8803_TranslvaniaCoMSWLF_GWMR_DIN26675_20160719

2211 West Meadowview Rd.
Greensboro, NC 27407
tel: [phone]
fax: [phone] www.JoyceEngineering.com

July 11, 2016

Mr. Ervin Lane
Compliance Hydrogeologist
Division of Waste Management/Solid Waste Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

RE: First Semiannual Groundwater Monitoring Report of 2016
Calvert Landfill, Permit No. 88-03
Transylvania County, North Carolina
JOYCE Project No. 00336.1601.12, Task No. 01

Dear Ervin:

On behalf of Transylvania County, Joyce Engineering is submitting the enclosed First
Semiannual Monitoring Report of 2016 in electronic format, plus a copy of the Environmental
Monitoring Form for the Calvert Landfill, Permit No. 88-03. This report completes the second
semiannual compliance monitoring event of 2016 as required by the North Carolina Division of
Waste Management, Solid Waste Section. Please feel free to contact Alex Everhart or me at
[phone] if you have any questions regarding this submittal.

Sincerely,
JOYCE ENGINEERING

Hannu Kemppinen P.G.
Senior Project Consultant

Enclosures

C: Jeff Brookshire – Transylvania County

PREPARED FOR:
TRANSYLVANIA COUNTY SOLID WASTE
500 HOWELL ROAD
BREVARD, NORTH CAROLINA 28712

TRANSYLVANIA COUNTY CALVERT LANDFILL
PERMIT NO. 88-03
FIRST SEMIANNUAL GROUNDWATER
MONITORING REPORT OF 2016

JULY 2016

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101 GREENSBORO, NORTH CAROLINA 27407 NC LICENSE NUMBER C-0782 PHONE: [phone] FAX: [phone]
JOYCE PROJECT NO. 00336.1601.12
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First Semiannual Groundwater Monitoring Report of 2016 Joyce Engineering
Transylvania County Calvert Landfill, Permit No. 88-03 July 2016
i
First Semiannual Groundwater Monitoring Report of 2016
Calvert Landfill
Transylvania County, North Carolina

TABLE OF CONTENTS

1.0 INTRODUCTION..............................................................................................................1
1.1 Site Information .................................................................................................................1
1.2 Site Geology ........................................................................................................................1
1.3 Regulatory Status ...............................................................................................................1
2.0 FACILITY MONITORING PROGRAM .......................................................................1
2.1 Groundwater Monitoring Program .................................................................................1
2.2 Surface Water Monitoring Program ................................................................................2
3.0 FIRST SEMIANNUAL SAMPLING EVENT OF 2016 ................................................2
3.1 Field Work and Visual Inspection ....................................................................................2
3.2 Laboratory Analysis and JOYCE Quality Control ........................................................3
4.0 DATA ANALYSIS .............................................................................................................4
4.1 Inorganic Analytical Results and Comparisons to Standards .......................................4
4.2 Organic Analytical Results and Comparisons to Standards..........................................4
5.0 CONCLUSION ..................................................................................................................5
6.0 REFERENCES ...................................................................................................................6

Tables
Table 1 Summary of Historical Groundwater Elevations
Table 2 Summary of Historical Inorganic Constituents
Table 3 Summary of Historical Organic Constituents Table 4 Horizontal Groundwater Flow Velocities

Figure

Figure No. 1 Site Location Map

Drawing

Drawing No. 1 Groundwater Surface Map

Appendices

Appendix 1 Laboratory Analytical Report and Field Forms
Appendix 2 Summary of Detections and Summary of Exceedances
Appendix 3 Summary of Field Parameters
Appendix 4 Summary of Monitoring Well Construction

First Semiannual Groundwater Monitoring Report of 2016 Joyce Engineering
Transylvania County Calvert Landfill, Permit No. 88-03 July 2016
1
1.0 INTRODUCTION

1.1 Site Information

Transylvania County’s closed Calvert Landfill (Permit #88-03) is located north of Rosman,
North Carolina between U.S. Highway 64 and Old U.S. Highway 64 (Figure No. 1). The unlined
landfill operated between 1973 and May 1992.

1.2 Site Geology

The Calvert Landfill is located in the Inner Piedmont physiographic province within the Chauga
Belt, just southeast of the Brevard Fault Zone. The unit within the Chauga Belt that underlies the
site is the Henderson Gneiss, which consists of augen gneisses. The mineralogy consists of
microcline, oligoclase, quartz, biotite, muscovite, epidote, and sphene.

1.3 Regulatory Status

The current groundwater monitoring at Calvert Landfill is in accordance with criteria set forth in
Rule .0500 of the North Carolina Solid Waste Management Rules (NCSWMR) for municipal
solid waste landfills (MSWLF) closed prior to April 9, 1993. Surface water will be monitored in
accordance with criteria set forth in Rule .0602 of the NCSWMR.

2.0 FACILITY MONITORING PROGRAM

2.1 Groundwater Monitoring Program

Groundwater monitoring at the Calvert Landfill is completed in accordance with the Detection
Monitoring Program for Rule .0500 sites. Groundwater samples are collected semiannually.
Eleven active groundwater monitoring wells and one homeowner well comprise the groundwater
monitoring network at the Calvert Landfill. The current compliance network consists of
monitoring wells MW-1, MW-2, MW-3, MW-4, MW-105S, MW-105D, MW-106S, MW-106D,
MW-107S, MW-107D, and MW-108, plus homeowner well HW-1. A site plan indicating the
facility and waste boundaries in addition to monitoring well locations can be found in Drawing
No. 1.

Four monitoring wells (MW-1, MW-2, MW-3, and MW-4) are monitored for RCRA metals and
NC Appendix I list of volatile organics. The eight remaining wells (MW-105S, MW-105D,
MW-106S, MW-106D, MW-107S, MW-107D, MW-108, and HW-1) are analyzed for NC
Appendix I list of volatile organics only. Monitoring wells MW-105S and MW-105D are also
analyzed for dichlorodifluoromethane.

Monitoring
Well
Date
Installed Classification Monitoring
Program
Total Depth
from TOC (ft)
Lithology of
Screened Interval
MW-1 9/91 Background Detection (.0500) 72.64 Bedrock
MW-2 9/91 Compliance Detection (.0500) 83.30 Bedrock
MW-3 8/89 Compliance Detection (.0500) 19.80 Saprolite
Continued Next Page
First Semiannual Groundwater Monitoring Report of 2016 Joyce Engineering
Transylvania County Calvert Landfill, Permit No. 88-03 July 2016
2
Monitoring
Well
Date
Installed Classification Monitoring
Program
Total Depth
from TOC (ft)
Lithology of
Screened Interval
MW-4 8/89 Compliance Detection (.0500) 70.80 Bedrock
MW-105S 7/97 Compliance Detection (.0500) 55.37 Saprolite
MW-105D 7/97 Compliance Detection (.0500) 87.10 Bedrock
MW-106S 3/10-11/99 Compliance Detection (.0500) 22.58 Saprolite
MW-106D 3/10-11/99 Compliance Detection (.0500) 75.38 Bedrock
MW-107S 3/10-11/99 Compliance Detection (.0500) 58.84 Saprolite
MW-107D 3/10-11/99 Compliance Detection (.0500) 90.30 Bedrock
MW-108 3/10-11/99 Compliance Detection (.0500) 108.44 Bedrock
HW-1 Not Avail. Compliance Detection (.0500) Not Avail. Bedrock (Estimated)

2.2 Surface Water Monitoring Program

Surface water monitoring at the Calvert Landfill is completed in accordance with Rule .0602 and
samples are collected semiannually. The one surface water monitoring point comprises the
surface water monitoring program for the Calvert Landfill and includes analysis for RCRA
metals and NC Appendix I list of volatile organics. Surface water point SMP-1 is located to
monitor water quality shortly before it enters Galloway Creek offsite.

Surface Point Classification Monitoring Program
SMP-1 Compliance Surface Water

3.0 FIRST SEMIANNUAL SAMPLING EVENT OF 2016

3.1 Field Work and Visual Inspection

In order to detect potential releases of leachate and/or landfill gas migration in a timely manner,
a visual inspection program has been implemented at the Calvert Landfill. This inspection
program involves field personnel making the following observations of negative changes around
the waste facility:

 Observation of stress induced on the biological community (i.e., dead or dying vegetation),
 Indications of leachate impact (i.e., seeps, impacted surface water), and
 Observations of erosion.

On April 26, 2016 personnel from Joyce Engineering (JOYCE) visited Calvert Landfill to purge
and sample monitoring wells MW-1, MW-2, MW-3, MW-105S, MW-105D, MW-106S, MW-
106D, MW-107S, MW-107D, and MW-108, including homeowner well HW-1. The area around
MW-4 was flooded and was not sampled. SMP-1 was dry and was not sampled during the April
2016 sampling event. Depth-to-water measurements were obtained to the nearest 0.01 foot using
an electronic water level indicator for all monitoring wells in the compliance network prior to
purging. Groundwater elevations can be found in Table 1.

Monitoring wells were purged and sampled using either a 12 volt pump or disposable bailers
while the homeowner well was purged by spigot for 15 minutes. Measurements of temperature,
pH, specific conductivity, and turbidity were recorded in the site specific log book prior to
First Semiannual Groundwater Monitoring Report of 2016 Joyce Engineering
Transylvania County Calvert Landfill, Permit No. 88-03 July 2016
3
purging, after each purge volume, and during sampling. Prior to sampling, laboratory-supplied
containers were prepared with the following information:

 Monitoring well number (completed by field personnel),
 Date and time of sample collection (completed by field personnel),
 Initials of sampling personnel (completed by field personnel),
 Project name and number (completed by the laboratory),
 Chemical preservative (completed by the laboratory); and
 Requested chemical analysis (completed by the laboratory).

Groundwater samples from each monitoring well were collected directly from the 12 volt pump
or disposable bailers in the provided laboratory containers either immediately after purging or
within 24 hours of the final purge volume. Immediately after collection, the samples were
placed on ice in a laboratory provided cooler. Field forms are provided in the Appendix 1.

When not dry, a surface water sample (SMP-1), is collected directly from stream by lowering the
prepared sample containers into the stream flow with the opening facing into the current. Care is
taken not to overflow the sample containers (which could lead to preservative loss) and to avoid
sample-induced turbidity. At the time of sampling, surface water is also measured for
temperature, pH, specific conductivity, and turbidity and the readings were recorded in the site
specific log book. After sample collection, the sample was placed on ice in a laboratory
provided cooler.

3.2 Laboratory Analysis and JOYCE Quality Control

The April 2016 groundwater samples were submitted to Pace Analytical Services, Inc. of
Asheville, North Carolina under chain-of-custody control for analysis. JOYCE requested a
Level II data report for the final laboratory report. The samples were received by the laboratory
on April 28, 2016 in good condition, properly preserved, and within analysis hold times.

In addition to samples collected for compliance monitoring at the Calvert Landfill, a Field Blank
was collected by JOYCE personnel as part of the April 2016 sampling event. A Trip Blank
prepared by the laboratory was to accompany the volatile sampling containers from the
laboratory to the field and back to the laboratory. The Field Blank was analyzed for the eight
RCRA metals and NC Appendix I list of volatile organic compounds plus dichloro-
difluoromethane while the Trip Blank was analyzed for NC Appendix I volatile organic
compounds plus dichlorodifluoromethane.

Upon receipt of the laboratory data packages, the data was reviewed by JOYCE personnel for the
following:

 Typographical errors,
 Correct analyses performed and within method specified hold times,
 Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike Duplicate,
and Laboratory Control Samples,
 Blank qualified data (B-flags),
First Semiannual Groundwater Monitoring Report of 2016 Joyce Engineering
Transylvania County Calvert Landfill, Permit No. 88-03 July 2016
4
 Detections above the NC 2L Groundwater Standards (NC2L), Groundwater Water Protection
Standards (GWPS), NC 2B Surface Water Standards, and
 Detections that are above historical levels.

No questions or problems were discovered based on the review to warrant laboratory
notification.

4.0 DATA ANALYSIS

Final results from the April 2016 sampling event were received May 9, 2016, from Pace
Analytical Services, Inc. and are found in Appendix 1. There were two quantified detections
above the NC 2L or GWPS in compliance monitoring wells.

4.1 Inorganic Analytical Results and Comparisons to Standards

As presented in Table 2, no inorganic constitutes were detected above its Solid Waste Section
Reporting Limit (SWSL) or Groundwater Protection Standards (GPS) during the April 2016
sampling event. Historical inorganic constituent data can be found in Table 2.

4.2 Organic Analytical Results and Comparisons to Standards

The following organic constituents were detected at quantified concentrations during the April
2016 sampling event. All concentrations are reported in micrograms per liter (µg/L).
Concentrations with a “J” are considered to be estimated. Concentrations with a “B” are
considered to be attributed to lab or field contamination. Highlighted data are concentrations
reported above the NC 2L.

Constituent NC 2L/
{NC 2B}
Background Downgradient
MW-1 MW-2 MW-3 MW-4 MW-
105S
MW-
105D
MW-
106S
Benzene 1 {51} ND 0.44 J 0.90 NS 0.75 J 1.8 ND
Chlorobenzene 50 {488} ND 0.37 J 11.6 NS 2.6 J 11.2 ND
1,4-Dichlorobenzene 6 {488} ND 0.35 J 13.2 NS 2.2 4.9 ND
Cis-1,2-Dichloroethylene 70 {NE} ND 0.84 J 0.96 J NS 0.62 J 9.7 ND
Chloromethane 3 {NE} ND ND 0.19 J NS 1.00 ND ND

Constituent NC 2L/
{NC 2B}
Downgradient
HW-1 SMP-1 Blanks MW-
106D
MW-
107S
MW-
107D
MW-
108
Benzene 1 {51} ND ND 0.57 J 0.54 J ND Dry ND
Chlorobenzene 50 {488} 4.0 ND 0.73 J 0.48 J ND Dry ND
1,4-Dichlorobenzene 6 {488} 4.0 ND 0.87 J 1.8 ND Dry ND
Cis-1,2-Dichloroethylene 70 {NE} 2.3 J ND 0.43 J 2.2 J ND Dry ND
Chloromethane 3 {NE} ND ND ND ND ND Dry ND

1. ND = Not detected above laboratory detection limits. 2. NC 2B are surface water standards. 3. NE = Not established.
4. NS = Not sampled 5. Dry = Dry and not sampled

First Semiannual Groundwater Monitoring Report of 2016 Joyce Engineering
Transylvania County Calvert Landfill, Permit No. 88-03 July 2016
5

There were two quantified organic detection above the NC2L. 1,4-dichlorobenzene was detected
above its NC2L in MW-3 and benzene was detected above its NC 2L in MW-105D during the
April 2016 monitoring event. No other organic constituents were detected above their NC 2L. In
general, the results are consistent with historical data. Historical volatile organic data can be
found in Table 3.

5.0 CONCLUSION

Based on a comparison to historical groundwater data, the April 2016 sampling event results are
generally consistent with previous events. The Transylvania County Calvert Landfill will
continue monitoring groundwater in accordance with Detection Monitoring Program for Rule
.0500 sites, while surface water will be monitored in accordance with Rule .0602. The next
semiannual monitoring event is tentatively scheduled for October 2016.

6.0 REFERENCES

Joyce Engineering, Inc., November 3, 1997. Monitoring Well Installation and Analysis.
Prepared for Transylvania County Solid Waste.

Joyce Engineering, Inc., March 13, 1998. Water Quality Assessment Plan. Prepared for
Transylvania County Solid Waste.

Joyce Engineering, Inc., December 13, 1999. Water Quality Assessment Plan. Prepared for
Transylvania County Solid Waste.

Horton, J.W., 1982, Geologic Map and Mineral Resources Summary of the Rosman Quadrangle,
North Carolina; North Carolina Geological Survey Geologic Map 185-NE, North Carolina
Department of Natural Resources and Community Development/Division of Land Resources.

North Carolina Dept. Environment, Health, and Natural Resources (NCDEHNR), 1995, N.C.
Water Quality Monitoring Guidance Document for Solid Waste Facilities.

North Carolina Department of Environment and Natural Resources, 1990-2011, Solid Waste
Management Regulations.

RCRA Ground Water Monitoring Technical Enforcement Guidance Document (TEGD), 1986.

U.S. Geological Survey. 1990 photo revision. Rosman, North Carolina Quadrangle, 7.5-minute
series (topographic); scale 1:24,000.

