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Home My WebLink About41B-DEMO_WileyDavisRdLF_DIN26639_20160714WATERS EDGE ENVIRONMENTAL, LLC 4901 WATERS EDGE DRIVE, SUITE 201  RALEIGH, NC 27606  PHONE 919.859.9987  FAX 919.859.9930 North Carolina Groundwater/Surface Water Exceedance Notification (July 14th, 2016) Well Parameter Concentration (mg/L) NCGS (mg/L) WD-2 Benzene 0.0014 0.001 WD-2 THF 0.17 0.0046* WD-2 Barium 0.72 0.7 WD-2D THF 0.073 0.0046* WD-3 Barium 0.72 0.7 WD-4 Barium 0.86 0.7 WD-4 THF 0.018 0.0046* WD-7 Chromium 0.35 0.01 WD-8 Arsenic 0.011 0.01 WD-8 Barium 1.1 0.7 WD-8 Chromium 0.27 0.01 WD-8 Lead 0.023 0.015 WD-9 Arsenic 0.019 0.01 WD-9 Cadmium 0.0056 0.002 WD-9 Chromium 0.025 0.01 WD-9 THF 0.010 0.0046* July 2016 Groundwater and Surface Water Sampling Report Former Wiley Davis Landfill Wiley Davis Road Greensboro, North Carolina Permit #41-B August 3, 2016 Prepared For Submittal To Griffin Industrial Services, LLC Greensboro, North Carolina 27407 Prepared By Waters Edge Environmental, LLC Raleigh, North Carolina WATERS EDGE ENVIRONMENTAL, LLC 4901 WATERS EDGE DRIVE, SUITE 201  RALEIGH, NC 27606  PHONE 919.859.9987  FAX 919.859.9930 August 3, 2016 Mr. David Griffin, Jr. Griffin Industrial Services, LLC 4700 Hilltop Road Greensboro, North Carolina 27407 Reference: July 2016 Groundwater and Surface Water Sampling Report Former Wiley David Landfill Wiley Davis Road Greensboro, North Carolina Permit #41-B Waters Edge Job No. R5-34 Dear Mr. Griffin: Waters Edge Environmental has completed the July 2016 groundwater and surface water sampling event at the above mentioned facility. If you have any questions regarding the information contained herein, please do not hesitate to contact our office at 919.859.9987. Sincerely, WATERS EDGE ENVIRONMENTAL, LLC Phillip L Rahn, P.G. President cc: Ms. Christine Ritter- NCDENR 16-063/PLR/aht ii Table of Contents 1 Introduction 1 2 Groundwater Sampling Activities 1 2.1 Monitor Well Sampling 1 2.2 Surface Water Sampling 1 3 Assessment Results 2 3.1 Groundwater Conditions 2 3.2 Groundwater Laboratory Analytical Results 2 3.3 Surface Water Laboratory Analytical Results 3 4 Conclusions and Recommendations 4 Figures Figure No. Title 1 Site Location Map 2 Aerial Photograph Map 3 Groundwater Potentiometric Surface (July 2016) Tables Table No. Title 1 Groundwater Elevation Data 2 Hydraulic Gradient Data 3 Groundwater / Surface Water Analytical Results Appendices Appendix Title A Laboratory Analytical Results Page 1 of 4 July 2016 Ground and Surface Water Sampling Report Former Wiley Davis Landfill Wiley Davis Road Greensboro, North Carolina Permit #41-B August 3, 2016 1 Introduction A groundwater and surface water assessment is ongoing at the former Wiley Davis Landfill (Permit #41-B) located on Wiley Davis Road in Greensboro, North Carolina (see Figures 1 and 2). The purpose of this assessment is to determine the presence, extent, and concentration of contaminants present in groundwater and/or surface water, the horizontal and vertical extent of contamination which may originate from the landfill, the direction and rate of migration of the contaminants in the groundwater, and the possible source(s) of contamination detected in the groundwater and/or surface water. This assessment is being performed in accordance with the Water Quality Monitoring Plan (Babb & Associates, P.A. and EcoLogic Associates, P.C. - Revised August 1999) and the Groundwater Assessment Plan (Babb & Associates, P.A. and EcoLogic Associates, P.C. - Revised August 1999). Since 2005 the sampling responsibilities have been contracted with Waters Edge Environmental, LLC (Waters Edge). Herein contains an account of the field sampling, laboratory analytical results and our conclusions and recommendations for the site. 2 Groundwater Sampling Activities 2.1 Monitoring Well Sampling On July 14, 2016. a Waters Edge environmental technician was mobilized to the site for the groundwater sampling activities. Prior to the sampling event, depth-to-groundwater measurements were made to the nearest 0.01 foot at each monitoring well using an electric water level indicator (see Tables 1 and 2). Groundwater samples were collected from wells WD-1, WD-2, WD-2D, WD-3, WD-3D, WD-4, WD-4D, WD-7, WD-8, and WD-9. Groundwater samples were analyzed for volatile organic compounds (VOCs) and tetrahydrofuran (THF) according to EPA Method 8260B and total RCRA metals (EPA Method 6010 and 7470- see summary of analytical results in Table 3 and documentation in Appendix A). 2.3 Surface Water Sampling On July 14, 2016, both upgradient (SW-1 see Figure 2) and downgradient (SW-2 see Figure 2) surface water samples were collected and analyzed for VOCs and THF according to EPA July 2016 Ground & Surface Water Sampling Report Wiley Davis Landfill Greensboro, North Carolina August 3, 2016 16-063 Page 2 of 4 Method 8260B and total RCRA metals (EPA Method 6010 and 7470- see summary of analytical results in Table 3 and documentation in Appendix A). 3 Assessment Results 3.1 Groundwater Conditions On July 14, 2016 water level measurements collected from the shallow wells indicate the shallow water table elevations range from 816.55 feet (WD-7) to 786.58 feet (WD-3) above mean sea level (msl). We would add that WD-2, WD-2D, WD-8 and WD-9 have not been surveyed to add as a data point. The groundwater elevations continue to indicate an overall southwesterly flow direction for shallow groundwater. The horizontal hydraulic gradient of the shallow water table has an average gradient of 0.0162 ft/ft (see Figure 3) The vertical gradient was calculated to be 0.0529 ft/ft downward between wells WD-3 and WD-3D and -0.0927 upward between wells WD-4 and WD-4D. We would also note that WD-2/WD-2D have not been surveyed. 3.2 Groundwater Laboratory Analytical Results Laboratory analysis of groundwater samples collected had the following exceedances of North Carolina Groundwater Standards (NCGS): WD-1 No NCGS exceedances WD-2 This well had the following NCGS exceedances:  Benzene at 0.0014 mg/L versus a NCGS at 0.001 mg/L  THF at 0.17 mg/L versus a North Carolina Occupational and Environmental Epidemiology Branch Recommended 2L Standard of 0.0046 mg/L (there is no codified NCGS)  Barium at 0.72 mg/L versus a NCGS at 0.7 mg/L WD-2D This well had the following NCGS exceedances:  THF at 0.073 mg/L versus a North Carolina Occupational and Environmental Epidemiology Branch Recommended 2L Standard of 0.0046 mg/L (there is no codified NCGS) WD-3 This well had the following NCGS exceedances:  Barium at 0.72 mg/L versus a NCGS at 0.7 mg/L WD-3D No NCGS exceedances July 2016 Ground & Surface Water Sampling Report Wiley Davis Landfill Greensboro, North Carolina August 3, 2016 16-063 Page 3 of 4 WD-4 This well had the following NCGS exceedances:  Barium at 0.86 mg/L versus a NCGS at 0.7 mg/L  THF at 0.018 mg/L versus a North Carolina Occupational and Environmental Epidemiology Branch Recommended 2L Standard of 0.0046 mg/L (there is no codified NCGS) WD-4D No NCGS exceedances WD-7 This well had the following NCGS exceedances:  Chromium at 0.35 mg/L versus a NCGS at 0.01 mg/L WD-8 This well had the following NCGS exceedances:  Arsenic at 0.011 mg/L versus a NCGS at 0.01 mg/L  Barium at 1.1 mg/L versus a NCGS at 0.7 mg/L  Chromium at 0.27 mg/L versus a NCGS at 0.01 mg/L  Lead at 0.023 mg/L versus a NCGS at 0.015 mg/L WD-9 This well had the following NCGS exceedances:  Arsenic at 0.019 mg/L versus a NCGS at 0.01 mg/L  Cadmium at 0.0056 mg/L versus a NCGS at 0.002 mg/L  Chromium at 0.025 mg/L versus a NCGS at 0.01 mg/L  THF at 0.010 mg/L versus a North Carolina Occupational and Environmental Epidemiology Branch Recommended 2L Standard of 0.0046 mg/L (there is no codified NCGS) 3.3 Surface Water Laboratory Analytical Results Low levels of one inorganic constituent was detected in upstream sampling point SW-1 (barium at 0.073 mg/L), and the downstream sampling point SW-2 had one inorganic (barium at 0.12 mg/L); however, no applicable Class C surface water standards were exceeded (15A NCAC 2B .0211). July 2016 Ground & Surface Water Sampling Report Wiley Davis Landfill Greensboro, North Carolina August 3, 2016 16-063 Page 4 of 4 4 Conclusions and Recommendations Information gathered during groundwater assessment activities to date indicates the general shallow and deep groundwater flow direction (horizontal gradient) beneath the site to be to the southwest. Using a horizontal hydraulic gradient of 0.0162 ft/ft and assuming an average hydraulic conductivity in saprolite of 1E-5 cm/sec and an effective porosity of 0.25, the rate of horizontal groundwater migration would be on the order of 0.612 ft/year. Now that the landfill is no longer active and has been graded to shed runoff and covered, the infiltration of rainfall should be significantly reduced. It follows that the driving head inside the landfill will gradually decline and both the quantity and rate of leachate production and release should decrease proportionately. Leachate strength should also continue to decline as the waste stabilizes, with no further introduction of potential contaminants. Based on these recent results, we would conclude that a continued positive trend in groundwater quality downgradient of the landfill has occurred. There were several low level NCGS exceedances for arsenic, barium, cadmium, chromium, and lead. THF was also detected at low concentrations in four of the wells sampled ranging from 0.010 mg/L (WD-9) to 0.17 mg/L (WD-2) which is above the interim NCGS at 4.6 g/L. Based upon our research into THF uses, it appears one major use is for PVC pipe cement which could have been mistakenly used in the older monitoring wells; however, it was detected in WD-9. The levels in the remaining wells appear to be either stable or decreasing to below NCGS with respect to time. There were also several inorganic constituents detected in the newly emplaced monitoring wells WD-8 and WD-9. Based on the total absence of VOCs, we would still conclude that these are potentially due to sediment causing false positive readings. We believe that with continued development and sampling that the inorganic constituents will decrease. We would conclude that the plume is adequately defined horizontally. Only one RCRA metal was detected in surface water samples (barium) at concentrations well below the 2B standards. As such, we conclude that no measurable impacts to surface water by VOCs or metals have been identified during this assessment. Given the aforementioned conclusions, it is our recommendation to Wiley Davis Landfill, Inc. that monitoring of the current system be continued on a semiannual schedule and once the offsite monitoring wells reduce to below NCGS, be reduced to an annual schedule. This next sampling event would be conducted in November 2016. We would also recommend that WD-2, WD-2D, WD-8, and WD-9 be surveyed for both horizontal and vertical control. Figures Au t h o r D r a w i n g Q u a d D a t e T i t l e R5 - 3 4 . x l s G r e e n s b o r o 7 / 6 / 2 0 0 5 Jo b N o . R e p o r t D a t e F i g u r e S c a l e R5 - 3 4 1 a s s h o w n Gr e e n s b o r o , N o r t h C a r o l i n a Wi l e y D a v i s L a n d f i l l Pr o j e c t L o c a t i o n M a p WA T E R S E D G E E N V I R O N M E N T A L , L L C Pr o j e c t SI T E Au t h o r D r a w i n g L a y e r s D a t e T i t l e R5 - 3 4 . x l s 7 / 6 / 2 0 0 5 Jo b N o . R e v i s i o n F i g u r e S c a l e R5 - 3 4 2 u n k n o w n Gr e e n s b o r o , N o r t h C a r o l i n a 20 0 3 GU I L F O R D C O U N T Y S P A T I A L D A T A E X P L O R E R Wi l e y D a v i s L a n d f i l l Ae r i a l P h o t o g r a p h M a p WA T E R S E D G E E N V I R O N M E N T A L , L L C Pr o j e c t Tables Table 1 Monitoring Well Reference Points and Groundwater Elevaltions Wiley Davis Landfill, Greensboro, North Carolina Well ID Reference Point Elevation Water Level Measurement (7.14.16) Water Level Elevation WD-1 836.65 32.43 804.22 WD-3 791.35 4.77 786.58 WD-3D 793.79 9.22 784.57 WD-4 793.28 5.21 788.07 WD-4D 799.11 6.73 792.38 WD-7 828.08 11.53 816.55 Table 1 GW Elevations Table 2 Hydraulic Gradient Information Wiley Davis Landfill Greensboro, North Carolina Water Level Elevation Well I.D. 7.14.16 Gradient (ft.) (ft.) WD-1 804.22 0.0181 WD-3 786.58 WD-1 804.22 0.0169 WD-4 788.07 WD-7 816.55 0.0189 WD-1 804.22 WD-7 816.55 0.0218 WD-4 788.07 WD-4D 792.38 0.0176 WD-3D 784.57 WD-3 786.58 0.0529 WD-3D 784.57 WD-4 788.07 -0.0927 WD-4D 792.38 A Negative Hydraulic Gradient Indicates Greater Hydraulic Head in the Deeper Well or Upward Flow. Waters Edge Job No. R5-34 Wiley Davis Groundwater Table.xls, Table 2 Hydraulic Grad Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 1 Pa r a m e t e r Un i t s 2 L S t a n d a r d A u g - 9 0 M a r - 9 1 A p r - 9 1 M a y - 9 3 O c t - 9 3 A p r - 9 4 F e b - 9 6 A u g - 9 6 A p r - 9 7 N o v - 9 7 O c t - 9 8 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . bi s - ( 2 - e t h y l h e x y l ) p h t h a l a t e ug / L 3. 0 . N o t S a m p l e d N o t S a m p l e d 16 .. . . . . . Ch l o r o b e n z e n e ug / L 50 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o e t h a n e ug / L 2, 8 0 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o m e t h a n e ug / L 3. No t S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . di - n - b u t y l p h t h a l a t e ug / L 70 0 1 2 No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 70 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Me t h y l e n e C h l o r i d e ug / L 5. 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Me t h y l I o d i d e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 4- ( o - c r e s o l ) M e t h y l p h e n o l ug / L 3. 5 . No t S a m p l e d N o t S a m p l e d . . N A N A N A N A N A N A Na p h t h a l e n e ug / L 21 . No t S a m p l e d N o t S a m p l e d .. . . . . . . N- N i t r o s o d i p h e n y l a m i n e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . No t S a m p l e d N o t S a m p l e d .. . . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 1 0 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 1 5 . No t S a m p l e d N o t S a m p l e d .. . . . . . . To t a l V O C s u g / L - - 1 2 1 6 00 0 0 0 0 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 . No t S a m p l e d NA. N A . . . . . . Ba r i u m mg / l 2. 0 0 . 3 8 0 No t S a m p l e d 0. 5 8 0 0 . 3 1 4 N A 0 . 4 5 0 0 . 3 0 0 0 . 2 7 0 0 . 2 9 1 0 . 3 2 0 0 . 2 0 0 Ca d m i u m mg / l 0. 0 0 5 . No t S a m p l e d NA. N A . . . 0.006 .. Ch r o m i u m mg / l 0. 0 5 0. 1 6 0 No t S a m p l e d 0. 3 6 0 0. 0 5 0 N A 0. 0 7 0 0. 0 4 0 . 0.110 0 . 0 7 1 0 . 0 8 4 Le a d mg / l 0. 0 1 5 . No t S a m p l e d 0. 0 0 6 . N A .. . . . . Me r c u r y mg / l 0. 0 0 1 1 . No t S a m p l e d NA. N A . . . . . . Se l e n i u m mg / l 0. 0 5 . No t S a m p l e d NA. N A . . . . . . Si l v e r mg / l 0. 0 1 8 . No t S a m p l e d NA. N A . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 1 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d M a r - 0 0 S e p - 0 0 M a y - 0 1 D e c - 0 1 J u l - 0 2 J a n - 0 3 M a y - 0 5 M a r - 0 6 M a y - 0 6 N o v - 0 6 J u n - 0 7 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . . . . . . bi s - ( 2 - e t h y l h e x y l ) p h t h a l a t e ug / L 3.0 . . . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . . . . . . Ch l o r o e t h a n e ug / L 2, 8 0 0 .. . . . . . . . . . Ch l o r o m e t h a n e ug / L 3. . . . . . . . . . 2 . 5 Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . . . . . . . . . di - n - b u t y l p h t h a l a t e ug / L 700 . . . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d .. . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d .. . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d .. . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 700 . . . . . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Me t h y l I o d i d e ug / L NS . . . . . 2 . 0 N A N A N A N A N A 4- ( o - c r e s o l ) M e t h y l p h e n o l ug / L 3.5 . . . . . . . . . . . Na p h t h a l e n e ug / L 21 . . . . . . . . . . . N- N i t r o s o d i p h e n y l a m i n e ug / L No S t a n d a r d .. . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * .. . . . . . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 1 0 0 .. . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 1 5 .. . . . . . . . . . To t a l V O C s u g / L - - 00 0 0 0 2 . 0 0 0 0 0 2 . 5 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 .. . . . . . . . . . Ba r i u m mg / l 2. 0 . . 0 . 2 9 4 . 0 . 2 8 1 0 . 2 9 0 0 . 3 5 0 . 3 7 0 . 3 7 0 . 4 7 0 . 4 7 Ca d m i u m mg / l 0. 0 0 5 . 0 . 0 0 1 3 0 . 0 0 1 4 .. . . . . 0.0020 . Ch r o m i u m mg / l 0. 0 5 .. . . . . 0. 0 1 4 . . 0.11 0.041 Le a d mg / l 0. 0 1 5 .. . . . . . . . . . Me r c u r y mg / l 0. 0 0 1 1 .. . . . . . . . . . Se l e n i u m mg / l 0. 0 5 . . 0 . 0 1 0 5 .. . . . . . . Si l v e r mg / l 0. 0 1 8 .. . . . . . . . 0.0075 . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 1 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d N o v - 0 7 M a y - 0 8 N o v - 0 8 M a y - 0 9 N o v - 0 9 J u n - 1 0 N o v - 1 0 M a y - 1 1 N o v - 1 1 M a y - 1 2 D e c - 1 2 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . . . . . . Ch l o r o e t h a n e ug / L 3, 0 0 0 .. . . . . . . . . . Ch l o r o m e t h a n e ug / L 3. . . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Na p h t h a l e n e ug / L 6. . . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * .. . . . . . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 .. . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . . . . . . To t a l V O C s u g / L - - 00 0 0 0 0 0 0 0 0 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 .. . . . . . . . . . Ba r i u m mg / l 0. 7 0 . 4 7 0 . 4 6 0 . 4 0 0 . 4 1 0 . 4 8 0 . 4 0 0 . 4 6 0 . 4 3 0 . 4 7 0 . 4 4 0 . 4 6 Ca d m i u m mg / l 0. 0 0 2 . 0 . 0 0 1 2 .. . . . . . . . Ch r o m i u m mg / l 0. 0 1 0. 0 5 2 0 . 0 9 6 0 . 0 4 4 0 . 0 2 5 0 . 0 4 0 0 . 0 2 5 0 . 0 6 1 0 . 0 2 7 0 . 0 4 1 0 . 0 2 0 0 . 0 1 4 Le a d mg / l 0. 0 1 5 .. . . . . . . . . . Me r c u r y mg / l 0. 0 0 1 .. . . . . . . . . . Se l e n i u m mg / l 0. 0 2 .. . . . . . . . . . Si l v e r mg / l 0. 0 2 . 0 . 0 0 7 4 .. . . 0. 0 0 5 8 ....Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 1 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d J u n - 1 3 D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . Ch l o r o e t h a n e ug / L 3, 0 0 0 .. . . . . Ch l o r o m e t h a n e ug / L 3. . . . . 1 . 1 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . Na p h t h a l e n e ug / L 6. . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * .. . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 .. . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . To t a l V O C s u g / L - - 00 0 0 0 1 . 1 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 .. . . . . Ba r i u m mg / l 0. 7 0 . 5 0 0 . 5 2 0 . 4 8 0 . 4 4 0 . 5 2 0 . 4 9 Ca d m i u m mg / l 0. 0 0 2 .. . . . . Ch r o m i u m mg / l 0. 0 1 0. 0 2 4 0 . 0 3 3 0 . 0 1 2 0. 0 1 0 0. 0 1 4 0. 0 0 8 6 Le a d mg / l 0. 0 1 5 .. . . . . Me r c u r y mg / l 0. 0 0 1 .. . . . . Se l e n i u m mg / l 0. 0 2 .. . . . . Si l v e r mg / l 0. 0 2 .. . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 2 s Pa r a m e t e r Un i t s 2 L S t a n d a r d A u g - 9 0 M a r - 9 1 A p r - 9 1 M a y - 9 3 O c t - 9 3 A p r - 9 4 F e b - 9 6 A u g - 9 6 A p r - 9 7 N o v - 9 7 O c t - 9 8 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 . No t S a m p l e d .. . . . . 2.24 .. bi s - ( 2 - e t h y l h e x y l ) p h t h a l a t e ug / L 3. 0 6 J No t S a m p l e d .. . . . . . . . se c - b u t y l b e n z e n e ug / L 70 . No t S a m p l e d .. . . . . . . . Ch l o r o b e n z e n e ug / L 50 35 0 No t S a m p l e d 23 0 1 4 0 . 15 0 6 2 8 9 1 1 0 1 1 0 7 8 Ch l o r o e t h a n e ug / L 2, 8 0 0 . No t S a m p l e d .. . . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d . No t S a m p l e d .. . . . . . . . di - n - b u t y l p h t h a l a t e ug / L 70 0 2 5 No t S a m p l e d .. . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d 62 No t S a m p l e d 39 1 2 . 1 3 . . 5 . 0 . . 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d 5 J No t S a m p l e d .. . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d 25 No t S a m p l e d 12. . 5 . 0 . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 70 0 . No t S a m p l e d 20 5 . 9 . 5 . 0 . . 1 . 1 9 . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . No t S a m p l e d .. . . . . . . . Et h y l b e n z e n e ug / L 55 0 . No t S a m p l e d .. . . . . . . . Is o p r o p y l b e n z e n e ug / L 70 . No t S a m p l e d .. . . . . . . . p- I s o p r o p y l b e n z e n e ug / L No S t a n d a r d . No t S a m p l e d .. . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5. 0 . No t S a m p l e d 6. 0 .. . . . . . . Me t h y l - t e r t b u t y l e t h e r ug / L 20 0 . 0 . No t S a m p l e d .. . . . . . . . 4- ( o - c r e s o l ) M e t h y l p h e n o l ug / L 3. 5 . No t S a m p l e d 47 . . N A N A N A N A N A N A Na p h t h a l e n e ug / L 21 . No t S a m p l e d 10 J .. . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . No t S a m p l e d .. . . . . . . . To l u e n e ug / L 1, 0 0 0 . No t S a m p l e d .. . . . . . . . 1, 2 , 4 - T r i m e t h y l b e n z e n e ug / L 35 0 . No t S a m p l e d .. . . . . . . . 1, 3 , 5 - T r i m e t h y l b e n z e n e ug / L 35 0 . No t S a m p l e d .. . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 1 5 . No t S a m p l e d 16 .. . . . . . . Xy l e n e s ug / L 53 0 . No t S a m p l e d .. . . . . . . . To t a l V O C s u g / L - - 4 7 3 3 8 0 1 5 7 . 9 0 1 7 3 6 2 8 9 1 1 8 . 4 3 1 1 0 7 8 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 . No t S a m p l e d NA. N A . . . . . . Ba r i u m mg / l 2. 0 0 . 8 0 0 No t S a m p l e d 1. 7 0 0 1 . 3 0 0 N A 2. 2 0 0 1. 9 0 0 2. 4 0 0 2 . 1 2 7 2 . 4 0 0 2 . 4 0 0 Ca d m i u m mg / l 0. 0 0 5 . No t S a m p l e d NA . N A . . . 0 . 0 0 3 . . Ch r o m i u m mg / l 0. 0 5 . No t S a m p l e d . . N A . . . 0 . 0 0 5 . . Le a d mg / l 0. 0 1 5 . No t S a m p l e d . . N A . . . 0 . 0 0 5 . . Me r c u r y mg / l 0. 0 0 1 1 . No t S a m p l e d .. N A . . . . . . Se l e n i u m mg / l 0. 0 5 . No t S a m p l e d .. N A . . . . . . Si l v e r mg / l 0. 0 1 8 . No t S a m p l e d .. N A . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 2 s ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d M a r - 0 0 N o v - 0 6 J u n - 0 7 N o v - 0 7 M a y - 0 8 N o v - 0 8 M a y - 0 9 N o v - 0 9 J u n - 1 0 N o v - 1 0 M a y - 1 1 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 . 