6004_DukeMcGuireLF1_SubsurfaceInvestigation_DIN26527_20160720

Groundwater Sampling Report
Duke Energy's McGuire Nuclear
Station No. 1 Landfill
Huntersville, North Carolina
S&ME Project No. 4226-16-060
Prepared for:
Duke Energy Carolinas, LLC
526 South Church Street, Mail Code EC13K
Charlotte, North Carolina 28202
Prepared by:
S&ME, Inc.
301 Zima Park Road
Spartanburg, South Carolina 29301
June 23, 2016
S&ME, Inc. | 301 Zima Park Road | Spartanburg, South Carolina 29301 | p 864.574.2360 | f 864.576.8730 | www.smeinc.com
June 23, 2016
Duke Energy Carolinas, LLC
526 South Church Street
Maile Code EC13K
Charlotte, North Carolina 28202
Attention:Ms. Tyler Hardin
[e-mail]
Reference:Groundwater Sampling Report
Duke Energy's McGuire Nuclear Station No. 1 Landfill
Huntersville, North Carolina
S&ME Project No. 4226-16-060
Dear Ms. Hardin:
S&ME has completed the groundwater sampling activities described in our proposal number 42-1600350,
dated March 17, 2016, and the results are presented herein.
We appreciate each and every opportunity to be of service to you and to Duke Energy. Please do not
hesitate to contact us if you have any questions.
Sincerely,
S&ME, Inc.
Richard Bonds John Whitehead
Project Professional Senior Professional
[e-mail] [e-mail]
cc: Mr. John Williamson, McGuire Nuclear Station
t:\projects\2016\env\4226-16-060 mcguire nuclear station number one landfill\groundwater sampling report.docx
Groundwater Sampling Report
Duke Energy's McGuire Nuclear Station No. 1 Landfill
Huntersville, North Carolina
S&ME Project No. 4226-16-060
June 23, 2016 ii
Table of Contents
1.0 Project Information...............................................................................................1
2.0 Regulatory Approval ............................................................................................1
3.0 Direct Push Borings ..............................................................................................1
4.0 Groundwater Sample Collection and Analysis...............................................1
5.0 Groundwater Sample Laboratory Results........................................................2
6.0 Conclusions ............................................................................................................3
Appendices
Appendix I – Figures
Appendix II – Tables
Appendix III – Mecklenburg County Subsurface Investigation Permit
Appendix IV – Boring Logs
Appendix V – Analytical Laboratory Report
Groundwater Sampling Report
Duke Energy's McGuire Nuclear Station No. 1 Landfill
Huntersville, North Carolina
S&ME Project No. 4226-16-060
June 23, 2016 1
1.0 Project Information
Duke Energy conducts routine groundwater monitoring in proximity to the closed No. 1 Landfill (unlined)
at the McGuire Nuclear Station. The approximate location of the No. 1 Landfill (unlined) is shown on
Figure 1 in Appendix I. Recent sampling results have shown an increase in concentrations of select
volatile organic compounds in several down gradient monitoring wells (MW-4/4D and MW-4R/4DR).
Duke Energy requested S&ME to prepare a proposal to assess the groundwater near the above
referenced well via direct push borings and groundwater sample collection and analysis. Our proposal
(No. 42-1600350) was submitted on March 17, 2016.
Presented below are the tasks we undertook and the results from the groundwater sampling.
2.0 Regulatory Approval
Prior to mobilizing to the site, the Mecklenburg County Health Department Groundwater & Wastewater
Services was notified of our intent to advance direct push borings and collect groundwater samples in
proximity to the No. 1 Landfill (unlined). Permit Number 70002341 was issued on May 3, 2016. A copy of
the permit is included in Appendix III.
3.0 Direct Push Borings
Beginning on May 18, 2016, S&ME and our drilling subcontractor, SAEDACCO were on-site to advance the
direct push borings. Boring depths ranged from 40 feet at DP-12 to 80 feet at DP-4,-5, and -6. Following
completion of each boring, horizontal coordinates of the borings were collected using a hand held GPS
unit. These coordinates were converted to North Carolina State Plane coordinates and used to locate the
borings on a scaled site plan –Figure 2. The boring coordinates (NC State Plane and latitude/longitude)
are included in Table 1 in Appendix II.
Continuous soils samples were collected at DP-1, DP-11, DP-17, and DP-25 for the purpose of describing
the lithological characteristics of the soils near the landfill. Lithological information for the remaining
direct push borings was interpolated from these four locations. Boring logs for each of the borings are
included in Appendix IV.
To minimize the risk of possible cross contamination between boring locations, down-hole direct push
equipment was rinsed with high pressure hot water. The rinse water was collected into a labeled 55-
gallon drum and staged at the landfill for later disposal. The results from the groundwater sample
analyses are considered representative of the drummed water and will be used to manifest the rinse water
off site for disposal. Documentation of the disposal will be submitted under separate cover.
4.0 Groundwater Sample Collection and Analysis
At the termination depth of each boring, the direct push rods were pulled back toward the ground surface
to deploy and expose the groundwater sample screen at the bottom of the direct push rod string. The
Groundwater Sampling Report
Duke Energy's McGuire Nuclear Station No. 1 Landfill
Huntersville, North Carolina
S&ME Project No. 4226-16-060
June 23, 2016 2
stainless steel screen section is four feet long. At three locations (DP-1, DP-17, and DP-18), the direct
push rods were removed and one-inch PVC screen and casing was installed. This procedure was used at
these locations due to the slowness of the groundwater to enter the boring. Groundwater was not
encountered within the boring depth of DP-13, so a sample was not collected. Groundwater sampling
details from the borings are also included on the boring logs in Appendix IV.
The groundwater samples were collected by using new disposable polyethylene tubing equipped with a
check value to bring the groundwater to the surface, where the water was decanted directly from the
tubing into laboratory supplied 40 milliliter vials. The vials were labeled with the sample identification,
date and time. The samples were stored on ice and relinquished to Duke Energy’s laboratory near the
McGuire Nuclear Station. Duke Energy relinquished the samples to Pace Analytical for analysis of volatile
organic compounds (VOCs) by Method 8260.
Following collection of the groundwater samples, each boring was abandoned by a North Carolina
certified well driller in general accordance with the North Carolina Well Construction Standards, NCAC
Title 15A Subchapter 2C Section .0100 and the Mecklenburg County Groundwater Regulations, Chapter VI
– Section VI. The borings were abandoned by pumping a mixture of Portland cement and powdered
bentonite through a tremie pipe and filling the boring from the bottom to the ground surface.
Documentation of the abandonment will be submitted to Mecklenburg County under separate cover.
5.0 Groundwater Sample Laboratory Results
The results of the groundwater sample analyses are summarized in Table 2, and copies of the laboratory
reports are included in Appendix V.
Volatile organic compounds were not detected above laboratory reporting detection limits (RDLs) at 20
(DP-1, DP-7, DP-9, DP-10, DP-11, DP-12, DP-14, DP-16, DP-17, DP-18, DP-19, DP-20, DP-21, DP-22, DP-
23, DP-24, DP-25, DP-26, DP-27, and DP-28) of the 27 sampled locations. One VOC, toluene, was
reported just above the RDL at DP-15; however, comments provided by the Pace Analytical Laboratory
indicated the sample may be biased high for toluene due to carryover from a previous sample. In
addition, Pace reported that the sample from DP-15 contained excess suspended soil particles, which
limited the volume of groundwater available for analysis.
Detected VOCs included 2-butanone (one time), benzene (one time), cis-1,2-dichloroethene (six times),
m&p-xylene (one time), methylene chloride (four times), o-xylene (six times), toluene (two times), and
trichloroethene (three times). Total xylenes (six times) were also reported but are a combination of the
m&p-xylene and o-xylene concentrations.
The reported VOC concentrations were compared to North Carolina 2L Groundwater Standards, 15A
NCAC 2L .0200 (April 2013), and to North Carolina Department of Environmental Quality (NCDEQ) Solid
Waste Section Limits (SWSLs). These criteria are also included in Table 2. From this comparison, three
compounds (benzene [one detection], methylene chloride [three of four detections], and trichloroethene
[one of three detections]) were detected at concentrations that exceed both the 2L Standards and SWSLs.
Cis-1,2-dichloroethene [six of six detections] was detected above the SWSL but not above the 2L
standard. Methylene chloride was also detected one time at a concentration that exceeded the SWSL but
not the 2L Standard. Each toluene detection (twice) also exceeded the SWSL but not the 2L Standard. As
Groundwater Sampling Report
Duke Energy's McGuire Nuclear Station No. 1 Landfill
Huntersville, North Carolina
S&ME Project No. 4226-16-060
June 23, 2016 3
mentioned previously, the toluene detection at DP-15 may be carryover from a preceding sample.
Trichloroethene was detected two out of three times at concentrations that exceed the SWSL but not the
2L Standard. Each total xylene concentration (six) exceeds the SWSL but not the 2L Standard.
6.0 Conclusions
Based on the laboratory results, it appears that groundwater impact is limited to the area along the landfill
boundary near monitoring wells MW-4 and MW-4D as indicated by results from DP-2, DP-3, DP-4, DP-5,
DP-6 and DP-8. Previous groundwater reports provided by Duke Energy have indicated detectable
concentrations of VOCs at MW-4R/MW-4DR, which is located at or near the Landfill Review Boundary.
However, during this assessment, no VOCs were detected in groundwater samples other than those listed
above between the landfill boundary, the Landfill Review Boundary, and the Landfill Compliance
Boundary.
VOCs are present in six of the 27 groundwater samples from this assessment in concentrations that
exceed one or both of the screening criteria used (2L Groundwater Standards and NCDEQ’s SWSLs). With
the exception of tetrachloroethene, the detected compounds from this assessment are also similar to
those detected in previous groundwater sampling events for the No. 1 Landfill (unlined).
Tetrachloroethene has been detected during prior sampling events of the monitoring wells but was not
detected in any of the 27 groundwater samples collected during this assessment.
Appendices
Appendix I – Figures
Figure 1 – Site Topographic Map
Figure 2 – Direct Push Boring Locations
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Appendix II – Tables
Table 1 – Summary of Direct Push Boring Coordinates and Water Levels
Table 2 – Summary of Laboratory Analysis
Boring ID Northing Easting Latitude Longitude Depth to Water
DP-1 611283.78 1418838.88 35° 24' 48" N 80° 57' 05" W 63
DP-2 611213.13 1418786.13 35° 24' 45" N 80° 57' 04" W 63
DP-3 611160.96 1418737.23 35° 24' 49" N 80° 57' 05" W 64
DP-4 611057.31 1418675.27 35° 24' 49" N 80° 57' 06" W 63
DP-5 611012.06 1418676.95 35° 24' 49" N 80° 57' 06" W 62
DP-6 610961.13 1418678.15 35° 24' 50" N 80° 57' 05" W 60
DP-7 610914.83 1418687.56 35° 24' 50" N 80° 57' 05" W 55
DP-8 610863.95 1418699.64 35° 24' 50" N 80° 57' 04" W 50
DP-9 610810.84 1418698.77 35° 24' 51" N 80° 57' 04" W 45
DP-10 610750.60 1418711.43 35° 24' 47" N 80° 57' 05" W 41
DP-11 610690.63 1418698.47 35° 24' 47" N 80° 57' 05" W 30
DP-12 610652.76 1418666.71 35° 24' 50" N 80° 57' 02" W 30
DP-13 611240.18 1418810.62 35° 24' 49" N 80° 57' 03" W Dry
DP-14 611315.67 1418802.30 35° 24' 49" N 80° 57' 04" W 55
DP-15 611275.86 1418762.74 35° 24' 49" N 80° 57' 04" W 57
DP-16 611230.62 1418726.39 35° 24' 47" N 80° 57' 04" W 54
DP-17 611042.68 1418582.52 35° 24' 47" N 80° 57' 04" W 39
DP-18 610995.14 1418591.13 35° 24' 46" N 80° 57' 04" W 43
DP-19 610929.82 1418595.86 35° 24' 46" N 80° 57' 04" W 39
DP-20 611208.56 1418689.68 35° 24' 45" N 80° 57' 04" W 52
DP-21 611188.08 1418639.35 35° 24' 44" N 80° 57' 04" W 40
DP-22 611151.81 1418602.51 35° 24' 44" N 80° 57' 04" W 45
DP-23 611159.21 1418514.20 35° 24' 50" N 80° 57' 03" W 42
DP-24 611201.27 1418549.73 35° 24' 50" N 80° 57' 03" W 41
DP-25 611231.37 1418593.49 35° 24' 50" N 80° 57' 03" W 40
DP-26 611273.94 1418629.97 35° 24' 49" N 80° 57' 04" W 46
DP-27 611316.24 1418680.22 35° 24' 49" N 80° 57' 04" W 52
DP-28 611370.64 1418720.28 35° 24' 49" N 80° 57' 05" W 44
Table 1
Summary of Direct Push Boring Coordinates and Water Levels
McGuire Nuclear Station No. 1 Landfill
Huntersville, North Carolina
S&ME Project Number 4226-16-060
2L Standard SWSL DP-1 DP-2 DP-3 DP-4 DP-5 DP-6 DP-7 DP-8 DP-9 DP-10 DP-11 DP-12 DP-13 DP-14 DP-15 DP-16 DP-17 DP-18 DP-19 DP-20 DP-21 DP-22 DP-23 DP-24 DP-25 DP-26 DP-27 DP-28
Compound CAS Number ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
1,1,1,2-Tetrachloroethane 630-20-6 NE 5 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
1,1,1-Trichloroethane 71-55-6 200 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
1,1,2,2-Tetrachloroethane 79-34-5 0.2 3 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
1,1,2-Trichloroethane 79-00-5 NE 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
1,1-Dichloroethane 75-34-3 6 5 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
1,1-Dichloroethene 75-35-4 350 5 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
1,2,3-Trichloropropane 96-18-4 0.005 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
1,2-Dibromo-3-chloropropane 96-12-8 0.04 13 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 NS < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2
1,2-Dibromoethane (EDB)106-93-4 0.02 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
1,2-Dichlorobenzene 95-50-1 20 5 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
1,2-Dichloroethane 107-06-2 0.4 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
1,2-Dichloropropane 78-87-5 0.6 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS NA NA NA < 1 < 1 < 1 NA NA NA NA NA NA NA NA NA
1,4-Dichlorobenzene 106-46-7 6 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
2-Butanone (MEK)78-93-3 4000 100 < 5 < 5 < 5 < 5 < 5 5.2 < 5 < 5 < 5 < 5 < 5 < 5 NS < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5
2-Hexanone 591-78-6 NE 50 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 NS < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5
4-Methyl-2-pentanone (MIBK)108-10-1 NE 100 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 NS < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5
Acetone 67-64-1 6000 100 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 NS < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25 < 25
Acrylonitrile 107-13-1 NE 200 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 NS < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10
Benzene 71-43-2 1 1 < 1 < 1 < 1 < 1 < 1 3.6 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Bromochloromethane 74-97-5 NE 3 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Bromodichloromethane 75-27-4 0.6 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Bromoform 75-25-2 4 3 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Bromomethane 74-83-9 NE 10 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 NS < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2
Carbon disulfide 75-15-0 700 100 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 NS < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2
Carbon tetrachloride 56-23-5 0.3 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Chlorobenzene 108-90-7 50 3 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Chloroethane 75-00-3 3000 10 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Chloroform 67-66-3 70 5 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Chloromethane 74-87-3 3 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
cis-1,2-Dichloroethene 156-59-2 70 5 < 1 45.3 19.7 23.8 8.4 54.3 < 1 13.1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
cis-1,3-Dichloropropene 10061-01-5 0.4 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS NA NA NA < 1 < 1 < 1 NA NA NA NA NA NA NA NA NA
Dibromochloromethane 124-48-1 0.4 3 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Dibromomethane 74-95-3 NE 10 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Ethylbenzene 100-41-4 600 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Iodomethane 74-88-4 NE 10 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 NS < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5
m&p-Xylene 179601-23-1 NL NL < 2 < 2 6.7 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 NS < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2
Methylene Chloride 75-09-2 5 1 < 2 9 7.7 11.5 < 2 4.9 < 2 < 2 < 2 < 2 < 2 < 2 NS < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2
o-Xylene 95-47-6 NE NE < 1 9.4 20.4 18.1 10.6 53.5 < 1 17.5 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Styrene 100-42-5 70 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Tetrachloroethene 127-18-4 0.7 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Toluene 108-88-3 600 1 < 1 < 1 < 1 < 1 < 1 1.2 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 1.7*< 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
trans-1,2-Dichloroethene 156-60-5 100 5 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
trans-1,3-Dichloropropene 10061-02-6 0.4 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS NA NA NA < 1 < 1 < 1 NA NA NA NA NA NA NA NA NA
trans-1,4-Dichloro-2-butene 110-57-6 NE 100 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Trichloroethene 79-01-6 3 1 < 1 2.3 3.3 1.6 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Trichlorofluoromethane 75-69-4 2000 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Vinyl acetate 108-05-4 NE 50 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 NS < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2
Vinyl chloride 75-01-4 0.03 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 NS < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1
Xylene (Total)1330-20-7 500 5 < 2 9.4 27.1 18.1 10.6 53.5 < 2 17.5 < 2 < 2 < 2 < 2 NS < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2
Notes:
ug/l = micrograms per liter
2L Standards as specified in 15A NCAC 2L .0200 - April 1, 2013
SWSL = NC DEQ Solid Waste Section Limits - June 13, 2011
NA = Not analyzed in these samples
NS = Not sampled due to absence of groundwater.
Bold value indicates a concentration above the laboratory detection limit.
Concentration exceeds the SWSL limit.
Concentration exceeds the 2L and SWSL limits.
* Laboratory data qualifier indicates sample is biased high for this compound.
Sample ID
Table 2
Summary of Laboratory Analysis
McGuire Nuclear Station No. 1 Landfill
Huntersville, North Carolina
S&ME Project Number 4226-16-060
Appendix III – Mecklenburg County Subsurface Investigation
Permit
SIP Form – revised 2/15/11
Mecklenburg County Health Department Groundwater & Wastewater Services 700 N. Tryon St., Suite 211 Charlotte, NC 28202
Phone: [phone] Fax: [phone] http://groundwater.charmeck.org
Permit Issuance Date: _______________
Permit Number: ____________________ 
SUBSURFACE INVESTIGATION PERMIT
I. Well Owner Information
Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
II. Agent Information (if applicable)

Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
III. Site Information

Site Name; ________________________________
Parcel ID Number: _____________________
Address: ________________________________
City: __________________________ State: _______ Zip: _____________

General Conditions of This Permit:
• This permit shall be VALID for a period not to exceed twelve (12) months from the date of issuance.
• This permit is VALID for the site specified aboveDQGmust be on-site during the course of the investigation
and made available to a Department representative upon request.
• A North Carolina Certified Well Contrator must perform any well contractor activities associated with this permit.
• All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VIof the Mecklenburg County Groundwater Well Regulations.
• All temporary wells, including those installed using Direct Push Technology, must be abandoned
to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations.
• Registration information for all wells must be submitted to the Department within thirty (30) days of well completion. If water samples are collected, it is recommended that the well NOT be registered until the
analytical results are received.

Owner
5/3/2016
70002341
Duke Energy
John Williamson
980.875.5894
12700 Hagers Ferry Road
Mailcode: MG01EM
Huntersville NC 28078
S&ME
John Whitehead
864.574.2360
301 Zima Park ROad
Spartanburg SC 29301
McGuire Nuclear Station
01315102
12700 HAGERS FERRY RD 7422
HUNTERSVILLE NC 28078
Appendix IV – Boring Logs
Leaves and Topsoil
Red Brown Clayey fine
Sandy Silt
Orange Purple TanSilty fine Sand
White Gray Silty fine
Sand
Boring Terminated at
68 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchPVC57 to 67 feet bls
Portland Cement and Powdered Bontonitegs to 67 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/19/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-1
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 48" N
80° 57' 05" W
611283.7796
1418838.875
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
One InchPVCgs to to 57 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
63 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
COMPLETION REPORT OF
WELL No. DP-1864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-1.Red Brown Clayey fineSandy Silt
Orange Purple TanSilty fine Sand
White Gray Silty fine
Sand
Boring Terminated at74 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel70 to 74 feet bls
Portland Cement and Powdered Bontonitegs to 74 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/20/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-2
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 45" N
80° 57' 04" W
611213.1331
1418786.129
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 70 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
63 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
COMPLETION REPORT OF
WELL No. DP-2864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-1.Red Brown Clayey fineSandy Silt
Orange Purple Tan
Silty fine Sand
White Gray Silty fineSand
Boring Terminated at
75 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel71 to 75 feet bls
Portland Cement and Powdered Bontonitegs to 75 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/20/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-3
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 49" N
80° 57' 05" W
611160.9642
1418737.232
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 71 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
64 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
75
COMPLETION REPORT OF
WELL No. DP-3864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-17.Red Brown ClayeySilty fine to medium
Sand
Tan Silty fine Sand
White Gray Silty fine tomedium Sand
Orange Tan fine
Sandy Silt
Boring Terminated at80 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel76 to 80 feet bls
Portland Cement and Powdered Bontonitegs to 80 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/20/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-4
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 49" N
80° 57' 06" W
611057.3089
1418675.274
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 76 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
63 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
75
80
COMPLETION REPORT OF
WELL No. DP-4864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-17.Red Brown ClayeySilty fine to medium
Sand
Tan Silty fine Sand
White Gray Silty fine tomedium Sand
Orange Tan fine
Sandy Silt
Boring Terminated at80 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel76 to 80 feet bls
Portland Cement and Powdered Bontonitegs to 80 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/20/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-5
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 49" N
80° 57' 06" W
611012.0564
1418676.948
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 76 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
62 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
75
80
COMPLETION REPORT OF
WELL No. DP-5864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-17.Red Brown ClayeySilty fine to medium
Sand
Tan Silty fine Sand
White Gray Silty fine tomedium Sand
Orange Tan fine
Sandy Silt
Boring Terminated at80 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel76 to 80 feet bls
Portland Cement and Powdered Bontonitegs to 80 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/23/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-6
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 50" N
80° 57' 05" W
610961.1284
1418678.15
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 76 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
60 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
75
80
COMPLETION REPORT OF
WELL No. DP-6864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-17.Red Brown ClayeySilty fine to medium
Sand
Tan Silty fine Sand
White Gray Silty fine tomedium Sand
Orange Tan fineSandy Silt
Boring Terminated at70 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel66 to 70 feet bls
Portland Cement and Powdered Bontonitegs to 70 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/23/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-7
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 50" N
80° 57' 05" W
610914.8261
1418687.557
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 66 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
55 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
COMPLETION REPORT OF
WELL No. DP-7864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-17.Red Brown ClayeySilty fine to medium
Sand
Tan Silty fine Sand
White Gray Silty fine tomedium Sand
Orange Tan fineSandy Silt
Boring Terminated at
70 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel66 to 70 feet bls
Portland Cement and Powdered Bontonitegs to 70 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/23/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-8
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 50" N
80° 57' 04" W
610863.9535
1418699.639
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 66 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
50 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
75
COMPLETION REPORT OF
WELL No. DP-8864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-11.Red Brown Clayey fineto medium Sandy Silt
Tan Brown Silty fine to
medium Sand
Tan fine Sandy Silt
Boring Terminated at60 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel61 to 65 feet bls
Portland Cement and Powdered Bontonitegs to 65 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/23/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-9
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 51" N
80° 57' 04" W
610810.8366
1418698.768
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 61 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
45 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
COMPLETION REPORT OF
WELL No. DP-9864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-11.
Tan Brown Silty fine to
medium Sand
Tan fine Sandy Silt
Boring Terminated at55 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel51 to 55 feet bls
Portland Cement and Powdered Bontonitegs to 55 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/23/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-10
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 47" N
80° 57' 05" W
610750.596
1418711.433
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 51 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
41 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
COMPLETION REPORT OF
WELL No. DP-10864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
Red Brown Clayey fineto medium Sandy Silt
Tan Brown Silty fine to
medium Sand
Tan fine Sandy Silt
Boring Terminated at45 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel41 to 45 feet bls
Portland Cement and Powdered Bontonitegs to 45 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/24/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-11
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 47" N
80° 57' 05" W
610690.6342
1418698.47
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 41 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
30 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
COMPLETION REPORT OF
WELL No. DP-11864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-11.