Tables

Table 1 Summary of Historical Groundwater Elevations
Table 2 Summary of Historical Inorganic Constituents
Table 3 Summary of Historical Organic Constituents
Table 4 Horizontal Groundwater Flow Velocities

TABLE 1
SUMMARY OF HISTORICAL GROUNDWATER ELEVATIONS
Background
MW-1 MW-2 MW-3 MW-4 MW-105S MW-105D MW-106S MW-106D MW-107S MW-107D MW-108
TOC Elevation 2306.09 2282.67 2210.21 2327.55 2270.55 2270.76 2197.12 2197.62 2272.79 2273.57 2334.28
Well Depth 72.64 83.30 19.80 70.80 55.37 87.10 22.58 75.38 58.84 90.30 108.44
Apr-04 2247.91 2222.67 2206.71 2262.90 2221.10 2213.05 2189.04 2195.45 2226.79 2220.72 2241.45
Oct-04 2249.13 2223.92 2206.56 2263.54 2220.87 2213.52 2188.37 2195.53 2230.31 2222.54 2242.48
12-Apr-05 2249.57 2224.20 2206.98 2263.64 2221.25 2213.74 2188.27 2195.80 2229.03 2222.32 2243.18
12-Oct-05 2246.09 2223.55 2206.37 2263.36 2224.84 2214.42 2187.93 2190.04 2225.76 2219.39 2241.49
19-Apr-06 2244.98 2219.75 2205.99 2262.41 2221.94 2213.06 2187.89 2194.01 2225.45 2219.82 2238.59
18-Oct-06 2242.96 2214.17 2206.11 2257.55 2217.79 2210.70 2188.18 2194.79 2219.28 2218.08 2227.28
24-Apr-07 2249.70 2220.75 2206.24 2263.33 2219.77 2212.41 2188.22 2195.08 2227.87 2220.06 2240.83
16-Oct-07 2237.99 2212.65 2203.92 2257.88 2216.54 2209.01 2187.64 2193.21 2217.58 2216.78 2231.38
22-Apr-08 2249.09 2215.83 2205.90 2262.48 2218.19 2210.90 2188.09 2195.02 2227.05 2219.87 2233.70
22-Oct-08 2238.71 2211.72 2203.79 2257.83 2216.49 2208.42 2187.66 2193.07 2216.98 2216.75 2231.52
15-Apr-09 2253.04 2214.58 2206.25 2257.60 Dry 2210.39 2188.39 2194.67 2222.71 2219.28 2231.53
13-Oct-09 2251.18 2217.12 2206.31 2260.81 2218.47 2211.71 2188.14 2190.57 2222.66 2220.27 2234.87
21-Apr-10 2253.34 2227.89 2207.06 2265.05 2224.69 2215.03 2188.36 2196.17 2232.68 2223.82 2246.63
27-Oct-10 2239.70 2218.56 2206.00 2259.86 2220.57 2212.24 2188.20 2194.54 2219.88 2218.33 2232.70
18-Apr-11 2253.12 2222.40 2207.27 2263.37 2220.62 2213.59 2188.84 2196.32 2232.54 2222.49 2238.39
03-Oct-11 2242.75 2217.72 2205.56 2259.72 2219.14 2211.59 2188.31 2194.25 2213.95 2218.42 2232.28
02-Apr-12 2249.85 2218.27 2207.26 2262.91 2220.30 2213.66 2188.52 2195.67 2228.54 2221.02 2236.69
01-Oct-12 2248.51 2219.12 2206.92 2260.37 2219.67 2213.17 2188.43 2194.38 2222.36 2219.54 2233.75
22-Apr-13 2251.88 2223.13 2207.41 2263.20 2223.05 2217.26 2188.72 2195.30 2230.89 2222.07 2239.78
21-Oct-13 2249.19 2225.45 2207.31 2263.20 2222.97 2215.48 2188.36 2195.17 2228.24 2221.60 2241.73
21-Apr-14 2250.79 2225.63 2207.73 2263.37 2222.83 2216.06 2189.22 2195.62 2230.26 2222.20 2241.31
06-Oct-14 2239.05 2219.67 2206.39 2260.41 2220.35 2213.86 2188.52 2193.93 2221.51 2218.87 2233.28
20-Apr-15 2240.91 2219.07 2207.45 ---2220.53 2214.01 2189.43 2193.52 2226.63 2220.42 2232.67
19-Oct-15 2242.29 2215.32 2206.46 ---2219.40 2213.11 2188.92 2194.92 2220.95 2219.02 2231.78
26-Apr-16 2248.89 2225.97 2207.41 ---2224.75 2216.66 2189.21 2195.22 2230.29 2222.87 2241.28
Notes:
1. All elevations are referenced as feet above mean sea level.
2. All depths measured in feet (ft).
3. Dry = Monitoring well considered to be dry with no measureable water.
Well I.D.Downgradient
Transylvania County Calvert Landfill Joyce Engineering
TABLE 2
SUMMARY OF HISTORICAL INORGANIC CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 MW-4 SMP-1 Field Blank
INORGANICS
Arsenic 04/22/10 2.7 10.0 3.40 B 7.40 B 9 B 5.8 B 3.20 B 4.00 J
NC 2L = 10 µg/L (01/01/10)10/27/10 2.7 10.0 3.00 J 10.2 4.9 J ND ND ND
NC 2B = 10 µg/L (05/01/07)04/18/11 2.7 10.0 ND ND ND ND ND ND
10/03/11 5.0 10.0 ND ND ND ND ---ND
04/02/12 5.0 10.0 ND 7.20 J ND ND ND ND
10/01/12 5.0 10.0 ND 6.70 J ND ND ND ND
04/22/13 5.0 10.0 ND ND ND ND ND ND
10/21/13 5.0 10.0 ND ND ND ND ND ND
04/21/14 5.0 10.0 ND ND ND ND ND ND
10/06/14 5.0 10.0 ND 18.7 ND ND ---ND
04/20/15 5.0 10.0 ND 9.0 J ND ---ND ND
10/19/15 2.5 10.0 ND ND ND ------ND
04/26/16 2.5 10.0 ND ND ND ------ND
Barium 04/22/10 0.2 100.0 77.9 B 148 67.8 B 31.4 B 150.0 25.50 J
NC 2L = 700 µg/L (01/01/10)10/27/10 0.2 100.0 83.4 J 88.1 J 71 J 32 J 44.2 J ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.2 100.0 78.3 J 88.8 J 72.8 J 19.1 B 130.0 13.40 J
10/03/11 5.0 100.0 91.0 J 95.6 J 80.7 J 33.5 J ---ND
04/02/12 5.0 100.0 102 109 75.7 J 20 J 178.0 ND
10/01/12 5.0 100.0 73.5 J 83.8 J 91.9 J 30.8 J 122.0 ND
04/22/13 5.0 100.0 67.7 J 92.3 J 79.5 J 27.7 J 93.3 J ND
10/21/13 5.0 100.0 67.0 J 125 97.5 J 34.2 J ---ND
04/21/14 5.0 100.0 67.5 J 126 88.6 J 22.5 J 68.9 J 36.10 J
10/06/14 5.0 100.0 51.9 J 165 80.3 J 18.8 J ---ND
04/20/15 5.0 100.0 53.8 J 90.8 J 80.0 J ---39.3 J ND
10/19/15 2.5 100.0 76.7 J 80.8 J 80.5 J ------ND
04/26/16 2.5 100.0 72.3 J 138.0 84.9 J ------ND
Cadmium 04/22/10 0.5 1.0 ND ND ND ND ND ND
NC 2L = 2 µg/L (01/01/10)10/27/10 0.5 1.0 ND ND ND ND ND ND
NC 2B = 2 µg/L (05/01/07)04/18/11 0.5 1.0 0.70 J ND ND ND ND ND
10/03/11 1.0 1.0 1.50 ND ND ND ---ND
04/02/12 1.0 1.0 ND 2.20 ND ND ND ND
10/01/12 1.0 1.0 ND ND ND ND ND ND
04/22/13 1.0 1.0 ND ND ND ND ND ND
10/21/13 1.0 1.0 ND ND 1.5 ND ND ND
04/21/14 1.0 1.0 ND ND ND ND ND ND
10/06/14 1.0 1.0 ND ND ND ND ---ND
04/20/15 1.0 1.0 0.68 J 0.57 J ND ---ND ND
10/19/15 0.5 1.0 1.9 ND ND ------ND
04/26/16 0.5 1.0 0.61 J ND ND ------ND
Chromium 04/22/10 0.4 10.0 ND 2.90 J 0.75 J ND ND ND
NC 2L = 10 µg/L (01/01/10)10/27/10 0.4 10.0 1.50 J ND 0.71 J ND ND ND
NC 2B = 50 µg/L (05/01/07)04/18/11 0.4 10.0 ND ND 1.2 J ND ND ND
10/03/11 5.0 10.0 ND ND ND ND ---ND
04/02/12 5.0 10.0 ND ND ND ND ND ND
10/01/12 5.0 10.0 ND ND ND ND ND ND
04/22/13 5.0 10.0 ND ND ND ND ND ND
10/21/13 5.0 10.0 ND ND ND ND ND ND
04/21/14 5.0 10.0 ND ND ND ND ND ND
10/06/14 5.0 10.0 ND ND ND ND ---ND
04/20/15 5.0 10.0 ND ND ND ---ND ND
10/19/15 2.5 10.0 4.7 J 3.4 J 3.0 J ------ND
04/26/16 2.5 10.0 3.1 J 2.8 J ND ------ND
Transylvania County Calvert Landfill Page 1 of 3 Joyce Engineering
TABLE 2
SUMMARY OF HISTORICAL INORGANIC CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 MW-4 SMP-1 Field Blank
Lead 04/22/10 4.0 10.0 ND ND ND 8.6 J ND ND
NC 2L = 15 µg/L (10/23/07)10/27/10 4.0 10.0 7.9 J ND ND 6 J ND ND
NC 2B = 25 µg/L (05/01/07)04/18/11 4.0 10.0 ND 4.10 J ND ND ND ND
10/03/11 5.0 10.0 5.9 J ND ND 20.7 ---ND
04/02/12 5.0 10.0 9.4 J 9.10 J ND ND ND ND
10/01/12 5.0 10.0 ND 5.10 J 5.4 J 17.8 ND ND
04/22/13 5.0 10.0 ND ND ND ND ND ND
10/21/13 5.0 10.0 ND ND ND 7.9 J ND ND
04/21/14 5.0 10.0 ND ND 5.8 J ND ND ND
10/06/14 5.0 10.0 ND ND ND ND ---ND
04/20/15 5.0 10.0 ND 4.5 J ND ---ND ND
10/19/15 2.5 10.0 7.5 J 3.9 J ND ------ND
04/26/16 2.5 10.0 3.9 J 4.5 J 3.7 J ------ND
Mercury 04/22/10 0.07 0.20 ND ND ND ND ND ND
NC 2L = 1 µg/L (01/01/10)10/27/10 0.07 0.20 ND ND ND ND ND ND
NC 2B = 0.012 µg/L (05/01/07)04/18/11 0.10 0.20 ND ND ND ND ND ND
10/03/11 0.10 0.20 ND ND ND ND ---ND
04/02/12 0.10 0.20 ND ND ND ND ND ND
10/01/12 0.10 0.20 ND ND ND ND ND ND
04/22/13 0.10 0.20 ND ND ND ND ND ND
10/21/13 0.10 0.20 ND ND ND ND ND 0.16 J
04/21/14 0.10 0.20 ND ND ND ND ND ND
10/06/14 0.10 0.20 ND ND ND ND ---ND
04/20/15 0.10 0.20 ND ND ND ---ND
10/19/15 0.10 0.20 ND ND ND ------ND
04/26/16 0.10 0.20 ND ND ND ------ND
Selenium 04/22/10 3.8 10.0 5.30 J ND ND ND ND ND
NC 2L = 20 µg/L (01/01/10)10/27/10 3.8 10.0 ND ND ND ND ND 4.60 J
NC 2B = 5 µg/L (05/01/07)04/18/11 3.8 10.0 ND ND ND ND ND ND
10/03/11 10.0 10.0 ND ND ND ND ---ND
04/02/12 10.0 10.0 ND ND ND ND ND ND
10/01/12 10.0 10.0 ND ND ND ND ND ND
04/22/13 10.0 10.0 ND ND ND ND ND ND
10/21/13 10.0 10.0 ND ND ND ND ND ND
04/21/14 10.0 10.0 ND ND ND ND ND ND
10/06/14 10.0 10.0 ND ND ND ND ---ND
04/20/15 10.0 10.0 ND ND ND ---ND ND
10/19/15 5.0 10.0 ND ND ND ------ND
04/26/16 5.0 10.0 ND ND ND ------ND
Transylvania County Calvert Landfill Page 2 of 3 Joyce Engineering
TABLE 2
SUMMARY OF HISTORICAL INORGANIC CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 MW-4 SMP-1 Field Blank
Silver 04/22/10 0.1 10.0 ND ND ND ND ND ND
NC 2L = 20 µg/L (01/01/10)10/27/10 0.1 10.0 ND ND ND ND ND ND
NC 2B = 0.06 µg/L (05/01/07)04/18/11 0.1 10.0 ND ND ND ND ND ND
10/03/11 5.0 10.0 ND ND ND ND ---ND
04/02/12 5.0 10.0 ND ND ND ND ND ND
10/01/12 5.0 10.0 ND ND ND ND ND ND
04/22/13 5.0 10.0 ND ND ND ND ND ND
10/21/13 5.0 10.0 ND ND ND ND ND ND
04/21/14 5.0 10.0 ND ND ND ND ND ND
10/06/14 5.0 10.0 ND ND ND ND ---ND
04/20/15 5.0 10.0 ND ND ND ---ND ND
10/19/15 2.5 10.0 ND 4.3 J ND ------ND
04/26/16 2.5 10.0 ND ND ND ------ND
Notes:
QL = Quantiation Limit
ND = Not detected at or above the detection or reporting limit.
J = Estimated value since the concentration is between the DL and the SWSL.
--- = Not sampled and or Not Reported
DL = Laboratory detection limit.
NC 2L = North Carolina's groundwater quality standard established under 15A NCAC 2L, .0202.
NC 2B = North Carolina 2B Surface Water Standards. The surface water at the sampling location is classified as Class C.
NC 2B Standard is used to define concentration limits for surface water constituents.
Bold concentrations are greater than the NC 2L for groundwater or NC 2B for surface water.
NE = Not established.
NV= Values considered to be not valid due to laboratory exceeding hold times for analysis
All historical data prior to April 2010 is avaliable upon request
Transylvania County Calvert Landfill Page 3 of 3 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL ORGANIC CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 MW-4 MW-105S MW-105D MW-106S MW-106D MW-107S MW-107D MW-108 HW-1 SMP-1 Field BlankOrganic Compounds
Acetone 04/22/10 2.2 100 ND ND ND 13.9 J 13.90 J ND ND ND 11.30 J ND 44.3 J ND ND ND
NC 2L = 6,000 µg/L (01/01/10) 10/27/10 2.2 100 3.00 B 2.40 B ND 248 5.90 B 9.70 B ND 2.5 B 8.10 B 4.20 B 28.7 B ND 2.90 B 4.50 J
NC 2B = NE µg/L (05/01/07)04/18/11 2.2 100 3.00 B ND ND 4.7 B 3.00 B ND ND ND 6.70 B 2.30 B 11.5 B ND 3.50 B 3.30 J10/03/11 2.2 100 ND ND ND 612 ND ND ND ND 5.00 J 4.10 J ND ND ---ND
04/02/12 2.2 100 ND ND ND 526 ND ND ND ND 11.10 J ND ND ND ND ND
10/01/12 10 100 ND ND ND 46.1 J ND ND ND ND ND ND ND ND ND ND
04/22/13 10 100 ND ND ND ND ND ND ND ND ND ND 21.5 B ND ND 38.6 J10/21/13 10 100 ND ND ND ND ND ND ND ND ND ND 71.6 J ND ND ND
04/21/14 10 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/06/14 10 100 ND ND ND 29.8 J ND ND ND ND ND ND ND ND ---ND
04/20/15 10 100 ND ND ND ---ND ND ND ND ND ND ND ND ND 10.0 J10/19/15 10 100 ND ND ND ---ND ND ND ND ND ND 19.8 J ND ---ND
04/26/16 10 100 ND ND 17.3 J ---ND ND ND ND ND ND 61.1 J ND ---ND
Benzene 04/22/10 0.25 1.0 ND 0.64 J 1.7 1.3 1.20 1.00 ND 0.48 J ND 0.97 J 0.69 J ND ND NDNC 2L = 1 µg/L (10/23/07)10/27/10 0.25 1.0 ND 0.75 J 1.3 0.85 J 0.93 J ND ND 0.45 J ND 0.46 J 0.51 J ND ND ND
NC 2B = 51 µg/L (05/01/07)04/18/11 0.25 1.0 ND 0.66 J 1.5 0.95 J 0.89 J 1.1 ND 0.47 J ND 0.64 J 0.47 J ND ND ND
10/03/11 0.25 1.0 ND 1.10 1.1 ND 0.89 J 1.3 ND 0.51 J ND 0.49 J 0.53 J ND ---ND
04/02/12 0.25 1.0 ND 0.59 J 1.2 1.2 0.81 J 1.3 ND ND ND ND ND ND ND ND10/01/12 0.25 1.0 ND 0.85 J 1.1 0.7 J 0.87 J 1.4 ND 0.44 J ND 0.51 J 0.47 J ND ND ND
04/22/13 0.25 1.0 ND 0.71 J 1.3 1.1 1.1 1.6 ND 0.4 J ND 0.94 J 0.66 J ND ND ND
10/21/13 0.25 1.0 ND 0.70 J 0.8 J 1.1 1.0 1.8 ND 0.31 J ND 0.64 J 0.52 J ND ND ND
04/21/14 0.25 1.0 ND 0.64 J 0.88 J 1.1 1.0 1.9 ND 0.33 J ND 0.71 J 0.52 J ND ND ND10/06/14 0.25 1.0 ND 0.48 J 0.68 J 0.98 J 0.83 J 1.9 ND 0.42 J ND 0.61 J ND ND ---ND04/20/15 0.25 1.0 ND 0.53 J 0.92 J ---0.57 J 0.92 J ND ND ND 0.41 J ND ND ND ND
10/19/15 0.25 1.0 ND 0.68 J 1.1 ---0.80 J 2.2 ND 0.40 J ND 0.49 J 0.39 J ND ---ND
04/26/16 0.25 1.0 ND 0.44 J 0.90 J ---0.75 J 1.8 ND ND ND 0.57 J 0.54 J ND ---ND
Carbon Disulfide 04/02/12 1.2 100.0 ND ND ND ND ND ND ND ND 1.80 J ND ND ND ND ND
NC 2L = 700 µg/L (10/23/07)10/01/12 1.2 100.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)04/22/13 1.2 100.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/21/13 1.2 100.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND04/21/14 1.2 100.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/06/14 1.2 100.0 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 1.2 100.0 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 1.2 100.0 ND ND ND ---ND ND ND ND ND ND ND ND ---ND04/26/16 1.2 100.0 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Chlorobenzene 04/22/10 0.23 3.00 ND 0.37 J 10.2 3.9 3.00 10.60 0.76 J 5.2 ND 1.40 J ND ND ND ND
NC 2L = 50 µg/L (10/23/07)10/27/10 0.23 3.00 ND 0.92 J 10.6 5.2 2.60 J 2.40 J 1.7 J 6.9 ND 0.89 J 0.59 J ND ND NDNC 2B = 488 µg/L (05/01/07)04/18/11 0.23 3.00 ND 0.63 J 11 3.2 2.40 J 8.60 0.42 J 6.3 0.27 J 1.10 J 0.4 J ND ND ND
10/03/11 0.23 3.00 ND 1.10 J 12.1 4.7 2.60 J 8.30 0.76 J 7.9 ND 0.77 J 0.63 J ND ---ND
04/02/12 0.23 3.00 ND 0.50 J 10.6 3.3 2.60 J 8.00 0.24 J 5.9 ND 0.89 J 0.75 J ND ND ND
10/01/12 0.23 3.00 ND 0.87 J 11.5 2.8 J 2.60 J 7.80 ND 7.1 ND 0.83 J 0.62 J ND ND ND04/22/13 0.2 3.0 ND 0.52 J 11.4 2.6 J 2.70 J 8.50 0.55 J 6.6 ND 1.20 0.5 J ND ND ND
10/21/13 0.2 3.0 ND 0.55 J 11.9 3.1 2.90 J 10.10 ND 4.9 ND 0.92 J 0.3 J ND ND ND
04/21/14 0.2 3.0 ND 0.51 J 13.7 3.5 2.7 J 10.0 ND 5.5 ND 1.0 J 0.34 J ND ND ND
10/06/14 0.2 3.0 ND 0.49 J 12.1 3.1 2.8 J 8.0 0.26 J 6.8 ND 0.88 J 0.58 J ND ---ND04/20/15 0.2 3.0 ND 0.59 J 10.7 ---2.3 J 6.0 ND ND ND 0.74 J 0.66 J ND ND ND
10/19/15 0.2 3.0 ND 0.59 J 10.8 ---2.6 J 12.2 ND 6.3 ND 0.61 J 0.56 J ND ---ND
04/26/16 0.2 3.0 ND 0.37 J 11.6 ---2.6 J 11.2 ND 4.0 ND 0.73 J 0.48 J ND ---ND
Chloroethane 04/22/10 0.54 10.0 ND ND ND ND ND ND ND ND ND 1.90 J ND ND ND ND
NC 2L = 3,000 µg/L (01/01/10) 10/27/10 0.54 10.0 ND ND ND 1.9 J ND ND ND ND ND ND 1.1 J ND ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.54 10.0 ND ND ND 2.4 J ND ND ND ND ND 1.20 J 1.7 J ND ND ND
10/03/11 0.54 10.0 ND ND ND 1.9 J ND ND ND ND ND 0.95 J 1.3 J ND ---ND
04/02/12 0.54 10.0 ND ND ND 2.9 J ND ND ND ND ND ND 2.3 J ND ND ND10/01/12 0.54 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/22/13 0.54 10.0 ND ND ND ND ND ND ND ND ND ND 0.98 J ND ND ND
10/21/13 0.54 10.0 ND ND ND 1.1 J ND ND ND ND ND 0.71 J 0.66 J ND ND ND
04/21/14 0.54 10.0 ND ND ND 1.6 J ND ND ND ND ND 0.92 J ND ND ND ND10/06/14 0.54 10.0 ND ND ND 1.5 J ND ND ND ND ND ND 0.96 J ND ---ND
04/20/15 0.54 10.0 ND ND ND ---ND ND ND ND ND 0.80 J ND ND ND ND
10/19/15 0.54 10.0 ND ND ND ---ND ND ND ND ND 0.75 J 1.2 J ND ---ND
04/26/16 0.54 10.0 ND ND ND ---ND ND ND ND ND ND 0.77 J ND ---ND
Transylvania County Calvert Landfill Page 1 of 7 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL ORGANIC CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 MW-4 MW-105S MW-105D MW-106S MW-106D MW-107S MW-107D MW-108 HW-1 SMP-1 Field BlankChloroform04/22/10 0.14 5.00 ND ND ND ND ND ND ND ND ND ND ND 1.6 J ND ND
NC 2L = 70 µg/L (10/23/07) 10/27/10 0.14 5.00 ND ND ND ND ND ND ND ND ND ND ND 0.52 J ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.14 5.00 ND ND ND ND ND ND ND ND ND ND ND 3.2 J ND ND
10/03/11 0.14 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND04/02/12 0.14 5.00 ND ND ND ND ND ND ND ND ND ND ND 1.8 J ND ND
10/01/12 0.14 5.00 ND ND ND ND ND ND ND ND ND ND ND 0.97 J ND ND
04/22/13 0.14 5.00 ND ND ND ND ND ND ND ND ND ND ND 2.7 J ND ND
10/21/13 0.14 5.00 ND ND ND ND ND ND ND ND ND ND ND 1.1 J ND ND04/21/14 0.14 5.00 ND ND ND ND ND ND ND ND ND ND ND 0.72 J ND ND
10/06/14 0.14 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 0.14 5.00 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.14 5.00 ND ND ND ---ND ND ND ND ND ND ND 0.56 J ---ND04/26/16 0.14 5.00 ND ND ND ---ND ND ND ND ND ND ND 0.79 J ---ND
Chloromethane 04/22/10 0.11 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 3 µg/L (01/01/10) 10/27/10 0.11 1.00 ND ND ND ND ND ND ND ND ND ND ND 0.13 B ND 0.19 JNC 2B = NE µg/L (05/01/07)04/18/11 0.11 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/03/11 0.11 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/02/12 0.11 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/01/12 0.11 1.0 0.19 J ND ND ND ND ND ND ND ND ND ND ND ND ND04/22/13 0.11 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/21/13 0.11 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/21/14 0.11 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/06/14 0.11 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND04/20/15 0.11 1.00 ND ND ND ---ND ND ND ND ND ND ND ND ND ND10/19/15 0.11 1.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
04/26/16 0.11 1.00 ND ND 0.19 J ---1.00 ND ND ND ND ND ND ND ---ND
1,2-Dichlorobenzene 04/22/10 0.3 5.00 ND ND 0.79 J ND ND ND ND 0.39 J ND ND ND ND ND NDNC 2L = 20 µg/L (01/01/10) 10/27/10 0.3 5.00 ND ND 0.8 J ND ND ND ND 0.46 J ND ND ND ND ND ND
NC 2B = 488 µg/L (05/01/07)04/18/11 0.3 5.00 ND ND 0.74 J ND ND ND ND 0.41 J ND ND ND ND ND ND
10/03/11 0.3 5.00 ND ND 0.95 J ND ND ND ND 0.48 J ND ND ND ND ---ND
04/02/12 0.3 5.00 ND ND 0.75 J ND ND ND ND ND ND ND ND ND ND ND10/01/12 0.3 5.00 ND ND 0.79 J ND ND ND ND 0.38 J ND ND ND ND ND ND
04/22/13 0.3 5.00 ND ND 0.79 J ND ND ND ND 0.41 J ND ND ND ND ND ND
10/21/13 0.3 5.00 ND ND 0.82 J ND ND ND ND ND ND ND ND ND ND ND
04/21/14 0.3 5.00 ND ND 0.89 J ND ND ND ND 0.30 J ND ND ND ND ND ND10/06/14 0.3 5.00 ND ND 0.82 J ND ND ND ND 0.36 J ND ND ND ND ---ND
04/20/15 0.3 5.00 ND ND 0.73 J ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.3 5.00 ND ND 0.75 J ---ND ND ND 0.37 J ND ND ND ND ---ND
04/26/16 0.3 5.00 ND ND 0.79 J ---2.3 J ND ND ND ND ND ND ND ---ND
1,4-Dichlorobenzene 04/22/10 0.3 1.0 ND 0.34 J 15.2 2.2 4.3 6.1 1.2 6.2 ND 1.8 1.6 ND ND ND
NC 2L = 6 µg/L (01/01/10) 10/27/10 0.3 1.0 ND 1.10 15.3 2.9 4.0 1.9 2.4 7.7 ND 1.5 1.3 ND ND ND
NC 2B = 488 µg/L (05/01/07)04/18/11 0.3 1.0 ND 0.62 J 14.5 3.2 2.7 5.8 0.71 J 6.5 ND 1.5 1.9 ND ND ND10/03/11 0.3 1.0 ND 1.30 14.7 2.6 3.1 5.9 1.2 7.8 ND 1.30 1.7 ND ---ND
04/02/12 0.3 1.0 ND ND 13.8 3 2.9 5.4 0.58 J 6.3 ND 1.30 2.1 ND ND ND
10/01/12 0.3 1.0 ND 0.9 J 14.2 2.3 2.7 5.6 0.72 J 7.1 ND 1.20 1.6 ND ND ND
04/22/13 0.3 1.0 ND 0.5 J 13.8 2.9 2.3 5.0 0.93 J 7.0 ND 1.40 3.2 ND ND ND10/21/13 0.3 1.0 ND 0.5 J 13.5 2.1 2.5 5.8 0.35 J 5.1 ND 1.20 1.8 ND ND ND
04/21/14 0.3 1.0 ND 0.5 J 14.1 2.2 2.5 5.1 0.37 J 5.5 ND 1.20 1.2 ND ND ND
10/06/14 0.3 1.0 ND 0.57 J 12.5 2.7 2.7 4.1 0.35 J 6.1 ND 1.20 1.1 ND ---ND
04/20/15 0.3 1.0 ND 0.56 J 12.6 ---2.2 3.4 ND ND ND 0.96 J 0.77 J ND ND ND10/19/15 0.3 1.0 ND 0.61 J 13.1 ---2.4 6.7 ND 5.7 ND 1.1 1.1 ND ---ND
04/26/16 0.3 1.0 ND 0.35 J 13.2 ---2.2 4.9 ND 4.0 ND 0.87 J 1.8 ND ---ND
Transylvania County Calvert Landfill Page 2 of 7 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL ORGANIC CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 MW-4 MW-105S MW-105D MW-106S MW-106D MW-107S MW-107D MW-108 HW-1 SMP-1 Field BlankDichlorodifluoromethane04/22/10 0.21 5.00 ------------0.72 J 1.40 J ---------------------ND
NC 2L = 1,000 µg/L (01/01/10) 10/27/10 0.21 5.00 ------------1.00 J ND ---------------------ND
NC 2B =NE µg/L (05/01/07)04/18/11 0.21 5.00 ------------1.10 J 0.64 J ---------------------ND
10/03/11 0.21 5.00 ------------1.20 J 0.70 J ---------------------ND04/02/12 0.21 5.00 ------------ND ND ---------------------ND
10/01/12 0.21 5.00 ------------2.0 J 0.52 J ---------------------ND
04/22/13 0.21 5.0 ------------2.6 J ND ---------------------ND
10/21/13 0.21 5.00 ------------2.0 J ND ---------------ND ---ND04/21/14 0.21 5.00 ------------2.7 J 0.47 J ---------------------ND
10/06/14 0.21 5.00 ------------1.7 J ND ---------------------ND
04/20/15 0.21 5.00 ------------1.3 J ND ---------------------ND
10/19/15 0.21 5.00 ------------1.5 J 0.82 J ---------------------ND04/26/16 0.21 5.00 ------------1.1 J 0.71 J ---------------------ND
1,1-Dichloroethane 04/22/10 0.32 5.0 ND ND ND 15.5 ND 0.37 J ND 0.37 J ND 2.50 J 1.4 J ND ND ND