1. 9 1 . 7 1 . 8 1 . 8 1 . 6 1 . 5 1 . 9 1 . 9 1 . 2 1 . 8 se c - b u t y l b e n z e n e ug / L 70 . 0 .. . . 2 . 0 . . . . . . Ch l o r o b e n z e n e ug / L 50 94 7.3 . . . . . . . . . Ch l o r o e t h a n e ug / L 3, 0 0 0 .. . . . . . . . . 1 Ch l o r o m e t h a n e ug / L 3. 1 . 6 . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 205 . 0 1 . 8 . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . . . . . . Di c h l o r o d i f l u o r o m e t h a n e (f r e o n ) u g / L 1, 0 0 0 . 1. 9 .. . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6 . . 1 . 5 3 . 6 1 . 6 2 . 0 . 3 . 9 . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Et h y l b e n z e n e ug / L 60 0 . . 1 . 2 1 . 4 1 . 0 1 . 7 1 . 5 1 . 7 . . . Is o p r o p y l b e n z e n e ( C u m e n e ) u g / L 70 . . 1 . 8 2 . 3 2 . 0 1 . 7 2 . 1 2 . 3 2 . 6 2 . 1 2 . 8 p- I s o p r o p y l b e n z e n e ug / L No S t a n d a r d .1. 8 1 . 1 . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Me t h y l - t e r t b u t y l e t h e r ug / L 20 . . 1 . 2 1 . 2 . . 1 . 1 . . . . 4- ( o - c r e s o l ) M e t h y l p h e n o l ug / L 40 . . . . . N A N A N A N A N A N A Na p h t h a l e n e ug / L 6 . 3 . 3 4 . 1 5 . 3 6 . 5 3 . 1 1 . 6 6 . 4 2 . 0 . 2 . 1 Te t r a h y d r o f u r a n ug / L 4. 6 * 54 1 1 0 1 8 0 1 9 0 1 1 0 1 7 1 1 1 6 0 1 5 0 9 1 8 9 To l u e n e ug / L 60 0 . . 2 . 1 1 . 5 1 . 1 . . 1 . 2 . . . 1, 2 , 4 - T r i m e t h y l b e n z e n e ug / L 40 0 . . 3 . 3 3 . 3 . 2 . 4 2 . 0 1 . 7 . . 1 . 2 1, 3 , 5 - T r i m e t h y l b e n z e n e ug / L 40 0 . .1. 1 1 . 1 1 . 1 . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . . . . . . Xy l e n e s ug / L 50 0 . . 5 . 6 5 . 3 4 . 8 3 . 9 4 . 1 4 . 0 2 . 3 . 2 . 9 To t a l V O C s u g / L - - 1 5 3 1 2 9 . 6 2 0 4 . 7 2 1 6 . 8 1 3 1 . 9 3 3 . 4 2 4 . 9 1 8 3 . 1 1 5 8 . 8 9 4 . 3 1 0 0.8 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 . . 0. 0 1 4 0. 0 0 7 4 0 . 0 0 6 7 . 0. 0 1 9 0. 0 0 9 7 0.024 0 . 0 1 5 . Ba r i u m mg / l 0. 7 2. 2 4 0. 3 4 0 . 3 6 0 . 4 7 0 . 5 3 0 . 3 1 0 . 5 2 0 . 3 7 0.72 0.41 0 . 3 9 Ca d m i u m mg / l 0. 0 0 2 0 . 0 0 3 3 .. . . . . . . . . Ch r o m i u m mg / l 0. 0 1 . 0 . 0 0 9 2 0 . 0 0 8 8 0. 0 2 2 0 . 0 1 2 0. 0 0 9 8 0 . 0 0 8 5 0 . 0 1 0 0.038 0.010 0 . 0 0 9 1 Le a d mg / l 0. 0 1 5 .. . . . . . . 0.0088 . . Me r c u r y mg / l 0. 0 0 1 .. . . . . . . . . . Se l e n i u m mg / l 0. 0 2 .. . . . . 0. 0 1 2 .... Si l v e r mg / l 0. 0 2 . 0 . 0 0 5 0 .. . . 0. 0 0 5 0 0 . 0 0 5 4 0 . 0 0 5 4 . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 2 s ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d N o v - 1 1 M a y - 1 2 D e c - 1 2 J u n - 1 3 D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 2. 2 1 . 3 1 . 4 1 . 6 1 . 5 2 . 1 1 . 7 1 . 3 1 . 4 se c - b u t y l b e n z e n e ug / L 70 . 0 .. . . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . . . . Ch l o r o e t h a n e ug / L 3, 0 0 0 .. . . . . . . . Ch l o r o m e t h a n e ug / L 3. . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . . . . Di c h l o r o d i f l u o r o m e t h a n e (f r e o n ) u g / L 1, 0 0 0 .. . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . Et h y l b e n z e n e ug / L 600 . . . . . . . . . Is o p r o p y l b e n z e n e ( C u m e n e ) u g / L 70 3 . 0 2 . 7 2 . 4 2 . 1 2 . 9 4 . 5 2 . 7 1 . 4 1 . 6 p- I s o p r o p y l b e n z e n e ug / L No S t a n d a r d .. . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . Me t h y l - t e r t b u t y l e t h e r ug / L 20 . . . . . . . . 1 . 1 4- ( o - c r e s o l ) M e t h y l p h e n o l ug / L 40 . . . . . . . . . Na p h t h a l e n e ug / L 6 1 . 9 . . 1 . 3 1 . 0 . . 1 . 6 . Te t r a h y d r o f u r a n ug / L 4. 6 * 13 0 8 5 1 9 0 9 2 1 5 0 1 4 0 1 0 0 1 0 0 1 7 0 To l u e n e ug / L 600 . . . . . . . . . 1, 2 , 4 - T r i m e t h y l b e n z e n e ug / L 400 . . . . . . . . . 1, 3 , 5 - T r i m e t h y l b e n z e n e ug / L 400 . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . . . . Xy l e n e s ug / L 500 . . . . . . . . . To t a l V O C s u g / L - - 1 3 7 . 1 8 9 . 0 1 9 3 . 8 9 7 . 0 1 5 5 . 4 1 4 6 . 6 1 0 4 . 4 1 0 4 . 3 1 7 4 . 1 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 0 . 0 0 7 3 0 . 0 0 8 2 .. . . . . . Ba r i u m mg / l 0. 7 0. 7 1 0. 6 8 0. 8 2 0 . 7 5 0 . 8 0 0 . 7 2 0 . 8 2 0. 5 9 0.72 Ca d m i u m mg / l 0. 0 0 2 .. . . . . . . . Ch r o m i u m mg / l 0. 0 1 0. 0 1 4 0 . 0 1 1 0 . 0 1 4 0 . 0 1 2 0 . 0 1 3 0 . 0 1 2 0 . 0 1 1 0. 0 0 7 9 0 . 0 0 8 0 Le a d mg / l 0. 0 1 5 .. . . . . 0. 0 0 5 0 . 0 0 5 . Me r c u r y mg / l 0. 0 0 1 .. . . . . . . . Se l e n i u m mg / l 0. 0 2 .. . . . . 0. 0 2 9 .. Si l v e r mg / l 0. 0 2 . . 0 . 0 0 5 1 .. . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 2 d Pa r a m e t e r Un i t s 2 L S t a n d a r d A u g - 9 0 M a r - 9 1 A p r - 9 1 M a y - 9 3 O c t - 9 3 A p r - 9 4 F e b - 9 6 A u g - 9 6 A p r - 9 7 N o v - 9 7 O c t - 9 8 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 . No t S a m p l e d N o t S a m p l e d .. . . . 1.79 .. Ch l o r o b e n z e n e ug / L 50 4 7 No t S a m p l e d N o t S a m p l e d 10 0 . 11 0 1 0 0 9 3 9 4 1 1 0 5 7 Ch l o r o e t h a n e ug / L 2, 8 0 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o m e t h a n e ug / L 3. No t S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d 26 . 3 4 1 2 2 2 1 5 6 . 6 1 0 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . 7 . 2 . . . 1, 1 - D i c h l o l o e t h a n e ug / L 70 0 . No t S a m p l e d N o t S a m p l e d 6. 3 . 5 . 0 . . 1 . 8 1 . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Me t h y l e n e C h l o r i d e ug / L 5. 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . 4- ( o - c r e s o l ) M e t h y l p h e n o l ug / L 3. 5 . No t S a m p l e d N o t S a m p l e d . . N A N A N A N A N A N A Na p h t h a l e n e ug / L 21 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . No t S a m p l e d N o t S a m p l e d .. . . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 1 0 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 1 5 . No t S a m p l e d N o t S a m p l e d .. . . . . . . To t a l V O C s u g / L - - 4 7 1 3 2 . 3 0 1 4 9 1 1 2 1 2 2 . 2 1 1 2 . 6 0 1 1 6 . 6 6 7 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 . N A N A .. . . . . . . Ba r i u m mg / l 2. 0 0 . 2 0 0 N A 0 . 3 1 0 0 . 1 1 2 N A 0 . 2 3 0 0 . 1 0 0 0 . 2 5 0 0 . 1 5 8 0 . 1 9 0 0 . 1 8 0 Ca d m i u m mg / l 0. 0 0 5 . N A N A . N A . 0. 0 0 6 .... Ch r o m i u m mg / l 0. 0 5 . N A 0 . 0 3 0 . N A . 0 . 0 1 5 . . . Le a d mg / l 0. 0 1 5 0. 4 4 0 . . 0 . 0 1 5 N A . . 0 . 0 0 5 . . . Me r c u r y mg / l 0. 0 0 1 1 . N A N A . N A .. . . . . Se l e n i u m mg / l 0. 0 5 . N A N A . N A .. . . . . Si l v e r mg / l 0. 0 1 8 . N A N A . N A .. . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 2 d ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d M a r - 0 0 N o v - 0 6 J u n - 0 7 N o v - 0 8 M a y - 0 8 N o v - 0 8 M a y - 0 9 N o v - 0 9 J u n - 1 0 N o v - 1 0 M a y - 1 1 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 . 1. 6 2 . 4 2 . 0 2 . 3 1 . 3 1 . 2 .... Ch l o r o b e n z e n e ug / L 50 68 . 7 . 8 8 . 8 9 . 4 4 . 6 5 . 8 5 . 5 2 . 5 4 . 5 3 . 5 Ch l o r o e t h a n e ug / L 3, 0 0 0 . 4 . 6 .. . . . . . . . Ch l o r o m e t h a n e ug / L 3. . . . . . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 1 0 . 1 . 3 1 . 6 1 . 9 . 1 . 2 1 . 4 1 . 0 1 . 2 1 . 2 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. 1 . 9 . . . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Di c h l o r o d i f l u o r o m e t h a n e ug / L 1, 0 0 0 . . 1 . 9 . 1 . 1 .. . . . . Is o p r o p y l b e n z e n e (c u m e n e ) u g / L 70 . 2 . 1 1 . 8 3 . 6 3 . 1 1 . 2 1 . 6 1 . 5 1 . 5 . 1 . 0 p- I s o p r o p y l b e n z e n e ug / L No S t a n d a r d .3. 9 . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . 2 . 3 . . . . . Me t h y l - t e r t b u t y l e t h e r ug / L 20 . 0 . 1 . 3 .. . . . . . . . 4- ( o - c r e s o l ) M e t h y l p h e n o l ug / L 40 . . . . . N A N A N A N A N A N A Na p h t h a l e n e ug / L 6. 8 . 9 1 . 2 1 . 1 . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * 51 1 8 0 1 7 0 1 1 0 1 3 0 1 3 1 1 1 2 0 5 1 6 2 5 5 Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 .. . . . . . . . . . 1, 2 , 4 - T r i m e t h y l b e n z e n e ug / L 400 . 2 . 5 . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . . . . . . Xy l e n e s (t o t a l ) u g / L 500 . 4 . 3 . . . . . . . . . To t a l V O C s u g / L - - 1 2 9 2 1 1 . 1 1 8 6 . 4 1 2 7 . 1 1 4 7 . 8 2 2 . 4 2 0 . 8 1 2 8 . 4 5 6 . 0 6 7 . 7 6 0 . 7 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 0 . 0 1 0 8 . 0 . 0 0 5 9 . 0 . 0 0 6 8 0 . 0 0 9 2 0 . 0 0 7 6 0 . 0 0 8 4 0 . 0 0 6 8 . . Ba r i u m mg / l 0. 7 . 0 . 4 5 0 . 2 1 0 . 1 9 0 . 1 9 0 . 2 6 0 . 1 5 0 . 1 9 2.2 0.13 0 . 2 3 Ca d m i u m mg / l 0. 0 0 2 0 . 0 0 2 0 0 . 0 0 1 6 . . 0 . 0 0 1 9 . . . 0.024 .. Ch r o m i u m mg / l 0. 0 1 . 0. 0 1 6 0 . 0 1 7 0. 0 0 8 0 . 0 2 1 0. 0 1 5 0 . 0 1 2 0 . 0 1 1 0 . 2 0.0058 0.018 Le a d mg / l 0. 0 1 5 .. . . . . . . 0.069 .. Me r c u r y mg / l 0. 0 0 1 .. . . . 0. 0 0 0 2 1 .. . . . Se l e n i u m mg / l 0. 0 2 .. . . . . . . . . . Si l v e r mg / l 0. 0 2 .. . . . . . . 0.0057 . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 2 d ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d N o v - 1 1 M a y - 1 2 D e c - 1 2 J u n - 1 3 D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 4 . 4 3 . 1 3 . 5 4 . 2 4 . 8 3 . 7 4 . 7 5 . 3 6 . 3 Ch l o r o e t h a n e ug / L 3, 0 0 0 .. . . . . . . . Ch l o r o m e t h a n e ug / L 3. . . 1 . 0 . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 1 . 1 . . 1 . 1 1 . 1 1 . 1 1 . 4 1 . 2 1 . 4 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . Di c h l o r o d i f l u o r o m e t h a n e ug / L 1, 0 0 0 .. . . . . . . . Is o p r o p y l b e n z e n e (c u m e n e ) u g / L 701 . 2 . . . . . . . . p- I s o p r o p y l b e n z e n e ug / L No S t a n d a r d .. . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . Me t h y l - t e r t b u t y l e t h e r ug / L 20 . 0 .. . . . . . . . 4- ( o - c r e s o l ) M e t h y l p h e n o l ug / L 40 . . . . . . . . . Na p h t h a l e n e ug / L 6. . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * 64 4 2 3 9 5 5 3 7 3 4 5 0 6 8 7 3 Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 .. . . . . . . . 1, 2 , 4 - T r i m e t h y l b e n z e n e ug / L 400 . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . . . . Xy l e n e s (t o t a l ) u g / L 500 . . . . . . . . . To t a l V O C s u g / L - - 7 0 . 7 4 5 . 1 4 2 . 5 6 1 . 3 4 2 . 9 3 8 . 8 5 6 . 1 7 4 . 5 8 0 . 7 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 .. . . . 0. 0 1 4 .. . Ba r i u m mg / l 0. 7 0 . 0 6 5 0 . 2 0 0 . 2 7 0 . 4 5 0 . 4 2 0 . 5 7 0 . 2 7 0 . 2 7 0 . 3 Ca d m i u m mg / l 0. 0 0 2 .. . . . . . . . Ch r o m i u m mg / l 0. 0 1 . 0 . 0 0 9 7 0. 0 1 2 0 . 0 1 7 0 . 0 1 2 0 . 0 3 1 . . 0 . 0 1 Le a d mg / l 0. 0 1 5 .. . . . 0. 0 1 7 . . 0 . 0 0 7 1 Me r c u r y mg / l 0. 0 0 1 .. . . . . . . . Se l e n i u m mg / l 0. 0 2 .. . . . . 0. 0 1 2 . . Si l v e r mg / l 0. 0 2 .. . . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 3 Pa r a m e t e r Un i t s 2 L S t a n d a r d A u g - 9 0 M a r - 9 1 A p r - 9 1 M a y - 9 3 O c t - 9 3 A p r - 9 4 F e b - 9 6 A u g - 9 6 A p r - 9 7 N o v - 9 7 O c t - 9 8 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . bi s - ( 2 - e t h y l h e x y l ) p h t h a l a t e ug / L 3.0 . N o t S a m p l e d N o t S a m p l e d .. . . . . 32 . Ch l o r o b e n z e n e ug / L 50 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o e t h a n e ug / L 2,8 0 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . di - n - b u t y l p h t h a l a t e ug / L 70 0 8 J No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 70 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . cis - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Me t h y l I o d i d e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 4- ( o - c r e s o l ) M e t h y l p h e n o l ug / L 3.5 . No t S a m p l e d N o t S a m p l e d . . N A N A N A N A N A N A Na p h t h a l e n e ug / L 21 . No t S a m p l e d N o t S a m p l e d .. . . . . . . N- N i t r o s o d i p h e n y l a m i n e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . No t S a m p l e d N o t S a m p l e d .. . . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2,1 0 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Vi n y l C h l o r i d e ug / L 0.0 1 5 . No t S a m p l e d N o t S a m p l e d .. . . . . . . To t a l V O C s u g / L - - 8 . 0 00 0 0 0 0 3 2 0 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 . No t S a m p l e d NA . N A . . . 0 . 0 0 4 . . Ba r i u m mg / l 2.0 1 . 5 0 No t S a m p l e d 1. 4 0 0 0 . 6 6 9 N A 0 . 8 4 0 0 . 7 0 0 0 . 9 5 0 0 . 7 7 8 0 . 7 4 0 0 . 4 4 0 Ca d m i u m mg / l 0.0 0 5 . No t S a m p l e d NA. N A . . . 0. 0 0 6 .. Ch r o m i u m mg / l 0. 0 5 . No t S a m p l e d 0. 0 3 0 . N A . 0 . 0 2 0 . 0 . 0 0 7 0 . 0 1 8 0 . 0 1 8 Le a d mg / l 0.0 1 5 . No t S a m p l e d 0. 0 0 6 0 . 0 1 5 N A . . 0 . 0 0 5 . . 0 . 0 1 1 Me r c u r y mg / l 0. 0 0 1 1 . No t S a m p l e d NA . N A . . 0 . 0 0 0 9 0 . 0 0 0 8 . 0 . 0 0 1 1 Se l e n i u m mg / l 0. 0 5 . No t S a m p l e d NA. N A . . . . . . Si l v e r mg / l 0.0 1 8 . No t S a m p l e d NA. N A . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 3 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d M a r - 0 0 S e p - 0 0 M a y - 0 1 D e c - 0 1 J u l - 0 2 J a n - 0 3 M a y - 0 5 M a r - 0 6 M a y - 0 6 N o v - 0 6 J u n - 0 7 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . . . . . . bi s - ( 2 - e t h y l h e x y l ) p h t h a l a t e ug / L 3.0 . . . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . . . . . . Ch l o r o e t h a n e ug / L 2,8 0 0 .. . . . . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . 2 . 0 . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d .. . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d .. . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d .. . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 700 . . . . . . . . . . . cis - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Na p h t h a l e n e ug / L 21 . . . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . 10 .. 15 2 4 1 5 5 9 1 5 2 2 1 8 Tr i c h l o r o f l u o r o m e t h a n e ug / L 2,1 0 0 .. . . . . . . . . . Vi n y l C h l o r i d e ug / L 0.0 1 5 .. . . . . . . . . . To t a l V O C s u g / L - - 0 1 0 0 2 . 0 1 5 2 4 1 5 5 9 1 5 2 2 1 8 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 0 . 0 1 1 7 .. . . . 0.0 0 7 5 . . 0 . 0 0 5 2 . Ba r i u m mg / l 2.0 0 . 6 0 2 . 0 . 3 2 5 . 0 . 2 9 7 0 . 5 0 5 1 . 5 0 0 . 9 6 0 . 2 7 0 . 8 8 0 . 8 3 Ca d m i u m mg / l 0.0 0 5 0 . 0 0 4 1 0 . 0 0 1 5 0 . 0 0 1 3 .. . . . . 0.0 0 4 3 0 . 0 0 3 Ch r o m i u m mg / l 0. 0 5 .. . . . . 0.0 0 7 3 . 0 . 0 0 2 3 0 . 0 1 7 0 . 0 0 7 9 Le a d mg / l 0.0 1 5 .. . . . . . . . . . Me r c u r y mg / l 0. 0 0 1 1 .. . . . . . . . . 0. 0 0 0 4 Se l e n i u m mg / l 0. 0 5 .. . . . . . . . . . Si l v e r mg / l 0.0 1 8 .. . . . . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 3 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d N o v - 0 7 M a y - 0 8 N o v - 0 8 M a y - 0 9 J u n - 1 0 N o v - 1 0 M a y - 1 1 N o v - 1 1 M a y - 1 2 D e c - 1 2 J u n - 1 3 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . . . . . . Ch l o r o e t h a n e ug / L 3,0 0 0 .. . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . . . . . . cis - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Na p h t h a l e n e ug / L 6. . . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * 27 3 4 2 8 1 7 1 1 3 1 2 3 2 1 2 3 1 2 2 0 To l u e n e ug / L 600 . . . . . 2 3 0 . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2,0 0 0 .. . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . . . . . . To t a l V O C s u g / L - - 2 7 3 4 2 8 1 7 1 1 2 6 1 2 3 2 1 2 3 1 2 2 0 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 . 0 . 0 0 7 6 0 . 0 0 6 7 0.0 1 2 0 . 0 1 3 0 . 0 1 5 . . 0 . 0 0 6 7 . . Ba r i u m mg / l 0.7 1.1 0 . 8 4 0 . 8 2 1 . 2 0 . 7 5 0 . 9 2 0 . 8 4 0 . 7 9 0.6 8 0. 9 0 0 . 9 5 Ca d m i u m mg / l 0.0 0 2 . 0. 0 0 5 . . . 0 . 0 0 3 9 . . 0 . 0 0 1 5 . . Ch r o m i u m mg / l 0. 0 1 0 . 0 0 8 9 0. 0 2 5 . 0 . 0 0 9 3 0 . 0 0 8 0. 0 2 5 0.0 0 7 9 0.0 1 2 .. . Le a d mg / l 0.0 1 5 .. . . . . . . . . . Me r c u r y mg / l 0.0 0 1 0 . 0 0 0 2 . . 0 . 0 0 0 3 . 0 . 0 0 0 3 3 .. . . . Se l e n i u m mg / l 0. 0 2 0 . 0 1 3 . 0 . 0 1 6 .. . . . . . . Si l v e r mg / l 0. 0 2 .. . . . . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 3 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . Ch l o r o e t h a n e ug / L 3,0 0 0 .. . . . Ch l o r o m e t h a n e ug / L 3 . . . 1 . 5 . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . cis - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . Na p h t h a l e n e ug / L 6. . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * 14 2 3 2 2 2 3 . To l u e n e ug / L 600 . . . . 2 8 0 Tr i c h l o r o f l u o r o m e t h a n e ug / L 2,0 0 0 .. . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . To t a l V O C s u g / L - - 1 4 2 3 2 2 2 4 . 5 2 8 0 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 .. . . . Ba r i u m mg / l 0.7 0 . 5 6 0.9 6 0 . 8 2 0 . 8 0 0 . 7 2 Ca d m i u m mg / l 0.0 0 2 .. . . . Ch r o m i u m mg / l 0. 0 1 . 0 . 0 0 6 7 0 . 0 0 6 0 . . Le a d mg / l 0.0 1 5 .. . . . Me r c u r y mg / l 0.0 0 1 .. . . . Se l e n i u m mg / l 0. 0 2 . . 0 . 0 1 3 . . Si l v e r mg / l 0. 0 2 .. . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 3 D Pa r a m e t e r Un i t s 2 L S t a n d a r d M a r - 0 0 S e p - 0 0 M a y - 0 1 D e c - 0 1 J u l - 0 2 J a n - 0 3 M a y - 0 5 M a r - 0 6 M a y - 0 6 N o v - 0 6 J u n - 0 7 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . 3 . 0 . . . . . . . Ch l o r o e t h a n e ug / L 2, 8 0 0 .. . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d . . . 5 . 0 3 . 0 3 . 0 1 . 8 . 1 . 0 1 . 2 1 . 2 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d .. . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d .. . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 700 . . . . . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Na p h t h a l e n e ug / L 21 . . . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * 9 . 0 27 .. 35 1 9 . 54 ... Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 1 0 0 .. . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 1 5 .. . . . . . . . . . To t a l V O C s u g / L - - 9 . 0 2 7 0 8 . 0 3 8 2 2 1 . 8 5 4 1 . 0 1 . 2 1 . 2 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 .. . . . . . . . . . Ba r i u m mg / l 2. 0 . . 0 . 3 4 1 . . . 0 . 9 2 0 . 0 7 1 0 . 0 4 2 0 . 1 3 0 . 0 8 4 Ca d m i u m mg / l 0. 0 0 5 0 . 0 0 1 7 . 0 . 0 0 1 1 .. . . . . 0.0011 . Ch r o m i u m mg / l 0. 0 5 .. . . . . . 0. 0 0 3 4 0 . 0 0 2 8 0 . 0 1 0 0 . 0 0 6 7 Le a d mg / l 0. 0 1 5 .. . . . . . . . . . Me r c u r y mg / l 0. 0 0 1 1 .. . . . . . . . . 0.00026 Se l e n i u m mg / l 0. 0 5 . . 0 . 0 1 0 2 . . . 0 . 0 0 6 9 .... Si l v e r mg / l 0. 0 1 8 .. . . . . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 3 D ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d N o v - 0 7 M a y - 0 8 N o v - 0 8 M a y - 0 9 N o v - 0 9 J u n - 1 0 N o v - 1 0 M a y - 1 1 N o v - 1 1 M a y - 1 2 D e c - 1 2 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 2 . 9 1 . 4 1 . 1 . 1 . 1 . . . 1 . 1 . . Ch l o r o e t h a n e ug / L 3, 0 0 0 .. . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 2 . 7 1 . 7 1 . 3 1 . 3 1 . 3 1 . 1 1 . 2 1 . 4 1 . 1 1 . 1 1 . 1 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Na p h t h a l e n e ug / L 6. . . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * 20 1 6 .. 10 . 1 0 1 1 1 1 .. Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 .. . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . . . . . . To t a l V O C s u g / L - - 2 5 . 6 1 9 . 1 2 . 4 1 . 3 1 2 . 4 1 . 1 1 1 . 2 1 2 . 4 1 3 . 2 1 . 1 1 . 1 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 . . . 0 . 0 0 5 4 . 0 . 0 0 5 6 . 0 . 0 0 5 2 . . . Ba r i u m mg / l 0. 7 0 0 . 0 6 8 0 . 1 1 0 . 1 4 0 . 1 4 0 . 0 8 0 . 1 5 0 . 1 2 0 . 1 4 0 . 1 3 0 . 1 6 Ca d m i u m mg / l 0. 0 0 2 .. . . . . . . . . . Ch r o m i u m mg / l 0. 0 1 . 0 . 0 0 5 6 0 . 0 0 7 2 0 . 0 0 9 6 0. 0 1 1 0. 0 0 9 0. 0 1 4 0 . 0 1 4 0 . 0 1 7 0 . 0 1 2 0 . 0 1 5 Le a d mg / l 0. 0 1 5 .. . . . . . . . . . Me r c u r y mg / l 0. 0 0 1 .. . . . . . . . . . Se l e n i u m mg / l 0. 0 2 .. . . . . . . . . . Si l v e r mg / l 0. 0 2 .. . . . . . . . . . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 3 D ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d J u n - 1 3 D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . Ch l o r o e t h a n e ug / L 3, 0 0 0 .. . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . Na p h t h a l e n e ug / L 6. . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * .. . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 .. . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . To t a l V O C s u g / L - - 0 . 0 0 . 0 0 . 0 0 . 0 0 . 0 0 . 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 .. . . . . Ba r i u m mg / l 0. 7 0 . 1 4 0 . 1 4 0 . 1 0 0 . 1 4 0 . 0 6 8 0 . 0 8 9 Ca d m i u m mg / l 0. 0 0 2 .. . . . . Ch r o m i u m mg / l 0. 0 1 0. 0 1 5 0 . 0 1 1 0 . 0 1 1 0. 0 0 7 9 0 . 0 0 6 3 0 . 0 0 8 8 Le a d mg / l 0. 0 1 5 .. . . . . Me r c u r y mg / l 0. 0 0 1 .. . . . . Se l e n i u m mg / l 0. 0 2 .. . . . . Si l v e r mg / l 0. 0 2 .. . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 4 Pa r a m e t e r Un i t s 2 L S t a n d a r d A u g - 9 0 M a r - 9 1 A p r - 9 1 M a y - 9 3 O c t - 9 3 A p r - 9 4 F e b - 9 6 A u g - 9 6 A p r - 9 7 N o v - 9 7 O c t - 9 8 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o b e n z e n e ug / L 50 . No t S a m p l e d N o t S a m p l e d .. . . . 2.0 9 . . Ch l o r o e t h a n e ug / L 2,8 0 0 9 J No t S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d . No t S a m p l e d N o t S a m p l e d .. . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 70 0 8 . 0 No t S a m p l e d N o t S a m p l e d .. . . . . . . cis - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Me t h y l e n e C h l o r i d e ug / L 5. 