1302-CDLF-2006_CabbarrusCountyCDLF_GWNReport_DIN26470_20160519

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5400 Glenwood Avenue, Suite 400
Raleigh, North Carolina 27612
tel: [phone]
fax: [phone]

July 12, 2016

Ms. Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
2090 U.S. 70 Highway
Swannanoa, North Carolina 28778

Subject: May 2016 Semi-Annual Sampling Report
Cabarrus County C&D Landfill
Facility Permit No. 13-02

Dear Ms. Drummond:
CDM Smith Inc., on behalf of Cabarrus County, is submitting an electronic copy of the May 2016
semi-annual sampling event report for the Cabarrus County C&D Landfill. This letter report presents the
results of the recently completed sampling at the C&D Landfill and constitutes the first semi-annual
sampling event for 2016.
The approved monitoring well network for the C&D Landfill consists of background wells CD-1s and -1d;
compliance wells CD-2, -3, -4 Rep, -7, and -8; and surface water sample location SW-3. CD-4 Rep was
installed in January 2009 as part of the proposed Phase 1 C&D Landfill expansion. Monitoring wells CD-7
and -8, formerly piezometers B-7 and -19 respectively, were added to the monitoring program in July
2014 as part of the Phase 2 C&D Landfill expansion. Field activities and sampling results for the
groundwater and surface water samples are discussed below.
Field Activities
Groundwater samples from the Cabarrus County C&D Landfill were collected on May 17-19, 2016.
Groundwater samples were collected from the monitoring wells by use of disposable, laboratory
decontaminated Teflon™ bailers or a QED bladder pump system using low-flow sampling techniques.
Monitoring well locations and the surface water location for the C&D Landfill are provided on Figure 1.
Groundwater elevations were measured at each well prior to sampling and are presented in Table 1.
Well construction details for each monitoring well are also provided in Table 1. These groundwater
elevations were used to construct potentiometric contours for this sampling event and are presented on
Figure 1. After depth to groundwater was measured, each well was purged prior to sampling to provide
fresh formation water within the well water column. Each purge volume was measured for pH,
conductivity, turbidity, temperature, dissolved oxygen, and oxidation-reduction potential using a YSI-556

Ms. Jaclynne Drummond
July 12, 2016
Page 2

multi-parameter water quality meter and Oakton T100 or Lamotte 2020 turbidity meters. The water
quality parameters at the time of sampling are presented in Table 2.
The headspace of each monitoring well was screened for methane gas using a RKI Eagle multi-gas
monitor. Screening results are provided in Appendix A.
Sampling Results
Analytical Services, Inc. located in Norcross, Georgia, analyzed the groundwater and surface water
samples for North Carolina Appendix I volatile organic compounds (VOCs) plus tetrahydrofuran, North
Carolina Appendix I metals plus iron, mercury, and manganese, alkalinity, total dissolved solids, chloride,
and sulfate with the exception of CD-4 Rep. Samples collected from CD-4 Rep were analyzed for North
Carolina Appendix I VOCs and metals.

In accordance with the North Carolina Department of Environmental Quality’s Solid Waste Section
(SWS) guidelines the analytical results were reported to the laboratory specific method detection limit
(MDL) and are quantifiable at or below SWS Limits (SWSLs). All monitoring wells for the C&D Landfill had
detections of analytes above the MDL but below the SWSL. These detections were qualified as
estimated or “J” flags.
The following list indicates the analytes detected above the laboratory specific MDL at each sampling
location. No “J” flag or general chemistry detections are provided. Underlined analytes exceeded the
15A NCAC 02L .0202 (NC 2L) Groundwater Quality Standard, Groundwater Protection Standard, or the
15A NCAC 02B Surface Water Quality Standard for Class C Waters.
CD-1s (Background)
Metals: Iron
Volatile Organic Compounds: None Detected

CD-1d (Background)
Metals: Copper, Iron, Manganese, Vanadium, Zinc
Volatile Organic Compounds: None Detected

CD-2
Metals: Iron, Manganese
Volatile Organic Compounds: None Detected
CD-3
Metals: Barium, Iron, Manganese
Volatile Organic Compounds: None Detected

Ms. Jaclynne Drummond
July 12, 2016
Page 3

CD-4 Rep
Metals: None Detected
Volatile Organic Compounds: None Detected
CD-7
Metals: Iron, Manganese
Volatile Organic Compounds: None Detected
CD-8
Metals: Barium, Copper, Iron, Manganese, Zinc
Volatile Organic Compounds: None Detected
SW-3
Metals: Arsenic, Barium, Beryllium, Chromium, Cobalt, Copper, Iron, Lead,
Manganese, Selenium, Vanadium, Zinc
Volatile Organic Compounds: None Detected
“J” flags were not included in the previous list, but several locations had “J” flag detections that
exceeded the standards. These constituents along with their location are listed below.
Cobalt: CD-1d, -2, -3, -4 Rep, and -8
Vanadium: CD-1s, -2, -3, -4 Rep, -7, and -8

A duplicate sample, identified as Dup, was collected from CD-8 and had similar analyte concentrations as
those detected in CD-8. An equipment blank was not collected due to an oversight by the sampling
team. Similar sampling equipment and supplies were used for the May 2016 sampling event compared
to historical events. Historical analytical data has never shown impacts from sampling equipment or
supplies. No analytes were detected above laboratory MDLs in the trip blank.
Total dissolved solids for SW-3 was analyzed outside of hold time due to laboratory error. The analysis
was performed in duplicate and showed similar concentrations in each. The data is interpreted to have
not been affected.
Metals detected above the standards are likely natural occurring based on concentrations in the
background monitoring wells or are from elevated turbidity at the time of sample collection. No VOCs
were detected above the NC 2L Standard. General chemistry results were below the NC 2L Standards. A
complete summary of all detected constituents from the May 2016 sampling event is presented in Table
3. The laboratory analytical report is provided in Appendix A. The next semi-annual sampling event will
be completed in the fall of 2016.

Ms. Jaclynne Drummond
July 12, 2016
Page 4

If you have any questions or require further explanation, do not hesitate to call me at [phone] or
by email at [e-mail].
Very truly yours,

Mathew F. Colone, P.G.
CDM Smith Inc.

cc: Kevin Grant, Cabarrus County
Table 1
Monitoring Well Construction Summary and Groundwater Elevations
May 2016 Semi-Annual Sampling Event
Cabarrus County C&D Landfill
Screen
Interval
Filter
Interval
Seal
Interval
TOC
Elevation
Depth to
Groundwater
(feet BTOC)
Groundwater
Elevation
13-02 CD-1s
(background well)8/7/2006 35.47788 80.52334 Saprolite 29.53 18.0-28.0 16.0-28.0 14.0-16.0 2.0 755.00 23.90 731.10
13-02 CD-1d
(background well)7/21/2004 35.47788 80.52340 PWR 52.15 40.0-50.0 38.0-50.0 36.0-38.0 2.0 757.40 26.51 730.89
13-02 CD-2 9/12/2006 35.47698 80.52494 Saprolite 25.69 9.0-24.0 7.0-24.0 5.0-7.0 2.0 733.00 14.00 719.00
13-02 CD-3 7/1/2014 35.47580 80.52502 Saprolite/PWR 53.50 35.0-50.0 32.0-50.0 30.0-32.0 2.0 744.48 38.25 706.23
13-02 CD-4 Rep 1/15/2009 35.47656 80.52210 Saprolite 19.41 6.0-16.0 4.0-16.0 2.0-4.0 2.0 739.15 8.70 730.45
13-02 CD-7 11/25/2002 35.47567 80.52551 Bedrock 46.31 34.0-44.0 32.0-44.0 30.0-32.0 2.0 744.81 39.65 705.16
13-02 CD-8 7/1/2014 35.47518 80.52497 PWR 43.40 33.0-43.0 31.0-43.0 29.0-31.0 2.0 738.39 31.98 706.41
Notes:
1. BTOC - Below Top of Casing
2. bgs - Below Ground Surface
3. PWR - Partially Weathered Rock
Facility Permit
Number
Groundwater Elevations - Measured 5/16/2016Depth (feet bgs)
Total Depth
(feet BTOC)
Monitoring Well
Diameter
(inches)
Monitoring Well
Code
Geology of
Screened Interval
Installation
Date Latitude Longitude
Page 1 of 1 July 2016
Table 2
Water Quality Measurements
May 2016 Semi-Annual Sampling Event
Cabarrus County C&D Landfill
pH
(S.U.)
Conductivity
(µS/cm)
Temperature
(degrees Celsius)
Dissolved
Oxygen
(mg/L)
ORP
(mVs)
Turbidity
(NTUs)
CD-1s
(background well)5.91 103 15.7 3.45 244.7 3.6
CD-1d
(background well)6.06 115 15.8 4.50 210.3 20
CD-2 5.28 71 14.9 3.31 162.6 64
CD-3*6.28 434 16.8 2.40 23.7 6.3
CD-4 Rep 6.90 242 14.2 2.68 -53.5 28
CD-7 6.16 317 15.8 2.02 40.2 13
CD-8 7.48 262 17.4 3.01 81.7 25
Surface Water Sample Location
SW-3 6.40 200 15.7 5.99 139.3 671
Notes:
1. CD-4 Rep was installed as part of the proposed Phase 1 C&D Landfill expansion in November 2010.
2. * CD-3 was relocated on July 1, 2014, as part of the Phase 2 C&D Landfill Expansion.
3. µS/cm - Microsiemens per centimeter
4. mg/L - Milligrams per liter
5. ORP - Oxidation-Reduction Potential
6. NTUs - Nephelometric Turbidity Units
7. mVs - Millivolts
8. S.U. - Standard Unit
Water Quality Measurements
Monitoring Well Code
Page 1 of 1 July 2016
Table 3a
Detected Groundwater Constituents - General Chemistry and Metals
May 2016 Semi-Annual Sampling Event
Cabarrus County C&D Landfill
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NE NE 250,000 NE 10,000 250,000 500,000 1*10 700 4*2 10 1*1,000 15 300 50 1 100 20 20 0.2*0.3*1,000
NE NE NE NE 10,000 250,000 NE 6 10 100 1 1 10 10 10 10 300 50 0.2 50 10 10 5.5 25 10
CD-1s 25-Sep-06
CD-1s 1-Nov-06
CD-1s 24-Apr-07 49J 0.01J 3.6J 1.6J 7.0J 1.7J 4.0J
CD-1s 29-Oct-07 52J 0.01J 4.4J 1.6J 5.2J 0.87J 2.8J
CD-1s 23-Apr-08 64J 0.01J 5.4J 2.2J 2.8J 0.19J 0.19J
CD-1s 19-Nov-08 1.15J 193 0.02J 18 7.12J
CD-1s 9-Apr-09 55.7J 0.03J 2.54J 2.65J
CD-1s 13-Oct-09 31.1J 0.25J
CD-1s 11-May-10 50,000 3,400 1,000 114,000 29.8J 0.15J 284 13.5 1.04J 5.74J
CD-1s 3-Nov-10 48,300 3,800 1,200J 0.63J 60.4J 0.17J 3.43J 2.53J 10.9 3.87J 5,870 129 0.023J 4.73J 0.02J 0.07J 22.6J 26.9
CD-1s 3-May-11 47,000 3,600 1,200J 146,000 81.4J 0.19J 5.45JB 4.23J 16.0 2.32J 7,770 190 5.93J 0.14J 20.6J 26.5
CD-1s 8-Nov-11 40,000 4,000 1,100J 65,000 59.7J 0.25JB 4.46J 2.67J 12.4 1.9J 5,350 127 4.41J 0.08J 11.2J 18.2
CD-1s 7-May-12 46,000 3,900 158,000 45.5J 3.30J 1.19J 8.75J 1.12J 3,120 63.4 3.01J 12.7J 12.6B
CD-1s 28-Nov-12 39,000 4,100 0 110,000 63.8J 0.11J 5.65J 3.05J 11.6 1.43J 5,210 139 4.66J 17.1J 16.9
CD-1s 7-May-13 42,000 4,000 220 120,000 0.94J 2.4JB 35.6J 0.88J 0.67J 4.04J 0.39J 1,340 37.7 1.78J 0.13J 6.06J 5.08J
CD-1s 5-Nov-13 30,000 3,800 2,420 80,500 46.8J 0.12J 3.59J 1.63J 10.2 1.35J 4,200 82.2 3.50J 18.4JB 15.4B
CD-1s 6-May-14 42,000 3,800 0 111,000 28.8J 4.14JB 1.48J 0.11J 347B 10.1B 1.03J 0.31J 3.40J 2.98JB
CD-1s 4-Nov-14 41,000 3,900 0 102,000 28.7J 0.13J 1.31J 0.06J 118 6.6J 1.04J 0.11J 2.57JB 1.58J
CD-1s 5-May-15 38,000 3,800 0 <5,000 113,000 1.63J 29.5JB 1.33J 0.15J 371 13.8 0.103JB 1.17J 2.40J 2.75JB
CD-1s 27-Oct-15 43,000 30,600 3,800 0 130J 110,000 1.00J 28.4J 0.80J 0.39J 0.75J 0.12J 234 35.9 1.21J 4.19CN,J 0.15J 4.10J 3.36B-01,J
CD-1s 17-May-16 43,000 <10,000 3,700 0 79J 1,000J 130,000 23.9J 0.94J 0.99J 0.12J 446 17.0J 1.01J 4.70J 1.93J
CD-1d 4-Oct-06 10.4
CD-1d 1-Nov-06
CD-1d 24-Apr-07 200 0.77J 0.02J 1.2J 9.3J 17 3.1J 6.5J 0.02J 0.02J
CD-1d 29-Oct-07 53J 0.13J 0.01J 2.8J 2J 6.8J 0.94J 2.3J 1.1J
CD-1d 23-Apr-08 54J 0.02J 2.3J 1.7J 0.24J 0.24J
CD-1d 18-Nov-08 29.9J 0.03J 0.46J 0.18J 0.03J 0.03J
CD-1d 9-Apr-09 26.5J 0.08J 0.11J
CD-1d 13-Oct-09 28.3J 0.18J
CD-1d 11-May-10 40,000 2,400 2,400 132,000 2.21J 359 23 32.6 175 22.5 81,800 1,230 34 0.43J 168 175
CD-1d 2-Nov-10 48,300 2,800 2,800J 0.46J 0.97J 33.1J 0.15J 1.17J 0.85J 6.56J 1.09J 1,730 47.7 0.046J 2.51J 0.05J 14.3J 23
CD-1d 3-May-11 57,000 2,600 3,000J 206,000 2.44J 231 2.03 16.7 18.6 112 14.0 49,400 659 22.3J 0.11J 101 103
CD-1d 8-Nov-11 30,000 2,900 3,000J 98,000 74.5J 0.51J 4.08J 4.27J 27 2.84J 9,190 144 5.68J 24.6J 26.3
CD-1d 7-May-12 50,000 2,800 150,000 72.4J 0.58J 3.91J 4.67J 25 2.81J 9,380 170 5.58J 26 27.9B
CD-1d 28-Nov-12 46,000 3,000 0 128,000 0.33J 37.7J 0.07J 2.38J 0.94J 12.6 1.14J 1,900 41.4 2.50J 8.90J 13
CD-1d 7-May-13 52,000 3,000 560 125,000 0.88J 1.02JB 31.2J 0.07J 0.78J 4.5J 0.49J 1,080 25.5 1.92J 6.18J 13.1
CD-1d 5-Nov-13 42,000 3,000 700 104,000 35.0J 0.86J 4.34J 1.13J 1.90J 812 46.2 17.1JB 10.8B
CD-1d 6-May-14 46,000 2,900 119,000 1.14J 37.8J 0.07J 0.05J 3.22JB 1.16J 7.34J 0.81J 1,610B 49.6B 2.74J 0.12J 6.16J 9.41JB
CD-1d 4-Nov-14 43,000 3,100 0 101,000 43.1J 0.16J 0.11J 2.25J 9.09J 0.87J 3,400 88.5 2.88J 10.2JB 10.7
CD-1d 5-May-15 44,000 2,900 0 <5000 115,000 34.5JB 0.84J 3.63J 0.39J 1,320 32.5 1.42J 5.18J 3.68JB
CD-1d 27-Oct-15 46,000 2,900 0 120,000 0.42J 42.3J 0.13J 1.87J 2.15J 8.18J 0.97J 3,170 87.4 2.49J 4.37CN,J 0.06J 10.9J 14.0B-01
CD-1d 17-May-16 96,000 18,000 0 <50 14,000J 202,000 81.3J 0.46J 4.86J 7.42J 26.0 3.13J 12,000 287 7.11J 2.11J 0.07J 29.3 29.7
13-02
13-02
North Carolina 2L or Groundwater
Protection Standard
Solid Waste Section Limit
MetalsGeneral Chemistry
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Page 1 of 7 July 2016
Table 3a
Detected Groundwater Constituents - General Chemistry and Metals
May 2016 Semi-Annual Sampling Event
Cabarrus County C&D Landfill
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NE NE 250,000 NE 10,000 250,000 500,000 1*10 700 4*2 10 1*1,000 15 300 50 1 100 20 20 0.2*0.3*1,000
NE NE NE NE 10,000 250,000 NE 6 10 100 1 1 10 10 10 10 300 50 0.2 50 10 10 5.5 25 10
13-02
North Carolina 2L or Groundwater
Protection Standard
Solid Waste Section Limit
MetalsGeneral Chemistry
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CD-2 25-Sep-06
CD-2 1-Nov-06
CD-2 24-Apr-07 35J 0.02J 1.1J 3.6J 1.5J 0.86J 2.6J
CD-2 29-Oct-07 48J 0.01J 3J 4.9J 2.6J 1.1J 2.7J
CD-2 23-Apr-08 33J 0.34J 0.93J 1.0J 2.7J 0.12J 0.12J
CD-2 18-Nov-08 46.7J 0.04J 3.0J
CD-2 9-Apr-09 25J 0.01J 0.32J
CD-2 13-Oct-09 31.9J 1.37J
CD-2 11-May-10 11,000 7,800 990J 98,000 1.73J 48.8J 3.99J 3.43J 1.32J 2,290 99 2.86J 8.83J 9.40J
CD-2 3-Nov-10 17,300 6,900 2,100J 1.49J 48.1J 0.22J 2.77J 3.58J 5.69J 2.06J 5,030 103 0.026J 2.96J 21.4J 9.90J
CD-2 3-May-11 2,850 6,800 1,300J 209,000 1.78J 55.9J 0.23J 3.04JB 3.62J 7.91J 2.75J 5,560 92.2 0.031J 3.60J 22.2J 12B
CD-2 8-Nov-11 9,000 7,500 1,400J 41,500 22.1J 0.21JB 1.41J 2.15J 3.53J 1.07J 1,660 47.4 1.9J 4.99J
CD-2 7-May-12 21,000 7,200 104,000 36.4J 0.19J 2.71J 3.38J 5.03J 1.94J 2,760 74.1 2.95J 9.8J 16.5B
CD-2 28-Nov-12 25,000 6,700 (1)39.5J 0.13J 2.89J 2.95J 4.40J 1.42J 2,720 67.2 2.72J 10.1J 7.92J
CD-2 7-May-13 20,000 7,200 80,000 0.34J 1.25JB 39.4J 0.23J 1.32J 2.8J 4.44J 1.34J 2,450 57.8 2.59J 0.08J 9.02J 8.79J
CD-2 5-Nov-13 28,000 6,600 55,000 45.1J 0.20J 0.64J 3.31J 4.01J 1.60J 1,600 68.8 0.087J 2.38J 14J 7.77JB
CD-2 7-May-14 16,000 8,200 135,000 37.5J 0.10J 1.98JB 2.48J 2.26J 0.78JB 1,130B 49.3 0.105J 2.00J 5.00J
CD-2 5-Nov-14 25,000 7,500 330,000 0.07J 46.0J 2.21JB 2.69J 3.59J 1.10J 2,000B 59.6 (1)2.47J 7.23J 6.92JB
CD-2 6-May-15 16,000 8,100 136,000 52.0JB 0.18J 2.10JB 2.90J 5.91J 1.37J 2240 57.6 0.158JB 3.74J 6.97J 8.02JB
CD-2 27-Oct-15 7,750 7,300 5,900J 178,000 0.83J 60.0J 0.42J 3.94B-01,J 3.71J 8.71J 2.67J 5,150 83.8 0.073J 5.50J 4.05CN,J 0.08J 16.3J 13.3
CD-2 18-May-16 20,000 7,900 <5,000 147,000 49.8J 0.22J 2.32J 3.41J 3.56J 1.20J 2,350 71.7 0.189J 2.68J 8.34J 7.62J
CD-3 26-Sep-06 175 190
CD-3 1-Nov-06
CD-3 24-Apr-07 38J 0.01J 2.0J 0.83J 2.7J 0.44J 2.5J 1.1J
CD-3 29-Oct-07 667J 0.19J 0.04J 3.9J 3.9J 10 1.5J 3.1J 1.4J
CD-3 23-Apr-08 46J 0.03J 1.1J 0.79J 0.12J 0.12J
CD-3 18-Nov-08 121 0.05J 0.74J 1.75J
CD-3 9-Apr-09 41.7J 0.12J 0.84J 0.02J 0.02J
CD-3 13-Oct-09 47.3J 0.90J
CD-3 11-May-10 95,000 3,800 2,700 168,000 35.5J 0.49J 2.51J 0.32J 680 19.8 1.36J 5.79J
CD-3 3-Nov-10 84,600 4,100 2,700J 0.63J 33.3J 0.03J 0.74J 3.67J 0.44J 1,160 28.3 0.09J 1.68J 5.99J 5.59J
CD-3 3-May-11 105,000 4,300 3,200J 404,000 48.9J 0.11J 2.36J 7.57J 1.30J 3,580 93.6 2.48J 12.2J 8.64JB
CD-3 8-Nov-11 85,000 5,400 3,900J 144,000 25.5J 0.65J 1.01J 178 24.9 1.48J 5.16J
CD-3 7-May-12 75,000 4,500 177,000 41.7J 0.84J 1.27J 3.84J 0.54J 1,170 32.6 3.37J 6.18J 6.81J,B
CD-3 28-Nov-12 104,000 5,100 (1)46.7J 1.41J 1.90J 4.35J 0.82J 1,740 68.9 1.86J 9.52J 6.93J
CD-3 7-May-13 122,000 4,800 181,000 33.8J 1.20J 2.35J 0.42J 880 56.3 1.41J 5.86J 2.89J
CD-3 5-Nov-13 59,000 4,500 121,000 64J 0.21J 0.74J 3.47J 10.6 2.06J 5,170 139 3.25J 21.2J 12.2B
CD-3 7-May-14 61,600 4,200 127,000 28.7J 1.66JB 0.72J 83.2B 4.4J 1.14J 2.42J
CD-3 5-Nov-14 82,000 13,000 13,000J 425,000 162 0.14J 1.85JB 3.00J 6.22J 1.21J 3,770B 1,030 (1)8.65J 12.9J 9.94JB
CD-3 6-May-15 89,000 13,000 22,000J 280,000 1.38J 159 0.11J 1.26J 2.84J 0.42J 1,230B 1,090 0.102JB 7.25J 5.29J 5.93J
CD-3 27-Oct-15 95,000 13,000 23,000J 255,000 155 0.10J 1.02B-01,J 1.82J 3.91J 0.68J 2,010 936 7.72J 2.60CN,J 6.03J 6.81J
CD-3 18-May-16 100,000 14,000 26,000J 311,000 194 0.12J 1.60J 1.35J 0.24J 607 1,010 7.88J 1.19J 4.02J 3.73J
13-02
13-02
Page 2 of 7 July 2016
Table 3a
Detected Groundwater Constituents - General Chemistry and Metals
May 2016 Semi-Annual Sampling Event
Cabarrus County C&D Landfill
Alk
a
l
i
n
i
t
y
Ch
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m
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c
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l

