8807_TransylvaniaCoSMSWLF_GWMR_DIN26612_20160119

2211 West Meadowview Rd.
Greensboro, NC 27407
tel: [phone]
fax: [phone] www.JoyceEngineering.com

January 19, 2016

Mr. Ervin Lane
Compliance Hydrogeologist
Division of Waste Management/Solid Waste Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

RE: Second Semiannual Water Quality Monitoring Reports of 2015
Woodruff Landfill, Permit No. 88-07 Transylvania County, North Carolina
JOYCE Project No. 00336.1601.12, Task No. 3

Dear Ervin:

On behalf of Transylvania County, Joyce Engineering is submitting the enclosed Second
Semiannual Monitoring Report of 2015 in electronic format, the Environmental Monitoring
Form for the Woodruff Landfill, Permit No. 88-07. This report completes the first semiannual
compliance monitoring event of 2015 as required by the North Carolina Division of Waste
Management, Solid Waste Section. Please feel free to contact Alex Everhart or me at (336) 323-
0092 if you have any questions regarding this submittal.

Sincerely,
JOYCE ENGINEERING

Hannu Kemppinen P.G.
Senior Project Consultant

Enclosures

C: Jeff Brookshire – Transylvania County

PREPARED FOR:
TRANSYLVANIA COUNTY SOLID WASTE
500 HOWELL ROAD
BREVARD, NORTH CAROLINA 28712

TRANSYLVANIA COUNTY WOODRUFF LANDFILL
PERMIT NO. 88-07

SECOND SEMIANNUAL WATER QUALITY MONITORING
REPORT OF 2015

JANUARY 2016

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101
GREENSBORO, NORTH CAROLINA 27407
NC LICENSE NUMBER C-0782
PHONE: [phone]
FAX: [phone]
JOYCE PROJECT NO. 00336.1601.12

Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Transylvania County Woodruff Landfill, Permit No. 88-07 January 2016
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Second Semiannual Water Quality Monitoring Report of 2015 Woodruff Landfill
Transylvania County, North Carolina
TABLE OF CONTENTS 1.0 INTRODUCTION....................................................................................................... 1
1.1 Site Information .......................................................................................................... 1 1.2 Site Geology ................................................................................................................. 1 1.3 Regulatory Status ........................................................................................................ 1
2.0 FACILITY MONITORING PROGRAM ................................................................ 2
2.1 Groundwater Monitoring Program .......................................................................... 2
2.2 Surface Water Monitoring Program ......................................................................... 2 2.3 Leachate Monitoring Program .................................................................................. 3 3.0 SECOND SEMIANNUAL SAMPLING EVENT OF 2015 ..................................... 3
3.1 Field Work ................................................................................................................... 3
3.2 Laboratory Analysis and JOYCE Quality Control ................................................. 4
4.0 HYDROGEOLOGICAL CONDITIONS ................................................................. 5 5.0 DATA ANALYSIS AND STATISTICAL RESULTS ............................................. 5 5.1 Analytical Results and Comparisons to Standards.................................................. 6
5.1.1 Groundwater ....................................................................................................... 6
5.1.2 Surface Waters .................................................................................................... 6
5.1.3 Leachate .............................................................................................................. 7 5.2 Statistical Methods ...................................................................................................... 7 6.0 CONCLUSION ........................................................................................................... 7
7.0 REFERENCES ............................................................................................................ 7

Tables
Table 1 Summary of Historical Groundwater Elevations
Table 2 Groundwater Gradient and Flow Rate Calculations
Table 3 Summary of Historical Groundwater Constituents
Table 4 Summary of Historical Groundwater Field Parameters
Table 5 Summary of Historical Surface Water Constituents Table 6 Summary of Historical Surface Water Field Parameters
Table 7 Summary of Historical Leachate Constituents
Table 8 Summary of Historical Leachate Field Parameters

Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Transylvania County Woodruff Landfill, Permit No. 88-07 January 2016
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Second Semiannual Water Quality Monitoring Report of 2015 Woodruff Landfill
Transylvania County, North Carolina
TABLE OF CONTENTS CONTINUED Figures Figure 1 Site Location Map Drawings Drawing 1 Potentiometric Surface Contour Map Appendices
Appendix 1 Laboratory Analytical Reports and Field Data Logs
Appendix 2 Summary of Detections
Appendix 3 Summary of Field Parameters Appendix 4 Summary of Monitoring Well Construction

Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Transylvania County Woodruff Landfill, Permit No. 88-07 January 2016
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1.0 INTRODUCTION
1.1 Site Information

The Woodruff Landfill is owned and operated by Transylvania County and is currently operating under North Carolina Solid Waste Permit No. 88-07. The landfill property is
located southwest of Rosman, North Carolina, between the French Broad River and the
Tennessee Valley Divide. The property boundary and disposal area are indicated on an
excerpt from enlarged USGS topographic maps for Eastatoe Gap and Rosman, North
Carolina (Figure No. 1). The disposal area is located on a topographic high that slopes downward to the west, southwest, and northwest.

Phases 1 and 2 were designed with a single geomembrane liner and a leachate collection
system. Waste disposal began in Phase 1 in May 1992. Phase 3 was constructed with a
composite liner, while Phase 4 was constructed using an alternate composite liner. Both Phase 3 and Phase 4 were constructed with a leachate collection system. Phases 1
through 4 comprise approximately 13.3 acres. A leachate lagoon was located at the
northwest corner of the approximately 8.5-acre lined area of Phases 1, 2, and 3. This
lagoon was abandoned in April 2003 during construction activities, and replaced with a
storage tank located northwest of Phase 4, as shown on Drawing No. 1. Leachate is sampled directly from this tank and the sample is identified as LMP-3. Waste disposal
began in May 1992 in the western (downgradient) portion of the landfill, and has
progressed to the east into Phase 4. The Phase 5 expansion of 5.5 acres was constructed
with a composite liner and leachate collection system in 2007. Waste disposal into Phase
5 will begin upon reaching capacity of Phase 4.
1.2 Site Geology
The Woodruff Landfill is located in the Inner Piedmont physiographic province within
the Chauga Belt, just southeast of the Brevard Fault Zone. The unit within the Chauga Belt that underlies the site is the Henderson Gneiss, which consists of mylonitic gneisses
(Brown, 1985). The mineralogy consists of biotite, muscovite, feldspar and quartz with
iron-manganese staining.

1.3 Regulatory Status
The Transylvania County Woodruff Landfill groundwater monitoring is completed in
accordance with North Carolina Division of Waste Management, Solid Waste Section
(SWS) Rule § 1633 (Detection Monitoring Program). Statistical analyses of the laboratory data when required is prepared in accordance with the required compliance
demonstration of the SWS Rule .1632(g), (h), and (i).

Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Transylvania County Woodruff Landfill, Permit No. 88-07 January 2016
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2.0 FACILITY MONITORING PROGRAM

2.1 Groundwater Monitoring Program
Groundwater monitoring at the Woodruff Landfill is completed in accordance with the
Detection Monitoring Program and the Water Quality Monitoring Plan for the facility.
Groundwater samples are collected semiannually and are analyzed for North Carolina
Solid Waste Section Appendix I constituents.
The monitoring network at the Woodruff Landfill consists of two upgradient wells
(MW-3 and MW-10) and eleven downgradient monitoring wells (MW-1, MW-2, MW-5,
MW-6, MW-8, MW-9SR, MW-9D, MW-11, MW-12S, MW-12D, and MW-13).
MW-9S was abandoned due to deterioration of the well casing. MW-9SR was installed on September 26, 2011, as the replacement for MW-9S in the groundwater monitoring
network.

Monitoring Well Date Installed Classification Monitoring Program Total Depth from TOC (ft) Lithology of Screened Interval
MW-1 4/16/91 Compliance Detection 32.66 Not Available MW-2 4/16/91 Compliance Detection 25.42 Not Available MW-3 4/16/91 Background Detection 42.55 Not Available MW-4 4/17/91 Abandoned - - - MW-5 4/17/91 Compliance Detection 35.02 Not Available MW-6 9/19/94 Compliance Detection 24.00 PWR/Bedrock MW-7 9/21/94 Abandoned - - - MW-8 9/20/94 Compliance Detection 34.56 PWR/Bedrock MW-9S 1/09/01 Abandoned - - -
MW-9SR 9/26/11 Compliance Detection 43.10 Fill/PWR
MW-9D 1/09/01 Compliance Detection 86.50 Bedrock
MW-10 11/13/06 Background Detection 40.50 Bedrock
MW-11 11/09/06 Compliance Detection 26.50 PWR/Bedrock
MW-12S 11/21/06 Compliance Detection 33.50 Saprolite/Fill
MW-12D 11/21/06 Compliance Detection 52.50 Bedrock
MW-13 11/20/06 Compliance Detection 48.41 Bedrock

2.2 Surface Water Monitoring Program

Surface water monitoring at the Woodruff Landfill is completed in accordance with NCSWMR §0602 (Surface Water Monitoring) and the approved Water Quality
Monitoring Plan for the facility. Surface Water samples are collected semiannually and
are analyzed for North Carolina Solid Waste Section Appendix I constituents.

The surface water monitoring network consists of two sampling points: SMP-1 is located downstream from the sediment pond, and SMP-3 is located approximately 150 feet
downstream from MW-11.

Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Transylvania County Woodruff Landfill, Permit No. 88-07 January 2016
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Surface Point Classification Monitoring Program
SMP-1 Compliance Surface Water SMP-3 Compliance Surface Water

2.3 Leachate Monitoring Program One leachate monitoring point (LMP-3) is sampled at the Woodruff Landfill on a
semiannual basis and the following constituents are included in the leachate laboratory
analysis:

• North Carolina Appendix I Metals
• North Carolina Appendix I 8260 Volatiles
• BOD
• COD
• Sulfate
• Phosphorus
• Nitrate

3.0 SECOND SEMIANNUAL SAMPLING EVENT OF 2015

3.1 Field Work
On October 20-21, 2015, personnel from Joyce Engineering (JOYCE) visited the
Woodruff Landfill to obtain water levels to the nearest 0.01 foot, purge, and sample
thirteen monitoring wells, two surface monitoring points, and one leachate monitoring point.
Monitoring wells were purged and sampled using either disposable bailers or a 12 volt
plastic pump during the October 2015 sampling event. Measurements of temperature,
pH, specific conductivity, and turbidity were recorded prior to purging, after each purge volume, and during sampling. Copies of the field data logs are presented in Appendix 1. Prior to sampling, laboratory-supplied containers were prepared with the following
information:

• Monitoring well number (completed by field personnel),
• Date and time of sample collection (completed by field personnel),
• Initials of sampling personnel (completed by field personnel),
• Project name and number (completed by the laboratory),
• Chemical preservative (completed by the laboratory); and
• Requested chemical analysis (completed by the laboratory).

Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
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Groundwater samples from each monitoring well were collected directly from the
disposable bailers or the 12 volt pump in the provided laboratory containers either
immediately after purging or within 24 hours of the final purge volume. Immediately
after collection, the samples were placed in a laboratory provided cooler and chilled on ice.

Surface water samples were collected directly from stream by lowering the prepared
sample containers into the stream flow with the opening facing into the current. Care was
taken not to overflow the sample containers (which could lead to preservative loss) and to avoid sample-induced turbidity. At the time of sampling, surface water was also
measured for temperature, pH, specific conductivity, and turbidity. After sample
collection, the samples were placed in a laboratory provided cooler and chilled on ice.

Leachate samples were collected from the leachate storage tank. Prepared sampling containers were filled, placed in a cooler, and chilled on ice. At the time of sampling,
leachate was measured for temperature, pH, specific conductivity, and turbidity.

3.2 Laboratory Analysis and JOYCE Quality Control
The October 2015 groundwater, surface water, and leachate samples were submitted to
Pace Analytical Services, Inc. of Asheville, North Carolina under chain-of-custody
control for analysis. As presented earlier, the groundwater and surface water samples
were analyzed for North Carolina Appendix I constituents, while leachate samples were
analyzed for North Carolina Appendix I constituents plus BOD, COD, Phosphorous, Sulfate, and Nitrate. The samples were received by the laboratory on October 21, 2015, in
good condition, properly preserved, and within analysis hold times.

In addition to samples collected for compliance monitoring at the Woodruff Landfill, a
Field Blank was collected by JOYCE personnel as part of the October 2015 sampling. A Trip Blank was prepared by the laboratory to accompany the volatile sampling containers
from the laboratory to the field and back to laboratory during the October 2015 event.
The Field Blank was analyzed for North Carolina Appendix I constituents, while the Trip
Blank was analyzed for North Carolina Appendix I volatile organics only.
Upon receipt of laboratory data packages, the data was reviewed by JOYCE personnel for
the following:

• General typographical errors,
• Correct analyses performed and within method specified hold times,
• Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike
Duplicate, and Laboratory Control Samples,
• Blank qualified data (B-flags); and

Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Transylvania County Woodruff Landfill, Permit No. 88-07 January 2016
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• Quantified detections above the North Carolina Groundwater Protection Standards
(GWPS), NC 2L Groundwater Standards (NC 2L), and NC 2B Surface Water
Standards (NC 2B). 4.0 HYDROGEOLOGICAL CONDITIONS
Depth to groundwater was measured in the compliance monitoring wells at the site prior
to sampling. The groundwater elevations were calculated relative to the surveyed measuring point (top of casing) for each monitoring well. The groundwater elevations are summarized in Table 1.

The potentiometric surface contours shown in Drawing 1 are based on data from the
October 2015 sampling event. Groundwater flow direction beneath the waste management unit is primarily to the west. Estimated horizontal groundwater gradients from the October 2015 groundwater elevations are presented in Table 2. The horizontal
gradients calculated for the facility from these data ranged from 0.0643 ft/ft to 0.0897
ft/ft. Based on this data, the groundwater monitoring network remains sufficient to
adequately monitor groundwater at the site. Linear groundwater flow velocities for wells screened in saprolite were computed using
the following modified Darcy equation:

V = Ki/n where V = average linear velocity (feet per day – ft/day), K = hydraulic conductivity
(ft/day), i = horizontal hydraulic gradient, and n = effective porosity. A hydraulic
conductivity (K) of 8.79 E 10–2 ft/day based on results from slug testing and an estimated
effective porosity of 20% based on soils typical of this region were used to estimate average linear groundwater flow velocities for Phases 1 through 4. A hydraulic conductivity (K) of 2.92 E 10–1 ft/day based on results from slug testing and an estimated
effective porosity of 20% based on soils typical of this region were used to estimate
average linear groundwater flow velocities for Phase 5. The calculated flow velocities are
summarized in Table 2. The estimated linear groundwater flow velocity under the waste management unit ranges from 0.028 ft/day to 0.031 ft/day under Phases 1 through 4, and 0.131 ft/day under Phase 5. The linear velocity equation and resulting rates make the
simplified assumptions of a homogeneous and isotropic aquifer. Application of this
equation to a fractured bedrock aquifer is likely to overestimate flow rates, therefore; the
calculated flow rates should be considered maximum possible flow rates. Actual flow rates are expected to be less. The regolith and fractured bedrock common in this terrain are characteristically heterogeneous. Site boring logs record that regolith sampled at the
site commonly exhibits relict foliation. These structures can result in locally anisotropic
groundwater flow. Although the regolith and bedrock are hydraulically connected, the
effective porosity generally decreases with depth into the underlying fractured bedrock.

Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Transylvania County Woodruff Landfill, Permit No. 88-07 January 2016
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5.0 DATA ANALYSIS AND STATISTICAL RESULTS
Final results from the October 2015 sampling event were received October 31, 2015,
from Pace Analytical Services, Inc. All analytical results can be found in Appendix 2.
Statistical comparisons of baseline monitoring data to compliance groundwater data are
part of the required compliance demonstration (Rule .1632(g), (h), and (i)) for the
Woodruff Landfill. Background data and statistical methods were not used to evaluate
the data from the Woodruff Landfill during this monitoring event because all results were below applicable standards.
5.1 Analytical Results and Comparisons to Standards

5.1.1 Groundwater
As presented in Appendix 2(Summary of Detections), two NC Appendix I inorganic
constituents were detected in samples from one or more downgradient compliance
monitoring wells at quantified concentrations above their respective Solid Waste Section
Reporting Limits (SWSLs).
• Beryllium: MW-1, MW-3, and MW-9SR
• Lead: MW-8 and MW-9SR ASDs for beryllium and lead have been approved and are on file for the Woodruff
Landfill

There were no detections of NC Appendix I organic constituents above their SWSLs during the October 2015 sampling event.
The inorganic and organic groundwater analytical results from the October 2015
sampling event are generally consistent with historical data at the Woodruff Landfill. The
analytical results are summarized in Table 3 and field parameters are summarized in Table 4. The results, as reported by the laboratory, the laboratory quality assurance/quality control information, and the chain of custody records are included in
Appendix 1.

5.1.2 Surface Waters There were no constituents detected at quantified concentrations or above the NC 2B
standards in surface waters during the October 2015 sampling event.

The inorganic and organic surface water analytical results from the October 2015 sampling event at the Woodruff Landfill are summarized in Table 5 and field parameters are summarized in Table 6. The results, as reported by the laboratory, the laboratory

Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
Transylvania County Woodruff Landfill, Permit No. 88-07 January 2016
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quality assurance/quality control information, and the chain-of-custody records are
included in Appendix 1.

5.1.3 Leachate

The following constituents were detected at quantified concentrations in leachate during
the October 2015 sampling event. All concentrations are reported in micrograms per liter
(µg/L).
Constituent LMP-3 Blanks
Antimony 7.5 ND Barium 441 ND
Chromium 18 ND Zinc 28.2 ND 1,4-Dichlorobenzene 1.6 ND Biochemical Oxygen Demand (BOD) 3,000 ND
Chemical Oxygen Demand (COD) 267,000 ND Phosphate (Total Phosphorus) 162 ND
ND = Not detected above laboratory reporting limits.

The analytical results from the October 2015 leachate sampling event at the Woodruff Landfill are summarized in Table 7 and field parameters are summarized in Table 8. The
results, as reported by the laboratory, the laboratory quality assurance/quality control
information, and the chain of custody records, are included in the Appendix 1.

5.2 Statistical Methods
No Appendix I constituents were detected above their respective GWPS or NC 2L
standards during the October 2015 sampling event. As a result, statistical calculations
were not required for the October 2015 sampling event.
6.0 CONCLUSION
Based on the analytical results from the October 2015 sampling event, the Transylvania
County Woodruff Landfill shall remain in the Detection Monitoring Program as outlined in Title 15A NCAC 13B .1633. The next semiannual monitoring event is tentatively scheduled for April 2015.

7.0 REFERENCES
Bouwer, H. and Rice, R.C., June 1976, A slug test for determining hydraulic conductivity of unconfined aquifers with completely or partially penetrating wells; Water
Resources Research, American Geophysical Union, pp. 423-428.

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Transylvania County Woodruff Landfill, Permit No. 88-07 January 2016
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Bouwer, H., 1989, The Bouwer and Rice slug test-an update; Ground Water, vol. 27, No.
3, May-June, pp. 304 - 309.

Brown, Philip M., Chief Geologist, 1985, Geologic Map of North Carolina, The North Carolina Geologic Survey, scale 1:500,000.

GAI Consultants, Inc., Design Hydrogeologic Study Phase 3 Transylvania County Lined
Landfill Rosman, North Carolina, for Municipal Engineering Services Company,
PA Garner, North Carolina, March 1995.

Harned, D.A., and Daniel, Charles C., III, 1989, The Transition Zone Between Bedrock
and Regolith: Conduit For Contamination?, in Ground Water in the Piedmont;
Edited by Daniel, C.,White, R., and Stone, P., Proceedings published by Clemson University, pp. 336-348.

Heath, R.C., 1989, The Piedmont ground-water system, in Ground Water in the
Piedmont; Edited by Daniel, C.,White, R., and Stone, P., Proceedings published
by Clemson University, pp. 1-13.
Horton, J. W., Jr., 1982, Geologic map and mineral resources summary of the Rosman
quadrangle, North Carolina: Raleigh, North Carolina, Department of the Natural
Resources and Community Development Division of Land Resources, Geologic
Survey Section, GM 185-NE, scale 1:24,000.
Horton, J. W., Jr., and McConnell, K. I., 1991, The Western Piedmont, in Horton, J. W.,
Jr., and Zullo, V. A., eds., The Geology of the Carolinas: The University of
Tennessee Press, p. 36-58.
North Carolina Dept. Environment, Health, and Natural Resources (NCDEHNR), 1995,
N.C. Water Quality Monitoring Guidance Document for Solid Waste Facilities.

North Carolina Department of Environment and Natural Resources, 1990-2011, Solid Waste Management Regulations.
RCRA Ground Water Monitoring Technical Enforcement Guidance Document (TEGD),
1986.

USEPA, 1986, RCRA Ground Water Monitoring Technical Enforcement Guidance Document (TEGD).

USEPA, 1992, “Statistical Analysis of Groundwater Monitoring Data at RCRA
Facilities, Addendum to Interim Final Guidance”, Chapter 2, July.

Second Semiannual Water Quality Monitoring Report of 2015 Joyce Engineering
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United States Geological Survey. Eastatoe Gap, S.C. – N.C. and Rosman, N.C. 7.5
minute Quadrangles.

Tables

Table 1 Summary of Historical Groundwater Elevations Table 2 Groundwater Gradient and Flow Rate Calculations
Table 3 Summary of Historical Groundwater Constituents
Table 4 Summary of Historical Groundwater Field Parameters
Table 5 Summary of Historical Surface Water Constituents
Table 6 Summary of Historical Surface Water Field Parameters Table 7 Summary of Historical Leachate Constituents
Table 8 Summary of Historical Leachate Field Parameters

