1403-MSWLF-1998_FoothillsEnvironmentalLandfill_GWMReport_DIN26477_20160316

PREPARED FOR:
REPUBLIC SERVICES OF NORTH CAROLINA, LLC
D.B.A. FOOTHILLS ENVIRONMENTAL
2800 CHERAW ROAD
LENOIR, NORTH CAROLINA 28645

FOOTHILLS REGIONAL LANDFILL
PERMIT NO. 14-03

FIRST SEMIANNUAL WATER QUALITY
MONITORING REPORT OF 2016

APRIL 2016

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101
GREENSBORO, NORTH CAROLINA 27407
NC LICENSE NUMBER C-0782
PHONE: [phone]
FAX: [phone]
JOYCE ENGINEERING PROJECT NO. 00890.1601.12

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First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
Foothills Regional Landfill, Permit No. 14-03 May 2016

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Executive Summary

This report presents the results of the first semiannual water quality monitoring event of 2016 for
the Foothills Regional Landfill, conducted on January 28, 2016. Samples were collected by
representatives of Joyce Engineering from groundwater monitoring wells, underdrains, surface
water monitoring points, and the leachate collection system. The analytical results from the
January 28, 2016, monitoring event have been reported by Analytical Services, Inc. of Norcross,
Georgia, NC, laboratory certification number 381.

Seven inorganic constituents (barium, chromium, cobalt, copper, lead, vanadium and zinc) were
detected in samples from one or more downgradient monitoring points at concentrations above
their respective Solid Waste Section Reporting Limits (SWSLs). Barium was detected above the
SWSL in MW-2R, MW-6, SW-3, UD-1 and UD-2. Copper was detected in SW-3 and UD-1.
Zinc was detected above the SWSL in MW-10, SW-3 and UD-1. Chromium, lead and vanadium
detections above the SWSL were limited to SW-3. Cobalt was detected in MW-4 and UD-1
above the SWSL and above the Solid Waste Section (SWS) Groundwater Protection Standard
(GWPS) during the January 2016 monitoring event. The cobalt detections were not above the
statistical background determined in accordance with 15A NCAC 13B.1632.(g-h); therefore,
they are not considered groundwater protection standard (GPS) exceedances as defined in 15A
NCAC 13B.1634.(g).

Three organic constituents (benzene, trichlorofluoromethane, and vinyl chloride) were reported
at a quantified concentration above their respective SWSLs. Trichlorofluoromethane was
detected in MW-3R2 but was below the North Carolina 15A NCAC 2L (NC2L) Groundwater
Standard. The detection of trichlorofluoromethane in MW-3R is consistent with historical data
and is likely related to the source presented in the approved ASD for VOCs detected in MW-3
and MW-3R. Trichlorofluoromethane has not been historically detected in the facility leachate
samples.

The initial reported concentrations of benzene and vinyl chloride in MW-2R were 1.1 and 1.0
µg/L, respectively, which were quantified above the SWSLs of 1.0 µg/L and the NC2Ls of 1.0
µg/L and 0.03 µg/L, respectively. (The listed NC2L standard for vinyl chloride is 0.03 µg/L;
however, an estimated detection below the SWSL is not considered an exceedance, so the
effective standard is the SWSL.) MW-2R was resampled on March 16, 2016, for benzene and
vinyl chloride and the results were estimated concentrations of 1.0 µg/L for benzene and 0.9
µg/L for vinyl chloride. Since they were estimated concentrations below the SWSL, they were
not considered exceedances, so the initial exceedances were refuted.

No other inorganic or organic constituents were detected at quantified concentrations above their
respective NC2L, GWPS, or NC 2B standards during the January 28, 2016, event. Based on the
results summarized herein, Republic Services of NC, LLC, will continue monitoring the
uppermost aquifer beneath the Foothills Regional Landfill in accordance with the requirements
for Detection Monitoring Program as outlined in Title 15A NCAC 13B .1633.

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First Semiannual Water Quality Monitoring Report of 2016 Joyce Engineering
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First Semiannual Water Quality Monitoring Report of 2016
Foothills Regional Landfill, Permit No. 14-03
Caldwell County, North Carolina

TABLE OF CONTENTS

1.0 INTRODUCTION..............................................................................................................1 
1.1  Site Description and Background ................................................................................ 1 
1.2 Compliance Monitoring History .................................................................................. 1 
1.3 Hydrogeologic Setting ................................................................................................... 2 
2.0 FIELD PROGRAM, MONITORING RESULTS, AND DISCUSSION ......................3 
2.1 Visual Inspection Program........................................................................................... 3 
2.2 Well Network and Groundwater Elevation Measurements...................................... 3 
2.3 January 2016 Monitoring Event .................................................................................. 4 
2.4 Laboratory Analysis Program ..................................................................................... 5 
2.5 January 2016 Sampling Results ................................................................................... 6 
3.0 LABORATORY AND FIELD QA/QC ............................................................................7 
4.0 DATA EVALUTION .........................................................................................................7 
4.1 Comparisons to Groundwater and Surface Water Standards ................................. 7 
4.2 Statistical Evaluations .................................................................................................. 7 
5.0 CONCLUSIONS ................................................................................................................8 
6.0 REFERENCES ...................................................................................................................8 

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TABLE OF CONTENTS (Continued)

Tables

Table 1 Historical Groundwater Elevations
Table 2 Hydraulic Gradients & Linear Groundwater Velocities
Table 3 Well Construction Information
Table 4 Field Parameters (January 2016)
Table 5 Quantified Detections in Groundwater & Surface Water (January 2016)
Table 6 Exceedances of Groundwater & Surface Water Standards (January 2016)
Table 7 Statistical Background Analyses

Drawing

Drawing 1 Groundwater Potentiometric Surface Map (January 28, 2016)

Appendices

Appendix A Groundwater and Surface Water Field Sampling Logs
Appendix B Laboratory Analytical Reports and Chains-of-Custody
Appendix C Statistical Analyses Worksheets
Appendix D Historical Constituents/Analytes in Groundwater
Appendix E Historical Constituents/Analytes in Surface Water
Appendix F Historical Constituents/Analytes in Leachate

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1.0 INTRODUCTION
This report summarizes the monitoring results from the January 28, 2016, water quality
monitoring event at the Foothills Regional Landfill in Caldwell County, North Carolina in
accordance with Title 15A of the North Carolina Administrative Code (NCAC) Subchapter 13B,
Section .1632. The approximately 230-acre facility, which is an active municipal solid waste
landfill, is maintained and operated by Republic Services of North Carolina, LLC (Republic)
under Permit Number 14-03, issued by the North Carolina Department of Environment and
Natural Resources (DENR).

1.1 Site Description and Background
The location of the facility is shown on the inlay on Drawing 1. The Foothills Regional Landfill
is located approximately two miles northwest of Lenoir, North Carolina in Caldwell County at
2800 Cheraw Road. The landfill is bounded to the north and east by mainly wooded and
agricultural properties, to the south by Cheraw Road, and to the west by rural residential/wooded
properties and Abingdon Road. Access to the facility is from Cheraw Road. The facility, which
began operating in 1998, is a lined Subtitle D facility.

Topographic elevations at the facility range from approximately 1,120 to nearly 1,400 feet above
mean sea level. Surface drainage from the landfill is toward an unnamed perennial tributary of
Abingdon Creek, which flows southeasterly to Lower Creek, a tributary of the easterly flowing
Catawba River.

1.2 Compliance Monitoring History
Groundwater monitoring at the facility was initiated in 1998 under the Detection Monitoring
Program for municipal solid waste landfills. The facility’s current monitoring network is
comprised of nine monitoring wells: MW-1R (background), MW-2R, MW-3R2, MW-4, MW-5,
MW-6, MW-7, MW-8, and MW-10, which monitor the uppermost aquifer beneath the facility.
The monitoring wells are routinely sampled on a semiannual basis, with the groundwater
samples submitted to a qualified laboratory for required analyses in accordance with the
facility’s environmental monitoring program and permit requirements. Well MW-3R2 was
added to the monitoring well network on August 17, 2006 as a replacement well for MW-3 and
MW-3R as approved by DENR (JOYCE, 2006). Monitoring wells MW-3 and MW-3R remain
for water level data collection purposes. Monitoring well MW-7 was installed in April 2010 to
monitor groundwater beneath Cell 4, which began receiving waste in September 2010. MW-8
was installed in April 2013 to monitor Cell 8A, which was constructed in January 2013. MW-10
was installed in October 2015 to monitor Cell 5A, which is currently under construction. The
former background well, MW-1, was abandoned in preparation for construction of Cell 5A and
the new background well, MW-1R, was installed in October 2015.

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In addition to the groundwater monitoring wells, four surface water sampling points are sampled
semiannually: upstream surface point SW-1 and downstream surface points SW-2, SW-3, and
SW-4. A sample from the facility’s leachate system is sampled semiannually as part of the
facility’s environmental monitoring program. A sample from the underdrain for Cell 1 (UD-1),
shown on Drawing 1, was added to the monitoring network prior to the January 2008 sampling
event. A sample from the underdrain for Cells 4 and 8A (UD-2), shown on Drawing 1, was
added to the monitoring network prior to the January 2014 sampling event.

The facility was in an Assessment Monitoring Program in 2006. An Alternate Source
Demonstration (ASD), for volatile organic compounds (VOCs) detected in wells MW-3 and
MW-3R, was approved by DENR on December 14, 2006, and the facility reverted to a Detection
Monitoring Program.

1.3 Hydrogeologic Setting
Geologically, the facility is located in the northwestern portion of the Inner Piedmont Belt of the
Piedmont Physiographic Province, approximately 20 miles east of the thrust belt (Brevard Shear
Zone) delineating the boundary between the westerly Blue Ridge Belt and the easterly Inner
Piedmont Belt. The metamorphic rocks of the Inner Piedmont Belt generally group within the
sillimanite facies of the amphibolite metamorphic sequence. Locally, the bedrock underlying the
facility has been mapped as migmatitic granitic gneiss of the Ordovician and older Cambrian
Periods. These rocks are described as ranging in composition from granitic to quartz dioritic with
smaller biotite gneiss and amphibolite facies present locally. The unit as a whole exhibits a
variable massive to foliated fabric (NCGS, 1985).

The uppermost aquifer beneath the facility is present within weathered bedrock saprolite and
fractured bedrock. The saprolite ranges in texture from clayey silt in the upper, most weathered
sections to micaceous sandy silt in the lower sections. Immediately above the competent
bedrock surface, a variable thickness transitional zone composed of highly weathered and
degraded friable bedrock is present.

The uppermost aquifer is laterally continuous across the site, with depth to water ranging from
less than 31 feet in low-lying areas to greater than 77 feet beneath topographic highs.
Groundwater in the uppermost aquifer generally flows from recharge areas associated with broad
gently sloping topographic areas towards topographically lower areas that are generally
delineated by the presence of stream channels, some of which are perennial receiving streams
(groundwater discharge areas) and others of which are intermittent discharging streams. In the
vicinity of the facility, the general groundwater flow direction is towards the south and west.

Groundwater elevations obtained during the January 28, 2016, monitoring event are summarized
in Table 1 and were used to prepare a potentiometric surface map presented as Drawing 1. The
groundwater flow in the uppermost aquifer beneath the site is toward south and west in the

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direction of Abingdon Creek. The potentiometric surface map and interpreted flow directions are
consistent with previously submitted potentiometric surface maps for this facility.

Based on the January 28, 2016, potentiometric surface map, the hydraulic gradient in the shallow
aquifer underlying the site as measured along the conceptual flow paths shown on Drawing 1
was calculated to be approximately 0.03 to 0.38 ft/ft. The effective porosity of the fractured
bedrock aquifer is estimated at 0.10, and the hydraulic conductivity is estimated at 0.374 ft/day
(GAI, 2006).

Using the above values, the estimated rate of groundwater flow for the uppermost aquifer
beneath the facility was calculated using the following modified Darcy equation:

Vgw = Ki/ne

where Vgw = average linear velocity (feet per day), K = hydraulic conductivity (feet per day), i =
horizontal hydraulic gradient, and ne = effective porosity.

The calculated linear groundwater flow velocities under the waste management unit range from
0.12 to 1.43 ft/day (Table 2). The linear velocity equation and resultant rates are based on the
simplified assumptions of a homogeneous and isotropic aquifer. The saprolite may have areas
that exhibit relict foliation and these structures can result in locally anisotropic groundwater
flow; and the fractured bedrock is likely to be highly inhomogeneous and anisotropic.

2.0 FIELD PROGRAM, MONITORING RESULTS, AND DISCUSSION
2.1 Visual Inspection Program
In order to detect potential releases of leachate and/or landfill gas migration in a timely manner,
a visual inspection program has been implemented at the Foothills Regional Landfill. This
inspection program involves field personnel making the following observations:

 Observation of stress induced on the biological community (i.e., dead or dying vegetation),
 Indications of leachate impact (i.e., seeps, impacted surface water),
 Observations of erosion; and
 Negative changes around the waste facility.

During the January, 2016, monitoring event, no physical indications of impacts were observed in
the vicinity of the waste management areas.

2.2 Well Network and Groundwater Elevation Measurements
The network of groundwater monitoring wells at the Foothills Regional Landfill consists of
MW-1R, MW-2R, MW-3R2, MW-4, MW-5, MW-6, MW-7, MW-8, and MW-10. Monitoring

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well construction information is summarized in Table 3 and the well locations are shown on
Drawing 1. A sample from the underdrain for Cell 1 (UD-1) was added to the monitoring
network to monitor groundwater from beneath the landfill prior to the July 2008 sampling event.
A sample from the underdrain for Cells 4 and 8A (UD-2) was added to the monitoring network
to monitor groundwater from beneath the landfill prior to the January 2014 sampling event. The
network of monitoring wells was constructed to target the flow path for groundwater underlying
waste disposal areas. MW-3R2 was added to the monitoring well network as part of the ASD
submitted by Golder (GAI, 2006). Also, as part of the ASD, wells MW-3 and MW-3R were
removed from the compliance network but remain for water level measurements.

Monitoring well MW-1R is the facility’s background well and is located hydraulically
upgradient of the waste disposal area. Monitoring wells MW-2R, MW-3R2, MW-4, MW-5,
MW-6, MW-7, MW-8, MW-10, and underdrains UD-1 and UD-2 are located downgradient or
sidegradient of the waste disposal area and represent the facility’s downgradient compliance
network.

Depth-to-water measurements were recorded to the nearest 0.01 foot prior to initiating
groundwater purging and sampling activities. The water level elevations for this event along
with historical data are presented in Table 1. The data indicate that the hydraulic head level in
the uppermost aquifer beneath the facility is fairly consistent, with temporal variation from the
long-term average limited to approximately 2 to 10 feet. As expected, the range in fluctuation
appears to be greater in the upgradient groundwater recharge area. The range of fluctuation in
the downgradient compliance wells, which are located near groundwater discharge areas, is
much less, presumably due to the stabilizing effect of the hydraulic discharge boundary.

2.3 January 2016 Monitoring Event
Personnel from Joyce Engineering (JOYCE) visited the facility on January 28, 2016, to purge
and sample monitoring wells MW-1R, MW-2R, MW-3R2, MW-4, MW-5, MW-6, MW-7,
MW-8, and MW-10, to sample the underdrains for Cell 1(UD-1) and Cells 4 and 8A (UD-2), to
sample surface water monitoring points SW-1, SW-2, SW-3, and SW-4, and to sample the
leachate. Depth-to-water measurements were obtained from the network monitoring wells prior
to purging.

Monitoring wells MW-1R, MW-2R, MW-3R2, MW-4, MW-5, MW-6, MW-7, MW-8, and
MW-10 were purged and sampled using dedicated bladder pumps and micropurge procedures.
Measurements of temperature, pH, specific conductivity, dissolved oxygen, oxidation-reduction
potential, and turbidity were recorded on approximately 1 to 5-minute intervals during the purge,
depending on the purge rate. In general, the purge rate for each well was matched to the yield of
the monitoring well, as determined by continuously monitoring the depth-to-water, up to a
maximum purge rate of 500 milliliters per minute. Purging was continued until stabilization was
indicated by the field parameters. In general, stabilization was deemed to be complete once the

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range in measured values for the required field parameters was less than 10% per parameter over
three monitoring intervals.

Prior to sampling, the laboratory-supplied sample containers were prepared. Each sample
container was labeled with the sample identification number, sampling personnel, date and time
of sample collection, project name and number, and requested laboratory analyses.

The groundwater samples were collected directly from the dedicated bladder pump discharge
lines in the labeled, laboratory-supplied, pre-preserved sample containers after purging was
completed based on stabilization of field parameters. After collection, the samples were placed in
a cooler on ice, under chain-of-custody control. Copies of the sampling logs are presented in
Appendix A. Included in each log is a description of the sampling equipment, sampling location,
sampling method, field observations, and field parameter measurements.

The underdrain samples were collected directly from the discharge of the underdrain pipes.
UD-1 and UD-2 were sampled on January 28, 2016. The surface water samples were collected
directly from the stream flow, by lowering the sample containers into the stream, taking care to
prevent the over flow of the sample containers and to minimize sample induced turbidity. SW-1,
SW-2, SW-3, and SW-4 samples were collected on January 28, 2016. The leachate sample was a
composite sample collected on January 28, 2016, directly from the leachate piping manifold that
serves the leachate holding tanks. Measurements of temperature, pH, specific conductivity,
turbidity, dissolved oxygen, and oxidation-reduction potential were recorded during the
collection of the surface water samples, and for the composite leachate sample.

After collection, the samples were placed in a cooler on ice, for delivery to the laboratory under
chain-of-custody control. Copies of the sampling logs are presented in Appendix A, and the
filed parameter data are summarized in Table 4. Included in each log is a description of the
sampling location, sampling equipment, sampling method, field observations, and field
parameter measurements.

2.4 Laboratory Analysis Program
The January 28, 2016, groundwater, surface water, and leachate samples were submitted to
Analytical Services, Inc. of Norcross, Georgia, NC laboratory certification number 381, under
chain-of-custody control for analysis. The groundwater, underdrain, surface water, and field
blank samples, were analyzed for North Carolina Appendix I list of constituents. The composite
leachate sample was analyzed for NC Appendix I constituents, Biochemical Oxygen Demand,
Chemical Oxygen Demand, Nitrate as N, Nitrate/Nitrite as N, Nitrite as N, Phosphorous, and
Sulfate. The Trip Blank was analyzed for North Carolina Appendix I organic constituents only.
JOYCE requested a Level II data report for the final laboratory report. The samples were
received by the laboratory on January 29, 2016, in good condition, properly preserved, and
within analysis hold times.

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2.5 January 2016 Sampling Results
Constituents with quantified detections in the January 28, 2016, groundwater and surface water
samples are summarized in Table 5, and exceedances of groundwater or surface water standards
are summarized in Table 6. Historical data tables for groundwater, surface water, and leachate
are included in Appendices D, E, and F, respectively. The laboratory certificates-of-analysis and
chains-of-custody for the monitoring event are included in Appendix B.

Seven inorganic constituents (barium, chromium, cobalt, copper, lead, vanadium and zinc) were
detected in samples from one or more downgradient monitoring points at concentrations above
their respective Solid Waste Section Reporting Limits (SWSLs). Barium was detected above the
SWSL in MW-2R, MW-6, SW-3, UD-1 and UD-2. Copper was detected in SW-3 and UD-1.
Zinc was detected above the SWSL in MW-10, SW-3 and UD-1. Chromium, lead and vanadium
detections above the SWSL were limited to SW-3. Cobalt was detected in MW-4 and UD-1
above the SWSL and above the Solid Waste Section (SWS) Groundwater Protection Standard
(GWPS) during the January 2016 monitoring event. The cobalt detections were not above the
statistical background determined in accordance with 15A NCAC 13B.1632.(g-h); therefore,
they are not consider groundwater protection standard (GPS) exceedances as defined in 15A
NCAC 13B.1634.(g).

Three organic constituents (benzene, trichlorofluoromethane, and vinyl chloride) were reported
at a quantified concentration above their respective SWSLs. Trichlorofluoromethane was
detected in MW-3R2 but was below the North Carolina 15A NCAC 2L (NC2L) Groundwater
Standard. The detection of trichlorofluoromethane in MW-3R2 is consistent with historical data
and is likely related to the source presented in the ASD approved be the NCDEQ in December
2006 for VOCs detected in MW-3 and MW-3R. Trichlorofluoromethane has not been
historically detected in the facility leachate samples.

The initial reported concentrations of benzene and vinyl chloride in MW-2R were 1.1 and 1.0
µg/L, respectively, which were quantified above the SWSLs of 1.0 µg/L and the NC2Ls of 1.0
and 0.03 µg/L, respectively. (The listed NC2L standard for vinyl chloride is 0.03 µg/L;
however, an estimated detection below the SWSL is not considered an exceedance, so the
effective standard is the SWSL.) MW-2R was resampled on March 16, 2016, for benzene and
vinyl chloride and the results were estimated concentrations of 1.0 µg/L for benzene and 0.90
µg/L for vinyl chloride. Since they were estimated concentrations below the SWSL, they were
not considered exceedances, so the initial exceedances were refuted.

No other organic constituents were detected above their respective SWSLs in monitoring wells
or surface water sampling points during the January 2016 event. Constituents detected in
samples collected from the leachate collection system during the January 28, 2016, monitoring
event were generally consistent with historical data.

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3.0 LABORATORY AND FIELD QA/QC
A Field Blank was collected by JOYCE personnel as part of the January 28, 2016, monitoring
event. In addition to the Field Blank, a laboratory-prepared Trip Blank accompanied the volatile
sample containers for the sampling event to and from the laboratory. The Field Blank was
analyzed for NC Appendix I constituents and the Trip Blank for NC Appendix I VOCs only. In
addition to the Field and Trip Blanks, at least one Method Blank was analyzed by the laboratory
for each method used.

Upon receipt of the laboratory data package, the data was reviewed by JOYCE personnel for the
following:

 General typographical errors;
 Correct analyses performed and within method specified hold times;
 Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike Duplicate;
and Laboratory Control Samples;
 Blank qualified data (B-flags);
 Detections above the groundwater and surface water standards; and
 Detections that are above historical levels.

4.0 DATA EVALUTION
4.1 Comparisons to Groundwater and Surface Water Standards
Cobalt was detected in MW-4 and UD-1 at a quantified concentration above its GWPS during
the January 28, 2016, monitoring event; however, it was not detected above the statistical
background (see Section 4.2).

The initial NC2L exceedances for benzene and vinyl chloride in MW-2R were refuted by the
results of the March 2016 resampling event. No other inorganic or organic constituents were
detected at quantified concentrations above their respective NC2L or GWPS during the January
28, 2016, monitoring event.

No inorganic or organic constituents were detected in surface water samples at quantified
concentrations above their respective NC2B surface water standards during the January 28, 2016,
monitoring event.

4.2 Statistical Evaluations
The data were evaluated through the use of the Shapiro-Wilk Test, Parametric Prediction Limits,
Parametric Tolerance Intervals, Aitchison’s Adjustment, Non-parametric Prediction Limits, and
Poisson Prediction Limits, as appropriate. Background data, tests for normality, outliers,
Aitchison’s adjustment, tolerance interval, or prediction limits are used, as appropriate based on
the background data. The statistical test by which downgradient data are compared to facility

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background data is based upon the nature of the data and the number of data values that are less
than the laboratory limit of detection. All statistical tests are evaluated at the 0.05 level of
significance, 95% confidence level, and are conducted as one-tailed tests.

Cobalt was detected in MW-4 and UD-2 at quantified concentrations above the GWPS during
the January 28, 2016, monitoring event. The cobalt detections were statistically evaluated in
accordance with the procedures outlined in 15A NCAC 13B.1632.(g) and (h) to determine if the
quantified concentration exceeded the facility background concentration. The statistical
worksheets and summary table cobalt are presented in Appendix C. Based on the statistical
evaluation, the cobalt detections were not identified as statistically significant and are considered
representative of historical background concentrations; therefore, the facility requests that the
background be considered the applicable groundwater protection standard for cobalt in
accordance with 15A NCAC 13B.1634.(g).(5).

5.0 CONCLUSIONS
Based on the results summarized herein, Republic Services of NC, LLC, will continue
monitoring the uppermost aquifer beneath the Foothills Regional Landfill in accordance with the
requirements for Detection Monitoring Program as outlined in Title 15A NCAC 13B .1633. The
relevant water quality standard for cobalt, used for monitoring result comparison, will be based
on the background concentration. The next compliance monitoring event for this facility is
tentatively scheduled for July 2016.

6.0 REFERENCES
Bunnell-Lamons Engineering, Inc., Groundwater Monitoring Well & Methane Gas Monitoring
Probe Installation Report: Cell No. 8A. June 10, 2013.

Bunnell-Lamons Engineering, Inc., Groundwater Monitoring Well & Methane Gas Monitoring
Probe Installation Report: Cell No. 5A. December 14, 2015.

Golder Associates NC, Inc. (GAI), Alternate Source Demonstration- Volatile Organic
Compounds, May 2006 and Addendum to Alternate Source Demonstration- Volatile Organic
Compounds, November 2006.

Golder Associates NC, Inc. (GAI), February, 2011. First Semi-Annual 2011 Sampling Event.
Prepared for Republic Services of North Carolina, LLC.

JOYCE (Joyce Engineering, Inc.), November 2006. MW-3R2 Installation & Sampling Results.

North Carolina Dept. Environment, Health, and Natural Resources (NCDEHNR), 1995, N.C.
Water Quality Monitoring Guidance Document for Solid Waste Facilities.

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North Carolina Geologic Survey, 1985, Geologic Map of North Carolina; North Carolina
Department of Natural Resources and Community Development, Geological Survey Section;
scale 1:500,000.