O
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g
e
n

D
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a
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Ch
l
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Fe
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o
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s

I
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n
Ni
t
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a
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Su
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To
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D
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S
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An
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Ar
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Ba
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Be
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Co
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Ni
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Sil
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Th
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Va
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Zin
c
NE NE 250,000 NE 10,000 250,000 500,000 1*10 700 4*2 10 1*1,000 15 300 50 1 100 20 20 0.2*0.3*1,000
NE NE NE NE 10,000 250,000 NE 6 10 100 1 1 10 10 10 10 300 50 0.2 50 10 10 5.5 25 10
13-02
North Carolina 2L or Groundwater
Protection Standard
Solid Waste Section Limit
MetalsGeneral Chemistry
Sa
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Mo
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CD-4 Rep 4-Nov-10 86,300 6,100 1,570 16,000J 136 5.62J 8.37J 0.84J 5.90J 16.3J 2.31J
CD-4 Rep 3-May-11 124,000 9,700 160J `206 0.9JB 17.6 0.62J 8.39J 2.72JB
CD-4 Rep (dup)3-May-11 0.21J 206 17.9 0.68J 8.98J 0.17J 2.85J
CD-4 Rep 8-Nov-11 0.14J 191 0.93J 18.2 1.00J 8.86J 9.44J
CD-4 Rep 9-May-12 184 1.69J 18.1 1.70J 0.17J 11.3J 3.03J 16.1B
CD-4 Rep 29-Nov-12 172 13.7 0.62J 7.03J 2.84J 2.14JB
CD-4 Rep 10-May-13 75.5J 0.5J 2.71J 7.87J 1.94J 0.88J 11.2J 11.1J 10.3
CD-4 Rep 7-Nov-13 1.36J 60.4J 0.35J 0.07J 0.77J 5.31J 1.83J 0.57J 5.11J 0.13J 32 4.40JB
CD-4 Rep 7-May-14 62.4J 0.31J 0.05J 3.25JB 5.02J 1.70J 0.32J 6.52J 22.2J 2.97JB
CD-4 Rep 5-Nov-14 70.0J 0.31J 2.59J 1.46J 0.72J 4.29J 14.8JB 6.85J
CD-4 Rep 6-May-15 58.4J 0.39J 1.13J 5.94J 1.90J 0.53J 4.72J 14.0J 2.99J
CD-4 Rep 27-Oct-15 0.79J 57.9J 0.32J 2.18J 5.86J 8.95J 1.26J 10.7J 4.14CN,J 13.9J 8.34B-01,J
CD-4 Rep 18-May-16 1.09J 56.2J 0.46J 1.24J 7.31J 1.02J 0.66J 5.43J 18.0J 3.70J
CD-7 1-Jul-14 66,000 7,600 15,000J 420,000 53.1J 0.131J 669 8.74J 4.11J 4.06J
CD-7 5-Nov-14 77,000 8,500 18,000J 1,170,000 1.32J 118 3.74 15.1B 3.71J 40.0 13.6 21,100B 341 (1)8.91J 0.24J 75.8 19.4B
CD-7 6-May-15 86,000 9,800 25,000J 660,000 1.71J 66.8J 0.28J 0.45J 4.36J 0.86J 1,630B 43.4 3.36J 4.14J 3.33J
CD-7 27-Oct-15 81,000 11,000 28,000J 291,000 87.2J 1.12 5.33B-01,J 1.52J 16.6 4.69J 6,560 145 0.138J 6.61J 3.81CN,J 23.4J 11.3
CD-7 18-May-16 90,000 10,000 29,000J 282,000 74.8J 0.43J 2.18J 0.36J 4.74J 1.20J 2,160 59.4 0.164J 4.90J 10.2J 4.03J
CD-8 1-Jul-14 75,000 3,900 3,700J 120,000 0.256J 421 0.191J 14.4 12.6 78 6.55J 26,600 1,360 13.8J 0.238J 93.3 79.6
CD-8 5-Nov-14 86,000 3,500 253,000 83.4J 1.64JB 1.20J 7.15J 0.59J 2,360B 131 (1)3.34J 8.18J 11.0B
CD-8 6-May-15 57,000 3,300 <5000 138,000 0.36J 53.8JB 0.48J 4.13J 0.27J 1,030 58.5 0.095JB 2.43J 4.03J 9.73JB
CD-8 27-Oct-15 72,000 3,600 1,100J 132,000 0.75J 1.79J 162 0.32J 0.21J 5.88B-01,J 1.90J 38.6 2.29J 2,960 95.2 9.53J 3.65CN,J 11.2J 1,430
CD-8 (dup)27-Oct-15 70,000 3,500 130,000 0.40J 1.72J 160 0.33J 0.21J 5.54B-01,J 1.80J 36.3 2.12J 2,630 82.4 8.69J 4.20CN,J 10.6J 1,310
CD-8 19-May-16 115,000 2,000 <5,000 205,000 0.49J 1.52J 133 0.20J 3.54J 1.40J 28.1 1.28J 2,320 123 8.72J 13.2J 1,250
CD-8 (dup)19-May-16 110,000 2,000 <5,000 215,000 1.27J 1.55J 136 0.23J 0.10J 4.41J 1.63J 31.2 1.87J 3,230 129 9.76J 14.8J 1,600
Notes:
1. All units are in micrograms per liter (parts per billion).
2. * - Groundwater Protection Standard
3. NE - Standard Not Established; dup - Duplicate Sample
4. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit.
6. CN - Detected silver concentrations were determined to be the result of contamination from the preservative acid used.
7. CD-4 Rep was installed as part of the proposed Phase 1 C&D Landfill expansion in January 2009. Beginning November 2011 samples collected from CD-4 Rep are only analyzed for Appendix I metals.
8. Alkalinity, chloride, ferrous iron, sulfate, and total dissolved solids were added to the sampling program in May 2010.
9. (1) - Not analyzed due to laboratory oversight.
10. CD-3 was relocated on July 1, 2014, as part of the Phase 2 C&D Landfill expansion.
11. CD-7 and -8 (formerly piezometers B-7 and -19) were added to the monitoring program in July 2014 as part of the Phase 2 C&D Landfill expansion.
12. Ferrous iron results for CD-1s and -1d are based on field testing and results for CD-4 Rep are laboratory derived.
- Concentration exceeds the 15A NCAC 02L .0202 or Groundwater Protection Standard
- Indicates the result is below the detection limit or not analyzed
13-02
5. B, B-01 - The analyte concentration detected in the method blank was greater than the method detection limit.
13-02
13-02
Page 3 of 7 July 2016
Table 3b
Detected Groundwater Constituents - Volatile Organic Compounds
May 2016 Semi-Annual Sampling Event
Cabarrus County C&D Landfill
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6,000 1 4 4,000 50 3,000 200 20 6 6 0.4 7 0.6 70 100 5 1,000 600 2,000 3 0.7 3 500 0.03 700 NE
100 1 3 100 3 10 1 5 1 5 1 5 1 5 5 1 5 1 1 1 1 1 5 1 100 NE
CD-1s 25-Sep-06
CD-1s 31-Oct-06
CD-1s 23-Apr-07
CD-1s 29-Oct-07
CD-1s 23-Apr-08 0.40J
CD-1s 18-Nov-08 1.1
CD-1s 8-Apr-09
CD-1s 13-Oct-09
CD-1s 11-May-10
CD-1s 2-Nov-10
CD-1s 3-May-11
CD-1s 8-Nov-11
CD-1s 7-May-12
CD-1s 27-Nov-12 0.4J 0.2J
CD-1s 7-May-13
CD-1s 5-Nov-13
CD-1s 6-May-14
CD-1s 4-Nov-14
CD-1s 5-May-15
CD-1s 27-Oct-15
CD-1s 17-May-16
CD-1d 4-Oct-06
CD-1d 31-Oct-06
CD-1d 23-Apr-07
CD-1d 29-Oct-07
CD-1d 23-Apr-08 0.43J
CD-1d 18-Nov-08 1.2
CD-1d 8-Apr-09
CD-1d 13-Oct-09
CD-1d 11-May-10
CD-1d 2-Nov-10
CD-1d 3-May-11
CD-1d 8-Nov-11
CD-1d 7-May-12
CD-1d 27-Nov-12
CD-1d 7-May-13
CD-1d 5-Nov-13
CD-1d 6-May-14
CD-1d 4-Nov-14
CD-1d 5-May-15
CD-1d 27-Oct-15
CD-1d 17-May-16
13-02
North Carolina 2L Standard
Solid Waste Section Limit
13-02
Page 4 of 7 July 2016
Table 3b
Detected Groundwater Constituents - Volatile Organic Compounds
May 2016 Semi-Annual Sampling Event
Cabarrus County C&D Landfill
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6,000 1 4 4,000 50 3,000 200 20 6 6 0.4 7 0.6 70 100 5 1,000 600 2,000 3 0.7 3 500 0.03 700 NE
100 1 3 100 3 10 1 5 1 5 1 5 1 5 5 1 5 1 1 1 1 1 5 1 100 NE
13-02
North Carolina 2L Standard
Solid Waste Section Limit
CD-2 25-Sep-06
CD-2 31-Oct-06
CD-2 23-Apr-07
CD-2 29-Oct-07
CD-2 22-Apr-08 0.57J 0.29J 0.34J
CD-2 18-Nov-08 1.2B
CD-2 8-Apr-09
CD-2 13-Oct-09
CD-2 11-May-10
CD-2 2-Nov-10
CD-2 3-May-11
CD-2 8-Nov-11
CD-2 7-May-12
CD-2 27-Nov-12 0.4J
CD-2 7-May-13
CD-2 5-Nov-13
CD-2 6-May-14
CD-2 4-Nov-14
CD-2 7-May-15
CD-2 27-Oct-15
CD-2 17-May-16
CD-3 26-Sep-06 1
CD-3 31-Oct-06
CD-3 23-Apr-07
CD-3 29-Oct-07
CD-3 22-Apr-08 0.32J 0.35J
CD-3 18-Nov-08 1.2B
CD-3 8-Apr-09
CD-3 13-Oct-09 0.5J
CD-3 11-May-10
CD-3 2-Nov-10
CD-3 3-May-11
CD-3 8-Nov-11 16J
CD-3 7-May-12
CD-3 27-Nov-12 0.4J
CD-3 7-May-13
CD-3 5-Nov-13
CD-3 6-May-14
CD-3 4-Nov-14
CD-3 6-May-15 2.4J
CD-3 27-Oct-15 1.6J
CD-3 17-May-16 0.6J 2.1J
13-02
13-02
Page 5 of 7 July 2016
Table 3b
Detected Groundwater Constituents - Volatile Organic Compounds
May 2016 Semi-Annual Sampling Event
Cabarrus County C&D Landfill
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6,000 1 4 4,000 50 3,000 200 20 6 6 0.4 7 0.6 70 100 5 1,000 600 2,000 3 0.7 3 500 0.03 700 NE
100 1 3 100 3 10 1 5 1 5 1 5 1 5 5 1 5 1 1 1 1 1 5 1 100 NE
13-02
North Carolina 2L Standard
Solid Waste Section Limit
CD-4 Rep 4-Nov-10
CD-4 Rep 3-May-11
CD-4 Rep (dup)3-May-11
CD-4 Rep 8-Nov-11
CD-4 Rep 8-May-12
CD-4 Rep 28-Nov-12 0.3J
CD-4 Rep 9-May-13
CD-4 Rep 7-Nov-13 0.6J
CD-4 Rep 6-May-14
CD-4 Rep 4-Nov-14
CD-4 Rep 6-May-15
CD-4 Rep 27-Oct-15
CD-4 Rep 17-May-16
CD-7 (B-7)22-Mar-12
CD-7 (B-7)3-May-12 0.65J 0.67J
CD-7 1-Jul-14
CD-7 4-Nov-14
CD-7 6-May-15 0.4J
CD-7 27-Oct-15 0.4J 0.5J
CD-7 17-May-16 0.7J 1.0J 1.9J
CD-8 (B-19)22-Jan-09 0.22J 3.34J 2.84J 0.89J 1.21 2.2 1.21
CD-8 (B-19)22-Mar-12 1.13 2.24 1.03
CD-8 (B-19)3-May-12 0.18J 0.80J 1.51 0.90J
CD-8 1-Jul-14 3.2J 0.57J 1.5 0.45J
CD-8 4-Nov-14 0.8J
CD-8 6-May-15 0.5J
CD-8 27-Oct-15 0.6J
CD-8 (dup)27-Oct-15 0.5J
CD-8 18-May-16
CD-8 (dup)18-May-16
Notes:
1. All units are in micrograms per liter (parts per billion).
2. dup - Duplicate Sample
3. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit.
5. NE - Standard Not Established
7. CD-3 was relocated on July 1, 2014, as part of the Phase 2 C&D Landfill expansion.
8. CD-7 and -8 (formerly piezometers B-7 and -19) were added to the monitoring program in July 2014 as part of the Phase 2 C&D Landfill expansion.
- Concentration exceeds the 15A NCAC 02L .0202 or Groundwater Protection Standard
- Indicates the result is below the detection limit
13-02
13-02
6. CD-4 Rep was installed as part of the proposed Phase 1 C&D Landfill expansion in January 2009.
4. B - The analyte concentration detected in the method blank was greater than the method detection limit.
13-02
Page 6 of 7 July 2016
Table 3c
Detected Surface Water Constituents - Metals, Volatile Organic Compounds, and General Chemistry
May 2016 Semi-Annual Sampling Event
Cabarrus County C&D Landfill
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640*10*200,000*6.5**0.15**24**4*2.7**NS 0.54**NS 0.012**16**5**0.06**0.47*NS 36**2,000**51*140**100**NS NS 230**NS NS
6 10 100 1 1 10 10 10 300 10 50 0.2 50 10 10 5.5 25 10 100 1 3 1 NE 1 NE 250 NE
SW-3 9-Nov-11
SW-3 9-May-12
SW-3 29-Nov-12
SW-3 10-May-13 0.27J 152 2.23J 3.07J 4.30J 996 0.49J 887B 4.68J 0.10J 3.01J 33.4 60 20 240J 482
SW-3 5-Nov-13
SW-3 6-May-14 7.70J 301 2.41 0.22J 30.1B 58.3 39.9 67,600B 21.4B 9,250 29.4J 3.71J 0.23J 101 354 22J 8.5J 530 71 440 1,430
SW-3 4-Nov-14
SW-3 5-May-15
SW-3 27-Oct-15
SW-3 19-May-16 11.1 200 5.95 38.1 17.1 22.4 59,700 48.1 576 15.5J 18.0 0.31J 180 85.3 5.6J 25 3.2 47J 908H-02
Notes:
1. Metal and volatile organic compound concentrations are in micrograms per liter (parts per billion).
2. General chemistry concentrations are in milligrams per liter (parts per million).
3. Standards obtained from section 15A NCAC 02B .0211 (North Carolina 2B) Surface Water Standards for Class C Waters (June 2016).
4. * - Human Health Standard
5. ** - Freshwater Aquatic Life
6. NS - No Standard; NE - Not Established
7. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit.
- Concentration exceeds the North Carolina 2B Human Health or Freshwater Aquatic Life Standard for Class C Waters.
- Blank cell indicates the analyte was not detected
9. H-02 - Total dissolved solids analysis was analyzed outside of hold time for SW-3.
DRY
13-02
DRY
DRY
DRY DRY DRY
8. B - The analyte concentration detected in the method blank was greater than the method detection limit.
DRY
DRY DRY
DRY
DRY
Solid Waste Section Limit
DRY
DRY
DRYDRY
DRYDRY
DRY
General ChemistryMetalsVolatile Organic Compounds
DRYDRY
Facility
Permit
Number
Surface
Water Code
Sample
Date
DRY
North Carolina 2B
Human Health or Freshwater Aquatic
Life Standard
Page 7 of 7 July 2016

