0601-MSWLF-1987_AveryCountyMSW_GWMReport_DIN26451_20160420

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April 2016 Semi-Annual Groundwater Monitoring Report

Avery County Closed MSW Landfill
Spruce Pine, North Carolina
NC Solid Waste Permit No. 06-01

Prepared for:

Avery County Solid Waste
175 Linville Street
Newland, North Carolina 28657

Prepared by:

June 2016

© 2016 Smith Gardner, Inc.
This document is intended for the sole use of the client for which it was prepared and
for the purpose agreed on by the client and Smith Gardner, Inc.

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Avery County Closed MSW Landfill April 2016 Semi-Annual Report
June 2016 Table of Contents Page i

Avery County Closed MSW Landfill
NC Solid Waste Permit No. 06-01

April 2016 Semi-Annual Groundwater Monitoring Report

Table of Contents
Page

1.0 INTRODUCTION ......................................................................................................... 1 
2.0 SITE GEOLOGY ........................................................................................................... 1 
3.0 SAMPLING PROCEDURES ......................................................................................... 1 
4.0 FIELD AND LABORATORY DATA ................................................................................ 2 
4.1 Field Measurements ................................................................................................. 2 
4.2 Laboratory Analysis ................................................................................................... 2 
4.3 Laboratory Results .................................................................................................... 2 
5.0 GROUNDWATER CHARACTERIZATION ...................................................................... 2 
6.0 CONCLUSIONS .......................................................................................................... 2 

FIGURES
Figure 1 Potentiometric Surface Map

TABLES
Table 1 Groundwater Elevation Data
Table 2 Field Parameters
Table 3 Detected Inorganic Constituents
Table 4 Detected Organic Constituents

APPENDICES
Appendix A Laboratory Analytical Report

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Avery County Closed MSW Landfill April 2016 Semi-Annual Report
June 2016 Page 1
1.0 INTRODUCTION
Avery County is required to submit semi-annual groundwater monitoring reports for the Closed
unlined MSW landfill (permit # 06-01) in accordance with Solid Waste Section Rule 15A NCAC
13B. This report, prepared by Smith Gardner, Inc (S+G), presents the semi-annual sampling for
the event conducted on April 19&20, 2016.

The groundwater monitoring network for the closed unlined MSW landfill includes three
groundwater monitoring wells and two surface water monitoring locations. This report includes
field procedure summaries, laboratory analyses and groundwater characterization for the
closed MSW facility.
2.0 SITE GEOLOGY
The Avery County Closed MSW Landfill is located in the North Carolina Blue Ridge province,
along the eastern limb of the Blue Ridge anticlinorium. Published geologic mapping1 places the
site approximately twelve miles west of the Brevard Zone (measured perpendicular to strike),
which is the boundary of the Blue Ridge Belt and the Piedmont. The principal geologic units
mapped in the immediate vicinity of the site include a mix of metamorphosed sedimentary and
igneous rocks – termed paragneiss and orthogneiss, respectively – interlayered with
contemporaneous schist, phyllite, and marble, later injected with various granitic intrusions,
including plutons, pegmatites, and hydrothermal veins. Regional metamorphic grades in the
region include kyanite-grade (high grade) and retrograde chlorite-biotite metamorphism (low
grade).
3.0 SAMPLING PROCEDURES
S+G personnel performed this sampling event that involved collecting samples from three
groundwater wells (MW-1, MW-2 and MW-3) and two surface water locations (SW-1 and SW-2).
Upgradient groundwater well (MW-3) was able to be sampled despite a deflection in the pipe.
No boring logs for these monitoring wells could be located in a NCDEQ file search.

Sampling methods followed the protocol outlined in the North Carolina Water Quality
Monitoring Guidance Document for Solid Waste Facilities2. The depth to water in each well was
gauged prior to purging and sampling.

Samples were collected using new factory sealed Teflon bailers and placed in laboratory
prepared containers for the specified analytical procedures. Groundwater samples were
properly preserved, placed on ice, and transported to the laboratory facility within the specified
hold times for each analysis.

1 North Carolina Geologic Survey at http://www.geology.enr.state.nc.us
2 Solid Waste Section Guidelines for Groundwater, Soil, and Surface Water Sampling, NCDENR, DWM, SWS, Rev 4-08.

