19070_Polo_Fmr_Gussman_Limited_CSA_20150910

Analytical Report 511162
for
Terraquest Environmental Consultants, P.C.
Project Manager: Jonathan Grubbs
Gussman Cleaners
17-JUL-15
05015
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (T104704215-15-19), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
Oklahoma (9218)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Texas (T104704477), Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)
Collected By: Client
Page 1 of 25 Final 1.000
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Project Manager: Jonathan Grubbs
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302

Reference: XENCO Report No(s): 511162
Gussman Cleaners
Project Address: NC
Jonathan Grubbs:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 511162. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 511162 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
17-JUL-15
Project Manager
Debbie Simmons
Page 2 of 25 Final 1.000
Sample Cross Reference 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
Sample Id
MW1 07-06-15 13:38
Date Collected Lab Sample Id
511162-001
Sample DepthMatrix
W
Page 3 of 25 Final 1.000
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4143 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd , Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
2505 North Falkenburg Rd, Tampa, FL 33619
12600 West I-20 East, Odessa, TX 79765
6017 Financial Drive, Norcross, GA 30071
3725 E. Atlanta Ave, Phoenix, AZ 85040
Phone Fax
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone]
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non-Calculable
+ NELAC certification not offered for this compound.

* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Page 4 of 25 Final 1.000
Hits Summary 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
07.09.15 09.53 Date Received :
% Moisture :
07.06.15 13.38 Date Collected : 511162-001Lab Sample Id :
Ground WaterMatrix : MW1Sample Id :
MADEP EPH
MADEP VPH
SVOCs by EPA 625 + 10 TICs
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
Analytical Method :
Analytical Method :
SW3510C
SW5030B
E625P
SM6200B_PREP
Prep Method:
Prep Method:
Prep Method:
Prep Method:
07.15.15 10.15
07.10.15 01.59
07.13.15 15.35
07.10.15 06.44
Date Prep:
Date Prep:
Date Prep:
Date Prep:
C11-C22 Aromatics
C19-C36 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
1-Methylnaphthalene +
Benzyl Alcohol
bis(2-ethylhexyl) phthalate
unknown hydrocarbon (TIC)
9-Hexacosene (TIC)
Hexadecanoic acid, methyl ester (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
Benzene, propyl- (TIC)
Benzene, 1,2,3,5-tetramethyl- (TIC)
unknown (TIC)
1-Docosanol (TIC)
4-Isopropyltoluene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
tert-Butylbenzene
Parameter
Parameter
Parameter
Parameter
Result
Result
Result
Result
J
J
JN
JN
JN
JN
JN
JN
JN
JN
JN
JN
Flag
Flag
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
Units
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Dil
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
Cas Number
C11C22
ALHYDRC19
HYDC9C10
ALHYDRC9C
90-12-0
100-51-6
117-81-7
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
99-87-6
104-51-8
103-65-1
135-98-8
98-06-6
117
102
185
260
2.95
1.57
24.9
7.34
12.2
7.52
9.00
10.5
7.69
9.71
16.9
8.59
26.2
5.59
3.16
32.0
19.4
15.7
972426
972113
972298
972014
Seq Number
Seq Number
Seq Number
Seq Number
07.16.15 13.58
07.15.15 22.32
07.10.15 07.12
07.10.15 07.12
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Page 5 of 25 Final 1.000
Certificate of Analytical Results 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
07.09.15 09.53 Date Received:
07.06.15 13.38 Date Collected:511162-001Lab Sample Id:
Ground WaterMatrix: MW1Sample Id:
MADEP EPH Analytical Method:
CLARAnalyst:
SW3510CPrep Method:
07.15.15 10.15 Date Prep:
BROTech:
C11-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
Parameter
98.5
98.5
98.5
Result
U
98.5
98.5
98.5
Flag
ug/L
ug/L
ug/L
Units
1
1
1
DilCas Number
C11C22
ALHYDRC9C18
ALHYDRC19C3
117
U
102
972426Seq Number:
RL MDL
07.16.15 13.58
07.15.15 22.32
07.15.15 22.32
Analysis Date
Surrogate
40-140
40-140
40-140
%
Recovery
**
Flag
%
%
%
31
60
73
07.15.15 22.32
07.16.15 13.58
07.16.15 13.58
Cas Number
3386-33-2
84-15-1
321-60-8
Units Analysis Date
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
Limits
% Moisture:
Page 6 of 25 Final 1.000
Certificate of Analytical Results 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
07.09.15 09.53 Date Received:
07.06.15 13.38 Date Collected:511162-001Lab Sample Id:
Ground WaterMatrix: MW1Sample Id:
SVOCs by EPA 625 + 10 TICs Analytical Method:
VICAnalyst:
E625PPrep Method:
07.13.15 15.35 Date Prep:
BROTech:
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Diphenylhydrazine (as Azobenzene)
1,3-Dichlorobenzene
1,3-Dinitrobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3-Dichlorobenzidine
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Alcohol
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Parameter
1.41
1.80
4.69
2.08
19.8
1.59
1.38
1.62
1.75
1.61
7.00
1.27
1.80
1.17
1.97
1.92
2.51
3.82
1.38
2.09
2.15
3.04
1.33
2.37
1.41
1.46
1.98
1.87
1.77
1.94
1.94
2.67
2.18
1.21
1.23
1.75
1.22
1.18
1.79
Result
U
U
U
UL
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ULF
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
9.85
9.85
9.85
9.85
49.3
9.85
9.85
9.85
9.85
9.85
19.7
9.85
9.85
9.85
9.85
9.85
19.7
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
19.7
9.85
9.85
9.85
9.85
9.85
9.85
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
120-82-1
95-50-1
122-66-7
541-73-1
99-65-0
106-46-7
90-12-0
88-06-2
120-83-2
105-67-9
51-28-5
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
15831-10-4
91-94-1
534-52-1
101-55-3
59-50-7
106-47-8
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
111-91-1
111-44-4
39638-32-9
117-81-7
85-68-7
U
U
U
U
U
U
2.95
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.57
U
U
U
24.9
U
972298Seq Number:
RL MDL
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
Analysis Date
% Moisture:
Page 7 of 25 Final 1.000
Certificate of Analytical Results 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
07.09.15 09.53 Date Received:
07.06.15 13.38 Date Collected:511162-001Lab Sample Id:
Ground WaterMatrix: MW1Sample Id:
SVOCs by EPA 625 + 10 TICs Analytical Method:
VICAnalyst:
E625PPrep Method:
07.13.15 15.35 Date Prep:
BROTech:
Chrysene
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-c,d)Pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodi-n-Propylamine
n-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1-Docosanol (TIC)
9-Hexacosene (TIC)
Benzene, 1,2,3,5-tetramethyl- (TIC)
Benzene, propyl- (TIC)
Hexadecanoic acid, methyl ester (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown hydrocarbon (TIC)
Parameter
2.06
1.80
1.62
1.87
1.94
2.05
1.36
1.78
1.54
2.18
1.75
1.84
2.34
1.84
1.39
1.50
1.47
1.34
2.46
2.23
2.01
1.73
2.36

Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UH
U
U
U
JN
JN
JN
JN
JN
JN
JN
JN
JN
JN
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85

Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
218-01-9
53-70-3
132-64-9
84-66-2
131-11-3
84-74-2
117-84-0
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
26.2
12.2
16.9
9.71
7.52
10.5
7.69
9.00
8.59
7.34
972298Seq Number:
RL MDL
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
Analysis Date
Surrogate
44-117
30-100
48-127
46-111
50-200
%
Recovery
**
Flag
%
%
%
%
%
65
21
48
69
54
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
07.14.15 15.24
Cas Number
321-60-8
367-12-4
118-79-6
4165-60-0
4165-62-2
Units Analysis Date
2-Fluorobiphenyl
2-Fluorophenol
2,4,6-Tribromophenol
Nitrobenzene-d5
Phenol-d5
Limits
% Moisture:
Page 8 of 25 Final 1.000
Certificate of Analytical Results 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
07.09.15 09.53 Date Received:
07.06.15 13.38 Date Collected:511162-001Lab Sample Id:
Ground WaterMatrix: MW1Sample Id:
SVOCs by EPA 625 + 10 TICs
MADEP VPH
Analytical Method:
Analytical Method:
VIC
ZHO
Analyst:
Analyst:
E625P
SW5030B
Prep Method:
Prep Method:
07.13.15 15.35
07.10.15 01.59
Date Prep:
Date Prep:
BRO
ZHO
Tech:
Tech:
C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
Parameter
0.0150
0.00500
0.0150
Result
U0.0150
0.00500
0.0150
Flag
ug/L
ug/L
ug/L
Units
1
1
1
DilCas Number
ALHYDRC5C8
HYDC9C10
ALHYDRC9C12
U
185
260
972298
972113
Seq Number:
Seq Number:
RL MDL
07.10.15 07.12
07.10.15 07.12
07.10.15 07.12
Analysis Date
Surrogate
Surrogate
46-126
70-130
70-130
%
Recovery
%
Recovery
Flag
Flag
%
%
%
84
111
95
07.14.15 15.24
07.10.15 07.12
07.10.15 07.12
Cas Number
Cas Number
1718-51-0
615-59-8
615-59-8
Units
Units
Analysis Date
Analysis Date
Terphenyl-D14
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Limits
Limits
% Moisture:
% Moisture:
Page 9 of 25 Final 1.000
Certificate of Analytical Results 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
07.09.15 09.53 Date Received:
07.06.15 13.38 Date Collected:511162-001Lab Sample Id:
Ground WaterMatrix: MW1Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
07.10.15 06.44 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
5.59
U
U
U
U
U
U
U
U
U
U
U
U
U
U
972014Seq Number:
RL MDL
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
Analysis Date
% Moisture:
Page 10 of 25 Final 1.000
Certificate of Analytical Results 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
07.09.15 09.53 Date Received:
07.06.15 13.38 Date Collected:511162-001Lab Sample Id:
Ground WaterMatrix: MW1Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
07.10.15 06.44 Date Prep:
ZHOTech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
UHF
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
3.16
32.0
19.4
U
15.7
U
U
U
U
U
U
U
U
U
U
972014Seq Number:
RL MDL
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
116
107
92
07.10.15 15.52
07.10.15 15.52
07.10.15 15.52
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 11 of 25 Final 1.000
QC Summary 511162
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
695254-1-BLKMB Sample Id:
WaterMatrix:
MADEP EPH Analytical Method:SW3510CPrep Method:
07.15.15Date Prep:
C11-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
Parameter %RPD Flag
40
40
40
RPD
Limit
3
35
36
972426Seq Number:
07.16.15 12:47
07.15.15 21:28
07.15.15 21:28
Analysis
Date
Limits
40-140
40-140
40-140
LCSD
%Rec
63
42
68
LCSD
Result
1070
252
546
LCS
%Rec
61
60
99
1040
358
788
Spike
Amount
1700
600
800
MB
Result
<100
<100
<100
695254-1-BKSLCS Sample Id:695254-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
UnitsLCS
Result
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
Surrogate LCSD
Flag
07.15.15 21:28
07.16.15 12:47
07.16.15 12:47
Analysis
DateLimits
40-140
40-140
40-140
LCSD
%Rec
74
111
65
LCS
%Rec
78
88
63
MB
%Rec
81
74
66
%
%
%
UnitsLCS
Flag
MB
Flag
Page 12 of 25 Final 1.000
QC Summary 511162
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
695090-1-BLKMB Sample Id:
WaterMatrix:
SVOCs by EPA 625 + 10 TICs Analytical Method:E625PPrep Method:
07.13.15Date Prep:
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Diphenylhydrazine (as Azobenzene)
1,3-Dichlorobenzene
1,3-Dinitrobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl Alcohol
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-c,d)Pyrene
Isophorone
Parameter %RPD
L
LF
Flag
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
RPD
Limit
9
10
7
8
6
7
4
4
6
9
7
1
10
7
9
9
10
6
5
2
168
6
9
4
1
5
6
6
1
7
18
8
7
11
10
6
5
6
7
6
6
6
5
6
5
4
8
6
6
9
7
2
972298Seq Number:
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
Analysis
Date
Limits
44-142
32-129
55-115
65-135
45-110
20-124
25-175
37-144
39-135
32-119
0-191
60-118
36-120
45-105
40-110
29-182
30-110
10-181
53-127
22-147
15-110
25-158
0-132
47-145
33-145
27-133
33-143
17-163
24-159
0-219
11-162
30-110
33-184
12-158
36-166
8-158
0-152
17-168
0-227
55-105
0-114
0-112
1-118
0-107
26-137
59-121
0-152
24-116
41-125
40-113
0-171
21-196
LCSD
%Rec
63
59
81
59
102
59
67
82
70
67
107
70
61
68
65
73
67
105
82
82
86
79
90
74
81
87
89
97
97
85
89
70
65
60
66
102
100
79
87
76
88
84
92
106
87
78
86
64
93
60
86
95
LCSD
Result
31.3
29.6
40.4
29.7
51.1
29.6
33.6
41.0
34.9
33.3
53.3
34.8
30.7
33.8
32.5
36.6
33.4
52.4
41.1
41.0
43.1
39.6
44.9
36.9
40.6
43.3
44.3
48.5
48.3
42.5
44.5
34.9
32.5
30.2
33.1
51.1
50.2
39.3
43.4
38.2
43.8
42.0
46.1
53.0
43.5
38.8
43.2
32.0
46.3
30.0
42.9
47.6
LCS
%Rec
68
66
75
64
96
64
70
79
74
73
99
70
68
72
71
80
74
99
78
81
8
75
82
71
80
82
84
91
96
79
74
76
70
68
73
96
96
74
81
72
82
79
88
99
82
74
80
68
99
66
80
97
34.1
32.8
37.6
32.2
47.9
31.9
35.1
39.4
37.0
36.4
49.6
35.0
34.0
36.2
35.5
40.2
37.0
49.4
39.0
40.3
3.75
37.3
41.0
35.6
40.0
41.0
41.9
45.5
48.0
39.5
37.2
37.9
34.9
33.8
36.7
48.1
47.9
36.9
40.3
36.1
41.2
39.5
43.8
49.7
41.2
37.1
39.9
34.1
49.4
32.8
40.1
48.6
Spike
Amount
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
MB
Result
<1.43
<1.83
<4.76
<2.11
<20.1
<1.61
<1.40
<1.64
<1.78
<1.63
<7.11
<1.29
<1.83
<1.19
<2.00
<1.95
<2.55
<1.40
<2.12
<2.18
<3.09
<1.35
<2.41
<1.43
<1.48
<2.01
<1.90
<1.80
<1.97
<1.97
<2.71
<1.23
<1.25
<1.78
<1.24
<1.20
<1.82
<2.09
<1.83
<1.64
<1.90
<1.97
<2.08
<1.38
<1.81
<1.56
<2.21
<1.78
<1.87
<2.38
<1.87
<1.41
695090-1-BKSLCS Sample Id:695090-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 13 of 25 Final 1.000
QC Summary 511162
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
695090-1-BLK
695065-1-BLK
511162-001
MB Sample Id:
MB Sample Id:
Parent Sample Id:
Water
Water
Ground Water
Matrix:
Matrix:
Matrix:
SVOCs by EPA 625 + 10 TICs
MADEP VPH
MADEP VPH
Analytical Method:
Analytical Method:
Analytical Method:
E625P
SW5030B
SW5030B
Prep Method:
Prep Method:
Prep Method:
07.13.15
07.10.15
07.10.15
Date Prep:
Date Prep:
Date Prep:
Naphthalene
Nitrobenzene
n-Nitrosodi-n-Propylamine
n-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
Parameter
Parameter
Parameter
%RPD
%RPD
H
Flag
Flag
Flag
30
30
30
30
30
30
30
30
25
25
25
RPD
Limit
RPD
Limit
8
8
6
6
8
7
0
3
11
3
6
972298
972113
972113
Seq Number:
Seq Number:
Seq Number:
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.10.15 10:10
07.10.15 10:10
07.10.15 10:10
07.10.15 07:57
07.10.15 07:57
07.10.15 07:57
Analysis
Date
Analysis
Date
Analysis
Date
Limits
Limits
Limits
21-133
35-180
10-230
50-110
14-76
54-120
5-112
23-152
70-130
70-130
70-130
70-130
70-130
70-130
LCSD
%Rec
LCSD
%Rec
62
66
78
106
83
79
63
90
108
100
106
LCSD
Result
LCSD
Result
30.9
33.0
38.8
52.8
41.4
39.7
31.3
45.2
162
49.9
159
LCS
%Rec
LCS
%Rec
MS
%Rec
67
71
83
100
77
74
63
87
97
103
100
95
92
94
33.6
35.7
41.4
49.8
38.3
37.1
31.3
43.7
145
51.3
150
143
231
401
Spike
Amount
Spike
Amount
Spike
Amount
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
150
50.0
150
150
50.0
150
MB
Result
MB
Result
Parent
Result
<1.52
<1.49
<1.36
<2.50
<2.26
<2.04
<1.76
<2.40
<0.0150
<0.00500
<0.0150
<0.0150
185
260
695090-1-BKS
695065-1-BKS
511162-001 S
LCS Sample Id:
LCS Sample Id:
MS Sample Id:
695090-1-BSD
695065-1-BSD
LCSD Sample Id:
LCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
Units
LCS
Result
LCS
Result
MS
Result
2-Fluorobiphenyl
2-Fluorophenol
2,4,6-Tribromophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-D14
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Surrogate
Surrogate
Surrogate
LCSD
Flag
LCSD
Flag
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.14.15 14:27
07.10.15 10:10
07.10.15 10:10
07.10.15 07:57
07.10.15 07:57
Analysis
Date
Analysis
Date
Analysis
Date
Limits
Limits
Limits
39-99
33-92
32-129
37-94
50-200
18-133
70-130
70-130
70-130
70-130
LCSD
%Rec
LCSD
%Rec
65
56
94
67
59
79
94
103
LCS
%Rec
LCS
%Rec
MS
%Rec
61
58
83
69
61
73
86
91
111
97
MB
%Rec
MB
%Rec
69
68
93
80
68
86
89
93
%
%
%
%
%
%
%
%
%
%
Units
Units
Units