Appendix A 
PACE ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
Camp Dresser & McKee Inc. - Raleigh
Project: Cabarrus Co - C&D
Raleigh, NC 27612
5400 Glenwood Ave., Suite 300
Mr. Mat Colone
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the
client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Pace Analytical Services, Inc. certifies
that the following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the
samples analyzed.
Laboratory Report
Project #:[none]
Prepared For:
Attention:
June 09, 2016
Report Number:AZE0546
Approved:
This report may not be reproduced, except in full, without written approval from Analytical Services, Inc.Page 1 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
1302-CD1S AZE0546-01 05/17/16 08:59 05/18/16 12:45Ground Water
1302-CD1D AZE0546-02 05/17/16 10:14 05/18/16 12:45Ground Water
1302-CD2 AZE0546-03 05/17/16 08:59 05/19/16 09:30Ground Water
1302-CD2 AZE0546-04 05/18/16 08:20 05/19/16 09:30Ground Water
1302-CD3 AZE0546-05 05/17/16 10:27 05/19/16 09:30Ground Water
1302-CD3 AZE0546-06 05/18/16 08:46 05/19/16 09:30Ground Water
1302-CD7 AZE0546-07 05/17/16 09:57 05/19/16 09:30Ground Water
1302-CD7 AZE0546-08 05/18/16 08:52 05/19/16 09:30Ground Water
1302-CD8 AZE0546-09 05/18/16 11:19 05/19/16 15:05Ground Water
1302-CD8 AZE0546-10 05/19/16 08:23 05/19/16 15:05Ground Water
1302-Duplicate AZE0546-11 05/18/16 00:00 05/19/16 15:05Ground Water
1302-Duplicate AZE0546-12 05/19/16 00:00 05/19/16 15:05Ground Water
1302-SW3 AZE0546-13 05/19/16 08:36 05/19/16 15:05Surface Water
1302-Trip Blank AZE0546-14 05/16/16 00:00 05/19/16 15:05Water
Page 2 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Total Dissolved Solids Analysis by Standard Method 2540C (H-02 Qualifier):
Due to a miscommunication between analyst and Project Manager, sample AZE0546-13 (1302-SW3) was analyzed outside the method-recommended holding time of 7 days.
The TDS analysis was performed in duplicate; the data was consistent with history for that sampling point and the relative percent difference between the duplicate values was
good. Data does not seem to be impacted by the missed holding time.
Case Narrative
Page 3 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte
SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD1S
Ground Water
AZE0546-01 AZE054605/17/16 08:59
Project:Cabarrus Co - C&D
05/18/16 12:45
On Site
EPA 9050A 103 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 08:5905/17/16 08:59
SM 4500-O G 3450 ug/L1Dissolved Oxygen 0.0 6050530NA0.0 NA 05/17/16 08:5905/17/16 08:59
NDNA ug/L1Field - Ferrous Iron 200 6050530NA200FE205/17/16 08:5905/17/16 08:59
EPA 9040C 5.91 pH Units1Field - pH 6050530NAPH05/17/16 08:5905/17/16 08:59
NA 245 mV1Field - Redox 6050530NAREDOX05/17/16 08:5905/17/16 08:59
SM 2550 B 15.7 °C1Field - Temperature 6050530NATEMP05/17/16 08:5905/17/16 08:59
EPA 180.1 3.63 NTU1Field - Turbidity 0.10 6050530NA0.10 TURB 05/17/16 08:5905/17/16 08:59
NA 23.90 feet1Field - Water Level 6050530NAWL05/17/16 08:5905/17/16 08:59
NA 29.62 feet1Field - Well Depth 6050530NA05/17/16 08:5905/17/16 08:59
General Chemistry
SM 2320 B 43000 ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
NDSM 5210 B ug/L1Biochemical Oxygen Demand 2000 6050434SM 5210 B 2000 E-10106 05/23/16 11:1505/18/16 17:15
NDSM 5220 D ug/L1Chemical Oxygen Demand 10000 6050509SM 5220 D 10000 E-10117 05/23/16 13:1005/21/16 10:15
NDSM 4500-S D ug/L1Total Sulfide 200 6050561SM 4500-S D 200 18496-25-8 05/24/16 09:3005/24/16 09:30
SM 2540 C 130000 ug/L1Total Dissolved Solids 10000 6050522SM 2540 C 10000 E-10173 05/23/16 12:0005/23/16 12:00
NDEPA 9060A ug/L1Total Organic Carbon 1000 6050505EPA 9060A 1000 E-10195 05/21/16 19:4505/21/16 13:00
Inorganic Anions
EPA 9056A 3700 ug/L1Chloride1000 6050405EPA 300.0 1000 16887-00-6 05/18/16 22:3505/18/16 09:53
EPA 9056A 79 ug/L1Nitrate as N 50 6050405EPA 300.0 50 14797-55-8 05/18/16 22:3505/18/16 09:53
EPA 9056A 1000 ug/L1Sulfate5000 J 6050405EPA 300.0 51 14808-79-8 05/18/16 22:3505/18/16 09:53
Page 4 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD1S
Ground Water
AZE0546-01 AZE054605/17/16 08:59
Project:Cabarrus Co - C&D
05/18/16 12:45
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6050611EPA 3005A 0.25 7440-36-0 05/26/16 14:3205/26/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6050611EPA 3005A 0.75 7440-38-2 05/26/16 14:3205/26/16 08:15
EPA 6020B 29.3 ug/L1Barium100 J 6050611EPA 3005A 0.30 7440-39-3 05/26/16 14:3205/26/16 08:15
NDEPA 6020B ug/L1Beryllium1.00 6050611EPA 3005A 0.09 7440-41-7 05/26/16 14:3205/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 14:3205/26/16 08:15
EPA 6020B 0.94 ug/L1Chromium10.0 J 6050611EPA 3005A 0.43 7440-47-3 05/26/16 14:3205/26/16 08:15
NDEPA 6020B ug/L1Cobalt10.0 6050611EPA 3005A 0.29 7440-48-4 05/26/16 14:3205/26/16 08:15
EPA 6020B 0.99 ug/L1Copper10.0 J 6050611EPA 3005A 0.41 7440-50-8 05/26/16 14:3205/26/16 08:15
EPA 6020B 0.12 ug/L1Lead10.0 J 6050611EPA 3005A 0.08 7439-92-1 05/26/16 14:3205/26/16 08:15
EPA 6020B 1.01 ug/L1Nickel50.0 J 6050611EPA 3005A 0.48 7440-02-0 05/26/16 14:3205/26/16 08:15
NDEPA 6020B ug/L1Selenium10.0 6050611EPA 3005A 0.85 7782-49-2 05/26/16 14:3205/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 14:3205/26/16 08:15
NDEPA 6020B ug/L1Thallium5.50 6050611EPA 3005A 0.06 7440-28-0 05/26/16 14:3205/26/16 08:15
EPA 6020B 4.70 ug/L1Vanadium25.0 J 6050611EPA 3005A 1.57 7440-62-2 05/26/16 14:3205/26/16 08:15
EPA 6020B 1.93 ug/L1Zinc10.0 J 6050611EPA 3005A 1.30 7440-66-6 05/26/16 14:3205/26/16 08:15
EPA 6020A 446 ug/L1Iron40.0 6050611EPA 3005A 5.7 7439-89-6 05/26/16 14:3205/26/16 08:15
EPA 6020A 17.0 ug/L1Manganese10.0 6050611EPA 3005A 1.0 7439-96-5 05/26/16 14:3205/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 16:0206/01/16 15:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050503EPA 5030B 4.9 67-64-1 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6050503EPA 5030B 1.8 107-13-1 05/20/16 18:5405/20/16 12:00
Page 5 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD1S
Ground Water
AZE0546-01 AZE054605/17/16 08:59
Project:Cabarrus Co - C&D
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Benzene1.0 6050503EPA 5030B 0.2 71-43-2 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Bromochloromethane3.0 6050503EPA 5030B 0.7 74-97-5 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050503EPA 5030B 0.6 75-27-4 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Bromoform3.0 6050503EPA 5030B 0.7 75-25-2 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6050503EPA 5030B 0.8 74-83-9 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6050503EPA 5030B 0.6 75-15-0 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050503EPA 5030B 0.6 56-23-5 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6050503EPA 5030B 0.4 108-90-7 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6050503EPA 5030B 0.4 75-00-3 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6050503EPA 5030B 0.3 67-66-3 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6050503EPA 5030B 0.4 74-87-3 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050503EPA 5030B 0.7 124-48-1 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050503EPA 5030B 2.0 96-12-8 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050503EPA 5030B 0.7 106-93-4 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6050503EPA 5030B 0.7 74-95-3 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050503EPA 5030B 0.5 95-50-1 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050503EPA 5030B 0.3 106-46-7 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050503EPA 5030B 1.5 110-57-6 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050503EPA 5030B 0.4 75-34-3 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050503EPA 5030B 0.3 107-06-2 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050503EPA 5030B 0.5 75-35-4 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050503EPA 5030B 0.5 156-59-2 05/20/16 18:5405/20/16 12:00
Page 6 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD1S
Ground Water
AZE0546-01 AZE054605/17/16 08:59
Project:Cabarrus Co - C&D
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050503EPA 5030B 0.4 156-60-5 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050503EPA 5030B 0.5 78-87-5 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050503EPA 5030B 0.4 10061-01-5 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050503EPA 5030B 0.4 10061-02-6 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6050503EPA 5030B 0.2 100-41-4 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6050503EPA 5030B 0.6 74-88-4 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050503EPA 5030B 0.9 591-78-6 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050503EPA 5030B 0.5 75-09-2 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050503EPA 5030B 1.1 78-93-3 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6050503EPA 5030B 1.7 108-10-1 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6050503EPA 5030B 0.4 100-42-5 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050503EPA 5030B 0.6 630-20-6 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050503EPA 5030B 0.5 79-34-5 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050503EPA 5030B 0.4 127-18-4 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6050503EPA 5030B 0.3 108-88-3 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050503EPA 5030B 0.4 71-55-6 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050503EPA 5030B 0.8 79-00-5 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6050503EPA 5030B 0.4 79-01-6 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050503EPA 5030B 0.5 75-69-4 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050503EPA 5030B 0.7 96-18-4 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6050503EPA 5030B 0.8 108-05-4 05/20/16 18:5405/20/16 12:00
Page 7 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD1S
Ground Water
AZE0546-01 AZE054605/17/16 08:59
Project:Cabarrus Co - C&D
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050503EPA 5030B 0.7 75-01-4 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Xylenes, total 5.0 6050503EPA 5030B 0.4 1330-20-7 05/20/16 18:5405/20/16 12:00
NDEPA 8260B ug/L1Tetrahydrofuran10 6050503EPA 5030B 1.5 109-99-9 05/20/16 18:5405/20/16 12:00
EPA 8260B 93 %Surr: Dibromofluoromethane 6050503EPA 5030B 1868-53-7 05/20/16 18:5405/20/16 12:0080-120
EPA 8260B 102 %Surr: 1,2-Dichloroethane-d4 6050503EPA 5030B 17060-07-0 05/20/16 18:5405/20/16 12:0078-120
EPA 8260B 102 %Surr: Toluene-d8 6050503EPA 5030B 2037-26-5 05/20/16 18:5405/20/16 12:0080-120
EPA 8260B 109 %Surr: 4-Bromofluorobenzene 6050503EPA 5030B 460-00-4 05/20/16 18:5405/20/16 12:0080-120
Page 8 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD1D
Ground Water
AZE0546-02 AZE054605/17/16 10:14
Project:Cabarrus Co - C&D
05/18/16 12:45
On Site
EPA 9050A 115 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 10:1405/17/16 10:14
SM 4500-O G 4500 ug/L1Dissolved Oxygen 0.0 6050530NA0.0 NA 05/17/16 10:1405/17/16 10:14
EPA 9040C 6.06 pH Units1Field - pH 6050530NAPH05/17/16 10:1405/17/16 10:14
NA 210 mV1Field - Redox 6050530NAREDOX05/17/16 10:1405/17/16 10:14
SM 2550 B 15.8 °C1Field - Temperature 6050530NATEMP05/17/16 10:1405/17/16 10:14
EPA 180.1 20.0 NTU1Field - Turbidity 0.10 6050530NA0.10 TURB 05/17/16 10:1405/17/16 10:14
NA 26.51 feet1Field - Water Level 6050530NAWL05/17/16 10:1405/17/16 10:14
NA 52.20 feet1Field - Well Depth 6050530NA05/17/16 10:1405/17/16 10:14
General Chemistry
SM 2320 B 96000 ug/L1Alkalinity as CaCO3 1000 6050450SM 2320 B 1000 ALK 05/19/16 10:4005/19/16 10:40
SM 2540 C 202000 ug/L1Total Dissolved Solids 10000 6050522SM 2540 C 10000 E-10173 05/23/16 12:0005/23/16 12:00
Inorganic Anions
EPA 9056A 18000 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 03:5505/25/16 13:58
NDEPA 9056A ug/L1Nitrate as N 50 6050603EPA 9056A 50 14797-55-8 05/26/16 03:5505/25/16 13:58
EPA 9056A 14000 ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 05/26/16 03:5505/25/16 13:58
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6050611EPA 3005A 0.25 7440-36-0 05/26/16 14:3705/26/16 08:15
NDEPA 6020B ug/L1Arsenic10.0 6050611EPA 3005A 0.75 7440-38-2 05/26/16 14:3705/26/16 08:15
EPA 6020B 81.3 ug/L1Barium100 J 6050611EPA 3005A 0.30 7440-39-3 05/26/16 14:3705/26/16 08:15
Page 9 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD1D
Ground Water
AZE0546-02 AZE054605/17/16 10:14
Project:Cabarrus Co - C&D
05/18/16 12:45
Metals, Total
EPA 6020B 0.46 ug/L1Beryllium1.00 J 6050611EPA 3005A 0.09 7440-41-7 05/26/16 14:3705/26/16 08:15
NDEPA 6020B ug/L1Cadmium1.00 6050611EPA 3005A 0.10 7440-43-9 05/26/16 14:3705/26/16 08:15
EPA 6020B 4.86 ug/L1Chromium10.0 J 6050611EPA 3005A 0.43 7440-47-3 05/26/16 14:3705/26/16 08:15
EPA 6020B 7.42 ug/L1Cobalt10.0 J 6050611EPA 3005A 0.29 7440-48-4 05/26/16 14:3705/26/16 08:15
EPA 6020B 26.0 ug/L1Copper10.0 6050611EPA 3005A 0.41 7440-50-8 05/26/16 14:3705/26/16 08:15
EPA 6020B 3.13 ug/L1Lead10.0 J 6050611EPA 3005A 0.08 7439-92-1 05/26/16 14:3705/26/16 08:15
EPA 6020B 7.11 ug/L1Nickel50.0 J 6050611EPA 3005A 0.48 7440-02-0 05/26/16 14:3705/26/16 08:15
EPA 6020B 2.11 ug/L1Selenium10.0 J 6050611EPA 3005A 0.85 7782-49-2 05/26/16 14:3705/26/16 08:15
NDEPA 6020B ug/L1Silver10.0 6050611EPA 3005A 0.22 7440-22-4 05/26/16 14:3705/26/16 08:15
EPA 6020B 0.07 ug/L1Thallium5.50 J 6050611EPA 3005A 0.06 7440-28-0 05/26/16 14:3705/26/16 08:15
EPA 6020B 29.3 ug/L1Vanadium25.0 6050611EPA 3005A 1.57 7440-62-2 05/26/16 14:3705/26/16 08:15
EPA 6020B 29.7 ug/L1Zinc10.0 6050611EPA 3005A 1.30 7440-66-6 05/26/16 14:3705/26/16 08:15
EPA 6020A 12000 ug/L10Iron400 6050611EPA 3005A 57.2 7439-89-6 06/03/16 16:0505/26/16 08:15
EPA 6020A 287 ug/L1Manganese10.0 6050611EPA 3005A 1.0 7439-96-5 05/26/16 14:3705/26/16 08:15
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 16:0406/01/16 15:00
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050503EPA 5030B 4.9 67-64-1 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Acrylonitrile200 6050503EPA 5030B 1.8 107-13-1 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Benzene1.0 6050503EPA 5030B 0.2 71-43-2 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Bromochloromethane3.0 6050503EPA 5030B 0.7 74-97-5 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050503EPA 5030B 0.6 75-27-4 05/20/16 19:1905/20/16 12:00
Page 10 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD1D
Ground Water
AZE0546-02 AZE054605/17/16 10:14
Project:Cabarrus Co - C&D
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 6050503EPA 5030B 0.7 75-25-2 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Bromomethane10 6050503EPA 5030B 0.8 74-83-9 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Carbon Disulfide 100 6050503EPA 5030B 0.6 75-15-0 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050503EPA 5030B 0.6 56-23-5 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Chlorobenzene3.0 6050503EPA 5030B 0.4 108-90-7 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Chloroethane10 6050503EPA 5030B 0.4 75-00-3 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Chloroform5.0 6050503EPA 5030B 0.3 67-66-3 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Chloromethane1.0 6050503EPA 5030B 0.4 74-87-3 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050503EPA 5030B 0.7 124-48-1 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050503EPA 5030B 2.0 96-12-8 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050503EPA 5030B 0.7 106-93-4 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Dibromomethane10 6050503EPA 5030B 0.7 74-95-3 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050503EPA 5030B 0.5 95-50-1 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050503EPA 5030B 0.3 106-46-7 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050503EPA 5030B 1.5 110-57-6 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050503EPA 5030B 0.4 75-34-3 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050503EPA 5030B 0.3 107-06-2 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050503EPA 5030B 0.5 75-35-4 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050503EPA 5030B 0.5 156-59-2 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050503EPA 5030B 0.4 156-60-5 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050503EPA 5030B 0.5 78-87-5 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050503EPA 5030B 0.4 10061-01-5 05/20/16 19:1905/20/16 12:00
Page 11 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD1D
Ground Water
AZE0546-02 AZE054605/17/16 10:14
Project:Cabarrus Co - C&D