Avery County Closed MSW Landfill April 2016 Semi-Annual Report
June 2016 Page 2
A map showing sampling locations is presented as Figure 1. Water table elevations and
available construction details are presented in Table 1.
4.0 FIELD AND LABORATORY DATA
4.1 Field Measurements
Following purging, field parameters for temperature, pH, turbidity and specific
conductance were measured and recorded at each sampling location. These results are
summarized in Table 2. In general these measurements were consistent with data from
previous events.
4.2 Laboratory Analysis
Ground and surface water samples were transported to Shealy Environmental Services,
Inc. (Columbia, SC3) where they were analyzed for Appendix I metals and volatile organic
compounds (VOC) via the SWS approved EPA Test Method presented in the laboratory
report. Samples were transported under proper chain of custody. The laboratory report
is attached for your review as Appendix A.
4.3 Laboratory Results
No inorganic constituents were detected above the 2L Standard for this event. Only
cobalt in the sample from MW-1 was detected above the GWP Standard.

No organic constituents were detected above the 2L Standard in this event.

Only arsenic in the sample collected from upgradient surface water location SW-1 was
detected at a concentration above the 2B Standard for Class C Waters. Laboratory
results are presented in Table 3.
5.0 GROUNDWATER CHARACTERIZATION
A potentiometric surface map was prepared from groundwater data from this sampling event.
The general groundwater flow is toward the southeast across the site toward Brushy Creek.
Hydraulic conductivity data was not available for these wells so groundwater velocities could not
be calculated. The potentiometric surface map is included as Figure 1.
6.0 CONCLUSIONS
Laboratory results indicate the water quality at the Avery County Closed unlined MSW Landfill is
generally consistent with historically reported results. Arsenic detection in SW-1 is likely
naturally occurring due to its presence in soils in this portion of North Carolina. Historic and

3 106 Vantage Point Drive, West Columbia, SC 29172; NELAC No: E87653, NCDEQ: 329, NC Field Parameters:5639.

Avery County Closed MSW Landfill April 2016 Semi-Annual Report
June 2016 Page 3
background detections indicate their presence is likely not due to landfill activity. The next
groundwater monitoring event is scheduled for September 2016. A report summarizing that
event will be submitted to NCDEQ with laboratory analyses.

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FIGURE

April 2016 – Semi-Annual Groundwater Report
Avery County Closed MSW Landfill
NC Solid Waste Permit No. 06-01

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MW-1
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April 2016 – Semi-Annual Groundwater Report
Avery County Closed MSW Landfill
NC Solid Waste Permit No. 06-01

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Appendix A
Laboratory Analytical Report

April 2016 – Semi-Annual Groundwater Report
Avery County Closed MSW Landfill
NC Solid Waste Permit No. 06-01

This page intentionally left blank.

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Smith Gardner, Inc.
14 North Boylan Avenue
Raleigh, NC 27603
Attention: Madeline German
RD21041Lot Number:
Avery County MSWProject Name:
04/28/2016Date Completed:
Kelly M. Nance
Project Manager

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Smith Gardner, Inc.
Lot Number: RD21041
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Inorganic Metals
The method blank associated with batch 11519 had copper detected at a concentration that was above the MDL but below the PQL. All samples
associated with this method blank that have detections for copper have been flagged with a "B”.
Page: 2 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Smith Gardner, Inc.
Lot Number: RD21041

Sample Number Sample ID Matrix Date Sampled Date Received
001 04/20/2016 1130MW-1 Aqueous 04/21/2016
002 04/20/2016 1215MW-2 Aqueous 04/21/2016
003 04/20/2016 1235MW-3 Aqueous 04/21/2016
004 04/20/2016 1250SW-1 Aqueous 04/21/2016
005 04/20/2016 1140SW-2 Aqueous 04/21/2016
(5 samples)
Page: 3 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Smith Gardner, Inc.
Lot Number: RD21041