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Na p h t h a l e n e ug / L 21 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . No t S a m p l e d N o t S a m p l e d .. . . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2,1 0 0 . No t S a m p l e d N o t S a m p l e d .. . . . . . . Vi n y l C h l o r i d e ug / L 0.0 1 5 . No t S a m p l e d N o t S a m p l e d .. . . . . . . To t a l V O C s u g / L - - 1 7 . 0 00 0 0 0 2.0 9 0 0 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 . No t S a m p l e d NA. N A . . . . . . Ba r i u m mg / l 2. 0 1 . 3 0 0 No t S a m p l e d 1.4 0 0 0 . 7 0 4 N A . 0 . 7 0 0 1 . 0 0 0 0 . 7 0 6 0 . 8 4 0 0 . 8 3 0 Ca d m i u m mg / l 0.0 0 5 . No t S a m p l e d NA . N A 1. 0 . . 0 . 0 0 2 . . Ch r o m i u m mg / l 0. 0 5 0 . 1 1 0 No t S a m p l e d 0.1 1 0 . N A .. . . . . Le a d mg / l 0.0 1 5 0 . 0 1 0 No t S a m p l e d 0.0 0 6 0 . 0 1 8 N A .. . . . . Me r c u r y mg / l 0. 0 0 1 1 . No t S a m p l e d NA. N A . . . . . . Se l e n i u m mg / l 0. 0 5 . No t S a m p l e d NA. N A . . . . . . Si l v e r mg / l 0.0 1 8 . No t S a m p l e d NA. N A . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 4 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d M a r - 0 0 S e p - 0 0 M a y - 0 1 D e c - 0 1 J u l - 0 2 J a n - 0 3 M a y - 0 5 M a r - 0 6 M a y - 0 6 N o v - 0 6 J u n - 0 7 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . 1 . 0 . . . . . Ch l o r o b e n z e n e ug / L 50 . . . 1 . 0 1 . 0 2 . 0 . 1 . 1 1 . 3 1 . 5 1 . 4 Ch l o r o e t h a n e ug / L 2,8 0 0 . . . 2 . 0 1 . 0 .. . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . . . . N A N A N A N A N A 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d .. . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d .. . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d .. . . . 2 . 0 . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 700 . . . . . . . . . . . cis - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Na p h t h a l e n e ug / L 21 . . . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . 16 .. 24 2 0 1 8 6 0 1 6 1 7 . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2,1 0 0 .. . . . . . . . . . Vi n y l C h l o r i d e ug / L 0.0 1 5 .. . . . . . . . . . To t a l V O C s u g / L - - 0 1 6 0 3 . 0 2 6 2 5 1 8 6 1 . 1 1 7 . 3 1 8 . 5 1 . 4 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 .. . . . . 0.0 0 6 0 .. . . Ba r i u m mg / l 2. 0 0 . 7 6 1 0 . 7 5 2 0 . 6 8 5 0 . 7 9 7 0 . 7 7 0 0 . 7 4 1 0 . 0 7 9 0 . 8 4 0 . 7 1 0 . 7 6 0 . 7 0 Ca d m i u m mg / l 0.0 0 5 0 . 0 0 2 1 0 . 0 0 1 5 0 . 0 0 1 7 .. . . . . . . Ch r o m i u m mg / l 0. 0 5 .. . . . . . . . 0.0 1 1 . Le a d mg / l 0.0 1 5 .. . . . . . . . . . Me r c u r y mg / l 0. 0 0 1 1 .. . . . . . . . . . Se l e n i u m mg / l 0. 0 5 .. . . . . . 0. 0 0 7 4 0 . 0 0 6 1 . . Si l v e r mg / l 0.0 1 8 . . 0 . 0 1 3 4 .. . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 4 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d N o v - 0 7 M a y - 0 8 N o v - 0 8 M a y - 0 9 J u n - 1 0 N o v - 1 0 M a y - 1 1 N o v - 1 1 M a y - 1 2 D e c - 1 2 J u n - 1 3 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 . 1 . 5 1 . 2 1 . 4 1 . 3 1 . 5 1 . 5 1 . 9 . 1 . 5 1 . 5 Ch l o r o e t h a n e ug / L 3,0 0 0 .. . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 61. 0 . . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . . . . . . cis - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Na p h t h a l e n e ug / L 6. . . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * 18 2 2 2 0 1 7 1 6 1 7 1 9 2 1 .. 20 Tr i c h l o r o f l u o r o m e t h a n e ug / L 2,0 0 0 .. . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . . . . . . To t a l V O C s u g / L - - 1 9 2 3 . 5 2 1 . 2 1 8 . 4 1 7 . 3 1 8 . 5 2 0 . 5 2 2 . 9 0 . 0 1 . 5 2 1 . 5 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 . . . 0 . 0 0 9 0 0 . 0 1 3 0 . 0 0 5 3 .. . . . Ba r i u m mg / l 0. 7 0. 7 7 0 . 7 8 0. 6 6 0.7 8 0 . 9 5 0 . 8 3 0 . 7 5 0 . 8 2 0 . 7 2 0 . 8 6 0 . 8 1 Ca d m i u m mg / l 0.0 0 2 .. . . 0.0 0 1 3 .. . . . . Ch r o m i u m mg / l 0. 0 1 0 . 0 2 0. 0 1 6 0. 0 0 5 9 . 0.0 1 6 0. 0 0 5 4 0 . 0 0 6 1 0 . 0 0 7 7 0 . 0 0 5 6 0 . 0 0 7 7 0 . 0 0 6 8 Le a d mg / l 0.0 1 5 .. . . . . . . . . . Me r c u r y mg / l 0.0 0 1 .. . . . . . . . . . Se l e n i u m mg / l 0. 0 2 .. . . . . . . . . . Si l v e r mg / l 0. 0 2 .. . . . . . 0. 0 0 5 0 . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 4 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . Ch l o r o b e n z e n e ug / L 50 1 . 5 1 . 6 1 . 6 1 . 5 1 . 6 Ch l o r o e t h a n e ug / L 3,0 0 0 .. . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . cis - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . Na p h t h a l e n e ug / L 6. . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * 25 1 4 1 6 1 5 1 8 Tr i c h l o r o f l u o r o m e t h a n e ug / L 2,0 0 0 .. . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . To t a l V O C s u g / L - - 2 7 1 5 . 6 1 7 . 6 1 6 . 5 1 9 . 6 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 .. . . . Ba r i u m mg / l 0. 7 0. 8 2 0 . 8 4 0 . 7 9 0 . 7 9 0 . 8 6 Ca d m i u m mg / l 0.0 0 2 .. . . . Ch r o m i u m mg / l 0. 0 1 0 . 0 0 6 4 0. 0 1 1 . 0 . 0 0 7 2 0 . 0 0 7 6 Le a d mg / l 0.0 1 5 .. . . . Me r c u r y mg / l 0.0 0 1 .. . . . Se l e n i u m mg / l 0. 0 2 . . 0 . 0 1 8 . . Si l v e r mg / l 0. 0 2 .. . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 4 D Pa r a m e t e r Un i t s 2 L S t a n d a r d M a r - 0 0 S e p - 0 0 M a y - 0 1 D e c - 0 1 J u l - 0 2 J a n - 0 3 M a y - 0 5 M a r - 0 6 M a y - 0 6 N o v - 0 6 J u n - 0 7 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . . . . . . Ch l o r o e t h a n e ug / L 2, 8 0 0 .. . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d .. . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d .. . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d .. . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 700 . . . . . 1 . 0 . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . 1 . 0 . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Me t h y l - t e r t - b u t y l e t h e r ug / L 200 . . . . . . 1 . 0 . . . . Na p h t h a l e n e ug / L 21 . . . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * 7 . 0 20 .. 33 2 3 1 3 6 1 .13 . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 1 0 0 .. . . 2 . 0 . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 1 5 .. . . . . . . . . . To t a l V O C s u g / L - - 7 . 0 2 0 0 0 3 5 2 5 1 4 6 1 0 1 3 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 .. . . . . . . . . . Ba r i u m mg / l 2.0 . . . . . . 0. 0 6 6 0 . 0 4 8 0 . 0 3 5 0 . 0 2 6 0 . 0 2 0 Ca d m i u m mg / l 0. 0 0 5 0 . 0 0 1 5 0 . 0 0 1 1 .. . . . . . . . Ch r o m i u m mg / l 0. 0 5 .. . . . . 0. 0 1 5 .... Le a d mg / l 0. 0 1 5 .. . . . . . . . . . Me r c u r y mg / l 0. 0 0 1 1 .. . . . . . . . . . Se l e n i u m mg / l 0. 0 5 . . 0 . 0 1 1 9 .. . . . . . . Si l v e r mg / l 0. 0 1 8 .. . . . . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 4 D ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d N o v - 0 7 M a y - 0 8 N o v - 0 8 M a y - 0 9 N o v - 0 9 J u n - 1 0 N o v - 1 0 M a y - 1 1 N o v - 1 1 M a y - 1 2 D e c - 1 2 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . . . . . . Br o m o m e t h a n e ug / L NSE . . . . . . 3 . 1 . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . . . . 1 . 4 . Ch l o r o e t h a n e ug / L 3, 0 0 0 .. . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . 1 . 0 . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . . . . . . Me t h y l - t e r t - b u t y l e t h e r ug / L 20 . . . . . . . . . . . Na p h t h a l e n e ug / L 6. . . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . 15 .. . . . . . 17 . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 .. . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . . . . . . To t a l V O C s u g / L - - 0 1 6 00 0 0 3 . 1 0 0 18.4 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 . . . 0 . 0 0 5 4 .. . . . . . Ba r i u m mg / l 0. 7 0 . 0 4 6 0 . 0 3 8 0 . 0 3 1 0 . 0 4 2 0 . 0 4 1 0 . 0 3 7 0 . 0 3 8 0 . 0 3 3 0 . 0 5 7 0 . 0 2 9 0 . 0 3 2 Ca d m i u m mg / l 0. 0 0 2 .. . . . . . . . . . Ch r o m i u m mg / l 0. 0 1 .. . . . . . . . . . Le a d mg / l 0. 0 1 5 .. . . . . . . . . . Me r c u r y mg / l 0. 0 0 1 .. . . . . . . . . . Se l e n i u m mg / l 0. 0 2 .. . . . . . . . . . Si l v e r mg / l 0. 0 2 .. . . . . . . . . . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 4 D ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d J u n - 1 3 D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . . . . . . Br o m o m e t h a n e ug / L NSE . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . Ch l o r o e t h a n e ug / L 3, 0 0 0 .. . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 200 . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . . . . . . Me t h y l - t e r t - b u t y l e t h e r ug / L 20 . . . . . . Na p h t h a l e n e ug / L 6. . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * .. . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 .. . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 .. . . . . To t a l V O C s u g / L - - 00 0 0 0 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 .. . . . . Ba r i u m mg / l 0. 7 0 . 0 3 5 0 . 0 3 1 0 . 0 3 0 0 . 0 2 9 0 . 0 2 5 0 . 0 3 2 Ca d m i u m mg / l 0. 0 0 2 .. . . . . Ch r o m i u m mg / l 0. 0 1 .. . . . . Le a d mg / l 0. 0 1 5 .. . . . . Me r c u r y mg / l 0. 0 0 1 .. . . . . Se l e n i u m mg / l 0. 0 2 .. . . . . Si l v e r mg / l 0. 0 2 .. . . . . NS E - N o S t a n d a r d E x i s t s NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 5 Pa r a m e t e r Un i t s 2 L S t a n d a r d A u g - 9 0 M a r - 9 1 A p r - 9 1 M a y - 9 3 O c t - 9 3 A p r - 9 4 F e b - 9 6 A u g - 9 6 A p r - 9 7 N o v - 9 7 O c t - 9 8 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1.0 . Not S a m p l e d N o t S a m p l e d .. . . . . . . bis - ( 2 - e t h y l h e x y l ) p h t h a l a t e ug / L 3.0 . N o t S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o b e n z e n e ug / L 50 . Not S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o e t h a n e ug / L 3, 0 0 0 . Not S a m p l e d N o t S a m p l e d .. . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d . Not S a m p l e d N o t S a m p l e d .. . . . . . . di- n - b u t y l p h t h a l a t e ug / L 70 0 6 J Not S a m p l e d N o t S a m p l e d .. . . . . . . 1,2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d . Not S a m p l e d N o t S a m p l e d .. . . . . . . 1,3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d . Not S a m p l e d N o t S a m p l e d .. . . . . . . 1,4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d . Not S a m p l e d N o t S a m p l e d .. . . . . . . 1,1 - D i c h l o l o e t h a n e ug / L 70 0 . Not S a m p l e d N o t S a m p l e d .. . . . . . . cis - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . Not S a m p l e d N o t S a m p l e d .. . . . . . . Me t h y l e n e C h l o r i d e ug / L 5.0 . Not S a m p l e d N o t S a m p l e d .. . . . . . . Me t h y l I o d i d e ug / L No S t a n d a r d . Not S a m p l e d N o t S a m p l e d .. . . . . . . 4- ( o - c r e s o l ) M e t h y l p h e n o l ug / L 3.5 . Not S a m p l e d N o t S a m p l e d . . N A N A N A N A N A N A Na p h t h a l e n e ug / L 21 . Not S a m p l e d N o t S a m p l e d .. . . . . . . N- N i t r o s o d i p h e n y l a m i n e ug / L No S t a n d a r d . Not S a m p l e d N o t S a m p l e d .. . . . . . . Te t r a h y d r o f u r a n ug / L 4.6 * . Not S a m p l e d N o t S a m p l e d .. . . . . . . Tri c h l o r o f l u o r o m e t h a n e ug / L 2, 1 0 0 . Not S a m p l e d N o t S a m p l e d .. . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 1 5 . Not S a m p l e d N o t S a m p l e d .. . . . . . . To t a l V O C s u g / L - - 6 . 0 00 0 0 0 0 0 0 Me t a l s (to t a l ) Ar s e n i c mg / l 0.0 1 . Not S a m p l e d NA. . . . . . . . Ba r i u m mg / l 0.7 0 . 4 6 0 Not S a m p l e d 0.4 9 0 0 . 1 2 8 N A . 0 . 3 0 0 0 . 0 5 6 0 . 1 9 1 1 . 0 1 . 1 Ca d m i u m mg / l 0. 0 0 2 . Not S a m p l e d NA 0 . 0 3 6 N A . . . 0 . 0 0 2 . . Ch r o m i u m mg / l 0.0 1 0 . 0 5 0 Not S a m p l e d 0.0 9 0 . N A . 0 . 0 2 0 . 0 . 0 2 1 0.1 8 0 0 . 1 9 0 Le a d mg / l 0. 0 1 5 0 . 0 0 9 Not S a m p l e d 0.0 1 1 0.0 1 7 NA . . . 0 . 0 0 4 0.0 3 9 0 . 0 3 5 Me r c u r y mg / l 0. 0 0 1 . Not S a m p l e d NA. N A . . . . . . Se l e n i u m mg / l 0.0 2 . Not S a m p l e d NA. N A . . . . . . Si l v e r mg / l 0.0 2 . Not S a m p l e d NA 0 . 0 0 6 N A . . . 0 . 0 0 4 . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bla n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 7 Pa r a m e t e r Un i t s 2 L S t a n d a r d M a r - 9 1 A p r - 9 1 M a r - 0 0 S e p - 0 0 M a y - 0 1 D e c - 0 1 J u l - 0 2 J a n - 0 3 M a y - 0 5 M a r - 0 6 M a y - 0 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 N A N A . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 . N A . . . . . . . . . Ch l o r o e t h a n e ug / L 2, 8 0 0 . N A . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L No S t a n d a r d .N A . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L No S t a n d a r d .N A . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L No S t a n d a r d .N A . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 70 0 . N A . . . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . N A . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5. 0 . N A . . . . . . . . . Na p h t h a l e n e ug / L 21 N A N A . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . N A . . . . . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 1 0 0 . N A . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 1 5 N A N A . . . . . . . . . To t a l V O C s u g / L - - 0 0 0 0 0 0 0 0 0 0 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 N A N A . . . . . . . . . Ba r i u m mg / l 2. 0 . 0 . 1 2 0 . . . . . . 0 . 0 4 5 0 . 0 8 1 0 . 0 5 4 Ca d m i u m mg / l 0. 0 0 5 N A N A . . 0 . 0 0 1 . . . . . . Ch r o m i u m mg / l 0. 0 5 . . . . 0 . 0 1 5 3 0 . 0 1 9 . . . 0 . 0 1 9 0 . 0 1 2 Le a d mg / l 0. 0 1 5 . . . . . . . . . . . Me r c u r y mg / l 0. 0 0 1 1 N A N A . . . . . . . . . Se l e n i u m mg / l 0. 0 5 N A N A . . . . . . . . . Si l v e r mg / l 0. 0 1 8 N A N A . . . . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 7 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d N o v - 0 6 J u n - 0 7 N o v - 0 7 M a y - 0 8 N o v - 0 8 M a y - 0 9 N o v - 0 9 J u n - 1 0 N o v - 1 0 M a y - 1 1 N o v - 1 1 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 . . . . . . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . . . . . . Ch l o r o e t h a n e ug / L 2, 8 0 0 . . . . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 20 0 . . . . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5. 0 . . . . . . . . . . . Na p h t h a l e n e ug / L 6. . . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . . . . . . . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 . . . . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 . . . . . . . . . . . To t a l V O C s u g / L - - 0 0 0 0 0 0 0 0 0 0 0 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 . . . . . . . . . . . Ba r i u m mg / l 0. 7 0 . 1 4 0 . 1 2 0 . 2 9 0 . 3 3 0 . 2 0 0 . 2 2 0 . 3 6 0 . 2 3 0 . 2 4 0 . 1 5 0.92 Ca d m i u m mg / l 0. 0 0 2 . . . 0 . 0 0 1 2 . . . . . . . Ch r o m i u m mg / l 0. 0 1 0. 0 5 6 0. 0 4 3 0. 2 1 0 . 2 5 0 . 0 7 5 0 . 1 3 0 . 1 7 0 . 1 5 0 . 1 4 0 . 0 9 2 0 . 5 7 Le a d mg / l 0. 0 1 5 . . . . . . . . . . . Me r c u r y mg / l 0. 0 0 1 . . . . . . . . . . . Se l e n i u m mg / l 0. 0 2 . . . . . . . . . . 0 . 0 1 4 Si l v e r mg / l 0. 0 2 . . . . . . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 7 ( c o n t i n u e d ) Pa r a m e t e r Un i t s 2 L S t a n d a r d M a y - 1 2 D e c - 1 2 J u n - 1 3 D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 . . . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . . . Ch l o r o e t h a n e ug / L 2, 8 0 0 . . . . . . . . 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 20 0 . . . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . . . Me t h y l e n e C h l o r i d e ug / L 5. 0 . . . . . . . . Na p h t h a l e n e ug / L 6. . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . . . . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 . . . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 . . . . . . . . To t a l V O C s u g / L - - 0 0 0 0 0 0 0 0 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 . . . . . . . . Ba r i u m mg / l 0. 7 0 . 4 2 0 . 6 1 0 . 5 6 0 . 5 8 0 . 8 6 0 . 2 9 0 . 1 6 0 . 6 1 Ca d m i u m mg / l 0. 0 0 2 0 . 0 0 1 3 . . . . . . . Ch r o m i u m mg / l 0. 0 1 0. 2 3 0 . 2 2 0 . 3 7 0 . 2 1 0 . 5 7 0 . 0 7 2 0 . 0 2 0 0 . 3 5 Le a d mg / l 0. 0 1 5 . . . . 0 . 0 1 3 . . 0 . 0 0 8 1 Me r c u r y mg / l 0. 0 0 1 . . . . . . . . Se l e n i u m mg / l 0. 0 2 . . . . . . . . Si l v e r mg / l 0. 0 2 . . . . . . . . NA - c o m p o u n d n o t a n a l y z e d * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 1 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 8 Pa r a m e t e r Un i t s 2 L S t a n d a r d O c t - 1 3 D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 . . . . . . Ch l o r o b e n z e n e ug / L 50 . . . . . . Ch l o r o e t h a n e ug / L 2, 8 0 0 . . . . . . Ch l o r o m e t h a n e ug / L 3 . . . . . 1 . 2 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 20 0 . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . Me t h y l e n e C h l o r i d e ug / L 5. 0 . . . . . . Na p h t h a l e n e ug / L 6. . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . . . . . . Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 . . . . . . To t a l V O C s u g / L - - 0 0 0 0 0 1 . 2 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 0. 0 2 3 .. . . 0. 0 1 1 Ba r i u m mg / l 0. 7 1. 4 2 . 0 1 . 8 0. 3 7 0. 8 4 1 . 1 Ca d m i u m mg / l 0. 0 0 2 0. 0 0 3 3 0 . 0 0 4 3 . 0. 0 0 6 7 .. Ch r o m i u m mg / l 0. 0 1 0. 4 5 0 . 5 5 0 . 4 6 0 . 0 1 2 0 . 0 1 3 0 . 2 7 Le a d mg / l 0. 0 1 5 0. 0 3 6 0 . 0 3 6 0 . 0 3 5 0. 0 0 7 3 . 0. 0 2 3 Me r c u r y mg / l 0. 0 0 1 . . . . 0 . 0 0 0 2 9 . Se l e n i u m mg / l 0. 0 2 . . . . . 0 . 0 1 3 Si l v e r mg / l 0. 0 2 . . * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Wiley Davis Groundwater Table.xls Ta b l e 1 . G r o u n d w a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v i s L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a WD - 9 Pa r a m e t e r Un i t s 2 L S t a n d a r d O c t - 1 3 D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Be n z e n e ug / L 1. 0 . . . . . . Ch l o r o b e n z e n e ug / L 50 . . 1 . 4 . . . Ch l o r o e t h a n e ug / L 2, 8 0 0 . . . . . . Ch l o r o m e t h a n e ug / L 3 . . . . . 1 . 0 1, 2 - D i c h l o r o b e n z e n e (o - D i c h l o r o ) u g / L 20 . . . . . . 1, 3 - D i c h l o r o b e n z e n e ug / L 20 0 . . . . . . 1, 4 - D i c h l o r o b e n z e n e (p - D i c h l o r o ) u g / L 6. . . . . . 1, 1 - D i c h l o l o e t h a n e ug / L 6. . . . . . ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L 70 . . . . . . Me t h y l e n e C h l o r i d e ug / L 5. 0 . . . . . . Na p h t h a l e n e ug / L 6. . . . . . Te t r a h y d r o f u r a n ug / L 4. 6 * . . 19 .. 10 Tr i c h l o r o f l u o r o m e t h a n e ug / L 2, 0 0 0 . . . . . . Vi n y l C h l o r i d e ug / L 0. 0 3 . . . . . . To t a l V O C s u g / L - - 0 0 2 0 . 4 0 0 1 1 Me t a l s (t o t a l ) Ar s e n i c mg / l 0. 0 1 . . . . . 0. 0 1 9 Ba r i u m mg / l 0. 7 0. 7 4 0. 3 8 0 . 4 1 1. 0 0. 2 6 0 . 5 5 Ca d m i u m mg / l 0. 0 0 2 0. 0 1 1 0 . 0 0 3 2 0 . 0 0 3 3 . 0. 0 0 2 8 0 . 0 0 5 6 Ch r o m i u m mg / l 0. 0 1 0. 0 3 0 . 0 1 6 0 . 0 1 5 0 . 0 2 8 0. 0 0 6 6 0. 0 2 5 Le a d mg / l 0. 0 1 5 . . 0 . 0 0 7 0 . 0 0 8 6 . 0 . 0 1 3 Me r c u r y mg / l 0. 0 0 1 . . . . . . Se l e n i u m mg / l 0. 0 2 . . . . . . Si l v e r mg / l 0. 0 2 . . . . . . * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Wiley Davis Groundwater Table.xls Ta b l e 3 . S u r f a c e W a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v is L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a SW - 1 ( u p s t r e a m ) Pa r a m e t e r Un i t s 2 B S t a n d a r d M a r - 0 0 S e p - 0 0 M a y - 0 1 D e c - 0 1 J u l - 0 2 J a n - 0 3 M a y - 0 5 M a r - 0 6 M a y - 0 6 N o v - 0 6 J u n - 0 7 Vo l a t i l e O r g a n i c C o m p o u n d s Ch l o r o b e n z e n e ug / L 488 . . . . d r y . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . . d r y . . . . . . Te t r a h y d r o f u r a n ug / L 4. 4 9 0 3 * .. . . d r y . . . . . . To t a l V O C s u g / L - - 00 0 0 0 0 0 0 0 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 .. . . d r y . . . . . . Ba r i u m mg / l 1.0 . . . . d r y . 0. 0 8 3 0 . 0 7 7 0 . 0 4 2 0 . 1 8 0 0 . 1 1 Ca d m i u m mg / l 0. 0 0 2 . 0 . 0 0 1 6 0 . 0 0 1 1 . d r y .. . . . . Ch r o m i u m mg / l 0. 0 5 .. . . d r y . . . . . . Le a d mg / l 0. 0 2 5 .. . . d r y . . . . . . Me r c u r y mg / l 0. 0 0 0 0 1 2 .. . . d r y . . . . . . Se l e n i u m mg / l 0. 0 0 5 .. . . d r y . . . . . . Si l v e r mg / l 0. 0 0 0 0 6 .. . . d r y . . . . . . SW - 1 ( u p s t r e a m c o n t . ) Pa r a m e t e r Un i t s 2 B S t a n d a r d N o v - 0 7 M a y - 0 8 N o v - 0 8 M a y - 0 9 N o v - 0 9 J u n - 1 0 N o v - 1 0 M a y - 1 1 N o v - 1 1 M a y - 1 2 D e c - 1 2 Vo l a t i l e O r g a n i c C o m p o u n d s Ch l o r o b e n z e n e ug / L 488 . . . . . . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 4 9 0 3 * .. . . . . . . . . . To t a l V O C s u g / L - - 00 0 0 0 0 0 0 0 0 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 .. . . . . . . . . . Ba r i u m mg / l 1. 0 0 . 1 1 0 . 1 2 0 . 0 8 5 0 . 0 9 9 0 . 1 5 0 . 0 7 9 0 . 0 7 3 0 . 0 5 4 0 . 0 8 6 0 . 2 8 0 . 0 6 0 Ca d m i u m mg / l 0. 0 0 2 .. . . . . . . . . . Ch r o m i u m mg / l 0. 0 5 .. . . . . 0. 0 0 7 5 .... Le a d mg / l 0. 0 2 5 .. . . . . . . . . . Me r c u r y mg / l 0. 0 0 0 0 1 2 .. . . . . . . . . . Se l e n i u m mg / l 0. 0 0 5 .. . . . . . . . . . Si l v e r mg / l 0. 0 0 0 0 6 .. . . . . . . . . . Wiley Davis Groundwater Table.xls Ta b l e 3 . S u r f a c e W a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v is L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a SW - 1 ( u p s t r e a m c o n t . ) Pa r a m e t e r Un i t s 2 B S t a n d a r d J u n - 1 3 D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Ch l o r o b e n z e n e ug / L 488 . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . . . . Te t r a h y d r o f u r a n ug / L 4. 4 9 0 3 * .. . . . . To t a l V O C s u g / L - - 00 0 0 0 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 .. . . . . Ba r i u m mg / l 1. 0 0 . 1 1 0 . 1 4 0 . 0 5 9 0 . 1 0 . 1 5 0 . 0 7 3 Ca d m i u m mg / l 0. 0 0 2 .. . . . . Ch r o m i u m mg / l 0. 0 5 .. . . . . Le a d mg / l 0. 0 2 5 .. . . . . Me r c u r y mg / l 0. 0 0 0 0 1 2 .. . . . . Se l e n i u m mg / l 0. 0 0 5 .. . . . . Si l v e r mg / l 0. 0 0 0 0 6 .. . . . . NA - c o m p o u n d n o t a n a l y z e d 2B - S t a n d a r d f o r C l a s s C S u r f a c e W a t e r * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Ta b l e 3 . S u r f a c e W a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v is L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a SW - 2 ( d o w n g r a d i e n t ) Pa r a m e t e r Un i t s 2 B S t a n d a r d M a r - 0 0 S e p - 0 0 M a y - 0 1 D e c - 0 1 J u l - 0 2 J a n - 0 3 M a y - 0 5 M a r - 0 6 M a y - 0 6 N o v - 0 6 J u n - 0 7 Vo l a t i l e O r g a n i c C o m p o u n d s Ch l o r o b e n z e n e ug / L 488 . . . 1 . 0 d r y 2 . 0 . . . . 1 . 3 Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . 1 . 0 d r y . . . . . . Te t r a h y d r o f u r a n ug / L 4. 4 9 0 3 * . 6. 0 . . d r y 8. 0 .. . . . To t a l V O C s u g / L - - 0 6 . 0 0 2 . 0 1 0 00 0 0 1 . 3 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 .. . . d r y . . . . . . Ba r i u m mg / l 1. 0 . . 0 . 1 5 0 . d r y 0 . 1 1 6 0 . 0 7 7 0 . 3 3 0 . 1 0 0 . 1 1 0 . 3 0 Ca d m i u m mg / l 0. 0 0 2 .. . . d r y . . . . . . Ch r o m i u m mg / l 0. 0 5 .. . . d r y . 0. 0 0 2 6 .... Le a d mg / l 0. 0 2 5 .. . . d r y . . . . . . Me r c u r y mg / l 0. 0 0 0 0 1 2 .. . . d r y . . . . . . Se l e n i u m mg / l 0. 0 0 5 . . 0. 0 1 4 8 .dr y . . . . . . Si l v e r mg / l 0. 0 0 0 0 6 .. . . d r y . 0. 0 0 2 6 .... SW - 2 ( d o w n g r a d i e n t c o n t . ) Pa r a m e t e r Un i t s 2 B S t a n d a r d N o v - 0 7 M a y - 0 8 N o v - 0 8 M a y - 0 9 N o v - 0 9 J u n - 1 0 N o v - 1 0 M a y - 1 1 N o v - 1 1 M a y - 1 2 D e c - 1 2 Vo l a t i l e O r g a n i c C o m p o u n d s Ch l o r o b e n z e n e ug / L 488 . . 1 . 1 . . . . . . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . . . . . . . . . Te t r a h y d r o f u r a n ug / L 4. 4 9 0 3 * .. . . . . . . . . . To t a l V O C s u g / L - - 0 0 1 . 1 00 0 0 0 0 0 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 .. . . . . . . . . . Ba r i u m mg / l 1. 0 0 . 1 0 0 . 1 2 0 . 1 5 0 . 1 2 0 . 1 6 0 . 1 1 0 . 0 9 5 0 . 0 9 6 0 . 1 8 0 . 0 7 9 0 . 1 2 Ca d m i u m mg / l 0. 0 0 2 .. . . . . . . . . . Ch r o m i u m mg / l 0. 0 5 .. . . . . . . . . . Le a d mg / l 0. 0 2 5 .. . . . . . . . . . Me r c u r y mg / l 0. 0 0 0 0 1 2 .. . . . . . . . . . Se l e n i u m mg / l 0. 0 0 5 .. . . . . . . . . . Si l v e r mg / l 0. 0 0 0 0 6 .. . . . . . . . . . Wiley Davis Groundwater Table.xls Ta b l e 3 . S u r f a c e W a t e r L a b o r a t o r y A n a l y t i c a l R e s u l t s , W i l e y D a v is L a n d f i l l , G r e e n s b o r o , N o r t h C a r o l i n a SW - 2 ( d o w n g r a d i e n t c o n t . ) Pa r a m e t e r Un i t s 2 B S t a n d a r d J u n - 1 3 D e c - 1 3 D e c - 1 4 J u n - 1 5 D e c - 1 5 J u l - 1 6 Vo l a t i l e O r g a n i c C o m p o u n d s Ch l o r o b e n z e n e ug / L 48 8 . . 1 . 0 . . . Ch l o r o f l u o r o m e t h a n e ug / L No S t a n d a r d .. . . . . Te t r a h y d r o f u r a n ug / L 4. 4 9 0 3 * .. . . . . To t a l V O C s u g / L - - 00 1 0 0 0 M et a l s (t o t a l ) Ar s e n i c mg / l 0. 0 5 .. . . . . Ba r i u m mg / l 1. 0 0 . 1 6 0 . 0 9 9 0 . 1 5 0 . 1 1 0 . 1 3 0 . 1 2 Ca d m i u m mg / l 0. 0 0 2 .. . . . . Ch r o m i u m mg / l 0. 0 5 .. . . . . Le a d mg / l 0. 0 2 5 .. . . . . Me r c u r y mg / l 0. 0 0 0 0 1 2 .. . . . . Se l e n i u m mg / l 0. 0 0 5 .. . . . . Si l v e r mg / l 0. 0 0 0 0 6 .. . . . . NA - c o m p o u n d n o t a n a l y z e d 2B - S t a n d a r d f o r C l a s s C S u r f a c e W a t e r * - R e c o m m e n d e d I n t e r i m M a x i u m A l l o w a b l e C o n c e n t r a t i o n ( I M A C ) Bl a n k c e l l s i n d i c a t e c o m p o u n d n o t d e t e c t e d a t t h e m e t h o d d e t e c t i o n l i m i t . Da t a t h r u 1 . 1 5 . 2 0 0 3 c o m p i l e d f r o m p r e v i o u s r e p o r t t a b l e s . Wiley Davis Groundwater Table.xls Appendix A #=CL# July 25, 2016 LIMS USE: FR - PHIL RAHN LIMS OBJECT ID: 92305482 92305482 Project: Pace Project No.: RE: Mr. Phil Rahn Waters Edge Environmental 4901 Water's Edge Drive Suite 201 Raleigh, NC 27606 WILEY DAVIS LANDFILL Dear Mr. Rahn: Enclosed are the analytical results for sample(s) received by the laboratory on July 18, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Brittany Gibson brittany.gibson@pacelabs.com Project Coordinator Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 1 of 56 #=CP# CERTIFICATIONS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 2 of 56 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Lab ID Sample ID Matrix Date Collected Date Received 92305482001 WD-1 Water 07/14/16 13:30 07/18/16 15:45 92305482002 WD-2 Water 07/14/16 12:30 07/18/16 15:45 92305482003 WD-2D Water 07/14/16 12:45 07/18/16 15:45 92305482004 WD-3 Water 07/14/16 12:15 07/18/16 15:45 92305482005 WD-3D Water 07/14/16 12:00 07/18/16 15:45 92305482006 WD-4 Water 07/14/16 11:15 07/18/16 15:45 92305482007 WD-4D Water 07/14/16 10:45 07/18/16 15:45 92305482008 WD-7 Water 07/14/16 10:20 07/18/16 15:45 92305482009 WD-8 Water 07/14/16 14:00 07/18/16 15:45 92305482010 WD-9 Water 07/14/16 14:30 07/18/16 15:45 92305482011 STREAM UPGRADIENT Water 07/14/16 11:30 07/18/16 15:45 92305482012 STREAM DOWNGRADIENT Water 07/14/16 13:00 07/18/16 15:45 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 3 of 56 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92305482001 WD-1 EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482002 WD-2 EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482003 WD-2D EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482004 WD-3 EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482005 WD-3D EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482006 WD-4 EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482007 WD-4D EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482008 WD-7 EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482009 WD-8 EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482010 WD-9 EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482011 STREAM UPGRADIENT EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB 92305482012 STREAM DOWNGRADIENT EPA 6010 7 PASI-ASH1 EPA 7470 1 PASI-ASER EPA 8260 65 PASI-CNB REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 4 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-1 Lab ID:92305482001 Collected:07/14/16 13:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND mg/L 07/22/16 20:52 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.49 mg/L 07/22/16 20:52 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 20:52 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium 0.0086 mg/L 07/22/16 20:52 7440-47-307/21/16 18:400.0050 0.0025 1 Lead ND mg/L 07/22/16 20:52 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 20:52 7782-49-207/21/16 18:400.010 0.0050 1 Silver ND mg/L 07/22/16 20:52 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:10 7439-97-607/20/16 05:500.00020 0.00010 1 Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/20/16 15:21 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 15:21 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 15:21 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 15:21 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 15:21 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 15:21 74-83-90.0020 0.00029 1 n-Butylbenzene ND mg/L 07/20/16 15:21 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 15:21 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 15:21 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 15:21 56-23-50.0010 0.00025 1 Chlorobenzene ND mg/L 07/20/16 15:21 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 15:21 75-00-30.0010 0.00054 1 Chloroform ND mg/L 07/20/16 15:21 67-66-30.0010 0.00014 1 Chloromethane 0.0011 mg/L 07/20/16 15:21 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 15:21 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 15:21 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 15:21 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 15:21 106-93-40.0010 0.00027 1 Dibromomethane ND mg/L 07/20/16 15:21 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene ND mg/L 07/20/16 15:21 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 15:21 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 15:21 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 15:21 75-71-80.0010 0.00021 1 1,1-Dichloroethane ND mg/L 07/20/16 15:21 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 15:21 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 15:21 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 15:21 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 15:21 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 15:21 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 15:21 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 15:21 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 15:21 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 15:21 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 15:21 108-20-30.0010 0.00012 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 5 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-1 Lab ID:92305482001 Collected:07/14/16 13:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Ethylbenzene ND mg/L 07/20/16 15:21 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 15:21 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)ND mg/L 07/20/16 15:21 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 15:21 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 15:21 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether ND mg/L 07/20/16 15:21 1634-04-40.0010 0.00021 1 Naphthalene ND mg/L 07/20/16 15:21 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 15:21 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 15:21 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 15:21 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 15:21 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 15:21 127-18-40.0010 0.00046 1 Tetrahydrofuran ND mg/L 07/20/16 15:21 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 15:21 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 15:21 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 15:21 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 15:21 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 15:21 79-00-50.0010 0.00029 1 Trichloroethene ND mg/L 07/20/16 15:21 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 15:21 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 15:21 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 15:21 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 15:21 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 15:21 108-05-40.0020 0.00035 1 Vinyl chloride ND mg/L 07/20/16 15:21 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 15:21 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 15:21 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 15:21 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)96 %07/20/16 15:21 460-00-470-130 1 1,2-Dichloroethane-d4 (S)102 %07/20/16 15:21 17060-07-070-130 1 Toluene-d8 (S)100 %07/20/16 15:21 2037-26-570-130 1 Sample:WD-2 Lab ID:92305482002 Collected:07/14/16 12:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND mg/L 07/22/16 20:55 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.72 mg/L 07/22/16 20:55 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 20:55 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium 0.0080 mg/L 07/22/16 20:55 7440-47-307/21/16 18:400.0050 0.0025 1 Lead ND mg/L 07/22/16 20:55 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 20:55 7782-49-207/21/16 18:400.010 0.0050 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 6 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-2 Lab ID:92305482002 Collected:07/14/16 12:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Silver ND mg/L 07/22/16 20:55 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:13 7439-97-607/20/16 05:500.00020 0.00010 1 Analytical Method: EPA 82608260 MSV Low Level Benzene 0.0014 mg/L 07/20/16 20:30 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 20:30 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 20:30 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 20:30 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 20:30 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 20:30 74-83-90.0020 0.00029 1 n-Butylbenzene ND mg/L 07/20/16 20:30 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 20:30 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 20:30 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 20:30 56-23-50.0010 0.00025 1 Chlorobenzene ND mg/L 07/20/16 20:30 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 20:30 75-00-30.0010 0.00054 1 Chloroform ND mg/L 07/20/16 20:30 67-66-30.0010 0.00014 1 Chloromethane ND mg/L 07/20/16 20:30 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 20:30 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 20:30 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 20:30 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 20:30 106-93-40.0010 0.00027 1 Dibromomethane ND mg/L 07/20/16 20:30 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene ND mg/L 07/20/16 20:30 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 20:30 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 20:30 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 20:30 75-71-80.0010 0.00021 1 1,1-Dichloroethane ND mg/L 07/20/16 20:30 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 20:30 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 20:30 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 20:30 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 20:30 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 20:30 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 20:30 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 20:30 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 20:30 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 20:30 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 20:30 108-20-30.0010 0.00012 1 Ethylbenzene ND mg/L 07/20/16 20:30 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 20:30 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)0.0016 mg/L 07/20/16 20:30 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 20:30 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 20:30 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether 0.0011 mg/L 07/20/16 20:30 1634-04-40.0010 0.00021 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 7 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-2 Lab ID:92305482002 Collected:07/14/16 12:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Naphthalene ND mg/L 07/20/16 20:30 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 20:30 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 20:30 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 20:30 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 20:30 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 20:30 127-18-40.0010 0.00046 1 Tetrahydrofuran 0.17 mg/L 07/20/16 20:30 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 20:30 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 20:30 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 20:30 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 20:30 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 20:30 79-00-50.0010 0.00029 1 Trichloroethene ND mg/L 07/20/16 20:30 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 20:30 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 20:30 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 20:30 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 20:30 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 20:30 108-05-40.0020 0.00035 1 Vinyl chloride ND mg/L 07/20/16 20:30 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 20:30 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 20:30 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 20:30 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)96 %07/20/16 20:30 460-00-470-130 1 1,2-Dichloroethane-d4 (S)102 %07/20/16 20:30 17060-07-070-130 1 Toluene-d8 (S)99 %07/20/16 20:30 2037-26-570-130 1 Sample:WD-2D Lab ID:92305482003 Collected:07/14/16 12:45 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND mg/L 07/22/16 20:58 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.30 mg/L 07/22/16 20:58 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 20:58 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium 0.010 mg/L 07/22/16 20:58 7440-47-307/21/16 18:400.0050 0.0025 1 Lead 0.0071 mg/L 07/22/16 20:58 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 20:58 7782-49-207/21/16 18:400.010 0.0050 1 Silver ND mg/L 07/22/16 20:58 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:15 7439-97-607/20/16 05:500.00020 0.00010 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 8 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-2D Lab ID:92305482003 Collected:07/14/16 12:45 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/20/16 20:47 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 20:47 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 20:47 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 20:47 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 20:47 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 20:47 74-83-90.0020 0.00029 1 n-Butylbenzene ND mg/L 07/20/16 20:47 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 20:47 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 20:47 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 20:47 56-23-50.0010 0.00025 1 Chlorobenzene 0.0063 mg/L 07/20/16 20:47 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 20:47 75-00-30.0010 0.00054 1 Chloroform ND mg/L 07/20/16 20:47 67-66-30.0010 0.00014 1 Chloromethane ND mg/L 07/20/16 20:47 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 20:47 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 20:47 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 20:47 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 20:47 106-93-40.0010 0.00027 1 Dibromomethane ND mg/L 07/20/16 20:47 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene 0.0014 mg/L 07/20/16 20:47 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 20:47 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 20:47 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 20:47 75-71-80.0010 0.00021 1 1,1-Dichloroethane ND mg/L 07/20/16 20:47 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 20:47 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 20:47 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 20:47 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 20:47 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 20:47 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 20:47 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 20:47 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 20:47 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 20:47 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 20:47 108-20-30.0010 0.00012 1 Ethylbenzene ND mg/L 07/20/16 20:47 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 20:47 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)ND mg/L 07/20/16 20:47 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 20:47 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 20:47 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether ND mg/L 07/20/16 20:47 1634-04-40.0010 0.00021 1 Naphthalene ND mg/L 07/20/16 20:47 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 20:47 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 20:47 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 20:47 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 20:47 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 20:47 127-18-40.0010 0.00046 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 9 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-2D Lab ID:92305482003 Collected:07/14/16 12:45 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Tetrahydrofuran 0.073 mg/L 07/20/16 20:47 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 20:47 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 20:47 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 20:47 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 20:47 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 20:47 79-00-50.0010 0.00029 1 Trichloroethene ND mg/L 07/20/16 20:47 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 20:47 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 20:47 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 20:47 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 20:47 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 20:47 108-05-40.0020 0.00035 1 Vinyl chloride ND mg/L 07/20/16 20:47 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 20:47 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 20:47 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 20:47 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)96 %07/20/16 20:47 460-00-470-130 1 1,2-Dichloroethane-d4 (S)103 %07/20/16 20:47 17060-07-070-130 1 Toluene-d8 (S)100 %07/20/16 20:47 2037-26-570-130 1 Sample:WD-3 Lab ID:92305482004 Collected:07/14/16 12:15 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND mg/L 07/22/16 21:10 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.72 mg/L 07/22/16 21:10 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 21:10 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium ND mg/L 07/22/16 21:10 7440-47-307/21/16 18:400.0050 0.0025 1 Lead ND mg/L 07/22/16 21:10 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 21:10 7782-49-207/21/16 18:400.010 0.0050 1 Silver ND mg/L 07/22/16 21:10 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:17 7439-97-607/20/16 05:500.00020 0.00010 1 Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/21/16 15:31 71-43-20.0020 0.00050 2 Bromobenzene ND mg/L 07/21/16 15:31 108-86-10.0020 0.00060 2 Bromochloromethane