Not Detected 11 Not Detected4-Methyl-2-pentanone
2.6 2.7 9.9 10Toluene
2.6 Not Detected 12 Not Detectedtrans-1,3-Dichloropropene
2.6 Not Detected 14 Not Detected1,1,2-Trichloroethane
2.6 Not Detected 18 Not DetectedTetrachloroethene
10 Not Detected 43 Not Detected2-Hexanone
Page 21 of 40
Client Sample ID: SV8
Lab ID#: 1602234A-08A
EPA METHOD TO-15 GC/MS FULL SCAN
3021607File Name:
Dil. Factor:5.27
Date of Collection: 2/10/16 9:20:00 AM
Date of Analysis: 2/16/16 01:20 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.6 Not Detected 22 Not DetectedDibromochloromethane
2.6 Not Detected 20 Not Detected1,2-Dibromoethane (EDB)
2.6 Not Detected 12 Not DetectedChlorobenzene
2.6 Not Detected 11 Not DetectedEthyl Benzene
2.6 Not Detected 11 Not Detectedm,p-Xylene
2.6 Not Detected 11 Not Detectedo-Xylene
2.6 Not Detected 11 Not DetectedStyrene
2.6 Not Detected 27 Not DetectedBromoform
2.6 Not Detected 13 Not DetectedCumene
2.6 Not Detected 18 Not Detected1,1,2,2-Tetrachloroethane
2.6 Not Detected 13 Not DetectedPropylbenzene
2.6 Not Detected 13 Not Detected4-Ethyltoluene
2.6 Not Detected 13 Not Detected1,3,5-Trimethylbenzene
2.6 Not Detected 13 Not Detected1,2,4-Trimethylbenzene
2.6 Not Detected 16 Not Detected1,3-Dichlorobenzene
2.6 Not Detected 16 Not Detected1,4-Dichlorobenzene
2.6 Not Detected 14 Not Detectedalpha-Chlorotoluene
2.6 Not Detected 16 Not Detected1,2-Dichlorobenzene
10 Not Detected 78 Not Detected1,2,4-Trichlorobenzene
10 Not Detected 110 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
104 70-130Toluene-d8
102 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 22 of 40
Client Sample ID: SV7
Lab ID#: 1602234A-09A
EPA METHOD TO-15 GC/MS FULL SCAN
p021517File Name:
Dil. Factor:2.52
Date of Collection: 2/10/16 8:26:00 AM
Date of Analysis: 2/16/16 12:50 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 6.2 Not DetectedFreon 12
1.3 Not Detected 8.8 Not DetectedFreon 114
13 Not Detected 26 Not DetectedChloromethane
1.3 Not Detected 3.2 Not DetectedVinyl Chloride
1.3 Not Detected 2.8 Not Detected1,3-Butadiene
13 Not Detected 49 Not DetectedBromomethane
5.0 Not Detected 13 Not DetectedChloroethane
1.3 Not Detected 7.1 Not DetectedFreon 11
5.0 Not Detected 9.5 Not DetectedEthanol
1.3 Not Detected 9.6 Not DetectedFreon 113
1.3 Not Detected 5.0 Not Detected1,1-Dichloroethene
13 Not Detected 30 Not DetectedAcetone
5.0 Not Detected 12 Not Detected2-Propanol
5.0 Not Detected 16 Not DetectedCarbon Disulfide
5.0 Not Detected 16 Not Detected3-Chloropropene
13 Not Detected 44 Not DetectedMethylene Chloride
1.3 Not Detected 4.5 Not DetectedMethyl tert-butyl ether
1.3 Not Detected 5.0 Not Detectedtrans-1,2-Dichloroethene
1.3 14 4.4 48Hexane
1.3 Not Detected 5.1 Not Detected1,1-Dichloroethane
5.0 Not Detected 15 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.3 Not Detected 5.0 Not Detectedcis-1,2-Dichloroethene
1.3 Not Detected 3.7 Not DetectedTetrahydrofuran
1.3 1.3 6.2 6.2Chloroform
1.3 Not Detected 6.9 Not Detected1,1,1-Trichloroethane
1.3 Not Detected 4.3 Not DetectedCyclohexane
1.3 Not Detected 7.9 Not DetectedCarbon Tetrachloride
1.3 Not Detected 5.9 Not Detected2,2,4-Trimethylpentane
1.3 Not Detected 4.0 Not DetectedBenzene
1.3 Not Detected 5.1 Not Detected1,2-Dichloroethane
1.3 Not Detected 5.2 Not DetectedHeptane
1.3 Not Detected 6.8 Not DetectedTrichloroethene
1.3 Not Detected 5.8 Not Detected1,2-Dichloropropane
5.0 Not Detected 18 Not Detected1,4-Dioxane
1.3 Not Detected 8.4 Not DetectedBromodichloromethane
1.3 Not Detected 5.7 Not Detectedcis-1,3-Dichloropropene
1.3 Not Detected 5.2 Not Detected4-Methyl-2-pentanone
1.3 Not Detected 4.7 Not DetectedToluene
1.3 Not Detected 5.7 Not Detectedtrans-1,3-Dichloropropene
1.3 Not Detected 6.9 Not Detected1,1,2-Trichloroethane
1.3 Not Detected 8.5 Not DetectedTetrachloroethene
5.0 Not Detected 21 Not Detected2-Hexanone
Page 23 of 40
Client Sample ID: SV7
Lab ID#: 1602234A-09A
EPA METHOD TO-15 GC/MS FULL SCAN
p021517File Name:
Dil. Factor:2.52
Date of Collection: 2/10/16 8:26:00 AM
Date of Analysis: 2/16/16 12:50 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 11 Not DetectedDibromochloromethane
1.3 Not Detected 9.7 Not Detected1,2-Dibromoethane (EDB)
1.3 Not Detected 5.8 Not DetectedChlorobenzene
1.3 Not Detected 5.5 Not DetectedEthyl Benzene
1.3 Not Detected 5.5 Not Detectedm,p-Xylene
1.3 Not Detected 5.5 Not Detectedo-Xylene
1.3 Not Detected 5.4 Not DetectedStyrene
1.3 Not Detected 13 Not DetectedBromoform
1.3 Not Detected 6.2 Not DetectedCumene
1.3 Not Detected 8.6 Not Detected1,1,2,2-Tetrachloroethane
1.3 Not Detected 6.2 Not DetectedPropylbenzene
1.3 Not Detected 6.2 Not Detected4-Ethyltoluene
1.3 Not Detected 6.2 Not Detected1,3,5-Trimethylbenzene
1.3 Not Detected 6.2 Not Detected1,2,4-Trimethylbenzene
1.3 Not Detected 7.6 Not Detected1,3-Dichlorobenzene
1.3 Not Detected 7.6 Not Detected1,4-Dichlorobenzene
1.3 Not Detected 6.5 Not Detectedalpha-Chlorotoluene
1.3 Not Detected 7.6 Not Detected1,2-Dichlorobenzene
5.0 Not Detected 37 Not Detected1,2,4-Trichlorobenzene
5.0 Not Detected 54 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
95 70-1301,2-Dichloroethane-d4
93 70-1304-Bromofluorobenzene
Page 24 of 40
Client Sample ID: Lab Blank
Lab ID#: 1602234A-10A
EPA METHOD TO-15 GC/MS FULL SCAN
p021506File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/15/16 12:13 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 2.5 Not DetectedFreon 12
0.50 Not Detected 3.5 Not DetectedFreon 114
5.0 Not Detected 10 Not DetectedChloromethane
0.50 Not Detected 1.3 Not DetectedVinyl Chloride
0.50 Not Detected 1.1 Not Detected1,3-Butadiene
5.0 Not Detected 19 Not DetectedBromomethane
2.0 Not Detected 5.3 Not DetectedChloroethane
0.50 Not Detected 2.8 Not DetectedFreon 11
2.0 Not Detected 3.8 Not DetectedEthanol
0.50 Not Detected 3.8 Not DetectedFreon 113
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethene
5.0 Not Detected 12 Not DetectedAcetone
2.0 Not Detected 4.9 Not Detected2-Propanol
2.0 Not Detected 6.2 Not DetectedCarbon Disulfide
2.0 Not Detected 6.3 Not Detected3-Chloropropene
5.0 Not Detected 17 Not DetectedMethylene Chloride
0.50 Not Detected 1.8 Not DetectedMethyl tert-butyl ether
0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene
0.50 Not Detected 1.8 Not DetectedHexane
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethane
2.0 Not Detected 5.9 Not Detected2-Butanone (Methyl Ethyl Ketone)
0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene
0.50 Not Detected 1.5 Not DetectedTetrahydrofuran
0.50 Not Detected 2.4 Not DetectedChloroform
0.50 Not Detected 2.7 Not Detected1,1,1-Trichloroethane
0.50 Not Detected 1.7 Not DetectedCyclohexane
0.50 Not Detected 3.1 Not DetectedCarbon Tetrachloride
0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane
0.50 Not Detected 1.6 Not DetectedBenzene
0.50 Not Detected 2.0 Not Detected1,2-Dichloroethane
0.50 Not Detected 2.0 Not DetectedHeptane
0.50 Not Detected 2.7 Not DetectedTrichloroethene
0.50 Not Detected 2.3 Not Detected1,2-Dichloropropane
2.0 Not Detected 7.2 Not Detected1,4-Dioxane
0.50 Not Detected 3.4 Not DetectedBromodichloromethane
0.50 Not Detected 2.3 Not Detectedcis-1,3-Dichloropropene
0.50 Not Detected 2.0 Not Detected4-Methyl-2-pentanone
0.50 Not Detected 1.9 Not DetectedToluene
0.50 Not Detected 2.3 Not Detectedtrans-1,3-Dichloropropene
0.50 Not Detected 2.7 Not Detected1,1,2-Trichloroethane
0.50 Not Detected 3.4 Not DetectedTetrachloroethene
2.0 Not Detected 8.2 Not Detected2-Hexanone
Page 25 of 40
Client Sample ID: Lab Blank
Lab ID#: 1602234A-10A
EPA METHOD TO-15 GC/MS FULL SCAN
p021506File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/15/16 12:13 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 4.2 Not DetectedDibromochloromethane
0.50 Not Detected 3.8 Not Detected1,2-Dibromoethane (EDB)
0.50 Not Detected 2.3 Not DetectedChlorobenzene
0.50 Not Detected 2.2 Not DetectedEthyl Benzene
0.50 Not Detected 2.2 Not Detectedm,p-Xylene
0.50 Not Detected 2.2 Not Detectedo-Xylene
0.50 Not Detected 2.1 Not DetectedStyrene
0.50 Not Detected 5.2 Not DetectedBromoform
0.50 Not Detected 2.4 Not DetectedCumene
0.50 Not Detected 3.4 Not Detected1,1,2,2-Tetrachloroethane
0.50 Not Detected 2.4 Not DetectedPropylbenzene
0.50 Not Detected 2.4 Not Detected4-Ethyltoluene
0.50 Not Detected 2.4 Not Detected1,3,5-Trimethylbenzene
0.50 Not Detected 2.4 Not Detected1,2,4-Trimethylbenzene
0.50 Not Detected 3.0 Not Detected1,3-Dichlorobenzene
0.50 Not Detected 3.0 Not Detected1,4-Dichlorobenzene
0.50 Not Detected 2.6 Not Detectedalpha-Chlorotoluene
0.50 Not Detected 3.0 Not Detected1,2-Dichlorobenzene
2.0 Not Detected 15 Not Detected1,2,4-Trichlorobenzene
2.0 Not Detected 21 Not DetectedHexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
94 70-1301,2-Dichloroethane-d4
95 70-1304-Bromofluorobenzene
Page 26 of 40
Client Sample ID: Lab Blank
Lab ID#: 1602234A-10B
EPA METHOD TO-15 GC/MS FULL SCAN
3021606File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 11:23 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 2.5 Not DetectedFreon 12
0.50 Not Detected 3.5 Not DetectedFreon 114
5.0 Not Detected 10 Not DetectedChloromethane
0.50 Not Detected 1.3 Not DetectedVinyl Chloride
0.50 Not Detected 1.1 Not Detected1,3-Butadiene
5.0 Not Detected 19 Not DetectedBromomethane
2.0 Not Detected 5.3 Not DetectedChloroethane
0.50 Not Detected 2.8 Not DetectedFreon 11
2.0 Not Detected 3.8 Not DetectedEthanol
0.50 Not Detected 3.8 Not DetectedFreon 113
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethene
5.0 Not Detected 12 Not DetectedAcetone
2.0 Not Detected 4.9 Not Detected2-Propanol
2.0 Not Detected 6.2 Not DetectedCarbon Disulfide
2.0 Not Detected 6.3 Not Detected3-Chloropropene
5.0 Not Detected 17 Not DetectedMethylene Chloride
0.50 Not Detected 1.8 Not DetectedMethyl tert-butyl ether
0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene
0.50 Not Detected 1.8 Not DetectedHexane
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethane
2.0 Not Detected 5.9 Not Detected2-Butanone (Methyl Ethyl Ketone)
0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene
0.50 Not Detected 1.5 Not DetectedTetrahydrofuran
0.50 Not Detected 2.4 Not DetectedChloroform
0.50 Not Detected 2.7 Not Detected1,1,1-Trichloroethane
0.50 Not Detected 1.7 Not DetectedCyclohexane
0.50 Not Detected 3.1 Not DetectedCarbon Tetrachloride
0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane
0.50 Not Detected 1.6 Not DetectedBenzene
0.50 Not Detected 2.0 Not Detected1,2-Dichloroethane
0.50 Not Detected 2.0 Not DetectedHeptane
0.50 Not Detected 2.7 Not DetectedTrichloroethene
0.50 Not Detected 2.3 Not Detected1,2-Dichloropropane
2.0 Not Detected 7.2 Not Detected1,4-Dioxane
0.50 Not Detected 3.4 Not DetectedBromodichloromethane
0.50 Not Detected 2.3 Not Detectedcis-1,3-Dichloropropene
0.50 Not Detected 2.0 Not Detected4-Methyl-2-pentanone
0.50 Not Detected 1.9 Not DetectedToluene
0.50 Not Detected 2.3 Not Detectedtrans-1,3-Dichloropropene
0.50 Not Detected 2.7 Not Detected1,1,2-Trichloroethane
0.50 Not Detected 3.4 Not DetectedTetrachloroethene
2.0 Not Detected 8.2 Not Detected2-Hexanone
Page 27 of 40
Client Sample ID: Lab Blank
Lab ID#: 1602234A-10B
EPA METHOD TO-15 GC/MS FULL SCAN
3021606File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 11:23 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 4.2 Not DetectedDibromochloromethane
0.50 Not Detected 3.8 Not Detected1,2-Dibromoethane (EDB)
0.50 Not Detected 2.3 Not DetectedChlorobenzene
0.50 Not Detected 2.2 Not DetectedEthyl Benzene
0.50 Not Detected 2.2 Not Detectedm,p-Xylene
0.50 Not Detected 2.2 Not Detectedo-Xylene
0.50 Not Detected 2.1 Not DetectedStyrene
0.50 Not Detected 5.2 Not DetectedBromoform
0.50 Not Detected 2.4 Not DetectedCumene
0.50 Not Detected 3.4 Not Detected1,1,2,2-Tetrachloroethane
0.50 Not Detected 2.4 Not DetectedPropylbenzene
0.50 Not Detected 2.4 Not Detected4-Ethyltoluene
0.50 Not Detected 2.4 Not Detected1,3,5-Trimethylbenzene
0.50 Not Detected 2.4 Not Detected1,2,4-Trimethylbenzene
0.50 Not Detected 3.0 Not Detected1,3-Dichlorobenzene
0.50 Not Detected 3.0 Not Detected1,4-Dichlorobenzene
0.50 Not Detected 2.6 Not Detectedalpha-Chlorotoluene
0.50 Not Detected 3.0 Not Detected1,2-Dichlorobenzene
2.0 Not Detected 15 Not Detected1,2,4-Trichlorobenzene
2.0 Not Detected 21 Not DetectedHexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
106 70-130Toluene-d8
100 70-1301,2-Dichloroethane-d4
99 70-1304-Bromofluorobenzene
Page 28 of 40
Client Sample ID: CCV
Lab ID#: 1602234A-11A
EPA METHOD TO-15 GC/MS FULL SCAN
p021502File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/15/16 10:32 AM
%RecoveryCompound
96Freon 12
98Freon 114
134 QChloromethane
114Vinyl Chloride
951,3-Butadiene
109Bromomethane
95Chloroethane
97Freon 11
105Ethanol
95Freon 113
941,1-Dichloroethene
89Acetone
872-Propanol
94Carbon Disulfide
943-Chloropropene
101Methylene Chloride
92Methyl tert-butyl ether
99trans-1,2-Dichloroethene
94Hexane
991,1-Dichloroethane
932-Butanone (Methyl Ethyl Ketone)
96cis-1,2-Dichloroethene
100Tetrahydrofuran
97Chloroform
961,1,1-Trichloroethane
89Cyclohexane
100Carbon Tetrachloride
982,2,4-Trimethylpentane
97Benzene
1021,2-Dichloroethane
85Heptane
98Trichloroethene
971,2-Dichloropropane
991,4-Dioxane
99Bromodichloromethane
99cis-1,3-Dichloropropene
1004-Methyl-2-pentanone
95Toluene
101trans-1,3-Dichloropropene
981,1,2-Trichloroethane
100Tetrachloroethene
1062-Hexanone
Page 29 of 40
Client Sample ID: CCV
Lab ID#: 1602234A-11A
EPA METHOD TO-15 GC/MS FULL SCAN
p021502File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/15/16 10:32 AM
%RecoveryCompound
101Dibromochloromethane
1011,2-Dibromoethane (EDB)
102Chlorobenzene
96Ethyl Benzene
98m,p-Xylene
99o-Xylene
109Styrene
100Bromoform
97Cumene
961,1,2,2-Tetrachloroethane
98Propylbenzene
964-Ethyltoluene
1041,3,5-Trimethylbenzene
1011,2,4-Trimethylbenzene
1001,3-Dichlorobenzene
991,4-Dichlorobenzene
100alpha-Chlorotoluene
1011,2-Dichlorobenzene
1171,2,4-Trichlorobenzene
118Hexachlorobutadiene
Q = Exceeds Quality Control limits.
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
97 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
97 70-1304-Bromofluorobenzene
Page 30 of 40
Client Sample ID: CCV
Lab ID#: 1602234A-11B
EPA METHOD TO-15 GC/MS FULL SCAN
3021603File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 09:55 AM
%RecoveryCompound
103Freon 12
100Freon 114
111Chloromethane
103Vinyl Chloride
981,3-Butadiene
101Bromomethane
102Chloroethane
100Freon 11
104Ethanol
98Freon 113
1041,1-Dichloroethene
105Acetone
1092-Propanol
102Carbon Disulfide
1023-Chloropropene
102Methylene Chloride
103Methyl tert-butyl ether
102trans-1,2-Dichloroethene
103Hexane
1051,1-Dichloroethane
982-Butanone (Methyl Ethyl Ketone)
104cis-1,2-Dichloroethene
102Tetrahydrofuran
101Chloroform
1001,1,1-Trichloroethane
101Cyclohexane
100Carbon Tetrachloride
1032,2,4-Trimethylpentane
98Benzene
1031,2-Dichloroethane
97Heptane
98Trichloroethene
971,2-Dichloropropane
961,4-Dioxane
99Bromodichloromethane
102cis-1,3-Dichloropropene
994-Methyl-2-pentanone
97Toluene
103trans-1,3-Dichloropropene
961,1,2-Trichloroethane
100Tetrachloroethene
1012-Hexanone
Page 31 of 40
Client Sample ID: CCV
Lab ID#: 1602234A-11B
EPA METHOD TO-15 GC/MS FULL SCAN
3021603File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 09:55 AM
%RecoveryCompound
101Dibromochloromethane
1011,2-Dibromoethane (EDB)
99Chlorobenzene
100Ethyl Benzene
102m,p-Xylene
100o-Xylene
103Styrene
104Bromoform
101Cumene
1001,1,2,2-Tetrachloroethane
100Propylbenzene
1004-Ethyltoluene
1001,3,5-Trimethylbenzene
1011,2,4-Trimethylbenzene
991,3-Dichlorobenzene
981,4-Dichlorobenzene
101alpha-Chlorotoluene
961,2-Dichlorobenzene
1031,2,4-Trichlorobenzene
104Hexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
104 70-130Toluene-d8
104 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 32 of 40
Client Sample ID: LCS
Lab ID#: 1602234A-12A
EPA METHOD TO-15 GC/MS FULL SCAN
p021503File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/15/16 10:56 AM
Limits%RecoveryCompound
Method
106 70-130Freon 12
113 70-130Freon 114
111 70-130Chloromethane
128 70-130Vinyl Chloride
100 70-1301,3-Butadiene
113 70-130Bromomethane
102 70-130Chloroethane
106 70-130Freon 11
111 70-130Ethanol
100 70-130Freon 113
103 70-1301,1-Dichloroethene
87 70-130Acetone
94 70-1302-Propanol
89 70-130Carbon Disulfide
94 70-1303-Chloropropene
109 70-130Methylene Chloride
95 70-130Methyl tert-butyl ether
111 70-130trans-1,2-Dichloroethene
102 70-130Hexane
106 70-1301,1-Dichloroethane
98 70-1302-Butanone (Methyl Ethyl Ketone)
101 70-130cis-1,2-Dichloroethene
104 70-130Tetrahydrofuran
103 70-130Chloroform
101 70-1301,1,1-Trichloroethane
94 70-130Cyclohexane
104 70-130Carbon Tetrachloride
103 70-1302,2,4-Trimethylpentane
105 70-130Benzene
110 70-1301,2-Dichloroethane
91 70-130Heptane
108 70-130Trichloroethene
105 70-1301,2-Dichloropropane
103 70-1301,4-Dioxane
110 70-130Bromodichloromethane
100 70-130cis-1,3-Dichloropropene
104 70-1304-Methyl-2-pentanone
104 70-130Toluene
108 70-130trans-1,3-Dichloropropene
107 70-1301,1,2-Trichloroethane
108 70-130Tetrachloroethene
114 70-1302-Hexanone
Page 33 of 40
Client Sample ID: LCS
Lab ID#: 1602234A-12A
EPA METHOD TO-15 GC/MS FULL SCAN
p021503File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/15/16 10:56 AM
Limits%RecoveryCompound
Method
110 70-130Dibromochloromethane
108 70-1301,2-Dibromoethane (EDB)
108 70-130Chlorobenzene
104 70-130Ethyl Benzene
105 70-130m,p-Xylene
105 70-130o-Xylene
117 70-130Styrene
111 70-130Bromoform
103 70-130Cumene
103 70-1301,1,2,2-Tetrachloroethane
105 70-130Propylbenzene
102 70-1304-Ethyltoluene
111 70-1301,3,5-Trimethylbenzene
108 70-1301,2,4-Trimethylbenzene
106 70-1301,3-Dichlorobenzene
104 70-1301,4-Dichlorobenzene
106 70-130alpha-Chlorotoluene
106 70-1301,2-Dichlorobenzene
132 Q 70-1301,2,4-Trichlorobenzene
132 Q 70-130Hexachlorobutadiene
Q = Exceeds Quality Control limits.
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
100 70-1301,2-Dichloroethane-d4
97 70-1304-Bromofluorobenzene
Page 34 of 40
Client Sample ID: LCSD
Lab ID#: 1602234A-12AA
EPA METHOD TO-15 GC/MS FULL SCAN
p021504File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/15/16 11:21 AM
Limits%RecoveryCompound
Method
106 70-130Freon 12
114 70-130Freon 114
113 70-130Chloromethane
126 70-130Vinyl Chloride
101 70-1301,3-Butadiene
113 70-130Bromomethane
104 70-130Chloroethane
107 70-130Freon 11
106 70-130Ethanol
100 70-130Freon 113
104 70-1301,1-Dichloroethene
88 70-130Acetone
96 70-1302-Propanol
89 70-130Carbon Disulfide
97 70-1303-Chloropropene
108 70-130Methylene Chloride
96 70-130Methyl tert-butyl ether
109 70-130trans-1,2-Dichloroethene
101 70-130Hexane
107 70-1301,1-Dichloroethane
98 70-1302-Butanone (Methyl Ethyl Ketone)
102 70-130cis-1,2-Dichloroethene
104 70-130Tetrahydrofuran
104 70-130Chloroform
99 70-1301,1,1-Trichloroethane
96 70-130Cyclohexane
104 70-130Carbon Tetrachloride
102 70-1302,2,4-Trimethylpentane
103 70-130Benzene
109 70-1301,2-Dichloroethane
89 70-130Heptane
107 70-130Trichloroethene
105 70-1301,2-Dichloropropane
105 70-1301,4-Dioxane
109 70-130Bromodichloromethane
99 70-130cis-1,3-Dichloropropene
105 70-1304-Methyl-2-pentanone
102 70-130Toluene
107 70-130trans-1,3-Dichloropropene
104 70-1301,1,2-Trichloroethane
106 70-130Tetrachloroethene
111 70-1302-Hexanone
Page 35 of 40
Client Sample ID: LCSD
Lab ID#: 1602234A-12AA
EPA METHOD TO-15 GC/MS FULL SCAN
p021504File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/15/16 11:21 AM
Limits%RecoveryCompound
Method
108 70-130Dibromochloromethane
106 70-1301,2-Dibromoethane (EDB)
106 70-130Chlorobenzene
102 70-130Ethyl Benzene
104 70-130m,p-Xylene
104 70-130o-Xylene
114 70-130Styrene
109 70-130Bromoform
101 70-130Cumene
101 70-1301,1,2,2-Tetrachloroethane
104 70-130Propylbenzene
100 70-1304-Ethyltoluene
111 70-1301,3,5-Trimethylbenzene
106 70-1301,2,4-Trimethylbenzene
105 70-1301,3-Dichlorobenzene
104 70-1301,4-Dichlorobenzene
104 70-130alpha-Chlorotoluene
106 70-1301,2-Dichlorobenzene
134 Q 70-1301,2,4-Trichlorobenzene
136 Q 70-130Hexachlorobutadiene
Q = Exceeds Quality Control limits.
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
97 70-1304-Bromofluorobenzene
Page 36 of 40
Client Sample ID: LCS
Lab ID#: 1602234A-12B
EPA METHOD TO-15 GC/MS FULL SCAN
3021604File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 10:20 AM
Limits%RecoveryCompound
Method
107 70-130Freon 12
103 70-130Freon 114
114 70-130Chloromethane
108 70-130Vinyl Chloride
96 70-1301,3-Butadiene
102 70-130Bromomethane
104 70-130Chloroethane
103 70-130Freon 11
110 70-130Ethanol
97 70-130Freon 113
102 70-1301,1-Dichloroethene
102 70-130Acetone
110 70-1302-Propanol
91 70-130Carbon Disulfide
98 70-1303-Chloropropene
104 70-130Methylene Chloride
101 70-130Methyl tert-butyl ether
106 70-130trans-1,2-Dichloroethene
104 70-130Hexane
105 70-1301,1-Dichloroethane
101 70-1302-Butanone (Methyl Ethyl Ketone)
97 70-130cis-1,2-Dichloroethene
100 70-130Tetrahydrofuran
104 70-130Chloroform
101 70-1301,1,1-Trichloroethane
102 70-130Cyclohexane
100 70-130Carbon Tetrachloride
105 70-1302,2,4-Trimethylpentane
99 70-130Benzene
100 70-1301,2-Dichloroethane
96 70-130Heptane
99 70-130Trichloroethene
98 70-1301,2-Dichloropropane
95 70-1301,4-Dioxane
101 70-130Bromodichloromethane
94 70-130cis-1,3-Dichloropropene
94 70-1304-Methyl-2-pentanone
96 70-130Toluene
101 70-130trans-1,3-Dichloropropene
95 70-1301,1,2-Trichloroethane
97 70-130Tetrachloroethene
95 70-1302-Hexanone
Page 37 of 40
Client Sample ID: LCS
Lab ID#: 1602234A-12B
EPA METHOD TO-15 GC/MS FULL SCAN
3021604File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 10:20 AM
Limits%RecoveryCompound
Method
100 70-130Dibromochloromethane
98 70-1301,2-Dibromoethane (EDB)
95 70-130Chlorobenzene
97 70-130Ethyl Benzene
98 70-130m,p-Xylene
99 70-130o-Xylene
102 70-130Styrene
104 70-130Bromoform
99 70-130Cumene
98 70-1301,1,2,2-Tetrachloroethane
98 70-130Propylbenzene
99 70-1304-Ethyltoluene
99 70-1301,3,5-Trimethylbenzene
100 70-1301,2,4-Trimethylbenzene
97 70-1301,3-Dichlorobenzene
95 70-1301,4-Dichlorobenzene
104 70-130alpha-Chlorotoluene
94 70-1301,2-Dichlorobenzene
105 70-1301,2,4-Trichlorobenzene
105 70-130Hexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
102 70-130Toluene-d8
99 70-1301,2-Dichloroethane-d4
100 70-1304-Bromofluorobenzene
Page 38 of 40
Client Sample ID: LCSD
Lab ID#: 1602234A-12BB
EPA METHOD TO-15 GC/MS FULL SCAN
3021605File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 10:45 AM
Limits%RecoveryCompound
Method
107 70-130Freon 12
105 70-130Freon 114
109 70-130Chloromethane
108 70-130Vinyl Chloride
97 70-1301,3-Butadiene
105 70-130Bromomethane
104 70-130Chloroethane
102 70-130Freon 11
110 70-130Ethanol
97 70-130Freon 113
100 70-1301,1-Dichloroethene
101 70-130Acetone
111 70-1302-Propanol
91 70-130Carbon Disulfide
98 70-1303-Chloropropene
106 70-130Methylene Chloride
101 70-130Methyl tert-butyl ether
106 70-130trans-1,2-Dichloroethene
105 70-130Hexane
106 70-1301,1-Dichloroethane
100 70-1302-Butanone (Methyl Ethyl Ketone)
102 70-130cis-1,2-Dichloroethene
101 70-130Tetrahydrofuran
103 70-130Chloroform
100 70-1301,1,1-Trichloroethane
102 70-130Cyclohexane
100 70-130Carbon Tetrachloride
105 70-1302,2,4-Trimethylpentane
102 70-130Benzene
102 70-1301,2-Dichloroethane
98 70-130Heptane
101 70-130Trichloroethene
100 70-1301,2-Dichloropropane
94 70-1301,4-Dioxane
105 70-130Bromodichloromethane
98 70-130cis-1,3-Dichloropropene
98 70-1304-Methyl-2-pentanone
99 70-130Toluene
102 70-130trans-1,3-Dichloropropene
95 70-1301,1,2-Trichloroethane
98 70-130Tetrachloroethene
99 70-1302-Hexanone
Page 39 of 40
Client Sample ID: LCSD
Lab ID#: 1602234A-12BB
EPA METHOD TO-15 GC/MS FULL SCAN
3021605File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 10:45 AM
Limits%RecoveryCompound
Method
101 70-130Dibromochloromethane
101 70-1301,2-Dibromoethane (EDB)
98 70-130Chlorobenzene
99 70-130Ethyl Benzene
99 70-130m,p-Xylene
102 70-130o-Xylene
101 70-130Styrene
105 70-130Bromoform
100 70-130Cumene
98 70-1301,1,2,2-Tetrachloroethane
100 70-130Propylbenzene
99 70-1304-Ethyltoluene
100 70-1301,3,5-Trimethylbenzene
102 70-1301,2,4-Trimethylbenzene
100 70-1301,3-Dichlorobenzene
97 70-1301,4-Dichlorobenzene
106 70-130alpha-Chlorotoluene
97 70-1301,2-Dichlorobenzene
111 70-1301,2,4-Trichlorobenzene
109 70-130Hexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
104 70-130Toluene-d8
103 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 40 of 40
2/17/2016
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte NC 28269
Project Name: E43
Project #: 20160086.001A
Dear Mr. Michael Sussman
The following report includes the data for the above referenced project for sample(s)
received on 2/12/2016 at Air Toxics Ltd.
The data and associated QC analyzed by Modified ASTM D-1946 are compliant with
the project requirements or laboratory criteria with the exception of the deviations
noted in the attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contactthe Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1602234B
Page 1 of 20
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
WORK ORDER #:1602234B
CLIENT:BILL TO:
PHONE:
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
704-598-1049
704-598-1050
02/12/2016
DATE COMPLETED:02/17/2016
P.O. #
PROJECT #20160086.001A E43
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A SV3 Modified ASTM D-1946 25.5 "Hg 15 psi
02A SV10 Modified ASTM D-1946 7.0 "Hg 15 psi
03A SV9 Modified ASTM D-1946 27.0 "Hg 15 psi
04A SV14 Modified ASTM D-1946 6.5 "Hg 15 psi
05A SV13 Modified ASTM D-1946 19.0 "Hg 15 psi
06A SV1 Modified ASTM D-1946 16.0 "Hg 15 psi
07A SV16 Modified ASTM D-1946 26.5 "Hg 15 psi
08A SV8 Modified ASTM D-1946 7.0 "Hg 15 psi
09A SV7 Modified ASTM D-1946 6.0 "Hg 15 psi
10A Lab Blank Modified ASTM D-1946 NA NA
10B Lab Blank Modified ASTM D-1946 NA NA
11A LCS Modified ASTM D-1946 NA NA
11AA LCSD Modified ASTM D-1946 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2014, Expiration date: 10/17/2015.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
[phone] . [phone] . FAX [phone]
02/17/16
Page 2 of 20
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704343-14-7, UT NELAP CA009332014-5, VA NELAP - 460197, WA NELAP - C935
LABORATORY NARRATIVEModified ASTM D-1946Kleinfelder Southeast, Inc.Workorder# 1602234B
Nine 1 Liter Summa Canister samples were received on February 12, 2016. The laboratory performed
analysis via Modified ASTM Method D-1946 for Methane and fixed gases in air using GC/FID or
GC/TCD. The method involves direct injection of 1.0 mL of sample.
On the analytical column employed for this analysis, Oxygen coelutes with Argon. The corresponding
peak is quantitated as Oxygen.
Since Nitrogen is used to pressurize samples, the reported Nitrogen values are calculated by adding all
the sample components and subtracting from 100%.
Method modifications taken to run these samples are summarized in the table below. Specific project
requirements may over-ride the ATL modifications.
Requirement ATL ModificationsASTM D-1946
Calibration A single point
calibration is
performed using a
reference standard
closely matching the
composition of the
unknown.
A minimum of 5-point calibration curve is performed.
Quantitation is based on average Response Factor.
Reference Standard The composition of any
reference standard
must be known to
within 0.01 mol % for
any component.
The standards used by ATL are blended to a >/= 95%
accuracy.
Sample Injection Volume Components whose
concentrations are in
excess of 5 % should
not be analyzed by
using sample volumes
greater than 0.5 mL.
The sample container is connected directly to a fixed
volume sample loop of 1.0 mL on the GC. Linear range
is defined by the calibration curve. Bags are loaded by
vacuum.
Normalization Normalize the mole
percent values by
multiplying each value
by 100 and dividing by
the sum of the original
values. The sum of the
original values should
not differ from 100%
by more than 1.0%.
Results are not normalized. The sum of the reported
values can differ from 100% by as much as 15%, either
due to analytical variability or an unusual sample matrix.
Precision Precision requirements
established at each
concentration level.
Duplicates should agree within 25% RPD for detections
> 5 X's the RL.
Page 3 of 20
Receiving Notes
Samples SV3, SV9, SV13, SV1 and SV16 were received with significant vacuum remaining in the
canister. The residual canister vacuum resulted in elevated reporting limits.
Sample collection date was incomplete on the Chain of Custody for samples SV3, SV10, SV9, SV14,
SV13, SV1, SV16, SV8 and SV7. The year of collection was assumed to be 2016.
There were no analytical discrepancies.
Analytical Notes
Seven qualifiers may have been used on the data analysis sheets and indicate as follows:
B - Compound present in laboratory blank greater than reporting limit.
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the detection limit.
M - Reported value may be biased due to apparent matrix interferences.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 4 of 20
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
Summary of Detected Compounds
Client Sample ID: SV3
Lab ID#: 1602234B-01A
(%)(%)Compound
AmountRpt. Limit
1.4 12Oxygen
1.4 88Nitrogen
0.14 0.37Carbon Dioxide
Client Sample ID: SV10
Lab ID#: 1602234B-02A
(%)(%)Compound
AmountRpt. Limit
0.26 13Oxygen
0.26 49Nitrogen
0.13 38Helium
Client Sample ID: SV9
Lab ID#: 1602234B-03A
(%)(%)Compound
AmountRpt. Limit
2.0 9.6Oxygen
2.0 90Nitrogen
0.20 0.33Carbon Dioxide
Client Sample ID: SV14
Lab ID#: 1602234B-04A
(%)(%)Compound
AmountRpt. Limit
0.26 2.6Oxygen
0.26 92Nitrogen
0.00026 0.00055Methane
0.026 5.6Carbon Dioxide
Client Sample ID: SV13
Lab ID#: 1602234B-05A
Page 5 of 20
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
Summary of Detected Compounds
Client Sample ID: SV13
Lab ID#: 1602234B-05A
(%)(%)Compound
AmountRpt. Limit
0.55 17Oxygen
0.55 82Nitrogen
0.00055 0.00074Methane
0.055 0.71Carbon Dioxide
Client Sample ID: SV1
Lab ID#: 1602234B-06A
(%)(%)Compound
AmountRpt. Limit
0.43 7.2Oxygen
0.43 81Nitrogen
0.00043 0.96Methane
0.043 11Carbon Dioxide
Client Sample ID: SV16
Lab ID#: 1602234B-07A
(%)(%)Compound
AmountRpt. Limit
1.7 9.9Oxygen
1.7 90Nitrogen
Client Sample ID: SV8
Lab ID#: 1602234B-08A
(%)(%)Compound
AmountRpt. Limit
0.26 3.3Oxygen
0.26 70Nitrogen
0.00026 9.4Methane
0.026 17Carbon Dioxide
Client Sample ID: SV7
Lab ID#: 1602234B-09A
Page 6 of 20
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
Summary of Detected Compounds
Client Sample ID: SV7
Lab ID#: 1602234B-09A
(%)(%)Compound
AmountRpt. Limit
0.25 3.8Oxygen
0.25 79Nitrogen
0.00025 9.4Methane
0.025 8.1Carbon Dioxide
Page 7 of 20
Client Sample ID: SV3
Lab ID#: 1602234B-01A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021611File Name:
Dil. Factor:13.5
Date of Collection: 2/10/16 1:20:00 PM
Date of Analysis: 2/16/16 01:06 PM
(%)(%)Compound
AmountRpt. Limit
1.4 12Oxygen
1.4 88Nitrogen
0.14 Not DetectedCarbon Monoxide
0.0014 Not DetectedMethane
0.14 0.37Carbon Dioxide
0.014 Not DetectedEthane
0.014 Not DetectedEthene
0.68 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 8 of 20
Client Sample ID: SV10