Tan Brown Silty fine tomedium Sand
Tan fine Sandy Silt
Boring Terminated at
40 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel36 to 40 feet bls
Portland Cement and Powdered Bontonitegs to 40 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/24/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-12
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 50" N
80° 57' 02" W
610652.7617
1418666.708
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 36 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
30 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
COMPLETION REPORT OF
WELL No. DP-12864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-1.Red Brown Clayey fineSandy Silt
Orange Purple TanSilty fine Sand
Boring Terminated at62 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel57 to 61 feet bls
Portland Cement and Powdered Bontonitegs to 61 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/24/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-13
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 49" N
80° 57' 03" W
611240.1779
1418810.618
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 57 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
Dry feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
COMPLETION REPORT OF
WELL No. DP-13864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-1.Red Brown Clayey fineSandy Silt
Orange Purple TanSilty fine Sand
White Gray Silty fineSand
Boring Terminated at70 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel66 to 70 feet bls
Portland Cement and Powdered Bontonitegs to 70 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/24/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-14
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 49" N
80° 57' 04" W
611315.6677
1418802.303
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 66 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
55 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
COMPLETION REPORT OF
WELL No. DP-14864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-1.Red Brown Clayey fineSandy Silt
Orange Purple TanSilty fine Sand
White Gray Silty fineSand
Boring Terminated at73 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel69 to 73 feet bls
Portland Cement and Powdered Bontonitegs to 73 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/24/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-15
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 49" N
80° 57' 04" W
611275.8577
1418762.742
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 69 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
57 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
COMPLETION REPORT OF
WELL No. DP-15864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-1.Red Brown Clayey fineSandy Silt
Orange Purple TanSilty fine Sand
White Gray Silty fineSand
Boring Terminated at70 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel66 to 70 feet bls
Portland Cement and Powdered Bontonitegs to 70 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/24/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-16
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 47" N
80° 57' 04" W
611230.6221
1418726.388
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 66 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
54 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
COMPLETION REPORT OF
WELL No. DP-16864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
Leaves and Topsoil
Red Brown ClayeySilty fine to medium
Sand
Tan Silty fine Sand
White Gray Silty fine to
medium Sand
Orange Tan fineSandy Silt
Boring Terminated at
48 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchPVC38 to 48 feet bls
Portland Cement and Powdered Bontonitegs to 48 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/18/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-17
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 47" N
80° 57' 04" W
611042.6758
1418582.519
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
One InchPVCgs to to 38 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
39 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
COMPLETION REPORT OF
WELL No. DP-17864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-17.Red Brown ClayeySilty fine to medium
Sand
Tan Silty fine Sand
White Gray Silty fine to
medium Sand
Orange Tan fineSandy Silt
Boring Terminated at
50 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchPVC40 to 50 feet bls
Portland Cement and Powdered Bontonitegs to 50 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/18/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-18
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 46" N
80° 57' 04" W
610995.1434
1418591.134
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
One InchPVCgs to to 40 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
43 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
COMPLETION REPORT OF
WELL No. DP-18864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-17.Red Brown ClayeySilty fine to medium
Sand
Tan Silty fine Sand
White Gray Silty fine to
medium Sand
Orange Tan fine
Sandy Silt
Boring Terminated at55 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel51 to 55 feet bls
Portland Cement and Powdered Bontonitegs to 55 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/19/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-19
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 46" N
80° 57' 04" W
610929.8163
1418595.861
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 51 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
39 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
COMPLETION REPORT OF
WELL No. DP-19864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-1.Red Brown Clayey fineSandy Silt
Orange Purple TanSilty fine Sand
White Gray Silty fineSandBoring Terminated at
65 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel61 to 65 feet bls
Portland Cement and Powdered Bontonitegs to 65 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/25/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-20
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 45" N
80° 57' 04" W
611208.5572
1418689.676
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 61 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
52 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
COMPLETION REPORT OF
WELL No. DP-20864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-1.Red Brown Clayey fineSandy Silt
Orange Purple TanSilty fine Sand
Boring Terminated at61 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel56 to 60 feet bls
Portland Cement and Powdered Bontonitegs to 60 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/25/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-21
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 44" N
80° 57' 04" W
611188.0785
1418639.347
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 56 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
40 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
COMPLETION REPORT OF
WELL No. DP-21864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-17.Red Brown ClayeySilty fine to medium
Sand
Tan Silty fine Sand
White Gray Silty fine tomedium Sand
Orange Tan fineSandy Silt
Boring Terminated at60 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel56 to 60 feet bls
Portland Cement and Powdered Bontonitegs to 60 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/25/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-22
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 44" N
80° 57' 04" W
611151.8136
1418602.509
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 56 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
45 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
COMPLETION REPORT OF
WELL No. DP-22864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-25.
Red Brown Clayey fine
Sandy Silt
Tan Brown Silty fine to
medium Sand
Brown White fine
Sandy Silt
Boring Terminated at
50 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel46 to 50 feet bls
Portland Cement and Powdered Bontonitegs to 50 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/25/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-23
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 50" N
80° 57' 03" W
611159.2051
1418514.2
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 46 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
42 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
COMPLETION REPORT OF
WELL No. DP-23864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-25.
Red Brown Clayey fineSandy Silt
Tan Brown Silty fine to
medium Sand
Brown White fineSandy Silt
Gray Brown WhiteSilty fine to mediumSand
Boring Terminated at55 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel51 to 55 feet bls
Portland Cement and Powdered Bontonitegs to 55 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/25/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-24
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 50" N
80° 57' 03" W
611201.2676
1418549.729
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 51 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
41 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
COMPLETION REPORT OF
WELL No. DP-24864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
Leaves and Topsoil
Red Brown Clayey fineSandy Silt
Tan Brown Silty fine tomedium Sand
Brown White fineSandy Silt
Gray Brown WhiteSilty fine to mediumSand
Boring Terminated at60 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel56 to 60 feet bls
Portland Cement and Powdered Bontonitegs to 60 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/26/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-25
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 50" N
80° 57' 03" W
611231.3661
1418593.489
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 56 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
40 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
COMPLETION REPORT OF
WELL No. DP-25864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-25.Red Brown Clayey fineSandy Silt
Tan Brown Silty fine tomedium Sand
Brown White fineSandy Silt
Gray Brown WhiteSilty fine to mediumSand
Boring Terminated at60 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel56 to 60 feet bls
Portland Cement and Powdered Bontonitegs to 60 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/25/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-26
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 49" N
80° 57' 04" W
611273.9397
1418629.966
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 56 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
46 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
COMPLETION REPORT OF
WELL No. DP-26864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-25.Red Brown Clayey fineSandy Silt
Tan Brown Silty fine tomedium Sand
Brown White fine
Sandy Silt
Gray Brown WhiteSilty fine to mediumSand
Boring Terminated at65 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel61 to 65 feet bls
Portland Cement and Powdered Bontonitegs to 65 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/26/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-27
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 49" N
80° 57' 04" W
611316.2425
1418680.224
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 61 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
52 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
65
COMPLETION REPORT OF
WELL No. DP-27864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
No soil samples
collected at this
location.Lithology interploated
from DP-25.Red Brown Clayey fineSandy Silt
Tan Brown Silty fine tomedium Sand
Brown White fineSandy Silt
Gray Brown WhiteSilty fine to mediumSand
Boring Terminated at60 Feet
WELL CONSTRUCTION DETAILS
DE
P T H
(f
t .)DESCRIPTION
S Y M B OL
L E GE
ND
E L E V A T I ON
(f
t .)
WELL
DETAILS
STRATA
DE
P T H
(f
t .)
One InchStainless Steel56 to 60 feet bls
Portland Cement and Powdered Bontonitegs to 60 feet bls
Diameter:
Type:
Interval:
SCREEN
0.0 GS
SAEDACCO
Direct Push
5/26/16
Richard Bonds
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
NORTHING:
EASTING:
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
WELL COMPLETION REPORT FOR DP-28
FILTERPACK
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
LOGGED BY:
35° 24' 49" N
80° 57' 05" W
611370.6445
1418720.281
Diameter:
Type:
Interval:
None
None
SEAL
GROUT
None
RISER CASING
Type:
Interval:
1.5 InchesDirect Push Rodsgs to to 56 feet bls
PROJECT:
PROJECT NO:
PROJECT LOCATION:
McGuire Nuclear Station4226-16-060Huntersville, North Carolina
Sheet 1 of 1
44 feet at TOBWATER LEVEL:
0
5
10
15
20
25
30
35
40
45
50
55
60
COMPLETION REPORT OF
WELL No. DP-28864.232.8987864.574.2360
FILTER PACK
K-PACKER
BENTONITE
CEMENT GROUT
SAPROLITE
STATIC WATER LEVEL
WATER LEVEL AT TOB
ALSBLS
TOCGSBS
BOCFP
TSC
BSCTD
CG
LEGEND
ABOVE LAND SURFACEBELOW LAND SURFACE
TOP OF CASINGGROUND SURFACEBENTONITE SEAL
BASE OF OUTER CASINGFILTER PACK
TOP OF SCREEN
BOTTOM OF SCREENTOTAL DEPTH
CEMENT GROUT
S&ME, Inc.Greenville, SCSpartanburg, SC
J W W
D P T
L O G S .G
P J
S &M E .G
D T
6 /2
2 /1
6
Sheet 1 of 1
Appendix V – Analytical Laboratory Report
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,*+0*+./02 A7<I>F9 +2'ANf'+0!!.4-/!DA F>7=5F8!6CB8G 8D'+2!!
,*+0*+./03 A7<I>F9 +3'ANf'+0!!+*4*/!5A F>7=5F8!6CB8G 8D'+3!!
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$?EN$
Oc{!38-!3127
NKOU!WUG<!HT!.!RTQITCO!OCPCIGT
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;33;979;
Rtqlgev<
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-
L271616;3!OEIWKTG!NH
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Gpenqugf!ctg!vjg!cpcn{vkecn!tguwnvu!hqt!ucorng)u*!tgegkxgf!d{!vjg!ncdqtcvqt{!qp!Oc{!34-!3127/!!Vjg
tguwnvu!tgncvg!qpn{!vq!vjg!ucorngu!kpenwfgf!kp!vjku!tgrqtv/!!Tguwnvu!tgrqtvgf!jgtgkp!eqphqto!vq!vjg
oquv!ewttgpv!VPK!uvcpfctfu!cpf!vjg!ncdqtcvqt{(u!Swcnkv{!Cuuwtcpeg!Ocpwcn-!yjgtg!crrnkecdng-!wpnguu
qvjgtykug!pqvgf!kp!vjg!dqf{!qh!vjg!tgrqtv/
Cpcn{ugu!ygtg!rgthqtogf!cv!vjg!Rceg!Cpcn{vkecn!Ugtxkegu!nqecvkqp!kpfkecvgf!qp!vjg!ucorng!cpcn{vg
rcig!hqt!cpcn{uku!wpnguu!qvjgtykug!hqqvpqvgf/
Kh!{qw!jcxg!cp{!swguvkqpu!eqpegtpkpi!vjku!tgrqtv-!rngcug!hggn!htgg!vq!eqpvcev!og/
Ukpegtgn{-
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JQTK\QP!Fcvcdcug!Cfokpkuvtcvqt
Gpenquwtgu
ee< Tkejctf!Dqpfu
Rtqitco!Ocpcigt-!Fwmg!Gpgti{
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 1 of 27
Rcig!22!qh!49
$?ER$
CERTIFICATIONS
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;33;979;
L271616;3!OEIWKTG!NH
Charlotte Certification IDs
;911!Mkpeg{!Cxg/!Uvg!211-!Jwpvgtuxknng-!PE!39189Pqtvj!Ectqnkpc!Ftkpmkpi!Ycvgt!Egtvkhkecvkqp!$<!48817
Pqtvj!Ectqnkpc!Hkgnf!Ugtxkegu!Egtvkhkecvkqp!$<!6453Pqtvj!Ectqnkpc!Ycuvgycvgt!Egtvkhkecvkqp!$<!23
Uqwvj!Ectqnkpc!Egtvkhkecvkqp!$<!;;117112Hnqtkfc0PGNCR!Egtvkhkecvkqp!$<!G98738
Mgpvwem{!WUV!Egtvkhkecvkqp!$<!95Xktikpkc0XGNCR!Egtvkhkecvkqp!$<!571332
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 2 of 27
Rcig!23!qh!49
$?UC$
SAMPLE ANALYTE COUNT
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L271616;3!OEIWKTG!NH
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92298689001 2016014567 DP-17 GRC!9371 63 RCUK.EECJ
92298689002 2016014568 DP-18 GRC!9371 63 RCUK.EECJ
92298689003 2016014569 DP-19 GRC!9371 63 RCUK.EECJ
92298689004 2016014570 DP-1 GRC!9371 63 RCUK.EECJ
92298689005 2016014571 DP-2 GRC!9371 63 RCUK.EECJ
92298689006 2016014572 DP-3 GRC!9371 63 RCUK.EECJ
92298689007 2016014573 DP-4 GRC!9371 63 RCUK.EECJ
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 3 of 27
Rcig!24!qh!49
$?JQ$
SUMMARY OF DETECTION
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Rctcogvgtu Cpcn{|gfTguwnv
Ncd!Ucorng!KF!
Tgrqtv!Nkokv SwcnkhkgtuWpkvuOgvjqf
Enkgpv!Ucorng!KF
92298689001 2016014567 DP-17
Vgvtcejnqtqgvjgpg >2/1 wi0N 16037027!29<542/1GRC!9371
Vtkejnqtqgvjgpg >2/1 wi0N 16037027!29<542/1GRC!9371
92298689002 2016014568 DP-18
Cegvqpg >36/1 wi0N 16037027!2;<1136/1GRC!9371
3.Jgzcpqpg >6/1 wi0N 16037027!2;<116/1GRC!9371
92298689004 2016014570 DP-1
Cegvqpg >36/1 wi0N 16037027!2;<4536/1GRC!9371
Vqnwgpg >2/1 wi0N 16037027!2;<452/1GRC!9371
92298689005 2016014571 DP-2
Dgp|gpg >2/1 wi0N 16037027!2;<622/1GRC!9371
eku.2-3.Fkejnqtqgvjgpg 56/4 wi0N 16037027!2;<622/1GRC!9371
Ogvj{ngpg!Ejnqtkfg ;/1 wi0N 16037027!2;<623/1GRC!9371
Vqnwgpg >2/1 wi0N 16037027!2;<622/1GRC!9371
Vtkejnqtqgvjgpg 3/4 wi0N 16037027!2;<622/1GRC!9371
Z{ngpg!)Vqvcn*;/5 wi0N 16037027!2;<623/1GRC!9371
q.Z{ngpg ;/5 wi0N 16037027!2;<622/1GRC!9371
92298689006 2016014572 DP-3
Cegvqpg >36/1 wi0N 16037027!31<1936/1GRC!9371
Dgp|gpg >2/1 wi0N 16037027!31<192/1GRC!9371
eku.2-3.Fkejnqtqgvjgpg 2;/8 wi0N 16037027!31<192/1GRC!9371
Ogvj{ngpg!Ejnqtkfg 8/8 wi0N 16037027!31<193/1GRC!9371
Vqnwgpg >2/1 wi0N 16037027!31<192/1GRC!9371
Vtkejnqtqgvjgpg 4/4 wi0N 16037027!31<192/1GRC!9371
Xkp{n!ejnqtkfg >2/1 wi0N 16037027!31<192/1GRC!9371
Z{ngpg!)Vqvcn*38/2 wi0N 16037027!31<193/1GRC!9371
o'r.Z{ngpg 7/8 wi0N 16037027!31<193/1GRC!9371
q.Z{ngpg 31/5 wi0N 16037027!31<192/1GRC!9371
92298689007 2016014573 DP-4
Dgp|gpg >2/1 wi0N 16037027!31<362/1GRC!9371
2-2.Fkejnqtqgvjcpg >2/1 wi0N 16037027!31<362/1GRC!9371
eku.2-3.Fkejnqtqgvjgpg 34/9 wi0N 16037027!31<362/1GRC!9371
Ogvj{ngpg!Ejnqtkfg 22/6 wi0N 16037027!31<363/1GRC!9371
Vqnwgpg >2/1 wi0N 16037027!31<362/1GRC!9371
Vtkejnqtqgvjgpg 2/7 wi0N 16037027!31<362/1GRC!9371
Z{ngpg!)Vqvcn*29/2 wi0N 16037027!31<363/1GRC!9371
o'r.Z{ngpg >3/1 wi0N 16037027!31<363/1GRC!9371
q.Z{ngpg 29/2 wi0N 16037027!31<362/1GRC!9371
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 4 of 27
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$?PC$
PROJECT NARRATIVE
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Method:
Client:Fwmg!Gpgti{
EPA 8260
Date:Oc{!38-!3127
Description:9371!OUX!Nqy!Ngxgn
General Information:
8!ucorngu!ygtg!cpcn{|gf!hqt!GRC!9371/!!Cnn!ucorngu!ygtg!tgegkxgf!kp!ceegrvcdng!eqpfkvkqp!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy!qt!qp!vjg
ejckp.qh!ewuvqf{!cpf0qt!vjg!ucorng!eqpfkvkqp!wrqp!tgegkrv!hqto!)UEWT*!cvvcejgf!cv!vjg!gpf!qh!vjku!tgrqtv/
Hold Time:
Vjg!ucorngu!ygtg!cpcn{|gf!ykvjkp!vjg!ogvjqf!tgswktgf!jqnf!vkogu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Initial Calibrations (including MS Tune as applicable):
Cnn!etkvgtkc!ygtg!ykvjkp!ogvjqf!tgswktgogpvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Continuing Calibration:
Cnn!etkvgtkc!ygtg!ykvjkp!ogvjqf!tgswktgogpvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Internal Standards:
Cnn!kpvgtpcn!uvcpfctfu!ygtg!ykvjkp!SE!nkokvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Surrogates:
Cnn!uwttqicvgu!ygtg!ykvjkp!SE!nkokvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Method Blank:
Cnn!cpcn{vgu!ygtg!dgnqy!vjg!tgrqtv!nkokv!kp!vjg!ogvjqf!dncpm-!yjgtg!crrnkecdng-!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Laboratory Control Spike:
Cnn!ncdqtcvqt{!eqpvtqn!urkmg!eqorqwpfu!ygtg!ykvjkp!SE!nkokvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Matrix Spikes:
Cnn!rgtegpv!tgeqxgtkgu!cpf!tgncvkxg!rgtegpv!fkhhgtgpegu!)TRFu*!ygtg!ykvjkp!ceegrvcpeg!etkvgtkc!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
SE!Dcvej<!OUX048123
C!ocvtkz!urkmg!cpf0qt!ocvtkz!urkmg!fwrnkecvg!)OU0OUF*!ygtg!rgthqtogf!qp!vjg!hqnnqykpi!ucorng)u*<!!;33;97;1114
O2<!Ocvtkz!urkmg!tgeqxgt{!gzeggfgf!SE!nkokvu/!!Dcvej!ceegrvgf!dcugf!qp!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!tgeqxgt{/
—!OU!!)Ncd!KF<!2854239*
—!Ectdqp!fkuwnhkfg
—!OUF!!)Ncd!KF<!285423;*
—!Dtqoqogvjcpg
—!Ectdqp!fkuwnhkfg
Additional Comments:
Vjku!fcvc!rcemcig!jcu!dggp!tgxkgygf!hqt!swcnkv{!cpf!eqorngvgpguu!cpf!ku!crrtqxgf!hqt!tgngcug/
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 5 of 27
Rcig!26!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014567 DP-17 Lab ID: 92298689001 Eqnngevgf< 16029027!25<41 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16037027!29<54 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16037027!29<54 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16037027!29<54 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16037027!29<54 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16037027!29<54 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16037027!29<54 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16037027!29<54 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16037027!29<54 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16037027!29<54 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16037027!29<54 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16037027!29<54 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16037027!29<54 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16037027!29<54 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16037027!29<54 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16037027!29<54 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16037027!29<54 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16037027!29<54 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16037027!29<54 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!29<54 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!29<54 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16037027!29<54 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16037027!29<54 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16037027!29<54 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16037027!29<54 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!29<54 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!29<54 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16037027!29<54 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!29<54 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!29<54 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16037027!29<54 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16037027!29<54 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16037027!29<54 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 16037027!29<54 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16037027!29<54 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16037027!29<54 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!29<54 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!29<54 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16037027!29<54 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16037027!29<54 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!29<54 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!29<54 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16037027!29<54 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16037027!29<54 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16037027!29<54 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16037027!29<54 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16037027!29<54 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 16037027!29<54 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 6 of 27
Rcig!27!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014567 DP-17 Lab ID: 92298689001 Eqnngevgf< 16029027!25<41 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16037027!29<54 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 16037027!29<54 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;8 &16037027!29<54 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*213 &16037027!29<54 28171.18.181.241 2
Vqnwgpg.f9!)U*211 &16037027!29<54 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 7 of 27
Rcig!28!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014568 DP-18 Lab ID: 92298689002 Eqnngevgf< 16029027!27<46 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16037027!2;<11 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16037027!2;<11 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16037027!2;<11 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16037027!2;<11 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16037027!2;<11 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16037027!2;<11 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16037027!2;<11 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16037027!2;<11 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16037027!2;<11 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16037027!2;<11 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16037027!2;<11 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16037027!2;<11 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16037027!2;<11 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16037027!2;<11 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16037027!2;<11 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16037027!2;<11 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16037027!2;<11 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16037027!2;<11 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!2;<11 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!2;<11 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16037027!2;<11 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16037027!2;<11 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16037027!2;<11 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<11 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<11 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<11 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16037027!2;<11 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!2;<11 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!2;<11 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16037027!2;<11 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16037027!2;<11 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16037027!2;<11 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 16037027!2;<11 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16037027!2;<11 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16037027!2;<11 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!2;<11 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!2;<11 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16037027!2;<11 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16037027!2;<11 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!2;<11 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!2;<11 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16037027!2;<11 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16037027!2;<11 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16037027!2;<11 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16037027!2;<11 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16037027!2;<11 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 16037027!2;<11 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 8 of 27
Rcig!29!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014568 DP-18 Lab ID: 92298689002 Eqnngevgf< 16029027!27<46 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16037027!2;<11 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 16037027!2;<11 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;9 &16037027!2;<11 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*214 &16037027!2;<11 28171.18.181.241 2
Vqnwgpg.f9!)U*211 &16037027!2;<11 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 9 of 27
Rcig!2;!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014569 DP-19 Lab ID: 92298689003 Eqnngevgf< 1602;027!21<16 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16037027!2;<28 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16037027!2;<28 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16037027!2;<28 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16037027!2;<28 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16037027!2;<28 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16037027!2;<28 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16037027!2;<28 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16037027!2;<28 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16037027!2;<28 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16037027!2;<28 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16037027!2;<28 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16037027!2;<28 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16037027!2;<28 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16037027!2;<28 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16037027!2;<28 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16037027!2;<28 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16037027!2;<28 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16037027!2;<28 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!2;<28 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!2;<28 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16037027!2;<28 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16037027!2;<28 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16037027!2;<28 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<28 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<28 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<28 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16037027!2;<28 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!2;<28 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!2;<28 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16037027!2;<28 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16037027!2;<28 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16037027!2;<28 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 16037027!2;<28 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16037027!2;<28 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16037027!2;<28 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!2;<28 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!2;<28 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16037027!2;<28 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16037027!2;<28 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!2;<28 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!2;<28 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16037027!2;<28 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16037027!2;<28 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16037027!2;<28 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16037027!2;<28 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16037027!2;<28 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 16037027!2;<28 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 10 of 27