ND mg/L 07/21/16 15:31 74-97-50.0020 0.00034 2 Bromodichloromethane ND mg/L 07/21/16 15:31 75-27-40.0020 0.00036 2 Bromoform ND mg/L 07/21/16 15:31 75-25-20.0020 0.00052 2 Bromomethane ND mg/L 07/21/16 15:31 74-83-90.0040 0.00058 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 10 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-3 Lab ID:92305482004 Collected:07/14/16 12:15 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level n-Butylbenzene ND mg/L 07/21/16 15:31 104-51-80.0020 0.00082 2 sec-Butylbenzene ND mg/L 07/21/16 15:31 135-98-80.0020 0.00076 2 tert-Butylbenzene ND mg/L 07/21/16 15:31 98-06-60.0020 0.00080 2 Carbon tetrachloride ND mg/L 07/21/16 15:31 56-23-50.0020 0.00050 2 Chlorobenzene ND mg/L 07/21/16 15:31 108-90-70.0020 0.00046 2 Chloroethane ND mg/L 07/21/16 15:31 75-00-30.0020 0.0011 2 Chloroform ND mg/L 07/21/16 15:31 67-66-30.0020 0.00028 2 Chloromethane ND mg/L 07/21/16 15:31 74-87-30.0020 0.00022 2 2-Chlorotoluene ND mg/L 07/21/16 15:31 95-49-80.0020 0.00070 2 4-Chlorotoluene ND mg/L 07/21/16 15:31 106-43-40.0020 0.00062 2 Dibromochloromethane ND mg/L 07/21/16 15:31 124-48-10.0020 0.00042 2 1,2-Dibromoethane (EDB)ND mg/L 07/21/16 15:31 106-93-40.0020 0.00054 2 Dibromomethane ND mg/L 07/21/16 15:31 74-95-30.0020 0.00042 2 1,2-Dichlorobenzene ND mg/L 07/21/16 15:31 95-50-10.0020 0.00060 2 1,3-Dichlorobenzene ND mg/L 07/21/16 15:31 541-73-10.0020 0.00048 2 1,4-Dichlorobenzene ND mg/L 07/21/16 15:31 106-46-70.0020 0.00066 2 Dichlorodifluoromethane ND mg/L 07/21/16 15:31 75-71-80.0020 0.00042 2 1,1-Dichloroethane ND mg/L 07/21/16 15:31 75-34-30.0020 0.00064 2 1,2-Dichloroethane ND mg/L 07/21/16 15:31 107-06-20.0020 0.00048 2 1,2-Dichloroethene (Total)ND mg/L 07/21/16 15:31 540-59-00.0020 0.00098 2 1,1-Dichloroethene ND mg/L 07/21/16 15:31 75-35-40.0020 0.0011 2 cis-1,2-Dichloroethene ND mg/L 07/21/16 15:31 156-59-20.0020 0.00038 2 trans-1,2-Dichloroethene ND mg/L 07/21/16 15:31 156-60-50.0020 0.00098 2 1,2-Dichloropropane ND mg/L 07/21/16 15:31 78-87-50.0020 0.00054 2 1,3-Dichloropropane ND mg/L 07/21/16 15:31 142-28-90.0020 0.00056 2 2,2-Dichloropropane ND mg/L 07/21/16 15:31 594-20-70.0020 0.00026 2 1,1-Dichloropropene ND mg/L 07/21/16 15:31 563-58-60.0020 0.00098 2 Diisopropyl ether ND mg/L 07/21/16 15:31 108-20-30.0020 0.00024 2 Ethylbenzene ND mg/L 07/21/16 15:31 100-41-40.0020 0.00060 2 Hexachloro-1,3-butadiene ND mg/L 07/21/16 15:31 87-68-30.0020 0.0014 2 Isopropylbenzene (Cumene)ND mg/L 07/21/16 15:31 98-82-80.0020 0.00080 2 p-Isopropyltoluene ND mg/L 07/21/16 15:31 99-87-60.0020 0.00062 2 Methylene Chloride ND mg/L 07/21/16 15:31 75-09-20.0040 0.0019 2 Methyl-tert-butyl ether ND mg/L 07/21/16 15:31 1634-04-40.0020 0.00042 2 Naphthalene ND mg/L 07/21/16 15:31 91-20-30.0020 0.00048 2 n-Propylbenzene ND mg/L 07/21/16 15:31 103-65-10.0020 0.00084 2 Styrene ND mg/L 07/21/16 15:31 100-42-50.0020 0.00052 2 1,1,1,2-Tetrachloroethane ND mg/L 07/21/16 15:31 630-20-60.0020 0.00066 2 1,1,2,2-Tetrachloroethane ND mg/L 07/21/16 15:31 79-34-50.0020 0.00080 2 Tetrachloroethene ND mg/L 07/21/16 15:31 127-18-40.0020 0.00092 2 Tetrahydrofuran ND mg/L 07/21/16 15:31 109-99-90.020 0.0062 2 Toluene 0.28 mg/L 07/21/16 15:31 108-88-30.0020 0.00052 2 1,2,3-Trichlorobenzene ND mg/L 07/21/16 15:31 87-61-60.0020 0.00066 2 1,2,4-Trichlorobenzene ND mg/L 07/21/16 15:31 120-82-10.0020 0.00070 2 1,1,1-Trichloroethane ND mg/L 07/21/16 15:31 71-55-60.0020 0.00096 2 1,1,2-Trichloroethane ND mg/L 07/21/16 15:31 79-00-50.0020 0.00058 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 11 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-3 Lab ID:92305482004 Collected:07/14/16 12:15 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Trichloroethene ND mg/L 07/21/16 15:31 79-01-60.0020 0.00094 2 Trichlorofluoromethane ND mg/L 07/21/16 15:31 75-69-40.0020 0.00040 2 1,2,3-Trichloropropane ND mg/L 07/21/16 15:31 96-18-40.0020 0.00082 2 1,2,4-Trimethylbenzene ND mg/L 07/21/16 15:31 95-63-60.0020 0.00062 2 1,3,5-Trimethylbenzene ND mg/L 07/21/16 15:31 108-67-80.0020 0.00072 2 Vinyl acetate ND mg/L 07/21/16 15:31 108-05-40.0040 0.00070 2 Vinyl chloride ND mg/L 07/21/16 15:31 75-01-40.0020 0.0012 2 Xylene (Total)ND mg/L 07/21/16 15:31 1330-20-70.0020 0.0013 2 m&p-Xylene ND mg/L 07/21/16 15:31 179601-23-10.0040 0.0013 2 o-Xylene ND mg/L 07/21/16 15:31 95-47-60.0020 0.00046 2 Surrogates 4-Bromofluorobenzene (S)95 %07/21/16 15:31 460-00-470-130 2 1,2-Dichloroethane-d4 (S)104 %07/21/16 15:31 17060-07-070-130 2 Toluene-d8 (S)101 %07/21/16 15:31 2037-26-570-130 2 Sample:WD-3D Lab ID:92305482005 Collected:07/14/16 12:00 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND mg/L 07/22/16 21:13 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.089 mg/L 07/22/16 21:13 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 21:13 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium 0.0088 mg/L 07/22/16 21:13 7440-47-307/21/16 18:400.0050 0.0025 1 Lead ND mg/L 07/22/16 21:13 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 21:13 7782-49-207/21/16 18:400.010 0.0050 1 Silver ND mg/L 07/22/16 21:13 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:20 7439-97-607/20/16 05:500.00020 0.00010 1 Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/20/16 21:21 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 21:21 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 21:21 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 21:21 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 21:21 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 21:21 74-83-90.0020 0.00029 1 n-Butylbenzene ND mg/L 07/20/16 21:21 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 21:21 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 21:21 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 21:21 56-23-50.0010 0.00025 1 Chlorobenzene ND mg/L 07/20/16 21:21 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 21:21 75-00-30.0010 0.00054 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 12 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-3D Lab ID:92305482005 Collected:07/14/16 12:00 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Chloroform ND mg/L 07/20/16 21:21 67-66-30.0010 0.00014 1 Chloromethane ND mg/L 07/20/16 21:21 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 21:21 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 21:21 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 21:21 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 21:21 106-93-40.0010 0.00027 1 Dibromomethane ND mg/L 07/20/16 21:21 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene ND mg/L 07/20/16 21:21 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 21:21 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 21:21 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 21:21 75-71-80.0010 0.00021 1 1,1-Dichloroethane ND mg/L 07/20/16 21:21 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 21:21 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 21:21 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 21:21 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 21:21 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 21:21 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 21:21 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 21:21 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 21:21 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 21:21 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 21:21 108-20-30.0010 0.00012 1 Ethylbenzene ND mg/L 07/20/16 21:21 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 21:21 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)ND mg/L 07/20/16 21:21 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 21:21 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 21:21 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether ND mg/L 07/20/16 21:21 1634-04-40.0010 0.00021 1 Naphthalene ND mg/L 07/20/16 21:21 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 21:21 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 21:21 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 21:21 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 21:21 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 21:21 127-18-40.0010 0.00046 1 Tetrahydrofuran ND mg/L 07/20/16 21:21 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 21:21 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 21:21 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 21:21 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 21:21 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 21:21 79-00-50.0010 0.00029 1 Trichloroethene ND mg/L 07/20/16 21:21 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 21:21 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 21:21 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 21:21 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 21:21 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 21:21 108-05-40.0020 0.00035 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 13 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-3D Lab ID:92305482005 Collected:07/14/16 12:00 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Vinyl chloride ND mg/L 07/20/16 21:21 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 21:21 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 21:21 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 21:21 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)95 %07/20/16 21:21 460-00-470-130 1 1,2-Dichloroethane-d4 (S)104 %07/20/16 21:21 17060-07-070-130 1 Toluene-d8 (S)99 %07/20/16 21:21 2037-26-570-130 1 Sample:WD-4 Lab ID:92305482006 Collected:07/14/16 11:15 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND mg/L 07/22/16 21:17 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.86 mg/L 07/22/16 21:17 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 21:17 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium 0.0076 mg/L 07/22/16 21:17 7440-47-307/21/16 18:400.0050 0.0025 1 Lead ND mg/L 07/22/16 21:17 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 21:17 7782-49-207/21/16 18:400.010 0.0050 1 Silver ND mg/L 07/22/16 21:17 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:27 7439-97-607/20/16 05:500.00020 0.00010 1 Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/20/16 21:38 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 21:38 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 21:38 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 21:38 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 21:38 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 21:38 74-83-90.0020 0.00029 1 n-Butylbenzene ND mg/L 07/20/16 21:38 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 21:38 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 21:38 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 21:38 56-23-50.0010 0.00025 1 Chlorobenzene 0.0016 mg/L 07/20/16 21:38 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 21:38 75-00-30.0010 0.00054 1 Chloroform ND mg/L 07/20/16 21:38 67-66-30.0010 0.00014 1 Chloromethane ND mg/L 07/20/16 21:38 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 21:38 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 21:38 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 21:38 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 21:38 106-93-40.0010 0.00027 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 14 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-4 Lab ID:92305482006 Collected:07/14/16 11:15 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Dibromomethane ND mg/L 07/20/16 21:38 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene ND mg/L 07/20/16 21:38 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 21:38 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 21:38 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 21:38 75-71-80.0010 0.00021 1 1,1-Dichloroethane ND mg/L 07/20/16 21:38 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 21:38 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 21:38 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 21:38 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 21:38 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 21:38 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 21:38 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 21:38 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 21:38 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 21:38 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 21:38 108-20-30.0010 0.00012 1 Ethylbenzene ND mg/L 07/20/16 21:38 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 21:38 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)ND mg/L 07/20/16 21:38 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 21:38 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 21:38 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether ND mg/L 07/20/16 21:38 1634-04-40.0010 0.00021 1 Naphthalene ND mg/L 07/20/16 21:38 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 21:38 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 21:38 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 21:38 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 21:38 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 21:38 127-18-40.0010 0.00046 1 Tetrahydrofuran 0.018 mg/L 07/20/16 21:38 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 21:38 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 21:38 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 21:38 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 21:38 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 21:38 79-00-50.0010 0.00029 1 Trichloroethene ND mg/L 07/20/16 21:38 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 21:38 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 21:38 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 21:38 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 21:38 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 21:38 108-05-40.0020 0.00035 1 Vinyl chloride ND mg/L 07/20/16 21:38 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 21:38 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 21:38 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 21:38 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)95 %07/20/16 21:38 460-00-470-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 15 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-4 Lab ID:92305482006 Collected:07/14/16 11:15 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Surrogates 1,2-Dichloroethane-d4 (S)102 %07/20/16 21:38 17060-07-070-130 1 Toluene-d8 (S)97 %07/20/16 21:38 2037-26-570-130 1 Sample:WD-4D Lab ID:92305482007 Collected:07/14/16 10:45 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND mg/L 07/22/16 21:20 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.032 mg/L 07/22/16 21:20 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 21:20 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium ND mg/L 07/22/16 21:20 7440-47-307/21/16 18:400.0050 0.0025 1 Lead ND mg/L 07/22/16 21:20 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 21:20 7782-49-207/21/16 18:400.010 0.0050 1 Silver ND mg/L 07/22/16 21:20 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:29 7439-97-607/20/16 05:500.00020 0.00010 1 Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/20/16 15:39 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 15:39 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 15:39 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 15:39 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 15:39 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 15:39 74-83-90.0020 0.00029 1 n-Butylbenzene ND mg/L 07/20/16 15:39 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 15:39 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 15:39 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 15:39 56-23-50.0010 0.00025 1 Chlorobenzene ND mg/L 07/20/16 15:39 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 15:39 75-00-30.0010 0.00054 1 Chloroform ND mg/L 07/20/16 15:39 67-66-30.0010 0.00014 1 Chloromethane ND mg/L 07/20/16 15:39 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 15:39 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 15:39 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 15:39 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 15:39 106-93-40.0010 0.00027 1 Dibromomethane ND mg/L 07/20/16 15:39 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene ND mg/L 07/20/16 15:39 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 15:39 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 15:39 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 15:39 75-71-80.0010 0.00021 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 16 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-4D Lab ID:92305482007 Collected:07/14/16 10:45 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level 1,1-Dichloroethane ND mg/L 07/20/16 15:39 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 15:39 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 15:39 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 15:39 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 15:39 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 15:39 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 15:39 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 15:39 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 15:39 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 15:39 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 15:39 108-20-30.0010 0.00012 1 Ethylbenzene ND mg/L 07/20/16 15:39 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 15:39 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)ND mg/L 07/20/16 15:39 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 15:39 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 15:39 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether ND mg/L 07/20/16 15:39 1634-04-40.0010 0.00021 1 Naphthalene ND mg/L 07/20/16 15:39 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 15:39 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 15:39 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 15:39 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 15:39 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 15:39 127-18-40.0010 0.00046 1 Tetrahydrofuran ND mg/L 07/20/16 15:39 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 15:39 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 15:39 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 15:39 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 15:39 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 15:39 79-00-50.0010 0.00029 1 Trichloroethene ND mg/L 07/20/16 15:39 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 15:39 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 15:39 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 15:39 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 15:39 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 15:39 108-05-40.0020 0.00035 1 Vinyl chloride ND mg/L 07/20/16 15:39 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 15:39 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 15:39 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 15:39 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)97 %07/20/16 15:39 460-00-470-130 1 1,2-Dichloroethane-d4 (S)102 %07/20/16 15:39 17060-07-070-130 1 Toluene-d8 (S)100 %07/20/16 15:39 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 17 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-7 Lab ID:92305482008 Collected:07/14/16 10:20 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND mg/L 07/22/16 21:23 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.61 mg/L 07/22/16 21:23 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 21:23 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium 0.35 mg/L 07/22/16 21:23 7440-47-307/21/16 18:400.0050 0.0025 1 Lead 0.0081 mg/L 07/22/16 21:23 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 21:23 7782-49-207/21/16 18:400.010 0.0050 1 Silver ND mg/L 07/22/16 21:23 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:32 7439-97-607/20/16 05:500.00020 0.00010 1 Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/20/16 15:56 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 15:56 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 15:56 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 15:56 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 15:56 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 15:56 74-83-90.0020 0.00029 1 n-Butylbenzene ND mg/L 07/20/16 15:56 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 15:56 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 15:56 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 15:56 56-23-50.0010 0.00025 1 Chlorobenzene ND mg/L 07/20/16 15:56 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 15:56 75-00-30.0010 0.00054 1 Chloroform ND mg/L 07/20/16 15:56 67-66-30.0010 0.00014 1 Chloromethane ND mg/L 07/20/16 15:56 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 15:56 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 15:56 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 15:56 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 15:56 106-93-40.0010 0.00027 1 Dibromomethane ND mg/L 07/20/16 15:56 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene ND mg/L 07/20/16 15:56 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 15:56 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 15:56 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 15:56 75-71-80.0010 0.00021 1 1,1-Dichloroethane ND mg/L 07/20/16 15:56 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 15:56 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 15:56 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 15:56 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 15:56 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 15:56 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 15:56 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 15:56 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 15:56 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 15:56 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 15:56 108-20-30.0010 0.00012 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 18 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-7 Lab ID:92305482008 Collected:07/14/16 10:20 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Ethylbenzene ND mg/L 07/20/16 15:56 