Lab ID#: 1602234B-02A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021612File Name:
Dil. Factor:2.64
Date of Collection: 2/9/16 10:20:00 AM
Date of Analysis: 2/16/16 01:53 PM
(%)(%)Compound
AmountRpt. Limit
0.26 13Oxygen
0.26 49Nitrogen
0.026 Not DetectedCarbon Monoxide
0.00026 Not DetectedMethane
0.026 Not DetectedCarbon Dioxide
0.0026 Not DetectedEthane
0.0026 Not DetectedEthene
0.13 38Helium
Container Type: 1 Liter Summa Canister
Page 9 of 20
Client Sample ID: SV9
Lab ID#: 1602234B-03A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021613File Name:
Dil. Factor:20.2
Date of Collection: 2/9/16 9:28:00 AM
Date of Analysis: 2/16/16 02:35 PM
(%)(%)Compound
AmountRpt. Limit
2.0 9.6Oxygen
2.0 90Nitrogen
0.20 Not DetectedCarbon Monoxide
0.0020 Not DetectedMethane
0.20 0.33Carbon Dioxide
0.020 Not DetectedEthane
0.020 Not DetectedEthene
1.0 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 10 of 20
Client Sample ID: SV14
Lab ID#: 1602234B-04A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021614File Name:
Dil. Factor:2.58
Date of Collection: 2/9/16 12:30:00 PM
Date of Analysis: 2/16/16 03:05 PM
(%)(%)Compound
AmountRpt. Limit
0.26 2.6Oxygen
0.26 92Nitrogen
0.026 Not DetectedCarbon Monoxide
0.00026 0.00055Methane
0.026 5.6Carbon Dioxide
0.0026 Not DetectedEthane
0.0026 Not DetectedEthene
0.13 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 11 of 20
Client Sample ID: SV13
Lab ID#: 1602234B-05A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021615File Name:
Dil. Factor:5.51
Date of Collection: 2/9/16 2:20:00 PM
Date of Analysis: 2/16/16 03:42 PM
(%)(%)Compound
AmountRpt. Limit
0.55 17Oxygen
0.55 82Nitrogen
0.055 Not DetectedCarbon Monoxide
0.00055 0.00074Methane
0.055 0.71Carbon Dioxide
0.0055 Not DetectedEthane
0.0055 Not DetectedEthene
0.28 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 12 of 20
Client Sample ID: SV1
Lab ID#: 1602234B-06A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021616File Name:
Dil. Factor:4.33
Date of Collection: 2/9/16 3:18:00 PM
Date of Analysis: 2/16/16 04:10 PM
(%)(%)Compound
AmountRpt. Limit
0.43 7.2Oxygen
0.43 81Nitrogen
0.043 Not DetectedCarbon Monoxide
0.00043 0.96Methane
0.043 11Carbon Dioxide
0.0043 Not DetectedEthane
0.0043 Not DetectedEthene
0.22 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 13 of 20
Client Sample ID: SV16
Lab ID#: 1602234B-07A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021617File Name:
Dil. Factor:17.3
Date of Collection: 2/9/16 1:20:00 PM
Date of Analysis: 2/16/16 04:38 PM
(%)(%)Compound
AmountRpt. Limit
1.7 9.9Oxygen
1.7 90Nitrogen
0.17 Not DetectedCarbon Monoxide
0.0017 Not DetectedMethane
0.17 Not DetectedCarbon Dioxide
0.017 Not DetectedEthane
0.017 Not DetectedEthene
0.86 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 14 of 20
Client Sample ID: SV8
Lab ID#: 1602234B-08A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021618File Name:
Dil. Factor:2.64
Date of Collection: 2/10/16 9:20:00 AM
Date of Analysis: 2/16/16 05:04 PM
(%)(%)Compound
AmountRpt. Limit
0.26 3.3Oxygen
0.26 70Nitrogen
0.026 Not DetectedCarbon Monoxide
0.00026 9.4Methane
0.026 17Carbon Dioxide
0.0026 Not DetectedEthane
0.0026 Not DetectedEthene
0.13 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 15 of 20
Client Sample ID: SV7
Lab ID#: 1602234B-09A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021619File Name:
Dil. Factor:2.52
Date of Collection: 2/10/16 8:26:00 AM
Date of Analysis: 2/16/16 05:27 PM
(%)(%)Compound
AmountRpt. Limit
0.25 3.8Oxygen
0.25 79Nitrogen
0.025 Not DetectedCarbon Monoxide
0.00025 9.4Methane
0.025 8.1Carbon Dioxide
0.0025 Not DetectedEthane
0.0025 Not DetectedEthene
0.13 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 16 of 20
Client Sample ID: Lab Blank
Lab ID#: 1602234B-10A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021604File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 09:48 AM
(%)(%)Compound
AmountRpt. Limit
0.10 Not DetectedOxygen
0.10 Not DetectedNitrogen
0.010 Not DetectedCarbon Monoxide
0.00010 Not DetectedMethane
0.010 Not DetectedCarbon Dioxide
0.0010 Not DetectedEthane
0.0010 Not DetectedEthene
Container Type: NA - Not Applicable
Page 17 of 20
Client Sample ID: Lab Blank
Lab ID#: 1602234B-10B
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021603bFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 09:24 AM
(%)(%)Compound
AmountRpt. Limit
0.050 Not DetectedHelium
Container Type: NA - Not Applicable
Page 18 of 20
Client Sample ID: LCS
Lab ID#: 1602234B-11A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021602File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 08:42 AM
Limits%RecoveryCompound
Method
95 85-115Oxygen
90 85-115Nitrogen
102 85-115Carbon Monoxide
94 85-115Methane
101 85-115Carbon Dioxide
93 85-115Ethane
94 85-115Ethene
102 85-115Helium
Container Type: NA - Not Applicable
Page 19 of 20
Client Sample ID: LCSD
Lab ID#: 1602234B-11AA
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9021625File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 2/16/16 09:19 PM
Limits%RecoveryCompound
Method
93 85-115Oxygen
88 85-115Nitrogen
100 85-115Carbon Monoxide
93 85-115Methane
99 85-115Carbon Dioxide
92 85-115Ethane
93 85-115Ethene
100 85-115Helium
Container Type: NA - Not Applicable
Page 20 of 20
4/12/2016
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte NC 28269
Project Name: E43
Project #: 20160086.001A
Dear Mr. Michael Sussman
The following report includes the data for the above referenced project for sample(s)
received on 4/7/2016 at Air Toxics Ltd.
The data and associated QC analyzed by TO-15 are compliant with the project
requirements or laboratory criteria with the exception of the deviations noted in the
attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free to
contactthe Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding the
data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1604137A
Page 1 of 31
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
WORK ORDER #:1604137A
CLIENT:BILL TO:
PHONE:
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
704-598-1049
704-598-1050
04/07/2016
DATE COMPLETED:04/12/2016
P.O. #
PROJECT #20160086.001A E43
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A IVP-1 TO-15 3.7 "Hg 14.7 psi
02A IVP-2 TO-15 4.1 "Hg 14.4 psi
03A IVP-4 TO-15 4.5 "Hg 15.1 psi
04A IVP-5 TO-15 3.5 "Hg 14.9 psi
05A IVP-6 TO-15 1 "Hg 14.9 psi
06A IVP-8 TO-15 4.1 "Hg 15 psi
07A IVP-9 TO-15 5.5 "Hg 14.9 psi
08A IVP-7 TO-15 5.5 "Hg 14.9 psi
09A Lab Blank TO-15 NA NA
10A CCV TO-15 NA NA
11A LCS TO-15 NA NA
11AA LCSD TO-15 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2015, Expiration date: 10/17/2016.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630
[phone] . [phone] . FAX [phone]
04/12/16
Page 2 of 31
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704434-15-9, UT NELAP CA0093332015-6, VA NELAP - 8113, WA NELAP - C935
LABORATORY NARRATIVEEPA Method TO-15Kleinfelder Southeast, Inc.Workorder# 1604137A
Eight 1 Liter Summa Canister (100% Certified) samples were received on April 07, 2016. The laboratory
performed analysis via EPA Method TO-15 using GC/MS in the full scan mode.
This workorder was independently validated prior to submittal using 'USEPA National Functional Guidelines' as
generally applied to the analysis of volatile organic compounds in air. A rules-based, logic driven, independent
validation engine was employed to assess completeness, evaluate pass/fail of relevant project quality control
requirements and verification of all quantified amounts.
Sample collection date was incomplete on the Chain of Custody. The year of collection was assumed to be
2016.
The Chain of Custody (COC) information for sample IVP-5 did not match the information on the canister with
regard to canister identification. The client was notified of the discrepancy and the information on the canister
was used to process and report the sample.
Receiving Notes
There were no analytical discrepancies.
Analytical Notes
Eight qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction not
performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. See data
page for project specific U-flag definition.
UJ- Non-detected compound associated with low bias in the CCV
N - The identification is based on presumptive evidence.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 3 of 31
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: IVP-1
Lab ID#: 1604137A-01A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
4.6 40 8.6 76Ethanol
11 50 27 120Acetone
1.1 1.3 4.0 4.5Hexane
1.1 1.3 3.4 3.8Tetrahydrofuran
1.1 5.0 3.9 17Cyclohexane
1.1 1.4 4.3 5.2Toluene
1.1 3.4 5.0 15m,p-Xylene
1.1 1.6 5.0 6.9o-Xylene
1.1 1.6 5.6 7.64-Ethyltoluene
1.1 1.4 5.6 6.81,2,4-Trimethylbenzene
Client Sample ID: IVP-2
Lab ID#: 1604137A-02A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
4.6 24 8.6 46Ethanol
11 32 27 77Acetone
4.6 14 11 332-Propanol
1.1 15 4.0 52Hexane
1.1 16 3.9 55Cyclohexane
1.1 65 5.3 3002,2,4-Trimethylpentane
1.1 8.2 3.6 26Benzene
1.1 22 4.7 90Heptane
1.1 110 4.3 430Toluene
1.1 18 5.0 77Ethyl Benzene
1.1 54 5.0 240m,p-Xylene
1.1 19 5.0 81o-Xylene
1.1 2.3 5.6 11Propylbenzene
1.1 9.8 5.6 484-Ethyltoluene
1.1 3.5 5.6 171,3,5-Trimethylbenzene
1.1 7.3 5.6 361,2,4-Trimethylbenzene
Page 4 of 31
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: IVP-4
Lab ID#: 1604137A-03A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
4.8 34 9.0 64Ethanol
12 38 28 90Acetone
1.2 1.2 5.6 5.72,2,4-Trimethylpentane
1.2 3.2 4.5 12Toluene
1.2 1.8 5.2 7.9m,p-Xylene
Client Sample ID: IVP-5
Lab ID#: 1604137A-04A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
4.6 170 8.6 320Ethanol
11 100 27 250Acetone
4.6 7.3 11 182-Propanol
1.1 1.9 4.0 6.8Hexane
1.1 1.2 3.4 3.5Tetrahydrofuran
1.1 2.1 3.9 7.3Cyclohexane
1.1 7.9 5.3 372,2,4-Trimethylpentane
1.1 2.7 4.7 11Heptane
1.1 2.0 4.7 8.14-Methyl-2-pentanone
1.1 14 4.3 54Toluene
1.1 2.5 4.9 11Ethyl Benzene
1.1 9.4 5.0 41m,p-Xylene
1.1 3.4 5.0 15o-Xylene
1.1 2.3 5.6 124-Ethyltoluene
1.1 2.2 5.6 111,2,4-Trimethylbenzene
Client Sample ID: IVP-6
Lab ID#: 1604137A-05A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
4.2 45 7.8 86Ethanol
10 42 25 100Acetone
4.2 11 10 262-Propanol
Page 5 of 31
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: IVP-6
Lab ID#: 1604137A-05A
1.0 9.3 3.7 33Hexane
1.0 9.6 3.6 33Cyclohexane
1.0 42 4.8 2002,2,4-Trimethylpentane
1.0 5.6 3.3 18Benzene
1.0 13 4.3 53Heptane
1.0 75 3.9 280Toluene
1.0 11 4.5 50Ethyl Benzene
1.0 38 4.5 160m,p-Xylene
1.0 14 4.5 61o-Xylene
1.0 1.7 5.1 8.4Propylbenzene
1.0 7.6 5.1 374-Ethyltoluene
1.0 2.4 5.1 121,3,5-Trimethylbenzene
1.0 6.0 5.1 291,2,4-Trimethylbenzene
Client Sample ID: IVP-8
Lab ID#: 1604137A-06A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
4.7 120 8.8 220Ethanol
12 310 28 740Acetone
4.7 4.8 12 122-Propanol
4.7 10 14 302-Butanone (Methyl Ethyl Ketone)
1.2 3.6 3.4 11Tetrahydrofuran
1.2 5.6 4.8 234-Methyl-2-pentanone
1.2 1.7 4.4 6.5Toluene
1.2 2.8 5.1 12m,p-Xylene
1.2 1.4 5.1 6.0o-Xylene
Client Sample ID: IVP-9
Lab ID#: 1604137A-07A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
4.9 62 9.3 120Ethanol
12 97 29 230Acetone
Page 6 of 31
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: IVP-9
Lab ID#: 1604137A-07A
1.2 1.5 3.6 4.3Tetrahydrofuran
1.2 2.1 5.0 8.54-Methyl-2-pentanone
1.2 1.3 4.6 4.9Toluene
1.2 2.4 5.3 10m,p-Xylene
1.2 1.2 6.0 6.04-Ethyltoluene
Client Sample ID: IVP-7
Lab ID#: 1604137A-08A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
4.9 75 9.3 140Ethanol
12 62 29 150Acetone
4.9 5.0 12 122-Propanol
1.2 1.7 3.6 5.0Tetrahydrofuran
1.2 1.6 5.7 7.42,2,4-Trimethylpentane
1.2 4.0 4.6 15Toluene
1.2 2.5 5.3 11m,p-Xylene
Page 7 of 31
Client Sample ID: IVP-1
Lab ID#: 1604137A-01A
EPA METHOD TO-15 GC/MS FULL SCAN
a041116File Name:
Dil. Factor:2.28
Date of Collection: 4/6/16 7:40:00 AM
Date of Analysis: 4/11/16 08:16 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 5.6 Not DetectedFreon 12
1.1 Not Detected 8.0 Not DetectedFreon 114
11 Not Detected 24 Not DetectedChloromethane
1.1 Not Detected 2.9 Not DetectedVinyl Chloride
1.1 Not Detected 2.5 Not Detected1,3-Butadiene
11 Not Detected 44 Not DetectedBromomethane
4.6 Not Detected 12 Not DetectedChloroethane
1.1 Not Detected 6.4 Not DetectedFreon 11
4.6 40 8.6 76Ethanol
1.1 Not Detected 8.7 Not DetectedFreon 113
1.1 Not Detected 4.5 Not Detected1,1-Dichloroethene
11 50 27 120Acetone
4.6 Not Detected 11 Not Detected2-Propanol
4.6 Not Detected 14 Not DetectedCarbon Disulfide
4.6 Not Detected 14 Not Detected3-Chloropropene
11 Not Detected 40 Not DetectedMethylene Chloride
1.1 Not Detected 4.1 Not DetectedMethyl tert-butyl ether
1.1 Not Detected 4.5 Not Detectedtrans-1,2-Dichloroethene
1.1 1.3 4.0 4.5Hexane
1.1 Not Detected 4.6 Not Detected1,1-Dichloroethane
4.6 Not Detected 13 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.1 Not Detected 4.5 Not Detectedcis-1,2-Dichloroethene
1.1 1.3 3.4 3.8Tetrahydrofuran
1.1 Not Detected 5.6 Not DetectedChloroform
1.1 Not Detected 6.2 Not Detected1,1,1-Trichloroethane
1.1 5.0 3.9 17Cyclohexane
1.1 Not Detected 7.2 Not DetectedCarbon Tetrachloride
1.1 Not Detected 5.3 Not Detected2,2,4-Trimethylpentane
1.1 Not Detected 3.6 Not DetectedBenzene
1.1 Not Detected 4.6 Not Detected1,2-Dichloroethane
1.1 Not Detected 4.7 Not DetectedHeptane
1.1 Not Detected 6.1 Not DetectedTrichloroethene
1.1 Not Detected 5.3 Not Detected1,2-Dichloropropane
4.6 Not Detected 16 Not Detected1,4-Dioxane
1.1 Not Detected 7.6 Not DetectedBromodichloromethane
1.1 Not Detected 5.2 Not Detectedcis-1,3-Dichloropropene
1.1 Not Detected 4.7 Not Detected4-Methyl-2-pentanone
1.1 1.4 4.3 5.2Toluene
1.1 Not Detected 5.2 Not Detectedtrans-1,3-Dichloropropene
1.1 Not Detected 6.2 Not Detected1,1,2-Trichloroethane
1.1 Not Detected 7.7 Not DetectedTetrachloroethene
4.6 Not Detected 19 Not Detected2-Hexanone
Page 8 of 31
Client Sample ID: IVP-1
Lab ID#: 1604137A-01A
EPA METHOD TO-15 GC/MS FULL SCAN
a041116File Name:
Dil. Factor:2.28
Date of Collection: 4/6/16 7:40:00 AM
Date of Analysis: 4/11/16 08:16 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 9.7 Not DetectedDibromochloromethane
1.1 Not Detected 8.8 Not Detected1,2-Dibromoethane (EDB)
1.1 Not Detected 5.2 Not DetectedChlorobenzene
1.1 Not Detected 4.9 Not DetectedEthyl Benzene
1.1 3.4 5.0 15m,p-Xylene
1.1 1.6 5.0 6.9o-Xylene
1.1 Not Detected 4.8 Not DetectedStyrene
1.1 Not Detected 12 Not DetectedBromoform
1.1 Not Detected 5.6 Not DetectedCumene
1.1 Not Detected 7.8 Not Detected1,1,2,2-Tetrachloroethane
1.1 Not Detected 5.6 Not DetectedPropylbenzene
1.1 1.6 5.6 7.64-Ethyltoluene
1.1 Not Detected 5.6 Not Detected1,3,5-Trimethylbenzene
1.1 1.4 5.6 6.81,2,4-Trimethylbenzene
1.1 Not Detected 6.8 Not Detected1,3-Dichlorobenzene
1.1 Not Detected 6.8 Not Detected1,4-Dichlorobenzene
1.1 Not Detected 5.9 Not Detectedalpha-Chlorotoluene
1.1 Not Detected 6.8 Not Detected1,2-Dichlorobenzene
4.6 Not Detected 34 Not Detected1,2,4-Trichlorobenzene
4.6 Not Detected 49 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
114 70-1304-Bromofluorobenzene
Page 9 of 31
Client Sample ID: IVP-2
Lab ID#: 1604137A-02A
EPA METHOD TO-15 GC/MS FULL SCAN
a041117File Name:
Dil. Factor:2.29
Date of Collection: 4/6/16 8:22:00 AM
Date of Analysis: 4/11/16 08:42 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 5.7 Not DetectedFreon 12
1.1 Not Detected 8.0 Not DetectedFreon 114
11 Not Detected 24 Not DetectedChloromethane
1.1 Not Detected 2.9 Not DetectedVinyl Chloride
1.1 Not Detected 2.5 Not Detected1,3-Butadiene
11 Not Detected 44 Not DetectedBromomethane
4.6 Not Detected 12 Not DetectedChloroethane
1.1 Not Detected 6.4 Not DetectedFreon 11
4.6 24 8.6 46Ethanol
1.1 Not Detected 8.8 Not DetectedFreon 113
1.1 Not Detected 4.5 Not Detected1,1-Dichloroethene
11 32 27 77Acetone
4.6 14 11 332-Propanol
4.6 Not Detected 14 Not DetectedCarbon Disulfide
4.6 Not Detected 14 Not Detected3-Chloropropene
11 Not Detected 40 Not DetectedMethylene Chloride
1.1 Not Detected 4.1 Not DetectedMethyl tert-butyl ether
1.1 Not Detected 4.5 Not Detectedtrans-1,2-Dichloroethene
1.1 15 4.0 52Hexane
1.1 Not Detected 4.6 Not Detected1,1-Dichloroethane
4.6 Not Detected 14 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.1 Not Detected 4.5 Not Detectedcis-1,2-Dichloroethene
1.1 Not Detected 3.4 Not DetectedTetrahydrofuran
1.1 Not Detected 5.6 Not DetectedChloroform
1.1 Not Detected 6.2 Not Detected1,1,1-Trichloroethane
1.1 16 3.9 55Cyclohexane
1.1 Not Detected 7.2 Not DetectedCarbon Tetrachloride
1.1 65 5.3 3002,2,4-Trimethylpentane
1.1 8.2 3.6 26Benzene
1.1 Not Detected 4.6 Not Detected1,2-Dichloroethane
1.1 22 4.7 90Heptane
1.1 Not Detected 6.2 Not DetectedTrichloroethene
1.1 Not Detected 5.3 Not Detected1,2-Dichloropropane
4.6 Not Detected 16 Not Detected1,4-Dioxane
1.1 Not Detected 7.7 Not DetectedBromodichloromethane
1.1 Not Detected 5.2 Not Detectedcis-1,3-Dichloropropene
1.1 Not Detected 4.7 Not Detected4-Methyl-2-pentanone
1.1 110 4.3 430Toluene
1.1 Not Detected 5.2 Not Detectedtrans-1,3-Dichloropropene
1.1 Not Detected 6.2 Not Detected1,1,2-Trichloroethane
1.1 Not Detected 7.8 Not DetectedTetrachloroethene
4.6 Not Detected 19 Not Detected2-Hexanone
Page 10 of 31
Client Sample ID: IVP-2
Lab ID#: 1604137A-02A
EPA METHOD TO-15 GC/MS FULL SCAN
a041117File Name:
Dil. Factor:2.29
Date of Collection: 4/6/16 8:22:00 AM
Date of Analysis: 4/11/16 08:42 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 9.8 Not DetectedDibromochloromethane
1.1 Not Detected 8.8 Not Detected1,2-Dibromoethane (EDB)
1.1 Not Detected 5.3 Not DetectedChlorobenzene
1.1 18 5.0 77Ethyl Benzene
1.1 54 5.0 240m,p-Xylene
1.1 19 5.0 81o-Xylene
1.1 Not Detected 4.9 Not DetectedStyrene
1.1 Not Detected 12 Not DetectedBromoform
1.1 Not Detected 5.6 Not DetectedCumene
1.1 Not Detected 7.9 Not Detected1,1,2,2-Tetrachloroethane
1.1 2.3 5.6 11Propylbenzene
1.1 9.8 5.6 484-Ethyltoluene
1.1 3.5 5.6 171,3,5-Trimethylbenzene
1.1 7.3 5.6 361,2,4-Trimethylbenzene
1.1 Not Detected 6.9 Not Detected1,3-Dichlorobenzene
1.1 Not Detected 6.9 Not Detected1,4-Dichlorobenzene
1.1 Not Detected 5.9 Not Detectedalpha-Chlorotoluene
1.1 Not Detected 6.9 Not Detected1,2-Dichlorobenzene
4.6 Not Detected 34 Not Detected1,2,4-Trichlorobenzene
4.6 Not Detected 49 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
114 70-1304-Bromofluorobenzene
Page 11 of 31
Client Sample ID: IVP-4
Lab ID#: 1604137A-03A
EPA METHOD TO-15 GC/MS FULL SCAN
a041118File Name:
Dil. Factor:2.38
Date of Collection: 4/6/16 8:55:00 AM
Date of Analysis: 4/11/16 09:09 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 5.9 Not DetectedFreon 12
1.2 Not Detected 8.3 Not DetectedFreon 114
12 Not Detected 24 Not DetectedChloromethane
1.2 Not Detected 3.0 Not DetectedVinyl Chloride
1.2 Not Detected 2.6 Not Detected1,3-Butadiene
12 Not Detected 46 Not DetectedBromomethane
4.8 Not Detected 12 Not DetectedChloroethane
1.2 Not Detected 6.7 Not DetectedFreon 11
4.8 34 9.0 64Ethanol
1.2 Not Detected 9.1 Not DetectedFreon 113
1.2 Not Detected 4.7 Not Detected1,1-Dichloroethene
12 38 28 90Acetone
4.8 Not Detected 12 Not Detected2-Propanol
4.8 Not Detected 15 Not DetectedCarbon Disulfide
4.8 Not Detected 15 Not Detected3-Chloropropene
12 Not Detected 41 Not DetectedMethylene Chloride
1.2 Not Detected 4.3 Not DetectedMethyl tert-butyl ether
1.2 Not Detected 4.7 Not Detectedtrans-1,2-Dichloroethene
1.2 Not Detected 4.2 Not DetectedHexane
1.2 Not Detected 4.8 Not Detected1,1-Dichloroethane
4.8 Not Detected 14 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.2 Not Detected 4.7 Not Detectedcis-1,2-Dichloroethene
1.2 Not Detected 3.5 Not DetectedTetrahydrofuran
1.2 Not Detected 5.8 Not DetectedChloroform
1.2 Not Detected 6.5 Not Detected1,1,1-Trichloroethane
1.2 Not Detected 4.1 Not DetectedCyclohexane
1.2 Not Detected 7.5 Not DetectedCarbon Tetrachloride
1.2 1.2 5.6 5.72,2,4-Trimethylpentane
1.2 Not Detected 3.8 Not DetectedBenzene
1.2 Not Detected 4.8 Not Detected1,2-Dichloroethane
1.2 Not Detected 4.9 Not DetectedHeptane
1.2 Not Detected 6.4 Not DetectedTrichloroethene
1.2 Not Detected 5.5 Not Detected1,2-Dichloropropane
4.8 Not Detected 17 Not Detected1,4-Dioxane
1.2 Not Detected 8.0 Not DetectedBromodichloromethane
1.2 Not Detected 5.4 Not Detectedcis-1,3-Dichloropropene
1.2 Not Detected 4.9 Not Detected4-Methyl-2-pentanone
1.2 3.2 4.5 12Toluene
1.2 Not Detected 5.4 Not Detectedtrans-1,3-Dichloropropene
1.2 Not Detected 6.5 Not Detected1,1,2-Trichloroethane
1.2 Not Detected 8.1 Not DetectedTetrachloroethene
4.8 Not Detected 19 Not Detected2-Hexanone
Page 12 of 31
Client Sample ID: IVP-4
Lab ID#: 1604137A-03A
EPA METHOD TO-15 GC/MS FULL SCAN
a041118File Name:
Dil. Factor:2.38
Date of Collection: 4/6/16 8:55:00 AM
Date of Analysis: 4/11/16 09:09 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 10 Not DetectedDibromochloromethane
1.2 Not Detected 9.1 Not Detected1,2-Dibromoethane (EDB)
1.2 Not Detected 5.5 Not DetectedChlorobenzene
1.2 Not Detected 5.2 Not DetectedEthyl Benzene
1.2 1.8 5.2 7.9m,p-Xylene
1.2 Not Detected 5.2 Not Detectedo-Xylene
1.2 Not Detected 5.1 Not DetectedStyrene
1.2 Not Detected 12 Not DetectedBromoform
1.2 Not Detected 5.8 Not DetectedCumene
1.2 Not Detected 8.2 Not Detected1,1,2,2-Tetrachloroethane
1.2 Not Detected 5.8 Not DetectedPropylbenzene
1.2 Not Detected 5.8 Not Detected4-Ethyltoluene
1.2 Not Detected 5.8 Not Detected1,3,5-Trimethylbenzene
1.2 Not Detected 5.8 Not Detected1,2,4-Trimethylbenzene
1.2 Not Detected 7.2 Not Detected1,3-Dichlorobenzene
1.2 Not Detected 7.2 Not Detected1,4-Dichlorobenzene
1.2 Not Detected 6.2 Not Detectedalpha-Chlorotoluene
1.2 Not Detected 7.2 Not Detected1,2-Dichlorobenzene
4.8 Not Detected 35 Not Detected1,2,4-Trichlorobenzene
4.8 Not Detected 51 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
111 70-1304-Bromofluorobenzene
Page 13 of 31
Client Sample ID: IVP-5
Lab ID#: 1604137A-04A
EPA METHOD TO-15 GC/MS FULL SCAN
a041119File Name:
Dil. Factor:2.28
Date of Collection: 4/6/16 9:28:00 AM
Date of Analysis: 4/11/16 11:38 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 5.6 Not DetectedFreon 12
1.1 Not Detected 8.0 Not DetectedFreon 114
11 Not Detected 24 Not DetectedChloromethane
1.1 Not Detected 2.9 Not DetectedVinyl Chloride
1.1 Not Detected 2.5 Not Detected1,3-Butadiene
11 Not Detected 44 Not DetectedBromomethane
4.6 Not Detected 12 Not DetectedChloroethane
1.1 Not Detected 6.4 Not DetectedFreon 11
4.6 170 8.6 320Ethanol
1.1 Not Detected 8.7 Not DetectedFreon 113
1.1 Not Detected 4.5 Not Detected1,1-Dichloroethene
11 100 27 250Acetone
4.6 7.3 11 182-Propanol
4.6 Not Detected 14 Not DetectedCarbon Disulfide
4.6 Not Detected 14 Not Detected3-Chloropropene
11 Not Detected 40 Not DetectedMethylene Chloride
1.1 Not Detected 4.1 Not DetectedMethyl tert-butyl ether
1.1 Not Detected 4.5 Not Detectedtrans-1,2-Dichloroethene
1.1 1.9 4.0 6.8Hexane
1.1 Not Detected 4.6 Not Detected1,1-Dichloroethane
4.6 Not Detected 13 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.1 Not Detected 4.5 Not Detectedcis-1,2-Dichloroethene
1.1 1.2 3.4 3.5Tetrahydrofuran
1.1 Not Detected 5.6 Not DetectedChloroform
1.1 Not Detected 6.2 Not Detected1,1,1-Trichloroethane
1.1 2.1 3.9 7.3Cyclohexane
1.1 Not Detected 7.2 Not DetectedCarbon Tetrachloride
1.1 7.9 5.3 372,2,4-Trimethylpentane
1.1 Not Detected 3.6 Not DetectedBenzene
1.1 Not Detected 4.6 Not Detected1,2-Dichloroethane
1.1 2.7 4.7 11Heptane
1.1 Not Detected 6.1 Not DetectedTrichloroethene
1.1 Not Detected 5.3 Not Detected1,2-Dichloropropane
4.6 Not Detected 16 Not Detected1,4-Dioxane
1.1 Not Detected 7.6 Not DetectedBromodichloromethane
1.1 Not Detected 5.2 Not Detectedcis-1,3-Dichloropropene
1.1 2.0 4.7 8.14-Methyl-2-pentanone
1.1 14 4.3 54Toluene
1.1 Not Detected 5.2 Not Detectedtrans-1,3-Dichloropropene
1.1 Not Detected 6.2 Not Detected1,1,2-Trichloroethane
1.1 Not Detected 7.7 Not DetectedTetrachloroethene
4.6 Not Detected 19 Not Detected2-Hexanone
Page 14 of 31
Client Sample ID: IVP-5
Lab ID#: 1604137A-04A
EPA METHOD TO-15 GC/MS FULL SCAN
a041119File Name:
Dil. Factor:2.28
Date of Collection: 4/6/16 9:28:00 AM
Date of Analysis: 4/11/16 11:38 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 9.7 Not DetectedDibromochloromethane
1.1 Not Detected 8.8 Not Detected1,2-Dibromoethane (EDB)
1.1 Not Detected 5.2 Not DetectedChlorobenzene
1.1 2.5 4.9 11Ethyl Benzene
1.1 9.4 5.0 41m,p-Xylene
1.1 3.4 5.0 15o-Xylene
1.1 Not Detected 4.8 Not DetectedStyrene
1.1 Not Detected 12 Not DetectedBromoform
1.1 Not Detected 5.6 Not DetectedCumene
1.1 Not Detected 7.8 Not Detected1,1,2,2-Tetrachloroethane
1.1 Not Detected 5.6 Not DetectedPropylbenzene
1.1 2.3 5.6 124-Ethyltoluene
1.1 Not Detected 5.6 Not Detected1,3,5-Trimethylbenzene
1.1 2.2 5.6 111,2,4-Trimethylbenzene
1.1 Not Detected 6.8 Not Detected1,3-Dichlorobenzene
1.1 Not Detected 6.8 Not Detected1,4-Dichlorobenzene
1.1 Not Detected 5.9 Not Detectedalpha-Chlorotoluene
1.1 Not Detected 6.8 Not Detected1,2-Dichlorobenzene
4.6 Not Detected 34 Not Detected1,2,4-Trichlorobenzene
4.6 Not Detected 49 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
99 70-1301,2-Dichloroethane-d4
112 70-1304-Bromofluorobenzene
Page 15 of 31
Client Sample ID: IVP-6
Lab ID#: 1604137A-05A
EPA METHOD TO-15 GC/MS FULL SCAN
a041120File Name:
Dil. Factor:2.08
Date of Collection: 4/6/16 10:00:00 AM
Date of Analysis: 4/12/16 12:05 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.0 Not Detected 5.1 Not DetectedFreon 12
1.0 Not Detected 7.3 Not DetectedFreon 114
10 Not Detected 21 Not DetectedChloromethane
1.0 Not Detected 2.6 Not DetectedVinyl Chloride
1.0 Not Detected 2.3 Not Detected1,3-Butadiene
10 Not Detected 40 Not DetectedBromomethane
4.2 Not Detected 11 Not DetectedChloroethane
1.0 Not Detected 5.8 Not DetectedFreon 11
4.2 45 7.8 86Ethanol
1.0 Not Detected 8.0 Not DetectedFreon 113
1.0 Not Detected 4.1 Not Detected1,1-Dichloroethene
10 42 25 100Acetone
4.2 11 10 262-Propanol
4.2 Not Detected 13 Not DetectedCarbon Disulfide
4.2 Not Detected 13 Not Detected3-Chloropropene
10 Not Detected 36 Not DetectedMethylene Chloride
1.0 Not Detected 3.7 Not DetectedMethyl tert-butyl ether
1.0 Not Detected 4.1 Not Detectedtrans-1,2-Dichloroethene
1.0 9.3 3.7 33Hexane
1.0 Not Detected 4.2 Not Detected1,1-Dichloroethane
4.2 Not Detected 12 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.0 Not Detected 4.1 Not Detectedcis-1,2-Dichloroethene
1.0 Not Detected 3.1 Not DetectedTetrahydrofuran
1.0 Not Detected 5.1 Not DetectedChloroform
1.0 Not Detected 5.7 Not Detected1,1,1-Trichloroethane
1.0 9.6 3.6 33Cyclohexane
1.0 Not Detected 6.5 Not DetectedCarbon Tetrachloride
1.0 42 4.8 2002,2,4-Trimethylpentane
1.0 5.6 3.3 18Benzene
1.0 Not Detected 4.2 Not Detected1,2-Dichloroethane
1.0 13 4.3 53Heptane
1.0 Not Detected 5.6 Not DetectedTrichloroethene
1.0 Not Detected 4.8 Not Detected1,2-Dichloropropane
4.2 Not Detected 15 Not Detected1,4-Dioxane
1.0 Not Detected 7.0 Not DetectedBromodichloromethane
1.0 Not Detected 4.7 Not Detectedcis-1,3-Dichloropropene
1.0 Not Detected 4.3 Not Detected4-Methyl-2-pentanone
1.0 75 3.9 280Toluene
1.0 Not Detected 4.7 Not Detectedtrans-1,3-Dichloropropene
1.0 Not Detected 5.7 Not Detected1,1,2-Trichloroethane
1.0 Not Detected 7.0 Not DetectedTetrachloroethene
4.2 Not Detected 17 Not Detected2-Hexanone
Page 16 of 31
Client Sample ID: IVP-6
Lab ID#: 1604137A-05A
EPA METHOD TO-15 GC/MS FULL SCAN
a041120File Name:
Dil. Factor:2.08
Date of Collection: 4/6/16 10:00:00 AM
Date of Analysis: 4/12/16 12:05 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.0 Not Detected 8.8 Not DetectedDibromochloromethane
1.0 Not Detected 8.0 Not Detected1,2-Dibromoethane (EDB)
1.0 Not Detected 4.8 Not DetectedChlorobenzene
1.0 11 4.5 50Ethyl Benzene
1.0 38 4.5 160m,p-Xylene
1.0 14 4.5 61o-Xylene
1.0 Not Detected 4.4 Not DetectedStyrene
1.0 Not Detected 11 Not DetectedBromoform
1.0 Not Detected 5.1 Not DetectedCumene
1.0 Not Detected 7.1 Not Detected1,1,2,2-Tetrachloroethane
1.0 1.7 5.1 8.4Propylbenzene
1.0 7.6 5.1 374-Ethyltoluene
1.0 2.4 5.1 121,3,5-Trimethylbenzene
1.0 6.0 5.1 291,2,4-Trimethylbenzene
1.0 Not Detected 6.2 Not Detected1,3-Dichlorobenzene
1.0 Not Detected 6.2 Not Detected1,4-Dichlorobenzene
1.0 Not Detected 5.4 Not Detectedalpha-Chlorotoluene
1.0 Not Detected 6.2 Not Detected1,2-Dichlorobenzene
4.2 Not Detected 31 Not Detected1,2,4-Trichlorobenzene
4.2 Not Detected 44 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
114 70-1304-Bromofluorobenzene
Page 17 of 31
Client Sample ID: IVP-8
Lab ID#: 1604137A-06A
EPA METHOD TO-15 GC/MS FULL SCAN
a041121File Name:
Dil. Factor:2.34
Date of Collection: 4/6/16 10:46:00 AM
Date of Analysis: 4/12/16 12:32 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 5.8 Not DetectedFreon 12
1.2 Not Detected 8.2 Not DetectedFreon 114
12 Not Detected 24 Not DetectedChloromethane
1.2 Not Detected 3.0 Not DetectedVinyl Chloride
1.2 Not Detected 2.6 Not Detected1,3-Butadiene
12 Not Detected 45 Not DetectedBromomethane
4.7 Not Detected 12 Not DetectedChloroethane
1.2 Not Detected 6.6 Not DetectedFreon 11
4.7 120 8.8 220Ethanol
1.2 Not Detected 9.0 Not DetectedFreon 113
1.2 Not Detected 4.6 Not Detected1,1-Dichloroethene
12 310 28 740Acetone
4.7 4.8 12 122-Propanol
4.7 Not Detected 14 Not DetectedCarbon Disulfide
4.7 Not Detected 15 Not Detected3-Chloropropene
12 Not Detected 41 Not DetectedMethylene Chloride
1.2 Not Detected 4.2 Not DetectedMethyl tert-butyl ether
1.2 Not Detected 4.6 Not Detectedtrans-1,2-Dichloroethene
1.2 Not Detected 4.1 Not DetectedHexane
1.2 Not Detected 4.7 Not Detected1,1-Dichloroethane
4.7 10 14 302-Butanone (Methyl Ethyl Ketone)
1.2 Not Detected 4.6 Not Detectedcis-1,2-Dichloroethene
1.2 3.6 3.4 11Tetrahydrofuran
1.2 Not Detected 5.7 Not DetectedChloroform
1.2 Not Detected 6.4 Not Detected1,1,1-Trichloroethane
1.2 Not Detected 4.0 Not DetectedCyclohexane
1.2 Not Detected 7.4 Not DetectedCarbon Tetrachloride
1.2 Not Detected 5.5 Not Detected2,2,4-Trimethylpentane
1.2 Not Detected 3.7 Not DetectedBenzene
1.2 Not Detected 4.7 Not Detected1,2-Dichloroethane
1.2 Not Detected 4.8 Not DetectedHeptane
1.2 Not Detected 6.3 Not DetectedTrichloroethene
1.2 Not Detected 5.4 Not Detected1,2-Dichloropropane
4.7 Not Detected 17 Not Detected1,4-Dioxane
1.2 Not Detected 7.8 Not DetectedBromodichloromethane
1.2 Not Detected 5.3 Not Detectedcis-1,3-Dichloropropene
1.2 5.6 4.8 234-Methyl-2-pentanone
1.2 1.7 4.4 6.5Toluene
1.2 Not Detected 5.3 Not Detectedtrans-1,3-Dichloropropene
1.2 Not Detected 6.4 Not Detected1,1,2-Trichloroethane
1.2 Not Detected 7.9 Not DetectedTetrachloroethene
4.7 Not Detected 19 Not Detected2-Hexanone
Page 18 of 31
Client Sample ID: IVP-8
Lab ID#: 1604137A-06A
EPA METHOD TO-15 GC/MS FULL SCAN
a041121File Name:
Dil. Factor:2.34
Date of Collection: 4/6/16 10:46:00 AM
Date of Analysis: 4/12/16 12:32 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 10 Not DetectedDibromochloromethane
1.2 Not Detected 9.0 Not Detected1,2-Dibromoethane (EDB)
1.2 Not Detected 5.4 Not DetectedChlorobenzene
1.2 Not Detected 5.1 Not DetectedEthyl Benzene
1.2 2.8 5.1 12m,p-Xylene
1.2 1.4 5.1 6.0o-Xylene
1.2 Not Detected 5.0 Not DetectedStyrene
1.2 Not Detected 12 Not DetectedBromoform
1.2 Not Detected 5.8 Not DetectedCumene