TABLE 1
SUMMARY OF HISTORICAL GROUNDWATER ELEVATIONS
MW-3 MW-10 MW-1 MW-2 MW-4 MW-5 MW-6 MW-7 MW-8 MW-9S MW-9SR MW-9D MW-11 MW-12S MW-12D MW-13
TOC Elevation 2754.44 2771.01 2705.74 2676.85 2701.43 2644.23 2665.26 2666.89 2674.19 2673.70 2674.40 2672.83 2679.95 2676.95 2677.04 2694.48
Well Depth 42.55 40.50 32.66 25.42 26.13 35.02 24.00 24.77 34.56 45.00 40.00 86.50 26.50 33.50 52.50 48.41
May-97 2729.67 NI 2689.53 2660.32 2692.29 2634.78 2648.83 2657.25 2644.98 NI NI NI NI NI NI NI
Oct-97 2722.90 NI 2686.06 2659.86 2691.70 2634.15 2647.73 2657.18 2644.30 NI NI NI NI NI NI NI
Apr-98 2729.37 NI 2689.20 2660.25 2693.23 2634.75 2647.30 2657.31 2644.91 NI NI NI NI NI NI NI
Oct-98 2721.48 NI 2685.24 2659.34 2691.02 2633.55 2647.64 2657.00 2644.19 NI NI NI NI NI NI NI
Apr-99 2728.23 NI 2688.07 2659.04 2692.06 2633.47 2648.11 2656.13 2641.19 NI NI NI NI NI NI NI
Oct-99 2722.09 NI 2686.36 2660.18 2693.17 2634.21 2649.09 2657.84 2644.94 NI NI NI NI NI NI NI
Apr-00 2728.61 NI 2687.85 2660.17 2693.17 2634.53 2649.04 2657.20 2644.93 NI NI NI NI NI NI NI
Oct-00 2721.55 NI 2685.61 2660.00 2691.09 2634.04 2647.91 2657.13 2644.66 NI NI NI NI NI NI NI
Apr-01 2727.01 NI 2688.39 2660.33 2693.46 2634.61 2649.24 2657.33 2645.14 2645.48 NI 2644.41 NI NI NI NI
Oct-01 2722.36 NI 2685.79 2659.69 2692.35 2634.13 2648.92 2658.92 2644.75 2645.22 NI 2643.99 NI NI NI NI
Apr-02 2727.82 NI 2688.50 2660.03 2693.40 2634.50 2648.95 2657.14 2644.89 2645.42 NI 2644.46 NI NI NI NI
Oct-02 2722.40 NI 2686.02 2660.19 AB 2634.28 2648.23 AB 2646.07 2646.19 NI 2643.53 NI NI NI NI
Apr-03 2712.59 NI 2682.66 2660.55 AB 2634.09 2652.73 AB 2647.21 2648.26 NI 2593.88 NI NI NI NI
Oct-03 2726.51 NI 2686.11 2660.25 AB 2634.23 2648.86 AB 2646.41 2647.57 NI 2645.73 NI NI NI NI
Apr-04 2726.61 NI 2686.05 2659.88 AB 2634.22 2648.34 AB 2646.09 2650.14 NI 2645.22 NI NI NI NI
Oct-04 2729.57 NI 2686.55 2659.85 AB 2634.28 2647.93 AB 2647.41 2648.58 NI 2646.36 NI NI NI NI
Apr-05 2728.98 NI 2687.42 2660.71 AB 2634.80 2649.36 AB 2647.35 2649.61 NI 2647.26 NI NI NI NI
Oct-05 2725.61 NI 2685.88 2660.58 AB 2634.16 2648.01 AB 2646.30 2647.70 NI 2646.14 NI NI NI NI
19-Apr-06 2725.76 NI 2685.56 2660.70 AB 2633.78 2647.73 AB 2645.49 2646.20 NI 2644.81 NI NI NI NI
19-Oct-06 2721.68 NI 2685.64 2661.27 AB 2634.48 2651.76 AB 2646.05 2647.54 NI 2646.28 NI NI NI NI
25-Apr-07 2727.21 2741.78 2686.52 2661.01 AB 2634.10 2648.45 AB 2646.65 2648.56 NI 2647.08 2661.01 2653.49 2650.49 2650.69
09-Jul-07 NS 2739.15 NS NS AB NS NS AB NS NS NI NS 2658.56 2652.08 2646.79 2651.70
16-Oct-07 2718.92 NS 2683.96 2660.33 AB 2633.23 2645.03 AB 2644.31 2644.82 NI 2643.25 NS NS NS NS
11-Mar-08 2728.27 2741.86 2687.56 2661.34 AB 2635.30 2650.33 AB 2645.60 2646.44 NI 2644.86 2661.67 2649.39 2646.86 2654.74
23-Apr-08 2728.90 2741.81 2686.82 2661.05 AB 2634.80 2645.36 AB 2645.61 2645.97 NI 2644.43 2658.28 2648.58 2646.07 2653.14
22-Oct-08 2720.82 2738.26 2684.18 2660.32 AB 2634.04 2646.00 AB 2643.99 2644.51 NI NS 2654.33 2646.05 2643.53 2649.82
17-Apr-09 2729.94 2741.89 2688.16 2661.30 AB 2635.58 2650.90 AB 2645.55 2646.90 NI 2645.24 2661.90 2650.23 2648.12 2655.80
14-Oct-09 2724.48 2741.81 2687.07 2661.51 AB 2635.59 2653.06 AB 2645.20 2646.64 NI 2644.85 2661.84 2649.44 2647.69 2655.43
22-Apr-10 2728.70 2741.80 2689.40 2661.15 AB 2634.65 2648.21 AB 2645.49 2646.55 NI 2644.40 2657.90 2648.62 2646.50 2653.56
27-Oct-10 2723.08 2739.75 2687.25 2661.44 AB 2635.44 2657.15 AB 2644.58 2645.30 NI 2643.33 2665.36 2646.04 2644.57 2651.51
19-Apr-11 2731.47 2741.94 2690.47 2661.75 AB 2635.22 2650.94 AB 2645.70 2646.86 NI 2644.85 2661.56 2650.11 2647.60 2655.56
04-Oct-11 2722.57 2738.96 2685.89 2661.35 AB 2634.68 2648.42 AB 2644.97 AB 2645.79 2643.54 2656.23 2647.10 2645.18 2652.36
03-Apr-12 2727.92 2741.78 2688.43 2661.31 AB 2635.08 2649.97 AB 2645.93 AB 2646.92 2644.13 2659.71 2648.30 2646.19 2653.72
02-Oct-12 2725.64 2741.83 2688.05 2662.05 AB 2635.91 2656.60 AB 2647.11 AB 2648.88 2644.48 2664.03 2648.74 2646.51 2655.56
23-Apr-13 2729.39 2739.60 2688.29 2661.64 AB 2634.59 2651.31 AB 2646.14 AB 2648.19 2644.72 2661.53 2650.08 2647.23 2655.51
22-Oct-13 2726.00 2739.62 2688.21 2660.69 AB 2634.61 2649.24 AB 2645.61 AB 2646.37 2643.53 2655.81 2648.65 2645.09 2653.21
22-Apr-14 2728.94 2741.90 2690.77 2661.45 AB 2634.53 2651.93 AB 2646.23 AB 2647.45 2644.78 2662.20 2650.93 2647.34 2656.13
07-Oct-14 2722.34 2738.05 2685.88 2660.94 AB 2634.63 2645.08 AB 2644.87 AB 2645.38 2643.18 2655.35 2648.75 2644.63 2652.86
21-Apr-15 2729.05 2742.20 2692.04 2661.96 AB 2635.60 2646.75 AB 2646.31 AB 2647.50 2644.61 2663.15 2652.11 2648.86 2660.42
20-Oct-15 2722.84 2738.81 2686.64 2661.00 AB 2633.78 2644.01 AB 2645.74 AB 2645.25 2643.73 2658.10 2648.50 2646.39 2655.53
Notes:
1. All elevations are referenced as feet above mean sea level.
2. All depths measured in feet (ft).
3. NS = Not sampled.
4. NI = Monitoring well not installed.
5. AB = Monitoring well abandoned.
BackgroundLocation Downgradient
Transylvania County Woodruff Landfill
Permit No. 88-07 Joyce Engineering
TABLE 2
GROUNDWATER GRADIENT AND FLOW RATE CALCULATIONS
HORIZONTAL HYDRAULIC EFFECTIVE LINEAR
GRADIENT CONDUCTIVITY POROSITY VELOCITY
i K n V
(ft/ft)(ft/day)(ft/day)
2740
2640
2720
2640
2730
2650
Average 0.0751 Average 0.063
Notes:
Segment i1 is calculated from Phase 5 hydrogeological report and segments i2 and i3 are calculated from the Phase 4 hydrogeological report.
2. Velocity = Ki/n; assume homogeneous isotropic porous aquifer and an effective porosity (n) of 0.20 for Phase 1-4 and 0.05 for Phase 5.
FLOW LINE
LENGTH
(feet)
GROUNDWATER
ELEVATION
(feet)
0.028
0.131
SW
1115 SW 0.0897 2.92E-01
8.79E-02
0.20
1. The geometric mean of K calculated from individual well slug tests was used to calculate the hydraulic conductivity.
1124 NW 0.0712 8.79E-02
0.0643 0.20
i 2
i 3 1244
GRADIENT
CALCULATION
SEGMENT
October-15
0.20i1
0.031
FLOW
DIRECTION
Transylvania County Woodruff Landfill
Permit No. 88-07 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL GROUNDWATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-3 MW-10 MW-1 MW-2 MW-5 MW-6 MW-8 MW-9S/9SR MW-9D MW-11 MW-12S MW-12D MW-13 Blanks
INORGANICS
Antimony 23-Apr-10 2.6 6.0 ND ND ND ND ND 2.7 J ND ND ND ND ND ND ND ND
GWPS = 1 µg/L (10/01/10)28-Oct-10 2.6 6.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Apr-11 2.6 6.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04-Oct-11 5.0 6.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 5.0 6.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 5.0 6.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 5.0 6.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 5.0 6.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 5.0 6.0 ND ND ND 6.7 ND ND 10.6 10.4 ND ND 7.2 ND ND ND
07-Oct-14 5.0 6.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 5.0 6.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 3.8 6.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND

Arsenic 23-Apr-10 2.7 10.0 ND ND ND ND ND ND ND ND ND ND 6.0 J ND ND ND
NC 2L = 100 µg/L (1/01/10)28-Oct-10 2.7 10.0 ND ND ND ND ND ND 4.8 J ND ND ND 3.8 J ND ND ND
20-Apr-11 2.7 10.0 ND ND ND ND ND ND ND ND ND ND 3.0 J ND ND ND
04-Oct-11 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 5.0 10.0 ND ND ND ND ND 105 ND ND ND ND ND ND ND ND
Resample 25-Oct-12 5.0 10.0 ---------------ND ---------------------ND
24-Apr-13 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Oct-13 5.0 10.0 ND ND 5.2 J ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 2.5 10.0 ND ND ND ND ND ---ND 2.9 J ND ND ND ND ND ND
Barium 23-Apr-10 0.20 100 0.99 B 6.5 B 72.0 B 28.9 B 0.31 B 15.1 B 17.2 B 14.2 B 0.47 B 9.7 B 121 B 18.6 B 12.8 B 27.0 J
NC 2L = 700 µg/L (1/01/10)28-Oct-10 0.20 100 ND 9.3 J 39.4 J 27.6 J 0.60 J 29.0 J 18.1 J 18.7 J 0.64 J 13.2 J 56.7 J 18.0 J 12.0 J ND
20-Apr-11 0.20 100 4.8 B 3.4 B 34.2 B 30.0 B 0.42 B 18.0 B 21.2 B 17.6 B 0.98 B 20.1 B 16.1 B 13.2 B 19.1 B 14.5 J
04-Oct-11 5.0 100 ND 8.9 J 67.8 J 35.6 J ND 30.2 J 25.9 J 20.9 J ND 14.8 J 21.5 J 11.7 J 9.3 J ND
03-Apr-12 5.0 100 1.7 J 7.7 J 39.8 J 29.3 J ND 20.0 J 20.1 J 42.9 J ND 17.0 J 32.3 J 9.9 J 7.9 J ND
03-Oct-12 5.0 100 ND 6.5 J 45.2 J 28.7 J ND 20.9 J 21.5 J 64.7 J ND 24.2 J 32.6 J 11.6 J 31.9 J ND
24-Apr-13 5.0 100 ND 12.5 J 21.6 J 26.7 J ND 15.7 J 21.8 J ---7.0 J 21.2 J 15.6 J 10.3 J 18.5 J ND
23-Oct-13 5.0 100 ND 7.2 J 65.0 J 36.7 J ND 17.8 J 19.8 J 40.6 J ND 13.4 J 34.4 J 13.5 J 15.4 J ND
23-Apr-14 5.0 100 ND 5.6 J 28.0 J 15.7 J ND 11.8 J 15.3 J 25.8 J ND 19.6 J 13.2 J 11.2 J 19.9 J ND
07-Oct-14 5.0 100 ND 14.9 J 42.9 J 47.3 J ND 23.1 J 17.6 J 34.7 J ND 14.4 J 13.6 J 12.7 J 9.8 J ND
22-Apr-15 5.0 100 9.0 J 3.1 J 20.8 J 16.2 J ND 13.2 J 12.8 J 21.7 J ND 19.1 J 23.2 J 15.2 J 33.0 J ND
20-Oct-15 2.5 100 5.9 J 5.3 J 27.8 J 36.6 J ND ---21.4 J 54.00 J ND 17.9 J 42.8 J 26.6 J 34.3 J ND

Beryllium 23-Apr-10 0.10 1.0 1.2 0.84 B 5.8 1.2 0.46 B 0.88 J 1.2 0.71 B 0.76 B 0.49 B 2.2 0.27 J 0.39 J 0.17 J
Resample 11-Jun-10 0.20 2.0 ------4.2 ------------------------------ND
GWPS = 4 µg/L (10/23/07)28-Oct-10 0.10 1.0 0.81 J 0.88 J 3.2 J 0.64 J 0.73 J 0.28 J 0.89 J 0.27 J 0.62 J 0.26 J 0.80 J 0.21 J 0.22 J ND
20-Apr-11 0.10 1.0 1.5 0.25 J 2.8 0.61 J 0.32 J 0.20 J 0.85 J 0.11 J 0.48 J 0.40 J 0.11 J 0.35 J 0.20 J ND
04-Oct-11 1.0 1.0 1.0 ND 3.2 ND ND ND 1.3 ND ND ND ND ND ND ND
03-Apr-12 1.0 1.0 1.7 ND 3.7 ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 1.0 1.0 1.3 ND 2.4 ND ND ND 1.1 ND ND ND ND ND ND ND
24-Apr-13 1.0 1.0 2.1 1.3 2.9 ND ND ND 1.4 ---1.2 ND ND 1.0 ND ND
23-Oct-13 1.0 1.0 1.6 ND 3.7 ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 1.0 1.0 1.3 ND 2.5 ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 1.0 1.0 1.6 1.9 2.4 ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 1.0 1.0 1.2 ND 2.0 ND ND ND 0.59 J ND 0.80 J ND ND ND ND ND
20-Oct-15 0.5 1.0 2.1 0.62 J 2.5 0.60 J ND ---0.91 J 1.2 0.82 J 0.75 J ND 0.85 J ND ND

Cadmium 23-Apr-10 0.50 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 2 µg/L (1/01/10)28-Oct-10 0.50 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.50 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04-Oct-11 1.0 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 1.0 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 1.0 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 1.0 1.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 1.0 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 1.0 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 1.0 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 1.0 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.5 1.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND
Chromium 23-Apr-10 0.40 10.0 0.70 B 1.1 B ND 0.40 B ND 0.86 B ND ND 0.45 B 1.4 B 6.6 J ND 1.1 B 0.41 J
NC 2L = 10 µg/L (1/01/10)28-Oct-10 0.40 10.0 ND ND ND ND ND ND ND ND ND 0.56 J 1.1 J ND ND ND
20-Apr-11 0.40 10.0 0.82 J 0.61 J 0.63 J 0.53 J ND 1.5 J 1.2 J 0.74 J ND 0.78 J 1.2 J ND ND ND
04-Oct-11 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 5.0 10.0 ND ND ND ND ND ND ND ---ND 5.9 J ND ND ND ND
23-Oct-13 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 2.5 10.0 ND ND ND ND ND ---ND 5.5 B ND 4.8 B ND ND ND 2.9 J

Cobalt 23-Apr-10 0.60 10.0 ND ND ND 4.4 J ND 0.94 J 7.7 J 3.5 J ND 3.5 J 4.3 J 10.6 ND ND
GWPS = 1 µg/L (10/01/10)28-Oct-10 0.60 10.0 1.0 B 2.1 B 11.2 B 3.7 B ND 1.0 B 9.9 B 6.9 B 2.7 B 6.0 B 29.1 11.2 B 2.1 B 2.4 J
Resample 21-Dec-10 0.6 10.0 ------------------------------13.4 ------2.1 J
20-Apr-11 0.60 10.0 0.99 J 3.0 J ND 5.4 J 5.1 J 4.3 J 7.6 J 4.5 J 3.1 J 1.3 J 15.3 6.6 J 4.4 J ND
04-Oct-11 5.0 10.0 ND ND ND 5.4 J ND ND 8.8 J 7.6 J ND ND 24.4 ND ND ND
03-Apr-12 5.0 10.0 ND ND ND ND ND ND 5.7 J ND ND ND 8.4 J ND ND ND
03-Oct-12 5.0 10.0 ND ND ND ND ND ND ND ND ND ND 9.2 J ND ND ND
24-Apr-13 5.0 10.0 ND ND ND 17.1 ND 8.6 J 13.7 ---ND ND 25.8 9.2 J ND ND
23-Oct-13 5.0 10.0 ND ND ND ND ND ND ND ND ND ND 6.9 J ND ND ND
23-Apr-14 5.0 10.0 ND ND ND ND ND ND ND ND ND ND 6.8 J ND ND ND
07-Oct-14 5.0 10.0 ND ND ND 16.4 ND ND 5.6 J 11.0 ND ND 14.5 7.7 J ND ND
22-Apr-15 5.0 10.0 ND ND ND ND ND ND 3.0 J ND ND ND 7.2 J ND ND ND
20-Oct-15 2.5 10.0 ND ND ND 3.7 J ND ---3.7 J ND ND 3.5 J 7.7 J 3.2 J ND ND

Copper 23-Apr-10 0.30 10.0 ND ND ND ND ND 0.43 J 4.2 J ND ND 4.6 J 26.1 ND ND ND
Resample 11-Jun-10 0.30 10.0 ------------------------------0.34 J ------ND
NC 2L = 1,000 µg/L (10/23/07)28-Oct-10 0.30 10.0 ND ND ND ND ND 0.36 J 0.41 J ND ND 2.5 J 10.1 ND ND ND
20-Apr-11 0.30 10.0 3.2 J 0.38 B 0.69 B 0.30 B 0.47 B 0.91 B 2.1 J 0.64 B 0.65 B 1.6 B 4.9 J 1.4 B 0.42 B 0.38 J
04-Oct-11 5.0 10.0 ND 6.2 J ND 9.6 J ND ND ND ND ND 7.6 J ND ND ND ND
03-Apr-12 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 5.0 10.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 5.0 10.0 ND ND ND ND ND ND ND ND ND ND 6.1 J ND ND ND
23-Apr-14 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 5.0 10.0 ND ND ND ND ND ND ND ND ND 5.9 J ND ND ND ND
22-Apr-15 5.0 10.0 ND ND ND ND ND ND 3.3 J ND ND ND 4.0 J ND ND ND
20-Oct-15 2.5 10.0 ND ND ND ND ND ---2.6 J 2.7 J ND 7.0 J 7.0 J ND ND ND

Transylvania County Woodruff Landfill
Permit No. 88-07 1 of 5 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL GROUNDWATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-3 MW-10 MW-1 MW-2 MW-5 MW-6 MW-8 MW-9S/9SR MW-9D MW-11 MW-12S MW-12D MW-13 Blanks
Lead 23-Apr-10 4.0 10.0 ND ND ND ND ND ND 8.9 J ND ND ND 42.3 ND ND ND
NC 2L = 15 µg/L (10/23/07)28-Oct-10 4.0 10.0 ND ND ND ND ND ND ND ND ND ND 16.3 ND ND ND
20-Apr-11 4.0 10.0 4.4 J ND 6.8 J ND ND ND 12.5 ND ND ND ND ND ND ND
04-Oct-11 5.0 10.0 ND ND 7.4 J ND ND ND 10.3 ND ND ND ND ND ND ND
03-Apr-12 5.0 10.0 ND ND ND ND ND ND 12.1 ND ND ND 7.1 J ND ND ND
03-Oct-12 5.0 10.0 ND ND ND ND ND ND 14.8 7.4 J ND ND 7.0 J ND ND ND
24-Apr-13 5.0 10.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 5.0 10.0 ND ND 23.0 5.3 J ND ND 13.9 7.2 J ND ND 8.7 J ND ND ND
23-Apr-14 5.0 10.0 ND ND 5.7 J ND ND ND 10.8 ND ND ND ND ND ND ND
07-Oct-14 5.0 10.0 ND 5.1 J ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 5.0 10.0 ND 6.1 7.1 J ND ND ND 4.3 J 4.2 J ND ND 5.4 J ND ND ND
20-Oct-15 2.5 10.0 4.2 J ND 5.6 J 6.1 J ND ---18.3 17.3 ND ND 9.5 J 4.1 J ND ND
Nickel 23-Apr-10 1.7 50.0 ND ND ND ND ND ND ND ND ND 20.0 J 8.0 J ND ND ND
NC 2L = 100 µg/L (10/23/07)28-Oct-10 1.7 50.0 ND ND ND ND ND ND ND ND ND 4.8 J 3.5 J ND ND ND
20-Apr-11 1.7 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND 5.8 J
04-Oct-11 5.0 50.0 ND ND ND ND ND ND ND ND ND 10.2 J ND ND ND ND
03-Apr-12 5.0 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 5.0 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 5.0 50.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 5.0 50.0 ND ND ND ND ND ND ND ND ND 8.2 J ND ND ND ND
23-Apr-14 5.0 50.0 ND ND ND ND ND ND ND ND ND ND ND 10.9 J ND ND
07-Oct-14 5.0 50.0 ND ND ND ND ND ND ND ND ND 16.1 J ND ND ND ND
22-Apr-15 5.0 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 2.5 50.0 ND ND ND ND ND ---ND ND ND 14.9 J ND ND ND ND

Selenium 23-Apr-10 3.8 10.0 ND ND ND ND ND ND ND ND ND ND 5.7 J ND ND ND
NC 2L = 20 µg/L (1/01/10)28-Oct-10 3.8 10.0 ND ND ND ND ND 5.2 J ND ND ND ND 3.8 J ND ND ND
20-Apr-11 3.8 10.0 ND ND ND ND ND ND ND ND ND ND 4.6 J ND ND ND
04-Oct-11 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 10.0 10.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 5.0 10.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND

Silver 23-Apr-10 0.10 10.0 ND ND 0.88 J ND ND ND ND ND ND 0.22 B ND ND ND 0.16 J
NC 2L = 20 µg/L (1/01/10)28-Oct-10 0.10 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.10 10.0 ND 0.23 J ND ND ND ND ND ND 0.20 J ND ND ND ND ND
04-Oct-11 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 5.0 10.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 5.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 2.5 10.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND

Thallium 23-Apr-10 3.0 5.5 ND ND ND 8.1 ND 5.9 8.4 ND ND ND 5.6 ND ND ND
GWPS = 0.2 µg/L (10/01/10)28-Oct-10 3.0 5.5 ND ND 19.1 J ND ND ND 4.7 J ND ND ND 5.4 J ND 3.8 J ND
20-Apr-11 3.0 5.5 ND ND ND 3.3 J ND ND ND ND ND ND ND ND ND ND
04-Oct-11 5.4 5.5 ND ND 6.3 ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 5.4 5.5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 5.4 5.5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 5.4 5.5 ND ND ND 7.4 ND ND ND ---ND ND ND ND ND ND
23-Oct-13 5.4 5.5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 5.4 5.5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 5.4 5.5 ND ND 6.0 ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 5.4 5.5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 5.0 5.5 ND ND ND ND ND ---ND ND ND ND ND ND ND ND

Vanadium 23-Apr-10 0.20 25.0 0.53 B 1.0 B 4.5 J 1.1 B 0.36 B 0.76 B 1.8 B 1.2 B 0.33 B 0.49 B 17.0 J 0.34 B 1.1 B 0.64 J
GWPS = 0.3 µg/L (10/01/10)28-Oct-10 0.20 25.0 0.22 B 0.73 B 2.4 J 0.35 B ND 0.84 B 1.1 B 0.42 B ND 0.23 B 5.4 J 0.25 B ND 0.30 J
20-Apr-11 0.20 25.0 0.39 J ND ND ND ND ND ND ND ND ND ND ND 0.28 J ND
04-Oct-11 5.0 25.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 5.0 25.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 5.0 25.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 5.0 25.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 5.0 25.0 ND ND ND 7.5 J ND ND 7.5 J 12.3 J ND ND 10.2 J ND ND ND
23-Apr-14 5.0 25.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 5.0 25.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 5.0 25.0 ND ND ND 5.2 J ND ND 7.9 J 9.3 J ND ND 8.1 J ND ND ND
20-Oct-15 2.5 25.0 ND ND ND ND ND ---ND ND ND ND ND 2.9 J ND ND

Zinc 23-Apr-10 0.40 10.0 1.5 B 3.2 B ND ND 8.0 B 3.3 B ND 2.5 B 1.4 B 6.6 B 22.4 B 2.9 B 3.1 B 4.5 J
NC 2L = 1,000 µg/L (1/01/10)28-Oct-10 0.40 10.0 ND ND ND ND 15.0 2.7 J 4.7 J 119 ND ND 3.4 J ND ND ND
Resample 21-Dec-10 0.4 10.0 ---------------------400 ---------------ND
20-Apr-11 0.40 10.0 13.9 B 3.7 B 2.2 B 5.8 B 10.2 B 1.7 B 7.1 B 2720 6.6 B 4.3 B 16.8 B 9.4 B 3.8 B 36.8
04-Oct-11 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND 12.2
24-Apr-13 10.0 10.0 ND ND ND ND 10.4 ND ND ---24.8 ND ND ND ND ND
23-Oct-13 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 10.0 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 10.0 10.0 10.6 B 8.1 B 5.4 B 5.4 B 11.6 B 5.8 B 7.4 B 6.6 B 6.1 B 8.1 B 10.0 B 7.9 B 8.8 B 6.1 J
20-Oct-15 5.0 10.0 ND ND ND ND 6.3 J ---5.3 J 7.9 J ND ND 6.9 J ND ND ND

Transylvania County Woodruff Landfill
Permit No. 88-07 2 of 5 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL GROUNDWATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-3 MW-10 MW-1 MW-2 MW-5 MW-6 MW-8 MW-9S/9SR MW-9D MW-11 MW-12S MW-12D MW-13 Blanks
Organic Compounds
Acetone 23-Apr-10 2.2 100 ND ND 5.1 J 3.4 J ND ND 4.6 J ND ND ND 5.6 J ND ND ND
NC 2L = 6,000 µg/L (1/01/10)28-Oct-10 2.2 100 ND ND 2.9 J 2.3 J ND ND 4.1 J 11.5 J ND ND 19.0 J ND ND ND
20-Apr-11 2.2 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04-Oct-11 2.2 100 ND ND 5.9 J 4.3 J ND ND 3.2 J 19.8 J ND ND 4.0 J ND ND ND
03-Apr-12 2.2 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 10.0 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 10.0 100 ND ND ND ND ND ND ND ---ND ND ND ND ND 41.9 J
23-Oct-13 10.0 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 10.0 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 10.0 100 ND ND ND ND ND ND ND ND ND ND ND ND ND 20.5 J
20-Oct-15 10.0 100 ND ND ND ND ND ---ND ND ND ND ND ND ND ND
Benzene 23-Apr-10 0.25 1.0 ND ND ND 0.80 J ND ND ND ND ND ND ND ND ND ND
NC2L = 1 µg/L (10/23/07)28-Oct-10 0.25 1.0 ND ND ND 0.30 J ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.25 1.0 ND ND ND 0.75 J ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.25 1.0 ND ND ND 1.1 ND ND ND ND ND ND ND ND ND ND
Resample 10-Nov-11 0.25 1.0 ---------0.76 J ---------------------------ND
03-Apr-12 0.25 1.0 ND ND ND 0.76 J ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.25 1.0 ND ND ND 0.61 J ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.25 1.0 ND ND ND 0.56 J ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.25 1.0 ND ND ND 0.73 J ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.25 1.0 ND ND ND 0.36 J ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.25 1.0 ND ND ND 0.65 J ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.25 1.0 ND ND ND 0.32 J ND ND 0.35 J ND ND ND ND ND ND ND
20-Oct-15 0.25 1.0 ND ND ND 0.43 J ND ---ND ND ND ND ND ND ND ND
Chlorobenzene 23-Apr-10 0.23 3.0 ND ND ND 0.40 J ND ND ND ND ND ND ND ND ND ND
NC 2L = 50 µg/L (10/23/07)28-Oct-10 0.23 3.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.23 3.0 ND ND ND 0.35 J ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.23 3.0 ND ND ND 0.61 J ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.23 3.0 ND ND ND 0.41 J ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.23 3.0 ND ND ND 0.32 J ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.23 3.0 ND ND ND 0.27 J ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.23 3.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.23 3.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.23 3.0 ND ND ND 0.33 J ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.23 3.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.23 3.0 ND ND ND 0.33 J ND ---ND ND ND ND ND ND ND ND
Chloroethane 23-Apr-10 0.54 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 3,000 µg/L (1/01/10)28-Oct-10 0.54 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.54 10.0 ND ND ND 0.82 J ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.54 10.0 ND ND ND 0.96 J ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.54 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.54 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.54 10.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.5 10.0 ND ND ND 0.84 J ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.5 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.5 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.5 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.5 10.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND
Chloromethane 15-Oct-09 0.11 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.25 J
Chloromethane 23-Apr-10 0.11 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 3 µg/L (1/01/10)28-Oct-10 0.11 1.0 ND ND ND ND ND ND ND ND ND 0.13 B ND ND ND 0.25 J
20-Apr-11 0.11 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.11 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.11 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.11 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.11 1.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.11 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.11 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.11 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.11 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.11 1.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND
1,4-Dichlorobenzene 20-Apr-11 0.33 1.0 ND ND ND 0.35 J ND ND ND ND ND ND ND ND ND ND
NC 2L = 6 µg/L (1/01/10)04-Oct-11 0.33 1.0 ND ND ND 0.49 J ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.33 1.0 ND ND ND 0.47 J ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.33 1.0 ND ND ND 0.38 J ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.33 1.0 ND ND ND 0.35 J ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.33 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.33 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.33 1.0 ND ND ND 0.47 J ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.33 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.33 1.0 ND ND ND 0.43 J ND ---ND ND ND ND ND ND ND ND
1,1-Dichloroethane 23-Apr-10 0.32 5.0 ND ND ND 0.94 J ND ND ND ND ND ND ND ND ND ND
NC 2L = 6 µg/L (1/01/10)28-Oct-10 0.32 5.0 ND ND ND 0.39 J ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.32 5.0 ND ND ND 0.91 J ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.32 5.0 ND ND ND 1.3 J ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.32 5.0 ND ND ND 0.68 J ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.32 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.32 5.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.3 5.0 ND ND ND 0.61 J ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.3 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.3 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.3 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.3 5.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND
Transylvania County Woodruff Landfill
Permit No. 88-07 3 of 5 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL GROUNDWATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-3 MW-10 MW-1 MW-2 MW-5 MW-6 MW-8 MW-9S/9SR MW-9D MW-11 MW-12S MW-12D MW-13 Blanks
Cis-1,2-Dichloroethene 23-Apr-10 0.19 5.0 ND ND ND 0.35 J ND ND ND ND ND ND ND ND ND ND
NC 2L = 70 µg/L (10/23/07)28-Oct-10 0.19 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.19 5.0 ND ND ND 0.45 J ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.19 5.0 ND ND ND 0.62 J ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.19 5.0 ND ND ND 0.22 J ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.19 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.19 5.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.19 5.0 ND ND ND 0.42 J ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.19 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.19 5.0 ND ND ND 0.28 J ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.19 5.0 ND ND ND 1.28 J ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.19 5.0 ND ND ND 0.27 J ND ---ND ND ND ND ND ND ND ND
2-Hexanone 23-Apr-10 0.46 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
GWPS = 280 µg/L (10/23/07) 28-Oct-10 0.46 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.46 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.46 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.46 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.46 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.46 50.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.46 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.46 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.46 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.46 50.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.46 50.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND

2-Butanone (MEK)23-Apr-10 0.96 100 ND ND ND ND ND ND 6.4 J ND ND ND ND ND ND ND
NC 2L = 4,000 µg/L (1/01/10)28-Oct-10 0.96 100 ND ND ND ND ND ND 2.7 J ND ND ND ND ND ND ND
20-Apr-11 0.96 100 ND ND ND ND ND ND 1.2 J ND ND ND ND ND ND ND
04-Oct-11 0.96 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.96 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.96 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.96 100 ND ND ND ND ND ND ND ---ND ND ND ND ND 4.5 J
23-Oct-13 0.96 100 ND ND ND ND ND ND 24.4 J ND ND ND ND ND ND ND
23-Apr-14 0.96 100 ND ND ND ND ND ND 3.2 J ND ND ND ND ND ND ND
07-Oct-14 0.96 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.96 100 ND ND ND ND ND ND 8.1 J ND ND ND ND ND ND ND
20-Oct-15 0.96 100 ND ND ND ND ND ---48.9 J ND ND ND ND ND ND ND
Methylene Chloride 23-Apr-10 0.97 2.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 5 µg/L (1/01/10)28-Oct-10 0.97 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND 21.9
20-Apr-11 0.97 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.97 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND 2.5
03-Apr-12 0.97 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.97 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.97 1.0 ND ND ND ND ND ND ND ---ND ND ND ND ND 1.5
23-Oct-13 0.97 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND 1.9
23-Apr-14 0.97 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.97 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.97 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND 14.8
20-Oct-15 0.97 1.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND
Tetrachloroethene 23-Apr-10 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 0.7 µg/L (10/23/07)28-Oct-10 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.46 1.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.46 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.46 1.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND
Toluene 23-Apr-10 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 600 µg/L (1/01/10)28-Oct-10 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.26 1.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.26 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.26 1.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND
Transylvania County Woodruff Landfill
Permit No. 88-07 4 of 5 Joyce Engineering
TABLE 3
SUMMARY OF HISTORICAL GROUNDWATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-3 MW-10 MW-1 MW-2 MW-5 MW-6 MW-8 MW-9S/9SR MW-9D MW-11 MW-12S MW-12D MW-13 Blanks
Xylene (Total)23-Apr-10 0.66 2.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NC 2L = 500 µg/L (1/01/10)28-Oct-10 0.66 2.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Apr-11 0.66 2.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04-Oct-11 0.66 2.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Apr-12 0.66 2.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
03-Oct-12 0.66 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
24-Apr-13 0.66 5.0 ND ND ND ND ND ND ND ---ND ND ND ND ND ND
23-Oct-13 0.66 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
23-Apr-14 0.66 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07-Oct-14 0.66 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
22-Apr-15 0.66 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20-Oct-15 0.66 5.0 ND ND ND ND ND ---ND ND ND ND ND ND ND ND
Notes:
QL = Quantitation Limit
NC SWSL = North Carolina Solid Waste Section Limits
ND = Not detected above the laboratory reporting limit (February 1994 - October 2006). Not detected above the laboratory detection limit (April 2007 to present).
J = Estimated value since the concentration is below the laboratory's reporting limit.
B = Reported value suspected to represent blank contamination.
L = Estimated value; value exceeded highest calibration sample.
NC 2L Standard = North Carolina's groundwater quality standard established under 15A NCAC 2L, ,0202.
All values above the NC 2L/GWP Standards are bold.
GWPS = Groundwater protection standard (used when NC 2L has not been established).
J1 = Qualifier used if the reported concentration has been rounded up to the RL due to EPA rounding rules. The concentration is considered to be estimated.
Dry = Monitoring well was considered to be dry and no sample collected.
--- = Not Monitored and/or Not Reported
NR = Not reported.
NA = Not available.
NI = Monitoring well was not installed.
MW-4 and MW-7 Were abandonded as part of the Phase 5 expansion historical data for these wells is avaliable upon request.
MW-9SR replaced MW-9R in October 2011
All historical data prior to April 2010 is avaliable upon request.
Transylvania County Woodruff Landfill
Permit No. 88-07 5 of 5 Joyce Engineering
TABLE 4
SUMMARY OF HISTORICAL GROUNDWATER FIELD PARAMETERS
Sample
Analyte Collection Date MW-3 MW-10 MW-1 MW-2 MW-5 MW-6 MW-8 MW-9S/9SR MW-9D MW-11 MW-12S MW-12D MW-13
pH 23-Apr-10 5.49 5.78 4.96 4.97 5.61 5.29 5.59 5.27 5.84 5.28 5.37 5.18 5.58
Resample 11-Jun-10 ------5.39 ---------------------5.63 ------
28-Oct-10 7.20 7.53 5.25 5.46 5.54 5.29 6.10 5.52 6.60 5.90 5.98 6.21 6.12
Resample 21-Dec-10 ---------------------5.10 ------5.62 ------
20-Apr-11 5.81 5.91 5.03 5.29 5.55 5.42 5.64 5.47 6.16 5.60 5.38 5.30 5.91
04-Oct-11 5.71 6.01 5.34 5.42 5.60 5.32 5.59 5.89 6.42 5.66 5.88 5.79 5.96
Resample 10-Nov-11 ---------5.59 ---------------------------
03-Apr-12 6.10 5.65 5.11 5.35 5.59 5.50 9.87 5.46 6.33 5.65 5.56 5.98 6.15
03-Oct-12 5.55 5.96 5.30 5.36 5.65 5.24 5.75 5.55 6.52 5.30 5.68 5.40 5.41
Resample 25-Oct-12 ---------------5.42 ---------------------
24-Apr-13 5.88 5.94 4.92 5.41 5.32 5.68 5.57 ---6.33 5.64 5.79 5.60 5.71
22-Oct-13 5.11 5.31 4.78 5.23 4.97 5.04 5.40 5.36 6.34 5.86 5.19 5.34 5.53
23-Apr-14 5.50 5.8 ---5.39 5.41 5.59 5.75 5.41 6.18 5.37 5.47 5.27 5.10
07-Oct-14 5.05 5.72 ---4.92 4.85 5.08 5.44 5.30 6.01 5.12 5.45 4.97 5.67
22-Apr-15 5.52 5.71 5.10 5.32 5.60 5.28 5.67 5.58 6.05 5.12 5.51 5.32 5.04
21-Oct-15 4.19 5.84 5.13 5.65 5.38 ---5.66 4.39 5.33 5.56 4.36 5.41 5.63
Conductivity 23-Apr-10 27.9 25.2 199 138.3 41.8 45.4 129.9 124.1 134.1 32.6 116.8 73.1 29.0
(µS/cm) Resample 11-Jun-10 ------299 ---------------------106.3 ------
28-Oct-10 68.1 27 138.9 132.6 86.8 65.8 152.9 152.5 197.7 51.0 177.0 59.7 35.7
Resample 21-Dec-10 ---------------------150.8 ------184.0 ------
20-Apr-11 22.7 70.7 141.1 174.4 47.8 78.5 145.8 160.3 186 46.1 114.3 53.1 48.9
04-Oct-11 31.1 28.3 243 191.5 45.7 80.9 135.6 176.4 188 39.8 183 43.0 33.4
Resample 10-Nov-11 ---------192 ---------------------------
03-Apr-12 27.10 41.1 184.60 157 41.10 76.40 153.0 153.9 182.0 41.1 124.7 50.1 38.3
03-Oct-12 27.8 19.2 167.8 139 40.1 61.3 147.2 159.4 198.2 59.5 118.7 46.6 30.8
Resample 25-Oct-12 ---------------67.4 ---------------------
24-Apr-13 26.3 17.19 84.6 152.9 40.9 63.6 133.2 ---181.4 36.7 118.4 61.6 46.2
22-Oct-13 25.00 17.9 152.3 171.9 38.9 64.5 127.0 164.0 171.9 38.3 96.1 66.9 37.3
23-Apr-14 38.20 19.51 ---124.8 39.2 74.8 163.4 175.2 199.1 32.0 103.8 75.8 36.3
07-Oct-14 28.20 24.3 ---183.2 42.1 84.9 158.8 191.0 185.0 31.8 120.8 77.0 41.6
22-Apr-15 26.00 13 83.0 114.0 34.0 62.0 141.0 179.0 182.0 27.0 94.0 72.0 32.0
21-Oct-15 28.00 36.0 109.0 201.0 39.0 ---137.0 172.0 189.0 32.0 109.0 90.0 43.0
Temperature 23-Apr-10 12.6 12.3 13.9 13.8 12.7 11.6 14.2 15.1 15.2 11.5 14.1 14.6 13.5
(degrees C) Resample 11-Jun-10 ------13.7 ---------------------13.5 ------
28-Oct-10 12.6 12.3 15.9 15.8 13.8 15.4 13.7 15.1 14.9 14.4 14.1 13.5 13.0
Resample 21-Dec-10 ---------------------14.6 ------13.3 ------
20-Apr-11 12.8 12.6 14.1 12.0 12.0 10.7 14.5 13.7 14.1 11.4 12.8 13.4 13.0
04-Oct-11 13.7 11.8 15.2 15.4 14.1 14.3 14.3 14.1 14.5 14.0 13.4 13.3 12.3
Resample 10-Nov-11 ---------14.0 ---------------------------
03-Apr-12 13.60 12.1 14.70 14.2 13.1 12.1 14.7 14.6 14.7 12.10 13.7 14.0 13.8
03-Oct-12 13.7 13.3 15.1 16.4 14.8 16.2 14.3 15.5 16.1 14.5 14.9 14.2 14.0
Resample 25-Oct-12 ---------------16.2 ---------------------
24-Apr-13 13.5 13.2 14.5 13.8 13.0 11.8 14.4 ---15.2 13.5 14.6 15.3 14.2
22-Oct-13 13.7 13.5 15.8 16.8 15.1 14.9 14.6 15.1 15.9 13.2 14.2 13.7 13.3
23-Apr-14 12.3 13.1 ---12.0 12.6 10.3 12.6 13.4 14.8 10.6 12.2 12.9 12.7
07-Oct-14 12.2 13.8 ---14.2 13.3 13.8 13.6 14.5 15.2 13.1 13.9 13.5 12.7
22-Apr-15 13.1 14.6 13.2 15.0 13.9 16.9 15.5 14.2 21.9 13.1 14.9 14.1 16.6
21-Oct-15 11.6 12.2 16.8 18.6 14.0 ---13.8 13.4 14.1 14.9 11.2 13.2 12.8
Turbidity 23-Apr-10 5.18 22.3 19.7 61.2 1.87 217 15.4 25.1 3.01 4.48 >1000 4.11 15.9
(NTUs) Resample 11-Jun-10 ------3.97 ---------------------6.09 ------
28-Oct-10 8.13 17.82 15.21 11.9 3.63 63.3 8.58 19.84 30.4 7.17 395 9.45 5.3
Resample 21-Dec-10 ---------------------37.7 ------320 ------
20-Apr-11 22.8 8.13 12.21 11.62 5.45 9.44 10.86 9.25 21.0 4.35 4.67 10.17 10.70
04-Oct-11 17.8 12.29 47.2 19.1 7.56 13.66 13.5 16.8 8.19 17.03 11.99 12.4 21.0
Resample 10-Nov-11 ---------86.7 ---------------------------
03-Apr-12 13.77 3.24 8.61 6.2 4.03 15.80 9.87 >1000 6.10 3.29 39.60 5.98 6.15
03-Oct-12 10.28 15.58 15.38 7.99 3.62 4.96 12.34 253 2.69 3.94 19.88 9.75 19.96
Resample 25-Oct-12 ---------------86.3 ---------------------
24-Apr-13 8.66 23 13.17 7.41 5.65 12.80 10.17 ---10.38 7.72 21.2 13.35 8.02
22-Oct-13 6.99 17.15 7.04 14.80 5.09 43.00 6.32 56.4 7.37 3.08 54.9 7.47 9.33
23-Apr-14 4.10 24 ---3.94 5.23 17.80 9.63 9.3 3.94 4.10 6.4 12.00 5.00
07-Oct-14 15.50 47.5 ---19.80 5.05 11.50 10.15 21.4 13.10 15.00 13.9 77.10 5.12
22-Apr-15 11.01 10.15 33.40 9.78 11.28 18.65 15.60 30.6 9.82 10.52 21.0 12.66 5.04
21-Oct-15 17.60 13.5 11.39 17.96 8.59 ---11.77 91.7 10.20 5.79 41.2 26.50 13.76
Notes:
All parameters were measured in the field.
Due to facility construction MW-4 and MW-7 were abandoned in July 2002.
MW-6 was dry during the October 2007 sampling event.
MW-4 and MW-7 Were abandonded as part of the Phase 5 expansion historical data for these wells is avaliable upon request.
MW-9SR replaced MW-9R in October 2011
--- = Not available and/or Not Sampled
All historical data prior to April 2010 is avaliable upon request.
Transylvania County Woodruff Landfill
Permit No. 88-07 1 of 1 Joyce Engineering
TABLE 5
SUMMARY OF HISTORICAL SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL SMP-1 SMP-3 Blanks
INORGANICS
Antimony 23-Apr-10 2.6 6.0 ND ND ND
NC2B= NE µg/L (05/01/07)28-Oct-10 2.6 6.0 ND ND ND
19-Apr-11 2.6 6.0 ND ND ND
05-Oct-11 5.0 6.0 ND ND ND
03-Apr-12 5.0 6.0 ND ND ND
03-Oct-12 5.0 6.0 ND ND ND
23-Apr-13 5.0 6.0 ND ND ND
22-Oct-13 5.0 6.0 ND ND ND
23-Apr-14 5.0 6.0 ND ND ND
07-Oct-14 5.0 6.0 ND ND ND
22-Apr-15 5.0 6.0 ND ND ND
20-Oct-15 3.8 6.0 ND Dry ND

Arsenic 23-Apr-10 2.7 10.0 ND ND ND
NC2B= 10 µg/L (05/01/07)28-Oct-10 2.7 10.0 10.5 ND ND
Resample 21-Dec-10 2.7 10.0 ND NS ND
19-Apr-11 2.7 10.0 ND ND ND
05-Oct-11 5.0 10.0 ND ND ND
03-Apr-12 5.0 10.0 ND ND ND
03-Oct-12 5.0 10.0 ND ND ND
23-Apr-13 5.0 10.0 ND ND ND
22-Oct-13 5.0 10.0 ND ND ND
23-Apr-14 5.0 10.0 ND ND ND
07-Oct-14 5.0 10.0 ND ND ND
22-Apr-15 5.0 10.0 ND ND ND
20-Oct-15 2.5 10.0 ND Dry ND
Barium 23-Apr-10 0.20 100 15.5 B 9.4 B 27.0 J
NC2B= NE µg/L (05/01/07)28-Oct-10 0.20 100 49.8 J 3.1 J ND
19-Apr-11 0.20 100 29.1 B 3.0 B 14.5 J
05-Oct-11 5.0 100 24 J 7.0 J ND
03-Apr-12 5.0 100 21.1 J 5.8 J ND
03-Oct-12 5.0 100 28.6 J ND ND
23-Apr-13 5.0 100 19.7 J ND ND
22-Oct-13 5.0 100 22.8 J 9.4 J ND
23-Apr-14 5.0 100 14.7 J ND ND
07-Oct-14 5.0 100 15.6 J ND ND
22-Apr-15 5.0 100 19.0 J 5.0 J ND
20-Oct-15 2.5 100 20.1 J Dry ND

Transylvania County Woodruff Landfill
Permit No. 88-07 1 of 7 Joyce Engineering
TABLE 5
SUMMARY OF HISTORICAL SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL SMP-1 SMP-3 Blanks
Beryllium 23-Apr-10 0.10 1.0 0.26 B 0.60 B 0.17 J
NC2B= 6.5 µg/L (05/01/07)28-Oct-10 0.10 1.0 0.34 J ND ND
19-Apr-11 0.10 1.0 ND ND ND
05-Oct-11 1.0 1.0 ND ND ND
03-Apr-12 1.0 1.0 ND ND ND
03-Oct-12 1.0 1.0 ND ND ND
23-Apr-13 1.0 1.0 ND ND ND
22-Oct-13 1.0 1.0 ND ND ND
23-Apr-14 1.0 1.0 ND ND ND
07-Oct-14 1.0 1.0 ND ND ND
22-Apr-15 1.0 1.0 ND ND ND
20-Oct-15 0.5 1.0 ND Dry ND

Cadmium 23-Apr-10 0.50 1.0 ND ND ND
NC2B= 0.4 µg/L (05/01/07)28-Oct-10 0.50 1.0 ND ND ND
19-Apr-11 0.50 1.0 ND ND ND
05-Oct-11 1.0 1.0 ND ND ND
03-Apr-12 1.0 1.0 ND ND ND
03-Oct-12 1.0 1.0 ND ND ND
23-Apr-13 1.0 1.0 ND ND ND
22-Oct-13 1.0 1.0 ND ND ND
23-Apr-14 1.0 1.0 ND ND ND
07-Oct-14 1.0 1.0 ND ND ND
22-Apr-15 1.0 1.0 ND ND ND
20-Oct-15 0.5 1.0 ND Dry ND
Chromium 23-Apr-10 0.40 10.0 1.0 B 0.88 B 0.41 J
NC2B= 50 µg/L (05/01/07)28-Oct-10 0.40 10.0 2.0 J ND ND
19-Apr-11 0.40 10.0 0.54 J 0.52 J ND
05-Oct-11 5.0 10.0 ND ND ND
03-Apr-12 5.0 10.0 ND ND ND
03-Oct-12 5.0 10.0 ND ND ND
23-Apr-13 5.0 10.0 ND ND ND
22-Oct-13 5.0 10.0 ND ND ND
23-Apr-14 5.0 10.0 ND ND ND
07-Oct-14 5.0 10.0 ND ND ND
22-Apr-15 5.0 10.0 ND ND ND
20-Oct-15 2.5 10.0 ND Dry 2.9 J

Transylvania County Woodruff Landfill
Permit No. 88-07 2 of 7 Joyce Engineering
TABLE 5
SUMMARY OF HISTORICAL SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL SMP-1 SMP-3 Blanks
Cobalt 23-Apr-10 0.60 10.0 2.6 J ND ND
NC2B= NE µg/L (05/01/07)28-Oct-10 0.60 10.0 0.96 B 1.6 B 3.2 J
19-Apr-11 0.60 10.0 5.2 J 1.4 J ND
05-Oct-11 5.0 10.0 ND ND ND
03-Apr-12 5.0 10.0 ND ND ND
03-Oct-12 5.0 10.0 ND ND ND
23-Apr-13 5.0 10.0 6.5 J ND ND
22-Oct-13 5.0 10.0 ND ND ND
23-Apr-14 5.0 10.0 ND ND ND
07-Oct-14 5.0 10.0 ND ND ND
22-Apr-15 5.0 10.0 ND ND ND
20-Oct-15 2.5 10.0 ND Dry ND
Copper 23-Apr-10 0.30 10.0 ND ND ND
NC2B= 7 µg/L (05/01/07)28-Oct-10 0.30 10.0 2.2 J ND ND
19-Apr-11 0.30 10.0 2.0 J 0.89 B 0.38 J
05-Oct-11 5.0 10.0 ND ND ND
03-Apr-12 5.0 10.0 ND ND ND
03-Oct-12 5.0 10.0 ND ND ND
23-Apr-13 5.0 10.0 ND ND ND
22-Oct-13 5.0 10.0 ND ND ND
23-Apr-14 5.0 10.0 ND ND ND
07-Oct-14 5.0 10.0 ND ND ND
22-Apr-15 5.0 10.0 ND ND ND
20-Oct-15 2.5 10.0 ND Dry ND

Lead 23-Apr-10 4.0 10.0 ND ND ND
NC2B= 25 µg/L (05/01/07)28-Oct-10 4.0 10.0 5.7 J ND ND
19-Apr-11 4.0 10.0 ND ND ND
05-Oct-11 5.0 10.0 ND ND ND
03-Apr-12 5.0 10.0 ND ND ND
03-Oct-12 5.0 10.0 ND ND ND
23-Apr-13 5.0 10.0 ND ND ND
22-Oct-13 5.0 10.0 ND ND ND
23-Apr-14 5.0 10.0 ND ND ND
07-Oct-14 5.0 10.0 ND ND ND
22-Apr-15 5.0 10.0 ND ND ND
20-Oct-15 2.5 10.0 ND Dry ND
Transylvania County Woodruff Landfill
Permit No. 88-07 3 of 7 Joyce Engineering
TABLE 5
SUMMARY OF HISTORICAL SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL SMP-1 SMP-3 Blanks
Nickel 23-Apr-10 1.7 50.0 ND ND ND
NC2B= 88 µg/L (05/01/07)28-Oct-10 1.7 50.0 ND ND ND
19-Apr-11 1.7 50.0 ND ND 5.8 J
05-Oct-11 5.0 50.0 ND ND ND
03-Apr-12 5.0 50.0 ND ND ND
03-Oct-12 5.0 50.0 ND ND ND
23-Apr-13 5.0 50.0 ND ND ND
22-Oct-13 5.0 50.0 ND ND ND
23-Apr-14 5.0 50.0 ND ND ND
07-Oct-14 5.0 50.0 ND ND ND
22-Apr-15 5.0 50.0 ND ND ND
20-Oct-15 2.5 50.0 ND Dry ND

Selenium 23-Apr-10 3.8 10.0 ND ND ND
NC2B= 5 µg/L (05/01/07)28-Oct-10 3.8 10.0 ND ND ND
19-Apr-11 3.8 10.0 ND ND ND
05-Oct-11 10.0 10.0 ND ND ND
03-Apr-12 10.0 10.0 ND ND ND
03-Oct-12 10.0 10.0 ND ND ND
23-Apr-13 10.0 10.0 ND ND ND
22-Oct-13 10.0 10.0 ND ND ND
23-Apr-14 10.0 10.0 ND ND ND
07-Oct-14 10.0 10.0 ND ND ND
22-Apr-15 10.0 10.0 ND ND ND
20-Oct-15 5.0 10.0 ND Dry ND

Silver 23-Apr-10 0.10 10.0 ND ND 0.16 J
NC2B= 0.06 µg/L (05/01/07)28-Oct-10 0.10 10.0 ND ND ND
19-Apr-11 0.10 10.0 ND ND ND
05-Oct-11 5.0 10.0 ND ND ND
03-Apr-12 5.0 10.0 ND ND ND
03-Oct-12 5.0 10.0 ND ND ND
23-Apr-13 5.0 10.0 ND ND ND
22-Oct-13 5.0 10.0 ND ND ND
23-Apr-14 5.0 10.0 ND ND ND
07-Oct-14 5.0 10.0 ND ND ND
22-Apr-15 5.0 10.0 ND ND ND
20-Oct-15 2.5 10.0 ND Dry ND

Transylvania County Woodruff Landfill
Permit No. 88-07 4 of 7 Joyce Engineering
TABLE 5
SUMMARY OF HISTORICAL SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL SMP-1 SMP-3 Blanks
Thallium 23-Apr-10 3.0 5.5 ND ND ND
NC2B= NE µg/L (05/01/07)28-Oct-10 3.0 5.5 ND ND ND
19-Apr-11 3.0 5.5 ND ND ND
05-Oct-11 5.4 5.5 ND ND ND
03-Apr-12 5.4 5.5 ND ND ND
03-Oct-12 5.4 5.5 ND ND ND
23-Apr-13 5.4 5.5 ND ND ND
22-Oct-13 5.4 5.5 ND ND ND
23-Apr-14 5.4 5.5 ND ND ND
07-Oct-14 5.4 5.5 ND ND ND
22-Apr-15 5.4 5.5 ND ND ND
20-Oct-15 5.0 5.5 ND Dry ND

Vanadium 23-Apr-10 0.20 25.0 0.54 B 0.94 B 0.64 J
NC2B= NE µg/L (05/01/07)28-Oct-10 0.20 25.0 3.2 J 0.24 J ND
19-Apr-11 0.20 25.0 0.74 J ND ND
05-Oct-11 5.0 25.0 ND ND ND
03-Apr-12 5.0 25.0 ND ND ND
03-Oct-12 5.0 25.0 ND ND ND
23-Apr-13 5.0 25.0 ND ND ND
22-Oct-13 5.0 25.0 ND ND ND
23-Apr-14 5.0 25.0 ND ND ND
07-Oct-14 5.0 25.0 ND ND ND
22-Apr-15 5.0 25.0 ND ND ND
20-Oct-15 2.5 25.0 ND Dry ND