LCS
Flag
LCS
Flag
MS
Flag
MB
Flag
MB
Flag
Page 14 of 25 Final 1.000
QC Summary 511162
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
694979-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
07.10.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD
HF
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
5
5
2
5
2
6
6
2
4
1
2
2
3
2
3
2
4
4
2
2
0
3
1
3
1
5
5
4
2
2
2
3
14
2
5
3
11
4
6
2
0
61
1
5
0
3
2
0
1
1
3
2
972014Seq Number:
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
Analysis
Date
Limits
75-127
62-128
77-129
86-120
82-114
73-123
83-125
57-127
79-118
59-125
84-118
83-126
83-128
56-133
85-121
86-118
90-126
85-121
88-121
76-126
66-133
80-128
70-130
82-130
80-128
74-129
51-143
81-123
84-114
89-127
79-129
73-140
53-143
66-136
88-118
73-139
70-123
72-118
65-125
85-125
92-126
48-143
61-133
87-123
77-125
82-115
53-149
75-119
52-116
83-130
84-122
86-120
LCSD
%Rec
105
102
111
105
99
95
104
105
96
107
105
104
102
107
105
104
102
108
100
101
98
106
117
107
104
103
99
98
108
91
111
110
95
103
102
99
99
99
99
96
112
148
102
105
102
106
98
102
113
108
108
102
LCSD
Result
26.2
25.4
27.7
26.3
24.8
23.8
25.9
26.3
24.0
26.8
26.3
26.1
25.4
26.8
26.3
26.1
25.5
27.0
25.0
25.3
49.1
26.4
58.7
26.7
26.0
51.7
49.6
24.4
27.0
22.8
27.8
27.5
23.7
25.7
25.4
24.8
24.8
24.8
24.8
24.1
28.1
36.9
1020
26.2
25.5
26.5
48.9
25.5
28.3
26.9
27.0
25.5
LCS
%Rec
100
97
109
100
97
90
98
107
92
108
103
102
99
105
102
103
98
104
98
100
98
103
119
103
103
108
104
94
106
93
109
106
82
101
97
96
89
96
94
94
112
78
103
100
102
102
99
102
112
106
105
100
25.0
24.2
27.2
25.1
24.3
22.5
24.4
26.8
23.0
27.1
25.8
25.5
24.7
26.3
25.5
25.7
24.6
26.0
24.4
24.9
49.2
25.7
59.3
25.8
25.8
54.2
52.1
23.5
26.4
23.2
27.2
26.6
20.5
25.2
24.2
24.1
22.2
23.9
23.4
23.6
28.1
19.6
1030
25.0
25.4
25.6
49.7
25.4
28.0
26.5
26.3
25.1
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
MB
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
694979-1-BKSLCS Sample Id:694979-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 15 of 25 Final 1.000
QC Summary 511162
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
694979-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
07.10.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
4
2
7
7
4
3
4
11
0
6
1
3
972014Seq Number:
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
Analysis
Date
Limits
85-123
79-126
64-131
89-116
78-118
86-127
82-119
46-144
58-141
76-122
90-125
86-119
LCSD
%Rec
102
103
98
103
95
119
99
104
110
99
99
100
LCSD
Result
25.5
25.8
24.5
25.7
23.8
29.8
24.7
25.9
27.4
24.7
49.5
25.0
LCS
%Rec
98
102
91
96
91
116
95
93
109
93
98
97
24.6
25.4
22.8
24.0
22.8
29.0
23.8
23.3
27.3
23.2
48.9
24.2
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
MB
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
694979-1-BKSLCS Sample Id:694979-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate LCSD
Flag
07.10.15 07:37
07.10.15 07:37
07.10.15 07:37
Analysis
Date
Limits
65-126
86-111
83-116
LCSD
%Rec
110
106
109
LCS
%Rec
109
107
110
MB
%Rec
117
111
107
%
%
%
UnitsLCS
Flag
MB
Flag
Page 16 of 25 Final 1.000
Blank Summary 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
694979-1-BLKLab Sample Id:
WATERMatrix: 694979-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
07.10.15 06:44Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
972014Seq Number:
MDLRL
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
Analysis
Date
Page 17 of 25 Final 1.000
Blank Summary 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
694979-1-BLKLab Sample Id:
WATERMatrix: 694979-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
07.10.15 06:44Date Prep:
ZHOTech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
972014Seq Number:
MDLRL
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
07.10.15 10:32
Analysis
Date
Page 18 of 25 Final 1.000
Blank Summary 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
695065-1-BLKLab Sample Id:
WATERMatrix: 695065-1-BLK Sample Id:
MADEP VPH Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
07.10.15 01:59Date Prep:
ZHOTech:
C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
Parameter
0.0150
0.00500
0.0150
Result
U
U
U
0.0150
0.00500
0.0150
Flag
ug/L
ug/L
ug/L
Units
1
1
1
DilCas Number
ALHYDRC5C8
HYDC9C10
ALHYDRC9C1
U
U
U
972113Seq Number:
MDLRL
07.10.15 05:43
07.10.15 05:43
07.10.15 05:43
Analysis
Date
Page 19 of 25 Final 1.000
Blank Summary 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
695090-1-BLKLab Sample Id:
WATERMatrix: 695090-1-BLK Sample Id:
SVOCs by EPA 625 + 10 TICs Analytical Method:
VICAnalyst:
E625PPrep Method:
07.13.15 15:35Date Prep:
BROTech:
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Diphenylhydrazine (as Azobenzene)
1,3-Dichlorobenzene
1,3-Dinitrobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene +
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3-Dichlorobenzidine
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Alcohol
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Parameter
1.43
1.83
4.76
2.11
20.1
1.61
1.40
1.64
1.78
1.63
7.11
1.29
1.83
1.19
2.00
1.95
2.55
3.88
1.40
2.12
2.18
3.09
1.35
2.41
1.43
1.48
2.01
1.90
1.80
1.97
1.97
2.71
2.21
1.23
1.25
1.78
1.24
1.20
1.82
2.09
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
10.0
10.0
10.0
10.0
50.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
120-82-1
95-50-1
122-66-7
541-73-1
99-65-0
106-46-7
90-12-0
88-06-2
120-83-2
105-67-9
51-28-5
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
15831-10-4
91-94-1
534-52-1
101-55-3
59-50-7
106-47-8
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
111-91-1
111-44-4
39638-32-9
117-81-7
85-68-7
218-01-9
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
972298Seq Number:
MDLRL
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
Analysis
Date
Page 20 of 25 Final 1.000
Blank Summary 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
695090-1-BLKLab Sample Id:
WATERMatrix: 695090-1-BLK Sample Id:
SVOCs by EPA 625 + 10 TICs Analytical Method:
VICAnalyst:
E625PPrep Method:
07.13.15 15:35Date Prep:
BROTech:
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-c,d)Pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodi-n-Propylamine
n-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Parameter
1.83
1.64
1.90
1.97
2.08
1.38
1.81
1.56
2.21
1.78
1.87
2.38
1.87
1.41
1.52
1.49
1.36
2.50
2.26
2.04
1.76
2.40
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
53-70-3
132-64-9
84-66-2
131-11-3
84-74-2
117-84-0
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
972298Seq Number:
MDLRL
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
07.14.15 13:59
Analysis
Date
Page 21 of 25 Final 1.000
Blank Summary 511162
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
695254-1-BLKLab Sample Id:
WATERMatrix: 695254-1-BLK Sample Id:
MADEP EPH Analytical Method:
CLARAnalyst:
SW3510CPrep Method:
07.15.15 10:15Date Prep:
BROTech:
C11-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
Parameter
100
100
100
Result
U
U
U
100
100
100
Flag
ug/L
ug/L
ug/L
Units
1
1
1
DilCas Number
C11C22
ALHYDRC9C1
ALHYDRC19C
U
U
U
972426Seq Number:
MDLRL
07.16.15 12:11
07.15.15 20:56
07.15.15 20:56
Analysis
Date
Page 22 of 25 Final 1.000
Page 23 of 25 Final 1.000
Page 24 of 25 Final 1.000
Prelogin/Nonconformance Report- Sample Log-In
XENCO Laboratories
511162Work Order #:
07/09/2015 09:53:00 AMDate/ Time Received:
Terraquest Environmental Consultants, PClient:
Sample Receipt Checklist
Checklist completed by: Date:
Checklist reviewed by:Date:
Debbie Simmons
07/09/2015
07/10/2015
#2 *Shipping container in good condition?
#3 *Samples received on ice?
#4 *Custody Seals intact on shipping container/ cooler?
#5 Custody Seals intact on sample bottles?
#6 *Custody Seals Signed and dated?
#7 *Chain of Custody present?
#8 Sample instructions complete on Chain of Custody?
#9 Any missing/extra samples?
#10 Chain of Custody signed when relinquished/ received?
#11 Chain of Custody agrees with sample label(s)?
#12 Container label(s) legible and intact?
#13 Sample matrix/ properties agree with Chain of Custody?
#14 Samples in proper container/ bottle?
#15 Samples properly preserved?
#16 Sample container(s) intact?
#17 Sufficient sample amount for indicated test(s)?
#18 All samples received within hold time?
#19 Subcontract of sample(s)?
#20 VOC samples have zero headspace (less than 1/4 inch bubble)?
#21 <2 for all samples preserved with HNO3,HCL, H2SO4? Except for
samples for the analysis of HEM or HEM-SGT which are verified by the
analysts.
#22 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH?
Yes
Yes
N/A
N/A
N/A
Yes
Yes
No
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
Yes
N/A