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050503EPA 5030B 0.4 10061-02-6 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Ethylbenzene1.0 6050503EPA 5030B 0.2 100-41-4 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Iodomethane10 6050503EPA 5030B 0.6 74-88-4 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050503EPA 5030B 0.9 591-78-6 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050503EPA 5030B 0.5 75-09-2 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050503EPA 5030B 1.1 78-93-3 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6050503EPA 5030B 1.7 108-10-1 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Styrene1.0 6050503EPA 5030B 0.4 100-42-5 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050503EPA 5030B 0.6 630-20-6 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050503EPA 5030B 0.5 79-34-5 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050503EPA 5030B 0.4 127-18-4 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Toluene1.0 6050503EPA 5030B 0.3 108-88-3 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050503EPA 5030B 0.4 71-55-6 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050503EPA 5030B 0.8 79-00-5 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Trichloroethene1.0 6050503EPA 5030B 0.4 79-01-6 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050503EPA 5030B 0.5 75-69-4 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050503EPA 5030B 0.7 96-18-4 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Vinyl Acetate 50 6050503EPA 5030B 0.8 108-05-4 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050503EPA 5030B 0.7 75-01-4 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Xylenes, total 5.0 6050503EPA 5030B 0.4 1330-20-7 05/20/16 19:1905/20/16 12:00
NDEPA 8260B ug/L1Tetrahydrofuran10 6050503EPA 5030B 1.5 109-99-9 05/20/16 19:1905/20/16 12:00
Page 12 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD1D
Ground Water
AZE0546-02 AZE054605/17/16 10:14
Project:Cabarrus Co - C&D
05/18/16 12:45
Volatile Organic Compounds by EPA 8260
EPA 8260B 91 %Surr: Dibromofluoromethane 6050503EPA 5030B 1868-53-7 05/20/16 19:1905/20/16 12:0080-120
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6050503EPA 5030B 17060-07-0 05/20/16 19:1905/20/16 12:0078-120
EPA 8260B 102 %Surr: Toluene-d8 6050503EPA 5030B 2037-26-5 05/20/16 19:1905/20/16 12:0080-120
EPA 8260B 107 %Surr: 4-Bromofluorobenzene 6050503EPA 5030B 460-00-4 05/20/16 19:1905/20/16 12:0080-120
Page 13 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD2
Ground Water
AZE0546-03 AZE054605/17/16 08:59
Project:Cabarrus Co - C&D
05/19/16 09:30
On Site
EPA 9050A 71 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 08:5905/17/16 08:59
SM 4500-O G 3310 ug/L1Dissolved Oxygen 0.0 6050530NA0.0 NA 05/17/16 08:5905/17/16 08:59
EPA 9040C 5.28 pH Units1Field - pH 6050530NAPH05/17/16 08:5905/17/16 08:59
NA 163 mV1Field - Redox 6050530NAREDOX05/17/16 08:5905/17/16 08:59
SM 2550 B 14.9 °C1Field - Temperature 6050530NATEMP05/17/16 08:5905/17/16 08:59
EPA 180.1 800 NTU1Field - Turbidity 0.10 >6050530NA0.10 TURB 05/17/16 08:5905/17/16 08:59
NA 14.00 feet1Field - Water Level 6050530NAWL05/17/16 08:5905/17/16 08:59
NA 25.64 feet1Field - Well Depth 6050530NA05/17/16 08:5905/17/16 08:59
General Chemistry
SM 2320 B 20000 ug/L1Alkalinity as CaCO3 1000 6050491SM 2320 B 1000 ALK 05/20/16 14:0005/20/16 14:00
SM 2540 C 147000 ug/L1Total Dissolved Solids 10000 6050523SM 2540 C 10000 E-10173 05/24/16 18:5005/24/16 18:50
Inorganic Anions
EPA 9056A 7900 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 04:1605/25/16 13:58
NDEPA 9056A ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 05/26/16 04:1605/25/16 13:58
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050513EPA 5030B 4.9 67-64-1 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Acrylonitrile200 6050513EPA 5030B 1.8 107-13-1 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Benzene1.0 6050513EPA 5030B 0.2 71-43-2 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6050513EPA 5030B 0.7 74-97-5 05/23/16 09:3105/23/16 05:30
Page 14 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD2
Ground Water
AZE0546-03 AZE054605/17/16 08:59
Project:Cabarrus Co - C&D
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050513EPA 5030B 0.6 75-27-4 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Bromoform3.0 6050513EPA 5030B 0.7 75-25-2 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Bromomethane10 6050513EPA 5030B 0.8 74-83-9 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6050513EPA 5030B 0.6 75-15-0 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050513EPA 5030B 0.6 56-23-5 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6050513EPA 5030B 0.4 108-90-7 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Chloroethane10 6050513EPA 5030B 0.4 75-00-3 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Chloroform5.0 6050513EPA 5030B 0.3 67-66-3 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Chloromethane1.0 6050513EPA 5030B 0.4 74-87-3 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050513EPA 5030B 0.7 124-48-1 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050513EPA 5030B 2.0 96-12-8 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050513EPA 5030B 0.7 106-93-4 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Dibromomethane10 6050513EPA 5030B 0.7 74-95-3 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050513EPA 5030B 0.5 95-50-1 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050513EPA 5030B 0.3 106-46-7 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050513EPA 5030B 1.5 110-57-6 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050513EPA 5030B 0.4 75-34-3 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050513EPA 5030B 0.3 107-06-2 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050513EPA 5030B 0.5 75-35-4 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.5 156-59-2 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.4 156-60-5 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050513EPA 5030B 0.5 78-87-5 05/23/16 09:3105/23/16 05:30
Page 15 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD2
Ground Water
AZE0546-03 AZE054605/17/16 08:59
Project:Cabarrus Co - C&D
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-01-5 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-02-6 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6050513EPA 5030B 0.2 100-41-4 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Iodomethane10 6050513EPA 5030B 0.6 74-88-4 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050513EPA 5030B 0.9 591-78-6 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050513EPA 5030B 0.5 75-09-2 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050513EPA 5030B 1.1 78-93-3 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6050513EPA 5030B 1.7 108-10-1 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Styrene1.0 6050513EPA 5030B 0.4 100-42-5 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050513EPA 5030B 0.6 630-20-6 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050513EPA 5030B 0.5 79-34-5 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050513EPA 5030B 0.4 127-18-4 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Toluene1.0 6050513EPA 5030B 0.3 108-88-3 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050513EPA 5030B 0.4 71-55-6 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050513EPA 5030B 0.8 79-00-5 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Trichloroethene1.0 6050513EPA 5030B 0.4 79-01-6 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050513EPA 5030B 0.5 75-69-4 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050513EPA 5030B 0.7 96-18-4 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6050513EPA 5030B 0.8 108-05-4 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050513EPA 5030B 0.7 75-01-4 05/23/16 09:3105/23/16 05:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6050513EPA 5030B 0.4 1330-20-7 05/23/16 09:3105/23/16 05:30
Page 16 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD2
Ground Water
AZE0546-03 AZE054605/17/16 08:59
Project:Cabarrus Co - C&D
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Tetrahydrofuran10 6050513EPA 5030B 1.5 109-99-9 05/23/16 09:3105/23/16 05:30
EPA 8260B 91 %Surr: Dibromofluoromethane 6050513EPA 5030B 1868-53-7 05/23/16 09:3105/23/16 05:3080-120
EPA 8260B 100 %Surr: 1,2-Dichloroethane-d4 6050513EPA 5030B 17060-07-0 05/23/16 09:3105/23/16 05:3078-120
EPA 8260B 103 %Surr: Toluene-d8 6050513EPA 5030B 2037-26-5 05/23/16 09:3105/23/16 05:3080-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 6050513EPA 5030B 460-00-4 05/23/16 09:3105/23/16 05:3080-120
Page 17 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD2
Ground Water
AZE0546-04 AZE054605/18/16 08:20
Project:Cabarrus Co - C&D
05/19/16 09:30
On Site
EPA 180.1 64.0 NTU1Field - Turbidity 0.10 6050530NA0.10 TURB 05/18/16 08:2005/18/16 08:20
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6060033EPA 3005A 0.25 7440-36-0 06/03/16 13:4306/02/16 09:30
NDEPA 6020B ug/L1Arsenic10.0 6060033EPA 3005A 0.75 7440-38-2 06/03/16 13:4306/02/16 09:30
EPA 6020B 49.8 ug/L1Barium100 J 6060033EPA 3005A 0.30 7440-39-3 06/03/16 13:4306/02/16 09:30
EPA 6020B 0.22 ug/L1Beryllium1.00 J 6060033EPA 3005A 0.09 7440-41-7 06/03/16 13:4306/02/16 09:30
NDEPA 6020B ug/L1Cadmium1.00 6060033EPA 3005A 0.10 7440-43-9 06/03/16 13:4306/02/16 09:30
EPA 6020B 2.32 ug/L1Chromium10.0 J 6060033EPA 3005A 0.43 7440-47-3 06/03/16 13:4306/02/16 09:30
EPA 6020B 3.41 ug/L1Cobalt10.0 J 6060033EPA 3005A 0.29 7440-48-4 06/03/16 13:4306/02/16 09:30
EPA 6020B 3.56 ug/L1Copper10.0 J 6060033EPA 3005A 0.41 7440-50-8 06/03/16 13:4306/02/16 09:30
EPA 6020B 1.20 ug/L1Lead10.0 J 6060033EPA 3005A 0.08 7439-92-1 06/03/16 13:4306/02/16 09:30
EPA 6020B 2.68 ug/L1Nickel50.0 J 6060033EPA 3005A 0.48 7440-02-0 06/03/16 13:4306/02/16 09:30
NDEPA 6020B ug/L1Selenium10.0 6060033EPA 3005A 0.85 7782-49-2 06/03/16 13:4306/02/16 09:30
NDEPA 6020B ug/L1Silver10.0 6060033EPA 3005A 0.22 7440-22-4 06/03/16 13:4306/02/16 09:30
NDEPA 6020B ug/L1Thallium5.50 6060033EPA 3005A 0.06 7440-28-0 06/03/16 13:4306/02/16 09:30
EPA 6020B 8.34 ug/L1Vanadium25.0 J 6060033EPA 3005A 1.57 7440-62-2 06/03/16 13:4306/02/16 09:30
EPA 6020B 7.62 ug/L1Zinc10.0 J 6060033EPA 3005A 1.30 7440-66-6 06/03/16 13:4306/02/16 09:30
EPA 6020A 2350 ug/L1Iron40.0 6060033EPA 3005A 5.7 7439-89-6 06/03/16 13:4306/02/16 09:30
EPA 6020A 71.7 ug/L1Manganese10.0 6060033EPA 3005A 1.0 7439-96-5 06/03/16 13:4306/02/16 09:30
EPA 7470A 0.189 ug/L1Mercury0.200 J 6060013EPA 7470A 0.132 7439-97-6 06/02/16 16:0606/01/16 15:00
Page 18 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD3
Ground Water
AZE0546-05 AZE054605/17/16 10:27
Project:Cabarrus Co - C&D
05/19/16 09:30
On Site
EPA 9050A 434 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 10:2705/17/16 10:27
SM 4500-O G 2400 ug/L1Dissolved Oxygen 0.0 6050530NA0.0 NA 05/17/16 10:2705/17/16 10:27
EPA 9040C 6.28 pH Units1Field - pH 6050530NAPH05/17/16 10:2705/17/16 10:27
NA 24 mV1Field - Redox 6050530NAREDOX05/17/16 10:2705/17/16 10:27
SM 2550 B 16.8 °C1Field - Temperature 6050530NATEMP05/17/16 10:2705/17/16 10:27
EPA 180.1 403 NTU1Field - Turbidity 0.10 6050530NA0.10 TURB 05/17/16 10:2705/17/16 10:27
NA 38.25 feet1Field - Water Level 6050530NAWL05/17/16 10:2705/17/16 10:27
NA 53.52 feet1Field - Well Depth 6050530NA05/17/16 10:2705/17/16 10:27
General Chemistry
SM 2320 B 100000 ug/L1Alkalinity as CaCO3 1000 6050491SM 2320 B 1000 ALK 05/20/16 14:0005/20/16 14:00
SM 2540 C 311000 ug/L1Total Dissolved Solids 10000 6050523SM 2540 C 10000 E-10173 05/24/16 18:5005/24/16 18:50
Inorganic Anions
EPA 9056A 14000 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 04:3605/25/16 13:58
EPA 9056A 26000 ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 06/01/16 20:1605/25/16 13:58
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050513EPA 5030B 4.9 67-64-1 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Acrylonitrile200 6050513EPA 5030B 1.8 107-13-1 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Benzene1.0 6050513EPA 5030B 0.2 71-43-2 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6050513EPA 5030B 0.7 74-97-5 05/23/16 09:5605/23/16 05:30
Page 19 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD3
Ground Water
AZE0546-05 AZE054605/17/16 10:27
Project:Cabarrus Co - C&D
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050513EPA 5030B 0.6 75-27-4 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Bromoform3.0 6050513EPA 5030B 0.7 75-25-2 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Bromomethane10 6050513EPA 5030B 0.8 74-83-9 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6050513EPA 5030B 0.6 75-15-0 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050513EPA 5030B 0.6 56-23-5 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6050513EPA 5030B 0.4 108-90-7 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Chloroethane10 6050513EPA 5030B 0.4 75-00-3 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Chloroform5.0 6050513EPA 5030B 0.3 67-66-3 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Chloromethane1.0 6050513EPA 5030B 0.4 74-87-3 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050513EPA 5030B 0.7 124-48-1 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050513EPA 5030B 2.0 96-12-8 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050513EPA 5030B 0.7 106-93-4 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Dibromomethane10 6050513EPA 5030B 0.7 74-95-3 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050513EPA 5030B 0.5 95-50-1 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050513EPA 5030B 0.3 106-46-7 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050513EPA 5030B 1.5 110-57-6 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050513EPA 5030B 0.4 75-34-3 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050513EPA 5030B 0.3 107-06-2 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050513EPA 5030B 0.5 75-35-4 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.5 156-59-2 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.4 156-60-5 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050513EPA 5030B 0.5 78-87-5 05/23/16 09:5605/23/16 05:30
Page 20 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD3
Ground Water
AZE0546-05 AZE054605/17/16 10:27
Project:Cabarrus Co - C&D
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-01-5 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-02-6 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6050513EPA 5030B 0.2 100-41-4 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Iodomethane10 6050513EPA 5030B 0.6 74-88-4 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050513EPA 5030B 0.9 591-78-6 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050513EPA 5030B 0.5 75-09-2 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050513EPA 5030B 1.1 78-93-3 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6050513EPA 5030B 1.7 108-10-1 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Styrene1.0 6050513EPA 5030B 0.4 100-42-5 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050513EPA 5030B 0.6 630-20-6 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050513EPA 5030B 0.5 79-34-5 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050513EPA 5030B 0.4 127-18-4 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Toluene1.0 6050513EPA 5030B 0.3 108-88-3 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050513EPA 5030B 0.4 71-55-6 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050513EPA 5030B 0.8 79-00-5 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Trichloroethene1.0 6050513EPA 5030B 0.4 79-01-6 05/23/16 09:5605/23/16 05:30
EPA 8260B 0.6 ug/L1Trichlorofluoromethane1.0 J 6050513EPA 5030B 0.5 75-69-4 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050513EPA 5030B 0.7 96-18-4 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6050513EPA 5030B 0.8 108-05-4 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050513EPA 5030B 0.7 75-01-4 05/23/16 09:5605/23/16 05:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6050513EPA 5030B 0.4 1330-20-7 05/23/16 09:5605/23/16 05:30
Page 21 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD3
Ground Water
AZE0546-05 AZE054605/17/16 10:27
Project:Cabarrus Co - C&D
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
EPA 8260B 2.1 ug/L1Tetrahydrofuran10 J 6050513EPA 5030B 1.5 109-99-9 05/23/16 09:5605/23/16 05:30
EPA 8260B 95 %Surr: Dibromofluoromethane 6050513EPA 5030B 1868-53-7 05/23/16 09:5605/23/16 05:3080-120
EPA 8260B 100 %Surr: 1,2-Dichloroethane-d4 6050513EPA 5030B 17060-07-0 05/23/16 09:5605/23/16 05:3078-120
EPA 8260B 100 %Surr: Toluene-d8 6050513EPA 5030B 2037-26-5 05/23/16 09:5605/23/16 05:3080-120
EPA 8260B 108 %Surr: 4-Bromofluorobenzene 6050513EPA 5030B 460-00-4 05/23/16 09:5605/23/16 05:3080-120
Page 22 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD3
Ground Water
AZE0546-06 AZE054605/18/16 08:46
Project:Cabarrus Co - C&D
05/19/16 09:30
On Site
EPA 180.1 6.29 NTU1Field - Turbidity 0.10 6050530NA0.10 TURB 05/18/16 08:4605/18/16 08:46
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6060033EPA 3005A 0.25 7440-36-0 06/03/16 13:4806/02/16 09:30
NDEPA 6020B ug/L1Arsenic10.0 6060033EPA 3005A 0.75 7440-38-2 06/03/16 13:4806/02/16 09:30
EPA 6020B 194 ug/L1Barium100 6060033EPA 3005A 0.30 7440-39-3 06/03/16 13:4806/02/16 09:30
EPA 6020B 0.12 ug/L1Beryllium1.00 J 6060033EPA 3005A 0.09 7440-41-7 06/03/16 13:4806/02/16 09:30
NDEPA 6020B ug/L1Cadmium1.00 6060033EPA 3005A 0.10 7440-43-9 06/03/16 13:4806/02/16 09:30
NDEPA 6020B ug/L1Chromium10.0 6060033EPA 3005A 0.43 7440-47-3 06/03/16 13:4806/02/16 09:30
EPA 6020B 1.60 ug/L1Cobalt10.0 J 6060033EPA 3005A 0.29 7440-48-4 06/03/16 13:4806/02/16 09:30
EPA 6020B 1.35 ug/L1Copper10.0 J 6060033EPA 3005A 0.41 7440-50-8 06/03/16 13:4806/02/16 09:30
EPA 6020B 0.24 ug/L1Lead10.0 J 6060033EPA 3005A 0.08 7439-92-1 06/03/16 13:4806/02/16 09:30
EPA 6020B 7.88 ug/L1Nickel50.0 J 6060033EPA 3005A 0.48 7440-02-0 06/03/16 13:4806/02/16 09:30
EPA 6020B 1.19 ug/L1Selenium10.0 J 6060033EPA 3005A 0.85 7782-49-2 06/03/16 13:4806/02/16 09:30