Zinc 23-Apr-10 0.40 10.0 7.5 B 5.4 B 4.5 J
NC2B= 50 µg/L (05/01/07)28-Oct-10 0.40 10.0 13.1 ND ND
19-Apr-11 0.40 10.0 18.1 B 4.2 B 36.8
05-Oct-11 10.0 10.0 ND ND ND
03-Apr-12 10.0 10.0 ND ND ND
03-Oct-12 10.0 10.0 ND ND 12.2
23-Apr-13 10.0 10.0 12.3 ND ND
22-Oct-13 10.0 10.0 ND ND ND
23-Apr-14 10.0 10.0 ND ND ND
07-Oct-14 10.0 10.0 ND ND ND
22-Apr-15 10.0 10.0 9.4 B 7.1 B 6.15 B
20-Oct-15 5.0 10.0 ND Dry ND

Transylvania County Woodruff Landfill
Permit No. 88-07 5 of 7 Joyce Engineering
TABLE 5
SUMMARY OF HISTORICAL SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL SMP-1 SMP-3 Blanks
Organic Compounds
Acetone 23-Apr-10 2.2 100 3.1 J ND ND
NC2B= NE µg/L (05/01/07)28-Oct-10 2.2 100 13.8 J ND ND
19-Apr-11 2.2 100 ND ND ND
05-Oct-11 2.2 100 2.6 J ND ND
03-Apr-12 2.2 100 ND ND ND
03-Oct-12 10.0 100 ND ND ND
23-Apr-13 10.0 100 ND ND ND
22-Oct-13 10.0 100 ND ND ND
23-Apr-14 10.0 100 ND ND ND
07-Oct-14 10.0 100 ND ND ND
22-Apr-15 10.0 100 ND ND 20.5 J
20-Oct-15 10.0 100 ND Dry ND
2-Butanone (MEK)23-Apr-10 0.96 100 ND ND ND
NC2B= NE µg/L (05/01/07)28-Oct-10 0.96 100 4.9 J ND ND
19-Apr-11 0.96 100 ND ND ND
05-Oct-11 0.96 100 ND ND ND
03-Apr-12 0.96 100 ND ND ND
03-Oct-12 0.96 100 ND ND ND
23-Apr-13 0.96 100 ND ND ND
22-Oct-13 0.96 100 ND ND ND
23-Apr-14 0.96 100 ND ND ND
07-Oct-14 0.96 100 ND ND ND
22-Apr-15 0.96 100 ND ND ND
20-Oct-15 0.96 100 ND Dry ND
2-Hexanone 23-Apr-10 0.46 50.0 ND ND ND
NC2B= NE µg/L (05/01/07)28-Oct-10 0.46 50.0 ND ND ND
19-Apr-11 0.46 50.0 ND ND ND
05-Oct-11 0.46 50.0 ND ND ND
03-Apr-12 0.46 50.0 ND ND ND
03-Oct-12 0.46 50.0 ND ND ND
23-Apr-13 0.46 50.0 ND ND ND
22-Oct-13 0.46 50.0 ND ND ND
23-Apr-14 0.46 50.0 ND ND ND
07-Oct-14 0.46 50.0 ND ND ND
22-Apr-15 0.46 50.0 ND ND ND
20-Oct-15 0.46 50.0 ND Dry ND
Transylvania County Woodruff Landfill
Permit No. 88-07 6 of 7 Joyce Engineering
TABLE 5
SUMMARY OF HISTORICAL SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL SMP-1 SMP-3 Blanks
Toluene 23-Apr-10 0.26 1.0 ND ND ND
NC2B= 0.36 µg/L (05/01/07)28-Oct-10 0.26 1.0 0.36 J ND ND
19-Apr-11 0.26 1.0 ND ND ND
05-Oct-11 0.26 1.0 ND ND ND
03-Apr-12 0.26 1.0 ND ND ND
03-Oct-12 0.26 1.0 ND ND ND
23-Apr-13 0.26 1.0 ND ND ND
22-Oct-13 0.26 1.0 ND ND ND
23-Apr-14 0.26 1.0 ND ND ND
07-Oct-14 0.26 1.0 ND ND ND
22-Apr-15 0.26 1.0 ND ND ND
20-Oct-15 0.26 1.0 ND Dry ND
Notes:
Notes:
SMP-1 is located immediately downstream of the last sediment pond.
QL = Quantitation Limit
J = Estimated value since the concentration is below the laboratory's quantitation limit.
B = Reported value suspected to represent blank contamination
Dry = Monitoring point considered to be dry.
NE = Not established.
NR = Not reported.
All historical data prior to April 2010 is avaliable upon request
NC 2B Standard = North Carolina 2B Surface Water Standards. The surface waters at the sampling locations are classified at Freshwater Aquatic Life and Trout Waters.
ND = Not detected above the laboratory detection limit
Transylvania County Woodruff Landfill
Permit No. 88-07 7 of 7 Joyce Engineering
TABLE 6
SUMMARY OF HISTORICAL SURFACE WATER FIELD PARAMETERS
Sample
Analyte Collection Date SMP-1 SMP-3
pH 23-Apr-10 5.59 5.54
28-Oct-10 6.80 6.94
Resample 21-Dec-10 5.63 NS
19-Apr-11 6.10 6.13
05-Oct-11 6.43 6.23
03-Apr-12 5.81 7.11
03-Oct-12 7.44 6.67
23-Apr-13 5.99 5.81
22-Oct-13 5.70 6.14
23-Apr-14 6.62 5.96
07-Oct-14 6.77 6.01
22-Apr-15 6.78 5.90
21-Oct-15 6.10 Dry
Conductivity 23-Apr-10 79.8 20.7
(µS/cm)28-Oct-10 138.0 55.8
Resample 21-Dec-10 91.8 NS
19-Apr-11 99.1 20.0
05-Oct-11 123.2 27.0
03-Apr-12 113.8 28.1
03-Oct-12 23.3 107.3
23-Apr-13 98.8 101.3
22-Oct-13 97.0 29.6
23-Apr-14 99.0 20.3
07-Oct-14 97.2 24.3
22-Apr-15 100.0 15
21-Oct-15 98.0 Dry
Transylvania County Woodruff Landfill
Permit No. 88-07 1 of 2 Joyce Engineering
TABLE 6
SUMMARY OF HISTORICAL SURFACE WATER FIELD PARAMETERS
Sample
Analyte Collection Date SMP-1 SMP-3
Temperature 23-Apr-10 14.4 10.8
(degrees C)28-Oct-10 17.8 13.9
Resample 21-Dec-10 5.9 NS
19-Apr-11 15.4 12.0
05-Oct-11 13.6 11.6
03-Apr-12 16.7 12.3
03-Oct-12 15.8 16.8
23-Apr-13 14.1 13.4
22-Oct-13 14.9 15.7
23-Apr-14 11.9 10.9
07-Oct-14 17.1 14.4
22-Apr-15 19.3 11.5
21-Oct-15 12.6 Dry
Turbidity 23-Apr-10 8.84 3.87
(NTUs)28-Oct-10 55.8 4.77
Resample 21-Dec-10 16.75 NS
19-Apr-11 28.9 4.91
05-Oct-11 9.06 10.96
03-Apr-12 4.80 5.68
03-Oct-12 6.75 21.3
23-Apr-13 10.66 20.8
22-Oct-13 3.86 8.93
23-Apr-14 28.20 4.33
07-Oct-14 12.15 10.17
22-Apr-15 25.70 8.97
21-Oct-15 7.71 Dry
Notes:
All parameters were measured in the field.
Dry = Surface water monitoring point considered to be dry.
Transylvania County Woodruff Landfill
Permit No. 88-07 2 of 2 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
INORGANICS
Antimony 23-Apr-10 2.6 6.0 3.3 J ND
28-Oct-10 2.6 6.0 ND ND
20-Apr-11 2.6 6.0 ND ND
05-Oct-11 5.0 6.0 ND ND
04-Apr-12 5.0 6.0 ND ND
03-Oct-12 5.0 6.0 ND ND
23-Apr-13 5.0 6.0 ND ND
23-Oct-13 5.0 6.0 ND ND
23-Apr-14 5.0 6.0 6.7 ND
08-Oct-14 5.0 6.0 5.6 J ND
22-Apr-15 3.8 6.0 6.7 ND
21-Oct-15 3.8 6.0 7.5 ND
Arsenic 23-Apr-10 2.7 10.0 41.1 ND
28-Oct-10 2.7 10.0 15.9 ND
20-Apr-11 2.7 10.0 ND ND
05-Oct-11 5.0 10.0 5.2 J ND
04-Apr-12 5.0 10.0 13.5 ND
03-Oct-12 5.0 10.0 ND ND
23-Apr-13 5.0 10.0 ND ND
23-Oct-13 5.0 10.0 8.1 J ND
23-Apr-14 5.0 10.0 5.5 J ND
08-Oct-14 5.0 10.0 6.2 J ND
22-Apr-15 2.5 10.0 5.2 J ND
21-Oct-15 2.5 10.0 4.5 J ND
Barium 23-Apr-10 0.20 100 819 27.0 J
28-Oct-10 0.20 100 401 ND
20-Apr-11 0.20 100 223 14.5 J
05-Oct-11 5.0 100 489 ND
04-Apr-12 5.0 100 479 ND
03-Oct-12 5.0 100 350 ND
23-Apr-13 5.0 100 380 ND
23-Oct-13 5.0 100 475 ND
23-Apr-14 5.0 100 282 ND
08-Oct-14 5.0 100 586 ND
22-Apr-15 2.5 100 434 ND
21-Oct-15 2.5 100 441 ND
Transylvania County Woodruff Landfill
Permit No. 88-07 1 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Beryllium 23-Apr-10 0.10 1.0 0.72 B 0.17 J
28-Oct-10 0.10 1.0 ND ND
20-Apr-11 0.10 1.0 ND ND
05-Oct-11 1.0 1.0 ND ND
04-Apr-12 1.0 1.0 ND ND
03-Oct-12 1.0 1.0 ND ND
23-Apr-13 1.0 1.0 ND ND
23-Oct-13 1.0 1.0 ND ND
23-Apr-14 1.0 1.0 ND ND
08-Oct-14 1.0 1.0 ND ND
22-Apr-15 0.5 1.0 ND ND
21-Oct-15 0.5 1.0 ND ND
Cadmium 23-Apr-10 0.50 1.0 ND ND
28-Oct-10 0.50 1.0 ND ND
20-Apr-11 0.50 1.0 ND ND
05-Oct-11 1.0 1.0 ND ND
04-Apr-12 1.0 1.0 ND ND
03-Oct-12 1.0 1.0 ND ND
23-Apr-13 1.0 1.0 ND ND
23-Oct-13 1.0 1.0 ND ND
23-Apr-14 1.0 1.0 ND ND
08-Oct-14 1.0 1.0 ND ND
22-Apr-15 0.5 1.0 ND ND
21-Oct-15 0.5 1.0 ND ND
Chromium 23-Apr-10 0.40 10.0 50.6 0.41 J
28-Oct-10 0.40 10.0 17.2 ND
20-Apr-11 0.40 10.0 10.4 ND
05-Oct-11 5.0 10.0 16.9 ND
04-Apr-12 5.0 10.0 28.7 ND
03-Oct-12 5.0 10.0 17.0 ND
23-Apr-13 5.0 10.0 23.6 ND
23-Oct-13 5.0 10.0 22.7 ND
23-Apr-14 5.0 10.0 13.1 ND
08-Oct-14 5.0 10.0 20.7 ND
22-Apr-15 2.5 10.0 15.4 ND
21-Oct-15 2.5 10.0 18.0 2.9 J
Transylvania County Woodruff Landfill
Permit No. 88-07 2 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Cobalt 23-Apr-10 0.60 10.0 27.1 ND
28-Oct-10 0.60 10.0 37.4 3.2 J
20-Apr-11 0.60 10.0 4.8 J ND
05-Oct-11 5.0 10.0 6.1 J ND
04-Apr-12 5.0 10.0 6.0 J ND
03-Oct-12 5.0 10.0 ND ND
23-Apr-13 5.0 10.0 14.1 ND
23-Oct-13 5.0 10.0 ND ND
23-Apr-14 5.0 10.0 ND ND
08-Oct-14 5.0 10.0 16.2 ND
22-Apr-15 2.5 10.0 3.4 J ND
21-Oct-15 2.5 10.0 5.2 J ND
Copper 23-Apr-10 0.30 10.0 8.5 J ND
28-Oct-10 0.30 10.0 3.9 J ND
20-Apr-11 0.30 10.0 6.6 J 0.38 J
05-Oct-11 5.0 10.0 ND ND
04-Apr-12 5.0 10.0 ND ND
03-Oct-12 5.0 10.0 ND ND
23-Apr-13 5.0 10.0 8.0 J ND
23-Oct-13 5.0 10.0 ND ND
23-Apr-14 5.0 10.0 5.1 J ND
08-Oct-14 5.0 10.0 ND ND
22-Apr-15 2.5 10.0 5.6 J ND
21-Oct-15 2.5 10.0 2.6 J ND
Lead 23-Apr-10 4.0 10.0 6.8 J ND
28-Oct-10 4.0 10.0 ND ND
20-Apr-11 4.0 10.0 ND ND
05-Oct-11 5.0 10.0 ND ND
04-Apr-12 5.0 10.0 ND ND
03-Oct-12 5.0 10.0 ND ND
23-Apr-13 5.0 10.0 ND ND
23-Oct-13 5.0 10.0 ND ND
23-Apr-14 5.0 10.0 ND ND
08-Oct-14 5.0 10.0 ND ND
22-Apr-15 2.5 10.0 ND ND
21-Oct-15 2.5 10.0 ND ND
Transylvania County Woodruff Landfill
Permit No. 88-07 3 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Nickel 23-Apr-10 1.7 50.0 28.1 J ND
28-Oct-10 1.7 50.0 12.8 J ND
20-Apr-11 1.7 50.0 10.4 B 5.8 J
05-Oct-11 5.0 50.0 18.4 J ND
04-Apr-12 5.0 50.0 20.8 J ND
03-Oct-12 5.0 50.0 17.2 J ND
23-Apr-13 5.0 50.0 23.6 J ND
23-Oct-13 5.0 50.0 26.0 J ND
23-Apr-14 5.0 50.0 14.8 J ND
08-Oct-14 5.0 50.0 21.7 J ND
22-Apr-15 2.5 50.0 18.1 J ND
21-Oct-15 2.5 50.0 17.0 J ND
Selenium 23-Apr-10 3.8 10.0 ND ND
28-Oct-10 3.8 10.0 ND ND
20-Apr-11 3.8 10.0 ND ND
05-Oct-11 10.0 10.0 ND ND
04-Apr-12 10.0 10.0 ND ND
03-Oct-12 10.0 10.0 ND ND
23-Apr-13 10.0 10.0 ND ND
23-Oct-13 10.0 10.0 ND ND
23-Apr-14 10.0 10.0 ND ND
08-Oct-14 10.0 10.0 12.5 ND
22-Apr-15 5.0 10.0 ND ND
21-Oct-15 5.0 10.0 ND ND
Silver 23-Apr-10 0.10 10.0 ND 0.16 J
28-Oct-10 0.10 10.0 ND ND
20-Apr-11 0.10 10.0 0.10 J ND
05-Oct-11 5.0 10.0 ND ND
04-Apr-12 5.0 10.0 ND ND
03-Oct-12 5.0 10.0 ND ND
23-Apr-13 5.0 10.0 ND ND
23-Oct-13 5.0 10.0 ND ND
23-Apr-14 5.0 10.0 ND ND
08-Oct-14 5.0 10.0 ND ND
22-Apr-15 2.5 10.0 ND ND
21-Oct-15 2.5 10.0 ND ND
Transylvania County Woodruff Landfill
Permit No. 88-07 4 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Thallium 28-Oct-10 3.0 5.5 ND ND
20-Apr-11 3.0 5.5 ND ND
05-Oct-11 5.4 5.5 ND ND
04-Apr-12 5.4 5.5 ND ND
03-Oct-12 5.4 5.5 ND ND
23-Apr-13 5.4 5.5 ND ND
23-Oct-13 5.4 5.5 ND ND
23-Apr-14 5.4 5.5 ND ND
08-Oct-14 5.4 5.5 ND ND
22-Apr-15 5.0 5.5 ND ND
21-Oct-15 5.0 5.5 ND ND
Vanadium 23-Apr-10 0.20 25.0 18.8 J 0.64 J
28-Oct-10 0.20 25.0 5.9 J ND
20-Apr-11 0.20 25.0 ND ND
05-Oct-11 5.0 25.0 ND ND
04-Apr-12 5.0 25.0 ND ND
03-Oct-12 5.0 25.0 ND ND
23-Apr-13 5.0 25.0 ND ND
23-Oct-13 5.0 25.0 5.7 J ND
23-Apr-14 5.0 25.0 ND ND
08-Oct-14 5.0 25.0 ND ND
22-Apr-15 2.5 25.0 4.0 J ND
21-Oct-15 2.5 25.0 3.6 J ND
Zinc 23-Apr-10 0.40 10.0 464 4.5 J
28-Oct-10 0.40 10.0 95.6 ND
20-Apr-11 0.40 10.0 68.1 B 36.8
05-Oct-11 10.0 10.0 28.3 ND
04-Apr-12 10.0 10.0 17.9 ND
03-Oct-12 10.0 10.0 16.7 B 12.2
23-Apr-13 10.0 10.0 107 ND
23-Oct-13 10.0 10.0 13.1 ND
23-Apr-14 10.0 10.0 58.1 ND
08-Oct-14 10.0 10.0 22.1 ND
22-Apr-15 5.0 10.0 61.8 6.15
21-Oct-15 5.0 10.0 28.2 ND
Transylvania County Woodruff Landfill
Permit No. 88-07 5 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Organic Compounds
Acetone 23-Apr-10 2.2 100 12.3 J ND
28-Oct-10 2.2 100 12.4 J ND
20-Apr-11 2.2 100 13.7 J ND
05-Oct-11 2.2 100 11.1 J ND
04-Apr-12 2.2 100 228 ND
25-Oct-12 10.0 100 ND ND
23-Apr-13 10.0 100 28.4 B 41.9 J
23-Oct-13 10.0 100 21.6 J ND
23-Apr-14 10.0 100 12.6 J ND
08-Oct-14 10.0 100 15.4 J ND
22-Apr-15 10.0 100 162 B 20.5 J
21-Oct-15 10.0 100 33.0 J ND
Benzene 23-Apr-10 0.25 1.0 ND ND
28-Oct-10 0.25 1.0 ND ND
20-Apr-11 0.25 1.0 ND ND
05-Oct-11 0.25 1.0 ND ND
04-Apr-12 0.25 1.0 ND ND
25-Oct-12 0.25 1.0 ND ND
23-Apr-13 0.25 1.0 0.46 J ND
23-Oct-13 0.25 1.0 ND ND
23-Apr-14 0.25 1.0 ND ND
08-Oct-14 0.25 1.0 ND ND
22-Apr-15 0.25 1.0 0.76 J ND
21-Oct-15 0.25 1.0 0.46 J ND
Bromomethane 22-Apr-15 0.29 10.0 1.0 J ND
21-Oct-15 0.29 10.0 ND ND
Chlorobenzene 23-Apr-10 0.23 3.0 0.23 J ND
28-Oct-10 0.23 3.0 ND ND
20-Apr-11 0.23 3.0 ND ND
05-Oct-11 0.23 3.0 ND ND
04-Apr-12 0.23 3.0 ND ND
25-Oct-12 0.23 3.0 ND ND
23-Apr-13 0.23 3.0 0.34 J ND
23-Oct-13 0.23 3.0 ND ND
23-Apr-14 0.23 3.0 0.23 J ND
08-Oct-14 0.23 3.0 0.28 J ND
22-Apr-15 0.23 3.0 0.64 J ND
21-Oct-15 0.23 3.0 0.42 J ND
Transylvania County Woodruff Landfill
Permit No. 88-07 6 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Chloroethane 23-Apr-10 0.54 10.0 ND ND
28-Oct-10 0.54 10.0 ND ND
20-Apr-11 0.54 10.0 ND ND
05-Oct-11 0.54 10.0 ND ND
04-Apr-12 0.54 10.0 ND ND
25-Oct-12 0.54 10.0 ND ND
23-Apr-13 0.54 10.0 ND ND
23-Oct-13 0.54 10.0 ND ND
23-Apr-14 0.54 10.0 ND ND
08-Oct-14 0.54 10.0 ND ND
22-Apr-15 0.54 10.0 ND ND
21-Oct-15 0.54 10.0 ND ND
1,2-Dichlorobenzene 23-Apr-10 0.30 5.0 ND ND
28-Oct-10 0.30 5.0 ND ND
20-Apr-11 0.30 5.0 ND ND
05-Oct-11 0.30 5.0 ND ND
04-Apr-12 0.30 5.0 ND ND
25-Oct-12 0.30 5.0 ND ND
23-Apr-13 0.30 5.0 ND ND
23-Oct-13 0.30 5.0 ND ND
23-Apr-14 0.30 5.0 ND ND
08-Oct-14 0.30 5.0 ND ND
22-Apr-15 0.30 5.0 ND ND
21-Oct-15 0.30 5.0 ND ND
1,4-Dichlorobenzene 23-Apr-10 0.33 1.0 2.7 ND
28-Oct-10 0.33 1.0 1.1 ND
20-Apr-11 0.33 1.0 1.4 ND
05-Oct-11 0.33 1.0 1.5 ND
04-Apr-12 0.33 1.0 1.7 ND
25-Oct-12 0.33 1.0 1.7 ND
23-Apr-13 0.33 1.0 1.4 ND
23-Oct-13 0.33 1.0 1.4 ND
23-Apr-14 0.33 1.0 1.3 ND
08-Oct-14 0.33 1.0 1.7 ND
22-Apr-15 0.33 1.0 1.6 ND
21-Oct-15 0.33 1.0 1.6 ND
Transylvania County Woodruff Landfill
Permit No. 88-07 7 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
1,1-Dichloroethane 23-Apr-10 0.32 5.0 0.93 J ND
28-Oct-10 0.32 5.0 ND ND
20-Apr-11 0.32 5.0 0.73 J ND
05-Oct-11 0.32 5.0 0.43 J ND
04-Apr-12 0.32 5.0 ND ND
25-Oct-12 0.32 5.0 0.41 J ND
23-Apr-13 0.32 5.0 ND ND
23-Oct-13 0.32 5.0 ND ND
23-Apr-14 0.32 5.0 ND ND
08-Oct-14 0.32 5.0 ND ND
22-Apr-15 0.32 5.0 0.36 J ND
21-Oct-15 0.32 5.0 ND ND
1,2-Dichloroethane 23-Apr-10 0.12 1.0 ND ND
28-Oct-10 0.12 1.0 ND ND
20-Apr-11 0.12 1.0 ND ND
05-Oct-11 0.12 1.0 ND ND
04-Apr-12 0.12 1.0 ND ND
25-Oct-12 0.12 1.0 ND ND
23-Apr-13 0.12 1.0 ND ND
23-Oct-13 0.12 1.0 ND ND
23-Apr-14 0.12 1.0 ND ND
08-Oct-14 0.12 1.0 ND ND
22-Apr-15 0.12 1.0 ND ND
21-Oct-15 0.24 1.0 ND ND
Cis-1,2-Dichloroethene 23-Apr-10 0.19 5.0 ND ND
28-Oct-10 0.19 5.0 ND ND
20-Apr-11 0.19 5.0 ND ND
05-Oct-11 0.19 5.0 ND ND
04-Apr-12 0.19 5.0 ND ND
25-Oct-12 0.19 5.0 ND ND
23-Apr-13 0.19 5.0 ND ND
23-Oct-13 0.19 5.0 ND ND
23-Apr-14 0.19 5.0 ND ND
08-Oct-14 0.19 5.0 ND ND
22-Apr-15 0.19 5.0 ND ND
21-Oct-15 0.19 5.0 ND ND
Transylvania County Woodruff Landfill
Permit No. 88-07 8 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Trans-1,2-Dichloroethene 23-Apr-10 0.49 5.0 ND ND
28-Oct-10 0.49 5.0 ND ND
20-Apr-11 0.49 5.0 ND ND
05-Oct-11 0.49 5.0 ND ND
04-Apr-12 0.49 5.0 ND ND
25-Oct-12 0.49 5.0 ND ND
23-Apr-13 0.49 5.0 ND ND
23-Oct-13 0.49 5.0 ND ND
23-Apr-14 0.49 5.0 ND ND
08-Oct-14 0.49 5.0 ND ND
22-Apr-15 0.49 5.0 ND ND
21-Oct-15 0.49 5.0 ND ND
Ethylbenzene 23-Apr-10 0.30 1.0 0.48 J ND
28-Oct-10 0.30 1.0 0.51 J ND
20-Apr-11 0.30 1.0 0.30 J ND
05-Oct-11 0.30 1.0 ND ND
04-Apr-12 0.30 1.0 4.5 ND
25-Oct-12 0.30 1.0 ND ND
23-Apr-13 0.30 1.0 ND ND
23-Oct-13 0.30 1.0 ND ND
23-Apr-14 0.30 1.0 ND ND
08-Oct-14 0.30 1.0 ND ND
22-Apr-15 0.30 1.0 ND ND
21-Oct-15 0.30 1.0 ND ND
2-Hexanone 23-Apr-10 0.46 50.0 ND ND
(Methyl butyl ketone)28-Oct-10 0.46 50.0 ND ND
20-Apr-11 0.46 50.0 ND ND
05-Oct-11 0.46 50.0 ND ND
04-Apr-12 0.46 50.0 3.6 J,D ND
25-Oct-12 0.46 50.0 ND ND
23-Apr-13 0.46 50.0 ND ND
23-Oct-13 0.46 50.0 ND ND
23-Apr-14 0.46 50.0 ND ND
08-Oct-14 0.46 50.0 ND ND
22-Apr-15 0.46 50.0 1.3 J ND
21-Oct-15 0.46 50.0 0.56 J ND
Transylvania County Woodruff Landfill
Permit No. 88-07 9 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Chloromethane 23-Apr-10 0.11 1.0 ND ND
28-Oct-10 0.11 1.0 ND 0.25 J
20-Apr-11 0.11 1.0 ND ND
05-Oct-11 0.11 1.0 ND ND
04-Apr-12 0.11 1.0 ND ND
25-Oct-12 0.11 1.0 ND ND
23-Apr-13 0.11 1.0 ND ND
23-Oct-13 0.11 1.0 ND ND
23-Apr-14 0.11 1.0 ND ND
08-Oct-14 0.11 1.0 ND ND
22-Apr-15 0.11 1.0 1.1 ND
21-Oct-15 0.11 1.0 ND ---
Methylene Chloride 23-Apr-10 0.97 2.0 ND ND
(Dichloromethane)28-Oct-10 0.97 1.0 ND 21.9
20-Apr-11 0.97 1.0 ND ND
05-Oct-11 0.97 1.0 ND 2.5
04-Apr-12 0.97 1.0 ND ND
25-Oct-12 0.97 1.0 ND ND
23-Apr-13 0.97 1.0 ND 1.5
23-Oct-13 0.97 1.0 ND ND
23-Apr-14 0.97 1.0 ND ND
08-Oct-14 0.97 1.0 ND ND
22-Apr-15 0.97 1.0 ND 14.8
21-Oct-15 0.97 1.0 ND ND
2-Butanone (MEK)23-Apr-10 0.96 100 ND ND
(Methyl Ethyl Ketone)28-Oct-10 0.96 100 ND ND
20-Apr-11 0.96 100 ND ND
05-Oct-11 0.96 100 ND ND
04-Apr-12 0.96 100 339 ND
25-Oct-12 0.96 100 ND ND
23-Apr-13 0.96 100 ND 4.5 J
23-Oct-13 0.96 100 ND ND
23-Apr-14 0.96 100 ND ND
08-Oct-14 0.96 100 ND ND
22-Apr-15 0.96 100 145 ND
21-Oct-15 0.96 100 1.6 J ND
Transylvania County Woodruff Landfill
Permit No. 88-07 10 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
4-Methyl-2-pentanone (MIBK)23-Apr-10 0.33 100 2.1 J ND
28-Oct-10 0.33 100 0.49 J ND
20-Apr-11 0.33 100 6.7 J ND
05-Oct-11 0.33 100 ND ND
04-Apr-12 0.33 100 1.3 J ND
25-Oct-12 0.33 100 ND ND
23-Apr-13 0.33 100 ND ND
23-Oct-13 0.33 100 0.98 J ND
23-Apr-14 0.33 100 ND ND
08-Oct-14 0.33 100 ND ND
22-Apr-15 0.33 100 4.3 J ND
21-Oct-15 0.33 100 2.0 J ND
Styrene 23-Apr-10 0.26 1.0 ND ND
28-Oct-10 0.26 1.0 ND ND
20-Apr-11 0.26 1.0 ND ND
05-Oct-11 0.26 1.0 ND ND
04-Apr-12 0.26 1.0 ND ND
25-Oct-12 0.26 1.0 ND ND
23-Apr-13 0.26 1.0 ND ND
23-Oct-13 0.26 1.0 ND ND
23-Apr-14 0.26 1.0 ND ND
08-Oct-14 0.26 1.0 ND ND
22-Apr-15 0.26 1.0 ND ND
21-Oct-15 0.26 1.0 ND ND
Tetrachloroethene 23-Apr-10 0.46 1.0 ND ND
28-Oct-10 0.46 1.0 ND ND
20-Apr-11 0.46 1.0 ND ND
05-Oct-11 0.46 1.0 ND ND
04-Apr-12 0.46 1.0 ND ND
25-Oct-12 0.46 1.0 ND ND
23-Apr-13 0.46 1.0 ND ND
23-Oct-13 0.46 1.0 ND ND
23-Apr-14 0.46 1.0 ND ND
08-Oct-14 0.46 1.0 ND ND
22-Apr-15 0.46 1.0 ND ND
21-Oct-15 0.46 1.0 ND ND
Transylvania County Woodruff Landfill
Permit No. 88-07 11 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Toluene 23-Apr-10 0.26 1.0 0.31 J ND
28-Oct-10 0.26 1.0 ND ND
20-Apr-11 0.26 1.0 ND ND
05-Oct-11 0.26 1.0 ND ND
04-Apr-12 0.26 1.0 1.3 ND
25-Oct-12 0.26 1.0 ND ND
23-Apr-13 0.26 1.0 0.28 J ND
23-Oct-13 0.26 1.0 ND ND
23-Apr-14 0.26 1.0 ND ND
08-Oct-14 0.26 1.0 ND ND
22-Apr-15 0.26 1.0 0.53 J ND
21-Oct-15 0.26 1.0 ND ND
Trichloroethene 23-Apr-10 0.47 1.0 ND ND
28-Oct-10 0.47 1.0 ND ND
20-Apr-11 0.47 1.0 ND ND
05-Oct-11 0.47 1.0 ND ND
04-Apr-12 0.47 1.0 ND ND
25-Oct-12 0.47 1.0 ND ND
23-Apr-13 0.47 1.0 ND ND
23-Oct-13 0.47 1.0 ND ND
23-Apr-14 0.47 1.0 ND ND
08-Oct-14 0.47 1.0 ND ND
22-Apr-15 0.47 1.0 ND ND
21-Oct-15 0.47 1.0 ND ND
Vinyl chloride 23-Apr-10 0.62 1.0 ND ND
28-Oct-10 0.62 1.0 ND ND
20-Apr-11 0.62 1.0 ND ND
05-Oct-11 0.62 1.0 ND ND
04-Apr-12 0.62 1.0 ND ND
25-Oct-12 0.62 1.0 ND ND
23-Apr-13 0.62 1.0 ND ND
23-Oct-13 0.62 1.0 ND ND
23-Apr-14 0.62 1.0 ND ND
08-Oct-14 0.62 1.0 ND ND
22-Apr-15 0.62 1.0 ND ND
21-Oct-15 0.62 1.0 ND ND
Transylvania County Woodruff Landfill
Permit No. 88-07 12 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Xylene (Total)23-Apr-10 0.66 2.0 3.3 ND
28-Oct-10 0.66 2.0 1.6 J ND
20-Apr-11 0.66 2.0 1.7 J ND
05-Oct-11 0.66 2.0 ND ND
04-Apr-12 0.66 2.0 13.2 ND
25-Oct-12 0.66 5.0 0.83 J ND
23-Apr-13 0.66 5.0 0.93 J ND
23-Oct-13 0.66 5.0 ND ND
23-Apr-14 0.66 5.0 ND ND
08-Oct-14 0.66 5.0 ND ND
22-Apr-15 0.66 5.0 9.7 ND
21-Oct-15 0.66 5.0 ND ND
BOD, 5 day 23-Apr-10 2,000 2,000 24,900 ND
28-Oct-10 2,000 2,000 4,200 ND
20-Apr-11 2,000 2,000 8,400 ND
05-Oct-11 2,000 2,000 8,400 ND
04-Apr-12 2,000 2,000 175,000 NM
03-Oct-12 2,000 2,000 2,400 NM
23-Apr-13 2,000 2,000 318,000 NM
23-Oct-13 2,000 2,000 15,500 NM
23-Apr-14 2,000 2,000 2,100 NM
08-Oct-14 2,000 2,000 24,000 NM
22-Apr-15 2,000 2,000 39,300 NM
21-Oct-15 2,000 2,000 3,000 ND
Chemical Oxygen Demand 23-Apr-10 NR 25,000 907,000 ND
28-Oct-10 25,000 25,000 250,000 ND
20-Apr-11 25,000 25,000 149,000 ND
05-Oct-11 25,000 25,000 320,000 ND
04-Apr-12 25,000 25,000 691,000 NM
03-Oct-12 25,000 25,000 275,000 NM
23-Apr-13 25,000 25,000 281,000 NM
23-Oct-13 25,000 25,000 443,000 NM
23-Apr-14 25,000 25,000 186,000 NM
08-Oct-14 12,500 25,000 396,000 NM
22-Apr-15 12,500 25,000 330,000 NM
21-Oct-15 12,500 25,000 267,000 ND
Transylvania County Woodruff Landfill
Permit No. 88-07 13 of 14 Joyce Engineering
TABLE 7
SUMMARY OF HISTORICAL LEACHATE CONSTITUENTS
Sample
Analyte Collection Date DL QL
Holding Tank
(LMP-3) Blanks
Nitrogen, Nitrate 23-Apr-10 100 10,000 ND ND
28-Oct-10 100 10,000 3,900 J ND
20-Apr-11 100 10,000 6,860 J ND
05-Oct-11 200 10,000 ND ND
04-Apr-12 200 10,000 ND ND
03-Oct-12 200 10,000 200 J ND
23-Apr-13 200 10,000 27,200 J ND
23-Oct-13 20.0 10,000 910 J ND
23-Apr-14 300.0 150,000 24000 J ND
08-Oct-14 20.0 10,000 1190 J ND
22-Apr-15 50.0 50,000 7330 J ND
21-Oct-15 50.0 50,000 12800 J ND
Phosphorus 23-Apr-10 100 100 190 ND
(as total phosphorus)28-Oct-10 100 100 962 ND
20-Apr-11 50 50 114 ND
05-Oct-11 50.0 50.0 139 ND
04-Apr-12 50.0 50.0 533 NM
03-Oct-12 50.0 50.0 135 ND
23-Apr-13 50.0 50.0 205 ND
23-Oct-13 50.0 50.0 166 ND
23-Apr-14 50.0 50.0 89.9 ND
08-Oct-14 25.0 50.0 272 ND
22-Apr-15 25.0 50.0 138 ND
21-Oct-15 25.0 50.0 162 ND
Sulfate 28-Oct-10 15,000 15,000 93,400 ND
20-Apr-11 15,000 750,000 59,000 J,D ND
05-Oct-11 10,000 10,000 56,900 D ND
04-Apr-12 5,000 5,000 20,100 NM
03-Oct-12 2,000 250,000 ND ND
23-Apr-13 20,000 2,500,000 159,000 J ND
23-Oct-13 10,000 1,250,000 75,600 J ND
23-Apr-14 10,000 1,250,000 90,800 J ND
08-Oct-14 10,000 1,250,000 84,900 J ND
22-Apr-15 2,000 500,000 56,600 J ND
21-Oct-15 5,000 1,250,000 51,500 J ND
Notes:
ND = Not detected at or above the laboratory's reporting or detection limit.
J = Estimated value since the concentration is below the laboratory quantitation limit.
All concentrations are in micrograms per liter (µg/L).
D = Indicates sample was diluted.
8260's sampled on 10/3/12 were not analyzed in hold time therefor the sample results are not reported.
A resample took place on 10/25/12 and those results are reported.
All data prior to April 2010 is avaliable upon request
Transylvania County Woodruff Landfill
Permit No. 88-07 14 of 14 Joyce Engineering
TABLE 8
SUMMARY OF HISTORICAL LEACHATE FIELD PARAMETERS
Sample
Analyte Collection Date
Holding
Tank (LMP-
3)
INORGANICS
pH 23-Apr-10 7.55
28-Oct-10 7.52
20-Apr-11 6.90
5-Oct-11 7.66
4-Apr-12 7.35
3-Oct-12 8.04
Resample 25-Oct-12 7.84
23-Apr-13 7.38
23-Oct-13 7.02
23-Apr-14 7.38
22-Apr-15 7.54
21-Oct-15 7.54
Temperature 23-Apr-10 20.2
(degrees C)28-Oct-10 21.8
20-Apr-11 18.4
5-Oct-11 15.9
4-Apr-12 19.7
3-Oct-12 17.9
Resample 25-Oct-12 17.3
23-Apr-13 18.8
23-Oct-13 14.9
23-Apr-14 16.5
22-Apr-15 22.2
21-Oct-15 17.1
Transylvania County Woodruff Landfill
Permit No. 88-07 1 of 2 Joyce Engineering
TABLE 8
SUMMARY OF HISTORICAL LEACHATE FIELD PARAMETERS
Sample
Analyte Collection Date
Holding
Tank (LMP-
3)
Conductivity 23-Apr-10 3,450
(µS/cm)28-Oct-10 2,780
20-Apr-11 2,360
5-Oct-11 4,240
4-Apr-12 4,430
3-Oct-12 2,980
Resample 25-Oct-12 3,980
23-Apr-13 4,020
23-Oct-13 4,090
23-Apr-14 2,780
22-Apr-15 3,542
21-Oct-15 17
Turbidity 23-Apr-10 197
(NTUs)28-Oct-10 40.3
20-Apr-11 12.72
5-Oct-11 21.0
4-Apr-12 6.09
3-Oct-12 17.55
Resample 25-Oct-12 16.15
23-Apr-13 19.89
23-Oct-13 21.4
23-Apr-14 62.8
22-Apr-15 29.3
21-Oct-15 17.5
Notes:
All parameters were measured in the field.
All data prior to April 2010 is avaliable upon request
Transylvania County Woodruff Landfill
Permit No. 88-07 2 of 2 Joyce Engineering