1.2 Not Detected 8.0 Not Detected1,1,2,2-Tetrachloroethane
1.2 Not Detected 5.8 Not DetectedPropylbenzene
1.2 Not Detected 5.8 Not Detected4-Ethyltoluene
1.2 Not Detected 5.8 Not Detected1,3,5-Trimethylbenzene
1.2 Not Detected 5.8 Not Detected1,2,4-Trimethylbenzene
1.2 Not Detected 7.0 Not Detected1,3-Dichlorobenzene
1.2 Not Detected 7.0 Not Detected1,4-Dichlorobenzene
1.2 Not Detected 6.0 Not Detectedalpha-Chlorotoluene
1.2 Not Detected 7.0 Not Detected1,2-Dichlorobenzene
4.7 Not Detected 35 Not Detected1,2,4-Trichlorobenzene
4.7 Not Detected 50 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
102 70-130Toluene-d8
96 70-1301,2-Dichloroethane-d4
111 70-1304-Bromofluorobenzene
Page 19 of 31
Client Sample ID: IVP-9
Lab ID#: 1604137A-07A
EPA METHOD TO-15 GC/MS FULL SCAN
a041122File Name:
Dil. Factor:2.46
Date of Collection: 4/6/16 11:19:00 AM
Date of Analysis: 4/12/16 12:59 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 6.1 Not DetectedFreon 12
1.2 Not Detected 8.6 Not DetectedFreon 114
12 Not Detected 25 Not DetectedChloromethane
1.2 Not Detected 3.1 Not DetectedVinyl Chloride
1.2 Not Detected 2.7 Not Detected1,3-Butadiene
12 Not Detected 48 Not DetectedBromomethane
4.9 Not Detected 13 Not DetectedChloroethane
1.2 Not Detected 6.9 Not DetectedFreon 11
4.9 62 9.3 120Ethanol
1.2 Not Detected 9.4 Not DetectedFreon 113
1.2 Not Detected 4.9 Not Detected1,1-Dichloroethene
12 97 29 230Acetone
4.9 Not Detected 12 Not Detected2-Propanol
4.9 Not Detected 15 Not DetectedCarbon Disulfide
4.9 Not Detected 15 Not Detected3-Chloropropene
12 Not Detected 43 Not DetectedMethylene Chloride
1.2 Not Detected 4.4 Not DetectedMethyl tert-butyl ether
1.2 Not Detected 4.9 Not Detectedtrans-1,2-Dichloroethene
1.2 Not Detected 4.3 Not DetectedHexane
1.2 Not Detected 5.0 Not Detected1,1-Dichloroethane
4.9 Not Detected 14 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.2 Not Detected 4.9 Not Detectedcis-1,2-Dichloroethene
1.2 1.5 3.6 4.3Tetrahydrofuran
1.2 Not Detected 6.0 Not DetectedChloroform
1.2 Not Detected 6.7 Not Detected1,1,1-Trichloroethane
1.2 Not Detected 4.2 Not DetectedCyclohexane
1.2 Not Detected 7.7 Not DetectedCarbon Tetrachloride
1.2 Not Detected 5.7 Not Detected2,2,4-Trimethylpentane
1.2 Not Detected 3.9 Not DetectedBenzene
1.2 Not Detected 5.0 Not Detected1,2-Dichloroethane
1.2 Not Detected 5.0 Not DetectedHeptane
1.2 Not Detected 6.6 Not DetectedTrichloroethene
1.2 Not Detected 5.7 Not Detected1,2-Dichloropropane
4.9 Not Detected 18 Not Detected1,4-Dioxane
1.2 Not Detected 8.2 Not DetectedBromodichloromethane
1.2 Not Detected 5.6 Not Detectedcis-1,3-Dichloropropene
1.2 2.1 5.0 8.54-Methyl-2-pentanone
1.2 1.3 4.6 4.9Toluene
1.2 Not Detected 5.6 Not Detectedtrans-1,3-Dichloropropene
1.2 Not Detected 6.7 Not Detected1,1,2-Trichloroethane
1.2 Not Detected 8.3 Not DetectedTetrachloroethene
4.9 Not Detected 20 Not Detected2-Hexanone
Page 20 of 31
Client Sample ID: IVP-9
Lab ID#: 1604137A-07A
EPA METHOD TO-15 GC/MS FULL SCAN
a041122File Name:
Dil. Factor:2.46
Date of Collection: 4/6/16 11:19:00 AM
Date of Analysis: 4/12/16 12:59 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 10 Not DetectedDibromochloromethane
1.2 Not Detected 9.4 Not Detected1,2-Dibromoethane (EDB)
1.2 Not Detected 5.7 Not DetectedChlorobenzene
1.2 Not Detected 5.3 Not DetectedEthyl Benzene
1.2 2.4 5.3 10m,p-Xylene
1.2 Not Detected 5.3 Not Detectedo-Xylene
1.2 Not Detected 5.2 Not DetectedStyrene
1.2 Not Detected 13 Not DetectedBromoform
1.2 Not Detected 6.0 Not DetectedCumene
1.2 Not Detected 8.4 Not Detected1,1,2,2-Tetrachloroethane
1.2 Not Detected 6.0 Not DetectedPropylbenzene
1.2 1.2 6.0 6.04-Ethyltoluene
1.2 Not Detected 6.0 Not Detected1,3,5-Trimethylbenzene
1.2 Not Detected 6.0 Not Detected1,2,4-Trimethylbenzene
1.2 Not Detected 7.4 Not Detected1,3-Dichlorobenzene
1.2 Not Detected 7.4 Not Detected1,4-Dichlorobenzene
1.2 Not Detected 6.4 Not Detectedalpha-Chlorotoluene
1.2 Not Detected 7.4 Not Detected1,2-Dichlorobenzene
4.9 Not Detected 36 Not Detected1,2,4-Trichlorobenzene
4.9 Not Detected 52 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
93 70-1301,2-Dichloroethane-d4
114 70-1304-Bromofluorobenzene
Page 21 of 31
Client Sample ID: IVP-7
Lab ID#: 1604137A-08A
EPA METHOD TO-15 GC/MS FULL SCAN
a041123File Name:
Dil. Factor:2.46
Date of Collection: 4/6/16 11:55:00 AM
Date of Analysis: 4/12/16 01:25 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 6.1 Not DetectedFreon 12
1.2 Not Detected 8.6 Not DetectedFreon 114
12 Not Detected 25 Not DetectedChloromethane
1.2 Not Detected 3.1 Not DetectedVinyl Chloride
1.2 Not Detected 2.7 Not Detected1,3-Butadiene
12 Not Detected 48 Not DetectedBromomethane
4.9 Not Detected 13 Not DetectedChloroethane
1.2 Not Detected 6.9 Not DetectedFreon 11
4.9 75 9.3 140Ethanol
1.2 Not Detected 9.4 Not DetectedFreon 113
1.2 Not Detected 4.9 Not Detected1,1-Dichloroethene
12 62 29 150Acetone
4.9 5.0 12 122-Propanol
4.9 Not Detected 15 Not DetectedCarbon Disulfide
4.9 Not Detected 15 Not Detected3-Chloropropene
12 Not Detected 43 Not DetectedMethylene Chloride
1.2 Not Detected 4.4 Not DetectedMethyl tert-butyl ether
1.2 Not Detected 4.9 Not Detectedtrans-1,2-Dichloroethene
1.2 Not Detected 4.3 Not DetectedHexane
1.2 Not Detected 5.0 Not Detected1,1-Dichloroethane
4.9 Not Detected 14 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.2 Not Detected 4.9 Not Detectedcis-1,2-Dichloroethene
1.2 1.7 3.6 5.0Tetrahydrofuran
1.2 Not Detected 6.0 Not DetectedChloroform
1.2 Not Detected 6.7 Not Detected1,1,1-Trichloroethane
1.2 Not Detected 4.2 Not DetectedCyclohexane
1.2 Not Detected 7.7 Not DetectedCarbon Tetrachloride
1.2 1.6 5.7 7.42,2,4-Trimethylpentane
1.2 Not Detected 3.9 Not DetectedBenzene
1.2 Not Detected 5.0 Not Detected1,2-Dichloroethane
1.2 Not Detected 5.0 Not DetectedHeptane
1.2 Not Detected 6.6 Not DetectedTrichloroethene
1.2 Not Detected 5.7 Not Detected1,2-Dichloropropane
4.9 Not Detected 18 Not Detected1,4-Dioxane
1.2 Not Detected 8.2 Not DetectedBromodichloromethane
1.2 Not Detected 5.6 Not Detectedcis-1,3-Dichloropropene
1.2 Not Detected 5.0 Not Detected4-Methyl-2-pentanone
1.2 4.0 4.6 15Toluene
1.2 Not Detected 5.6 Not Detectedtrans-1,3-Dichloropropene
1.2 Not Detected 6.7 Not Detected1,1,2-Trichloroethane
1.2 Not Detected 8.3 Not DetectedTetrachloroethene
4.9 Not Detected 20 Not Detected2-Hexanone
Page 22 of 31
Client Sample ID: IVP-7
Lab ID#: 1604137A-08A
EPA METHOD TO-15 GC/MS FULL SCAN
a041123File Name:
Dil. Factor:2.46
Date of Collection: 4/6/16 11:55:00 AM
Date of Analysis: 4/12/16 01:25 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 10 Not DetectedDibromochloromethane
1.2 Not Detected 9.4 Not Detected1,2-Dibromoethane (EDB)
1.2 Not Detected 5.7 Not DetectedChlorobenzene
1.2 Not Detected 5.3 Not DetectedEthyl Benzene
1.2 2.5 5.3 11m,p-Xylene
1.2 Not Detected 5.3 Not Detectedo-Xylene
1.2 Not Detected 5.2 Not DetectedStyrene
1.2 Not Detected 13 Not DetectedBromoform
1.2 Not Detected 6.0 Not DetectedCumene
1.2 Not Detected 8.4 Not Detected1,1,2,2-Tetrachloroethane
1.2 Not Detected 6.0 Not DetectedPropylbenzene
1.2 Not Detected 6.0 Not Detected4-Ethyltoluene
1.2 Not Detected 6.0 Not Detected1,3,5-Trimethylbenzene
1.2 Not Detected 6.0 Not Detected1,2,4-Trimethylbenzene
1.2 Not Detected 7.4 Not Detected1,3-Dichlorobenzene
1.2 Not Detected 7.4 Not Detected1,4-Dichlorobenzene
1.2 Not Detected 6.4 Not Detectedalpha-Chlorotoluene
1.2 Not Detected 7.4 Not Detected1,2-Dichlorobenzene
4.9 Not Detected 36 Not Detected1,2,4-Trichlorobenzene
4.9 Not Detected 52 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
101 70-130Toluene-d8
95 70-1301,2-Dichloroethane-d4
114 70-1304-Bromofluorobenzene
Page 23 of 31
Client Sample ID: Lab Blank
Lab ID#: 1604137A-09A
EPA METHOD TO-15 GC/MS FULL SCAN
a041105File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/11/16 11:41 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 2.5 Not DetectedFreon 12
0.50 Not Detected 3.5 Not DetectedFreon 114
5.0 Not Detected 10 Not DetectedChloromethane
0.50 Not Detected 1.3 Not DetectedVinyl Chloride
0.50 Not Detected 1.1 Not Detected1,3-Butadiene
5.0 Not Detected 19 Not DetectedBromomethane
2.0 Not Detected 5.3 Not DetectedChloroethane
0.50 Not Detected 2.8 Not DetectedFreon 11
2.0 Not Detected 3.8 Not DetectedEthanol
0.50 Not Detected 3.8 Not DetectedFreon 113
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethene
5.0 Not Detected 12 Not DetectedAcetone
2.0 Not Detected 4.9 Not Detected2-Propanol
2.0 Not Detected 6.2 Not DetectedCarbon Disulfide
2.0 Not Detected 6.3 Not Detected3-Chloropropene
5.0 Not Detected 17 Not DetectedMethylene Chloride
0.50 Not Detected 1.8 Not DetectedMethyl tert-butyl ether
0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene
0.50 Not Detected 1.8 Not DetectedHexane
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethane
2.0 Not Detected 5.9 Not Detected2-Butanone (Methyl Ethyl Ketone)
0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene
0.50 Not Detected 1.5 Not DetectedTetrahydrofuran
0.50 Not Detected 2.4 Not DetectedChloroform
0.50 Not Detected 2.7 Not Detected1,1,1-Trichloroethane
0.50 Not Detected 1.7 Not DetectedCyclohexane
0.50 Not Detected 3.1 Not DetectedCarbon Tetrachloride
0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane
0.50 Not Detected 1.6 Not DetectedBenzene
0.50 Not Detected 2.0 Not Detected1,2-Dichloroethane
0.50 Not Detected 2.0 Not DetectedHeptane
0.50 Not Detected 2.7 Not DetectedTrichloroethene
0.50 Not Detected 2.3 Not Detected1,2-Dichloropropane
2.0 Not Detected 7.2 Not Detected1,4-Dioxane
0.50 Not Detected 3.4 Not DetectedBromodichloromethane
0.50 Not Detected 2.3 Not Detectedcis-1,3-Dichloropropene
0.50 Not Detected 2.0 Not Detected4-Methyl-2-pentanone
0.50 Not Detected 1.9 Not DetectedToluene
0.50 Not Detected 2.3 Not Detectedtrans-1,3-Dichloropropene
0.50 Not Detected 2.7 Not Detected1,1,2-Trichloroethane
0.50 Not Detected 3.4 Not DetectedTetrachloroethene
2.0 Not Detected 8.2 Not Detected2-Hexanone
Page 24 of 31
Client Sample ID: Lab Blank
Lab ID#: 1604137A-09A
EPA METHOD TO-15 GC/MS FULL SCAN
a041105File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/11/16 11:41 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 4.2 Not DetectedDibromochloromethane
0.50 Not Detected 3.8 Not Detected1,2-Dibromoethane (EDB)
0.50 Not Detected 2.3 Not DetectedChlorobenzene
0.50 Not Detected 2.2 Not DetectedEthyl Benzene
0.50 Not Detected 2.2 Not Detectedm,p-Xylene
0.50 Not Detected 2.2 Not Detectedo-Xylene
0.50 Not Detected 2.1 Not DetectedStyrene
0.50 Not Detected 5.2 Not DetectedBromoform
0.50 Not Detected 2.4 Not DetectedCumene
0.50 Not Detected 3.4 Not Detected1,1,2,2-Tetrachloroethane
0.50 Not Detected 2.4 Not DetectedPropylbenzene
0.50 Not Detected 2.4 Not Detected4-Ethyltoluene
0.50 Not Detected 2.4 Not Detected1,3,5-Trimethylbenzene
0.50 Not Detected 2.4 Not Detected1,2,4-Trimethylbenzene
0.50 Not Detected 3.0 Not Detected1,3-Dichlorobenzene
0.50 Not Detected 3.0 Not Detected1,4-Dichlorobenzene
0.50 Not Detected 2.6 Not Detectedalpha-Chlorotoluene
0.50 Not Detected 3.0 Not Detected1,2-Dichlorobenzene
2.0 Not Detected 15 Not Detected1,2,4-Trichlorobenzene
2.0 Not Detected 21 Not DetectedHexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
96 70-1301,2-Dichloroethane-d4
115 70-1304-Bromofluorobenzene
Page 25 of 31
Client Sample ID: CCV
Lab ID#: 1604137A-10A
EPA METHOD TO-15 GC/MS FULL SCAN
a041102File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/11/16 08:15 AM
%RecoveryCompound
100Freon 12
97Freon 114
84Chloromethane
98Vinyl Chloride
921,3-Butadiene
93Bromomethane
94Chloroethane
94Freon 11
85Ethanol
95Freon 113
991,1-Dichloroethene
94Acetone
902-Propanol
95Carbon Disulfide
973-Chloropropene
88Methylene Chloride
95Methyl tert-butyl ether
98trans-1,2-Dichloroethene
92Hexane
951,1-Dichloroethane
922-Butanone (Methyl Ethyl Ketone)
96cis-1,2-Dichloroethene
86Tetrahydrofuran
95Chloroform
921,1,1-Trichloroethane
94Cyclohexane
92Carbon Tetrachloride
952,2,4-Trimethylpentane
90Benzene
891,2-Dichloroethane
94Heptane
92Trichloroethene
851,2-Dichloropropane
891,4-Dioxane
90Bromodichloromethane
90cis-1,3-Dichloropropene
864-Methyl-2-pentanone
89Toluene
78trans-1,3-Dichloropropene
791,1,2-Trichloroethane
83Tetrachloroethene
742-Hexanone
Page 26 of 31
Client Sample ID: CCV
Lab ID#: 1604137A-10A
EPA METHOD TO-15 GC/MS FULL SCAN
a041102File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/11/16 08:15 AM
%RecoveryCompound
79Dibromochloromethane
791,2-Dibromoethane (EDB)
80Chlorobenzene
81Ethyl Benzene
81m,p-Xylene
83o-Xylene
82Styrene
82Bromoform
82Cumene
751,1,2,2-Tetrachloroethane
79Propylbenzene
854-Ethyltoluene
801,3,5-Trimethylbenzene
831,2,4-Trimethylbenzene
821,3-Dichlorobenzene
801,4-Dichlorobenzene
80alpha-Chlorotoluene
821,2-Dichlorobenzene
791,2,4-Trichlorobenzene
81Hexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
101 70-1301,2-Dichloroethane-d4
111 70-1304-Bromofluorobenzene
Page 27 of 31
Client Sample ID: LCS
Lab ID#: 1604137A-11A
EPA METHOD TO-15 GC/MS FULL SCAN
a041103File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/11/16 10:36 AM
Limits%RecoveryCompound
Method
98 70-130Freon 12
98 70-130Freon 114
83 70-130Chloromethane
98 70-130Vinyl Chloride
86 70-1301,3-Butadiene
98 70-130Bromomethane
95 70-130Chloroethane
93 70-130Freon 11
87 70-130Ethanol
91 70-130Freon 113
97 70-1301,1-Dichloroethene
86 70-130Acetone
90 70-1302-Propanol
80 70-130Carbon Disulfide
90 70-1303-Chloropropene
85 70-130Methylene Chloride
92 70-130Methyl tert-butyl ether
93 70-130trans-1,2-Dichloroethene
89 70-130Hexane
92 70-1301,1-Dichloroethane
93 70-1302-Butanone (Methyl Ethyl Ketone)
93 70-130cis-1,2-Dichloroethene
82 70-130Tetrahydrofuran
90 70-130Chloroform
88 70-1301,1,1-Trichloroethane
91 70-130Cyclohexane
87 70-130Carbon Tetrachloride
92 70-1302,2,4-Trimethylpentane
88 70-130Benzene
89 70-1301,2-Dichloroethane
91 70-130Heptane
90 70-130Trichloroethene
84 70-1301,2-Dichloropropane
86 70-1301,4-Dioxane
89 70-130Bromodichloromethane
83 70-130cis-1,3-Dichloropropene
88 70-1304-Methyl-2-pentanone
88 70-130Toluene
79 70-130trans-1,3-Dichloropropene
79 70-1301,1,2-Trichloroethane
85 70-130Tetrachloroethene
80 70-1302-Hexanone
Page 28 of 31
Client Sample ID: LCS
Lab ID#: 1604137A-11A
EPA METHOD TO-15 GC/MS FULL SCAN
a041103File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/11/16 10:36 AM
Limits%RecoveryCompound
Method
79 70-130Dibromochloromethane
79 70-1301,2-Dibromoethane (EDB)
80 70-130Chlorobenzene
81 70-130Ethyl Benzene
82 70-130m,p-Xylene
84 70-130o-Xylene
85 70-130Styrene
85 70-130Bromoform
82 70-130Cumene
76 70-1301,1,2,2-Tetrachloroethane
80 70-130Propylbenzene
87 70-1304-Ethyltoluene
81 70-1301,3,5-Trimethylbenzene
84 70-1301,2,4-Trimethylbenzene
81 70-1301,3-Dichlorobenzene
81 70-1301,4-Dichlorobenzene
83 70-130alpha-Chlorotoluene
82 70-1301,2-Dichlorobenzene
85 70-1301,2,4-Trichlorobenzene
88 70-130Hexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
111 70-1304-Bromofluorobenzene
Page 29 of 31
Client Sample ID: LCSD
Lab ID#: 1604137A-11AA
EPA METHOD TO-15 GC/MS FULL SCAN
a041104File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/11/16 11:12 AM
Limits%RecoveryCompound
Method
97 70-130Freon 12
97 70-130Freon 114
85 70-130Chloromethane
96 70-130Vinyl Chloride
88 70-1301,3-Butadiene
97 70-130Bromomethane
95 70-130Chloroethane
92 70-130Freon 11
86 70-130Ethanol
91 70-130Freon 113
96 70-1301,1-Dichloroethene
85 70-130Acetone
90 70-1302-Propanol
80 70-130Carbon Disulfide
86 70-1303-Chloropropene
85 70-130Methylene Chloride
92 70-130Methyl tert-butyl ether
97 70-130trans-1,2-Dichloroethene
87 70-130Hexane
92 70-1301,1-Dichloroethane
91 70-1302-Butanone (Methyl Ethyl Ketone)
93 70-130cis-1,2-Dichloroethene
81 70-130Tetrahydrofuran
90 70-130Chloroform
88 70-1301,1,1-Trichloroethane
92 70-130Cyclohexane
86 70-130Carbon Tetrachloride
92 70-1302,2,4-Trimethylpentane
90 70-130Benzene
87 70-1301,2-Dichloroethane
94 70-130Heptane
90 70-130Trichloroethene
84 70-1301,2-Dichloropropane
88 70-1301,4-Dioxane
90 70-130Bromodichloromethane
84 70-130cis-1,3-Dichloropropene
87 70-1304-Methyl-2-pentanone
86 70-130Toluene
79 70-130trans-1,3-Dichloropropene
80 70-1301,1,2-Trichloroethane
84 70-130Tetrachloroethene
81 70-1302-Hexanone
Page 30 of 31
Client Sample ID: LCSD
Lab ID#: 1604137A-11AA
EPA METHOD TO-15 GC/MS FULL SCAN
a041104File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/11/16 11:12 AM
Limits%RecoveryCompound
Method
80 70-130Dibromochloromethane
79 70-1301,2-Dibromoethane (EDB)
80 70-130Chlorobenzene
81 70-130Ethyl Benzene
82 70-130m,p-Xylene
85 70-130o-Xylene
84 70-130Styrene
85 70-130Bromoform
82 70-130Cumene
77 70-1301,1,2,2-Tetrachloroethane
82 70-130Propylbenzene
87 70-1304-Ethyltoluene
82 70-1301,3,5-Trimethylbenzene
84 70-1301,2,4-Trimethylbenzene
83 70-1301,3-Dichlorobenzene
82 70-1301,4-Dichlorobenzene
84 70-130alpha-Chlorotoluene
83 70-1301,2-Dichlorobenzene
88 70-1301,2,4-Trichlorobenzene
91 70-130Hexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
114 70-1304-Bromofluorobenzene
Page 31 of 31
4/12/2016
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte NC 28269
Project Name: E43
Project #: 20160086.001A
Dear Mr. Michael Sussman
The following report includes the data for the above referenced project for sample(s)
received on 4/7/2016 at Air Toxics Ltd.
The data and associated QC analyzed by Modified ASTM D-1946 are compliant with
the project requirements or laboratory criteria with the exception of the deviations
noted in the attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contactthe Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1604137B
Page 1 of 18
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
WORK ORDER #:1604137B
CLIENT:BILL TO:
PHONE:
Mr. Michael Sussman
Kleinfelder Southeast, Inc.
6200 Harris Technology Boulevard
Charlotte, NC 28269
704-598-1049
704-598-1050
04/07/2016
DATE COMPLETED:04/12/2016
P.O. #
PROJECT #20160086.001A E43
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A IVP-1 Modified ASTM D-1946 3.7 "Hg 14.7 psi
02A IVP-2 Modified ASTM D-1946 4.1 "Hg 14.4 psi
03A IVP-4 Modified ASTM D-1946 4.5 "Hg 15.1 psi
04A IVP-5 Modified ASTM D-1946 3.5 "Hg 14.9 psi
05A IVP-6 Modified ASTM D-1946 1 "Hg 14.9 psi
06A IVP-8 Modified ASTM D-1946 4.1 "Hg 15 psi
07A IVP-9 Modified ASTM D-1946 5.5 "Hg 14.9 psi
08A IVP-7 Modified ASTM D-1946 5.5 "Hg 14.9 psi
09A Lab Blank Modified ASTM D-1946 NA NA
09B Lab Blank Modified ASTM D-1946 NA NA
10A LCS Modified ASTM D-1946 NA NA
10AA LCSD Modified ASTM D-1946 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2015, Expiration date: 10/17/2016.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630
[phone] . [phone] . FAX [phone]
04/12/16
Page 2 of 18
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704434-15-9, UT NELAP CA0093332015-6, VA NELAP - 8113, WA NELAP - C935
LABORATORY NARRATIVEModified ASTM D-1946Kleinfelder Southeast, Inc.Workorder# 1604137B
Eight 1 Liter Summa Canister (100% Certified) samples were received on April 07, 2016. The
laboratory performed analysis via Modified ASTM Method D-1946 for Methane and fixed gases in air
using GC/FID or GC/TCD. The method involves direct injection of 1.0 mL of sample.
On the analytical column employed for this analysis, Oxygen coelutes with Argon. The corresponding
peak is quantitated as Oxygen.
Since Nitrogen is used to pressurize samples, the reported Nitrogen values are calculated by adding all
the sample components and subtracting from 100%.
Method modifications taken to run these samples are summarized in the table below. Specific project
requirements may over-ride the ATL modifications.
Requirement ATL ModificationsASTM D-1946
Calibration A single point
calibration is
performed using a
reference standard
closely matching the
composition of the
unknown.
A minimum of 5-point calibration curve is performed.
Quantitation is based on average Response Factor.
Reference Standard The composition of any
reference standard
must be known to
within 0.01 mol % for
any component.
The standards used by ATL are blended to a >/= 95%
accuracy.
Sample Injection Volume Components whose
concentrations are in
excess of 5 % should
not be analyzed by
using sample volumes
greater than 0.5 mL.
The sample container is connected directly to a fixed
volume sample loop of 1.0 mL on the GC. Linear range
is defined by the calibration curve. Bags are loaded by
vacuum.
Normalization Normalize the mole
percent values by
multiplying each value
by 100 and dividing by
the sum of the original
values. The sum of the
original values should
not differ from 100%
by more than 1.0%.
Results are not normalized. The sum of the reported
values can differ from 100% by as much as 15%, either
due to analytical variability or an unusual sample matrix.
Precision Precision requirements
established at each
concentration level.
Duplicates should agree within 25% RPD for detections
> 5 X's the RL.
Page 3 of 18
Receiving Notes
Sample collection date was incomplete on the Chain of Custody. The year of collection was assumed
to be 2016.
The Chain of Custody (COC) information for sample IVP-5 did not match the information on the
canister with regard to canister identification. The client was notified of the discrepancy and the
information on the canister was used to process and report the sample.
There were no analytical discrepancies.
Analytical Notes
Seven qualifiers may have been used on the data analysis sheets and indicate as follows:
B - Compound present in laboratory blank greater than reporting limit.
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the detection limit.
M - Reported value may be biased due to apparent matrix interferences.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 4 of 18
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
Summary of Detected Compounds
Client Sample ID: IVP-1
Lab ID#: 1604137B-01A
(%)(%)Compound
AmountRpt. Limit
0.23 21Oxygen
0.23 79Nitrogen
0.00023 0.00023Methane
0.023 0.22Carbon Dioxide
Client Sample ID: IVP-2
Lab ID#: 1604137B-02A
(%)(%)Compound
AmountRpt. Limit
0.23 21Oxygen
0.23 78Nitrogen
0.023 0.43Carbon Dioxide
Client Sample ID: IVP-4
Lab ID#: 1604137B-03A
(%)(%)Compound
AmountRpt. Limit
0.24 21Oxygen
0.24 79Nitrogen
0.00024 0.00026Methane
0.024 0.20Carbon Dioxide
0.12 0.13Helium
Client Sample ID: IVP-5
Lab ID#: 1604137B-04A
(%)(%)Compound
AmountRpt. Limit
0.23 20Oxygen
0.23 80Nitrogen
0.00023 0.00032Methane
0.023 0.085Carbon Dioxide
Page 5 of 18
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
Summary of Detected Compounds
Client Sample ID: IVP-6
Lab ID#: 1604137B-05A
(%)(%)Compound
AmountRpt. Limit
0.21 21Oxygen
0.21 79Nitrogen
0.021 0.051Carbon Dioxide
0.10 0.29Helium
Client Sample ID: IVP-8
Lab ID#: 1604137B-06A
(%)(%)Compound
AmountRpt. Limit
0.23 21Oxygen
0.23 79Nitrogen
Client Sample ID: IVP-9
Lab ID#: 1604137B-07A
(%)(%)Compound
AmountRpt. Limit
0.25 21Oxygen
0.25 79Nitrogen
0.025 0.16Carbon Dioxide
Client Sample ID: IVP-7
Lab ID#: 1604137B-08A
(%)(%)Compound
AmountRpt. Limit
0.25 21Oxygen
0.25 79Nitrogen
Page 6 of 18
Client Sample ID: IVP-1
Lab ID#: 1604137B-01A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040905File Name:
Dil. Factor:2.28
Date of Collection: 4/6/16 7:40:00 AM
Date of Analysis: 4/9/16 08:22 AM
(%)(%)Compound
AmountRpt. Limit
0.23 21Oxygen
0.23 79Nitrogen
0.023 Not DetectedCarbon Monoxide
0.00023 0.00023Methane
0.023 0.22Carbon Dioxide
0.0023 Not DetectedEthane
0.0023 Not DetectedEthene
0.11 Not DetectedHelium
Container Type: 1 Liter Summa Canister (100% Certified)
Page 7 of 18
Client Sample ID: IVP-2
Lab ID#: 1604137B-02A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040906File Name:
Dil. Factor:2.29
Date of Collection: 4/6/16 8:22:00 AM
Date of Analysis: 4/9/16 08:48 AM
(%)(%)Compound
AmountRpt. Limit
0.23 21Oxygen
0.23 78Nitrogen
0.023 Not DetectedCarbon Monoxide
0.00023 Not DetectedMethane
0.023 0.43Carbon Dioxide
0.0023 Not DetectedEthane
0.0023 Not DetectedEthene
0.11 Not DetectedHelium
Container Type: 1 Liter Summa Canister (100% Certified)
Page 8 of 18
Client Sample ID: IVP-4
Lab ID#: 1604137B-03A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040907File Name:
Dil. Factor:2.38
Date of Collection: 4/6/16 8:55:00 AM
Date of Analysis: 4/9/16 09:13 AM
(%)(%)Compound
AmountRpt. Limit
0.24 21Oxygen
0.24 79Nitrogen
0.024 Not DetectedCarbon Monoxide
0.00024 0.00026Methane
0.024 0.20Carbon Dioxide
0.0024 Not DetectedEthane
0.0024 Not DetectedEthene
0.12 0.13Helium
Container Type: 1 Liter Summa Canister (100% Certified)
Page 9 of 18
Client Sample ID: IVP-5
Lab ID#: 1604137B-04A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040908File Name:
Dil. Factor:2.28
Date of Collection: 4/6/16 9:28:00 AM
Date of Analysis: 4/9/16 09:40 AM
(%)(%)Compound
AmountRpt. Limit
0.23 20Oxygen
0.23 80Nitrogen
0.023 Not DetectedCarbon Monoxide
0.00023 0.00032Methane
0.023 0.085Carbon Dioxide
0.0023 Not DetectedEthane
0.0023 Not DetectedEthene
0.11 Not DetectedHelium
Container Type: 1 Liter Summa Canister (100% Certified)
Page 10 of 18
Client Sample ID: IVP-6
Lab ID#: 1604137B-05A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040909File Name:
Dil. Factor:2.08
Date of Collection: 4/6/16 10:00:00 AM
Date of Analysis: 4/9/16 10:04 AM
(%)(%)Compound
AmountRpt. Limit
0.21 21Oxygen
0.21 79Nitrogen
0.021 Not DetectedCarbon Monoxide
0.00021 Not DetectedMethane
0.021 0.051Carbon Dioxide
0.0021 Not DetectedEthane
0.0021 Not DetectedEthene
0.10 0.29Helium
Container Type: 1 Liter Summa Canister (100% Certified)
Page 11 of 18
Client Sample ID: IVP-8
Lab ID#: 1604137B-06A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040910File Name:
Dil. Factor:2.34
Date of Collection: 4/6/16 10:46:00 AM
Date of Analysis: 4/9/16 10:28 AM
(%)(%)Compound
AmountRpt. Limit
0.23 21Oxygen
0.23 79Nitrogen
0.023 Not DetectedCarbon Monoxide
0.00023 Not DetectedMethane
0.023 Not DetectedCarbon Dioxide
0.0023 Not DetectedEthane
0.0023 Not DetectedEthene
0.12 Not DetectedHelium
Container Type: 1 Liter Summa Canister (100% Certified)
Page 12 of 18
Client Sample ID: IVP-9
Lab ID#: 1604137B-07A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040911File Name:
Dil. Factor:2.47
Date of Collection: 4/6/16 11:19:00 AM
Date of Analysis: 4/9/16 10:52 AM
(%)(%)Compound
AmountRpt. Limit
0.25 21Oxygen
0.25 79Nitrogen
0.025 Not DetectedCarbon Monoxide
0.00025 Not DetectedMethane
0.025 0.16Carbon Dioxide
0.0025 Not DetectedEthane
0.0025 Not DetectedEthene
0.12 Not DetectedHelium
Container Type: 1 Liter Summa Canister (100% Certified)
Page 13 of 18
Client Sample ID: IVP-7
Lab ID#: 1604137B-08A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040912File Name:
Dil. Factor:2.47
Date of Collection: 4/6/16 11:55:00 AM
Date of Analysis: 4/9/16 11:14 AM
(%)(%)Compound
AmountRpt. Limit
0.25 21Oxygen
0.25 79Nitrogen
0.025 Not DetectedCarbon Monoxide
0.00025 Not DetectedMethane
0.025 Not DetectedCarbon Dioxide
0.0025 Not DetectedEthane
0.0025 Not DetectedEthene
0.12 Not DetectedHelium
Container Type: 1 Liter Summa Canister (100% Certified)
Page 14 of 18
Client Sample ID: Lab Blank
Lab ID#: 1604137B-09A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040903File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/9/16 07:30 AM
(%)(%)Compound
AmountRpt. Limit
0.10 Not DetectedOxygen
0.10 Not DetectedNitrogen
0.010 Not DetectedCarbon Monoxide
0.00010 Not DetectedMethane
0.010 Not DetectedCarbon Dioxide
0.0010 Not DetectedEthane
0.0010 Not DetectedEthene
Container Type: NA - Not Applicable
Page 15 of 18
Client Sample ID: Lab Blank
Lab ID#: 1604137B-09B
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040904cFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/9/16 07:56 AM
(%)(%)Compound
AmountRpt. Limit
0.050 Not DetectedHelium
Container Type: NA - Not Applicable
Page 16 of 18
Client Sample ID: LCS
Lab ID#: 1604137B-10A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040902File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/9/16 07:02 AM
Limits%RecoveryCompound
Method
99 85-115Oxygen
92 85-115Nitrogen
94 85-115Carbon Monoxide
101 85-115Methane
96 85-115Carbon Dioxide
101 85-115Ethane
102 85-115Ethene
102 85-115Helium
Container Type: NA - Not Applicable
Page 17 of 18
Client Sample ID: LCSD
Lab ID#: 1604137B-10AA
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10040918File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 4/9/16 01:50 PM
Limits%RecoveryCompound
Method
99 85-115Oxygen
92 85-115Nitrogen
94 85-115Carbon Monoxide
100 85-115Methane
99 85-115Carbon Dioxide
100 85-115Ethane
100 85-115Ethene
102 85-115Helium
Container Type: NA - Not Applicable
Page 18 of 18
#=CL#
March 25, 2016
LIMS USE: FR - MICHAEL BURNS
LIMS OBJECT ID: 92290871
92290871
Project:
Pace Project No.:
RE:
Michael J. Burns
Kleinfelder
3500 Gatway Center Blvd.
Suite 200
Morrisville, NC 27560
E43
Dear Michael Burns:
Enclosed are the analytical results for sample(s) received by the laboratory on March 22, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
cc:Chris Hollinger, Kleinfelder
, Trigon
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 44
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92290871
E43
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 44
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92290871
E43
Lab ID Sample ID Matrix Date Collected Date Received
92290871001 DF1 2-3 Solid 03/21/16 08:30 03/22/16 08:46
92290871002 DP2 2-3 Solid 03/21/16 08:45 03/22/16 08:46
92290871003 DP3 4-5 Solid 03/21/16 09:30 03/22/16 08:46
92290871004 DP4 2-3 Solid 03/21/16 10:30 03/22/16 08:46
92290871005 DP5 0-0.5 Solid 03/21/16 10:40 03/22/16 08:46
92290871006 DP6 0.5-1 Solid 03/21/16 11:11 03/22/16 08:46
92290871007 DP7 0-0.5 Solid 03/21/16 11:30 03/22/16 08:46
92290871008 DP8 0-0.5 Solid 03/21/16 11:50 03/22/16 08:46
92290871009 DP9 0.5-1 Solid 03/21/16 12:20 03/22/16 08:46
92290871010 DP10 0-1 Solid 03/21/16 12:40 03/22/16 08:46
92290871011 TMW-1 Water 03/21/16 14:20 03/22/16 08:46
92290871012 TMW-2 Water 03/21/16 14:40 03/22/16 08:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 44
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92290871
E43
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92290871001 DF1 2-3 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92290871002 DP2 2-3 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92290871003 DP3 4-5 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92290871004 DP4 2-3 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92290871005 DP5 0-0.5 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92290871006 DP6 0.5-1 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92290871007 DP7 0-0.5 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92290871008 DP8 0-0.5 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92290871009 DP9 0.5-1 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92290871010 DP10 0-1 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92290871011 TMW-1 EPA 8260 63 PASI-CNB
92290871012 TMW-2 EPA 8260 63 PASI-CNB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DF1 2-3 Lab ID:92290871001 Collected:03/21/16 08:30 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 56.3J ug/kg 03/22/16 19:11 67-64-192.3 9.2 1