NC 2L = 6 µg/L (01/01/10) 10/27/10 0.32 5.0 ND ND 0.39 J 13.3 ND ND 0.42 J 0.4 J ND 1.70 J 3.7 J ND ND NDNC 2B =NE µg/L (05/01/07)04/18/11 0.32 5.0 ND ND ND 10.0 ND 0.41 J ND 0.36 J ND 1.90 J 3.8 J ND ND ND
10/03/11 0.32 5.0 ND ND ND 10.8 ND 0.56 J ND ND ND 1.70 J 3 J ND ---ND
04/02/12 0.32 5.0 ND ND ND 6.6 ND ND ND ND ND 1.30 J 3.2 J ND ND ND
10/01/12 0.32 5.0 ND ND 0.35 J 6.7 ND 0.37 J ND 0.39 J ND 1.20 J 2.6 J ND ND ND04/22/13 0.32 5.0 ND ND ND 9.4 ND ND ND 0.38 J ND 1.60 J 2.7 J ND ND ND
10/21/13 0.32 5.0 ND ND ND 5.9 ND ND ND ND ND 1.00 J 0.61 J ND ND ND
04/21/14 0.32 5.0 ND ND ND 6.2 ND ND ND ND ND 0.99 J 0.81 J ND ND ND
10/06/14 0.32 5.0 ND ND ND 4.7 J ND ND ND ND ND 0.67 J 1.5 J ND ND ND04/20/15 0.32 5.0 ND ND ND ---ND ND ND ND ND 0.78 J 2.3 J ND ND ND10/19/15 0.32 5.0 ND ND ND ---ND ND ND ND ND 0.74 J 1.6 J ND ---ND
04/26/16 0.32 5.0 ND ND ND ---ND ND ND ND ND 0.51 J 0.87 J ND ---ND
1,2-Dichloroethane 04/22/10 0.12 1.00 ND ND ND ND ND 0.49 J ND 0.26 J ND ND ND ND ND NDNC 2L = 0.4 µg/L (01/01/10) 10/27/10 0.12 1.00 ND ND ND ND ND ND ND 0.29 J ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.12 1.00 ND ND 0.34 J ND ND ND ND ND 0.49 J ND ND ND ND ND
10/03/11 0.12 1.00 ND ND ND ND ND 0.34 J ND ND ND ND ND ND ---ND
04/02/12 0.12 1.00 0.18 J ND ND ND ND ND ND ND ND ND ND ND ND ND10/01/12 0.12 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/22/13 0.12 1.00 ND ND ND ND ND 0.29 J ND ND ND ND ND ND ND ND
10/21/13 0.12 1.00 ND ND ND ND ND 0.25 J ND ND ND ND ND ND ND ND
04/21/14 0.12 1.00 ND ND ND ND ND 0.32 J ND 0.17 J ND ND ND ND ND ND10/06/14 0.12 1.00 ND ND ND ND ND 0.15 J ND ND ND ND ND ND ---ND
04/20/15 0.12 1.00 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.24 1.00 ND ND ND ---ND 0.50 J ND 0.29 J ND ND ND ND ---ND
04/26/16 0.24 1.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Transylvania County Calvert Landfill Page 3 of 7 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL ORGANIC CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 MW-4 MW-105S MW-105D MW-106S MW-106D MW-107S MW-107D MW-108 HW-1 SMP-1 Field Blank1,1-Dichloroethene 04/22/10 0.56 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 7 µg/L (10/23/07)10/27/10 0.56 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.56 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/03/11 0.56 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND04/02/12 0.56 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/01/12 0.56 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 350 µg/L (04/01/2013)04/22/13 0.56 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/21/13 0.56 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND04/21/14 0.56 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/06/14 0.56 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 0.56 5.00 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.56 5.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND04/26/16 0.56 5.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Cis-1,2-Dichloroethene 04/22/10 0.19 5.00 ND 1.60 J 1.2 J 10.6 2.50 J 16.90 1.9 J 4.1 J ND 1.20 J 3.6 J ND ND ND
NC 2L = 70 µg/L (10/23/07)10/27/10 0.19 5.00 ND 2.20 J 1.5 J 11.1 2.40 J 5.4 3.1 J 4.1 J ND 1.10 J 2.9 J ND ND NDNC 2B = NE µg/L (05/01/07)04/18/11 0.19 5.00 ND 1.50 J 1.4 J 9.5 1.60 J 18.6 1.4 J 4 J ND 1.10 J 4.6 J ND ND ND
10/03/11 0.19 5.00 ND 2.40 J 1.4 J 10.4 1.70 J 18.4 2.1 J 4.5 J ND 1.00 J 3.5 J ND ---ND
04/02/12 0.19 5.00 ND 1.30 J 0.99 J 7.4 1.20 J 15.8 1.1 J 3.9 J ND 0.69 J 4.8 J ND ND ND
10/01/12 0.19 5.00 ND 1.80 J 1 J 5.7 1.00 J 15.0 1 J 3.7 J ND 0.80 J 3.3 J ND ND ND04/22/13 0.19 5.00 ND 1.40 J 1.1 J 8.6 0.97 J 15.1 1.7 J 4.1 J ND 0.76 J 8 ND ND ND
10/21/13 0.19 5.00 ND 1.10 J 0.97 J 4.7 J 0.83 J 12.1 0.93 J 2.6 J ND 0.71 J 2.2 J ND ND ND
04/21/14 0.19 5.00 ND 1.10 J 1.3 J 4.9 J 0.79 J 12.6 1.0 J 2.8 J ND 0.67 J 2.1 J ND ND ND
10/06/14 0.19 5.00 ND 0.94 J 1.2 J 4.4 J 0.87 J 12.3 1.0 J 3.0 J ND 0.58 J 1.2 J ND ---ND04/20/15 0.19 5.00 ND 0.89 J 0.99 J ---0.78 J 8.9 0.80 2.7 ND 0.58 J 1.2 J ND ND ND10/19/15 0.19 5.00 ND 0.95 J 0.90 J ---0.65 J 13.4 0.91 J 2.5 J ND 0.75 J 1.4 J ND ---ND
04/26/16 0.19 5.00 ND 0.84 J 0.96 J ---0.62 J 9.7 0.76 J 2.3 J ND 0.43 J 2.2 J ND ---ND
Trans-1,2-Dichloroethene 04/22/10 0.49 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND NDNC 2L = 100 µg/L (10/23/07)10/27/10 0.49 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.49 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/03/11 0.49 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/02/12 0.49 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/01/12 0.49 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/22/13 0.49 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/21/13 0.49 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/21/14 0.49 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/06/14 0.49 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 0.49 5.00 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.49 5.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
04/26/16 0.49 5.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Transylvania County Calvert Landfill Page 4 of 7 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL ORGANIC CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 MW-4 MW-105S MW-105D MW-106S MW-106D MW-107S MW-107D MW-108 HW-1 SMP-1 Field Blank1,2-Dichloropropane 04/22/10 0.27 1.00 ND ND 0.41 J ND 0.99 J 1.20 ND 0.58 J ND ND ND ND ND ND
NC 2L = 0.6 µg/L (01/01/10) 10/27/10 0.27 1.00 ND ND ND ND 0.61 J ND 0.27 J 0.56 J ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.27 1.00 ND ND ND ND 0.43 J 1.30 ND 0.54 J ND ND ND ND ND ND
10/03/11 0.27 1.00 ND ND ND ND ND 1.10 ND 0.58 J ND ND ND ND ---ND04/02/12 0.27 1.00 ND ND ND ND ND 1.00 ND ND ND ND ND ND ND ND
10/01/12 0.27 1.00 ND ND 0.41 J ND ND 1.10 ND 0.58 J ND ND ND ND ND ND
04/22/13 0.27 1.00 ND ND ND ND ND 0.92 J ND 0.5 J ND ND ND ND ND ND
10/21/13 0.27 1.00 ND ND 0.39 J ND ND 0.92 J ND 0.41 J ND ND ND ND ND ND04/21/14 0.27 1.00 ND ND ND ND ND 0.86 J ND ND ND ND ND ND ND ND
10/06/14 0.27 1.00 ND ND ND ND ND 0.94 J ND ND ND ND ND ND ---ND
04/20/15 0.27 1.00 ND ND ND ---ND 0.55 J ND ND ND ND ND ND ND ND
10/19/15 0.27 1.00 ND ND ND ---ND 0.99 J ND 0.37 J ND ND ND ND ---ND04/26/16 0.27 1.00 ND ND ND ---ND 0.64 J ND ND ND ND ND ND ---ND
Ethylbenzene 04/22/10 0.3 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 600 µg/L (01/01/10)10/27/10 0.3 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND NDNC 2B = NE µg/L (05/01/07)04/18/11 0.3 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/03/11 0.3 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/02/12 0.3 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/01/12 0.3 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND04/22/13 0.3 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/21/13 0.3 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/21/14 0.3 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/06/14 0.3 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ---ND04/20/15 0.3 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ND ND10/19/15 0.3 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
04/26/16 0.3 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
2-Hexanone 04/22/10 0.46 50.000 ND ND ND ND ND ND ND ND ND ND ND ND ND NDGWPS = 280 µg/L (10/23/07)10/27/10 0.46 50.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.46 50.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/03/11 0.46 50.000 4.20 J ND ND ND ND ND ND ND 12.10 J ND ND ND ---ND
04/02/12 0.46 50.000 ND ND ND ND ND ND 0.95 J ND ND ND ND ND ND ND10/01/12 0.46 50.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/22/13 0.46 50.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/21/13 0.46 50.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/21/14 0.46 50.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/06/14 0.46 50.000 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 0.46 50.000 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.46 50.000 ND ND ND ---ND ND ND ND 0.71 J ND ND ND ---ND
04/26/16 0.46 50.000 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Iodomethane 04/18/11 0.32 10.000 ND ND 16.1 ND ND ND ND ND ND ND ND ND ND ND
NC 2L = NE µg/L (01/01/10) 10/03/11 0.32 10.000 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
NC 2B = NE µg/L (05/01/07)04/02/12 0.32 10.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/01/12 0.32 10.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/22/13 0.32 10.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/21/13 0.32 10.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/21/14 0.32 10.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/06/14 0.32 10.000 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 0.32 10.000 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.32 10.000 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
04/26/16 0.32 10.000 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Methylene Chloride 04/22/10 0.97 2.000 ND ND ND ND ND ND ND ND ND ND ND ND ND 2.00
NC 2L = 5 µg/L (01/01/10) 10/27/10 0.97 1.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.97 1.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/03/11 0.97 1.000 ND ND ND ND ND ND ND ND ND ND ND ND ---2.6004/02/12 0.97 1.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/01/12 0.97 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/22/13 0.97 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND 2.60
10/21/13 0.97 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND04/21/14 0.97 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/06/14 0.97 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ---2.90
04/20/15 0.97 1.00 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.97 1.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND04/26/16 0.97 1.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Transylvania County Calvert Landfill Page 5 of 7 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL ORGANIC CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 MW-4 MW-105S MW-105D MW-106S MW-106D MW-107S MW-107D MW-108 HW-1 SMP-1 Field Blank2-Butanone (MEK)04/22/10 0.96 100.000 ND ND ND ND ND ND ND ND ND ND 3.6 J ND ND ND
(Methyl Ethyl Keytone)10/27/10 0.96 100.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 4,000 µg/L (01/01/10) 04/18/11 0.96 100.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)10/03/11 0.96 100.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND04/02/12 0.96 100.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/01/12 0.96 100.00 ND ND ND ND ND ND ND ND 5.30 J ND ND ND ND ND
04/22/13 0.96 100.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/21/13 0.96 100.00 ND ND ND ND ND ND ND ND ND ND 7.8 J ND ND ND04/21/14 0.96 100.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/06/14 0.96 100.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 0.96 100.00 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.96 100.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND04/26/16 0.96 100.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Tetrachloroethene 04/22/10 0.46 1.00 ND ND ND ND ND 0.55 J 0.62 J ND ND ND ND ND ND ND
NC 2L = 0.7 µg/L (10/23/07)10/27/10 0.46 1.00 ND ND ND ND ND ND 0.87 J ND ND ND ND ND ND NDNC 2B = 3.3 µg/L (05/01/07)04/18/11 0.46 1.00 ND ND ND ND ND 0.52 J 0.49 J ND ND ND ND ND ND ND
10/03/11 0.46 1.00 ND ND ND ND ND 0.47 J 0.51 J ND ND ND ND ND ---ND
04/02/12 0.46 1.00 ND ND ND ND ND 0.63 J ND ND ND ND ND ND ND ND
10/01/12 0.46 1.0 ND ND ND ND ND 0.54 J ND ND ND ND ND ND ND ND04/22/13 0.46 1.0 ND ND ND ND ND 0.64 J ND ND ND ND ND ND ND ND
10/21/13 0.46 1.0 ND ND ND ND ND 0.82 J ND ND ND ND ND ND ND ND
04/21/14 0.46 1.0 ND ND ND ND ND 0.64 J ND ND ND ND ND ND ND ND
10/06/14 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ---ND04/20/15 0.46 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ND ND10/19/15 0.46 1.0 ND ND ND ---ND 0.60 J ND ND ND ND ND ND ---ND
04/26/16 0.46 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Toluene 04/22/10 0.26 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND NDNC 2L = 600 µg/L (01/01/10) 10/27/10 0.26 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2B = 11 µg/L (05/01/07)04/18/11 0.26 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/03/11 0.26 1.00 ND ND ND 1.3 ND ND ND ND 0.31 J ND ND ND ---ND
04/02/12 0.26 1.00 ND ND ND 0.3 J ND ND ND ND ND ND ND ND ND ND10/01/12 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/22/13 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/21/13 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/21/14 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/06/14 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 0.26 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.26 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
04/26/16 0.26 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
1,1,1-Trichloroethane 04/22/10 0.48 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 200 µg/L (10/23/07)10/27/10 0.48 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.48 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/03/11 0.48 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/02/12 0.48 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/01/12 0.48 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/22/13 0.48 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/21/13 0.48 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/21/14 0.48 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/06/14 0.48 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 0.48 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ND ND10/19/15 0.48 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
04/26/16 0.48 1.0 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Trichloroethene 04/22/10 0.47 1.00 ND ND ND 0.47 J ND 1.60 ND 0.47 J ND ND ND ND ND ND
NC 2L = 3 µg/L (01/01/10) 10/27/10 0.47 1.00 ND ND ND ND ND ND 0.53 J ND ND ND ND ND ND NDNC 2B = 30 µg/L (05/01/07)04/18/11 0.47 1.00 ND ND ND 0.45 J ND 1.70 ND ND ND ND ND ND ND ND
10/03/11 0.47 1.00 ND ND ND ND ND 1.40 ND ND ND ND ND ND ---ND
04/02/12 0.47 1.00 ND ND ND ND ND 1.20 ND ND ND ND ND ND ND ND
10/01/12 0.47 1.0 ND ND ND ND ND 1.10 ND ND ND ND ND ND ND ND04/22/13 0.47 1.0 ND ND ND 0.54 J ND 0.97 J ND ND ND ND ND ND ND ND
10/21/13 0.47 1.0 ND ND ND ND ND 1.00 ND ND ND ND ND ND ND ND
04/21/14 0.47 1.0 ND ND ND ND ND 0.95 J ND ND ND ND ND ND ND ND
10/06/14 0.47 1.0 ND ND ND ND ND 0.80 J ND ND ND ND ND ND ---ND04/20/15 0.47 1.0 ND ND ND ---ND 0.59 J ND ND ND ND ND ND ND ND
10/19/15 0.47 1.0 ND ND ND ---ND 1.1 ND ND ND ND ND ND ---ND
04/26/16 0.47 1.0 ND ND ND ---ND 0.76 J ND ND ND ND ND ND ---ND
Transylvania County Calvert Landfill Page 6 of 7 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL ORGANIC CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1 MW-2 MW-3 MW-4 MW-105S MW-105D MW-106S MW-106D MW-107S MW-107D MW-108 HW-1 SMP-1 Field Blank
Trichlorofluoromethane 04/22/10 0.2 1.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 2,000 µg/L (01/01/10)10/27/10 0.2 1.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.2 1.000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/03/11 0.2 1.000 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/02/12 0.2 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/01/12 0.2 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/22/13 0.2 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND10/21/13 0.2 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/21/14 0.2 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/06/14 0.2 1.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 0.2 1.00 ND ND ND ---ND ND ND ND ND ND ND ND ND ND10/19/15 0.2 1.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
04/26/16 0.2 1.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Vinyl Chloride 04/22/10 0.62 1.00 ND ND 1.8 0.72 J ND 1.60 ND ND ND 1.10 ND ND ND NDNC 2L = 0.03 µg/L (01/01/10) 10/27/10 0.62 1.00 ND ND 1.3 0.7 J ND ND ND ND ND ND ND ND ND ND
NC 2B = 2.4 µg/L (05/01/07)04/18/11 0.62 1.00 ND ND 1.0 ND ND 1.5 ND ND ND 0.63 J ND ND ND ND
10/03/11 0.62 1.00 ND ND 1.1 0.96 J ND 1.7 ND ND ND ND ND ND ---ND
04/02/12 0.62 1.00 ND ND 1.0 0.78 J ND 1.3 ND ND ND ND ND ND ND ND10/01/12 0.62 1.0 ND ND 1.0 ND ND 1.1 ND ND ND ND ND ND ND ND
04/22/13 0.62 1.0 ND ND 0.78 J ND ND 0.83 J ND ND ND ND ND ND ND ND
10/21/13 0.62 1.0 ND ND ND ND ND 0.92 J ND ND ND ND ND ND ND ND
04/21/14 0.62 1.0 ND ND ND 0.64 J ND 1.0 ND ND ND ND ND ND ND ND10/06/14 0.62 1.0 ND ND ND ND ND 0.99 J ND ND ND ND ND ND ---ND04/20/15 0.62 1.0 ND ND 0.88 J ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.62 1.0 ND ND 0.91 J ---ND 1.0 J ND ND ND ND ND ND ---ND
04/26/16 0.62 1.0 ND ND 0.62 J ---ND 0.81 J ND ND ND ND ND ND ---ND
Xylene (Total)04/22/10 0.66 2.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 500 µg/L (01/01/10)10/27/10 0.66 2.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2B = NE µg/L (05/01/07)04/18/11 0.66 2.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/03/11 0.66 2.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND04/02/12 0.66 2.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/01/12 0.66 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/22/13 0.66 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/21/13 0.66 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND04/21/14 0.66 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/06/14 0.66 5.00 ND ND ND ND ND ND ND ND ND ND ND ND ---ND
04/20/15 0.66 5.00 ND ND ND ---ND ND ND ND ND ND ND ND ND ND
10/19/15 0.66 5.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND04/26/16 0.66 5.00 ND ND ND ---ND ND ND ND ND ND ND ND ---ND
Notes:QL = Quantiation Limit
ND = Not detected at or above the detection or reporting limit.
J = Estimated value since the concentration is between the DL and the SWSL.
--- = Not sampled and or Not Reported
DL = Laboratory detection limit.
9. Dry = Monitoring well/surface water monitoring point is considered to be dry and no sample collected.
NC 2L = North Carolina's groundwater quality standard established under 15A NCAC 2L, .0202.
NC 2B = North Carolina 2B Surface Water Standards. The surface water at the sampling location is classified as Class C.
NC 2B Standard is used to define concentration limits for surface water constituents. NC SWSL = North Carolina Solid Waste Section Limits.
Bold concentrations are greater than the NC 2L for groundwater or NC 2B for surface water.
NE = Not established.
NV= Values considered to be not valid due to laboratory exceeding hold times for analysis
Transylvania County Calvert Landfill Page 7 of 7 Joyce Engineering
TABLE 4: Horizontal Groundwater Flow Velocities
Date of Water Table Measurements: April 26, 2016
SEGMENT HORIZ.HYDRAULIC EFFECTIVE LINEAR
FLOW BEGIN & END GRADIENT CONDUCTIVITY POROSITY VELOCITY
DIRECTION GW ELEVATION i K n e V
(feet-AMSL)(ft/ft) (ft/day)(ft/year)
2,240
2,220
2,240
2,210
2,250
2,220
.0.0591 Average 186.51
Notes:
Linear flow velocity: V = Ki/ne (modified Darcy equation).
Hydraulic conductivity (K ) is based on the arithmetic mean of values from slug tests conducted at the facility by Joyce Engineering in April, 1999.
Assumed effective porosity (n) of 0.20 for porous regolith
Refer to Drawing 1 for flow line segments.
0.20 259.501.73E+00
FLOW LINE
SEGMENT
SEGMENT
LENGTH
(feet)
i 3 365 NE 0.0822
179.05
i 1 522 S 0.0383 0.20 120.97
0.20
1.73E+00
1.73E+00i2529SE0.0567
Transylvania Co. Calvert Landfill
Permit No. 88-03 Joyce Engineering