Figure
Figure 1 Site Location Map

Drawing
Drawing 1 Potentiometric Surface Contour Map

Appendices

Appendix 1 Laboratory Analytical Reports and Field Data Logs
Appendix 2 Summary of Detections
Appendix 3 Summary of Field Parameters Appendix 4 Summary of Monitoring Well Construction

Appendix 1 Laboratory Analytical Reports and Field Data Logs

#=CL#
October 31, 2015
LIMS USE: FR - ALEX EVERHART
LIMS OBJECT ID: 92272822
92272822
Project:
Pace Project No.:
RE:
Mr. Alex Everhart
Joyce Engineering-NC
2211 W. Meadowview Road
Suite 101
Greensboro, NC 27407
TRANSYLVANIA-WOODRUFF
Dear Mr. Everhart:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
cc:Mr. Van Burbach, Joyce Engineering-NC
Alex Everhart, Joyce Engineering-NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 50
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 50
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Lab ID Sample ID Matrix Date Collected Date Received
92272822001 8807-MW1 Water 10/20/15 14:21 10/21/15 14:45
92272822002 8807-MW2 Water 10/20/15 13:51 10/21/15 14:45
92272822003 8807-MW3 Water 10/20/15 09:25 10/21/15 14:45
92272822004 8807-MW5 Water 10/20/15 14:56 10/21/15 14:45
92272822005 8807-MW8 Water 10/20/15 13:08 10/21/15 14:45
92272822006 8807-MW9SR Water 10/21/15 09:53 10/21/15 14:45
92272822007 8807-MW9D Water 10/21/15 10:00 10/21/15 14:45
92272822008 8807-MW10 Water 10/21/15 09:12 10/21/15 14:45
92272822009 8807-MW11 Water 10/21/15 13:14 10/21/15 14:45
92272822010 8807-MW12S Water 10/21/15 09:38 10/21/15 14:45
92272822011 8807-MW12D Water 10/20/15 11:33 10/21/15 14:45
92272822012 8807-MW13 Water 10/20/15 10:22 10/21/15 14:45
92272822013 8807-SMP1 Water 10/20/15 14:58 10/21/15 14:45
92272822014 8807-FIELD BLANK Water 10/21/15 13:20 10/21/15 14:45
92272822015 8807-TRIP BLANK Water 10/19/15 05:30 10/21/15 14:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 50
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92272822001 8807-MW1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822002 8807-MW2 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822003 8807-MW3 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822004 8807-MW5 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822005 8807-MW8 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822006 8807-MW9SR EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822007 8807-MW9D EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822008 8807-MW10 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822009 8807-MW11 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822010 8807-MW12S EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822011 8807-MW12D EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822012 8807-MW13 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822013 8807-SMP1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822014 8807-FIELD BLANK EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
92272822015 8807-TRIP BLANK EPA 8260 50 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 4 of 50
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92272822001 8807-MW1
Barium 27.8J ug/L 10/27/15 21:17100EPA 6010
Beryllium 2.5 ug/L 10/27/15 21:171.0EPA 6010
Lead 5.6J ug/L 10/27/15 21:1710.0EPA 6010
92272822002 8807-MW2
Barium 36.6J ug/L 10/27/15 21:29100EPA 6010
Beryllium 0.60J ug/L 10/27/15 21:291.0EPA 6010
Cobalt 3.7J ug/L 10/27/15 21:2910.0EPA 6010
Lead 6.1J ug/L 10/27/15 21:2910.0EPA 6010
Benzene 0.43J ug/L 10/30/15 13:251.0EPA 8260
Chlorobenzene 0.33J ug/L 10/30/15 13:253.0EPA 8260
1,4-Dichlorobenzene 0.43J ug/L 10/30/15 13:251.0EPA 8260
cis-1,2-Dichloroethene 0.27J ug/L 10/30/15 13:255.0EPA 8260
92272822003 8807-MW3
Barium 5.9J ug/L 10/27/15 21:32100EPA 6010
Beryllium 2.1 ug/L 10/27/15 21:321.0EPA 6010
Lead 4.2J ug/L 10/27/15 21:3210.0EPA 6010
92272822004 8807-MW5
Zinc 6.3J ug/L 10/27/15 21:3610.0EPA 6010
92272822005 8807-MW8
Barium 21.4J ug/L 10/27/15 21:39100EPA 6010
Beryllium 0.91J ug/L 10/27/15 21:391.0EPA 6010
Cobalt 3.7J ug/L 10/27/15 21:3910.0EPA 6010
Copper 2.6J ug/L 10/27/15 21:3910.0EPA 6010
Lead 18.3 ug/L 10/27/15 21:3910.0EPA 6010
Zinc 5.3J ug/L 10/27/15 21:3910.0EPA 6010
2-Butanone (MEK)48.9J ug/L 10/30/15 14:15100EPA 8260
92272822006 8807-MW9SR
Arsenic 2.9J ug/L 10/27/15 21:4210.0EPA 6010
Barium 54.0J ug/L 10/27/15 21:42100EPA 6010
Beryllium 1.2 ug/L 10/27/15 21:421.0EPA 6010
Chromium 5.5J ug/L 10/27/15 21:4210.0EPA 6010
Copper 2.7J ug/L 10/27/15 21:4210.0EPA 6010
Lead 17.3 ug/L 10/27/15 21:4210.0EPA 6010
Zinc 7.9J ug/L 10/27/15 21:4210.0EPA 6010
92272822007 8807-MW9D
Beryllium 0.82J ug/L 10/27/15 21:451.0EPA 6010
92272822008 8807-MW10
Barium 5.3J ug/L 10/27/15 21:48100EPA 6010
Beryllium 0.62J ug/L 10/27/15 21:481.0EPA 6010
92272822009 8807-MW11
Barium 17.9J ug/L 10/27/15 21:51100EPA 6010
Beryllium 0.75J ug/L 10/27/15 21:511.0EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 50
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92272822009 8807-MW11
Chromium 4.8J ug/L 10/27/15 21:5110.0EPA 6010
Cobalt 3.5J ug/L 10/27/15 21:5110.0EPA 6010
Copper 7.0J ug/L 10/27/15 21:5110.0EPA 6010
Nickel 14.9J ug/L 10/27/15 21:5150.0EPA 6010
92272822010 8807-MW12S
Barium 42.8J ug/L 10/27/15 21:54100EPA 6010
Cobalt 7.7J ug/L 10/27/15 21:5410.0EPA 6010
Copper 7.0J ug/L 10/27/15 21:5410.0EPA 6010
Lead 9.5J ug/L 10/27/15 21:5410.0EPA 6010
Zinc 6.9J ug/L 10/27/15 21:5410.0EPA 6010
92272822011 8807-MW12D
Barium 26.6J ug/L 10/27/15 21:58100EPA 6010
Beryllium 0.85J ug/L 10/27/15 21:581.0EPA 6010
Cobalt 3.2J ug/L 10/27/15 21:5810.0EPA 6010
Lead 4.1J ug/L 10/27/15 21:5810.0EPA 6010
Vanadium 2.9J ug/L 10/27/15 21:5825.0EPA 6010
92272822012 8807-MW13
Barium 34.3J ug/L 10/27/15 22:10100EPA 6010
92272822013 8807-SMP1
Barium 20.1J ug/L 10/27/15 22:13100EPA 6010
92272822014 8807-FIELD BLANK
Chromium 2.9J ug/L 10/29/15 01:5310.0EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 6 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW1 Lab ID:92272822001 Collected:10/20/15 14:21 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:17 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 21:17 7440-38-210/22/15 18:3010.0 2.5 1
Barium 27.8J ug/L 10/27/15 21:17 7440-39-310/22/15 18:301002.5 1
Beryllium 2.5 ug/L 10/27/15 21:17 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:17 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 21:17 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt ND ug/L 10/27/15 21:17 7440-48-410/22/15 18:3010.0 2.5 1
Copper ND ug/L 10/27/15 21:17 7440-50-810/22/15 18:3010.0 2.5 1
Lead 5.6J ug/L 10/27/15 21:17 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 21:17 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:17 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:17 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:17 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 21:17 7440-62-210/22/15 18:3025.0 2.5 1
Zinc ND ug/L 10/27/15 21:17 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 13:08 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 13:08 107-13-12001.9 1
Benzene ND ug/L 10/30/15 13:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 13:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 13:08 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 13:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 13:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 13:08 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 13:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 13:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 13:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 13:08 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 13:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 13:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 13:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 13:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 13:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 13:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 13:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 13:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 13:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 13:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 13:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 13:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 13:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 13:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 13:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 13:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 13:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW1 Lab ID:92272822001 Collected:10/20/15 14:21 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 13:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 13:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 13:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 13:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 13:08 108-10-11000.33 1
Styrene ND ug/L 10/30/15 13:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 13:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 13:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 13:08 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 13:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 13:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 13:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 13:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 13:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 13:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 13:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 13:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 13:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/30/15 13:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/30/15 13:08 17060-07-070-130 1
Toluene-d8 (S)99 %10/30/15 13:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW2 Lab ID:92272822002 Collected:10/20/15 13:51 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:29 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 21:29 7440-38-210/22/15 18:3010.0 2.5 1
Barium 36.6J ug/L 10/27/15 21:29 7440-39-310/22/15 18:301002.5 1
Beryllium 0.60J ug/L 10/27/15 21:29 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:29 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 21:29 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt 3.7J ug/L 10/27/15 21:29 7440-48-410/22/15 18:3010.0 2.5 1
Copper ND ug/L 10/27/15 21:29 7440-50-810/22/15 18:3010.0 2.5 1
Lead 6.1J ug/L 10/27/15 21:29 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 21:29 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:29 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:29 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:29 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 21:29 7440-62-210/22/15 18:3025.0 2.5 1
Zinc ND ug/L 10/27/15 21:29 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 13:25 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 13:25 107-13-12001.9 1
Benzene 0.43J ug/L 10/30/15 13:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 13:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 13:25 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 13:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 13:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 13:25 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 13:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 13:25 56-23-51.0 0.25 1
Chlorobenzene 0.33J ug/L 10/30/15 13:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 13:25 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 13:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 13:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 13:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 13:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 13:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 13:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 13:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.43J ug/L 10/30/15 13:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 13:25 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 13:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 13:25 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 13:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.27J ug/L 10/30/15 13:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 13:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 13:25 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 13:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 13:25 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW2 Lab ID:92272822002 Collected:10/20/15 13:51 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 13:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 13:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 13:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 13:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 13:25 108-10-11000.33 1
Styrene ND ug/L 10/30/15 13:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 13:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 13:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 13:25 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 13:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 13:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 13:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 13:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 13:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 13:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 13:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 13:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 13:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %10/30/15 13:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/30/15 13:25 17060-07-070-130 1
Toluene-d8 (S)99 %10/30/15 13:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW3 Lab ID:92272822003 Collected:10/20/15 09:25 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:32 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 21:32 7440-38-210/22/15 18:3010.0 2.5 1
Barium 5.9J ug/L 10/27/15 21:32 7440-39-310/22/15 18:301002.5 1
Beryllium 2.1 ug/L 10/27/15 21:32 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:32 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 21:32 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt ND ug/L 10/27/15 21:32 7440-48-410/22/15 18:3010.0 2.5 1
Copper ND ug/L 10/27/15 21:32 7440-50-810/22/15 18:3010.0 2.5 1
Lead 4.2J ug/L 10/27/15 21:32 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 21:32 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:32 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:32 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:32 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 21:32 7440-62-210/22/15 18:3025.0 2.5 1
Zinc ND ug/L 10/27/15 21:32 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 13:42 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 13:42 107-13-12001.9 1
Benzene ND ug/L 10/30/15 13:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 13:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 13:42 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 13:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 13:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 13:42 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 13:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 13:42 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 13:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 13:42 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 13:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 13:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 13:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 13:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 13:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 13:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 13:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 13:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 13:42 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 13:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 13:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 13:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 13:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 13:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 13:42 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 13:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 13:42 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW3 Lab ID:92272822003 Collected:10/20/15 09:25 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 13:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 13:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 13:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 13:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 13:42 108-10-11000.33 1
Styrene ND ug/L 10/30/15 13:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 13:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 13:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 13:42 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 13:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 13:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 13:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 13:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 13:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 13:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 13:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 13:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 13:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/30/15 13:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/30/15 13:42 17060-07-070-130 1
Toluene-d8 (S)100 %10/30/15 13:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW5 Lab ID:92272822004 Collected:10/20/15 14:56 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:36 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 21:36 7440-38-210/22/15 18:3010.0 2.5 1
Barium ND ug/L 10/27/15 21:36 7440-39-310/22/15 18:301002.5 1
Beryllium ND ug/L 10/27/15 21:36 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:36 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 21:36 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt ND ug/L 10/27/15 21:36 7440-48-410/22/15 18:3010.0 2.5 1
Copper ND ug/L 10/27/15 21:36 7440-50-810/22/15 18:3010.0 2.5 1
Lead ND ug/L 10/27/15 21:36 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 21:36 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:36 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:36 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:36 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 21:36 7440-62-210/22/15 18:3025.0 2.5 1
Zinc 6.3J ug/L 10/27/15 21:36 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 13:58 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 13:58 107-13-12001.9 1
Benzene ND ug/L 10/30/15 13:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 13:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 13:58 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 13:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 13:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 13:58 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 13:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 13:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 13:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 13:58 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 13:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 13:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 13:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 13:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 13:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 13:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 13:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 13:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 13:58 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 13:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 13:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 13:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 13:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 13:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 13:58 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 13:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 13:58 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW5 Lab ID:92272822004 Collected:10/20/15 14:56 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 13:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 13:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 13:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 13:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 13:58 108-10-11000.33 1
Styrene ND ug/L 10/30/15 13:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 13:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 13:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 13:58 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 13:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 13:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 13:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 13:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 13:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 13:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 13:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 13:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 13:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/30/15 13:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/30/15 13:58 17060-07-070-130 1
Toluene-d8 (S)98 %10/30/15 13:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW8 Lab ID:92272822005 Collected:10/20/15 13:08 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:39 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 21:39 7440-38-210/22/15 18:3010.0 2.5 1
Barium 21.4J ug/L 10/27/15 21:39 7440-39-310/22/15 18:301002.5 1
Beryllium 0.91J ug/L 10/27/15 21:39 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:39 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 21:39 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt 3.7J ug/L 10/27/15 21:39 7440-48-410/22/15 18:3010.0 2.5 1
Copper 2.6J ug/L 10/27/15 21:39 7440-50-810/22/15 18:3010.0 2.5 1
Lead 18.3 ug/L 10/27/15 21:39 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 21:39 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:39 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:39 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:39 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 21:39 7440-62-210/22/15 18:3025.0 2.5 1
Zinc 5.3J ug/L 10/27/15 21:39 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 14:15 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 14:15 107-13-12001.9 1
Benzene ND ug/L 10/30/15 14:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 14:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 14:15 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 14:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 14:15 74-83-910.0 0.29 1
2-Butanone (MEK)48.9J ug/L 10/30/15 14:15 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 14:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 14:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 14:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 14:15 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 14:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 14:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 14:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 14:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 14:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 14:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 14:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 14:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 14:15 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 14:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 14:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 14:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 14:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 14:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 14:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 14:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 14:15 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW8 Lab ID:92272822005 Collected:10/20/15 13:08 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 14:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 14:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 14:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 14:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 14:15 108-10-11000.33 1
Styrene ND ug/L 10/30/15 14:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 14:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 14:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 14:15 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 14:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 14:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 14:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 14:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 14:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 14:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 14:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 14:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 14:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %10/30/15 14:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/30/15 14:15 17060-07-070-130 1
Toluene-d8 (S)99 %10/30/15 14:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW9SR Lab ID:92272822006 Collected:10/21/15 09:53 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:42 7440-36-010/22/15 18:306.0 3.8 1
Arsenic 2.9J ug/L 10/27/15 21:42 7440-38-210/22/15 18:3010.0 2.5 1
Barium 54.0J ug/L 10/27/15 21:42 7440-39-310/22/15 18:301002.5 1
Beryllium 1.2 ug/L 10/27/15 21:42 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:42 7440-43-910/22/15 18:301.0 0.50 1
Chromium 5.5J ug/L 10/27/15 21:42 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt ND ug/L 10/27/15 21:42 7440-48-410/22/15 18:3010.0 2.5 1
Copper 2.7J ug/L 10/27/15 21:42 7440-50-810/22/15 18:3010.0 2.5 1
Lead 17.3 ug/L 10/27/15 21:42 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 21:42 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:42 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:42 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:42 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 21:42 7440-62-210/22/15 18:3025.0 2.5 1
Zinc 7.9J ug/L 10/27/15 21:42 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 14:32 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 14:32 107-13-12001.9 1
Benzene ND ug/L 10/30/15 14:32 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 14:32 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 14:32 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 14:32 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 14:32 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 14:32 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 14:32 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 14:32 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 14:32 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 14:32 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 14:32 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 14:32 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 14:32 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 14:32 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 14:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 14:32 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 14:32 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 14:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 14:32 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 14:32 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 14:32 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 14:32 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 14:32 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 14:32 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 14:32 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 14:32 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 14:32 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW9SR Lab ID:92272822006 Collected:10/21/15 09:53 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 14:32 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 14:32 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 14:32 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 14:32 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 14:32 108-10-11000.33 1
Styrene ND ug/L 10/30/15 14:32 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 14:32 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 14:32 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 14:32 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 14:32 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 14:32 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 14:32 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 14:32 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 14:32 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 14:32 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 14:32 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 14:32 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 14:32 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %10/30/15 14:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/30/15 14:32 17060-07-070-130 1
Toluene-d8 (S)101 %10/30/15 14:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW9D Lab ID:92272822007 Collected:10/21/15 10:00 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:45 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 21:45 7440-38-210/22/15 18:3010.0 2.5 1
Barium ND ug/L 10/27/15 21:45 7440-39-310/22/15 18:301002.5 1
Beryllium 0.82J ug/L 10/27/15 21:45 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:45 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 21:45 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt ND ug/L 10/27/15 21:45 7440-48-410/22/15 18:3010.0 2.5 1
Copper ND ug/L 10/27/15 21:45 7440-50-810/22/15 18:3010.0 2.5 1
Lead ND ug/L 10/27/15 21:45 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 21:45 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:45 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:45 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:45 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 21:45 7440-62-210/22/15 18:3025.0 2.5 1
Zinc ND ug/L 10/27/15 21:45 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 14:49 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 14:49 107-13-12001.9 1
Benzene ND ug/L 10/30/15 14:49 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 14:49 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 14:49 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 14:49 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 14:49 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 14:49 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 14:49 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 14:49 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 14:49 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 14:49 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 14:49 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 14:49 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 14:49 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 14:49 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 14:49 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 14:49 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 14:49 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 14:49 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 14:49 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 14:49 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 14:49 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 14:49 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 14:49 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 14:49 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 14:49 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 14:49 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 14:49 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW9D Lab ID:92272822007 Collected:10/21/15 10:00 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 14:49 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 14:49 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 14:49 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 14:49 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 14:49 108-10-11000.33 1
Styrene ND ug/L 10/30/15 14:49 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 14:49 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 14:49 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 14:49 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 14:49 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 14:49 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 14:49 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 14:49 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 14:49 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 14:49 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 14:49 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 14:49 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 14:49 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %10/30/15 14:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/30/15 14:49 17060-07-070-130 1
Toluene-d8 (S)101 %10/30/15 14:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW10 Lab ID:92272822008 Collected:10/21/15 09:12 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:48 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 21:48 7440-38-210/22/15 18:3010.0 2.5 1
Barium 5.3J ug/L 10/27/15 21:48 7440-39-310/22/15 18:301002.5 1
Beryllium 0.62J ug/L 10/27/15 21:48 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:48 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 21:48 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt ND ug/L 10/27/15 21:48 7440-48-410/22/15 18:3010.0 2.5 1
Copper ND ug/L 10/27/15 21:48 7440-50-810/22/15 18:3010.0 2.5 1
Lead ND ug/L 10/27/15 21:48 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 21:48 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:48 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:48 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:48 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 21:48 7440-62-210/22/15 18:3025.0 2.5 1
Zinc ND ug/L 10/27/15 21:48 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 15:05 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 15:05 107-13-12001.9 1
Benzene ND ug/L 10/30/15 15:05 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 15:05 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 15:05 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 15:05 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 15:05 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 15:05 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 15:05 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 15:05 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 15:05 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 15:05 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 15:05 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 15:05 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 15:05 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 15:05 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 15:05 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 15:05 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 15:05 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 15:05 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 15:05 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 15:05 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 15:05 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 15:05 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 15:05 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 15:05 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 15:05 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 15:05 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 15:05 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW10 Lab ID:92272822008 Collected:10/21/15 09:12 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 15:05 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 15:05 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 15:05 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 15:05 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 15:05 108-10-11000.33 1