NDEPA 6020B ug/L1Silver10.0 6060033EPA 3005A 0.22 7440-22-4 06/03/16 13:4806/02/16 09:30
NDEPA 6020B ug/L1Thallium5.50 6060033EPA 3005A 0.06 7440-28-0 06/03/16 13:4806/02/16 09:30
EPA 6020B 4.02 ug/L1Vanadium25.0 J 6060033EPA 3005A 1.57 7440-62-2 06/03/16 13:4806/02/16 09:30
EPA 6020B 3.73 ug/L1Zinc10.0 J 6060033EPA 3005A 1.30 7440-66-6 06/03/16 13:4806/02/16 09:30
EPA 6020A 607 ug/L1Iron40.0 6060033EPA 3005A 5.7 7439-89-6 06/03/16 13:4806/02/16 09:30
EPA 6020A 1010 ug/L5Manganese50.0 6060033EPA 3005A 5.2 7439-96-5 06/07/16 11:1806/02/16 09:30
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 16:0906/01/16 15:00
Page 23 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD7
Ground Water
AZE0546-07 AZE054605/17/16 09:57
Project:Cabarrus Co - C&D
05/19/16 09:30
On Site
EPA 9050A 317 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 09:5705/17/16 09:57
SM 4500-O G 2020 ug/L1Dissolved Oxygen 0.0 6050530NA0.0 NA 05/17/16 09:5705/17/16 09:57
EPA 9040C 6.16 pH Units1Field - pH 6050530NAPH05/17/16 09:5705/17/16 09:57
NA 40 mV1Field - Redox 6050530NAREDOX05/17/16 09:5705/17/16 09:57
SM 2550 B 15.8 °C1Field - Temperature 6050530NATEMP05/17/16 09:5705/17/16 09:57
EPA 180.1 800 NTU1Field - Turbidity 0.10 >6050530NA0.10 TURB 05/17/16 09:5705/17/16 09:57
NA 39.65 feet1Field - Water Level 6050530NAWL05/17/16 09:5705/17/16 09:57
NA 46.29 feet1Field - Well Depth 6050530NA05/17/16 09:5705/17/16 09:57
General Chemistry
SM 2320 B 90000 ug/L1Alkalinity as CaCO3 1000 6050491SM 2320 B 1000 ALK 05/20/16 14:0005/20/16 14:00
SM 2540 C 282000 ug/L1Total Dissolved Solids 10000 6050523SM 2540 C 10000 E-10173 05/24/16 18:5005/24/16 18:50
Inorganic Anions
EPA 9056A 10000 ug/L2Chloride2000 6050603EPA 9056A 2000 16887-00-6 05/26/16 04:5705/25/16 13:58
EPA 9056A 29000 ug/L2Sulfate10000 6050603EPA 9056A 10000 14808-79-8 05/26/16 04:5705/25/16 13:58
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050513EPA 5030B 4.9 67-64-1 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Acrylonitrile200 6050513EPA 5030B 1.8 107-13-1 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Benzene1.0 6050513EPA 5030B 0.2 71-43-2 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6050513EPA 5030B 0.7 74-97-5 05/23/16 10:2105/23/16 05:30
Page 24 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD7
Ground Water
AZE0546-07 AZE054605/17/16 09:57
Project:Cabarrus Co - C&D
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050513EPA 5030B 0.6 75-27-4 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Bromoform3.0 6050513EPA 5030B 0.7 75-25-2 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Bromomethane10 6050513EPA 5030B 0.8 74-83-9 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6050513EPA 5030B 0.6 75-15-0 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050513EPA 5030B 0.6 56-23-5 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6050513EPA 5030B 0.4 108-90-7 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Chloroethane10 6050513EPA 5030B 0.4 75-00-3 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Chloroform5.0 6050513EPA 5030B 0.3 67-66-3 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Chloromethane1.0 6050513EPA 5030B 0.4 74-87-3 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050513EPA 5030B 0.7 124-48-1 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050513EPA 5030B 2.0 96-12-8 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050513EPA 5030B 0.7 106-93-4 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Dibromomethane10 6050513EPA 5030B 0.7 74-95-3 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050513EPA 5030B 0.5 95-50-1 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050513EPA 5030B 0.3 106-46-7 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050513EPA 5030B 1.5 110-57-6 05/23/16 10:2105/23/16 05:30
EPA 8260B 0.7 ug/L11,1-Dichloroethane 5.0 J 6050513EPA 5030B 0.4 75-34-3 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050513EPA 5030B 0.3 107-06-2 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050513EPA 5030B 0.5 75-35-4 05/23/16 10:2105/23/16 05:30
EPA 8260B 1.0 ug/L1cis-1,2-Dichloroethene 5.0 J 6050513EPA 5030B 0.5 156-59-2 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.4 156-60-5 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050513EPA 5030B 0.5 78-87-5 05/23/16 10:2105/23/16 05:30
Page 25 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD7
Ground Water
AZE0546-07 AZE054605/17/16 09:57
Project:Cabarrus Co - C&D
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-01-5 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-02-6 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6050513EPA 5030B 0.2 100-41-4 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Iodomethane10 6050513EPA 5030B 0.6 74-88-4 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050513EPA 5030B 0.9 591-78-6 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050513EPA 5030B 0.5 75-09-2 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050513EPA 5030B 1.1 78-93-3 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6050513EPA 5030B 1.7 108-10-1 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Styrene1.0 6050513EPA 5030B 0.4 100-42-5 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050513EPA 5030B 0.6 630-20-6 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050513EPA 5030B 0.5 79-34-5 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050513EPA 5030B 0.4 127-18-4 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Toluene1.0 6050513EPA 5030B 0.3 108-88-3 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050513EPA 5030B 0.4 71-55-6 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050513EPA 5030B 0.8 79-00-5 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Trichloroethene1.0 6050513EPA 5030B 0.4 79-01-6 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050513EPA 5030B 0.5 75-69-4 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050513EPA 5030B 0.7 96-18-4 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6050513EPA 5030B 0.8 108-05-4 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050513EPA 5030B 0.7 75-01-4 05/23/16 10:2105/23/16 05:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6050513EPA 5030B 0.4 1330-20-7 05/23/16 10:2105/23/16 05:30
Page 26 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD7
Ground Water
AZE0546-07 AZE054605/17/16 09:57
Project:Cabarrus Co - C&D
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
EPA 8260B 1.9 ug/L1Tetrahydrofuran10 J 6050513EPA 5030B 1.5 109-99-9 05/23/16 10:2105/23/16 05:30
EPA 8260B 95 %Surr: Dibromofluoromethane 6050513EPA 5030B 1868-53-7 05/23/16 10:2105/23/16 05:3080-120
EPA 8260B 99 %Surr: 1,2-Dichloroethane-d4 6050513EPA 5030B 17060-07-0 05/23/16 10:2105/23/16 05:3078-120
EPA 8260B 102 %Surr: Toluene-d8 6050513EPA 5030B 2037-26-5 05/23/16 10:2105/23/16 05:3080-120
EPA 8260B 106 %Surr: 4-Bromofluorobenzene 6050513EPA 5030B 460-00-4 05/23/16 10:2105/23/16 05:3080-120
Page 27 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD7
Ground Water
AZE0546-08 AZE054605/18/16 08:52
Project:Cabarrus Co - C&D
05/19/16 09:30
On Site
EPA 180.1 13.0 NTU1Field - Turbidity 0.10 6050530NA0.10 TURB 05/18/16 08:5205/18/16 08:52
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6060033EPA 3005A 0.25 7440-36-0 06/03/16 13:5306/02/16 09:30
NDEPA 6020B ug/L1Arsenic10.0 6060033EPA 3005A 0.75 7440-38-2 06/03/16 13:5306/02/16 09:30
EPA 6020B 74.8 ug/L1Barium100 J 6060033EPA 3005A 0.30 7440-39-3 06/03/16 13:5306/02/16 09:30
EPA 6020B 0.43 ug/L1Beryllium1.00 J 6060033EPA 3005A 0.09 7440-41-7 06/03/16 13:5306/02/16 09:30
NDEPA 6020B ug/L1Cadmium1.00 6060033EPA 3005A 0.10 7440-43-9 06/03/16 13:5306/02/16 09:30
EPA 6020B 2.18 ug/L1Chromium10.0 J 6060033EPA 3005A 0.43 7440-47-3 06/03/16 13:5306/02/16 09:30
EPA 6020B 0.36 ug/L1Cobalt10.0 J 6060033EPA 3005A 0.29 7440-48-4 06/03/16 13:5306/02/16 09:30
EPA 6020B 4.74 ug/L1Copper10.0 J 6060033EPA 3005A 0.41 7440-50-8 06/03/16 13:5306/02/16 09:30
EPA 6020B 1.20 ug/L1Lead10.0 J 6060033EPA 3005A 0.08 7439-92-1 06/03/16 13:5306/02/16 09:30
EPA 6020B 4.90 ug/L1Nickel50.0 J 6060033EPA 3005A 0.48 7440-02-0 06/03/16 13:5306/02/16 09:30
NDEPA 6020B ug/L1Selenium10.0 6060033EPA 3005A 0.85 7782-49-2 06/03/16 13:5306/02/16 09:30
NDEPA 6020B ug/L1Silver10.0 6060033EPA 3005A 0.22 7440-22-4 06/03/16 13:5306/02/16 09:30
NDEPA 6020B ug/L1Thallium5.50 6060033EPA 3005A 0.06 7440-28-0 06/03/16 13:5306/02/16 09:30
EPA 6020B 10.2 ug/L1Vanadium25.0 J 6060033EPA 3005A 1.57 7440-62-2 06/03/16 13:5306/02/16 09:30
EPA 6020B 4.03 ug/L1Zinc10.0 J 6060033EPA 3005A 1.30 7440-66-6 06/03/16 13:5306/02/16 09:30
EPA 6020A 2160 ug/L1Iron40.0 6060033EPA 3005A 5.7 7439-89-6 06/03/16 13:5306/02/16 09:30
EPA 6020A 59.4 ug/L1Manganese10.0 6060033EPA 3005A 1.0 7439-96-5 06/03/16 13:5306/02/16 09:30
EPA 7470A 0.164 ug/L1Mercury0.200 J 6060013EPA 7470A 0.132 7439-97-6 06/02/16 16:1106/01/16 15:00
Page 28 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD8
Ground Water
AZE0546-09 AZE054605/18/16 11:19
Project:Cabarrus Co - C&D
05/19/16 15:05
On Site
EPA 9050A 262 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/18/16 11:1905/18/16 11:19
SM 4500-O G 3010 ug/L1Dissolved Oxygen 0.0 6050530NA0.0 NA 05/18/16 11:1905/18/16 11:19
EPA 9040C 7.48 pH Units1Field - pH 6050530NAPH05/18/16 11:1905/18/16 11:19
NA 82 mV1Field - Redox 6050530NAREDOX05/18/16 11:1905/18/16 11:19
SM 2550 B 17.4 °C1Field - Temperature 6050530NATEMP05/18/16 11:1905/18/16 11:19
EPA 180.1 800 NTU1Field - Turbidity 0.10 >6050530NA0.10 TURB 05/18/16 11:1905/18/16 11:19
NA 31.98 feet1Field - Water Level 6050530NAWL05/18/16 11:1905/18/16 11:19
NA 43.34 feet1Field - Well Depth 6050530NA05/18/16 11:1905/18/16 11:19
General Chemistry
SM 2320 B 115000 ug/L1Alkalinity as CaCO3 1000 6050491SM 2320 B 1000 ALK 05/20/16 14:0005/20/16 14:00
SM 2540 C 205000 ug/L1Total Dissolved Solids 10000 6050523SM 2540 C 10000 E-10173 05/24/16 18:5005/24/16 18:50
Inorganic Anions
EPA 9056A 2000 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 05:1805/25/16 13:58
NDEPA 9056A ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 05/26/16 05:1805/25/16 13:58
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050513EPA 5030B 4.9 67-64-1 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Acrylonitrile200 6050513EPA 5030B 1.8 107-13-1 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Benzene1.0 6050513EPA 5030B 0.2 71-43-2 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6050513EPA 5030B 0.7 74-97-5 05/23/16 10:4705/23/16 05:30
Page 29 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD8
Ground Water
AZE0546-09 AZE054605/18/16 11:19
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050513EPA 5030B 0.6 75-27-4 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Bromoform3.0 6050513EPA 5030B 0.7 75-25-2 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Bromomethane10 6050513EPA 5030B 0.8 74-83-9 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6050513EPA 5030B 0.6 75-15-0 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050513EPA 5030B 0.6 56-23-5 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6050513EPA 5030B 0.4 108-90-7 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Chloroethane10 6050513EPA 5030B 0.4 75-00-3 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Chloroform5.0 6050513EPA 5030B 0.3 67-66-3 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Chloromethane1.0 6050513EPA 5030B 0.4 74-87-3 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050513EPA 5030B 0.7 124-48-1 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050513EPA 5030B 2.0 96-12-8 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050513EPA 5030B 0.7 106-93-4 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Dibromomethane10 6050513EPA 5030B 0.7 74-95-3 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050513EPA 5030B 0.5 95-50-1 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050513EPA 5030B 0.3 106-46-7 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050513EPA 5030B 1.5 110-57-6 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050513EPA 5030B 0.4 75-34-3 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050513EPA 5030B 0.3 107-06-2 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050513EPA 5030B 0.5 75-35-4 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.5 156-59-2 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.4 156-60-5 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050513EPA 5030B 0.5 78-87-5 05/23/16 10:4705/23/16 05:30
Page 30 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD8
Ground Water
AZE0546-09 AZE054605/18/16 11:19
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-01-5 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-02-6 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6050513EPA 5030B 0.2 100-41-4 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Iodomethane10 6050513EPA 5030B 0.6 74-88-4 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050513EPA 5030B 0.9 591-78-6 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050513EPA 5030B 0.5 75-09-2 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050513EPA 5030B 1.1 78-93-3 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6050513EPA 5030B 1.7 108-10-1 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Styrene1.0 6050513EPA 5030B 0.4 100-42-5 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050513EPA 5030B 0.6 630-20-6 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050513EPA 5030B 0.5 79-34-5 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050513EPA 5030B 0.4 127-18-4 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Toluene1.0 6050513EPA 5030B 0.3 108-88-3 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050513EPA 5030B 0.4 71-55-6 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050513EPA 5030B 0.8 79-00-5 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Trichloroethene1.0 6050513EPA 5030B 0.4 79-01-6 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050513EPA 5030B 0.5 75-69-4 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050513EPA 5030B 0.7 96-18-4 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6050513EPA 5030B 0.8 108-05-4 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050513EPA 5030B 0.7 75-01-4 05/23/16 10:4705/23/16 05:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6050513EPA 5030B 0.4 1330-20-7 05/23/16 10:4705/23/16 05:30
Page 31 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD8
Ground Water
AZE0546-09 AZE054605/18/16 11:19
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Tetrahydrofuran10 6050513EPA 5030B 1.5 109-99-9 05/23/16 10:4705/23/16 05:30
EPA 8260B 96 %Surr: Dibromofluoromethane 6050513EPA 5030B 1868-53-7 05/23/16 10:4705/23/16 05:3080-120
EPA 8260B 102 %Surr: 1,2-Dichloroethane-d4 6050513EPA 5030B 17060-07-0 05/23/16 10:4705/23/16 05:3078-120
EPA 8260B 96 %Surr: Toluene-d8 6050513EPA 5030B 2037-26-5 05/23/16 10:4705/23/16 05:3080-120
EPA 8260B 106 %Surr: 4-Bromofluorobenzene 6050513EPA 5030B 460-00-4 05/23/16 10:4705/23/16 05:3080-120
Page 32 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD8
Ground Water
AZE0546-10 AZE054605/19/16 08:23
Project:Cabarrus Co - C&D
05/19/16 15:05
On Site
EPA 180.1 25.0 NTU1Field - Turbidity 0.10 6050530NA0.10 TURB 05/19/16 08:2305/19/16 08:23
Metals, Total
EPA 6020B 0.49 ug/L1Antimony6.00 J, B-01 6060033EPA 3005A 0.25 7440-36-0 06/03/16 13:5806/02/16 09:30
EPA 6020B 1.52 ug/L1Arsenic10.0 J 6060033EPA 3005A 0.75 7440-38-2 06/03/16 13:5806/02/16 09:30
EPA 6020B 133 ug/L1Barium100 6060033EPA 3005A 0.30 7440-39-3 06/03/16 13:5806/02/16 09:30
EPA 6020B 0.20 ug/L1Beryllium1.00 J 6060033EPA 3005A 0.09 7440-41-7 06/03/16 13:5806/02/16 09:30
NDEPA 6020B ug/L1Cadmium1.00 6060033EPA 3005A 0.10 7440-43-9 06/03/16 13:5806/02/16 09:30
EPA 6020B 3.54 ug/L1Chromium10.0 J 6060033EPA 3005A 0.43 7440-47-3 06/03/16 13:5806/02/16 09:30
EPA 6020B 1.40 ug/L1Cobalt10.0 J 6060033EPA 3005A 0.29 7440-48-4 06/03/16 13:5806/02/16 09:30
EPA 6020B 28.1 ug/L1Copper10.0 6060033EPA 3005A 0.41 7440-50-8 06/03/16 13:5806/02/16 09:30
EPA 6020B 1.28 ug/L1Lead10.0 J 6060033EPA 3005A 0.08 7439-92-1 06/03/16 13:5806/02/16 09:30
EPA 6020B 8.72 ug/L1Nickel50.0 J 6060033EPA 3005A 0.48 7440-02-0 06/03/16 13:5806/02/16 09:30
NDEPA 6020B ug/L1Selenium10.0 6060033EPA 3005A 0.85 7782-49-2 06/03/16 13:5806/02/16 09:30
NDEPA 6020B ug/L1Silver10.0 6060033EPA 3005A 0.22 7440-22-4 06/03/16 13:5806/02/16 09:30
NDEPA 6020B ug/L1Thallium5.50 6060033EPA 3005A 0.06 7440-28-0 06/03/16 13:5806/02/16 09:30
EPA 6020B 13.2 ug/L1Vanadium25.0 J 6060033EPA 3005A 1.57 7440-62-2 06/03/16 13:5806/02/16 09:30
EPA 6020B 1250 ug/L5Zinc50.0 6060033EPA 3005A 6.52 7440-66-6 06/07/16 11:2206/02/16 09:30
EPA 6020A 2320 ug/L1Iron40.0 6060033EPA 3005A 5.7 7439-89-6 06/03/16 13:5806/02/16 09:30
EPA 6020A 123 ug/L1Manganese10.0 6060033EPA 3005A 1.0 7439-96-5 06/03/16 13:5806/02/16 09:30
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 16:1306/01/16 15:00
Page 33 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-Duplicate
Ground Water
AZE0546-11 AZE054605/18/16 00:00
Project:Cabarrus Co - C&D
05/19/16 15:05
General Chemistry
SM 2320 B 110000 ug/L1Alkalinity as CaCO3 1000 6050491SM 2320 B 1000 ALK 05/20/16 14:0005/20/16 14:00
SM 2540 C 215000 ug/L1Total Dissolved Solids 50000 6050523SM 2540 C 50000 E-10173 05/24/16 18:5005/24/16 18:50
Inorganic Anions