Rcig!31!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014569 DP-19 Lab ID: 92298689003 Eqnngevgf< 1602;027!21<16 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16037027!2;<28 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 16037027!2;<28 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;8 &16037027!2;<28 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*214 &16037027!2;<28 28171.18.181.241 2
Vqnwgpg.f9!)U*211 &16037027!2;<28 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 11 of 27
Rcig!32!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014570 DP-1 Lab ID: 92298689004 Eqnngevgf< 1602;027!26<56 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16037027!2;<45 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16037027!2;<45 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16037027!2;<45 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16037027!2;<45 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16037027!2;<45 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16037027!2;<45 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16037027!2;<45 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16037027!2;<45 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16037027!2;<45 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16037027!2;<45 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16037027!2;<45 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16037027!2;<45 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16037027!2;<45 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16037027!2;<45 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16037027!2;<45 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16037027!2;<45 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16037027!2;<45 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16037027!2;<45 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!2;<45 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!2;<45 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16037027!2;<45 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16037027!2;<45 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16037027!2;<45 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<45 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<45 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<45 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16037027!2;<45 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!2;<45 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!2;<45 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16037027!2;<45 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16037027!2;<45 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16037027!2;<45 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 16037027!2;<45 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16037027!2;<45 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16037027!2;<45 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!2;<45 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!2;<45 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16037027!2;<45 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16037027!2;<45 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!2;<45 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!2;<45 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16037027!2;<45 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16037027!2;<45 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16037027!2;<45 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16037027!2;<45 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16037027!2;<45 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 16037027!2;<45 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 12 of 27
Rcig!33!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014570 DP-1 Lab ID: 92298689004 Eqnngevgf< 1602;027!26<56 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16037027!2;<45 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 16037027!2;<45 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;8 &16037027!2;<45 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*215 &16037027!2;<45 28171.18.181.241 2
Vqnwgpg.f9!)U*213 &16037027!2;<45 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 13 of 27
Rcig!34!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014571 DP-2 Lab ID: 92298689005 Eqnngevgf< 16031027!1;<61 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16037027!2;<62 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16037027!2;<62 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16037027!2;<62 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16037027!2;<62 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16037027!2;<62 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16037027!2;<62 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16037027!2;<62 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16037027!2;<62 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16037027!2;<62 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16037027!2;<62 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16037027!2;<62 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16037027!2;<62 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16037027!2;<62 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16037027!2;<62 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16037027!2;<62 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16037027!2;<62 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16037027!2;<62 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16037027!2;<62 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!2;<62 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!2;<62 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16037027!2;<62 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16037027!2;<62 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16037027!2;<62 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<62 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg 45.3 wi0N 16037027!2;<62 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!2;<62 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16037027!2;<62 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!2;<62 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!2;<62 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16037027!2;<62 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16037027!2;<62 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16037027!2;<62 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg 9.0 wi0N 16037027!2;<62 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16037027!2;<62 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16037027!2;<62 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!2;<62 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!2;<62 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16037027!2;<62 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16037027!2;<62 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!2;<62 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!2;<62 8;.11.62/1 2
Vtkejnqtqgvjgpg 2.3 wi0N 16037027!2;<62 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16037027!2;<62 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16037027!2;<62 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16037027!2;<62 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16037027!2;<62 86.12.52/1 2
Z{ngpg!)Vqvcn*9.4 wi0N 16037027!2;<62 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 14 of 27
Rcig!35!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014571 DP-2 Lab ID: 92298689005 Eqnngevgf< 16031027!1;<61 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16037027!2;<62 28;712.34.23/1 2
q.Z{ngpg 9.4 wi0N 16037027!2;<62 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;7 &16037027!2;<62 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*214 &16037027!2;<62 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &16037027!2;<62 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 15 of 27
Rcig!36!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014572 DP-3 Lab ID: 92298689006 Eqnngevgf< 16031027!22<46 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16037027!31<19 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16037027!31<19 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16037027!31<19 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16037027!31<19 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16037027!31<19 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16037027!31<19 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16037027!31<19 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16037027!31<19 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16037027!31<19 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16037027!31<19 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16037027!31<19 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16037027!31<19 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16037027!31<19 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16037027!31<19 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16037027!31<19 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16037027!31<19 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16037027!31<19 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16037027!31<19 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!31<19 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!31<19 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16037027!31<19 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16037027!31<19 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16037027!31<19 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16037027!31<19 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg 19.7 wi0N 16037027!31<19 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!31<19 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16037027!31<19 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!31<19 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!31<19 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16037027!31<19 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16037027!31<19 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16037027!31<19 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg 7.7 wi0N 16037027!31<19 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16037027!31<19 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16037027!31<19 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!31<19 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!31<19 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16037027!31<19 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16037027!31<19 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!31<19 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!31<19 8;.11.62/1 2
Vtkejnqtqgvjgpg 3.3 wi0N 16037027!31<19 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16037027!31<19 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16037027!31<19 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16037027!31<19 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16037027!31<19 86.12.52/1 2
Z{ngpg!)Vqvcn*27.1 wi0N 16037027!31<19 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 16 of 27
Rcig!37!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014572 DP-3 Lab ID: 92298689006 Eqnngevgf< 16031027!22<46 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg 6.7 wi0N 16037027!31<19 28;712.34.23/1 2
q.Z{ngpg 20.4 wi0N 16037027!31<19 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;8 &16037027!31<19 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*214 &16037027!31<19 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &16037027!31<19 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 17 of 27
Rcig!38!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014573 DP-4 Lab ID: 92298689007 Eqnngevgf< 16031027!25<36 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16037027!31<36 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16037027!31<36 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16037027!31<36 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16037027!31<36 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16037027!31<36 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16037027!31<36 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16037027!31<36 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16037027!31<36 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16037027!31<36 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16037027!31<36 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16037027!31<36 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16037027!31<36 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16037027!31<36 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16037027!31<36 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16037027!31<36 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16037027!31<36 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16037027!31<36 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16037027!31<36 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!31<36 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16037027!31<36 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16037027!31<36 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16037027!31<36 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16037027!31<36 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16037027!31<36 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg 23.8 wi0N 16037027!31<36 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16037027!31<36 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16037027!31<36 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!31<36 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16037027!31<36 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16037027!31<36 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16037027!31<36 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16037027!31<36 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg 11.5 wi0N 16037027!31<36 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16037027!31<36 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16037027!31<36 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!31<36 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16037027!31<36 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16037027!31<36 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16037027!31<36 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!31<36 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16037027!31<36 8;.11.62/1 2
Vtkejnqtqgvjgpg 1.6 wi0N 16037027!31<36 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16037027!31<36 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16037027!31<36 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16037027!31<36 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16037027!31<36 86.12.52/1 2
Z{ngpg!)Vqvcn*18.1 wi0N 16037027!31<36 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 18 of 27
Rcig!39!qh!49
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Sample: 2016014573 DP-4 Lab ID: 92298689007 Eqnngevgf< 16031027!25<36 Tgegkxgf< 16034027!24<52 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16037027!31<36 28;712.34.23/1 2
q.Z{ngpg 18.1 wi0N 16037027!31<36 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;8 &16037027!31<36 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*214 &16037027!31<36 28171.18.181.241 2
Vqnwgpg.f9!)U*211 &16037027!31<36 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 19 of 27
Rcig!3;!qh!49
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
SE!Dcvej<
SE!Dcvej!Ogvjqf<
Cpcn{uku!Ogvjqf<
Cpcn{uku!Fguetkrvkqp<
OUX048123
GRC!9371
GRC!9371
9371!OUX!Nqy!Ngxgn
Cuuqekcvgf!Ncd!Ucorngu< ;33;979;112-!;33;979;113-!;33;979;114-!;33;979;115-!;33;979;116-!;33;979;117-!;33;979;118
Rctcogvgt Wpkvu
Dncpm
Tguwnv
Tgrqtvkpi
Nkokv Swcnkhkgtu
OGVJQF!DNCPM< 2854237
Cuuqekcvgf!Ncd!Ucorngu<;33;979;112-!;33;979;113-!;33;979;114-!;33;979;115-!;33;979;116-!;33;979;117-!;33;979;118
Ocvtkz< Ycvgt
Cpcn{|gf
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N >2/1 2/1 16037027!27<1;
2-2-2.Vtkejnqtqgvjcpg wi0N >2/1 2/1 16037027!27<1;
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N >2/1 2/1 16037027!27<1;
2-2-3.Vtkejnqtqgvjcpg wi0N >2/1 2/1 16037027!27<1;
2-2.Fkejnqtqgvjcpg wi0N >2/1 2/1 16037027!27<1;
2-2.Fkejnqtqgvjgpg wi0N >2/1 2/1 16037027!27<1;
2-3-4.Vtkejnqtqrtqrcpg wi0N >2/1 2/1 16037027!27<1;
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N >3/1 3/1 16037027!27<1;
2-3.Fkdtqoqgvjcpg!)GFD*wi0N >2/1 2/1 16037027!27<1;
2-3.Fkejnqtqdgp|gpg wi0N >2/1 2/1 16037027!27<1;
2-3.Fkejnqtqgvjcpg wi0N >2/1 2/1 16037027!27<1;
2-3.Fkejnqtqrtqrcpg wi0N >2/1 2/1 16037027!27<1;
2-5.Fkejnqtqdgp|gpg wi0N >2/1 2/1 16037027!27<1;
3.Dwvcpqpg!)OGM*wi0N >6/1 6/1 16037027!27<1;
3.Jgzcpqpg wi0N >6/1 6/1 16037027!27<1;
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N >6/1 6/1 16037027!27<1;
Cegvqpg wi0N >36/1 36/1 16037027!27<1;
Cet{nqpkvtkng wi0N >21/1 21/1 16037027!27<1;
Dgp|gpg wi0N >2/1 2/1 16037027!27<1;
Dtqoqejnqtqogvjcpg wi0N >2/1 2/1 16037027!27<1;
Dtqoqfkejnqtqogvjcpg wi0N >2/1 2/1 16037027!27<1;
Dtqoqhqto wi0N >2/1 2/1 16037027!27<1;
Dtqoqogvjcpg wi0N >3/1 3/1 16037027!27<1;
Ectdqp!fkuwnhkfg wi0N >3/1 3/1 16037027!27<1;
Ectdqp!vgvtcejnqtkfg wi0N >2/1 2/1 16037027!27<1;
Ejnqtqdgp|gpg wi0N >2/1 2/1 16037027!27<1;
Ejnqtqgvjcpg wi0N >2/1 2/1 16037027!27<1;
Ejnqtqhqto wi0N >2/1 2/1 16037027!27<1;
Ejnqtqogvjcpg wi0N >2/1 2/1 16037027!27<1;
eku.2-3.Fkejnqtqgvjgpg wi0N >2/1 2/1 16037027!27<1;
eku.2-4.Fkejnqtqrtqrgpg wi0N >2/1 2/1 16037027!27<1;
Fkdtqoqejnqtqogvjcpg wi0N >2/1 2/1 16037027!27<1;
Fkdtqoqogvjcpg wi0N >2/1 2/1 16037027!27<1;
Gvj{ndgp|gpg wi0N >2/1 2/1 16037027!27<1;
Kqfqogvjcpg wi0N >6/1 6/1 16037027!27<1;
o'r.Z{ngpg wi0N >3/1 3/1 16037027!27<1;
Ogvj{ngpg!Ejnqtkfg wi0N >3/1 3/1 16037027!27<1;
q.Z{ngpg wi0N >2/1 2/1 16037027!27<1;
Uv{tgpg wi0N >2/1 2/1 16037027!27<1;
Vgvtcejnqtqgvjgpg wi0N >2/1 2/1 16037027!27<1;
Vqnwgpg wi0N >2/1 2/1 16037027!27<1;
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
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)815*986.;1;3
Page 20 of 27
Rcig!41!qh!49
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
Dncpm
Tguwnv
Tgrqtvkpi
Nkokv Swcnkhkgtu
OGVJQF!DNCPM< 2854237
Cuuqekcvgf!Ncd!Ucorngu<;33;979;112-!;33;979;113-!;33;979;114-!;33;979;115-!;33;979;116-!;33;979;117-!;33;979;118
Ocvtkz< Ycvgt
Cpcn{|gf
vtcpu.2-3.Fkejnqtqgvjgpg wi0N >2/1 2/1 16037027!27<1;
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N >2/1 2/1 16037027!27<1;
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N >2/1 2/1 16037027!27<1;
Vtkejnqtqgvjgpg wi0N >2/1 2/1 16037027!27<1;
Vtkejnqtqhnwqtqogvjcpg wi0N >2/1 2/1 16037027!27<1;
Xkp{n!cegvcvg wi0N >3/1 3/1 16037027!27<1;
Xkp{n!ejnqtkfg wi0N >2/1 2/1 16037027!27<1;
Z{ngpg!)Vqvcn*wi0N >3/1 3/1 16037027!27<1;
2-3.Fkejnqtqgvjcpg.f5!)U*&214 81.241 16037027!27<1;
5.Dtqoqhnwqtqdgp|gpg!)U*&;9 81.241 16037027!27<1;
Vqnwgpg.f9!)U*&211 81.241 16037027!27<1;
Rctcogvgt Wpkvu
NEU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2854238NCDQTCVQT[!EQPVTQN!UCORNG<
NEUUrkmg
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N 57/261 ;3 81.241
2-2-2.Vtkejnqtqgvjcpg wi0N 66/661 222 81.241
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N 56/;61 ;3 81.241
2-2-3.Vtkejnqtqgvjcpg wi0N 58/661 ;6 81.241
2-2.Fkejnqtqgvjcpg wi0N 63/;61 217 81.241
2-2.Fkejnqtqgvjgpg wi0N 71/761 232 81.243
2-3-4.Vtkejnqtqrtqrcpg wi0N 55/761 9;81.241
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N 58/461 ;6 81.241
2-3.Fkdtqoqgvjcpg!)GFD*wi0N 61/361 211 81.241
2-3.Fkejnqtqdgp|gpg wi0N 59/561 ;8 81.241
2-3.Fkejnqtqgvjcpg wi0N 58/661 ;6 81.241
2-3.Fkejnqtqrtqrcpg wi0N 59/961 ;9 81.241
2-5.Fkejnqtqdgp|gpg wi0N 59/961 ;9 81.241
3.Dwvcpqpg!)OGM*wi0N 211211 211 81.256
3.Jgzcpqpg wi0N ;7/6211 ;8 81.255
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N 213211 213 81.251
Cegvqpg wi0N 212211 212 61.286
Cet{nqpkvtkng wi0N 368361 214 81.254
Dgp|gpg wi0N 61/761 212 81.241
Dtqoqejnqtqogvjcpg wi0N 63/961 217 81.241
Dtqoqfkejnqtqogvjcpg wi0N 59/661 ;8 81.241
Dtqoqhqto wi0N 56/661 ;2 81.241
Dtqoqogvjcpg wi0N 66/161 221 65.241
Ectdqp!fkuwnhkfg wi0N 73/561 236 81.242
Ectdqp!vgvtcejnqtkfg wi0N 65/361 219 81.243
Ejnqtqdgp|gpg wi0N 5;/361 ;9 81.241
Ejnqtqgvjcpg wi0N 61/;61 213 75.245
Ejnqtqhqto wi0N 61/861 212 81.241
Ejnqtqogvjcpg wi0N 62/461 214 75.241
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 21 of 27
Rcig!42!qh!49
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
NEU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2854238NCDQTCVQT[!EQPVTQN!UCORNG<
NEUUrkmg
eku.2-3.Fkejnqtqgvjgpg wi0N 65/561 21;81.242
eku.2-4.Fkejnqtqrtqrgpg wi0N 5;/;61 211 81.241
Fkdtqoqejnqtqogvjcpg wi0N 57/861 ;4 81.241
Fkdtqoqogvjcpg wi0N 5;/361 ;9 81.242
Gvj{ndgp|gpg wi0N 5;/461 ;;81.241
Kqfqogvjcpg wi0N ;9/1211 ;9 5;.291
o'r.Z{ngpg wi0N ;7/4211 ;7 81.241
Ogvj{ngpg!Ejnqtkfg wi0N 62/261 213 74.241
q.Z{ngpg wi0N 58/461 ;6 81.241
Uv{tgpg wi0N 5;/461 ;;81.241
Vgvtcejnqtqgvjgpg wi0N 58/861 ;6 81.241
Vqnwgpg wi0N 61/;61 213 81.241
vtcpu.2-3.Fkejnqtqgvjgpg wi0N 69/161 227 81.241
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N 58/461 ;6 81.243
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N 53/;61 97 81.252
Vtkejnqtqgvjgpg wi0N 61/861 212 81.241
Vtkejnqtqhnwqtqogvjcpg wi0N 58/461 ;6 73.244
Xkp{n!cegvcvg wi0N 217211 217 77.268
Xkp{n!ejnqtkfg wi0N 63/661 216 61.261
Z{ngpg!)Vqvcn*wi0N 255261 ;7 81.241
2-3.Fkejnqtqgvjcpg.f5!)U*&215 81.241
5.Dtqoqhnwqtqdgp|gpg!)U*&;;81.241
Vqnwgpg.f9!)U*&212 81.241
Rctcogvgt Wpkvu
OU
Tguwnv
&!Tge
Nkokvu Swcn&!TgeEqpe/
2854239OCVTKZ!URKMG!'!OCVTKZ!URKMG!FWRNKECVG<
OUUrkmg
Tguwnv
;33;97;1114
285423;
OUF
Tguwnv
OUF
&!Tge TRF
OUFOU
Urkmg
Eqpe/
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N 31 ;7 81.241;7 131PF2;/4 2;/3
2-2-2.Vtkejnqtqgvjcpg wi0N 31 239 81.241235 431PF36/7 35/;
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N 31 ;6 81.241;7 331PF29/;2;/3
2-2-3.Vtkejnqtqgvjcpg wi0N 31 215 81.241212 431PF31/8 31/3
2-2.Fkejnqtqgvjcpg wi0N 31 22;81.241227 431PF34/;34/2
2-2.Fkejnqtqgvjgpg wi0N 31 253 81.277246 631PF39/4 38/1
2-3-4.Vtkejnqtqrtqrcpg wi0N 31 ;6 81.241;2 531PF2;/1 29/3
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N 31 ;3 81.241;5 331PF29/5 29/9
2-3.Fkdtqoqgvjcpg!)GFD*wi0N 31 216 81.241215 231PF32/1 31/8
2-3.Fkejnqtqdgp|gpg wi0N 31 214 81.241212 331PF31/7 31/4
2-3.Fkejnqtqgvjcpg wi0N 31 218 81.241212 731PF32/5 31/3
2-3.Fkejnqtqrtqrcpg wi0N 31 219 81.241218 231PF32/7 32/6
2-5.Fkejnqtqdgp|gpg wi0N 31 213 81.241212 231PF31/6 31/3
3.Dwvcpqpg!)OGM*wi0N 51 221 81.241219 351PF55/1 54/4
3.Jgzcpqpg wi0N 51 ;;81.241212 451PF4;/7 51/7
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N 51 222 81.24121;351PF55/4 54/6
Cegvqpg wi0N 51 223 81.241218 551PF57/3 55/3
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
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)815*986.;1;3
Page 22 of 27
Rcig!43!qh!49
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;979;
L271616;3!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
OU
Tguwnv
&!Tge
Nkokvu Swcn&!TgeEqpe/
2854239OCVTKZ!URKMG!'!OCVTKZ!URKMG!FWRNKECVG<
OUUrkmg
Tguwnv
;33;97;1114
285423;
OUF
Tguwnv
OUF
&!Tge TRF
OUFOU
Urkmg
Eqpe/
Cet{nqpkvtkng wi0N 211 216 81.24121;5211PF21621;
Dgp|gpg wi0N 31 225 81.259224 231PF33/9 33/6
Dtqoqejnqtqogvjcpg wi0N 31 229 81.241223 631PF34/7 33/5
Dtqoqfkejnqtqogvjcpg wi0N 31 215 81.241214 231PF31/;31/7
Dtqoqhqto wi0N 31 94 81.24194 131PF27/6 27/7
Dtqoqogvjcpg wi0N O23122;81.241242 2131PF34/9 37/3
Ectdqp!fkuwnhkfg wi0N O23124;81.241245 531PF38/;37/9
Ectdqp!vgvtcejnqtkfg wi0N 31 233 81.241233 131PF35/6 35/5
Ejnqtqdgp|gpg wi0N 31 217 81.257217 131PF32/2 32/2
Ejnqtqgvjcpg wi0N 31 234 81.241231 331PF35/6 35/1
Ejnqtqhqto wi0N 31 225 81.24121;531PF33/9 32/9
Ejnqtqogvjcpg wi0N 31 235 81.241235 231PF35/;35/8
eku.2-3.Fkejnqtqgvjgpg wi0N 31 233 81.24122;331PF35/5 34/9
eku.2-4.Fkejnqtqrtqrgpg wi0N 31 216 81.241214 431PF32/2 31/6
Fkdtqoqejnqtqogvjcpg wi0N 31 ;3 81.241;3 131PF29/6 29/6
Fkdtqoqogvjcpg wi0N 31 216 81.241212 531PF32/2 31/3
Gvj{ndgp|gpg wi0N 31 219 81.241217 331PF32/7 32/3
Kqfqogvjcpg wi0N 51 212 81.241238 3451PF51/4 61/9
o'r.Z{ngpg wi0N 51 215 81.241215 151PF52/7 52/7
Ogvj{ngpg!Ejnqtkfg wi0N 31 225 81.241219 631PF34/2 33/1
q.Z{ngpg wi0N 31 213 81.241213 231PF31/4 31/6
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Vgvtcejnqtqgvjgpg wi0N 31 216 81.241216 13124/4 45/3 45/5
Vqnwgpg wi0N 31 226 81.266224 331PF34/1 33/7
vtcpu.2-3.Fkejnqtqgvjgpg wi0N 31 23;81.241236 431PF36/9 36/2
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N 31 211 81.241;9 331PF2;/;2;/6
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N 31 85 81.24187 331PF25/9 26/2
Vtkejnqtqgvjgpg wi0N 31 226 7;.262223 431PF34/1 33/4
Vtkejnqtqhnwqtqogvjcpg wi0N 31 223 81.241222 231PF33/5 33/4
Xkp{n!cegvcvg wi0N 51 ;7 81.241;2 651PF49/4 47/4
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5.Dtqoqhnwqtqdgp|gpg!)U*&;6 81.241;9
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REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
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$?SN$
QUALIFIERS
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DEFINITIONS
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PF!.!Pqv!Fgvgevgf!cv!qt!cdqxg!cflwuvgf!tgrqtvkpi!nkokv/
L!.!Guvkocvgf!eqpegpvtcvkqp!cdqxg!vjg!cflwuvgf!ogvjqf!fgvgevkqp!nkokv!cpf!dgnqy!vjg!cflwuvgf!tgrqtvkpi!nkokv/
OFN!.!Cflwuvgf!Ogvjqf!Fgvgevkqp!Nkokv/
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TN!.!Tgrqtvkpi!Nkokv/
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c!eqodkpgf!eqpegpvtcvkqp/
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NEU)F*!.!Ncdqtcvqt{!Eqpvtqn!Ucorng!)Fwrnkecvg*
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Cekf!rtgugtxcvkqp!oc{!pqv!dg!crrtqrtkcvg!hqt!3!Ejnqtqgvj{nxkp{n!gvjgt-!Uv{tgpg-!cpf!Xkp{n!ejnqtkfg/
C!ugrctcvg!xkcn!rtgugtxgf!vq!c!rJ!qh!5.6!ku!tgeqoogpfgf!kp!UY957!Ejcrvgt!5!hqt!vjg!cpcn{uku!qh!Cetqngkp!cpf!Cet{nqpkvtkng!d{!GRC
Ogvjqf!9371/
P.Pkvtquqfkrjgp{ncokpg!fgeqorqugu!cpf!ecppqv!dg!ugrctcvgf!htqo!Fkrjgp{ncokpg!wukpi!Ogvjqf!9381/!!Vjg!tguwnv!tgrqtvgf!hqtgcej!cpcn{vg!ku!c!eqodkpgf!eqpegpvtcvkqp/
Rceg!Cpcn{vkecn!ku!VPK!ceetgfkvgf/!Eqpvcev!{qwt!Rceg!RO!hqt!vjg!ewttgpv!nkuv!qh!ceetgfkvgf!cpcn{vgu/
VPK!.!Vjg!PGNCE!Kpuvkvwvg/
LABORATORIES
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ANALYTE QUALIFIERS
Ocvtkz!urkmg!tgeqxgt{!gzeggfgf!SE!nkokvu/!!Dcvej!ceegrvgf!dcugf!qp!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!tgeqxgt{/O2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
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$?ET$
QUALITY CONTROL DATA CROSS REFERENCE TABLE
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Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92298689001 OUX0481232016014567 DP-17 GRC!9371
92298689002 OUX0481232016014568 DP-18 GRC!9371
92298689003 OUX0481232016014569 DP-19 GRC!9371
92298689004 OUX0481232016014570 DP-1 GRC!9371
92298689005 OUX0481232016014571 DP-2 GRC!9371
92298689006 OUX0481232016014572 DP-3 GRC!9371
92298689007 OUX0481232016014573 DP-4 GRC!9371
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1603803127!15<24!RO
Pace Analytical Services, Inc.
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Page 25 of 27
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Page 26 of 27
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Page 27 of 27
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oquv!ewttgpv!VPK!uvcpfctfu!cpf!vjg!ncdqtcvqt{(u!Swcnkv{!Cuuwtcpeg!Ocpwcn-!yjgtg!crrnkecdng-!wpnguu
qvjgtykug!pqvgf!kp!vjg!dqf{!qh!vjg!tgrqtv/
Cpcn{ugu!ygtg!rgthqtogf!cv!vjg!Rceg!Cpcn{vkecn!Ugtxkegu!nqecvkqp!kpfkecvgf!qp!vjg!ucorng!cpcn{vg
rcig!hqt!cpcn{uku!wpnguu!qvjgtykug!hqqvpqvgf/
RTQLGEV!TGXKUGF!7032027!.!UCORNG!KF(U!EJCPIGF!CV!ENKGPV!TGSWGUV
Kh!{qw!jcxg!cp{!swguvkqpu!eqpegtpkpi!vjku!tgrqtv-!rngcug!hggn!htgg!vq!eqpvcev!og/
Ukpegtgn{-
Mgxkp!Jgttkpi
mgxkp/jgttkpiBrcegncdu/eqo
JQTK\QP!Fcvcdcug!Cfokpkuvtcvqt
Gpenquwtgu
ee< Tkejctf!Dqpfu
Rtqitco!Ocpcigt-!Fwmg!Gpgti{
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 1 of 44
27!qh!71
$?ER$
CERTIFICATIONS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Charlotte Certification IDs
;911!Mkpeg{!Cxg/!Uvg!211-!Jwpvgtuxknng-!PE!39189
Pqtvj!Ectqnkpc!Ftkpmkpi!Ycvgt!Egtvkhkecvkqp!$<!48817
Pqtvj!Ectqnkpc!Hkgnf!Ugtxkegu!Egtvkhkecvkqp!$<!6453
Pqtvj!Ectqnkpc!Ycuvgycvgt!Egtvkhkecvkqp!$<!23
Uqwvj!Ectqnkpc!Egtvkhkecvkqp!$<!;;117112
Hnqtkfc0PGNCR!Egtvkhkecvkqp!$<!G98738
Mgpvwem{!WUV!Egtvkhkecvkqp!$<!95
Xktikpkc0XGNCR!Egtvkhkecvkqp!$<!571332
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 2 of 44
28!qh!71
$?UC$
SAMPLE ANALYTE COUNT
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92299441001 2016015254 DP-14 GRC!9371 5;RCUK.EPD
92299441002 2016015255 DP-15 GRC!9371 5;RCUK.EPD
92299441003 2016015256 DP-16 GRC!9371 5;RCUK.EPD
92299441004 2016015257 DP-20 GRC!9371 5;RCUK.EPD
92299441005 2016015258 DP-21 GRC!9371 5;RCUK.EPD
92299441006 2016015259 DP-22 GRC!9371 5;RCUK.EPD
92299441007 2016015260 DP-23 GRC!9371 5;RCUK.EPD
92299441008 2016015261 DP-24 GRC!9371 5;RCUK.EPD
92299441009 2016015262 DP-26 GRC!9371 5;RCUK.EPD
92299441010 2016015263 DP-25 GRC!9371 5;RCUK.EPD
92299441011 2016015264 DP-27 GRC!9371 5;RCUK.EPD
92299441012 2016015265 DP-28 GRC!9371 5;RCUK.EPD
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 3 of 44
29!qh!71
$?JQ$
SUMMARY OF DETECTION
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Rctcogvgtu Cpcn{|gfTguwnv
Ncd!Ucorng!KF!