#1 *Temperature of cooler(s)?4.8
Acceptable Temperature Range: 0 - 6 degC
Air and Metal samples Acceptable Range: Ambient
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: PH Device/Lot#:JDR I016662-9
Comments
Jeff Wilmoth
Temperature Measuring device used :
Page 25 of 25 Final 1.000
Analytical Report 513503
for
Terraquest Environmental Consultants, P.C.
Project Manager: Jonathan Grubbs
Gussman Cleaners
22-AUG-15
05015
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (T104704215-15-19), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
Oklahoma (9218)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Texas (T104704477), Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)
Collected By: Client
Page 1 of 35 Final 1.000

Page 2 of 35 Final 1.000
Table of Contents
Cover Page 1
Cover Letter 3
Sample ID Cross Reference 4
Explanation of Qualifiers (Flags) 5
Hits Summary 6
Certificate of Analysis (Detailed Report) 8
Summary of Quality control 20
Blank Summary 27
Chain of Custody 33
Sample Receipt Conformance Report 35
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Project Manager: Jonathan Grubbs
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302

Reference: XENCO Report No(s): 513503
Gussman Cleaners
Project Address: NC
Jonathan Grubbs:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 513503. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 513503 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
22-AUG-15
Project Manager
Debbie Simmons
Page 3 of 35 Final 1.000
Sample Cross Reference 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
Sample Id
MW2
MW3
08-11-15 16:47
08-11-15 16:57
Date Collected Lab Sample Id
513503-001
513503-002

Sample DepthMatrix
W
W
Page 4 of 35 Final 1.000
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4143 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd , Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
2505 North Falkenburg Rd, Tampa, FL 33619
12600 West I-20 East, Odessa, TX 79765
6017 Financial Drive, Norcross, GA 30071
3725 E. Atlanta Ave, Phoenix, AZ 85040
Phone Fax
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone]
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non-Calculable
+ NELAC certification not offered for this compound.

* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Page 5 of 35 Final 1.000
Hits Summary 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received :
% Moisture :
08.11.15 16.47 Date Collected : 513503-001Lab Sample Id :
Ground WaterMatrix : MW2Sample Id :
MADEP EPH
MADEP VPH
SVOCs by EPA 625 + 10 TICs
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
Analytical Method :
Analytical Method :
SW3510C
SW5030B
E625P
SM6200B_PREP
Prep Method:
Prep Method:
Prep Method:
Prep Method:
08.17.15 14.44
08.19.15 04.43
08.17.15 07.55
08.20.15 09.03
Date Prep:
Date Prep:
Date Prep:
Date Prep:
C11-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
1-Methylnaphthalene +
unknown (TIC)
unknown (TIC)
Benzene, 1,2,4,5-tetramethyl- (TIC)
1-Docosene (TIC)
unknown (TIC)
Benz[e]acephenanthrylene (TIC)
2(1H)-Naphthalenone, octahydro-, t (TIC)
unknown (TIC)
unknown (TIC)
Benzoic acid, 2,4,5-trimethyl- (TIC)
1,2,4-Trimethylbenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Isopropylbenzene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Xylene
Parameter
Parameter
Parameter
Parameter
Result
Result
Result
Result
F
D
J
JN
JN
JN
JN
JN
JN
JN
JN
JN
JN
Flag
Flag
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
Units
Units
1
1
1
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Dil
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
Cas Number
C11C22
ALHYDRC9C
ALHYDRC19
HYDC9C10
ALHYDRC9C
90-12-0
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
95-63-6
95-50-1
541-73-1
98-82-8
104-51-8
103-65-1
135-98-8
98-06-6
95-47-6
602
391
1350
332
1360
7.90
15.4
23.9
14.2
17.6
14.4
15.8
16.6
17.5
20.6
26.4
1.01
1.95
4.75
10.9
10.3
19.5
13.9
10.9
3.36
974791
975112
974761
975118
Seq Number
Seq Number
Seq Number
Seq Number
08.18.15 05.21
08.18.15 08.17
08.18.15 08.17
08.19.15 14.33
08.19.15 13.04
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Page 6 of 35 Final 1.000
Hits Summary 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received :
% Moisture :
08.11.15 16.57 Date Collected : 513503-002Lab Sample Id :
Ground WaterMatrix : MW3Sample Id :
MADEP VPH
SVOCs by EPA 625 + 10 TICs
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
Analytical Method :
SW5030B
E625P
SM6200B_PREP
Prep Method:
Prep Method:
Prep Method:
08.19.15 04.43
08.17.15 07.55
08.20.15 09.03
Date Prep:
Date Prep:
Date Prep:
C9-C10 Aromatics
C9-C12 Aliphatics
1-Methylnaphthalene +
unknown (TIC)
Ethanol, 2-(2-methoxyethoxy)- (TIC)
Benzene, 1,2,4,5-tetramethyl- (TIC)
Naphthalene, 2,3-dimethyl- (TIC)
Benzene, 1,2,4,5-tetramethyl- (TIC)
unknown (TIC)
unknown (TIC)
Benzene, propyl- (TIC)
unknown (TIC)
Benzene, 1,4-diethyl- (TIC)
Chlorobenzene
Isopropylbenzene
n-Propylbenzene
sec-Butylbenzene
tert-Butylbenzene
Parameter
Parameter
Parameter
Result
Result
Result
J
JN
JN
JN
JN
JN
JN
JN
JN
JN
JN
Flag
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
HYDC9C10
ALHYDRC9C
90-12-0
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
108-90-7
98-82-8
103-65-1
135-98-8
98-06-6
294
346
6.21
11.8
9.68
12.1
6.88
18.1
8.41
8.05
11.7
6.85
6.34
4.28
17.9
36.3
16.7
13.2
975112
974761
975118
Seq Number
Seq Number
Seq Number
08.19.15 12.20
08.19.15 12.20
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
Analysis Date
Analysis Date
Analysis Date
Page 7 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.47 Date Collected:513503-001Lab Sample Id:
Ground WaterMatrix: MW2Sample Id:
MADEP EPH Analytical Method:
CLARAnalyst:
SW3510CPrep Method:
08.17.15 14.44 Date Prep:
BROTech:
C11-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
Parameter
98.5
98.5
98.5
Result
F
98.5
98.5
98.5
Flag
ug/L
ug/L
ug/L
Units
1
1
1
DilCas Number
C11C22
ALHYDRC9C18
ALHYDRC19C3
602
391
1350
974791Seq Number:
RL MDL
08.18.15 05.21
08.18.15 08.17
08.18.15 08.17
Analysis Date
Surrogate
40-140
40-140
40-140
%
Recovery Flag
%
%
%
63
76
75
08.18.15 08.17
08.18.15 05.21
08.18.15 05.21
Cas Number
3386-33-2
84-15-1
321-60-8
Units Analysis Date
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
Limits
% Moisture:
Page 8 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.47 Date Collected:513503-001Lab Sample Id:
Ground WaterMatrix: MW2Sample Id:
SVOCs by EPA 625 + 10 TICs Analytical Method:
VICAnalyst:
E625PPrep Method:
08.17.15 07.55 Date Prep:
BROTech:
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Diphenylhydrazine (as Azobenzene)
1,3-Dichlorobenzene
1,3-Dinitrobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3-Dichlorobenzidine
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Alcohol
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Parameter
1.43
1.83
4.76
2.11
20.1
1.61
1.40
1.64
1.78
1.63
7.11
1.29
1.83
1.19
2.00
1.95
2.55
3.88
1.40
2.12
2.18
3.09
1.35
2.41
1.43
1.48
2.01
1.90
1.80
1.97
1.97
2.71
2.21
1.23
1.25
1.78
1.24
1.20
1.82
Result
U
U
U
UL
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
10.0
10.0
10.0
10.0
50.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
120-82-1
95-50-1
122-66-7
541-73-1
99-65-0
106-46-7
90-12-0
88-06-2
120-83-2
105-67-9
51-28-5
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
15831-10-4
91-94-1
534-52-1
101-55-3
59-50-7
106-47-8
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
111-91-1
111-44-4
39638-32-9
117-81-7
85-68-7
U
U
U
U
U
U
7.90
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
974761Seq Number:
RL MDL
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
Analysis Date
% Moisture:
Page 9 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.47 Date Collected:513503-001Lab Sample Id:
Ground WaterMatrix: MW2Sample Id:
SVOCs by EPA 625 + 10 TICs Analytical Method:
VICAnalyst:
E625PPrep Method:
08.17.15 07.55 Date Prep:
BROTech:
Chrysene
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-c,d)Pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodi-n-Propylamine
n-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1-Docosene (TIC)
2(1H)-Naphthalenone, octahydro-, t (TIC)
Benz[e]acephenanthrylene (TIC)
Benzene, 1,2,4,5-tetramethyl- (TIC)
Benzoic acid, 2,4,5-trimethyl- (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
Parameter
2.09
1.83
1.64
1.90
1.97
2.08
1.38
1.81
1.56
2.21
1.78
1.87
2.38
1.87
1.41
1.52
1.49
1.36
2.50
2.26
2.04
1.76
2.40