Benzene ND ug/kg 03/22/16 19:11 71-43-24.6 1.5 1
Bromobenzene ND ug/kg 03/22/16 19:11 108-86-14.6 1.8 1
Bromochloromethane ND ug/kg 03/22/16 19:11 74-97-54.6 1.6 1
Bromodichloromethane ND ug/kg 03/22/16 19:11 75-27-44.6 1.8 1
Bromoform ND ug/kg 03/22/16 19:11 75-25-24.6 2.1 1
Bromomethane ND ug/kg 03/22/16 19:11 74-83-99.2 2.3 1
2-Butanone (MEK)ND ug/kg 03/22/16 19:11 78-93-392.3 2.7 1
n-Butylbenzene ND ug/kg 03/22/16 19:11 104-51-84.6 1.7 1
sec-Butylbenzene ND ug/kg 03/22/16 19:11 135-98-84.6 1.5 1
tert-Butylbenzene ND ug/kg 03/22/16 19:11 98-06-64.6 1.8 1
Carbon tetrachloride ND ug/kg 03/22/16 19:11 56-23-54.6 2.4 1
Chlorobenzene ND ug/kg 03/22/16 19:11 108-90-74.6 1.8 1
Chloroethane ND ug/kg 03/22/16 19:11 75-00-39.2 2.2 1
Chloroform ND ug/kg 03/22/16 19:11 67-66-34.6 1.5 1
Chloromethane ND ug/kg 03/22/16 19:11 74-87-39.2 2.2 1
2-Chlorotoluene ND ug/kg 03/22/16 19:11 95-49-84.6 1.6 1
4-Chlorotoluene ND ug/kg 03/22/16 19:11 106-43-44.6 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/16 19:11 96-12-84.6 3.3 1
Dibromochloromethane ND ug/kg 03/22/16 19:11 124-48-14.6 1.7 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/16 19:11 106-93-44.6 1.7 1
Dibromomethane ND ug/kg 03/22/16 19:11 74-95-34.6 2.3 1
1,2-Dichlorobenzene ND ug/kg 03/22/16 19:11 95-50-14.6 1.8 1
1,3-Dichlorobenzene ND ug/kg 03/22/16 19:11 541-73-14.6 1.8 1
1,4-Dichlorobenzene ND ug/kg 03/22/16 19:11 106-46-74.6 1.6 1
Dichlorodifluoromethane ND ug/kg 03/22/16 19:11 75-71-89.2 3.3 1
1,1-Dichloroethane ND ug/kg 03/22/16 19:11 75-34-34.6 1.4 1
1,2-Dichloroethane ND ug/kg 03/22/16 19:11 107-06-24.6 2.0 1
1,1-Dichloroethene ND ug/kg 03/22/16 19:11 75-35-44.6 1.7 1
cis-1,2-Dichloroethene ND ug/kg 03/22/16 19:11 156-59-24.6 1.3 1
trans-1,2-Dichloroethene ND ug/kg 03/22/16 19:11 156-60-54.6 1.8 1
1,2-Dichloropropane ND ug/kg 03/22/16 19:11 78-87-54.6 1.6 1
1,3-Dichloropropane ND ug/kg 03/22/16 19:11 142-28-94.6 1.8 1
2,2-Dichloropropane ND ug/kg 03/22/16 19:11 594-20-74.6 1.6 1
1,1-Dichloropropene ND ug/kg 03/22/16 19:11 563-58-64.6 1.4 1
cis-1,3-Dichloropropene ND ug/kg 03/22/16 19:11 10061-01-54.6 1.7 1
trans-1,3-Dichloropropene ND ug/kg 03/22/16 19:11 10061-02-64.6 1.4 1
Diisopropyl ether ND ug/kg 03/22/16 19:11 108-20-34.6 1.6 1
Ethylbenzene ND ug/kg 03/22/16 19:11 100-41-44.6 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/16 19:11 87-68-34.6 1.8 1
2-Hexanone ND ug/kg 03/22/16 19:11 591-78-646.2 3.6 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/16 19:11 98-82-84.6 1.8 1
p-Isopropyltoluene ND ug/kg 03/22/16 19:11 99-87-64.6 1.6 1
Methylene Chloride ND ug/kg 03/22/16 19:11 75-09-218.5 2.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/16 19:11 108-10-146.2 3.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DF1 2-3 Lab ID:92290871001 Collected:03/21/16 08:30 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 03/22/16 19:11 1634-04-44.6 1.4 1
Naphthalene ND ug/kg 03/22/16 19:11 91-20-34.6 1.1 1
n-Propylbenzene ND ug/kg 03/22/16 19:11 103-65-14.6 1.6 1
Styrene ND ug/kg 03/22/16 19:11 100-42-54.6 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/16 19:11 630-20-64.6 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/16 19:11 79-34-54.6 1.8 1
Tetrachloroethene ND ug/kg 03/22/16 19:11 127-18-44.6 1.6 1
Toluene ND ug/kg 03/22/16 19:11 108-88-34.6 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/16 19:11 87-61-64.6 2.0 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/16 19:11 120-82-14.6 1.5 1
1,1,1-Trichloroethane ND ug/kg 03/22/16 19:11 71-55-64.6 1.7 1
1,1,2-Trichloroethane ND ug/kg 03/22/16 19:11 79-00-54.6 1.9 1
Trichloroethene ND ug/kg 03/22/16 19:11 79-01-64.6 1.9 1
Trichlorofluoromethane ND ug/kg 03/22/16 19:11 75-69-44.6 2.0 1
1,2,3-Trichloropropane ND ug/kg 03/22/16 19:11 96-18-44.6 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/16 19:11 95-63-64.6 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/16 19:11 108-67-84.6 1.7 1
Vinyl acetate ND ug/kg 03/22/16 19:11 108-05-446.2 8.1 1
Vinyl chloride ND ug/kg 03/22/16 19:11 75-01-49.2 1.7 1
Xylene (Total)ND ug/kg 03/22/16 19:11 1330-20-79.2 3.3 1
m&p-Xylene ND ug/kg 03/22/16 19:11 179601-23-19.2 3.3 1
o-Xylene ND ug/kg 03/22/16 19:11 95-47-64.6 1.8 1
Surrogates
Toluene-d8 (S)103 %03/22/16 19:11 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %03/22/16 19:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %03/22/16 19:11 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.1 %03/23/16 06:220.10 0.10 1
Sample:DP2 2-3 Lab ID:92290871002 Collected:03/21/16 08:45 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 34.7J ug/kg 03/22/16 19:31 67-64-110110.1 1
Benzene ND ug/kg 03/22/16 19:31 71-43-25.1 1.6 1
Bromobenzene ND ug/kg 03/22/16 19:31 108-86-15.1 2.0 1
Bromochloromethane ND ug/kg 03/22/16 19:31 74-97-55.1 1.7 1
Bromodichloromethane ND ug/kg 03/22/16 19:31 75-27-45.1 1.9 1
Bromoform ND ug/kg 03/22/16 19:31 75-25-25.1 2.3 1
Bromomethane ND ug/kg 03/22/16 19:31 74-83-910.1 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP2 2-3 Lab ID:92290871002 Collected:03/21/16 08:45 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
2-Butanone (MEK)ND ug/kg 03/22/16 19:31 78-93-31012.9 1
n-Butylbenzene ND ug/kg 03/22/16 19:31 104-51-85.1 1.8 1
sec-Butylbenzene ND ug/kg 03/22/16 19:31 135-98-85.1 1.6 1
tert-Butylbenzene ND ug/kg 03/22/16 19:31 98-06-65.1 2.0 1
Carbon tetrachloride ND ug/kg 03/22/16 19:31 56-23-55.1 2.6 1
Chlorobenzene ND ug/kg 03/22/16 19:31 108-90-75.1 1.9 1
Chloroethane ND ug/kg 03/22/16 19:31 75-00-310.1 2.4 1
Chloroform ND ug/kg 03/22/16 19:31 67-66-35.1 1.6 1
Chloromethane ND ug/kg 03/22/16 19:31 74-87-310.1 2.4 1
2-Chlorotoluene ND ug/kg 03/22/16 19:31 95-49-85.1 1.7 1
4-Chlorotoluene ND ug/kg 03/22/16 19:31 106-43-45.1 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/16 19:31 96-12-85.1 3.7 1
Dibromochloromethane ND ug/kg 03/22/16 19:31 124-48-15.1 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/16 19:31 106-93-45.1 1.8 1
Dibromomethane ND ug/kg 03/22/16 19:31 74-95-35.1 2.5 1
1,2-Dichlorobenzene ND ug/kg 03/22/16 19:31 95-50-15.1 1.9 1
1,3-Dichlorobenzene ND ug/kg 03/22/16 19:31 541-73-15.1 2.0 1
1,4-Dichlorobenzene ND ug/kg 03/22/16 19:31 106-46-75.1 1.7 1
Dichlorodifluoromethane ND ug/kg 03/22/16 19:31 75-71-810.1 3.7 1
1,1-Dichloroethane ND ug/kg 03/22/16 19:31 75-34-35.1 1.5 1
1,2-Dichloroethane ND ug/kg 03/22/16 19:31 107-06-25.1 2.2 1
1,1-Dichloroethene ND ug/kg 03/22/16 19:31 75-35-45.1 1.8 1
cis-1,2-Dichloroethene ND ug/kg 03/22/16 19:31 156-59-25.1 1.4 1
trans-1,2-Dichloroethene ND ug/kg 03/22/16 19:31 156-60-55.1 1.9 1
1,2-Dichloropropane ND ug/kg 03/22/16 19:31 78-87-55.1 1.7 1
1,3-Dichloropropane ND ug/kg 03/22/16 19:31 142-28-95.1 1.9 1
2,2-Dichloropropane ND ug/kg 03/22/16 19:31 594-20-75.1 1.7 1
1,1-Dichloropropene ND ug/kg 03/22/16 19:31 563-58-65.1 1.5 1
cis-1,3-Dichloropropene ND ug/kg 03/22/16 19:31 10061-01-55.1 1.8 1
trans-1,3-Dichloropropene ND ug/kg 03/22/16 19:31 10061-02-65.1 1.5 1
Diisopropyl ether ND ug/kg 03/22/16 19:31 108-20-35.1 1.7 1
Ethylbenzene ND ug/kg 03/22/16 19:31 100-41-45.1 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/16 19:31 87-68-35.1 2.0 1
2-Hexanone ND ug/kg 03/22/16 19:31 591-78-650.7 4.0 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/16 19:31 98-82-85.1 1.9 1
p-Isopropyltoluene ND ug/kg 03/22/16 19:31 99-87-65.1 1.7 1
Methylene Chloride 5.0J ug/kg 03/22/16 19:31 75-09-220.3 3.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/16 19:31 108-10-150.7 3.8 1
Methyl-tert-butyl ether ND ug/kg 03/22/16 19:31 1634-04-45.1 1.5 1
Naphthalene ND ug/kg 03/22/16 19:31 91-20-35.1 1.2 1
n-Propylbenzene ND ug/kg 03/22/16 19:31 103-65-15.1 1.7 1
Styrene ND ug/kg 03/22/16 19:31 100-42-55.1 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/16 19:31 630-20-65.1 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/16 19:31 79-34-55.1 1.9 1
Tetrachloroethene ND ug/kg 03/22/16 19:31 127-18-45.1 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP2 2-3 Lab ID:92290871002 Collected:03/21/16 08:45 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Toluene ND ug/kg 03/22/16 19:31 108-88-35.1 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/16 19:31 87-61-65.1 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/16 19:31 120-82-15.1 1.6 1
1,1,1-Trichloroethane ND ug/kg 03/22/16 19:31 71-55-65.1 1.8 1
1,1,2-Trichloroethane ND ug/kg 03/22/16 19:31 79-00-55.1 2.1 1
Trichloroethene ND ug/kg 03/22/16 19:31 79-01-65.1 2.1 1
Trichlorofluoromethane ND ug/kg 03/22/16 19:31 75-69-45.1 2.2 1
1,2,3-Trichloropropane ND ug/kg 03/22/16 19:31 96-18-45.1 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/16 19:31 95-63-65.1 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/16 19:31 108-67-85.1 1.8 1
Vinyl acetate ND ug/kg 03/22/16 19:31 108-05-450.7 8.9 1
Vinyl chloride ND ug/kg 03/22/16 19:31 75-01-410.1 1.8 1
Xylene (Total)ND ug/kg 03/22/16 19:31 1330-20-710.1 3.7 1
m&p-Xylene ND ug/kg 03/22/16 19:31 179601-23-110.1 3.7 1
o-Xylene ND ug/kg 03/22/16 19:31 95-47-65.1 1.9 1
Surrogates
Toluene-d8 (S)102 %03/22/16 19:31 2037-26-570-130 1
4-Bromofluorobenzene (S)91 %03/22/16 19:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %03/22/16 19:31 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.5 %03/23/16 06:220.10 0.10 1
Sample:DP3 4-5 Lab ID:92290871003 Collected:03/21/16 09:30 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/22/16 19:51 67-64-110110.1 1
Benzene ND ug/kg 03/22/16 19:51 71-43-25.0 1.6 1
Bromobenzene ND ug/kg 03/22/16 19:51 108-86-15.0 2.0 1
Bromochloromethane ND ug/kg 03/22/16 19:51 74-97-55.0 1.7 1
Bromodichloromethane ND ug/kg 03/22/16 19:51 75-27-45.0 1.9 1
Bromoform ND ug/kg 03/22/16 19:51 75-25-25.0 2.3 1
Bromomethane ND ug/kg 03/22/16 19:51 74-83-910.1 2.5 1
2-Butanone (MEK)ND ug/kg 03/22/16 19:51 78-93-31012.9 1
n-Butylbenzene ND ug/kg 03/22/16 19:51 104-51-85.0 1.8 1
sec-Butylbenzene ND ug/kg 03/22/16 19:51 135-98-85.0 1.6 1
tert-Butylbenzene ND ug/kg 03/22/16 19:51 98-06-65.0 2.0 1
Carbon tetrachloride ND ug/kg 03/22/16 19:51 56-23-55.0 2.6 1
Chlorobenzene ND ug/kg 03/22/16 19:51 108-90-75.0 1.9 1
Chloroethane ND ug/kg 03/22/16 19:51 75-00-310.1 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP3 4-5 Lab ID:92290871003 Collected:03/21/16 09:30 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroform ND ug/kg 03/22/16 19:51 67-66-35.0 1.6 1
Chloromethane ND ug/kg 03/22/16 19:51 74-87-310.1 2.4 1
2-Chlorotoluene ND ug/kg 03/22/16 19:51 95-49-85.0 1.7 1
4-Chlorotoluene ND ug/kg 03/22/16 19:51 106-43-45.0 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/16 19:51 96-12-85.0 3.6 1
Dibromochloromethane ND ug/kg 03/22/16 19:51 124-48-15.0 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/16 19:51 106-93-45.0 1.8 1
Dibromomethane ND ug/kg 03/22/16 19:51 74-95-35.0 2.5 1
1,2-Dichlorobenzene ND ug/kg 03/22/16 19:51 95-50-15.0 1.9 1
1,3-Dichlorobenzene ND ug/kg 03/22/16 19:51 541-73-15.0 2.0 1
1,4-Dichlorobenzene ND ug/kg 03/22/16 19:51 106-46-75.0 1.7 1
Dichlorodifluoromethane ND ug/kg 03/22/16 19:51 75-71-810.1 3.6 1
1,1-Dichloroethane ND ug/kg 03/22/16 19:51 75-34-35.0 1.5 1
1,2-Dichloroethane ND ug/kg 03/22/16 19:51 107-06-25.0 2.2 1
1,1-Dichloroethene ND ug/kg 03/22/16 19:51 75-35-45.0 1.8 1
cis-1,2-Dichloroethene ND ug/kg 03/22/16 19:51 156-59-25.0 1.4 1
trans-1,2-Dichloroethene ND ug/kg 03/22/16 19:51 156-60-55.0 1.9 1
1,2-Dichloropropane ND ug/kg 03/22/16 19:51 78-87-55.0 1.7 1
1,3-Dichloropropane ND ug/kg 03/22/16 19:51 142-28-95.0 1.9 1
2,2-Dichloropropane ND ug/kg 03/22/16 19:51 594-20-75.0 1.7 1
1,1-Dichloropropene ND ug/kg 03/22/16 19:51 563-58-65.0 1.5 1
cis-1,3-Dichloropropene ND ug/kg 03/22/16 19:51 10061-01-55.0 1.8 1
trans-1,3-Dichloropropene ND ug/kg 03/22/16 19:51 10061-02-65.0 1.5 1
Diisopropyl ether ND ug/kg 03/22/16 19:51 108-20-35.0 1.7 1
Ethylbenzene ND ug/kg 03/22/16 19:51 100-41-45.0 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/16 19:51 87-68-35.0 2.0 1
2-Hexanone ND ug/kg 03/22/16 19:51 591-78-650.4 3.9 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/16 19:51 98-82-85.0 1.9 1
p-Isopropyltoluene ND ug/kg 03/22/16 19:51 99-87-65.0 1.7 1
Methylene Chloride ND ug/kg 03/22/16 19:51 75-09-220.2 3.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/16 19:51 108-10-150.4 3.7 1
Methyl-tert-butyl ether ND ug/kg 03/22/16 19:51 1634-04-45.0 1.5 1
Naphthalene ND ug/kg 03/22/16 19:51 91-20-35.0 1.2 1
n-Propylbenzene ND ug/kg 03/22/16 19:51 103-65-15.0 1.7 1
Styrene ND ug/kg 03/22/16 19:51 100-42-55.0 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/16 19:51 630-20-65.0 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/16 19:51 79-34-55.0 1.9 1
Tetrachloroethene ND ug/kg 03/22/16 19:51 127-18-45.0 1.7 1
Toluene ND ug/kg 03/22/16 19:51 108-88-35.0 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/16 19:51 87-61-65.0 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/16 19:51 120-82-15.0 1.6 1
1,1,1-Trichloroethane ND ug/kg 03/22/16 19:51 71-55-65.0 1.8 1
1,1,2-Trichloroethane ND ug/kg 03/22/16 19:51 79-00-55.0 2.1 1
Trichloroethene ND ug/kg 03/22/16 19:51 79-01-65.0 2.1 1
Trichlorofluoromethane ND ug/kg 03/22/16 19:51 75-69-45.0 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP3 4-5 Lab ID:92290871003 Collected:03/21/16 09:30 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,2,3-Trichloropropane ND ug/kg 03/22/16 19:51 96-18-45.0 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/16 19:51 95-63-65.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/16 19:51 108-67-85.0 1.8 1
Vinyl acetate ND ug/kg 03/22/16 19:51 108-05-450.4 8.9 1
Vinyl chloride ND ug/kg 03/22/16 19:51 75-01-410.1 1.8 1
Xylene (Total)ND ug/kg 03/22/16 19:51 1330-20-710.1 3.6 1
m&p-Xylene ND ug/kg 03/22/16 19:51 179601-23-110.1 3.6 1
o-Xylene ND ug/kg 03/22/16 19:51 95-47-65.0 1.9 1
Surrogates
Toluene-d8 (S)101 %03/22/16 19:51 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %03/22/16 19:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %03/22/16 19:51 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.3 %03/23/16 06:220.10 0.10 1
Sample:DP4 2-3 Lab ID:92290871004 Collected:03/21/16 10:30 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 609 ug/kg 03/22/16 20:10 67-64-1 E10710.7 1
Benzene ND ug/kg 03/22/16 20:10 71-43-25.3 1.7 1
Bromobenzene ND ug/kg 03/22/16 20:10 108-86-15.3 2.1 1
Bromochloromethane ND ug/kg 03/22/16 20:10 74-97-55.3 1.8 1
Bromodichloromethane ND ug/kg 03/22/16 20:10 75-27-45.3 2.0 1
Bromoform ND ug/kg 03/22/16 20:10 75-25-25.3 2.5 1
Bromomethane ND ug/kg 03/22/16 20:10 74-83-910.7 2.7 1
2-Butanone (MEK)57.7J ug/kg 03/22/16 20:10 78-93-31073.1 1
n-Butylbenzene ND ug/kg 03/22/16 20:10 104-51-85.3 1.9 1
sec-Butylbenzene ND ug/kg 03/22/16 20:10 135-98-85.3 1.7 1
tert-Butylbenzene ND ug/kg 03/22/16 20:10 98-06-65.3 2.1 1
Carbon tetrachloride ND ug/kg 03/22/16 20:10 56-23-55.3 2.8 1
Chlorobenzene ND ug/kg 03/22/16 20:10 108-90-75.3 2.0 1
Chloroethane ND ug/kg 03/22/16 20:10 75-00-310.7 2.6 1
Chloroform ND ug/kg 03/22/16 20:10 67-66-35.3 1.7 1
Chloromethane ND ug/kg 03/22/16 20:10 74-87-310.7 2.6 1
2-Chlorotoluene ND ug/kg 03/22/16 20:10 95-49-85.3 1.8 1
4-Chlorotoluene ND ug/kg 03/22/16 20:10 106-43-45.3 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/16 20:10 96-12-85.3 3.8 1
Dibromochloromethane ND ug/kg 03/22/16 20:10 124-48-15.3 1.9 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/16 20:10 106-93-45.3 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP4 2-3 Lab ID:92290871004 Collected:03/21/16 10:30 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Dibromomethane ND ug/kg 03/22/16 20:10 74-95-35.3 2.7 1
1,2-Dichlorobenzene ND ug/kg 03/22/16 20:10 95-50-15.3 2.0 1
1,3-Dichlorobenzene ND ug/kg 03/22/16 20:10 541-73-15.3 2.1 1
1,4-Dichlorobenzene ND ug/kg 03/22/16 20:10 106-46-75.3 1.8 1
Dichlorodifluoromethane ND ug/kg 03/22/16 20:10 75-71-810.7 3.8 1
1,1-Dichloroethane ND ug/kg 03/22/16 20:10 75-34-35.3 1.6 1
1,2-Dichloroethane ND ug/kg 03/22/16 20:10 107-06-25.3 2.3 1
1,1-Dichloroethene ND ug/kg 03/22/16 20:10 75-35-45.3 1.9 1
cis-1,2-Dichloroethene ND ug/kg 03/22/16 20:10 156-59-25.3 1.5 1
trans-1,2-Dichloroethene ND ug/kg 03/22/16 20:10 156-60-55.3 2.0 1
1,2-Dichloropropane ND ug/kg 03/22/16 20:10 78-87-55.3 1.8 1
1,3-Dichloropropane ND ug/kg 03/22/16 20:10 142-28-95.3 2.0 1
2,2-Dichloropropane ND ug/kg 03/22/16 20:10 594-20-75.3 1.8 1
1,1-Dichloropropene ND ug/kg 03/22/16 20:10 563-58-65.3 1.6 1
cis-1,3-Dichloropropene ND ug/kg 03/22/16 20:10 10061-01-55.3 1.9 1
trans-1,3-Dichloropropene ND ug/kg 03/22/16 20:10 10061-02-65.3 1.6 1
Diisopropyl ether ND ug/kg 03/22/16 20:10 108-20-35.3 1.8 1
Ethylbenzene ND ug/kg 03/22/16 20:10 100-41-45.3 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/16 20:10 87-68-35.3 2.1 1
2-Hexanone ND ug/kg 03/22/16 20:10 591-78-653.4 4.2 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/16 20:10 98-82-85.3 2.0 1
p-Isopropyltoluene 6.9 ug/kg 03/22/16 20:10 99-87-65.3 1.8 1
Methylene Chloride 6.7J ug/kg 03/22/16 20:10 75-09-221.4 3.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/16 20:10 108-10-153.4 4.0 1
Methyl-tert-butyl ether ND ug/kg 03/22/16 20:10 1634-04-45.3 1.6 1
Naphthalene ND ug/kg 03/22/16 20:10 91-20-35.3 1.3 1
n-Propylbenzene ND ug/kg 03/22/16 20:10 103-65-15.3 1.8 1
Styrene ND ug/kg 03/22/16 20:10 100-42-55.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/16 20:10 630-20-65.3 2.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/16 20:10 79-34-55.3 2.0 1
Tetrachloroethene ND ug/kg 03/22/16 20:10 127-18-45.3 1.8 1
Toluene ND ug/kg 03/22/16 20:10 108-88-35.3 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/16 20:10 87-61-65.3 2.3 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/16 20:10 120-82-15.3 1.7 1
1,1,1-Trichloroethane ND ug/kg 03/22/16 20:10 71-55-65.3 1.9 1
1,1,2-Trichloroethane ND ug/kg 03/22/16 20:10 79-00-55.3 2.2 1
Trichloroethene ND ug/kg 03/22/16 20:10 79-01-65.3 2.2 1
Trichlorofluoromethane ND ug/kg 03/22/16 20:10 75-69-45.3 2.3 1
1,2,3-Trichloropropane ND ug/kg 03/22/16 20:10 96-18-45.3 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/16 20:10 95-63-65.3 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/16 20:10 108-67-85.3 1.9 1
Vinyl acetate ND ug/kg 03/22/16 20:10 108-05-453.4 9.4 1
Vinyl chloride ND ug/kg 03/22/16 20:10 75-01-410.7 1.9 1
Xylene (Total)ND ug/kg 03/22/16 20:10 1330-20-710.7 3.8 1
m&p-Xylene ND ug/kg 03/22/16 20:10 179601-23-110.7 3.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP4 2-3 Lab ID:92290871004 Collected:03/21/16 10:30 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
o-Xylene ND ug/kg 03/22/16 20:10 95-47-65.3 2.0 1
Surrogates
Toluene-d8 (S)101 %03/22/16 20:10 2037-26-570-130 1
4-Bromofluorobenzene (S)90 %03/22/16 20:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %03/22/16 20:10 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.0 %03/23/16 06:230.10 0.10 1
Sample:DP5 0-0.5 Lab ID:92290871005 Collected:03/21/16 10:40 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 30.6J ug/kg 03/22/16 20:30 67-64-197.6 9.8 1
Benzene ND ug/kg 03/22/16 20:30 71-43-24.9 1.6 1
Bromobenzene ND ug/kg 03/22/16 20:30 108-86-14.9 2.0 1
Bromochloromethane ND ug/kg 03/22/16 20:30 74-97-54.9 1.7 1
Bromodichloromethane ND ug/kg 03/22/16 20:30 75-27-44.9 1.9 1
Bromoform ND ug/kg 03/22/16 20:30 75-25-24.9 2.2 1
Bromomethane ND ug/kg 03/22/16 20:30 74-83-99.8 2.4 1
2-Butanone (MEK)ND ug/kg 03/22/16 20:30 78-93-397.6 2.8 1
n-Butylbenzene ND ug/kg 03/22/16 20:30 104-51-84.9 1.8 1
sec-Butylbenzene ND ug/kg 03/22/16 20:30 135-98-84.9 1.6 1
tert-Butylbenzene ND ug/kg 03/22/16 20:30 98-06-64.9 2.0 1
Carbon tetrachloride ND ug/kg 03/22/16 20:30 56-23-54.9 2.5 1
Chlorobenzene ND ug/kg 03/22/16 20:30 108-90-74.9 1.9 1
Chloroethane ND ug/kg 03/22/16 20:30 75-00-39.8 2.3 1
Chloroform ND ug/kg 03/22/16 20:30 67-66-34.9 1.6 1
Chloromethane ND ug/kg 03/22/16 20:30 74-87-39.8 2.3 1
2-Chlorotoluene ND ug/kg 03/22/16 20:30 95-49-84.9 1.7 1
4-Chlorotoluene ND ug/kg 03/22/16 20:30 106-43-44.9 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/16 20:30 96-12-84.9 3.5 1
Dibromochloromethane ND ug/kg 03/22/16 20:30 124-48-14.9 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/16 20:30 106-93-44.9 1.8 1
Dibromomethane ND ug/kg 03/22/16 20:30 74-95-34.9 2.4 1
1,2-Dichlorobenzene ND ug/kg 03/22/16 20:30 95-50-14.9 1.9 1
1,3-Dichlorobenzene ND ug/kg 03/22/16 20:30 541-73-14.9 2.0 1
1,4-Dichlorobenzene ND ug/kg 03/22/16 20:30 106-46-74.9 1.7 1
Dichlorodifluoromethane ND ug/kg 03/22/16 20:30 75-71-89.8 3.5 1
1,1-Dichloroethane ND ug/kg 03/22/16 20:30 75-34-34.9 1.5 1
1,2-Dichloroethane ND ug/kg 03/22/16 20:30 107-06-24.9 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP5 0-0.5 Lab ID:92290871005 Collected:03/21/16 10:40 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 03/22/16 20:30 75-35-44.9 1.8 1
cis-1,2-Dichloroethene ND ug/kg 03/22/16 20:30 156-59-24.9 1.4 1
trans-1,2-Dichloroethene ND ug/kg 03/22/16 20:30 156-60-54.9 1.9 1
1,2-Dichloropropane ND ug/kg 03/22/16 20:30 78-87-54.9 1.7 1
1,3-Dichloropropane ND ug/kg 03/22/16 20:30 142-28-94.9 1.9 1
2,2-Dichloropropane ND ug/kg 03/22/16 20:30 594-20-74.9 1.7 1
1,1-Dichloropropene ND ug/kg 03/22/16 20:30 563-58-64.9 1.5 1
cis-1,3-Dichloropropene ND ug/kg 03/22/16 20:30 10061-01-54.9 1.8 1
trans-1,3-Dichloropropene ND ug/kg 03/22/16 20:30 10061-02-64.9 1.5 1
Diisopropyl ether ND ug/kg 03/22/16 20:30 108-20-34.9 1.7 1
Ethylbenzene ND ug/kg 03/22/16 20:30 100-41-44.9 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/16 20:30 87-68-34.9 2.0 1
2-Hexanone ND ug/kg 03/22/16 20:30 591-78-648.8 3.8 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/16 20:30 98-82-84.9 1.9 1
p-Isopropyltoluene ND ug/kg 03/22/16 20:30 99-87-64.9 1.7 1
Methylene Chloride 5.9J ug/kg 03/22/16 20:30 75-09-219.5 2.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/16 20:30 108-10-148.8 3.6 1
Methyl-tert-butyl ether ND ug/kg 03/22/16 20:30 1634-04-44.9 1.5 1
Naphthalene ND ug/kg 03/22/16 20:30 91-20-34.9 1.2 1
n-Propylbenzene ND ug/kg 03/22/16 20:30 103-65-14.9 1.7 1
Styrene ND ug/kg 03/22/16 20:30 100-42-54.9 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/16 20:30 630-20-64.9 2.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/16 20:30 79-34-54.9 1.9 1
Tetrachloroethene ND ug/kg 03/22/16 20:30 127-18-44.9 1.7 1
Toluene ND ug/kg 03/22/16 20:30 108-88-34.9 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/16 20:30 87-61-64.9 2.1 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/16 20:30 120-82-14.9 1.6 1
1,1,1-Trichloroethane ND ug/kg 03/22/16 20:30 71-55-64.9 1.8 1
1,1,2-Trichloroethane ND ug/kg 03/22/16 20:30 79-00-54.9 2.0 1
Trichloroethene ND ug/kg 03/22/16 20:30 79-01-64.9 2.0 1
Trichlorofluoromethane ND ug/kg 03/22/16 20:30 75-69-44.9 2.1 1
1,2,3-Trichloropropane ND ug/kg 03/22/16 20:30 96-18-44.9 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/16 20:30 95-63-64.9 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/16 20:30 108-67-84.9 1.8 1
Vinyl acetate ND ug/kg 03/22/16 20:30 108-05-448.8 8.6 1
Vinyl chloride ND ug/kg 03/22/16 20:30 75-01-49.8 1.8 1
Xylene (Total)ND ug/kg 03/22/16 20:30 1330-20-79.8 3.5 1
m&p-Xylene ND ug/kg 03/22/16 20:30 179601-23-19.8 3.5 1
o-Xylene ND ug/kg 03/22/16 20:30 95-47-64.9 1.9 1
Surrogates
Toluene-d8 (S)101 %03/22/16 20:30 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %03/22/16 20:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %03/22/16 20:30 17060-07-070-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP5 0-0.5 Lab ID:92290871005 Collected:03/21/16 10:40 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 10.8 %03/23/16 06:230.10 0.10 1
Sample:DP6 0.5-1 Lab ID:92290871006 Collected:03/21/16 11:11 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 13.0J ug/kg 03/22/16 20:50 67-64-194.1 9.4 1
Benzene ND ug/kg 03/22/16 20:50 71-43-24.7 1.5 1
Bromobenzene ND ug/kg 03/22/16 20:50 108-86-14.7 1.9 1
Bromochloromethane ND ug/kg 03/22/16 20:50 74-97-54.7 1.6 1
Bromodichloromethane ND ug/kg 03/22/16 20:50 75-27-44.7 1.8 1
Bromoform ND ug/kg 03/22/16 20:50 75-25-24.7 2.2 1
Bromomethane ND ug/kg 03/22/16 20:50 74-83-99.4 2.4 1
2-Butanone (MEK)ND ug/kg 03/22/16 20:50 78-93-394.1 2.7 1
n-Butylbenzene ND ug/kg 03/22/16 20:50 104-51-84.7 1.7 1
sec-Butylbenzene ND ug/kg 03/22/16 20:50 135-98-84.7 1.5 1
tert-Butylbenzene ND ug/kg 03/22/16 20:50 98-06-64.7 1.9 1
Carbon tetrachloride ND ug/kg 03/22/16 20:50 56-23-54.7 2.4 1
Chlorobenzene ND ug/kg 03/22/16 20:50 108-90-74.7 1.8 1
Chloroethane ND ug/kg 03/22/16 20:50 75-00-39.4 2.3 1
Chloroform ND ug/kg 03/22/16 20:50 67-66-34.7 1.5 1
Chloromethane ND ug/kg 03/22/16 20:50 74-87-39.4 2.3 1
2-Chlorotoluene ND ug/kg 03/22/16 20:50 95-49-84.7 1.6 1
4-Chlorotoluene ND ug/kg 03/22/16 20:50 106-43-44.7 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/16 20:50 96-12-84.7 3.4 1
Dibromochloromethane ND ug/kg 03/22/16 20:50 124-48-14.7 1.7 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/16 20:50 106-93-44.7 1.7 1
Dibromomethane ND ug/kg 03/22/16 20:50 74-95-34.7 2.4 1
1,2-Dichlorobenzene ND ug/kg 03/22/16 20:50 95-50-14.7 1.8 1
1,3-Dichlorobenzene ND ug/kg 03/22/16 20:50 541-73-14.7 1.9 1
1,4-Dichlorobenzene ND ug/kg 03/22/16 20:50 106-46-74.7 1.6 1
Dichlorodifluoromethane ND ug/kg 03/22/16 20:50 75-71-89.4 3.4 1
1,1-Dichloroethane ND ug/kg 03/22/16 20:50 75-34-34.7 1.4 1
1,2-Dichloroethane ND ug/kg 03/22/16 20:50 107-06-24.7 2.1 1
1,1-Dichloroethene ND ug/kg 03/22/16 20:50 75-35-44.7 1.7 1
cis-1,2-Dichloroethene ND ug/kg 03/22/16 20:50 156-59-24.7 1.3 1
trans-1,2-Dichloroethene ND ug/kg 03/22/16 20:50 156-60-54.7 1.8 1
1,2-Dichloropropane ND ug/kg 03/22/16 20:50 78-87-54.7 1.6 1
1,3-Dichloropropane ND ug/kg 03/22/16 20:50 142-28-94.7 1.8 1
2,2-Dichloropropane ND ug/kg 03/22/16 20:50 594-20-74.7 1.6 1
1,1-Dichloropropene ND ug/kg 03/22/16 20:50 563-58-64.7 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP6 0.5-1 Lab ID:92290871006 Collected:03/21/16 11:11 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
cis-1,3-Dichloropropene ND ug/kg 03/22/16 20:50 10061-01-54.7 1.7 1
trans-1,3-Dichloropropene ND ug/kg 03/22/16 20:50 10061-02-64.7 1.4 1
Diisopropyl ether ND ug/kg 03/22/16 20:50 108-20-34.7 1.6 1
Ethylbenzene ND ug/kg 03/22/16 20:50 100-41-44.7 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/16 20:50 87-68-34.7 1.9 1
2-Hexanone ND ug/kg 03/22/16 20:50 591-78-647.1 3.7 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/16 20:50 98-82-84.7 1.8 1
p-Isopropyltoluene ND ug/kg 03/22/16 20:50 99-87-64.7 1.6 1
Methylene Chloride ND ug/kg 03/22/16 20:50 75-09-218.8 2.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/16 20:50 108-10-147.1 3.5 1
Methyl-tert-butyl ether ND ug/kg 03/22/16 20:50 1634-04-44.7 1.4 1
Naphthalene ND ug/kg 03/22/16 20:50 91-20-34.7 1.1 1
n-Propylbenzene ND ug/kg 03/22/16 20:50 103-65-14.7 1.6 1
Styrene ND ug/kg 03/22/16 20:50 100-42-54.7 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/16 20:50 630-20-64.7 2.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/16 20:50 79-34-54.7 1.8 1
Tetrachloroethene ND ug/kg 03/22/16 20:50 127-18-44.7 1.6 1
Toluene ND ug/kg 03/22/16 20:50 108-88-34.7 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/16 20:50 87-61-64.7 2.1 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/16 20:50 120-82-14.7 1.5 1
1,1,1-Trichloroethane ND ug/kg 03/22/16 20:50 71-55-64.7 1.7 1
1,1,2-Trichloroethane ND ug/kg 03/22/16 20:50 79-00-54.7 2.0 1
Trichloroethene ND ug/kg 03/22/16 20:50 79-01-64.7 2.0 1
Trichlorofluoromethane ND ug/kg 03/22/16 20:50 75-69-44.7 2.1 1
1,2,3-Trichloropropane ND ug/kg 03/22/16 20:50 96-18-44.7 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/16 20:50 95-63-64.7 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/16 20:50 108-67-84.7 1.7 1
Vinyl acetate ND ug/kg 03/22/16 20:50 108-05-447.1 8.3 1
Vinyl chloride ND ug/kg 03/22/16 20:50 75-01-49.4 1.7 1
Xylene (Total)ND ug/kg 03/22/16 20:50 1330-20-79.4 3.4 1
m&p-Xylene ND ug/kg 03/22/16 20:50 179601-23-19.4 3.4 1
o-Xylene ND ug/kg 03/22/16 20:50 95-47-64.7 1.8 1
Surrogates
Toluene-d8 (S)104 %03/22/16 20:50 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %03/22/16 20:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %03/22/16 20:50 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.9 %03/23/16 06:230.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP7 0-0.5 Lab ID:92290871007 Collected:03/21/16 11:30 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/22/16 21:10 67-64-111411.4 1
Benzene ND ug/kg 03/22/16 21:10 71-43-25.7 1.8 1
Bromobenzene ND ug/kg 03/22/16 21:10 108-86-15.7 2.3 1
Bromochloromethane ND ug/kg 03/22/16 21:10 74-97-55.7 1.9 1
Bromodichloromethane ND ug/kg 03/22/16 21:10 75-27-45.7 2.2 1
Bromoform ND ug/kg 03/22/16 21:10 75-25-25.7 2.6 1
Bromomethane ND ug/kg 03/22/16 21:10 74-83-911.4 2.9 1
2-Butanone (MEK)ND ug/kg 03/22/16 21:10 78-93-31143.3 1
n-Butylbenzene ND ug/kg 03/22/16 21:10 104-51-85.7 2.1 1
sec-Butylbenzene ND ug/kg 03/22/16 21:10 135-98-85.7 1.8 1
tert-Butylbenzene ND ug/kg 03/22/16 21:10 98-06-65.7 2.3 1
Carbon tetrachloride ND ug/kg 03/22/16 21:10 56-23-55.7 3.0 1
Chlorobenzene ND ug/kg 03/22/16 21:10 108-90-75.7 2.2 1
Chloroethane ND ug/kg 03/22/16 21:10 75-00-311.4 2.7 1
Chloroform ND ug/kg 03/22/16 21:10 67-66-35.7 1.8 1
Chloromethane ND ug/kg 03/22/16 21:10 74-87-311.4 2.7 1
2-Chlorotoluene ND ug/kg 03/22/16 21:10 95-49-85.7 1.9 1
4-Chlorotoluene ND ug/kg 03/22/16 21:10 106-43-45.7 2.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/16 21:10 96-12-85.7 4.1 1
Dibromochloromethane ND ug/kg 03/22/16 21:10 124-48-15.7 2.1 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/16 21:10 106-93-45.7 2.1 1
Dibromomethane ND ug/kg 03/22/16 21:10 74-95-35.7 2.9 1
1,2-Dichlorobenzene ND ug/kg 03/22/16 21:10 95-50-15.7 2.2 1
1,3-Dichlorobenzene ND ug/kg 03/22/16 21:10 541-73-15.7 2.3 1
1,4-Dichlorobenzene ND ug/kg 03/22/16 21:10 106-46-75.7 1.9 1
Dichlorodifluoromethane ND ug/kg 03/22/16 21:10 75-71-811.4 4.1 1
1,1-Dichloroethane ND ug/kg 03/22/16 21:10 75-34-35.7 1.7 1
1,2-Dichloroethane ND ug/kg 03/22/16 21:10 107-06-25.7 2.5 1
1,1-Dichloroethene ND ug/kg 03/22/16 21:10 75-35-45.7 2.1 1
cis-1,2-Dichloroethene ND ug/kg 03/22/16 21:10 156-59-25.7 1.6 1
trans-1,2-Dichloroethene ND ug/kg 03/22/16 21:10 156-60-55.7 2.2 1
1,2-Dichloropropane ND ug/kg 03/22/16 21:10 78-87-55.7 1.9 1
1,3-Dichloropropane ND ug/kg 03/22/16 21:10 142-28-95.7 2.2 1
2,2-Dichloropropane ND ug/kg 03/22/16 21:10 594-20-75.7 1.9 1
1,1-Dichloropropene ND ug/kg 03/22/16 21:10 563-58-65.7 1.7 1
cis-1,3-Dichloropropene ND ug/kg 03/22/16 21:10 10061-01-55.7 2.1 1
trans-1,3-Dichloropropene ND ug/kg 03/22/16 21:10 10061-02-65.7 1.7 1
Diisopropyl ether ND ug/kg 03/22/16 21:10 108-20-35.7 1.9 1
Ethylbenzene ND ug/kg 03/22/16 21:10 100-41-45.7 2.1 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/16 21:10 87-68-35.7 2.3 1
2-Hexanone ND ug/kg 03/22/16 21:10 591-78-657.0 4.4 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/16 21:10 98-82-85.7 2.2 1
p-Isopropyltoluene ND ug/kg 03/22/16 21:10 99-87-65.7 1.9 1
Methylene Chloride 4.0J ug/kg 03/22/16 21:10 75-09-222.8 3.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/16 21:10 108-10-157.0 4.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP7 0-0.5 Lab ID:92290871007 Collected:03/21/16 11:30 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 03/22/16 21:10 1634-04-45.7 1.7 1