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0
8
19
-
J
u
l
-
9
9

1
3
1
2
.
8
6

N
I
NI

1
1
8
8
.
6
9

N
I
NI

1
1
3
0
.
2
2

N
I
NI
NI
NI NI
21
-
J
u
l
-
0
0

1
3
1
0
.
1
6

N
I
NI

1
1
8
9
.
0
8

N
I
NI

1
1
2
7
.
5
9

N
I
NI
NI
NI NI
9-
J
a
n
-
0
1
13
1
0
.
0
9

N
I
NI

1
1
8
6
.
6
2

N
I
NI

1
1
2
7
.
6
0

N
I
NI
NI
NI NI
16
-
J
u
l
-
0
1

1
3
0
9
.
6
9

N
I
NI

1
1
8
6
.
8
9

N
I
NI

1
1
2
7
.
4
0

N
I
NI
NI
NI NI
21
-
J
a
n
-
0
2

1
3
1
0
.
5
5

N
I
NI

1
1
8
5
.
7
3

N
I
NI

1
1
2
7
.
2
8

1
1
2
5
.
8
3

N
I
NI
NI NI
15
-
J
u
l
-
0
2

1
3
0
8
.
7
0

N
I
NI

1
1
8
6
.
1
9

N
I
NI

1
1
2
7
.
3
7

1
1
2
5
.
5
3

N
I
NI
NI NI
29
-
J
a
n
-
0
3

1
3
0
8
.
1
7

N
I

1
2
0
9
.
3
4

1
1
8
9
.
0
7

1
1
8
7
.
0
2

N
I

1
1
2
7
.
6
4

1
1
2
5
.
9
6

N
I
NI
NI NI
30
-
J
u
l
-
0
3

1
3
1
0
.
2
3

N
I

1
2
1
2
.
7
6

1
1
9
3
.
6
0

1
1
8
8
.
1
1

N
I

1
1
3
0
.
0
8

1
1
2
8
.
5
7

N
I
NI
NI NI
14
-
J
a
n
-
0
4

1
3
1
6
.
5
8

N
I

1
2
1
3
.
7
3

1
1
9
1
.
7
2

1
1
8
8
.
2
3

N
I

1
1
2
8
.
9
2

1
1
2
8
.
2
3

N
I
NI
NI NI
15
-
J
u
l
-
0
4

1
3
1
6
.
4
0

N
I

1
2
1
3
.
1
0

1
1
8
4
.
4
9

1
1
8
8
.
3
4

N
I

1
1
2
8
.
6
5

1
1
2
7
.
7
7

N
I
NI
NI NI
27
-
J
a
n
-
0
5

1
3
1
4
.
8
8

N
I

1
2
1
1
.
8
6

1
1
9
3
.
3
5

1
1
8
9
.
3
2

N
I

1
1
3
0
.
1
8

1
1
2
8
.
3
2

N
I
NI
NI NI
21
-
J
u
l
-
0
5

1
3
1
4
.
8
3

N
I

1
2
1
2
.
3
7

1
1
9
3
.
0
1

1
1
9
0
.
9
8

N
I

1
1
2
9
.
8
4

1
1
2
8
.
5
1

N
I
NI
NI NI
18
-
J
a
n
-
0
6

1
3
1
5
.
7
0

N
I

1
2
1
1
.
8
3

1
1
9
2
.
8
2

1
1
9
1
.
0
6

N
I

1
1
2
6
.
6
7

1
1
2
7
.
6
2

1
1
3
1
.
6
9

N
I
NI NI
14
-
M
a
r
-
0
6

1
3
1
5
.
3
3

N
I

1
2
1
1
.
7
1

1
1
8
6
.
6
3

1
1
9
1
.
0
9

N
I

1
1
2
9
.
3
2

1
1
2
7
.
2
8

1
1
3
0
.
4
5

N
I
NI NI
23
-
J
a
n
-
0
7

1
3
1
1
.
2
4

N
I

1
2
1
0
.
1
8
--
--

1
2
0
9
.
8
5

1
1
2
9
.
2
1

1
1
2
6
.
6
5

1
1
2
8
.
9
5

N
I
NI NI
25
-
J
u
l
-
0
7

1
3
1
2
.
4
9

N
I

1
2
1
0
.
3
6

1
1
8
8
.
7
5

1
1
8
5
.
9
3

1
2
0
6
.
3
4

1
1
2
8
.
1
0

1
1
2
5
.
6
9

1
1
2
8
.
0
5

N
I
NI NI
7-
J
a
n
-
0
8
13
1
2
.
0
7

N
I

1
2
0
9
.
1
9

1
1
8
6
.
4
2

1
1
8
4
.
6
1

1
2
0
3
.
3
2

1
1
2
6
.
7
8

1
1
2
4
.
8
0

1
1
2
7
.
2
4

N
I
NI NI
6-
F
e
b
-
0
8
--
NI
--
--
--

1
2
0
3
.
6
3
--
--
--
NI
NI NI
23
-
J
u
l
-
0
8

1
3
1
1
.
0
7

N
I

1
2
0
8
.
4
4

1
1
8
6
.
6
6

1
1
8
4
.
4
9

1
2
0
5
.
8
6

1
1
2
6
.
5
4

1
1
2
4
.
7
2

1
1
2
9
.
0
7

N
I
NI NI
6-
J
a
n
-
0
9
13
1
0
.
1
8

N
I

1
2
0
7
.
9
2

1
1
8
7
.
8
0

1
1
8
6
.
4
4

1
2
0
6
.
1
7

1
1
2
7
.
0
8

1
1
2
5
.
4
0

1
1
2
9
.
4
4

N
I
NI NI
8-
J
u
l
-
0
9
13
0
9
.
4
7

N
I

1
2
0
8
.
6
3

1
1
9
4
.
0
3

1
1
9
0
.
4
2

1
2
1
0
.
2
6

1
1
2
8
.
2
9

1
1
2
6
.
4
9

1
1
3
1
.
5
9

N
I
NI NI
20
-
J
a
n
-
1
0

1
3
1
0
.
5
6

N
I

1
2
1
0
.
6
0

1
1
9
2
.
9
0

1
1
8
8
.
8
8

1
2
1
0
.
2
6

1
1
2
9
.
0
8

1
1
2
7
.
0
0

1
1
3
1
.
5
6

N
I
NI NI
27
-
J
u
l
-
1
0

1
3
1
5
.
1
9

N
I

1
2
1
1
.
8
7

1
1
9
1
.
4
5

1
1
8
7
.
5
0

1
2
0
7
.
7
8

1
1
2
7
.
3
0

1
1
2
6
.
1
0

1
1
3
0
.
4
5

1
1
5
4
.
6
8

N
I
NI
24
-
J
a
n
-
1
1

1
3
1
3
.
7
0

N
I

1
2
1
0
.
9
4

1
1
8
8
.
5
1

1
1
8
5
.
6
9

1
2
0
5
.
7
5

1
1
2
7
.
2
7

1
1
2
5
.
8
0

1
1
2
9
.
5
0

1
1
5
0
.
9
6

N
I
NI
25
-
J
u
l
-
1
1

1
3
1
1
.
8
6

N
I

1
2
1
1
.
3
2

1
1
9
0
.
2
5

1
1
8
7
.
2
4

1
2
0
8
.
0
3

1
1
2
7
.
5
9

1
1
2
6
.
4
5

1
1
2
9
.
4
7

1
1
5
0
.
3
5

N
I
NI
5-
J
a
n
-
1
2
13
1
0
.
6
3

N
I

1
2
1
0
.
1
7
--
--

1
2
0
7
.
9
0

1
1
2
7
.
7
6

1
1
2
6
.
0
7

1
1
2
8
.
8
5

1
1
4
9
.
6
8

N
I
NI
3-
J
u
l
-
1
2
13
1
0
.
0
5

N
I

1
1
7
2
.
7
3
--
--

1
2
0
7
.
9
0

1
1
2
8
.
2
3

1
1
2
6
.
6
2

1
1
2
9
.
2
4

1
1
4
9
.
6
8

N
I
NI
30
-
J
a
n
-
1
3

1
3
1
0
.
0
7

N
I

1
2
1
0
.
8
1

1
1
9
7
.
1
7

1
1
8
7
.
0
3

1
2
0
8
.
3
5

1
1
2
9
.
1
3

1
1
2
6
.
8
6

1
1
2
5
.
9
4

1
1
5
0
.
5
8

N
I
NI
15
-
J
u
l
-
1
3

1
3
1
3
.
0
2

N
I

1
2
0
3
.
9
6

1
1
9
1
.
0
4

1
1
9
0
.
8
0

1
2
1
2
.
9
4

1
1
3
1
.
0
3

1
1
2
8
.
0
2

1
1
3
1
.
4
0

1
1
5
8
.
7
3

1
1
6
4
.
9
0

N
I
30
-
J
a
n
-
1
4

1
3
1
0
.
2
3

N
I

1
2
1
0
.
9
5

1
1
9
3
.
0
3

1
1
8
7
.
0
0

1
2
0
8
.
3
5

1
1
2
9
.
1
7

1
1
2
6
.
9
0

1
1
2
5
.
9
6

1
1
5
0
.
5
8

1
1
6
2
.
1
3

N
I
22
-
J
u
l
-
1
4

1
3
1
3
.
7
3

N
I

1
2
1
3
.
4
7

1
1
9
1
.
9
7

1
1
8
9
.
1
9

1
2
0
9
.
7
8

1
1
2
8
.
0
3

1
1
2
6
.
9
7

1
1
2
9
.
8
9

1
1
5
2
.
8
0

1
1
6
2
.
3
8

N
I
26
-
J
a
n
-
1
5

1
3
1
3
.
3
3

N
I

1
2
1
2
.
4
2

1
1
9
0
.
3
0

1
1
8
8
.
0
8

1
2
0
9
.
2
8

1
1
2
8
.
6
3

1
1
2
7
.
3
7

1
1
2
9
.
8
6

1
1
5
1
.
4
5

1
1
6
3
.
8
1

N
I
28
-
J
u
l
-
1
5

1
3
1
2
.
2
3

N
I

1
2
1
1
.
6
8

1
1
8
9
.
5
3

1
1
8
6
.
9
9

1
2
0
7
.
5
3

1
1
2
8
.
0
3

1
1
2
6
.
5
7

1
1
2
9
.
1
5

1
1
5
0
.
7
8

1
1
6
2
.
7
8

N
I
28
-
J
a
n
-
1
6
AB

1
5
2
7
.
4
5

1
2
1
1
.
3
8

1
1
8
9
.
8
0

1
1
8
8
.
9
4

1
2
1
2
.
8
7

1
1
2
9
.
5
3

1
1
2
7
.
4
2

1
1
3
0
.
7
7

1
1
5
3
.
6
8

1
1
6
4
.
7
8

1
2
8
0
.
9
7
ME
A
N
13
1
2
.
0
4

1
5
2
7
.
4
5

1
2
0
9
.
4
0

1
1
8
9
.
9
2

1
1
8
8
.
0
6

1
2
0
8
.
1
1

1
1
2
8
.
3
5

1
1
2
6
.
7
4

1
1
2
9
.
4
5

1
1
5
2
.
0
0

1
1
6
3
.
4
6

1
2
8
0
.
9
7
MA
X
I
M
U
M
13
1
6
.
5
8

1
5
2
7
.
4
5

1
2
1
3
.
7
3

1
1
9
7
.
1
7

1
1
9
1
.
0
9

1
2
1
2
.
9
4

1
1
3
1
.
0
3

1
1
2
8
.
5
7

1
1
3
1
.
6
9

1
1
5
8
.
7
3

1
1
6
4
.
9
0

1
2
8
0
.
9
7
MI
N
I
M
U
M
13
0
8
.
1
7

1
5
2
7
.
4
5

1
1
7
2
.
7
3

1
1
8
4
.
4
9

1
1
8
4
.
4
9

1
2
0
3
.
3
2

1
1
2
6
.
5
4

1
1
2
4
.
7
2

1
1
2
5
.
9
4

1
1
4
9
.
6
8

1
1
6
2
.
1
3

1
2
8
0
.
9
7
No
t
e
s
:
--

=

N
o

d
a
t
a

a
v
a
i
l
a
b
l
e
.
DT
W

=

D
e
p
t
h

t
o

w
a
t
e
r

f
r
o
m

T
O
C

(
i
n

f
e
e
t
)
.
NI

=

W
e
l
l

n
o
t

y
e
t

i
n
s
t
a
l
l
e
d
.
GW

E
l
e
v
.

=

E
l
e
v
a
t
i
o
n

o
f

G
r
o
u
n
d
w
a
t
e
r

(
i
n

F
t
-
A
M
S
L
)
.
AB

=

A
b
a
n
d
o
n
e
d
.
TO
C

=

T
o
p

o
f

c
a
s
i
n
g
.
All

d
a
t
a

p
r
i
o
r

t
o

2
0
1
2

t
a
k
e
n

f
r
o
m

p
r
e
v
i
o
u
s

r
e
p
o
r
t
s

b
y

G
o
l
d
e
r

A
s
s
o
c
i
a
t
e
s

N
C
,

I
n
c
.

MW
-
5

M
W
-
6

M
W
-
7

M
W
-
8

M
W
-
1
0
MW
-
1
R
Ba
c
k
g
r
o
u
n
d
Do
w
n
g
r
a
d
i
e
n
t
MW
-
1
MW
-
2
R

M
W
-
3

M
W
-
3
R

M
W
-
3
R
2

M
W
-
4
Fo
o
t
h
i
l
l
s

R
e
g
i
o
n
a
l

L
a
n
d
f
i
l
l
Pe
r
m
i
t

N
o
.

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TABLE 4: Field Parameters (January 2016)
WELL ID PARAMETER RESULT UNITS COLLECT DATE
1403-MW1R Temperature 11.40 °C 1/28/2016
1403-MW1R Dissolved Oxygen 5.73 mg/L 1/28/2016
1403-MW1R Conductivity 103.40 µS/cm 1/28/2016
1403-MW1R pH 6.08 S.U 1/28/2016
1403-MW1R Oxidation Reduction Potential 162.80 mV 1/28/2016
1403-MW1R Turbidity 21.60 ntu 1/28/2016
1403-MW1R Static Water Level 66.67 ft 1/28/2016
1403-MW1R Well Depth 78.08 ft 1/28/2016
1403-MW2R Temperature 15.30 °C 1/28/2016
1403-MW2R Dissolved Oxygen 0.44 mg/L 1/28/2016
1403-MW2R Conductivity 109.20 µS/cm 1/28/2016
1403-MW2R pH 6.42 S.U 1/28/2016
1403-MW2R Oxidation Reduction Potential 152.10 mV 1/28/2016
1403-MW2R Turbidity 43.27 ntu 1/28/2016
1403-MW2R Static Water Level 41.98 ft 1/28/2016
1403-MW2R Well Depth 63.70 ft 1/28/2016
1403-MW2R*Temperature 19.70 °C 3/16/2016
1403-MW2R*Dissolved Oxygen 1.10 mg/L 3/16/2016
1403-MW2R*Conductivity 121.40 µS/cm 3/16/2016
1403-MW2R*pH 5.31 S.U 3/16/2016
1403-MW2R* Oxidation Reduction Potential 74.50 mV 3/16/2016
1403-MW2R*Turbidity 12.10 ntu 3/16/2016
1403-MW2R*Static Water Level 41.35 ft 3/16/2016
1403-MW2R*Well Depth 63.60 ft 3/16/2016
1403-MW3 Static Water Level 52.15 ft 1/28/2016
1403-MW3 Well Depth 78.42 ft 1/28/2016
1403-MW3R Static Water Level 53.75 ft 1/28/2016
1403-MW3R Well Depth 77.89 ft 1/28/2016
1403-MW3R2 Temperature 15.40 °C 1/28/2016
1403-MW3R2 Dissolved Oxygen 4.58 mg/L 1/28/2016
1403-MW3R2 Conductivity 79.00 µS/cm 1/28/2016
1403-MW3R2 pH 8.12 S.U 1/28/2016
1403-MW3R2 Oxidation Reduction Potential 4.30 mV 1/28/2016
1403-MW3R2 Turbidity 10.10 ntu 1/28/2016
1403-MW3R2 Static Water Level 27.96 ft 1/28/2016
1403-MW3R2 Well Depth 73.91 ft 1/28/2016
1403-MW4 Temperature 15.20 °C 1/28/2016
1403-MW4 Dissolved Oxygen 0.49 mg/L 1/28/2016
1403-MW4 Conductivity 26.20 µS/cm 1/28/2016
1403-MW4 pH 5.14 S.U 1/28/2016
1403-MW4 Oxidation Reduction Potential 56.80 mV 1/28/2016
1403-MW4 Turbidity 3.40 ntu 1/28/2016
1403-MW4 Static Water Level 41.65 ft 1/28/2016
1403-MW4 Well Depth 52.20 ft 1/28/2016
Republic- Foothills Landfill
Permit No. 14-03 Page 1 of 4
Joyce Engineering
TABLE 4: Field Parameters (January 2016)
WELL ID PARAMETER RESULT UNITS COLLECT DATE
1403-MW5 Temperature 14.20 °C 1/28/2016
1403-MW5 Dissolved Oxygen 3.27 mg/L 1/28/2016
1403-MW5 Conductivity 112.70 µS/cm 1/28/2016
1403-MW5 pH 5.93 S.U 1/28/2016
1403-MW5 Oxidation Reduction Potential 133.10 mV 1/28/2016
1403-MW5 Turbidity 6.10 ntu 1/28/2016
1403-MW5 Static Water Level 47.65 ft 1/28/2016
1403-MW5 Well Depth 54.50 ft 1/28/2016
1403-MW6 Temperature 14.20 °C 1/28/2016
1403-MW6 Dissolved Oxygen 1.01 mg/L 1/28/2016
1403-MW6 Conductivity 89.50 µS/cm 1/28/2016
1403-MW6 pH 5.12 S.U 1/28/2016
1403-MW6 Oxidation Reduction Potential 191.70 mV 1/28/2016
1403-MW6 Turbidity 7.20 ntu 1/28/2016
1403-MW6 Static Water Level 42.98 ft 1/28/2016
1403-MW6 Well Depth 56.57 ft 1/28/2016
1403-MW7 Temperature 14.20 °C 1/28/2016
1403-MW7 Dissolved Oxygen 7.23 mg/L 1/28/2016
1403-MW7 Conductivity 106.10 µS/cm 1/28/2016
1403-MW7 pH 5.52 S.U 1/28/2016
1403-MW7 Oxidation Reduction Potential 157.60 mV 1/28/2016
1403-MW7 Turbidity 14.70 ntu 1/28/2016
1403-MW7 Static Water Level 29.45 ft 1/28/2016
1403-MW7 Well Depth 40.39 ft 1/28/2016
1403-MW8 Temperature 14.20 °C 1/28/2016
1403-MW8 Dissolved Oxygen 0.92 mg/L 1/28/2016
1403-MW8 Conductivity 46.60 µS/cm 1/28/2016
1403-MW8 pH 5.20 S.U 1/28/2016
1403-MW8 Oxidation Reduction Potential 95.90 mV 1/28/2016
1403-MW8 Turbidity 6.50 ntu 1/28/2016
1403-MW8 Static Water Level 30.40 ft 1/28/2016
1403-MW8 Well Depth 49.56 ft 1/28/2016
1403-MW10 Temperature 11.80 °C 1/28/2016
1403-MW10 Dissolved Oxygen 7.38 mg/L 1/28/2016
1403-MW10 Conductivity 50.2 µS/cm 1/28/2016
1403-MW10 pH 6.56 S.U 1/28/2016
1403-MW10 Oxidation Reduction Potential 156.9 mV 1/28/2016
1403-MW10 Turbidity 5.65 ntu 1/28/2016
1403-MW10 Static Water Level 75.11 ft 1/28/2016
1403-MW10 Well Depth 88.21 ft 1/28/2016
Republic- Foothills Landfill
Permit No. 14-03 Page 2 of 4
Joyce Engineering
TABLE 4: Field Parameters (January 2016)
WELL ID PARAMETER RESULT UNITS COLLECT DATE
1403-UD1 Temperature 5.80 °C 1/28/2016
1403-UD1 Dissolved Oxygen 16.62 mg/L 1/28/2016
1403-UD1 Conductivity 473.70 µS/cm 1/28/2016
1403-UD1 pH 5.74 S.U 1/28/2016
1403-UD1 Oxidation Reduction Potential 22.30 mV 1/28/2016
1403-UD1 Turbidity 28.30 ntu 1/28/2016
1403-UD2 Temperature 5.60 °C 1/28/2016
1403-UD2 Dissolved Oxygen 17.82 mg/L 1/28/2016
1403-UD2 Conductivity 379.80 µS/cm 1/28/2016
1403-UD2 pH 5.89 S.U 1/28/2016
1403-UD2 Oxidation Reduction Potential 54.10 mV 1/28/2016
1403-UD2 Turbidity 25.70 ntu 1/28/2016
1403-SW1 Temperature 5.50 °C 1/28/2016
1403-SW1 Dissolved Oxygen 19.60 mg/L 1/28/2016
1403-SW1 Conductivity 32.00 µS/cm 1/28/2016
1403-SW1 pH 5.83 S.U 1/28/2016
1403-SW1 Oxidation Reduction Potential 55.30 mV 1/28/2016
1403-SW1 Turbidity 17.10 ntu 1/28/2016
1403-SW2 Temperature 5.50 °C 1/28/2016
1403-SW2 Dissolved Oxygen 19.60 mg/L 1/28/2016
1403-SW2 Conductivity 32.00 µS/cm 1/28/2016
1403-SW2 pH 5.83 S.U 1/28/2016
1403-SW2 Oxidation Reduction Potential 55.30 mV 1/28/2016
1403-SW2 Turbidity 17.10 ntu 1/28/2016
1403-SW3 Temperature 6.80 °C 1/28/2016
1403-SW3 Dissolved Oxygen 10.89 mg/L 1/28/2016
1403-SW3 Conductivity 101.40 µS/cm 1/28/2016
1403-SW3 pH 7.12 S.U 1/28/2016
1403-SW3 Oxidation Reduction Potential 3.30 mV 1/28/2016
1403-SW3 Turbidity 33.00 ntu 1/28/2016
1403-SW4 Temperature 7.50 °C 1/28/2016
1403-SW4 Dissolved Oxygen 14.45 mg/L 1/28/2016
1403-SW4 Conductivity 52.70 µS/cm 1/28/2016
1403-SW4 pH 7.89 S.U 1/28/2016
1403-SW4 Oxidation Reduction Potential 17.20 mV 1/28/2016
1403-SW4 Turbidity 12.80 ntu 1/28/2016
1403-Leachate Temperature 7.50 °C 1/28/2016
1403-Leachate Dissolved Oxygen 4.04 mg/L 1/28/2016
1403-Leachate Conductivity 6019.00 µS/cm 1/28/2016
1403-Leachate pH 7.28 S.U 1/28/2016
1403-Leachate Oxidation Reduction Potential -101.50 mV 1/28/2016
1403-Leachate Turbidity >1000 ntu 1/28/2016
Republic- Foothills Landfill
Permit No. 14-03 Page 3 of 4
Joyce Engineering
TABLE 4: Field Parameters (January 2016)
WELL ID PARAMETER RESULT UNITS COLLECT DATE
Notes: ºC= degrees Centigrade
mg/L - milligrams per liter
µS/cm = microSiemens per centimeter
S.U.= Standard Units
mV = millivolt
ntu = Nephelometric Turbidity Units
ft = feet
* = Resample (verification) Event.
Republic- Foothills Landfill
Permit No. 14-03 Page 4 of 4
Joyce Engineering
TABLE 5: Quantified Detections in Groundwater and Surface Water
WELL ID PARAMETER RESULT UNITS SWSL DATE
1403-MW2R Barium 211 µg/L 100 1/28/2016
1403-MW2R Benzene 1.1 µg/L 1 1/28/2016
1403-MW2R Benzene*1.0 J µg/L 1 3/16/2016
1403-MW2R Vinyl Chloride 1.0 µg/L 1 1/28/2016
1403-MW2R Vinyl Chloride*0.9 J µg/L 1 3/16/2016
1403-MW3R2 Trichlorofluoromethane 1.4 µg/L 1 1/28/2016
1403-MW4 Cobalt 19.1 µg/L 10 1/28/2016
1403-MW6 Barium 192 µg/L 100 1/28/2016
1403-MW-10 Zinc 14.5 µg/L 10 1/28/2016
1403-SW-3 Barium 224 µg/L 100 1/28/2016
1403-SW-3 Chromium 19.3 µg/L 10 1/28/2016
1403-SW-3 Cobalt 13.2 µg/L 10 1/28/2016
1403-SW-3 Copper 16.2 µg/L 10 1/28/2016
1403-SW-3 Lead 11.1 µg/L 10 1/28/2016
1403-SW-3 Vanadium 42.9 µg/L 25 1/28/2016
1403-SW-3 Zinc 91.8 µg/L 10 1/28/2016
1403-UD1 Barium 179 µg/L 100 1/28/2016
1403-UD1 Cobalt 10.3 µg/L 10 1/28/2016
1403-UD1 Copper 10.3 µg/L 10 1/28/2016
1403-UD1 Zinc 18.4 µg/L 10 1/28/2016
1403-UD2 Barium 140 µg/L 100 1/28/2016
Notes: µg/L = Micorgrams per liter.
SWSL = NC Soild Waste Section Reporting Limit.
Laboratory Reporting limit used when SWSL has not been established.
* = Resample (verification) Event.
J = Estimated concentration below the SWSL.
Republic - Foothills Landfill
Permit No. 14-03 Joyce Engineering
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Appendix B