Result
U
U
U
U
U
U
UH
U
U
U
U
U
U
U
U
U
U
U
UH
U
U
U
U
JN
JN
JN
JN
JN
JN
JN
JN
JN
JN
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0

Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
218-01-9
53-70-3
132-64-9
84-66-2
131-11-3
84-74-2
117-84-0
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
17.6
16.6
15.8
14.2
26.4
17.5
15.4
14.4
20.6
23.9
974761Seq Number:
RL MDL
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
Analysis Date
Surrogate
30-100
44-117
48-127
46-111
50-200
%
Recovery Flag
%
%
%
%
%
74
72
85
76
84
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
08.17.15 16.50
Cas Number
367-12-4
321-60-8
118-79-6
4165-60-0
4165-62-2
Units Analysis Date
2-Fluorophenol
2-Fluorobiphenyl
2,4,6-Tribromophenol
Nitrobenzene-d5
Phenol-d5
Limits
% Moisture:
Page 10 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.47 Date Collected:513503-001Lab Sample Id:
Ground WaterMatrix: MW2Sample Id:
SVOCs by EPA 625 + 10 TICs
MADEP VPH
Analytical Method:
Analytical Method:
VIC
ZHO
Analyst:
Analyst:
E625P
SW5030B
Prep Method:
Prep Method:
08.17.15 07.55
08.19.15 04.43
Date Prep:
Date Prep:
BRO
ZHO
Tech:
Tech:
C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
Parameter
0.0150
0.0500
0.0150
Result
U
D
0.0150
0.0500
0.0150
Flag
ug/L
ug/L
ug/L
Units
1
10
1
DilCas Number
ALHYDRC5C8
HYDC9C10
ALHYDRC9C12
U
332
1360
974761
975112
Seq Number:
Seq Number:
RL MDL
08.19.15 13.04
08.19.15 14.33
08.19.15 13.04
Analysis Date
Surrogate
Surrogate
46-126
70-130
70-130
%
Recovery
%
Recovery
Flag
Flag
%
%
%
87
123
116
08.17.15 16.50
08.19.15 13.04
08.19.15 13.04
Cas Number
Cas Number
1718-51-0
615-59-8
615-59-8
Units
Units
Analysis Date
Analysis Date
Terphenyl-D14
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Limits
Limits
% Moisture:
% Moisture:
Page 11 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.47 Date Collected:513503-001Lab Sample Id:
Ground WaterMatrix: MW2Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
1.01
U
1.95
U
U
U
4.75
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
975118Seq Number:
RL MDL
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
Analysis Date
% Moisture:
Page 12 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.47 Date Collected:513503-001Lab Sample Id:
Ground WaterMatrix: MW2Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
10.9
U
U
U
10.3
19.5
13.9
U
10.9
U
U
U
U
U
U
U
U
U
3.36
975118Seq Number:
RL MDL
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
94
103
100
08.20.15 16.14
08.20.15 16.14
08.20.15 16.14
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 13 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.57 Date Collected:513503-002Lab Sample Id:
Ground WaterMatrix: MW3Sample Id:
MADEP EPH Analytical Method:
CLARAnalyst:
SW3510CPrep Method:
08.17.15 14.44 Date Prep:
BROTech:
C11-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
Parameter
100
100
100
Result
U
UF
U
100
100
100
Flag
ug/L
ug/L
ug/L
Units
1
1
1
DilCas Number
C11C22
ALHYDRC9C18
ALHYDRC19C3
U
U
U
974791Seq Number:
RL MDL
08.18.15 08.28
08.18.15 08.50
08.18.15 08.50
Analysis Date
Surrogate
40-140
40-140
40-140
%
Recovery Flag
%
%
%
43
82
78
08.18.15 08.50
08.18.15 08.28
08.18.15 08.28
Cas Number
3386-33-2
84-15-1
321-60-8
Units Analysis Date
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
Limits
% Moisture:
Page 14 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.57 Date Collected:513503-002Lab Sample Id:
Ground WaterMatrix: MW3Sample Id:
SVOCs by EPA 625 + 10 TICs Analytical Method:
VICAnalyst:
E625PPrep Method:
08.17.15 07.55 Date Prep:
BROTech:
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Diphenylhydrazine (as Azobenzene)
1,3-Dichlorobenzene
1,3-Dinitrobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3-Dichlorobenzidine
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Alcohol
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Parameter
1.43
1.83
4.76
2.11
20.1
1.61
1.40
1.64
1.78
1.63
7.11
1.29
1.83
1.19
2.00
1.95
2.55
3.88
1.40
2.12
2.18
3.09
1.35
2.41
1.43
1.48
2.01
1.90
1.80
1.97
1.97
2.71
2.21
1.23
1.25
1.78
1.24
1.20
1.82
Result
U
U
U
UL
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
10.0
10.0
10.0
10.0
50.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
120-82-1
95-50-1
122-66-7
541-73-1
99-65-0
106-46-7
90-12-0
88-06-2
120-83-2
105-67-9
51-28-5
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
15831-10-4
91-94-1
534-52-1
101-55-3
59-50-7
106-47-8
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
111-91-1
111-44-4
39638-32-9
117-81-7
85-68-7
U
U
U
U
U
U
6.21
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
974761Seq Number:
RL MDL
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
Analysis Date
% Moisture:
Page 15 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.57 Date Collected:513503-002Lab Sample Id:
Ground WaterMatrix: MW3Sample Id:
SVOCs by EPA 625 + 10 TICs Analytical Method:
VICAnalyst:
E625PPrep Method:
08.17.15 07.55 Date Prep:
BROTech:
Chrysene
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-c,d)Pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodi-n-Propylamine
n-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Benzene, 1,2,4,5-tetramethyl- (TIC)
Benzene, 1,2,4,5-tetramethyl- (TIC)
Benzene, 1,4-diethyl- (TIC)
Benzene, propyl- (TIC)
Ethanol, 2-(2-methoxyethoxy)- (TIC)
Naphthalene, 2,3-dimethyl- (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
Parameter
2.09
1.83
1.64
1.90
1.97
2.08
1.38
1.81
1.56
2.21
1.78
1.87
2.38
1.87
1.41
1.52
1.49
1.36
2.50
2.26
2.04
1.76
2.40