Figure

Figure No. 1 Site Location Map

Drawing

Drawing No. 1 Groundwater Surface Map

Appendices

Appendix 1 Laboratory Analytical Report and Field Forms
Appendix 2 Summary of Detections and Summary of Exceedances
Appendix 3 Summary of Field Parameters
Appendix 4 Summary of Monitoring Well Construction

Appendix 1 Laboratory Analytical Report and Field Forms

#=CL#
May 09, 2016
LIMS USE: FR - ALEX EVERHART
LIMS OBJECT ID: 92295593
92295593
Project:
Pace Project No.:
RE:
Mr. Alex Everhart
Joyce Engineering-NC
2211 W. Meadowview Road
Suite 101
Greensboro, NC 27407
TRANSYLVANIA-CALVERT
Dear Mr. Everhart:
Enclosed are the analytical results for sample(s) received by the laboratory on April 28, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
cc:Mr. Van Burbach, Joyce Engineering-NC
Alex Everhart, Joyce Engineering-NC
REPORT OF LABORATORY ANALYSIS
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Page 1 of 49
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
Asheville Certification IDs2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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Page 2 of 49
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Lab ID Sample ID Matrix Date Collected Date Received
92295593001 8803-MW1 Water 04/26/16 12:11 04/28/16 13:30
92295593002 8803-MW2 Water 04/26/16 12:52 04/28/16 13:30
92295593003 8803-MW3 Water 04/26/16 17:48 04/28/16 13:30
92295593004 8803-MW105S Water 04/26/16 15:18 04/28/16 13:30
92295593005 8803-MW105D Water 04/26/16 15:30 04/28/16 13:30
92295593006 8803-MW106S Water 04/26/16 17:55 04/28/16 13:30
92295593007 8803-MW106D Water 04/26/16 17:43 04/28/16 13:30
92295593008 8803-MW107S Water 04/26/16 13:55 04/28/16 13:30
92295593009 8803-MW107D Water 04/26/16 14:15 04/28/16 13:30
92295593010 8803-MW108 Water 04/26/16 11:41 04/28/16 13:30
92295593011 8803-HW1 Water 04/26/16 16:47 04/28/16 13:30
92295593012 8803-FIELD BLANK Water 04/26/16 18:00 04/28/16 13:30
92295593013 8803-TRIP BLANK Water 04/26/16 16:30 04/28/16 13:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 3 of 49
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92295593001 8803-MW1 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 50 PASI-CGAW
92295593002 8803-MW2 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 50 PASI-CGAW
92295593003 8803-MW3 EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 50 PASI-CGAW
92295593004 8803-MW105S EPA 8260 51 PASI-CGAW
92295593005 8803-MW105D EPA 8260 51 PASI-CGAW
92295593006 8803-MW106S EPA 8260 50 PASI-CGAW
92295593007 8803-MW106D EPA 8260 50 PASI-CGAW
92295593008 8803-MW107S EPA 8260 50 PASI-CGAW
92295593009 8803-MW107D EPA 8260 50 PASI-CGAW
92295593010 8803-MW108 EPA 8260 50 PASI-CGAW
92295593011 8803-HW1 EPA 8260 50 PASI-CGAW
92295593012 8803-FIELD BLANK EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 51 PASI-CGAW
92295593013 8803-TRIP BLANK EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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Page 4 of 49
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92295593001 8803-MW1
Barium 72.3J ug/L 05/06/16 02:19100EPA 6010
Cadmium 0.61J ug/L 05/06/16 02:191.0EPA 6010
Chromium 3.1J ug/L 05/06/16 02:1910.0EPA 6010
Lead 3.9J ug/L 05/06/16 02:1910.0EPA 6010
92295593002 8803-MW2
Barium 138 ug/L 05/06/16 02:22100EPA 6010
Chromium 2.8J ug/L 05/06/16 02:2210.0EPA 6010
Lead 4.5J ug/L 05/06/16 02:2210.0EPA 6010
Benzene 0.44J ug/L 05/04/16 02:191.0EPA 8260
Chlorobenzene 0.37J ug/L 05/04/16 02:193.0EPA 8260
1,4-Dichlorobenzene 0.35J ug/L 05/04/16 02:191.0EPA 8260
cis-1,2-Dichloroethene 0.84J ug/L 05/04/16 02:195.0EPA 8260
92295593003 8803-MW3
Barium 84.9J ug/L 05/06/16 02:26100EPA 6010
Lead 3.7J ug/L 05/06/16 02:2610.0EPA 6010
Acetone 17.3J ug/L 05/04/16 02:36100EPA 8260
Benzene 0.90J ug/L 05/04/16 02:361.0EPA 8260
Chlorobenzene 11.6 ug/L 05/04/16 02:363.0EPA 8260
Chloromethane 0.19J ug/L 05/04/16 02:361.0EPA 8260
1,2-Dichlorobenzene 0.79J ug/L 05/04/16 02:365.0EPA 8260
1,4-Dichlorobenzene 13.2 ug/L 05/04/16 02:361.0EPA 8260
cis-1,2-Dichloroethene 0.96J ug/L 05/04/16 02:365.0EPA 8260
Vinyl chloride 0.62J ug/L 05/04/16 02:361.0EPA 8260
92295593004 8803-MW105S
Benzene 0.75J ug/L 05/04/16 02:531.0EPA 8260
Chlorobenzene 2.6J ug/L 05/04/16 02:533.0EPA 8260
Chloromethane 1.0 ug/L 05/04/16 02:531.0EPA 8260
1,2-Dichlorobenzene 2.3J ug/L 05/04/16 02:535.0EPA 8260
1,4-Dichlorobenzene 2.2 ug/L 05/04/16 02:531.0EPA 8260
Dichlorodifluoromethane 1.1J ug/L 05/04/16 02:535.0EPA 8260
cis-1,2-Dichloroethene 0.62J ug/L 05/04/16 02:535.0EPA 8260
92295593005 8803-MW105D
Benzene 1.8 ug/L 05/04/16 03:101.0EPA 8260
Chlorobenzene 11.2 ug/L 05/04/16 03:103.0EPA 8260
1,4-Dichlorobenzene 4.9 ug/L 05/04/16 03:101.0EPA 8260
Dichlorodifluoromethane 0.71J ug/L 05/04/16 03:105.0EPA 8260
cis-1,2-Dichloroethene 9.7 ug/L 05/04/16 03:105.0EPA 8260
1,2-Dichloropropane 0.64J ug/L 05/04/16 03:101.0EPA 8260
Trichloroethene 0.76J ug/L 05/04/16 03:101.0EPA 8260
Vinyl chloride 0.81J ug/L 05/04/16 03:101.0EPA 8260
92295593006 8803-MW106S
cis-1,2-Dichloroethene 0.76J ug/L 05/04/16 03:285.0EPA 8260
92295593007 8803-MW106D
Chlorobenzene 4.0 ug/L 05/04/16 03:453.0EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 5 of 49
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92295593007 8803-MW106D
1,4-Dichlorobenzene 4.0 ug/L 05/04/16 03:451.0EPA 8260
cis-1,2-Dichloroethene 2.3J ug/L 05/04/16 03:455.0EPA 8260
92295593009 8803-MW107D
Benzene 0.57J ug/L 05/04/16 04:191.0EPA 8260
Chlorobenzene 0.73J ug/L 05/04/16 04:193.0EPA 8260
1,4-Dichlorobenzene 0.87J ug/L 05/04/16 04:191.0EPA 8260
1,1-Dichloroethane 0.51J ug/L 05/04/16 04:195.0EPA 8260
cis-1,2-Dichloroethene 0.43J ug/L 05/04/16 04:195.0EPA 8260
92295593010 8803-MW108
Acetone 61.1J ug/L 05/04/16 04:53 M1100EPA 8260
Benzene 0.54J ug/L 05/04/16 04:531.0EPA 8260
Chlorobenzene 0.48J ug/L 05/04/16 04:533.0EPA 8260
Chloroethane 0.77J ug/L 05/04/16 04:5310.0EPA 8260
1,4-Dichlorobenzene 1.8 ug/L 05/04/16 04:531.0EPA 8260
1,1-Dichloroethane 0.87J ug/L 05/04/16 04:535.0EPA 8260
cis-1,2-Dichloroethene 2.2J ug/L 05/04/16 04:535.0EPA 8260
92295593011 8803-HW1
Chloroform 0.79J ug/L 05/05/16 13:165.0EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 6 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW1 Lab ID:92295593001 Collected:04/26/16 12:11 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 02:19 7440-38-204/29/16 12:0510.0 2.5 1
Barium 72.3J ug/L 05/06/16 02:19 7440-39-304/29/16 12:051002.5 1
Cadmium 0.61J ug/L 05/06/16 02:19 7440-43-904/29/16 12:051.0 0.50 1
Chromium 3.1J ug/L 05/06/16 02:19 7440-47-304/29/16 12:0510.0 2.5 1
Lead 3.9J ug/L 05/06/16 02:19 7439-92-104/29/16 12:0510.0 2.5 1
Selenium ND ug/L 05/06/16 02:19 7782-49-204/29/16 12:0510.0 5.0 1
Silver ND ug/L 05/06/16 02:19 7440-22-404/29/16 12:0510.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/04/16 14:13 7439-97-605/03/16 02:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/04/16 02:02 67-64-110010.0 1
Acrylonitrile ND ug/L 05/04/16 02:02 107-13-12001.9 1
Benzene ND ug/L 05/04/16 02:02 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/04/16 02:02 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/04/16 02:02 75-27-41.0 0.18 1
Bromoform ND ug/L 05/04/16 02:02 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/04/16 02:02 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/04/16 02:02 78-93-31000.96 1
Carbon disulfide ND ug/L 05/04/16 02:02 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/04/16 02:02 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/04/16 02:02 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/04/16 02:02 75-00-310.0 0.54 1
Chloroform ND ug/L 05/04/16 02:02 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/04/16 02:02 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/16 02:02 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/04/16 02:02 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/16 02:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/04/16 02:02 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/04/16 02:02 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/04/16 02:02 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/04/16 02:02 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/04/16 02:02 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/04/16 02:02 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/04/16 02:02 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/04/16 02:02 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/04/16 02:02 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/04/16 02:02 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/04/16 02:02 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/04/16 02:02 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/04/16 02:02 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/04/16 02:02 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/04/16 02:02 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/04/16 02:02 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/16 02:02 108-10-11000.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 7 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW1 Lab ID:92295593001 Collected:04/26/16 12:11 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Styrene ND ug/L 05/04/16 02:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/16 02:02 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/16 02:02 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/04/16 02:02 127-18-41.0 0.46 1
Toluene ND ug/L 05/04/16 02:02 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/04/16 02:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/04/16 02:02 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/04/16 02:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/04/16 02:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/04/16 02:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/04/16 02:02 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/04/16 02:02 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/04/16 02:02 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %05/04/16 02:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %05/04/16 02:02 17060-07-070-130 1
Toluene-d8 (S)96 %05/04/16 02:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 8 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW2 Lab ID:92295593002 Collected:04/26/16 12:52 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 02:22 7440-38-204/29/16 12:0510.0 2.5 1
Barium 138 ug/L 05/06/16 02:22 7440-39-304/29/16 12:051002.5 1
Cadmium ND ug/L 05/06/16 02:22 7440-43-904/29/16 12:051.0 0.50 1
Chromium 2.8J ug/L 05/06/16 02:22 7440-47-304/29/16 12:0510.0 2.5 1
Lead 4.5J ug/L 05/06/16 02:22 7439-92-104/29/16 12:0510.0 2.5 1
Selenium ND ug/L 05/06/16 02:22 7782-49-204/29/16 12:0510.0 5.0 1
Silver ND ug/L 05/06/16 02:22 7440-22-404/29/16 12:0510.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/04/16 14:16 7439-97-605/03/16 02:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/04/16 02:19 67-64-110010.0 1
Acrylonitrile ND ug/L 05/04/16 02:19 107-13-12001.9 1
Benzene 0.44J ug/L 05/04/16 02:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/04/16 02:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/04/16 02:19 75-27-41.0 0.18 1
Bromoform ND ug/L 05/04/16 02:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/04/16 02:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/04/16 02:19 78-93-31000.96 1
Carbon disulfide ND ug/L 05/04/16 02:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/04/16 02:19 56-23-51.0 0.25 1
Chlorobenzene 0.37J ug/L 05/04/16 02:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/04/16 02:19 75-00-310.0 0.54 1
Chloroform ND ug/L 05/04/16 02:19 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/04/16 02:19 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/16 02:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/04/16 02:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/16 02:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/04/16 02:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/04/16 02:19 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.35J ug/L 05/04/16 02:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/04/16 02:19 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/04/16 02:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/04/16 02:19 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/04/16 02:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.84J ug/L 05/04/16 02:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/04/16 02:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/04/16 02:19 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/04/16 02:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/04/16 02:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/04/16 02:19 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/04/16 02:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/04/16 02:19 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/04/16 02:19 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/16 02:19 108-10-11000.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW2 Lab ID:92295593002 Collected:04/26/16 12:52 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Styrene ND ug/L 05/04/16 02:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/16 02:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/16 02:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/04/16 02:19 127-18-41.0 0.46 1
Toluene ND ug/L 05/04/16 02:19 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/04/16 02:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/04/16 02:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/04/16 02:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/04/16 02:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/04/16 02:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/04/16 02:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/04/16 02:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/04/16 02:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %05/04/16 02:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %05/04/16 02:19 17060-07-070-130 1
Toluene-d8 (S)101 %05/04/16 02:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW3 Lab ID:92295593003 Collected:04/26/16 17:48 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 02:26 7440-38-204/29/16 12:0510.0 2.5 1
Barium 84.9J ug/L 05/06/16 02:26 7440-39-304/29/16 12:051002.5 1
Cadmium ND ug/L 05/06/16 02:26 7440-43-904/29/16 12:051.0 0.50 1
Chromium ND ug/L 05/06/16 02:26 7440-47-304/29/16 12:0510.0 2.5 1
Lead 3.7J ug/L 05/06/16 02:26 7439-92-104/29/16 12:0510.0 2.5 1
Selenium ND ug/L 05/06/16 02:26 7782-49-204/29/16 12:0510.0 5.0 1
Silver ND ug/L 05/06/16 02:26 7440-22-404/29/16 12:0510.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/04/16 14:18 7439-97-605/03/16 02:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 17.3J ug/L 05/04/16 02:36 67-64-110010.0 1
Acrylonitrile ND ug/L 05/04/16 02:36 107-13-12001.9 1
Benzene 0.90J ug/L 05/04/16 02:36 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/04/16 02:36 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/04/16 02:36 75-27-41.0 0.18 1
Bromoform ND ug/L 05/04/16 02:36 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/04/16 02:36 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/04/16 02:36 78-93-31000.96 1
Carbon disulfide ND ug/L 05/04/16 02:36 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/04/16 02:36 56-23-51.0 0.25 1
Chlorobenzene 11.6 ug/L 05/04/16 02:36 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/04/16 02:36 75-00-310.0 0.54 1
Chloroform ND ug/L 05/04/16 02:36 67-66-35.0 0.14 1
Chloromethane 0.19J ug/L 05/04/16 02:36 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/16 02:36 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/04/16 02:36 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/16 02:36 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/04/16 02:36 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.79J ug/L 05/04/16 02:36 95-50-15.0 0.30 1
1,4-Dichlorobenzene 13.2 ug/L 05/04/16 02:36 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/04/16 02:36 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/04/16 02:36 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/04/16 02:36 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/04/16 02:36 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.96J ug/L 05/04/16 02:36 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/04/16 02:36 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/04/16 02:36 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/04/16 02:36 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/04/16 02:36 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/04/16 02:36 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/04/16 02:36 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/04/16 02:36 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/04/16 02:36 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/16 02:36 108-10-11000.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW3 Lab ID:92295593003 Collected:04/26/16 17:48 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Styrene ND ug/L 05/04/16 02:36 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/16 02:36 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/16 02:36 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/04/16 02:36 127-18-41.0 0.46 1
Toluene ND ug/L 05/04/16 02:36 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/04/16 02:36 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/04/16 02:36 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/04/16 02:36 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/04/16 02:36 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/04/16 02:36 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/04/16 02:36 108-05-450.0 0.35 1
Vinyl chloride 0.62J ug/L 05/04/16 02:36 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/04/16 02:36 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %05/04/16 02:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %05/04/16 02:36 17060-07-070-130 1
Toluene-d8 (S)98 %05/04/16 02:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW105S Lab ID:92295593004 Collected:04/26/16 15:18 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/04/16 02:53 67-64-110010.0 1
Acrylonitrile ND ug/L 05/04/16 02:53 107-13-12001.9 1
Benzene 0.75J ug/L 05/04/16 02:53 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/04/16 02:53 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/04/16 02:53 75-27-41.0 0.18 1
Bromoform ND ug/L 05/04/16 02:53 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/04/16 02:53 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/04/16 02:53 78-93-31000.96 1
Carbon disulfide ND ug/L 05/04/16 02:53 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/04/16 02:53 56-23-51.0 0.25 1
Chlorobenzene 2.6J ug/L 05/04/16 02:53 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/04/16 02:53 75-00-310.0 0.54 1
Chloroform ND ug/L 05/04/16 02:53 67-66-35.0 0.14 1
Chloromethane 1.0 ug/L 05/04/16 02:53 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/16 02:53 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/04/16 02:53 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/16 02:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/04/16 02:53 74-95-310.0 0.21 1
1,2-Dichlorobenzene 2.3J ug/L 05/04/16 02:53 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.2 ug/L 05/04/16 02:53 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/04/16 02:53 110-57-61001.0 1
Dichlorodifluoromethane 1.1J ug/L 05/04/16 02:53 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 05/04/16 02:53 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/04/16 02:53 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/04/16 02:53 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.62J ug/L 05/04/16 02:53 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/04/16 02:53 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/04/16 02:53 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/04/16 02:53 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/04/16 02:53 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/04/16 02:53 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/04/16 02:53 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/04/16 02:53 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/04/16 02:53 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/16 02:53 108-10-11000.33 1
Styrene ND ug/L 05/04/16 02:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/16 02:53 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/16 02:53 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/04/16 02:53 127-18-41.0 0.46 1
Toluene ND ug/L 05/04/16 02:53 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/04/16 02:53 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/04/16 02:53 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/04/16 02:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/04/16 02:53 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/04/16 02:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/04/16 02:53 108-05-450.0 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW105S Lab ID:92295593004 Collected:04/26/16 15:18 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride ND ug/L 05/04/16 02:53 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/04/16 02:53 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %05/04/16 02:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %05/04/16 02:53 17060-07-070-130 1
Toluene-d8 (S)101 %05/04/16 02:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW105D Lab ID:92295593005 Collected:04/26/16 15:30 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/04/16 03:10 67-64-110010.0 1
Acrylonitrile ND ug/L 05/04/16 03:10 107-13-12001.9 1
Benzene 1.8 ug/L 05/04/16 03:10 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/04/16 03:10 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/04/16 03:10 75-27-41.0 0.18 1
Bromoform ND ug/L 05/04/16 03:10 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/04/16 03:10 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/04/16 03:10 78-93-31000.96 1
Carbon disulfide ND ug/L 05/04/16 03:10 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/04/16 03:10 56-23-51.0 0.25 1
Chlorobenzene 11.2 ug/L 05/04/16 03:10 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/04/16 03:10 75-00-310.0 0.54 1
Chloroform ND ug/L 05/04/16 03:10 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/04/16 03:10 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/16 03:10 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/04/16 03:10 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/16 03:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/04/16 03:10 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/04/16 03:10 95-50-15.0 0.30 1
1,4-Dichlorobenzene 4.9 ug/L 05/04/16 03:10 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/04/16 03:10 110-57-61001.0 1
Dichlorodifluoromethane 0.71J ug/L 05/04/16 03:10 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 05/04/16 03:10 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/04/16 03:10 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/04/16 03:10 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 9.7 ug/L 05/04/16 03:10 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/04/16 03:10 156-60-55.0 0.49 1
1,2-Dichloropropane 0.64J ug/L 05/04/16 03:10 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/04/16 03:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/04/16 03:10 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/04/16 03:10 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/04/16 03:10 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/04/16 03:10 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/04/16 03:10 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/16 03:10 108-10-11000.33 1
Styrene ND ug/L 05/04/16 03:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/16 03:10 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/16 03:10 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/04/16 03:10 127-18-41.0 0.46 1
Toluene ND ug/L 05/04/16 03:10 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/04/16 03:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/04/16 03:10 79-00-51.0 0.29 1