Naphthalene ND ug/kg 03/22/16 21:10 91-20-35.7 1.4 1
n-Propylbenzene ND ug/kg 03/22/16 21:10 103-65-15.7 1.9 1
Styrene ND ug/kg 03/22/16 21:10 100-42-55.7 2.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/16 21:10 630-20-65.7 2.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/16 21:10 79-34-55.7 2.2 1
Tetrachloroethene ND ug/kg 03/22/16 21:10 127-18-45.7 1.9 1
Toluene ND ug/kg 03/22/16 21:10 108-88-35.7 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/16 21:10 87-61-65.7 2.5 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/16 21:10 120-82-15.7 1.8 1
1,1,1-Trichloroethane ND ug/kg 03/22/16 21:10 71-55-65.7 2.1 1
1,1,2-Trichloroethane ND ug/kg 03/22/16 21:10 79-00-55.7 2.4 1
Trichloroethene ND ug/kg 03/22/16 21:10 79-01-65.7 2.4 1
Trichlorofluoromethane ND ug/kg 03/22/16 21:10 75-69-45.7 2.5 1
1,2,3-Trichloropropane ND ug/kg 03/22/16 21:10 96-18-45.7 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/16 21:10 95-63-65.7 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/16 21:10 108-67-85.7 2.1 1
Vinyl acetate ND ug/kg 03/22/16 21:10 108-05-457.0 10.0 1
Vinyl chloride ND ug/kg 03/22/16 21:10 75-01-411.4 2.1 1
Xylene (Total)ND ug/kg 03/22/16 21:10 1330-20-711.4 4.1 1
m&p-Xylene ND ug/kg 03/22/16 21:10 179601-23-111.4 4.1 1
o-Xylene ND ug/kg 03/22/16 21:10 95-47-65.7 2.2 1
Surrogates
Toluene-d8 (S)102 %03/22/16 21:10 2037-26-570-130 1
4-Bromofluorobenzene (S)92 %03/22/16 21:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %03/22/16 21:10 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.0 %03/23/16 06:230.10 0.10 1
Sample:DP8 0-0.5 Lab ID:92290871008 Collected:03/21/16 11:50 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/22/16 21:29 67-64-188.0 8.8 1
Benzene ND ug/kg 03/22/16 21:29 71-43-24.4 1.4 1
Bromobenzene ND ug/kg 03/22/16 21:29 108-86-14.4 1.8 1
Bromochloromethane ND ug/kg 03/22/16 21:29 74-97-54.4 1.5 1
Bromodichloromethane ND ug/kg 03/22/16 21:29 75-27-44.4 1.7 1
Bromoform ND ug/kg 03/22/16 21:29 75-25-24.4 2.0 1
Bromomethane ND ug/kg 03/22/16 21:29 74-83-98.8 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP8 0-0.5 Lab ID:92290871008 Collected:03/21/16 11:50 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
2-Butanone (MEK)ND ug/kg 03/22/16 21:29 78-93-388.0 2.6 1
n-Butylbenzene ND ug/kg 03/22/16 21:29 104-51-84.4 1.6 1
sec-Butylbenzene ND ug/kg 03/22/16 21:29 135-98-84.4 1.4 1
tert-Butylbenzene ND ug/kg 03/22/16 21:29 98-06-64.4 1.8 1
Carbon tetrachloride ND ug/kg 03/22/16 21:29 56-23-54.4 2.3 1
Chlorobenzene ND ug/kg 03/22/16 21:29 108-90-74.4 1.7 1
Chloroethane ND ug/kg 03/22/16 21:29 75-00-38.8 2.1 1
Chloroform ND ug/kg 03/22/16 21:29 67-66-34.4 1.4 1
Chloromethane ND ug/kg 03/22/16 21:29 74-87-38.8 2.1 1
2-Chlorotoluene ND ug/kg 03/22/16 21:29 95-49-84.4 1.5 1
4-Chlorotoluene ND ug/kg 03/22/16 21:29 106-43-44.4 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/16 21:29 96-12-84.4 3.2 1
Dibromochloromethane ND ug/kg 03/22/16 21:29 124-48-14.4 1.6 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/16 21:29 106-93-44.4 1.6 1
Dibromomethane ND ug/kg 03/22/16 21:29 74-95-34.4 2.2 1
1,2-Dichlorobenzene ND ug/kg 03/22/16 21:29 95-50-14.4 1.7 1
1,3-Dichlorobenzene ND ug/kg 03/22/16 21:29 541-73-14.4 1.8 1
1,4-Dichlorobenzene ND ug/kg 03/22/16 21:29 106-46-74.4 1.5 1
Dichlorodifluoromethane ND ug/kg 03/22/16 21:29 75-71-88.8 3.2 1
1,1-Dichloroethane ND ug/kg 03/22/16 21:29 75-34-34.4 1.3 1
1,2-Dichloroethane ND ug/kg 03/22/16 21:29 107-06-24.4 1.9 1
1,1-Dichloroethene ND ug/kg 03/22/16 21:29 75-35-44.4 1.6 1
cis-1,2-Dichloroethene ND ug/kg 03/22/16 21:29 156-59-24.4 1.2 1
trans-1,2-Dichloroethene ND ug/kg 03/22/16 21:29 156-60-54.4 1.7 1
1,2-Dichloropropane ND ug/kg 03/22/16 21:29 78-87-54.4 1.5 1
1,3-Dichloropropane ND ug/kg 03/22/16 21:29 142-28-94.4 1.7 1
2,2-Dichloropropane ND ug/kg 03/22/16 21:29 594-20-74.4 1.5 1
1,1-Dichloropropene ND ug/kg 03/22/16 21:29 563-58-64.4 1.3 1
cis-1,3-Dichloropropene ND ug/kg 03/22/16 21:29 10061-01-54.4 1.6 1
trans-1,3-Dichloropropene ND ug/kg 03/22/16 21:29 10061-02-64.4 1.3 1
Diisopropyl ether ND ug/kg 03/22/16 21:29 108-20-34.4 1.5 1
Ethylbenzene ND ug/kg 03/22/16 21:29 100-41-44.4 1.6 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/16 21:29 87-68-34.4 1.8 1
2-Hexanone ND ug/kg 03/22/16 21:29 591-78-644.0 3.4 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/16 21:29 98-82-84.4 1.7 1
p-Isopropyltoluene ND ug/kg 03/22/16 21:29 99-87-64.4 1.5 1
Methylene Chloride ND ug/kg 03/22/16 21:29 75-09-217.6 2.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/16 21:29 108-10-144.0 3.3 1
Methyl-tert-butyl ether ND ug/kg 03/22/16 21:29 1634-04-44.4 1.3 1
Naphthalene ND ug/kg 03/22/16 21:29 91-20-34.4 1.1 1
n-Propylbenzene ND ug/kg 03/22/16 21:29 103-65-14.4 1.5 1
Styrene ND ug/kg 03/22/16 21:29 100-42-54.4 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/16 21:29 630-20-64.4 1.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/16 21:29 79-34-54.4 1.7 1
Tetrachloroethene ND ug/kg 03/22/16 21:29 127-18-44.4 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP8 0-0.5 Lab ID:92290871008 Collected:03/21/16 11:50 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Toluene ND ug/kg 03/22/16 21:29 108-88-34.4 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/16 21:29 87-61-64.4 1.9 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/16 21:29 120-82-14.4 1.4 1
1,1,1-Trichloroethane ND ug/kg 03/22/16 21:29 71-55-64.4 1.6 1
1,1,2-Trichloroethane ND ug/kg 03/22/16 21:29 79-00-54.4 1.8 1
Trichloroethene ND ug/kg 03/22/16 21:29 79-01-64.4 1.8 1
Trichlorofluoromethane ND ug/kg 03/22/16 21:29 75-69-44.4 1.9 1
1,2,3-Trichloropropane ND ug/kg 03/22/16 21:29 96-18-44.4 1.4 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/16 21:29 95-63-64.4 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/16 21:29 108-67-84.4 1.6 1
Vinyl acetate ND ug/kg 03/22/16 21:29 108-05-444.0 7.7 1
Vinyl chloride ND ug/kg 03/22/16 21:29 75-01-48.8 1.6 1
Xylene (Total)ND ug/kg 03/22/16 21:29 1330-20-78.8 3.2 1
m&p-Xylene ND ug/kg 03/22/16 21:29 179601-23-18.8 3.2 1
o-Xylene ND ug/kg 03/22/16 21:29 95-47-64.4 1.7 1
Surrogates
Toluene-d8 (S)102 %03/22/16 21:29 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %03/22/16 21:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %03/22/16 21:29 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 9.8 %03/23/16 06:230.10 0.10 1
Sample:DP9 0.5-1 Lab ID:92290871009 Collected:03/21/16 12:20 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 23.6J ug/kg 03/22/16 21:49 67-64-110810.8 1
Benzene ND ug/kg 03/22/16 21:49 71-43-25.4 1.7 1
Bromobenzene ND ug/kg 03/22/16 21:49 108-86-15.4 2.2 1
Bromochloromethane ND ug/kg 03/22/16 21:49 74-97-55.4 1.8 1
Bromodichloromethane ND ug/kg 03/22/16 21:49 75-27-45.4 2.1 1
Bromoform ND ug/kg 03/22/16 21:49 75-25-25.4 2.5 1
Bromomethane ND ug/kg 03/22/16 21:49 74-83-910.8 2.7 1
2-Butanone (MEK)ND ug/kg 03/22/16 21:49 78-93-31083.1 1
n-Butylbenzene ND ug/kg 03/22/16 21:49 104-51-85.4 1.9 1
sec-Butylbenzene ND ug/kg 03/22/16 21:49 135-98-85.4 1.7 1
tert-Butylbenzene ND ug/kg 03/22/16 21:49 98-06-65.4 2.2 1
Carbon tetrachloride ND ug/kg 03/22/16 21:49 56-23-55.4 2.8 1
Chlorobenzene ND ug/kg 03/22/16 21:49 108-90-75.4 2.1 1
Chloroethane ND ug/kg 03/22/16 21:49 75-00-310.8 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP9 0.5-1 Lab ID:92290871009 Collected:03/21/16 12:20 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroform ND ug/kg 03/22/16 21:49 67-66-35.4 1.7 1
Chloromethane ND ug/kg 03/22/16 21:49 74-87-310.8 2.6 1
2-Chlorotoluene ND ug/kg 03/22/16 21:49 95-49-85.4 1.8 1
4-Chlorotoluene ND ug/kg 03/22/16 21:49 106-43-45.4 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/16 21:49 96-12-85.4 3.9 1
Dibromochloromethane ND ug/kg 03/22/16 21:49 124-48-15.4 1.9 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/16 21:49 106-93-45.4 1.9 1
Dibromomethane ND ug/kg 03/22/16 21:49 74-95-35.4 2.7 1
1,2-Dichlorobenzene ND ug/kg 03/22/16 21:49 95-50-15.4 2.1 1
1,3-Dichlorobenzene ND ug/kg 03/22/16 21:49 541-73-15.4 2.2 1
1,4-Dichlorobenzene ND ug/kg 03/22/16 21:49 106-46-75.4 1.8 1
Dichlorodifluoromethane ND ug/kg 03/22/16 21:49 75-71-810.8 3.9 1
1,1-Dichloroethane ND ug/kg 03/22/16 21:49 75-34-35.4 1.6 1
1,2-Dichloroethane ND ug/kg 03/22/16 21:49 107-06-25.4 2.4 1
1,1-Dichloroethene ND ug/kg 03/22/16 21:49 75-35-45.4 1.9 1
cis-1,2-Dichloroethene ND ug/kg 03/22/16 21:49 156-59-25.4 1.5 1
trans-1,2-Dichloroethene ND ug/kg 03/22/16 21:49 156-60-55.4 2.1 1
1,2-Dichloropropane ND ug/kg 03/22/16 21:49 78-87-55.4 1.8 1
1,3-Dichloropropane ND ug/kg 03/22/16 21:49 142-28-95.4 2.1 1
2,2-Dichloropropane ND ug/kg 03/22/16 21:49 594-20-75.4 1.8 1
1,1-Dichloropropene ND ug/kg 03/22/16 21:49 563-58-65.4 1.6 1
cis-1,3-Dichloropropene ND ug/kg 03/22/16 21:49 10061-01-55.4 1.9 1
trans-1,3-Dichloropropene ND ug/kg 03/22/16 21:49 10061-02-65.4 1.6 1
Diisopropyl ether ND ug/kg 03/22/16 21:49 108-20-35.4 1.8 1
Ethylbenzene ND ug/kg 03/22/16 21:49 100-41-45.4 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/16 21:49 87-68-35.4 2.2 1
2-Hexanone ND ug/kg 03/22/16 21:49 591-78-654.0 4.2 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/16 21:49 98-82-85.4 2.1 1
p-Isopropyltoluene ND ug/kg 03/22/16 21:49 99-87-65.4 1.8 1
Methylene Chloride 6.9J ug/kg 03/22/16 21:49 75-09-221.6 3.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/16 21:49 108-10-154.0 4.0 1
Methyl-tert-butyl ether ND ug/kg 03/22/16 21:49 1634-04-45.4 1.6 1
Naphthalene ND ug/kg 03/22/16 21:49 91-20-35.4 1.3 1
n-Propylbenzene ND ug/kg 03/22/16 21:49 103-65-15.4 1.8 1
Styrene ND ug/kg 03/22/16 21:49 100-42-55.4 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/16 21:49 630-20-65.4 2.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/16 21:49 79-34-55.4 2.1 1
Tetrachloroethene ND ug/kg 03/22/16 21:49 127-18-45.4 1.8 1
Toluene ND ug/kg 03/22/16 21:49 108-88-35.4 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/16 21:49 87-61-65.4 2.4 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/16 21:49 120-82-15.4 1.7 1
1,1,1-Trichloroethane ND ug/kg 03/22/16 21:49 71-55-65.4 1.9 1
1,1,2-Trichloroethane ND ug/kg 03/22/16 21:49 79-00-55.4 2.3 1
Trichloroethene ND ug/kg 03/22/16 21:49 79-01-65.4 2.3 1
Trichlorofluoromethane ND ug/kg 03/22/16 21:49 75-69-45.4 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP9 0.5-1 Lab ID:92290871009 Collected:03/21/16 12:20 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,2,3-Trichloropropane ND ug/kg 03/22/16 21:49 96-18-45.4 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/16 21:49 95-63-65.4 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/16 21:49 108-67-85.4 1.9 1
Vinyl acetate ND ug/kg 03/22/16 21:49 108-05-454.0 9.5 1
Vinyl chloride ND ug/kg 03/22/16 21:49 75-01-410.8 1.9 1
Xylene (Total)ND ug/kg 03/22/16 21:49 1330-20-710.8 3.9 1
m&p-Xylene ND ug/kg 03/22/16 21:49 179601-23-110.8 3.9 1
o-Xylene ND ug/kg 03/22/16 21:49 95-47-65.4 2.1 1
Surrogates
Toluene-d8 (S)102 %03/22/16 21:49 2037-26-570-130 1
4-Bromofluorobenzene (S)92 %03/22/16 21:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %03/22/16 21:49 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.7 %03/23/16 06:230.10 0.10 1
Sample:DP10 0-1 Lab ID:92290871010 Collected:03/21/16 12:40 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/22/16 22:09 67-64-192.5 9.2 1
Benzene ND ug/kg 03/22/16 22:09 71-43-24.6 1.5 1
Bromobenzene ND ug/kg 03/22/16 22:09 108-86-14.6 1.8 1
Bromochloromethane ND ug/kg 03/22/16 22:09 74-97-54.6 1.6 1
Bromodichloromethane ND ug/kg 03/22/16 22:09 75-27-44.6 1.8 1
Bromoform ND ug/kg 03/22/16 22:09 75-25-24.6 2.1 1
Bromomethane ND ug/kg 03/22/16 22:09 74-83-99.2 2.3 1
2-Butanone (MEK)ND ug/kg 03/22/16 22:09 78-93-392.5 2.7 1
n-Butylbenzene ND ug/kg 03/22/16 22:09 104-51-84.6 1.7 1
sec-Butylbenzene ND ug/kg 03/22/16 22:09 135-98-84.6 1.5 1
tert-Butylbenzene ND ug/kg 03/22/16 22:09 98-06-64.6 1.8 1
Carbon tetrachloride ND ug/kg 03/22/16 22:09 56-23-54.6 2.4 1
Chlorobenzene ND ug/kg 03/22/16 22:09 108-90-74.6 1.8 1
Chloroethane ND ug/kg 03/22/16 22:09 75-00-39.2 2.2 1
Chloroform ND ug/kg 03/22/16 22:09 67-66-34.6 1.5 1
Chloromethane ND ug/kg 03/22/16 22:09 74-87-39.2 2.2 1
2-Chlorotoluene ND ug/kg 03/22/16 22:09 95-49-84.6 1.6 1
4-Chlorotoluene ND ug/kg 03/22/16 22:09 106-43-44.6 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/16 22:09 96-12-84.6 3.3 1
Dibromochloromethane ND ug/kg 03/22/16 22:09 124-48-14.6 1.7 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/16 22:09 106-93-44.6 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP10 0-1 Lab ID:92290871010 Collected:03/21/16 12:40 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Dibromomethane ND ug/kg 03/22/16 22:09 74-95-34.6 2.3 1
1,2-Dichlorobenzene ND ug/kg 03/22/16 22:09 95-50-14.6 1.8 1
1,3-Dichlorobenzene ND ug/kg 03/22/16 22:09 541-73-14.6 1.8 1
1,4-Dichlorobenzene ND ug/kg 03/22/16 22:09 106-46-74.6 1.6 1
Dichlorodifluoromethane ND ug/kg 03/22/16 22:09 75-71-89.2 3.3 1
1,1-Dichloroethane ND ug/kg 03/22/16 22:09 75-34-34.6 1.4 1
1,2-Dichloroethane ND ug/kg 03/22/16 22:09 107-06-24.6 2.0 1
1,1-Dichloroethene ND ug/kg 03/22/16 22:09 75-35-44.6 1.7 1
cis-1,2-Dichloroethene ND ug/kg 03/22/16 22:09 156-59-24.6 1.3 1
trans-1,2-Dichloroethene ND ug/kg 03/22/16 22:09 156-60-54.6 1.8 1
1,2-Dichloropropane ND ug/kg 03/22/16 22:09 78-87-54.6 1.6 1
1,3-Dichloropropane ND ug/kg 03/22/16 22:09 142-28-94.6 1.8 1
2,2-Dichloropropane ND ug/kg 03/22/16 22:09 594-20-74.6 1.6 1
1,1-Dichloropropene ND ug/kg 03/22/16 22:09 563-58-64.6 1.4 1
cis-1,3-Dichloropropene ND ug/kg 03/22/16 22:09 10061-01-54.6 1.7 1
trans-1,3-Dichloropropene ND ug/kg 03/22/16 22:09 10061-02-64.6 1.4 1
Diisopropyl ether ND ug/kg 03/22/16 22:09 108-20-34.6 1.6 1
Ethylbenzene ND ug/kg 03/22/16 22:09 100-41-44.6 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/16 22:09 87-68-34.6 1.8 1
2-Hexanone ND ug/kg 03/22/16 22:09 591-78-646.2 3.6 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/16 22:09 98-82-84.6 1.8 1
p-Isopropyltoluene ND ug/kg 03/22/16 22:09 99-87-64.6 1.6 1
Methylene Chloride ND ug/kg 03/22/16 22:09 75-09-218.5 2.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/16 22:09 108-10-146.2 3.4 1
Methyl-tert-butyl ether ND ug/kg 03/22/16 22:09 1634-04-44.6 1.4 1
Naphthalene ND ug/kg 03/22/16 22:09 91-20-34.6 1.1 1
n-Propylbenzene ND ug/kg 03/22/16 22:09 103-65-14.6 1.6 1
Styrene ND ug/kg 03/22/16 22:09 100-42-54.6 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/16 22:09 630-20-64.6 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/16 22:09 79-34-54.6 1.8 1
Tetrachloroethene ND ug/kg 03/22/16 22:09 127-18-44.6 1.6 1
Toluene ND ug/kg 03/22/16 22:09 108-88-34.6 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/16 22:09 87-61-64.6 2.0 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/16 22:09 120-82-14.6 1.5 1
1,1,1-Trichloroethane ND ug/kg 03/22/16 22:09 71-55-64.6 1.7 1
1,1,2-Trichloroethane ND ug/kg 03/22/16 22:09 79-00-54.6 1.9 1
Trichloroethene ND ug/kg 03/22/16 22:09 79-01-64.6 1.9 1
Trichlorofluoromethane ND ug/kg 03/22/16 22:09 75-69-44.6 2.0 1
1,2,3-Trichloropropane ND ug/kg 03/22/16 22:09 96-18-44.6 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/16 22:09 95-63-64.6 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/16 22:09 108-67-84.6 1.7 1
Vinyl acetate ND ug/kg 03/22/16 22:09 108-05-446.2 8.1 1
Vinyl chloride ND ug/kg 03/22/16 22:09 75-01-49.2 1.7 1
Xylene (Total)ND ug/kg 03/22/16 22:09 1330-20-79.2 3.3 1
m&p-Xylene ND ug/kg 03/22/16 22:09 179601-23-19.2 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:DP10 0-1 Lab ID:92290871010 Collected:03/21/16 12:40 Received:03/22/16 08:46 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
o-Xylene ND ug/kg 03/22/16 22:09 95-47-64.6 1.8 1
Surrogates
Toluene-d8 (S)101 %03/22/16 22:09 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %03/22/16 22:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %03/22/16 22:09 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.8 %03/23/16 06:230.10 0.10 1
Sample:TMW-1 Lab ID:92290871011 Collected:03/21/16 14:20 Received:03/22/16 08:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/24/16 05:03 67-64-125.0 10.0 1
Benzene ND ug/L 03/24/16 05:03 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/24/16 05:03 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/24/16 05:03 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/24/16 05:03 75-27-41.0 0.18 1
Bromoform ND ug/L 03/24/16 05:03 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/24/16 05:03 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/24/16 05:03 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/24/16 05:03 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/24/16 05:03 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/24/16 05:03 75-00-31.0 0.54 1
Chloroform 0.30J ug/L 03/24/16 05:03 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/24/16 05:03 74-87-3 L31.0 0.11 1
2-Chlorotoluene ND ug/L 03/24/16 05:03 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/24/16 05:03 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/24/16 05:03 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/24/16 05:03 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/24/16 05:03 106-93-4 L31.0 0.27 1
Dibromomethane ND ug/L 03/24/16 05:03 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/24/16 05:03 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/24/16 05:03 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/24/16 05:03 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/24/16 05:03 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/24/16 05:03 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/24/16 05:03 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/24/16 05:03 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/24/16 05:03 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/24/16 05:03 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/24/16 05:03 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:TMW-1 Lab ID:92290871011 Collected:03/21/16 14:20 Received:03/22/16 08:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,3-Dichloropropane ND ug/L 03/24/16 05:03 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/24/16 05:03 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/24/16 05:03 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/24/16 05:03 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/24/16 05:03 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/24/16 05:03 108-20-3 L31.0 0.12 1
Ethylbenzene ND ug/L 03/24/16 05:03 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/24/16 05:03 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/24/16 05:03 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/24/16 05:03 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/24/16 05:03 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/24/16 05:03 108-10-1 M15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/24/16 05:03 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/24/16 05:03 91-20-31.0 0.24 1
Styrene ND ug/L 03/24/16 05:03 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/24/16 05:03 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/24/16 05:03 79-34-51.0 0.40 1
Tetrachloroethene 0.58J ug/L 03/24/16 05:03 127-18-4 B,C81.0 0.46 1
Toluene 0.26J ug/L 03/24/16 05:03 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/24/16 05:03 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/24/16 05:03 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/24/16 05:03 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/24/16 05:03 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/24/16 05:03 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/24/16 05:03 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/24/16 05:03 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/24/16 05:03 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/24/16 05:03 75-01-4 M11.0 0.62 1
Xylene (Total)ND ug/L 03/24/16 05:03 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/24/16 05:03 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/24/16 05:03 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)92 %03/24/16 05:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %03/24/16 05:03 17060-07-070-130 1
Toluene-d8 (S)122 %03/24/16 05:03 2037-26-570-130 1
Sample:TMW-2 Lab ID:92290871012 Collected:03/21/16 14:40 Received:03/22/16 08:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/24/16 05:20 67-64-125.0 10.0 1
Benzene ND ug/L 03/24/16 05:20 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/24/16 05:20 108-86-11.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:TMW-2 Lab ID:92290871012 Collected:03/21/16 14:40 Received:03/22/16 08:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Bromochloromethane ND ug/L 03/24/16 05:20 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/24/16 05:20 75-27-41.0 0.18 1
Bromoform ND ug/L 03/24/16 05:20 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/24/16 05:20 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/24/16 05:20 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/24/16 05:20 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/24/16 05:20 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/24/16 05:20 75-00-31.0 0.54 1
Chloroform ND ug/L 03/24/16 05:20 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/24/16 05:20 74-87-3 L31.0 0.11 1
2-Chlorotoluene ND ug/L 03/24/16 05:20 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/24/16 05:20 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/24/16 05:20 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/24/16 05:20 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/24/16 05:20 106-93-4 L31.0 0.27 1
Dibromomethane ND ug/L 03/24/16 05:20 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/24/16 05:20 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/24/16 05:20 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/24/16 05:20 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/24/16 05:20 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/24/16 05:20 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/24/16 05:20 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/24/16 05:20 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/24/16 05:20 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/24/16 05:20 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/24/16 05:20 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/24/16 05:20 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/24/16 05:20 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/24/16 05:20 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/24/16 05:20 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/24/16 05:20 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/24/16 05:20 108-20-3 L31.0 0.12 1
Ethylbenzene ND ug/L 03/24/16 05:20 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/24/16 05:20 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/24/16 05:20 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/24/16 05:20 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/24/16 05:20 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/24/16 05:20 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/24/16 05:20 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/24/16 05:20 91-20-31.0 0.24 1
Styrene ND ug/L 03/24/16 05:20 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/24/16 05:20 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/24/16 05:20 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/24/16 05:20 127-18-41.0 0.46 1
Toluene 0.42J ug/L 03/24/16 05:20 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/24/16 05:20 87-61-61.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92290871
E43
Sample:TMW-2 Lab ID:92290871012 Collected:03/21/16 14:40 Received:03/22/16 08:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 03/24/16 05:20 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/24/16 05:20 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/24/16 05:20 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/24/16 05:20 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/24/16 05:20 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/24/16 05:20 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/24/16 05:20 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/24/16 05:20 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/24/16 05:20 1330-20-72.0 0.66 1
m&p-Xylene 0.71J ug/L 03/24/16 05:20 179601-23-12.0 0.66 1
o-Xylene 0.25J ug/L 03/24/16 05:20 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %03/24/16 05:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %03/24/16 05:20 17060-07-070-130 1
Toluene-d8 (S)109 %03/24/16 05:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36103
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92290871011, 92290871012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1693608
Associated Lab Samples:92290871011, 92290871012
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/24/16 01:110.33
1,1,1-Trichloroethane ug/L ND 1.0 03/24/16 01:110.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/24/16 01:110.40
1,1,2-Trichloroethane ug/L ND 1.0 03/24/16 01:110.29
1,1-Dichloroethane ug/L ND 1.0 03/24/16 01:110.32
1,1-Dichloroethene ug/L ND 1.0 03/24/16 01:110.56
1,1-Dichloropropene ug/L ND 1.0 03/24/16 01:110.49
1,2,3-Trichlorobenzene ug/L ND 1.0 03/24/16 01:110.33
1,2,3-Trichloropropane ug/L ND 1.0 03/24/16 01:110.41
1,2,4-Trichlorobenzene ug/L ND 1.0 03/24/16 01:110.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/24/16 01:112.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/24/16 01:110.27
1,2-Dichlorobenzene ug/L ND 1.0 03/24/16 01:110.30
1,2-Dichloroethane ug/L ND 1.0 03/24/16 01:110.24
1,2-Dichloropropane ug/L ND 1.0 03/24/16 01:110.27
1,3-Dichlorobenzene ug/L ND 1.0 03/24/16 01:110.24
1,3-Dichloropropane ug/L ND 1.0 03/24/16 01:110.28
1,4-Dichlorobenzene ug/L ND 1.0 03/24/16 01:110.33
2,2-Dichloropropane ug/L ND 1.0 03/24/16 01:110.13
2-Butanone (MEK)ug/L ND 5.0 03/24/16 01:110.96
2-Chlorotoluene ug/L ND 1.0 03/24/16 01:110.35
2-Hexanone ug/L ND 5.0 03/24/16 01:110.46
4-Chlorotoluene ug/L ND 1.0 03/24/16 01:110.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/24/16 01:110.33
Acetone ug/L ND 25.0 03/24/16 01:1110.0
Benzene ug/L ND 1.0 03/24/16 01:110.25
Bromobenzene ug/L ND 1.0 03/24/16 01:110.30
Bromochloromethane ug/L ND 1.0 03/24/16 01:110.17
Bromodichloromethane ug/L ND 1.0 03/24/16 01:110.18
Bromoform ug/L ND 1.0 03/24/16 01:110.26
Bromomethane ug/L ND 2.0 03/24/16 01:110.29
Carbon tetrachloride ug/L ND 1.0 03/24/16 01:110.25
Chlorobenzene ug/L ND 1.0 03/24/16 01:110.23
Chloroethane ug/L ND 1.0 03/24/16 01:110.54
Chloroform ug/L ND 1.0 03/24/16 01:110.14
Chloromethane ug/L ND 1.0 03/24/16 01:110.11
cis-1,2-Dichloroethene ug/L ND 1.0 03/24/16 01:110.19
cis-1,3-Dichloropropene ug/L ND 1.0 03/24/16 01:110.13
Dibromochloromethane ug/L ND 1.0 03/24/16 01:110.21
Dibromomethane ug/L ND 1.0 03/24/16 01:110.21
Dichlorodifluoromethane ug/L ND 1.0 03/24/16 01:110.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1693608
Associated Lab Samples:92290871011, 92290871012
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 03/24/16 01:110.12
Ethylbenzene ug/L ND 1.0 03/24/16 01:110.30
Hexachloro-1,3-butadiene ug/L ND 1.0 03/24/16 01:110.71
m&p-Xylene ug/L ND 2.0 03/24/16 01:110.66
Methyl-tert-butyl ether ug/L ND 1.0 03/24/16 01:110.21
Methylene Chloride ug/L ND 2.0 03/24/16 01:110.97
Naphthalene ug/L ND 1.0 03/24/16 01:110.24
o-Xylene ug/L ND 1.0 03/24/16 01:110.23
p-Isopropyltoluene ug/L ND 1.0 03/24/16 01:110.31
Styrene ug/L ND 1.0 03/24/16 01:110.26
Tetrachloroethene ug/L 1.3 1.0 C803/24/16 01:110.46
Toluene ug/L ND 1.0 03/24/16 01:110.26
trans-1,2-Dichloroethene ug/L ND 1.0 03/24/16 01:110.49
trans-1,3-Dichloropropene ug/L ND 1.0 03/24/16 01:110.26
Trichloroethene ug/L ND 1.0 03/24/16 01:110.47
Trichlorofluoromethane ug/L ND 1.0 03/24/16 01:110.20
Vinyl acetate ug/L ND 2.0 03/24/16 01:110.35
Vinyl chloride ug/L ND 1.0 03/24/16 01:110.62
Xylene (Total)ug/L ND 2.0 03/24/16 01:110.66
1,2-Dichloroethane-d4 (S)%99 70-130 03/24/16 01:11
4-Bromofluorobenzene (S)%94 70-130 03/24/16 01:11
Toluene-d8 (S)%99 70-130 03/24/16 01:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1693609LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 59.350 119 70-130
1,1,1-Trichloroethane ug/L 59.150 118 70-130
1,1,2,2-Tetrachloroethane ug/L 58.350 117 70-130
1,1,2-Trichloroethane ug/L 54.150 108 70-130
1,1-Dichloroethane ug/L 62.750 125 70-130
1,1-Dichloroethene ug/L 59.550 119 70-132
1,1-Dichloropropene ug/L 60.750 121 70-130
1,2,3-Trichlorobenzene ug/L 59.050 118 70-135
1,2,3-Trichloropropane ug/L 56.950 114 70-130
1,2,4-Trichlorobenzene ug/L 59.550 119 70-134
1,2-Dibromo-3-chloropropane ug/L 59.950 120 70-130
1,2-Dibromoethane (EDB)ug/L 65.4 L05013170-130
1,2-Dichlorobenzene ug/L 59.450 119 70-130
1,2-Dichloroethane ug/L 58.350 117 70-130
1,2-Dichloropropane ug/L 61.550 123 70-130
1,3-Dichlorobenzene ug/L 59.950 120 70-130
1,3-Dichloropropane ug/L 61.550 123 70-130
1,4-Dichlorobenzene ug/L 60.650 121 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
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Huntersville, NC 28078
[phone]
Page 28 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1693609LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 59.250 118 58-145
2-Butanone (MEK)ug/L 130100 130 70-145
2-Chlorotoluene ug/L 53.350 107 70-130
2-Hexanone ug/L 138100 138 70-144
4-Chlorotoluene ug/L 57.650 115 70-130
4-Methyl-2-pentanone (MIBK)ug/L 117100 117 70-140
Acetone ug/L 125100 125 50-175
Benzene ug/L 60.450 121 70-130
Bromobenzene ug/L 58.750 117 70-130
Bromochloromethane ug/L 62.150 124 70-130
Bromodichloromethane ug/L 60.450 121 70-130
Bromoform ug/L 56.150 112 70-130
Bromomethane ug/L 54.350 109 54-130
Carbon tetrachloride ug/L 57.450 115 70-132
Chlorobenzene ug/L 58.850 118 70-130
Chloroethane ug/L 59.350 119 64-134
Chloroform ug/L 60.650 121 70-130
Chloromethane ug/L 71.4 L05014364-130
cis-1,2-Dichloroethene ug/L 62.150 124 70-131
cis-1,3-Dichloropropene ug/L 61.550 123 70-130
Dibromochloromethane ug/L 64.550 129 70-130
Dibromomethane ug/L 59.850 120 70-131
Dichlorodifluoromethane ug/L 64.250 128 56-130
Diisopropyl ether ug/L 67.8 L05013670-130
Ethylbenzene ug/L 61.350 123 70-130
Hexachloro-1,3-butadiene ug/L 59.350 119 70-130
m&p-Xylene ug/L 123100 123 70-130
Methyl-tert-butyl ether ug/L 60.950 122 70-130
Methylene Chloride ug/L 54.150 108 63-130
Naphthalene ug/L 65.250 130 70-138
o-Xylene ug/L 59.150 118 70-130
p-Isopropyltoluene ug/L 60.150 120 70-130
Styrene ug/L 60.050 120 70-130
Tetrachloroethene ug/L 64.450 129 70-130
Toluene ug/L 56.150 112 70-130
trans-1,2-Dichloroethene ug/L 60.150 120 70-130
trans-1,3-Dichloropropene ug/L 48.350 97 70-132
Trichloroethene ug/L 60.750 121 70-130
Trichlorofluoromethane ug/L 63.450 127 62-133
Vinyl acetate ug/L 122100 122 66-157
Vinyl chloride ug/L 73.950 148 50-150