EPA 9056A 2000 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 07:0405/25/16 13:58
NDEPA 9056A ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 05/26/16 07:0405/25/16 13:58
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050513EPA 5030B 4.9 67-64-1 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Acrylonitrile200 6050513EPA 5030B 1.8 107-13-1 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Benzene1.0 6050513EPA 5030B 0.2 71-43-2 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6050513EPA 5030B 0.7 74-97-5 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050513EPA 5030B 0.6 75-27-4 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Bromoform3.0 6050513EPA 5030B 0.7 75-25-2 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Bromomethane10 6050513EPA 5030B 0.8 74-83-9 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6050513EPA 5030B 0.6 75-15-0 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050513EPA 5030B 0.6 56-23-5 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6050513EPA 5030B 0.4 108-90-7 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Chloroethane10 6050513EPA 5030B 0.4 75-00-3 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Chloroform5.0 6050513EPA 5030B 0.3 67-66-3 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Chloromethane1.0 6050513EPA 5030B 0.4 74-87-3 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050513EPA 5030B 0.7 124-48-1 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050513EPA 5030B 2.0 96-12-8 05/23/16 11:1205/23/16 05:30
Page 34 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-Duplicate
Ground Water
AZE0546-11 AZE054605/18/16 00:00
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050513EPA 5030B 0.7 106-93-4 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Dibromomethane10 6050513EPA 5030B 0.7 74-95-3 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050513EPA 5030B 0.5 95-50-1 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050513EPA 5030B 0.3 106-46-7 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050513EPA 5030B 1.5 110-57-6 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050513EPA 5030B 0.4 75-34-3 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050513EPA 5030B 0.3 107-06-2 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050513EPA 5030B 0.5 75-35-4 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.5 156-59-2 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.4 156-60-5 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050513EPA 5030B 0.5 78-87-5 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-01-5 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-02-6 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6050513EPA 5030B 0.2 100-41-4 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Iodomethane10 6050513EPA 5030B 0.6 74-88-4 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050513EPA 5030B 0.9 591-78-6 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050513EPA 5030B 0.5 75-09-2 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050513EPA 5030B 1.1 78-93-3 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6050513EPA 5030B 1.7 108-10-1 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Styrene1.0 6050513EPA 5030B 0.4 100-42-5 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050513EPA 5030B 0.6 630-20-6 05/23/16 11:1205/23/16 05:30
Page 35 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-Duplicate
Ground Water
AZE0546-11 AZE054605/18/16 00:00
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050513EPA 5030B 0.5 79-34-5 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050513EPA 5030B 0.4 127-18-4 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Toluene1.0 6050513EPA 5030B 0.3 108-88-3 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050513EPA 5030B 0.4 71-55-6 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050513EPA 5030B 0.8 79-00-5 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Trichloroethene1.0 6050513EPA 5030B 0.4 79-01-6 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050513EPA 5030B 0.5 75-69-4 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050513EPA 5030B 0.7 96-18-4 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6050513EPA 5030B 0.8 108-05-4 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050513EPA 5030B 0.7 75-01-4 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6050513EPA 5030B 0.4 1330-20-7 05/23/16 11:1205/23/16 05:30
NDEPA 8260B ug/L1Tetrahydrofuran10 6050513EPA 5030B 1.5 109-99-9 05/23/16 11:1205/23/16 05:30
EPA 8260B 92 %Surr: Dibromofluoromethane 6050513EPA 5030B 1868-53-7 05/23/16 11:1205/23/16 05:3080-120
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6050513EPA 5030B 17060-07-0 05/23/16 11:1205/23/16 05:3078-120
EPA 8260B 98 %Surr: Toluene-d8 6050513EPA 5030B 2037-26-5 05/23/16 11:1205/23/16 05:3080-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 6050513EPA 5030B 460-00-4 05/23/16 11:1205/23/16 05:3080-120
Page 36 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-Duplicate
Ground Water
AZE0546-12 AZE054605/19/16 00:00
Project:Cabarrus Co - C&D
05/19/16 15:05
Metals, Total
EPA 6020B 1.27 ug/L1Antimony6.00 J, B-01 6060033EPA 3005A 0.25 7440-36-0 06/03/16 14:0306/02/16 09:30
EPA 6020B 1.55 ug/L1Arsenic10.0 J 6060033EPA 3005A 0.75 7440-38-2 06/03/16 14:0306/02/16 09:30
EPA 6020B 136 ug/L1Barium100 6060033EPA 3005A 0.30 7440-39-3 06/03/16 14:0306/02/16 09:30
EPA 6020B 0.23 ug/L1Beryllium1.00 J 6060033EPA 3005A 0.09 7440-41-7 06/03/16 14:0306/02/16 09:30
EPA 6020B 0.10 ug/L1Cadmium1.00 J 6060033EPA 3005A 0.10 7440-43-9 06/03/16 14:0306/02/16 09:30
EPA 6020B 4.41 ug/L1Chromium10.0 J 6060033EPA 3005A 0.43 7440-47-3 06/03/16 14:0306/02/16 09:30
EPA 6020B 1.63 ug/L1Cobalt10.0 J 6060033EPA 3005A 0.29 7440-48-4 06/03/16 14:0306/02/16 09:30
EPA 6020B 31.2 ug/L1Copper10.0 6060033EPA 3005A 0.41 7440-50-8 06/03/16 14:0306/02/16 09:30
EPA 6020B 1.87 ug/L1Lead10.0 J 6060033EPA 3005A 0.08 7439-92-1 06/03/16 14:0306/02/16 09:30
EPA 6020B 9.76 ug/L1Nickel50.0 J 6060033EPA 3005A 0.48 7440-02-0 06/03/16 14:0306/02/16 09:30
NDEPA 6020B ug/L1Selenium10.0 6060033EPA 3005A 0.85 7782-49-2 06/03/16 14:0306/02/16 09:30
NDEPA 6020B ug/L1Silver10.0 6060033EPA 3005A 0.22 7440-22-4 06/03/16 14:0306/02/16 09:30
NDEPA 6020B ug/L1Thallium5.50 6060033EPA 3005A 0.06 7440-28-0 06/03/16 14:0306/02/16 09:30
EPA 6020B 14.8 ug/L1Vanadium25.0 J 6060033EPA 3005A 1.57 7440-62-2 06/03/16 14:0306/02/16 09:30
EPA 6020B 1600 ug/L5Zinc50.0 6060033EPA 3005A 6.52 7440-66-6 06/07/16 11:2706/02/16 09:30
EPA 6020A 3230 ug/L1Iron40.0 6060033EPA 3005A 5.7 7439-89-6 06/03/16 14:0306/02/16 09:30
EPA 6020A 129 ug/L1Manganese10.0 6060033EPA 3005A 1.0 7439-96-5 06/03/16 14:0306/02/16 09:30
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 16:1606/01/16 15:00
Page 37 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD4Rep
Ground Water
AZE0545-19 AZE054505/17/16 11:28
Project:Cabarrus Co - 2 & 3
05/19/16 09:30
On Site
EPA 9050A 242 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/17/16 11:2805/17/16 11:28
SM 4500-O G 2680 ug/L1Dissolved Oxygen 0.0 6050530NA0.0 NA 05/17/16 11:2805/17/16 11:28
EPA 9040C 6.90 pH Units1Field - pH 6050530NAPH05/17/16 11:2805/17/16 11:28
NA -54 mV1Field - Redox 6050530NAREDOX05/17/16 11:2805/17/16 11:28
SM 2550 B 14.2 °C1Field - Temperature 6050530NATEMP05/17/16 11:2805/17/16 11:28
EPA 180.1 800 NTU1Field - Turbidity 0.10 >6050530NA0.10 TURB 05/17/16 11:2805/17/16 11:28
NA 8.70 feet1Field - Water Level 6050530NAWL05/17/16 11:2805/17/16 11:28
NA 19.63 feet1Field - Well Depth 6050530NA05/17/16 11:2805/17/16 11:28
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050511EPA 5030B 4.9 67-64-1 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Acrylonitrile200 6050511EPA 5030B 1.8 107-13-1 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Benzene1.0 6050511EPA 5030B 0.2 71-43-2 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Bromochloromethane3.0 6050511EPA 5030B 0.7 74-97-5 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050511EPA 5030B 0.6 75-27-4 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Bromoform3.0 6050511EPA 5030B 0.7 75-25-2 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Bromomethane10 6050511EPA 5030B 0.8 74-83-9 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Carbon Disulfide 100 6050511EPA 5030B 0.6 75-15-0 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050511EPA 5030B 0.6 56-23-5 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Chlorobenzene3.0 6050511EPA 5030B 0.4 108-90-7 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Chloroethane10 6050511EPA 5030B 0.4 75-00-3 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Chloroform5.0 6050511EPA 5030B 0.3 67-66-3 05/21/16 11:5005/21/16 05:50
Page 71 of 182
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD4Rep
Ground Water
AZE0545-19 AZE054505/17/16 11:28
Project:Cabarrus Co - 2 & 3
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chloromethane1.0 6050511EPA 5030B 0.4 74-87-3 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050511EPA 5030B 0.7 124-48-1 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050511EPA 5030B 2.0 96-12-8 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050511EPA 5030B 0.7 106-93-4 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Dibromomethane10 6050511EPA 5030B 0.7 74-95-3 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050511EPA 5030B 0.5 95-50-1 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050511EPA 5030B 0.3 106-46-7 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050511EPA 5030B 1.5 110-57-6 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050511EPA 5030B 0.4 75-34-3 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050511EPA 5030B 0.3 107-06-2 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050511EPA 5030B 0.5 75-35-4 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050511EPA 5030B 0.5 156-59-2 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050511EPA 5030B 0.4 156-60-5 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050511EPA 5030B 0.5 78-87-5 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050511EPA 5030B 0.4 10061-01-5 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050511EPA 5030B 0.4 10061-02-6 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Ethylbenzene1.0 6050511EPA 5030B 0.2 100-41-4 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Iodomethane10 6050511EPA 5030B 0.6 74-88-4 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050511EPA 5030B 0.9 591-78-6 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050511EPA 5030B 0.5 75-09-2 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050511EPA 5030B 1.1 78-93-3 05/21/16 11:5005/21/16 05:50
Page 72 of 182
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD4Rep
Ground Water
AZE0545-19 AZE054505/17/16 11:28
Project:Cabarrus Co - 2 & 3
05/19/16 09:30
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6050511EPA 5030B 1.7 108-10-1 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Styrene1.0 6050511EPA 5030B 0.4 100-42-5 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050511EPA 5030B 0.6 630-20-6 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050511EPA 5030B 0.5 79-34-5 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050511EPA 5030B 0.4 127-18-4 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Toluene1.0 6050511EPA 5030B 0.3 108-88-3 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050511EPA 5030B 0.4 71-55-6 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050511EPA 5030B 0.8 79-00-5 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Trichloroethene1.0 6050511EPA 5030B 0.4 79-01-6 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050511EPA 5030B 0.5 75-69-4 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050511EPA 5030B 0.7 96-18-4 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Vinyl Acetate 50 6050511EPA 5030B 0.8 108-05-4 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050511EPA 5030B 0.7 75-01-4 05/21/16 11:5005/21/16 05:50
NDEPA 8260B ug/L1Xylenes, total 5.0 6050511EPA 5030B 0.4 1330-20-7 05/21/16 11:5005/21/16 05:50
EPA 8260B 91 %Surr: Dibromofluoromethane 6050511EPA 5030B 1868-53-7 05/21/16 11:5005/21/16 05:5080-120
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6050511EPA 5030B 17060-07-0 05/21/16 11:5005/21/16 05:5078-120
EPA 8260B 101 %Surr: Toluene-d8 6050511EPA 5030B 2037-26-5 05/21/16 11:5005/21/16 05:5080-120
EPA 8260B 107 %Surr: 4-Bromofluorobenzene 6050511EPA 5030B 460-00-4 05/21/16 11:5005/21/16 05:5080-120
Page 73 of 182
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-CD4Rep
Ground Water
AZE0545-20 AZE054505/18/16 08:28
Project:Cabarrus Co - 2 & 3
05/19/16 09:30
On Site
EPA 180.1 28.0 NTU1Field - Turbidity 0.10 6050530NA0.10 TURB 05/18/16 08:2805/18/16 08:28
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6050664EPA 3005A 0.25 7440-36-0 05/31/16 14:5505/31/16 08:45
EPA 6020B 1.09 ug/L1Arsenic10.0 J 6050664EPA 3005A 0.75 7440-38-2 05/31/16 14:5505/31/16 08:45
EPA 6020B 56.2 ug/L1Barium100 J 6050664EPA 3005A 0.30 7440-39-3 05/31/16 14:5505/31/16 08:45
EPA 6020B 0.46 ug/L1Beryllium1.00 J 6050664EPA 3005A 0.09 7440-41-7 05/31/16 14:5505/31/16 08:45
NDEPA 6020B ug/L1Cadmium1.00 6050664EPA 3005A 0.10 7440-43-9 05/31/16 14:5505/31/16 08:45
EPA 6020B 1.24 ug/L1Chromium10.0 J 6050664EPA 3005A 0.43 7440-47-3 05/31/16 14:5505/31/16 08:45
EPA 6020B 7.31 ug/L1Cobalt10.0 J 6050664EPA 3005A 0.29 7440-48-4 05/31/16 14:5505/31/16 08:45
EPA 6020B 1.02 ug/L1Copper10.0 J 6050664EPA 3005A 0.41 7440-50-8 05/31/16 14:5505/31/16 08:45
EPA 6020B 0.66 ug/L1Lead10.0 J 6050664EPA 3005A 0.08 7439-92-1 05/31/16 14:5505/31/16 08:45
EPA 6020B 5.43 ug/L1Nickel50.0 J 6050664EPA 3005A 0.48 7440-02-0 05/31/16 14:5505/31/16 08:45
NDEPA 6020B ug/L1Selenium10.0 6050664EPA 3005A 0.85 7782-49-2 05/31/16 14:5505/31/16 08:45
NDEPA 6020B ug/L1Silver10.0 6050664EPA 3005A 0.22 7440-22-4 05/31/16 14:5505/31/16 08:45
NDEPA 6020B ug/L1Thallium5.50 6050664EPA 3005A 0.06 7440-28-0 05/31/16 14:5505/31/16 08:45
EPA 6020B 18.0 ug/L1Vanadium25.0 J 6050664EPA 3005A 1.57 7440-62-2 05/31/16 14:5505/31/16 08:45
EPA 6020B 3.70 ug/L1Zinc10.0 J 6050664EPA 3005A 1.30 7440-66-6 05/31/16 14:5505/31/16 08:45
Page 74 of 182
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-SW3
Surface Water
AZE0546-13 AZE054605/19/16 08:36
Project:Cabarrus Co - C&D
05/19/16 15:05
On Site
EPA 9050A 200 umhos/cm1Field - Specific Conductance 1 6050530NA1COND05/19/16 08:3605/19/16 08:36
SM 4500-O G 5990 ug/L1Dissolved Oxygen 0.0 6050530NA0.0 NA 05/19/16 08:3605/19/16 08:36
EPA 9040C 6.40 pH Units1Field - pH 6050530NAPH05/19/16 08:3605/19/16 08:36
NA 139 mV1Field - Redox 6050530NAREDOX05/19/16 08:3605/19/16 08:36
SM 2550 B 15.7 °C1Field - Temperature 6050530NATEMP05/19/16 08:3605/19/16 08:36
EPA 180.1 671 NTU1Field - Turbidity 0.10 6050530NA0.10 TURB 05/19/16 08:3605/19/16 08:36
General Chemistry
SM 2320 B 25000 ug/L1Alkalinity as CaCO3 1000 6050491SM 2320 B 1000 ALK 05/20/16 14:0005/20/16 14:00
SM 2540 C 908000 ug/L1Total Dissolved Solids 40000 H-02 6060067SM 2540 C 40000 E-10173 06/03/16 10:4006/03/16 10:40
Inorganic Anions
EPA 9056A 3200 ug/L1Chloride1000 6050603EPA 9056A 1000 16887-00-6 05/26/16 07:2605/25/16 13:58
EPA 9056A 47000 ug/L1Sulfate5000 6050603EPA 9056A 5000 14808-79-8 06/04/16 05:0405/25/16 13:58
Metals, Total
NDEPA 6020B ug/L1Antimony6.00 6060033EPA 3005A 0.25 7440-36-0 06/03/16 14:0806/02/16 09:30
EPA 6020B 11.1 ug/L1Arsenic10.0 6060033EPA 3005A 0.75 7440-38-2 06/03/16 14:0806/02/16 09:30
EPA 6020B 200 ug/L1Barium100 6060033EPA 3005A 0.30 7440-39-3 06/03/16 14:0806/02/16 09:30
EPA 6020B 5.95 ug/L5Beryllium5.00 6060033EPA 3005A 0.47 7440-41-7 06/07/16 12:1006/02/16 09:30
NDEPA 6020B ug/L1Cadmium1.00 6060033EPA 3005A 0.10 7440-43-9 06/03/16 14:0806/02/16 09:30
EPA 6020B 38.1 ug/L1Chromium10.0 6060033EPA 3005A 0.43 7440-47-3 06/03/16 14:0806/02/16 09:30
Page 38 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-SW3
Surface Water
AZE0546-13 AZE054605/19/16 08:36
Project:Cabarrus Co - C&D
05/19/16 15:05
Metals, Total
EPA 6020B 17.1 ug/L1Cobalt10.0 6060033EPA 3005A 0.29 7440-48-4 06/03/16 14:0806/02/16 09:30
EPA 6020B 22.4 ug/L1Copper10.0 6060033EPA 3005A 0.41 7440-50-8 06/03/16 14:0806/02/16 09:30
EPA 6020B 41.8 ug/L1Lead10.0 6060033EPA 3005A 0.08 7439-92-1 06/03/16 14:0806/02/16 09:30
EPA 6020B 15.5 ug/L1Nickel50.0 J 6060033EPA 3005A 0.48 7440-02-0 06/03/16 14:0806/02/16 09:30
EPA 6020B 18.0 ug/L1Selenium10.0 6060033EPA 3005A 0.85 7782-49-2 06/03/16 14:0806/02/16 09:30
NDEPA 6020B ug/L1Silver10.0 6060033EPA 3005A 0.22 7440-22-4 06/03/16 14:0806/02/16 09:30
EPA 6020B 0.31 ug/L1Thallium5.50 J 6060033EPA 3005A 0.06 7440-28-0 06/03/16 14:0806/02/16 09:30
EPA 6020B 180 ug/L1Vanadium25.0 6060033EPA 3005A 1.57 7440-62-2 06/03/16 14:0806/02/16 09:30
EPA 6020B 85.3 ug/L1Zinc10.0 6060033EPA 3005A 1.30 7440-66-6 06/03/16 14:0806/02/16 09:30
EPA 6020A 59700 ug/L20Iron800 6060033EPA 3005A 114 7439-89-6 06/07/16 11:3206/02/16 09:30
EPA 6020A 576 ug/L1Manganese10.0 6060033EPA 3005A 1.0 7439-96-5 06/03/16 14:0806/02/16 09:30
NDEPA 7470A ug/L1Mercury0.200 6060013EPA 7470A 0.132 7439-97-6 06/02/16 16:1806/01/16 15:00
Volatile Organic Compounds by EPA 8260