Tgrqtv!Nkokv SwcnkhkgtuWpkvuOgvjqf
Enkgpv!Ucorng!KF
92299441002 2016015255 DP-15
Vqnwgpg 2/8 wi0N 17012027!17<13 E92/1GRC!9371
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 4 of 44
2;!qh!71
$?PC$
PROJECT NARRATIVE
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Method:
Client:Fwmg!Gpgti{
EPA 8260
Date:Lwpg!32-!3127
Description:9371!OUX!Nqy!Ngxgn
General Information:
23!ucorngu!ygtg!cpcn{|gf!hqt!GRC!9371/!!Cnn!ucorngu!ygtg!tgegkxgf!kp!ceegrvcdng!eqpfkvkqp!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy!qt!qp!vjg
ejckp.qh!ewuvqf{!cpf0qt!vjg!ucorng!eqpfkvkqp!wrqp!tgegkrv!hqto!)UEWT*!cvvcejgf!cv!vjg!gpf!qh!vjku!tgrqtv/
Hold Time:
Vjg!ucorngu!ygtg!cpcn{|gf!ykvjkp!vjg!ogvjqf!tgswktgf!jqnf!vkogu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Initial Calibrations (including MS Tune as applicable):
Cnn!etkvgtkc!ygtg!ykvjkp!ogvjqf!tgswktgogpvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Continuing Calibration:
Cnn!etkvgtkc!ygtg!ykvjkp!ogvjqf!tgswktgogpvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Internal Standards:
Cnn!kpvgtpcn!uvcpfctfu!ygtg!ykvjkp!SE!nkokvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Surrogates:
Cnn!uwttqicvgu!ygtg!ykvjkp!SE!nkokvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Method Blank:
Cnn!cpcn{vgu!ygtg!dgnqy!vjg!tgrqtv!nkokv!kp!vjg!ogvjqf!dncpm-!yjgtg!crrnkecdng-!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Laboratory Control Spike:
Cnn!ncdqtcvqt{!eqpvtqn!urkmg!eqorqwpfu!ygtg!ykvjkp!SE!nkokvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
SE!Dcvej<!OUX0481;8
N1<!Cpcn{vg!tgeqxgt{!kp!vjg!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!ycu!qwvukfg!SE!nkokvu/
—!NEU!!)Ncd!KF<!2857613*
—!Dtqoqogvjcpg
—!vtcpu.2-5.Fkejnqtq.3.dwvgpg
Matrix Spikes:
Cnn!rgtegpv!tgeqxgtkgu!cpf!tgncvkxg!rgtegpv!fkhhgtgpegu!)TRFu*!ygtg!ykvjkp!ceegrvcpeg!etkvgtkc!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
SE!Dcvej<!OUX048191
C!ocvtkz!urkmg!cpf0qt!ocvtkz!urkmg!fwrnkecvg!)OU0OUF*!ygtg!rgthqtogf!qp!vjg!hqnnqykpi!ucorng)u*<!!;33;;552116
O2<!Ocvtkz!urkmg!tgeqxgt{!gzeggfgf!SE!nkokvu/!!Dcvej!ceegrvgf!dcugf!qp!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!tgeqxgt{/
—!OU!!)Ncd!KF<!2857252*
—!2-2-2.Vtkejnqtqgvjcpg
—!3.Jgzcpqpg
—!5.Ogvj{n.3.rgpvcpqpg!)OKDM*
—!Dtqoqogvjcpg
—!Ectdqp!fkuwnhkfg
—!Ectdqp!vgvtcejnqtkfg
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 5 of 44
31!qh!71
$?PC$
PROJECT NARRATIVE
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Method:
Client:Fwmg!Gpgti{
EPA 8260
Date:Lwpg!32-!3127
Description:9371!OUX!Nqy!Ngxgn
SE!Dcvej<!OUX048191
C!ocvtkz!urkmg!cpf0qt!ocvtkz!urkmg!fwrnkecvg!)OU0OUF*!ygtg!rgthqtogf!qp!vjg!hqnnqykpi!ucorng)u*<!!;33;;552116
O2<!Ocvtkz!urkmg!tgeqxgt{!gzeggfgf!SE!nkokvu/!!Dcvej!ceegrvgf!dcugf!qp!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!tgeqxgt{/
—!Ejnqtqgvjcpg
—!Ejnqtqogvjcpg
—!Uv{tgpg
—!Vtkejnqtqhnwqtqogvjcpg
—!Xkp{n!ejnqtkfg
—!eku.2-3.Fkejnqtqgvjgpg
—!vtcpu.2-3.Fkejnqtqgvjgpg
SE!Dcvej<!OUX0481;8
C!ocvtkz!urkmg!cpf0qt!ocvtkz!urkmg!fwrnkecvg!)OU0OUF*!ygtg!rgthqtogf!qp!vjg!hqnnqykpi!ucorng)u*<!!;33;;32;116
O1<!Ocvtkz!urkmg!tgeqxgt{!cpf0qt!ocvtkz!urkmg!fwrnkecvg!tgeqxgt{!ycu!qwvukfg!ncdqtcvqt{!eqpvtqn!nkokvu/
—!OU!!)Ncd!KF<!2857614*
—!Dtqoqogvjcpg
O2<!Ocvtkz!urkmg!tgeqxgt{!gzeggfgf!SE!nkokvu/!!Dcvej!ceegrvgf!dcugf!qp!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!tgeqxgt{/
—!OU!!)Ncd!KF<!2857614*
—!2-2-2-3.Vgvtcejnqtqgvjcpg
—!2-2-2.Vtkejnqtqgvjcpg
—!2-2-3.Vtkejnqtqgvjcpg
—!2-2.Fkejnqtqgvjcpg
—!2-3.Fkdtqoq.4.ejnqtqrtqrcpg
—!2-3.Fkdtqoqgvjcpg!)GFD*
—!2-3.Fkejnqtqdgp|gpg
—!2-3.Fkejnqtqgvjcpg
—!2-5.Fkejnqtqdgp|gpg
—!Dtqoqejnqtqogvjcpg
—!Dtqoqfkejnqtqogvjcpg
—!Ectdqp!vgvtcejnqtkfg
—!Ejnqtqgvjcpg
—!Ejnqtqhqto
—!Ejnqtqogvjcpg
—!Fkdtqoqogvjcpg
—!Gvj{ndgp|gpg
—!Ogvj{ngpg!Ejnqtkfg
—!Uv{tgpg
—!Vtkejnqtqhnwqtqogvjcpg
—!Xkp{n!ejnqtkfg
—!eku.2-3.Fkejnqtqgvjgpg
—!o'r.Z{ngpg
—!q.Z{ngpg
—!vtcpu.2-3.Fkejnqtqgvjgpg
—!OUF!!)Ncd!KF<!2857615*
—!Ectdqp!fkuwnhkfg
—!Vtkejnqtqhnwqtqogvjcpg
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 6 of 44
32!qh!71
$?PC$
PROJECT NARRATIVE
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Method:
Client:Fwmg!Gpgti{
EPA 8260
Date:Lwpg!32-!3127
Description:9371!OUX!Nqy!Ngxgn
SE!Dcvej<!OUX0481;8
C!ocvtkz!urkmg!cpf0qt!ocvtkz!urkmg!fwrnkecvg!)OU0OUF*!ygtg!rgthqtogf!qp!vjg!hqnnqykpi!ucorng)u*<!!;33;;32;116
T2<!TRF!xcnwg!ycu!qwvukfg!eqpvtqn!nkokvu/
—!OUF!!)Ncd!KF<!2857615*
—!Kqfqogvjcpg
Duplicate Sample:
Cnn!fwrnkecvg!ucorng!tguwnvu!ygtg!ykvjkp!ogvjqf!ceegrvcpeg!etkvgtkc!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Additional Comments:
Cpcn{vg!Eqoogpvu<
SE!Dcvej<!OUX048191
2i<!Enkgpv!rtqxkfgf!4!xkcnu/!!Cnn!4!xkcnu!ygtg!61&!uqkn/!!Jcf!vq!eqodkpg!3!xkcnu!kpvq!2!xkcn!vq!jcxg!gpqwij!xqnwog!hqt!c!2z!twp/!!Vjku
twp!eqpvckpgf!ectt{qxgt!hqt!vqnwgpg/!!Ecppqv!rtghqto!eqttgevkxg!cevkqp!)tgtwp!2z!*!dgecwug!vjg!tgockpkpi!xkcn!jcu!vqq!owej!uqkn/
Vjgtghqtg-!tgrqtvgf!twp!yknn!jcxg!crrtqrtkcvg!ectt{qxgt!hnci!qp!vqnwgpg/
—!3127126366!FR.26!!)Ncd!KF<!;33;;552113*
—!5.Dtqoqhnwqtqdgp|gpg!)U*
E9<!Tguwnv!oc{!dg!dkcugf!jkij!fwg!vq!ectt{qxgt!htqo!rtgxkqwun{!cpcn{|gf!ucorng/
—!3127126366!FR.26!!)Ncd!KF<!;33;;552113*
—!Vqnwgpg
Vjku!fcvc!rcemcig!jcu!dggp!tgxkgygf!hqt!swcnkv{!cpf!eqorngvgpguu!cpf!ku!crrtqxgf!hqt!tgngcug/
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 7 of 44
33!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015254 DP-14 Lab ID: 92299441001 Eqnngevgf< 16035027!26<21 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!31<25 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!31<25 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!31<25 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!31<25 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!31<25 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!31<25 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!31<25 85.94.;N43/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!31<25 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!31<25 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!31<25 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!31<25 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!31<25 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!31<25 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!31<25 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!31<25 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!31<25 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!31<25 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!31<25 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!31<25 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!31<25 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!31<25 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!31<25 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!31<25 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!31<25 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!31<25 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!31<25 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!31<25 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!31<25 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!31<25 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!31<25 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!31<25 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!31<25 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!31<25 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!31<25 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!31<25 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!31<25 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!31<25 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!31<25 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!31<25 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!31<25 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!31<25 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!31<25 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!31<25 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!31<25 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!31<25 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!31<25 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 8 of 44
34!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015254 DP-14 Lab ID: 92299441001 Eqnngevgf< 16035027!26<21 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;9 &17012027!31<25 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*212 &17012027!31<25 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &17012027!31<25 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 9 of 44
35!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015255 DP-15 Lab ID: 92299441002 Eqnngevgf< 16035027!27<36 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!17<13 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!17<13 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!17<13 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!17<13 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!17<13 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!17<13 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!17<13 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!17<13 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!17<13 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!17<13 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!17<13 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!17<13 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!17<13 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!17<13 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!17<13 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!17<13 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!17<13 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!17<13 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!17<13 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!17<13 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!17<13 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!17<13 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!17<13 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!17<13 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!17<13 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!17<13 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!17<13 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!17<13 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!17<13 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!17<13 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!17<13 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!17<13 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!17<13 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!17<13 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!17<13 238.29.52/1 2
Vqnwgpg 1.7 wi0N 17012027!17<13 219.99.4 E92/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!17<13 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!17<13 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!17<13 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!17<13 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!17<13 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!17<13 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!17<13 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!17<13 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!17<13 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!17<13 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 10 of 44
36!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015255 DP-15 Lab ID: 92299441002 Eqnngevgf< 16035027!27<36 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;;&17012027!17<13 571.11.5 2i81.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*215 &17012027!17<13 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &17012027!17<13 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 11 of 44
37!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015256 DP-16 Lab ID: 92299441003 Eqnngevgf< 16035027!28<31 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!31<42 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!31<42 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!31<42 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!31<42 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!31<42 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!31<42 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!31<42 85.94.;N43/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!31<42 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!31<42 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!31<42 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!31<42 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!31<42 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!31<42 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!31<42 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!31<42 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!31<42 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!31<42 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!31<42 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!31<42 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!31<42 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!31<42 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!31<42 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!31<42 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!31<42 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!31<42 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!31<42 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!31<42 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!31<42 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!31<42 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!31<42 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!31<42 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!31<42 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!31<42 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!31<42 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!31<42 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!31<42 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!31<42 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!31<42 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!31<42 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!31<42 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!31<42 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!31<42 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!31<42 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!31<42 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!31<42 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!31<42 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 12 of 44
38!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015256 DP-16 Lab ID: 92299441003 Eqnngevgf< 16035027!28<31 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;8 &17012027!31<42 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*211 &17012027!31<42 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &17012027!31<42 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 13 of 44
39!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015257 DP-20 Lab ID: 92299441004 Eqnngevgf< 16035027!21<16 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!31<59 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!31<59 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!31<59 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!31<59 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!31<59 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!31<59 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!31<59 85.94.;N43/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!31<59 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!31<59 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!31<59 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!31<59 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!31<59 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!31<59 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!31<59 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!31<59 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!31<59 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!31<59 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!31<59 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!31<59 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!31<59 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!31<59 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!31<59 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!31<59 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!31<59 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!31<59 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!31<59 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!31<59 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!31<59 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!31<59 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!31<59 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!31<59 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!31<59 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!31<59 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!31<59 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!31<59 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!31<59 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!31<59 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!31<59 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!31<59 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!31<59 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!31<59 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!31<59 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!31<59 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!31<59 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!31<59 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!31<59 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 14 of 44
3;!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015257 DP-20 Lab ID: 92299441004 Eqnngevgf< 16035027!21<16 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;;&17012027!31<59 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*;;&17012027!31<59 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &17012027!31<59 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 15 of 44
41!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015258 DP-21 Lab ID: 92299441005 Eqnngevgf< 16035027!22<26 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!18<21 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!18<21 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!18<21 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!18<21 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!18<21 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!18<21 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!18<21 85.94.;O23/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!18<21 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!18<21 86.26.1 O23/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!18<21 67.34.6 O22/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!18<21 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!18<21 86.11.4 O22/1 2
Ejnqtqhqto <1.0 wi0N 17012027!18<21 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!18<21 85.98.4 O22/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!18<21 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!18<21 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!18<21 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!18<21 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!18<21 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!18<21 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!18<21 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!18<21 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!18<21 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!18<21 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!18<21 267.6;.3 O22/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!18<21 267.71.6 O22/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!18<21 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!18<21 6;2.89.7 O26/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!18<21 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!18<21 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!18<21 219.21.2 O26/1 2
Uv{tgpg <1.0 wi0N 17012027!18<21 211.53.6 O22/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!18<21 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!18<21 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!18<21 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!18<21 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!18<21 82.66.7 O22/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!18<21 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!18<21 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!18<21 86.7;.5 O22/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!18<21 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!18<21 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!18<21 86.12.5 O22/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!18<21 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!18<21 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!18<21 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 16 of 44
42!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015258 DP-21 Lab ID: 92299441005 Eqnngevgf< 16035027!22<26 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*212 &17012027!18<21 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*213 &17012027!18<21 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &17012027!18<21 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 17 of 44
43!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015259 DP-22 Lab ID: 92299441006 Eqnngevgf< 16035027!24<36 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!18<38 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!18<38 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!18<38 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!18<38 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!18<38 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!18<38 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!18<38 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!18<38 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!18<38 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!18<38 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!18<38 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!18<38 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!18<38 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!18<38 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!18<38 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!18<38 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!18<38 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!18<38 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!18<38 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!18<38 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!18<38 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!18<38 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!18<38 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!18<38 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!18<38 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!18<38 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!18<38 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!18<38 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!18<38 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!18<38 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!18<38 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!18<38 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!18<38 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!18<38 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!18<38 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!18<38 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!18<38 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!18<38 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!18<38 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!18<38 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!18<38 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!18<38 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!18<38 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!18<38 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!18<38 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!18<38 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 18 of 44
44!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015259 DP-22 Lab ID: 92299441006 Eqnngevgf< 16035027!24<36 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;;&17012027!18<38 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*214 &17012027!18<38 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &17012027!18<38 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 19 of 44