Trichloroethene 0.76J ug/L 05/04/16 03:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/04/16 03:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/04/16 03:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/04/16 03:10 108-05-450.0 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW105D Lab ID:92295593005 Collected:04/26/16 15:30 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride 0.81J ug/L 05/04/16 03:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/04/16 03:10 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %05/04/16 03:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %05/04/16 03:10 17060-07-070-130 1
Toluene-d8 (S)99 %05/04/16 03:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW106S Lab ID:92295593006 Collected:04/26/16 17:55 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/04/16 03:28 67-64-110010.0 1
Acrylonitrile ND ug/L 05/04/16 03:28 107-13-12001.9 1
Benzene ND ug/L 05/04/16 03:28 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/04/16 03:28 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/04/16 03:28 75-27-41.0 0.18 1
Bromoform ND ug/L 05/04/16 03:28 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/04/16 03:28 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/04/16 03:28 78-93-31000.96 1
Carbon disulfide ND ug/L 05/04/16 03:28 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/04/16 03:28 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/04/16 03:28 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/04/16 03:28 75-00-310.0 0.54 1
Chloroform ND ug/L 05/04/16 03:28 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/04/16 03:28 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/16 03:28 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/04/16 03:28 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/16 03:28 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/04/16 03:28 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/04/16 03:28 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/04/16 03:28 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/04/16 03:28 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/04/16 03:28 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/04/16 03:28 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/04/16 03:28 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.76J ug/L 05/04/16 03:28 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/04/16 03:28 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/04/16 03:28 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/04/16 03:28 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/04/16 03:28 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/04/16 03:28 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/04/16 03:28 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/04/16 03:28 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/04/16 03:28 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/16 03:28 108-10-11000.33 1
Styrene ND ug/L 05/04/16 03:28 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/16 03:28 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/16 03:28 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/04/16 03:28 127-18-41.0 0.46 1
Toluene ND ug/L 05/04/16 03:28 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/04/16 03:28 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/04/16 03:28 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/04/16 03:28 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/04/16 03:28 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/04/16 03:28 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/04/16 03:28 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/04/16 03:28 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 17 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW106S Lab ID:92295593006 Collected:04/26/16 17:55 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 05/04/16 03:28 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %05/04/16 03:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %05/04/16 03:28 17060-07-070-130 1
Toluene-d8 (S)100 %05/04/16 03:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW106D Lab ID:92295593007 Collected:04/26/16 17:43 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/04/16 03:45 67-64-110010.0 1
Acrylonitrile ND ug/L 05/04/16 03:45 107-13-12001.9 1
Benzene ND ug/L 05/04/16 03:45 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/04/16 03:45 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/04/16 03:45 75-27-41.0 0.18 1
Bromoform ND ug/L 05/04/16 03:45 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/04/16 03:45 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/04/16 03:45 78-93-31000.96 1
Carbon disulfide ND ug/L 05/04/16 03:45 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/04/16 03:45 56-23-51.0 0.25 1
Chlorobenzene 4.0 ug/L 05/04/16 03:45 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/04/16 03:45 75-00-310.0 0.54 1
Chloroform ND ug/L 05/04/16 03:45 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/04/16 03:45 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/16 03:45 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/04/16 03:45 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/16 03:45 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/04/16 03:45 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/04/16 03:45 95-50-15.0 0.30 1
1,4-Dichlorobenzene 4.0 ug/L 05/04/16 03:45 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/04/16 03:45 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/04/16 03:45 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/04/16 03:45 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/04/16 03:45 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.3J ug/L 05/04/16 03:45 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/04/16 03:45 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/04/16 03:45 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/04/16 03:45 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/04/16 03:45 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/04/16 03:45 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/04/16 03:45 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/04/16 03:45 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/04/16 03:45 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/16 03:45 108-10-11000.33 1
Styrene ND ug/L 05/04/16 03:45 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/16 03:45 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/16 03:45 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/04/16 03:45 127-18-41.0 0.46 1
Toluene ND ug/L 05/04/16 03:45 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/04/16 03:45 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/04/16 03:45 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/04/16 03:45 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/04/16 03:45 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/04/16 03:45 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/04/16 03:45 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/04/16 03:45 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW106D Lab ID:92295593007 Collected:04/26/16 17:43 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 05/04/16 03:45 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %05/04/16 03:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %05/04/16 03:45 17060-07-070-130 1
Toluene-d8 (S)101 %05/04/16 03:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW107S Lab ID:92295593008 Collected:04/26/16 13:55 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/04/16 04:02 67-64-110010.0 1
Acrylonitrile ND ug/L 05/04/16 04:02 107-13-12001.9 1
Benzene ND ug/L 05/04/16 04:02 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/04/16 04:02 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/04/16 04:02 75-27-41.0 0.18 1
Bromoform ND ug/L 05/04/16 04:02 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/04/16 04:02 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/04/16 04:02 78-93-31000.96 1
Carbon disulfide ND ug/L 05/04/16 04:02 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/04/16 04:02 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/04/16 04:02 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/04/16 04:02 75-00-310.0 0.54 1
Chloroform ND ug/L 05/04/16 04:02 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/04/16 04:02 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/16 04:02 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/04/16 04:02 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/16 04:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/04/16 04:02 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/04/16 04:02 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/04/16 04:02 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/04/16 04:02 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/04/16 04:02 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/04/16 04:02 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/04/16 04:02 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/04/16 04:02 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/04/16 04:02 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/04/16 04:02 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/04/16 04:02 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/04/16 04:02 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/04/16 04:02 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/04/16 04:02 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/04/16 04:02 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/04/16 04:02 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/16 04:02 108-10-11000.33 1
Styrene ND ug/L 05/04/16 04:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/16 04:02 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/16 04:02 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/04/16 04:02 127-18-41.0 0.46 1
Toluene ND ug/L 05/04/16 04:02 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/04/16 04:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/04/16 04:02 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/04/16 04:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/04/16 04:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/04/16 04:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/04/16 04:02 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/04/16 04:02 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW107S Lab ID:92295593008 Collected:04/26/16 13:55 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 05/04/16 04:02 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %05/04/16 04:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %05/04/16 04:02 17060-07-070-130 1
Toluene-d8 (S)99 %05/04/16 04:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW107D Lab ID:92295593009 Collected:04/26/16 14:15 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/04/16 04:19 67-64-110010.0 1
Acrylonitrile ND ug/L 05/04/16 04:19 107-13-12001.9 1
Benzene 0.57J ug/L 05/04/16 04:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/04/16 04:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/04/16 04:19 75-27-41.0 0.18 1
Bromoform ND ug/L 05/04/16 04:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/04/16 04:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/04/16 04:19 78-93-31000.96 1
Carbon disulfide ND ug/L 05/04/16 04:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/04/16 04:19 56-23-51.0 0.25 1
Chlorobenzene 0.73J ug/L 05/04/16 04:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/04/16 04:19 75-00-310.0 0.54 1
Chloroform ND ug/L 05/04/16 04:19 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/04/16 04:19 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/16 04:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/04/16 04:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/16 04:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/04/16 04:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/04/16 04:19 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.87J ug/L 05/04/16 04:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/04/16 04:19 110-57-61001.0 1
1,1-Dichloroethane 0.51J ug/L 05/04/16 04:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/04/16 04:19 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/04/16 04:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.43J ug/L 05/04/16 04:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/04/16 04:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/04/16 04:19 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/04/16 04:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/04/16 04:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/04/16 04:19 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/04/16 04:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/04/16 04:19 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/04/16 04:19 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/16 04:19 108-10-11000.33 1
Styrene ND ug/L 05/04/16 04:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/16 04:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/16 04:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/04/16 04:19 127-18-41.0 0.46 1
Toluene ND ug/L 05/04/16 04:19 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/04/16 04:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/04/16 04:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/04/16 04:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/04/16 04:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/04/16 04:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/04/16 04:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/04/16 04:19 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW107D Lab ID:92295593009 Collected:04/26/16 14:15 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 05/04/16 04:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %05/04/16 04:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %05/04/16 04:19 17060-07-070-130 1
Toluene-d8 (S)99 %05/04/16 04:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW108 Lab ID:92295593010 Collected:04/26/16 11:41 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 61.1J ug/L 05/04/16 04:53 67-64-1 M110010.0 1
Acrylonitrile ND ug/L 05/04/16 04:53 107-13-12001.9 1
Benzene 0.54J ug/L 05/04/16 04:53 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/04/16 04:53 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/04/16 04:53 75-27-41.0 0.18 1
Bromoform ND ug/L 05/04/16 04:53 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/04/16 04:53 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/04/16 04:53 78-93-3 M11000.96 1
Carbon disulfide ND ug/L 05/04/16 04:53 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/04/16 04:53 56-23-5 M11.0 0.25 1
Chlorobenzene 0.48J ug/L 05/04/16 04:53 108-90-73.0 0.23 1
Chloroethane 0.77J ug/L 05/04/16 04:53 75-00-310.0 0.54 1
Chloroform ND ug/L 05/04/16 04:53 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/04/16 04:53 74-87-3 M11.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/16 04:53 96-12-8 M113.0 2.0 1
Dibromochloromethane ND ug/L 05/04/16 04:53 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/16 04:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/04/16 04:53 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/04/16 04:53 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.8 ug/L 05/04/16 04:53 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/04/16 04:53 110-57-61001.0 1
1,1-Dichloroethane 0.87J ug/L 05/04/16 04:53 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/04/16 04:53 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/04/16 04:53 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.2J ug/L 05/04/16 04:53 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/04/16 04:53 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/04/16 04:53 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/04/16 04:53 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/04/16 04:53 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/04/16 04:53 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/04/16 04:53 591-78-6 M150.0 0.46 1
Iodomethane ND ug/L 05/04/16 04:53 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/04/16 04:53 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/16 04:53 108-10-1 M11000.33 1
Styrene ND ug/L 05/04/16 04:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/16 04:53 630-20-6 M15.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/16 04:53 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/04/16 04:53 127-18-4 M11.0 0.46 1
Toluene ND ug/L 05/04/16 04:53 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/04/16 04:53 71-55-6 M11.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/04/16 04:53 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/04/16 04:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/04/16 04:53 75-69-4 M11.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/04/16 04:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/04/16 04:53 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/04/16 04:53 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-MW108 Lab ID:92295593010 Collected:04/26/16 11:41 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 05/04/16 04:53 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)107 %05/04/16 04:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %05/04/16 04:53 17060-07-070-130 1
Toluene-d8 (S)98 %05/04/16 04:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
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Huntersville, NC 28078
[phone]
Page 26 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-HW1 Lab ID:92295593011 Collected:04/26/16 16:47 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/05/16 13:16 67-64-110010.0 1
Acrylonitrile ND ug/L 05/05/16 13:16 107-13-12001.9 1
Benzene ND ug/L 05/05/16 13:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/05/16 13:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/05/16 13:16 75-27-41.0 0.18 1
Bromoform ND ug/L 05/05/16 13:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/05/16 13:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/05/16 13:16 78-93-31000.96 1
Carbon disulfide ND ug/L 05/05/16 13:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/05/16 13:16 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/05/16 13:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/05/16 13:16 75-00-310.0 0.54 1
Chloroform 0.79J ug/L 05/05/16 13:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/05/16 13:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/05/16 13:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/05/16 13:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/05/16 13:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/05/16 13:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/05/16 13:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/05/16 13:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/05/16 13:16 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/05/16 13:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/05/16 13:16 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/05/16 13:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/05/16 13:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/05/16 13:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/05/16 13:16 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/05/16 13:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/05/16 13:16 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/05/16 13:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/05/16 13:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/05/16 13:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/05/16 13:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/05/16 13:16 108-10-11000.33 1
Styrene ND ug/L 05/05/16 13:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/05/16 13:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/05/16 13:16 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/05/16 13:16 127-18-41.0 0.46 1
Toluene ND ug/L 05/05/16 13:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/05/16 13:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/05/16 13:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/05/16 13:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/05/16 13:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/05/16 13:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/05/16 13:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/05/16 13:16 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 27 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-HW1 Lab ID:92295593011 Collected:04/26/16 16:47 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 05/05/16 13:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %05/05/16 13:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %05/05/16 13:16 17060-07-070-130 1
Toluene-d8 (S)98 %05/05/16 13:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 28 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-FIELD BLANK Lab ID:92295593012 Collected:04/26/16 18:00 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Arsenic ND ug/L 05/06/16 02:29 7440-38-204/29/16 12:0510.0 2.5 1
Barium ND ug/L 05/06/16 02:29 7440-39-304/29/16 12:051002.5 1
Cadmium ND ug/L 05/06/16 02:29 7440-43-904/29/16 12:051.0 0.50 1
Chromium ND ug/L 05/06/16 02:29 7440-47-304/29/16 12:0510.0 2.5 1
Lead ND ug/L 05/06/16 02:29 7439-92-104/29/16 12:0510.0 2.5 1
Selenium ND ug/L 05/06/16 02:29 7782-49-204/29/16 12:0510.0 5.0 1
Silver ND ug/L 05/06/16 02:29 7440-22-404/29/16 12:0510.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/04/16 14:20 7439-97-605/03/16 02:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/05/16 11:51 67-64-110010.0 1
Acrylonitrile ND ug/L 05/05/16 11:51 107-13-12001.9 1
Benzene ND ug/L 05/05/16 11:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/05/16 11:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/05/16 11:51 75-27-41.0 0.18 1
Bromoform ND ug/L 05/05/16 11:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/05/16 11:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/05/16 11:51 78-93-31000.96 1
Carbon disulfide ND ug/L 05/05/16 11:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/05/16 11:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/05/16 11:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/05/16 11:51 75-00-310.0 0.54 1
Chloroform ND ug/L 05/05/16 11:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/05/16 11:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/05/16 11:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/05/16 11:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/05/16 11:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/05/16 11:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/05/16 11:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/05/16 11:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/05/16 11:51 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 05/05/16 11:51 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 05/05/16 11:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/05/16 11:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/05/16 11:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/05/16 11:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/05/16 11:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/05/16 11:51 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/05/16 11:51 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/05/16 11:51 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/05/16 11:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/05/16 11:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/05/16 11:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/05/16 11:51 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-FIELD BLANK Lab ID:92295593012 Collected:04/26/16 18:00 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
4-Methyl-2-pentanone (MIBK)ND ug/L 05/05/16 11:51 108-10-11000.33 1
Styrene ND ug/L 05/05/16 11:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/05/16 11:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/05/16 11:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/05/16 11:51 127-18-41.0 0.46 1