EPA 8260B 5.6 ug/L1Acetone100 J 6050513EPA 5030B 4.9 67-64-1 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Acrylonitrile200 6050513EPA 5030B 1.8 107-13-1 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Benzene1.0 6050513EPA 5030B 0.2 71-43-2 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Bromochloromethane3.0 6050513EPA 5030B 0.7 74-97-5 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050513EPA 5030B 0.6 75-27-4 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Bromoform3.0 6050513EPA 5030B 0.7 75-25-2 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Bromomethane10 6050513EPA 5030B 0.8 74-83-9 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Carbon Disulfide 100 6050513EPA 5030B 0.6 75-15-0 05/23/16 11:3705/23/16 05:30
Page 39 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-SW3
Surface Water
AZE0546-13 AZE054605/19/16 08:36
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050513EPA 5030B 0.6 56-23-5 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Chlorobenzene3.0 6050513EPA 5030B 0.4 108-90-7 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Chloroethane10 6050513EPA 5030B 0.4 75-00-3 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Chloroform5.0 6050513EPA 5030B 0.3 67-66-3 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Chloromethane1.0 6050513EPA 5030B 0.4 74-87-3 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050513EPA 5030B 0.7 124-48-1 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050513EPA 5030B 2.0 96-12-8 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050513EPA 5030B 0.7 106-93-4 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Dibromomethane10 6050513EPA 5030B 0.7 74-95-3 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050513EPA 5030B 0.5 95-50-1 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050513EPA 5030B 0.3 106-46-7 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050513EPA 5030B 1.5 110-57-6 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050513EPA 5030B 0.4 75-34-3 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050513EPA 5030B 0.3 107-06-2 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050513EPA 5030B 0.5 75-35-4 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.5 156-59-2 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050513EPA 5030B 0.4 156-60-5 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050513EPA 5030B 0.5 78-87-5 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-01-5 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050513EPA 5030B 0.4 10061-02-6 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Ethylbenzene1.0 6050513EPA 5030B 0.2 100-41-4 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Iodomethane10 6050513EPA 5030B 0.6 74-88-4 05/23/16 11:3705/23/16 05:30
Page 40 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-SW3
Surface Water
AZE0546-13 AZE054605/19/16 08:36
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050513EPA 5030B 0.9 591-78-6 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050513EPA 5030B 0.5 75-09-2 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050513EPA 5030B 1.1 78-93-3 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6050513EPA 5030B 1.7 108-10-1 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Styrene1.0 6050513EPA 5030B 0.4 100-42-5 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050513EPA 5030B 0.6 630-20-6 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050513EPA 5030B 0.5 79-34-5 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050513EPA 5030B 0.4 127-18-4 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Toluene1.0 6050513EPA 5030B 0.3 108-88-3 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050513EPA 5030B 0.4 71-55-6 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050513EPA 5030B 0.8 79-00-5 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Trichloroethene1.0 6050513EPA 5030B 0.4 79-01-6 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050513EPA 5030B 0.5 75-69-4 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050513EPA 5030B 0.7 96-18-4 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Vinyl Acetate 50 6050513EPA 5030B 0.8 108-05-4 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050513EPA 5030B 0.7 75-01-4 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Xylenes, total 5.0 6050513EPA 5030B 0.4 1330-20-7 05/23/16 11:3705/23/16 05:30
NDEPA 8260B ug/L1Tetrahydrofuran10 6050513EPA 5030B 1.5 109-99-9 05/23/16 11:3705/23/16 05:30
EPA 8260B 93 %Surr: Dibromofluoromethane 6050513EPA 5030B 1868-53-7 05/23/16 11:3705/23/16 05:3080-120
EPA 8260B 101 %Surr: 1,2-Dichloroethane-d4 6050513EPA 5030B 17060-07-0 05/23/16 11:3705/23/16 05:3078-120
EPA 8260B 96 %Surr: Toluene-d8 6050513EPA 5030B 2037-26-5 05/23/16 11:3705/23/16 05:3080-120
Page 41 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-SW3
Surface Water
AZE0546-13 AZE054605/19/16 08:36
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 6050513EPA 5030B 460-00-4 05/23/16 11:3705/23/16 05:3080-120
Page 42 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-Trip Blank
Water
AZE0546-14 AZE054605/16/16 00:00
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 6050502EPA 5030B 4.9 67-64-1 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Acrylonitrile200 6050502EPA 5030B 1.8 107-13-1 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Benzene1.0 6050502EPA 5030B 0.2 71-43-2 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Bromochloromethane3.0 6050502EPA 5030B 0.7 74-97-5 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Bromodichloromethane1.0 6050502EPA 5030B 0.6 75-27-4 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Bromoform3.0 6050502EPA 5030B 0.7 75-25-2 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Bromomethane10 6050502EPA 5030B 0.8 74-83-9 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Carbon Disulfide 100 6050502EPA 5030B 0.6 75-15-0 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 6050502EPA 5030B 0.6 56-23-5 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Chlorobenzene3.0 6050502EPA 5030B 0.4 108-90-7 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Chloroethane10 6050502EPA 5030B 0.4 75-00-3 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Chloroform5.0 6050502EPA 5030B 0.3 67-66-3 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Chloromethane1.0 6050502EPA 5030B 0.4 74-87-3 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Dibromochloromethane1.0 6050502EPA 5030B 0.7 124-48-1 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 6050502EPA 5030B 2.0 96-12-8 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 6050502EPA 5030B 0.7 106-93-4 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Dibromomethane10 6050502EPA 5030B 0.7 74-95-3 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 6050502EPA 5030B 0.5 95-50-1 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 6050502EPA 5030B 0.3 106-46-7 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 6050502EPA 5030B 1.5 110-57-6 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 6050502EPA 5030B 0.4 75-34-3 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 6050502EPA 5030B 0.3 107-06-2 05/20/16 08:4705/20/16 05:15
Page 43 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-Trip Blank
Water
AZE0546-14 AZE054605/16/16 00:00
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 6050502EPA 5030B 0.5 75-35-4 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.5 156-59-2 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 6050502EPA 5030B 0.4 156-60-5 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 6050502EPA 5030B 0.5 78-87-5 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-01-5 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 6050502EPA 5030B 0.4 10061-02-6 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Ethylbenzene1.0 6050502EPA 5030B 0.2 100-41-4 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Iodomethane10 6050502EPA 5030B 0.6 74-88-4 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 6050502EPA 5030B 0.9 591-78-6 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Methylene Chloride 1.0 6050502EPA 5030B 0.5 75-09-2 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 6050502EPA 5030B 1.1 78-93-3 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 6050502EPA 5030B 1.7 108-10-1 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Styrene1.0 6050502EPA 5030B 0.4 100-42-5 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 6050502EPA 5030B 0.6 630-20-6 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 6050502EPA 5030B 0.5 79-34-5 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Tetrachloroethene1.0 6050502EPA 5030B 0.4 127-18-4 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Toluene1.0 6050502EPA 5030B 0.3 108-88-3 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 6050502EPA 5030B 0.4 71-55-6 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 6050502EPA 5030B 0.8 79-00-5 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Trichloroethene1.0 6050502EPA 5030B 0.4 79-01-6 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 6050502EPA 5030B 0.5 75-69-4 05/20/16 08:4705/20/16 05:15
Page 44 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
1302-Trip Blank
Water
AZE0546-14 AZE054605/16/16 00:00
Project:Cabarrus Co - C&D
05/19/16 15:05
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 6050502EPA 5030B 0.7 96-18-4 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Vinyl Acetate 50 6050502EPA 5030B 0.8 108-05-4 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Vinyl Chloride 1.0 6050502EPA 5030B 0.7 75-01-4 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Xylenes, total 5.0 6050502EPA 5030B 0.4 1330-20-7 05/20/16 08:4705/20/16 05:15
NDEPA 8260B ug/L1Tetrahydrofuran10 6050502EPA 5030B 1.5 109-99-9 05/20/16 08:4705/20/16 05:15
EPA 8260B 93 %Surr: Dibromofluoromethane 6050502EPA 5030B 1868-53-7 05/20/16 08:4705/20/16 05:1580-120
EPA 8260B 100 %Surr: 1,2-Dichloroethane-d4 6050502EPA 5030B 17060-07-0 05/20/16 08:4705/20/16 05:1578-120
EPA 8260B 104 %Surr: Toluene-d8 6050502EPA 5030B 2037-26-5 05/20/16 08:4705/20/16 05:1580-120
EPA 8260B 107 %Surr: 4-Bromofluorobenzene 6050502EPA 5030B 460-00-4 05/20/16 08:4705/20/16 05:1580-120
Page 45 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6050434 - SM 5210 B
Blank (6050434-BLK1)Prepared: 05/18/16 Analyzed: 05/23/16
Biochemical Oxygen Demand ug/LND2000
LCS (6050434-BS1)Prepared: 05/18/16 Analyzed: 05/23/16
Biochemical Oxygen Demand ug/L2000002000 198000 85-115101
Duplicate (6050434-DUP1)Prepared: 05/18/16 Analyzed: 05/23/16 Source: AZE0504-01
Biochemical Oxygen Demand ug/LND10000 ND 20
Batch 6050450 - SM 2320 B
Blank (6050450-BLK1)Prepared & Analyzed: 05/19/16
Alkalinity as CaCO3 ug/LND1000
LCS (6050450-BS1)Prepared & Analyzed: 05/19/16
Alkalinity as CaCO3 ug/L1000001000 100000 85-115100
Duplicate (6050450-DUP1)Prepared & Analyzed: 05/19/16 Source: AZE0540-01
Alkalinity as CaCO3 ug/L850001000 85000 100
Batch 6050491 - SM 2320 B
Blank (6050491-BLK1)Prepared & Analyzed: 05/20/16
Alkalinity as CaCO3 ug/LND1000
LCS (6050491-BS1)Prepared & Analyzed: 05/20/16
Alkalinity as CaCO3 ug/L1000001000 100000 85-115100
Page 46 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6050491 - SM 2320 B
Duplicate (6050491-DUP1)Prepared & Analyzed: 05/20/16 Source: AZE0545-06
Alkalinity as CaCO3 ug/L4200001000 425000 101
Batch 6050505 - EPA 9060A
Blank (6050505-BLK1)Prepared & Analyzed: 05/21/16
Total Organic Carbon ug/LND1000
LCS (6050505-BS1)Prepared & Analyzed: 05/21/16
Total Organic Carbon ug/L197001000 20000 88-11298
Matrix Spike (6050505-MS1)Prepared & Analyzed: 05/21/16 Source: AZE0475-01
Total Organic Carbon ug/L210001000 20000 1060 67-141100
Matrix Spike Dup (6050505-MSD1)Prepared & Analyzed: 05/21/16 Source: AZE0475-01
Total Organic Carbon ug/L208001000 20000 1060 1667-14199 1
Batch 6050509 - SM 5220 D
Blank (6050509-BLK1)Prepared & Analyzed: 05/23/16
Chemical Oxygen Demand ug/LND10000
LCS (6050509-BS1)Prepared & Analyzed: 05/23/16
Chemical Oxygen Demand ug/L20400010000 200000 90-110102
Matrix Spike (6050509-MS1)Prepared & Analyzed: 05/23/16 Source: AZE0494-01RE1
Chemical Oxygen Demand ug/L4660000160000 800000 488000 QM-0590-110521
Page 47 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6050509 - SM 5220 D
Matrix Spike (6050509-MS2)Prepared & Analyzed: 05/23/16 Source: AZE0618-01
Chemical Oxygen Demand ug/L23700010000 200000 ND QM-0590-110119
Matrix Spike Dup (6050509-MSD1)Prepared & Analyzed: 05/23/16 Source: AZE0494-01RE1
Chemical Oxygen Demand ug/L4660000160000 800000 488000 10 QM-0590-110521 0
Batch 6050522 - SM 2540 C
Blank (6050522-BLK1)Prepared & Analyzed: 05/23/16
Total Dissolved Solids ug/LND10000
LCS (6050522-BS1)Prepared & Analyzed: 05/23/16
Total Dissolved Solids ug/L40000010000 400000 84-108100
Duplicate (6050522-DUP1)Prepared & Analyzed: 05/23/16 Source: AZE0540-03
Total Dissolved Solids ug/L9600010000 103000 107
Duplicate (6050522-DUP2)Prepared & Analyzed: 05/23/16 Source: AZE0540-10
Total Dissolved Solids ug/L14100010000 128000 1010
Batch 6050523 - SM 2540 C
Blank (6050523-BLK1)Prepared & Analyzed: 05/24/16
Total Dissolved Solids ug/LND10000
LCS (6050523-BS1)Prepared & Analyzed: 05/24/16
Total Dissolved Solids ug/L40100010000 400000 84-108100
Page 48 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 6050523 - SM 2540 C
Duplicate (6050523-DUP1)Prepared & Analyzed: 05/24/16 Source: AZE0546-11
Total Dissolved Solids ug/L23000050000 215000 107
Batch 6050561 - SM 4500-S D
Blank (6050561-BLK1)Prepared & Analyzed: 05/24/16
Total Sulfide ug/LND200
LCS (6050561-BS1)Prepared & Analyzed: 05/24/16
Total Sulfide ug/L499200 538.80 80-12092.6
Matrix Spike (6050561-MS1)Prepared & Analyzed: 05/24/16 Source: AZE0468-01
Total Sulfide ug/L608200 538.80 ND 30-129113
Matrix Spike Dup (6050561-MSD1)Prepared & Analyzed: 05/24/16 Source: AZE0468-01
Total Sulfide ug/L591200 538.80 ND 1030-129110 2.84
Batch 6060067 - SM 2540 C
Blank (6060067-BLK1)Prepared & Analyzed: 06/03/16
Total Dissolved Solids ug/LND10000
LCS (6060067-BS1)Prepared & Analyzed: 06/03/16
Total Dissolved Solids ug/L40400010000 400000 84-108101
Duplicate (6060067-DUP1)Prepared & Analyzed: 06/03/16 Source: AZE0546-13
Total Dissolved Solids ug/L84400040000 908000 107
Page 49 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Inorganic Anions - Quality Control
Batch 6050405 - EPA 300.0
Blank (6050405-BLK1)Prepared & Analyzed: 05/18/16
Chloride ug/LND1000
Nitrate as N ug/LND50
Sulfate ug/LND5000
LCS (6050405-BS1)Prepared & Analyzed: 05/18/16
Chloride ug/L97601000 10010 90-11098
Nitrate as N ug/L981050 10010 90-11098
Sulfate ug/L100005000 10010 90-110100
Matrix Spike (6050405-MS1)Prepared & Analyzed: 05/18/16 Source: AZE0497-01
Chloride ug/L732001000 10010 67500 QM-0290-11058
Nitrate as N ug/L970050 10010 177 90-11095
Sulfate ug/L185005000 10010 9040 90-11094
Matrix Spike (6050405-MS2)Prepared & Analyzed: 05/18/16 Source: AZE0544-01
Chloride ug/L134001000 10010 3730 90-11097
Nitrate as N ug/L961050 10010 79.0 90-11095
Sulfate ug/L107005000 10010 1040 90-11096
Matrix Spike Dup (6050405-MSD1)Prepared & Analyzed: 05/18/16 Source: AZE0497-01
Chloride ug/L732001000 10010 67500 15 QM-0290-11057 0.06
Nitrate as N ug/L971050 10010 177 1590-11095 0.1
Sulfate ug/L185005000 10010 9040 1590-11095 0.09
Batch 6050603 - EPA 9056A
Blank (6050603-BLK1)Prepared & Analyzed: 05/25/16
Chloride ug/LND1000
Page 50 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Inorganic Anions - Quality Control
Batch 6050603 - EPA 9056A
Blank (6050603-BLK1)Prepared & Analyzed: 05/25/16
Nitrate as N ug/LND50
Sulfate ug/LND5000
LCS (6050603-BS1)Prepared & Analyzed: 05/25/16
Chloride ug/L96701000 10010 90-11097
Nitrate as N ug/L996050 10010 90-110100
Sulfate ug/L97705000 10010 90-11098
Matrix Spike (6050603-MS1)Prepared & Analyzed: 05/25/16 Source: AZE0694-01
Chloride ug/L731001000 10010 86100 QM-0290-1100
Nitrate as N ug/L992050 10010 126 90-11098
Sulfate ug/L183005000 10010 ND QM-0590-110183
Matrix Spike (6050603-MS2)Prepared: 05/25/16 Analyzed: 05/26/16 Source: AZE0540-09
Chloride ug/L149001000 10010 5010 90-11099
Nitrate as N ug/L1000050 10010 520 90-11095
Sulfate ug/L128005000 10010 3330 90-11094
Matrix Spike Dup (6050603-MSD1)Prepared & Analyzed: 05/25/16 Source: AZE0694-01
Chloride ug/L730001000 10010 86100 15 QM-0290-1100 0.1
Nitrate as N ug/L990050 10010 126 1590-11098 0.2
Sulfate ug/L183005000 10010 ND 15 QM-0590-110183 0.1
Page 51 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6050611 - EPA 3005A
Blank (6050611-BLK1)Prepared & Analyzed: 05/26/16
Antimony ug/LND6.00
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Iron ug/LND40.0
Lead ug/LND10.0
Manganese ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/LND10.0
LCS (6050611-BS1)Prepared & Analyzed: 05/26/16
Antimony ug/L98.6 6.00 100.00 80-12099
Arsenic ug/L98.7 10.0 100.00 80-12099
Barium ug/L99.8 100 100.00 J80-120100
Beryllium ug/L98.6 1.00 100.00 80-12099
Cadmium ug/L96.9 1.00 100.00 80-12097
Chromium ug/L10010.0 100.00 80-120100
Cobalt ug/L97.2 10.0 100.00 80-12097
Copper ug/L96.4 10.0 100.00 80-12096
Page 52 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6050611 - EPA 3005A
LCS (6050611-BS1)Prepared & Analyzed: 05/26/16
Iron ug/L100040.0 1000.0 80-120100
Lead ug/L95.9 10.0 100.00 80-12096
Manganese ug/L10410.0 100.00 80-120104
Nickel ug/L99.2 50.0 100.00 80-12099
Selenium ug/L10210.0 100.00 80-120102
Silver ug/L10010.0 100.00 80-120100
Thallium ug/L97.4 5.50 100.00 80-12097
Vanadium ug/L99.9 25.0 100.00 80-120100
Zinc ug/L99.1 10.0 100.00 80-12099
Matrix Spike (6050611-MS1)Prepared & Analyzed: 05/26/16 Source: AZE0540-01