45!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015260 DP-23 Lab ID: 92299441007 Eqnngevgf< 16035027!25<36 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!18<56 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!18<56 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!18<56 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!18<56 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!18<56 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!18<56 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!18<56 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!18<56 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!18<56 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!18<56 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!18<56 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!18<56 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!18<56 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!18<56 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!18<56 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!18<56 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!18<56 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!18<56 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!18<56 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!18<56 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!18<56 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!18<56 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!18<56 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!18<56 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!18<56 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!18<56 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!18<56 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!18<56 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!18<56 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!18<56 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!18<56 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!18<56 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!18<56 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!18<56 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!18<56 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!18<56 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!18<56 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!18<56 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!18<56 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!18<56 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!18<56 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!18<56 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!18<56 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!18<56 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!18<56 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!18<56 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 20 of 44
46!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015260 DP-23 Lab ID: 92299441007 Eqnngevgf< 16035027!25<36 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*211 &17012027!18<56 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*212 &17012027!18<56 28171.18.181.241 2
Vqnwgpg.f9!)U*213 &17012027!18<56 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 21 of 44
47!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015261 DP-24 Lab ID: 92299441008 Eqnngevgf< 16035027!26<46 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!19<13 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!19<13 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!19<13 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!19<13 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!19<13 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!19<13 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!19<13 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!19<13 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!19<13 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!19<13 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!19<13 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!19<13 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!19<13 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!19<13 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!19<13 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!19<13 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!19<13 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!19<13 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!19<13 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!19<13 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!19<13 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!19<13 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!19<13 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<13 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<13 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<13 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!19<13 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!19<13 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!19<13 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!19<13 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!19<13 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!19<13 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!19<13 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!19<13 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!19<13 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!19<13 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!19<13 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!19<13 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!19<13 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!19<13 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!19<13 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!19<13 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!19<13 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!19<13 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!19<13 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!19<13 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 22 of 44
48!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015261 DP-24 Lab ID: 92299441008 Eqnngevgf< 16035027!26<46 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*211 &17012027!19<13 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*214 &17012027!19<13 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &17012027!19<13 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 23 of 44
49!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015262 DP-26 Lab ID: 92299441009 Eqnngevgf< 16035027!27<56 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!19<2; 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!19<2; 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!19<2; 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!19<2; 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!19<2; 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!19<2; 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!19<2; 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!19<2; 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!19<2; 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!19<2; 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!19<2; 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!19<2; 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!19<2; 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!19<2; 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!19<2; ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!19<2; 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!19<2; 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!19<2; 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!19<2; ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!19<2; 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!19<2; 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!19<2; 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!19<2; 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<2; 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<2; 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<2; 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!19<2; 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!19<2; 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!19<2; 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!19<2; 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!19<2; 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!19<2; 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!19<2; 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!19<2; 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!19<2; 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!19<2; 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!19<2; 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!19<2; 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!19<2; 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!19<2; 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!19<2; ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!19<2; 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!19<2; 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!19<2; 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!19<2; 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!19<2; ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 24 of 44
4;!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015262 DP-26 Lab ID: 92299441009 Eqnngevgf< 16035027!27<56 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*212 &17012027!19<2; 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*214 &17012027!19<2; 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &17012027!19<2; 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 25 of 44
51!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015263 DP-25 Lab ID: 92299441010 Eqnngevgf< 16035027!23<11 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!19<47 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!19<47 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!19<47 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!19<47 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!19<47 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!19<47 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!19<47 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!19<47 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!19<47 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!19<47 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!19<47 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!19<47 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!19<47 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!19<47 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!19<47 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!19<47 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!19<47 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!19<47 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!19<47 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!19<47 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!19<47 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!19<47 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!19<47 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<47 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<47 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<47 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!19<47 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!19<47 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!19<47 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!19<47 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!19<47 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!19<47 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!19<47 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!19<47 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!19<47 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!19<47 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!19<47 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!19<47 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!19<47 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!19<47 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!19<47 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!19<47 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!19<47 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!19<47 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!19<47 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!19<47 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 26 of 44
52!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015263 DP-25 Lab ID: 92299441010 Eqnngevgf< 16035027!23<11 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*211 &17012027!19<47 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*213 &17012027!19<47 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &17012027!19<47 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 27 of 44
53!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015264 DP-27 Lab ID: 92299441011 Eqnngevgf< 16035027!25<46 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!19<64 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!19<64 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!19<64 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!19<64 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!19<64 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!19<64 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!19<64 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!19<64 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!19<64 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!19<64 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!19<64 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!19<64 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!19<64 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!19<64 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!19<64 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!19<64 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!19<64 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!19<64 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!19<64 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!19<64 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!19<64 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!19<64 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!19<64 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<64 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<64 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!19<64 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!19<64 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!19<64 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!19<64 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!19<64 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!19<64 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!19<64 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!19<64 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!19<64 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!19<64 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!19<64 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!19<64 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!19<64 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!19<64 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!19<64 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!19<64 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!19<64 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!19<64 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!19<64 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!19<64 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!19<64 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 28 of 44
54!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015264 DP-27 Lab ID: 92299441011 Eqnngevgf< 16035027!25<46 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*212 &17012027!19<64 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*212 &17012027!19<64 28171.18.181.241 2
Vqnwgpg.f9!)U*212 &17012027!19<64 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 29 of 44
55!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015265 DP-28 Lab ID: 92299441012 Eqnngevgf< 16035027!26<46 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 17012027!1;<21 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 17012027!1;<21 218.24.221/1 2
Dgp|gpg <1.0 wi0N 17012027!1;<21 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 17012027!1;<21 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 17012027!1;<21 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 17012027!1;<21 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 17012027!1;<21 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 17012027!1;<21 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 17012027!1;<21 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 17012027!1;<21 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 17012027!1;<21 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 17012027!1;<21 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 17012027!1;<21 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 17012027!1;<21 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 17012027!1;<21 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 17012027!1;<21 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 17012027!1;<21 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 17012027!1;<21 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!1;<21 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 17012027!1;<21 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 17012027!1;<21 221.68.72/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 17012027!1;<21 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 17012027!1;<21 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 17012027!1;<21 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!1;<21 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 17012027!1;<21 267.71.62/1 2
Gvj{ndgp|gpg <1.0 wi0N 17012027!1;<21 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 17012027!1;<21 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 17012027!1;<21 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 17012027!1;<21 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 17012027!1;<21 219.21.26/1 2
Uv{tgpg <1.0 wi0N 17012027!1;<21 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!1;<21 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 17012027!1;<21 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 17012027!1;<21 238.29.52/1 2
Vqnwgpg <1.0 wi0N 17012027!1;<21 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!1;<21 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 17012027!1;<21 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 17012027!1;<21 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 17012027!1;<21 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 17012027!1;<21 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 17012027!1;<21 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 17012027!1;<21 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 17012027!1;<21 2441.31.83/1 2
o'r.Z{ngpg <2.0 wi0N 17012027!1;<21 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 17012027!1;<21 ;6.58.72/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 30 of 44
56!qh!71
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Sample: 2016015265 DP-28 Lab ID: 92299441012 Eqnngevgf< 16035027!26<46 Tgegkxgf< 16038027!25<25 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;;&17012027!1;<21 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*214 &17012027!1;<21 28171.18.181.241 2
Vqnwgpg.f9!)U*213 &17012027!1;<21 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 31 of 44
57!qh!71
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
SE!Dcvej<
SE!Dcvej!Ogvjqf<
Cpcn{uku!Ogvjqf<
Cpcn{uku!Fguetkrvkqp<
OUX048191
GRC!9371
GRC!9371
9371!OUX!Nqy!Ngxgn
Cuuqekcvgf!Ncd!Ucorngu<;33;;552113-!;33;;552116-!;33;;552117-!;33;;552118-!;33;;552119-!;33;;55211;-!;33;;552121-
;33;;552122-!;33;;552123
Rctcogvgt Wpkvu
Dncpm
Tguwnv
Tgrqtvkpi
Nkokv Swcnkhkgtu
OGVJQF!DNCPM< 2856612
Cuuqekcvgf!Ncd!Ucorngu< ;33;;552113-!;33;;552116-!;33;;552117-!;33;;552118-!;33;;552119-!;33;;55211;-!;33;;552121-
;33;;552122-!;33;;552123
Ocvtkz< Ycvgt
Cpcn{|gf
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N >2/1 2/1 16042027!34<58
2-2-2.Vtkejnqtqgvjcpg wi0N >2/1 2/1 16042027!34<58
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N >2/1 2/1 16042027!34<58
2-2-3.Vtkejnqtqgvjcpg wi0N >2/1 2/1 16042027!34<58
2-2.Fkejnqtqgvjcpg wi0N >2/1 2/1 16042027!34<58
2-2.Fkejnqtqgvjgpg wi0N >2/1 2/1 16042027!34<58
2-3-4.Vtkejnqtqrtqrcpg wi0N >2/1 2/1 16042027!34<58
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N >3/1 3/1 16042027!34<58
2-3.Fkdtqoqgvjcpg!)GFD*wi0N >2/1 2/1 16042027!34<58
2-3.Fkejnqtqdgp|gpg wi0N >2/1 2/1 16042027!34<58
2-3.Fkejnqtqgvjcpg wi0N >2/1 2/1 16042027!34<58
2-5.Fkejnqtqdgp|gpg wi0N >2/1 2/1 16042027!34<58
3.Dwvcpqpg!)OGM*wi0N >6/1 6/1 16042027!34<58
3.Jgzcpqpg wi0N >6/1 6/1 16042027!34<58
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N >6/1 6/1 16042027!34<58
Cegvqpg wi0N >36/1 36/1 16042027!34<58
Cet{nqpkvtkng wi0N >21/1 21/1 16042027!34<58
Dgp|gpg wi0N >2/1 2/1 16042027!34<58
Dtqoqejnqtqogvjcpg wi0N >2/1 2/1 16042027!34<58
Dtqoqfkejnqtqogvjcpg wi0N >2/1 2/1 16042027!34<58
Dtqoqhqto wi0N >2/1 2/1 16042027!34<58
Dtqoqogvjcpg wi0N >3/1 3/1 16042027!34<58
Ectdqp!fkuwnhkfg wi0N >3/1 3/1 16042027!34<58
Ectdqp!vgvtcejnqtkfg wi0N >2/1 2/1 16042027!34<58
Ejnqtqdgp|gpg wi0N >2/1 2/1 16042027!34<58
Ejnqtqgvjcpg wi0N >2/1 2/1 16042027!34<58
Ejnqtqhqto wi0N >2/1 2/1 16042027!34<58
Ejnqtqogvjcpg wi0N >2/1 2/1 16042027!34<58
eku.2-3.Fkejnqtqgvjgpg wi0N >2/1 2/1 16042027!34<58
Fkdtqoqejnqtqogvjcpg wi0N >2/1 2/1 16042027!34<58
Fkdtqoqogvjcpg wi0N >2/1 2/1 16042027!34<58
Gvj{ndgp|gpg wi0N >2/1 2/1 16042027!34<58
Kqfqogvjcpg wi0N >6/1 6/1 16042027!34<58
o'r.Z{ngpg wi0N >3/1 3/1 16042027!34<58
Ogvj{ngpg!Ejnqtkfg wi0N >3/1 3/1 16042027!34<58
q.Z{ngpg wi0N >2/1 2/1 16042027!34<58
Uv{tgpg wi0N >2/1 2/1 16042027!34<58
Vgvtcejnqtqgvjgpg wi0N >2/1 2/1 16042027!34<58
Vqnwgpg wi0N >2/1 2/1 16042027!34<58
vtcpu.2-3.Fkejnqtqgvjgpg wi0N >2/1 2/1 16042027!34<58
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 32 of 44
58!qh!71
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
Dncpm
Tguwnv
Tgrqtvkpi
Nkokv Swcnkhkgtu
OGVJQF!DNCPM< 2856612
Cuuqekcvgf!Ncd!Ucorngu< ;33;;552113-!;33;;552116-!;33;;552117-!;33;;552118-!;33;;552119-!;33;;55211;-!;33;;552121-
;33;;552122-!;33;;552123
Ocvtkz< Ycvgt
Cpcn{|gf
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N >2/1 2/1 16042027!34<58
Vtkejnqtqgvjgpg wi0N >2/1 2/1 16042027!34<58
Vtkejnqtqhnwqtqogvjcpg wi0N >2/1 2/1 16042027!34<58
Xkp{n!cegvcvg wi0N >3/1 3/1 16042027!34<58
Xkp{n!ejnqtkfg wi0N >2/1 2/1 16042027!34<58
Z{ngpg!)Vqvcn*wi0N >3/1 3/1 16042027!34<58
2-3.Fkejnqtqgvjcpg.f5!)U*&213 81.241 16042027!34<58
5.Dtqoqhnwqtqdgp|gpg!)U*&;;81.241 16042027!34<58
Vqnwgpg.f9!)U*&;;81.241 16042027!34<58
Rctcogvgt Wpkvu
NEU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2856613NCDQTCVQT[!EQPVTQN!UCORNG<
NEUUrkmg
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N 35/736 ;9 81.241
2-2-2.Vtkejnqtqgvjcpg wi0N 37/;36 219 81.241
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N 35/236 ;7 81.241
2-2-3.Vtkejnqtqgvjcpg wi0N 37/436 216 81.241
2-2.Fkejnqtqgvjcpg wi0N 37/236 215 81.241
2-2.Fkejnqtqgvjgpg wi0N 37/436 216 81.243
2-3-4.Vtkejnqtqrtqrcpg wi0N 35/;36 ;;81.241
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N 34/636 ;5 81.241
2-3.Fkdtqoqgvjcpg!)GFD*wi0N 37/836 218 81.241
2-3.Fkejnqtqdgp|gpg wi0N 37/636 217 81.241
2-3.Fkejnqtqgvjcpg wi0N 37/136 215 81.241
2-5.Fkejnqtqdgp|gpg wi0N 35/336 ;8 81.241
3.Dwvcpqpg!)OGM*wi0N 69/861 228 81.256
3.Jgzcpqpg wi0N 64/261 217 81.255
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N 67/561 224 81.251
Cegvqpg wi0N 71/961 233 61.286
Cet{nqpkvtkng wi0N 242236 216 81.254
Dgp|gpg wi0N 36/736 214 81.241
Dtqoqejnqtqogvjcpg wi0N 38/736 221 81.241
Dtqoqfkejnqtqogvjcpg wi0N 37/536 216 81.241
Dtqoqhqto wi0N 33/736 ;1 81.241
Dtqoqogvjcpg wi0N 27/836 78 65.241
Ectdqp!fkuwnhkfg wi0N 38/736 222 81.242
Ectdqp!vgvtcejnqtkfg wi0N 37/836 218 81.243
Ejnqtqdgp|gpg wi0N 36/636 213 81.241
Ejnqtqgvjcpg wi0N 35/536 ;9 75.245
Ejnqtqhqto wi0N 37/436 216 81.241
Ejnqtqogvjcpg wi0N 28/836 82 75.241
eku.2-3.Fkejnqtqgvjgpg wi0N 38/436 21;81.242
Fkdtqoqejnqtqogvjcpg wi0N 36/136 211 81.241
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 33 of 44
59!qh!71
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
NEU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2856613NCDQTCVQT[!EQPVTQN!UCORNG<
NEUUrkmg
Fkdtqoqogvjcpg wi0N 37/936 218 81.242
Gvj{ndgp|gpg wi0N 35/736 ;9 81.241
Kqfqogvjcpg wi0N 44/861 78 5;.291
o'r.Z{ngpg wi0N 59/361 ;7 81.241
Ogvj{ngpg!Ejnqtkfg wi0N 37/536 217 74.241
q.Z{ngpg wi0N 35/236 ;7 81.241
Uv{tgpg wi0N 36/836 214 81.241
Vgvtcejnqtqgvjgpg wi0N 33/336 9;81.241
Vqnwgpg wi0N 36/736 213 81.241
vtcpu.2-3.Fkejnqtqgvjgpg wi0N 38/436 21;81.241
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N 45/336 248 81.252
Vtkejnqtqgvjgpg wi0N 36/336 212 81.241
Vtkejnqtqhnwqtqogvjcpg wi0N 39/736 225 73.244
Xkp{n!cegvcvg wi0N 68/361 225 77.268
Xkp{n!ejnqtkfg wi0N 37/336 216 61.261
Z{ngpg!)Vqvcn*wi0N 83/486 ;7 81.241
2-3.Fkejnqtqgvjcpg.f5!)U*&213 81.241
5.Dtqoqhnwqtqdgp|gpg!)U*&212 81.241
Vqnwgpg.f9!)U*&213 81.241
Rctcogvgt Wpkvu
OU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2857252OCVTKZ!URKMG!UCORNG<
OUUrkmg
Tguwnv
;33;;552116
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N 35/731 234 81.241>2/1
2-2-2.Vtkejnqtqgvjcpg wi0N 37/8 O23124481.241>2/1
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N 34/931 22;81.241>2/1