Styrene ND ug/L 10/30/15 15:05 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 15:05 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 15:05 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 15:05 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 15:05 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 15:05 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 15:05 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 15:05 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 15:05 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 15:05 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 15:05 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 15:05 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 15:05 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/30/15 15:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %10/30/15 15:05 17060-07-070-130 1
Toluene-d8 (S)100 %10/30/15 15:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW11 Lab ID:92272822009 Collected:10/21/15 13:14 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:51 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 21:51 7440-38-210/22/15 18:3010.0 2.5 1
Barium 17.9J ug/L 10/27/15 21:51 7440-39-310/22/15 18:301002.5 1
Beryllium 0.75J ug/L 10/27/15 21:51 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:51 7440-43-910/22/15 18:301.0 0.50 1
Chromium 4.8J ug/L 10/27/15 21:51 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt 3.5J ug/L 10/27/15 21:51 7440-48-410/22/15 18:3010.0 2.5 1
Copper 7.0J ug/L 10/27/15 21:51 7440-50-810/22/15 18:3010.0 2.5 1
Lead ND ug/L 10/27/15 21:51 7439-92-110/22/15 18:3010.0 2.5 1
Nickel 14.9J ug/L 10/27/15 21:51 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:51 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:51 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:51 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 21:51 7440-62-210/22/15 18:3025.0 2.5 1
Zinc ND ug/L 10/27/15 21:51 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 15:22 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 15:22 107-13-12001.9 1
Benzene ND ug/L 10/30/15 15:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 15:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 15:22 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 15:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 15:22 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 15:22 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 15:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 15:22 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 15:22 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 15:22 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 15:22 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 15:22 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 15:22 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 15:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 15:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 15:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 15:22 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 15:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 15:22 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 15:22 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 15:22 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 15:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 15:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 15:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 15:22 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 15:22 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 15:22 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW11 Lab ID:92272822009 Collected:10/21/15 13:14 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 15:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 15:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 15:22 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 15:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 15:22 108-10-11000.33 1
Styrene ND ug/L 10/30/15 15:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 15:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 15:22 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 15:22 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 15:22 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 15:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 15:22 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 15:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 15:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 15:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 15:22 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 15:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 15:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/30/15 15:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/30/15 15:22 17060-07-070-130 1
Toluene-d8 (S)100 %10/30/15 15:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW12S Lab ID:92272822010 Collected:10/21/15 09:38 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:54 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 21:54 7440-38-210/22/15 18:3010.0 2.5 1
Barium 42.8J ug/L 10/27/15 21:54 7440-39-310/22/15 18:301002.5 1
Beryllium ND ug/L 10/27/15 21:54 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:54 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 21:54 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt 7.7J ug/L 10/27/15 21:54 7440-48-410/22/15 18:3010.0 2.5 1
Copper 7.0J ug/L 10/27/15 21:54 7440-50-810/22/15 18:3010.0 2.5 1
Lead 9.5J ug/L 10/27/15 21:54 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 21:54 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:54 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:54 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:54 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 21:54 7440-62-210/22/15 18:3025.0 2.5 1
Zinc 6.9J ug/L 10/27/15 21:54 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 15:39 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 15:39 107-13-12001.9 1
Benzene ND ug/L 10/30/15 15:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 15:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 15:39 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 15:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 15:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 15:39 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 15:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 15:39 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 15:39 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 15:39 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 15:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 15:39 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 15:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 15:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 15:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 15:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 15:39 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 15:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 15:39 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 15:39 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 15:39 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 15:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 15:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 15:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 15:39 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 15:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 15:39 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW12S Lab ID:92272822010 Collected:10/21/15 09:38 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 15:39 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 15:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 15:39 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 15:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 15:39 108-10-11000.33 1
Styrene ND ug/L 10/30/15 15:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 15:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 15:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 15:39 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 15:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 15:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 15:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 15:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 15:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 15:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 15:39 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 15:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 15:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/30/15 15:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/30/15 15:39 17060-07-070-130 1
Toluene-d8 (S)100 %10/30/15 15:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW12D Lab ID:92272822011 Collected:10/20/15 11:33 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 21:58 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 21:58 7440-38-210/22/15 18:3010.0 2.5 1
Barium 26.6J ug/L 10/27/15 21:58 7440-39-310/22/15 18:301002.5 1
Beryllium 0.85J ug/L 10/27/15 21:58 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 21:58 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 21:58 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt 3.2J ug/L 10/27/15 21:58 7440-48-410/22/15 18:3010.0 2.5 1
Copper ND ug/L 10/27/15 21:58 7440-50-810/22/15 18:3010.0 2.5 1
Lead 4.1J ug/L 10/27/15 21:58 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 21:58 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 21:58 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 21:58 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 21:58 7440-28-010/22/15 18:305.5 5.0 1
Vanadium 2.9J ug/L 10/27/15 21:58 7440-62-210/22/15 18:3025.0 2.5 1
Zinc ND ug/L 10/27/15 21:58 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 15:55 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 15:55 107-13-12001.9 1
Benzene ND ug/L 10/30/15 15:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 15:55 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 15:55 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 15:55 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 15:55 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 15:55 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 15:55 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 15:55 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 15:55 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 15:55 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 15:55 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 15:55 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 15:55 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 15:55 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 15:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 15:55 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 15:55 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 15:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 15:55 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 15:55 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 15:55 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 15:55 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 15:55 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 15:55 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 15:55 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 15:55 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 15:55 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW12D Lab ID:92272822011 Collected:10/20/15 11:33 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 15:55 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 15:55 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 15:55 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 15:55 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 15:55 108-10-11000.33 1
Styrene ND ug/L 10/30/15 15:55 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 15:55 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 15:55 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 15:55 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 15:55 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 15:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 15:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 15:55 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 15:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 15:55 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 15:55 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 15:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 15:55 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/30/15 15:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/30/15 15:55 17060-07-070-130 1
Toluene-d8 (S)100 %10/30/15 15:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW13 Lab ID:92272822012 Collected:10/20/15 10:22 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 22:10 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 22:10 7440-38-210/22/15 18:3010.0 2.5 1
Barium 34.3J ug/L 10/27/15 22:10 7440-39-310/22/15 18:301002.5 1
Beryllium ND ug/L 10/27/15 22:10 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 22:10 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 22:10 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt ND ug/L 10/27/15 22:10 7440-48-410/22/15 18:3010.0 2.5 1
Copper ND ug/L 10/27/15 22:10 7440-50-810/22/15 18:3010.0 2.5 1
Lead ND ug/L 10/27/15 22:10 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 22:10 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 22:10 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 22:10 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 22:10 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 22:10 7440-62-210/22/15 18:3025.0 2.5 1
Zinc ND ug/L 10/27/15 22:10 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 16:12 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 16:12 107-13-12001.9 1
Benzene ND ug/L 10/30/15 16:12 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 16:12 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 16:12 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 16:12 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 16:12 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 16:12 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 16:12 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 16:12 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 16:12 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 16:12 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 16:12 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 16:12 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 16:12 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 16:12 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 16:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 16:12 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 16:12 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 16:12 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 16:12 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 16:12 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 16:12 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 16:12 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 16:12 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 16:12 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 16:12 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 16:12 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 16:12 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
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Page 29 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-MW13 Lab ID:92272822012 Collected:10/20/15 10:22 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 16:12 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 16:12 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 16:12 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 16:12 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 16:12 108-10-11000.33 1
Styrene ND ug/L 10/30/15 16:12 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 16:12 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 16:12 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 16:12 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 16:12 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 16:12 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 16:12 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 16:12 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 16:12 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 16:12 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 16:12 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 16:12 75-01-4 M11.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 16:12 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %10/30/15 16:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/30/15 16:12 17060-07-070-130 1
Toluene-d8 (S)99 %10/30/15 16:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-SMP1 Lab ID:92272822013 Collected:10/20/15 14:58 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/27/15 22:13 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/27/15 22:13 7440-38-210/22/15 18:3010.0 2.5 1
Barium 20.1J ug/L 10/27/15 22:13 7440-39-310/22/15 18:301002.5 1
Beryllium ND ug/L 10/27/15 22:13 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/27/15 22:13 7440-43-910/22/15 18:301.0 0.50 1
Chromium ND ug/L 10/27/15 22:13 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt ND ug/L 10/27/15 22:13 7440-48-410/22/15 18:3010.0 2.5 1
Copper ND ug/L 10/27/15 22:13 7440-50-810/22/15 18:3010.0 2.5 1
Lead ND ug/L 10/27/15 22:13 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/27/15 22:13 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/27/15 22:13 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/27/15 22:13 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/27/15 22:13 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/27/15 22:13 7440-62-210/22/15 18:3025.0 2.5 1
Zinc ND ug/L 10/27/15 22:13 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 16:29 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 16:29 107-13-12001.9 1
Benzene ND ug/L 10/30/15 16:29 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 16:29 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 16:29 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 16:29 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 16:29 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 16:29 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 16:29 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 16:29 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 16:29 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 16:29 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 16:29 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 16:29 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 16:29 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 16:29 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 16:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 16:29 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 16:29 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 16:29 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 16:29 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 16:29 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 16:29 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 16:29 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 16:29 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 16:29 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 16:29 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 16:29 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 16:29 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-SMP1 Lab ID:92272822013 Collected:10/20/15 14:58 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 16:29 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 16:29 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 16:29 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 16:29 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 16:29 108-10-11000.33 1
Styrene ND ug/L 10/30/15 16:29 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 16:29 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 16:29 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 16:29 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 16:29 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 16:29 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 16:29 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 16:29 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 16:29 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 16:29 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 16:29 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 16:29 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 16:29 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/30/15 16:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/30/15 16:29 17060-07-070-130 1
Toluene-d8 (S)100 %10/30/15 16:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-FIELD BLANK Lab ID:92272822014 Collected:10/21/15 13:20 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 10/29/15 01:53 7440-36-010/22/15 18:306.0 3.8 1
Arsenic ND ug/L 10/29/15 01:53 7440-38-210/22/15 18:3010.0 2.5 1
Barium ND ug/L 10/29/15 01:53 7440-39-310/22/15 18:301002.5 1
Beryllium ND ug/L 10/29/15 01:53 7440-41-710/22/15 18:301.0 0.50 1
Cadmium ND ug/L 10/29/15 01:53 7440-43-910/22/15 18:301.0 0.50 1
Chromium 2.9J ug/L 10/29/15 01:53 7440-47-310/22/15 18:3010.0 2.5 1
Cobalt ND ug/L 10/29/15 01:53 7440-48-410/22/15 18:3010.0 2.5 1
Copper ND ug/L 10/29/15 01:53 7440-50-810/22/15 18:3010.0 2.5 1
Lead ND ug/L 10/29/15 01:53 7439-92-110/22/15 18:3010.0 2.5 1
Nickel ND ug/L 10/29/15 01:53 7440-02-010/22/15 18:3050.0 2.5 1
Selenium ND ug/L 10/29/15 01:53 7782-49-210/22/15 18:3010.0 5.0 1
Silver ND ug/L 10/29/15 01:53 7440-22-410/22/15 18:3010.0 2.5 1
Thallium ND ug/L 10/29/15 01:53 7440-28-010/22/15 18:305.5 5.0 1
Vanadium ND ug/L 10/29/15 01:53 7440-62-210/22/15 18:3025.0 2.5 1
Zinc ND ug/L 10/29/15 01:53 7440-66-610/22/15 18:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 17:02 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 17:02 107-13-12001.9 1
Benzene ND ug/L 10/30/15 17:02 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 17:02 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 17:02 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 17:02 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 17:02 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 17:02 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 17:02 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 17:02 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 17:02 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 17:02 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 17:02 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 17:02 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 17:02 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 17:02 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 17:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 17:02 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 17:02 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 17:02 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 17:02 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 17:02 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 17:02 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 17:02 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 17:02 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 17:02 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 17:02 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 17:02 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 17:02 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-FIELD BLANK Lab ID:92272822014 Collected:10/21/15 13:20 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/15 17:02 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 17:02 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 17:02 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 17:02 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 17:02 108-10-11000.33 1
Styrene ND ug/L 10/30/15 17:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 17:02 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 17:02 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 17:02 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 17:02 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 17:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 17:02 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 17:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 17:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 17:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 17:02 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 17:02 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/15 17:02 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %10/30/15 17:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/30/15 17:02 17060-07-070-130 1
Toluene-d8 (S)98 %10/30/15 17:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-TRIP BLANK Lab ID:92272822015 Collected:10/19/15 05:30 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/15 17:19 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/15 17:19 107-13-12001.9 1
Benzene ND ug/L 10/30/15 17:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/15 17:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/15 17:19 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/15 17:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/15 17:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/15 17:19 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/15 17:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/15 17:19 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/15 17:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/15 17:19 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/15 17:19 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/15 17:19 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/15 17:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/15 17:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/15 17:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/15 17:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/15 17:19 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/15 17:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/15 17:19 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/15 17:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/15 17:19 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/15 17:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/15 17:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/15 17:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/15 17:19 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/15 17:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/15 17:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/30/15 17:19 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/15 17:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/15 17:19 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/15 17:19 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/15 17:19 108-10-11000.33 1
Styrene ND ug/L 10/30/15 17:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/15 17:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/15 17:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/15 17:19 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/15 17:19 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/15 17:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/15 17:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/15 17:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/15 17:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/15 17:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/15 17:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/15 17:19 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Sample:8807-TRIP BLANK Lab ID:92272822015 Collected:10/19/15 05:30 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 10/30/15 17:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/30/15 17:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/30/15 17:19 17060-07-070-130 1
Toluene-d8 (S)101 %10/30/15 17:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19872
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92272822001, 92272822002, 92272822003, 92272822004, 92272822005, 92272822006, 92272822007,
92272822008, 92272822009, 92272822010, 92272822011, 92272822012, 92272822013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1589124
Associated Lab Samples:92272822001, 92272822002, 92272822003, 92272822004, 92272822005, 92272822006, 92272822007,
92272822008, 92272822009, 92272822010, 92272822011, 92272822012, 92272822013
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 10/27/15 20:283.8
Arsenic ug/L ND 10.0 10/27/15 20:282.5
Barium ug/L ND 100 10/27/15 20:282.5
Beryllium ug/L ND 1.0 10/27/15 20:280.50
Cadmium ug/L ND 1.0 10/27/15 20:280.50
Chromium ug/L ND 10.0 10/27/15 20:282.5
Cobalt ug/L ND 10.0 10/27/15 20:282.5
Copper ug/L ND 10.0 10/27/15 20:282.5
Lead ug/L ND 10.0 10/27/15 20:282.5
Nickel ug/L ND 50.0 10/27/15 20:282.5
Selenium ug/L ND 10.0 10/27/15 20:285.0
Silver ug/L ND 10.0 10/27/15 20:282.5
Thallium ug/L ND 5.5 10/27/15 20:285.0
Vanadium ug/L ND 25.0 10/27/15 20:282.5
Zinc ug/L ND 10.0 10/27/15 20:285.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1589125LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 500500 100 80-120
Arsenic ug/L 472500 94 80-120
Barium ug/L 496500 99 80-120
Beryllium ug/L 497500 99 80-120
Cadmium ug/L 490500 98 80-120
Chromium ug/L 491500 98 80-120
Cobalt ug/L 488500 98 80-120
Copper ug/L 496500 99 80-120
Lead ug/L 484500 97 80-120
Nickel ug/L 491500 98 80-120
Selenium ug/L 480500 96 80-120
Silver ug/L 238250 95 80-120
Thallium ug/L 478500 96 80-120
Vanadium ug/L 491500 98 80-120
Zinc ug/L 478500 96 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1589126MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272853001
1589127
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 97 75-12598 2 25500ND484493
Arsenic ug/L 500 91 75-12593 2 25500ND456464
Barium ug/L 500 97 75-12598 1 2550036.3 522 529
Beryllium ug/L 500 98 75-12599 1 25500ND490494
Cadmium ug/L 500 95 75-12596 1 25500ND476482
Chromium ug/L 500 96 75-12597 1 2550031.6 510 515
Cobalt ug/L 500 94 75-12596 2 25500ND471480
Copper ug/L 500 97 75-12599 2 25500ND487496
Lead ug/L 500 93 75-12595 2 25500ND466473
Nickel ug/L 500 95 75-12596 2 2550020.5 494 502
Selenium ug/L 500 92 75-12593 2 25500ND460470
Silver ug/L 250 93 75-12594 1 25250ND233236
Thallium ug/L 500 94 75-12594 1 25500ND468470
Vanadium ug/L 500 95 75-12597 1 25500ND480486
Zinc ug/L 500 92 75-12593 2 255005.1J 464 471
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1589128MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272854004
1589129
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 93 75-12593 1 25500ND468465
Arsenic ug/L 500 91 75-12590 2 25500ND457449
Barium ug/L 500 99 75-12597 1 25500108601592
Beryllium ug/L 500 97 75-12595 2 25500ND486476
Cadmium ug/L 500 94 75-12592 2 25500ND469461
Chromium ug/L 500 96 75-12594 2 2550017.3 497 486
Cobalt ug/L 500 91 75-12590 1 255003.7J 461 454
Copper ug/L 500 97 75-12595 2 2550010.4 496 488
Lead ug/L 500 90 75-12589 1 255007.1 459 453
Nickel ug/L 500 92 75-12591 2 255008.1 470 462
Selenium ug/L 500 90 75-12589 1 25500ND452447
Silver ug/L 250 93 75-12591 2 25250ND232227
Thallium ug/L 500 89 75-12587 2 25500ND444436
Vanadium ug/L 500 97 75-12595 2 2550017.7 503 494
Zinc ug/L 500 90 75-12589 2 2550028.0 479 472
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19873
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92272822014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1589142
Associated Lab Samples:92272822014
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 10/29/15 01:473.8
Arsenic ug/L ND 10.0 10/29/15 01:472.5
Barium ug/L ND 100 10/29/15 01:472.5
Beryllium ug/L ND 1.0 10/29/15 01:470.50
Cadmium ug/L ND 1.0 10/29/15 01:470.50
Chromium ug/L ND 10.0 10/29/15 01:472.5
Cobalt ug/L ND 10.0 10/29/15 01:472.5
Copper ug/L ND 10.0 10/29/15 01:472.5
Lead ug/L ND 10.0 10/29/15 01:472.5
Nickel ug/L ND 50.0 10/29/15 01:472.5
Selenium ug/L ND 10.0 10/29/15 01:475.0
Silver ug/L ND 10.0 10/29/15 01:472.5
Thallium ug/L ND 5.5 10/29/15 01:475.0
Vanadium ug/L ND 25.0 10/29/15 01:472.5
Zinc ug/L ND 10.0 10/29/15 01:475.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1589143LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 504500 101 80-120
Arsenic ug/L 479500 96 80-120
Barium ug/L 479500 96 80-120
Beryllium ug/L 479500 96 80-120
Cadmium ug/L 480500 96 80-120
Chromium ug/L 479500 96 80-120
Cobalt ug/L 528500 106 80-120
Copper ug/L 490500 98 80-120
Lead ug/L 478500 96 80-120
Nickel ug/L 479500 96 80-120
Selenium ug/L 466500 93 80-120
Silver ug/L 239250 96 80-120
Thallium ug/L 484500 97 80-120
Vanadium ug/L 497500 99 80-120
Zinc ug/L 500500 100 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1589145MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272822014
1589146
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 100 75-12599 1 25500ND502496
Arsenic ug/L 500 94 75-12594 1 25500ND471468
Barium ug/L 500 94 75-12593 1 25500ND471466
Beryllium ug/L 500 94 75-12593 1 25500ND472467
Cadmium ug/L 500 95 75-12594 1 25500ND476470
Chromium ug/L 500 94 75-12593 1 255002.9J 473 469
Cobalt ug/L 500 105 75-125103 2 25500ND524516
Copper ug/L 500 96 75-12596 0 25500ND480482
Lead ug/L 500 95 75-12593 2 25500ND476468
Nickel ug/L 500 95 75-12593 1 25500ND474467
Selenium ug/L 500 92 75-12591 2 25500ND461454
Silver ug/L 250 94 75-12594 0 25250ND234234
Thallium ug/L 500 96 75-12596 0 25500ND480481
Vanadium ug/L 500 98 75-12598 0 25500ND492490
Zinc ug/L 500 98 75-12596 2 25500ND491481
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1589147MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272855003
1589148
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 102 75-12598 4 25500ND509491
Arsenic ug/L 500 96 75-12592 5 25500ND481460
Barium ug/L 500 96 75-12593 3 2550078.4 560 542
Beryllium ug/L 500 97 75-12594 3 25500ND486471
Cadmium ug/L 500 97 75-12593 4 25500ND487468
Chromium ug/L 500 97 75-12594 3 25500ND487471
Cobalt ug/L 500 107 75-125103 3 25500ND533515
Copper ug/L 500 100 75-12596 4 25500ND501479
Lead ug/L 500 96 75-12593 3 25500ND483466
Nickel ug/L 500 97 75-12593 4 25500ND483466
Selenium ug/L 500 94 75-12590 4 25500ND470449
Silver ug/L 250 97 75-12593 4 25250ND242233
Thallium ug/L 500 99 75-12595 4 25500ND493473
Vanadium ug/L 500 102 75-12598 3 25500ND509492
Zinc ug/L 500 100 75-12597 3 25500ND501485
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34056
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92272822001, 92272822002, 92272822003, 92272822004, 92272822005, 92272822006, 92272822007,
92272822008, 92272822009, 92272822010, 92272822011, 92272822012, 92272822013, 92272822014,
92272822015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1595562
Associated Lab Samples:92272822001, 92272822002, 92272822003, 92272822004, 92272822005, 92272822006, 92272822007,
92272822008, 92272822009, 92272822010, 92272822011, 92272822012, 92272822013, 92272822014,
92272822015
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 10/30/15 11:450.33
1,1,1-Trichloroethane ug/L ND 1.0 10/30/15 11:450.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 10/30/15 11:450.40
1,1,2-Trichloroethane ug/L ND 1.0 10/30/15 11:450.29
1,1-Dichloroethane ug/L ND 5.0 10/30/15 11:450.32
1,1-Dichloroethene ug/L ND 5.0 10/30/15 11:450.56
1,2,3-Trichloropropane ug/L ND 1.0 10/30/15 11:450.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 10/30/15 11:452.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/30/15 11:450.27
1,2-Dichlorobenzene ug/L ND 5.0 10/30/15 11:450.30
1,2-Dichloroethane ug/L ND 1.0 10/30/15 11:450.24
1,2-Dichloropropane ug/L ND 1.0 10/30/15 11:450.27
1,4-Dichlorobenzene ug/L ND 1.0 10/30/15 11:450.33
2-Butanone (MEK)ug/L ND 100 10/30/15 11:450.96
2-Hexanone ug/L ND 50.0 10/30/15 11:450.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 10/30/15 11:450.33
Acetone ug/L ND 100 10/30/15 11:4510.0
Acrylonitrile ug/L ND 200 10/30/15 11:451.9
Benzene ug/L ND 1.0 10/30/15 11:450.25
Bromochloromethane ug/L ND 3.0 10/30/15 11:450.17
Bromodichloromethane ug/L ND 1.0 10/30/15 11:450.18
Bromoform ug/L ND 3.0 10/30/15 11:450.26