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 15:56 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)ND mg/L 07/20/16 15:56 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 15:56 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 15:56 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether ND mg/L 07/20/16 15:56 1634-04-40.0010 0.00021 1 Naphthalene ND mg/L 07/20/16 15:56 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 15:56 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 15:56 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 15:56 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 15:56 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 15:56 127-18-40.0010 0.00046 1 Tetrahydrofuran ND mg/L 07/20/16 15:56 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 15:56 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 15:56 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 15:56 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 15:56 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 15:56 79-00-50.0010 0.00029 1 Trichloroethene ND mg/L 07/20/16 15:56 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 15:56 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 15:56 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 15:56 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 15:56 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 15:56 108-05-40.0020 0.00035 1 Vinyl chloride ND mg/L 07/20/16 15:56 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 15:56 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 15:56 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 15:56 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)95 %07/20/16 15:56 460-00-470-130 1 1,2-Dichloroethane-d4 (S)102 %07/20/16 15:56 17060-07-070-130 1 Toluene-d8 (S)101 %07/20/16 15:56 2037-26-570-130 1 Sample:WD-8 Lab ID:92305482009 Collected:07/14/16 14:00 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic 0.011 mg/L 07/22/16 21:26 7440-38-207/21/16 18:400.010 0.0050 1 Barium 1.1 mg/L 07/22/16 21:26 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 21:26 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium 0.27 mg/L 07/22/16 21:26 7440-47-307/21/16 18:400.0050 0.0025 1 Lead 0.023 mg/L 07/22/16 21:26 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium 0.013 mg/L 07/22/16 21:26 7782-49-207/21/16 18:400.010 0.0050 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 19 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-8 Lab ID:92305482009 Collected:07/14/16 14:00 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Silver ND mg/L 07/22/16 21:26 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:34 7439-97-607/20/16 05:500.00020 0.00010 1 Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/20/16 16:13 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 16:13 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 16:13 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 16:13 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 16:13 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 16:13 74-83-90.0020 0.00029 1 n-Butylbenzene ND mg/L 07/20/16 16:13 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 16:13 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 16:13 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 16:13 56-23-50.0010 0.00025 1 Chlorobenzene ND mg/L 07/20/16 16:13 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 16:13 75-00-30.0010 0.00054 1 Chloroform ND mg/L 07/20/16 16:13 67-66-30.0010 0.00014 1 Chloromethane 0.0012 mg/L 07/20/16 16:13 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 16:13 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 16:13 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 16:13 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 16:13 106-93-40.0010 0.00027 1 Dibromomethane ND mg/L 07/20/16 16:13 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene ND mg/L 07/20/16 16:13 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 16:13 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 16:13 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 16:13 75-71-80.0010 0.00021 1 1,1-Dichloroethane ND mg/L 07/20/16 16:13 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 16:13 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 16:13 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 16:13 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 16:13 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 16:13 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 16:13 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 16:13 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 16:13 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 16:13 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 16:13 108-20-30.0010 0.00012 1 Ethylbenzene ND mg/L 07/20/16 16:13 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 16:13 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)ND mg/L 07/20/16 16:13 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 16:13 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 16:13 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether ND mg/L 07/20/16 16:13 1634-04-40.0010 0.00021 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 20 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-8 Lab ID:92305482009 Collected:07/14/16 14:00 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Naphthalene ND mg/L 07/20/16 16:13 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 16:13 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 16:13 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 16:13 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 16:13 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 16:13 127-18-40.0010 0.00046 1 Tetrahydrofuran ND mg/L 07/20/16 16:13 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 16:13 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 16:13 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 16:13 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 16:13 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 16:13 79-00-50.0010 0.00029 1 Trichloroethene ND mg/L 07/20/16 16:13 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 16:13 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 16:13 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 16:13 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 16:13 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 16:13 108-05-40.0020 0.00035 1 Vinyl chloride ND mg/L 07/20/16 16:13 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 16:13 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 16:13 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 16:13 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)95 %07/20/16 16:13 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %07/20/16 16:13 17060-07-070-130 1 Toluene-d8 (S)101 %07/20/16 16:13 2037-26-570-130 1 Sample:WD-9 Lab ID:92305482010 Collected:07/14/16 14:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic 0.019 mg/L 07/22/16 21:29 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.55 mg/L 07/22/16 21:29 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium 0.0056 mg/L 07/22/16 21:29 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium 0.025 mg/L 07/22/16 21:29 7440-47-307/21/16 18:400.0050 0.0025 1 Lead 0.013 mg/L 07/22/16 21:29 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 21:29 7782-49-207/21/16 18:400.010 0.0050 1 Silver ND mg/L 07/22/16 21:29 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:36 7439-97-607/20/16 05:500.00020 0.00010 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 21 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-9 Lab ID:92305482010 Collected:07/14/16 14:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/20/16 16:30 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 16:30 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 16:30 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 16:30 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 16:30 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 16:30 74-83-90.0020 0.00029 1 n-Butylbenzene ND mg/L 07/20/16 16:30 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 16:30 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 16:30 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 16:30 56-23-50.0010 0.00025 1 Chlorobenzene ND mg/L 07/20/16 16:30 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 16:30 75-00-30.0010 0.00054 1 Chloroform ND mg/L 07/20/16 16:30 67-66-30.0010 0.00014 1 Chloromethane 0.0010 mg/L 07/20/16 16:30 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 16:30 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 16:30 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 16:30 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 16:30 106-93-40.0010 0.00027 1 Dibromomethane ND mg/L 07/20/16 16:30 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene ND mg/L 07/20/16 16:30 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 16:30 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 16:30 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 16:30 75-71-80.0010 0.00021 1 1,1-Dichloroethane ND mg/L 07/20/16 16:30 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 16:30 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 16:30 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 16:30 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 16:30 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 16:30 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 16:30 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 16:30 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 16:30 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 16:30 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 16:30 108-20-30.0010 0.00012 1 Ethylbenzene ND mg/L 07/20/16 16:30 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 16:30 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)ND mg/L 07/20/16 16:30 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 16:30 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 16:30 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether ND mg/L 07/20/16 16:30 1634-04-40.0010 0.00021 1 Naphthalene ND mg/L 07/20/16 16:30 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 16:30 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 16:30 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 16:30 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 16:30 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 16:30 127-18-40.0010 0.00046 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 22 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:WD-9 Lab ID:92305482010 Collected:07/14/16 14:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Tetrahydrofuran 0.010 mg/L 07/20/16 16:30 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 16:30 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 16:30 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 16:30 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 16:30 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 16:30 79-00-50.0010 0.00029 1 Trichloroethene ND mg/L 07/20/16 16:30 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 16:30 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 16:30 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 16:30 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 16:30 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 16:30 108-05-40.0020 0.00035 1 Vinyl chloride ND mg/L 07/20/16 16:30 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 16:30 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 16:30 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 16:30 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)96 %07/20/16 16:30 460-00-470-130 1 1,2-Dichloroethane-d4 (S)103 %07/20/16 16:30 17060-07-070-130 1 Toluene-d8 (S)100 %07/20/16 16:30 2037-26-570-130 1 Sample:STREAM UPGRADIENT Lab ID:92305482011 Collected:07/14/16 11:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND mg/L 07/22/16 23:23 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.073 mg/L 07/22/16 23:23 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 23:23 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium ND mg/L 07/22/16 23:23 7440-47-307/21/16 18:400.0050 0.0025 1 Lead ND mg/L 07/22/16 23:23 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 23:23 7782-49-207/21/16 18:400.010 0.0050 1 Silver ND mg/L 07/22/16 23:23 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 07:39 7439-97-607/20/16 05:500.00020 0.00010 1 Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/20/16 16:47 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 16:47 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 16:47 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 16:47 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 16:47 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 16:47 74-83-90.0020 0.00029 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 23 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:STREAM UPGRADIENT Lab ID:92305482011 Collected:07/14/16 11:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level n-Butylbenzene ND mg/L 07/20/16 16:47 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 16:47 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 16:47 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 16:47 56-23-50.0010 0.00025 1 Chlorobenzene ND mg/L 07/20/16 16:47 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 16:47 75-00-30.0010 0.00054 1 Chloroform ND mg/L 07/20/16 16:47 67-66-30.0010 0.00014 1 Chloromethane ND mg/L 07/20/16 16:47 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 16:47 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 16:47 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 16:47 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 16:47 106-93-40.0010 0.00027 1 Dibromomethane ND mg/L 07/20/16 16:47 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene ND mg/L 07/20/16 16:47 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 16:47 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 16:47 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 16:47 75-71-80.0010 0.00021 1 1,1-Dichloroethane ND mg/L 07/20/16 16:47 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 16:47 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 16:47 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 16:47 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 16:47 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 16:47 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 16:47 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 16:47 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 16:47 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 16:47 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 16:47 108-20-30.0010 0.00012 1 Ethylbenzene ND mg/L 07/20/16 16:47 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 16:47 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)ND mg/L 07/20/16 16:47 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 16:47 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 16:47 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether ND mg/L 07/20/16 16:47 1634-04-40.0010 0.00021 1 Naphthalene ND mg/L 07/20/16 16:47 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 16:47 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 16:47 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 16:47 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 16:47 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 16:47 127-18-40.0010 0.00046 1 Tetrahydrofuran ND mg/L 07/20/16 16:47 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 16:47 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 16:47 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 16:47 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 16:47 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 16:47 79-00-50.0010 0.00029 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 24 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:STREAM UPGRADIENT Lab ID:92305482011 Collected:07/14/16 11:30 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Trichloroethene ND mg/L 07/20/16 16:47 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 16:47 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 16:47 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 16:47 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 16:47 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 16:47 108-05-40.0020 0.00035 1 Vinyl chloride ND mg/L 07/20/16 16:47 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 16:47 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 16:47 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 16:47 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)97 %07/20/16 16:47 460-00-470-130 1 1,2-Dichloroethane-d4 (S)102 %07/20/16 16:47 17060-07-070-130 1 Toluene-d8 (S)100 %07/20/16 16:47 2037-26-570-130 1 Sample:STREAM DOWNGRADIENT Lab ID:92305482012 Collected:07/14/16 13:00 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP Arsenic ND mg/L 07/22/16 23:31 7440-38-207/21/16 18:400.010 0.0050 1 Barium 0.12 mg/L 07/22/16 23:31 7440-39-307/21/16 18:400.0050 0.0025 1 Cadmium ND mg/L 07/22/16 23:31 7440-43-907/21/16 18:400.0010 0.00050 1 Chromium ND mg/L 07/22/16 23:31 7440-47-307/21/16 18:400.0050 0.0025 1 Lead ND mg/L 07/22/16 23:31 7439-92-107/21/16 18:400.0050 0.0025 1 Selenium ND mg/L 07/22/16 23:31 7782-49-207/21/16 18:400.010 0.0050 1 Silver ND mg/L 07/22/16 23:31 7440-22-407/21/16 18:400.0050 0.0025 1 Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury Mercury ND mg/L 07/21/16 04:47 7439-97-607/20/16 05:500.00020 0.00010 1 Analytical Method: EPA 82608260 MSV Low Level Benzene ND mg/L 07/20/16 17:04 71-43-20.0010 0.00025 1 Bromobenzene ND mg/L 07/20/16 17:04 108-86-10.0010 0.00030 1 Bromochloromethane ND mg/L 07/20/16 17:04 74-97-50.0010 0.00017 1 Bromodichloromethane ND mg/L 07/20/16 17:04 75-27-40.0010 0.00018 1 Bromoform ND mg/L 07/20/16 17:04 75-25-20.0010 0.00026 1 Bromomethane ND mg/L 07/20/16 17:04 74-83-90.0020 0.00029 1 n-Butylbenzene ND mg/L 07/20/16 17:04 104-51-80.0010 0.00041 1 sec-Butylbenzene ND mg/L 07/20/16 17:04 135-98-80.0010 0.00038 1 tert-Butylbenzene ND mg/L 07/20/16 17:04 98-06-60.0010 0.00040 1 Carbon tetrachloride ND mg/L 07/20/16 17:04 56-23-50.0010 0.00025 1 Chlorobenzene ND mg/L 07/20/16 17:04 108-90-70.0010 0.00023 1 Chloroethane ND mg/L 07/20/16 17:04 75-00-30.0010 0.00054 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 25 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:STREAM DOWNGRADIENT Lab ID:92305482012 Collected:07/14/16 13:00 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Chloroform ND mg/L 07/20/16 17:04 67-66-30.0010 0.00014 1 Chloromethane ND mg/L 07/20/16 17:04 74-87-30.0010 0.00011 1 2-Chlorotoluene ND mg/L 07/20/16 17:04 95-49-80.0010 0.00035 1 4-Chlorotoluene ND mg/L 07/20/16 17:04 106-43-40.0010 0.00031 1 Dibromochloromethane ND mg/L 07/20/16 17:04 124-48-10.0010 0.00021 1 1,2-Dibromoethane (EDB)ND mg/L 07/20/16 17:04 106-93-40.0010 0.00027 1 Dibromomethane ND mg/L 07/20/16 17:04 74-95-30.0010 0.00021 1 1,2-Dichlorobenzene ND mg/L 07/20/16 17:04 95-50-10.0010 0.00030 1 1,3-Dichlorobenzene ND mg/L 07/20/16 17:04 541-73-10.0010 0.00024 1 1,4-Dichlorobenzene ND mg/L 07/20/16 17:04 106-46-70.0010 0.00033 1 Dichlorodifluoromethane ND mg/L 07/20/16 17:04 75-71-80.0010 0.00021 1 1,1-Dichloroethane ND mg/L 07/20/16 17:04 75-34-30.0010 0.00032 1 1,2-Dichloroethane ND mg/L 07/20/16 17:04 107-06-20.0010 0.00024 1 1,2-Dichloroethene (Total)ND mg/L 07/20/16 17:04 540-59-00.0010 0.00049 1 1,1-Dichloroethene ND mg/L 07/20/16 17:04 75-35-40.0010 0.00056 1 cis-1,2-Dichloroethene ND mg/L 07/20/16 17:04 156-59-20.0010 0.00019 1 trans-1,2-Dichloroethene ND mg/L 07/20/16 17:04 156-60-50.0010 0.00049 1 1,2-Dichloropropane ND mg/L 07/20/16 17:04 78-87-50.0010 0.00027 1 1,3-Dichloropropane ND mg/L 07/20/16 17:04 142-28-90.0010 0.00028 1 2,2-Dichloropropane ND mg/L 07/20/16 17:04 594-20-70.0010 0.00013 1 1,1-Dichloropropene ND mg/L 07/20/16 17:04 563-58-60.0010 0.00049 1 Diisopropyl ether ND mg/L 07/20/16 17:04 108-20-30.0010 0.00012 1 Ethylbenzene ND mg/L 07/20/16 17:04 100-41-40.0010 0.00030 1 Hexachloro-1,3-butadiene ND mg/L 07/20/16 17:04 87-68-30.0010 0.00071 1 Isopropylbenzene (Cumene)ND mg/L 07/20/16 17:04 98-82-80.0010 0.00040 1 p-Isopropyltoluene ND mg/L 07/20/16 17:04 99-87-60.0010 0.00031 1 Methylene Chloride ND mg/L 07/20/16 17:04 75-09-20.0020 0.00097 1 Methyl-tert-butyl ether ND mg/L 07/20/16 17:04 1634-04-40.0010 0.00021 1 Naphthalene ND mg/L 07/20/16 17:04 91-20-30.0010 0.00024 1 n-Propylbenzene ND mg/L 07/20/16 17:04 103-65-10.0010 0.00042 1 Styrene ND mg/L 07/20/16 17:04 100-42-50.0010 0.00026 1 1,1,1,2-Tetrachloroethane ND mg/L 07/20/16 17:04 630-20-60.0010 0.00033 1 1,1,2,2-Tetrachloroethane ND mg/L 07/20/16 17:04 79-34-50.0010 0.00040 1 Tetrachloroethene ND mg/L 07/20/16 17:04 127-18-40.0010 0.00046 1 Tetrahydrofuran ND mg/L 07/20/16 17:04 109-99-90.010 0.0031 1 Toluene ND mg/L 07/20/16 17:04 108-88-30.0010 0.00026 1 1,2,3-Trichlorobenzene ND mg/L 07/20/16 17:04 87-61-60.0010 0.00033 1 1,2,4-Trichlorobenzene ND mg/L 07/20/16 17:04 120-82-10.0010 0.00035 1 1,1,1-Trichloroethane ND mg/L 07/20/16 17:04 71-55-60.0010 0.00048 1 1,1,2-Trichloroethane ND mg/L 07/20/16 17:04 79-00-50.0010 0.00029 1 Trichloroethene ND mg/L 07/20/16 17:04 79-01-60.0010 0.00047 1 Trichlorofluoromethane ND mg/L 07/20/16 17:04 75-69-40.0010 0.00020 1 1,2,3-Trichloropropane ND mg/L 07/20/16 17:04 96-18-40.0010 0.00041 1 1,2,4-Trimethylbenzene ND mg/L 07/20/16 17:04 95-63-60.0010 0.00031 1 1,3,5-Trimethylbenzene ND mg/L 07/20/16 17:04 108-67-80.0010 0.00036 1 Vinyl acetate ND mg/L 07/20/16 17:04 108-05-40.0020 0.00035 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 26 of 56 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Sample:STREAM DOWNGRADIENT Lab ID:92305482012 Collected:07/14/16 13:00 Received:07/18/16 15:45 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Vinyl chloride ND mg/L 07/20/16 17:04 75-01-40.0010 0.00062 1 Xylene (Total)ND mg/L 07/20/16 17:04 1330-20-70.0010 0.00066 1 m&p-Xylene ND mg/L 07/20/16 17:04 179601-23-10.0020 0.00066 1 o-Xylene ND mg/L 07/20/16 17:04 95-47-60.0010 0.00023 1 Surrogates 4-Bromofluorobenzene (S)97 %07/20/16 17:04 460-00-470-130 1 1,2-Dichloroethane-d4 (S)102 %07/20/16 17:04 17060-07-070-130 1 Toluene-d8 (S)100 %07/20/16 17:04 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 27 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 321781 EPA 7470 EPA 7470 7470 Mercury Associated Lab Samples:92305482001, 92305482002, 92305482003, 92305482004, 92305482005, 92305482006, 92305482007, 92305482008, 92305482009, 92305482010, 92305482011 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1783132 Associated Lab Samples:92305482001, 92305482002, 92305482003, 92305482004, 92305482005, 92305482006, 92305482007, 92305482008, 92305482009, 92305482010, 92305482011 Matrix:Water AnalyzedMDL Mercury mg/L ND 0.00020 07/21/16 06:320.00010 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1783133LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/L 0.0024.0025 94 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1783134MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92305513005 1783135 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury mg/L .0025 83 75-12583 0 25.0025ND 0.0021 0.0021 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 28 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 321782 EPA 7470 EPA 7470 7470 Mercury Associated Lab Samples:92305482012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1783136 Associated Lab Samples:92305482012 Matrix:Water AnalyzedMDL Mercury mg/L ND 0.00020 07/21/16 04:420.00010 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1783137LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/L 0.0025.0025 101 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1783138MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92305482012 1783139 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury mg/L .0025 100 75-12595 5 25.0025ND 0.0025 0.0024 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 29 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 321935 EPA 3010A EPA 6010 6010 MET Associated Lab Samples:92305482001, 92305482002, 92305482003, 92305482004, 92305482005, 92305482006, 92305482007, 92305482008, 92305482009, 92305482010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1784269 Associated Lab Samples:92305482001, 92305482002, 92305482003, 92305482004, 92305482005, 92305482006, 92305482007, 92305482008, 92305482009, 92305482010 Matrix:Water AnalyzedMDL Arsenic mg/L ND 0.010 07/22/16 20:000.0050 Barium mg/L ND 0.0050 07/22/16 20:000.0025 Cadmium mg/L ND 0.0010 07/22/16 20:000.00050 Chromium mg/L ND 0.0050 07/22/16 20:000.0025 Lead mg/L ND 0.0050 07/22/16 20:000.0025 Selenium mg/L ND 0.010 07/22/16 20:000.0050 Silver mg/L ND 0.0050 07/22/16 20:000.0025 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1784270LABORATORY CONTROL SAMPLE: LCSSpike Arsenic mg/L 0.47.5 95 80-120 Barium mg/L 0.54.5 107 80-120 Cadmium mg/L 0.50.5 100 80-120 Chromium mg/L 0.50.5 100 80-120 Lead mg/L 0.49.5 97 80-120 Selenium mg/L 0.49.5 98 80-120 Silver mg/L 0.24.25 97 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1784271MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92305513005 1784272 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic mg/L .5 95 75-12594 1 20.5ND 0.47 0.47 Barium mg/L .5 107 75-125106 1 20.570.2 ug/L 0.60 0.60 Cadmium mg/L .5 100 75-12599 0 20.5ND 0.50 0.50 Chromium mg/L .5 100 75-12599 1 20.52.6J ug/L 0.50 0.50 Lead mg/L .5 95 75-12594 1 20.5ND 0.47 0.47 Selenium mg/L .5 97 75-12597 0 20.5ND 0.49 0.49 Silver mg/L .25 97 75-12596 1 20.25ND 0.24 0.24 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 30 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 321936 EPA 3010A EPA 6010 6010 MET Associated Lab Samples:92305482011, 92305482012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1784273 Associated Lab Samples:92305482011, 92305482012 Matrix:Water AnalyzedMDL Arsenic mg/L ND 0.010 07/22/16 23:170.0050 Barium mg/L ND 0.0050 07/22/16 23:170.0025 Cadmium mg/L ND 0.0010 07/22/16 23:170.00050 Chromium mg/L ND 0.0050 07/22/16 23:170.0025 Lead mg/L ND 0.0050 07/22/16 23:170.0025 Selenium mg/L ND 0.010 07/22/16 23:170.0050 Silver mg/L ND 0.0050 07/22/16 23:170.0025 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1784274LABORATORY CONTROL SAMPLE: LCSSpike Arsenic mg/L 0.47.5 95 80-120 Barium mg/L 0.53.5 106 80-120 Cadmium mg/L 0.50.5 100 80-120 Chromium mg/L 0.51.5 101 80-120 Lead mg/L 0.49.5 98 80-120 Selenium mg/L 0.49.5 99 80-120 Silver mg/L 0.24.25 97 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1784275MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92305482011 1784276 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic mg/L .5 95 75-12595 0 20.5ND 0.48 0.47 Barium mg/L .5 107 75-125107 0 20.50.073 0.61 0.61 Cadmium mg/L .5 100 75-125100 0 20.5ND 0.50 0.50 Chromium mg/L .5 101 75-125100 1 20.5ND 0.51 0.50 Lead mg/L .5 96 75-12596 0 20.5ND 0.48 0.48 Selenium mg/L .5 98 75-12598 0 20.5ND 0.49 0.49 Silver mg/L .25 97 75-12597 0 20.25ND 0.24 0.24 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 31 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 321858 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples:92305482001, 92305482007, 92305482008, 92305482009, 92305482010, 92305482011, 92305482012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1783453 Associated Lab Samples:92305482001, 92305482007, 92305482008, 92305482009, 92305482010, 92305482011, 92305482012 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane mg/L ND 0.0010 07/20/16 12:130.00033 1,1,1-Trichloroethane mg/L ND 0.0010 07/20/16 12:130.00048 1,1,2,2-Tetrachloroethane mg/L ND 0.0010 07/20/16 12:130.00040 1,1,2-Trichloroethane mg/L ND 0.0010 07/20/16 12:130.00029 1,1-Dichloroethane mg/L ND 0.0010 07/20/16 12:130.00032 1,1-Dichloroethene mg/L ND 0.0010 07/20/16 12:130.00056 1,1-Dichloropropene mg/L ND 0.0010 07/20/16 12:130.00049 1,2,3-Trichlorobenzene mg/L ND 0.0010 07/20/16 12:130.00033 1,2,3-Trichloropropane mg/L ND 0.0010 07/20/16 12:130.00041 1,2,4-Trichlorobenzene mg/L ND 0.0010 07/20/16 12:130.00035 1,2,4-Trimethylbenzene mg/L ND 0.0010 07/20/16 12:130.00031 1,2-Dibromoethane (EDB)mg/L ND 0.0010 07/20/16 12:130.00027 1,2-Dichlorobenzene mg/L ND 0.0010 07/20/16 12:130.00030 1,2-Dichloroethane mg/L ND 0.0010 07/20/16 12:130.00024 1,2-Dichloroethene (Total)mg/L ND 0.0010 07/20/16 12:130.00049 1,2-Dichloropropane mg/L ND 0.0010 07/20/16 12:130.00027 1,3,5-Trimethylbenzene mg/L ND 0.0010 07/20/16 12:130.00036 1,3-Dichlorobenzene mg/L ND 0.0010 07/20/16 12:130.00024 1,3-Dichloropropane mg/L ND 0.0010 07/20/16 12:130.00028 1,4-Dichlorobenzene mg/L ND 0.0010 07/20/16 12:130.00033 2,2-Dichloropropane mg/L ND 0.0010 07/20/16 12:130.00013 2-Chlorotoluene mg/L ND 0.0010 07/20/16 12:130.00035 4-Chlorotoluene mg/L ND 0.0010 07/20/16 12:130.00031 Benzene mg/L ND 0.0010 07/20/16 12:130.00025 Bromobenzene mg/L ND 0.0010 07/20/16 12:130.00030 Bromochloromethane mg/L ND 0.0010 07/20/16 12:130.00017 Bromodichloromethane mg/L ND 0.0010 07/20/16 12:130.00018 Bromoform mg/L ND 0.0010 07/20/16 12:130.00026 Bromomethane mg/L ND 0.0020 07/20/16 12:130.00029 Carbon tetrachloride mg/L ND 0.0010 07/20/16 12:130.00025 Chlorobenzene mg/L ND 0.0010 07/20/16 12:130.00023 Chloroethane mg/L ND 0.0010 07/20/16 12:130.00054 Chloroform mg/L ND 0.0010 07/20/16 12:130.00014 Chloromethane mg/L ND 0.0010 07/20/16 12:130.00011 cis-1,2-Dichloroethene mg/L ND 0.0010 07/20/16 12:130.00019 Dibromochloromethane mg/L ND 0.0010 07/20/16 12:130.00021 Dibromomethane mg/L ND 0.0010 07/20/16 12:130.00021 Dichlorodifluoromethane mg/L ND 0.0010 07/20/16 12:130.00021 Diisopropyl ether mg/L ND 0.0010 07/20/16 12:130.00012 Ethylbenzene mg/L ND 0.0010 07/20/16 12:130.00030 Hexachloro-1,3-butadiene mg/L ND 0.0010 07/20/16 12:130.00071 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 32 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1783453 Associated Lab Samples:92305482001, 92305482007, 92305482008, 92305482009, 92305482010, 92305482011, 92305482012 Matrix:Water AnalyzedMDL Isopropylbenzene (Cumene)mg/L ND 0.0010 07/20/16 12:130.00040 m&p-Xylene mg/L ND 0.0020 07/20/16 12:130.00066 Methyl-tert-butyl ether mg/L ND 0.0010 07/20/16 12:130.00021 Methylene Chloride mg/L ND 0.0020 07/20/16 12:130.00097 n-Butylbenzene mg/L ND 0.0010 07/20/16 12:130.00041 n-Propylbenzene mg/L ND 0.0010 07/20/16 12:130.00042 Naphthalene mg/L ND 0.0010 07/20/16 12:130.00024 o-Xylene mg/L ND 0.0010 07/20/16 12:130.00023 p-Isopropyltoluene mg/L ND 0.0010 07/20/16 12:130.00031 sec-Butylbenzene mg/L ND 0.0010 07/20/16 12:130.00038 Styrene mg/L ND 0.0010 07/20/16 12:130.00026 tert-Butylbenzene mg/L ND 0.0010 07/20/16 12:130.00040 Tetrachloroethene mg/L ND 0.0010 07/20/16 12:130.00046 Tetrahydrofuran mg/L ND 0.010 07/20/16 12:130.0031 Toluene mg/L ND 0.0010 07/20/16 12:130.00026 trans-1,2-Dichloroethene mg/L ND 0.0010 07/20/16 12:130.00049 Trichloroethene mg/L ND 0.0010 07/20/16 12:130.00047 Trichlorofluoromethane mg/L ND 0.0010 07/20/16 12:130.00020 Vinyl acetate mg/L ND 0.0020 07/20/16 12:130.00035 Vinyl chloride mg/L ND 0.0010 07/20/16 12:130.00062 Xylene (Total)mg/L ND 0.0010 07/20/16 12:130.00066 1,2-Dichloroethane-d4 (S)%102 70-130 07/20/16 12:13 4-Bromofluorobenzene (S)%96 70-130 07/20/16 12:13 Toluene-d8 (S)%100 70-130 07/20/16 12:13 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1783454LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane mg/L 0.048.05 96 70-130 1,1,1-Trichloroethane mg/L 0.049.05 98 70-130 1,1,2,2-Tetrachloroethane mg/L 0.050.05 99 70-130 1,1,2-Trichloroethane mg/L 0.049.05 98 70-130 1,1-Dichloroethane mg/L 0.050.05 100 70-130 1,1-Dichloroethene mg/L 0.056.05 112 70-132 1,1-Dichloropropene mg/L 0.047.05 94 70-130 1,2,3-Trichlorobenzene mg/L 0.054.05 108 70-135 1,2,3-Trichloropropane mg/L 0.050.05 100 70-130 1,2,4-Trichlorobenzene mg/L 0.052.05 105 70-134 1,2,4-Trimethylbenzene mg/L 0.052.05 104 70-130 1,2-Dibromoethane (EDB)mg/L 0.052.05 105 70-130 1,2-Dichlorobenzene mg/L 0.053.05 106 70-130 1,2-Dichloroethane mg/L 0.047.05 94 70-130 1,2-Dichloroethene (Total)mg/L 0.10.1 101 70-130 1,2-Dichloropropane mg/L 0.048.05 96 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 33 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1783454LABORATORY CONTROL SAMPLE: LCSSpike 1,3,5-Trimethylbenzene mg/L 0.050.05 99 70-130 1,3-Dichlorobenzene mg/L 0.051.05 101 70-130 1,3-Dichloropropane mg/L 0.048.05 95 70-130 1,4-Dichlorobenzene mg/L 0.051.05 103 70-130 2,2-Dichloropropane mg/L 0.051.05 102 58-145 2-Chlorotoluene mg/L 0.051.05 101 70-130 4-Chlorotoluene mg/L 0.051.05 102 70-130 Benzene mg/L 0.050.05 100 70-130 Bromobenzene mg/L 0.051.05 102 70-130 Bromochloromethane mg/L 0.052.05 103 70-130 Bromodichloromethane mg/L 0.050.05 101 70-130 Bromoform mg/L 0.050.05 99 70-130 Bromomethane mg/L 0.046.05 92 54-130 Carbon tetrachloride mg/L 0.051.05 103 70-132 Chlorobenzene mg/L 0.050.05 100 70-130 Chloroethane mg/L 0.048.05 96 64-134 Chloroform mg/L 0.049.05 99 70-130 Chloromethane mg/L 0.049.05 98 64-130 cis-1,2-Dichloroethene mg/L 0.050.05 99 70-131 Dibromochloromethane mg/L 0.050.05 100 70-130 Dibromomethane mg/L 0.049.05 99 70-131 Dichlorodifluoromethane mg/L 0.051.05 102 56-130 Diisopropyl ether mg/L 0.052.05 105 70-130 Ethylbenzene mg/L 0.049.05 98 70-130 Hexachloro-1,3-butadiene mg/L 0.054.05 108 70-130 Isopropylbenzene (Cumene)mg/L 0.049.05 99 70-130 m&p-Xylene mg/L 0.097.1 97 70-130 Methyl-tert-butyl ether mg/L 0.052.05 104 70-130 Methylene Chloride mg/L 0.049.05 98 63-130 n-Butylbenzene mg/L 0.051.05 102 70-130 n-Propylbenzene mg/L 0.049.05 97 70-130 Naphthalene mg/L 0.050.05 101 70-138 o-Xylene mg/L 0.049.05 97 70-130 p-Isopropyltoluene mg/L 0.051.05 103 70-130 sec-Butylbenzene mg/L 0.049.05 99 70-130 Styrene mg/L 0.052.05 105 70-130 tert-Butylbenzene mg/L 0.040.05 81 70-130 Tetrachloroethene mg/L 0.044.05 87 70-130 Tetrahydrofuran mg/L 0.51.5 102 70-130 Toluene mg/L 0.049.05 99 70-130 trans-1,2-Dichloroethene mg/L 0.051.05 102 70-130 Trichloroethene mg/L 0.047.05 94 70-130 Trichlorofluoromethane mg/L 0.048.05 96 62-133 Vinyl acetate mg/L 0.099.1 99 66-157 Vinyl chloride mg/L 0.046.05 92 50-150 Xylene (Total)mg/L 0.15.15 97 70-130 1,2-Dichloroethane-d4 (S)%101 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 34 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1783454LABORATORY CONTROL SAMPLE: LCSSpike 4-Bromofluorobenzene (S)%99 70-130 Toluene-d8 (S)%101 70-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1783455MATRIX SPIKE SAMPLE: MSSpike Result 92305323003 1,1,1,2-Tetrachloroethane mg/L 0.020.02 99 70-130ND 1,1,1-Trichloroethane mg/L 0.023.02 113 70-130ND 1,1,2,2-Tetrachloroethane mg/L 0.020.02 99 70-130ND 1,1,2-Trichloroethane mg/L 0.020.02 101 70-130ND 1,1-Dichloroethane mg/L 0.023.02 115 70-130ND 1,1-Dichloroethene mg/L 0.018.02 91 70-166ND 1,1-Dichloropropene mg/L 0.0043 M1.02 22 70-130ND 1,2,3-Trichlorobenzene mg/L 0.022.02 112 70-130ND 1,2,3-Trichloropropane mg/L 0.020.02 101 70-130ND 1,2,4-Trichlorobenzene mg/L 0.022.02 109 70-130ND 1,2,4-Trimethylbenzene mg/L 0.014.02 70 70-130ND 1,2-Dibromoethane (EDB)mg/L 0.022.02 110 70-130ND 1,2-Dichlorobenzene mg/L 0.022.02 109 70-130ND 1,2-Dichloroethane mg/L 0.021.02 104 70-130ND 1,2-Dichloropropane mg/L 0.020.02 101 70-130ND 1,3,5-Trimethylbenzene mg/L .00061J M1.02 3 70-130ND 1,3-Dichlorobenzene mg/L 0.021.02 107 70-130ND 1,3-Dichloropropane mg/L 0.020.02 99 70-130ND 1,4-Dichlorobenzene mg/L 0.023.02 107 70-1301.1 ug/L 2,2-Dichloropropane mg/L 0.021.02 104 70-130ND 2-Chlorotoluene mg/L 0.031 M1.02 153 70-130ND 4-Chlorotoluene mg/L 0.027 M1.02 134 70-130ND Benzene mg/L 0.022.02 110 70-148ND Bromobenzene mg/L 0.019.02 97 70-130ND Bromochloromethane mg/L 0.022.02 112 70-130ND Bromodichloromethane mg/L 0.021.02 107 70-130ND Bromoform mg/L 0.018.02 89 70-130ND Bromomethane mg/L 0.0052 M1.02 26 70-130ND Carbon tetrachloride mg/L 0.023.02 115 70-130ND Chlorobenzene mg/L 0.022.02 109 70-146ND Chloroethane mg/L 0.023.02 116 70-130ND Chloroform mg/L 0.023.02 110 70-130ND Chloromethane mg/L 0.028 M1.02 142 70-130ND cis-1,2-Dichloroethene mg/L 0.023.02 116 70-130ND Dibromochloromethane mg/L 0.020.02 100 70-130ND Dibromomethane mg/L 0.020.02 99 70-130ND Dichlorodifluoromethane mg/L 0.024.02 122 70-130ND Diisopropyl ether mg/L 0.024.02 119 70-130ND Ethylbenzene mg/L 0.011 M1.02 54 70-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 35 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1783455MATRIX SPIKE SAMPLE: MSSpike Result 92305323003 Hexachloro-1,3-butadiene mg/L 0.023.02 116 70-130ND Isopropylbenzene (Cumene)mg/L 0.013 M1.02 63 70-130ND m&p-Xylene mg/L ND M1.04 1 70-130ND Methyl-tert-butyl ether mg/L 0.023.02 113 70-130ND Methylene Chloride mg/L 0.022.02 111 70-130ND n-Butylbenzene mg/L 0.0095 M1.02 48 70-130ND n-Propylbenzene mg/L 0.011 M1.02 54 70-130ND Naphthalene mg/L ND M1.02 1 70-130ND o-Xylene mg/L .00087J M1.02 4 70-130ND p-Isopropyltoluene mg/L .00081J M1.02 4 70-130ND sec-Butylbenzene mg/L 0.012 M1.02 61 70-130ND Styrene mg/L .0006J M1.02 3 70-130ND tert-Butylbenzene mg/L 0.013 M1.02 64 70-130ND Tetrachloroethene mg/L 0.020.02 102 70-130ND Tetrahydrofuran mg/L 0.22.2 111 70-130ND Toluene mg/L 0.0094 M1.02 47 70-155ND trans-1,2-Dichloroethene mg/L 0.024.02 121 70-130ND Trichloroethene mg/L 0.021.02 106 69-151ND Trichlorofluoromethane mg/L 0.023.02 116 70-130ND Vinyl acetate mg/L 0.0059 M1.04 15 70-130ND Vinyl chloride mg/L 0.0024 M1.02 12 70-130ND 1,2-Dichloroethane-d4 (S)%101 70-130 4-Bromofluorobenzene (S)%99 70-130 Toluene-d8 (S)%100 70-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92305323004 1783456SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane mg/L ND 30ND 1,1,1-Trichloroethane mg/L ND 30ND 1,1,2,2-Tetrachloroethane mg/L ND 30ND 1,1,2-Trichloroethane mg/L ND 30ND 1,1-Dichloroethane mg/L ND 30ND 1,1-Dichloroethene mg/L ND 30ND 1,1-Dichloropropene mg/L ND 30ND 1,2,3-Trichlorobenzene mg/L ND 30ND 1,2,3-Trichloropropane mg/L ND 30ND 1,2,4-Trichlorobenzene mg/L ND 30ND 1,2,4-Trimethylbenzene mg/L ND 30ND 1,2-Dibromoethane (EDB)mg/L ND 30ND 1,2-Dichlorobenzene mg/L ND 30ND 1,2-Dichloroethane mg/L ND 30ND 1,2-Dichloroethene (Total)mg/L ND 30ND 1,2-Dichloropropane mg/L ND 30ND 1,3,5-Trimethylbenzene mg/L ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 36 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92305323004 1783456SAMPLE DUPLICATE: 1,3-Dichlorobenzene mg/L ND 30ND 1,3-Dichloropropane mg/L ND 30ND 1,4-Dichlorobenzene mg/L 0.0010 6 301.1 ug/L 2,2-Dichloropropane mg/L ND 30ND 2-Chlorotoluene mg/L ND 30ND 4-Chlorotoluene mg/L ND 30ND Benzene mg/L ND 30ND Bromobenzene mg/L ND 30ND Bromochloromethane mg/L ND 30ND Bromodichloromethane mg/L ND 30ND Bromoform mg/L ND 30ND Bromomethane mg/L ND 30ND Carbon tetrachloride mg/L ND 30ND Chlorobenzene mg/L ND 30ND Chloroethane mg/L ND 30ND Chloroform mg/L .00059J 30ND Chloromethane mg/L ND 30ND cis-1,2-Dichloroethene mg/L ND 30ND Dibromochloromethane mg/L ND 30ND Dibromomethane mg/L ND 30ND Dichlorodifluoromethane mg/L ND 30ND Diisopropyl ether mg/L ND 30ND Ethylbenzene mg/L ND 30ND Hexachloro-1,3-butadiene mg/L ND 30ND Isopropylbenzene (Cumene)mg/L ND 30ND m&p-Xylene mg/L ND 30ND Methyl-tert-butyl ether mg/L ND 30ND Methylene Chloride mg/L ND 30ND n-Butylbenzene mg/L ND 30ND n-Propylbenzene mg/L ND 30ND Naphthalene mg/L ND 30ND o-Xylene mg/L ND 30ND p-Isopropyltoluene mg/L ND 30ND sec-Butylbenzene mg/L ND 30ND Styrene mg/L ND 30ND tert-Butylbenzene mg/L ND 30ND Tetrachloroethene mg/L ND 30ND Tetrahydrofuran mg/L ND 30ND Toluene mg/L ND 30ND trans-1,2-Dichloroethene mg/L ND 30ND Trichloroethene mg/L ND 30ND Trichlorofluoromethane mg/L ND 30ND Vinyl acetate mg/L ND 30ND Vinyl chloride mg/L ND 30ND Xylene (Total)mg/L ND 30ND 1,2-Dichloroethane-d4 (S)%103 1102 4-Bromofluorobenzene (S)%95 095 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 37 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92305323004 1783456SAMPLE DUPLICATE: Toluene-d8 (S)%101 0100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 38 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 321861 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples:92305482002, 92305482003, 92305482005, 92305482006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1783462 Associated Lab Samples:92305482002, 92305482003, 92305482005, 92305482006 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane mg/L ND 0.0010 07/20/16 12:300.00033 1,1,1-Trichloroethane mg/L ND 0.0010 07/20/16 12:300.00048 1,1,2,2-Tetrachloroethane mg/L ND 0.0010 07/20/16 12:300.00040 1,1,2-Trichloroethane mg/L ND 0.0010 07/20/16 12:300.00029 1,1-Dichloroethane mg/L ND 0.0010 07/20/16 12:300.00032 1,1-Dichloroethene mg/L ND 0.0010 07/20/16 12:300.00056 1,1-Dichloropropene mg/L ND 0.0010 07/20/16 12:300.00049 1,2,3-Trichlorobenzene mg/L ND 0.0010 07/20/16 12:300.00033 1,2,3-Trichloropropane mg/L ND 0.0010 07/20/16 12:300.00041 1,2,4-Trichlorobenzene mg/L ND 0.0010 07/20/16 12:300.00035 1,2,4-Trimethylbenzene mg/L ND 0.0010 07/20/16 12:300.00031 1,2-Dibromoethane (EDB)mg/L ND 0.0010 07/20/16 12:300.00027 1,2-Dichlorobenzene mg/L ND 0.0010 07/20/16 12:300.00030 1,2-Dichloroethane mg/L ND 0.0010 07/20/16 12:300.00024 1,2-Dichloroethene (Total)mg/L ND 0.0010 07/20/16 12:300.00049 1,2-Dichloropropane mg/L ND 0.0010 07/20/16 12:300.00027 1,3,5-Trimethylbenzene mg/L ND 0.0010 07/20/16 12:300.00036 1,3-Dichlorobenzene mg/L ND 0.0010 07/20/16 12:300.00024 1,3-Dichloropropane mg/L ND 0.0010 07/20/16 12:300.00028 1,4-Dichlorobenzene mg/L ND 0.0010 07/20/16 12:300.00033 2,2-Dichloropropane mg/L ND 0.0010 07/20/16 12:300.00013 2-Chlorotoluene mg/L ND 0.0010 07/20/16 12:300.00035 4-Chlorotoluene mg/L ND 0.0010 07/20/16 12:300.00031 Benzene mg/L ND 0.0010 07/20/16 12:300.00025 Bromobenzene mg/L ND 0.0010 07/20/16 12:300.00030 Bromochloromethane mg/L ND 0.0010 07/20/16 12:300.00017 Bromodichloromethane mg/L ND 0.0010 07/20/16 12:300.00018 Bromoform mg/L ND 0.0010 07/20/16 12:300.00026 Bromomethane mg/L ND 0.0020 07/20/16 12:300.00029 Carbon tetrachloride mg/L ND 0.0010 07/20/16 12:300.00025 Chlorobenzene mg/L ND 0.0010 07/20/16 12:300.00023 Chloroethane mg/L ND 0.0010 07/20/16 12:300.00054 Chloroform mg/L ND 0.0010 07/20/16 12:300.00014 Chloromethane mg/L ND 0.0010 07/20/16 12:300.00011 cis-1,2-Dichloroethene mg/L ND 0.0010 07/20/16 12:300.00019 Dibromochloromethane mg/L ND 0.0010 07/20/16 12:300.00021 Dibromomethane mg/L ND 0.0010 07/20/16 12:300.00021 Dichlorodifluoromethane mg/L ND 0.0010 07/20/16 12:300.00021 Diisopropyl ether mg/L ND 0.0010 07/20/16 12:300.00012 Ethylbenzene mg/L ND 0.0010 07/20/16 12:300.00030 Hexachloro-1,3-butadiene mg/L ND 0.0010 07/20/16 12:300.00071 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 39 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1783462 Associated Lab Samples:92305482002, 92305482003, 92305482005, 92305482006 Matrix:Water AnalyzedMDL Isopropylbenzene (Cumene)mg/L ND 0.0010 07/20/16 12:300.00040 m&p-Xylene mg/L ND 0.0020 07/20/16 12:300.00066 Methyl-tert-butyl ether mg/L ND 0.0010 07/20/16 12:300.00021 Methylene Chloride mg/L ND 0.0020 07/20/16 12:300.00097 n-Butylbenzene mg/L ND 0.0010 07/20/16 12:300.00041 n-Propylbenzene mg/L ND 0.0010 07/20/16 12:300.00042 Naphthalene mg/L ND 0.0010 07/20/16 12:300.00024 o-Xylene mg/L ND 0.0010 07/20/16 12:300.00023 p-Isopropyltoluene mg/L ND 0.0010 07/20/16 12:300.00031 sec-Butylbenzene mg/L ND 0.0010 07/20/16 12:300.00038 Styrene mg/L ND 0.0010 07/20/16 12:300.00026 tert-Butylbenzene mg/L ND 0.0010 07/20/16 12:300.00040 Tetrachloroethene mg/L ND 0.0010 07/20/16 12:300.00046 Tetrahydrofuran mg/L ND 0.010 07/20/16 12:300.0031 Toluene mg/L ND 0.0010 07/20/16 12:300.00026 trans-1,2-Dichloroethene mg/L ND 0.0010 07/20/16 12:300.00049 Trichloroethene mg/L ND 0.0010 07/20/16 12:300.00047 Trichlorofluoromethane mg/L ND 0.0010 07/20/16 12:300.00020 Vinyl acetate mg/L ND 0.0020 07/20/16 12:300.00035 Vinyl chloride mg/L ND 0.0010 07/20/16 12:300.00062 Xylene (Total)mg/L ND 0.0010 07/20/16 12:300.00066 1,2-Dichloroethane-d4 (S)%102 70-130 07/20/16 12:30 4-Bromofluorobenzene (S)%97 70-130 07/20/16 12:30 Toluene-d8 (S)%100 70-130 07/20/16 12:30 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1783463LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane mg/L 0.047.05 93 70-130 1,1,1-Trichloroethane mg/L 0.048.05 96 70-130 1,1,2,2-Tetrachloroethane mg/L 0.048.05 96 70-130 1,1,2-Trichloroethane mg/L 0.047.05 93 70-130 1,1-Dichloroethane mg/L 0.049.05 98 70-130 1,1-Dichloroethene mg/L 0.054.05 107 70-132 1,1-Dichloropropene mg/L 0.046.05 93 70-130 1,2,3-Trichlorobenzene mg/L 0.053.05 106 70-135 1,2,3-Trichloropropane mg/L 0.048.05 96 70-130 1,2,4-Trichlorobenzene mg/L 0.051.05 103 70-134 1,2,4-Trimethylbenzene mg/L 0.050.05 101 70-130 1,2-Dibromoethane (EDB)mg/L 0.051.05 102 70-130 1,2-Dichlorobenzene mg/L 0.051.05 101 70-130 