Laboratory Analytical Reports
and Chains-of-Custody

ASI ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
Republic Services of North Carolina, LLC
Project: Foothills Environmental Landfill
Conover, NC 28613
1220 Commerce Street, SW
Mr. Ray Hoffman
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Analytical Services, Inc. certifies that the
following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the samples analyzed.
Laboratory Report
Project #:[none]
Prepared For:
Attention:
February 19, 2016
Report Number:AZA0693
Approved:
This report may not be reproduced, except in full, without written approval from Analytical Services, Inc.Page 1 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
1403-MW1R AZA0693-01 01/28/16 11:34 01/29/16 07:31Ground Water
1403-MW2R AZA0693-02 01/28/16 14:18 01/29/16 07:31Ground Water
1403-MW3R2 AZA0693-03 01/28/16 13:48 01/29/16 07:31Ground Water
1403-MW4 AZA0693-04 01/28/16 13:08 01/29/16 07:31Ground Water
1403-MW5 AZA0693-05 01/28/16 12:53 01/29/16 07:31Ground Water
1403-MW6 AZA0693-06 01/28/16 12:34 01/29/16 07:31Ground Water
1403-MW7 AZA0693-07 01/28/16 12:21 01/29/16 07:31Ground Water
1403-MW8 AZA0693-08 01/28/16 12:01 01/29/16 07:31Ground Water
1403-MW10 AZA0693-09 01/28/16 10:34 01/29/16 07:31Ground Water
1403-UD1 AZA0693-10 01/28/16 13:18 01/29/16 07:31Ground Water
1403-UD2 AZA0693-11 01/28/16 12:35 01/29/16 07:31Ground Water
1403-SW1 AZA0693-12 01/28/16 12:04 01/29/16 07:31Surface Water
1403-SW2 AZA0693-13 01/28/16 13:12 01/29/16 07:31Surface Water
1403-SW3 AZA0693-14 01/28/16 15:15 01/29/16 07:31Surface Water
1403-SW4 AZA0693-15 01/28/16 15:05 01/29/16 07:31Surface Water
1403-Field Blank AZA0693-16 01/28/16 15:20 01/29/16 07:31Water
1403-Trip Blank AZA0693-17 01/26/16 00:00 01/29/16 07:31Water
Page 2 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW1R
Ground Water
AZA0693-01 AZA069301/28/16 11:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020096EPA 3005A 0.25 7440-36-0 02/05/16 14:0702/05/16 09:00
NDEPA 6020B ug/L1Arsenic10.0 6020096EPA 3005A 0.75 7440-38-2 02/05/16 14:0702/05/16 09:00
EPA 6020B 90.7 ug/L1Barium100 J 6020096EPA 3005A 0.30 7440-39-3 02/05/16 14:0702/05/16 09:00
NDEPA 6020B ug/L1Beryllium1.00 6020096EPA 3005A 0.09 7440-41-7 02/05/16 14:0702/05/16 09:00
NDEPA 6020B ug/L1Cadmium1.00 6020096EPA 3005A 0.10 7440-43-9 02/05/16 14:0702/05/16 09:00
EPA 6020B 0.70 ug/L1Chromium10.0 J 6020096EPA 3005A 0.43 7440-47-3 02/05/16 14:0702/05/16 09:00
EPA 6020B 0.55 ug/L1Cobalt10.0 J 6020096EPA 3005A 0.29 7440-48-4 02/05/16 14:0702/05/16 09:00
EPA 6020B 0.94 ug/L1Copper10.0 J 6020096EPA 3005A 0.41 7440-50-8 02/05/16 14:0702/05/16 09:00
EPA 6020B 0.12 ug/L1Lead10.0 J 6020096EPA 3005A 0.08 7439-92-1 02/05/16 14:0702/05/16 09:00
EPA 6020B 1.24 ug/L1Nickel50.0 J 6020096EPA 3005A 0.48 7440-02-0 02/05/16 14:0702/05/16 09:00
NDEPA 6020B ug/L1Selenium10.0 6020096EPA 3005A 0.85 7782-49-2 02/05/16 14:0702/05/16 09:00
NDEPA 6020B ug/L1Silver10.0 6020096EPA 3005A 0.22 7440-22-4 02/05/16 14:0702/05/16 09:00
NDEPA 6020B ug/L1Thallium5.50 6020096EPA 3005A 0.06 7440-28-0 02/05/16 14:0702/05/16 09:00
EPA 6020B 2.67 ug/L1Vanadium25.0 J 6020096EPA 3005A 1.57 7440-62-2 02/05/16 14:0702/05/16 09:00
EPA 6020B 2.90 ug/L1Zinc10.0 J 6020096EPA 3005A 1.30 7440-66-6 02/05/16 14:0702/05/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 13:0401/29/16 11:30
Page 3 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW1R
Ground Water
AZA0693-01 AZA069301/28/16 11:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 13:0401/29/16 11:30
Page 4 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW1R
Ground Water
AZA0693-01 AZA069301/28/16 11:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 13:0401/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 13:0401/29/16 11:30
EPA 8260B 96 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 13:0401/29/16 11:3080-120
Page 5 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW1R
Ground Water
AZA0693-01 AZA069301/28/16 11:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 103 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 13:0401/29/16 11:3078-120
EPA 8260B 104 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 13:0401/29/16 11:3080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 13:0401/29/16 11:3080-120
Page 6 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW2R
Ground Water
AZA0693-02 AZA069301/28/16 14:18
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020096EPA 3005A 0.25 7440-36-0 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Arsenic10.0 6020096EPA 3005A 0.75 7440-38-2 02/05/16 14:1202/05/16 09:00
EPA 6020B 211 ug/L1Barium100 6020096EPA 3005A 0.30 7440-39-3 02/05/16 14:1202/05/16 09:00
EPA 6020B 0.10 ug/L1Beryllium1.00 J 6020096EPA 3005A 0.09 7440-41-7 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Cadmium1.00 6020096EPA 3005A 0.10 7440-43-9 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Chromium10.0 6020096EPA 3005A 0.43 7440-47-3 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Cobalt10.0 6020096EPA 3005A 0.29 7440-48-4 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Copper10.0 6020096EPA 3005A 0.41 7440-50-8 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Lead10.0 6020096EPA 3005A 0.08 7439-92-1 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Nickel50.0 6020096EPA 3005A 0.48 7440-02-0 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Selenium10.0 6020096EPA 3005A 0.85 7782-49-2 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Silver10.0 6020096EPA 3005A 0.22 7440-22-4 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Thallium5.50 6020096EPA 3005A 0.06 7440-28-0 02/05/16 14:1202/05/16 09:00
NDEPA 6020B ug/L1Vanadium25.0 6020096EPA 3005A 1.57 7440-62-2 02/05/16 14:1202/05/16 09:00
EPA 6020B 1.52 ug/L1Zinc10.0 J 6020096EPA 3005A 1.30 7440-66-6 02/05/16 14:1202/05/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 13:3101/29/16 11:30
EPA 8260B 1.1 ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 13:3101/29/16 11:30
Page 7 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW2R
Ground Water
AZA0693-02 AZA069301/28/16 14:18
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 13:3101/29/16 11:30
EPA 8260B 0.8 ug/L11,1-Dichloroethane 5.0 J 6010632EPA 5030B 0.4 75-34-3 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 13:3101/29/16 11:30
EPA 8260B 1.7 ug/L1cis-1,2-Dichloroethene 5.0 J 6010632EPA 5030B 0.5 156-59-2 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 13:3101/29/16 11:30
Page 8 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW2R
Ground Water
AZA0693-02 AZA069301/28/16 14:18
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 13:3101/29/16 11:30
EPA 8260B 0.7 ug/L1Tetrachloroethene1.0 J 6010632EPA 5030B 0.4 127-18-4 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 13:3101/29/16 11:30
EPA 8260B 0.5 ug/L1Trichloroethene1.0 J 6010632EPA 5030B 0.4 79-01-6 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 13:3101/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 13:3101/29/16 11:30
EPA 8260B 1.0 ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 13:3101/29/16 11:30
EPA 8260B 0.7 ug/L1Xylenes, total 5.0 J 6010632EPA 5030B 0.4 1330-20-7 01/29/16 13:3101/29/16 11:30
EPA 8260B 95 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 13:3101/29/16 11:3080-120
Page 9 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW2R
Ground Water
AZA0693-02 AZA069301/28/16 14:18
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 13:3101/29/16 11:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 13:3101/29/16 11:3080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 13:3101/29/16 11:3080-120
Page 10 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW3R2
Ground Water
AZA0693-03 AZA069301/28/16 13:48
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
EPA 6020B 0.90 ug/L1Antimony6.00 J 6020235EPA 3005A 0.25 7440-36-0 02/11/16 13:4502/10/16 10:05
NDEPA 6020B ug/L1Arsenic10.0 6020235EPA 3005A 0.75 7440-38-2 02/11/16 13:4502/10/16 10:05
EPA 6020B 16.5 ug/L1Barium100 J 6020235EPA 3005A 0.30 7440-39-3 02/11/16 13:4502/10/16 10:05
NDEPA 6020B ug/L1Beryllium1.00 6020235EPA 3005A 0.09 7440-41-7 02/11/16 13:4502/10/16 10:05
NDEPA 6020B ug/L1Cadmium1.00 6020235EPA 3005A 0.10 7440-43-9 02/11/16 13:4502/10/16 10:05
EPA 6020B 0.75 ug/L1Chromium10.0 J 6020235EPA 3005A 0.43 7440-47-3 02/11/16 13:4502/10/16 10:05
EPA 6020B 0.37 ug/L1Cobalt10.0 J 6020235EPA 3005A 0.29 7440-48-4 02/11/16 13:4502/10/16 10:05
NDEPA 6020B ug/L1Copper10.0 6020235EPA 3005A 0.41 7440-50-8 02/11/16 13:4502/10/16 10:05
EPA 6020B 0.10 ug/L1Lead10.0 J 6020235EPA 3005A 0.08 7439-92-1 02/11/16 13:4502/10/16 10:05
EPA 6020B 1.18 ug/L1Nickel50.0 J 6020235EPA 3005A 0.48 7440-02-0 02/11/16 13:4502/10/16 10:05
NDEPA 6020B ug/L1Selenium10.0 6020235EPA 3005A 0.85 7782-49-2 02/11/16 13:4502/10/16 10:05
NDEPA 6020B ug/L1Silver10.0 6020235EPA 3005A 0.22 7440-22-4 02/11/16 13:4502/10/16 10:05
EPA 6020B 0.13 ug/L1Thallium5.50 J 6020235EPA 3005A 0.06 7440-28-0 02/11/16 13:4502/10/16 10:05
NDEPA 6020B ug/L1Vanadium25.0 6020235EPA 3005A 1.57 7440-62-2 02/11/16 13:4502/10/16 10:05
EPA 6020B 2.34 ug/L1Zinc10.0 J 6020235EPA 3005A 1.30 7440-66-6 02/11/16 13:4502/10/16 10:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 13:5701/29/16 11:30
Page 11 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW3R2
Ground Water
AZA0693-03 AZA069301/28/16 13:48
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 13:5701/29/16 11:30
Page 12 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW3R2
Ground Water
AZA0693-03 AZA069301/28/16 13:48
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 13:5701/29/16 11:30
EPA 8260B 1.4 ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 13:5701/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 13:5701/29/16 11:30
EPA 8260B 94 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 13:5701/29/16 11:3080-120
Page 13 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW3R2
Ground Water
AZA0693-03 AZA069301/28/16 13:48
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 102 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 13:5701/29/16 11:3078-120
EPA 8260B 103 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 13:5701/29/16 11:3080-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 13:5701/29/16 11:3080-120
Page 14 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW4
Ground Water
AZA0693-04 AZA069301/28/16 13:08
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020096EPA 3005A 0.25 7440-36-0 02/05/16 14:1702/05/16 09:00
NDEPA 6020B ug/L1Arsenic10.0 6020096EPA 3005A 0.75 7440-38-2 02/05/16 14:1702/05/16 09:00
EPA 6020B 27.3 ug/L1Barium100 J 6020096EPA 3005A 0.30 7440-39-3 02/05/16 14:1702/05/16 09:00
EPA 6020B 0.11 ug/L1Beryllium1.00 J 6020096EPA 3005A 0.09 7440-41-7 02/05/16 14:1702/05/16 09:00
NDEPA 6020B ug/L1Cadmium1.00 6020096EPA 3005A 0.10 7440-43-9 02/05/16 14:1702/05/16 09:00
NDEPA 6020B ug/L1Chromium10.0 6020096EPA 3005A 0.43 7440-47-3 02/05/16 14:1702/05/16 09:00
EPA 6020B 19.1 ug/L1Cobalt10.0 6020096EPA 3005A 0.29 7440-48-4 02/05/16 14:1702/05/16 09:00
NDEPA 6020B ug/L1Copper10.0 6020096EPA 3005A 0.41 7440-50-8 02/05/16 14:1702/05/16 09:00
NDEPA 6020B ug/L1Lead10.0 6020096EPA 3005A 0.08 7439-92-1 02/05/16 14:1702/05/16 09:00
EPA 6020B 0.64 ug/L1Nickel50.0 J 6020096EPA 3005A 0.48 7440-02-0 02/05/16 14:1702/05/16 09:00
NDEPA 6020B ug/L1Selenium10.0 6020096EPA 3005A 0.85 7782-49-2 02/05/16 14:1702/05/16 09:00
EPA 6020B 0.23 ug/L1Silver10.0 J 6020096EPA 3005A 0.22 7440-22-4 02/05/16 14:1702/05/16 09:00
EPA 6020B 0.09 ug/L1Thallium5.50 J 6020096EPA 3005A 0.06 7440-28-0 02/05/16 14:1702/05/16 09:00
NDEPA 6020B ug/L1Vanadium25.0 6020096EPA 3005A 1.57 7440-62-2 02/05/16 14:1702/05/16 09:00
EPA 6020B 2.95 ug/L1Zinc10.0 J 6020096EPA 3005A 1.30 7440-66-6 02/05/16 14:1702/05/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 15:1601/29/16 11:30
Page 15 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW4
Ground Water
AZA0693-04 AZA069301/28/16 13:08
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 15:1601/29/16 11:30
Page 16 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW4
Ground Water
AZA0693-04 AZA069301/28/16 13:08
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 15:1601/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 15:1601/29/16 11:30
EPA 8260B 94 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 15:1601/29/16 11:3080-120
Page 17 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW4
Ground Water
AZA0693-04 AZA069301/28/16 13:08
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 103 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 15:1601/29/16 11:3078-120
EPA 8260B 104 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 15:1601/29/16 11:3080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 15:1601/29/16 11:3080-120
Page 18 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW5
Ground Water
AZA0693-05 AZA069301/28/16 12:53
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020096EPA 3005A 0.25 7440-36-0 02/05/16 14:2102/05/16 09:00
NDEPA 6020B ug/L1Arsenic10.0 6020096EPA 3005A 0.75 7440-38-2 02/05/16 14:2102/05/16 09:00
EPA 6020B 81.5 ug/L1Barium100 J 6020096EPA 3005A 0.30 7440-39-3 02/05/16 14:2102/05/16 09:00
NDEPA 6020B ug/L1Beryllium1.00 6020096EPA 3005A 0.09 7440-41-7 02/05/16 14:2102/05/16 09:00
NDEPA 6020B ug/L1Cadmium1.00 6020096EPA 3005A 0.10 7440-43-9 02/05/16 14:2102/05/16 09:00
EPA 6020B 0.76 ug/L1Chromium10.0 J 6020096EPA 3005A 0.43 7440-47-3 02/05/16 14:2102/05/16 09:00
NDEPA 6020B ug/L1Cobalt10.0 6020096EPA 3005A 0.29 7440-48-4 02/05/16 14:2102/05/16 09:00
NDEPA 6020B ug/L1Copper10.0 6020096EPA 3005A 0.41 7440-50-8 02/05/16 14:2102/05/16 09:00
NDEPA 6020B ug/L1Lead10.0 6020096EPA 3005A 0.08 7439-92-1 02/05/16 14:2102/05/16 09:00
NDEPA 6020B ug/L1Nickel50.0 6020096EPA 3005A 0.48 7440-02-0 02/05/16 14:2102/05/16 09:00
NDEPA 6020B ug/L1Selenium10.0 6020096EPA 3005A 0.85 7782-49-2 02/05/16 14:2102/05/16 09:00
EPA 6020B 0.27 ug/L1Silver10.0 J 6020096EPA 3005A 0.22 7440-22-4 02/05/16 14:2102/05/16 09:00
NDEPA 6020B ug/L1Thallium5.50 6020096EPA 3005A 0.06 7440-28-0 02/05/16 14:2102/05/16 09:00
EPA 6020B 2.60 ug/L1Vanadium25.0 J 6020096EPA 3005A 1.57 7440-62-2 02/05/16 14:2102/05/16 09:00
EPA 6020B 1.87 ug/L1Zinc10.0 J 6020096EPA 3005A 1.30 7440-66-6 02/05/16 14:2102/05/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 15:4201/29/16 11:30
Page 19 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW5
Ground Water
AZA0693-05 AZA069301/28/16 12:53
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 15:4201/29/16 11:30
Page 20 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW5
Ground Water
AZA0693-05 AZA069301/28/16 12:53
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 15:4201/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 15:4201/29/16 11:30
EPA 8260B 93 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 15:4201/29/16 11:3080-120
Page 21 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW5
Ground Water
AZA0693-05 AZA069301/28/16 12:53
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 15:4201/29/16 11:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 15:4201/29/16 11:3080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 15:4201/29/16 11:3080-120
Page 22 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW6
Ground Water
AZA0693-06 AZA069301/28/16 12:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020096EPA 3005A 0.25 7440-36-0 02/05/16 14:2602/05/16 09:00
NDEPA 6020B ug/L1Arsenic10.0 6020096EPA 3005A 0.75 7440-38-2 02/05/16 14:2602/05/16 09:00
EPA 6020B 192 ug/L1Barium100 6020096EPA 3005A 0.30 7440-39-3 02/05/16 14:2602/05/16 09:00
EPA 6020B 0.70 ug/L1Beryllium1.00 J 6020096EPA 3005A 0.09 7440-41-7 02/05/16 14:2602/05/16 09:00
EPA 6020B 0.11 ug/L1Cadmium1.00 J 6020096EPA 3005A 0.10 7440-43-9 02/05/16 14:2602/05/16 09:00
EPA 6020B 0.57 ug/L1Chromium10.0 J 6020096EPA 3005A 0.43 7440-47-3 02/05/16 14:2602/05/16 09:00
EPA 6020B 4.94 ug/L1Cobalt10.0 J 6020096EPA 3005A 0.29 7440-48-4 02/05/16 14:2602/05/16 09:00
NDEPA 6020B ug/L1Copper10.0 6020096EPA 3005A 0.41 7440-50-8 02/05/16 14:2602/05/16 09:00
EPA 6020B 0.23 ug/L1Lead10.0 J 6020096EPA 3005A 0.08 7439-92-1 02/05/16 14:2602/05/16 09:00
EPA 6020B 0.53 ug/L1Nickel50.0 J 6020096EPA 3005A 0.48 7440-02-0 02/05/16 14:2602/05/16 09:00
EPA 6020B 1.08 ug/L1Selenium10.0 J 6020096EPA 3005A 0.85 7782-49-2 02/05/16 14:2602/05/16 09:00
EPA 6020B 1.15 ug/L1Silver10.0 J 6020096EPA 3005A 0.22 7440-22-4 02/05/16 14:2602/05/16 09:00
EPA 6020B 0.07 ug/L1Thallium5.50 J 6020096EPA 3005A 0.06 7440-28-0 02/05/16 14:2602/05/16 09:00
EPA 6020B 2.13 ug/L1Vanadium25.0 J 6020096EPA 3005A 1.57 7440-62-2 02/05/16 14:2602/05/16 09:00
EPA 6020B 2.43 ug/L1Zinc10.0 J 6020096EPA 3005A 1.30 7440-66-6 02/05/16 14:2602/05/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 16:0901/29/16 11:30
Page 23 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW6
Ground Water
AZA0693-06 AZA069301/28/16 12:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 16:0901/29/16 11:30
Page 24 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW6
Ground Water
AZA0693-06 AZA069301/28/16 12:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 16:0901/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 16:0901/29/16 11:30
EPA 8260B 94 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 16:0901/29/16 11:3080-120
Page 25 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW6
Ground Water
AZA0693-06 AZA069301/28/16 12:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 103 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 16:0901/29/16 11:3078-120
EPA 8260B 104 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 16:0901/29/16 11:3080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 16:0901/29/16 11:3080-120
Page 26 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW7
Ground Water
AZA0693-07 AZA069301/28/16 12:21
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020096EPA 3005A 0.25 7440-36-0 02/05/16 14:3102/05/16 09:00
NDEPA 6020B ug/L1Arsenic10.0 6020096EPA 3005A 0.75 7440-38-2 02/05/16 14:3102/05/16 09:00
EPA 6020B 67.6 ug/L1Barium100 J 6020096EPA 3005A 0.30 7440-39-3 02/05/16 14:3102/05/16 09:00
EPA 6020B 0.36 ug/L1Beryllium1.00 J 6020096EPA 3005A 0.09 7440-41-7 02/05/16 14:3102/05/16 09:00
NDEPA 6020B ug/L1Cadmium1.00 6020096EPA 3005A 0.10 7440-43-9 02/05/16 14:3102/05/16 09:00
EPA 6020B 4.01 ug/L1Chromium10.0 J 6020096EPA 3005A 0.43 7440-47-3 02/05/16 14:3102/05/16 09:00
EPA 6020B 0.62 ug/L1Cobalt10.0 J 6020096EPA 3005A 0.29 7440-48-4 02/05/16 14:3102/05/16 09:00
EPA 6020B 1.79 ug/L1Copper10.0 J 6020096EPA 3005A 0.41 7440-50-8 02/05/16 14:3102/05/16 09:00
EPA 6020B 0.53 ug/L1Lead10.0 J 6020096EPA 3005A 0.08 7439-92-1 02/05/16 14:3102/05/16 09:00
EPA 6020B 2.01 ug/L1Nickel50.0 J 6020096EPA 3005A 0.48 7440-02-0 02/05/16 14:3102/05/16 09:00
EPA 6020B 1.27 ug/L1Selenium10.0 J 6020096EPA 3005A 0.85 7782-49-2 02/05/16 14:3102/05/16 09:00
EPA 6020B 2.62 ug/L1Silver10.0 J 6020096EPA 3005A 0.22 7440-22-4 02/05/16 14:3102/05/16 09:00
NDEPA 6020B ug/L1Thallium5.50 6020096EPA 3005A 0.06 7440-28-0 02/05/16 14:3102/05/16 09:00
EPA 6020B 3.99 ug/L1Vanadium25.0 J 6020096EPA 3005A 1.57 7440-62-2 02/05/16 14:3102/05/16 09:00
EPA 6020B 4.24 ug/L1Zinc10.0 J 6020096EPA 3005A 1.30 7440-66-6 02/05/16 14:3102/05/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 16:3501/29/16 11:30
Page 27 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW7
Ground Water
AZA0693-07 AZA069301/28/16 12:21
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 16:3501/29/16 11:30
Page 28 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW7
Ground Water
AZA0693-07 AZA069301/28/16 12:21
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 16:3501/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 16:3501/29/16 11:30
EPA 8260B 95 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 16:3501/29/16 11:3080-120
Page 29 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW7
Ground Water
AZA0693-07 AZA069301/28/16 12:21
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 103 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 16:3501/29/16 11:3078-120
EPA 8260B 106 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 16:3501/29/16 11:3080-120
EPA 8260B 106 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 16:3501/29/16 11:3080-120
Page 30 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW8
Ground Water
AZA0693-08 AZA069301/28/16 12:01
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020096EPA 3005A 0.25 7440-36-0 02/05/16 14:5102/05/16 09:00
NDEPA 6020B ug/L1Arsenic10.0 6020096EPA 3005A 0.75 7440-38-2 02/05/16 14:5102/05/16 09:00
EPA 6020B 50.5 ug/L1Barium100 J 6020096EPA 3005A 0.30 7440-39-3 02/05/16 14:5102/05/16 09:00
EPA 6020B 0.35 ug/L1Beryllium1.00 J 6020096EPA 3005A 0.09 7440-41-7 02/05/16 14:5102/05/16 09:00
NDEPA 6020B ug/L1Cadmium1.00 6020096EPA 3005A 0.10 7440-43-9 02/05/16 14:5102/05/16 09:00
NDEPA 6020B ug/L1Chromium10.0 6020096EPA 3005A 0.43 7440-47-3 02/05/16 14:5102/05/16 09:00
EPA 6020B 4.19 ug/L1Cobalt10.0 J 6020096EPA 3005A 0.29 7440-48-4 02/05/16 14:5102/05/16 09:00
NDEPA 6020B ug/L1Copper10.0 6020096EPA 3005A 0.41 7440-50-8 02/05/16 14:5102/05/16 09:00
NDEPA 6020B ug/L1Lead10.0 6020096EPA 3005A 0.08 7439-92-1 02/05/16 14:5102/05/16 09:00
EPA 6020B 1.61 ug/L1Nickel50.0 J 6020096EPA 3005A 0.48 7440-02-0 02/05/16 14:5102/05/16 09:00
NDEPA 6020B ug/L1Selenium10.0 6020096EPA 3005A 0.85 7782-49-2 02/05/16 14:5102/05/16 09:00
NDEPA 6020B ug/L1Silver10.0 6020096EPA 3005A 0.22 7440-22-4 02/05/16 14:5102/05/16 09:00
NDEPA 6020B ug/L1Thallium5.50 6020096EPA 3005A 0.06 7440-28-0 02/05/16 14:5102/05/16 09:00
NDEPA 6020B ug/L1Vanadium25.0 6020096EPA 3005A 1.57 7440-62-2 02/05/16 14:5102/05/16 09:00
EPA 6020B 2.96 ug/L1Zinc10.0 J 6020096EPA 3005A 1.30 7440-66-6 02/05/16 14:5102/05/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 17:0101/29/16 11:30
Page 31 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW8
Ground Water
AZA0693-08 AZA069301/28/16 12:01
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 17:0101/29/16 11:30
Page 32 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW8
Ground Water
AZA0693-08 AZA069301/28/16 12:01
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 17:0101/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 17:0101/29/16 11:30
EPA 8260B 93 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 17:0101/29/16 11:3080-120
Page 33 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW8
Ground Water
AZA0693-08 AZA069301/28/16 12:01
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 102 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 17:0101/29/16 11:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 17:0101/29/16 11:3080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 17:0101/29/16 11:3080-120
Page 34 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW10
Ground Water
AZA0693-09 AZA069301/28/16 10:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020096EPA 3005A 0.25 7440-36-0 02/05/16 14:5602/05/16 09:00
NDEPA 6020B ug/L1Arsenic10.0 6020096EPA 3005A 0.75 7440-38-2 02/05/16 14:5602/05/16 09:00
EPA 6020B 38.2 ug/L1Barium100 J 6020096EPA 3005A 0.30 7440-39-3 02/05/16 14:5602/05/16 09:00
EPA 6020B 0.12 ug/L1Beryllium1.00 J 6020096EPA 3005A 0.09 7440-41-7 02/05/16 14:5602/05/16 09:00
NDEPA 6020B ug/L1Cadmium1.00 6020096EPA 3005A 0.10 7440-43-9 02/05/16 14:5602/05/16 09:00
EPA 6020B 3.91 ug/L1Chromium10.0 J 6020096EPA 3005A 0.43 7440-47-3 02/05/16 14:5602/05/16 09:00
EPA 6020B 1.85 ug/L1Cobalt10.0 J 6020096EPA 3005A 0.29 7440-48-4 02/05/16 14:5602/05/16 09:00
EPA 6020B 3.87 ug/L1Copper10.0 J 6020096EPA 3005A 0.41 7440-50-8 02/05/16 14:5602/05/16 09:00
EPA 6020B 1.29 ug/L1Lead10.0 J 6020096EPA 3005A 0.08 7439-92-1 02/05/16 14:5602/05/16 09:00
EPA 6020B 2.55 ug/L1Nickel50.0 J 6020096EPA 3005A 0.48 7440-02-0 02/05/16 14:5602/05/16 09:00
EPA 6020B 0.95 ug/L1Selenium10.0 J 6020096EPA 3005A 0.85 7782-49-2 02/05/16 14:5602/05/16 09:00
NDEPA 6020B ug/L1Silver10.0 6020096EPA 3005A 0.22 7440-22-4 02/05/16 14:5602/05/16 09:00
EPA 6020B 0.08 ug/L1Thallium5.50 J 6020096EPA 3005A 0.06 7440-28-0 02/05/16 14:5602/05/16 09:00
EPA 6020B 7.60 ug/L1Vanadium25.0 J 6020096EPA 3005A 1.57 7440-62-2 02/05/16 14:5602/05/16 09:00
EPA 6020B 14.5 ug/L1Zinc10.0 6020096EPA 3005A 1.30 7440-66-6 02/05/16 14:5602/05/16 09:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 17:2701/29/16 11:30
Page 35 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW10
Ground Water
AZA0693-09 AZA069301/28/16 10:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 17:2701/29/16 11:30
Page 36 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW10
Ground Water
AZA0693-09 AZA069301/28/16 10:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 17:2701/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 17:2701/29/16 11:30
EPA 8260B 93 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 17:2701/29/16 11:3080-120
Page 37 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW10
Ground Water
AZA0693-09 AZA069301/28/16 10:34
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 104 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 17:2701/29/16 11:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 17:2701/29/16 11:3080-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 17:2701/29/16 11:3080-120
Page 38 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-UD1
Ground Water
AZA0693-10 AZA069301/28/16 13:18
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
EPA 6020B 4.37 ug/L1Antimony6.00 J 6020096EPA 3005A 0.25 7440-36-0 02/05/16 15:0002/05/16 09:00
EPA 6020B 1.82 ug/L1Arsenic10.0 J 6020096EPA 3005A 0.75 7440-38-2 02/05/16 15:0002/05/16 09:00
EPA 6020B 179 ug/L1Barium100 6020096EPA 3005A 0.30 7440-39-3 02/05/16 15:0002/05/16 09:00
EPA 6020B 0.55 ug/L1Beryllium1.00 J 6020096EPA 3005A 0.09 7440-41-7 02/05/16 15:0002/05/16 09:00
NDEPA 6020B ug/L1Cadmium1.00 6020096EPA 3005A 0.10 7440-43-9 02/05/16 15:0002/05/16 09:00
EPA 6020B 9.71 ug/L1Chromium10.0 J 6020096EPA 3005A 0.43 7440-47-3 02/05/16 15:0002/05/16 09:00
EPA 6020B 10.3 ug/L1Cobalt10.0 6020096EPA 3005A 0.29 7440-48-4 02/05/16 15:0002/05/16 09:00
EPA 6020B 10.3 ug/L1Copper10.0 6020096EPA 3005A 0.41 7440-50-8 02/05/16 15:0002/05/16 09:00
EPA 6020B 5.34 ug/L1Lead10.0 J 6020096EPA 3005A 0.08 7439-92-1 02/05/16 15:0002/05/16 09:00
EPA 6020B 13.5 ug/L1Nickel50.0 J 6020096EPA 3005A 0.48 7440-02-0 02/05/16 15:0002/05/16 09:00
EPA 6020B 3.29 ug/L1Selenium10.0 J 6020096EPA 3005A 0.85 7782-49-2 02/05/16 15:0002/05/16 09:00
NDEPA 6020B ug/L1Silver10.0 6020096EPA 3005A 0.22 7440-22-4 02/05/16 15:0002/05/16 09:00
EPA 6020B 0.14 ug/L1Thallium5.50 J 6020096EPA 3005A 0.06 7440-28-0 02/05/16 15:0002/05/16 09:00
EPA 6020B 22.8 ug/L1Vanadium25.0 J 6020096EPA 3005A 1.57 7440-62-2 02/05/16 15:0002/05/16 09:00
EPA 6020B 18.4 ug/L1Zinc10.0 6020096EPA 3005A 1.30 7440-66-6 02/05/16 15:0002/05/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 21 ug/L1Acetone100 J 6010632EPA 5030B 4.9 67-64-1 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 17:5401/29/16 11:30
Page 39 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-UD1
Ground Water
AZA0693-10 AZA069301/28/16 13:18
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 17:5401/29/16 11:30
Page 40 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-UD1
Ground Water
AZA0693-10 AZA069301/28/16 13:18
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 17:5401/29/16 11:30
EPA 8260B 3.0 ug/L1Methyl Ethyl Ketone
(2-Butanone)100 J 6010632EPA 5030B 1.1 78-93-3 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 17:5401/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 17:5401/29/16 11:30
Page 41 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-UD1
Ground Water
AZA0693-10 AZA069301/28/16 13:18
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 94 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 17:5401/29/16 11:3080-120
EPA 8260B 99 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 17:5401/29/16 11:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 17:5401/29/16 11:3080-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 17:5401/29/16 11:3080-120
Page 42 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-UD2
Ground Water
AZA0693-11 AZA069301/28/16 12:35
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
EPA 6020B 1.98 ug/L1Antimony6.00 J 6020235EPA 3005A 0.25 7440-36-0 02/11/16 13:5002/10/16 10:05
EPA 6020B 1.27 ug/L1Arsenic10.0 J 6020235EPA 3005A 0.75 7440-38-2 02/11/16 13:5002/10/16 10:05
EPA 6020B 140 ug/L1Barium100 6020235EPA 3005A 0.30 7440-39-3 02/11/16 13:5002/10/16 10:05
EPA 6020B 0.19 ug/L1Beryllium1.00 J 6020235EPA 3005A 0.09 7440-41-7 02/11/16 13:5002/10/16 10:05
NDEPA 6020B ug/L1Cadmium1.00 6020235EPA 3005A 0.10 7440-43-9 02/11/16 13:5002/10/16 10:05
EPA 6020B 6.04 ug/L1Chromium10.0 J 6020235EPA 3005A 0.43 7440-47-3 02/11/16 13:5002/10/16 10:05
EPA 6020B 8.85 ug/L1Cobalt10.0 J 6020235EPA 3005A 0.29 7440-48-4 02/11/16 13:5002/10/16 10:05
EPA 6020B 4.33 ug/L1Copper10.0 J 6020235EPA 3005A 0.41 7440-50-8 02/11/16 13:5002/10/16 10:05
EPA 6020B 2.18 ug/L1Lead10.0 J 6020235EPA 3005A 0.08 7439-92-1 02/11/16 13:5002/10/16 10:05
EPA 6020B 11.9 ug/L1Nickel50.0 J 6020235EPA 3005A 0.48 7440-02-0 02/11/16 13:5002/10/16 10:05
EPA 6020B 1.56 ug/L1Selenium10.0 J 6020235EPA 3005A 0.85 7782-49-2 02/11/16 13:5002/10/16 10:05
NDEPA 6020B ug/L1Silver10.0 6020235EPA 3005A 0.22 7440-22-4 02/11/16 13:5002/10/16 10:05
EPA 6020B 0.11 ug/L1Thallium5.50 J 6020235EPA 3005A 0.06 7440-28-0 02/11/16 13:5002/10/16 10:05
EPA 6020B 12.0 ug/L1Vanadium25.0 J 6020235EPA 3005A 1.57 7440-62-2 02/11/16 13:5002/10/16 10:05
EPA 6020B 7.18 ug/L1Zinc10.0 J 6020235EPA 3005A 1.30 7440-66-6 02/11/16 13:5002/10/16 10:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 20:5701/29/16 11:30
Page 43 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-UD2
Ground Water
AZA0693-11 AZA069301/28/16 12:35
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 20:5701/29/16 11:30
Page 44 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-UD2
Ground Water
AZA0693-11 AZA069301/28/16 12:35
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 20:5701/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 20:5701/29/16 11:30
EPA 8260B 95 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 20:5701/29/16 11:3080-120
Page 45 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-UD2
Ground Water
AZA0693-11 AZA069301/28/16 12:35
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 20:5701/29/16 11:3078-120
EPA 8260B 106 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 20:5701/29/16 11:3080-120
EPA 8260B 106 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 20:5701/29/16 11:3080-120
Page 46 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW1
Surface Water
AZA0693-12 AZA069301/28/16 12:04
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020235EPA 3005A 0.25 7440-36-0 02/11/16 13:5502/10/16 10:05
NDEPA 6020B ug/L1Arsenic10.0 6020235EPA 3005A 0.75 7440-38-2 02/11/16 13:5502/10/16 10:05
EPA 6020B 19.6 ug/L1Barium100 J 6020235EPA 3005A 0.30 7440-39-3 02/11/16 13:5502/10/16 10:05
NDEPA 6020B ug/L1Beryllium1.00 6020235EPA 3005A 0.09 7440-41-7 02/11/16 13:5502/10/16 10:05
NDEPA 6020B ug/L1Cadmium1.00 6020235EPA 3005A 0.10 7440-43-9 02/11/16 13:5502/10/16 10:05
EPA 6020B 1.14 ug/L1Chromium10.0 J 6020235EPA 3005A 0.43 7440-47-3 02/11/16 13:5502/10/16 10:05
EPA 6020B 0.51 ug/L1Cobalt10.0 J 6020235EPA 3005A 0.29 7440-48-4 02/11/16 13:5502/10/16 10:05
NDEPA 6020B ug/L1Copper10.0 6020235EPA 3005A 0.41 7440-50-8 02/11/16 13:5502/10/16 10:05
EPA 6020B 0.37 ug/L1Lead10.0 J 6020235EPA 3005A 0.08 7439-92-1 02/11/16 13:5502/10/16 10:05
EPA 6020B 0.54 ug/L1Nickel50.0 J 6020235EPA 3005A 0.48 7440-02-0 02/11/16 13:5502/10/16 10:05
NDEPA 6020B ug/L1Selenium10.0 6020235EPA 3005A 0.85 7782-49-2 02/11/16 13:5502/10/16 10:05
NDEPA 6020B ug/L1Silver10.0 6020235EPA 3005A 0.22 7440-22-4 02/11/16 13:5502/10/16 10:05
NDEPA 6020B ug/L1Thallium5.50 6020235EPA 3005A 0.06 7440-28-0 02/11/16 13:5502/10/16 10:05
EPA 6020B 2.86 ug/L1Vanadium25.0 J 6020235EPA 3005A 1.57 7440-62-2 02/11/16 13:5502/10/16 10:05
EPA 6020B 1.75 ug/L1Zinc10.0 J 6020235EPA 3005A 1.30 7440-66-6 02/11/16 13:5502/10/16 10:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 18:2001/29/16 11:30
Page 47 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW1
Surface Water
AZA0693-12 AZA069301/28/16 12:04
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 18:2001/29/16 11:30
Page 48 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW1
Surface Water
AZA0693-12 AZA069301/28/16 12:04
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 18:2001/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 18:2001/29/16 11:30
EPA 8260B 95 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 18:2001/29/16 11:3080-120
Page 49 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW1
Surface Water
AZA0693-12 AZA069301/28/16 12:04
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 105 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 18:2001/29/16 11:3078-120
EPA 8260B 104 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 18:2001/29/16 11:3080-120
EPA 8260B 106 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 18:2001/29/16 11:3080-120
Page 50 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW2
Surface Water
AZA0693-13 AZA069301/28/16 13:12
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020235EPA 3005A 0.25 7440-36-0 02/11/16 14:0002/10/16 10:05
NDEPA 6020B ug/L1Arsenic10.0 6020235EPA 3005A 0.75 7440-38-2 02/11/16 14:0002/10/16 10:05
EPA 6020B 23.9 ug/L1Barium100 J 6020235EPA 3005A 0.30 7440-39-3 02/11/16 14:0002/10/16 10:05
NDEPA 6020B ug/L1Beryllium1.00 6020235EPA 3005A 0.09 7440-41-7 02/11/16 14:0002/10/16 10:05
NDEPA 6020B ug/L1Cadmium1.00 6020235EPA 3005A 0.10 7440-43-9 02/11/16 14:0002/10/16 10:05
EPA 6020B 0.63 ug/L1Chromium10.0 J 6020235EPA 3005A 0.43 7440-47-3 02/11/16 14:0002/10/16 10:05
EPA 6020B 0.92 ug/L1Cobalt10.0 J 6020235EPA 3005A 0.29 7440-48-4 02/11/16 14:0002/10/16 10:05
NDEPA 6020B ug/L1Copper10.0 6020235EPA 3005A 0.41 7440-50-8 02/11/16 14:0002/10/16 10:05
EPA 6020B 0.20 ug/L1Lead10.0 J 6020235EPA 3005A 0.08 7439-92-1 02/11/16 14:0002/10/16 10:05
EPA 6020B 0.54 ug/L1Nickel50.0 J 6020235EPA 3005A 0.48 7440-02-0 02/11/16 14:0002/10/16 10:05
NDEPA 6020B ug/L1Selenium10.0 6020235EPA 3005A 0.85 7782-49-2 02/11/16 14:0002/10/16 10:05
NDEPA 6020B ug/L1Silver10.0 6020235EPA 3005A 0.22 7440-22-4 02/11/16 14:0002/10/16 10:05
NDEPA 6020B ug/L1Thallium5.50 6020235EPA 3005A 0.06 7440-28-0 02/11/16 14:0002/10/16 10:05
EPA 6020B 2.49 ug/L1Vanadium25.0 J 6020235EPA 3005A 1.57 7440-62-2 02/11/16 14:0002/10/16 10:05
NDEPA 6020B ug/L1Zinc10.0 6020235EPA 3005A 1.30 7440-66-6 02/11/16 14:0002/10/16 10:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 18:4601/29/16 11:30
Page 51 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW2
Surface Water
AZA0693-13 AZA069301/28/16 13:12
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 18:4601/29/16 11:30
Page 52 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW2
Surface Water
AZA0693-13 AZA069301/28/16 13:12
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 18:4601/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 18:4601/29/16 11:30
EPA 8260B 94 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 18:4601/29/16 11:3080-120
Page 53 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW2
Surface Water
AZA0693-13 AZA069301/28/16 13:12
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 18:4601/29/16 11:3078-120
EPA 8260B 103 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 18:4601/29/16 11:3080-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 18:4601/29/16 11:3080-120
Page 54 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW3
Surface Water
AZA0693-14 AZA069301/28/16 15:15
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020235EPA 3005A 0.25 7440-36-0 02/11/16 14:0502/10/16 10:05
EPA 6020B 1.33 ug/L1Arsenic10.0 J 6020235EPA 3005A 0.75 7440-38-2 02/11/16 14:0502/10/16 10:05
EPA 6020B 224 ug/L1Barium100 6020235EPA 3005A 0.30 7440-39-3 02/11/16 14:0502/10/16 10:05
EPA 6020B 0.82 ug/L1Beryllium1.00 J 6020235EPA 3005A 0.09 7440-41-7 02/11/16 14:0502/10/16 10:05
NDEPA 6020B ug/L1Cadmium1.00 6020235EPA 3005A 0.10 7440-43-9 02/11/16 14:0502/10/16 10:05
EPA 6020B 19.3 ug/L1Chromium10.0 6020235EPA 3005A 0.43 7440-47-3 02/11/16 14:0502/10/16 10:05
EPA 6020B 13.2 ug/L1Cobalt10.0 6020235EPA 3005A 0.29 7440-48-4 02/11/16 14:0502/10/16 10:05
EPA 6020B 16.2 ug/L1Copper10.0 6020235EPA 3005A 0.41 7440-50-8 02/11/16 14:0502/10/16 10:05
EPA 6020B 11.1 ug/L1Lead10.0 6020235EPA 3005A 0.08 7439-92-1 02/11/16 14:0502/10/16 10:05
EPA 6020B 13.2 ug/L1Nickel50.0 J 6020235EPA 3005A 0.48 7440-02-0 02/11/16 14:0502/10/16 10:05
EPA 6020B 2.24 ug/L1Selenium10.0 J 6020235EPA 3005A 0.85 7782-49-2 02/11/16 14:0502/10/16 10:05
NDEPA 6020B ug/L1Silver10.0 6020235EPA 3005A 0.22 7440-22-4 02/11/16 14:0502/10/16 10:05
EPA 6020B 0.42 ug/L1Thallium5.50 J 6020235EPA 3005A 0.06 7440-28-0 02/11/16 14:0502/10/16 10:05
EPA 6020B 42.9 ug/L1Vanadium25.0 6020235EPA 3005A 1.57 7440-62-2 02/11/16 14:0502/10/16 10:05
EPA 6020B 91.8 ug/L1Zinc10.0 6020235EPA 3005A 1.30 7440-66-6 02/11/16 14:0502/10/16 10:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 19:1301/29/16 11:30
Page 55 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW3
Surface Water
AZA0693-14 AZA069301/28/16 15:15
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 19:1301/29/16 11:30
Page 56 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW3
Surface Water
AZA0693-14 AZA069301/28/16 15:15
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 19:1301/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 19:1301/29/16 11:30
EPA 8260B 95 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 19:1301/29/16 11:3080-120
Page 57 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW3
Surface Water
AZA0693-14 AZA069301/28/16 15:15
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 102 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 19:1301/29/16 11:3078-120
EPA 8260B 104 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 19:1301/29/16 11:3080-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 19:1301/29/16 11:3080-120
Page 58 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW4
Surface Water
AZA0693-15 AZA069301/28/16 15:05
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020235EPA 3005A 0.25 7440-36-0 02/11/16 14:2002/10/16 10:05
NDEPA 6020B ug/L1Arsenic10.0 6020235EPA 3005A 0.75 7440-38-2 02/11/16 14:2002/10/16 10:05
EPA 6020B 25.8 ug/L1Barium100 J 6020235EPA 3005A 0.30 7440-39-3 02/11/16 14:2002/10/16 10:05
NDEPA 6020B ug/L1Beryllium1.00 6020235EPA 3005A 0.09 7440-41-7 02/11/16 14:2002/10/16 10:05
NDEPA 6020B ug/L1Cadmium1.00 6020235EPA 3005A 0.10 7440-43-9 02/11/16 14:2002/10/16 10:05
EPA 6020B 0.71 ug/L1Chromium10.0 J 6020235EPA 3005A 0.43 7440-47-3 02/11/16 14:2002/10/16 10:05
EPA 6020B 0.67 ug/L1Cobalt10.0 J 6020235EPA 3005A 0.29 7440-48-4 02/11/16 14:2002/10/16 10:05
NDEPA 6020B ug/L1Copper10.0 6020235EPA 3005A 0.41 7440-50-8 02/11/16 14:2002/10/16 10:05
EPA 6020B 0.27 ug/L1Lead10.0 J 6020235EPA 3005A 0.08 7439-92-1 02/11/16 14:2002/10/16 10:05
EPA 6020B 0.58 ug/L1Nickel50.0 J 6020235EPA 3005A 0.48 7440-02-0 02/11/16 14:2002/10/16 10:05
NDEPA 6020B ug/L1Selenium10.0 6020235EPA 3005A 0.85 7782-49-2 02/11/16 14:2002/10/16 10:05
NDEPA 6020B ug/L1Silver10.0 6020235EPA 3005A 0.22 7440-22-4 02/11/16 14:2002/10/16 10:05
NDEPA 6020B ug/L1Thallium5.50 6020235EPA 3005A 0.06 7440-28-0 02/11/16 14:2002/10/16 10:05
EPA 6020B 2.18 ug/L1Vanadium25.0 J 6020235EPA 3005A 1.57 7440-62-2 02/11/16 14:2002/10/16 10:05
EPA 6020B 1.39 ug/L1Zinc10.0 J 6020235EPA 3005A 1.30 7440-66-6 02/11/16 14:2002/10/16 10:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 19:3901/29/16 11:30
Page 59 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW4
Surface Water
AZA0693-15 AZA069301/28/16 15:05
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 19:3901/29/16 11:30
Page 60 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW4
Surface Water
AZA0693-15 AZA069301/28/16 15:05
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 19:3901/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 19:3901/29/16 11:30
EPA 8260B 94 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 19:3901/29/16 11:3080-120
Page 61 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-SW4
Surface Water
AZA0693-15 AZA069301/28/16 15:05
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 104 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 19:3901/29/16 11:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 19:3901/29/16 11:3080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 19:3901/29/16 11:3080-120
Page 62 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Field Blank
Water
AZA0693-16 AZA069301/28/16 15:20
Project:Foothills Environmental Landfill
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6020235EPA 3005A 0.25 7440-36-0 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Arsenic10.0 6020235EPA 3005A 0.75 7440-38-2 02/11/16 14:2502/10/16 10:05
EPA 6020B 0.37 ug/L1Barium100 J 6020235EPA 3005A 0.30 7440-39-3 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Beryllium1.00 6020235EPA 3005A 0.09 7440-41-7 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Cadmium1.00 6020235EPA 3005A 0.10 7440-43-9 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Chromium10.0 6020235EPA 3005A 0.43 7440-47-3 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Cobalt10.0 6020235EPA 3005A 0.29 7440-48-4 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Copper10.0 6020235EPA 3005A 0.41 7440-50-8 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Lead10.0 6020235EPA 3005A 0.08 7439-92-1 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Nickel50.0 6020235EPA 3005A 0.48 7440-02-0 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Selenium10.0 6020235EPA 3005A 0.85 7782-49-2 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Silver10.0 6020235EPA 3005A 0.22 7440-22-4 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Thallium5.50 6020235EPA 3005A 0.06 7440-28-0 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Vanadium25.0 6020235EPA 3005A 1.57 7440-62-2 02/11/16 14:2502/10/16 10:05
NDEPA 6020B ug/L1Zinc10.0 6020235EPA 3005A 1.30 7440-66-6 02/11/16 14:2502/10/16 10:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 20:0501/29/16 11:30
Page 63 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Field Blank
Water
AZA0693-16 AZA069301/28/16 15:20
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 20:0501/29/16 11:30
Page 64 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Field Blank
Water
AZA0693-16 AZA069301/28/16 15:20
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 20:0501/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 20:0501/29/16 11:30