2-2-3.Vtkejnqtqgvjcpg wi0N 35/631 234 81.241>2/1
2-2.Fkejnqtqgvjcpg wi0N 36/831 23;81.241>2/1
2-2.Fkejnqtqgvjgpg wi0N 39/531 253 81.277>2/1
2-3-4.Vtkejnqtqrtqrcpg wi0N 34/131 226 81.241>2/1
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N 36/131 236 81.241>3/1
2-3.Fkdtqoqgvjcpg!)GFD*wi0N 36/731 239 81.241>2/1
2-3.Fkejnqtqdgp|gpg wi0N 36/931 23;81.241>2/1
2-3.Fkejnqtqgvjcpg wi0N 34/;31 22;81.241>2/1
2-5.Fkejnqtqdgp|gpg wi0N 36/131 236 81.241>2/1
3.Dwvcpqpg!)OGM*wi0N 62/251 239 81.241>6/1
3.Jgzcpqpg wi0N 63/8 O25124381.241>6/1
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N 63/8 O25124381.241>6/1
Cegvqpg wi0N 61/;51 232 81.241>36/1
Cet{nqpkvtkng wi0N 231211 231 81.241>21/1
Dgp|gpg wi0N 36/;31 241 81.259>2/1
Dtqoqejnqtqogvjcpg wi0N 35/831 235 81.241>2/1
Dtqoqfkejnqtqogvjcpg wi0N 36/731 239 81.241>2/1
Dtqoqhqto wi0N 33/731 224 81.241>2/1
Dtqoqogvjcpg wi0N 3;/2 O23125681.241>3/1
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 34 of 44
5;!qh!71
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
OU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2857252OCVTKZ!URKMG!UCORNG<
OUUrkmg
Tguwnv
;33;;552116
Ectdqp!fkuwnhkfg wi0N 3;/1 O23125681.241>3/1
Ectdqp!vgvtcejnqtkfg wi0N 38/9 O23124;81.241>2/1
Ejnqtqdgp|gpg wi0N 37/231 242 81.257>2/1
Ejnqtqgvjcpg wi0N 39/8 O23125581.241>2/1
Ejnqtqhqto wi0N 36/531 238 81.241>2/1
Ejnqtqogvjcpg wi0N 3;/2 O23125681.241>2/1
eku.2-3.Fkejnqtqgvjgpg wi0N 37/3 O23124281.241>2/1
Fkdtqoqejnqtqogvjcpg wi0N 35/231 232 81.241>2/1
Fkdtqoqogvjcpg wi0N 35/631 234 81.241>2/1
Gvj{ndgp|gpg wi0N 37/231 241 81.241>2/1
Kqfqogvjcpg wi0N 4;/951 ;;81.241>6/1
o'r.Z{ngpg wi0N 62/751 239 81.241>3/1
Ogvj{ngpg!Ejnqtkfg wi0N 36/831 23;81.241>3/1
q.Z{ngpg wi0N 36/231 237 81.241>2/1
Uv{tgpg wi0N 37/3 O23124281.241>2/1
Vgvtcejnqtqgvjgpg wi0N 36/131 236 81.241>2/1
Vqnwgpg wi0N 37/531 23;81.266>2/1
vtcpu.2-3.Fkejnqtqgvjgpg wi0N 38/4 O23124781.241>2/1
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N 33/331 222 81.241>2/1
Vtkejnqtqgvjgpg wi0N 35/731 234 7;.262>2/1
Vtkejnqtqhnwqtqogvjcpg wi0N 43/8 O23127481.241>2/1
Xkp{n!cegvcvg wi0N 59/751 233 81.241>3/1
Xkp{n!ejnqtkfg wi0N 3;/3 O23125781.241>2/1
2-3.Fkejnqtqgvjcpg.f5!)U*&212 81.241
5.Dtqoqhnwqtqdgp|gpg!)U*&211 81.241
Vqnwgpg.f9!)U*&211 81.241
Rctcogvgt Wpkvu
Fwr
Tguwnv SwcnkhkgtuTRFTguwnv
;33;;552117
2857253UCORNG!FWRNKECVG<
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N >2/1>2/1
2-2-2.Vtkejnqtqgvjcpg wi0N >2/1>2/1
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N >2/1>2/1
2-2-3.Vtkejnqtqgvjcpg wi0N >2/1>2/1
2-2.Fkejnqtqgvjcpg wi0N >2/1>2/1
2-2.Fkejnqtqgvjgpg wi0N >2/1>2/1
2-3-4.Vtkejnqtqrtqrcpg wi0N >2/1>2/1
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N >3/1>3/1
2-3.Fkdtqoqgvjcpg!)GFD*wi0N >2/1>2/1
2-3.Fkejnqtqdgp|gpg wi0N >2/1>2/1
2-3.Fkejnqtqgvjcpg wi0N >2/1>2/1
2-5.Fkejnqtqdgp|gpg wi0N >2/1>2/1
3.Dwvcpqpg!)OGM*wi0N >6/1>6/1
3.Jgzcpqpg wi0N >6/1>6/1
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N >6/1>6/1
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 35 of 44
61!qh!71
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
Fwr
Tguwnv SwcnkhkgtuTRFTguwnv
;33;;552117
2857253UCORNG!FWRNKECVG<
Cegvqpg wi0N >36/1>36/1
Cet{nqpkvtkng wi0N >21/1>21/1
Dgp|gpg wi0N >2/1>2/1
Dtqoqejnqtqogvjcpg wi0N >2/1>2/1
Dtqoqfkejnqtqogvjcpg wi0N >2/1>2/1
Dtqoqhqto wi0N >2/1>2/1
Dtqoqogvjcpg wi0N >3/1>3/1
Ectdqp!fkuwnhkfg wi0N >3/1>3/1
Ectdqp!vgvtcejnqtkfg wi0N >2/1>2/1
Ejnqtqdgp|gpg wi0N >2/1>2/1
Ejnqtqgvjcpg wi0N >2/1>2/1
Ejnqtqhqto wi0N >2/1>2/1
Ejnqtqogvjcpg wi0N >2/1>2/1
eku.2-3.Fkejnqtqgvjgpg wi0N >2/1>2/1
Fkdtqoqejnqtqogvjcpg wi0N >2/1>2/1
Fkdtqoqogvjcpg wi0N >2/1>2/1
Gvj{ndgp|gpg wi0N >2/1>2/1
Kqfqogvjcpg wi0N >6/1>6/1
o'r.Z{ngpg wi0N >3/1>3/1
Ogvj{ngpg!Ejnqtkfg wi0N >3/1>3/1
q.Z{ngpg wi0N >2/1>2/1
Uv{tgpg wi0N >2/1>2/1
Vgvtcejnqtqgvjgpg wi0N >2/1>2/1
Vqnwgpg wi0N >2/1>2/1
vtcpu.2-3.Fkejnqtqgvjgpg wi0N >2/1>2/1
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N >2/1>2/1
Vtkejnqtqgvjgpg wi0N >2/1>2/1
Vtkejnqtqhnwqtqogvjcpg wi0N >2/1>2/1
Xkp{n!cegvcvg wi0N >3/1>3/1
Xkp{n!ejnqtkfg wi0N >2/1>2/1
Z{ngpg!)Vqvcn*wi0N >3/1>3/1
2-3.Fkejnqtqgvjcpg.f5!)U*&212 3214
5.Dtqoqhnwqtqdgp|gpg!)U*&;9 2;;
Vqnwgpg.f9!)U*&;;3212
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 36 of 44
62!qh!71
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
SE!Dcvej<
SE!Dcvej!Ogvjqf<
Cpcn{uku!Ogvjqf<
Cpcn{uku!Fguetkrvkqp<
OUX0481;8
GRC!9371
GRC!9371
9371!OUX!Nqy!Ngxgn
Cuuqekcvgf!Ncd!Ucorngu< ;33;;552112-!;33;;552114-!;33;;552115
Rctcogvgt Wpkvu
Dncpm
Tguwnv
Tgrqtvkpi
Nkokv Swcnkhkgtu
OGVJQF!DNCPM< 2857612
Cuuqekcvgf!Ncd!Ucorngu<;33;;552112-!;33;;552114-!;33;;552115
Ocvtkz< Ycvgt
Cpcn{|gf
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N >2/1 2/1 17012027!29<26
2-2-2.Vtkejnqtqgvjcpg wi0N >2/1 2/1 17012027!29<26
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N >2/1 2/1 17012027!29<26
2-2-3.Vtkejnqtqgvjcpg wi0N >2/1 2/1 17012027!29<26
2-2.Fkejnqtqgvjcpg wi0N >2/1 2/1 17012027!29<26
2-2.Fkejnqtqgvjgpg wi0N >2/1 2/1 17012027!29<26
2-3-4.Vtkejnqtqrtqrcpg wi0N >2/1 2/1 17012027!29<26
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N >3/1 3/1 17012027!29<26
2-3.Fkdtqoqgvjcpg!)GFD*wi0N >2/1 2/1 17012027!29<26
2-3.Fkejnqtqdgp|gpg wi0N >2/1 2/1 17012027!29<26
2-3.Fkejnqtqgvjcpg wi0N >2/1 2/1 17012027!29<26
2-5.Fkejnqtqdgp|gpg wi0N >2/1 2/1 17012027!29<26
3.Dwvcpqpg!)OGM*wi0N >6/1 6/1 17012027!29<26
3.Jgzcpqpg wi0N >6/1 6/1 17012027!29<26
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N >6/1 6/1 17012027!29<26
Cegvqpg wi0N >36/1 36/1 17012027!29<26
Cet{nqpkvtkng wi0N >21/1 21/1 17012027!29<26
Dgp|gpg wi0N >2/1 2/1 17012027!29<26
Dtqoqejnqtqogvjcpg wi0N >2/1 2/1 17012027!29<26
Dtqoqfkejnqtqogvjcpg wi0N >2/1 2/1 17012027!29<26
Dtqoqhqto wi0N >2/1 2/1 17012027!29<26
Dtqoqogvjcpg wi0N >3/1 3/1 17012027!29<26
Ectdqp!fkuwnhkfg wi0N >3/1 3/1 17012027!29<26
Ectdqp!vgvtcejnqtkfg wi0N >2/1 2/1 17012027!29<26
Ejnqtqdgp|gpg wi0N >2/1 2/1 17012027!29<26
Ejnqtqgvjcpg wi0N >2/1 2/1 17012027!29<26
Ejnqtqhqto wi0N >2/1 2/1 17012027!29<26
Ejnqtqogvjcpg wi0N >2/1 2/1 17012027!29<26
eku.2-3.Fkejnqtqgvjgpg wi0N >2/1 2/1 17012027!29<26
Fkdtqoqejnqtqogvjcpg wi0N >2/1 2/1 17012027!29<26
Fkdtqoqogvjcpg wi0N >2/1 2/1 17012027!29<26
Gvj{ndgp|gpg wi0N >2/1 2/1 17012027!29<26
Kqfqogvjcpg wi0N >6/1 6/1 17012027!29<26
o'r.Z{ngpg wi0N >3/1 3/1 17012027!29<26
Ogvj{ngpg!Ejnqtkfg wi0N >3/1 3/1 17012027!29<26
q.Z{ngpg wi0N >2/1 2/1 17012027!29<26
Uv{tgpg wi0N >2/1 2/1 17012027!29<26
Vgvtcejnqtqgvjgpg wi0N >2/1 2/1 17012027!29<26
Vqnwgpg wi0N >2/1 2/1 17012027!29<26
vtcpu.2-3.Fkejnqtqgvjgpg wi0N >2/1 2/1 17012027!29<26
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N >2/1 2/1 17012027!29<26
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 37 of 44
63!qh!71
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
Dncpm
Tguwnv
Tgrqtvkpi
Nkokv Swcnkhkgtu
OGVJQF!DNCPM< 2857612
Cuuqekcvgf!Ncd!Ucorngu<;33;;552112-!;33;;552114-!;33;;552115
Ocvtkz< Ycvgt
Cpcn{|gf
Vtkejnqtqgvjgpg wi0N >2/1 2/1 17012027!29<26
Vtkejnqtqhnwqtqogvjcpg wi0N >2/1 2/1 17012027!29<26
Xkp{n!cegvcvg wi0N >3/1 3/1 17012027!29<26
Xkp{n!ejnqtkfg wi0N >2/1 2/1 17012027!29<26
Z{ngpg!)Vqvcn*wi0N >3/1 3/1 17012027!29<26
2-3.Fkejnqtqgvjcpg.f5!)U*&211 81.241 17012027!29<26
5.Dtqoqhnwqtqdgp|gpg!)U*&211 81.241 17012027!29<26
Vqnwgpg.f9!)U*&212 81.241 17012027!29<26
Rctcogvgt Wpkvu
NEU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2857613NCDQTCVQT[!EQPVTQN!UCORNG<
NEUUrkmg
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N 67/361 223 81.241
2-2-2.Vtkejnqtqgvjcpg wi0N 68/461 226 81.241
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N 64/761 218 81.241
2-2-3.Vtkejnqtqgvjcpg wi0N 63/;61 217 81.241
2-2.Fkejnqtqgvjcpg wi0N 66/861 222 81.241
2-2.Fkejnqtqgvjgpg wi0N 71/461 232 81.243
2-3-4.Vtkejnqtqrtqrcpg wi0N 62/661 214 81.241
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N 6;/561 22;81.241
2-3.Fkdtqoqgvjcpg!)GFD*wi0N 68/961 227 81.241
2-3.Fkejnqtqdgp|gpg wi0N 69/261 227 81.241
2-3.Fkejnqtqgvjcpg wi0N 62/961 215 81.241
2-5.Fkejnqtqdgp|gpg wi0N 66/161 221 81.241
3.Dwvcpqpg!)OGM*wi0N 21;211 21;81.256
3.Jgzcpqpg wi0N 227211 227 81.255
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N 227211 227 81.251
Cegvqpg wi0N 219211 219 61.286
Cet{nqpkvtkng wi0N 36;361 215 81.254
Dgp|gpg wi0N 66/761 222 81.241
Dtqoqejnqtqogvjcpg wi0N 67/;61 225 81.241
Dtqoqfkejnqtqogvjcpg wi0N 67/561 224 81.241
Dtqoqhqto wi0N 59/461 ;8 81.241
Dtqoqogvjcpg wi0N 78/2 N16124565.241
Ectdqp!fkuwnhkfg wi0N 71/661 232 81.242
Ectdqp!vgvtcejnqtkfg wi0N 6;/961 231 81.243
Ejnqtqdgp|gpg wi0N 68/561 226 81.241
Ejnqtqgvjcpg wi0N 63/861 216 75.245
Ejnqtqhqto wi0N 66/761 222 81.241
Ejnqtqogvjcpg wi0N 73/561 236 75.241
eku.2-3.Fkejnqtqgvjgpg wi0N 66/561 222 81.242
Fkdtqoqejnqtqogvjcpg wi0N 61/561 212 81.241
Fkdtqoqogvjcpg wi0N 65/961 221 81.242
Gvj{ndgp|gpg wi0N 67/461 224 81.241
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 38 of 44
64!qh!71
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
NEU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2857613NCDQTCVQT[!EQPVTQN!UCORNG<
NEUUrkmg
Kqfqogvjcpg wi0N 9;/3211 9;5;.291
o'r.Z{ngpg wi0N 223211 223 81.241
Ogvj{ngpg!Ejnqtkfg wi0N 65/461 21;74.241
q.Z{ngpg wi0N 65/;61 221 81.241
Uv{tgpg wi0N 68/961 227 81.241
Vgvtcejnqtqgvjgpg wi0N 64/261 217 81.241
Vqnwgpg wi0N 66/661 222 81.241
vtcpu.2-3.Fkejnqtqgvjgpg wi0N 69/361 227 81.241
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N 96/3 N16128181.252
Vtkejnqtqgvjgpg wi0N 63/861 216 81.241
Vtkejnqtqhnwqtqogvjcpg wi0N 76/661 242 73.244
Xkp{n!cegvcvg wi0N 219211 219 77.268
Xkp{n!ejnqtkfg wi0N 73/461 236 61.261
Z{ngpg!)Vqvcn*wi0N 278261 222 81.241
2-3.Fkejnqtqgvjcpg.f5!)U*&;;81.241
5.Dtqoqhnwqtqdgp|gpg!)U*&213 81.241
Vqnwgpg.f9!)U*&211 81.241
Rctcogvgt Wpkvu
OU
Tguwnv
&!Tge
Nkokvu Swcn&!TgeEqpe/
2857614OCVTKZ!URKMG!'!OCVTKZ!URKMG!FWRNKECVG<
OUUrkmg
Tguwnv
;33;;32;116
2857615
OUF
Tguwnv
OUF
&!Tge TRF
OUFOU
Urkmg
Eqpe/
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N O23124381.241215 3531PF37/4 31/8
2-2-2.Vtkejnqtqgvjcpg wi0N O23125481.241227 3231PF39/7 34/2
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N 31 238 81.241;5 3;31PF 36/5 29/;
2-2-3.Vtkejnqtqgvjcpg wi0N O23124481.241212 3831PF37/6 31/4
2-2.Fkejnqtqgvjcpg wi0N O23125381.241223 3431PF39/4 33/5
2-2.Fkejnqtqgvjgpg wi0N 31 259 81.277232 3131PF3;/8 35/4
2-3-4.Vtkejnqtqrtqrcpg wi0N 31 239 81.241;;3631PF36/7 2;/;
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N O23124481.241213 3831PF37/7 31/5
2-3.Fkdtqoqgvjcpg!)GFD*wi0N O23125381.24121;3731PF39/5 32/;
2-3.Fkejnqtqdgp|gpg wi0N O23124981.241221 3431PF38/7 32/;
2-3.Fkejnqtqgvjcpg wi0N O23124581.241214 3731PF37/9 31/7
2-5.Fkejnqtqdgp|gpg wi0N O23124281.241217 3231PF37/3 32/3
3.Dwvcpqpg!)OGM*wi0N 51 21;81.24121;251PF54/5 54/7
3.Jgzcpqpg wi0N 51 225 81.241225 151PF56/8 56/8
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N 51 226 81.24122;551PF56/9 58/9
Cegvqpg wi0N 51 21;81.241221 251PF54/8 55/1
Cet{nqpkvtkng wi0N 211 232 81.241;6 35211PF232;6/2
Dgp|gpg wi0N 31 24;81.259223 3331PF38/9 33/4
Dtqoqejnqtqogvjcpg wi0N O23124981.241221 3431PF38/6 33/1
Dtqoqfkejnqtqogvjcpg wi0N O23124681.241218 3431PF38/1 32/5
Dtqoqhqto wi0N 31 228 81.241;3 3531PF34/6 29/6
Dtqoqogvjcpg wi0N O1317581.24195 3931PF23/9 27/;
Ectdqp!fkuwnhkfg wi0N O23123281.241242 931PF35/3 37/3
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 39 of 44
65!qh!71
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
OU
Tguwnv
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2857614OCVTKZ!URKMG!'!OCVTKZ!URKMG!FWRNKECVG<
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2857615
OUF
Tguwnv
OUF
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OUFOU
Urkmg
Eqpe/
Ectdqp!vgvtcejnqtkfg wi0N O23125981.241231 3231PF3;/6 35/1
Ejnqtqdgp|gpg wi0N 31 24;81.25721;3531PF38/9 32/;
Ejnqtqgvjcpg wi0N O23126381.241233 3231PF41/4 35/5
Ejnqtqhqto wi0N O23125181.241222 3431PF38/;33/3
Ejnqtqogvjcpg wi0N O23125681.241227 3331PF3;/1 34/3
eku.2-3.Fkejnqtqgvjgpg wi0N O23125181.241221 3531PF39/1 33/2
Fkdtqoqejnqtqogvjcpg wi0N 31 241 81.241;;3831PF36/;2;/9
Fkdtqoqogvjcpg wi0N O23124981.241215 3831PF38/6 31/;
Gvj{ndgp|gpg wi0N O23124881.24121;3431PF38/5 32/9
Kqfqogvjcpg wi0N T2518181.241;7 4351PF38/;49/6
o'r.Z{ngpg wi0N O25124581.241218 3351PF64/6 53/;
Ogvj{ngpg!Ejnqtkfg wi0N O23124881.241218 3531PF38/9 32/;
q.Z{ngpg wi0N O23124281.241216 3331PF37/3 32/2
Uv{tgpg wi0N O23124981.241221 3431PF38/8 33/1
Vgvtcejnqtqgvjgpg wi0N 31 234 81.241215 2831PF35/8 31/9
Vqnwgpg wi0N 31 245 81.266222 2;31PF 37/;33/2
vtcpu.2-3.Fkejnqtqgvjgpg wi0N O23125881.241225 3631PF3;/6 33/9
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N 31 ;4 81.24198 831PF29/8 28/6
Vtkejnqtqgvjgpg wi0N 31 243 7;.262221 2931PF37/6 33/2
Vtkejnqtqhnwqtqogvjcpg wi0N O23128281.241251 3131PF45/3 39/1
Xkp{n!cegvcvg wi0N 51 233 81.241;5 3751PF5;/1 48/7
Xkp{n!ejnqtkfg wi0N O23126581.241235 3331PF41/;35/;
2-3.Fkejnqtqgvjcpg.f5!)U*&;;81.241;8
5.Dtqoqhnwqtqdgp|gpg!)U*&;;81.241;8
Vqnwgpg.f9!)U*&;9 81.241;;
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 40 of 44
66!qh!71
$?SN$
QUALIFIERS
Rceg!Rtqlgev!Pq/<
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L27161871!OEIWKTG!NH
DEFINITIONS
FH!.!Fknwvkqp!Hcevqt-!kh!tgrqtvgf-!tgrtgugpvu!vjg!hcevqt!crrnkgf!vq!vjg!tgrqtvgf!fcvc!fwg!vq!fknwvkqp!qh!vjg!ucorng!cnkswqv/
PF!.!Pqv!Fgvgevgf!cv!qt!cdqxg!cflwuvgf!tgrqtvkpi!nkokv/
L!.!Guvkocvgf!eqpegpvtcvkqp!cdqxg!vjg!cflwuvgf!ogvjqf!fgvgevkqp!nkokv!cpf!dgnqy!vjg!cflwuvgf!tgrqtvkpi!nkokv/
OFN!.!Cflwuvgf!Ogvjqf!Fgvgevkqp!Nkokv/
RSN!.!Rtcevkecn!Swcpvkvcvkqp!Nkokv/
TN!.!Tgrqtvkpi!Nkokv/
U!.!Uwttqicvg
2-3.Fkrjgp{nj{ftc|kpg!fgeqorqugu!vq!cpf!ecppqv!dg!ugrctcvgf!htqo!C|qdgp|gpg!wukpi!Ogvjqf!9381/!Vjg!tguwnv!hqt!gcej!cpcn{vg!ku
c!eqodkpgf!eqpegpvtcvkqp/
Eqpukuvgpv!ykvj!GRC!iwkfgnkpgu-!wptqwpfgf!fcvc!ctg!fkurnc{gf!cpf!jcxg!dggp!wugf!vq!ecnewncvg!&!tgeqxgt{!cpf!TRF!xcnwgu/
NEU)F*!.!Ncdqtcvqt{!Eqpvtqn!Ucorng!)Fwrnkecvg*
OU)F*!.!Ocvtkz!Urkmg!)Fwrnkecvg*
FWR!.!Ucorng!Fwrnkecvg
TRF!.!Tgncvkxg!Rgtegpv!Fkhhgtgpeg
PE!.!Pqv!Ecnewncdng/
UI!.!Uknkec!Ign!.!Engcp.Wr
W!.!Kpfkecvgu!vjg!eqorqwpf!ycu!cpcn{|gf!hqt-!dwv!pqv!fgvgevgf/
Cekf!rtgugtxcvkqp!oc{!pqv!dg!crrtqrtkcvg!hqt!3!Ejnqtqgvj{nxkp{n!gvjgt-!Uv{tgpg-!cpf!Xkp{n!ejnqtkfg/
C!ugrctcvg!xkcn!rtgugtxgf!vq!c!rJ!qh!5.6!ku!tgeqoogpfgf!kp!UY957!Ejcrvgt!5!hqt!vjg!cpcn{uku!qh!Cetqngkp!cpf!Cet{nqpkvtkng!d{!GRC
Ogvjqf!9371/
P.Pkvtquqfkrjgp{ncokpg!fgeqorqugu!cpf!ecppqv!dg!ugrctcvgf!htqo!Fkrjgp{ncokpg!wukpi!Ogvjqf!9381/!!Vjg!tguwnv!tgrqtvgf!hqtgcej!cpcn{vg!ku!c!eqodkpgf!eqpegpvtcvkqp/
Rceg!Cpcn{vkecn!ku!VPK!ceetgfkvgf/!Eqpvcev!{qwt!Rceg!RO!hqt!vjg!ewttgpv!nkuv!qh!ceetgfkvgf!cpcn{vgu/
VPK!.!Vjg!PGNCE!Kpuvkvwvg/
LABORATORIES
Rceg!Cpcn{vkecn!Ugtxkegu!.!EjctnqvvgRCUK.E
ANALYTE QUALIFIERS
Enkgpv!rtqxkfgf!4!xkcnu/!!Cnn!4!xkcnu!ygtg!61&!uqkn/!!Jcf!vq!eqodkpg!3!xkcnu!kpvq!2!xkcn!vq!jcxg!gpqwij!xqnwog!hqt!c!2z!twp/
Vjku!twp!eqpvckpgf!ectt{qxgt!hqt!vqnwgpg/!!Ecppqv!rtghqto!eqttgevkxg!cevkqp!)tgtwp!2z!*!dgecwug!vjg!tgockpkpi!xkcn!jcu!vqq
owej!uqkn/!!Vjgtghqtg-!tgrqtvgf!twp!yknn!jcxg!crrtqrtkcvg!ectt{qxgt!hnci!qp!vqnwgpg/
2i
Tguwnv!oc{!dg!dkcugf!jkij!fwg!vq!ectt{qxgt!htqo!rtgxkqwun{!cpcn{|gf!ucorng/E9
Cpcn{vg!tgeqxgt{!kp!vjg!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!ycu!qwvukfg!SE!nkokvu/N1
Cpcn{vg!tgeqxgt{!kp!vjg!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!gzeggfgf!SE!nkokvu/!Cpcn{vg!rtgugpeg!dgnqy!tgrqtvkpi!nkokvu!kp
cuuqekcvgf!ucorngu/!!Tguwnvu!wpchhgevgf!d{!jkij!dkcu/N4
Ocvtkz!urkmg!tgeqxgt{!cpf0qt!ocvtkz!urkmg!fwrnkecvg!tgeqxgt{!ycu!qwvukfg!ncdqtcvqt{!eqpvtqn!nkokvu/O1
Ocvtkz!urkmg!tgeqxgt{!gzeggfgf!SE!nkokvu/!!Dcvej!ceegrvgf!dcugf!qp!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!tgeqxgt{/O2
TRF!xcnwg!ycu!qwvukfg!eqpvtqn!nkokvu/T2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 41 of 44
67!qh!71
$?ET$
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;;552
L27161871!OEIWKTG!NH
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92299441001 OUX0481;82016015254 DP-14 GRC!9371
92299441002 OUX0481912016015255 DP-15 GRC!9371
92299441003 OUX0481;82016015256 DP-16 GRC!9371
92299441004 OUX0481;82016015257 DP-20 GRC!9371
92299441005 OUX0481912016015258 DP-21 GRC!9371
92299441006 OUX0481912016015259 DP-22 GRC!9371
92299441007 OUX0481912016015260 DP-23 GRC!9371
92299441008 OUX0481912016015261 DP-24 GRC!9371
92299441009 OUX0481912016015262 DP-26 GRC!9371
92299441010 OUX0481912016015263 DP-25 GRC!9371
92299441011 OUX0481912016015264 DP-27 GRC!9371
92299441012 OUX0481912016015265 DP-28 GRC!9371
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<1;!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 42 of 44
68!qh!71
Page 43 of 44
69!qh!71
Page 44 of 44
6;!qh!71
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Lwpg!32-!3127
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Gpenqugf!ctg!vjg!cpcn{vkecn!tguwnvu!hqt!ucorng)u*!tgegkxgf!d{!vjg!ncdqtcvqt{!qp!Oc{!36-!3127/!!Vjg
tguwnvu!tgncvg!qpn{!vq!vjg!ucorngu!kpenwfgf!kp!vjku!tgrqtv/!!Tguwnvu!tgrqtvgf!jgtgkp!eqphqto!vq!vjg
oquv!ewttgpv!VPK!uvcpfctfu!cpf!vjg!ncdqtcvqt{(u!Swcnkv{!Cuuwtcpeg!Ocpwcn-!yjgtg!crrnkecdng-!wpnguu
qvjgtykug!pqvgf!kp!vjg!dqf{!qh!vjg!tgrqtv/
Cpcn{ugu!ygtg!rgthqtogf!cv!vjg!Rceg!Cpcn{vkecn!Ugtxkegu!nqecvkqp!kpfkecvgf!qp!vjg!ucorng!cpcn{vg
rcig!hqt!cpcn{uku!wpnguu!qvjgtykug!hqqvpqvgf/
RTQLGEV!TGXKUGF!7032027!.!UCORNG!KF(U!EJCPIGF!CV!ENKGPV!TGSWGUV
Kh!{qw!jcxg!cp{!swguvkqpu!eqpegtpkpi!vjku!tgrqtv-!rngcug!hggn!htgg!vq!eqpvcev!og/
Ukpegtgn{-
Ejtku!Dkujqr!hqt
mgxkp/jgttkpiBrcegncdu/eqo
JQTK\QP!Fcvcdcug!Cfokpkuvtcvqt
Mgxkp!Jgttkpi
Gpenquwtgu
ee< Tkejctf!Dqpfu
Rtqitco!Ocpcigt-!Fwmg!Gpgti{
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 1 of 36
23!qh!59
$?ER$
CERTIFICATIONS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Charlotte Certification IDs
;911!Mkpeg{!Cxg/!Uvg!211-!Jwpvgtuxknng-!PE!39189
Pqtvj!Ectqnkpc!Ftkpmkpi!Ycvgt!Egtvkhkecvkqp!$<!48817
Pqtvj!Ectqnkpc!Hkgnf!Ugtxkegu!Egtvkhkecvkqp!$<!6453
Pqtvj!Ectqnkpc!Ycuvgycvgt!Egtvkhkecvkqp!$<!23
Uqwvj!Ectqnkpc!Egtvkhkecvkqp!$<!;;117112
Hnqtkfc0PGNCR!Egtvkhkecvkqp!$<!G98738
Mgpvwem{!WUV!Egtvkhkecvkqp!$<!95
Xktikpkc0XGNCR!Egtvkhkecvkqp!$<!571332
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 2 of 36
24!qh!59
$?UC$
SAMPLE ANALYTE COUNT
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92298969001 2016014828 DP-5 GRC!9371 63 RCUK.EECJ
92298969002 2016014829 DP-6 GRC!9371 63 RCUK.EECJ
92298969003 2016014830 DP-7 GRC!9371 63 RCUK.EECJ
92298969004 2016014831 DP-8 GRC!9371 63 RCUK.EECJ
92298969005 2016014832 DP-9 GRC!9371 63 RCUK.EECJ
92298969006 2016014833 DP-10 GRC!9371 63 RCUK.EECJ
92298969007 2016014834 DP-11 GRC!9371 63 RCUK.EECJ
92298969008 2016014835 DP-12 GRC!9371 63 RCUK.EECJ
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 3 of 36
25!qh!59
$?JQ$
SUMMARY OF DETECTION
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Rctcogvgtu Cpcn{|gfTguwnv
Ncd!Ucorng!KF!
Tgrqtv!Nkokv SwcnkhkgtuWpkvuOgvjqf
Enkgpv!Ucorng!KF
92298969001 2016014828 DP-5
eku.2-3.Fkejnqtqgvjgpg 9/5 wi0N 16038027!34<242/1GRC!9371
Ogvj{ngpg!Ejnqtkfg 3/1 wi0N 16038027!34<24 E;3/1GRC!9371
Z{ngpg!)Vqvcn*21/7 wi0N 16038027!34<243/1GRC!9371
q.Z{ngpg 21/7 wi0N 16038027!34<242/1GRC!9371
92298969002 2016014829 DP-6
Dgp|gpg 4/7 wi0N 16038027!34<412/1GRC!9371
3.Dwvcpqpg!)OGM*6/3 wi0N 16038027!34<416/1GRC!9371
eku.2-3.Fkejnqtqgvjgpg 65/4 wi0N 16038027!34<412/1GRC!9371
Ogvj{ngpg!Ejnqtkfg 5/;wi0N 16038027!34<41 E;3/1GRC!9371
Vqnwgpg 2/3 wi0N 16038027!34<412/1GRC!9371
Z{ngpg!)Vqvcn*64/6 wi0N 16038027!34<413/1GRC!9371
q.Z{ngpg 64/6 wi0N 16038027!34<412/1GRC!9371
92298969004 2016014831 DP-8
eku.2-3.Fkejnqtqgvjgpg 24/2 wi0N 16039027!11<152/1GRC!9371
Z{ngpg!)Vqvcn*28/6 wi0N 16039027!11<153/1GRC!9371
q.Z{ngpg 28/6 wi0N 16039027!11<152/1GRC!9371
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 4 of 36
26!qh!59
$?PC$
PROJECT NARRATIVE
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Method:
Client:Fwmg!Gpgti{
EPA 8260
Date:Lwpg!32-!3127
Description:9371!OUX!Nqy!Ngxgn
General Information:
9!ucorngu!ygtg!cpcn{|gf!hqt!GRC!9371/!!Cnn!ucorngu!ygtg!tgegkxgf!kp!ceegrvcdng!eqpfkvkqp!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy!qt!qp!vjg
ejckp.qh!ewuvqf{!cpf0qt!vjg!ucorng!eqpfkvkqp!wrqp!tgegkrv!hqto!)UEWT*!cvvcejgf!cv!vjg!gpf!qh!vjku!tgrqtv/
Hold Time:
Vjg!ucorngu!ygtg!cpcn{|gf!ykvjkp!vjg!ogvjqf!tgswktgf!jqnf!vkogu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Initial Calibrations (including MS Tune as applicable):
Cnn!etkvgtkc!ygtg!ykvjkp!ogvjqf!tgswktgogpvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Continuing Calibration:
Cnn!etkvgtkc!ygtg!ykvjkp!ogvjqf!tgswktgogpvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Internal Standards:
Cnn!kpvgtpcn!uvcpfctfu!ygtg!ykvjkp!SE!nkokvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Surrogates:
Cnn!uwttqicvgu!ygtg!ykvjkp!SE!nkokvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Method Blank:
Cnn!cpcn{vgu!ygtg!dgnqy!vjg!tgrqtv!nkokv!kp!vjg!ogvjqf!dncpm-!yjgtg!crrnkecdng-!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Laboratory Control Spike:
Cnn!ncdqtcvqt{!eqpvtqn!urkmg!eqorqwpfu!ygtg!ykvjkp!SE!nkokvu!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
SE!Dcvej<!OUX048132
N1<!Cpcn{vg!tgeqxgt{!kp!vjg!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!ycu!qwvukfg!SE!nkokvu/
—!NEU!!)Ncd!KF<!2854551*
—!vtcpu.2-5.Fkejnqtq.3.dwvgpg
SE!Dcvej<!OUX048133
N1<!Cpcn{vg!tgeqxgt{!kp!vjg!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!ycu!qwvukfg!SE!nkokvu/
—!NEU!!)Ncd!KF<!2854556*
—!vtcpu.2-5.Fkejnqtq.3.dwvgpg
Matrix Spikes:
Cnn!rgtegpv!tgeqxgtkgu!cpf!tgncvkxg!rgtegpv!fkhhgtgpegu!)TRFu*!ygtg!ykvjkp!ceegrvcpeg!etkvgtkc!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
SE!Dcvej<!OUX048132
C!ocvtkz!urkmg!cpf0qt!ocvtkz!urkmg!fwrnkecvg!)OU0OUF*!ygtg!rgthqtogf!qp!vjg!hqnnqykpi!ucorng)u*<!!;33;99;7114
O2<!Ocvtkz!urkmg!tgeqxgt{!gzeggfgf!SE!nkokvu/!!Dcvej!ceegrvgf!dcugf!qp!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!tgeqxgt{/
—!OU!!)Ncd!KF<!2854553*
—!2-2-2.Vtkejnqtqgvjcpg
—!3.Dwvcpqpg!)OGM*
—!Cegvqpg
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 5 of 36
27!qh!59
$?PC$
PROJECT NARRATIVE
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Method:
Client:Fwmg!Gpgti{
EPA 8260
Date:Lwpg!32-!3127
Description:9371!OUX!Nqy!Ngxgn
SE!Dcvej<!OUX048132
C!ocvtkz!urkmg!cpf0qt!ocvtkz!urkmg!fwrnkecvg!)OU0OUF*!ygtg!rgthqtogf!qp!vjg!hqnnqykpi!ucorng)u*<!!;33;99;7114
O2<!Ocvtkz!urkmg!tgeqxgt{!gzeggfgf!SE!nkokvu/!!Dcvej!ceegrvgf!dcugf!qp!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!tgeqxgt{/
—!Ectdqp!fkuwnhkfg
—!Ectdqp!vgvtcejnqtkfg
—!Ejnqtqgvjcpg
—!Vtkejnqtqhnwqtqogvjcpg
—!Xkp{n!cegvcvg
—!Xkp{n!ejnqtkfg
—!eku.2-3.Fkejnqtqgvjgpg
—!vtcpu.2-3.Fkejnqtqgvjgpg
SE!Dcvej<!OUX048133
C!ocvtkz!urkmg!cpf0qt!ocvtkz!urkmg!fwrnkecvg!)OU0OUF*!ygtg!rgthqtogf!qp!vjg!hqnnqykpi!ucorng)u*<!!;33;;199115
O2<!Ocvtkz!urkmg!tgeqxgt{!gzeggfgf!SE!nkokvu/!!Dcvej!ceegrvgf!dcugf!qp!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!tgeqxgt{/
—!OU!!)Ncd!KF<!2855814*
—!Gvj{ndgp|gpg
—!o'r.Z{ngpg
Duplicate Sample:
Cnn!fwrnkecvg!ucorng!tguwnvu!ygtg!ykvjkp!ogvjqf!ceegrvcpeg!etkvgtkc!ykvj!cp{!gzegrvkqpu!pqvgf!dgnqy/
Additional Comments:
Cpcn{vg!Eqoogpvu<
SE!Dcvej<!OUX048132
E;<!Eqooqp!Ncdqtcvqt{!Eqpvcokpcpv/
—!3127125939!FR.6!!)Ncd!KF<!;33;9;7;112*
—!Ogvj{ngpg!Ejnqtkfg
—!312712593;!FR.7!!)Ncd!KF<!;33;9;7;113*
—!Ogvj{ngpg!Ejnqtkfg
Vjku!fcvc!rcemcig!jcu!dggp!tgxkgygf!hqt!swcnkv{!cpf!eqorngvgpguu!cpf!ku!crrtqxgf!hqt!tgngcug/
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 6 of 36
28!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014828 DP-5 Lab ID: 92298969001 Eqnngevgf< 16031027!26<61 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16038027!34<24 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16038027!34<24 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16038027!34<24 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16038027!34<24 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16038027!34<24 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16038027!34<24 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16038027!34<24 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16038027!34<24 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16038027!34<24 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16038027!34<24 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16038027!34<24 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16038027!34<24 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16038027!34<24 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16038027!34<24 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16038027!34<24 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16038027!34<24 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16038027!34<24 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16038027!34<24 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16038027!34<24 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16038027!34<24 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16038027!34<24 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16038027!34<24 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16038027!34<24 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16038027!34<24 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg 8.4 wi0N 16038027!34<24 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16038027!34<24 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16038027!34<24 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16038027!34<24 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16038027!34<24 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16038027!34<24 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16038027!34<24 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16038027!34<24 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg 2.0 wi0N 16038027!34<24 86.1;.3 E;3/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16038027!34<24 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16038027!34<24 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16038027!34<24 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16038027!34<24 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16038027!34<24 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16038027!34<24 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16038027!34<24 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16038027!34<24 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16038027!34<24 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16038027!34<24 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16038027!34<24 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16038027!34<24 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16038027!34<24 86.12.52/1 2