1,2-Dichloroethane mg/L 0.046.05 92 70-130 1,2-Dichloroethene (Total)mg/L 0.098.1 98 70-130 1,2-Dichloropropane mg/L 0.046.05 92 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 40 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1783463LABORATORY CONTROL SAMPLE: LCSSpike 1,3,5-Trimethylbenzene mg/L 0.048.05 96 70-130 1,3-Dichlorobenzene mg/L 0.049.05 99 70-130 1,3-Dichloropropane mg/L 0.046.05 92 70-130 1,4-Dichlorobenzene mg/L 0.049.05 97 70-130 2,2-Dichloropropane mg/L 0.050.05 101 58-145 2-Chlorotoluene mg/L 0.049.05 97 70-130 4-Chlorotoluene mg/L 0.049.05 97 70-130 Benzene mg/L 0.049.05 97 70-130 Bromobenzene mg/L 0.049.05 98 70-130 Bromochloromethane mg/L 0.049.05 98 70-130 Bromodichloromethane mg/L 0.049.05 98 70-130 Bromoform mg/L 0.047.05 94 70-130 Bromomethane mg/L 0.045.05 89 54-130 Carbon tetrachloride mg/L 0.049.05 99 70-132 Chlorobenzene mg/L 0.049.05 97 70-130 Chloroethane mg/L 0.046.05 92 64-134 Chloroform mg/L 0.048.05 96 70-130 Chloromethane mg/L 0.047.05 93 64-130 cis-1,2-Dichloroethene mg/L 0.049.05 97 70-131 Dibromochloromethane mg/L 0.047.05 95 70-130 Dibromomethane mg/L 0.047.05 94 70-131 Dichlorodifluoromethane mg/L 0.050.05 100 56-130 Diisopropyl ether mg/L 0.052.05 103 70-130 Ethylbenzene mg/L 0.048.05 96 70-130 Hexachloro-1,3-butadiene mg/L 0.052.05 104 70-130 Isopropylbenzene (Cumene)mg/L 0.047.05 95 70-130 m&p-Xylene mg/L 0.094.1 94 70-130 Methyl-tert-butyl ether mg/L 0.052.05 103 70-130 Methylene Chloride mg/L 0.048.05 96 63-130 n-Butylbenzene mg/L 0.050.05 99 70-130 n-Propylbenzene mg/L 0.047.05 94 70-130 Naphthalene mg/L 0.049.05 98 70-138 o-Xylene mg/L 0.048.05 95 70-130 p-Isopropyltoluene mg/L 0.050.05 99 70-130 sec-Butylbenzene mg/L 0.047.05 95 70-130 Styrene mg/L 0.050.05 100 70-130 tert-Butylbenzene mg/L 0.039.05 79 70-130 Tetrachloroethene mg/L 0.043.05 87 70-130 Tetrahydrofuran mg/L 0.51.5 101 70-130 Toluene mg/L 0.048.05 96 70-130 trans-1,2-Dichloroethene mg/L 0.049.05 99 70-130 Trichloroethene mg/L 0.046.05 92 70-130 Trichlorofluoromethane mg/L 0.047.05 94 62-133 Vinyl acetate mg/L 0.096.1 96 66-157 Vinyl chloride mg/L 0.045.05 89 50-150 Xylene (Total)mg/L 0.14.15 94 70-130 1,2-Dichloroethane-d4 (S)%100 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 41 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1783463LABORATORY CONTROL SAMPLE: LCSSpike 4-Bromofluorobenzene (S)%99 70-130 Toluene-d8 (S)%100 70-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1783464MATRIX SPIKE SAMPLE: MSSpike Result 92305480001 1,1,1,2-Tetrachloroethane mg/L 0.020.02 100 70-130ND 1,1,1-Trichloroethane mg/L 0.022.02 112 70-130ND 1,1,2,2-Tetrachloroethane mg/L 0.020.02 99 70-130ND 1,1,2-Trichloroethane mg/L 0.019.02 95 70-130ND 1,1-Dichloroethane mg/L 0.023.02 110 70-130ND 1,1-Dichloroethene mg/L 0.023.02 116 70-166ND 1,1-Dichloropropene mg/L 0.022.02 109 70-130ND 1,2,3-Trichlorobenzene mg/L 0.022.02 108 70-130ND 1,2,3-Trichloropropane mg/L 0.020.02 99 70-130ND 1,2,4-Trichlorobenzene mg/L 0.021.02 104 70-130ND 1,2,4-Trimethylbenzene mg/L 0.021.02 107 70-130ND 1,2-Dibromoethane (EDB)mg/L 0.022.02 108 70-130ND 1,2-Dichlorobenzene mg/L 0.021.02 106 70-130ND 1,2-Dichloroethane mg/L 0.020.02 101 70-130ND 1,2-Dichloropropane mg/L 0.020.02 100 70-130ND 1,3,5-Trimethylbenzene mg/L 0.021.02 105 70-130ND 1,3-Dichlorobenzene mg/L 0.021.02 106 70-130ND 1,3-Dichloropropane mg/L 0.020.02 99 70-130ND 1,4-Dichlorobenzene mg/L 0.021.02 104 70-130ND 2,2-Dichloropropane mg/L 0.020.02 100 70-130ND 2-Chlorotoluene mg/L 0.022.02 109 70-130ND 4-Chlorotoluene mg/L 0.022.02 109 70-130ND Benzene mg/L 0.022.02 109 70-148ND Bromobenzene mg/L 0.021.02 107 70-130ND Bromochloromethane mg/L 0.021.02 106 70-130ND Bromodichloromethane mg/L 0.021.02 103 70-130ND Bromoform mg/L 0.018.02 91 70-130ND Bromomethane mg/L 0.0093 M1.02 47 70-130ND Carbon tetrachloride mg/L 0.023.02 113 70-130ND Chlorobenzene mg/L 0.021.02 106 70-146ND Chloroethane mg/L 0.023.02 114 70-130ND Chloroform mg/L 0.022.02 109 70-130ND Chloromethane mg/L 0.020.02 98 70-130ND cis-1,2-Dichloroethene mg/L 0.022.02 112 70-130ND Dibromochloromethane mg/L 0.020.02 98 70-130ND Dibromomethane mg/L 0.020.02 102 70-130ND Dichlorodifluoromethane mg/L 0.023.02 115 70-130ND Diisopropyl ether mg/L 0.023.02 115 70-130ND Ethylbenzene mg/L 0.021.02 106 70-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 42 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1783464MATRIX SPIKE SAMPLE: MSSpike Result 92305480001 Hexachloro-1,3-butadiene mg/L 0.023.02 113 70-130ND Isopropylbenzene (Cumene)mg/L 0.021.02 105 70-130ND m&p-Xylene mg/L 0.042.04 104 70-130ND Methyl-tert-butyl ether mg/L 0.022.02 110 70-130ND Methylene Chloride mg/L 0.021.02 106 70-130ND n-Butylbenzene mg/L 0.021.02 104 70-130ND n-Propylbenzene mg/L 0.021.02 106 70-130ND Naphthalene mg/L 0.020.02 99 70-130ND o-Xylene mg/L 0.020.02 102 70-130ND p-Isopropyltoluene mg/L 0.021.02 106 70-130ND sec-Butylbenzene mg/L 0.021.02 105 70-130ND Styrene mg/L 0.020.02 98 70-130ND tert-Butylbenzene mg/L 0.017.02 87 70-130ND Tetrachloroethene mg/L 0.020.02 99 70-130ND Tetrahydrofuran mg/L 0.23.2 113 70-130ND Toluene mg/L 0.021.02 103 70-155ND trans-1,2-Dichloroethene mg/L 0.023.02 117 70-130ND Trichloroethene mg/L 0.021.02 103 69-151ND Trichlorofluoromethane mg/L 0.022.02 108 70-130ND Vinyl acetate mg/L 0.036.04 90 70-130ND Vinyl chloride mg/L 0.021.02 107 70-130ND 1,2-Dichloroethane-d4 (S)%100 70-130 4-Bromofluorobenzene (S)%98 70-130 Toluene-d8 (S)%97 70-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92305402002 1783465SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane mg/L ND 30ND 1,1,1-Trichloroethane mg/L ND 30ND 1,1,2,2-Tetrachloroethane mg/L ND 30ND 1,1,2-Trichloroethane mg/L ND 30ND 1,1-Dichloroethane mg/L ND 30ND 1,1-Dichloroethene mg/L ND 30ND 1,1-Dichloropropene mg/L ND 30ND 1,2,3-Trichlorobenzene mg/L ND 30ND 1,2,3-Trichloropropane mg/L ND 30ND 1,2,4-Trichlorobenzene mg/L ND 30ND 1,2,4-Trimethylbenzene mg/L ND 30ND 1,2-Dibromoethane (EDB)mg/L ND 30ND 1,2-Dichlorobenzene mg/L ND 30ND 1,2-Dichloroethane mg/L ND 30ND 1,2-Dichloroethene (Total)mg/L ND 30ND 1,2-Dichloropropane mg/L ND 30ND 1,3,5-Trimethylbenzene mg/L ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 43 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92305402002 1783465SAMPLE DUPLICATE: 1,3-Dichlorobenzene mg/L ND 30ND 1,3-Dichloropropane mg/L ND 30ND 1,4-Dichlorobenzene mg/L .00084J 30ND 2,2-Dichloropropane mg/L ND 30ND 2-Chlorotoluene mg/L ND 30ND 4-Chlorotoluene mg/L ND 30ND Benzene mg/L ND 30ND Bromobenzene mg/L ND 30ND Bromochloromethane mg/L ND 30ND Bromodichloromethane mg/L 0.0027 3 302.8 ug/L Bromoform mg/L ND 30ND Bromomethane mg/L ND 30ND Carbon tetrachloride mg/L ND 30ND Chlorobenzene mg/L ND 30ND Chloroethane mg/L ND 30ND Chloroform mg/L 0.012 2 3012.4 ug/L Chloromethane mg/L .00037J 30ND cis-1,2-Dichloroethene mg/L ND 30ND Dibromochloromethane mg/L ND 30ND Dibromomethane mg/L ND 30ND Dichlorodifluoromethane mg/L ND 30ND Diisopropyl ether mg/L ND 30ND Ethylbenzene mg/L ND 30ND Hexachloro-1,3-butadiene mg/L ND 30ND Isopropylbenzene (Cumene)mg/L ND 30ND m&p-Xylene mg/L ND 30ND Methyl-tert-butyl ether mg/L ND 30ND Methylene Chloride mg/L ND 30ND n-Butylbenzene mg/L ND 30ND n-Propylbenzene mg/L ND 30ND Naphthalene mg/L ND 30ND o-Xylene mg/L ND 30ND p-Isopropyltoluene mg/L ND 30ND sec-Butylbenzene mg/L ND 30ND Styrene mg/L ND 30ND tert-Butylbenzene mg/L ND 30ND Tetrachloroethene mg/L ND 30ND Tetrahydrofuran mg/L ND 30ND Toluene mg/L ND 30ND trans-1,2-Dichloroethene mg/L ND 30ND Trichloroethene mg/L ND 30ND Trichlorofluoromethane mg/L ND 30ND Vinyl acetate mg/L ND 30ND Vinyl chloride mg/L ND 30ND Xylene (Total)mg/L ND 30ND 1,2-Dichloroethane-d4 (S)%100 0100 4-Bromofluorobenzene (S)%94 397 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 44 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92305402002 1783465SAMPLE DUPLICATE: Toluene-d8 (S)%100 397 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 45 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 322061 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples:92305482004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1784770 Associated Lab Samples:92305482004 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane mg/L ND 0.0010 07/21/16 12:220.00033 1,1,1-Trichloroethane mg/L ND 0.0010 07/21/16 12:220.00048 1,1,2,2-Tetrachloroethane mg/L ND 0.0010 07/21/16 12:220.00040 1,1,2-Trichloroethane mg/L ND 0.0010 07/21/16 12:220.00029 1,1-Dichloroethane mg/L ND 0.0010 07/21/16 12:220.00032 1,1-Dichloroethene mg/L ND 0.0010 07/21/16 12:220.00056 1,1-Dichloropropene mg/L ND 0.0010 07/21/16 12:220.00049 1,2,3-Trichlorobenzene mg/L ND 0.0010 07/21/16 12:220.00033 1,2,3-Trichloropropane mg/L ND 0.0010 07/21/16 12:220.00041 1,2,4-Trichlorobenzene mg/L ND 0.0010 07/21/16 12:220.00035 1,2,4-Trimethylbenzene mg/L ND 0.0010 07/21/16 12:220.00031 1,2-Dibromoethane (EDB)mg/L ND 0.0010 07/21/16 12:220.00027 1,2-Dichlorobenzene mg/L ND 0.0010 07/21/16 12:220.00030 1,2-Dichloroethane mg/L ND 0.0010 07/21/16 12:220.00024 1,2-Dichloroethene (Total)mg/L ND 0.0010 07/21/16 12:220.00049 1,2-Dichloropropane mg/L ND 0.0010 07/21/16 12:220.00027 1,3,5-Trimethylbenzene mg/L ND 0.0010 07/21/16 12:220.00036 1,3-Dichlorobenzene mg/L ND 0.0010 07/21/16 12:220.00024 1,3-Dichloropropane mg/L ND 0.0010 07/21/16 12:220.00028 1,4-Dichlorobenzene mg/L ND 0.0010 07/21/16 12:220.00033 2,2-Dichloropropane mg/L ND 0.0010 07/21/16 12:220.00013 2-Chlorotoluene mg/L ND 0.0010 07/21/16 12:220.00035 4-Chlorotoluene mg/L ND 0.0010 07/21/16 12:220.00031 Benzene mg/L ND 0.0010 07/21/16 12:220.00025 Bromobenzene mg/L ND 0.0010 07/21/16 12:220.00030 Bromochloromethane mg/L ND 0.0010 07/21/16 12:220.00017 Bromodichloromethane mg/L ND 0.0010 07/21/16 12:220.00018 Bromoform mg/L ND 0.0010 07/21/16 12:220.00026 Bromomethane mg/L ND 0.0020 07/21/16 12:220.00029 Carbon tetrachloride mg/L ND 0.0010 07/21/16 12:220.00025 Chlorobenzene mg/L ND 0.0010 07/21/16 12:220.00023 Chloroethane mg/L ND 0.0010 07/21/16 12:220.00054 Chloroform mg/L ND 0.0010 07/21/16 12:220.00014 Chloromethane mg/L ND 0.0010 07/21/16 12:220.00011 cis-1,2-Dichloroethene mg/L ND 0.0010 07/21/16 12:220.00019 Dibromochloromethane mg/L ND 0.0010 07/21/16 12:220.00021 Dibromomethane mg/L ND 0.0010 07/21/16 12:220.00021 Dichlorodifluoromethane mg/L ND 0.0010 07/21/16 12:220.00021 Diisopropyl ether mg/L ND 0.0010 07/21/16 12:220.00012 Ethylbenzene mg/L ND 0.0010 07/21/16 12:220.00030 Hexachloro-1,3-butadiene mg/L ND 0.0010 07/21/16 12:220.00071 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 46 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1784770 Associated Lab Samples:92305482004 Matrix:Water AnalyzedMDL Isopropylbenzene (Cumene)mg/L ND 0.0010 07/21/16 12:220.00040 m&p-Xylene mg/L ND 0.0020 07/21/16 12:220.00066 Methyl-tert-butyl ether mg/L ND 0.0010 07/21/16 12:220.00021 Methylene Chloride mg/L ND 0.0020 07/21/16 12:220.00097 n-Butylbenzene mg/L ND 0.0010 07/21/16 12:220.00041 n-Propylbenzene mg/L ND 0.0010 07/21/16 12:220.00042 Naphthalene mg/L ND 0.0010 07/21/16 12:220.00024 o-Xylene mg/L ND 0.0010 07/21/16 12:220.00023 p-Isopropyltoluene mg/L ND 0.0010 07/21/16 12:220.00031 sec-Butylbenzene mg/L ND 0.0010 07/21/16 12:220.00038 Styrene mg/L ND 0.0010 07/21/16 12:220.00026 tert-Butylbenzene mg/L ND 0.0010 07/21/16 12:220.00040 Tetrachloroethene mg/L ND 0.0010 07/21/16 12:220.00046 Tetrahydrofuran mg/L ND 0.010 07/21/16 12:220.0031 Toluene mg/L ND 0.0010 07/21/16 12:220.00026 trans-1,2-Dichloroethene mg/L ND 0.0010 07/21/16 12:220.00049 Trichloroethene mg/L ND 0.0010 07/21/16 12:220.00047 Trichlorofluoromethane mg/L ND 0.0010 07/21/16 12:220.00020 Vinyl acetate mg/L ND 0.0020 07/21/16 12:220.00035 Vinyl chloride mg/L ND 0.0010 07/21/16 12:220.00062 Xylene (Total)mg/L ND 0.0010 07/21/16 12:220.00066 1,2-Dichloroethane-d4 (S)%103 70-130 07/21/16 12:22 4-Bromofluorobenzene (S)%95 70-130 07/21/16 12:22 Toluene-d8 (S)%101 70-130 07/21/16 12:22 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1784771LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane mg/L 0.048.05 97 70-130 1,1,1-Trichloroethane mg/L 0.052.05 104 70-130 1,1,2,2-Tetrachloroethane mg/L 0.050.05 100 70-130 1,1,2-Trichloroethane mg/L 0.048.05 97 70-130 1,1-Dichloroethane mg/L 0.052.05 104 70-130 1,1-Dichloroethene mg/L 0.059.05 117 70-132 1,1-Dichloropropene mg/L 0.053.05 107 70-130 1,2,3-Trichlorobenzene mg/L 0.053.05 105 70-135 1,2,3-Trichloropropane mg/L 0.049.05 97 70-130 1,2,4-Trichlorobenzene mg/L 0.052.05 104 70-134 1,2,4-Trimethylbenzene mg/L 0.052.05 103 70-130 1,2-Dibromoethane (EDB)mg/L 0.053.05 105 70-130 1,2-Dichlorobenzene mg/L 0.052.05 103 70-130 1,2-Dichloroethane mg/L 0.048.05 96 70-130 1,2-Dichloroethene (Total)mg/L 0.11.1 108 70-130 1,2-Dichloropropane mg/L 0.050.05 99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 47 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1784771LABORATORY CONTROL SAMPLE: LCSSpike 1,3,5-Trimethylbenzene mg/L 0.051.05 101 70-130 1,3-Dichlorobenzene mg/L 0.052.05 105 70-130 1,3-Dichloropropane mg/L 0.050.05 100 70-130 1,4-Dichlorobenzene mg/L 0.052.05 104 70-130 2,2-Dichloropropane mg/L 0.054.05 108 58-145 2-Chlorotoluene mg/L 0.048.05 97 70-130 4-Chlorotoluene mg/L 0.052.05 103 70-130 Benzene mg/L 0.050.05 100 70-130 Bromobenzene mg/L 0.052.05 103 70-130 Bromochloromethane mg/L 0.052.05 105 70-130 Bromodichloromethane mg/L 0.050.05 100 70-130 Bromoform mg/L 0.050.05 100 70-130 Bromomethane mg/L 0.031.05 63 54-130 Carbon tetrachloride mg/L 0.052.05 104 70-132 Chlorobenzene mg/L 0.050.05 101 70-130 Chloroethane mg/L 0.050.05 100 64-134 Chloroform mg/L 0.051.05 101 70-130 Chloromethane mg/L 0.045.05 90 64-130 cis-1,2-Dichloroethene mg/L 0.053.05 106 70-131 Dibromochloromethane mg/L 0.050.05 100 70-130 Dibromomethane mg/L 0.048.05 97 70-131 Dichlorodifluoromethane mg/L 0.054.05 108 56-130 Diisopropyl ether mg/L 0.056.05 112 70-130 Ethylbenzene mg/L 0.050.05 99 70-130 Hexachloro-1,3-butadiene mg/L 0.054.05 109 70-130 Isopropylbenzene (Cumene)mg/L 0.050.05 100 70-130 m&p-Xylene mg/L 0.099.1 99 70-130 Methyl-tert-butyl ether mg/L 0.054.05 109 70-130 Methylene Chloride mg/L 0.052.05 103 63-130 n-Butylbenzene mg/L 0.053.05 105 70-130 n-Propylbenzene mg/L 0.049.05 99 70-130 Naphthalene mg/L 0.053.05 105 70-138 o-Xylene mg/L 0.049.05 98 70-130 p-Isopropyltoluene mg/L 0.051.05 101 70-130 sec-Butylbenzene mg/L 0.050.05 100 70-130 Styrene mg/L 0.052.05 104 70-130 tert-Butylbenzene mg/L 0.041.05 82 70-130 Tetrachloroethene mg/L 0.047.05 94 70-130 Tetrahydrofuran mg/L 0.55.5 111 70-130 Toluene mg/L 0.049.05 98 70-130 trans-1,2-Dichloroethene mg/L 0.055.05 110 70-130 Trichloroethene mg/L 0.047.05 95 70-130 Trichlorofluoromethane mg/L 0.047.05 94 62-133 Vinyl acetate mg/L 0.10.1 105 66-157 Vinyl chloride mg/L 0.051.05 102 50-150 Xylene (Total)mg/L 0.15.15 99 70-130 1,2-Dichloroethane-d4 (S)%99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 48 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1784771LABORATORY CONTROL SAMPLE: LCSSpike 4-Bromofluorobenzene (S)%98 70-130 Toluene-d8 (S)%100 70-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1784772MATRIX SPIKE SAMPLE: MSSpike Result 92305910001 1,1,1,2-Tetrachloroethane mg/L 0.020.02 101 70-130ND 1,1,1-Trichloroethane mg/L 0.023.02 114 70-130ND 1,1,2,2-Tetrachloroethane mg/L 0.020.02 98 70-130ND 1,1,2-Trichloroethane mg/L 0.021.02 103 70-130ND 1,1-Dichloroethane mg/L 0.024.02 119 70-130ND 1,1-Dichloroethene mg/L 0.026.02 129 70-166ND 1,1-Dichloropropene mg/L 0.023.02 115 70-130ND 1,2,3-Trichlorobenzene mg/L 0.022.02 111 70-130ND 1,2,3-Trichloropropane mg/L 0.019.02 96 70-130ND 1,2,4-Trichlorobenzene mg/L 0.022.02 108 70-130ND 1,2,4-Trimethylbenzene mg/L 0.023.02 113 70-130ND 1,2-Dibromoethane (EDB)mg/L 0.022.02 108 70-130ND 1,2-Dichlorobenzene mg/L 0.023.02 114 70-130ND 1,2-Dichloroethane mg/L 0.021.02 105 70-130ND 1,2-Dichloropropane mg/L 0.021.02 106 70-130ND 1,3,5-Trimethylbenzene mg/L 0.023.02 113 70-130ND 1,3-Dichlorobenzene mg/L 0.022.02 111 70-130ND 1,3-Dichloropropane mg/L 0.020.02 102 70-130ND 1,4-Dichlorobenzene mg/L 0.022.02 110 70-130ND 2,2-Dichloropropane mg/L 0.023.02 113 70-130ND 2-Chlorotoluene mg/L 0.023.02 117 70-130ND 4-Chlorotoluene mg/L 0.023.02 116 70-130ND Benzene mg/L 0.023.02 113 70-148ND Bromobenzene mg/L 0.023.02 114 70-130ND Bromochloromethane mg/L 0.023.02 114 70-130ND Bromodichloromethane mg/L 0.022.02 109 70-130ND Bromoform mg/L 0.018.02 92 70-130ND Bromomethane mg/L 0.0099 M1.02 49 70-130ND Carbon tetrachloride mg/L 0.023.02 115 70-130ND Chlorobenzene mg/L 0.022.02 109 70-146ND Chloroethane mg/L 0.024.02 118 70-130ND Chloroform mg/L 0.023.02 113 70-130ND Chloromethane mg/L 0.020.02 100 70-130ND cis-1,2-Dichloroethene mg/L 0.024.02 118 70-130ND Dibromochloromethane mg/L 0.020.02 102 70-130ND Dibromomethane mg/L 0.020.02 101 70-130ND Dichlorodifluoromethane mg/L 0.025.02 124 70-130ND Diisopropyl ether mg/L 0.024.02 121 70-130ND Ethylbenzene mg/L 0.022.02 110 70-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 49 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1784772MATRIX SPIKE SAMPLE: MSSpike Result 92305910001 Hexachloro-1,3-butadiene mg/L 0.023.02 114 70-130ND Isopropylbenzene (Cumene)mg/L 0.022.02 108 70-130ND m&p-Xylene mg/L 0.043.04 108 70-130ND Methyl-tert-butyl ether mg/L 0.022.02 111 70-130ND Methylene Chloride mg/L 0.023.02 113 70-130ND n-Butylbenzene mg/L 0.022.02 112 70-130ND n-Propylbenzene mg/L 0.023.02 114 70-130ND Naphthalene mg/L 0.020.02 99 70-130ND o-Xylene mg/L 0.021.02 107 70-130ND p-Isopropyltoluene mg/L 0.022.02 112 70-130ND sec-Butylbenzene mg/L 0.022.02 112 70-130ND Styrene mg/L 0.022.02 110 70-130ND tert-Butylbenzene mg/L 0.018.02 92 70-130ND Tetrachloroethene mg/L 0.020.02 100 70-130ND Tetrahydrofuran mg/L 0.21.2 104 70-130ND Toluene mg/L 0.022.02 110 70-155ND trans-1,2-Dichloroethene mg/L 0.025.02 126 70-130ND Trichloroethene mg/L 0.021.02 105 69-151ND Trichlorofluoromethane mg/L 0.022.02 109 70-130ND Vinyl acetate mg/L 0.039.04 98 70-130ND Vinyl chloride mg/L 0.022.02 112 70-130ND 1,2-Dichloroethane-d4 (S)%101 70-130 4-Bromofluorobenzene (S)%95 70-130 Toluene-d8 (S)%99 70-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92305875001 1784773SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane mg/L ND 30ND 1,1,1-Trichloroethane mg/L ND 30ND 1,1,2,2-Tetrachloroethane mg/L ND 30ND 1,1,2-Trichloroethane mg/L ND 30ND 1,1-Dichloroethane mg/L ND 30ND 1,1-Dichloroethene mg/L ND 30ND 1,1-Dichloropropene mg/L ND 30ND 1,2,3-Trichlorobenzene mg/L ND 30ND 1,2,3-Trichloropropane mg/L ND 30ND 1,2,4-Trichlorobenzene mg/L ND 30ND 1,2,4-Trimethylbenzene mg/L ND 30ND 1,2-Dibromoethane (EDB)mg/L ND 30ND 1,2-Dichlorobenzene mg/L ND 30ND 1,2-Dichloroethane mg/L ND 30ND 1,2-Dichloroethene (Total)mg/L ND 30ND 1,2-Dichloropropane mg/L ND 30ND 1,3,5-Trimethylbenzene mg/L ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 50 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92305875001 1784773SAMPLE DUPLICATE: 1,3-Dichlorobenzene mg/L ND 30ND 1,3-Dichloropropane mg/L ND 30ND 1,4-Dichlorobenzene mg/L ND 30ND 2,2-Dichloropropane mg/L ND 30ND 2-Chlorotoluene mg/L ND 30ND 4-Chlorotoluene mg/L ND 30ND Benzene mg/L 0.0017 14 301.5 ug/L Bromobenzene mg/L ND 30ND Bromochloromethane mg/L ND 30ND Bromodichloromethane mg/L ND 30ND Bromoform mg/L ND 30ND Bromomethane mg/L ND 30ND Carbon tetrachloride mg/L ND 30ND Chlorobenzene mg/L ND 30ND Chloroethane mg/L ND 30ND Chloroform mg/L ND 30ND Chloromethane mg/L ND 30ND cis-1,2-Dichloroethene mg/L ND 30ND Dibromochloromethane mg/L ND 30ND Dibromomethane mg/L ND 30ND Dichlorodifluoromethane mg/L ND 30ND Diisopropyl ether mg/L ND 30ND Ethylbenzene mg/L ND 30ND Hexachloro-1,3-butadiene mg/L ND 30ND Isopropylbenzene (Cumene)mg/L ND 30ND m&p-Xylene mg/L ND 30ND Methyl-tert-butyl ether mg/L ND 30ND Methylene Chloride mg/L ND 30ND n-Butylbenzene mg/L ND 30ND n-Propylbenzene mg/L ND 30ND Naphthalene mg/L ND 30ND o-Xylene mg/L ND 30ND p-Isopropyltoluene mg/L ND 30ND sec-Butylbenzene mg/L ND 30ND Styrene mg/L ND 30ND tert-Butylbenzene mg/L ND 30ND Tetrachloroethene mg/L ND 30ND Tetrahydrofuran mg/L ND 30ND Toluene mg/L .00032J 30ND trans-1,2-Dichloroethene mg/L ND 30ND Trichloroethene mg/L ND 30ND Trichlorofluoromethane mg/L ND 30ND Vinyl acetate mg/L ND 30ND Vinyl chloride mg/L ND 30ND Xylene (Total)mg/L ND 30ND 1,2-Dichloroethane-d4 (S)%103 0103 4-Bromofluorobenzene (S)%93 396 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 51 of 56 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92305875001 1784773SAMPLE DUPLICATE: Toluene-d8 (S)%99 2101 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 52 of 56 #=QL# QUALIFIERS Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 53 of 56 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92305482 WILEY DAVIS LANDFILL Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92305482001 321935 322133WD-1 EPA 3010A EPA 6010 92305482002 321935 322133WD-2 EPA 3010A EPA 6010 92305482003 321935 322133WD-2D EPA 3010A EPA 6010 92305482004 321935 322133WD-3 EPA 3010A EPA 6010 92305482005 321935 322133WD-3D EPA 3010A EPA 6010 92305482006 321935 322133WD-4 EPA 3010A EPA 6010 92305482007 321935 322133WD-4D EPA 3010A EPA 6010 92305482008 321935 322133WD-7 EPA 3010A EPA 6010 92305482009 321935 322133WD-8 EPA 3010A EPA 6010 92305482010 321935 322133WD-9 EPA 3010A EPA 6010 92305482011 321936 322135STREAM UPGRADIENT EPA 3010A EPA 6010 92305482012 321936 322135STREAM DOWNGRADIENT EPA 3010A EPA 6010 92305482001 321781 321791WD-1 EPA 7470 EPA 7470 92305482002 321781 321791WD-2 EPA 7470 EPA 7470 92305482003 321781 321791WD-2D EPA 7470 EPA 7470 92305482004 321781 321791WD-3 EPA 7470 EPA 7470 92305482005 321781 321791WD-3D EPA 7470 EPA 7470 92305482006 321781 321791WD-4 EPA 7470 EPA 7470 92305482007 321781 321791WD-4D EPA 7470 EPA 7470 92305482008 321781 321791WD-7 EPA 7470 EPA 7470 92305482009 321781 321791WD-8 EPA 7470 EPA 7470 92305482010 321781 321791WD-9 EPA 7470 EPA 7470 92305482011 321781 321791STREAM UPGRADIENT EPA 7470 EPA 7470 92305482012 321782 321792STREAM DOWNGRADIENT EPA 7470 EPA 7470 92305482001 321858WD-1 EPA 8260 92305482002 321861WD-2 EPA 8260 92305482003 321861WD-2D EPA 8260 92305482004 322061WD-3 EPA 8260 92305482005 321861WD-3D EPA 8260 92305482006 321861WD-4 EPA 8260 92305482007 321858WD-4D EPA 8260 92305482008 321858WD-7 EPA 8260 92305482009 321858WD-8 EPA 8260 92305482010 321858WD-9 EPA 8260 92305482011 321858STREAM UPGRADIENT EPA 8260 92305482012 321858STREAM DOWNGRADIENT EPA 8260 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 07/25/2016 11:52 AM Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 54 of 56 Page 55 of 56 Page 56 of 56