Toluene ND ug/L 05/05/16 11:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/05/16 11:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/05/16 11:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/05/16 11:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/05/16 11:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/05/16 11:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/05/16 11:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/05/16 11:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/05/16 11:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %05/05/16 11:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %05/05/16 11:51 17060-07-070-130 1
Toluene-d8 (S)99 %05/05/16 11:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
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Page 30 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-TRIP BLANK Lab ID:92295593013 Collected:04/26/16 16:30 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/05/16 11:34 67-64-110010.0 1
Acrylonitrile ND ug/L 05/05/16 11:34 107-13-12001.9 1
Benzene ND ug/L 05/05/16 11:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/05/16 11:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/05/16 11:34 75-27-41.0 0.18 1
Bromoform ND ug/L 05/05/16 11:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/05/16 11:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/05/16 11:34 78-93-31000.96 1
Carbon disulfide ND ug/L 05/05/16 11:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/05/16 11:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/05/16 11:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/05/16 11:34 75-00-310.0 0.54 1
Chloroform ND ug/L 05/05/16 11:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/05/16 11:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/05/16 11:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/05/16 11:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/05/16 11:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/05/16 11:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/05/16 11:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/05/16 11:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/05/16 11:34 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 05/05/16 11:34 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 05/05/16 11:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/05/16 11:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/05/16 11:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/05/16 11:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/05/16 11:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/05/16 11:34 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/05/16 11:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/05/16 11:34 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/05/16 11:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/05/16 11:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/05/16 11:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/05/16 11:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/05/16 11:34 108-10-11000.33 1
Styrene ND ug/L 05/05/16 11:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/05/16 11:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/05/16 11:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/05/16 11:34 127-18-41.0 0.46 1
Toluene ND ug/L 05/05/16 11:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/05/16 11:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/05/16 11:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/05/16 11:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/05/16 11:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/05/16 11:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/05/16 11:34 108-05-450.0 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Sample:8803-TRIP BLANK Lab ID:92295593013 Collected:04/26/16 16:30 Received:04/28/16 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride ND ug/L 05/05/16 11:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/05/16 11:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %05/05/16 11:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %05/05/16 11:34 17060-07-070-130 1
Toluene-d8 (S)98 %05/05/16 11:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 32 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/9334
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92295593001, 92295593002, 92295593003, 92295593012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1722568
Associated Lab Samples:92295593001, 92295593002, 92295593003, 92295593012
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 05/04/16 13:230.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1722569LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1722570MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92295449003
1722571
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 105 75-125105 0 252.5ND 2.6 2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
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Page 33 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/21549
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92295593001, 92295593002, 92295593003, 92295593012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1722476
Associated Lab Samples:92295593001, 92295593002, 92295593003, 92295593012
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 10.0 05/06/16 01:542.5
Barium ug/L ND 100 05/06/16 01:542.5
Cadmium ug/L ND 1.0 05/06/16 01:540.50
Chromium ug/L ND 10.0 05/06/16 01:542.5
Lead ug/L ND 10.0 05/06/16 01:542.5
Selenium ug/L ND 10.0 05/06/16 01:545.0
Silver ug/L ND 10.0 05/06/16 01:542.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1722477LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 464500 93 80-120
Barium ug/L 484500 97 80-120
Cadmium ug/L 488500 98 80-120
Chromium ug/L 477500 95 80-120
Lead ug/L 492500 98 80-120
Selenium ug/L 487500 97 80-120
Silver ug/L 234250 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1722478MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92295585001
1722479
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 98 75-125100 2 2550031.5 520 530
Barium ug/L 500 94 75-12587 2 25500136018301790
Cadmium ug/L 500 98 75-12599 1 25500ND492495
Chromium ug/L 500 92 75-12593 1 2550050.3 510 517
Lead ug/L 500 89 75-12589 1 255005.9J 450 452
Selenium ug/L 500 97 75-12597 0 25500ND489490
Silver ug/L 250 93 75-12595 2 25250ND233238
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36663
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92295593001, 92295593002, 92295593003, 92295593004, 92295593005, 92295593006, 92295593007,
92295593008, 92295593009, 92295593010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1724921
Associated Lab Samples:92295593001, 92295593002, 92295593003, 92295593004, 92295593005, 92295593006, 92295593007,
92295593008, 92295593009, 92295593010
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/03/16 22:530.33
1,1,1-Trichloroethane ug/L ND 1.0 05/03/16 22:530.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/03/16 22:530.40
1,1,2-Trichloroethane ug/L ND 1.0 05/03/16 22:530.29
1,1-Dichloroethane ug/L ND 5.0 05/03/16 22:530.32
1,1-Dichloroethene ug/L ND 5.0 05/03/16 22:530.56
1,2,3-Trichloropropane ug/L ND 1.0 05/03/16 22:530.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/03/16 22:532.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/03/16 22:530.27
1,2-Dichlorobenzene ug/L ND 5.0 05/03/16 22:530.30
1,2-Dichloroethane ug/L ND 1.0 05/03/16 22:530.24
1,2-Dichloropropane ug/L ND 1.0 05/03/16 22:530.27
1,4-Dichlorobenzene ug/L ND 1.0 05/03/16 22:530.33
2-Butanone (MEK)ug/L ND 100 05/03/16 22:530.96
2-Hexanone ug/L ND 50.0 05/03/16 22:530.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 05/03/16 22:530.33
Acetone ug/L ND 100 05/03/16 22:5310.0
Acrylonitrile ug/L ND 200 05/03/16 22:531.9
Benzene ug/L ND 1.0 05/03/16 22:530.25
Bromochloromethane ug/L ND 3.0 05/03/16 22:530.17
Bromodichloromethane ug/L ND 1.0 05/03/16 22:530.18
Bromoform ug/L ND 3.0 05/03/16 22:530.26
Bromomethane ug/L ND 10.0 05/03/16 22:530.29
Carbon disulfide ug/L ND 100 05/03/16 22:531.2
Carbon tetrachloride ug/L ND 1.0 05/03/16 22:530.25
Chlorobenzene ug/L ND 3.0 05/03/16 22:530.23
Chloroethane ug/L ND 10.0 05/03/16 22:530.54
Chloroform ug/L ND 5.0 05/03/16 22:530.14
Chloromethane ug/L ND 1.0 05/03/16 22:530.11
cis-1,2-Dichloroethene ug/L ND 5.0 05/03/16 22:530.19
cis-1,3-Dichloropropene ug/L ND 1.0 05/03/16 22:530.13
Dibromochloromethane ug/L ND 3.0 05/03/16 22:530.21
Dibromomethane ug/L ND 10.0 05/03/16 22:530.21
Dichlorodifluoromethane ug/L ND 5.0 05/03/16 22:530.21
Ethylbenzene ug/L ND 1.0 05/03/16 22:530.30
Iodomethane ug/L ND 10.0 05/03/16 22:530.32
Methylene Chloride ug/L ND 1.0 05/03/16 22:530.97
Styrene ug/L ND 1.0 05/03/16 22:530.26
Tetrachloroethene ug/L ND 1.0 05/03/16 22:530.46
Toluene ug/L ND 1.0 05/03/16 22:530.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1724921
Associated Lab Samples:92295593001, 92295593002, 92295593003, 92295593004, 92295593005, 92295593006, 92295593007,
92295593008, 92295593009, 92295593010
Matrix:Water
AnalyzedMDL
trans-1,2-Dichloroethene ug/L ND 5.0 05/03/16 22:530.49
trans-1,3-Dichloropropene ug/L ND 1.0 05/03/16 22:530.26
trans-1,4-Dichloro-2-butene ug/L ND 100 05/03/16 22:531.0
Trichloroethene ug/L ND 1.0 05/03/16 22:530.47
Trichlorofluoromethane ug/L ND 1.0 05/03/16 22:530.20
Vinyl acetate ug/L ND 50.0 05/03/16 22:530.35
Vinyl chloride ug/L ND 1.0 05/03/16 22:530.62
Xylene (Total)ug/L ND 5.0 05/03/16 22:530.66
1,2-Dichloroethane-d4 (S)%108 70-130 05/03/16 22:53
4-Bromofluorobenzene (S)%105 70-130 05/03/16 22:53
Toluene-d8 (S)%100 70-130 05/03/16 22:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1724922LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.150 110 80-125
1,1,1-Trichloroethane ug/L 54.250 108 71-129
1,1,2,2-Tetrachloroethane ug/L 49.050 98 79-124
1,1,2-Trichloroethane ug/L 48.750 97 85-125
1,1-Dichloroethane ug/L 45.750 91 73-126
1,1-Dichloroethene ug/L 51.550 103 66-135
1,2,3-Trichloropropane ug/L 54.250 108 75-130
1,2-Dibromo-3-chloropropane ug/L 57.550 115 71-133
1,2-Dibromoethane (EDB)ug/L 53.350 107 83-124
1,2-Dichlorobenzene ug/L 47.650 95 80-133
1,2-Dichloroethane ug/L 52.450 105 67-128
1,2-Dichloropropane ug/L 47.150 94 75-132
1,4-Dichlorobenzene ug/L 49.750 99 78-130
2-Butanone (MEK)ug/L 121100 121 61-144
2-Hexanone ug/L 132100 132 68-143
4-Methyl-2-pentanone (MIBK)ug/L 125100 125 72-135
Acetone ug/L 130100 130 48-146
Acrylonitrile ug/L 263250 105 40-160
Benzene ug/L 44.850 90 80-125
Bromochloromethane ug/L 43.750 87 71-125
Bromodichloromethane ug/L 52.450 105 78-124
Bromoform ug/L 51.650 103 71-128
Bromomethane ug/L 46.050 92 40-160
Carbon disulfide ug/L 45.7J50 91 50-160
Carbon tetrachloride ug/L 55.550 111 69-131
Chlorobenzene ug/L 48.850 98 81-122
Chloroethane ug/L 44.750 89 39-148
Chloroform ug/L 49.650 99 73-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1724922LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 54.850 110 44-146
cis-1,2-Dichloroethene ug/L 47.950 96 74-124
cis-1,3-Dichloropropene ug/L 50.850 102 72-132
Dibromochloromethane ug/L 52.950 106 78-125
Dibromomethane ug/L 51.150 102 82-120
Dichlorodifluoromethane ug/L 57.750 115 34-157
Ethylbenzene ug/L 49.650 99 79-121
Iodomethane ug/L 105100 105 39-154
Methylene Chloride ug/L 53.150 106 64-133
Styrene ug/L 50.750 101 84-126
Tetrachloroethene ug/L 50.950 102 78-122
Toluene ug/L 47.850 96 80-121
trans-1,2-Dichloroethene ug/L 47.850 96 71-127
trans-1,3-Dichloropropene ug/L 52.750 105 69-141
trans-1,4-Dichloro-2-butene ug/L 60.3J50 121 40-160
Trichloroethene ug/L 49.050 98 78-122
Trichlorofluoromethane ug/L 54.050 108 53-137
Vinyl acetate ug/L 111100 111 40-160
Vinyl chloride ug/L 49.350 99 58-137
Xylene (Total)ug/L 149150 99 81-126
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1724924MATRIX SPIKE SAMPLE:
MSSpike
Result
92295593010
1,1,1,2-Tetrachloroethane ug/L 26.3 M12013270-130ND
1,1,1-Trichloroethane ug/L 26.4 M12013270-130ND
1,1,2,2-Tetrachloroethane ug/L 21.820 109 70-130ND
1,1,2-Trichloroethane ug/L 20.320 102 70-130ND
1,1-Dichloroethane ug/L 22.620 109 70-1300.87J
1,1-Dichloroethene ug/L 26.620 133 70-166ND
1,2,3-Trichloropropane ug/L 25.020 125 70-130ND
1,2-Dibromo-3-chloropropane ug/L 26.7 M12013470-130ND
1,2-Dibromoethane (EDB)ug/L 24.920 124 70-130ND
1,2-Dichlorobenzene ug/L 23.020 115 70-130ND
1,2-Dichloroethane ug/L 24.720 124 70-130ND
1,2-Dichloropropane ug/L 21.320 106 70-130ND
1,4-Dichlorobenzene ug/L 25.220 117 70-1301.8
2-Butanone (MEK)ug/L 59.7J M14014970-130ND
2-Hexanone ug/L 57.6 M14014470-130ND
4-Methyl-2-pentanone (MIBK)ug/L 53.2J M14013370-130ND
Acetone ug/L 159 M14024470-13061.1J
Acrylonitrile ug/L 119J100 119 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1724924MATRIX SPIKE SAMPLE:
MSSpike
Result
92295593010
Benzene ug/L 22.420 109 70-1480.54J
Bromochloromethane ug/L 21.620 108 70-130ND
Bromodichloromethane ug/L 25.620 128 70-130ND
Bromoform ug/L 23.820 119 70-130ND
Bromomethane ug/L 19.720 99 70-130ND
Carbon disulfide ug/L 23.7J20 118 70-130ND
Carbon tetrachloride ug/L 28.7 M12014370-130ND
Chlorobenzene ug/L 23.720 116 70-1460.48J
Chloroethane ug/L 24.420 118 70-1300.77J
Chloroform ug/L 23.820 119 70-130ND
Chloromethane ug/L 28.4 M12014270-130ND
cis-1,2-Dichloroethene ug/L 25.720 117 70-1302.2J
cis-1,3-Dichloropropene ug/L 21.620 108 70-130ND
Dibromochloromethane ug/L 25.020 125 70-130ND
Dibromomethane ug/L 22.920 114 70-130ND
Dichlorodifluoromethane ug/L 32.4 M12016270-130ND
Ethylbenzene ug/L 24.920 124 70-130ND
Iodomethane ug/L 40.840 102 70-130ND
Methylene Chloride ug/L 24.520 122 70-130ND
Styrene ug/L 23.620 118 70-130ND
Tetrachloroethene ug/L 26.6 M12013370-130ND
Toluene ug/L 22.320 112 70-155ND
trans-1,2-Dichloroethene ug/L 23.120 116 70-130ND
trans-1,3-Dichloropropene ug/L 22.720 114 70-130ND
trans-1,4-Dichloro-2-butene ug/L 25.7J20 128 70-130ND
Trichloroethene ug/L 24.020 120 69-151ND
Trichlorofluoromethane ug/L 29.5 M12014870-130ND
Vinyl acetate ug/L 41.3J40 103 70-130ND
Vinyl chloride ug/L 24.620 122 70-130ND
1,2-Dichloroethane-d4 (S)%110 70-130
4-Bromofluorobenzene (S)%112 70-130
Toluene-d8 (S)%94 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92295593009
1724923SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.51J 300.51J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92295593009
1724923SAMPLE DUPLICATE:
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 0.94J 300.87J
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.56J 300.57J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 0.78J 300.73J
Chloroethane ug/L 0.64J 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.39J 300.43J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%115 1114
4-Bromofluorobenzene (S)%102 4106
Toluene-d8 (S)%98 099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36693
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92295593011, 92295593012, 92295593013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1726481
Associated Lab Samples:92295593011, 92295593012, 92295593013
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/05/16 11:170.33
1,1,1-Trichloroethane ug/L ND 1.0 05/05/16 11:170.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/05/16 11:170.40
1,1,2-Trichloroethane ug/L ND 1.0 05/05/16 11:170.29
1,1-Dichloroethane ug/L ND 5.0 05/05/16 11:170.32
1,1-Dichloroethene ug/L ND 5.0 05/05/16 11:170.56
1,2,3-Trichloropropane ug/L ND 1.0 05/05/16 11:170.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/05/16 11:172.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/05/16 11:170.27
1,2-Dichlorobenzene ug/L ND 5.0 05/05/16 11:170.30
1,2-Dichloroethane ug/L ND 1.0 05/05/16 11:170.24
1,2-Dichloropropane ug/L ND 1.0 05/05/16 11:170.27
1,4-Dichlorobenzene ug/L ND 1.0 05/05/16 11:170.33
2-Butanone (MEK)ug/L ND 100 05/05/16 11:170.96
2-Hexanone ug/L ND 50.0 05/05/16 11:170.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 05/05/16 11:170.33
Acetone ug/L ND 100 05/05/16 11:1710.0
Acrylonitrile ug/L ND 200 05/05/16 11:171.9
Benzene ug/L ND 1.0 05/05/16 11:170.25
Bromochloromethane ug/L ND 3.0 05/05/16 11:170.17
Bromodichloromethane ug/L ND 1.0 05/05/16 11:170.18
Bromoform ug/L ND 3.0 05/05/16 11:170.26
Bromomethane ug/L ND 10.0 05/05/16 11:170.29
Carbon disulfide ug/L ND 100 05/05/16 11:171.2
Carbon tetrachloride ug/L ND 1.0 05/05/16 11:170.25
Chlorobenzene ug/L ND 3.0 05/05/16 11:170.23
Chloroethane ug/L ND 10.0 05/05/16 11:170.54
Chloroform ug/L ND 5.0 05/05/16 11:170.14
Chloromethane ug/L ND 1.0 05/05/16 11:170.11
cis-1,2-Dichloroethene ug/L ND 5.0 05/05/16 11:170.19
cis-1,3-Dichloropropene ug/L ND 1.0 05/05/16 11:170.13
Dibromochloromethane ug/L ND 3.0 05/05/16 11:170.21
Dibromomethane ug/L ND 10.0 05/05/16 11:170.21
Dichlorodifluoromethane ug/L ND 5.0 05/05/16 11:170.21
Ethylbenzene ug/L ND 1.0 05/05/16 11:170.30
Iodomethane ug/L ND 10.0 05/05/16 11:170.32
Methylene Chloride ug/L ND 1.0 05/05/16 11:170.97
Styrene ug/L ND 1.0 05/05/16 11:170.26
Tetrachloroethene ug/L ND 1.0 05/05/16 11:170.46
Toluene ug/L ND 1.0 05/05/16 11:170.26
trans-1,2-Dichloroethene ug/L ND 5.0 05/05/16 11:170.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1726481
Associated Lab Samples:92295593011, 92295593012, 92295593013
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 05/05/16 11:170.26
trans-1,4-Dichloro-2-butene ug/L ND 100 05/05/16 11:171.0
Trichloroethene ug/L ND 1.0 05/05/16 11:170.47
Trichlorofluoromethane ug/L ND 1.0 05/05/16 11:170.20
Vinyl acetate ug/L ND 50.0 05/05/16 11:170.35
Vinyl chloride ug/L ND 1.0 05/05/16 11:170.62
Xylene (Total)ug/L ND 5.0 05/05/16 11:170.66
1,2-Dichloroethane-d4 (S)%88 70-130 05/05/16 11:17
4-Bromofluorobenzene (S)%97 70-130 05/05/16 11:17
Toluene-d8 (S)%101 70-130 05/05/16 11:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1726482LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 80-125
1,1,1-Trichloroethane ug/L 48.650 97 71-129
1,1,2,2-Tetrachloroethane ug/L 47.950 96 79-124
1,1,2-Trichloroethane ug/L 47.750 95 85-125
1,1-Dichloroethane ug/L 46.150 92 73-126
1,1-Dichloroethene ug/L 46.450 93 66-135
1,2,3-Trichloropropane ug/L 48.350 97 75-130
1,2-Dibromo-3-chloropropane ug/L 39.850 80 71-133
1,2-Dibromoethane (EDB)ug/L 53.350 107 83-124
1,2-Dichlorobenzene ug/L 47.650 95 80-133
1,2-Dichloroethane ug/L 41.250 82 67-128
1,2-Dichloropropane ug/L 45.250 90 75-132
1,4-Dichlorobenzene ug/L 49.250 98 78-130
2-Butanone (MEK)ug/L 73.6J100 74 61-144
2-Hexanone ug/L 81.7100 82 68-143
4-Methyl-2-pentanone (MIBK)ug/L 82.2J100 82 72-135
Acetone ug/L 74.2J100 74 48-146
Acrylonitrile ug/L 202250 81 40-160
Benzene ug/L 50.450 101 80-125
Bromochloromethane ug/L 48.150 96 71-125
Bromodichloromethane ug/L 48.750 97 78-124
Bromoform ug/L 48.550 97 71-128
Bromomethane ug/L 51.950 104 40-160
Carbon disulfide ug/L 52.2J50 104 50-160
Carbon tetrachloride ug/L 50.450 101 69-131
Chlorobenzene ug/L 48.650 97 81-122
Chloroethane ug/L 47.350 95 39-148
Chloroform ug/L 47.050 94 73-127
Chloromethane ug/L 36.550 73 44-146
cis-1,2-Dichloroethene ug/L 45.750 91 74-124
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1726482LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,3-Dichloropropene ug/L 52.650 105 72-132
Dibromochloromethane ug/L 51.750 103 78-125
Dibromomethane ug/L 49.350 99 82-120
Dichlorodifluoromethane ug/L 46.450 93 34-157
Ethylbenzene ug/L 48.450 97 79-121
Iodomethane ug/L 105100 105 39-154
Methylene Chloride ug/L 34.650 69 64-133
Styrene ug/L 47.350 95 84-126
Tetrachloroethene ug/L 50.250 100 78-122
Toluene ug/L 49.550 99 80-121
trans-1,2-Dichloroethene ug/L 45.250 90 71-127
trans-1,3-Dichloropropene ug/L 49.950 100 69-141
trans-1,4-Dichloro-2-butene ug/L 43.2J50 86 40-160
Trichloroethene ug/L 49.750 99 78-122
Trichlorofluoromethane ug/L 46.250 92 53-137
Vinyl acetate ug/L 84.5100 85 40-160
Vinyl chloride ug/L 46.950 94 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1726484MATRIX SPIKE SAMPLE:
MSSpike
Result
92295598003
1,1,1,2-Tetrachloroethane ug/L 21.820 109 70-130ND
1,1,1-Trichloroethane ug/L 22.220 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.120 100 70-130ND
1,1,2-Trichloroethane ug/L 19.120 96 70-130ND
1,1-Dichloroethane ug/L 20.620 103 70-130ND
1,1-Dichloroethene ug/L 19.920 99 70-166ND
1,2,3-Trichloropropane ug/L 19.220 96 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.720 84 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.820 114 70-130ND
1,2-Dichlorobenzene ug/L 19.520 98 70-130ND
1,2-Dichloroethane ug/L 18.020 89 70-130ND
1,2-Dichloropropane ug/L 18.820 94 70-130ND
1,4-Dichlorobenzene ug/L 20.420 102 70-130ND
2-Butanone (MEK)ug/L 30.1J40 75 70-130ND
2-Hexanone ug/L 31.9J40 80 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 32.1J40 80 70-130ND
Acetone ug/L 31.9J40 77 70-130ND
Acrylonitrile ug/L 79.4J100 79 70-130ND
Benzene ug/L 21.420 107 70-148ND
Bromochloromethane ug/L 20.820 104 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1726484MATRIX SPIKE SAMPLE:
MSSpike
Result
92295598003
Bromodichloromethane ug/L 21.120 105 70-130ND
Bromoform ug/L 19.920 100 70-130ND
Bromomethane ug/L 17.320 87 70-130ND
Carbon disulfide ug/L 22.4J20 112 70-130ND
Carbon tetrachloride ug/L 23.620 118 70-130ND
Chlorobenzene ug/L 21.320 106 70-146ND
Chloroethane ug/L 20.420 102 70-130ND
Chloroform ug/L 21.020 105 70-130ND
Chloromethane ug/L 14.220 71 70-130ND
cis-1,2-Dichloroethene ug/L 19.820 99 70-130ND
cis-1,3-Dichloropropene ug/L 21.620 108 70-130ND
Dibromochloromethane ug/L 21.720 108 70-130ND
Dibromomethane ug/L 21.820 109 70-130ND
Dichlorodifluoromethane ug/L 18.020 90 70-130ND
Ethylbenzene ug/L 21.320 106 70-130ND
Iodomethane ug/L 34.840 87 70-130ND
Methylene Chloride ug/L 12.2 M1206170-130ND
Styrene ug/L 20.720 103 70-130ND
Tetrachloroethene ug/L 23.020 115 70-130ND
Toluene ug/L 20.920 105 70-155ND
trans-1,2-Dichloroethene ug/L 19.620 98 70-130ND
trans-1,3-Dichloropropene ug/L 20.920 104 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.0J20 85 70-130ND
Trichloroethene ug/L 21.920 110 69-151ND
Trichlorofluoromethane ug/L 21.720 109 70-130ND
Vinyl acetate ug/L 30.6J40 77 70-130ND
Vinyl chloride ug/L 19.420 97 70-130ND
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92295598002
1726483SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 300.33J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92295598002
1726483SAMPLE DUPLICATE:
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 0.58J 300.57J
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.51J 300.58J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 0.43J 300.42J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.28J 300.30J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%91 388
4-Bromofluorobenzene (S)%98 2100
Toluene-d8 (S)%98 2100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 49
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 49
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92295593
TRANSYLVANIA-CALVERT
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92295593001 MPRP/21549 ICP/193528803-MW1 EPA 3010A EPA 6010
92295593002 MPRP/21549 ICP/193528803-MW2 EPA 3010A EPA 6010
92295593003 MPRP/21549 ICP/193528803-MW3 EPA 3010A EPA 6010
92295593012 MPRP/21549 ICP/193528803-FIELD BLANK EPA 3010A EPA 6010
92295593001 MERP/9334 MERC/89878803-MW1 EPA 7470 EPA 7470
92295593002 MERP/9334 MERC/89878803-MW2 EPA 7470 EPA 7470
92295593003 MERP/9334 MERC/89878803-MW3 EPA 7470 EPA 7470
92295593012 MERP/9334 MERC/89878803-FIELD BLANK EPA 7470 EPA 7470
92295593001 MSV/366638803-MW1 EPA 8260
92295593002 MSV/366638803-MW2 EPA 8260
92295593003 MSV/366638803-MW3 EPA 8260
92295593004 MSV/366638803-MW105S EPA 8260
92295593005 MSV/366638803-MW105D EPA 8260
92295593006 MSV/366638803-MW106S EPA 8260
92295593007 MSV/366638803-MW106D EPA 8260
92295593008 MSV/366638803-MW107S EPA 8260
92295593009 MSV/366638803-MW107D EPA 8260
92295593010 MSV/366638803-MW108 EPA 8260
92295593011 MSV/366938803-HW1 EPA 8260
92295593012 MSV/366938803-FIELD BLANK EPA 8260
92295593013 MSV/366938803-TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/09/2016 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 49
Page 47 of 49
Page 48 of 49
Page 49 of 49
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Appendix 2 Summary of Detections and Summary of Exceedances