Result
U
U
U
U
U
U
UH
U
U
U
U
U
U
U
U
U
U
U
UH
U
U
U
U
JN
JN
JN
JN
JN
JN
JN
JN
JN
JN
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0

Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
218-01-9
53-70-3
132-64-9
84-66-2
131-11-3
84-74-2
117-84-0
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
18.1
12.1
6.34
11.7
9.68
6.88
8.41
8.05
6.85
11.8
974761Seq Number:
RL MDL
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
Analysis Date
Surrogate
44-117
30-100
48-127
46-111
50-200
%
Recovery Flag
%
%
%
%
%
78
75
86
78
86
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
08.17.15 17.18
Cas Number
321-60-8
367-12-4
118-79-6
4165-60-0
4165-62-2
Units Analysis Date
2-Fluorobiphenyl
2-Fluorophenol
2,4,6-Tribromophenol
Nitrobenzene-d5
Phenol-d5
Limits
% Moisture:
Page 16 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.57 Date Collected:513503-002Lab Sample Id:
Ground WaterMatrix: MW3Sample Id:
SVOCs by EPA 625 + 10 TICs
MADEP VPH
Analytical Method:
Analytical Method:
VIC
ZHO
Analyst:
Analyst:
E625P
SW5030B
Prep Method:
Prep Method:
08.17.15 07.55
08.19.15 04.43
Date Prep:
Date Prep:
BRO
ZHO
Tech:
Tech:
C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
Parameter
0.0150
0.00500
0.0150
Result
U0.0150
0.00500
0.0150
Flag
ug/L
ug/L
ug/L
Units
1
1
1
DilCas Number
ALHYDRC5C8
HYDC9C10
ALHYDRC9C12
U
294
346
974761
975112
Seq Number:
Seq Number:
RL MDL
08.19.15 12.20
08.19.15 12.20
08.19.15 12.20
Analysis Date
Surrogate
Surrogate
46-126
70-130
70-130
%
Recovery
%
Recovery
Flag
Flag
%
%
%
90
87
95
08.17.15 17.18
08.19.15 12.20
08.19.15 12.20
Cas Number
Cas Number
1718-51-0
615-59-8
615-59-8
Units
Units
Analysis Date
Analysis Date
Terphenyl-D14
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Limits
Limits
% Moisture:
% Moisture:
Page 17 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.57 Date Collected:513503-002Lab Sample Id:
Ground WaterMatrix: MW3Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
4.28
U
U
U
U
975118Seq Number:
RL MDL
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
Analysis Date
% Moisture:
Page 18 of 35 Final 1.000
Certificate of Analytical Results 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
08.14.15 09.50 Date Received:
08.11.15 16.57 Date Collected:513503-002Lab Sample Id:
Ground WaterMatrix: MW3Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
17.9
U
U
U
U
36.3
16.7
U
13.2
U
U
U
U
U
U
U
U
U
U
975118Seq Number:
RL MDL
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
96
99
97
08.20.15 15.48
08.20.15 15.48
08.20.15 15.48
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 19 of 35 Final 1.000
QC Summary 513503
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
696738-1-BLKMB Sample Id:
WaterMatrix:
MADEP EPH Analytical Method:SW3510CPrep Method:
08.17.15Date Prep:
C11-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
Parameter %RPD
F
Flag
40
40
40
RPD
Limit
21
56
5
974791Seq Number:
08.18.15 04:10
08.18.15 07:13
08.18.15 07:13
Analysis
Date
Limits
40-140
40-140
40-140
LCSD
%Rec
80
94
125
LCSD
Result
1360
561
996
LCS
%Rec
65
53
119
1100
315
951
Spike
Amount
1700
600
800
MB
Result
<100
<100
<100
696738-1-BKSLCS Sample Id:696738-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
UnitsLCS
Result
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
Surrogate LCSD
Flag
08.18.15 07:13
08.18.15 04:10
08.18.15 04:10
Analysis
DateLimits
40-140
40-140
40-140
LCSD
%Rec
115
112
86
LCS
%Rec
82
85
85
MB
%Rec
96
101
84
%
%
%
UnitsLCS
Flag
MB
Flag
Page 20 of 35 Final 1.000
QC Summary 513503
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
696705-1-BLKMB Sample Id:
WaterMatrix:
SVOCs by EPA 625 + 10 TICs Analytical Method:E625PPrep Method:
08.17.15Date Prep:
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Diphenylhydrazine (as Azobenzene)
1,3-Dichlorobenzene
1,3-Dinitrobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl Alcohol
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-c,d)Pyrene
Isophorone
Parameter %RPD
L
H
Flag
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
RPD
Limit
11
15
15
14
12
15
11
13
12
11
10
11
14
11
11
11
11
17
16
11
11
12
14
11
13
14
15
15
10
16
16
13
11
13
13
14
14
15
16
12
10
14
15
15
15
12
17
12
15
13
16
12
974761Seq Number:
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
Analysis
Date
Limits
44-142
32-129
55-115
65-135
45-110
20-124
25-175
37-144
39-135
32-119
0-191
60-118
36-120
45-105
40-110
29-182
30-110
10-181
53-127
22-147
15-110
25-158
0-132
47-145
33-145
27-133
33-143
17-163
24-159
0-219
11-162
30-110
33-184
12-158
36-166
8-158
0-152
17-168
0-227
55-105
0-114
0-112
1-118
0-107
26-137
59-121
0-152
24-116
41-125
40-113
0-171
21-196
LCSD
%Rec
73
72
97
71
102
71
77
81
80
83
78
82
76
83
84
77
89
90
88
93
89
90
98
87
93
99
100
106
105
98
104
88
85
83
100
108
106
98
99
88
90
95
91
110
101
95
90
70
88
75
99
116
LCSD
Result
36.7
36.2
48.5
35.6
51.0
35.7
38.7
40.7
40.0
41.7
38.9
41.1
38.1
41.3
41.9
38.4
44.5
45.0
44.0
46.5
44.4
45.1
49.1
43.3
46.6
49.5
50.1
52.8
52.7
49.1
52.0
44.2
42.3
41.4
49.8
54.1
53.0
49.2
49.3
44.1
45.0
47.6
45.5
55.0
50.4
47.7
45.1
35.0
43.8
37.3
49.3
58.2
LCS
%Rec
66
62
84
62
90
61
70
72
71
74
70
74
66
74
75
69
79
76
75
83
79
80
85
77
82
86
86
91
95
84
89
77
76
73
87
94
92
85
84
78
81
83
78
95
87
84
76
62
76
65
84
103
32.9
31.2
41.9
30.9
45.1
30.6
34.8
35.9
35.6
37.2
35.2
36.9
33.0
37.1
37.6
34.3
39.7
38.1
37.4
41.6
39.6
39.8
42.6
38.6
41.0
42.9
43.0
45.5
47.6
42.0
44.5
38.7
37.9
36.4
43.7
46.9
45.9
42.4
41.9
39.0
40.7
41.3
39.1
47.3
43.5
42.2
37.9
31.0
37.8
32.6
42.2
51.7
Spike
Amount
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
MB
Result
<1.43
<1.83
<4.76
<2.11
<20.1
<1.61
<1.40
<1.64
<1.78
<1.63
<7.11
<1.29
<1.83
<1.19
<2.00
<1.95
<2.55
<1.40
<2.12
<2.18
<3.09
<1.35
<2.41
<1.43
<1.48
<2.01
<1.90
<1.80
<1.97
<1.97
<2.71
<1.23
<1.25
<1.78
<1.24
<1.20
<1.82
<2.09
<1.83
<1.64
<1.90
<1.97
<2.08
<1.38
<1.81
<1.56
<2.21
<1.78
<1.87
<2.38
<1.87
<1.41
696705-1-BKSLCS Sample Id:696705-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 21 of 35 Final 1.000
QC Summary 513503
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
696705-1-BLK
696981-1-BLK
MB Sample Id:
MB Sample Id:
Water
Water
Matrix:
Matrix:
SVOCs by EPA 625 + 10 TICs
MADEP VPH
Analytical Method:
Analytical Method:
E625P
SW5030B
Prep Method:
Prep Method:
08.17.15
08.19.15
Date Prep:
Date Prep:
Naphthalene
Nitrobenzene
n-Nitrosodi-n-Propylamine
n-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
Parameter
Parameter
%RPD
%RPD
H
Flag
Flag
30
30
30
30
30
30
30
30
25
25
25
RPD
Limit
RPD
Limit
12
11
11
15
16
15
13
15
3
5
5
974761
975112
Seq Number:
Seq Number:
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.19.15 05:28
08.19.15 05:28
08.19.15 05:28
Analysis
Date
Analysis
Date
Limits
Limits
21-133
35-180
10-230
50-110
14-76
54-120
5-112
23-152
70-130
70-130
70-130
LCSD
%Rec
LCSD
%Rec
76
78
103
128
72
95
84
101
105
89
100
LCSD
Result
LCSD
Result
38.1
39.2
51.5
63.8
36.1
47.5
41.9
50.3
158
44.3
150
LCS
%Rec
LCS
%Rec
68
70
92
110
62
82
73
86
108
93
105
33.9
35.2
46.1
54.9
30.8
40.8
36.7
43.2
162
46.7
158
Spike
Amount
Spike
Amount
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
150
50.0
150
MB
Result
MB
Result
<1.52
<1.49
<1.36
<2.50
<2.26
<2.04
<1.76
<2.40
<0.0150
<0.00500
<0.0150
696705-1-BKS
696981-1-BKS
LCS Sample Id:
LCS Sample Id:
696705-1-BSD
696981-1-BSD
LCSD Sample Id:
LCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
LCS
Result
LCS
Result
2-Fluorobiphenyl
2-Fluorophenol
2,4,6-Tribromophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-D14
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Surrogate
Surrogate
LCSD
Flag
LCSD
Flag
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.17.15 14:34
08.19.15 05:28
08.19.15 05:28
Analysis
Date
Analysis
Date
Limits
Limits
39-99
33-92
32-129
37-94
50-200
18-133
70-130
70-130
LCSD
%Rec
LCSD
%Rec
77
71
87
77
82
96
81
93
LCS
%Rec
LCS
%Rec
70
61
74