EPA 8260B 93 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 20:0501/29/16 11:3080-120
Page 65 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Field Blank
Water
AZA0693-16 AZA069301/28/16 15:20
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 20:0501/29/16 11:3078-120
EPA 8260B 103 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 20:0501/29/16 11:3080-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 20:0501/29/16 11:3080-120
Page 66 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Trip Blank
Water
AZA0693-17 AZA069301/26/16 00:00
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6010632EPA 5030B 4.9 67-64-1 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Acrylonitrile200 6010632EPA 5030B 1.8 107-13-1 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Benzene1.0 6010632EPA 5030B 0.2 71-43-2 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6010632EPA 5030B 0.7 74-97-5 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010632EPA 5030B 0.6 75-27-4 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Bromoform3.0 6010632EPA 5030B 0.5 75-25-2 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Bromomethane10 6010632EPA 5030B 0.8 74-83-9 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6010632EPA 5030B 0.9 75-15-0 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010632EPA 5030B 0.6 56-23-5 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6010632EPA 5030B 0.4 108-90-7 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Chloroethane10 6010632EPA 5030B 0.6 75-00-3 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Chloroform5.0 6010632EPA 5030B 0.3 67-66-3 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Chloromethane1.0 6010632EPA 5030B 0.4 74-87-3 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010632EPA 5030B 0.4 124-48-1 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010632EPA 5030B 2.0 96-12-8 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010632EPA 5030B 0.7 106-93-4 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Dibromomethane10 6010632EPA 5030B 0.7 74-95-3 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010632EPA 5030B 0.5 95-50-1 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6010632EPA 5030B 0.2 106-46-7 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010632EPA 5030B 1.5 110-57-6 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010632EPA 5030B 0.4 75-34-3 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010632EPA 5030B 0.3 107-06-2 01/29/16 20:3101/29/16 11:30
Page 67 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Trip Blank
Water
AZA0693-17 AZA069301/26/16 00:00
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010632EPA 5030B 0.5 75-35-4 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-59-2 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010632EPA 5030B 0.5 156-60-5 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010632EPA 5030B 0.5 78-87-5 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-01-5 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010632EPA 5030B 0.4 10061-02-6 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6010632EPA 5030B 0.3 100-41-4 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Iodomethane10 6010632EPA 5030B 0.6 74-88-4 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Methyl Butyl Ketone (2-Hexanone)50 6010632EPA 5030B 0.9 591-78-6 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010632EPA 5030B 0.5 75-09-2 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6010632EPA 5030B 1.1 78-93-3 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6010632EPA 5030B 1.7 108-10-1 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Styrene1.0 6010632EPA 5030B 0.4 100-42-5 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010632EPA 5030B 0.5 630-20-6 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010632EPA 5030B 0.5 79-34-5 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010632EPA 5030B 0.4 127-18-4 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Toluene1.0 6010632EPA 5030B 0.3 108-88-3 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010632EPA 5030B 0.4 71-55-6 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010632EPA 5030B 0.8 79-00-5 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Trichloroethene1.0 6010632EPA 5030B 0.4 79-01-6 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010632EPA 5030B 0.5 75-69-4 01/29/16 20:3101/29/16 11:30
Page 68 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Trip Blank
Water
AZA0693-17 AZA069301/26/16 00:00
Project:Foothills Environmental Landfill
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010632EPA 5030B 0.7 96-18-4 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6010632EPA 5030B 0.6 108-05-4 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6010632EPA 5030B 0.7 75-01-4 01/29/16 20:3101/29/16 11:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6010632EPA 5030B 0.4 1330-20-7 01/29/16 20:3101/29/16 11:30
EPA 8260B 92 %Surr: Dibromofluoromethane 6010632EPA 5030B 1868-53-7 01/29/16 20:3101/29/16 11:3080-120
EPA 8260B 102 %Surr: 1,2-Dichloroethane-d4 6010632EPA 5030B 17060-07-0 01/29/16 20:3101/29/16 11:3078-120
EPA 8260B 105 %Surr: Toluene-d8 6010632EPA 5030B 2037-26-5 01/29/16 20:3101/29/16 11:3080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6010632EPA 5030B 460-00-4 01/29/16 20:3101/29/16 11:3080-120
Page 69 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020096 - EPA 3005A
Blank (6020096-BLK1)Prepared & Analyzed: 02/05/16
Antimony ug/LND6.00
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Lead ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/LND10.0
LCS (6020096-BS1)Prepared & Analyzed: 02/05/16
Antimony ug/L1046.00 100.00 80-120104
Arsenic ug/L98.2 10.0 100.00 80-12098
Barium ug/L96.8 100 100.00 J80-12097
Beryllium ug/L1071.00 100.00 80-120107
Cadmium ug/L1011.00 100.00 80-120101
Chromium ug/L99.0 10.0 100.00 80-12099
Cobalt ug/L96.4 10.0 100.00 80-12096
Copper ug/L98.4 10.0 100.00 80-12098
Lead ug/L96.6 10.0 100.00 80-12097
Nickel ug/L97.5 50.0 100.00 80-12097
Page 70 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020096 - EPA 3005A
LCS (6020096-BS1)Prepared & Analyzed: 02/05/16
Selenium ug/L96.0 10.0 100.00 80-12096
Silver ug/L99.6 10.0 100.00 80-120100
Thallium ug/L96.4 5.50 100.00 80-12096
Vanadium ug/L99.0 25.0 100.00 80-12099
Zinc ug/L10210.0 100.00 80-120102
Matrix Spike (6020096-MS1)Prepared & Analyzed: 02/05/16 Source: AZA0647-02
Antimony ug/L1036.00 100.00 1.17 75-125102
Arsenic ug/L98.3 10.0 100.00 0.75 75-12598
Barium ug/L144100 100.00 46.9 75-12597
Beryllium ug/L1031.00 100.00 1.94 75-125101
Cadmium ug/L98.1 1.00 100.00 0.10 75-12598
Chromium ug/L10510.0 100.00 1.90 75-125103
Cobalt ug/L13310.0 100.00 34.0 75-12599
Copper ug/L10110.0 100.00 1.24 75-125100
Lead ug/L96.7 10.0 100.00 0.78 75-12596
Nickel ug/L11250.0 100.00 9.75 75-125103
Selenium ug/L10110.0 100.00 3.63 75-12597
Silver ug/L98.7 10.0 100.00 1.27 75-12597
Thallium ug/L95.0 5.50 100.00 0.17 75-12595
Vanadium ug/L10325.0 100.00 ND 75-125103
Zinc ug/L10710.0 100.00 6.70 75-125100
Matrix Spike Dup (6020096-MSD1)Prepared & Analyzed: 02/05/16 Source: AZA0647-02
Antimony ug/L1036.00 100.00 1.17 2075-125102 0.4
Arsenic ug/L10110.0 100.00 0.75 2075-125100 2
Barium ug/L142100 100.00 46.9 2075-12595 1
Page 71 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020096 - EPA 3005A
Matrix Spike Dup (6020096-MSD1)Prepared & Analyzed: 02/05/16 Source: AZA0647-02
Beryllium ug/L1121.00 100.00 1.94 2075-125110 8
Cadmium ug/L1031.00 100.00 0.10 2075-125103 5
Chromium ug/L10810.0 100.00 1.90 2075-125106 3
Cobalt ug/L13610.0 100.00 34.0 2075-125102 2
Copper ug/L10410.0 100.00 1.24 2075-125103 3
Lead ug/L96.9 10.0 100.00 0.78 2075-12596 0.2
Nickel ug/L11550.0 100.00 9.75 2075-125105 2
Selenium ug/L10210.0 100.00 3.63 2075-12598 1
Silver ug/L99.0 10.0 100.00 1.27 2075-12598 0.2
Thallium ug/L95.6 5.50 100.00 0.17 2075-12595 0.7
Vanadium ug/L10725.0 100.00 ND 2075-125107 3
Zinc ug/L11010.0 100.00 6.70 2075-125104 3
Post Spike (6020096-PS1)Prepared & Analyzed: 02/05/16 Source: AZA0647-02
Antimony ug/L99.2 100.00 1.17 80-12098
Arsenic ug/L102 100.00 0.75 80-120101
Barium ug/L148 100.00 46.9 80-120101
Beryllium ug/L105 100.00 1.94 80-120103
Cadmium ug/L102 100.00 0.10 80-120102
Chromium ug/L104 100.00 1.90 80-120102
Cobalt ug/L136 100.00 34.0 80-120102
Copper ug/L105 100.00 1.24 80-120104
Lead ug/L99.5 100.00 0.78 80-12099
Nickel ug/L114 100.00 9.75 80-120104
Selenium ug/L107 100.00 3.63 80-120103
Silver ug/L99.3 100.00 1.27 80-12098
Thallium ug/L99.2 100.00 0.17 80-12099
Page 72 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020096 - EPA 3005A
Post Spike (6020096-PS1)Prepared & Analyzed: 02/05/16 Source: AZA0647-02
Vanadium ug/L106 100.00 0.83 80-120105
Zinc ug/L110 100.00 6.70 80-120104
Batch 6020235 - EPA 3005A
Blank (6020235-BLK1)Prepared: 02/10/16 Analyzed: 02/11/16
Antimony ug/LND6.00
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Lead ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/LND10.0
LCS (6020235-BS1)Prepared: 02/10/16 Analyzed: 02/11/16
Antimony ug/L1016.00 100.00 80-120101
Arsenic ug/L10110.0 100.00 80-120101
Barium ug/L98.3 100 100.00 J80-12098
Beryllium ug/L96.8 1.00 100.00 80-12097
Page 73 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020235 - EPA 3005A
LCS (6020235-BS1)Prepared: 02/10/16 Analyzed: 02/11/16
Cadmium ug/L1051.00 100.00 80-120105
Chromium ug/L10610.0 100.00 80-120106
Cobalt ug/L10210.0 100.00 80-120102
Copper ug/L10010.0 100.00 80-120100
Lead ug/L10110.0 100.00 80-120101
Nickel ug/L10250.0 100.00 80-120102
Selenium ug/L10310.0 100.00 80-120103
Silver ug/L98.7 10.0 100.00 80-12099
Thallium ug/L98.7 5.50 100.00 80-12099
Vanadium ug/L10525.0 100.00 80-120105
Zinc ug/L10610.0 100.00 80-120106
Matrix Spike (6020235-MS1)Prepared: 02/10/16 Analyzed: 02/11/16 Source: AZA0693-03
Antimony ug/L1026.00 100.00 0.90 75-125101
Arsenic ug/L98.8 10.0 100.00 ND 75-12599
Barium ug/L115100 100.00 16.5 75-12599
Beryllium ug/L97.1 1.00 100.00 ND 75-12597
Cadmium ug/L1041.00 100.00 ND 75-125104
Chromium ug/L10110.0 100.00 0.75 75-125101
Cobalt ug/L96.7 10.0 100.00 0.37 75-12596
Copper ug/L10010.0 100.00 ND 75-125100
Lead ug/L97.4 10.0 100.00 0.10 75-12597
Nickel ug/L10350.0 100.00 1.18 75-125102
Selenium ug/L97.7 10.0 100.00 ND 75-12598
Silver ug/L97.7 10.0 100.00 ND 75-12598
Thallium ug/L96.6 5.50 100.00 0.13 75-12596
Vanadium ug/L10425.0 100.00 ND 75-125104
Page 74 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020235 - EPA 3005A
Matrix Spike (6020235-MS1)Prepared: 02/10/16 Analyzed: 02/11/16 Source: AZA0693-03
Zinc ug/L10810.0 100.00 2.34 75-125105
Matrix Spike Dup (6020235-MSD1)Prepared: 02/10/16 Analyzed: 02/11/16 Source: AZA0693-03
Antimony ug/L1036.00 100.00 0.90 2075-125103 1
Arsenic ug/L10410.0 100.00 ND 2075-125104 5
Barium ug/L115100 100.00 16.5 2075-12599 0.2
Beryllium ug/L97.1 1.00 100.00 ND 2075-12597 0.004
Cadmium ug/L1091.00 100.00 ND 2075-125109 5
Chromium ug/L10710.0 100.00 0.75 2075-125106 5
Cobalt ug/L10310.0 100.00 0.37 2075-125103 6
Copper ug/L10310.0 100.00 ND 2075-125103 3
Lead ug/L10110.0 100.00 0.10 2075-125101 4
Nickel ug/L10850.0 100.00 1.18 2075-125107 4
Selenium ug/L10110.0 100.00 ND 2075-125101 3
Silver ug/L98.0 10.0 100.00 ND 2075-12598 0.3
Thallium ug/L1015.50 100.00 0.13 2075-125101 4
Vanadium ug/L11025.0 100.00 ND 2075-125110 6
Zinc ug/L11610.0 100.00 2.34 2075-125114 8
Post Spike (6020235-PS1)Prepared: 02/10/16 Analyzed: 02/11/16 Source: AZA0693-03
Antimony ug/L97.5 100.00 0.90 80-12097
Arsenic ug/L100 100.00 0.08 80-120100
Barium ug/L117 100.00 16.5 80-120100
Beryllium ug/L96.4 100.00 0.02 80-12096
Cadmium ug/L103 100.00 0.009 80-120103
Chromium ug/L108 100.00 0.75 80-120107
Cobalt ug/L106 100.00 0.37 80-120106
Page 75 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020235 - EPA 3005A
Post Spike (6020235-PS1)Prepared: 02/10/16 Analyzed: 02/11/16 Source: AZA0693-03
Copper ug/L104 100.00 -0.39 80-120105
Lead ug/L99.3 100.00 0.10 80-12099
Nickel ug/L105 100.00 1.18 80-120104
Selenium ug/L101 100.00 0.33 80-120100
Silver ug/L97.9 100.00 0.04 80-12098
Thallium ug/L99.6 100.00 0.13 80-120100
Vanadium ug/L110 100.00 1.12 80-120109
Zinc ug/L115 100.00 2.34 80-120113
Page 76 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010632 - EPA 5030B
Blank (6010632-BLK1)Prepared & Analyzed: 01/29/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND3.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Page 77 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010632 - EPA 5030B
Blank (6010632-BLK1)Prepared & Analyzed: 01/29/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND100
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND3.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
ug/L 50.000 80-120Surr: Dibromofluoromethane 9648
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10251
ug/L 50.000 80-120Surr: Toluene-d8 10452
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10452
LCS (6010632-BS1)Prepared & Analyzed: 01/29/16
Page 78 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010632 - EPA 5030B
LCS (6010632-BS1)Prepared & Analyzed: 01/29/16
Benzene ug/L48 50.000 67-13495
Chlorobenzene ug/L50 50.000 69-122100
1,1-Dichloroethene ug/L41 50.000 58-14283
Toluene ug/L50 50.000 68-127101
Trichloroethene ug/L50 50.000 72-132100
ug/L 50.000 80-120Surr: Dibromofluoromethane 9548
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10150
ug/L 50.000 80-120Surr: Toluene-d8 10452
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10552
Matrix Spike (6010632-MS1)Prepared & Analyzed: 01/29/16 Source: AZA0693-03
Benzene ug/L44 50.000 ND 67-13489
Chlorobenzene ug/L47 50.000 ND 69-12294
1,1-Dichloroethene ug/L38 50.000 ND 58-14276
Toluene ug/L48 50.000 ND 68-12796
Trichloroethene ug/L47 50.000 ND 72-13294
ug/L 50.000 80-120Surr: Dibromofluoromethane 9548
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10452
ug/L 50.000 80-120Surr: Toluene-d8 10452
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10452
Matrix Spike Dup (6010632-MSD1)Prepared & Analyzed: 01/29/16 Source: AZA0693-03
Benzene ug/L46 50.000 ND 967-13493 4
Chlorobenzene ug/L48 50.000 ND 1369-12295 1
1,1-Dichloroethene ug/L39 50.000 ND 958-14277 1
Page 79 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010632 - EPA 5030B
Matrix Spike Dup (6010632-MSD1)Prepared & Analyzed: 01/29/16 Source: AZA0693-03
Toluene ug/L48 50.000 ND 968-12796 0.06
Trichloroethene ug/L48 50.000 ND 1172-13296 2
ug/L 50.000 80-120Surr: Dibromofluoromethane 9548
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10653
ug/L 50.000 80-120Surr: Toluene-d8 10352
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10452
Page 80 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Laboratory Certifications
Code Description Number Expires
02069Louisiana 06/30/2016LA
381North Carolina 12/31/2016NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2015 06/30/2016NELAC
98011001South Carolina 06/30/2016SC
T104704397-08-TXTexas 03/31/2016TX
1340Virginia 12/14/2016VA
Page 81 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
Note: Unless otherwise noted, all results are reported on an as received basis.
Page 82 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
COC Goes Here
Page 83 of 84
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
COC Goes Here
Page 84 of 84
LOG-IN CHECKLIST
Republic Services of North Carolina, LLC
Foothills Environmental LandfillProject:
Client:
Printed: 2/19/2016 3:57:33PM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Norcross, GA 30092
ANALYTICAL SERVICES, INC.ASI
Date Received:01/29/16 07:31 Logged In By:Charles Hawks
Work Order:AZA0693
OBSERVATIONS
Attn: Mr. Ray Hoffman
#Samples: 17 #Containers: 75
2.0 2.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:Yes
Comments:
Page 1 of 1
ASI ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
Republic Services of North Carolina, LLC
Project: Foothills Environmental Landfill Leachate
Conover, NC 28613
1220 Commerce Street, SW
Mr. Ray Hoffman
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Analytical Services, Inc. certifies that the
following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the samples analyzed.
Laboratory Report
Project #:[none]
Prepared For:
Attention:
February 19, 2016
Report Number:AZA0692
Approved:
This report may not be reproduced, except in full, without written approval from Analytical Services, Inc.Page 1 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
1403-Leachate AZA0692-01 01/28/16 14:28 01/29/16 07:31Water
Page 2 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Leachate
Water
AZA0692-01 AZA069201/28/16 14:28
Project:Foothills Environmental Landfill Leachate
01/29/16 07:31
General Chemistry
SM 5210 B 126000 ug/L1Biochemical Oxygen Demand 17000 6010625SM 5210 B 2.0 E-10106 02/03/16 07:4401/29/16 08:52
SM 5220 D 1060000 ug/L5Chemical Oxygen Demand 50000 6020050SM 5220 D 50000 E-10117 02/02/16 14:4502/02/16 11:45
SM 4500-P B,E 2540 ug/L1.11Phosphorus-Total 222 6020213SM 4500-P B 222 7723-14-0 02/09/16 17:2002/09/16 09:50
Inorganic Anions
NDEPA 9056A ug/L1Nitrate/Nitrite as N 50 6020015EPA 9056A 50 E-10128 01/29/16 13:1801/29/16 13:18
NDEPA 9056A ug/L1Nitrate as N 50 6020015EPA 9056A 50 14797-55-8 01/29/16 13:1801/29/16 13:18
NDEPA 9056A ug/L1Nitrite as N 50 6020015EPA 9056A 50 1594-56-5 01/29/16 13:1801/29/16 13:18
EPA 9056A 13000 ug/L1Sulfate5000 6020015EPA 9056A 5000 14808-79-8 01/29/16 13:1801/29/16 13:18
Metals, Total
EPA 6020B 14.1 ug/L1Antimony6.00 6020096EPA 3005A 0.25 7440-36-0 02/05/16 15:1702/05/16 09:00
EPA 6020B 17.9 ug/L1Arsenic10.0 6020096EPA 3005A 0.75 7440-38-2 02/05/16 15:1702/05/16 09:00
EPA 6020B 450 ug/L1Barium100 6020096EPA 3005A 0.30 7440-39-3 02/05/16 15:1702/05/16 09:00
NDEPA 6020B ug/L1Beryllium1.00 6020096EPA 3005A 0.09 7440-41-7 02/05/16 15:1702/05/16 09:00
NDEPA 6020B ug/L1Cadmium1.00 6020096EPA 3005A 0.10 7440-43-9 02/05/16 15:1702/05/16 09:00
EPA 6020B 70.1 ug/L1Chromium10.0 6020096EPA 3005A 0.43 7440-47-3 02/05/16 15:1702/05/16 09:00
EPA 6020B 32.9 ug/L1Cobalt10.0 6020096EPA 3005A 0.29 7440-48-4 02/05/16 15:1702/05/16 09:00
EPA 6020B 13.9 ug/L1Copper10.0 6020096EPA 3005A 0.41 7440-50-8 02/05/16 15:1702/05/16 09:00
EPA 6020B 1.68 ug/L1Lead10.0 J 6020096EPA 3005A 0.08 7439-92-1 02/05/16 15:1702/05/16 09:00
EPA 6020B 150 ug/L1Nickel50.0 6020096EPA 3005A 0.48 7440-02-0 02/05/16 15:1702/05/16 09:00
EPA 6020B 1.84 ug/L1Selenium10.0 J 6020096EPA 3005A 0.85 7782-49-2 02/05/16 15:1702/05/16 09:00
Page 3 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Leachate
Water
AZA0692-01 AZA069201/28/16 14:28
Project:Foothills Environmental Landfill Leachate
01/29/16 07:31
Metals, Total
NDEPA 6020B ug/L1Silver10.0 6020096EPA 3005A 0.22 7440-22-4 02/05/16 15:1702/05/16 09:00
NDEPA 6020B ug/L1Thallium5.50 6020096EPA 3005A 0.06 7440-28-0 02/05/16 15:1702/05/16 09:00
EPA 6020B 30.3 ug/L1Vanadium25.0 6020096EPA 3005A 1.57 7440-62-2 02/05/16 15:1702/05/16 09:00
EPA 6020B 132 ug/L1Zinc10.0 6020096EPA 3005A 1.30 7440-66-6 02/05/16 15:1702/05/16 09:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 140 ug/L1Acetone100 6010635EPA 5030B 4.9 67-64-1 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Acrylonitrile200 6010635EPA 5030B 1.8 107-13-1 01/29/16 19:2201/29/16 15:00
EPA 8260B 18 ug/L1Benzene1.0 6010635EPA 5030B 0.2 71-43-2 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Bromochloromethane3.0 6010635EPA 5030B 0.7 74-97-5 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6010635EPA 5030B 0.6 75-27-4 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Bromoform3.0 6010635EPA 5030B 0.5 75-25-2 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Bromomethane10 6010635EPA 5030B 0.8 74-83-9 01/29/16 19:2201/29/16 15:00
EPA 8260B 4.3 ug/L1Carbon Disulfide 100 J 6010635EPA 5030B 0.9 75-15-0 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6010635EPA 5030B 0.6 56-23-5 01/29/16 19:2201/29/16 15:00
EPA 8260B 1.0 ug/L1Chlorobenzene3.0 J 6010635EPA 5030B 0.4 108-90-7 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Chloroethane10 6010635EPA 5030B 0.6 75-00-3 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Chloroform5.0 6010635EPA 5030B 0.3 67-66-3 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Chloromethane1.0 6010635EPA 5030B 0.4 74-87-3 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 6010635EPA 5030B 0.4 124-48-1 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6010635EPA 5030B 2.0 96-12-8 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6010635EPA 5030B 0.7 106-93-4 01/29/16 19:2201/29/16 15:00
Page 4 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Leachate
Water
AZA0692-01 AZA069201/28/16 14:28
Project:Foothills Environmental Landfill Leachate
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Dibromomethane10 6010635EPA 5030B 0.7 74-95-3 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6010635EPA 5030B 0.5 95-50-1 01/29/16 19:2201/29/16 15:00
EPA 8260B 9.2 ug/L11,4-Dichlorobenzene 1.0 6010635EPA 5030B 0.2 106-46-7 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6010635EPA 5030B 1.5 110-57-6 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6010635EPA 5030B 0.4 75-34-3 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6010635EPA 5030B 0.3 107-06-2 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6010635EPA 5030B 0.5 75-35-4 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6010635EPA 5030B 0.5 156-59-2 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6010635EPA 5030B 0.5 156-60-5 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6010635EPA 5030B 0.5 78-87-5 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6010635EPA 5030B 0.4 10061-01-5 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6010635EPA 5030B 0.4 10061-02-6 01/29/16 19:2201/29/16 15:00
EPA 8260B 79 ug/L1Ethylbenzene1.0 6010635EPA 5030B 0.3 100-41-4 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Iodomethane10 6010635EPA 5030B 0.6 74-88-4 01/29/16 19:2201/29/16 15:00
EPA 8260B 4.9 ug/L1Methyl Butyl Ketone (2-Hexanone)50 J 6010635EPA 5030B 0.9 591-78-6 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6010635EPA 5030B 0.5 75-09-2 01/29/16 19:2201/29/16 15:00
EPA 8260B 160 ug/L1Methyl Ethyl Ketone (2-Butanone)100 6010635EPA 5030B 1.1 78-93-3 01/29/16 19:2201/29/16 15:00
EPA 8260B 36 ug/L14-Methyl-2-pentanone (MIBK)100 J 6010635EPA 5030B 1.7 108-10-1 01/29/16 19:2201/29/16 15:00
EPA 8260B 4.2 ug/L1Styrene1.0 6010635EPA 5030B 0.4 100-42-5 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6010635EPA 5030B 0.5 630-20-6 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 6010635EPA 5030B 0.5 79-34-5 01/29/16 19:2201/29/16 15:00
Page 5 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Leachate
Water
AZA0692-01 AZA069201/28/16 14:28
Project:Foothills Environmental Landfill Leachate
01/29/16 07:31
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Tetrachloroethene1.0 6010635EPA 5030B 0.4 127-18-4 01/29/16 19:2201/29/16 15:00
EPA 8260B 13 ug/L1Toluene1.0 6010635EPA 5030B 0.3 108-88-3 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6010635EPA 5030B 0.4 71-55-6 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6010635EPA 5030B 0.8 79-00-5 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Trichloroethene1.0 6010635EPA 5030B 0.4 79-01-6 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6010635EPA 5030B 0.5 75-69-4 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6010635EPA 5030B 0.7 96-18-4 01/29/16 19:2201/29/16 15:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6010635EPA 5030B 0.6 108-05-4 01/29/16 19:2201/29/16 15:00
EPA 8260B 1.2 ug/L1Vinyl Chloride 1.0 6010635EPA 5030B 0.7 75-01-4 01/29/16 19:2201/29/16 15:00
EPA 8260B 96 ug/L1Xylenes, total 5.0 6010635EPA 5030B 0.4 1330-20-7 01/29/16 19:2201/29/16 15:00
EPA 8260B 101 %Surr: Dibromofluoromethane 6010635EPA 5030B 1868-53-7 01/29/16 19:2201/29/16 15:0080-120
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6010635EPA 5030B 17060-07-0 01/29/16 19:2201/29/16 15:0078-120
EPA 8260B 91 %Surr: Toluene-d8 6010635EPA 5030B 2037-26-5 01/29/16 19:2201/29/16 15:0080-120
EPA 8260B 89 %Surr: 4-Bromofluorobenzene 6010635EPA 5030B 460-00-4 01/29/16 19:2201/29/16 15:0080-120
Page 6 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
General Chemistry - Quality Control
Batch 6010625 - SM 5210 B
Blank (6010625-BLK1)Prepared: 01/29/16 Analyzed: 02/03/16
Biochemical Oxygen Demand ug/L1102000 J
LCS (6010625-BS1)Prepared: 01/29/16 Analyzed: 02/03/16
Biochemical Oxygen Demand ug/L1920002000 198000 85-11597
Duplicate (6010625-DUP1)Prepared: 01/29/16 Analyzed: 02/03/16 Source: AZA0687-04
Biochemical Oxygen Demand ug/L82800042000 810000 202
Batch 6020050 - SM 5220 D
Blank (6020050-BLK1)Prepared & Analyzed: 02/02/16
Chemical Oxygen Demand ug/LND10000
LCS (6020050-BS1)Prepared & Analyzed: 02/02/16
Chemical Oxygen Demand ug/L21000010000 200000 90-110105
Matrix Spike (6020050-MS1)Prepared & Analyzed: 02/02/16 Source: AZA0684-02
Chemical Oxygen Demand ug/L87400010000 200000 706000 QM-0590-11084
Matrix Spike (6020050-MS2)Prepared & Analyzed: 02/02/16 Source: AZA0689-01
Chemical Oxygen Demand ug/L31500010000 200000 104000 90-110105
Matrix Spike Dup (6020050-MSD1)Prepared & Analyzed: 02/02/16 Source: AZA0684-02
Chemical Oxygen Demand ug/L88600010000 200000 706000 1090-11090 1
Batch 6020213 - SM 4500-P B
Blank (6020213-BLK1)Prepared & Analyzed: 02/09/16
Phosphorus-Total ug/LND20.0
Page 7 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
General Chemistry - Quality Control
Batch 6020213 - SM 4500-P B
LCS (6020213-BS1)Prepared & Analyzed: 02/09/16
Phosphorus-Total ug/L48620.0 500.00 88-11097
Matrix Spike (6020213-MS1)Prepared & Analyzed: 02/09/16 Source: AZB0159-24
Phosphorus-Total ug/L54720.0 500.00 ND 72-123109
Matrix Spike Dup (6020213-MSD1)Prepared & Analyzed: 02/09/16 Source: AZB0159-24
Phosphorus-Total ug/L56520.0 500.00 ND 1172-123113 3
Page 8 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Inorganic Anions - Quality Control
Batch 6020015 - EPA 9056A
Blank (6020015-BLK1)Prepared & Analyzed: 01/29/16
Nitrate/Nitrite as N ug/LND50
Nitrate as N ug/LND50
Nitrite as N ug/LND50
Sulfate ug/LND5000
LCS (6020015-BS1)Prepared & Analyzed: 01/29/16
Nitrate/Nitrite as N ug/L2100050 20000 90-110105
Nitrate as N ug/L1050050 10000 90-110105
Nitrite as N ug/L1050050 10000 90-110105
Sulfate ug/L104005000 10000 90-110104
Matrix Spike (6020015-MS1)Prepared & Analyzed: 01/29/16 Source: AZA0692-01
Nitrate/Nitrite as N ug/L1810050 20000 ND 90-11091
Nitrate as N ug/L884050 10000 ND QM-0590-11088
Nitrite as N ug/L928050 10000 ND 90-11093
Sulfate ug/L211005000 10000 13200 QM-0590-11079
Matrix Spike Dup (6020015-MSD1)Prepared & Analyzed: 01/29/16 Source: AZA0692-01
Nitrate/Nitrite as N ug/L1830050 20000 ND 1590-11092 1
Nitrate as N ug/L890050 10000 ND 15 QM-0590-11089 0.7
Nitrite as N ug/L941050 10000 ND 1590-11094 1
Sulfate ug/L212005000 10000 13200 15 QM-0590-11080 0.4
Page 9 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020096 - EPA 3005A
Blank (6020096-BLK1)Prepared & Analyzed: 02/05/16
Antimony ug/LND6.00
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Lead ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/LND10.0
LCS (6020096-BS1)Prepared & Analyzed: 02/05/16
Antimony ug/L1046.00 100.00 80-120104
Arsenic ug/L98.2 10.0 100.00 80-12098
Barium ug/L96.8 100 100.00 J80-12097
Beryllium ug/L1071.00 100.00 80-120107
Cadmium ug/L1011.00 100.00 80-120101
Chromium ug/L99.0 10.0 100.00 80-12099
Cobalt ug/L96.4 10.0 100.00 80-12096
Copper ug/L98.4 10.0 100.00 80-12098
Lead ug/L96.6 10.0 100.00 80-12097
Nickel ug/L97.5 50.0 100.00 80-12097
Page 10 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020096 - EPA 3005A
LCS (6020096-BS1)Prepared & Analyzed: 02/05/16
Selenium ug/L96.0 10.0 100.00 80-12096
Silver ug/L99.6 10.0 100.00 80-120100
Thallium ug/L96.4 5.50 100.00 80-12096
Vanadium ug/L99.0 25.0 100.00 80-12099
Zinc ug/L10210.0 100.00 80-120102
Matrix Spike (6020096-MS1)Prepared & Analyzed: 02/05/16 Source: AZA0647-02
Antimony ug/L1036.00 100.00 1.17 75-125102
Arsenic ug/L98.3 10.0 100.00 0.75 75-12598
Barium ug/L144100 100.00 46.9 75-12597
Beryllium ug/L1031.00 100.00 1.94 75-125101
Cadmium ug/L98.1 1.00 100.00 0.10 75-12598
Chromium ug/L10510.0 100.00 1.90 75-125103
Cobalt ug/L13310.0 100.00 34.0 75-12599
Copper ug/L10110.0 100.00 1.24 75-125100
Lead ug/L96.7 10.0 100.00 0.78 75-12596
Nickel ug/L11250.0 100.00 9.75 75-125103
Selenium ug/L10110.0 100.00 3.63 75-12597
Silver ug/L98.7 10.0 100.00 1.27 75-12597
Thallium ug/L95.0 5.50 100.00 0.17 75-12595
Vanadium ug/L10325.0 100.00 ND 75-125103
Zinc ug/L10710.0 100.00 6.70 75-125100
Matrix Spike Dup (6020096-MSD1)Prepared & Analyzed: 02/05/16 Source: AZA0647-02
Antimony ug/L1036.00 100.00 1.17 2075-125102 0.4
Arsenic ug/L10110.0 100.00 0.75 2075-125100 2
Barium ug/L142100 100.00 46.9 2075-12595 1
Page 11 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020096 - EPA 3005A
Matrix Spike Dup (6020096-MSD1)Prepared & Analyzed: 02/05/16 Source: AZA0647-02
Beryllium ug/L1121.00 100.00 1.94 2075-125110 8
Cadmium ug/L1031.00 100.00 0.10 2075-125103 5
Chromium ug/L10810.0 100.00 1.90 2075-125106 3
Cobalt ug/L13610.0 100.00 34.0 2075-125102 2
Copper ug/L10410.0 100.00 1.24 2075-125103 3
Lead ug/L96.9 10.0 100.00 0.78 2075-12596 0.2
Nickel ug/L11550.0 100.00 9.75 2075-125105 2
Selenium ug/L10210.0 100.00 3.63 2075-12598 1
Silver ug/L99.0 10.0 100.00 1.27 2075-12598 0.2
Thallium ug/L95.6 5.50 100.00 0.17 2075-12595 0.7
Vanadium ug/L10725.0 100.00 ND 2075-125107 3
Zinc ug/L11010.0 100.00 6.70 2075-125104 3
Post Spike (6020096-PS1)Prepared & Analyzed: 02/05/16 Source: AZA0647-02
Antimony ug/L99.2 100.00 1.17 80-12098
Arsenic ug/L102 100.00 0.75 80-120101
Barium ug/L148 100.00 46.9 80-120101
Beryllium ug/L105 100.00 1.94 80-120103
Cadmium ug/L102 100.00 0.10 80-120102
Chromium ug/L104 100.00 1.90 80-120102
Cobalt ug/L136 100.00 34.0 80-120102
Copper ug/L105 100.00 1.24 80-120104
Lead ug/L99.5 100.00 0.78 80-12099
Nickel ug/L114 100.00 9.75 80-120104
Selenium ug/L107 100.00 3.63 80-120103
Silver ug/L99.3 100.00 1.27 80-12098
Thallium ug/L99.2 100.00 0.17 80-12099
Page 12 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Metals, Total - Quality Control
Batch 6020096 - EPA 3005A
Post Spike (6020096-PS1)Prepared & Analyzed: 02/05/16 Source: AZA0647-02
Vanadium ug/L106 100.00 0.83 80-120105
Zinc ug/L110 100.00 6.70 80-120104
Page 13 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010635 - EPA 5030B
Blank (6010635-BLK1)Prepared & Analyzed: 01/29/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND3.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Page 14 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010635 - EPA 5030B
Blank (6010635-BLK1)Prepared & Analyzed: 01/29/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND100
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND3.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
ug/L 50.000 80-120Surr: Dibromofluoromethane 10151
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9648
ug/L 50.000 80-120Surr: Toluene-d8 9246
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10753
Blank (6010635-BLK2)Prepared & Analyzed: 02/01/16
Page 15 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010635 - EPA 5030B
Blank (6010635-BLK2)Prepared & Analyzed: 02/01/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND3.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Page 16 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010635 - EPA 5030B
Blank (6010635-BLK2)Prepared & Analyzed: 02/01/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND100
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND3.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
ug/L 50.000 80-120Surr: Dibromofluoromethane 9950
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9346
ug/L 50.000 80-120Surr: Toluene-d8 8844
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10251
LCS (6010635-BS1)Prepared & Analyzed: 01/29/16
Page 17 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010635 - EPA 5030B
LCS (6010635-BS1)Prepared & Analyzed: 01/29/16
Benzene ug/L55 50.000 67-134109
Chlorobenzene ug/L48 50.000 69-12297
1,1-Dichloroethene ug/L54 50.000 58-142108
Toluene ug/L51 50.000 68-127103
Trichloroethene ug/L49 50.000 72-13297
ug/L 50.000 80-120Surr: Dibromofluoromethane 10954
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10452
ug/L 50.000 80-120Surr: Toluene-d8 9347
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 8643
Matrix Spike (6010635-MS1)Prepared & Analyzed: 01/29/16 Source: AZA0692-01RE1
Benzene ug/L77 50.000 18 67-134117
Chlorobenzene ug/L55 50.000 1.0 69-122108
1,1-Dichloroethene ug/L52 50.000 ND 58-142103
Toluene ug/L69 50.000 13 68-127112
Trichloroethene ug/L54 50.000 ND 72-132108
ug/L 50.000 80-120Surr: Dibromofluoromethane 9748
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10050
ug/L 50.000 80-120Surr: Toluene-d8 8945
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 9246
Matrix Spike Dup (6010635-MSD1)Prepared & Analyzed: 01/29/16 Source: AZA0692-01RE1
Benzene ug/L76 50.000 18 967-134116 0.8
Chlorobenzene ug/L62 50.000 1.0 1369-122122 12
1,1-Dichloroethene ug/L52 50.000 ND 958-142103 0
Page 18 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6010635 - EPA 5030B
Matrix Spike Dup (6010635-MSD1)Prepared & Analyzed: 01/29/16 Source: AZA0692-01RE1
Toluene ug/L72 50.000 13 968-127118 4
Trichloroethene ug/L57 50.000 ND 1172-132114 6
ug/L 50.000 80-120Surr: Dibromofluoromethane 9447
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9648
ug/L 50.000 80-120Surr: Toluene-d8 9145
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 9648
Page 19 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Laboratory Certifications
Code Description Number Expires
02069Louisiana 06/30/2016LA
381North Carolina 12/31/2016NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2015 06/30/2016NELAC
98011001South Carolina 06/30/2016SC
T104704397-08-TXTexas 03/31/2016TX
1340Virginia 12/14/2016VA
Page 20 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
QM-05 The spike recovery was outside acceptance limits for the MS and/or MSD and/or PDS due to suspected matrix interference. Sample results for the QC batch were accepted based on acceptable LCS recoveries.
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
Note: Unless otherwise noted, all results are reported on an as received basis.
Page 21 of 22
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman February 19, 2016
COC Goes Here
Page 22 of 22
LOG-IN CHECKLIST
Republic Services of North Carolina, LLC
Foothills Environmental Landfill LeachateProject:
Client:
Printed: 2/19/2016 4:04:33PM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Norcross, GA 30092
ANALYTICAL SERVICES, INC.ASI
Date Received:01/29/16 07:31 Logged In By:Charles Hawks
Work Order:AZA0692
OBSERVATIONS
Attn: Mr. Ray Hoffman
#Samples: 1 #Containers: 7
2.0 2.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
NO
YES
YES
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:Yes
The sample type was not listed on the COC. The pH's for Metals and NO3+NO2 were adjusted from 7 and 5 respectively to
<2 with HNO3 and H2SO4 respectively. CFH
Comments:
Page 1 of 1
ASI ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
Republic Services of North Carolina, LLC
Project: Foothills Environmental Landfill Resample
Conover, NC 28613
1220 Commerce Street, SW
Mr. Ray Hoffman
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Analytical Services, Inc. certifies that the
following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the samples analyzed.
Laboratory Report
Project #:[none]
Prepared For:
Attention:
March 29, 2016
Report Number:AZC0538
Approved:
This report may not be reproduced, except in full, without written approval from Analytical Services, Inc.Page 1 of 10
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman March 29, 2016
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
1403-MW2R AZC0538-01 03/16/16 13:32 03/17/16 09:15Ground Water
1403-Field Blank AZC0538-02 03/16/16 13:45 03/17/16 09:15Water
1403-Trip Blank AZC0538-03 03/16/16 09:00 03/17/16 09:15Water
Page 2 of 10
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman March 29, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-MW2R
Ground Water
AZC0538-01 AZC053803/16/16 13:32
Project:Foothills Environmental Landfill Resample
03/17/16 09:15
Volatile Organic Compounds by EPA 8260
EPA 8260B 1.0 ug/L1Benzene1.0 J 6030376EPA 5030B 0.2 71-43-2 03/17/16 17:3803/17/16 13:30
EPA 8260B 0.9 ug/L1Vinyl Chloride 1.0 J 6030376EPA 5030B 0.7 75-01-4 03/17/16 17:3803/17/16 13:30
EPA 8260B 86 %Surr: Dibromofluoromethane 6030376EPA 5030B 1868-53-7 03/17/16 17:3803/17/16 13:3080-120
EPA 8260B 85 %Surr: 1,2-Dichloroethane-d4 6030376EPA 5030B 17060-07-0 03/17/16 17:3803/17/16 13:3078-120
EPA 8260B 99 %Surr: Toluene-d8 6030376EPA 5030B 2037-26-5 03/17/16 17:3803/17/16 13:3080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6030376EPA 5030B 460-00-4 03/17/16 17:3803/17/16 13:3080-120
Page 3 of 10
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman March 29, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Field Blank
Water
AZC0538-02 AZC053803/16/16 13:45
Project:Foothills Environmental Landfill Resample
03/17/16 09:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Benzene1.0 6030376EPA 5030B 0.2 71-43-2 03/17/16 17:0803/17/16 13:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6030376EPA 5030B 0.7 75-01-4 03/17/16 17:0803/17/16 13:30
EPA 8260B 86 %Surr: Dibromofluoromethane 6030376EPA 5030B 1868-53-7 03/17/16 17:0803/17/16 13:3080-120
EPA 8260B 83 %Surr: 1,2-Dichloroethane-d4 6030376EPA 5030B 17060-07-0 03/17/16 17:0803/17/16 13:3078-120
EPA 8260B 98 %Surr: Toluene-d8 6030376EPA 5030B 2037-26-5 03/17/16 17:0803/17/16 13:3080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 6030376EPA 5030B 460-00-4 03/17/16 17:0803/17/16 13:3080-120
Page 4 of 10
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman March 29, 2016
ResultAnalyte SWSL/ RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1403-Trip Blank
Water
AZC0538-03 AZC053803/16/16 09:00
Project:Foothills Environmental Landfill Resample
03/17/16 09:15
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Benzene1.0 6030376EPA 5030B 0.2 71-43-2 03/17/16 16:3803/17/16 13:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6030376EPA 5030B 0.7 75-01-4 03/17/16 16:3803/17/16 13:30
EPA 8260B 87 %Surr: Dibromofluoromethane 6030376EPA 5030B 1868-53-7 03/17/16 16:3803/17/16 13:3080-120
EPA 8260B 82 %Surr: 1,2-Dichloroethane-d4 6030376EPA 5030B 17060-07-0 03/17/16 16:3803/17/16 13:3078-120
EPA 8260B 98 %Surr: Toluene-d8 6030376EPA 5030B 2037-26-5 03/17/16 16:3803/17/16 13:3080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 6030376EPA 5030B 460-00-4 03/17/16 16:3803/17/16 13:3080-120
Page 5 of 10
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman March 29, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6030376 - EPA 5030B
Blank (6030376-BLK1)Prepared & Analyzed: 03/17/16
Benzene ug/LND1.0
Vinyl Chloride ug/LND1.0
ug/L 50.000 80-120Surr: Dibromofluoromethane 9146
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9045
ug/L 50.000 80-120Surr: Toluene-d8 9648
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10351
LCS (6030376-BS1)Prepared & Analyzed: 03/17/16
Benzene ug/L43 50.000 67-13486
Chlorobenzene ug/L56 50.000 69-122112
1,1-Dichloroethene ug/L35 50.000 58-14270
Toluene ug/L46 50.000 68-12792
Trichloroethene ug/L46 50.000 72-13292
ug/L 50.000 80-120Surr: Dibromofluoromethane 8844
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9347
ug/L 50.000 80-120Surr: Toluene-d8 9648
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10151
Matrix Spike (6030376-MS1)Prepared & Analyzed: 03/17/16 Source: AZC0538-01
Benzene ug/L46 50.000 1.0 67-13491
Chlorobenzene ug/L59 50.000 0.8 69-122116
1,1-Dichloroethene ug/L35 50.000 ND 58-14271
Toluene ug/L49 50.000 0.3 68-12798
Trichloroethene ug/L50 50.000 0.6 72-13299
Page 6 of 10
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman March 29, 2016
Result LimitReporting
Units LevelSpike ResultSource %REC %RECLimits RPD RPDLimit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6030376 - EPA 5030B
Matrix Spike (6030376-MS1)Prepared & Analyzed: 03/17/16 Source: AZC0538-01
ug/L 50.000 80-120Surr: Dibromofluoromethane 8743
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9045
ug/L 50.000 80-120Surr: Toluene-d8 9849
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10552
Matrix Spike Dup (6030376-MSD1)Prepared & Analyzed: 03/17/16 Source: AZC0538-01
Benzene ug/L50 50.000 1.0 967-13498 8
Chlorobenzene ug/L65 50.000 0.8 13 QM-0969-122129 11
1,1-Dichloroethene ug/L37 50.000 ND 958-14275 5
Toluene ug/L55 50.000 0.3 9 QR-0268-127109 10
Trichloroethene ug/L54 50.000 0.6 1172-132108 8
ug/L 50.000 80-120Surr: Dibromofluoromethane 8643
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9045
ug/L 50.000 80-120Surr: Toluene-d8 9749
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10251
Page 7 of 10
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman March 29, 2016
Laboratory Certifications
Code Description Number Expires
02069Louisiana 06/30/2016LA
381North Carolina 12/31/2016NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2015 06/30/2016NELAC
98011001South Carolina 06/30/2016SC
T104704397-08-TXTexas 03/31/2016TX
1340Virginia 12/14/2016VA
Page 8 of 10
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman March 29, 2016
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries.
QM-09 MS and/or MSD and/or RPD and/or PDS recoveries were outside acceptance limits biased high. Target analyte was not detected at levels at or above reporting limit and data was not affected.
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
Note: Unless otherwise noted, all results are reported on an as received basis.
Page 9 of 10
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
Republic Services of North Carolina, LLC
1220 Commerce Street, SW
Conover NC, 28613
Attention: Mr. Ray Hoffman March 29, 2016
COC Goes Here
Page 10 of 10
LOG-IN CHECKLIST
Republic Services of North Carolina, LLC
Foothills Environmental Landfill ResampleProject:
Client:
Printed: 3/29/2016 2:01:15PM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Norcross, GA 30092
ANALYTICAL SERVICES, INC.ASI
Date Received:03/17/16 09:15 Logged In By:Charles Hawks
Work Order:AZC0538
OBSERVATIONS
Attn: Mr. Ray Hoffman
#Samples: 3 #Containers: 9
5.0 5.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
NO
YES
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:Yes
The COC listed the collection date as 05/16/16. The container labels listed the collection date as 03/16/16. The container
labels were used for login purposes secondary to the samples arriving on 03/17/16. CFH
Comments:
Page 1 of 1