Z{ngpg!)Vqvcn*10.6 wi0N 16038027!34<24 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 7 of 36
29!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014828 DP-5 Lab ID: 92298969001 Eqnngevgf< 16031027!26<61 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16038027!34<24 28;712.34.23/1 2
q.Z{ngpg 10.6 wi0N 16038027!34<24 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;8 &16038027!34<24 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*213 &16038027!34<24 28171.18.181.241 2
Vqnwgpg.f9!)U*;;&16038027!34<24 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 8 of 36
2;!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014829 DP-6 Lab ID: 92298969002 Eqnngevgf< 16034027!23<41 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16038027!34<41 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16038027!34<41 218.24.221/1 2
Dgp|gpg 3.6 wi0N 16038027!34<41 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16038027!34<41 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16038027!34<41 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16038027!34<41 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16038027!34<41 85.94.;3/1 2
3.Dwvcpqpg!)OGM*5.2 wi0N 16038027!34<41 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16038027!34<41 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16038027!34<41 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16038027!34<41 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16038027!34<41 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16038027!34<41 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16038027!34<41 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16038027!34<41 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16038027!34<41 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16038027!34<41 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16038027!34<41 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16038027!34<41 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16038027!34<41 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16038027!34<41 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16038027!34<41 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16038027!34<41 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16038027!34<41 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg 54.3 wi0N 16038027!34<41 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16038027!34<41 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16038027!34<41 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16038027!34<41 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16038027!34<41 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16038027!34<41 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16038027!34<41 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16038027!34<41 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg 4.9 wi0N 16038027!34<41 86.1;.3 E;3/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16038027!34<41 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16038027!34<41 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16038027!34<41 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16038027!34<41 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16038027!34<41 238.29.52/1 2
Vqnwgpg 1.2 wi0N 16038027!34<41 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16038027!34<41 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16038027!34<41 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16038027!34<41 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16038027!34<41 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16038027!34<41 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16038027!34<41 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16038027!34<41 86.12.52/1 2
Z{ngpg!)Vqvcn*53.5 wi0N 16038027!34<41 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 9 of 36
31!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014829 DP-6 Lab ID: 92298969002 Eqnngevgf< 16034027!23<41 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16038027!34<41 28;712.34.23/1 2
q.Z{ngpg 53.5 wi0N 16038027!34<41 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*211 &16038027!34<41 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*213 &16038027!34<41 28171.18.181.241 2
Vqnwgpg.f9!)U*;;&16038027!34<41 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 10 of 36
32!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014830 DP-7 Lab ID: 92298969003 Eqnngevgf< 16034027!25<41 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16038027!34<58 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16038027!34<58 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16038027!34<58 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16038027!34<58 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16038027!34<58 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16038027!34<58 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16038027!34<58 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16038027!34<58 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16038027!34<58 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16038027!34<58 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16038027!34<58 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16038027!34<58 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16038027!34<58 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16038027!34<58 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16038027!34<58 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16038027!34<58 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16038027!34<58 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16038027!34<58 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16038027!34<58 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16038027!34<58 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16038027!34<58 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16038027!34<58 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16038027!34<58 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16038027!34<58 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16038027!34<58 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16038027!34<58 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16038027!34<58 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16038027!34<58 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16038027!34<58 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16038027!34<58 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16038027!34<58 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16038027!34<58 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 16038027!34<58 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16038027!34<58 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16038027!34<58 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16038027!34<58 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16038027!34<58 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16038027!34<58 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16038027!34<58 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16038027!34<58 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16038027!34<58 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16038027!34<58 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16038027!34<58 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16038027!34<58 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16038027!34<58 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16038027!34<58 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 16038027!34<58 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 11 of 36
33!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014830 DP-7 Lab ID: 92298969003 Eqnngevgf< 16034027!25<41 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16038027!34<58 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 16038027!34<58 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;2 &16038027!34<58 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*;5 &16038027!34<58 28171.18.181.241 2
Vqnwgpg.f9!)U*;;&16038027!34<58 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 12 of 36
34!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014831 DP-8 Lab ID: 92298969004 Eqnngevgf< 16034027!26<21 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16039027!11<15 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16039027!11<15 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16039027!11<15 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16039027!11<15 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16039027!11<15 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16039027!11<15 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16039027!11<15 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16039027!11<15 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16039027!11<15 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16039027!11<15 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16039027!11<15 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16039027!11<15 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16039027!11<15 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16039027!11<15 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16039027!11<15 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16039027!11<15 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16039027!11<15 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16039027!11<15 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16039027!11<15 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16039027!11<15 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16039027!11<15 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16039027!11<15 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16039027!11<15 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<15 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg 13.1 wi0N 16039027!11<15 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<15 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16039027!11<15 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16039027!11<15 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16039027!11<15 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16039027!11<15 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16039027!11<15 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16039027!11<15 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 16039027!11<15 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16039027!11<15 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16039027!11<15 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16039027!11<15 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16039027!11<15 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16039027!11<15 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16039027!11<15 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16039027!11<15 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16039027!11<15 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16039027!11<15 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16039027!11<15 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16039027!11<15 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16039027!11<15 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16039027!11<15 86.12.52/1 2
Z{ngpg!)Vqvcn*17.5 wi0N 16039027!11<15 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 13 of 36
35!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014831 DP-8 Lab ID: 92298969004 Eqnngevgf< 16034027!26<21 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16039027!11<15 28;712.34.23/1 2
q.Z{ngpg 17.5 wi0N 16039027!11<15 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;;&16039027!11<15 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*211 &16039027!11<15 28171.18.181.241 2
Vqnwgpg.f9!)U*211 &16039027!11<15 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 14 of 36
36!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014832 DP-9 Lab ID: 92298969005 Eqnngevgf< 16034027!26<66 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16039027!11<32 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16039027!11<32 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16039027!11<32 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16039027!11<32 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16039027!11<32 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16039027!11<32 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16039027!11<32 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16039027!11<32 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16039027!11<32 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16039027!11<32 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16039027!11<32 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16039027!11<32 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16039027!11<32 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16039027!11<32 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16039027!11<32 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16039027!11<32 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16039027!11<32 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16039027!11<32 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16039027!11<32 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16039027!11<32 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16039027!11<32 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16039027!11<32 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16039027!11<32 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<32 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<32 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<32 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16039027!11<32 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16039027!11<32 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16039027!11<32 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16039027!11<32 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16039027!11<32 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16039027!11<32 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 16039027!11<32 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16039027!11<32 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16039027!11<32 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16039027!11<32 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16039027!11<32 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16039027!11<32 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16039027!11<32 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16039027!11<32 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16039027!11<32 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16039027!11<32 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16039027!11<32 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16039027!11<32 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16039027!11<32 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16039027!11<32 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 16039027!11<32 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 15 of 36
37!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014832 DP-9 Lab ID: 92298969005 Eqnngevgf< 16034027!26<66 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16039027!11<32 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 16039027!11<32 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*211 &16039027!11<32 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*213 &16039027!11<32 28171.18.181.241 2
Vqnwgpg.f9!)U*211 &16039027!11<32 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 16 of 36
38!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014833 DP-10 Lab ID: 92298969006 Eqnngevgf< 16034027!27<46 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16039027!11<49 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16039027!11<49 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16039027!11<49 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16039027!11<49 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16039027!11<49 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16039027!11<49 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16039027!11<49 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16039027!11<49 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16039027!11<49 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16039027!11<49 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16039027!11<49 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16039027!11<49 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16039027!11<49 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16039027!11<49 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16039027!11<49 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16039027!11<49 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16039027!11<49 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16039027!11<49 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16039027!11<49 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16039027!11<49 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16039027!11<49 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16039027!11<49 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16039027!11<49 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<49 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<49 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<49 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16039027!11<49 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16039027!11<49 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16039027!11<49 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16039027!11<49 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16039027!11<49 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16039027!11<49 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 16039027!11<49 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16039027!11<49 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16039027!11<49 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16039027!11<49 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16039027!11<49 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16039027!11<49 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16039027!11<49 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16039027!11<49 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16039027!11<49 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16039027!11<49 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16039027!11<49 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16039027!11<49 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16039027!11<49 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16039027!11<49 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 16039027!11<49 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 17 of 36
39!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014833 DP-10 Lab ID: 92298969006 Eqnngevgf< 16034027!27<46 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16039027!11<49 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 16039027!11<49 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;8 &16039027!11<49 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*212 &16039027!11<49 28171.18.181.241 2
Vqnwgpg.f9!)U*;;&16039027!11<49 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 18 of 36
3;!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014834 DP-11 Lab ID: 92298969007 Eqnngevgf< 16035027!21<66 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16039027!11<66 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16039027!11<66 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16039027!11<66 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16039027!11<66 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16039027!11<66 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16039027!11<66 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16039027!11<66 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16039027!11<66 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16039027!11<66 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16039027!11<66 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16039027!11<66 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16039027!11<66 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16039027!11<66 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16039027!11<66 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16039027!11<66 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16039027!11<66 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16039027!11<66 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16039027!11<66 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16039027!11<66 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16039027!11<66 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16039027!11<66 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16039027!11<66 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16039027!11<66 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<66 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<66 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16039027!11<66 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16039027!11<66 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16039027!11<66 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16039027!11<66 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16039027!11<66 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16039027!11<66 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16039027!11<66 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 16039027!11<66 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16039027!11<66 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16039027!11<66 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16039027!11<66 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16039027!11<66 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16039027!11<66 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16039027!11<66 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16039027!11<66 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16039027!11<66 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16039027!11<66 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16039027!11<66 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16039027!11<66 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16039027!11<66 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16039027!11<66 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 16039027!11<66 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 19 of 36
41!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014834 DP-11 Lab ID: 92298969007 Eqnngevgf< 16035027!21<66 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16039027!11<66 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 16039027!11<66 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*;;&16039027!11<66 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*213 &16039027!11<66 28171.18.181.241 2
Vqnwgpg.f9!)U*211 &16039027!11<66 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 20 of 36
42!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014835 DP-12 Lab ID: 92298969008 Eqnngevgf< 16035027!22<51 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
Cegvqpg <25.0 wi0N 16038027!28<27 78.75.236/1 2
Cet{nqpkvtkng <10.0 wi0N 16038027!28<27 218.24.221/1 2
Dgp|gpg <1.0 wi0N 16038027!28<27 82.54.32/1 2
Dtqoqejnqtqogvjcpg <1.0 wi0N 16038027!28<27 85.;8.62/1 2
Dtqoqfkejnqtqogvjcpg <1.0 wi0N 16038027!28<27 86.38.52/1 2
Dtqoqhqto <1.0 wi0N 16038027!28<27 86.36.32/1 2
Dtqoqogvjcpg <2.0 wi0N 16038027!28<27 85.94.;3/1 2
3.Dwvcpqpg!)OGM*<5.0 wi0N 16038027!28<27 89.;4.46/1 2
Ectdqp!fkuwnhkfg <2.0 wi0N 16038027!28<27 86.26.13/1 2
Ectdqp!vgvtcejnqtkfg <1.0 wi0N 16038027!28<27 67.34.62/1 2
Ejnqtqdgp|gpg <1.0 wi0N 16038027!28<27 219.;1.82/1 2
Ejnqtqgvjcpg <1.0 wi0N 16038027!28<27 86.11.42/1 2
Ejnqtqhqto <1.0 wi0N 16038027!28<27 78.77.42/1 2
Ejnqtqogvjcpg <1.0 wi0N 16038027!28<27 85.98.42/1 2
2-3.Fkdtqoq.4.ejnqtqrtqrcpg <2.0 wi0N 16038027!28<27 ;7.23.93/1 2
Fkdtqoqejnqtqogvjcpg <1.0 wi0N 16038027!28<27 235.59.22/1 2
2-3.Fkdtqoqgvjcpg!)GFD*<1.0 wi0N 16038027!28<27 217.;4.52/1 2
Fkdtqoqogvjcpg <1.0 wi0N 16038027!28<27 85.;6.42/1 2
2-3.Fkejnqtqdgp|gpg <1.0 wi0N 16038027!28<27 ;6.61.22/1 2
2-5.Fkejnqtqdgp|gpg <1.0 wi0N 16038027!28<27 217.57.82/1 2