69
73
84
92
95
MB
%Rec
MB
%Rec
87
83
88
90
93
108
80
86
%
%
%
%
%
%
%
%
Units
Units
LCS
Flag
LCS
Flag
MB
Flag
MB
Flag
Page 22 of 35 Final 1.000
QC Summary 513503
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
696985-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
7
14
6
4
11
12
10
8
19
6
5
2
9
3
1
5
5
2
6
5
5
4
1
4
6
6
9
6
3
7
6
1
4
12
6
2
4
9
6
8
1
9
11
5
7
3
6
2
5
7
3
6
975118Seq Number:
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
Analysis
Date
Limits
75-127
62-128
77-129
86-120
82-114
73-123
83-125
57-127
79-118
59-125
84-118
83-126
83-128
56-133
85-121
86-118
90-126
85-121
88-121
76-126
66-133
80-128
70-130
82-130
80-128
74-129
51-143
81-123
84-114
89-127
79-129
73-140
53-143
66-136
88-118
73-139
70-123
72-118
65-125
85-125
92-126
48-143
61-133
87-123
77-125
82-115
53-149
75-119
52-116
83-130
84-122
86-120
LCSD
%Rec
106
101
98
96
101
105
107
94
104
96
92
100
91
101
101
93
92
96
91
106
104
92
105
92
93
99
111
99
92
113
113
116
104
108
92
98
95
101
100
100
106
109
108
95
109
92
107
119
98
95
92
90
LCSD
Result
26.4
25.2
24.5
24.1
25.3
26.3
26.7
23.5
26.1
23.9
23.0
25.1
22.7
25.2
25.3
23.3
23.1
24.1
22.7
26.6
52.2
22.9
52.5
23.0
23.3
49.4
55.4
24.7
23.1
28.3
28.3
29.1
26.1
27.1
23.1
24.5
23.8
25.2
25.1
24.9
26.6
27.3
1080
23.7
27.3
23.1
53.7
29.8
24.5
23.7
22.9
22.5
LCS
%Rec
113
116
104
100
113
119
118
102
86
102
97
102
99
104
102
98
98
98
96
112
110
95
104
96
99
105
121
105
96
122
120
117
109
122
98
100
99
111
106
108
108
120
121
100
117
95
114
117
103
102
95
96
28.3
29.0
26.0
25.0
28.2
29.8
29.6
25.4
21.6
25.5
24.3
25.6
24.8
26.0
25.6
24.4
24.4
24.5
24.0
28.1
54.9
23.8
51.9
24.0
24.8
52.6
60.6
26.3
23.9
30.4
30.1
29.3
27.2
30.6
24.6
25.0
24.7
27.7
26.6
27.0
26.9
29.9
1210
24.9
29.2
23.7
56.8
29.2
25.8
25.5
23.7
23.9
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
MB
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
696985-1-BKSLCS Sample Id:696985-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 23 of 35 Final 1.000
QC Summary 513503
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
696985-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
7
3
0
7
8
3
10
2
4
4
7
9
975118Seq Number:
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
Analysis
Date
Limits
85-123
79-126
64-131
89-116
78-118
86-127
82-119
46-144
58-141
76-122
90-125
86-119
LCSD
%Rec
97
92
104
93
110
89
91
118
107
106
94
94
LCSD
Result
24.3
22.9
26.1
23.2
27.4
22.2
22.8
29.5
26.8
26.5
46.9
23.5
LCS
%Rec
104
95
104
100
102
92
100
120
112
110
100
103
26.1
23.7
26.1
25.0
25.4
22.9
25.1
30.0
27.9
27.6
50.2
25.7
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
MB
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
696985-1-BKSLCS Sample Id:696985-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate LCSD
Flag
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
Analysis
Date
Limits
65-126
86-111
83-116
LCSD
%Rec
99
99
97
LCS
%Rec
100
97
99
MB
%Rec
102
104
96
%
%
%
UnitsLCS
Flag
MB
Flag
Page 24 of 35 Final 1.000
QC Summary 513503
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
513500-004Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD
X
X
XF
X
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
1
3
4
0
3
0
5
2
3
4
7
0
5
2
4
6
6
1
5
1
200
6
0
8
4
12
2
5
5
3
4
1
6
1
1
0
2
2
3
5
0
4
11
2
2
7
0
5
6
6
8
7
975118Seq Number:
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
Analysis
Date
Limits
76-126
63-128
79-133
82-126
77-120
67-123
76-126
41-136
77-125
41-132
53-141
82-130
83-128
59-134
79-125
69-125
83-126
85-124
82-121
56-122
66-136
73-129
63-140
76-129
73-126
71-140
47-138
70-135
76-120
83-132
66-132
63-143
60-134
59-139
83-120
68-140
67-125
72-120
59-128
80-125
74-122
48-138
55-140
70-140
77-125
75-117
51-155
75-119
34-135
73-128
75-125
77-122
MSD
%Rec
92
88
99
97
86
90
93
88
92
84
78
98
83
92
92
79
80
94
79
82
0
78
116
77
80
108
112
88
82
103
100
107
90
90
82
90
84
88
86
86
94
98
103
83
99
77
102
86
97
81
78
77
MSD
Result
23.1
22.1
24.8
24.2
21.5
22.6
23.2
22.0
22.9
21.1
19.6
24.5
20.7
23.0
22.9
19.7
19.9
23.6
19.7
20.4
<0.378
19.4
58.0
19.2
20.0
53.8
55.8
22.1
20.6
25.8
25.1
26.8
22.6
22.4
20.6
22.4
20.9
21.9
21.5
21.4
23.5
24.4
1030
20.8
24.7
19.3
50.8
21.6
24.3
20.3
19.4
19.2
MS
%Rec
94
91
103
97
89
90
98
90
94
88
84
98
87
94
95
84
85
96
83
80
117
82
116
83
84
122
113
93
87
106
104
106
96
91
83
90
85
90
89
90
94
102
115
85
101
83
101
82
104
86
84
82
23.4
22.8
25.8
24.3
22.2
22.6
24.4
22.5
23.6
21.9
21.0
24.4
21.8
23.4
23.8
20.9
21.2
23.9
20.8
20.1
58.4
20.5
57.9
20.7
20.9
60.8
56.7
23.2
21.7
26.5
26.1
26.5
23.9
22.7
20.8
22.5
21.3
22.4
22.2
22.4
23.5
25.5
1150
21.3
25.3
20.8
50.6
20.5
25.9
21.6
21.0
20.6
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
Parent
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
513500-004 SMS Sample Id:513500-004 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
Page 25 of 35 Final 1.000
QC Summary 513503
Terraquest Environmental Consultants, P.C.
Gussman Cleaners
513500-004Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
0
6
4
4
0
0
4
3
7
2
3
3
975118Seq Number:
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
Analysis
Date
Limits
54-137
74-124
57-130
81-125
69-122
73-129
73-124
49-139
57-134
70-121
65-151
58-148
MSD
%Rec
85
79
84
82
94
80
83
94
94
84
82
81
MSD
Result
21.3
19.8
21.1
20.6
23.5
20.1
20.8
23.6
23.5
21.1
40.8
20.3
MS
%Rec
86
84
88
86
94
80
87
92
100
86
84
84
21.4
21.0
22.0
21.4
23.6
20.1
21.7
23.0
25.1
21.6
42.0
21.0
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
Parent
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
513500-004 SMS Sample Id:513500-004 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate MSD
Flag
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
Analysis
Date
Limits
65-126
86-111
83-116
MSD
%Rec
98
98
98
MS
%Rec
99
101
96
%
%
%
UnitsMS
Flag
Page 26 of 35 Final 1.000
Blank Summary 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
696705-1-BLKLab Sample Id:
WATERMatrix: 696705-1-BLK Sample Id:
SVOCs by EPA 625 + 10 TICs Analytical Method:
VICAnalyst:
E625PPrep Method:
08.17.15 07:55Date Prep:
BROTech:
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Diphenylhydrazine (as Azobenzene)
1,3-Dichlorobenzene
1,3-Dinitrobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene +
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3&4-Methylphenol
3,3-Dichlorobenzidine
4,6-Dinitro-2-methyl phenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Alcohol
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrysene
Parameter
1.43
1.83
4.76
2.11
20.1
1.61
1.40
1.64
1.78
1.63
7.11
1.29
1.83
1.19
2.00
1.95
2.55
3.88
1.40
2.12
2.18
3.09
1.35
2.41
1.43
1.48
2.01
1.90
1.80
1.97
1.97
2.71
2.21
1.23
1.25
1.78
1.24
1.20
1.82
2.09
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
10.0
10.0
10.0
10.0
50.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
120-82-1
95-50-1
122-66-7
541-73-1
99-65-0
106-46-7
90-12-0
88-06-2
120-83-2
105-67-9
51-28-5
91-58-7
95-57-8
91-57-6
95-48-7
88-75-5
15831-10-4
91-94-1
534-52-1
101-55-3
59-50-7
106-47-8
7005-72-3
100-02-7
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
111-91-1
111-44-4
39638-32-9
117-81-7
85-68-7
218-01-9
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
974761Seq Number:
MDLRL
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
Analysis
Date
Page 27 of 35 Final 1.000
Blank Summary 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
696705-1-BLKLab Sample Id:
WATERMatrix: 696705-1-BLK Sample Id:
SVOCs by EPA 625 + 10 TICs Analytical Method:
VICAnalyst:
E625PPrep Method:
08.17.15 07:55Date Prep:
BROTech:
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-c,d)Pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodi-n-Propylamine
n-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
unknown (TIC)
Parameter
1.83
1.64
1.90
1.97
2.08
1.38
1.81
1.56
2.21
1.78
1.87
2.38
1.87
1.41
1.52
1.49
1.36
2.50
2.26
2.04
1.76
2.40

Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
JN
JN
JN
JN
JN
JN
JN
JN
JN
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0

Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
53-70-3
132-64-9
84-66-2
131-11-3
84-74-2
117-84-0
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
TIC
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
5.94
8.43
4.90
4.21
7.73
4.23
5.70
8.66
6.13
974761Seq Number:
MDLRL
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
08.17.15 14:06
Analysis
Date
Page 28 of 35 Final 1.000
Blank Summary 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
696738-1-BLKLab Sample Id:
WATERMatrix: 696738-1-BLK Sample Id:
MADEP EPH Analytical Method:
CLARAnalyst:
SW3510CPrep Method:
08.17.15 14:44Date Prep:
BROTech:
C11-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
Parameter
100
100
100
Result
U
U
U
100
100
100
Flag
ug/L
ug/L
ug/L
Units
1
1
1
DilCas Number
C11C22
ALHYDRC9C1
ALHYDRC19C
U
U
U
974791Seq Number:
MDLRL
08.18.15 03:35
08.18.15 06:42
08.18.15 06:42
Analysis
Date
Page 29 of 35 Final 1.000
Blank Summary 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
696981-1-BLKLab Sample Id:
WATERMatrix: 696981-1-BLK Sample Id:
MADEP VPH Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
08.19.15 04:43Date Prep:
ZHOTech:
C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
Parameter
0.0150
0.00500
0.0150
Result
U
U
U
0.0150
0.00500
0.0150
Flag
ug/L
ug/L
ug/L
Units
1
1
1
DilCas Number
ALHYDRC5C8
HYDC9C10
ALHYDRC9C1
U
U
U
975112Seq Number:
MDLRL
08.19.15 06:57
08.19.15 06:57
08.19.15 06:57
Analysis
Date
Page 30 of 35 Final 1.000
Blank Summary 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
696985-1-BLKLab Sample Id:
WATERMatrix: 696985-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09:03Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
975118Seq Number:
MDLRL
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
Analysis
Date
Page 31 of 35 Final 1.000
Blank Summary 513503
Terraquest Environmental Consultants, P.C., Mebane, NC
Gussman Cleaners
696985-1-BLKLab Sample Id:
WATERMatrix: 696985-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09:03Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
975118Seq Number:
MDLRL
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
Analysis
Date
Page 32 of 35 Final 1.000
Page 33 of 35 Final 1.000
Page 34 of 35 Final 1.000
Prelogin/Nonconformance Report- Sample Log-In
XENCO Laboratories
513503Work Order #:
08/14/2015 09:50:00 AMDate/ Time Received:
Terraquest Environmental Consultants, PClient:
Sample Receipt Checklist
Checklist completed by: Date:
Checklist reviewed by:Date:
Debbie Simmons
08/15/2015
08/17/2015
#2 *Shipping container in good condition?
#3 *Samples received on ice?
#4 *Custody Seals intact on shipping container/ cooler?
#5 Custody Seals intact on sample bottles?
#6 *Custody Seals Signed and dated?
#7 *Chain of Custody present?
#8 Sample instructions complete on Chain of Custody?
#9 Any missing/extra samples?
#10 Chain of Custody signed when relinquished/ received?
#11 Chain of Custody agrees with sample label(s)?
#12 Container label(s) legible and intact?
#13 Sample matrix/ properties agree with Chain of Custody?
#14 Samples in proper container/ bottle?
#15 Samples properly preserved?
#16 Sample container(s) intact?
#17 Sufficient sample amount for indicated test(s)?
#18 All samples received within hold time?
#19 Subcontract of sample(s)?
#20 VOC samples have zero headspace (less than 1/4 inch bubble)?
#21 <2 for all samples preserved with HNO3,HCL, H2SO4? Except for
samples for the analysis of HEM or HEM-SGT which are verified by the
analysts.
#22 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH?
Yes
Yes
N/A
N/A
N/A
Yes
Yes
No
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
N/A
N/A

#1 *Temperature of cooler(s)?2.5
Acceptable Temperature Range: 0 - 6 degC
Air and Metal samples Acceptable Range: Ambient
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: PH Device/Lot#:
Comments
Dario Lagunas
Temperature Measuring device used : #61
Page 35 of 35 Final 1.000