Bromomethane ug/L ND 10.0 10/30/15 11:450.29
Carbon disulfide ug/L ND 100 10/30/15 11:451.2
Carbon tetrachloride ug/L ND 1.0 10/30/15 11:450.25
Chlorobenzene ug/L ND 3.0 10/30/15 11:450.23
Chloroethane ug/L ND 10.0 10/30/15 11:450.54
Chloroform ug/L ND 5.0 10/30/15 11:450.14
Chloromethane ug/L ND 1.0 10/30/15 11:450.11
cis-1,2-Dichloroethene ug/L ND 5.0 10/30/15 11:450.19
cis-1,3-Dichloropropene ug/L ND 1.0 10/30/15 11:450.13
Dibromochloromethane ug/L ND 3.0 10/30/15 11:450.21
Dibromomethane ug/L ND 10.0 10/30/15 11:450.21
Ethylbenzene ug/L ND 1.0 10/30/15 11:450.30
Iodomethane ug/L ND 10.0 10/30/15 11:450.32
Methylene Chloride ug/L ND 1.0 10/30/15 11:450.97
Styrene ug/L ND 1.0 10/30/15 11:450.26
Tetrachloroethene ug/L ND 1.0 10/30/15 11:450.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1595562
Associated Lab Samples:92272822001, 92272822002, 92272822003, 92272822004, 92272822005, 92272822006, 92272822007,
92272822008, 92272822009, 92272822010, 92272822011, 92272822012, 92272822013, 92272822014,
92272822015
Matrix:Water
AnalyzedMDL
Toluene ug/L ND 1.0 10/30/15 11:450.26
trans-1,2-Dichloroethene ug/L ND 5.0 10/30/15 11:450.49
trans-1,3-Dichloropropene ug/L ND 1.0 10/30/15 11:450.26
trans-1,4-Dichloro-2-butene ug/L ND 100 10/30/15 11:451.0
Trichloroethene ug/L ND 1.0 10/30/15 11:450.47
Trichlorofluoromethane ug/L ND 1.0 10/30/15 11:450.20
Vinyl acetate ug/L ND 50.0 10/30/15 11:450.35
Vinyl chloride ug/L ND 1.0 10/30/15 11:450.62
Xylene (Total)ug/L ND 5.0 10/30/15 11:450.66
1,2-Dichloroethane-d4 (S)%101 70-130 10/30/15 11:45
4-Bromofluorobenzene (S)%102 70-130 10/30/15 11:45
Toluene-d8 (S)%99 70-130 10/30/15 11:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1595563LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.150 98 80-125
1,1,1-Trichloroethane ug/L 51.850 104 71-129
1,1,2,2-Tetrachloroethane ug/L 51.050 102 79-124
1,1,2-Trichloroethane ug/L 48.550 97 85-125
1,1-Dichloroethane ug/L 50.450 101 73-126
1,1-Dichloroethene ug/L 52.750 105 66-135
1,2,3-Trichloropropane ug/L 48.750 97 75-130
1,2-Dibromo-3-chloropropane ug/L 51.550 103 71-133
1,2-Dibromoethane (EDB)ug/L 50.650 101 83-124
1,2-Dichlorobenzene ug/L 49.850 100 80-133
1,2-Dichloroethane ug/L 46.350 93 67-128
1,2-Dichloropropane ug/L 48.250 96 75-132
1,4-Dichlorobenzene ug/L 49.150 98 78-130
2-Butanone (MEK)ug/L 98.0J100 98 61-144
2-Hexanone ug/L 101100 101 68-143
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 72-135
Acetone ug/L 94.6J100 95 48-146
Acrylonitrile ug/L 246250 98 40-160
Benzene ug/L 49.750 99 80-125
Bromochloromethane ug/L 52.150 104 71-125
Bromodichloromethane ug/L 52.350 105 78-124
Bromoform ug/L 50.250 100 71-128
Bromomethane ug/L 41.750 83 40-160
Carbon disulfide ug/L 50.8J50 102 50-160
Carbon tetrachloride ug/L 53.450 107 69-131
Chlorobenzene ug/L 49.050 98 81-122
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1595563LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroethane ug/L 46.450 93 39-148
Chloroform ug/L 50.350 101 73-127
Chloromethane ug/L 43.550 87 44-146
cis-1,2-Dichloroethene ug/L 49.150 98 74-124
cis-1,3-Dichloropropene ug/L 51.850 104 72-132
Dibromochloromethane ug/L 52.550 105 78-125
Dibromomethane ug/L 50.250 100 82-120
Ethylbenzene ug/L 49.950 100 79-121
Iodomethane ug/L 91.1100 91 39-154
Methylene Chloride ug/L 52.350 105 64-133
Styrene ug/L 50.650 101 84-126
Tetrachloroethene ug/L 50.550 101 78-122
Toluene ug/L 49.450 99 80-121
trans-1,2-Dichloroethene ug/L 49.950 100 71-127
trans-1,3-Dichloropropene ug/L 50.950 102 69-141
trans-1,4-Dichloro-2-butene ug/L 49.1J50 98 40-160
Trichloroethene ug/L 48.150 96 78-122
Trichlorofluoromethane ug/L 50.350 101 53-137
Vinyl acetate ug/L 106100 106 40-160
Vinyl chloride ug/L 53.050 106 58-137
Xylene (Total)ug/L 150150 100 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1595564MATRIX SPIKE SAMPLE:
MSSpike
Result
92272822012
1,1,1,2-Tetrachloroethane ug/L 21.820 109 70-130ND
1,1,1-Trichloroethane ug/L 24.620 123 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.220 111 70-130ND
1,1,2-Trichloroethane ug/L 20.520 103 70-130ND
1,1-Dichloroethane ug/L 24.220 121 70-130ND
1,1-Dichloroethene ug/L 26.020 130 70-166ND
1,2,3-Trichloropropane ug/L 21.520 108 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.320 102 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.020 110 70-130ND
1,2-Dichlorobenzene ug/L 21.720 108 70-130ND
1,2-Dichloroethane ug/L 20.920 104 70-130ND
1,2-Dichloropropane ug/L 21.620 108 70-130ND
1,4-Dichlorobenzene ug/L 21.520 107 70-130ND
2-Butanone (MEK)ug/L 42.3J40 106 70-130ND
2-Hexanone ug/L 43.4J40 108 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.3J40 108 70-130ND
Acetone ug/L 42.5J40 103 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1595564MATRIX SPIKE SAMPLE:
MSSpike
Result
92272822012
Acrylonitrile ug/L 111J100 111 70-130ND
Benzene ug/L 22.920 114 70-148ND
Bromochloromethane ug/L 24.320 122 70-130ND
Bromodichloromethane ug/L 22.220 111 70-130ND
Bromoform ug/L 19.820 99 70-130ND
Bromomethane ug/L 16.620 83 70-130ND
Carbon disulfide ug/L 24.0J20 120 70-130ND
Carbon tetrachloride ug/L 24.320 122 70-130ND
Chlorobenzene ug/L 22.620 113 70-146ND
Chloroethane ug/L 24.320 121 70-130ND
Chloroform ug/L 23.020 115 70-130ND
Chloromethane ug/L 24.120 120 70-130ND
cis-1,2-Dichloroethene ug/L 22.720 114 70-130ND
cis-1,3-Dichloropropene ug/L 21.420 107 70-130ND
Dibromochloromethane ug/L 21.620 108 70-130ND
Dibromomethane ug/L 21.420 107 70-130ND
Ethylbenzene ug/L 22.820 114 70-130ND
Iodomethane ug/L 30.740 77 70-130ND
Methylene Chloride ug/L 23.520 118 70-130ND
Styrene ug/L 22.120 111 70-130ND
Tetrachloroethene ug/L 23.020 115 70-130ND
Toluene ug/L 22.320 111 70-155ND
trans-1,2-Dichloroethene ug/L 23.920 120 70-130ND
trans-1,3-Dichloropropene ug/L 21.420 107 70-130ND
trans-1,4-Dichloro-2-butene ug/L 21.0J20 105 70-130ND
Trichloroethene ug/L 22.420 112 69-151ND
Trichlorofluoromethane ug/L 26.020 130 70-130ND
Vinyl acetate ug/L 42.2J40 106 70-130ND
Vinyl chloride ug/L 27.7 M12013970-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92272822013
1595565SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 44 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92272822013
1595565SAMPLE DUPLICATE:
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%102 2100
4-Bromofluorobenzene (S)%97 299
Toluene-d8 (S)%100 0100
REPORT OF LABORATORY ANALYSIS
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Page 45 of 50
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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Page 46 of 50
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92272822
TRANSYLVANIA-WOODRUFF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92272822001 MPRP/19872 ICP/179208807-MW1 EPA 3010 EPA 6010
92272822002 MPRP/19872 ICP/179208807-MW2 EPA 3010 EPA 6010
92272822003 MPRP/19872 ICP/179208807-MW3 EPA 3010 EPA 6010
92272822004 MPRP/19872 ICP/179208807-MW5 EPA 3010 EPA 6010
92272822005 MPRP/19872 ICP/179208807-MW8 EPA 3010 EPA 6010
92272822006 MPRP/19872 ICP/179208807-MW9SR EPA 3010 EPA 6010
92272822007 MPRP/19872 ICP/179208807-MW9D EPA 3010 EPA 6010
92272822008 MPRP/19872 ICP/179208807-MW10 EPA 3010 EPA 6010
92272822009 MPRP/19872 ICP/179208807-MW11 EPA 3010 EPA 6010
92272822010 MPRP/19872 ICP/179208807-MW12S EPA 3010 EPA 6010
92272822011 MPRP/19872 ICP/179208807-MW12D EPA 3010 EPA 6010
92272822012 MPRP/19872 ICP/179208807-MW13 EPA 3010 EPA 6010
92272822013 MPRP/19872 ICP/179208807-SMP1 EPA 3010 EPA 6010
92272822014 MPRP/19873 ICP/179218807-FIELD BLANK EPA 3010 EPA 6010
92272822001 MSV/340568807-MW1 EPA 8260
92272822002 MSV/340568807-MW2 EPA 8260
92272822003 MSV/340568807-MW3 EPA 8260
92272822004 MSV/340568807-MW5 EPA 8260
92272822005 MSV/340568807-MW8 EPA 8260
92272822006 MSV/340568807-MW9SR EPA 8260
92272822007 MSV/340568807-MW9D EPA 8260
92272822008 MSV/340568807-MW10 EPA 8260
92272822009 MSV/340568807-MW11 EPA 8260
92272822010 MSV/340568807-MW12S EPA 8260
92272822011 MSV/340568807-MW12D EPA 8260
92272822012 MSV/340568807-MW13 EPA 8260
92272822013 MSV/340568807-SMP1 EPA 8260
92272822014 MSV/340568807-FIELD BLANK EPA 8260
92272822015 MSV/340568807-TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
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Page 47 of 50
Page 48 of 50
Page 49 of 50
Page 50 of 50
#=CL#
October 31, 2015
LIMS USE: FR - ALEX EVERHART
LIMS OBJECT ID: 92272826
92272826
Project:
Pace Project No.:
RE:
Mr. Alex Everhart
Joyce Engineering-NC
2211 W. Meadowview Road
Suite 101
Greensboro, NC 27407
TRANSYLVANIA WOODRUFF LEACHATE
Dear Mr. Everhart:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
cc:Mr. Van Burbach, Joyce Engineering-NC
Alex Everhart, Joyce Engineering-NC
REPORT OF LABORATORY ANALYSIS
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Page 1 of 22
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 22
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Lab ID Sample ID Matrix Date Collected Date Received
92272826001 8807-LMP3 Water 10/21/15 13:15 10/21/15 14:45
REPORT OF LABORATORY ANALYSIS
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Page 3 of 22
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92272826001 8807-LMP3 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CCAH
SM 5210B 1 PASI-ABRJ
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-ADMN
EPA 365.1 1 PASI-AAES2
SM 5220D 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
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#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92272826001 8807-LMP3
Antimony 7.5 ug/L 10/29/15 00:176.0EPA 6010
Arsenic 4.5J ug/L 10/29/15 00:1710.0EPA 6010
Barium 441 ug/L 10/29/15 00:17100EPA 6010
Chromium 18.0 ug/L 10/29/15 00:1710.0EPA 6010
Cobalt 5.2J ug/L 10/29/15 00:1710.0EPA 6010
Copper 2.6J ug/L 10/29/15 00:1710.0EPA 6010
Nickel 17.0J ug/L 10/29/15 00:1750.0EPA 6010
Vanadium 3.6J ug/L 10/29/15 00:1725.0EPA 6010
Zinc 28.2 ug/L 10/29/15 00:1710.0EPA 6010
Acetone 33.0J ug/L 10/31/15 00:16100EPA 8260
Benzene 0.46J ug/L 10/31/15 00:161.0EPA 8260
2-Butanone (MEK)1.6J ug/L 10/31/15 00:16100EPA 8260
Chlorobenzene 0.42J ug/L 10/31/15 00:163.0EPA 8260
1,4-Dichlorobenzene 1.6 ug/L 10/31/15 00:161.0EPA 8260
2-Hexanone 0.56J ug/L 10/31/15 00:1650.0EPA 8260
4-Methyl-2-pentanone (MIBK)2.0J ug/L 10/31/15 00:16100EPA 8260
BOD, 5 day 3000 ug/L 10/27/15 22:49 B22000SM 5210B
Sulfate 51500J ug/L 10/29/15 17:071250000EPA 300.0
Nitrogen, Nitrate 12800J ug/L 10/22/15 10:1750000EPA 353.2
Phosphorus 162 ug/L 10/29/15 13:2050.0EPA 365.1
Chemical Oxygen Demand 267000 ug/L 10/22/15 21:0025000SM 5220D
REPORT OF LABORATORY ANALYSIS
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Page 5 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Sample:8807-LMP3 Lab ID:92272826001 Collected:10/21/15 13:15 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony 7.5 ug/L 10/29/15 00:17 7440-36-010/28/15 20:006.0 3.8 1
Arsenic 4.5J ug/L 10/29/15 00:17 7440-38-210/28/15 20:0010.0 2.5 1
Barium 441 ug/L 10/29/15 00:17 7440-39-310/28/15 20:001002.5 1
Beryllium ND ug/L 10/29/15 00:17 7440-41-710/28/15 20:001.0 0.50 1
Cadmium ND ug/L 10/29/15 00:17 7440-43-910/28/15 20:001.0 0.50 1
Chromium 18.0 ug/L 10/29/15 00:17 7440-47-310/28/15 20:0010.0 2.5 1
Cobalt 5.2J ug/L 10/29/15 00:17 7440-48-410/28/15 20:0010.0 2.5 1
Copper 2.6J ug/L 10/29/15 00:17 7440-50-810/28/15 20:0010.0 2.5 1
Lead ND ug/L 10/29/15 00:17 7439-92-110/28/15 20:0010.0 2.5 1
Nickel 17.0J ug/L 10/29/15 00:17 7440-02-010/28/15 20:0050.0 2.5 1
Selenium ND ug/L 10/29/15 00:17 7782-49-210/28/15 20:0010.0 5.0 1
Silver ND ug/L 10/29/15 00:17 7440-22-410/28/15 20:0010.0 2.5 1
Thallium ND ug/L 10/29/15 00:17 7440-28-010/28/15 20:005.5 5.0 1
Vanadium 3.6J ug/L 10/29/15 00:17 7440-62-210/28/15 20:0025.0 2.5 1
Zinc 28.2 ug/L 10/29/15 00:17 7440-66-610/28/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 33.0J ug/L 10/31/15 00:16 67-64-110010.0 1
Acrylonitrile ND ug/L 10/31/15 00:16 107-13-12001.9 1
Benzene 0.46J ug/L 10/31/15 00:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/31/15 00:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/31/15 00:16 75-27-41.0 0.18 1
Bromoform ND ug/L 10/31/15 00:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/31/15 00:16 74-83-910.0 0.29 1
2-Butanone (MEK)1.6J ug/L 10/31/15 00:16 78-93-31000.96 1
Carbon disulfide ND ug/L 10/31/15 00:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/31/15 00:16 56-23-51.0 0.25 1
Chlorobenzene 0.42J ug/L 10/31/15 00:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/31/15 00:16 75-00-310.0 0.54 1
Chloroform ND ug/L 10/31/15 00:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/31/15 00:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/31/15 00:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/31/15 00:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/31/15 00:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/31/15 00:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/31/15 00:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.6 ug/L 10/31/15 00:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/31/15 00:16 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/31/15 00:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/31/15 00:16 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/31/15 00:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/31/15 00:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/31/15 00:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/31/15 00:16 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/31/15 00:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/31/15 00:16 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Sample:8807-LMP3 Lab ID:92272826001 Collected:10/21/15 13:15 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/31/15 00:16 100-41-41.0 0.30 1
2-Hexanone 0.56J ug/L 10/31/15 00:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/31/15 00:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/31/15 00:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)2.0J ug/L 10/31/15 00:16 108-10-11000.33 1
Styrene ND ug/L 10/31/15 00:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/31/15 00:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/31/15 00:16 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/31/15 00:16 127-18-41.0 0.46 1
Toluene ND ug/L 10/31/15 00:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/31/15 00:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/31/15 00:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/31/15 00:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/31/15 00:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/31/15 00:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/31/15 00:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/31/15 00:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/31/15 00:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/31/15 00:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/31/15 00:16 17060-07-070-130 1
Toluene-d8 (S)101 %10/31/15 00:16 2037-26-570-130 1
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 3000 ug/L 10/27/15 22:49 B210/23/15 04:03200020001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 51500J ug/L 10/29/15 17:07 14808-79-8125000050005
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 12800J ug/L 10/22/15 10:175000050.0 5
Analytical Method: EPA 365.1365.1 Phosphorus, Total
Phosphorus 162 ug/L 10/29/15 13:20 7723-14-050.0 25.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 267000 ug/L 10/22/15 21:0025000125001
REPORT OF LABORATORY ANALYSIS
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Page 7 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19904
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92272826001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1593018
Associated Lab Samples:92272826001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 10/29/15 17:533.8
Arsenic ug/L ND 10.0 10/29/15 17:532.5
Barium ug/L ND 100 10/29/15 17:532.5
Beryllium ug/L ND 1.0 10/29/15 17:530.50
Cadmium ug/L ND 1.0 10/29/15 17:530.50
Chromium ug/L ND 10.0 10/29/15 17:532.5
Cobalt ug/L ND 10.0 10/29/15 17:532.5
Copper ug/L ND 10.0 10/29/15 17:532.5
Lead ug/L ND 10.0 10/29/15 17:532.5
Nickel ug/L ND 50.0 10/29/15 17:532.5
Selenium ug/L ND 10.0 10/29/15 17:535.0
Silver ug/L ND 10.0 10/29/15 17:532.5
Thallium ug/L ND 5.5 10/29/15 17:535.0
Vanadium ug/L ND 25.0 10/29/15 17:532.5
Zinc ug/L ND 10.0 10/29/15 17:535.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1593019LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 498500 100 80-120
Arsenic ug/L 472500 94 80-120
Barium ug/L 469500 94 80-120
Beryllium ug/L 472500 94 80-120
Cadmium ug/L 473500 95 80-120
Chromium ug/L 471500 94 80-120
Cobalt ug/L 521500 104 80-120
Copper ug/L 484500 97 80-120
Lead ug/L 472500 94 80-120
Nickel ug/L 471500 94 80-120
Selenium ug/L 462500 92 80-120
Silver ug/L 241250 96 80-120
Thallium ug/L 476500 95 80-120
Vanadium ug/L 494500 99 80-120
Zinc ug/L 488500 98 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1593020MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272955001
1593021
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 107 75-12597 10 25500ND540489
Arsenic ug/L 500 104 75-12594 10 25500ND519470
Barium ug/L 500 102 75-12592 8 25500108618569
Beryllium ug/L 500 105 75-12594 11 25500ND523471
Cadmium ug/L 500 103 75-12593 10 25500ND514465
Chromium ug/L 500 103 75-12593 10 255003.2J 520 470
Cobalt ug/L 500 111 75-125101 9 2550039.3 594 542
Copper ug/L 500 107 75-12595 12 255002.7J 536 476
Lead ug/L 500 100 75-12590 10 255004.2J 504 457
Nickel ug/L 500 100 75-12591 10 255005.9 506 459
Selenium ug/L 500 100 75-12590 10 25500ND499452
Silver ug/L 250 106 75-12595 11 25250ND267239
Thallium ug/L 500 98 75-12590 8 25500ND489452
Vanadium ug/L 500 110 75-12599 10 25500ND550496
Zinc ug/L 500 106 75-12596 10 25500ND530480
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1593032MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272955006
1593033
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12595 1 25500ND482477
Arsenic ug/L 500 93 75-12592 1 25500ND464459
Barium ug/L 500 90 75-12589 1 25500103555548
Beryllium ug/L 500 92 75-12591 1 255000.61J 462 457
Cadmium ug/L 500 92 75-12591 1 25500ND460455
Chromium ug/L 500 91 75-12590 1 25500ND459455
Cobalt ug/L 500 100 75-12599 1 25500ND500495
Copper ug/L 500 93 75-12592 1 25500ND465459
Lead ug/L 500 90 75-12589 1 25500ND452448
Nickel ug/L 500 90 75-12589 1 25500ND453448
Selenium ug/L 500 88 75-12587 1 25500ND442436
Silver ug/L 250 93 75-12592 1 25250ND232230
Thallium ug/L 500 92 75-12590 1 25500ND458452
Vanadium ug/L 500 96 75-12595 1 25500ND483477
Zinc ug/L 500 95 75-12594 1 25500ND480476
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34069
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92272826001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1596018
Associated Lab Samples:92272826001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 10/30/15 23:430.33
1,1,1-Trichloroethane ug/L ND 1.0 10/30/15 23:430.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 10/30/15 23:430.40
1,1,2-Trichloroethane ug/L ND 1.0 10/30/15 23:430.29
1,1-Dichloroethane ug/L ND 5.0 10/30/15 23:430.32
1,1-Dichloroethene ug/L ND 5.0 10/30/15 23:430.56
1,2,3-Trichloropropane ug/L ND 1.0 10/30/15 23:430.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 10/30/15 23:432.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/30/15 23:430.27
1,2-Dichlorobenzene ug/L ND 5.0 10/30/15 23:430.30
1,2-Dichloroethane ug/L ND 1.0 10/30/15 23:430.24
1,2-Dichloropropane ug/L ND 1.0 10/30/15 23:430.27
1,4-Dichlorobenzene ug/L ND 1.0 10/30/15 23:430.33
2-Butanone (MEK)ug/L ND 100 10/30/15 23:430.96
2-Hexanone ug/L ND 50.0 10/30/15 23:430.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 10/30/15 23:430.33
Acetone ug/L ND 100 10/30/15 23:4310.0
Acrylonitrile ug/L ND 200 10/30/15 23:431.9
Benzene ug/L ND 1.0 10/30/15 23:430.25
Bromochloromethane ug/L ND 3.0 10/30/15 23:430.17
Bromodichloromethane ug/L ND 1.0 10/30/15 23:430.18
Bromoform ug/L ND 3.0 10/30/15 23:430.26
Bromomethane ug/L ND 10.0 10/30/15 23:430.29
Carbon disulfide ug/L ND 100 10/30/15 23:431.2
Carbon tetrachloride ug/L ND 1.0 10/30/15 23:430.25
Chlorobenzene ug/L ND 3.0 10/30/15 23:430.23
Chloroethane ug/L ND 10.0 10/30/15 23:430.54
Chloroform ug/L ND 5.0 10/30/15 23:430.14
Chloromethane ug/L ND 1.0 10/30/15 23:430.11
cis-1,2-Dichloroethene ug/L ND 5.0 10/30/15 23:430.19
cis-1,3-Dichloropropene ug/L ND 1.0 10/30/15 23:430.13
Dibromochloromethane ug/L ND 3.0 10/30/15 23:430.21
Dibromomethane ug/L ND 10.0 10/30/15 23:430.21
Ethylbenzene ug/L ND 1.0 10/30/15 23:430.30
Iodomethane ug/L ND 10.0 10/30/15 23:430.32
Methylene Chloride ug/L ND 1.0 10/30/15 23:430.97
Styrene ug/L ND 1.0 10/30/15 23:430.26
Tetrachloroethene ug/L ND 1.0 10/30/15 23:430.46
Toluene ug/L ND 1.0 10/30/15 23:430.26
trans-1,2-Dichloroethene ug/L ND 5.0 10/30/15 23:430.49
trans-1,3-Dichloropropene ug/L ND 1.0 10/30/15 23:430.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1596018
Associated Lab Samples:92272826001
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 10/30/15 23:431.0
Trichloroethene ug/L ND 1.0 10/30/15 23:430.47
Trichlorofluoromethane ug/L ND 1.0 10/30/15 23:430.20
Vinyl acetate ug/L ND 50.0 10/30/15 23:430.35
Vinyl chloride ug/L ND 1.0 10/30/15 23:430.62
Xylene (Total)ug/L ND 5.0 10/30/15 23:430.66
1,2-Dichloroethane-d4 (S)%103 70-130 10/30/15 23:43
4-Bromofluorobenzene (S)%101 70-130 10/30/15 23:43
Toluene-d8 (S)%100 70-130 10/30/15 23:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1596019LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.150 104 80-125
1,1,1-Trichloroethane ug/L 55.250 110 71-129
1,1,2,2-Tetrachloroethane ug/L 52.050 104 79-124
1,1,2-Trichloroethane ug/L 48.750 97 85-125
1,1-Dichloroethane ug/L 53.750 107 73-126
1,1-Dichloroethene ug/L 56.850 114 66-135
1,2,3-Trichloropropane ug/L 50.350 101 75-130
1,2-Dibromo-3-chloropropane ug/L 51.950 104 71-133
1,2-Dibromoethane (EDB)ug/L 52.350 105 83-124
1,2-Dichlorobenzene ug/L 51.950 104 80-133
1,2-Dichloroethane ug/L 46.650 93 67-128
1,2-Dichloropropane ug/L 49.850 100 75-132
1,4-Dichlorobenzene ug/L 51.950 104 78-130
2-Butanone (MEK)ug/L 98.2J100 98 61-144
2-Hexanone ug/L 104100 104 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 93.6J100 94 48-146
Acrylonitrile ug/L 252250 101 40-160
Benzene ug/L 52.950 106 80-125
Bromochloromethane ug/L 53.850 108 71-125
Bromodichloromethane ug/L 54.150 108 78-124
Bromoform ug/L 51.050 102 71-128
Bromomethane ug/L 51.550 103 40-160
Carbon disulfide ug/L 55.0J50 110 50-160
Carbon tetrachloride ug/L 55.750 111 69-131
Chlorobenzene ug/L 51.250 102 81-122
Chloroethane ug/L 51.550 103 39-148
Chloroform ug/L 53.350 107 73-127
Chloromethane ug/L 51.650 103 44-146
cis-1,2-Dichloroethene ug/L 50.850 102 74-124
cis-1,3-Dichloropropene ug/L 51.650 103 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1596019LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 53.750 107 78-125
Dibromomethane ug/L 50.350 101 82-120
Ethylbenzene ug/L 53.050 106 79-121
Iodomethane ug/L 104100 104 39-154
Methylene Chloride ug/L 55.250 110 64-133
Styrene ug/L 52.950 106 84-126
Tetrachloroethene ug/L 53.750 107 78-122
Toluene ug/L 51.450 103 80-121
trans-1,2-Dichloroethene ug/L 53.350 107 71-127
trans-1,3-Dichloropropene ug/L 51.450 103 69-141
trans-1,4-Dichloro-2-butene ug/L 49.8J50 100 40-160
Trichloroethene ug/L 50.050 100 78-122
Trichlorofluoromethane ug/L 55.050 110 53-137
Vinyl acetate ug/L 107100 107 40-160
Vinyl chloride ug/L 60.950 122 58-137
Xylene (Total)ug/L 158150 105 81-126
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1596020MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272855003
1596021
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 100 70-130103 3 3020ND20.0 20.6
1,1,1-Trichloroethane ug/L 20 114 70-130115 1 3020ND22.7 23.1
1,1,2,2-Tetrachloroethane ug/L 20 102 70-130105 2 3020ND20.5 21.0
1,1,2-Trichloroethane ug/L 20 100 70-130102 2 3020ND20.0 20.5
1,1-Dichloroethane ug/L 20 114 70-130114 0 3020ND22.8 22.7
1,1-Dichloroethene ug/L 20 121 70-166124 2 3020ND24.2 24.7
1,2,3-Trichloropropane ug/L 20 98 70-130101 4 3020ND19.5 20.2
1,2-Dibromo-3-
chloropropane
ug/L 20 91 70-130102 12 3020ND18.1 20.4
1,2-Dibromoethane (EDB)ug/L 20 102 70-130105 3 3020ND20.3 21.0
1,2-Dichlorobenzene ug/L 20 101 70-130103 2 3020ND20.1 20.5
1,2-Dichloroethane ug/L 20 94 70-13098 4 3020ND19.1 19.8
1,2-Dichloropropane ug/L 20 105 70-130106 1 3020ND20.9 21.1
1,4-Dichlorobenzene ug/L 20 100 70-130102 2 3020ND20.1 20.5
2-Butanone (MEK)ug/L 40 95 70-130104 10 3040ND37.8J 41.6J
2-Hexanone ug/L 40 97 70-130107 10 3040ND38.6J 42.6J
4-Methyl-2-pentanone(MIBK)ug/L 40 101 70-130107 6 3040ND40.2J 42.9J
Acetone ug/L 40 99 70-130106 7 3040ND42.6J 45.5J
Acrylonitrile ug/L 100 96 70-130104 8 30100ND96.5J 104J
Benzene ug/L 20 108 70-148110 2 3020ND21.6 22.0
Bromochloromethane ug/L 20 112 70-130114 2 3020ND22.5 22.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1596020MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272855003
1596021
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromodichloromethane ug/L 20 105 70-130108 3 3020ND21.0 21.7
Bromoform ug/L 20 89 70-13094 6 3020ND17.8 18.9
Bromomethane ug/L 20 71 70-13088 21 3020ND14.2 17.6
Carbon disulfide ug/L 20 107 70-130114 6 3020ND21.4J 22.8J
Carbon tetrachloride ug/L 20 112 70-130116 4 3020ND22.3 23.3
Chlorobenzene ug/L 20 102 70-146104 2 3020ND20.5 20.9
Chloroethane ug/L 20 113 70-130116 2 3020ND22.6 23.2
Chloroform ug/L 20 111 70-130111 0 3020ND22.1 22.2
Chloromethane ug/L 20 113 70-130118 5 3020ND22.5 23.7
cis-1,2-Dichloroethene ug/L 20 107 70-130108 1 3020ND21.4 21.7
cis-1,3-Dichloropropene ug/L 20 100 70-130100 0 3020ND20.0 20.1
Dibromochloromethane ug/L 20 100 70-130104 4 3020ND19.9 20.8
Dibromomethane ug/L 20 102 70-130105 3 3020ND20.5 21.0
Ethylbenzene ug/L 20 104 70-130107 3 3020ND20.8 21.4
Iodomethane ug/L M1406970-13094 30 3040ND27.6 37.5
Methylene Chloride ug/L 20 117 70-130117 1 3020ND23.5 23.3
Styrene ug/L 20 100 70-130102 2 3020ND20.0 20.4
Tetrachloroethene ug/L 20 104 70-130107 3 3020ND20.8 21.4
Toluene ug/L 20 105 70-155107 2 3020ND21.0 21.3
trans-1,2-Dichloroethene ug/L 20 112 70-130113 1 3020ND22.5 22.6
trans-1,3-Dichloropropene ug/L 20 99 70-130100 1 3020ND19.8 19.9
trans-1,4-Dichloro-2-butene ug/L 20 85 70-13092 8 3020ND17.0J 18.4J
Trichloroethene ug/L 20 103 69-151104 1 3020ND20.5 20.8
Trichlorofluoromethane ug/L 20 119 70-130120 1 3020ND23.7 24.1
Vinyl acetate ug/L 40 88 70-13086 2 3040ND35.1J 34.5J
Vinyl chloride ug/L M12012870-130132 3 3020ND25.6 26.4
1,2-Dichloroethane-d4 (S)%98 70-13098
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41003
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92272826001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1589958
Associated Lab Samples:92272826001
Matrix:Water
AnalyzedMDL
BOD, 5 day ug/L ND 2000 10/27/15 22:492000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1589959LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 198000198000 100 84.6-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92272904001
1589960SAMPLE DUPLICATE:
BOD, 5 day ug/L 75500 B111074.5 mg/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25138
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92272826001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1592556
Associated Lab Samples:92272826001
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 10/29/15 15:271000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1592557LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19100J20000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1592558MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272638001
1592559
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 96 90-110100 3 10200004.0 mg/L 23100J 23900J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25076
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92272826001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1588710
Associated Lab Samples:92272826001
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 10000 10/22/15 09:4310.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1588711LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 2390J2500 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1588712MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272845009
1588713
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L M125005090-11051 0 1025008.6 mg/L 9830J 9830J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/31/2015 03:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25158
EPA 365.1
EPA 365.1
365.1 Phosphorus, Total
Associated Lab Samples:92272826001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1593803
Associated Lab Samples:92272826001
Matrix:Water
AnalyzedMDL
Phosphorus ug/L ND 50.0 10/29/15 12:5925.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1593804LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus ug/L 26002500 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1593805MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272626002
1593806
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 100 90-11099 1 1025000.34 mg/L 2850 2830
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1593808MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92273245001
1593809
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L M125009190-11086 1 1025006.0 mg/L 8220 8110
REPORT OF LABORATORY ANALYSIS
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Page 17 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25072
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92272826001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1588663
Associated Lab Samples:92272826001
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 10/22/15 21:0012500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1588664LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 694000750000 93 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1588665MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272562001
1588666
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M130000008690-11086 0 33000000870 mg/L 3460000 3460000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1588667MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272550001
1588668
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 90 90-11090 0 3750000ND672000672000
REPORT OF LABORATORY ANALYSIS
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Page 18 of 22
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Less than 1.0 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is
calculated for the dilution using the least amount of sample.B1
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.B2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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Page 19 of 22
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92272826
TRANSYLVANIA WOODRUFF LEACHATE
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92272826001 MPRP/19904 ICP/179448807-LMP3 EPA 3010 EPA 6010
92272826001 MSV/340698807-LMP3 EPA 8260
92272826001 WET/41003 WET/410068807-LMP3 SM 5210B SM 5210B
92272826001 WETA/251388807-LMP3 EPA 300.0
92272826001 WETA/250768807-LMP3 EPA 353.2
92272826001 WETA/251588807-LMP3 EPA 365.1
92272826001 WETA/250728807-LMP3 SM 5220D
REPORT OF LABORATORY ANALYSIS
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Page 20 of 22
Page 21 of 22
Page 22 of 22
#=CL#
October 29, 2015
LIMS USE: FR - ALEX EVERHART
LIMS OBJECT ID: 92272816
92272816
Project:
Pace Project No.:
RE:
Mr. Alex Everhart
Joyce Engineering-NC
2211 W. Meadowview Road
Suite 101
Greensboro, NC 27407
TRANSYLVANIA WOODRUFF STORM WA
Dear Mr. Everhart:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
cc:Mr. Van Burbach, Joyce Engineering-NC
Alex Everhart, Joyce Engineering-NC
REPORT OF LABORATORY ANALYSIS
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Page 1 of 14
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
Asheville Certification IDs2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
West Virginia Certification #: 356Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 14
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
Lab ID Sample ID Matrix Date Collected Date Received
92272816001 8807-STORM WATER 1 Water 10/21/15 12:15 10/21/15 14:45
92272816002 8807-STORM WATER 2 Water 10/21/15 12:25 10/21/15 14:45
92272816003 8807-STORM WATER 3 Water 10/21/15 12:35 10/21/15 14:45
REPORT OF LABORATORY ANALYSIS
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Page 3 of 14
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92272816001 8807-STORM WATER 1 SM 9222D 1 PASI-AMLS
SM 5220D 1 PASI-AWRC
92272816002 8807-STORM WATER 2 SM 9222D 1 PASI-AMLS
SM 5220D 1 PASI-AWRC
92272816003 8807-STORM WATER 3 SM 9222D 1 PASI-AMLS
SM 5220D 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
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Page 4 of 14
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92272816001 8807-STORM WATER 1
Fecal Coliforms 66.0 CFU/100 mL 10/21/15 17:101.0SM 9222D
92272816002 8807-STORM WATER 2
Fecal Coliforms 5.0 CFU/100 mL 10/21/15 17:10 u11.0SM 9222D
92272816003 8807-STORM WATER 3
Fecal Coliforms 9.0 CFU/100 mL 10/21/15 17:10 u11.0SM 9222D
REPORT OF LABORATORY ANALYSIS
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Page 5 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
Sample:8807-STORM WATER 1 Lab ID:92272816001 Collected:10/21/15 12:15 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 9222DMBIO 9222D Fecal Coliform AVL
Fecal Coliforms 66.0 CFU/100 mL 10/21/15 17:101.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 10/22/15 21:0025000125001
REPORT OF LABORATORY ANALYSIS
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Page 6 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
Sample:8807-STORM WATER 2 Lab ID:92272816002 Collected:10/21/15 12:25 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 9222DMBIO 9222D Fecal Coliform AVL
Fecal Coliforms 5.0 CFU/100 mL 10/21/15 17:10 u11.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 10/22/15 21:0025000125001
REPORT OF LABORATORY ANALYSIS
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Page 7 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
Sample:8807-STORM WATER 3 Lab ID:92272816003 Collected:10/21/15 12:35 Received:10/21/15 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 9222DMBIO 9222D Fecal Coliform AVL
Fecal Coliforms 9.0 CFU/100 mL 10/21/15 17:10 u11.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 10/22/15 21:0025000125001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 06:42 PM
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Page 8 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/40995
SM 9222D
SM 9222D
9222D MBIO Fecal Coliform - AVL
Associated Lab Samples:92272816001, 92272816002, 92272816003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1589564
Associated Lab Samples:92272816001, 92272816002, 92272816003
Matrix:Water
AnalyzedMDL
Fecal Coliforms CFU/100 mL 0.0J 1.0 10/21/15 17:10
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92272742001
1589565SAMPLE DUPLICATE:
Fecal Coliforms CFU/100 mL 27.0 u1122524.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 06:42 PM
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Page 9 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25072
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92272816001, 92272816002, 92272816003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1588663
Associated Lab Samples:92272816001, 92272816002, 92272816003
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 10/22/15 21:0012500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1588664LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 694000750000 93 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1588665MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272562001
1588666
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M130000008690-11086 0 33000000870 mg/L 3460000 3460000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1588667MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92272550001
1588668
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 90 90-11090 0 3750000ND672000672000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 06:42 PM
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Huntersville, NC 28078
[phone]
Page 10 of 14
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Results based upon colony counts outside acceptable range.u1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 06:42 PM
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[phone]
Page 11 of 14
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92272816
TRANSYLVANIA WOODRUFF STORM WA
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92272816001 WET/409958807-STORM WATER 1 SM 9222D
92272816002 WET/409958807-STORM WATER 2 SM 9222D
92272816003 WET/409958807-STORM WATER 3 SM 9222D
92272816001 WETA/250728807-STORM WATER 1 SM 5220D
92272816002 WETA/250728807-STORM WATER 2 SM 5220D
92272816003 WETA/250728807-STORM WATER 3 SM 5220D
REPORT OF LABORATORY ANALYSIS
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Page 12 of 14
Page 13 of 14
Page 14 of 14