Appendix C

Statistical Analyses Worksheets

JOYCE Project:Foothills Regional Landfill
Project No: 890.1501.12
Task No:02
Date: January 2016
Analyte:Cobalt
Concentration PQL/RL
Sample No. Sample Date Location (µg/L) (µg/L)
1 10-Aug-98 MW-1 ND 10
2 27-Jan-99 MW-1 ND 10
3 19-Jul-99 MW-1 ND 10
4 9-Sep-99 MW-1 ND 10
5 25-Jan-00 MW-1 ND 10
6 21-Jul-00 MW-1 ND 10
7 9-Jan-01 MW-1 ND 10
8 17-Jul-01 MW-1 ND 10
9 22-Jan-02 MW-1 ND 10
10 15-Jul-02 MW-1 ND 10
11 30-Jan-03 MW-1 ND 5
12 30-Jul-03 MW-1 ND 5
13 15-Jan-04 MW-1 ND 10
14 16-Jul-04 MW-1 ND 10
15 28-Jan-05 MW-1 ND 10
16 21-Jul-05 MW-1 ND 10
17 18-Jan-06 MW-1 ND 10
18 26-Jul-06 MW-1 ND 10
19 23-Jan-07 MW-1 ND 10
20 25-Jul-07 MW-1 ND 10
21 7-Jan-08 MW-1 ND 10
22 23-Jul-08 MW-1 ND 10
23 6-Jan-09 MW-1 ND 10
24 8-Jul-09 MW-1 ND 10
25 19-Jan-10 MW-1 ND 10
26 27-Jul-10 MW-1 ND 10
27 24-Jan-11 MW-1 ND 10
28 25-Jul-11 MW-1 ND 10
29 5-Jan-12 MW-1 ND 10
30 3-Jul-12 MW-1 ND 10
31 30-Jan-13 MW-1 ND 10
32 15-Jul-13 MW-1 ND 10
33 30-Jan-14 MW-1 ND 10
34 22-Jul-14 MW-1 ND 10
35 26-Jan-15 MW-1 ND 10
36 26-Jul-15 MW-1 ND 10
37 28-Jan-16 MW-1R .55 J 10
Number of Data: 37
Number of Truncated Data: 36
Percentage of Truncated Data: 97%
Upper Poisson Prediction Limit: 45.2 µg/L
All concentrations in micrograms per liter (µg/L).
ND = Not detected above the method detection limit (truncated).
J = Estimated concentration below the Reporting Limit (SWSL).
Joyce Project:Foothills Regional Landfill
Project No: 890.1501.12
Task No: 02
Date: January 2016
Upper Poisson Prediction Limit
Analyte:Cobalt
Background Data Discrete
Concentration PQL/RL Half Poisson
Sample No. Sample Date Location (µg/l) (µg/l) RL Count
1 10-Aug-98 MW-1 ND 10 5 5
2 27-Jan-99 MW-1 ND 10 5 5
3 19-Jul-99 MW-1 ND 10 5 5
4 9-Sep-99 MW-1 ND 10 5 5
5 25-Jan-00 MW-1 ND 10 5 5
6 21-Jul-00 MW-1 ND 10 5 5
7 9-Jan-01 MW-1 ND 10 5 5
8 17-Jul-01 MW-1 ND 10 5 5
9 22-Jan-02 MW-1 ND 10 5 5
10 15-Jul-02 MW-1 ND 10 5 5
11 30-Jan-03 MW-1 ND 5 2.5 2.5
12 30-Jul-03 MW-1 ND 5 2.5 2.5
13 15-Jan-04 MW-1 ND 10 5 5
14 16-Jul-04 MW-1 ND 10 5 5
15 28-Jan-05 MW-1 ND 10 5 5
16 21-Jul-05 MW-1 ND 10 5 5
17 18-Jan-06 MW-1 ND 10 5 5
18 26-Jul-06 MW-1 ND 10 5 5
19 23-Jan-07 MW-1 ND 10 5 5
20 25-Jul-07 MW-1 ND 10 5 5
21 7-Jan-08 MW-1 ND 10 5 5
22 23-Jul-08 MW-1 ND 10 5 5
23 6-Jan-09 MW-1 ND 10 5 5
24 8-Jul-09 MW-1 ND 10 5 5
25 19-Jan-10 MW-1 ND 10 5 5
30 3-Jul-12 MW-1 ND 10 5 5
26 27-Jul-10 MW-1 ND 10 5 5
27 24-Jan-11 MW-1 ND 10 5 5
28 25-Jul-11 MW-1 ND 10 5 5
29 5-Jan-12 MW-1 ND 10 5 5
30 3-Jul-12 MW-1 ND 10 5 5
31 30-Jan-13 MW-1 ND 10 5 5
32 15-Jul-13 MW-1 ND 10 5 5
33 30-Jan-14 MW-1 ND 10 5 5
34 22-Jul-14 MW-1 ND 10 5 5
35 26-Jan-15 MW-1 ND 10 5 5
36 26-Jul-15 MW-1 ND 10 5 5
37 28-Jan-16 MW-1R .55 J 10 0.55 0.55
Note: All sample concentrations are micrograms per liter (µg/L)
Using the background data, the upper Poisson Prediction Limit, y*, is determined by:
y* =
c y + [(t^2) c / 2] + t c [y (1 + (1/c)) + ((t^2) / 4)]^0.5
where:
c = k / n
y = Poisson count
t = t(n-1, 0.95), Student's t-distribution
n-1 = degrees of freedom (number of samples - 1)
k = number of downgradient samples per event (7)
.95 = confidence interval
n = number of background samples
For:
c = 0.189
k = 7 = 7 d.g. MW's
y = 180.55
t = 1.689
n = 37
y* = 45.2 µg/L

Appendix D

Historical Constituents/Analytes
in Groundwater

AP
P
E
N
D
I
X

D
:

H
i
s
t
o
r
i
c
a
l

G
r
o
u
n
d
w
a
t
e
r

C
o
n
s
t
i
t
u
e
n
t
s
/
A
n
a
l
y
t
e
s
An
a
l
y
t
e
Sa
m
p
l
e

Co
l
l
e
c
t
i
o
n

Da
t
e
SW
S
L
MW
-
1

M
W
-
1
R

M
W
-
2

M
W
-
2
R

M
W
-
3

M
W
-
3
R

M
W
-
3
R
2

M
W
-
4

M
W
-
5

M
W
-
6

M
W
-
7

M
W
-
8

M
W
-
1
0

U
D
-
1

U
D
-
2
In
o
r
g
a
n
i
c

C
o
m
p
u
n
d
s
An
t
i
m
o
n
y
01
/
0
5
/
1
2

6
.
0
0

0
.
3
6

J

-
-
-
--
-
0.
1
8

J

-
-
-
--
-
0.
1
3

J

N
D
ND
ND
ND
------ND ---
GW
P
S

=

1
.
4

µ
g
/
L
07
/
0
3
/
1
2

6
.
0
0

0
.
5
0

J

-
-
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
ND
------ND ---
01
/
3
0
/
1
3

6
.
0
0

0
.
5
5

J

-
-
-
--
-
0.
3
4

J

-
-
-
--
-
0.
2
0

J

N
D
ND
ND
ND
------28.3 ---
02
/
1
8
/
1
3

6
.
0
0

-
-
-
--
-
--
-
---
--
-
--
-
---
--
-
--
-
---
--
-
------ND ---
04
/
1
0
/
1
3

6
.
0
0

-
-
-
--
-
--
-
---
--
-
--
-
---
--
-
--
-
---
--
-
ND ---------
05
/
0
9
/
1
3

6
.
0
0

-
-
-
--
-
--
-
---
--
-
--
-
---
--
-
--
-
---
--
-
ND ---------
06
/
1
2
/
1
3

6
.
0
0

-
-
-
--
-
--
-
---
--
-
--
-
---
--
-
--
-
---
--
-
1.6
4

J

-
-
-
------
07
/
1
5
/
1
3

6
.
0
0

N
D
--
-
--
-
ND
--
-
--
-
0.
6
6

B

0
.
2
9

B

N
D
ND
ND
0.6
2

B

-
-
-
10.6

B

-
-
-
01
/
3
0
/
1
4

6
.
0
0

0
.
4
3

B

-
-
-
--
-
ND
--
-
--
-
0.
3
1

B

N
D
ND
ND
ND
ND ---------
07
/
2
2
/
1
4

6
.
0
0

N
D
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
ND
ND ---ND ND
01
/
2
6
/
1
5

6
.
0
0

N
D
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
ND
ND ---ND ND
07
/
2
8
/
1
5

6
.
0
0

N
D
--
-
--
-
ND
--
-
--
-
1.
9
0

J

N
D
ND
ND
ND
0.5
0

J

-
-
-
ND ND
01
/
2
8
/
1
6

6
.
0
0

-
-
-
ND
--
-
ND
--
-
--
-
0.
9
0

J

N
D
ND
ND
ND
ND ND 4.37

J

1
.
9
8

J
Ar
s
e
n
i
c
08
/
1
0
/
9
8
10
ND

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
NC

2
L

=

1
0

µ
g
/
L
01
/
2
7
/
9
9
10
ND

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
07
/
1
9
/
9
9
10
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
09
/
0
7
/
9
9
10
---

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
09
/
0
9
/
9
9
10
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
10
/
1
2
/
9
9
10
---

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
12
/
0
6
/
9
9
10
---

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
01
/
2
5
/
0
0
10
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
07
/
2
1
/
0
0
10
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
01
/
0
9
/
0
1
10
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
07
/
1
7
/
0
1
10
ND

-
-
-

D
r
y
---
ND
--
-
---
ND
--
-
--
-
--
-
------------
11
/
2
7
/
0
1
10
---
--
-
--
-
---
--
-
--
-
---
--
-
ND
--
-
--
-
------------
01
/
2
2
/
0
2
10
ND
--
-
Dr
y
---
ND
--
-
---
ND
ND
--
-
--
-
------------
07
/
1
5
/
0
2
10
ND
--
-
Dr
y
---
ND
--
-
---
ND
ND
--
-
--
-
------------
01
/
3
0
/
0
3
5
ND
--
-
--
-
ND
ND
ND
---
ND
ND
--
-
--
-
------------
07
/
3
0
/
0
3
5
ND
--
-
--
-
ND
ND
ND
---
ND
ND
--
-
--
-
------------
01
/
1
5
/
0
4
10
ND
--
-
--
-
ND
ND
ND
---
ND
ND
--
-
--
-
------------
07
/
1
6
/
0
4
10
ND
--
-
--
-
ND
ND
ND
---
ND
ND
--
-
--
-
------------
01
/
2
8
/
0
5
10
ND
--
-
--
-
ND
ND
ND
---
ND
ND
---
--
-
------------
07
/
2
1
/
0
5
10
ND
--
-
--
-
ND
ND
ND
---
ND
ND
---
--
-
------------
10
/
2
1
/
0
5
10
---
--
-
--
-
---
--
-
--
-
---
--
-
--
-
ND
--
-
------------
01
/
1
8
/
0
6
10
ND
--
-
--
-
ND
ND
ND
---
ND
ND
ND
--
-
------------
03
/
1
4
/
0
6
10
ND
--
-
--
-
ND
ND
ND
---
ND
ND
ND
--
-
------------
07
/
2
6
/
0
6
10
ND
--
-
--
-
ND
ND
ND
---
ND
ND
ND
--
-
------------
08
/
2
1
/
0
6
20
---
--
-
--
-
---
--
-
--
-
ND
--
-
--
-
---
--
-
------------
10
/
0
3
/
0
6
10
---
--
-
--
-
---
--
-
--
-
ND
--
-
--
-
---
--
-
------------
01
/
2
3
/
0
7
10
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
3.
8
0

B

-
-
-
------------
07
/
2
5
/
0
7
10
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
01
/
0
7
/
0
8
10
ND
--
-
--
-
ND
--
-
--
-
ND
2.1
0

J

N
D
ND
--
-
------------
07
/
2
3
/
0
8
10
ND
--
-
--
-
ND
--
-
--
-
3.
4
0

J

N
D
ND
ND
--
-
------------
08
/
1
1
/
0
8
10
---
--
-
--
-
---
--
-
--
-
---
--
-
--
-
---
--
-
------ND ---
01
/
0
6
/
0
9
10
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
07
/
0
8
/
0
9
10
ND
--
-
--
-
3.9
5

B

-
-
-
--
-
ND
ND
ND
3.
6
5

B

-
-
-
------8.48

J

-
-
-
01
/
1
9
/
1
0
10
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------ND ---
06
/
0
2
/
1
0
10
---
--
-
--
-
---
--
-
--
-
---
--
-
--
-
---
4.1
7
------------
07
/
2
7
/
1
0
10
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
3.
7
9

J

4
.
0
4
------ND ---
11
/
2
2
/
1
0
10
---
--
-
--
-
---
--
-
--
-
---
--
-
--
-
---
ND
------------
01
/
2
4
/
1
1
10
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
ND
------ND ---
07
/
2
5
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Da
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09
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10
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Fo
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1
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Joyce Engineering
AP
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D
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D
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09
/
0
7
/
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9
1
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10
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1
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-
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12
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0
6
/
9
9
1
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D

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N
D

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D

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01
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D

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D

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01
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9
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ND

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D

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-
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D

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07
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1
ND

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D
r
y
---
ND
--
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---
ND
--
-
--
-
--
-
------------
11
/
2
7
/
0
1
1
---
--
-
--
-
---
--
-
--
-
---
--
-
ND
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S
L
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-
1

M
W
-
1
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M
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-
2

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W
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2
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M
W
-
3

M
W
-
3
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M
W
-
3
R
2

M
W
-
4

M
W
-
5

M
W
-
6

M
W
-
7

M
W
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8

M
W
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1
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9
8

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-
-
-

-
-
-

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-
-

-
-
-

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-
-

-
-
-

-
-
-

-
-
-
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-
--
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-
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-

-
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NC

2
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=

1
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g
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L
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2
7
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9
9

2
0
0
ND

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
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-
-
-

-
-
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-
-
-
07
/
1
9
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9
9

2
0
0
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
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N
D

-
-
-

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-
-

-
-
-

-
-
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-
09
/
0
7
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9
9

2
0
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---

-
-
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-
-
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-
-
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-
-
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-
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-
-
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-
-
-

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-
-
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-
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-
-
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09
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0
9
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9
9

2
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ND

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-
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N
D

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-
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-
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-
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-
-
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-
10
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1
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9
9

2
0
0
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N
D

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-
-

N
D

-
-
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N
D

-
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-
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-
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-
-
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12
/
0
6
/
9
9

2
0
0
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N
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-
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N
D

-
-
-

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N
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-
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09
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9
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11
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ND
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Joyce Engineering
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12
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3
1
Joyce Engineering
AP
P
E
N
D
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D
:

H
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G
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10
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
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-
-
-
09
/
0
7
/
9
9
10
---

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
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-
-
-

-
-
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-
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-
-
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-
-
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-
-
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-
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09
/
0
9
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9
9
10
ND

-
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N
D

-
-
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N
D

-
-
-

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N
D

-
-
-

-
-
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-
-
-

-
-
-

-
-
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-
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-
-
-
10
/
1
2
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9
9
10
---

-
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N
D

-
-
-

N
D

-
-
-

-
-
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N
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-
-
-

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12
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0
6
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9
9
10
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N
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-
-
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N
D

-
-
-

-
-
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-
-
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07
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-
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N
D

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-
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-
-
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-
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10
ND

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---
ND
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11
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2
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10
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-
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ND
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2
2
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2
10
ND
--
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Dr
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ND
--
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ND
--
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1
5
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2
10
ND
--
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Dr
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ND
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--
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ND
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ND
ND
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ND
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5
ND
--
-
--
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ND
ND
ND
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ND
ND
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--
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1
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0
4
10
ND
--
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--
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ND
ND
ND
---
ND
ND
--
-
--
-
------------
07
/
1
6
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0
4
10
ND
--
-
--
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ND
ND
ND
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ND
ND
--
-
--
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01
/
2
8
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0
5
10
ND
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ND
ND
ND
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ND
ND
---
--
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------------
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2
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0
5
10
ND
--
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ND
ND
ND
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ND
ND
---
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-
------------
10
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2
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0
5
10
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ND
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01
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1
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0
6
10
ND
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ND
ND
ND
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ND
ND
ND
--
-
------------
03
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1
4
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0
6
10
ND
--
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ND
ND
ND
---
ND
ND
ND
--
-
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07
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2
6
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0
6
10
ND
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ND
ND
ND
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ND
ND
ND
--
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08
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2
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ND
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10
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6
10
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J

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3
1
Joyce Engineering
AP
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08
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=

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-
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-
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-
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6
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-
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-
09
/
0
7
/
9
9
40
---

-
-
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-
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9
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9
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ND

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-
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10
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1
2
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9
40
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N
D

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-
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-
-
-

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-

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-
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12
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0
6
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9
9
40
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-
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N
D

-
-
-

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-
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-
-
-

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---
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7
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ND
ND
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6.4
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ND
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ND
ND
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ND
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ND
ND
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ND
ND
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ND
--
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5
40
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6
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ND
ND
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ND
ND
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------------
03
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1
4
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0
6
10
ND
--
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--
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ND
ND
ND
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ND
ND
--
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------------
07
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2
6
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6
40
ND
--
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--
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ND
ND
ND
---
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ND
ND
--
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------------
08
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6
10
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--
-
---
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-
ND
--
-
--
-
---
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-
------------
10
/
0
3
/
0
6
10
---
--
-
--
-
---
--
-
--
-
ND
--
-
--
-
---
--
-
------------
01
/
2
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-
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-

-
-
-

-
-
-
09
/
0
9
/
9
9
5
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
10
/
1
2
/
9
9
5
---

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
12
/
0
6
/
9
9
5
---

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
01
/
2
5
/
0
0
5
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
07
/
2
1
/
0
0
5
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
01
/
0
9
/
0
1
5
ND

-
-
-

N
D

-
-
-

N
D

-
-
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
07
/
1
7
/
0
1
5
ND

-
-
-

D
r
y
---
5.0
0
--
-

-
-
-

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
11
/
2
7
/
0
1
5
---
--
-
--
-
---
--
-
--
-
---
--
-
ND
--
-
--
-
------------
01
/
2
2
/
0
2
5
ND
--
-
Dr
y
---
14
.
0
--
-

-
-
-

N
D

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
07
/
1
5
/
0
2
5
ND
--
-
Dr
y
---
10
.
0
--
-

-
-
-

N
D

N
D

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-

-
-
-
01
/
3
0
/
0
3
1
ND
--
-
--
-
ND
6.6
3
ND
---
ND
ND
--
-
--
-
------------
07
/
3
0
/
0
3
1
ND
--
-
--
-
ND
ND
ND
---
ND
ND
--
-
--
-
------------
01
/
1
5
/
0
4
1
ND
--
-
--
-
ND
1.6
9
ND
---
ND
ND
--
-
--
-
------------
07
/
1
6
/
0
4
1
ND
--
-
--
-
ND
ND
ND
---
ND
ND
--
-
--
-
------------
01
/
2
8
/
0
5
1
ND
--
-
--
-
ND
ND
ND
---
ND
ND
--
-
--
-
------------
07
/
2
1
/
0
5
1
ND
--
-
--
-
ND
2.0
4
ND
---
ND
ND
--
-
--
-
------------
10
/
2
1
/
0
5
1
---
--
-
--
-
---
--
-
--
-
---
--
-
--
-
ND
--
-
------------
01
/
1
8
/
0
6
1
ND
--
-
--
-
ND
ND
ND
---
ND
ND
ND
--
-
------------
03
/
1
4
/
0
6
1
ND
--
-
--
-
ND
ND
1.
2
---
ND
ND
ND
--
-
------------
07
/
2
6
/
0
6
1
ND
--
-
--
-
ND
ND
2.0
2
---
ND
ND
ND
--
-
------------
08
/
2
1
/
0
6
1
---
--
-
--
-
---
--
-
--
-
ND
--
-
--
-
--
-
--
-
------------
10
/
0
3
/
0
6
1
---
--
-
--
-
---
--
-
--
-
ND
--
-
--
-
--
-
--
-
------------
01
/
2
3
/
0
7
3
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
07
/
2
5
/
0
7
1
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
01
/
0
7
/
0
8
1
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
07
/
2
3
/
0
8
1
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
08
/
1
1
/
0
8
1
---
--
-
--
-
---
--
-
--
-
--
-
--
-
--
-
--
-
--
-
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01
/
0
6
/
0
9
1
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
07
/
0
8
/
0
9
1
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
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01
/
1
9
/
1
0
1
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
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06
/
0
2
/
1
0
1
---
--
-
--
-
---
--
-
--
-
--
-
--
-
--
-
--
-
ND
------------
07
/
2
7
/
1
0
1
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
ND
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11
/
2
2
/
1
0
1
---
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-
--
-
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-
--
-
--
-
--
-
--
-
--
-
ND
------------
01
/
2
4
/
1
1
1
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
ND
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07
/
2
5
/
1
1
1
ND
--
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--
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--
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ND
ND
ND
ND
ND
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01
/
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5
/
1
2

1
.
0

N
D
--
-
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ND
--
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ND
ND
ND
ND
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07
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0
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1
2

1
.
0

N
D
--
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ND
--
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1
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J

-
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1
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05
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1
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-
-
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06
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07
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07
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1
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D
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-
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01
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0.6

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07
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Ve
r
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S
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p
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---
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Fo
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R
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1
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3
1
Joyce Engineering
AP
P
E
N
D
I
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D
:

H
i
s
t
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c
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l

G
r
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d
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C
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t
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/
A
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a
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t
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s
An
a
l
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t
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Sa
m
p
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e

Co
l
l
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c
t
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Da
t
e
SW
S
L
MW
-
1

M
W
-
1
R

M
W
-
2

M
W
-
2
R

M
W
-
3

M
W
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3
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M
W
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3
R
2

M
W
-
4

M
W
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W
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1
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D
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D
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08
/
1
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/
9
8
10
0
ND
--
-
--
-
---
--
-
--
-
---
--
-
--
-
--
-
--
-
------------
NC

2
L

=

7
0
0

µ
g
/
L
01
/
2
7
/
9
9
10
0
ND
--
-
--
-
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--
-
--
-
---
--
-
--
-
--
-
--
-
------------
07
/
1
9
/
9
9
10
0
ND
--
-
ND
---
ND
--
-
---
ND
--
-
--
-
--
-
------------
09
/
0
7
/
9
9
10
0
---
--
-
--
-
---
--
-
--
-
---
--
-
--
-
--
-
--
-
------------
09
/
0
9
/
9
9
10
0
ND
--
-
ND
---
ND
--
-
---
ND
--
-
--
-
--
-
------------
10
/
1
2
/
9
9
10
0
---
--
-
ND
---
ND
--
-
---
ND
--
-
--
-
--
-
------------
12
/
0
6
/
9
9
10
0
---
--
-
ND
---
ND
--
-
---
ND
--
-
--
-
--
-
------------
01
/
2
5
/
0
0
10
0
ND
--
-
ND
---
ND
--
-
---
ND
--
-
--
-
--
-
------------
07
/
2
1
/
0
0
10
0
ND
--
-
ND
---
ND
--
-
--
-
ND
--
-
--
-
--
-
------------
01
/
0
9
/
0
1
10
0
ND
--
-
ND
---
ND
--
-
--
-
ND
--
-
--
-
--
-
------------
07
/
1
7
/
0
1
10
0
ND
--
-
Dr
y
---
ND
--
-
--
-
ND
--
-
--
-
--
-
------------
11
/
2
7
/
0
1
10
0
---
--
-
--
-
---
--
-
--
-
--
-
--
-
ND
--
-
--
-
------------
01
/
2
2
/
0
2
10
0
ND
--
-
Dr
y
---
ND
--
-
--
-
ND
ND
--
-
--
-
------------
07
/
1
5
/
0
2
10
0
ND
--
-
Dr
y
---
ND
--
-
--
-
ND
ND
--
-
--
-
------------
01
/
3
0
/
0
3
5
ND
--
-
--
-
ND
ND
ND
--
-
ND
ND
--
-
--
-
------------
07
/
3
0
/
0
3
5
10
.
3
0
--
-
--
-
ND
ND
8.6
2
--
-
ND
ND
--
-
--
-
------------
01
/
1
5
/
0
4
70
0
ND
--
-
--
-
ND
ND
ND
--
-
ND
ND
--
-
--
-
------------
07
/
1
6
/
0
4
70
0
ND
--
-
--
-
ND
ND
ND
--
-
ND
ND
--
-
--
-
------------
01
/
2
8
/
0
5
70
0
ND
--
-
--
-
ND
ND
ND
--
-
ND
ND
--
-
--
-
------------
07
/
2
1
/
0
5
70
0
ND
--
-
--
-
ND
ND
ND
--
-
ND
ND
--
-
--
-
------------
10
/
2
1
/
0
5
70
0
---
--
-
--
-
---
--
-
--
-
--
-
--
-
--
-
ND
--
-
------------
01
/
1
8
/
0
6
70
0
ND
--
-
--
-
ND
ND
ND
--
-
ND
ND
ND
--
-
------------
03
/
1
4
/
0
6
2
ND
--
-
--
-
ND
ND
ND
--
-
ND
ND
ND
--
-
------------
07
/
2
6
/
0
6
70
0
ND
--
-
--
-
ND
ND
ND
--
-
ND
ND
ND
--
-
------------
08
/
2
1
/
0
6
5
---
--
-
--
-
--
-
--
-
--
-
ND
--
-
--
-
--
-
--
-
------------
10
/
0
3
/
0
6
5
---
--
-
--
-
--
-
--
-
--
-
ND
--
-
--
-
--
-
--
-
------------
01
/
2
3
/
0
7
10
0
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
07
/
2
5
/
0
7
10
0
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
01
/
0
7
/
0
8
10
0
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
07
/
2
3
/
0
8
10
0
ND
--
-
ND
ND
ND
ND
ND
--
-
------------
08
/
1
1
/
0
8
10
0
---
--
-
--
-
--
-
--
-
--
-
--
-
--
-
--
-
--
-
--
-
------ND ---
01
/
0
6
/
0
9
10
0
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------------
07
/
0
8
/
0
9
10
0
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------ND ---
01
/
1
9
/
1
0
10
0
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
--
-
------ND ---
06
/
0
2
/
1
0
10
0
---
--
-
--
-
---
--
-
--
-
---
--
-
--
-
--
-
ND
------------
07
/
2
7
/
1
0
10
0
ND
--
-
--
-
ND
--
-
--
-
ND
ND
ND
ND
ND
------ND ---
11
/
2
2
/
1
0
10
0
---
--
-
--
-
---
--
-
--
-
---
--
-
--
-
--
-
ND
------------
01
/
2
4
/
1
1
10
0
ND
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3
1
Joyce Engineering
AP
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D
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3
1
Joyce Engineering
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3
1
Joyce Engineering
AP
P
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N
D
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D
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H
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s
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G
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3
1
Joyce Engineering
AP
P
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N
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D
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H
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12
/
0
6
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9
9
5
---
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ND
---
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--
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ND
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01
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2
5
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0
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5
ND
--
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ND
---
ND
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ND
--
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07
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5
ND
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ND
---
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9
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5
ND
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ND
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ND
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5
ND
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11
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7
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5
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08
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10
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11
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3
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Joyce Engineering
AP
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12
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N
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7
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N
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---
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0
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N
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11
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------------
01
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4
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1
ND
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1.8
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07
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5
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2.1
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01
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5
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1
2
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2.0
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07
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1
2
1
ND
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--
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2.6
ND
ND
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ND
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01
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3
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1
3
1
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--
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2.6
ND
ND
ND
ND
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04
/
1
0
/
1
3
1
---
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--
-
---
--
-
--
-
---
--
-
--
-
--
-
--
-
ND ---------
05
/
0
9
/
1
3
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---
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3
1
Joyce Engineering
AP
P
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Joyce Engineering
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01
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------5.70 ---
11
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07
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2
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5.6
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4.8
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------5.61 ---
01
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5
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------6.29 ---
07
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6.0
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5.3
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------6.08 ---
01
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3
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1
3

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11
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1
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8
2
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07
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-
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1
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4
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23
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26
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2
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2
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1
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2
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7
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---27.80 ---
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3
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1
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2
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2
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Joyce Engineering