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 MW-1 Aqueous Benzene 8260B 0.48 J ug/L 5
001 MW-1 Aqueous Chlorobenzene 8260B 0.25 J ug/L 5
001 MW-1 Aqueous 1,4-Dichlorobenzene 8260B 1.1 ug/L 5
001 MW-1 Aqueous cis-1,2-Dichloroethene 8260B 0.58 J ug/L 5
001 MW-1 Aqueous Antimony 6020A 0.23 J ug/L 7
001 MW-1 Aqueous Barium 6020A 130 ug/L 7
001 MW-1 Aqueous Cadmium 6020A 0.43 ug/L 7
001 MW-1 Aqueous Cobalt 6020A 15 ug/L 7
001 MW-1 Aqueous Copper 6020A 0.32 BJ ug/L 7
001 MW-1 Aqueous Nickel 6020A 4.0 J ug/L 7
001 MW-1 Aqueous Thallium 6020A 0.086 J ug/L 7
001 MW-1 Aqueous Zinc 6020A 17 ug/L 7
002 MW-2 Aqueous Antimony 6020A 0.29 J ug/L 10
002 MW-2 Aqueous Barium 6020A 29 ug/L 10
002 MW-2 Aqueous Copper 6020A 3.2 B ug/L 10
002 MW-2 Aqueous Vanadium 6020A 1.2 J ug/L 10
002 MW-2 Aqueous Zinc 6020A 2.0 J ug/L 10
003 MW-3 Aqueous Benzene 8260B 0.33 J ug/L 11
003 MW-3 Aqueous 1,4-Dichlorobenzene 8260B 0.73 J ug/L 11
003 MW-3 Aqueous Arsenic 6020A 0.53 J ug/L 13
003 MW-3 Aqueous Barium 6020A 35 ug/L 13
003 MW-3 Aqueous Cadmium 6020A 0.078 J ug/L 13
003 MW-3 Aqueous Cobalt 6020A 2.6 J ug/L 13
003 MW-3 Aqueous Copper 6020A 1.2 B ug/L 13
003 MW-3 Aqueous Lead 6020A 0.46 J ug/L 13
003 MW-3 Aqueous Nickel 6020A 1.5 J ug/L 13
003 MW-3 Aqueous Vanadium 6020A 1.6 J ug/L 13
003 MW-3 Aqueous Zinc 6020A 33 ug/L 13
004 SW-1 Aqueous Barium 6020A 13 ug/L 16
004 SW-1 Aqueous Copper 6020A 0.62 BJ ug/L 16
004 SW-1 Aqueous Lead 6020A 0.15 J ug/L 16
004 SW-1 Aqueous Vanadium 6020A 1.2 J ug/L 16
004 SW-1 Aqueous Zinc 6020A 5.2 J ug/L 16
005 SW-2 Aqueous Chloroethane 8260B 2.1 ug/L 17
005 SW-2 Aqueous 1,1-Dichloroethane 8260B 1.1 ug/L 17
005 SW-2 Aqueous Antimony 6020A 0.24 J ug/L 19
005 SW-2 Aqueous Barium 6020A 12 ug/L 19
005 SW-2 Aqueous Cadmium 6020A 0.044 J ug/L 19
005 SW-2 Aqueous Cobalt 6020A 0.67 J ug/L 19
005 SW-2 Aqueous Copper 6020A 0.65 BJ ug/L 19
005 SW-2 Aqueous Thallium 6020A 0.15 J ug/L 19
005 SW-2 Aqueous Vanadium 6020A 1.2 J ug/L 19
005 SW-2 Aqueous Zinc 6020A 1.7 J ug/L 19
(43 detections)
Page: 4 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
MW-1
RD21041-001
04/20/2016 1130
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/26/2016 1049 RAG 11786
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/L1.620
Acrylonitrile 107-13-1 8260B ND 1ug/L0.6220
Benzene 71-43-2 8260B 0.48 J 1ug/L0.211.0
Bromochloromethane 74-97-5 8260B ND 1ug/L0.451.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.231.0
Bromoform 75-25-2 8260B ND 1ug/L0.351.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.192.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L1.810
Carbon disulfide 75-15-0 8260B ND 1ug/L0.451.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.311.0
Chlorobenzene 108-90-7 8260B 0.25 J 1ug/L0.201.0
Chloroethane 75-00-3 8260B ND 1ug/L0.282.0
Chloroform 67-66-3 8260B ND 1ug/L0.211.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.191.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.571.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.231.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.171.0
Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.261.0
trans-1,4-Dichloro-2-butene 110-57-6 8260B ND 1ug/L1.42.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.461.0
1,4-Dichlorobenzene 106-46-7 8260B 1.1 1ug/L0.191.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.191.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.231.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.311.0
cis-1,2-Dichloroethene 156-59-2 8260B 0.58 J 1ug/L0.201.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.331.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.291.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.301.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.221.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.211.0
2-Hexanone 591-78-6 8260B ND 1ug/L0.2610
Methyl iodide (Iodomethane)74-88-4 8260B ND 1ug/L0.285.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L0.2910
Methylene chloride 75-09-2 8260B ND 1ug/L0.421.0
Styrene 100-42-5 8260B ND 1ug/L0.131.0
1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.191.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.131.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.221.0
Tetrahydrofuran 109-99-9 8260B ND 1ug/L0.575.0
Toluene 108-88-3 8260B ND 1ug/L0.241.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.241.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.221.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.161.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.741.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
MW-1
RD21041-001
04/20/2016 1130
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/26/2016 1049 RAG 11786
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.351.0
Vinyl acetate 108-05-4 8260B ND 1ug/L1.05.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.501.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.321.0
m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.191.0
o - Xylenes 95-47-6 8260B ND 1ug/L0.141.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 70-130