vtcpu.2-5.Fkejnqtq.3.dwvgpg <1.0 wi0N 16038027!28<27 221.68.7 N42/1 2
2-2.Fkejnqtqgvjcpg <1.0 wi0N 16038027!28<27 86.45.42/1 2
2-3.Fkejnqtqgvjcpg <1.0 wi0N 16038027!28<27 218.17.32/1 2
2-2.Fkejnqtqgvjgpg <1.0 wi0N 16038027!28<27 86.46.52/1 2
eku.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16038027!28<27 267.6;.32/1 2
vtcpu.2-3.Fkejnqtqgvjgpg <1.0 wi0N 16038027!28<27 267.71.62/1 2
2-3.Fkejnqtqrtqrcpg <1.0 wi0N 16038027!28<27 89.98.62/1 2
eku.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16038027!28<27 21172.12.62/1 2
vtcpu.2-4.Fkejnqtqrtqrgpg <1.0 wi0N 16038027!28<27 21172.13.72/1 2
Gvj{ndgp|gpg <1.0 wi0N 16038027!28<27 211.52.52/1 2
3.Jgzcpqpg <5.0 wi0N 16038027!28<27 6;2.89.76/1 2
Kqfqogvjcpg <5.0 wi0N 16038027!28<27 85.99.56/1 2
Ogvj{ngpg!Ejnqtkfg <2.0 wi0N 16038027!28<27 86.1;.33/1 2
5.Ogvj{n.3.rgpvcpqpg!)OKDM*<5.0 wi0N 16038027!28<27 219.21.26/1 2
Uv{tgpg <1.0 wi0N 16038027!28<27 211.53.62/1 2
2-2-2-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16038027!28<27 741.31.72/1 2
2-2-3-3.Vgvtcejnqtqgvjcpg <1.0 wi0N 16038027!28<27 8;.45.62/1 2
Vgvtcejnqtqgvjgpg <1.0 wi0N 16038027!28<27 238.29.52/1 2
Vqnwgpg <1.0 wi0N 16038027!28<27 219.99.42/1 2
2-2-2.Vtkejnqtqgvjcpg <1.0 wi0N 16038027!28<27 82.66.72/1 2
2-2-3.Vtkejnqtqgvjcpg <1.0 wi0N 16038027!28<27 8;.11.62/1 2
Vtkejnqtqgvjgpg <1.0 wi0N 16038027!28<27 8;.12.72/1 2
Vtkejnqtqhnwqtqogvjcpg <1.0 wi0N 16038027!28<27 86.7;.52/1 2
2-3-4.Vtkejnqtqrtqrcpg <1.0 wi0N 16038027!28<27 ;7.29.52/1 2
Xkp{n!cegvcvg <2.0 wi0N 16038027!28<27 219.16.53/1 2
Xkp{n!ejnqtkfg <1.0 wi0N 16038027!28<27 86.12.52/1 2
Z{ngpg!)Vqvcn*<2.0 wi0N 16038027!28<27 2441.31.83/1 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 21 of 36
43!qh!59
$?CT$
ANALYTICAL RESULTS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Sample: 2016014835 DP-12 Lab ID: 92298969008 Eqnngevgf< 16035027!22<51 Tgegkxgf< 16036027!23<31 Ocvtkz< Ycvgt
Rctcogvgtu Tguwnvu Wpkvu FH Rtgrctgf Cpcn{|gf ECU!Pq/SwcnTgrqtv!Nkokv
Cpcn{vkecn!Ogvjqf<!GRC!93718260 MSV Low Level
o'r.Z{ngpg <2.0 wi0N 16038027!28<27 28;712.34.23/1 2
q.Z{ngpg <1.0 wi0N 16038027!28<27 ;6.58.72/1 2
Surrogates
5.Dtqoqhnwqtqdgp|gpg!)U*9;&16038027!28<27 571.11.581.241 2
2-3.Fkejnqtqgvjcpg.f5!)U*;2 &16038027!28<27 28171.18.181.241 2
Vqnwgpg.f9!)U*;9 &16038027!28<27 3148.37.681.241 2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 22 of 36
44!qh!59
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
SE!Dcvej<
SE!Dcvej!Ogvjqf<
Cpcn{uku!Ogvjqf<
Cpcn{uku!Fguetkrvkqp<
OUX048132
GRC!9371
GRC!9371
9371!OUX!Nqy!Ngxgn
Cuuqekcvgf!Ncd!Ucorngu< ;33;9;7;112-!;33;9;7;113-!;33;9;7;114-!;33;9;7;115-!;33;9;7;116-!;33;9;7;117-!;33;9;7;118
Rctcogvgt Wpkvu
Dncpm
Tguwnv
Tgrqtvkpi
Nkokv Swcnkhkgtu
OGVJQF!DNCPM< 285454;
Cuuqekcvgf!Ncd!Ucorngu<;33;9;7;112-!;33;9;7;113-!;33;9;7;114-!;33;9;7;115-!;33;9;7;116-!;33;9;7;117-!;33;9;7;118
Ocvtkz< Ycvgt
Cpcn{|gf
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<6;
2-2-2.Vtkejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<6;
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<6;
2-2-3.Vtkejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<6;
2-2.Fkejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<6;
2-2.Fkejnqtqgvjgpg wi0N >2/1 2/1 16038027!27<6;
2-3-4.Vtkejnqtqrtqrcpg wi0N >2/1 2/1 16038027!27<6;
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N >3/1 3/1 16038027!27<6;
2-3.Fkdtqoqgvjcpg!)GFD*wi0N >2/1 2/1 16038027!27<6;
2-3.Fkejnqtqdgp|gpg wi0N >2/1 2/1 16038027!27<6;
2-3.Fkejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<6;
2-3.Fkejnqtqrtqrcpg wi0N >2/1 2/1 16038027!27<6;
2-5.Fkejnqtqdgp|gpg wi0N >2/1 2/1 16038027!27<6;
3.Dwvcpqpg!)OGM*wi0N >6/1 6/1 16038027!27<6;
3.Jgzcpqpg wi0N >6/1 6/1 16038027!27<6;
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N >6/1 6/1 16038027!27<6;
Cegvqpg wi0N >36/1 36/1 16038027!27<6;
Cet{nqpkvtkng wi0N >21/1 21/1 16038027!27<6;
Dgp|gpg wi0N >2/1 2/1 16038027!27<6;
Dtqoqejnqtqogvjcpg wi0N >2/1 2/1 16038027!27<6;
Dtqoqfkejnqtqogvjcpg wi0N >2/1 2/1 16038027!27<6;
Dtqoqhqto wi0N >2/1 2/1 16038027!27<6;
Dtqoqogvjcpg wi0N >3/1 3/1 16038027!27<6;
Ectdqp!fkuwnhkfg wi0N >3/1 3/1 16038027!27<6;
Ectdqp!vgvtcejnqtkfg wi0N >2/1 2/1 16038027!27<6;
Ejnqtqdgp|gpg wi0N >2/1 2/1 16038027!27<6;
Ejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<6;
Ejnqtqhqto wi0N >2/1 2/1 16038027!27<6;
Ejnqtqogvjcpg wi0N >2/1 2/1 16038027!27<6;
eku.2-3.Fkejnqtqgvjgpg wi0N >2/1 2/1 16038027!27<6;
eku.2-4.Fkejnqtqrtqrgpg wi0N >2/1 2/1 16038027!27<6;
Fkdtqoqejnqtqogvjcpg wi0N >2/1 2/1 16038027!27<6;
Fkdtqoqogvjcpg wi0N >2/1 2/1 16038027!27<6;
Gvj{ndgp|gpg wi0N >2/1 2/1 16038027!27<6;
Kqfqogvjcpg wi0N >6/1 6/1 16038027!27<6;
o'r.Z{ngpg wi0N >3/1 3/1 16038027!27<6;
Ogvj{ngpg!Ejnqtkfg wi0N >3/1 3/1 16038027!27<6;
q.Z{ngpg wi0N >2/1 2/1 16038027!27<6;
Uv{tgpg wi0N >2/1 2/1 16038027!27<6;
Vgvtcejnqtqgvjgpg wi0N >2/1 2/1 16038027!27<6;
Vqnwgpg wi0N >2/1 2/1 16038027!27<6;
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 23 of 36
45!qh!59
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
Dncpm
Tguwnv
Tgrqtvkpi
Nkokv Swcnkhkgtu
OGVJQF!DNCPM< 285454;
Cuuqekcvgf!Ncd!Ucorngu<;33;9;7;112-!;33;9;7;113-!;33;9;7;114-!;33;9;7;115-!;33;9;7;116-!;33;9;7;117-!;33;9;7;118
Ocvtkz< Ycvgt
Cpcn{|gf
vtcpu.2-3.Fkejnqtqgvjgpg wi0N >2/1 2/1 16038027!27<6;
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N >2/1 2/1 16038027!27<6;
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N >2/1 2/1 16038027!27<6;
Vtkejnqtqgvjgpg wi0N >2/1 2/1 16038027!27<6;
Vtkejnqtqhnwqtqogvjcpg wi0N >2/1 2/1 16038027!27<6;
Xkp{n!cegvcvg wi0N >3/1 3/1 16038027!27<6;
Xkp{n!ejnqtkfg wi0N >2/1 2/1 16038027!27<6;
Z{ngpg!)Vqvcn*wi0N >3/1 3/1 16038027!27<6;
2-3.Fkejnqtqgvjcpg.f5!)U*&212 81.241 16038027!27<6;
5.Dtqoqhnwqtqdgp|gpg!)U*&;;81.241 16038027!27<6;
Vqnwgpg.f9!)U*&;;81.241 16038027!27<6;
Rctcogvgt Wpkvu
NEU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2854551NCDQTCVQT[!EQPVTQN!UCORNG<
NEUUrkmg
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N 64/361 217 81.241
2-2-2.Vtkejnqtqgvjcpg wi0N 65/461 21;81.241
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N 61/361 211 81.241
2-2-3.Vtkejnqtqgvjcpg wi0N 62/261 213 81.241
2-2.Fkejnqtqgvjcpg wi0N 63/861 216 81.241
2-2.Fkejnqtqgvjgpg wi0N 63/461 216 81.243
2-3-4.Vtkejnqtqrtqrcpg wi0N 62/461 214 81.241
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N 61/561 212 81.241
2-3.Fkdtqoqgvjcpg!)GFD*wi0N 66/961 223 81.241
2-3.Fkejnqtqdgp|gpg wi0N 67/161 223 81.241
2-3.Fkejnqtqgvjcpg wi0N 61/461 212 81.241
2-3.Fkejnqtqrtqrcpg wi0N 61/361 211 81.241
2-5.Fkejnqtqdgp|gpg wi0N 63/861 216 81.241
3.Dwvcpqpg!)OGM*wi0N 221211 221 81.256
3.Jgzcpqpg wi0N 222211 222 81.255
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N 224211 224 81.251
Cegvqpg wi0N 219211 219 61.286
Cet{nqpkvtkng wi0N 365361 213 81.254
Dgp|gpg wi0N 63/461 216 81.241
Dtqoqejnqtqogvjcpg wi0N 65/861 21;81.241
Dtqoqfkejnqtqogvjcpg wi0N 64/761 218 81.241
Dtqoqhqto wi0N 55/561 9;81.241
Dtqoqogvjcpg wi0N 62/761 214 65.241
Ectdqp!fkuwnhkfg wi0N 68/561 226 81.242
Ectdqp!vgvtcejnqtkfg wi0N 65/861 21;81.243
Ejnqtqdgp|gpg wi0N 64/561 218 81.241
Ejnqtqgvjcpg wi0N 59/961 ;9 75.245
Ejnqtqhqto wi0N 63/561 216 81.241
Ejnqtqogvjcpg wi0N 66/561 222 75.241
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 24 of 36
46!qh!59
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
NEU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2854551NCDQTCVQT[!EQPVTQN!UCORNG<
NEUUrkmg
eku.2-3.Fkejnqtqgvjgpg wi0N 64/761 218 81.242
eku.2-4.Fkejnqtqrtqrgpg wi0N 64/161 217 81.241
Fkdtqoqejnqtqogvjcpg wi0N 64/961 219 81.241
Fkdtqoqogvjcpg wi0N 63/961 217 81.242
Gvj{ndgp|gpg wi0N 63/461 216 81.241
Kqfqogvjcpg wi0N ;8/8211 ;9 5;.291
o'r.Z{ngpg wi0N 214211 214 81.241
Ogvj{ngpg!Ejnqtkfg wi0N 65/761 21;74.241
q.Z{ngpg wi0N 62/561 214 81.241
Uv{tgpg wi0N 65/361 219 81.241
Vgvtcejnqtqgvjgpg wi0N 5;/361 ;9 81.241
Vqnwgpg wi0N 63/561 216 81.241
vtcpu.2-3.Fkejnqtqgvjgpg wi0N 65/261 219 81.241
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N 62/461 214 81.243
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N 8;/2 N16126981.252
Vtkejnqtqgvjgpg wi0N 62/661 214 81.241
Vtkejnqtqhnwqtqogvjcpg wi0N 66/861 222 73.244
Xkp{n!cegvcvg wi0N 21;211 21;77.268
Xkp{n!ejnqtkfg wi0N 64/661 218 61.261
Z{ngpg!)Vqvcn*wi0N 266261 214 81.241
2-3.Fkejnqtqgvjcpg.f5!)U*&212 81.241
5.Dtqoqhnwqtqdgp|gpg!)U*&211 81.241
Vqnwgpg.f9!)U*&212 81.241
Rctcogvgt Wpkvu
OU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2854553OCVTKZ!URKMG!UCORNG<
OUUrkmg
Tguwnv
;33;99;7114
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N 35/631 233 81.241PF
2-2-2.Vtkejnqtqgvjcpg wi0N 37/9 O23124581.241PF
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N 34/331 227 81.241PF
2-2-3.Vtkejnqtqgvjcpg wi0N 35/331 232 81.241PF
2-2.Fkejnqtqgvjcpg wi0N 36/831 239 81.241PF
2-2.Fkejnqtqgvjgpg wi0N 38/531 248 81.277PF
2-3-4.Vtkejnqtqrtqrcpg wi0N 35/131 231 81.241PF
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N 33/431 223 81.241PF
2-3.Fkdtqoqgvjcpg!)GFD*wi0N 36/931 23;81.241PF
2-3.Fkejnqtqdgp|gpg wi0N 36/131 236 81.241PF
2-3.Fkejnqtqgvjcpg wi0N 34/731 229 81.241PF
2-3.Fkejnqtqrtqrcpg wi0N 35/331 232 81.241PF
2-5.Fkejnqtqdgp|gpg wi0N 35/931 235 81.241PF
3.Dwvcpqpg!)OGM*wi0N 63/3 O25124281.241PF
3.Jgzcpqpg wi0N 62/951 23;81.241PF
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N 63/151 241 81.241PF
Cegvqpg wi0N 66/1 O25124981.241PF
Cet{nqpkvtkng wi0N 237211 237 81.241PF
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 25 of 36
47!qh!59
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
OU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2854553OCVTKZ!URKMG!UCORNG<
OUUrkmg
Tguwnv
;33;99;7114
Dgp|gpg wi0N 36/131 236 81.259PF
Dtqoqejnqtqogvjcpg wi0N 36/931 23;81.241PF
Dtqoqfkejnqtqogvjcpg wi0N 35/631 234 81.241PF
Dtqoqhqto wi0N 32/;31 21;81.241PF
Dtqoqogvjcpg wi0N 26/731 89 81.241PF
Ectdqp!fkuwnhkfg wi0N 38/2 O23124681.241PF
Ectdqp!vgvtcejnqtkfg wi0N 37/7 O23124481.241PF
Ejnqtqdgp|gpg wi0N 36/731 239 81.257PF
Ejnqtqgvjcpg wi0N 39/6 O23125481.241PF
Ejnqtqhqto wi0N 36/131 236 81.241PF
Ejnqtqogvjcpg wi0N 35/231 229 81.241PF
eku.2-3.Fkejnqtqgvjgpg wi0N 38/2 O23124681.241PF
eku.2-4.Fkejnqtqrtqrgpg wi0N 33/831 224 81.241PF
Fkdtqoqejnqtqogvjcpg wi0N 35/831 234 81.241PF
Fkdtqoqogvjcpg wi0N 35/731 234 81.241PF
Gvj{ndgp|gpg wi0N 36/531 238 81.241PF
Kqfqogvjcpg wi0N 42/851 8;81.241PF
o'r.Z{ngpg wi0N 5;/251 234 81.241PF
Ogvj{ngpg!Ejnqtkfg wi0N 34/131 226 81.241PF
q.Z{ngpg wi0N 35/431 233 81.241PF
Uv{tgpg wi0N 33/831 225 81.241PF
Vgvtcejnqtqgvjgpg wi0N 34/931 22;81.241PF
Vqnwgpg wi0N 36/231 236 81.266PF
vtcpu.2-3.Fkejnqtqgvjgpg wi0N 38/2 O23124681.241PF
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N 32/931 21;81.241PF
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N 31/831 215 81.241PF
Vtkejnqtqgvjgpg wi0N 36/331 237 7;.262PF
Vtkejnqtqhnwqtqogvjcpg wi0N 39/2 O23125181.241PF
Xkp{n!cegvcvg wi0N 37/7 O2517881.241PF
Xkp{n!ejnqtkfg wi0N 38/9 O23124;81.241PF
2-3.Fkejnqtqgvjcpg.f5!)U*&211 81.241
5.Dtqoqhnwqtqdgp|gpg!)U*&211 81.241
Vqnwgpg.f9!)U*&211 81.241
Rctcogvgt Wpkvu
Fwr
Tguwnv SwcnkhkgtuTRFTguwnv
;33;9;7;118
2855813UCORNG!FWRNKECVG<
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N >2/1>2/1
2-2-2.Vtkejnqtqgvjcpg wi0N >2/1>2/1
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N >2/1>2/1
2-2-3.Vtkejnqtqgvjcpg wi0N >2/1>2/1
2-2.Fkejnqtqgvjcpg wi0N >2/1>2/1
2-2.Fkejnqtqgvjgpg wi0N >2/1>2/1
2-3-4.Vtkejnqtqrtqrcpg wi0N >2/1>2/1
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N >3/1>3/1
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 26 of 36
48!qh!59
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
Fwr
Tguwnv SwcnkhkgtuTRFTguwnv
;33;9;7;118
2855813UCORNG!FWRNKECVG<
2-3.Fkdtqoqgvjcpg!)GFD*wi0N >2/1>2/1
2-3.Fkejnqtqdgp|gpg wi0N >2/1>2/1
2-3.Fkejnqtqgvjcpg wi0N >2/1>2/1
2-3.Fkejnqtqrtqrcpg wi0N >2/1>2/1
2-5.Fkejnqtqdgp|gpg wi0N >2/1>2/1
3.Dwvcpqpg!)OGM*wi0N >6/1>6/1
3.Jgzcpqpg wi0N >6/1>6/1
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N >6/1>6/1
Cegvqpg wi0N >36/1>36/1
Cet{nqpkvtkng wi0N >21/1>21/1
Dgp|gpg wi0N >2/1>2/1
Dtqoqejnqtqogvjcpg wi0N >2/1>2/1
Dtqoqfkejnqtqogvjcpg wi0N >2/1>2/1
Dtqoqhqto wi0N >2/1>2/1
Dtqoqogvjcpg wi0N >3/1>3/1
Ectdqp!fkuwnhkfg wi0N >3/1>3/1
Ectdqp!vgvtcejnqtkfg wi0N >2/1>2/1
Ejnqtqdgp|gpg wi0N >2/1>2/1
Ejnqtqgvjcpg wi0N >2/1>2/1
Ejnqtqhqto wi0N >2/1>2/1
Ejnqtqogvjcpg wi0N >2/1>2/1
eku.2-3.Fkejnqtqgvjgpg wi0N >2/1>2/1
eku.2-4.Fkejnqtqrtqrgpg wi0N >2/1>2/1
Fkdtqoqejnqtqogvjcpg wi0N >2/1>2/1
Fkdtqoqogvjcpg wi0N >2/1>2/1
Gvj{ndgp|gpg wi0N >2/1>2/1
Kqfqogvjcpg wi0N >6/1>6/1
o'r.Z{ngpg wi0N >3/1>3/1
Ogvj{ngpg!Ejnqtkfg wi0N >3/1>3/1
q.Z{ngpg wi0N >2/1>2/1
Uv{tgpg wi0N >2/1>2/1
Vgvtcejnqtqgvjgpg wi0N >2/1>2/1
Vqnwgpg wi0N >2/1>2/1
vtcpu.2-3.Fkejnqtqgvjgpg wi0N >2/1>2/1
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N >2/1>2/1
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N >2/1>2/1
Vtkejnqtqgvjgpg wi0N >2/1>2/1
Vtkejnqtqhnwqtqogvjcpg wi0N >2/1>2/1
Xkp{n!cegvcvg wi0N >3/1>3/1
Xkp{n!ejnqtkfg wi0N >2/1>2/1
Z{ngpg!)Vqvcn*wi0N >3/1>3/1
2-3.Fkejnqtqgvjcpg.f5!)U*&214 3213
5.Dtqoqhnwqtqdgp|gpg!)U*&;;2;;
Vqnwgpg.f9!)U*&211 1211
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 27 of 36
49!qh!59
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
SE!Dcvej<
SE!Dcvej!Ogvjqf<
Cpcn{uku!Ogvjqf<
Cpcn{uku!Fguetkrvkqp<
OUX048133
GRC!9371
GRC!9371
9371!OUX!Nqy!Ngxgn
Cuuqekcvgf!Ncd!Ucorngu< ;33;9;7;119
Rctcogvgt Wpkvu
Dncpm
Tguwnv
Tgrqtvkpi
Nkokv Swcnkhkgtu
OGVJQF!DNCPM< 2854555
Cuuqekcvgf!Ncd!Ucorngu<;33;9;7;119
Ocvtkz< Ycvgt
Cpcn{|gf
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<52
2-2-2.Vtkejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<52
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<52
2-2-3.Vtkejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<52
2-2.Fkejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<52
2-2.Fkejnqtqgvjgpg wi0N >2/1 2/1 16038027!27<52
2-3-4.Vtkejnqtqrtqrcpg wi0N >2/1 2/1 16038027!27<52
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N >3/1 3/1 16038027!27<52
2-3.Fkdtqoqgvjcpg!)GFD*wi0N >2/1 2/1 16038027!27<52
2-3.Fkejnqtqdgp|gpg wi0N >2/1 2/1 16038027!27<52
2-3.Fkejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<52
2-3.Fkejnqtqrtqrcpg wi0N >2/1 2/1 16038027!27<52
2-5.Fkejnqtqdgp|gpg wi0N >2/1 2/1 16038027!27<52
3.Dwvcpqpg!)OGM*wi0N >6/1 6/1 16038027!27<52
3.Jgzcpqpg wi0N >6/1 6/1 16038027!27<52
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N >6/1 6/1 16038027!27<52
Cegvqpg wi0N >36/1 36/1 16038027!27<52
Cet{nqpkvtkng wi0N >21/1 21/1 16038027!27<52
Dgp|gpg wi0N >2/1 2/1 16038027!27<52
Dtqoqejnqtqogvjcpg wi0N >2/1 2/1 16038027!27<52
Dtqoqfkejnqtqogvjcpg wi0N >2/1 2/1 16038027!27<52
Dtqoqhqto wi0N >2/1 2/1 16038027!27<52
Dtqoqogvjcpg wi0N >3/1 3/1 16038027!27<52
Ectdqp!fkuwnhkfg wi0N >3/1 3/1 16038027!27<52
Ectdqp!vgvtcejnqtkfg wi0N >2/1 2/1 16038027!27<52
Ejnqtqdgp|gpg wi0N >2/1 2/1 16038027!27<52
Ejnqtqgvjcpg wi0N >2/1 2/1 16038027!27<52
Ejnqtqhqto wi0N >2/1 2/1 16038027!27<52
Ejnqtqogvjcpg wi0N >2/1 2/1 16038027!27<52
eku.2-3.Fkejnqtqgvjgpg wi0N >2/1 2/1 16038027!27<52
eku.2-4.Fkejnqtqrtqrgpg wi0N >2/1 2/1 16038027!27<52
Fkdtqoqejnqtqogvjcpg wi0N >2/1 2/1 16038027!27<52
Fkdtqoqogvjcpg wi0N >2/1 2/1 16038027!27<52
Gvj{ndgp|gpg wi0N >2/1 2/1 16038027!27<52
Kqfqogvjcpg wi0N >6/1 6/1 16038027!27<52
o'r.Z{ngpg wi0N >3/1 3/1 16038027!27<52
Ogvj{ngpg!Ejnqtkfg wi0N >3/1 3/1 16038027!27<52
q.Z{ngpg wi0N >2/1 2/1 16038027!27<52
Uv{tgpg wi0N >2/1 2/1 16038027!27<52
Vgvtcejnqtqgvjgpg wi0N >2/1 2/1 16038027!27<52
Vqnwgpg wi0N >2/1 2/1 16038027!27<52
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 28 of 36
4;!qh!59
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
Dncpm
Tguwnv
Tgrqtvkpi
Nkokv Swcnkhkgtu
OGVJQF!DNCPM< 2854555
Cuuqekcvgf!Ncd!Ucorngu<;33;9;7;119
Ocvtkz< Ycvgt
Cpcn{|gf
vtcpu.2-3.Fkejnqtqgvjgpg wi0N >2/1 2/1 16038027!27<52
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N >2/1 2/1 16038027!27<52
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N >2/1 2/1 16038027!27<52
Vtkejnqtqgvjgpg wi0N >2/1 2/1 16038027!27<52
Vtkejnqtqhnwqtqogvjcpg wi0N >2/1 2/1 16038027!27<52
Xkp{n!cegvcvg wi0N >3/1 3/1 16038027!27<52
Xkp{n!ejnqtkfg wi0N >2/1 2/1 16038027!27<52
Z{ngpg!)Vqvcn*wi0N >3/1 3/1 16038027!27<52
2-3.Fkejnqtqgvjcpg.f5!)U*&213 81.241 16038027!27<52
5.Dtqoqhnwqtqdgp|gpg!)U*&;;81.241 16038027!27<52
Vqnwgpg.f9!)U*&212 81.241 16038027!27<52
Rctcogvgt Wpkvu
NEU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2854556NCDQTCVQT[!EQPVTQN!UCORNG<
NEUUrkmg
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N 62/;61 215 81.241
2-2-2.Vtkejnqtqgvjcpg wi0N 62/561 214 81.241
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N 61/161 211 81.241
2-2-3.Vtkejnqtqgvjcpg wi0N 5;/361 ;9 81.241
2-2.Fkejnqtqgvjcpg wi0N 61/961 213 81.241
2-2.Fkejnqtqgvjgpg wi0N 61/461 212 81.243
2-3-4.Vtkejnqtqrtqrcpg wi0N 61/;61 213 81.241
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N 59/661 ;8 81.241
2-3.Fkdtqoqgvjcpg!)GFD*wi0N 66/861 222 81.241
2-3.Fkejnqtqdgp|gpg wi0N 65/561 21;81.241
2-3.Fkejnqtqgvjcpg wi0N 59/661 ;8 81.241
2-3.Fkejnqtqrtqrcpg wi0N 59/961 ;9 81.241
2-5.Fkejnqtqdgp|gpg wi0N 61/561 212 81.241
3.Dwvcpqpg!)OGM*wi0N 219211 219 81.256
3.Jgzcpqpg wi0N 222211 222 81.255
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N 223211 223 81.251
Cegvqpg wi0N 215211 215 61.286
Cet{nqpkvtkng wi0N 35;361 211 81.254
Dgp|gpg wi0N 61/261 211 81.241
Dtqoqejnqtqogvjcpg wi0N 63/961 217 81.241
Dtqoqfkejnqtqogvjcpg wi0N 63/361 215 81.241
Dtqoqhqto wi0N 55/661 9;81.241
Dtqoqogvjcpg wi0N 61/261 211 65.241
Ectdqp!fkuwnhkfg wi0N 64/861 218 81.242
Ectdqp!vgvtcejnqtkfg wi0N 62/;61 215 81.243
Ejnqtqdgp|gpg wi0N 63/661 216 81.241
Ejnqtqgvjcpg wi0N 56/561 ;2 75.245
Ejnqtqhqto wi0N 62/261 213 81.241
Ejnqtqogvjcpg wi0N 61/561 212 75.241
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 29 of 36
51!qh!59
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
NEU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2854556NCDQTCVQT[!EQPVTQN!UCORNG<
NEUUrkmg
eku.2-3.Fkejnqtqgvjgpg wi0N 63/161 215 81.242
eku.2-4.Fkejnqtqrtqrgpg wi0N 62/561 214 81.241
Fkdtqoqejnqtqogvjcpg wi0N 64/361 217 81.241
Fkdtqoqogvjcpg wi0N 62/461 214 81.242
Gvj{ndgp|gpg wi0N 62/161 213 81.241
Kqfqogvjcpg wi0N 9;/3211 9;5;.291
o'r.Z{ngpg wi0N 212211 212 81.241
Ogvj{ngpg!Ejnqtkfg wi0N 65/261 219 74.241
q.Z{ngpg wi0N 61/561 212 81.241
Uv{tgpg wi0N 64/961 219 81.241
Vgvtcejnqtqgvjgpg wi0N 57/;61 ;5 81.241
Vqnwgpg wi0N 61/161 211 81.241
vtcpu.2-3.Fkejnqtqgvjgpg wi0N 62/861 214 81.241
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N 61/361 211 81.243
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N 89/1 N16126781.252
Vtkejnqtqgvjgpg wi0N 5;/461 ;;81.241
Vtkejnqtqhnwqtqogvjcpg wi0N 62/;61 215 73.244
Xkp{n!cegvcvg wi0N 219211 219 77.268
Xkp{n!ejnqtkfg wi0N 5;/;61 211 61.261
Z{ngpg!)Vqvcn*wi0N 263261 212 81.241
2-3.Fkejnqtqgvjcpg.f5!)U*&211 81.241
5.Dtqoqhnwqtqdgp|gpg!)U*&213 81.241
Vqnwgpg.f9!)U*&212 81.241
Rctcogvgt Wpkvu
OU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2855814OCVTKZ!URKMG!UCORNG<
OUUrkmg
Tguwnv
;33;;199115
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N 37/4
2-2-2.Vtkejnqtqgvjcpg wi0N 3;/2
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N 34/7
2-2-3.Vtkejnqtqgvjcpg wi0N 35/9
2-2.Fkejnqtqgvjcpg wi0N 38/8
2-2.Fkejnqtqgvjgpg wi0N 3;/1
2-3-4.Vtkejnqtqrtqrcpg wi0N 35/3
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N 35/;
2-3.Fkdtqoqgvjcpg!)GFD*wi0N 37/7
2-3.Fkejnqtqdgp|gpg wi0N 38/2
2-3.Fkejnqtqgvjcpg wi0N 36/3
2-3.Fkejnqtqrtqrcpg wi0N 36/6
2-5.Fkejnqtqdgp|gpg wi0N 37/2
3.Dwvcpqpg!)OGM*wi0N 58/;
3.Jgzcpqpg wi0N 58/8
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N 61/1
Cegvqpg wi0N 56/7
Cet{nqpkvtkng wi0N 229
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 30 of 36
52!qh!59
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
OU
Tguwnv
&!Tge
Nkokvu Swcnkhkgtu&!TgeEqpe/
2855814OCVTKZ!URKMG!UCORNG<
OUUrkmg
Tguwnv
;33;;199115
Dgp|gpg wi0N 38/331 247 81.259PF
Dtqoqejnqtqogvjcpg wi0N 37/;
Dtqoqfkejnqtqogvjcpg wi0N 37/7
Dtqoqhqto wi0N 34/;
Dtqoqogvjcpg wi0N 41/5
Ectdqp!fkuwnhkfg wi0N 3;/2
Ectdqp!vgvtcejnqtkfg wi0N 41/2
Ejnqtqdgp|gpg wi0N 38/2
Ejnqtqgvjcpg wi0N 41/9
Ejnqtqhqto wi0N 3;/4
Ejnqtqogvjcpg wi0N 41/5
eku.2-3.Fkejnqtqgvjgpg wi0N 38/;
eku.2-4.Fkejnqtqrtqrgpg wi0N 37/8
Fkdtqoqejnqtqogvjcpg wi0N 37/1
Fkdtqoqogvjcpg wi0N 36/7
Gvj{ndgp|gpg wi0N 38/3 O23124681.241PF
Kqfqogvjcpg wi0N 62/5
o'r.Z{ngpg wi0N 64/3 O25124481.241PF
Ogvj{ngpg!Ejnqtkfg wi0N 35/;
q.Z{ngpg wi0N 36/931 23;81.241PF
Uv{tgpg wi0N 37/9
Vgvtcejnqtqgvjgpg wi0N 36/9
Vqnwgpg wi0N 38/331 247 81.266PF
vtcpu.2-3.Fkejnqtqgvjgpg wi0N 39/8
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N 36/7
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N 34/3
Vtkejnqtqgvjgpg wi0N 37/;
Vtkejnqtqhnwqtqogvjcpg wi0N 43/2
Xkp{n!cegvcvg wi0N 64/;
Xkp{n!ejnqtkfg wi0N 39/4
2-3.Fkejnqtqgvjcpg.f5!)U*&212 81.241
5.Dtqoqhnwqtqdgp|gpg!)U*&211 81.241
Vqnwgpg.f9!)U*&211 81.241
Rctcogvgt Wpkvu
Fwr
Tguwnv SwcnkhkgtuTRFTguwnv
;33;;199116
2855815UCORNG!FWRNKECVG<
2-2-2-3.Vgvtcejnqtqgvjcpg wi0N >2/1
2-2-2.Vtkejnqtqgvjcpg wi0N >2/1
2-2-3-3.Vgvtcejnqtqgvjcpg wi0N >2/1
2-2-3.Vtkejnqtqgvjcpg wi0N >2/1
2-2.Fkejnqtqgvjcpg wi0N >2/1
2-2.Fkejnqtqgvjgpg wi0N >2/1
2-3-4.Vtkejnqtqrtqrcpg wi0N >2/1
2-3.Fkdtqoq.4.ejnqtqrtqrcpg wi0N >3/1
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 31 of 36
53!qh!59
$?SE$
QUALITY CONTROL DATA
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Rctcogvgt Wpkvu
Fwr
Tguwnv SwcnkhkgtuTRFTguwnv
;33;;199116
2855815UCORNG!FWRNKECVG<
2-3.Fkdtqoqgvjcpg!)GFD*wi0N >2/1
2-3.Fkejnqtqdgp|gpg wi0N >2/1
2-3.Fkejnqtqgvjcpg wi0N >2/1
2-3.Fkejnqtqrtqrcpg wi0N >2/1
2-5.Fkejnqtqdgp|gpg wi0N >2/1
3.Dwvcpqpg!)OGM*wi0N >6/1
3.Jgzcpqpg wi0N >6/1
5.Ogvj{n.3.rgpvcpqpg!)OKDM*wi0N >6/1
Cegvqpg wi0N >36/1
Cet{nqpkvtkng wi0N >21/1
Dgp|gpg wi0N >2/1PF
Dtqoqejnqtqogvjcpg wi0N >2/1
Dtqoqfkejnqtqogvjcpg wi0N >2/1
Dtqoqhqto wi0N >2/1
Dtqoqogvjcpg wi0N >3/1
Ectdqp!fkuwnhkfg wi0N >3/1
Ectdqp!vgvtcejnqtkfg wi0N >2/1
Ejnqtqdgp|gpg wi0N >2/1
Ejnqtqgvjcpg wi0N >2/1
Ejnqtqhqto wi0N 5/2
Ejnqtqogvjcpg wi0N >2/1
eku.2-3.Fkejnqtqgvjgpg wi0N >2/1
eku.2-4.Fkejnqtqrtqrgpg wi0N >2/1
Fkdtqoqejnqtqogvjcpg wi0N >2/1
Fkdtqoqogvjcpg wi0N >2/1
Gvj{ndgp|gpg wi0N >2/1PF
Kqfqogvjcpg wi0N >6/1
o'r.Z{ngpg wi0N >3/1PF
Ogvj{ngpg!Ejnqtkfg wi0N >3/1
q.Z{ngpg wi0N >2/1PF
Uv{tgpg wi0N >2/1
Vgvtcejnqtqgvjgpg wi0N >2/1
Vqnwgpg wi0N >2/1PF
vtcpu.2-3.Fkejnqtqgvjgpg wi0N >2/1
vtcpu.2-4.Fkejnqtqrtqrgpg wi0N >2/1
vtcpu.2-5.Fkejnqtq.3.dwvgpg wi0N >2/1
Vtkejnqtqgvjgpg wi0N >2/1
Vtkejnqtqhnwqtqogvjcpg wi0N >2/1
Xkp{n!cegvcvg wi0N >3/1
Xkp{n!ejnqtkfg wi0N >2/1
Z{ngpg!)Vqvcn*wi0N >3/1PF
2-3.Fkejnqtqgvjcpg.f5!)U*&216 5211
5.Dtqoqhnwqtqdgp|gpg!)U*&;8 2;9
Vqnwgpg.f9!)U*&211 2212
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
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$?SN$
QUALIFIERS
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
DEFINITIONS
FH!.!Fknwvkqp!Hcevqt-!kh!tgrqtvgf-!tgrtgugpvu!vjg!hcevqt!crrnkgf!vq!vjg!tgrqtvgf!fcvc!fwg!vq!fknwvkqp!qh!vjg!ucorng!cnkswqv/
PF!.!Pqv!Fgvgevgf!cv!qt!cdqxg!cflwuvgf!tgrqtvkpi!nkokv/
L!.!Guvkocvgf!eqpegpvtcvkqp!cdqxg!vjg!cflwuvgf!ogvjqf!fgvgevkqp!nkokv!cpf!dgnqy!vjg!cflwuvgf!tgrqtvkpi!nkokv/
OFN!.!Cflwuvgf!Ogvjqf!Fgvgevkqp!Nkokv/
RSN!.!Rtcevkecn!Swcpvkvcvkqp!Nkokv/
TN!.!Tgrqtvkpi!Nkokv/
U!.!Uwttqicvg
2-3.Fkrjgp{nj{ftc|kpg!fgeqorqugu!vq!cpf!ecppqv!dg!ugrctcvgf!htqo!C|qdgp|gpg!wukpi!Ogvjqf!9381/!Vjg!tguwnv!hqt!gcej!cpcn{vg!ku
c!eqodkpgf!eqpegpvtcvkqp/
Eqpukuvgpv!ykvj!GRC!iwkfgnkpgu-!wptqwpfgf!fcvc!ctg!fkurnc{gf!cpf!jcxg!dggp!wugf!vq!ecnewncvg!&!tgeqxgt{!cpf!TRF!xcnwgu/
NEU)F*!.!Ncdqtcvqt{!Eqpvtqn!Ucorng!)Fwrnkecvg*
OU)F*!.!Ocvtkz!Urkmg!)Fwrnkecvg*
FWR!.!Ucorng!Fwrnkecvg
TRF!.!Tgncvkxg!Rgtegpv!Fkhhgtgpeg
PE!.!Pqv!Ecnewncdng/
UI!.!Uknkec!Ign!.!Engcp.Wr
W!.!Kpfkecvgu!vjg!eqorqwpf!ycu!cpcn{|gf!hqt-!dwv!pqv!fgvgevgf/
Cekf!rtgugtxcvkqp!oc{!pqv!dg!crrtqrtkcvg!hqt!3!Ejnqtqgvj{nxkp{n!gvjgt-!Uv{tgpg-!cpf!Xkp{n!ejnqtkfg/
C!ugrctcvg!xkcn!rtgugtxgf!vq!c!rJ!qh!5.6!ku!tgeqoogpfgf!kp!UY957!Ejcrvgt!5!hqt!vjg!cpcn{uku!qh!Cetqngkp!cpf!Cet{nqpkvtkng!d{!GRC
Ogvjqf!9371/
P.Pkvtquqfkrjgp{ncokpg!fgeqorqugu!cpf!ecppqv!dg!ugrctcvgf!htqo!Fkrjgp{ncokpg!wukpi!Ogvjqf!9381/!!Vjg!tguwnv!tgrqtvgf!hqtgcej!cpcn{vg!ku!c!eqodkpgf!eqpegpvtcvkqp/
Rceg!Cpcn{vkecn!ku!VPK!ceetgfkvgf/!Eqpvcev!{qwt!Rceg!RO!hqt!vjg!ewttgpv!nkuv!qh!ceetgfkvgf!cpcn{vgu/
VPK!.!Vjg!PGNCE!Kpuvkvwvg/
LABORATORIES
Rceg!Cpcn{vkecn!Ugtxkegu!.!EjctnqvvgRCUK.E
ANALYTE QUALIFIERS
Eqooqp!Ncdqtcvqt{!Eqpvcokpcpv/E;
Cpcn{vg!tgeqxgt{!kp!vjg!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!ycu!qwvukfg!SE!nkokvu/N1
Cpcn{vg!tgeqxgt{!kp!vjg!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!gzeggfgf!SE!nkokvu/!Cpcn{vg!rtgugpeg!dgnqy!tgrqtvkpi!nkokvu!kp
cuuqekcvgf!ucorngu/!!Tguwnvu!wpchhgevgf!d{!jkij!dkcu/N4
Ocvtkz!urkmg!tgeqxgt{!gzeggfgf!SE!nkokvu/!!Dcvej!ceegrvgf!dcugf!qp!ncdqtcvqt{!eqpvtqn!ucorng!)NEU*!tgeqxgt{/O2
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 33 of 36
55!qh!59
$?ET$
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Rceg!Rtqlgev!Pq/<
Rtqlgev<
;33;9;7;
L27161762!OEIWKTG!NH
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92298969001 OUX0481322016014828 DP-5 GRC!9371
92298969002 OUX0481322016014829 DP-6 GRC!9371
92298969003 OUX0481322016014830 DP-7 GRC!9371
92298969004 OUX0481322016014831 DP-8 GRC!9371
92298969005 OUX0481322016014832 DP-9 GRC!9371
92298969006 OUX0481322016014833 DP-10 GRC!9371
92298969007 OUX0481322016014834 DP-11 GRC!9371
92298969008 OUX0481332016014835 DP-12 GRC!9371
REPORT OF LABORATORY ANALYSIS
Vjku!tgrqtv!ujcnn!pqv!dg!tgrtqfwegf-!gzegrv!kp!hwnn-
ykvjqwv!vjg!ytkvvgp!eqpugpv!qh!Rceg!Cpcn{vkecn!Ugtxkegu-!Kpe//Fcvg<!1703203127!1;<25!CO
Pace Analytical Services, Inc.
;911!Mkpeg{!Cxg/!!Uwkvg!211
Jwpvgtuxknng-!PE!39189
)815*986.;1;3
Page 34 of 36
56!qh!59
Page 35 of 36
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Page 36 of 36
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5 9 !q h !5 9