Xylene (Total)ug/L 182150 121 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%93 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1693610MATRIX SPIKE SAMPLE:
MSSpike
Result
92290871011
1,1,1,2-Tetrachloroethane ug/L 21.820 109 70-130ND
1,1,1-Trichloroethane ug/L 22.320 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.520 112 70-130ND
1,1,2-Trichloroethane ug/L 23.920 119 70-130ND
1,1-Dichloroethane ug/L 22.220 111 70-130ND
1,1-Dichloroethene ug/L 25.420 127 70-166ND
1,1-Dichloropropene ug/L 25.120 125 70-130ND
1,2,3-Trichlorobenzene ug/L 21.320 106 70-130ND
1,2,3-Trichloropropane ug/L 20.820 104 70-130ND
1,2,4-Trichlorobenzene ug/L 21.620 108 70-130ND
1,2-Dibromo-3-chloropropane ug/L 22.620 113 70-130ND
1,2-Dibromoethane (EDB)ug/L 23.920 119 70-130ND
1,2-Dichlorobenzene ug/L 22.120 111 70-130ND
1,2-Dichloroethane ug/L 22.320 112 70-130ND
1,2-Dichloropropane ug/L 24.520 123 70-130ND
1,3-Dichlorobenzene ug/L 22.320 112 70-130ND
1,3-Dichloropropane ug/L 24.220 121 70-130ND
1,4-Dichlorobenzene ug/L 22.820 114 70-130ND
2,2-Dichloropropane ug/L 22.120 110 70-130ND
2-Butanone (MEK)ug/L 50.140 125 70-130ND
2-Chlorotoluene ug/L 23.820 119 70-130ND
2-Hexanone ug/L 50.240 126 70-130ND
4-Chlorotoluene ug/L 22.920 114 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 55.4 M14013870-130ND
Acetone ug/L 42.440 99 70-130ND
Benzene ug/L 25.920 130 70-148ND
Bromobenzene ug/L 24.220 121 70-130ND
Bromochloromethane ug/L 22.620 113 70-130ND
Bromodichloromethane ug/L 23.920 120 70-130ND
Bromoform ug/L 18.520 93 70-130ND
Bromomethane ug/L 19.120 96 70-130ND
Carbon tetrachloride ug/L 23.220 116 70-130ND
Chlorobenzene ug/L 22.620 113 70-146ND
Chloroethane ug/L 23.120 115 70-130ND
Chloroform ug/L 24.220 119 70-1300.30J
Chloromethane ug/L 25.720 129 70-130ND
cis-1,2-Dichloroethene ug/L 24.120 120 70-130ND
cis-1,3-Dichloropropene ug/L 25.420 127 70-130ND
Dibromochloromethane ug/L 22.220 111 70-130ND
Dibromomethane ug/L 20.820 104 70-130ND
Dichlorodifluoromethane ug/L 24.920 125 70-130ND
Diisopropyl ether ug/L 21.720 108 70-130ND
Ethylbenzene ug/L 24.320 122 70-130ND
Hexachloro-1,3-butadiene ug/L 20.820 104 70-130ND
m&p-Xylene ug/L 46.540 115 70-130ND
Methyl-tert-butyl ether ug/L 19.820 99 70-130ND
Methylene Chloride ug/L 18.820 94 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1693610MATRIX SPIKE SAMPLE:
MSSpike
Result
92290871011
Naphthalene ug/L 21.920 110 70-130ND
o-Xylene ug/L 22.420 111 70-130ND
p-Isopropyltoluene ug/L 24.220 121 70-130ND
Styrene ug/L 22.520 112 70-130ND
Tetrachloroethene ug/L 23.820 116 70-1300.58J
Toluene ug/L 26.020 129 70-1550.26J
trans-1,2-Dichloroethene ug/L 21.920 110 70-130ND
trans-1,3-Dichloropropene ug/L 22.320 112 70-130ND
Trichloroethene ug/L 23.520 118 69-151ND
Trichlorofluoromethane ug/L 24.220 121 70-130ND
Vinyl acetate ug/L 31.440 79 70-130ND
Vinyl chloride ug/L 27.5 M12013770-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%93 70-130
Toluene-d8 (S)%108 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92290871012
1693611SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92290871012
1693611SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 300.71J
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 300.25J
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 0.35J 300.42J
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%103 1102
4-Bromofluorobenzene (S)%77 27100
Toluene-d8 (S)%103 6109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36088
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92290871001, 92290871002, 92290871003, 92290871004, 92290871005, 92290871006, 92290871007,
92290871008, 92290871009, 92290871010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1692330
Associated Lab Samples:92290871001, 92290871002, 92290871003, 92290871004, 92290871005, 92290871006, 92290871007,
92290871008, 92290871009, 92290871010
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 6.1 03/22/16 17:132.6
1,1,1-Trichloroethane ug/kg ND 6.1 03/22/16 17:132.2
1,1,2,2-Tetrachloroethane ug/kg ND 6.1 03/22/16 17:132.3
1,1,2-Trichloroethane ug/kg ND 6.1 03/22/16 17:132.6
1,1-Dichloroethane ug/kg ND 6.1 03/22/16 17:131.8
1,1-Dichloroethene ug/kg ND 6.1 03/22/16 17:132.2
1,1-Dichloropropene ug/kg ND 6.1 03/22/16 17:131.8
1,2,3-Trichlorobenzene ug/kg ND 6.1 03/22/16 17:132.7
1,2,3-Trichloropropane ug/kg ND 6.1 03/22/16 17:132.0
1,2,4-Trichlorobenzene ug/kg ND 6.1 03/22/16 17:132.0
1,2,4-Trimethylbenzene ug/kg ND 6.1 03/22/16 17:132.4
1,2-Dibromo-3-chloropropane ug/kg ND 6.1 03/22/16 17:134.4
1,2-Dibromoethane (EDB)ug/kg ND 6.1 03/22/16 17:132.2
1,2-Dichlorobenzene ug/kg ND 6.1 03/22/16 17:132.3
1,2-Dichloroethane ug/kg ND 6.1 03/22/16 17:132.7
1,2-Dichloropropane ug/kg ND 6.1 03/22/16 17:132.1
1,3,5-Trimethylbenzene ug/kg ND 6.1 03/22/16 17:132.2
1,3-Dichlorobenzene ug/kg ND 6.1 03/22/16 17:132.4
1,3-Dichloropropane ug/kg ND 6.1 03/22/16 17:132.3
1,4-Dichlorobenzene ug/kg ND 6.1 03/22/16 17:132.1
2,2-Dichloropropane ug/kg ND 6.1 03/22/16 17:132.1
2-Butanone (MEK)ug/kg ND 122 03/22/16 17:133.5
2-Chlorotoluene ug/kg ND 6.1 03/22/16 17:132.1
2-Hexanone ug/kg ND 61.0 03/22/16 17:134.8
4-Chlorotoluene ug/kg ND 6.1 03/22/16 17:132.2
4-Methyl-2-pentanone (MIBK)ug/kg ND 61.0 03/22/16 17:134.5
Acetone ug/kg ND 122 03/22/16 17:1312.2
Benzene ug/kg ND 6.1 03/22/16 17:132.0
Bromobenzene ug/kg ND 6.1 03/22/16 17:132.4
Bromochloromethane ug/kg ND 6.1 03/22/16 17:132.1
Bromodichloromethane ug/kg ND 6.1 03/22/16 17:132.3
Bromoform ug/kg ND 6.1 03/22/16 17:132.8
Bromomethane ug/kg ND 12.2 03/22/16 17:133.0
Carbon tetrachloride ug/kg ND 6.1 03/22/16 17:133.2
Chlorobenzene ug/kg ND 6.1 03/22/16 17:132.3
Chloroethane ug/kg ND 12.2 03/22/16 17:132.9
Chloroform ug/kg ND 6.1 03/22/16 17:132.0
Chloromethane ug/kg ND 12.2 03/22/16 17:132.9
cis-1,2-Dichloroethene ug/kg ND 6.1 03/22/16 17:131.7
cis-1,3-Dichloropropene ug/kg ND 6.1 03/22/16 17:132.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1692330
Associated Lab Samples:92290871001, 92290871002, 92290871003, 92290871004, 92290871005, 92290871006, 92290871007,
92290871008, 92290871009, 92290871010
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 6.1 03/22/16 17:132.2
Dibromomethane ug/kg ND 6.1 03/22/16 17:133.0
Dichlorodifluoromethane ug/kg ND 12.2 03/22/16 17:134.4
Diisopropyl ether ug/kg ND 6.1 03/22/16 17:132.1
Ethylbenzene ug/kg ND 6.1 03/22/16 17:132.2
Hexachloro-1,3-butadiene ug/kg ND 6.1 03/22/16 17:132.4
Isopropylbenzene (Cumene)ug/kg ND 6.1 03/22/16 17:132.3
m&p-Xylene ug/kg ND 12.2 03/22/16 17:134.4
Methyl-tert-butyl ether ug/kg ND 6.1 03/22/16 17:131.8
Methylene Chloride ug/kg ND 24.4 03/22/16 17:133.7
n-Butylbenzene ug/kg ND 6.1 03/22/16 17:132.2
n-Propylbenzene ug/kg ND 6.1 03/22/16 17:132.1
Naphthalene ug/kg ND 6.1 03/22/16 17:131.5
o-Xylene ug/kg ND 6.1 03/22/16 17:132.3
p-Isopropyltoluene ug/kg ND 6.1 03/22/16 17:132.1
sec-Butylbenzene ug/kg ND 6.1 03/22/16 17:132.0
Styrene ug/kg ND 6.1 03/22/16 17:132.2
tert-Butylbenzene ug/kg ND 6.1 03/22/16 17:132.4
Tetrachloroethene ug/kg ND 6.1 03/22/16 17:132.1
Toluene ug/kg ND 6.1 03/22/16 17:132.2
trans-1,2-Dichloroethene ug/kg ND 6.1 03/22/16 17:132.3
trans-1,3-Dichloropropene ug/kg ND 6.1 03/22/16 17:131.8
Trichloroethene ug/kg ND 6.1 03/22/16 17:132.6
Trichlorofluoromethane ug/kg ND 6.1 03/22/16 17:132.7
Vinyl acetate ug/kg ND 61.0 03/22/16 17:1310.7
Vinyl chloride ug/kg ND 12.2 03/22/16 17:132.2
Xylene (Total)ug/kg ND 12.2 03/22/16 17:134.4
1,2-Dichloroethane-d4 (S)%133 70-132 S303/22/16 17:13
4-Bromofluorobenzene (S)%93 70-130 03/22/16 17:13
Toluene-d8 (S)%102 70-130 03/22/16 17:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1692331LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 53.255.6 96 74-137
1,1,1-Trichloroethane ug/kg 57.755.6 104 67-140
1,1,2,2-Tetrachloroethane ug/kg 51.855.6 93 72-141
1,1,2-Trichloroethane ug/kg 55.155.6 99 78-138
1,1-Dichloroethane ug/kg 56.255.6 101 69-134
1,1-Dichloroethene ug/kg 57.755.6 104 67-138
1,1-Dichloropropene ug/kg 58.855.6 106 69-139
1,2,3-Trichlorobenzene ug/kg 54.555.6 98 70-146
1,2,3-Trichloropropane ug/kg 51.455.6 92 69-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1692331LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 54.755.6 98 68-148
1,2,4-Trimethylbenzene ug/kg 58.055.6 104 74-137
1,2-Dibromo-3-chloropropane ug/kg 55.755.6 100 65-140
1,2-Dibromoethane (EDB)ug/kg 55.655.6 100 77-135
1,2-Dichlorobenzene ug/kg 54.955.6 99 77-141
1,2-Dichloroethane ug/kg 55.055.6 99 65-137
1,2-Dichloropropane ug/kg 57.055.6 103 72-136
1,3,5-Trimethylbenzene ug/kg 56.555.6 102 76-133
1,3-Dichlorobenzene ug/kg 56.255.6 101 74-138
1,3-Dichloropropane ug/kg 54.855.6 99 71-139
1,4-Dichlorobenzene ug/kg 55.755.6 100 76-138
2,2-Dichloropropane ug/kg 56.555.6 102 68-137
2-Butanone (MEK)ug/kg 117111 106 58-147
2-Chlorotoluene ug/kg 56.555.6 102 73-139
2-Hexanone ug/kg 120111 108 62-145
4-Chlorotoluene ug/kg 56.455.6 102 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 120111 108 64-149
Acetone ug/kg 125111 112 53-153
Benzene ug/kg 57.355.6 103 73-135
Bromobenzene ug/kg 57.555.6 103 75-133
Bromochloromethane ug/kg 58.055.6 104 73-134
Bromodichloromethane ug/kg 55.955.6 101 71-135
Bromoform ug/kg 52.055.6 94 66-141
Bromomethane ug/kg 60.455.6 109 53-160
Carbon tetrachloride ug/kg 55.255.6 99 60-145
Chlorobenzene ug/kg 54.455.6 98 78-130
Chloroethane ug/kg 64.455.6 116 64-149
Chloroform ug/kg 57.755.6 104 70-134
Chloromethane ug/kg 63.655.6 114 52-150
cis-1,2-Dichloroethene ug/kg 57.155.6 103 70-133
cis-1,3-Dichloropropene ug/kg 56.955.6 102 68-134
Dibromochloromethane ug/kg 53.655.6 96 71-138
Dibromomethane ug/kg 54.755.6 98 74-130
Dichlorodifluoromethane ug/kg 57.755.6 104 40-160
Diisopropyl ether ug/kg 60.555.6 109 69-141
Ethylbenzene ug/kg 55.355.6 100 75-133
Hexachloro-1,3-butadiene ug/kg 52.555.6 94 68-143
Isopropylbenzene (Cumene)ug/kg 54.655.6 98 76-143
m&p-Xylene ug/kg 109111 99 75-136
Methyl-tert-butyl ether ug/kg 57.855.6 104 68-144
Methylene Chloride ug/kg 60.455.6 109 45-154
n-Butylbenzene ug/kg 58.755.6 106 72-137
n-Propylbenzene ug/kg 56.655.6 102 76-136
Naphthalene ug/kg 57.455.6 103 68-151
o-Xylene ug/kg 53.655.6 97 76-141
p-Isopropyltoluene ug/kg 56.855.6 102 76-140
sec-Butylbenzene ug/kg 56.755.6 102 79-139
REPORT OF LABORATORY ANALYSIS
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Page 35 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1692331LABORATORY CONTROL SAMPLE:
LCSSpike
Styrene ug/kg 54.755.6 99 79-137
tert-Butylbenzene ug/kg 51.455.6 93 74-143
Tetrachloroethene ug/kg 43.355.6 78 71-138
Toluene ug/kg 57.155.6 103 74-131
trans-1,2-Dichloroethene ug/kg 58.455.6 105 67-135
trans-1,3-Dichloropropene ug/kg 55.855.6 101 65-146
Trichloroethene ug/kg 55.455.6 100 67-135
Trichlorofluoromethane ug/kg 61.055.6 110 59-144
Vinyl acetate ug/kg 107 F31119640-160
Vinyl chloride ug/kg 63.155.6 114 56-141
Xylene (Total)ug/kg 163167 98 76-137
1,2-Dichloroethane-d4 (S)%100 70-132
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1692772MATRIX SPIKE SAMPLE:
MSSpike
Result
92290932001
1,1,1,2-Tetrachloroethane ug/kg 22.827.4 84 70-130ND
1,1,1-Trichloroethane ug/kg 26.827.4 98 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 24.927.4 91 70-130ND
1,1,2-Trichloroethane ug/kg 25.127.4 92 70-130ND
1,1-Dichloroethane ug/kg 27.227.4 99 70-130ND
1,1-Dichloroethene ug/kg 28.027.4 102 49-180ND
1,1-Dichloropropene ug/kg 27.227.4 99 70-130ND
1,2,3-Trichlorobenzene ug/kg 24.227.4 88 70-130ND
1,2,3-Trichloropropane ug/kg 22.027.4 80 70-130ND
1,2,4-Trichlorobenzene ug/kg 24.027.4 88 70-130ND
1,2,4-Trimethylbenzene ug/kg 25.927.4 95 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 21.827.4 80 70-130ND
1,2-Dibromoethane (EDB)ug/kg 24.627.4 90 70-130ND
1,2-Dichlorobenzene ug/kg 24.527.4 90 70-130ND
1,2-Dichloroethane ug/kg 25.027.4 92 70-130ND
1,2-Dichloropropane ug/kg 24.627.4 90 70-130ND
1,3,5-Trimethylbenzene ug/kg 25.927.4 95 70-130ND
1,3-Dichlorobenzene ug/kg 25.227.4 92 70-130ND
1,3-Dichloropropane ug/kg 24.527.4 90 70-130ND
1,4-Dichlorobenzene ug/kg 25.627.4 94 70-130ND
2,2-Dichloropropane ug/kg 24.527.4 89 70-130ND
2-Butanone (MEK)ug/kg 58.0J54.7 106 70-130ND
2-Chlorotoluene ug/kg 25.427.4 93 70-130ND
2-Hexanone ug/kg 50.5J54.7 92 70-130ND
4-Chlorotoluene ug/kg 25.627.4 93 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 52.3J54.7 96 70-130ND
Acetone ug/kg 80.3J M154.7 141 70-130ND
REPORT OF LABORATORY ANALYSIS
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Page 36 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1692772MATRIX SPIKE SAMPLE:
MSSpike
Result
92290932001
Benzene ug/kg 26.127.4 96 50-166ND
Bromobenzene ug/kg 25.127.4 92 70-130ND
Bromochloromethane ug/kg 26.027.4 95 70-130ND
Bromodichloromethane ug/kg 23.827.4 87 70-130ND
Bromoform ug/kg 22.127.4 81 70-130ND
Bromomethane ug/kg 33.227.4 121 70-130ND
Carbon tetrachloride ug/kg 23.827.4 87 70-130ND
Chlorobenzene ug/kg 25.327.4 93 43-169ND
Chloroethane ug/kg 31.127.4 114 70-130ND
Chloroform ug/kg 26.727.4 98 70-130ND
Chloromethane ug/kg 29.427.4 108 70-130ND
cis-1,2-Dichloroethene ug/kg 27.327.4 100 70-130ND
cis-1,3-Dichloropropene ug/kg 24.327.4 89 70-130ND
Dibromochloromethane ug/kg 22.627.4 83 70-130ND
Dibromomethane ug/kg 24.627.4 90 70-130ND
Dichlorodifluoromethane ug/kg 26.427.4 96 70-130ND
Diisopropyl ether ug/kg 28.627.4 105 70-130ND
Ethylbenzene ug/kg 26.227.4 96 70-130ND
Hexachloro-1,3-butadiene ug/kg 24.627.4 90 70-130ND
Isopropylbenzene (Cumene)ug/kg 25.727.4 94 70-130ND
m&p-Xylene ug/kg 52.054.7 95 70-130ND
Methyl-tert-butyl ether ug/kg 26.427.4 96 70-130ND
Methylene Chloride ug/kg 30.927.4 94 70-130ND
n-Butylbenzene ug/kg 27.127.4 99 70-130ND
n-Propylbenzene ug/kg 25.927.4 95 70-130ND
Naphthalene ug/kg 24.327.4 89 70-130ND
o-Xylene ug/kg 24.427.4 89 70-130ND
p-Isopropyltoluene ug/kg 26.027.4 95 70-130ND
sec-Butylbenzene ug/kg 26.327.4 96 70-130ND
Styrene ug/kg 24.327.4 89 70-130ND
tert-Butylbenzene ug/kg 23.527.4 86 70-130ND
Tetrachloroethene ug/kg 19.927.4 73 70-130ND
Toluene ug/kg 26.527.4 96 52-163ND
trans-1,2-Dichloroethene ug/kg 27.827.4 101 70-130ND
trans-1,3-Dichloropropene ug/kg 23.127.4 84 70-130ND
Trichloroethene ug/kg 24.427.4 89 49-167ND
Trichlorofluoromethane ug/kg 29.127.4 106 70-130ND
Vinyl acetate ug/kg 66.5J54.7 122 70-130ND
Vinyl chloride ug/kg 29.827.4 109 70-130ND
1,2-Dichloroethane-d4 (S)%108 70-132
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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Page 37 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92290871001
1692771SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 33.7J 3056.3J
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 38 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92290871001
1692771SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%104 3108
4-Bromofluorobenzene (S)%94 196
Toluene-d8 (S)%103 1103
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 39 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92290871
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/8906
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92290871001, 92290871002, 92290871003, 92290871004, 92290871005, 92290871006, 92290871007,
92290871008, 92290871009, 92290871010
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92290808001
1692110SAMPLE DUPLICATE:
Percent Moisture %13.7 1 2513.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92290812001
1692111SAMPLE DUPLICATE:
Percent Moisture %59.2 1 2559.8
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 40 of 44
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92290871
E43
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Result may be biased high due to carryover from previously analyzed sample.C8
Analyte concentration exceeded the calibration range. The reported result is estimated.E
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside thelaboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples.
Results unaffected by high bias.S3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/25/2016 06:21 PM
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[phone]
Page 41 of 44
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92290871
E43
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92290871011 MSV/36103TMW-1 EPA 8260
92290871012 MSV/36103TMW-2 EPA 8260
92290871001 MSV/36088DF1 2-3 EPA 8260
92290871002 MSV/36088DP2 2-3 EPA 8260
92290871003 MSV/36088DP3 4-5 EPA 8260
92290871004 MSV/36088DP4 2-3 EPA 8260
92290871005 MSV/36088DP5 0-0.5 EPA 8260
92290871006 MSV/36088DP6 0.5-1 EPA 8260
92290871007 MSV/36088DP7 0-0.5 EPA 8260
92290871008 MSV/36088DP8 0-0.5 EPA 8260
92290871009 MSV/36088DP9 0.5-1 EPA 8260
92290871010 MSV/36088DP10 0-1 EPA 8260
92290871001 PMST/8906DF1 2-3 ASTM D2974-87
92290871002 PMST/8906DP2 2-3 ASTM D2974-87
92290871003 PMST/8906DP3 4-5 ASTM D2974-87
92290871004 PMST/8906DP4 2-3 ASTM D2974-87
92290871005 PMST/8906DP5 0-0.5 ASTM D2974-87
92290871006 PMST/8906DP6 0.5-1 ASTM D2974-87
92290871007 PMST/8906DP7 0-0.5 ASTM D2974-87
92290871008 PMST/8906DP8 0-0.5 ASTM D2974-87
92290871009 PMST/8906DP9 0.5-1 ASTM D2974-87
92290871010 PMST/8906DP10 0-1 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 42 of 44
Page 43 of 44
Page 44 of 44
#=CL#
March 28, 2016
LIMS USE: FR - MICHAEL BURNS
LIMS OBJECT ID: 92291164
92291164
Project:
Pace Project No.:
RE:
Michael J. Burns
Kleinfelder
3500 Gatway Center Blvd.
Suite 200
Morrisville, NC 27560
E43
Dear Michael Burns:
Enclosed are the analytical results for sample(s) received by the laboratory on March 23, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
cc:Chris Hollinger, Kleinfelder
, Trigon
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Page 1 of 27
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92291164
E43
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 2 of 27
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92291164
E43
Lab ID Sample ID Matrix Date Collected Date Received
92291164001 CS-1 Solid 03/22/16 10:20 03/23/16 09:40
92291164002 CS-2 Solid 03/22/16 10:26 03/23/16 09:40
92291164003 CS-3 Solid 03/22/16 10:35 03/23/16 09:40
92291164004 CS-4 Solid 03/22/16 10:42 03/23/16 09:40
92291164005 CS-5 Solid 03/22/16 10:55 03/23/16 09:40
92291164006 TMW-3 Water 03/22/16 07:44 03/23/16 09:40
REPORT OF LABORATORY ANALYSIS
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Page 3 of 27
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92291164
E43
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92291164001 CS-1 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92291164002 CS-2 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92291164003 CS-3 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92291164004 CS-4 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92291164005 CS-5 EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92291164006 TMW-3 EPA 8260 63 PASI-CNB
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:CS-1 Lab ID:92291164001 Collected:03/22/16 10:20 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 12.5J ug/kg 03/24/16 12:37 67-64-189.3 8.9 1
Benzene ND ug/kg 03/24/16 12:37 71-43-24.5 1.4 1
Bromobenzene ND ug/kg 03/24/16 12:37 108-86-14.5 1.8 1
Bromochloromethane ND ug/kg 03/24/16 12:37 74-97-54.5 1.5 1
Bromodichloromethane ND ug/kg 03/24/16 12:37 75-27-44.5 1.7 1
Bromoform ND ug/kg 03/24/16 12:37 75-25-24.5 2.1 1
Bromomethane ND ug/kg 03/24/16 12:37 74-83-98.9 2.2 1
2-Butanone (MEK)ND ug/kg 03/24/16 12:37 78-93-389.3 2.6 1
n-Butylbenzene ND ug/kg 03/24/16 12:37 104-51-84.5 1.6 1
sec-Butylbenzene ND ug/kg 03/24/16 12:37 135-98-84.5 1.4 1
tert-Butylbenzene ND ug/kg 03/24/16 12:37 98-06-64.5 1.8 1
Carbon tetrachloride ND ug/kg 03/24/16 12:37 56-23-54.5 2.3 1
Chlorobenzene ND ug/kg 03/24/16 12:37 108-90-74.5 1.7 1
Chloroethane ND ug/kg 03/24/16 12:37 75-00-38.9 2.1 1
Chloroform ND ug/kg 03/24/16 12:37 67-66-34.5 1.4 1
Chloromethane ND ug/kg 03/24/16 12:37 74-87-38.9 2.1 1
2-Chlorotoluene ND ug/kg 03/24/16 12:37 95-49-84.5 1.5 1
4-Chlorotoluene ND ug/kg 03/24/16 12:37 106-43-44.5 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/24/16 12:37 96-12-84.5 3.2 1
Dibromochloromethane ND ug/kg 03/24/16 12:37 124-48-14.5 1.6 1
1,2-Dibromoethane (EDB)ND ug/kg 03/24/16 12:37 106-93-44.5 1.6 1
Dibromomethane ND ug/kg 03/24/16 12:37 74-95-34.5 2.2 1
1,2-Dichlorobenzene ND ug/kg 03/24/16 12:37 95-50-14.5 1.7 1
1,3-Dichlorobenzene ND ug/kg 03/24/16 12:37 541-73-14.5 1.8 1
1,4-Dichlorobenzene ND ug/kg 03/24/16 12:37 106-46-74.5 1.5 1
Dichlorodifluoromethane ND ug/kg 03/24/16 12:37 75-71-88.9 3.2 1
1,1-Dichloroethane ND ug/kg 03/24/16 12:37 75-34-34.5 1.3 1
1,2-Dichloroethane ND ug/kg 03/24/16 12:37 107-06-24.5 2.0 1
1,1-Dichloroethene ND ug/kg 03/24/16 12:37 75-35-44.5 1.6 1
cis-1,2-Dichloroethene ND ug/kg 03/24/16 12:37 156-59-24.5 1.2 1
trans-1,2-Dichloroethene ND ug/kg 03/24/16 12:37 156-60-54.5 1.7 1
1,2-Dichloropropane ND ug/kg 03/24/16 12:37 78-87-54.5 1.5 1
1,3-Dichloropropane ND ug/kg 03/24/16 12:37 142-28-94.5 1.7 1
2,2-Dichloropropane ND ug/kg 03/24/16 12:37 594-20-74.5 1.5 1
1,1-Dichloropropene ND ug/kg 03/24/16 12:37 563-58-64.5 1.3 1
cis-1,3-Dichloropropene ND ug/kg 03/24/16 12:37 10061-01-54.5 1.6 1
trans-1,3-Dichloropropene ND ug/kg 03/24/16 12:37 10061-02-64.5 1.3 1
Diisopropyl ether ND ug/kg 03/24/16 12:37 108-20-34.5 1.5 1
Ethylbenzene ND ug/kg 03/24/16 12:37 100-41-44.5 1.6 1
Hexachloro-1,3-butadiene ND ug/kg 03/24/16 12:37 87-68-34.5 1.8 1
2-Hexanone ND ug/kg 03/24/16 12:37 591-78-644.6 3.5 1
Isopropylbenzene (Cumene)ND ug/kg 03/24/16 12:37 98-82-84.5 1.7 1
p-Isopropyltoluene ND ug/kg 03/24/16 12:37 99-87-64.5 1.5 1
Methylene Chloride 6.5J ug/kg 03/24/16 12:37 75-09-217.9 2.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/24/16 12:37 108-10-144.6 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:CS-1 Lab ID:92291164001 Collected:03/22/16 10:20 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 03/24/16 12:37 1634-04-44.5 1.3 1
Naphthalene ND ug/kg 03/24/16 12:37 91-20-34.5 1.1 1
n-Propylbenzene ND ug/kg 03/24/16 12:37 103-65-14.5 1.5 1
Styrene ND ug/kg 03/24/16 12:37 100-42-54.5 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/24/16 12:37 630-20-64.5 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/24/16 12:37 79-34-54.5 1.7 1
Tetrachloroethene ND ug/kg 03/24/16 12:37 127-18-44.5 1.5 1
Toluene ND ug/kg 03/24/16 12:37 108-88-34.5 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 03/24/16 12:37 87-61-64.5 2.0 1
1,2,4-Trichlorobenzene ND ug/kg 03/24/16 12:37 120-82-14.5 1.4 1
1,1,1-Trichloroethane ND ug/kg 03/24/16 12:37 71-55-64.5 1.6 1
1,1,2-Trichloroethane ND ug/kg 03/24/16 12:37 79-00-54.5 1.9 1
Trichloroethene ND ug/kg 03/24/16 12:37 79-01-64.5 1.9 1
Trichlorofluoromethane ND ug/kg 03/24/16 12:37 75-69-44.5 2.0 1
1,2,3-Trichloropropane ND ug/kg 03/24/16 12:37 96-18-44.5 1.4 1
1,2,4-Trimethylbenzene ND ug/kg 03/24/16 12:37 95-63-64.5 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 03/24/16 12:37 108-67-84.5 1.6 1
Vinyl acetate ND ug/kg 03/24/16 12:37 108-05-444.6 7.9 1
Vinyl chloride ND ug/kg 03/24/16 12:37 75-01-48.9 1.6 1
Xylene (Total)ND ug/kg 03/24/16 12:37 1330-20-78.9 3.2 1
m&p-Xylene ND ug/kg 03/24/16 12:37 179601-23-18.9 3.2 1
o-Xylene ND ug/kg 03/24/16 12:37 95-47-64.5 1.7 1
Surrogates
Toluene-d8 (S)98 %03/24/16 12:37 2037-26-5 1g70-130 1
4-Bromofluorobenzene (S)80 %03/24/16 12:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %03/24/16 12:37 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.3 %03/24/16 11:580.10 0.10 1
Sample:CS-2 Lab ID:92291164002 Collected:03/22/16 10:26 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 376 ug/kg 03/24/16 14:55 67-64-111511.5 1
Benzene ND ug/kg 03/24/16 14:55 71-43-25.7 1.8 1
Bromobenzene ND ug/kg 03/24/16 14:55 108-86-15.7 2.3 1
Bromochloromethane ND ug/kg 03/24/16 14:55 74-97-55.7 2.0 1
Bromodichloromethane ND ug/kg 03/24/16 14:55 75-27-45.7 2.2 1
Bromoform ND ug/kg 03/24/16 14:55 75-25-25.7 2.6 1
Bromomethane ND ug/kg 03/24/16 14:55 74-83-911.5 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:CS-2 Lab ID:92291164002 Collected:03/22/16 10:26 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
2-Butanone (MEK)51.3J ug/kg 03/24/16 14:55 78-93-31153.3 1
n-Butylbenzene ND ug/kg 03/24/16 14:55 104-51-85.7 2.1 1
sec-Butylbenzene ND ug/kg 03/24/16 14:55 135-98-85.7 1.8 1
tert-Butylbenzene ND ug/kg 03/24/16 14:55 98-06-65.7 2.3 1
Carbon tetrachloride ND ug/kg 03/24/16 14:55 56-23-55.7 3.0 1
Chlorobenzene ND ug/kg 03/24/16 14:55 108-90-75.7 2.2 1
Chloroethane ND ug/kg 03/24/16 14:55 75-00-311.5 2.8 1
Chloroform ND ug/kg 03/24/16 14:55 67-66-35.7 1.8 1
Chloromethane ND ug/kg 03/24/16 14:55 74-87-311.5 2.8 1
2-Chlorotoluene ND ug/kg 03/24/16 14:55 95-49-85.7 2.0 1
4-Chlorotoluene ND ug/kg 03/24/16 14:55 106-43-45.7 2.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/24/16 14:55 96-12-85.7 4.1 1
Dibromochloromethane ND ug/kg 03/24/16 14:55 124-48-15.7 2.1 1
1,2-Dibromoethane (EDB)ND ug/kg 03/24/16 14:55 106-93-45.7 2.1 1
Dibromomethane ND ug/kg 03/24/16 14:55 74-95-35.7 2.9 1
1,2-Dichlorobenzene ND ug/kg 03/24/16 14:55 95-50-15.7 2.2 1
1,3-Dichlorobenzene ND ug/kg 03/24/16 14:55 541-73-15.7 2.3 1
1,4-Dichlorobenzene ND ug/kg 03/24/16 14:55 106-46-75.7 2.0 1
Dichlorodifluoromethane ND ug/kg 03/24/16 14:55 75-71-811.5 4.1 1
1,1-Dichloroethane ND ug/kg 03/24/16 14:55 75-34-35.7 1.7 1
1,2-Dichloroethane ND ug/kg 03/24/16 14:55 107-06-25.7 2.5 1
1,1-Dichloroethene ND ug/kg 03/24/16 14:55 75-35-45.7 2.1 1
cis-1,2-Dichloroethene ND ug/kg 03/24/16 14:55 156-59-25.7 1.6 1
trans-1,2-Dichloroethene ND ug/kg 03/24/16 14:55 156-60-55.7 2.2 1
1,2-Dichloropropane ND ug/kg 03/24/16 14:55 78-87-55.7 2.0 1
1,3-Dichloropropane ND ug/kg 03/24/16 14:55 142-28-95.7 2.2 1
2,2-Dichloropropane ND ug/kg 03/24/16 14:55 594-20-75.7 2.0 1
1,1-Dichloropropene ND ug/kg 03/24/16 14:55 563-58-65.7 1.7 1
cis-1,3-Dichloropropene ND ug/kg 03/24/16 14:55 10061-01-55.7 2.1 1
trans-1,3-Dichloropropene ND ug/kg 03/24/16 14:55 10061-02-65.7 1.7 1
Diisopropyl ether ND ug/kg 03/24/16 14:55 108-20-35.7 2.0 1
Ethylbenzene 23.6 ug/kg 03/24/16 14:55 100-41-45.7 2.1 1
Hexachloro-1,3-butadiene ND ug/kg 03/24/16 14:55 87-68-35.7 2.3 1
2-Hexanone ND ug/kg 03/24/16 14:55 591-78-657.4 4.5 1
Isopropylbenzene (Cumene)ND ug/kg 03/24/16 14:55 98-82-85.7 2.2 1
p-Isopropyltoluene 23.3 ug/kg 03/24/16 14:55 99-87-65.7 2.0 1
Methylene Chloride 80.0 ug/kg 03/24/16 14:55 75-09-223.0 3.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/24/16 14:55 108-10-157.4 4.3 1
Methyl-tert-butyl ether ND ug/kg 03/24/16 14:55 1634-04-45.7 1.7 1
Naphthalene ND ug/kg 03/24/16 14:55 91-20-35.7 1.4 1
n-Propylbenzene ND ug/kg 03/24/16 14:55 103-65-15.7 2.0 1
Styrene ND ug/kg 03/24/16 14:55 100-42-55.7 2.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/24/16 14:55 630-20-65.7 2.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/24/16 14:55 79-34-55.7 2.2 1
Tetrachloroethene ND ug/kg 03/24/16 14:55 127-18-45.7 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:CS-2 Lab ID:92291164002 Collected:03/22/16 10:26 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Toluene 23.7 ug/kg 03/24/16 14:55 108-88-35.7 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 03/24/16 14:55 87-61-65.7 2.5 1
1,2,4-Trichlorobenzene ND ug/kg 03/24/16 14:55 120-82-15.7 1.8 1
1,1,1-Trichloroethane ND ug/kg 03/24/16 14:55 71-55-65.7 2.1 1
1,1,2-Trichloroethane ND ug/kg 03/24/16 14:55 79-00-55.7 2.4 1
Trichloroethene ND ug/kg 03/24/16 14:55 79-01-65.7 2.4 1
Trichlorofluoromethane ND ug/kg 03/24/16 14:55 75-69-45.7 2.5 1
1,2,3-Trichloropropane ND ug/kg 03/24/16 14:55 96-18-45.7 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 03/24/16 14:55 95-63-65.7 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 03/24/16 14:55 108-67-85.7 2.1 1
Vinyl acetate ND ug/kg 03/24/16 14:55 108-05-457.4 10.1 1
Vinyl chloride ND ug/kg 03/24/16 14:55 75-01-411.5 2.1 1
Xylene (Total)ND ug/kg 03/24/16 14:55 1330-20-711.5 4.1 1
m&p-Xylene ND ug/kg 03/24/16 14:55 179601-23-111.5 4.1 1
o-Xylene ND ug/kg 03/24/16 14:55 95-47-65.7 2.2 1
Surrogates
Toluene-d8 (S)98 %03/24/16 14:55 2037-26-570-130 1
4-Bromofluorobenzene (S)85 %03/24/16 14:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %03/24/16 14:55 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.8 %03/24/16 11:590.10 0.10 1
Sample:CS-3 Lab ID:92291164003 Collected:03/22/16 10:35 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 108 ug/kg 03/24/16 15:15 67-64-196.3 9.6 1
Benzene ND ug/kg 03/24/16 15:15 71-43-24.8 1.5 1
Bromobenzene ND ug/kg 03/24/16 15:15 108-86-14.8 1.9 1
Bromochloromethane ND ug/kg 03/24/16 15:15 74-97-54.8 1.6 1
Bromodichloromethane ND ug/kg 03/24/16 15:15 75-27-44.8 1.8 1
Bromoform ND ug/kg 03/24/16 15:15 75-25-24.8 2.2 1
Bromomethane ND ug/kg 03/24/16 15:15 74-83-99.6 2.4 1
2-Butanone (MEK)18.2J ug/kg 03/24/16 15:15 78-93-396.3 2.8 1
n-Butylbenzene ND ug/kg 03/24/16 15:15 104-51-84.8 1.7 1
sec-Butylbenzene ND ug/kg 03/24/16 15:15 135-98-84.8 1.5 1
tert-Butylbenzene ND ug/kg 03/24/16 15:15 98-06-64.8 1.9 1
Carbon tetrachloride ND ug/kg 03/24/16 15:15 56-23-54.8 2.5 1
Chlorobenzene ND ug/kg 03/24/16 15:15 108-90-74.8 1.8 1
Chloroethane ND ug/kg 03/24/16 15:15 75-00-39.6 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:CS-3 Lab ID:92291164003 Collected:03/22/16 10:35 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroform ND ug/kg 03/24/16 15:15 67-66-34.8 1.5 1
Chloromethane ND ug/kg 03/24/16 15:15 74-87-39.6 2.3 1
2-Chlorotoluene ND ug/kg 03/24/16 15:15 95-49-84.8 1.6 1
4-Chlorotoluene ND ug/kg 03/24/16 15:15 106-43-44.8 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/24/16 15:15 96-12-84.8 3.5 1
Dibromochloromethane ND ug/kg 03/24/16 15:15 124-48-14.8 1.7 1
1,2-Dibromoethane (EDB)ND ug/kg 03/24/16 15:15 106-93-44.8 1.7 1
Dibromomethane ND ug/kg 03/24/16 15:15 74-95-34.8 2.4 1
1,2-Dichlorobenzene ND ug/kg 03/24/16 15:15 95-50-14.8 1.8 1
1,3-Dichlorobenzene ND ug/kg 03/24/16 15:15 541-73-14.8 1.9 1
1,4-Dichlorobenzene ND ug/kg 03/24/16 15:15 106-46-74.8 1.6 1
Dichlorodifluoromethane ND ug/kg 03/24/16 15:15 75-71-89.6 3.5 1
1,1-Dichloroethane ND ug/kg 03/24/16 15:15 75-34-34.8 1.4 1
1,2-Dichloroethane ND ug/kg 03/24/16 15:15 107-06-24.8 2.1 1
1,1-Dichloroethene ND ug/kg 03/24/16 15:15 75-35-44.8 1.7 1
cis-1,2-Dichloroethene ND ug/kg 03/24/16 15:15 156-59-24.8 1.3 1
trans-1,2-Dichloroethene ND ug/kg 03/24/16 15:15 156-60-54.8 1.8 1
1,2-Dichloropropane ND ug/kg 03/24/16 15:15 78-87-54.8 1.6 1
1,3-Dichloropropane ND ug/kg 03/24/16 15:15 142-28-94.8 1.8 1
2,2-Dichloropropane ND ug/kg 03/24/16 15:15 594-20-74.8 1.6 1
1,1-Dichloropropene ND ug/kg 03/24/16 15:15 563-58-64.8 1.4 1
cis-1,3-Dichloropropene ND ug/kg 03/24/16 15:15 10061-01-54.8 1.7 1
trans-1,3-Dichloropropene ND ug/kg 03/24/16 15:15 10061-02-64.8 1.4 1
Diisopropyl ether ND ug/kg 03/24/16 15:15 108-20-34.8 1.6 1
Ethylbenzene 77.6 ug/kg 03/24/16 15:15 100-41-44.8 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 03/24/16 15:15 87-68-34.8 1.9 1
2-Hexanone ND ug/kg 03/24/16 15:15 591-78-648.2 3.8 1
Isopropylbenzene (Cumene)ND ug/kg 03/24/16 15:15 98-82-84.8 1.8 1
p-Isopropyltoluene 41.2 ug/kg 03/24/16 15:15 99-87-64.8 1.6 1
Methylene Chloride 25.7 ug/kg 03/24/16 15:15 75-09-2 C919.3 2.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/24/16 15:15 108-10-148.2 3.6 1
Methyl-tert-butyl ether ND ug/kg 03/24/16 15:15 1634-04-44.8 1.4 1