Bromofluorobenzene 99 70-130
Toluene-d8 104 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
MW-1
RD21041-001
04/20/2016 1130
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 04/25/2016 1527 BNW 04/22/2016 0841 11519
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.23 J 1ug/L0.171.0
Arsenic 7440-38-2 6020A ND 1ug/L0.261.0
Barium 7440-39-3 6020A 130 1ug/L0.535.0
Beryllium 7440-41-7 6020A ND 1ug/L0.120.40
Cadmium 7440-43-9 6020A 0.43 1ug/L0.0440.10
Chromium 7440-47-3 6020A ND 1ug/L0.635.0
Cobalt 7440-48-4 6020A 15 1ug/L0.265.0
Copper 7440-50-8 6020A 0.32 BJ 1ug/L0.151.0
Lead 7439-92-1 6020A ND 1ug/L0.151.0
Nickel 7440-02-0 6020A 4.0 J 1ug/L0.635.0
Selenium 7782-49-2 6020A ND 1ug/L0.951.0
Silver 7440-22-4 6020A ND 1ug/L0.171.0
Thallium 7440-28-0 6020A 0.086 J 1ug/L0.0750.50
Vanadium 7440-62-2 6020A ND 1ug/L1.05.0
Zinc 7440-66-6 6020A 17 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
MW-2
RD21041-002
04/20/2016 1215
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/26/2016 1112 RAG 11786
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/L1.620
Acrylonitrile 107-13-1 8260B ND 1ug/L0.6220
Benzene 71-43-2 8260B ND 1ug/L0.211.0
Bromochloromethane 74-97-5 8260B ND 1ug/L0.451.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.231.0
Bromoform 75-25-2 8260B ND 1ug/L0.351.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.192.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L1.810
Carbon disulfide 75-15-0 8260B ND 1ug/L0.451.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.311.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.201.0
Chloroethane 75-00-3 8260B ND 1ug/L0.282.0
Chloroform 67-66-3 8260B ND 1ug/L0.211.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.191.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.571.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.231.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.171.0
Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.261.0
trans-1,4-Dichloro-2-butene 110-57-6 8260B ND 1ug/L1.42.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.461.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.191.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.191.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.231.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.311.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.201.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.331.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.291.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.301.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.221.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.211.0
2-Hexanone 591-78-6 8260B ND 1ug/L0.2610
Methyl iodide (Iodomethane)74-88-4 8260B ND 1ug/L0.285.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L0.2910
Methylene chloride 75-09-2 8260B ND 1ug/L0.421.0
Styrene 100-42-5 8260B ND 1ug/L0.131.0
1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.191.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.131.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.221.0
Tetrahydrofuran 109-99-9 8260B ND 1ug/L0.575.0
Toluene 108-88-3 8260B ND 1ug/L0.241.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.241.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.221.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.161.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.741.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
MW-2
RD21041-002
04/20/2016 1215
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/26/2016 1112 RAG 11786
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.351.0
Vinyl acetate 108-05-4 8260B ND 1ug/L1.05.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.501.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.321.0
m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.191.0
o - Xylenes 95-47-6 8260B ND 1ug/L0.141.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 103 70-130
Bromofluorobenzene 97 70-130
Toluene-d8 104 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
MW-2
RD21041-002
04/20/2016 1215
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 04/25/2016 1553 BNW 04/22/2016 0841 11519
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.29 J 1ug/L0.171.0
Arsenic 7440-38-2 6020A ND 1ug/L0.261.0
Barium 7440-39-3 6020A 29 1ug/L0.535.0
Beryllium 7440-41-7 6020A ND 1ug/L0.120.40
Cadmium 7440-43-9 6020A ND 1ug/L0.0440.10
Chromium 7440-47-3 6020A ND 1ug/L0.635.0
Cobalt 7440-48-4 6020A ND 1ug/L0.265.0
Copper 7440-50-8 6020A 3.2 B 1ug/L0.151.0
Lead 7439-92-1 6020A ND 1ug/L0.151.0
Nickel 7440-02-0 6020A ND 1ug/L0.635.0
Selenium 7782-49-2 6020A ND 1ug/L0.951.0
Silver 7440-22-4 6020A ND 1ug/L0.171.0
Thallium 7440-28-0 6020A ND 1ug/L0.0750.50
Vanadium 7440-62-2 6020A 1.2 J 1ug/L1.05.0
Zinc 7440-66-6 6020A 2.0 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
MW-3
RD21041-003
04/20/2016 1235
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/26/2016 1135 RAG 11786
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/L1.620