Antimony ug/L99.4 6.00 100.00 1.32 75-12598
Arsenic ug/L95.9 10.0 100.00 ND 75-12596
Barium ug/L176100 100.00 68.4 75-125107
Beryllium ug/L98.7 1.00 100.00 ND 75-12599
Cadmium ug/L93.9 1.00 100.00 ND 75-12594
Chromium ug/L10210.0 100.00 ND 75-125102
Cobalt ug/L98.3 10.0 100.00 ND 75-12598
Copper ug/L96.5 10.0 100.00 1.03 75-12595
Iron ug/L101040.0 1000.0 37.8 75-12597
Lead ug/L96.0 10.0 100.00 ND 75-12596
Manganese ug/L10810.0 100.00 6.13 75-125102
Nickel ug/L95.9 50.0 100.00 ND 75-12596
Selenium ug/L95.5 10.0 100.00 0.95 75-12595
Silver ug/L98.9 10.0 100.00 ND 75-12599
Thallium ug/L98.2 5.50 100.00 0.12 75-12598
Vanadium ug/L10525.0 100.00 4.10 75-125101
Page 53 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6050611 - EPA 3005A
Matrix Spike (6050611-MS1)Prepared & Analyzed: 05/26/16 Source: AZE0540-01
Zinc ug/L98.6 10.0 100.00 ND 75-12599
Matrix Spike Dup (6050611-MSD1)Prepared & Analyzed: 05/26/16 Source: AZE0540-01
Antimony ug/L96.1 6.00 100.00 1.32 2075-12595 3
Arsenic ug/L96.7 10.0 100.00 ND 2075-12597 0.8
Barium ug/L173100 100.00 68.4 2075-125105 1
Beryllium ug/L1021.00 100.00 ND 2075-125102 4
Cadmium ug/L97.7 1.00 100.00 ND 2075-12598 4
Chromium ug/L10510.0 100.00 ND 2075-125105 3
Cobalt ug/L10210.0 100.00 ND 2075-125102 3
Copper ug/L97.9 10.0 100.00 1.03 2075-12597 1
Iron ug/L104040.0 1000.0 37.8 2075-125100 3
Lead ug/L96.7 10.0 100.00 ND 2075-12597 0.8
Manganese ug/L10910.0 100.00 6.13 2075-125103 1
Nickel ug/L10050.0 100.00 ND 2075-125100 4
Selenium ug/L98.7 10.0 100.00 0.95 2075-12598 3
Silver ug/L99.2 10.0 100.00 ND 2075-12599 0.3
Thallium ug/L98.2 5.50 100.00 0.12 2075-12598 0.06
Vanadium ug/L10625.0 100.00 4.10 2075-125101 0.7
Zinc ug/L97.6 10.0 100.00 ND 2075-12598 1
Post Spike (6050611-PS1)Prepared & Analyzed: 05/26/16 Source: AZE0540-01
Antimony ug/L90.5 100.00 1.32 80-12089
Arsenic ug/L95.0 100.00 0.58 80-12094
Barium ug/L174 100.00 68.4 80-120105
Beryllium ug/L104 100.00 0.02 80-120104
Cadmium ug/L97.7 100.00 0.007 80-12098
Page 54 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6050611 - EPA 3005A
Post Spike (6050611-PS1)Prepared & Analyzed: 05/26/16 Source: AZE0540-01
Chromium ug/L101 100.00 0.15 80-120101
Cobalt ug/L102 100.00 0.03 80-120102
Copper ug/L96.9 100.00 1.03 80-12096
Iron ug/L1020 1000.0 37.8 80-12098
Lead ug/L95.0 100.00 0.01 80-12095
Manganese ug/L109 100.00 6.13 80-120103
Nickel ug/L99.3 100.00 0.11 80-12099
Selenium ug/L99.5 100.00 0.95 80-12099
Silver ug/L99.4 100.00 0.10 80-12099
Thallium ug/L97.1 100.00 0.12 80-12097
Vanadium ug/L107 100.00 4.10 80-120103
Zinc ug/L97.4 100.00 0.52 80-12097
Batch 6060013 - EPA 7470A
Blank (6060013-BLK1)Prepared: 06/01/16 Analyzed: 06/02/16
Mercury ug/LND0.200
LCS (6060013-BS1)Prepared: 06/01/16 Analyzed: 06/02/16
Mercury ug/L2.13 0.200 2.5000 80-12085
Duplicate (6060013-DUP1)Prepared: 06/01/16 Analyzed: 06/02/16 Source: AZE0475-19RE1
Mercury ug/L1.35 0.200 1.19 2012
Duplicate (6060013-DUP2)Prepared: 06/01/16 Analyzed: 06/02/16 Source: AZE0475-57RE1
Mercury ug/L0.659 0.200 0.675 202
Page 55 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6060013 - EPA 7470A
Matrix Spike (6060013-MS1)Prepared: 06/01/16 Analyzed: 06/02/16 Source: AZE0546-06
Mercury ug/L1.84 0.200 2.5000 ND QM-0575-12574
Matrix Spike Dup (6060013-MSD1)Prepared: 06/01/16 Analyzed: 06/02/16 Source: AZE0546-06
Mercury ug/L1.77 0.200 2.5000 ND 20 QM-0575-12571 4
Post Spike (6060013-PS1)Prepared: 06/01/16 Analyzed: 06/02/16 Source: AZE0546-06
Mercury ug/L1.30 1.6667 0.074 QM-0580-12073
Batch 6060033 - EPA 3005A
Blank (6060033-BLK1)Prepared: 06/02/16 Analyzed: 06/03/16
Antimony ug/L0.29 6.00 J
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Iron ug/LND40.0
Lead ug/LND10.0
Manganese ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/LND10.0
Page 56 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6060033 - EPA 3005A
LCS (6060033-BS1)Prepared: 06/02/16 Analyzed: 06/03/16
Antimony ug/L1046.00 100.00 80-120104
Arsenic ug/L97.3 10.0 100.00 80-12097
Barium ug/L97.1 100 100.00 J80-12097
Beryllium ug/L1031.00 100.00 80-120103
Cadmium ug/L1011.00 100.00 80-120101
Chromium ug/L10410.0 100.00 80-120104
Cobalt ug/L10210.0 100.00 80-120102
Copper ug/L10110.0 100.00 80-120101
Iron ug/L105040.0 1000.0 80-120105
Lead ug/L95.9 10.0 100.00 80-12096
Manganese ug/L10210.0 100.00 80-120102
Nickel ug/L99.9 50.0 100.00 80-120100
Selenium ug/L99.0 10.0 100.00 80-12099
Silver ug/L98.8 10.0 100.00 80-12099
Thallium ug/L95.8 5.50 100.00 80-12096
Vanadium ug/L10225.0 100.00 80-120102
Zinc ug/L10310.0 100.00 80-120103
Matrix Spike (6060033-MS1)Prepared: 06/02/16 Analyzed: 06/03/16 Source: AZE0545-37
Antimony ug/L1026.00 100.00 0.37 75-125101
Arsenic ug/L98.2 10.0 100.00 ND 75-12598
Barium ug/L122100 100.00 20.7 75-125101
Beryllium ug/L90.6 1.00 100.00 0.20 75-12590
Cadmium ug/L1011.00 100.00 ND 75-125101
Chromium ug/L10510.0 100.00 1.07 75-125104
Cobalt ug/L99.9 10.0 100.00 ND 75-125100
Copper ug/L98.8 10.0 100.00 ND 75-12599
Page 57 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6060033 - EPA 3005A
Matrix Spike (6060033-MS1)Prepared: 06/02/16 Analyzed: 06/03/16 Source: AZE0545-37
Iron ug/L137040.0 1000.0 293 75-125108
Lead ug/L93.8 10.0 100.00 0.33 75-12593
Manganese ug/L10810.0 100.00 5.67 75-125102
Nickel ug/L99.8 50.0 100.00 1.75 75-12598
Selenium ug/L10210.0 100.00 ND 75-125102
Silver ug/L96.9 10.0 100.00 ND 75-12597
Thallium ug/L96.0 5.50 100.00 ND 75-12596
Vanadium ug/L10525.0 100.00 3.09 75-125102
Zinc ug/L10110.0 100.00 2.42 75-12599
Matrix Spike Dup (6060033-MSD1)Prepared: 06/02/16 Analyzed: 06/03/16 Source: AZE0545-37
Antimony ug/L1056.00 100.00 0.37 2075-125105 3
Arsenic ug/L99.9 10.0 100.00 ND 2075-125100 2
Barium ug/L127100 100.00 20.7 2075-125106 4
Beryllium ug/L94.9 1.00 100.00 0.20 2075-12595 5
Cadmium ug/L1041.00 100.00 ND 2075-125104 3
Chromium ug/L10810.0 100.00 1.07 2075-125106 2
Cobalt ug/L10210.0 100.00 ND 2075-125102 3
Copper ug/L10210.0 100.00 ND 2075-125102 3
Iron ug/L136040.0 1000.0 293 2075-125107 0.7
Lead ug/L97.9 10.0 100.00 0.33 2075-12598 4
Manganese ug/L11110.0 100.00 5.67 2075-125106 3
Nickel ug/L10450.0 100.00 1.75 2075-125102 4
Selenium ug/L99.7 10.0 100.00 ND 2075-125100 3
Silver ug/L10010.0 100.00 ND 2075-125100 3
Thallium ug/L98.1 5.50 100.00 ND 2075-12598 2
Vanadium ug/L10825.0 100.00 3.09 2075-125105 4
Page 58 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 6060033 - EPA 3005A
Matrix Spike Dup (6060033-MSD1)Prepared: 06/02/16 Analyzed: 06/03/16 Source: AZE0545-37
Zinc ug/L10510.0 100.00 2.42 2075-125103 4
Post Spike (6060033-PS1)Prepared: 06/02/16 Analyzed: 06/03/16 Source: AZE0545-37
Antimony ug/L87.5 100.00 0.37 80-12087
Arsenic ug/L98.4 100.00 -0.04 80-12098
Barium ug/L122 100.00 20.7 80-120101
Beryllium ug/L93.2 100.00 0.20 80-12093
Cadmium ug/L101 100.00 0.006 80-120101
Chromium ug/L104 100.00 1.07 80-120103
Cobalt ug/L101 100.00 0.08 80-120101
Copper ug/L98.8 100.00 0.26 80-12099
Iron ug/L1310 1000.0 293 80-120101
Lead ug/L94.6 100.00 0.33 80-12094
Manganese ug/L108 100.00 5.67 80-120102
Nickel ug/L99.8 100.00 1.75 80-12098
Selenium ug/L98.2 100.00 -0.34 80-12099
Silver ug/L96.1 100.00 0.004 80-12096
Thallium ug/L95.3 100.00 0.02 80-12095
Vanadium ug/L106 100.00 3.09 80-120103
Zinc ug/L104 100.00 2.42 80-120102
Page 59 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050502 - EPA 5030B
Blank (6050502-BLK1)Prepared & Analyzed: 05/20/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND1.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
Page 60 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050502 - EPA 5030B
Blank (6050502-BLK1)Prepared & Analyzed: 05/20/16
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND50
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND1.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND4.0
Tetrahydrofuran ug/LND10
ug/L 50.000 80-120Surr: Dibromofluoromethane 9346
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10050
ug/L 50.000 80-120Surr: Toluene-d8 10251
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10753
Page 61 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050502 - EPA 5030B
LCS (6050502-BS1)Prepared & Analyzed: 05/20/16
Benzene ug/L51 50.000 67-134101
Chlorobenzene ug/L51 50.000 69-122103
1,1-Dichloroethene ug/L49 50.000 58-14298
Toluene ug/L50 50.000 68-127101
Trichloroethene ug/L53 50.000 72-132106
ug/L 50.000 80-120Surr: Dibromofluoromethane 9548
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10150
ug/L 50.000 80-120Surr: Toluene-d8 10151
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10653
Matrix Spike (6050502-MS1)Prepared & Analyzed: 05/20/16 Source: AZE0496-20
Benzene ug/L51 50.000 ND 67-134101
Chlorobenzene ug/L50 50.000 ND 69-122101
1,1-Dichloroethene ug/L52 50.000 ND 58-142103
Toluene ug/L50 50.000 ND 68-127100
Trichloroethene ug/L53 50.000 ND 72-132107
ug/L 50.000 80-120Surr: Dibromofluoromethane 9146
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10251
ug/L 50.000 80-120Surr: Toluene-d8 10151
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10753
Matrix Spike Dup (6050502-MSD1)Prepared & Analyzed: 05/20/16 Source: AZE0496-20
Benzene ug/L52 50.000 ND 967-134104 3
Chlorobenzene ug/L52 50.000 ND 1369-122104 3
1,1-Dichloroethene ug/L53 50.000 ND 958-142105 2
Page 62 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050502 - EPA 5030B
Matrix Spike Dup (6050502-MSD1)Prepared & Analyzed: 05/20/16 Source: AZE0496-20
Toluene ug/L50 50.000 ND 968-127101 0.6
Trichloroethene ug/L54 50.000 ND 1172-132109 2
ug/L 50.000 80-120Surr: Dibromofluoromethane 9347
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10251
ug/L 50.000 80-120Surr: Toluene-d8 10150
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10753
Batch 6050503 - EPA 5030B
Blank (6050503-BLK1)Prepared & Analyzed: 05/20/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND1.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Page 63 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050503 - EPA 5030B
Blank (6050503-BLK1)Prepared & Analyzed: 05/20/16
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND50
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND1.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
Page 64 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050503 - EPA 5030B
Blank (6050503-BLK1)Prepared & Analyzed: 05/20/16
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND4.0
Tetrahydrofuran ug/LND10
ug/L 50.000 80-120Surr: Dibromofluoromethane 9447
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10151
ug/L 50.000 80-120Surr: Toluene-d8 10351
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10553
LCS (6050503-BS1)Prepared & Analyzed: 05/20/16
Benzene ug/L52 50.000 67-134104
Chlorobenzene ug/L55 50.000 69-122109
1,1-Dichloroethene ug/L53 50.000 58-142105
Toluene ug/L51 50.000 68-127101
Trichloroethene ug/L53 50.000 72-132106
ug/L 50.000 80-120Surr: Dibromofluoromethane 9447
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10151
ug/L 50.000 80-120Surr: Toluene-d8 10351
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10653
Matrix Spike (6050503-MS1)Prepared & Analyzed: 05/20/16 Source: AZE0540-10
Benzene ug/L51 50.000 ND 67-134103
Chlorobenzene ug/L52 50.000 ND 69-122104
1,1-Dichloroethene ug/L51 50.000 ND 58-142103
Page 65 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050503 - EPA 5030B
Matrix Spike (6050503-MS1)Prepared & Analyzed: 05/20/16 Source: AZE0540-10
Toluene ug/L50 50.000 ND 68-127100
Trichloroethene ug/L53 50.000 ND 72-132105
ug/L 50.000 80-120Surr: Dibromofluoromethane 9346
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10251
ug/L 50.000 80-120Surr: Toluene-d8 10251
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10553
Matrix Spike Dup (6050503-MSD1)Prepared & Analyzed: 05/20/16 Source: AZE0540-10
Benzene ug/L51 50.000 ND 967-134102 0.9
Chlorobenzene ug/L51 50.000 ND 1369-122103 0.7
1,1-Dichloroethene ug/L51 50.000 ND 958-142102 0.4
Toluene ug/L49 50.000 ND 968-12799 1
Trichloroethene ug/L52 50.000 ND 1172-132105 0.8
ug/L 50.000 80-120Surr: Dibromofluoromethane 9347
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10452
ug/L 50.000 80-120Surr: Toluene-d8 10251
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10754
Batch 6050513 - EPA 5030B
Blank (6050513-BLK1)Prepared & Analyzed: 05/23/16
Acetone ug/LND100
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Page 66 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050513 - EPA 5030B
Blank (6050513-BLK1)Prepared & Analyzed: 05/23/16
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chloroethane ug/LND10
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Dibromochloromethane ug/LND1.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Iodomethane ug/LND10
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Page 67 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050513 - EPA 5030B
Blank (6050513-BLK1)Prepared & Analyzed: 05/23/16
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND100
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND1.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
Tetrahydrofuran ug/LND10
ug/L 50.000 80-120Surr: Dibromofluoromethane 9246
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9849
ug/L 50.000 80-120Surr: Toluene-d8 9849
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10653
LCS (6050513-BS1)Prepared & Analyzed: 05/23/16
Benzene ug/L51 50.000 67-134103
Chlorobenzene ug/L52 50.000 69-122105
1,1-Dichloroethene ug/L48 50.000 58-14295
Page 68 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050513 - EPA 5030B
LCS (6050513-BS1)Prepared & Analyzed: 05/23/16
Toluene ug/L50 50.000 68-127100
Trichloroethene ug/L54 50.000 72-132108
ug/L 50.000 80-120Surr: Dibromofluoromethane 9548
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 9950
ug/L 50.000 80-120Surr: Toluene-d8 9749
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10653
Matrix Spike (6050513-MS1)Prepared & Analyzed: 05/23/16 Source: AZE0545-40
Benzene ug/L51 50.000 0.2 67-134101
Chlorobenzene ug/L53 50.000 2.2 69-122101
1,1-Dichloroethene ug/L49 50.000 ND 58-14299
Toluene ug/L49 50.000 ND 68-12799
Trichloroethene ug/L53 50.000 ND 72-132106
ug/L 50.000 80-120Surr: Dibromofluoromethane 9648
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10753
ug/L 50.000 80-120Surr: Toluene-d8 10150
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10151
Matrix Spike Dup (6050513-MSD1)Prepared & Analyzed: 05/23/16 Source: AZE0545-40
Benzene ug/L53 50.000 0.2 967-134105 4
Chlorobenzene ug/L54 50.000 2.2 1369-122105 3
1,1-Dichloroethene ug/L50 50.000 ND 958-142100 2
Toluene ug/L52 50.000 ND 968-127103 4
Trichloroethene ug/L55 50.000 ND 1172-132111 4
Page 69 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 6050513 - EPA 5030B
Matrix Spike Dup (6050513-MSD1)Prepared & Analyzed: 05/23/16 Source: AZE0545-40
ug/L 50.000 80-120Surr: Dibromofluoromethane 9648
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 10251
ug/L 50.000 80-120Surr: Toluene-d8 9748
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 11055
Page 70 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Laboratory Certifications
Code Description Number Expires
02069Louisiana 06/30/2016LA
381North Carolina 12/31/2016NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2015 06/30/2016NELAC
E87315FL DOH NELAC (Drinking Water) Eff: 07/01/2015 06/30/2016NELDW
98011001South Carolina 06/30/2016SC
T104704397-08-TXTexas 03/31/2017TX
1340Virginia 12/14/2016VA
Page 71 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
QM-05 The spike recovery was outside acceptance limits for the MS and/or MSD and/or PDS due to suspected matrix interference. Sample results for the QC batch
were accepted based on acceptable LCS recoveries.
QM-02 The spike recovery is outside acceptance limits due to insignificant spike amount as compared to sample concentration.
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
H-02 Sample was prepared and/or analyzed outside of the EPA recommended holding time. See Case Narrative.
B-01 Analyte was detected in the associated method blank at an estimated level equal to or greater than the MDL. Sample values reported as greater than the MDL
and less than 10x the method blank value are reported as estimated values.
>Greater than the result value reported.
Note: Unless otherwise noted, all results are reported on an as received basis.
Page 72 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
COC Goes Here
Page 73 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
COC Goes Here
Page 74 of 75
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, INC.
Camp Dresser & McKee Inc. - Raleigh
5400 Glenwood Ave., Suite 300
Raleigh NC, 27612
Attention: Mr. Mat Colone June 09, 2016
COC Goes Here
Page 75 of 75
LOG-IN CHECKLIST
Camp Dresser & McKee Inc. - Raleigh
Cabarrus Co - C&DProject:
Client:
Printed: 6/9/2016 4:51:58PM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Peachtree Corners, GA 30092
PACE ANALYTICAL SERVICES, INC.
Date Received:05/18/16 12:45 Logged In By:Mohammad M. Rahman
Work Order:AZE0546
OBSERVATIONS
Attn: Mr. Mat Colone
#Samples: 14 #Containers: 47
4.0 4.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
NO
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:No
The samples were received over 2 days on 05/18/2016 @12:45 and 05/19/2016 @09:30 and @15:05. MMR
Comments:
Page 1 of 1
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