Appendix 2
Summary of Detections

Summary of Detections
WELL ID PARAMETER RESULT UNITS SWSL COLLECT DATE
8807-MW1 Beryllium 2.5 µg/L 1 10/20/2015
8807-MW3 Beryllium 2.1 µg/L 1 10/20/2015
8807-MW8 Lead 18.3 µg/L 10 10/20/2015
8807-MW9SR Beryllium 1.2 µg/L 1 10/21/2015
8807-MW9SR Lead 17.3 µg/L 10 10/21/2015
Notes:µg/L = Micorgrams per liter
SWSL = NC Soild Waste Section Reporting Limit
Laboratory Reporting limit used when SWSL has not been established
Transylvania Co. Woodruff Landfill
Permit No. 88-07 Page 1 of 1 Joyce Engineering

Appendix 3
Summary of Field Parameters

Summary of Field Parameters
WELL ID PARAMETER RESULT UNITS COLLECT DATE
8807-MW1 pH 5.13 S.U.10/20/2015
8807-MW1 Temperature 16.8 ºC 10/20/2015
8807-MW1 Conductivity 109 µS 10/20/2015
8807-MW1 Turbidity 11.39 NTU 10/20/2015
8807-MW1 Static Water Level 19.10 ft 10/20/2015
8807-MW1 Well Depth 32.66 ft 10/20/2015
8807-MW2 pH 5.65 S.U.10/20/2015
8807-MW2 Temperature 18.6 ºC 10/20/2015
8807-MW2 Conductivity 201 µS 10/20/2015
8807-MW2 Turbidity 17.96 NTU 10/20/2015
8807-MW2 Static Water Level 15.85 ft 10/20/2015
8807-MW2 Well Depth 26.45 ft 10/20/2015
8807-MW3 pH 4.19 S.U.10/20/2015
8807-MW3 Temperature 11.6 ºC 10/20/2015
8807-MW3 Conductivity 28 µS 10/20/2015
8807-MW3 Turbidity 17.6 NTU 10/20/2015
8807-MW3 Static Water Level 31.6 ft 10/20/2015
8807-MW3 Well Depth 43.32 ft 10/20/2015
8807-MW5 pH 5.38 S.U.10/20/2015
8807-MW5 Temperature 14.0 ºC 10/20/2015
8807-MW5 Conductivity 39 µS 10/20/2015
8807-MW5 Turbidity 8.59 NTU 10/20/2015
8807-MW5 Static Water Level 10.45 ft 10/20/2015
8807-MW5 Well Depth 35.15 ft 10/20/2015
8807-MW8 pH 5.66 S.U.10/20/2015
8807-MW8 Temperature 13.8 ºC 10/20/2015
8807-MW8 Turbidity 11.77 NTU 10/20/2015
8807-MW8 Conductivity 137 µS 10/20/2015
8807-MW8 Static Water Level 28.45 ft 10/20/2015
8807-MW8 Well Depth 34.45 ft 10/20/2015
8807-MW9SR pH 4.39 S.U.10/21/2015
8807-MW9SR Temperature 13.4 ºC 10/21/2015
8807-MW9SR Conductivity 172 µS 10/21/2015
8807-MW9SR Turbidity 91.7 NTU 10/21/2015
8807-MW9SR Static Water Level 29.15 ft 10/21/2015
8807-MW9SR Well Depth 43.10 ft 10/21/2015
8807-MW9D pH 5.33 S.U.10/21/2015
8807-MW9D Temperature 14.1 ºC 10/21/2015
8807-MW9D Conductivity 189 µS 10/21/2015
8807-MW9D Turbidity 10.2 NTU 10/21/2015
8807-MW9D Static Water Level 29.1 ft 10/21/2015
8807-MW9D Well Depth 86.50 ft 10/21/2015
8807-MW10 pH 5.84 S.U.10/21/2015
8807-MW10 Temperature 12.2 ºC 10/21/2015
8807-MW10 Conductivity 36 µS 10/21/2015
8807-MW10 Turbidity 13.5 NTU 10/21/2015
8807-MW10 Static Water Level 32.2 ft 10/21/2015
8807-MW10 Well Depth 38.00 ft 10/21/2015
Transylvania County Woodruff Landfill
Permit No. 88-07 Page 1 of 2 Joyce Engineering
Summary of Field Parameters
WELL ID PARAMETER RESULT UNITS COLLECT DATE
8807-MW11 pH 5.56 S.U.10/20/2015
8807-MW11 Temperature 14.9 ºC 10/20/2015
8807-MW11 Conductivity 32 µS 10/20/2015
8807-MW11 Turbidity 5.79 NTU 10/20/2015
8807-MW11 Static Water Level 21.85 ft 10/20/2015
8807-MW11 Well Depth 26.90 ft 10/20/2015
8807-MW12D pH 5.41 S.U.10/20/2015
8807-MW12D Temperature 13.2 ºC 10/20/2015
8807-MW12D Conductivity 90 µS 10/20/2015
8807-MW12D Turbidity 26.5 NTU 10/20/2015
8807-MW12D Static Water Level 30.65 ft 10/20/2015
8807-MW12D Well Depth 53.44 ft 10/20/2015
8807-MW12S pH 4.36 S.U.10/21/2015
8807-MW12S Temperature 11.2 ºC 10/21/2015
8807-MW12S Conductivity 109 µS 10/21/2015
8807-MW12S Turbidity 41.2 NTU 10/21/2015
8807-MW12S Static Water Level 28.45 ft 10/21/2015
8807-MW12S Well Depth 32.50 ft 10/21/2015
8807-MW13 pH 5.63 S.U.10/20/2015
8807-MW13 Temperature 12.8 ºC 10/20/2015
8807-MW13 Conductivity 43 µS 10/20/2015
8807-MW13 Turbidity 13.76 NTU 10/20/2015
8807-MW13 Static Water Level 38.95 ft 10/20/2015
8807-MW13 Well Depth 48.41 ft 10/20/2015
Notes:ºC= degrees Centigrade
S.U.= Standard Units
µS = microsemens
NTU = Nephelometric Turbidity Units
ft = feet
Transylvania County Woodruff Landfill
Permit No. 88-07 Page 2 of 2 Joyce Engineering

Appendix 4
Summary of Monitoring Well Construction
Summary of Monitoring Well Construction
CASING GROUND
DIAMETER SURFACE DEPTH ELEV. DEPTH ELEV.
inches feet B.G.S.feet M.S.L.feet B.G.S.feet M.S.L.from to from to
MW-1 04/16/91 2 2702.83 2705.74 29.75 2673.08 na na 14.5 29.5 2688.33 2673.33 na
MW-2 04/16/91 2 2675.43 2676.85 24 2651.43 na na 8.7 23.7 2666.73 2651.73 na
MW-3 04/16/91 2 2752.14 2754.44 40.25 2711.89 na na 25 40 2727.14 2712.14 na
MW-5 04/17/91 2 2641.46 2644.23 32.25 2609.21 na na 17 32 2624.46 2609.46 na
MW-6 09/19/94 2 2663.26 2665.26 22 2641.26 8 2655.26 6 21 2657.26 2642.26 PWR/Bedrock
MW-8 09/20/94 2 2672.13 2674.19 32.5 2639.63 20.5 2651.63 16.5 31.5 2655.63 2640.63 PWR/Bedrock
MW-9SR 09/26/11 2 2670.55 2674.40 43.1 2627.45 32.85 2637.70 23.1 43.1 2647.45 2627.45 PWR/Bedrock
MW-9D 01/09/01 2 2670.12 2672.82 83.8 2586.32 32.85 2637.27 73.8 83.8 2596.32 2586.32 Bedrock
MW-10 11/13/06 2 2768.51 2771.01 38 2730.51 20 2748.51 28 38 2740.51 2730.51 Bedrock
MW-11 11/09/06 2 2677.45 2679.95 24 2653.45 4 2673.45 14 24 2663.45 2653.45 PWR/Bedrock
MW-12S 11/21/06 2 2674.45 2676.95 31 2643.45 31 2643.45 16 31 2658.45 2643.45 Saprolite/Fill
MW-12D 11/21/06 2 2674.54 2677.04 50 2624.54 33 2641.54 40 50 2634.54 2624.54 Bedrock
MW-13 11/20/06 2 2677.07 2679.57 35 2642.07 18 2659.07 25 35 2652.07 2642.07 Bedrock
NOTES:
1. All elevations are referenced to mean sea level (M.S.L.); depths are referenced to ground surface (G.S.).
2. All wells were constructed using 2-inch (inside diameter) casing.
3. na = not available.
4. B.G.S. = below ground surface.
5. T.O.C. = top of casing.
7. Well construction information for MW-1 through MW-8 taken from GAI's Design Hydrogeologic Study for Phase 3 (March 1995).
Well construction information for MW-9S & -9D and P-15 through P-16 taken from JEI's Design Hydrogeologic Study for Phase 4 (April 2001).
6. PWR = partially weathered rock
LITHOLOGY OF
SCREENED INTERVALT.O.C.
WELL ELEVATIONS
feet above M.S.L.
TOP OF BEDROCK
DEPTH B.G.S.
TOTAL DEPTH
DRILLED SCREENED INTERVAL
ELEVATION (feet M.S.L.)
SCREENED INTERVAL
WELL
NUMBER
DATE
INSTALLED
Transylvania Co. Woodruff Landfill
Permit No. 88-07 Page 1 of 1 Joyce Engineering