Acrylonitrile 107-13-1 8260B ND 1ug/L0.6220
Benzene 71-43-2 8260B 0.33 J 1ug/L0.211.0
Bromochloromethane 74-97-5 8260B ND 1ug/L0.451.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.231.0
Bromoform 75-25-2 8260B ND 1ug/L0.351.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.192.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L1.810
Carbon disulfide 75-15-0 8260B ND 1ug/L0.451.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.311.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.201.0
Chloroethane 75-00-3 8260B ND 1ug/L0.282.0
Chloroform 67-66-3 8260B ND 1ug/L0.211.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.191.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.571.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.231.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.171.0
Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.261.0
trans-1,4-Dichloro-2-butene 110-57-6 8260B ND 1ug/L1.42.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.461.0
1,4-Dichlorobenzene 106-46-7 8260B 0.73 J 1ug/L0.191.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.191.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.231.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.311.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.201.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.331.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.291.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.301.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.221.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.211.0
2-Hexanone 591-78-6 8260B ND 1ug/L0.2610
Methyl iodide (Iodomethane)74-88-4 8260B ND 1ug/L0.285.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L0.2910
Methylene chloride 75-09-2 8260B ND 1ug/L0.421.0
Styrene 100-42-5 8260B ND 1ug/L0.131.0
1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.191.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.131.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.221.0
Tetrahydrofuran 109-99-9 8260B ND 1ug/L0.575.0
Toluene 108-88-3 8260B ND 1ug/L0.241.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.241.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.221.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.161.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.741.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
MW-3
RD21041-003
04/20/2016 1235
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/26/2016 1135 RAG 11786
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.351.0
Vinyl acetate 108-05-4 8260B ND 1ug/L1.05.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.501.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.321.0
m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.191.0
o - Xylenes 95-47-6 8260B ND 1ug/L0.141.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 70-130
Bromofluorobenzene 97 70-130
Toluene-d8 101 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
MW-3
RD21041-003
04/20/2016 1235
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 04/25/2016 1558 BNW 04/22/2016 0841 11519
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A ND 1ug/L0.171.0
Arsenic 7440-38-2 6020A 0.53 J 1ug/L0.261.0
Barium 7440-39-3 6020A 35 1ug/L0.535.0
Beryllium 7440-41-7 6020A ND 1ug/L0.120.40
Cadmium 7440-43-9 6020A 0.078 J 1ug/L0.0440.10
Chromium 7440-47-3 6020A ND 1ug/L0.635.0
Cobalt 7440-48-4 6020A 2.6 J 1ug/L0.265.0
Copper 7440-50-8 6020A 1.2 B 1ug/L0.151.0
Lead 7439-92-1 6020A 0.46 J 1ug/L0.151.0
Nickel 7440-02-0 6020A 1.5 J 1ug/L0.635.0
Selenium 7782-49-2 6020A ND 1ug/L0.951.0
Silver 7440-22-4 6020A ND 1ug/L0.171.0
Thallium 7440-28-0 6020A ND 1ug/L0.0750.50
Vanadium 7440-62-2 6020A 1.6 J 1ug/L1.05.0
Zinc 7440-66-6 6020A 33 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
SW-1
RD21041-004
04/20/2016 1250
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/26/2016 1157 RAG 11786
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/L1.620
Acrylonitrile 107-13-1 8260B ND 1ug/L0.6220
Benzene 71-43-2 8260B ND 1ug/L0.211.0
Bromochloromethane 74-97-5 8260B ND 1ug/L0.451.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.231.0
Bromoform 75-25-2 8260B ND 1ug/L0.351.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.192.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L1.810
Carbon disulfide 75-15-0 8260B ND 1ug/L0.451.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.311.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.201.0
Chloroethane 75-00-3 8260B ND 1ug/L0.282.0
Chloroform 67-66-3 8260B ND 1ug/L0.211.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.191.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.571.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.231.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.171.0
Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.261.0