Summary of Detections
WELL ID PARAMETER RESULT UNITS SWSL COLLECT DATE
8803-MW105D 1,4-Dichlorobenzene 4.9 µg/L 1 4/26/2016
8803-MW105D Benzene 1.8 µg/L 1 4/26/2016
8803-MW105D Cis-1,2-Dichloroethene 9.7 µg/L 5 4/26/2016
8803-MW105D Chlorobenzene 11.2 µg/L 3 4/26/2016
8803-MW105S Chloromethane 1 µg/L 1 4/26/2016
8803-MW105S 1,4-Dichlorobenzene 2.2 µg/L 1 4/26/2016
8803-MW106D 1,4-Dichlorobenzene 4.0 µg/L 1 4/26/2016
8803-MW106D Chlorobenzene 4.8 µg/L 3 4/26/2016
8803-MW108 1,4-Dichlorobenzene 1.8 µg/L 1 4/26/2016
8803-MW2 Barium 138 µg/L 100 4/26/2016
8803-MW3 1,4-Dichlorobenzene 13.2 µg/L 1 4/26/2016
8803-MW3 Chlorobenzene 11.6 µg/L 3 4/26/2016
Notes:µg/L = Micorgrams per liter
SWSL = NC Soild Waste Section Reporting Limit
Laboratory Reporting limit used when SWSL has not been established
Transylvania Co. Calvert Landfill
Permit No. 88-03 Page 1 of 1 Joyce Engineering
Summary of Exceedances
WELL ID PARAMETER RESULT UNITS SWSL NC 2L GPS COLLECT DATE
8803-MW3 1,4-Dichlorobenzene 13.2 µg/L 1 6 6 4/26/2016
8803-MW105D Benzene 1.8 µg/L 1 1 1 4/26/2016
Notes:µg/L = Micorgrams per liter
SWSL = NC Soild Waste Section Reporting Limit
Laboratory Reporting limit used when SWSL has not been established
NC2L = NC Groundwater Standard from 15A NCAC 2L.0202
GPS = Groundwater Protection Standard as defined by 15A NCAC 13B.1634(g)
Transylvania Co. Calvert Landfill
Permit No. 88-03 Page 1 of 1 Joyce Engineering