Naphthalene ND ug/kg 03/24/16 15:15 91-20-34.8 1.2 1
n-Propylbenzene 3.7J ug/kg 03/24/16 15:15 103-65-14.8 1.6 1
Styrene ND ug/kg 03/24/16 15:15 100-42-54.8 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/24/16 15:15 630-20-64.8 2.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/24/16 15:15 79-34-54.8 1.8 1
Tetrachloroethene ND ug/kg 03/24/16 15:15 127-18-44.8 1.6 1
Toluene 143 ug/kg 03/24/16 15:15 108-88-34.8 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/24/16 15:15 87-61-64.8 2.1 1
1,2,4-Trichlorobenzene ND ug/kg 03/24/16 15:15 120-82-14.8 1.5 1
1,1,1-Trichloroethane ND ug/kg 03/24/16 15:15 71-55-64.8 1.7 1
1,1,2-Trichloroethane ND ug/kg 03/24/16 15:15 79-00-54.8 2.0 1
Trichloroethene ND ug/kg 03/24/16 15:15 79-01-64.8 2.0 1
Trichlorofluoromethane ND ug/kg 03/24/16 15:15 75-69-44.8 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:CS-3 Lab ID:92291164003 Collected:03/22/16 10:35 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,2,3-Trichloropropane ND ug/kg 03/24/16 15:15 96-18-44.8 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 03/24/16 15:15 95-63-64.8 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 03/24/16 15:15 108-67-84.8 1.7 1
Vinyl acetate ND ug/kg 03/24/16 15:15 108-05-448.2 8.5 1
Vinyl chloride ND ug/kg 03/24/16 15:15 75-01-49.6 1.7 1
Xylene (Total)ND ug/kg 03/24/16 15:15 1330-20-79.6 3.5 1
m&p-Xylene ND ug/kg 03/24/16 15:15 179601-23-19.6 3.5 1
o-Xylene ND ug/kg 03/24/16 15:15 95-47-64.8 1.8 1
Surrogates
Toluene-d8 (S)98 %03/24/16 15:15 2037-26-570-130 1
4-Bromofluorobenzene (S)83 %03/24/16 15:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %03/24/16 15:15 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.6 %03/24/16 11:590.10 0.10 1
Sample:CS-4 Lab ID:92291164004 Collected:03/22/16 10:42 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 52.3J ug/kg 03/24/16 13:36 67-64-111111.1 1
Benzene ND ug/kg 03/24/16 13:36 71-43-25.5 1.8 1
Bromobenzene ND ug/kg 03/24/16 13:36 108-86-15.5 2.2 1
Bromochloromethane ND ug/kg 03/24/16 13:36 74-97-55.5 1.9 1
Bromodichloromethane ND ug/kg 03/24/16 13:36 75-27-45.5 2.1 1
Bromoform ND ug/kg 03/24/16 13:36 75-25-25.5 2.5 1
Bromomethane ND ug/kg 03/24/16 13:36 74-83-911.1 2.8 1
2-Butanone (MEK)ND ug/kg 03/24/16 13:36 78-93-31113.2 1
n-Butylbenzene ND ug/kg 03/24/16 13:36 104-51-85.5 2.0 1
sec-Butylbenzene ND ug/kg 03/24/16 13:36 135-98-85.5 1.8 1
tert-Butylbenzene ND ug/kg 03/24/16 13:36 98-06-65.5 2.2 1
Carbon tetrachloride ND ug/kg 03/24/16 13:36 56-23-55.5 2.9 1
Chlorobenzene ND ug/kg 03/24/16 13:36 108-90-75.5 2.1 1
Chloroethane ND ug/kg 03/24/16 13:36 75-00-311.1 2.7 1
Chloroform ND ug/kg 03/24/16 13:36 67-66-35.5 1.8 1
Chloromethane ND ug/kg 03/24/16 13:36 74-87-311.1 2.7 1
2-Chlorotoluene ND ug/kg 03/24/16 13:36 95-49-85.5 1.9 1
4-Chlorotoluene ND ug/kg 03/24/16 13:36 106-43-45.5 2.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/24/16 13:36 96-12-85.5 4.0 1
Dibromochloromethane ND ug/kg 03/24/16 13:36 124-48-15.5 2.0 1
1,2-Dibromoethane (EDB)ND ug/kg 03/24/16 13:36 106-93-45.5 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:CS-4 Lab ID:92291164004 Collected:03/22/16 10:42 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Dibromomethane ND ug/kg 03/24/16 13:36 74-95-35.5 2.8 1
1,2-Dichlorobenzene ND ug/kg 03/24/16 13:36 95-50-15.5 2.1 1
1,3-Dichlorobenzene ND ug/kg 03/24/16 13:36 541-73-15.5 2.2 1
1,4-Dichlorobenzene ND ug/kg 03/24/16 13:36 106-46-75.5 1.9 1
Dichlorodifluoromethane ND ug/kg 03/24/16 13:36 75-71-811.1 4.0 1
1,1-Dichloroethane ND ug/kg 03/24/16 13:36 75-34-35.5 1.7 1
1,2-Dichloroethane ND ug/kg 03/24/16 13:36 107-06-25.5 2.4 1
1,1-Dichloroethene ND ug/kg 03/24/16 13:36 75-35-45.5 2.0 1
cis-1,2-Dichloroethene ND ug/kg 03/24/16 13:36 156-59-25.5 1.6 1
trans-1,2-Dichloroethene ND ug/kg 03/24/16 13:36 156-60-55.5 2.1 1
1,2-Dichloropropane ND ug/kg 03/24/16 13:36 78-87-55.5 1.9 1
1,3-Dichloropropane ND ug/kg 03/24/16 13:36 142-28-95.5 2.1 1
2,2-Dichloropropane ND ug/kg 03/24/16 13:36 594-20-75.5 1.9 1
1,1-Dichloropropene ND ug/kg 03/24/16 13:36 563-58-65.5 1.7 1
cis-1,3-Dichloropropene ND ug/kg 03/24/16 13:36 10061-01-55.5 2.0 1
trans-1,3-Dichloropropene ND ug/kg 03/24/16 13:36 10061-02-65.5 1.7 1
Diisopropyl ether ND ug/kg 03/24/16 13:36 108-20-35.5 1.9 1
Ethylbenzene ND ug/kg 03/24/16 13:36 100-41-45.5 2.0 1
Hexachloro-1,3-butadiene ND ug/kg 03/24/16 13:36 87-68-35.5 2.2 1
2-Hexanone ND ug/kg 03/24/16 13:36 591-78-655.4 4.3 1
Isopropylbenzene (Cumene)ND ug/kg 03/24/16 13:36 98-82-85.5 2.1 1
p-Isopropyltoluene 3.9J ug/kg 03/24/16 13:36 99-87-65.5 1.9 1
Methylene Chloride 12.2J ug/kg 03/24/16 13:36 75-09-222.2 3.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/24/16 13:36 108-10-155.4 4.1 1
Methyl-tert-butyl ether ND ug/kg 03/24/16 13:36 1634-04-45.5 1.7 1
Naphthalene ND ug/kg 03/24/16 13:36 91-20-35.5 1.3 1
n-Propylbenzene ND ug/kg 03/24/16 13:36 103-65-15.5 1.9 1
Styrene ND ug/kg 03/24/16 13:36 100-42-55.5 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/24/16 13:36 630-20-65.5 2.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/24/16 13:36 79-34-55.5 2.1 1
Tetrachloroethene ND ug/kg 03/24/16 13:36 127-18-45.5 1.9 1
Toluene 4.8J ug/kg 03/24/16 13:36 108-88-35.5 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 03/24/16 13:36 87-61-65.5 2.4 1
1,2,4-Trichlorobenzene ND ug/kg 03/24/16 13:36 120-82-15.5 1.8 1
1,1,1-Trichloroethane ND ug/kg 03/24/16 13:36 71-55-65.5 2.0 1
1,1,2-Trichloroethane ND ug/kg 03/24/16 13:36 79-00-55.5 2.3 1
Trichloroethene ND ug/kg 03/24/16 13:36 79-01-65.5 2.3 1
Trichlorofluoromethane ND ug/kg 03/24/16 13:36 75-69-45.5 2.4 1
1,2,3-Trichloropropane ND ug/kg 03/24/16 13:36 96-18-45.5 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 03/24/16 13:36 95-63-65.5 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 03/24/16 13:36 108-67-85.5 2.0 1
Vinyl acetate ND ug/kg 03/24/16 13:36 108-05-455.4 9.8 1
Vinyl chloride ND ug/kg 03/24/16 13:36 75-01-411.1 2.0 1
Xylene (Total)ND ug/kg 03/24/16 13:36 1330-20-711.1 4.0 1
m&p-Xylene ND ug/kg 03/24/16 13:36 179601-23-111.1 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:CS-4 Lab ID:92291164004 Collected:03/22/16 10:42 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
o-Xylene ND ug/kg 03/24/16 13:36 95-47-65.5 2.1 1
Surrogates
Toluene-d8 (S)97 %03/24/16 13:36 2037-26-570-130 1
4-Bromofluorobenzene (S)82 %03/24/16 13:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %03/24/16 13:36 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 10.9 %03/24/16 11:590.10 0.10 1
Sample:CS-5 Lab ID:92291164005 Collected:03/22/16 10:55 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/24/16 13:56 67-64-111711.7 1
Benzene ND ug/kg 03/24/16 13:56 71-43-25.9 1.9 1
Bromobenzene ND ug/kg 03/24/16 13:56 108-86-15.9 2.3 1
Bromochloromethane ND ug/kg 03/24/16 13:56 74-97-55.9 2.0 1
Bromodichloromethane ND ug/kg 03/24/16 13:56 75-27-45.9 2.2 1
Bromoform ND ug/kg 03/24/16 13:56 75-25-25.9 2.7 1
Bromomethane ND ug/kg 03/24/16 13:56 74-83-911.7 2.9 1
2-Butanone (MEK)ND ug/kg 03/24/16 13:56 78-93-31173.4 1
n-Butylbenzene ND ug/kg 03/24/16 13:56 104-51-85.9 2.1 1
sec-Butylbenzene ND ug/kg 03/24/16 13:56 135-98-85.9 1.9 1
tert-Butylbenzene ND ug/kg 03/24/16 13:56 98-06-65.9 2.3 1
Carbon tetrachloride ND ug/kg 03/24/16 13:56 56-23-55.9 3.1 1
Chlorobenzene ND ug/kg 03/24/16 13:56 108-90-75.9 2.2 1
Chloroethane ND ug/kg 03/24/16 13:56 75-00-311.7 2.8 1
Chloroform ND ug/kg 03/24/16 13:56 67-66-35.9 1.9 1
Chloromethane ND ug/kg 03/24/16 13:56 74-87-311.7 2.8 1
2-Chlorotoluene ND ug/kg 03/24/16 13:56 95-49-85.9 2.0 1
4-Chlorotoluene ND ug/kg 03/24/16 13:56 106-43-45.9 2.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/24/16 13:56 96-12-85.9 4.2 1
Dibromochloromethane ND ug/kg 03/24/16 13:56 124-48-15.9 2.1 1
1,2-Dibromoethane (EDB)ND ug/kg 03/24/16 13:56 106-93-45.9 2.1 1
Dibromomethane ND ug/kg 03/24/16 13:56 74-95-35.9 2.9 1
1,2-Dichlorobenzene ND ug/kg 03/24/16 13:56 95-50-15.9 2.2 1
1,3-Dichlorobenzene ND ug/kg 03/24/16 13:56 541-73-15.9 2.3 1
1,4-Dichlorobenzene ND ug/kg 03/24/16 13:56 106-46-75.9 2.0 1
Dichlorodifluoromethane ND ug/kg 03/24/16 13:56 75-71-811.7 4.2 1
1,1-Dichloroethane ND ug/kg 03/24/16 13:56 75-34-35.9 1.8 1
1,2-Dichloroethane ND ug/kg 03/24/16 13:56 107-06-25.9 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:CS-5 Lab ID:92291164005 Collected:03/22/16 10:55 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 03/24/16 13:56 75-35-45.9 2.1 1
cis-1,2-Dichloroethene ND ug/kg 03/24/16 13:56 156-59-25.9 1.6 1
trans-1,2-Dichloroethene ND ug/kg 03/24/16 13:56 156-60-55.9 2.2 1
1,2-Dichloropropane ND ug/kg 03/24/16 13:56 78-87-55.9 2.0 1
1,3-Dichloropropane ND ug/kg 03/24/16 13:56 142-28-95.9 2.2 1
2,2-Dichloropropane ND ug/kg 03/24/16 13:56 594-20-75.9 2.0 1
1,1-Dichloropropene ND ug/kg 03/24/16 13:56 563-58-65.9 1.8 1
cis-1,3-Dichloropropene ND ug/kg 03/24/16 13:56 10061-01-55.9 2.1 1
trans-1,3-Dichloropropene ND ug/kg 03/24/16 13:56 10061-02-65.9 1.8 1
Diisopropyl ether ND ug/kg 03/24/16 13:56 108-20-35.9 2.0 1
Ethylbenzene ND ug/kg 03/24/16 13:56 100-41-45.9 2.1 1
Hexachloro-1,3-butadiene ND ug/kg 03/24/16 13:56 87-68-35.9 2.3 1
2-Hexanone ND ug/kg 03/24/16 13:56 591-78-658.7 4.6 1
Isopropylbenzene (Cumene)ND ug/kg 03/24/16 13:56 98-82-85.9 2.2 1
p-Isopropyltoluene ND ug/kg 03/24/16 13:56 99-87-65.9 2.0 1
Methylene Chloride 12.6J ug/kg 03/24/16 13:56 75-09-223.5 3.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/24/16 13:56 108-10-158.7 4.3 1
Methyl-tert-butyl ether ND ug/kg 03/24/16 13:56 1634-04-45.9 1.8 1
Naphthalene ND ug/kg 03/24/16 13:56 91-20-35.9 1.4 1
n-Propylbenzene ND ug/kg 03/24/16 13:56 103-65-15.9 2.0 1
Styrene ND ug/kg 03/24/16 13:56 100-42-55.9 2.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/24/16 13:56 630-20-65.9 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/24/16 13:56 79-34-55.9 2.2 1
Tetrachloroethene ND ug/kg 03/24/16 13:56 127-18-45.9 2.0 1
Toluene ND ug/kg 03/24/16 13:56 108-88-35.9 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 03/24/16 13:56 87-61-65.9 2.6 1
1,2,4-Trichlorobenzene ND ug/kg 03/24/16 13:56 120-82-15.9 1.9 1
1,1,1-Trichloroethane ND ug/kg 03/24/16 13:56 71-55-65.9 2.1 1
1,1,2-Trichloroethane ND ug/kg 03/24/16 13:56 79-00-55.9 2.5 1
Trichloroethene ND ug/kg 03/24/16 13:56 79-01-65.9 2.5 1
Trichlorofluoromethane ND ug/kg 03/24/16 13:56 75-69-45.9 2.6 1
1,2,3-Trichloropropane ND ug/kg 03/24/16 13:56 96-18-45.9 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 03/24/16 13:56 95-63-65.9 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 03/24/16 13:56 108-67-85.9 2.1 1
Vinyl acetate ND ug/kg 03/24/16 13:56 108-05-458.7 10.3 1
Vinyl chloride ND ug/kg 03/24/16 13:56 75-01-411.7 2.1 1
Xylene (Total)ND ug/kg 03/24/16 13:56 1330-20-711.7 4.2 1
m&p-Xylene ND ug/kg 03/24/16 13:56 179601-23-111.7 4.2 1
o-Xylene ND ug/kg 03/24/16 13:56 95-47-65.9 2.2 1
Surrogates
Toluene-d8 (S)98 %03/24/16 13:56 2037-26-570-130 1
4-Bromofluorobenzene (S)83 %03/24/16 13:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %03/24/16 13:56 17060-07-070-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:CS-5 Lab ID:92291164005 Collected:03/22/16 10:55 Received:03/23/16 09:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 9.0 %03/24/16 11:590.10 0.10 1
Sample:TMW-3 Lab ID:92291164006 Collected:03/22/16 07:44 Received:03/23/16 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/26/16 18:31 67-64-125.0 10.0 1
Benzene ND ug/L 03/26/16 18:31 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/26/16 18:31 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/26/16 18:31 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/26/16 18:31 75-27-41.0 0.18 1
Bromoform ND ug/L 03/26/16 18:31 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/26/16 18:31 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/26/16 18:31 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/26/16 18:31 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/26/16 18:31 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/26/16 18:31 75-00-31.0 0.54 1
Chloroform ND ug/L 03/26/16 18:31 67-66-31.0 0.14 1
Chloromethane 0.26J ug/L 03/26/16 18:31 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/26/16 18:31 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/26/16 18:31 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/26/16 18:31 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/26/16 18:31 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/26/16 18:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/26/16 18:31 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/26/16 18:31 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/26/16 18:31 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/26/16 18:31 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/26/16 18:31 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/26/16 18:31 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/26/16 18:31 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 03/26/16 18:31 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/26/16 18:31 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/26/16 18:31 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/26/16 18:31 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/26/16 18:31 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/26/16 18:31 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/26/16 18:31 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/26/16 18:31 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/26/16 18:31 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/26/16 18:31 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/26/16 18:31 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291164
E43
Sample:TMW-3 Lab ID:92291164006 Collected:03/22/16 07:44 Received:03/23/16 09:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Hexachloro-1,3-butadiene ND ug/L 03/26/16 18:31 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/26/16 18:31 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/26/16 18:31 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/26/16 18:31 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/26/16 18:31 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/26/16 18:31 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/26/16 18:31 91-20-31.0 0.24 1
Styrene 0.42J ug/L 03/26/16 18:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/26/16 18:31 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/26/16 18:31 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/26/16 18:31 127-18-41.0 0.46 1
Toluene 0.53J ug/L 03/26/16 18:31 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/26/16 18:31 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/26/16 18:31 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/26/16 18:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/26/16 18:31 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/26/16 18:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/26/16 18:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/26/16 18:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/26/16 18:31 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/26/16 18:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/26/16 18:31 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/26/16 18:31 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/26/16 18:31 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %03/26/16 18:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %03/26/16 18:31 17060-07-070-130 1
Toluene-d8 (S)101 %03/26/16 18:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291164
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36132
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92291164006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1695528
Associated Lab Samples:92291164006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/26/16 16:190.33
1,1,1-Trichloroethane ug/L ND 1.0 03/26/16 16:190.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/26/16 16:190.40
1,1,2-Trichloroethane ug/L ND 1.0 03/26/16 16:190.29
1,1-Dichloroethane ug/L ND 1.0 03/26/16 16:190.32
1,1-Dichloroethene ug/L ND 1.0 03/26/16 16:190.56
1,1-Dichloropropene ug/L ND 1.0 03/26/16 16:190.49
1,2,3-Trichlorobenzene ug/L ND 1.0 03/26/16 16:190.33
1,2,3-Trichloropropane ug/L ND 1.0 03/26/16 16:190.41
1,2,4-Trichlorobenzene ug/L ND 1.0 03/26/16 16:190.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/26/16 16:192.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/26/16 16:190.27
1,2-Dichlorobenzene ug/L ND 1.0 03/26/16 16:190.30
1,2-Dichloroethane ug/L ND 1.0 03/26/16 16:190.24
1,2-Dichloropropane ug/L ND 1.0 03/26/16 16:190.27
1,3-Dichlorobenzene ug/L ND 1.0 03/26/16 16:190.24
1,3-Dichloropropane ug/L ND 1.0 03/26/16 16:190.28
1,4-Dichlorobenzene ug/L ND 1.0 03/26/16 16:190.33
2,2-Dichloropropane ug/L ND 1.0 03/26/16 16:190.13
2-Butanone (MEK)ug/L ND 5.0 03/26/16 16:190.96
2-Chlorotoluene ug/L ND 1.0 03/26/16 16:190.35
2-Hexanone ug/L ND 5.0 03/26/16 16:190.46
4-Chlorotoluene ug/L ND 1.0 03/26/16 16:190.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/26/16 16:190.33
Acetone ug/L ND 25.0 03/26/16 16:1910.0
Benzene ug/L ND 1.0 03/26/16 16:190.25
Bromobenzene ug/L ND 1.0 03/26/16 16:190.30
Bromochloromethane ug/L ND 1.0 03/26/16 16:190.17
Bromodichloromethane ug/L ND 1.0 03/26/16 16:190.18
Bromoform ug/L ND 1.0 03/26/16 16:190.26
Bromomethane ug/L ND 2.0 03/26/16 16:190.29
Carbon tetrachloride ug/L ND 1.0 03/26/16 16:190.25
Chlorobenzene ug/L ND 1.0 03/26/16 16:190.23
Chloroethane ug/L ND 1.0 03/26/16 16:190.54
Chloroform ug/L ND 1.0 03/26/16 16:190.14
Chloromethane ug/L ND 1.0 03/26/16 16:190.11
cis-1,2-Dichloroethene ug/L ND 1.0 03/26/16 16:190.19
cis-1,3-Dichloropropene ug/L ND 1.0 03/26/16 16:190.13
Dibromochloromethane ug/L ND 1.0 03/26/16 16:190.21
Dibromomethane ug/L ND 1.0 03/26/16 16:190.21
Dichlorodifluoromethane ug/L ND 1.0 03/26/16 16:190.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
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Page 16 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291164
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1695528
Associated Lab Samples:92291164006
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 03/26/16 16:190.12
Ethylbenzene ug/L ND 1.0 03/26/16 16:190.30
Hexachloro-1,3-butadiene ug/L ND 1.0 03/26/16 16:190.71
m&p-Xylene ug/L ND 2.0 03/26/16 16:190.66
Methyl-tert-butyl ether ug/L ND 1.0 03/26/16 16:190.21
Methylene Chloride ug/L ND 2.0 03/26/16 16:190.97
Naphthalene ug/L ND 1.0 03/26/16 16:190.24
o-Xylene ug/L ND 1.0 03/26/16 16:190.23
p-Isopropyltoluene ug/L ND 1.0 03/26/16 16:190.31
Styrene ug/L ND 1.0 03/26/16 16:190.26
Tetrachloroethene ug/L ND 1.0 03/26/16 16:190.46
Toluene ug/L ND 1.0 03/26/16 16:190.26
trans-1,2-Dichloroethene ug/L ND 1.0 03/26/16 16:190.49
trans-1,3-Dichloropropene ug/L ND 1.0 03/26/16 16:190.26
Trichloroethene ug/L ND 1.0 03/26/16 16:190.47
Trichlorofluoromethane ug/L ND 1.0 03/26/16 16:190.20
Vinyl acetate ug/L ND 2.0 03/26/16 16:190.35
Vinyl chloride ug/L ND 1.0 03/26/16 16:190.62
Xylene (Total)ug/L ND 2.0 03/26/16 16:190.66
1,2-Dichloroethane-d4 (S)%98 70-130 03/26/16 16:19
4-Bromofluorobenzene (S)%97 70-130 03/26/16 16:19
Toluene-d8 (S)%99 70-130 03/26/16 16:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1695529LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.550 107 70-130
1,1,1-Trichloroethane ug/L 51.950 104 70-130
1,1,2,2-Tetrachloroethane ug/L 49.650 99 70-130
1,1,2-Trichloroethane ug/L 49.350 99 70-130
1,1-Dichloroethane ug/L 49.850 100 70-130
1,1-Dichloroethene ug/L 53.250 106 70-132
1,1-Dichloropropene ug/L 53.350 107 70-130
1,2,3-Trichlorobenzene ug/L 54.750 109 70-135
1,2,3-Trichloropropane ug/L 51.250 102 70-130
1,2,4-Trichlorobenzene ug/L 54.450 109 70-134
1,2-Dibromo-3-chloropropane ug/L 54.350 109 70-130
1,2-Dibromoethane (EDB)ug/L 54.950 110 70-130
1,2-Dichlorobenzene ug/L 50.050 100 70-130
1,2-Dichloroethane ug/L 48.250 96 70-130
1,2-Dichloropropane ug/L 50.450 101 70-130
1,3-Dichlorobenzene ug/L 51.450 103 70-130
1,3-Dichloropropane ug/L 50.650 101 70-130
1,4-Dichlorobenzene ug/L 50.550 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
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Page 17 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291164
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1695529LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 51.850 104 58-145
2-Butanone (MEK)ug/L 104100 104 70-145
2-Chlorotoluene ug/L 47.550 95 70-130
2-Hexanone ug/L 105100 105 70-144
4-Chlorotoluene ug/L 49.650 99 70-130
4-Methyl-2-pentanone (MIBK)ug/L 105100 105 70-140
Acetone ug/L 103100 103 50-175
Benzene ug/L 49.950 100 70-130
Bromobenzene ug/L 50.650 101 70-130
Bromochloromethane ug/L 50.050 100 70-130
Bromodichloromethane ug/L 51.950 104 70-130
Bromoform ug/L 46.750 93 70-130
Bromomethane ug/L 57.350 115 54-130
Carbon tetrachloride ug/L 52.650 105 70-132
Chlorobenzene ug/L 50.450 101 70-130
Chloroethane ug/L 47.350 95 64-134
Chloroform ug/L 52.250 104 70-130
Chloromethane ug/L 50.850 102 64-130
cis-1,2-Dichloroethene ug/L 50.750 101 70-131
cis-1,3-Dichloropropene ug/L 52.350 105 70-130
Dibromochloromethane ug/L 52.850 106 70-130
Dibromomethane ug/L 50.050 100 70-131
Dichlorodifluoromethane ug/L 48.950 98 56-130
Diisopropyl ether ug/L 52.750 105 70-130
Ethylbenzene ug/L 52.150 104 70-130
Hexachloro-1,3-butadiene ug/L 56.750 113 70-130
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 53.750 107 70-130
Methylene Chloride ug/L 51.950 104 63-130
Naphthalene ug/L 53.150 106 70-138
o-Xylene ug/L 49.550 99 70-130
p-Isopropyltoluene ug/L 53.250 106 70-130
Styrene ug/L 51.050 102 70-130
Tetrachloroethene ug/L 52.350 105 70-130
Toluene ug/L 49.450 99 70-130
trans-1,2-Dichloroethene ug/L 54.050 108 70-130
trans-1,3-Dichloropropene ug/L 52.050 104 70-132
Trichloroethene ug/L 48.950 98 70-130
Trichlorofluoromethane ug/L 55.250 110 62-133
Vinyl acetate ug/L 96.1100 96 66-157
Vinyl chloride ug/L 54.750 109 50-150
Xylene (Total)ug/L 150150 100 70-130
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
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Page 18 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291164
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36108
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92291164001, 92291164002, 92291164003, 92291164004, 92291164005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1694122
Associated Lab Samples:92291164001, 92291164002, 92291164003, 92291164004, 92291164005
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 7.0 03/24/16 10:382.9
1,1,1-Trichloroethane ug/kg ND 7.0 03/24/16 10:382.5
1,1,2,2-Tetrachloroethane ug/kg ND 7.0 03/24/16 10:382.7
1,1,2-Trichloroethane ug/kg ND 7.0 03/24/16 10:382.9
1,1-Dichloroethane ug/kg ND 7.0 03/24/16 10:382.1
1,1-Dichloroethene ug/kg ND 7.0 03/24/16 10:382.5
1,1-Dichloropropene ug/kg ND 7.0 03/24/16 10:382.1
1,2,3-Trichlorobenzene ug/kg ND 7.0 03/24/16 10:383.1
1,2,3-Trichloropropane ug/kg ND 7.0 03/24/16 10:382.2
1,2,4-Trichlorobenzene ug/kg ND 7.0 03/24/16 10:382.2
1,2,4-Trimethylbenzene ug/kg ND 7.0 03/24/16 10:382.8
1,2-Dibromo-3-chloropropane ug/kg ND 7.0 03/24/16 10:385.0
1,2-Dibromoethane (EDB)ug/kg ND 7.0 03/24/16 10:382.5
1,2-Dichlorobenzene ug/kg ND 7.0 03/24/16 10:382.7
1,2-Dichloroethane ug/kg ND 7.0 03/24/16 10:383.1
1,2-Dichloropropane ug/kg ND 7.0 03/24/16 10:382.4
1,3,5-Trimethylbenzene ug/kg ND 7.0 03/24/16 10:382.5
1,3-Dichlorobenzene ug/kg ND 7.0 03/24/16 10:382.8
1,3-Dichloropropane ug/kg ND 7.0 03/24/16 10:382.7
1,4-Dichlorobenzene ug/kg ND 7.0 03/24/16 10:382.4
2,2-Dichloropropane ug/kg ND 7.0 03/24/16 10:382.4
2-Butanone (MEK)ug/kg ND 140 03/24/16 10:384.1
2-Chlorotoluene ug/kg ND 7.0 03/24/16 10:382.4
2-Hexanone ug/kg ND 69.8 03/24/16 10:385.4
4-Chlorotoluene ug/kg ND 7.0 03/24/16 10:382.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 69.8 03/24/16 10:385.2
Acetone ug/kg ND 140 03/24/16 10:3814.0
Benzene ug/kg ND 7.0 03/24/16 10:382.2
Bromobenzene ug/kg ND 7.0 03/24/16 10:382.8
Bromochloromethane ug/kg ND 7.0 03/24/16 10:382.4
Bromodichloromethane ug/kg ND 7.0 03/24/16 10:382.7
Bromoform ug/kg ND 7.0 03/24/16 10:383.2
Bromomethane ug/kg ND 14.0 03/24/16 10:383.5
Carbon tetrachloride ug/kg ND 7.0 03/24/16 10:383.6
Chlorobenzene ug/kg ND 7.0 03/24/16 10:382.7
Chloroethane ug/kg ND 14.0 03/24/16 10:383.4
Chloroform ug/kg ND 7.0 03/24/16 10:382.2
Chloromethane ug/kg ND 14.0 03/24/16 10:383.4
cis-1,2-Dichloroethene ug/kg ND 7.0 03/24/16 10:382.0
cis-1,3-Dichloropropene ug/kg ND 7.0 03/24/16 10:382.5
Dibromochloromethane ug/kg ND 7.0 03/24/16 10:382.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
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Page 19 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291164
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1694122
Associated Lab Samples:92291164001, 92291164002, 92291164003, 92291164004, 92291164005
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg ND 7.0 03/24/16 10:383.5
Dichlorodifluoromethane ug/kg ND 14.0 03/24/16 10:385.0
Diisopropyl ether ug/kg ND 7.0 03/24/16 10:382.4
Ethylbenzene ug/kg ND 7.0 03/24/16 10:382.5
Hexachloro-1,3-butadiene ug/kg ND 7.0 03/24/16 10:382.8
Isopropylbenzene (Cumene)ug/kg ND 7.0 03/24/16 10:382.7
m&p-Xylene ug/kg ND 14.0 03/24/16 10:385.0
Methyl-tert-butyl ether ug/kg ND 7.0 03/24/16 10:382.1
Methylene Chloride ug/kg ND 27.9 03/24/16 10:384.2
n-Butylbenzene ug/kg ND 7.0 03/24/16 10:382.5
n-Propylbenzene ug/kg ND 7.0 03/24/16 10:382.4
Naphthalene ug/kg 2.2J 7.0 03/24/16 10:381.7
o-Xylene ug/kg ND 7.0 03/24/16 10:382.7
p-Isopropyltoluene ug/kg ND 7.0 03/24/16 10:382.4
sec-Butylbenzene ug/kg ND 7.0 03/24/16 10:382.2
Styrene ug/kg ND 7.0 03/24/16 10:382.5
tert-Butylbenzene ug/kg ND 7.0 03/24/16 10:382.8
Tetrachloroethene ug/kg ND 7.0 03/24/16 10:382.4
Toluene ug/kg ND 7.0 03/24/16 10:382.5
trans-1,2-Dichloroethene ug/kg ND 7.0 03/24/16 10:382.7
trans-1,3-Dichloropropene ug/kg ND 7.0 03/24/16 10:382.1
Trichloroethene ug/kg ND 7.0 03/24/16 10:382.9
Trichlorofluoromethane ug/kg ND 7.0 03/24/16 10:383.1
Vinyl acetate ug/kg ND 69.8 03/24/16 10:3812.3
Vinyl chloride ug/kg ND 14.0 03/24/16 10:382.5
Xylene (Total)ug/kg ND 14.0 03/24/16 10:385.0
1,2-Dichloroethane-d4 (S)%112 70-132 03/24/16 10:38
4-Bromofluorobenzene (S)%95 70-130 03/24/16 10:38
Toluene-d8 (S)%101 70-130 03/24/16 10:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1694123LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 72.074 97 74-137
1,1,1-Trichloroethane ug/kg 78.674 106 67-140
1,1,2,2-Tetrachloroethane ug/kg 71.874 97 72-141
1,1,2-Trichloroethane ug/kg 73.674 99 78-138
1,1-Dichloroethane ug/kg 77.974 105 69-134
1,1-Dichloroethene ug/kg 80.374 109 67-138
1,1-Dichloropropene ug/kg 79.974 108 69-139
1,2,3-Trichlorobenzene ug/kg 71.874 97 70-146
1,2,3-Trichloropropane ug/kg 72.274 98 69-144
1,2,4-Trichlorobenzene ug/kg 71.874 97 68-148
1,2,4-Trimethylbenzene ug/kg 74.974 101 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291164
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1694123LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 77.374 105 65-140
1,2-Dibromoethane (EDB)ug/kg 74.974 101 77-135
1,2-Dichlorobenzene ug/kg 71.774 97 77-141
1,2-Dichloroethane ug/kg 75.274 102 65-137
1,2-Dichloropropane ug/kg 77.574 105 72-136
1,3,5-Trimethylbenzene ug/kg 75.074 101 76-133
1,3-Dichlorobenzene ug/kg 73.774 100 74-138
1,3-Dichloropropane ug/kg 75.374 102 71-139
1,4-Dichlorobenzene ug/kg 73.774 100 76-138
2,2-Dichloropropane ug/kg 77.474 105 68-137
2-Butanone (MEK)ug/kg 172148 116 58-147
2-Chlorotoluene ug/kg 73.674 100 73-139
2-Hexanone ug/kg 164148 111 62-145
4-Chlorotoluene ug/kg 74.474 101 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 166148 112 64-149
Acetone ug/kg 179148 121 53-153
Benzene ug/kg 76.974 104 73-135
Bromobenzene ug/kg 76.174 103 75-133
Bromochloromethane ug/kg 80.674 109 73-134
Bromodichloromethane ug/kg 74.974 101 71-135
Bromoform ug/kg 70.374 95 66-141
Bromomethane ug/kg 88.674 120 53-160
Carbon tetrachloride ug/kg 74.974 101 60-145
Chlorobenzene ug/kg 74.274 100 78-130
Chloroethane ug/kg 86.574 117 64-149
Chloroform ug/kg 77.174 104 70-134
Chloromethane ug/kg 92.674 125 52-150
cis-1,2-Dichloroethene ug/kg 79.674 108 70-133
cis-1,3-Dichloropropene ug/kg 78.474 106 68-134
Dibromochloromethane ug/kg 73.674 99 71-138
Dibromomethane ug/kg 73.574 99 74-130
Dichlorodifluoromethane ug/kg 85.874 116 40-160
Diisopropyl ether ug/kg 82.674 112 69-141
Ethylbenzene ug/kg 75.874 102 75-133
Hexachloro-1,3-butadiene ug/kg 68.474 92 68-143
Isopropylbenzene (Cumene)ug/kg 73.974 100 76-143
m&p-Xylene ug/kg 148148 100 75-136
Methyl-tert-butyl ether ug/kg 78.974 107 68-144
Methylene Chloride ug/kg 83.774 113 45-154
n-Butylbenzene ug/kg 77.074 104 72-137
n-Propylbenzene ug/kg 75.274 102 76-136
Naphthalene ug/kg 76.574 103 68-151
o-Xylene ug/kg 72.874 98 76-141
p-Isopropyltoluene ug/kg 74.274 100 76-140
sec-Butylbenzene ug/kg 74.174 100 79-139
Styrene ug/kg 74.174 100 79-137
tert-Butylbenzene ug/kg 67.374 91 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 21 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291164
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1694123LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 58.974 80 71-138
Toluene ug/kg 75.974 103 74-131
trans-1,2-Dichloroethene ug/kg 78.374 106 67-135
trans-1,3-Dichloropropene ug/kg 75.474 102 65-146
Trichloroethene ug/kg 73.474 99 67-135
Trichlorofluoromethane ug/kg 81.574 110 59-144
Vinyl acetate ug/kg 162 F314811040-160
Vinyl chloride ug/kg 90.374 122 56-141
Xylene (Total)ug/kg 221222 100 76-137
1,2-Dichloroethane-d4 (S)%106 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291164
E43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/8914
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92291164001, 92291164002, 92291164003, 92291164004, 92291164005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92290901001
1693656SAMPLE DUPLICATE:
Percent Moisture %47.1 17 2539.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92291164005
1693657SAMPLE DUPLICATE:
Percent Moisture %9.9 10 259.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
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Huntersville, NC 28078
[phone]
Page 23 of 27
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92291164
E43
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.1g
Common Laboratory Contaminant.C9
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 27
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92291164
E43
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92291164006 MSV/36132TMW-3 EPA 8260
92291164001 MSV/36108CS-1 EPA 8260
92291164002 MSV/36108CS-2 EPA 8260
92291164003 MSV/36108CS-3 EPA 8260
92291164004 MSV/36108CS-4 EPA 8260
92291164005 MSV/36108CS-5 EPA 8260
92291164001 PMST/8914CS-1 ASTM D2974-87
92291164002 PMST/8914CS-2 ASTM D2974-87
92291164003 PMST/8914CS-3 ASTM D2974-87
92291164004 PMST/8914CS-4 ASTM D2974-87
92291164005 PMST/8914CS-5 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/28/2016 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 27
Page 26 of 27
Page 27 of 27