Appendix E

Historical Constituents/Analytes
in Surface Water

APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Inorganic Compounds
Antimony 01/30/13 6.00 ND 0.50 J ND ND ND
No NC 2B Standard 07/15/13 6.00 ND ND ND ND 0.45 J
01/30/14 6.00 ND ND 0.57 B ND 0.62 J
07/22/14 6.00 ND ND ND ND ND
01/26/15 6.00 ND ND ND ND ND
07/28/15 6.00 ND 0.55 J ND ND ND
01/28/16 6.00 ND ND ND ND ND
Arsenic 09/07/99 10.0 ND ND ND ND ---
NC 2B = 50 ug/L 01/25/00 10.0 ND ND ND ND ---
07/21/00 10.0 ND Dry ND Dry ND
01/09/01 10.0 ND ND ND ND ND
07/17/01 10.0 ND ND ND ND ND
01/22/02 10.0 ND ND ND ND ND
07/15/02 10.0 ND ND ND ND ND
01/30/03 5.0 ND ND ND ND ND
07/30/03 5.0 ND ND ND ND ND
01/15/04 10.0 ND ND ND ND ND
07/16/04 10.0 ND ND ND ND ND
01/28/05 10.0 ND ND ND ND ND
07/21/05 10.0 ND ND ND ND ND
01/18/06 10.0 ND ND ND ND ND
01/23/07 10.0 ND ND ND ND 2.70 J
07/25/07 10.0 ND ND ND ND ND
01/07/08 10.0 ND 2.50 J ND ND ND
07/23/08 10.0 3.50 J 2.90 J ND 5.10 J ND
01/07/09 10.0 ND ND ND ND 3.60 J
07/08/09 10.0 ND 3.25 B ND ND 2.92 J
01/19/10 10.0 ND ND ND ND ND
07/27/10 10.0 ND ND 3.70 J ND ND
01/24/11 10.0 ND ND ND ND ND
07/25/11 10.0 3.13 J ND ND ND ND
01/05/12 10.0 ND ND ND ND ND
07/03/12 10.0 NS 1.72 B 1.55 B ND 1.79 J
01/30/13 10.0 ND ND ND ND ND
07/15/13 10.0 ND ND ND ND ND
01/30/14 10.0 ND ND ND ND ND
07/22/14 10.0 ND ND ND ND ND
01/26/15 10.0 ND ND ND ND ND
07/28/15 10.0 ND ND ND 2.10 J ND
01/28/16 10.0 ND ND 1.33 J ND ND
Foothills Regional Landfill
Permit No. 14-03 Page 1 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Barium 09/07/99 500 ND ND ND ND ---
No NC 2B Standard 01/25/00 500 ND ND ND ND ---
07/21/00 500 ND Dry ND Dry ND
01/09/01 500 ND ND ND ND ND
07/17/01 500 ND ND ND ND ND
01/22/02 500 ND ND ND ND ND
07/15/02 500 ND ND ND ND ND
01/30/03 5 21.2 23.50 37.40 61.60 ND
07/30/03 5 26.4 90.50 14.30 76.20 46.30
01/15/04 500 ND ND ND ND ND
07/16/04 500 ND ND ND ND ND
01/28/05 500 ND ND ND ND ND
07/21/05 500 ND ND ND ND ND
01/18/06 500 ND ND ND ND ND
03/14/06 20 ------------ND
07/26/06 500 ND ND ND ND ND
01/23/07 100 18.6 J 23.0 J 23.1 J 24.1 J ND
07/25/07 100 23.5 J 20.0 J 22.0 J 26.9 J ND
01/07/08 100 20.8 J 26.7 J 23.3 J 25.2 J 0.30 J
07/23/08 100 22.0 J 26.3 J 25.6 J 27.5 J 1.30 J
01/07/09 100 51.2 J 87.6 J 101.0 139.0 ND
07/08/09 100 20.7 J 56.3 J 31.3 J 31.1 J ND
01/19/10 100 19.5 J 26.4 J 26.2 J 25.8 J 0.30 J
07/27/10 100 18.7 J 78.5 J 29.3 J 27.4 J ND
01/24/11 100 17.2 J 39.2 J 24.3 J 26.0 J ND
07/25/11 100 43.2 J 30.2 J 30.0 J 33.4 J ND
01/05/12 100 16.9 J 25.2 J 25.7 J 27.2 J 0.13 J
07/03/12 100 NS 31.2 J 26.8 J 23.8 J 0.78 J
01/30/13 100 17.1 J 51.7 J 26.6 J 26.3 J ND
07/15/13 100 49.0 J 49.3 J 37.3 J 36.9 J 0.31 J
01/30/14 100 17.9 J 32.6 J 24.5 J 46.9 J ND
07/22/14 100 20.6 J 30.1 J 22.9 J 34.5 J 0.26 J
01/26/15 100 15.3 J 35.9 J 29.8 J 27.6 J ND
07/28/15 100 18.5 J 22.5 J 21.8 J 23.4 J 0.41 J
01/28/16 100 19.6 J 23.9 J 224 25.8 J 0.37 J
Beryllium 09/07/99 2.00 ND ND ND ND ---
NC 2B = 6.5 ug/L 01/25/00 2.00 ND ND ND ND ---
07/21/00 2.00 ND Dry ND Dry ND
01/09/01 2.00 ND ND ND ND ND
07/17/01 2.00 ND ND ND ND ND
01/22/02 2.00 ND ND ND ND ND
07/15/02 2.00 ND ND ND ND ND
01/30/03 0.20 ND ND ND 0.28 ND
07/30/03 0.20 ND 0.77 ND 0.39 ND
01/15/04 2.00 ND ND ND ND ND
07/16/04 2.00 ND ND ND ND ND
01/28/05 2.00 ND ND ND ND ND
07/21/05 2.00 ND ND ND ND ND
01/18/06 2.00 ND ND ND ND ND
07/26/06 2.00 ND ND ND ND ND
01/23/07 1.00 ND ND ND ND ND
07/25/07 1.00 ND ND ND ND ND
01/07/08 1.00 ND ND ND ND ND
07/23/08 1.00 ND ND ND ND ND
01/07/09 1.00 0.1 J 0.30 J 0.4 J 0.5 J ND
07/08/09 1.00 ND 0.36 J ND ND ND
01/19/10 1.00 ND ND ND ND ND
07/27/10 1.00 ND ND ND ND ND
01/24/11 1.00 ND ND ND ND ND
07/25/11 1.00 ND ND ND ND ND
01/05/12 1.00 ND ND ND ND ND
07/03/12 1.00 NS ND ND ND ND
01/30/13 1.00 ND 0.09 J ND ND ND
07/15/13 1.00 0.30 J 0.29 J 0.16 J 0.14 J ND
01/30/14 1.00 ND ND ND ND ND
07/22/14 1.00 ND ND ND 0.05 J ND
01/26/15 1.00 ND 0.06 J 0.05 J 0.05 J ND
07/28/15 1.00 ND ND ND ND ND
01/28/16 1.00 ND ND 0.82 J ND ND
Foothills Regional Landfill
Permit No. 14-03 Page 2 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Cadmium 09/07/99 1.00 ND ND ND ND ---
NC 2B = 2 ug/L 07/17/01 1.00 ND ND ND ND ND
01/22/02 1.00 ND ND ND ND ND
07/15/02 1.00 ND ND ND ND ND
01/30/03 5.00 ND ND ND ND ND
01/15/04 5.00 ND ND ND ND ND
07/16/04 5.00 ND ND ND ND ND
01/28/05 5.00 ND ND ND ND ND
07/21/05 5.00 ND ND ND ND ND
01/18/06 5.00 ND ND ND ND ND
07/26/06 5.00 ND ND ND ND ND
01/23/07 1.00 ND ND ND ND ND
07/25/07 1.00 ND ND ND ND ND
01/07/08 1.00 ND ND ND ND ND
07/08/09 1.00 0.13 B 0.25 B 0.24 B 0.15 B 0.14 J
01/24/11 1.00 ND ND ND ND ND
07/25/11 1.00 ND ND ND ND ND
01/05/12 1.00 ND ND ND ND ND
07/03/12 1.00 NS ND ND ND ND
01/30/13 1.00 ND ND ND ND ND
07/15/13 1.00 ND ND ND ND ND
01/30/14 1.00 ND ND ND ND ND
07/22/14 1.00 ND ND ND ND ND
01/26/15 1.00 ND ND ND ND ND
07/28/15 1.00 ND ND ND ND ND
01/28/16 1.00 ND ND ND ND ND
Chromium 09/07/99 10.0 ND ND ND ND ---
NC 2B = 50 ug/L 01/25/00 10.0 ND ND ND ND ---
07/21/00 10.0 ND Dry ND Dry ND
01/09/01 10.0 30.00 ND ND ND ND
07/17/01 10.0 ND ND ND ND ND
01/22/02 10.0 ND ND ND ND ND
07/15/02 10.0 ND ND ND ND ND
01/30/03 5.0 ND ND ND ND ND
07/30/03 5.0 ND 7.32 ND 5.26 ND
01/15/04 10.0 ND ND ND ND ND
07/16/04 10.0 ND ND ND ND ND
01/28/05 10.0 ND ND ND ND ND
07/21/05 10.0 ND ND ND ND ND
01/18/06 10.0 ND ND ND ND ND
07/26/06 10.0 ND ND ND ND ND
01/23/07 10.0 ND ND ND ND ND
07/25/07 10.0 ND ND ND ND ND
01/07/08 10.0 5.40 J ND ND ND ND
07/23/08 10.0 ND ND ND ND ND
01/07/09 10.0 6.80 B 11.40 B 12.80 18.60 2.50 J
07/08/09 10.0 1.37 J 3.88 J 1.58 J 1.50 J ND
01/19/10 10.0 ND ND ND ND ND
07/27/10 10.0 1.07 J 5.54 J 1.34 J 1.41 J ND
01/24/11 10.0 ND ND ND ND ND
07/25/11 10.0 5.27 J ND 1.02 J 1.36 J ND
01/05/12 10.0 ND ND ND ND ND
07/03/12 10.0 NS ND ND ND ND
01/30/13 10.0 1.47 J 1.06 J 0.87 J 1.08 J ND
07/15/13 10.0 3.95 B 4.21 B 2.61 B 2.81 B 0.73 J
01/30/14 10.0 1.83 B 1.84 B 2.00 B 3.09 B 2.84 J
07/22/14 10.0 1.52 B 1.75 B 1.30 B 2.55 B 3.14 J
01/26/15 10.0 ND 0.78 J 1.51 J 0.89 J ND
07/28/15 10.0 ND 1.78 J 0.45 J ND ND
01/28/16 10.0 1.14 J 0.63 J 19.3 0.71 J ND
Foothills Regional Landfill
Permit No. 14-03 Page 3 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Cobalt 09/07/99 10.0 ND ND ND ND ---
No NC 2B Standard 01/25/00 10.0 ND ND ND ND ---
07/21/00 10.0 ND Dry ND Dry ND
01/09/01 10.0 20.00 ND ND ND ND
07/17/01 10.0 ND ND ND ND ND
01/22/02 10.0 ND ND ND ND ND
07/15/02 10.0 ND ND ND ND ND
01/30/03 5.0 ND ND ND ND ND
07/30/03 5.0 ND 6.08 ND ND ND
01/15/04 10.0 ND ND ND ND ND
07/16/04 10.0 ND ND ND ND ND
01/28/05 10.0 ND ND ND ND 31.60
07/21/05 10.0 ND ND ND ND ND
01/18/06 10.0 ND ND ND ND ND
07/26/06 10.0 ND ND ND ND ND
01/23/07 10.0 ND ND ND ND ND
07/25/07 10.0 ND ND ND ND ND
01/07/08 10.0 2.00 J 2.40 J ND ND ND
07/23/08 10.0 1.70 J 1.10 J ND 1.30 J ND
01/07/09 10.0 1.40 J 3.50 J 4.00 J 6.30 J ND
07/08/09 10.0 0.71 J 2.81 J 1.05 J 0.91 J ND
01/19/10 10.0 ND 0.88 J 0.63 J ND ND
07/27/10 10.0 ND 3.01 J ND ND ND
01/24/11 10.0 ND 1.84 J ND ND ND
07/25/11 10.0 1.9 J 1.13 J ND ND ND
01/05/12 10.0 0.17 J 1.06 J 0.45 J 0.38 J ND
07/03/12 10.0 NS 1.09 J 0.42 J 0.38 J ND
01/30/13 10.0 ND 2.92 J 0.39 J 0.53 J ND
07/15/13 10.0 2.89 J 2.88 J 1.37 J 1.49 J ND
01/30/14 10.0 0.38 J 1.52 J 0.58 J 3.08 J ND
07/22/14 10.0 0.36 J 1.34 J 0.48 J 1.26 J ND
01/26/15 10.0 ND 1.64 J 1.06 J 0.71 J ND
07/28/15 10.0 ND 0.60 J 0.37 J ND ND
01/28/16 10.0 0.51 J 0.92 J 13.2 0.67 J ND
Copper 01/25/00 200 ND ND ND ND ---
NC 2B = 7 ug/L 07/21/00 200 ND Dry ND Dry ND
01/09/01 200 ND ND ND ND ND
07/17/01 200 ND ND ND ND ND
01/22/02 200 ND ND ND ND ND
07/15/02 200 ND ND ND ND ND
01/30/03 5 ND ND ND ND ND
07/30/03 5 ND 5.77 14.10 ND ND
01/15/04 200 ND ND ND ND ND
07/16/04 200 ND ND ND ND ND
01/28/05 200 ND ND ND ND ND
07/21/05 200 ND ND ND ND ND
01/18/06 200 ND ND ND ND ND
07/26/06 200 ND ND ND ND ND
01/23/07 10.0 ND ND ND ND ND
07/25/07 10.0 ND ND ND ND ND
01/07/08 10.0 0.90 B ND ND ND 0.60 J
07/23/08 10.0 1.90 J ND ND ND ND
01/07/09 10.0 ND 1.80 J 3.00 J 3.80 J ND
07/08/09 10.0 1.21 J 3.42 J 1.17 J 1.38 J ND
01/19/10 10.0 ND 2.02 B ND ND 1.98 J
07/27/10 10.0 2.19 B 6.43 B 2.66 B 2.04 B 2.00 J
01/24/11 10.0 ND ND ND ND ND
07/25/11 10.0 3.70 B ND 1.64 B 1.86 B 2.02 J
01/05/12 10.0 0.41 J 0.48 J 0.65 J 0.57 J ND
07/03/12 10.0 NS 0.59 J 0.60 J ND ND
01/30/13 10.0 0.92 B 2.01 B 0.99 B 1.04 B 0.96 J
07/15/13 10.0 3.59 J 3.77 J 2.68 J 2.61 J ND
01/30/14 10.0 0.83 J 1.16 J 0.61 J 2.00 J ND
07/22/14 10.0 0.68 B 1.30 B 0.89 B 2.51 B 1.23 J
01/26/15 10.0 0.52 J 1.66 J 1.52 J 1.62 J ND
07/28/15 10.0 0.68 B 0.64 B 0.79 B 0.86 B 1.62 J
01/28/16 10.0 ND ND 16.2 ND ND
Foothills Regional Landfill
Permit No. 14-03 Page 4 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Lead 09/07/99 10.0 ND ND ND ND ---
NC 2B = 25 ug/L 01/25/00 10.0 ND ND ND ND ---
07/21/00 10.0 ND Dry ND Dry ND
01/09/01 10.0 30.00 ND ND ND ND
07/17/01 10.0 ND ND ND ND ND
01/22/02 10.0 ND ND ND ND ND
07/15/02 10.0 ND ND ND ND ND
01/30/03 5.0 ND ND ND 5.12 ND
07/30/03 5.0 ND 7.11 ND ND ND
01/15/04 10.0 ND ND ND ND ND
07/16/04 10.0 ND ND ND ND ND
01/28/05 10.0 ND ND ND ND ND
07/21/05 10.0 ND ND ND ND ND
01/18/06 10.0 ND ND ND ND ND
07/26/06 10.0 ND ND ND ND ND
01/23/07 10.0 ND ND ND ND ND
07/25/07 10.0 ND 2.80 J 2.50 J 3.30 J ND
01/07/08 10.0 ND ND ND ND ND
07/23/08 10.0 ND ND ND ND ND
01/07/09 10.0 ND ND 3.20 J 6.70 J ND
07/08/09 10.0 ND 2.6 J ND ND ND
01/19/10 10.0 ND ND ND ND ND
07/27/10 10.0 ND 4.17 J ND ND ND
01/24/11 10.0 ND ND ND ND ND
07/25/11 10.0 4.02 J ND ND ND ND
01/05/12 10.0 ND ND ND ND ND
07/03/12 10.0 NS 0.43 J 0.35 J 0.12 J ND
01/30/13 10.0 0.20 J 0.85 J 0.32 J 0.41 J ND
07/15/13 10.0 2.34 J 2.44 J 1.78 J 1.88 J ND
01/30/14 10.0 0.20 J 0.47 J 0.23 J 2.90 J ND
07/22/14 10.0 0.22 B 0.50 B 0.27 B 1.05 B 0.26 J
01/26/15 10.0 ND 0.64 J 0.57 J 0.33 J ND
07/28/15 10.0 0.09 J ND 0.19 J 0.20 J ND
01/28/16 10.0 0.37 J 0.20 J 11.1 0.27 J ND
Nickel 09/07/99 50.0 ND ND ND ND ---
NC 2B = 88 ug/L 01/25/00 50.0 ND ND ND ND ---
07/21/00 50.0 ND Dry ND Dry ND
01/09/01 50.0 ND ND ND ND ND
07/17/01 50.0 ND ND ND ND ND
01/22/02 50.0 ND ND ND ND ND
07/15/02 50.0 ND ND ND ND ND
01/30/03 5.0 ND ND ND ND ND
07/30/03 5.0 ND ND ND ND ND
01/15/04 50.0 ND ND ND ND ND
07/16/04 50.0 ND ND ND ND ND
01/28/05 50.0 ND ND ND ND ND
07/21/05 50.0 ND ND ND ND ND
01/18/06 50.0 ND ND ND ND ND
07/26/06 50.0 ND ND ND ND ND
01/23/07 50.0 ND ND ND ND ND
07/25/07 50.0 ND ND ND ND ND
01/07/08 50.0 2.50 J ND ND ND ND
07/23/08 50.0 ND ND ND ND ND
01/07/09 50.0 4.70 J 6.80 J 7.50 J 10.90 J ND
07/08/09 50.0 0.84 B 2.26 B 1.36 B 1.09 B 1.09 J
01/19/10 50.0 ND ND ND ND ND
07/27/10 50.0 ND 2.52 J ND ND ND
01/24/11 50.0 ND ND ND ND ND
07/25/11 50.0 ND ND ND ND ND
01/05/12 50.0 0.27 J 0.59 J 0.56 J 0.44 J ND
07/03/12 50.0 NS 0.68 J 0.41 J 0.23 J ND
01/30/13 50.0 0.37 J 2.06 J 0.55 J 0.62 J ND
07/15/13 50.0 2.22 J 2.39 J 1.68 J 1.68 J ND
01/30/14 50.0 0.48 J 1.06 J 0.48 J 1.51 J ND
07/22/14 50.0 0.47 B 1.12 B 0.59 B 1.63 B 0.33 J
01/26/15 50.0 0.32 J 1.13 J 0.95 J 0.79 J ND
07/28/15 50.0 1.35 B 1.85 B 1.83 B 1.89 B 1.66 J
01/28/16 50.0 0.54 J 0.54 J 13.2 J 0.58 J ND
Foothills Regional Landfill
Permit No. 14-03 Page 5 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Selenium 09/07/99 20.0 ND ND ND ND ---
NC 2B = 5 ug/L 01/25/00 20.0 ND ND ND ND ---
07/21/00 20.0 ND Dry ND Dry ND
01/09/01 20.0 ND ND ND ND ND
07/17/01 20.0 ND ND ND ND ND
01/22/02 20.0 ND ND ND ND ND
07/15/02 20.0 ND ND ND ND ND
01/30/03 5.0 ND ND 6.67 ND ND
07/30/03 5.0 ND ND ND ND ND
01/15/04 20.0 ND ND ND ND ND
07/16/04 20.0 ND ND ND ND ND
01/28/05 20.0 ND ND ND ND ND
07/21/05 20.0 ND ND ND ND ND
01/18/06 20.0 ND ND ND ND ND
07/26/06 20.0 ND ND ND ND ND
01/23/07 10.0 ND ND ND ND ND
07/25/07 10.0 ND ND ND ND ND
01/07/08 10.0 ND ND ND ND ND
07/23/08 10.0 ND ND ND ND ND
01/07/09 10.0 ND ND ND ND ND
07/08/09 10.0 ND ND ND ND ND
01/19/10 10.0 ND ND ND ND ND
07/27/10 10.0 ND ND ND ND ND
01/24/11 10.0 ND ND ND ND ND
07/25/11 10.0 ND ND ND ND ND
01/05/12 10.0 ND ND ND ND ND
07/03/12 10.0 NS ND ND ND ND
01/30/13 10.0 ND ND ND ND ND
07/15/13 10.0 ND ND ND ND ND
01/30/14 10.0 ND ND ND ND ND
07/22/14 10.0 ND ND ND ND ND
01/26/15 10.0 ND ND ND ND ND
07/28/15 10.0 ND ND ND ND ND
01/28/16 10.0 ND ND 2.24 J ND ND
Silver 09/07/99 10.0 ND ND ND ND ---
NC 2B = 0.06 ug/L 01/25/00 10.0 ND ND ND ND ---
07/21/00 10.0 ND Dry ND Dry ND
01/09/01 10.0 ND ND ND ND ND
07/17/01 10.0 ND ND ND ND ND
01/22/02 10.0 ND ND ND ND ND
07/15/02 10.0 ND ND ND ND ND
01/30/03 5.0 ND ND ND ND ND
07/30/03 5.0 ND ND ND ND ND
01/15/04 10.0 ND ND ND ND ND
07/16/04 10.0 ND ND ND ND ND
01/28/05 10.0 ND ND ND ND ND
07/21/05 10.0 ND ND ND ND ND
01/18/06 10.0 ND ND ND ND ND
01/23/07 10.0 ND ND ND ND ND
07/25/07 10.0 ND ND ND ND ND
01/07/08 10.0 ND ND ND ND ND
07/23/08 10.0 2.40 J ND ND ND ND
01/07/09 10.0 ND ND ND ND ND
07/08/09 10.0 ND ND ND ND ND
01/19/10 10.0 ND ND ND ND ND
07/27/10 10.0 ND ND ND ND ND
01/24/11 10.0 ND ND ND ND ND
07/25/11 10.0 ND ND ND ND ND
01/05/12 10.0 ND ND ND ND ND
07/03/12 10.0 NS ND ND ND ND
01/30/13 10.0 ND ND ND ND ND
07/15/13 10.0 ND ND ND ND ND
01/30/14 10.0 ND ND ND ND ND
07/22/14 10.0 ND ND ND ND ND
01/26/15 10.0 ND ND ND ND ND
07/28/15 10.0 ND ND ND ND ND
01/28/16 10.0 ND ND ND ND ND
Foothills Regional Landfill
Permit No. 14-03 Page 6 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Thallium 01/28/16 5.5 ND ND 0.42 J ND ND
No NC 2B Standard
Vanadium 09/07/99 40.0 ND ND ND ND ---
No NC 2B Standard 01/25/00 40.0 ND ND ND ND ---
07/21/00 40.0 ND Dry ND Dry ND
01/09/01 40.0 60.00 ND ND ND ND
07/17/01 40.0 ND ND ND ND ND
01/22/02 40.0 ND ND ND ND ND
07/15/02 40.0 ND ND ND ND ND
01/30/03 5.0 ND ND ND 8.53 ND
07/30/03 5.0 ND 25.20 ND 14.80 ND
01/15/04 40.0 ND ND ND ND ND
07/16/04 40.0 ND ND ND ND ND
01/28/05 40.0 ND ND ND ND ND
07/21/05 40.0 ND ND ND ND ND
07/26/06 40.0 ND ND ND ND ND
07/25/07 25.0 ND ND ND ND ND
01/07/09 25.0 10.40 J 20.60 J 28.50 38.40 ND
07/08/09 25.0 1.04 J 9.22 J 2.59 J 1.57 J ND
01/19/10 25.0 0.80 J 1.53 J 0.54 J 0.45 J ND
07/27/10 25.0 1.79 J 14.50 J 2.66 J 2.46 J ND
01/24/11 25.0 ND 1.97 J ND ND ND
07/25/11 25.0 8.96 J ND 2.34 J 3.00 J ND
01/05/12 25.0 ND ND ND ND ND
07/03/12 25.0 NS 2.04 J ND ND ND
01/30/13 25.0 ND ND ND ND ND
07/15/13 25.0 9.69 J 12.40 J 6.15 J 6.01 J ND
01/30/14 25.0 ND 3.28 B 2.16 B 5.35 B 9.89 J
07/22/14 25.0 1.22 B 2.02 B 1.22 B 5.05 B 1.02 J
01/26/15 25.0 ND 0.99 J 2.78 J ND ND
07/28/15 25.0 ND ND ND ND ND
01/28/16 25.0 2.86 J 2.49 J 42.90 2.18 J ND
Zinc 09/07/99 50.0 ND 70.0 ND ND ---
NC 2B = 50 ug/L 01/25/00 50.0 ND ND ND ND ---
07/21/00 50.0 ND Dry ND Dry 60.0
01/09/01 50.0 90.0 ND ND ND ND
07/17/01 50.0 130 90.0 ND ND ND
01/22/02 50.0 ND ND ND ND ND
07/15/02 50.0 ND ND ND ND ND
01/30/03 5.0 ND ND ND 25.7 ND
07/30/03 5.0 ND 29.3 B 38.1 B 16.7 B 7.70
01/15/04 50.0 ND ND ND ND ND
07/16/04 50.0 ND ND ND ND ND
01/28/05 50.0 ND ND ND ND ND
07/21/05 50.0 ND ND ND ND ND
01/18/06 50.0 ND ND ND ND ND
07/26/06 50.0 ND ND ND ND ND
01/23/07 10.0 ND ND ND 4.30 J ND
07/25/07 10.0 14.80 ND ND ND 1.40 J
01/07/08 10.0 3.9 J 4.2 J 2.1 J 2.0 J ND
07/23/08 10.0 ND ND ND ND ND
01/07/09 10.0 15.7 34.5 30.9 62.7 ND
07/08/09 10.0 11.5 6.97 J 87.0 79.8 ND
01/19/10 10.0 5.68 B 4.24 B 3.16 B 3.07 B 3.07 J
07/27/10 10.0 3.88 J 11.1 4.57 J ND ND
01/24/11 10.0 ND ND ND ND 4.41 J
07/25/11 10.0 10.1 B ND ND ND 13.8
01/05/12 10.0 ND ND 8.87 B 2.97 B 2.14 J
07/03/12 10.0 NS 3.07 B 2.43 B 1.20 B 0.87 J
01/30/13 10.0 3.17 B 4.88 B 2.01 B 2.28 B 1.25 J
07/15/13 10.0 5.80 J 6.73 J 6.57 J 5.90 J ND
01/30/14 10.0 1.27 J 1.24 J ND 5.91 J ND
07/22/14 10.0 1.65 B 3.14 B 1.81 B 5.77 B 1.31 J
01/26/15 10.0 1.71 B 3.22 B 4.23 B 4.14 B 1.05 J
07/28/15 10.0 1.66 J ND ND 2.30 J 1.35 J
01/28/16 10.0 1.75 J ND 91.8 1.39 J ND
Foothills Regional Landfill
Permit No. 14-03 Page 7 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Organic Compounds
Acetone 07/30/03 5 ND ND ND 5.70 ND
No NC 2B Standard 01/15/04 100 ND ND ND ND ND
07/16/04 100 ND ND ND ND ND
01/28/05 100 ND ND ND ND ND
07/21/05 100 ND ND ND ND ND
01/18/06 100 ND ND ND ND ND
07/26/06 100 ND ND ND ND ND
01/23/07 100 ND ND ND ND ND
07/25/07 100 ND ND ND ND ND
01/07/08 100 4.00 J ND 2.80 J 2.80 J ND
07/23/08 100 ND ND 4.00 J ND ND
01/07/09 100 ND 25.00 J ND ND ND
07/08/09 100 ND ND ND ND ND
01/19/10 100 ND 16.00 J ND ND ND
07/27/10 100 ND ND ND ND ND
01/24/11 100 ND ND ND ND ND
07/25/11 100 ND ND ND ND ND
01/05/12 100 ND ND ND ND ND
07/03/12 100 NS ND ND ND ND
01/30/13 100 ND 13.00 J ND ND ND
07/15/13 100 7.40 J 5.10 J ND ND ND
01/30/14 100 ND ND ND ND ND
07/22/14 100 ND ND ND ND ND
01/26/15 100 ND ND ND ND ND
07/28/15 100 ND ND ND ND ND
01/28/16 100 ND ND ND ND ND
Carbon disulfide 07/17/01 100 ND 110.00 ND ND ND
No NC 2B Standard 01/22/02 100 ND ND ND ND ND
07/15/02 100 ND ND ND ND ND
01/30/03 5 ND ND ND ND ND
07/30/03 5 ND ND 13.70 ND 11.40
01/15/04 700 ND ND ND ND ND
07/16/04 700 ND ND ND ND ND
01/28/05 700 ND ND ND ND ND
07/21/05 700 ND ND ND ND ND
01/18/06 700 ND ND ND ND ND
07/26/06 700 ND ND ND ND ND
01/23/07 100 ND ND ND ND ND
07/25/07 100 ND ND ND ND ND
01/07/08 100 ND ND ND ND ND
07/23/08 100 ND ND ND ND ND
01/07/09 100 ND ND ND ND ND
07/08/09 100 ND ND ND ND ND
01/19/10 100 ND ND ND ND ND
07/27/10 100 ND ND ND ND ND
01/24/11 100 ND ND ND ND ND
07/25/11 100 ND ND ND ND ND
01/05/12 100 ND ND ND ND ND
07/03/12 100 NS ND ND ND ND
01/30/13 100 ND ND ND ND ND
07/15/13 100 ND ND ND ND ND
01/30/14 100 ND ND ND ND ND
07/22/14 100 ND ND ND ND ND
01/26/15 100 ND ND ND ND ND
07/28/15 100 ND ND ND ND ND
01/28/16 100 ND ND ND ND ND
Chloromethane 07/15/13 1.0 0.70 J ND ND ND ND
No NC 2B Standard 01/30/14 1.0 ND ND ND ND ND
07/22/14 1.0 ND ND ND ND ND
01/26/15 1.0 ND ND ND ND ND
07/28/15 1.0 ND ND ND ND ND
01/28/16 1.0 ND ND ND ND ND
Foothills Regional Landfill
Permit No. 14-03 Page 8 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Methyl Ethyl Ketone (2-Butanone)01/07/09 100 ND 2.30 J ND ND ND
No NC 2B Standard 07/08/09 100 ND ND ND ND ND
01/19/10 100 ND 2.90 J ND ND ND
07/27/10 100 ND ND ND ND ND
01/24/11 100 ND ND ND ND ND
07/25/11 100 ND ND ND ND ND
01/05/12 100 ND ND ND ND ND
07/03/12 100 NS ND ND ND ND
01/30/13 100 ND ND ND ND ND
07/15/13 100 2.20 J 2.60 J ND ND ND
01/30/14 100 ND ND ND ND 2.3 J
07/22/14 100 ND ND ND ND ND
01/26/15 100 ND ND ND ND ND
07/28/15 100 ND ND ND ND ND
01/28/16 100 ND ND ND ND ND
Field Parameters
pH 09/07/99 --- 7.56 7.65 7.56 7.79 ---
(S.U.)01/25/00 --- 7.62 7.75 7.70 7.75 ---
07/21/00 --- 6.90 Dry 7.59 Dry ---
01/09/01 --- 7.45 7.99 8.29 7.66 ---
07/17/01 --- 7.93 7.65 7.91 7.75 ---
01/22/02 --- 7.44 7.41 7.45 7.06 ---
07/15/02 --- 6.73 7.05 7.28 6.95 ---
01/30/03 --- 7.50 7.60 7.50 7.30 ---
07/30/03 --- 7.40 7.50 7.40 7.80 ---
01/15/04 --- 6.77 7.03 7.23 7.26 ---
07/16/04 --- 6.47 6.73 6.94 7.05 ---
01/28/05 --- 6.80 6.67 6.99 6.97 ---
07/21/05 --- 8.34 6.70 7.10 7.20 ---
01/18/06 --- 7.30 7.40 6.00 8.90 ---
07/26/06 --- 6.86 7.16 7.31 7.26 ---
01/23/07 --- 6.11 7.73 7.95 8.60 ---
07/25/07 --- 5.58 9.62 6.00 5.80 ---
01/07/08 --- 6.15 5.81 6.26 6.38 ---
07/23/08 --- 6.42 6.61 5.63 6.29 ---
01/07/09 --- 6.31 6.57 6.45 6.22 ---
07/08/09 --- 6.86 6.67 6.94 6.75 ---
01/19/10 --- 5.70 9.02 7.73 7.68 ---
07/27/10 --- 7.90 7.23 6.95 6.87 ---
01/24/11 --- 6.11 6.50 6.88 6.81 ---
07/25/11 --- 6.17 6.35 7.05 7.05 ---
01/02/12 --- 6.39 6.77 6.54 6.73 ---
07/03/12 --- NS 6.98 6.65 7.26 ---
01/30/13 --- 7.38 7.87 8.35 7.12 ---
07/15/13 --- 7.97 7.84 6.52 6.58 ---
01/30/14 --- 5.13 5.49 7.37 7.66 ---
07/22/14 --- 6.28 7.17 7.59 7.82 ---
01/26/15 FIELD 5.44 5.33 7.03 7.10 ---
07/28/15 --- 6.75 5.63 8.24 7.68 ---
Foothills Regional Landfill
Permit No. 14-03 Page 9 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Conductivity 09/07/99 --- 37.0 42.0 37.0 43.0 ---
(µS/cm)01/25/00 --- 52.0 53.0 55.0 75.0 ---
07/21/00 --- 38.0 Dry 42.0 Dry ---
01/09/01 --- 30.0 33.0 33.0 39.0 ---
07/17/01 --- 61.0 149.0 75.0 62.0 ---
01/22/02 --- 33.0 28.0 30.0 31.0 ---
07/15/02 --- 32.0 31.0 33.0 32.0 ---
01/30/03 --- 40.8 43.1 100.4 91.6 ---
07/30/03 --- 560.0 53.0 62.0 53.0 ---
01/15/04 --- 45.6 44.0 44.5 46.9 ---
07/16/04 --- 57.9 54.5 53.5 58.9 ---
01/28/05 --- 98.1 101.3 99.5 114.8 ---
07/21/05 --- 75.1 71.7 75.8 69.5 ---
01/18/06 --- 43.9 36.1 43.2 52.7 ---
07/26/06 --- 95.8 82.3 77.0 77.7 ---
01/23/07 --- 38.0 51.0 48.0 5.0 ---
07/25/07 --- 89.0 72.0 67.0 69.0 ---
01/07/08 --- 98.0 108.0 113.0 105.0 ---
07/23/08 --- 74.0 98.0 137.0 94.0 ---
01/07/09 --- 37.0 29.0 40.0 41.0 ---
07/08/09 --- 60.0 68.0 72.0 73.0 ---
01/19/10 --- 45.0 65.0 63.0 64.0 ---
07/27/10 --- 70.0 104.0 81.0 80.0 ---
01/24/11 --- 56.0 79.0 72.0 72.0 ---
07/25/11 --- 50.0 236.0 81.0 85.0 ---
01/05/12 --- 33.0 50.0 46.0 45.0 ---
07/03/12 --- NS 91.4 933.0 83.5 ---
01/30/13 --- 38.4 106.9 65.7 47.1 ---
07/15/13 --- 102.8 68.3 49.5 48.8 ---
01/30/14 --- 30.0 61.4 37.5 62.8 ---
07/22/14 --- 60.6 74.1 71.7 73.5 ---
01/26/15 FIELD 36.4 53.4 17.8 43.7 ---
07/28/15 --- 67.0 56.1 74.0 91.0 ---
Temperature 09/07/99 --- 19.8 20.4 18.8 21.7 ---
(°C)01/25/00 --- 6.9 7.2 6.8 5.7 ---
07/21/00 --- 29.9 Dry 25.3 Dry ---
01/09/01 --- 3.5 3.6 3.3 3.5 ---
07/17/01 --- 23.5 24.6 24.6 24.4 ---
01/22/02 --- 10.0 7.8 7.5 8.2 ---
07/15/02 --- 21.8 22.9 22.3 23.1 ---
01/30/03 --- 4.1 4.3 5.1 3.5 ---
07/30/03 --- 20.0 20.6 21.8 20.8 ---
01/15/04 --- 6.3 7.7 8.3 7.4 ---
07/16/04 --- 17.4 17.3 19.0 19.2 ---
01/28/05 --- 2.6 4.2 3.9 2.4 ---
07/21/05 --- 22.9 22.8 24.8 24.1 ---
01/18/06 --- 6.7 7.1 6.9 6.3 ---
07/26/06 --- 24.9 24.3 24.3 25.1 ---
01/23/07 --- 4.7 5.4 6.0 5.6 ---
07/25/07 --- 17.9 18.4 19.2 19.0 ---
01/07/08 --- 8.5 8.7 9.0 9.5 ---
07/23/08 --- 20.9 22.2 17.8 18.0 ---
01/07/09 --- 8.4 8.8 8.2 8.2 ---
07/08/09 --- 18.0 19.7 18.7 18.6 ---
01/19/10 --- 6.4 7.6 5.6 5.6 ---
07/27/10 --- 21.2 26.0 23.5 23.3 ---
01/24/11 --- 4.3 5.2 2.9 2.6 ---
07/25/11 --- 21.1 20.1 21.1 20.9 ---
01/05/12 --- 4.2 2.7 5.7 5.7 ---
07/03/12 --- NS 22.5 24.7 24.2 ---
01/30/13 --- 13.1 11.0 11.7 10.9 ---
07/15/13 --- 21.5 22.1 19.8 20.0 ---
01/30/14 --- 1.9 3.1 0.04 0.01 ---
07/22/14 --- 21.1 18.4 21.90 22.80 ---
01/26/15 FIELD 9.7 8.3 7.4 7.9 ---
07/28/15 --- 24.23 22.16 23.76 26.64 ---
Foothills Regional Landfill
Permit No. 14-03 Page 10 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Turbidity 09/07/99 --- 138.0 10.0 21.0 14.0 ---
(NTU)07/21/00 --- 2.9 Dry 15.0 Dry ---
01/09/01 --- 823.0 45.0 6.3 17.0 ---
07/17/01 --- 27.0 75.0 21.0 22.0 ---
01/22/02 --- 128.0 133.0 32.0 63.0 ---
07/15/02 --- 55.0 53.0 77.0 47.0 ---
01/30/03 --- 35.1 49.1 32.5 126.0 ---
07/30/03 --- 6.0 45.0 14.0 9.0 ---
01/15/04 --- 7.0 4.0 7.3 4.7 ---
07/16/04 --- 10.2 7.1 9.8 6.9 ---
01/28/05 --- 8.7 12.2 11.9 21.3 ---
07/21/05 --- 54.7 24.0 28.3 30.3 ---
01/18/06 --- 41.4 15.4 13.9 32.0 ---
07/26/06 --- 27.5 19.3 9.1 25.4 ---
07/25/07 --- 10.7 4.8 14.3 2.9 ---
01/07/08 --- 76.8 147.0 152.0 70.0 ---
07/23/08 --- 12.1 18.1 19.6 8.7 ---
01/07/09 --- 98.5 234.0 291.0 380.0 ---
07/08/09 --- 18.7 102.0 35.1 29.0 ---
01/19/10 --- 8.9 32.1 28.9 19.9 ---
07/27/10 --- 13.0 110.0 31.2 29.8 ---
01/24/11 --- 3.6 60.7 4.0 3.5 ---
07/25/11 --- 41.3 13.1 18.9 20.0 ---
01/05/12 --- 20.0 2.8 7.8 5.8 ---
07/03/12 --- NS 14.0 21.8 29.6 ---
01/30/13 --- 19.5 12.7 10.1 11.5 ---
07/15/13 --- 38.1 27.2 39.8 37.4 ---
01/30/14 --- 6.21 5.09 6.21 4.82 ---
07/22/14 --- 15.41 12.85 26.40 30.70 ---
01/26/15 FIELD 4.39 43.4 25.0 20 ---
07/28/15 --- 12.80 16.2 23.4 25 ---
Dissolved oxygen 01/23/07 --- 11.00 11.50 11.00 11.00 ---
(mg/L)07/25/07 --- 9.80 9.80 9.80 10.10 ---
01/07/08 --- 10.30 10.95 11.64 11.19 ---
07/23/08 --- 10.76 10.77 8.70 8.59 ---
01/07/09 --- 11.73 10.60 12.05 11.88 ---
07/08/09 --- 8.25 8.08 8.63 7.54 ---
01/19/10 --- 11.47 10.58 10.84 10.96 ---
07/27/10 --- 8.12 7.72 7.56 8.29 ---
01/24/11 --- 13.61 12.96 14.78 14.78 ---
07/25/11 --- 6.88 4.20 23.04 15.13 ---
01/05/12 --- 12.39 4.47 10.71 10.11 ---
07/03/12 --- NS 6.76 6.05 6.92 ---
01/30/13 --- 8.49 10.77 8.22 9.47 ---
07/15/13 --- 6.38 5.94 6.39 6.32 ---
01/30/14 --- 13.13 17.87 12.42 14.95 ---
07/22/14 --- 6.61 8.92 7.70 7.50 ---
01/26/15 FIELD 12.44 10.66 10.34 15.47 ---
07/28/15 --- 7.81 7.65 8.47 7.80 ---
Oxidation Reduction Potential 01/23/07 --- 109.0 23.0 37.0 76.0 ---
(mV)07/25/07 --- 173.0 -60.0 177.0 206.0 ---
01/07/08 --- 129.0 67.0 131.0 107.0 ---
07/23/08 --- 40.0 65.0 150.0 19.0 ---
01/07/09 --- 122.1 101.1 145.8 100.5 ---
07/08/09 --- 61.7 35.4 59.8 40.0 ---
01/19/10 --- 184.2 -68.6 14.2 23.7 ---
07/27/10 --- -4.6 -17.9 10.6 26.2 ---
01/24/11 --- 96.3 89.6 66.4 80.7 ---
07/25/11 --- 91.9 200.8 86.2 84.3 ---
01/05/12 --- 14.0 -56.5 9.4 26.4 ---
07/03/12 --- NS 4.8 160.3 53.9 ---
01/30/13 --- 61.0 1.6 95.8 108.8 ---
07/15/13 --- 20.7 -3.4 104.7 79.8 ---
01/30/14 --- 140.1 116.2 66.8 74.4 ---
07/22/14 --- 6.2 65.5 35.5 36.0 ---
01/26/15 FIELD 114.9 113.3 120.3 105.3 ---
07/28/15 --- 115.7 95.1 8.08 51.1 ---
Foothills Regional Landfill
Permit No. 14-03 Page 11 of 12
Joyce Engineering
APPENDIX E
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date SWSL SW-1 SW-2 SW-3 SW-4 Blanks
Notes:
DL = Method Detection Limit.
RL = Reporting Limit = PQL prior to 2007 and SWSL starting January 2007.
PQL = Practical Quantitation Limit.
SWSL = NC-DENR Solid Waste Section Limit.
NC 2B = Surface Water Standard established in 15A NCAC 2B (NC Freshwater Aquatic Life Standards)
ND = Not detected above the DL.
J = Estimated concentration below the RL.
B = Blank qualified data.
dry = Insufficient water flow for sampling.
--- = No data.
All inorganic and organic compunds are reported in µg/L
µg/L = micrograms per liter
S.U. = Standard Units.
NTU = Nephelometric Turbidity Units.
µS/cm= microsiemens per centimeter.
mV = Millivolts.
Bold = Concentrations above the NC 2B Standards.
Blanks = field, trip and/or method blanks.
All data prior to 2012 taken from previous reports by Golder Associates NC, Inc.
Foothills Regional Landfill
Permit No. 14-03 Page 12 of 12
Joyce Engineering