Appendix 3 Summary of Field Parameters

Summary of Field Parameters
WELL ID PARAMETER RESULT UNITS COLLECT DATE
8803-HW1 pH 6.23 S.U.4/26/2016
8803-HW1 Temperature 18.1 ºC 4/26/2016
8803-HW1 Conductivity 46 µS/cm 4/26/2016
8803-HW1 Turbidity 5.16 NTU 4/26/2016
8803-MW1 pH 5.85 S.U.4/26/2016
8803-MW1 Temperature 15.7 ºC 4/26/2016
8803-MW1 Conductivity 106 µS/cm 4/26/2016
8803-MW1 Turbidity 3.65 NTU 4/26/2016
8803-MW1 Static Water Level 57.20 ft 4/26/2016
8803-MW1 Well Depth 72.64 ft 4/26/2016
8803-MW105D pH 5.84 S.U.4/26/2016
8803-MW105D Temperature 17.9 ºC 4/26/2016
8803-MW105D Conductivity 803 µS/cm 4/26/2016
8803-MW105D Turbidity 5.09 NTU 4/26/2016
8803-MW105D Static Water Level 54.10 ft 4/26/2016
8803-MW105D Well Depth 87.10 ft 4/26/2016
8803-MW105S pH 6.05 S.U.4/26/2016
8803-MW105S Temperature 16.5 ºC 4/26/2016
8803-MW105S Conductivity 319 µS/cm 4/26/2016
8803-MW105S Turbidity 14.90 NTU 4/26/2016
8803-MW105S Static Water Level 45.80 ft 4/26/2016
8803-MW105S Well Depth 55.37 ft 4/26/2016
8803-MW106D pH 6.15 S.U.4/26/2016
8803-MW106D Temperature 15.1 ºC 4/26/2016
8803-MW106D Conductivity 1099 µS/cm 4/26/2016
8803-MW106D Turbidity 4.85 NTU 4/26/2016
8803-MW106D Static Water Level 2.40 ft 4/26/2016
8803-MW106D Well Depth 75.38 ft 4/26/2016
8803-MW106S pH 5.86 S.U.4/26/2016
8803-MW106S Temperature 15.1 ºC 4/26/2016
8803-MW106S Conductivity 312 µS/cm 4/26/2016
8803-MW106S Turbidity 21 NTU 4/26/2016
8803-MW106S Static Water Level 7.91 ft 4/26/2016
8803-MW106S Well Depth 22.58 ft 4/26/2016
8803-MW107D pH 6.21 S.U.4/26/2016
8803-MW107D Temperature 15.2 ºC 4/26/2016
8803-MW107D Conductivity 436 µS/cm 4/26/2016
8803-MW107D Turbidity 18.1 NTU 4/26/2016
8803-MW107D Static Water Level 50.7 ft 4/26/2016
8803-MW107D Well Depth 90.30 ft 4/26/2016
8803-MW107S pH 6.64 S.U.4/26/2016
8803-MW107S Temperature 14.9 ºC 4/26/2016
8803-MW107S Conductivity 413 µS/cm 4/26/2016
8803-MW107S Turbidity 5.94 NTU 4/26/2016
8803-MW107S Static Water Level 42.50 ft 4/26/2016
8803-MW107S Well Depth 58.84 ft 4/26/2016
8803-MW108 pH 6.49 S.U.4/26/2016
8803-MW108 Temperature 18.7 ºC 4/26/2016
8803-MW108 Conductivity 574 µS/cm 4/26/2016
8803-MW108 Turbidity 18.25 NTU 4/26/2016
8803-MW108 Static Water Level 93.00 ft 4/26/2016
8803-MW108 Well Depth 105.00 ft 4/26/2016
Transylvania Co. Calvert Landfill
Permit No. 88-03 Page 1 of 2 Joyce Engineering
Summary of Field Parameters
WELL ID PARAMETER RESULT UNITS COLLECT DATE
8803-MW2 pH 6.65 S.U.4/26/2016
8803-MW2 Temperature 15.9 ºC 4/26/2016
8803-MW2 Conductivity 521 µS/cm 4/26/2016
8803-MW2 Turbidity 6.02 NTU 4/26/2016
8803-MW2 Static Water Level 56.70 ft 4/26/2016
8803-MW2 Well Depth 83.30 ft 4/26/2016
8803-MW3 pH 6.41 S.U.4/26/2016
8803-MW3 Temperature 14.8 ºC 4/26/2016
8803-MW3 Conductivity 925 µS/cm 4/26/2016
8803-MW3 Turbidity 6.09 NTU 4/26/2016
8803-MW3 Static Water Level 2.80 ft 4/26/2016
8803-MW3 Well Depth 19.80 ft 4/26/2016
Notes:ºC= degrees Centigrade
S.U.= Standard Units
µS/cm = microsemens per cm
NTU= Nephelometric Turbidity Units
ft = feet
Transylvania Co. Calvert Landfill
Permit No. 88-03 Page 1 of 2 Joyce Engineering

Appendix 4 Summary of Monitoring Well Construction
SUMMARY OF MONITORING WELL CONSTRUCTION
GROUND TOP OF WELL DEPTH (ft.)SCREENED INTERVAL (ft.)SCREENED INTERVAL
WELL SURFACE CASING Below Below Ground Surface Elevation LITHOLOGY
NO.Elevation (ft.)Elevation (ft.)Ground Surface From:To:Top:Bottom:
MW-1 2303 2306.09 70 55 70 2248 2233 Bedrock
MW-2 2280 2282.67 80 65 80 2215 2200 Bedrock
MW-3 2208 2210.21 20 10 20 2198 2188 Saprolite
MW-4 2326 2327.55 70 60 70 2266 2256 Bedrock
MW-105S 2271 2270.55 55 40 55 2231 2216 Saprolite; Paired with MW-105D
MW-105D 2271 2270.76 87 82 87 2189 2184 Bedrock; Paired with MW-105S
MW-106S 2198 2197.12 22 7 22 2191 2176 Saprolite; Paired with MW-106D
MW-106D 2198 2197.62 75 65 75 2133 2123 Bedrock; Paired with MW-106S
MW-107S 2271 2272.79 57 42 57 2229 2214 Saprolite; Paired with MW-107D
MW-107D 2271 2273.57 87 77 87 2194 2184 Bedrock; Paired with MW-107S
MW-108 2332 2334.28 102 85 102 2247 2230 Bedrock
Notes:
Wells MW-1 and MW-2 were installed by Westinghouse Environmental and Geotechnical Services, Inc. in September 1991.
Wells MW-3 and MW-4 were installed by Merrill Well and Pump Co., Inc. in August 1989.
Wells MW-105S and MW-105D were installed by Joyce Engineering, Inc. in July 1997
Wells MW-106S, -106D, -107S, -107D, and 108 were installed by Joyce Engineering, Inc. in March 1999
All elevations are referenced to mean sea level.
Top of casing elevations were surveyed by Clarence A. Jenkins on August 15, 1997 and May 26, 1999.
All wells were constructed using 2-inch (inside diameter) casing.
Transylvania Co. Calvert Landfill
Permit No. 88-03 Page 1 of 1 Joyce Engineering