APPENDIX C
SAMPLE POINT CONSTRUCTION RECORDS

~12" #3 SAND
1/4" OUTSIDE DIAMETER NYLAFLOW TUBING
TYPE I / II PORTLAND CEMENT
6" STAINLESS IMPLANT
CENTERED IN FILTER PACK
~6" DRY GRANULAR BENTONITE CHIPS
GROUND SURFACE
5' OR 10'
NOT TO SCALE
2 1/8" DIRECT PUSH POINT OR 3" HAND PUSH POINT
CA
D

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DRAWN BY:
PROJECT NO.
CHECKED BY:
REVISED:
DATE:
PAGE: of
FIGURESHALLOW SOIL GAS PROBE
CONSTRUCTION DETAIL
E-43 ELEMENTARY SCHOOL
11500 HOLLY SPRINGS NEW HILL ROAD
HOLLY SPRINGS, NORTH CAROLINA
20160086.001A
NL
MAS
3/2016
1
GB
sample submittedfor laboratory
analysis
5.0
SANDY LEAN CLAY Red silty CLAY
Boring termination
Bottom of borehole at 5.0 feet.
FID = 0
FID = 0
FID = 0
FID = 8.5
FID = 44.2
NOTES
GROUND ELEVATION
LOGGED BY C. Hollinger
DRILLING METHOD direct push
DRILLING CONTRACTOR Quantex GROUND WATER LEVELS:
CHECKED BY M. Burns
DATE STARTED 3/21/16 COMPLETED 3/21/16
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2 inches
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
DE
P
T
H
(f
t
)
0.0
2.5
5.0
PAGE 1 OF 1
BORING NUMBER DP-1
CLIENT Wake County Public School System
PROJECT NUMBER 20160086.001A
PROJECT NAME E-43
PROJECT LOCATION Holly Springs, NC
GE
N
E
R
A
L

B
H

/

T
P

/

W
E
L
L

-

G
I
N
T

S
T
D

U
S

L
A
B
.
G
D
T

-

6
/
7
/
1
6

0
9
:
1
8

-

U
:
\
M
B
U
R
N
S
\
W
C
P
S
S
\
G
I
N
T

S
T
D

U
S

L
A
B
.
G
P
J
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
REMARKS
GR
A
P
H
I
C
LO
G MATERIAL DESCRIPTION
EN
V
I
R
O
N
M
E
N
T
A
L
DA
T
A
sample submittedfor laboratory
analysis
5.0
LEAN CLAY WITH SAND Red silty CLAY
Boring termination
Bottom of borehole at 5.0 feet.
FID = 0
FID = 13.3
FID = 165
FID = 291
FID = 398
NOTES
GROUND ELEVATION
LOGGED BY C. Hollinger
DRILLING METHOD direct push
DRILLING CONTRACTOR Quantex GROUND WATER LEVELS:
CHECKED BY M. Burns
DATE STARTED 3/21/16 COMPLETED 3/21/16
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2 inches
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
DE
P
T
H
(f
t
)
0.0
2.5
5.0
PAGE 1 OF 1
BORING NUMBER DP-2
CLIENT Wake County Public School System
PROJECT NUMBER 20160086.001A
PROJECT NAME E-43
PROJECT LOCATION Holly Springs, NC
GE
N
E
R
A
L

B
H

/

T
P

/

W
E
L
L

-

G
I
N
T

S
T
D

U
S

L
A
B
.
G
D
T

-

6
/
7
/
1
6

0
9
:
1
8

-

U
:
\
M
B
U
R
N
S
\
W
C
P
S
S
\
G
I
N
T

S
T
D

U
S

L
A
B
.
G
P
J
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
REMARKS
GR
A
P
H
I
C
LO
G MATERIAL DESCRIPTION
EN
V
I
R
O
N
M
E
N
T
A
L
DA
T
A
sample submitted
for laboratoryanalysis
4.0
10.0
13.0
15.0
17.0
21.0
Red silty CLAY
Tan clayey SILT
Light brown fine sandy SILT w/ rock fragments
Saprolite: weathered arkosic sandstone
Red and tan clayey SILT
Saprolite: weathered arkosic sandstone
Probe refusal Refusal at 21.0 feet.
Bottom of borehole at 21.0 feet.
1" PVC Riser
BentoniteSeal
Sand Pack
1" PVC Well
Screen
FID = 2
FID = 106
FID = 47.5
FID = 351
NOTES
GROUND ELEVATION
LOGGED BY C. Hollinger
DRILLING METHOD direct push
DRILLING CONTRACTOR Quantex GROUND WATER LEVELS:
CHECKED BY M. Burns
DATE STARTED 3/21/16 COMPLETED 3/21/16
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING 16.27 ft
HOLE SIZE 2 inches
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
DE
P
T
H
(f
t
)
0
5
10
15
20
PAGE 1 OF 1
WELL NUMBER DP-3/TMW-1
CLIENT Wake County Public School System
PROJECT NUMBER 20160086.001A
PROJECT NAME E-43
PROJECT LOCATION Holly Springs, NC
GE
N
E
R
A
L

B
H

/

T
P

/

W
E
L
L

-

G
I
N
T

S
T
D

U
S

L
A
B
.
G
D
T

-

6
/
7
/
1
6

0
9
:
1
8

-

U
:
\
M
B
U
R
N
S
\
W
C
P
S
S
\
G
I
N
T

S
T
D

U
S

L
A
B
.
G
P
J
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
REMARKS
GR
A
P
H
I
C
LO
G MATERIAL DESCRIPTION
Casing Type: PVC
WELL DIAGRAM
EN
V
I
R
O
N
M
E
N
T
A
L
DA
T
A
sample submittedfor laboratory
analysis
5.0
Red and tan clayey SILT
Boring termination
Bottom of borehole at 5.0 feet.
FID = 21.2
FID = 219
FID = 515
FID = 930
FID = 861
NOTES
GROUND ELEVATION
LOGGED BY C. Hollinger
DRILLING METHOD direct push
DRILLING CONTRACTOR Quantex GROUND WATER LEVELS:
CHECKED BY M. Burns
DATE STARTED 3/21/16 COMPLETED 3/21/16
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2 inches
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
DE
P
T
H
(f
t
)
0.0
2.5
5.0
PAGE 1 OF 1
BORING NUMBER DP-4
CLIENT Wake County Public School System
PROJECT NUMBER 20160086.001A
PROJECT NAME E-43
PROJECT LOCATION Holly Springs, NC
GE
N
E
R
A
L

B
H

/

T
P

/

W
E
L
L

-

G
I
N
T

S
T
D

U
S

L
A
B
.
G
D
T

-

6
/
7
/
1
6

0
9
:
1
8

-

U
:
\
M
B
U
R
N
S
\
W
C
P
S
S
\
G
I
N
T

S
T
D

U
S

L
A
B
.
G
P
J
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
REMARKS
GR
A
P
H
I
C
LO
G MATERIAL DESCRIPTION
EN
V
I
R
O
N
M
E
N
T
A
L
DA
T
A
sample submittedfor laboratoryanalysis
5.0
Red and tan silty CLAY
Boring termination
Bottom of borehole at 5.0 feet.
FID = 680
FID = 520
FID = 636
FID = 541
NOTES
GROUND ELEVATION
LOGGED BY C. Hollinger
DRILLING METHOD direct push
DRILLING CONTRACTOR Quantex GROUND WATER LEVELS:
CHECKED BY M. Burns
DATE STARTED 3/21/16 COMPLETED 3/21/16
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2 inches
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
DE
P
T
H
(f
t
)
0.0
2.5
5.0
PAGE 1 OF 1
BORING NUMBER DP-5
CLIENT Wake County Public School System
PROJECT NUMBER 20160086.001A
PROJECT NAME E-43
PROJECT LOCATION Holly Springs, NC
GE
N
E
R
A
L

B
H

/

T
P

/

W
E
L
L

-

G
I
N
T

S
T
D

U
S

L
A
B
.
G
D
T

-

6
/
7
/
1
6

0
9
:
1
8

-

U
:
\
M
B
U
R
N
S
\
W
C
P
S
S
\
G
I
N
T

S
T
D

U
S

L
A
B
.
G
P
J
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
REMARKS
GR
A
P
H
I
C
LO
G MATERIAL DESCRIPTION
EN
V
I
R
O
N
M
E
N
T
A
L
DA
T
A
sample submittedfor laboratoryanalysis
5.0
Tan silty CLAY
Boring termination
Bottom of borehole at 5.0 feet.
FID = 121
FID = 1045
FID = 719
FID = 700
FID = 335
NOTES
GROUND ELEVATION
LOGGED BY C. Hollinger
DRILLING METHOD direct push
DRILLING CONTRACTOR Quantex GROUND WATER LEVELS:
CHECKED BY M. Burns
DATE STARTED 3/21/16 COMPLETED 3/21/16
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2 inches
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
DE
P
T
H
(f
t
)
0.0
2.5
5.0
PAGE 1 OF 1
BORING NUMBER DP-6
CLIENT Wake County Public School System
PROJECT NUMBER 20160086.001A
PROJECT NAME E-43
PROJECT LOCATION Holly Springs, NC
GE
N
E
R
A
L

B
H

/

T
P

/

W
E
L
L

-

G
I
N
T

S
T
D

U
S

L
A
B
.
G
D
T

-

6
/
7
/
1
6

0
9
:
1
8

-

U
:
\
M
B
U
R
N
S
\
W
C
P
S
S
\
G
I
N
T

S
T
D

U
S

L
A
B
.
G
P
J
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
REMARKS
GR
A
P
H
I
C
LO
G MATERIAL DESCRIPTION
EN
V
I
R
O
N
M
E
N
T
A
L
DA
T
A
sample submittedfor laboratory
analysis
5.0
Tan silty CLAY
Boring termination
Bottom of borehole at 5.0 feet.
FID = 1
FID = 1
FID = 1
FID = 5
FID = 36
NOTES
GROUND ELEVATION
LOGGED BY C. Hollinger
DRILLING METHOD direct push
DRILLING CONTRACTOR Quantex GROUND WATER LEVELS:
CHECKED BY M. Burns
DATE STARTED 3/21/16 COMPLETED 3/21/16
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2 inches
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
DE
P
T
H
(f
t
)
0.0
2.5
5.0
PAGE 1 OF 1
BORING NUMBER DP-7
CLIENT Wake County Public School System
PROJECT NUMBER 20160086.001A
PROJECT NAME E-43
PROJECT LOCATION Holly Springs, NC
GE
N
E
R
A
L

B
H

/

T
P

/

W
E
L
L

-

G
I
N
T

S
T
D

U
S

L
A
B
.
G
D
T

-

6
/
7
/
1
6

0
9
:
1
9

-

U
:
\
M
B
U
R
N
S
\
W
C
P
S
S
\
G
I
N
T

S
T
D

U
S

L
A
B
.
G
P
J
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
REMARKS
GR
A
P
H
I
C
LO
G MATERIAL DESCRIPTION
EN
V
I
R
O
N
M
E
N
T
A
L
DA
T
A
sample submitted
for laboratoryanalysis
7.0
10.0
15.0
Tan silty CLAY
Red and tan fine sandy SILT
Saprolite: weathered arkosic sandstone
Probe refusal
Refusal at 15.0 feet.Bottom of borehole at 15.0 feet.
1" PVC Riser
Bentoniteseal
Sand pack
1" PVC Well
Screen
FID = 2
FID = 1.5
FID = 2
FID = 2
FID = 2
FID = 2
FID = 2
FID = 0
FID = 0
NOTES
GROUND ELEVATION
LOGGED BY C. Hollinger
DRILLING METHOD direct push
DRILLING CONTRACTOR Quantex GROUND WATER LEVELS:
CHECKED BY M. Burns
DATE STARTED 3/21/16 COMPLETED 3/21/16
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING 14.50 ft
HOLE SIZE 2 inches
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
DE
P
T
H
(f
t
)
0
5
10
15
PAGE 1 OF 1
WELL NUMBER DP-8/TMW-2
CLIENT Wake County Public School System
PROJECT NUMBER 20160086.001A
PROJECT NAME E-43
PROJECT LOCATION Holly Springs, NC
GE
N
E
R
A
L

B
H

/

T
P

/

W
E
L
L

-

G
I
N
T

S
T
D

U
S

L
A
B
.
G
D
T

-

6
/
7
/
1
6

0
9
:
1
9

-

U
:
\
M
B
U
R
N
S
\
W
C
P
S
S
\
G
I
N
T

S
T
D

U
S

L
A
B
.
G
P
J
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
REMARKS
GR
A
P
H
I
C
LO
G MATERIAL DESCRIPTION
Casing Type: PVC
WELL DIAGRAM
EN
V
I
R
O
N
M
E
N
T
A
L
DA
T
A
sample submitted
for laboratoryanalysis
0.5
5.0
Gravel from construction activities
Red silty CLAY
Boring termination
Bottom of borehole at 5.0 feet.
FID = 2
FID = 2
FID = 2
NOTES
GROUND ELEVATION
LOGGED BY C. Hollinger
DRILLING METHOD direct push
DRILLING CONTRACTOR Quantex GROUND WATER LEVELS:
CHECKED BY M. Burns
DATE STARTED 3/21/16 COMPLETED 3/21/16
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2 inches
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
DE
P
T
H
(f
t
)
0.0
2.5
5.0
PAGE 1 OF 1
BORING NUMBER DP-9
CLIENT Wake County Public School System
PROJECT NUMBER 20160086.001A
PROJECT NAME E-43
PROJECT LOCATION Holly Springs, NC
GE
N
E
R
A
L

B
H

/

T
P

/

W
E
L
L

-

G
I
N
T

S
T
D

U
S

L
A
B
.
G
D
T

-

6
/
7
/
1
6

0
9
:
1
9

-

U
:
\
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J
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
REMARKS
GR
A
P
H
I
C
LO
G MATERIAL DESCRIPTION
EN
V
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O
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E
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T
A
L
DA
T
A
sample submittedfor laboratory
analysis
6.0
14.0
17.5
Red silty CLAY
Tan fine sandy SILT
Saprolite: weathered arkosic sandstone
Probe refusal Refusal at 17.5 feet.Bottom of borehole at 17.5 feet.
1" PVC riser
bentonite seal
sand pack
1" PVC
screen
FID = 1
FID = 1
FID = 1
FID = 3
FID = 3
FID = 1
FID = 1
FID = 1
NOTES
GROUND ELEVATION
LOGGED BY C. Hollinger
DRILLING METHOD direct push
DRILLING CONTRACTOR Quantex GROUND WATER LEVELS:
CHECKED BY M. Burns
DATE STARTED 3/21/16 COMPLETED 3/21/16
AT TIME OF DRILLING ---
AT END OF DRILLING ---
24hrs AFTER DRILLING 16.00 ft
HOLE SIZE 2 inches
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
DE
P
T
H
(f
t
)
0
5
10
15
PAGE 1 OF 1
WELL NUMBER DP-10/TMW-3
CLIENT Wake County Public School System
PROJECT NUMBER 20160086.001A
PROJECT NAME E-43
PROJECT LOCATION Holly Springs, NC
GE
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A
B
.
G
P
J
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
KLEINFELDER, INC.
3500 GATEWAY CENTRE BLVD.
MORRISVILLE, NC 27560
919.755.5011
919.755.1414
REMARKS
GR
A
P
H
I
C
LO
G MATERIAL DESCRIPTION WELL DIAGRAM
EN
V
I
R
O
N
M
E
N
T
A
L
DA
T
A

APPENDIX D
FIELD DATA

FIELD SAMPLING EQUIPMENT

Typical sampling manifold (photo from Eurofins Air Toxics)

Photo of field apparatus showing helium source and shroud for leak testing, sample canister and
manifold, and pump for purging.

APPENDIX E
BUILDING CONSTRUCTION DETAILS

3

APPENDIX F
ALTERNATIVE METHODOLOGY FOR SUB-SLAB VAPOR MONITORING
NCDEQ APPROVAL

1
Michael Sussman
From:Drummond, Jaclynne <[e-mail]>
Sent:Thursday, March 31, 2016 2:33 PM
To:Michael Sussman
Subject:RE: Alternative Methodology for Sub-Slab Vapor Monitoring
Mike,
The request to use vapor pins is approved.
Thanks,
Jackie

Jaclynne Drummond
Compliance Hydrogeologist
Division of Waste Management - Solid Waste Section
NC Department of Environmental Quality (DEQ)

828.296.4706 Office
828.299.7043 Fax
[e-mail]

Asheville Regional Office (ARO)
2090 US Highway 70
Swannanoa, NC 28778

2
slab. I’ve included some photos below, we would use the metal caps in the second two photos and not the plastic insert
shown in the first.

I know these have been used extensively in the DSCA work. I hope to get your approval for the method for this site by
tomorrow if possible as we would like to proceed on Monday.