Appendix F

Historical Constituents/Analytes
in Leachate

APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Inorganic Compounds
Antimony 01/23/07 6.00 4.40 ND
07/25/07 6.00 3.91 J ND
01/08/08 6.00 ND ND
07/24/08 6.00 2.82 J ND
01/07/09 6.00 5.73 J ND
07/09/09 6.00 1.64 J ND
01/20/10 6.00 3.00 J ND
07/27/10 6.00 6.22 J ND
01/24/11 6.00 6.51 J ND
07/25/11 6.00 5.91 J ND
01/05/12 6.00 9.83 ND
07/02/12 6.00 10.80 ND
01/30/13 6.00 11.10 ND
07/15/13 6.00 5.87 J 0.45 J
01/30/14 6.00 9.55 J 0.62 J
07/22/14 6.00 15.1 ND
01/26/15 6.00 14.5 ND
07/28/15 6.00 18.3 ND
Arsenic 07/09/09 10.0 9.27 B 2.92 J
01/20/10 10.0 ND ND
07/27/10 10.0 8.90 J ND
01/24/11 10.0 4.75 J ND
07/25/11 10.0 6.12 J ND
01/05/12 10.0 15.70 ND
07/02/12 10.0 14.90 ND
01/30/13 10.0 12.30 ND
07/15/13 10.0 10.20 ND
01/30/14 10.0 7.79 J ND
07/22/14 10.0 19.5 ND
01/26/15 10.0 14.3 ND
07/28/15 10.0 22.2 ND
Barium 07/21/00 500 120.00 ND
04/01/04 500 ND ---
07/16/04 500 ND ND
10/18/04 500 ND ---
01/28/05 500 ND ND
04/27/05 500 ND ---
07/21/05 500 ND ND
10/21/05 500 ND ---
01/19/06 500 2990 ---
01/23/07 100 303 ND
07/25/07 100 182 ND
01/08/08 --- 33.8 J 0.30 J
07/24/08 100 230 1.30 J
01/07/09 100 239 ND
07/09/09 100 397 ND
01/20/10 100 538 0.30 J
07/27/10 100 253 ND
01/24/11 100 431 ND
07/25/11 100 347 ND
01/05/12 100 334 0.13 J
07/02/12 100 324 0.49 J
01/30/13 100 365 ND
07/15/13 100 324 ND
01/30/14 100 348 ND
07/22/14 100 407 0.26 J
01/26/15 100 409 ND
07/28/15 100 428 ND
Foothills Regional Landfill
Permit No. 14-03 Page 1 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Beryllium 01/19/06 2.00 2.10 ---
01/23/07 1.00 ND ND
07/25/07 1.00 ND ND
01/08/08 1.00 ND ND
07/24/08 1.00 ND ND
01/07/09 1.00 ND ND
07/09/09 1.00 ND ND
01/20/10 1.00 ND ND
07/27/10 1.00 ND ND
01/24/11 1.00 ND ND
07/25/11 1.00 ND ND
01/05/12 1.00 0.06 J ND
07/02/12 1.00 ND ND
01/30/13 1.00 ND ND
07/15/13 1.00 ND ND
01/30/14 1.00 0.13 J ND
07/22/14 1.00 0.05 J ND
01/26/15 1.00 0.05 J ND
07/28/15 1.00 ND ND
Cadmium 07/09/09 1.00 0.37 B 0.14 J
01/20/10 1.00 ND ND
07/27/10 1.00 ND ND
01/24/11 1.00 ND ND
07/25/11 1.00 7.91 ND
01/05/12 1.00 ND ND
07/02/12 1.00 ND ND
01/30/13 1.00 0.16 J ND
07/15/13 1.00 ND ND
01/30/14 1.00 0.17 J ND
07/22/14 1.00 0.11 J ND
01/26/15 1.00 0.16 J ND
07/28/15 1.00 0.68 J ND
Chromium 04/01/04 10.0 12.30 ---
07/16/04 10.0 13.20 ND
10/18/04 10.0 ND ---
01/28/05 10.0 16.10 ND
04/27/05 10.0 43.50 ---
07/21/05 10.0 33.4 ND
10/21/05 10.0 41.80 ---
01/19/06 10.0 148 ---
01/23/07 10.0 ND ND
07/25/07 10.0 ND ND
01/08/08 10.0 ND ND
07/24/08 10.0 5.20 J ND
01/07/09 10.0 ND 2.50 J
07/09/09 10.0 24.7 ND
01/20/10 10.0 32.0 ND
07/27/10 10.0 42.0 ND
01/24/11 10.0 31.7 ND
07/25/11 10.0 61.7 ND
01/05/12 10.0 58.8 ND
07/02/12 10.0 66.8 0.76 J
01/30/13 10.0 55.1 ND
07/15/13 10.0 34.2 0.73 J
01/30/14 10.0 50.2 1.92 J
07/22/14 10.0 57.2 0.94 J
01/26/15 10.0 48.6 ND
07/28/15 10.0 89.6 ND
Foothills Regional Landfill
Permit No. 14-03 Page 2 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Cobalt 12/06/99 10.0 10.0 ---
07/21/00 10.0 ND ND
04/01/04 10.0 ND ---
07/16/04 10.0 ND ND
10/18/04 10.0 ND ---
01/28/05 10.0 ND 31.60
04/27/05 10.0 ND ---
07/21/05 10.0 ND ND
10/21/05 10.0 12.4 ---
01/19/06 10.0 41.2 ---
01/23/07 10.0 8.6 J ND
07/25/07 10.0 18.2 ND
01/08/08 10.0 3.90 J ND
07/24/08 10.0 20.0 ND
01/07/09 10.0 8.10 J ND
07/09/09 10.0 8.91 J ND
01/20/10 10.0 12.5 ND
07/27/10 10.0 14.2 ND
01/24/11 10.0 24.6 ND
07/25/11 10.0 22.1 ND
01/05/12 10.0 21.6 ND
07/02/12 10.0 23.2 ND
01/30/13 10.0 23.8 ND
07/15/13 10.0 16.8 ND
01/30/14 10.0 19.1 ND
07/22/14 10.0 18.2 ND
01/26/15 10.0 18.7 ND
07/28/15 10.0 25.4 ND
Copper 07/21/00 200 200 ND
04/01/04 200 ND ---
07/16/04 200 ND ND
10/18/04 200 ND ---
01/28/05 200 ND ND
04/27/05 200 ND ---
07/21/05 200 ND ND
10/21/05 200 ND ---
01/19/06 200 ND ---
01/23/07 10.0 ND ND
07/25/07 10.0 ND ND
01/08/08 10.0 ND 0.60 J
07/24/08 10.0 ND ND
01/07/09 10.0 ND ND
07/09/09 10.0 ND ND
01/20/10 10.0 ND 1.98 J
07/27/10 10.0 ND 2.00 J
01/24/11 10.0 ND ND
07/25/11 10.0 ND 2.02 J
01/05/12 10.0 5.31 J ND
07/02/12 10.0 8.64 J ND
01/30/13 10.0 44.20 0.96 J
07/15/13 10.0 120 ND
01/30/14 50.0 3050 ND
07/22/14 10.0 8.97 J 1.23 J
01/26/15 10.0 5.67 J ND
07/28/15 10.0 1.76 J ND
Foothills Regional Landfill
Permit No. 14-03 Page 3 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Lead 12/06/99 10.0 20 ---
07/21/00 10.0 30 ND
04/01/04 10.0 ND ---
07/16/04 10.0 ND ND
10/18/04 10.0 ND ---
01/28/05 10.0 ND ND
04/27/05 10.0 ND ---
07/21/05 10.0 ND ND
10/21/05 10.0 ND ---
01/19/06 10.0 27.60 ---
01/23/07 10.0 ND ND
07/25/07 10.0 ND ND
01/08/08 10.0 ND ND
07/24/08 10.0 ND ND
01/07/09 10.0 ND ND
07/09/09 10.0 2.15 J ND
01/20/10 10.0 4.31 J ND
07/27/10 10.0 ND ND
01/24/11 10.0 ND ND
07/25/11 10.0 ND ND
01/05/12 10.0 0.59 J ND
07/02/12 10.0 0.49 J ND
01/30/13 10.0 3.21 J ND
07/15/13 10.0 4.40 J ND
01/30/14 10.0 37.6 ND
07/22/14 10.0 0.46 B 0.14 J
01/26/15 10.0 0.30 J ND
07/28/15 10.0 0.63 J ND
Nickel 04/01/04 50.0 51.3 ---
07/16/04 50.0 50.3 ND
10/18/04 50.0 ND ---
01/28/05 50.0 ND ND
04/27/05 50.0 72.3 ---
07/21/05 50.0 87.5 ND
10/21/05 50.0 117 ---
01/19/06 50.0 133 ---
01/23/07 50.0 99 ND
07/25/07 50.0 160 ND
01/08/08 50.0 16.6 J ND
07/24/08 50.0 142 ND
01/07/09 50.0 48.4 J ND
07/09/09 50.0 53.9 1.09 J
01/20/10 50.0 74.5 ND
07/27/10 50.0 112 ND
01/24/11 50.0 85.8 ND
07/25/11 50.0 141 ND
01/05/12 50.0 171 ND
07/02/12 50.0 205 ND
01/30/13 50.0 178 ND
07/15/13 50.0 117 ND
01/30/14 50.0 126 ND
07/22/14 50.0 156 0.33 J
01/26/15 50.0 140 ND
07/28/15 50.0 207 ND
Foothills Regional Landfill
Permit No. 14-03 Page 4 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Selenium 07/25/07 10.0 2.40 J ND
01/08/08 10.0 ND ND
07/24/08 10.0 ND ND
01/07/09 10.0 ND ND
07/09/09 10.0 ND ND
01/20/10 10.0 ND ND
07/27/10 10.0 3.39 B 3.83 J
01/24/11 10.0 3.66 J ND
07/25/11 10.0 3.93 J ND
01/05/12 10.0 20.60 ND
07/02/12 10.0 12.20 ND
01/30/13 10.0 11.00 ND
07/15/13 10.0 6.23 J ND
01/30/14 10.0 0.88 J ND
07/22/14 10.0 8.18 J ND
01/26/15 10.0 8.09 J ND
07/28/15 10.0 3.25 J ND
Silver 01/20/10 10.0 4.32 J 0.82 J
07/27/10 10.0 ND ND
01/24/11 10.0 ND ND
07/25/11 10.0 ND ND
01/05/12 10.0 0.19 J ND
07/02/12 10.0 0.26 J ND
01/30/13 10.0 0.16 J ND
07/15/13 10.0 ND ND
01/30/14 10.0 ND ND
07/22/14 10.0 ND ND
01/26/15 10.0 0.23 J ND
07/28/15 10.0 ND ND
Thallium 07/27/10 5.50 4.42 J ND
01/24/11 5.50 ND ND
07/25/11 5.50 ND ND
01/05/12 5.50 ND ND
07/02/12 5.50 ND ND
01/30/13 5.50 ND ND
07/15/13 5.50 0.08 J ND
01/30/14 5.50 ND ND
07/22/14 5.50 ND ND
01/26/15 5.50 ND ND
07/28/15 5.50 ND ND
Vanadium 01/19/06 40.0 94.6 ---
01/23/07 25.0 ND ND
07/25/07 25.0 11.1 J ND
01/08/08 25.0 2.5 J ND
07/24/08 25.0 17.1 J ND
01/07/09 25.0 ND ND
07/09/09 25.0 10.7 J ND
01/20/10 25.0 17.0 J ND
07/27/10 25.0 28.4 ND
01/24/11 25.0 20.1 J ND
07/25/11 25.0 32.3 ND
01/05/12 25.0 27.3 ND
07/02/12 25.0 30.4 ND
01/30/13 25.0 20.3 J ND
07/15/13 25.0 14.5 J ND
01/30/14 25.0 19.7 B 9.89 J
07/22/14 25.0 25.7 1.95 J
01/26/15 25.0 20.8 J ND
07/28/15 25.0 49.6 ND
Foothills Regional Landfill
Permit No. 14-03 Page 5 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Zinc 12/06/99 50.0 380 ---
07/21/00 50.0 130 B 60.00
04/01/04 50.0 ND ---
07/16/04 50.0 62.8 ND
10/18/04 50.0 ND ---
01/28/05 50.0 ND ND
04/27/05 50.0 ND ---
07/21/05 50.0 ND ND
10/21/05 50.0 61.1 ---
01/19/06 50.0 589 ---
01/23/07 10.0 2.00 J ND
07/25/07 10.0 ND 1.40 J
01/08/08 10.0 2.10 J ND
07/24/08 10.0 ND ND
01/07/09 10.0 3.90 J ND
07/09/09 10.0 7.05 J ND
01/20/10 10.0 10.9 B 3.07 J
07/27/10 10.0 6.45 J ND
01/24/11 10.0 15.1 B 4.41 J
07/25/11 10.0 20.2 B 13.80
01/05/12 10.0 44.5 2.14 J
07/02/12 10.0 29.4 0.94 J
01/30/13 10.0 113 1.25 J
07/15/13 10.0 95.6 ND
01/30/14 10.0 330 ND
07/22/14 10.0 34.3 1.60 J
01/26/15 10.0 41.5 1.05 J
07/28/15 10.0 128.0 ND
Organic Compounds
Acetone 12/06/99 100 9200 ---
07/21/00 100 ND ND
04/01/04 100 3460 ---
07/16/04 100 2640 ND
10/18/04 100 7650 ---
01/28/05 100 8980 ND
04/27/05 100 18600 ---
07/21/05 100 ND ND
10/21/05 100 311 ---
01/19/06 100 250 ---
03/14/06 2 ND ND
01/23/07 100 1900 ND
07/25/07 100 ND ND
01/08/08 100 650 ND
07/24/08 100 ND ND
01/07/09 100 2600 ND
07/09/09 100 41.0 J ND
01/20/10 100 2500 ND
07/27/10 100 690 ND
01/24/11 100 12000 ND
07/25/11 100 160 ND
01/05/12 100 7000 3.80 J
07/02/12 100 49 ND
01/30/13 100 3600 ND
07/15/13 100 21 J ND
01/30/14 2000 2100 ND
07/22/14 100 290 ND
01/26/15 100 2400 ND
07/28/15 100 23 J ND
Foothills Regional Landfill
Permit No. 14-03 Page 6 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Benzene 04/01/04 1.00 8.77 ---
07/16/04 1.00 1.90 ND
10/18/04 1.00 ND ---
01/28/05 1.00 1.69 ND
04/27/05 1.00 12.2 ---
07/21/05 1.00 8.90 ND
10/21/05 1.00 4.66 ---
01/19/06 1.00 4.10 ---
03/14/06 1.00 ND ND
01/23/07 3.00 16.0 ND
07/25/07 1.00 7.5 J ND
01/08/08 1.00 18.0 ND
07/24/08 1.00 6.10 J ND
01/07/09 1.00 18.0 ND
07/09/09 1.00 14.0 ND
01/20/10 1.00 19.0 ND
07/27/10 1.00 9.1 J ND
01/24/11 1.00 ND ND
07/25/11 1.00 8.8 J ND
01/05/12 1.00 15.0 ND
07/02/12 1.00 11.0 ND
01/30/13 1.00 12.0 ND
07/15/13 1.00 12.0 ND
01/30/14 1.00 16.0 ND
07/22/14 1.00 6.8 ND
01/26/15 1.00 13 ND
07/28/15 1.00 8 ND
Carbon Disulfide 01/30/13 100 3.2 J ND
07/15/13 100 ND ND
01/30/14 100 ND ND
07/28/15 100 35.0 ND
Chlorobenzene 07/02/12 3.00 0.40 J ND
01/30/13 3.00 0.60 J ND
07/15/13 3.00 0.80 J ND
01/30/14 3.00 0.60 J ND
07/22/14 3.00 0.40 J ND
01/26/15 3.00 0.6 J ND
07/28/15 3.00 ND ND
Chloroethane 01/30/13 10.0 3.4 J ND
07/15/13 10.0 ND ND
01/30/14 10.0 1.0 J ND
07/22/14 10.0 ND ND
01/26/15 10.0 ND ND
07/28/15 10.0 ND ND
1,2-Dichlorobenzene 01/26/15 5.0 0.30 J ND
07/28/15 5.0 ND ---
1,4-Dichlorobenzene 01/08/08 1.0 7.2 J ND
07/24/08 1.0 ND ND
01/07/09 1.0 7.6 J ND
07/09/09 1.0 8.2 ND
01/20/10 1.0 11.0 ND
07/27/10 1.0 6.40 J ND
01/24/11 1.0 ND ND
07/25/11 1.0 ND ND
01/05/12 1.0 9.5 ND
07/02/12 1.0 5.5 ND
01/30/13 1.0 6.1 ND
07/15/13 1.0 7.2 ND
01/30/14 1.0 8.4 ND
07/22/14 1.0 3.7 ND
01/26/15 1.0 8.9 ND
07/28/15 1.0 4.4 ND
Foothills Regional Landfill
Permit No. 14-03 Page 7 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
1,1-Dichloroethane 12/06/99 5.0 5.00 ---
07/21/00 5.0 ND ND
04/01/04 5.0 ND ---
07/16/04 5.0 ND ND
10/18/04 5.0 ND ---
01/28/05 5.0 ND ND
04/27/05 5.0 ND ---
07/21/05 5.0 ND ND
10/21/05 5.0 ND ---
01/19/06 5.0 ND ---
03/14/06 1.0 ND ND
01/23/07 5.0 ND ND
07/25/07 5.0 ND ND
01/08/08 5.0 ND ND
07/24/08 5.0 ND ND
01/07/09 5.0 ND ND
07/09/09 5.0 ND ND
01/20/10 5.0 ND ND
07/27/10 5.0 ND ND
01/24/11 5.0 ND ND
07/25/11 5.0 ND ND
01/05/12 5.0 ND ND
07/02/12 5.0 ND ND
01/30/13 5.0 0.90 J ND
07/15/13 5.0 ND ND
01/30/14 5.0 0.90 J ND
07/22/14 5.0 ND ND
01/26/15 5.0 0.3 J ND
07/28/15 5.0 ND ND
1,2-Dichloroethane 01/30/13 1.0 2.7 ND
07/15/13 1.0 0.7 J ND
01/30/14 1.0 4.2 ND
07/22/14 1.0 ND ND
01/26/15 1.0 1.2 ND
07/28/15 1.0 ND ND
cis-1,2-Dichloroethene 07/21/00 5.0 9.00 ND
04/01/04 5.0 6.06 ---
07/16/04 5.0 ND ND
10/18/04 5.0 ND ---
01/28/05 5.0 ND ND
04/27/05 5.0 ND ---
07/21/05 5.0 ND ND
10/21/05 5.0 ND ---
01/19/06 5.0 ND ---
03/14/06 1.0 ND ND
01/23/07 5.0 ND ND
07/25/07 5.0 ND ND
01/08/08 5.0 ND ND
07/24/08 5.0 ND ND
01/07/09 5.0 ND ND
07/09/09 5.0 ND ND
01/20/10 5.0 ND ND
07/27/10 5.0 ND ND
01/24/11 5.0 ND ND
07/25/11 5.0 ND ND
01/05/12 5.0 ND ND
07/02/12 5.0 ND ND
01/30/13 5.0 ND ND
07/15/13 5.0 ND ND
01/30/14 5.0 2.4 J ND
07/22/14 5.0 ND ND
01/26/15 5.0 ND ND
07/28/15 5.0 ND ND
Foothills Regional Landfill
Permit No. 14-03 Page 8 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Trans-1,2-dichloroethene 01/05/12 5.0 0.80 J ND
07/02/12 5.0 0.40 J ND
01/30/13 5.0 0.60 J ND
07/15/13 5.0 0.50 J ND
01/30/14 5.0 0.90 J ND
07/22/14 5.0 0.40 J ND
01/26/15 5.0 0.30 J ND
07/28/15 5.0 ND ND
Ethylbenzene 12/06/99 5.0 39.0 ---
07/21/00 5.0 22.0 ND
04/01/04 5.0 49.7 ---
07/16/04 5.0 11.6 ND
10/18/04 5.0 22.6 ---
01/28/05 5.0 24.1 ND
04/27/05 5.0 60.1 ---
07/21/05 5.0 34.0 ND
10/21/05 5.0 20.9 ---
01/19/06 5.0 16.5 ---
03/14/06 1.0 ND ND
01/23/07 5.0 110 ND
07/25/07 1.0 26.0 ND
01/08/08 1.0 41.0 ND
07/24/08 1.0 27.0 ND
01/07/09 1.0 110 ND
07/09/09 1.0 92.0 ND
01/20/10 1.0 130 ND
07/27/10 1.0 57.0 ND
01/24/11 1.0 80.0 J ND
07/25/11 1.0 45.0 ND
01/05/12 1.0 82.0 ND
07/02/12 1.0 42.0 ND
01/30/13 1.0 50.0 ND
07/15/13 1.0 47.0 ND
01/30/14 1.0 71.0 ND
07/22/14 1.0 26.0 ND
01/26/15 1.0 62.0 ND
07/28/15 1.0 30.0 ND
Methylene chloride 12/06/99 10.0 16.00 ---
07/21/00 10.0 ND ND
04/01/04 10.0 ND ---
07/16/04 10.0 ND ND
10/18/04 10.0 ND ---
01/28/05 10.0 ND ND
04/27/05 10.0 ND ---
07/21/05 10.0 ND ND
10/21/05 10.0 ND ---
01/19/06 10.0 64.90 ---
03/14/06 1.0 ND ND
01/23/07 5.5 3.20 J ND
07/25/07 1.0 ND ND
01/08/08 1.0 ND ND
07/24/08 1.0 ND ND
01/07/09 1.0 60.00 ND
07/09/09 1.0 ND ND
01/20/10 1.0 ND ND
07/27/10 1.0 ND ND
01/24/11 1.0 ND ND
07/25/11 1.0 ND ND
01/05/12 1.0 ND ND
07/02/12 1.0 ND ND
01/30/13 1.0 1.60 B 0.30 J
07/15/13 1.0 ND ND
01/30/14 1.0 5.90 B 1.20
07/22/14 1.0 ND ND
01/26/15 1.0 ND ND
07/28/15 1.0 ND ND
Foothills Regional Landfill
Permit No. 14-03 Page 9 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Methyl Butyl Ketone (2-Hexanone)07/02/12 100 1.80 J ND
01/30/13 50 17.0 J ND
07/15/13 50 ND ND
01/30/14 50 5.80 J ND
07/22/14 50 6.70 J ND
01/26/15 50 6.0 J ND
07/28/15 50 ND ---
Methyl Ethyl Ketone (2-Butanone)12/06/99 100 2600 ---
07/21/00 100 ND ND
04/01/04 100 1190 ---
07/16/04 100 895 ND
10/18/04 100 5320 ---
01/28/05 100 3770 ND
04/27/05 100 4020 ---
07/21/05 100 ND ND
10/21/05 100 599 ---
01/19/06 100 198 ---
03/14/06 2 ND ND
01/23/07 100 960 ND
07/25/07 100 ND ND
01/08/08 100 510 ND
07/24/08 100 ND ND
01/07/09 100 1000 ND
07/09/09 100 ND ND
01/20/10 100 2800 ND
07/27/10 100 340 ND
01/24/11 100 7800 ND
07/25/11 100 82 J ND
01/05/12 100 6200 ND
07/02/12 100 160 ND
01/30/13 2000 3900 ND
07/15/13 100 160 ND
01/30/14 2000 2100 2.30 J
07/22/14 100 ND ND
01/26/15 100 1600 ND
07/28/15 100 ND ND
4-Methyl-2-pentanone (MIBK)01/28/05 100 114 ND
04/27/05 100 ND ---
07/21/05 100 ND ND
10/21/05 100 ND ---
01/19/06 100 ND ---
03/14/06 2 ND ND
01/23/07 100 67.0 ND
07/25/07 100 ND ND
01/08/08 100 25.0 J ND
07/24/08 100 ND ND
01/07/09 100 ND ND
07/09/09 100 ND ND
01/20/10 100 100 ND
07/27/10 100 20.0 J ND
01/24/11 100 ND ND
07/25/11 100 24.0 J ND
01/05/12 100 110 ND
07/02/12 100 16.0 J ND
01/30/13 100 64.0 ND
07/15/13 100 14.0 J ND
01/30/14 100 61.0 J ND
07/22/14 100 26.0 J ND
01/26/15 100 44 J ND
07/28/15 100 22 J ND
1,2-Dichloropropane 01/26/15 1.0 0.3 J ND
07/28/15 1.0 ND ND
Foothills Regional Landfill
Permit No. 14-03 Page 10 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Styrene 01/19/06 10.0 12.30 ---
03/14/06 1.0 ND ND
01/23/07 10.0 ND ND
07/25/07 1.00 ND ND
01/08/08 1.00 ND ND
07/24/08 1.0 ND ND
01/07/09 1.0 ND ND
07/09/09 1.0 ND ND
01/20/10 1.0 ND ND
07/27/10 1.0 ND ND
01/24/11 1.0 ND ND
07/25/11 1.0 ND ND
01/05/12 1.0 ND ND
07/02/12 1.0 ND ND
01/30/13 1.0 ND ND
07/15/13 1.0 ND ND
01/30/14 1.0 4.9 ND
07/22/14 1.0 ND ND
01/26/15 1.0 3.2 ND
07/28/15 1.0 2.7 ND
Toluene 12/06/99 5.0 76 ---
07/21/00 5.0 77 ND
04/01/04 5.0 125 ---
07/16/04 5.0 26 ND
10/18/04 5.0 69 ---
01/28/05 5.0 59 7.02
04/27/05 5.0 359 ---
07/21/05 5.0 160 ND
10/21/05 5.0 29 ---
01/19/06 5.0 181 ---
03/14/06 1.0 ND ND
01/23/07 5.0 150 ND
07/25/07 1.0 14 0.40 J
01/08/08 1.0 30.0 ND
07/24/08 1.0 4.5 J ND
01/07/09 1.0 90 ND
07/09/09 1.0 14 ND
01/20/10 1.0 43 ND
07/27/10 1.0 11 ND
01/24/11 1.0 68 J ND
07/25/11 1.0 35 ND
01/05/12 1.0 55 ND
07/02/12 1.0 12 ND
01/30/13 1.0 54 ND
07/15/13 1.0 27 ND
01/30/14 1.0 72 ND
07/22/14 1.0 13 ND
01/26/15 1.0 78 ND
07/28/15 1.0 14 ND
Foothills Regional Landfill
Permit No. 14-03 Page 11 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Trichloroethene 01/19/06 2.0 3.11 ---
03/14/06 1.0 ND ND
01/23/07 3.0 ND ND
07/25/07 1.0 ND ND
01/08/08 1.0 ND ND
07/24/08 1.0 ND ND
01/07/09 1.0 ND ND
07/09/09 1.0 ND ND
01/20/10 1.0 ND ND
07/27/10 1.0 ND ND
01/24/11 1.0 ND ND
07/25/11 1.0 ND ND
01/05/12 1.0 ND ND
07/02/12 1.0 ND ND
01/30/13 1.0 ND ND
07/15/13 1.0 ND ND
01/30/14 1.0 0.4 J ND
07/22/14 1.0 ND ND
01/26/15 1.0 0.6 J ND
07/28/15 1.0 ND ND
Vinyl chloride 04/01/04 1.0 17.3 ---
07/16/04 1.0 ND ND
10/18/04 1.0 ND ---
01/28/05 1.0 5.5 ND
04/27/05 1.0 ND ---
07/21/05 1.0 ND ND
10/21/05 1.0 ND ---
01/19/06 1.0 ND ---
03/14/06 1.0 ND ND
01/23/07 5.5 4.8 J ND
07/25/07 1.0 ND ND
01/08/08 1.0 ND ND
07/24/08 1.0 ND ND
01/07/09 1.0 4.1 J ND
07/09/09 1.0 2.0 ND
01/20/10 1.0 ND ND
07/27/10 1.0 ND ND
01/24/11 1.0 ND ND
07/25/11 1.0 ND ND
01/05/12 1.0 2.7 ND
07/02/12 1.0 0.6 J ND
01/30/13 1.0 1.5 ND
07/15/13 1.0 1.8 ND
01/30/14 1.0 2.2 ND
07/22/14 1.0 0.4 J ND
01/26/15 1.0 0.5 J ND
07/28/15 1.0 ND ND
Foothills Regional Landfill
Permit No. 14-03 Page 12 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Xylenes, total 12/06/99 5.0 21.0 ---
07/21/00 5.0 12.0 ND
04/01/04 5.0 45.5 ---
07/16/04 5.0 11.3 ND
10/18/04 5.0 17.3 ---
01/28/05 5.0 20.5 ND
04/27/05 5.0 54.9 ---
07/21/05 5.0 33.3 ND
10/21/05 5.0 21.0 ---
01/19/06 5.0 24.0 ---
03/14/06 1.0 ND ND
01/23/07 4.0 64.0 ND
07/25/07 4.0 23 ND
01/08/08 5.0 100 ND
07/24/08 5.0 33 ND
01/07/09 5.0 110 ND
07/09/09 5.0 96 ND
01/20/10 5.0 130 ND
07/27/10 5.0 62 ND
01/24/11 5.0 ND ND
07/25/11 5.0 52 ND
01/05/12 5.0 94 ND
07/02/12 5.0 53 ND
01/30/13 5.0 62 ND
07/15/13 5.0 68 ND
01/30/14 5.0 93 ND
07/22/14 5.0 33 ND
01/26/15 5.0 79 ND
07/28/15 5.0 40 ND
Other Parameters
Nitrate 01/23/07 0.1 0.07 J ---
07/25/07 10.0 0.04 ---
01/08/08 10.0 0.22 J ---
07/24/08 10.0 0.06 B 0.03 J
01/07/09 10.0 0.06 J ND
07/09/09 10.0 0.05 J ND
01/20/10 10.0 0.06 J ND
07/27/10 10.0 0.05 J -
01/24/11 10.0 0.03 J -
07/25/11 10.0 0.05 J ND
01/05/12 50 46.0 J ND
07/02/12 50 ND ND
01/30/13 500 ND ND
07/15/13 100 910 ND
01/30/14 100 ND ND
07/22/14 50 ND ND
07/28/15 50 160 ND
Foothills Regional Landfill
Permit No. 14-03 Page 13 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Sulfate 04/01/04 0.4 0.62 ---
07/16/04 0.4 0.55 ---
10/18/04 0.4 1.00 ---
01/28/05 0.4 0.71 ---
04/27/05 0.4 0.45 ---
07/21/05 0.4 ND ---
10/21/05 0.4 0.58 ---
01/19/06 0.4 ND ---
01/23/07 0.4 15.0 ---
07/25/07 250 46.0 J ND
01/08/08 250 130.0 J ND
07/24/08 250 34.0 J ND
01/07/09 250 10.0 J ND
07/09/09 250 2.4 J ND
01/20/10 250 1.5 J ND
07/27/10 250 2.1 J ND
01/24/11 250 2.3 J ND
07/25/11 250 2.4 J ND
01/05/12 5000 82.0 J ND
07/02/12 5000 23000 ND
01/30/13 50000 ND ND
07/15/13 10000 11000 ND
01/30/14 10000 ND ND
07/22/14 50 ND ND
01/26/15 250000 ND ND
07/28/15 500 ND ND
Biochemical Oxygen Demand 04/01/04 120 339 ---
07/16/04 120 32.3 ---
10/18/04 120 543 ---
01/28/05 120 624 ---
04/27/05 120 1130 ---
07/21/05 120 129 ---
10/21/05 120 167 ---
01/19/06 120 ND ---
01/23/07 120 310 ---
07/25/07 250 43 ND
01/08/08 --- <33 J ND
07/24/08 --- 38.0 ND
01/07/09 --- >222.36 ND
07/09/09 --- 41.0 ND
01/20/10 --- 310 ND
07/27/10 --- 120 ND
01/24/11 --- 790 ND
07/25/11 --- 83.0 ND
01/05/12 20000 510000 ND
07/02/12 17000 66000 0.11 J
01/30/13 26000 1300000 ND
07/15/13 13000 42000 ND
01/30/14 18000 121000 250 J
07/22/14 9000 123000 10.0 J
01/26/15 378000 ---
07/28/15 15000 90000 D ND
Foothills Regional Landfill
Permit No. 14-03 Page 14 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Chemical Oxygen Demand 04/01/04 20.0 458 ---
07/16/04 20.0 279 ---
10/18/04 20.0 557 ---
01/28/05 20.0 964 ---
04/27/05 20.0 1960 ---
07/21/05 20.0 678 ---
10/21/05 20.0 860 ---
01/19/06 20.0 608 ---
01/23/07 20.0 880 ---
07/25/07 --- 790 ND
01/08/08 --- 680 ND
07/24/08 --- 690 ND
01/07/09 --- 710 ND
07/09/09 --- 370 ND
01/20/10 --- 690 ND
07/27/10 --- 970 ND
01/24/11 --- 1600 ND
07/25/11 --- 750 ND
01/05/12 100000 1570000 D ND
07/02/12 10.0 1100000 ND
01/30/13 200 4140000 5830
07/15/13 100 412000 ND
01/30/14 100 2170000 ND
07/22/14 200000 1310000 ND
01/26/15 1220000 ---
07/28/15 100000 1070000 ND
Phosphorus-Total 10/18/04 0.1 0.49 ---
01/28/05 0.1 0.22 ---
04/27/05 0.1 0.25 ---
07/21/05 0.1 0.25 ---
10/21/05 0.1 0.58 ---
01/19/06 0.1 ND ---
01/23/07 0.1 0.47 ---
07/25/07 --- 0.92 ND
01/08/08 --- 1.10 ND
07/24/08 --- 0.69 ND
01/07/09 --- 1.00 ND
07/09/09 --- 0.33 ND
01/20/10 --- 0.32 ND
07/27/10 --- 1.00 ND
01/24/11 --- 0.52 ND
07/25/11 --- 0.61 ND
01/05/12 20.0 ND D ND
07/02/12 0.02 753.0 D ND
01/30/13 0.02 350.0 ND
07/15/13 0.02 759.0 ND
01/30/14 0.22 0.97 ND
07/22/14 200 1030.00 ND
01/26/15 1620.00 D ---
07/28/15 0 4270.00 D ND
Foothills Regional Landfill
Permit No. 14-03 Page 15 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Field Parameters
pH 12/06/99 --- 6.86 ---
(S.U.) 07/21/00 --- 6.89 ---
04/01/04 --- 6.92 ---
07/16/04 --- 7.53 ---
10/18/04 --- 7.26 ---
01/28/05 --- 7.13 ---
04/27/05 --- 7.37 ---
07/21/05 --- 7.50 ---
10/21/05 --- 7.50 ---
01/19/06 --- 6.20 ---
03/14/06 --- 9.93 ---
01/23/07 --- 7.27 ---
07/24/07 --- 7.99 ---
01/08/08 --- 7.65 ---
07/24/08 --- 7.90 ---
01/07/09 --- 6.89 ---
07/09/09 --- 7.26 ---
01/20/10 --- 6.83 ---
07/27/10 --- 7.70 ---
01/24/11 --- 6.77 ---
07/25/11 --- 7.22 ---
01/05/12 --- 7.31 ---
07/02/12 --- 7.72 ---
01/30/13 --- 7.50 ---
07/15/13 --- 7.24 ---
01/30/14 --- 5.08 ---
07/22/14 --- 7.33 ---
01/26/15 --- 7.15 ---
07/28/15 --- 7.81 ---
Conductivity 12/06/99 --- 1000 ---
(µS/cm) 07/21/00 --- 1138 ---
04/01/04 --- 2499 ---
07/16/04 --- 2598 ---
10/18/04 --- 2414 ---
01/28/05 --- 1650 ---
04/27/05 --- 1904 ---
07/21/05 --- 7720 ---
10/21/05 --- 5930 ---
01/19/06 --- 4020 ---
03/14/06 --- 6190 ---
01/23/07 --- 6270 ---
07/25/07 --- 8003 ---
01/08/08 --- 7650 ---
07/24/08 --- 7890 ---
01/07/09 --- 3866 ---
07/09/09 --- 4517 ---
01/20/10 --- 5228 ---
07/27/10 --- 9276 ---
01/24/11 --- 5290 ---
07/25/11 --- 8197 ---
01/05/12 --- 6424 ---
07/02/12 --- 12115 ---
01/30/13 --- 7607 ---
07/15/13 --- 6531 ---
01/30/14 --- 454 ---
07/22/14 --- 10027 ---
01/26/15 FIELD 283.1 ---
07/28/15 --- 13207.0 ---
Foothills Regional Landfill
Permit No. 14-03 Page 16 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Temperature 07/21/00 --- 29.3 ---
(°C)04/01/04 --- 13.2 ---
07/16/04 --- 28.7 ---
10/18/04 --- 20.1 ---
01/28/05 --- 6.2 ---
04/27/05 --- 17.3 ---
10/21/05 --- 26.4 ---
01/19/06 --- 12.1 ---
03/14/06 --- 18.9 ---
01/23/07 --- 9.4 ---
07/25/07 --- 24.28 ---
01/08/08 --- 8.74 ---
07/24/08 --- 24.17 ---
01/07/09 --- 9.69 ---
07/09/09 --- 25.32 ---
01/20/10 --- 6.59 ---
07/27/10 --- 26.89 ---
01/24/11 --- 5.20 ---
07/25/11 --- 25.15 ---
01/05/12 --- 13.09 ---
07/02/12 --- 32.0 ---
01/30/13 --- 16.0 ---
07/15/13 --- 33.5 ---
01/30/14 --- 8.0 ---
07/22/14 --- 28.6 ---
01/26/15 FIELD 9.4 ---
07/28/15 --- 31.8 ---
Turbidity 01/05/12 --- 1000 ---
(NTU)07/02/12 --- 421 ---
01/30/13 --- 1000 ---
07/15/13 --- 1000 ---
01/30/14 --- 1000 ---
07/22/14 --- 80.5 ---
01/26/15 FIELD 80.5 ---
07/28/15 --- 80.5 ---
Oxidation Reduction Potential 01/05/12 --- -49.9 ---
(mV)07/02/12 --- 24.2 ---
01/30/13 --- -154.4 ---
07/15/13 --- -186.5 ---
01/30/14 --- 6.7 ---
07/22/14 ----5.5 ---
01/26/15 FIELD -15.1 ---
07/28/15 --- 7.1 ---
Dissolved Oxygen 01/26/15 FIELD 4.26 ---
07/28/15 --- 2.23 ---
Foothills Regional Landfill
Permit No. 14-03 Page 17 of 18 Joyce Engineering
APPENDIX F
Historical Leachate Constituents/Analytes
Analyte
Sample
Collection Date SWSL Leachate Blanks
Notes:
DL = Method Detection Limit.
RL = Reporting Limit = PQL prior to 2007 and SWSL starting January 2007.
PQL = Practical Quantitation Limit.
SWSL = NC-DENR Solid Waste Section Limit.
ND = Not detected above the DL.
J = Estimated concentration below the RL.
B = Blank qualified data.
--- = No data.
All inorganic and organic compounds are reported in µg/L
Prior to 2012 all "Other Parameters" were reported in mg/L beginning with the 1/5/12 event they are reported in µg/L
mg/L = milligrams per liter
µg/L = micrograms per liter
S.U. = Standard Units.
NTU = Nephelometric Turbidity Units.
µS/cm= microsiemens per centimeter.
mV = Millivolts.
Bold = Concentrations above the NC 2L or Groundwater Protection standards (GWPS) have been bolded.
Blanks = field, trip and/or method blanks.
All data prior to 2012 taken from previous reports by Golder Associates NC, Inc.
R = Anomalous data.
*8260B analysis diluted by a factor of 10x for the July 2011 event.
*6020A analysis for Antimony and Thallium diluted by a factor of 10x for the July 2011 event.
*Acetone & MEK DF 50x; C.O.D. DF 10x for the January 2012 event.
Phosphorous, total DF 1.11x for Jan. & July 2012 events.
Foothills Regional Landfill
Permit No. 14-03 Page 18 of 18 Joyce Engineering