trans-1,4-Dichloro-2-butene 110-57-6 8260B ND 1ug/L1.42.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.461.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.191.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.191.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.231.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.311.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.201.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.331.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.291.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.301.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.221.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.211.0
2-Hexanone 591-78-6 8260B ND 1ug/L0.2610
Methyl iodide (Iodomethane)74-88-4 8260B ND 1ug/L0.285.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L0.2910
Methylene chloride 75-09-2 8260B ND 1ug/L0.421.0
Styrene 100-42-5 8260B ND 1ug/L0.131.0
1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.191.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.131.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.221.0
Tetrahydrofuran 109-99-9 8260B ND 1ug/L0.575.0
Toluene 108-88-3 8260B ND 1ug/L0.241.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.241.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.221.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.161.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.741.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
SW-1
RD21041-004
04/20/2016 1250
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/26/2016 1157 RAG 11786
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.351.0
Vinyl acetate 108-05-4 8260B ND 1ug/L1.05.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.501.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.321.0
m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.191.0
o - Xylenes 95-47-6 8260B ND 1ug/L0.141.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 104 70-130
Bromofluorobenzene 97 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 32
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Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
SW-1
RD21041-004
04/20/2016 1250
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 04/25/2016 1604 BNW 04/22/2016 0841 11519
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A ND 1ug/L0.171.0
Arsenic 7440-38-2 6020A ND 1ug/L0.261.0
Barium 7440-39-3 6020A 13 1ug/L0.535.0
Beryllium 7440-41-7 6020A ND 1ug/L0.120.40
Cadmium 7440-43-9 6020A ND 1ug/L0.0440.10
Chromium 7440-47-3 6020A ND 1ug/L0.635.0
Cobalt 7440-48-4 6020A ND 1ug/L0.265.0
Copper 7440-50-8 6020A 0.62 BJ 1ug/L0.151.0
Lead 7439-92-1 6020A 0.15 J 1ug/L0.151.0
Nickel 7440-02-0 6020A ND 1ug/L0.635.0
Selenium 7782-49-2 6020A ND 1ug/L0.951.0
Silver 7440-22-4 6020A ND 1ug/L0.171.0
Thallium 7440-28-0 6020A ND 1ug/L0.0750.50
Vanadium 7440-62-2 6020A 1.2 J 1ug/L1.05.0
Zinc 7440-66-6 6020A 5.2 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 32
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
SW-2
RD21041-005
04/20/2016 1140
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/26/2016 1220 RAG 11786
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/L1.620
Acrylonitrile 107-13-1 8260B ND 1ug/L0.6220
Benzene 71-43-2 8260B ND 1ug/L0.211.0
Bromochloromethane 74-97-5 8260B ND 1ug/L0.451.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.231.0
Bromoform 75-25-2 8260B ND 1ug/L0.351.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.192.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L1.810
Carbon disulfide 75-15-0 8260B ND 1ug/L0.451.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.311.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.201.0
Chloroethane 75-00-3 8260B 2.1 1ug/L0.282.0
Chloroform 67-66-3 8260B ND 1ug/L0.211.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.191.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.571.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.231.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.171.0
Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.261.0
trans-1,4-Dichloro-2-butene 110-57-6 8260B ND 1ug/L1.42.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.461.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.191.0
1,1-Dichloroethane 75-34-3 8260B 1.1 1ug/L0.191.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.231.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.311.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.201.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.331.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.291.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.301.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.221.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.211.0
2-Hexanone 591-78-6 8260B ND 1ug/L0.2610
Methyl iodide (Iodomethane)74-88-4 8260B ND 1ug/L0.285.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L0.2910
Methylene chloride 75-09-2 8260B ND 1ug/L0.421.0
Styrene 100-42-5 8260B ND 1ug/L0.131.0
1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.191.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.131.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.221.0
Tetrahydrofuran 109-99-9 8260B ND 1ug/L0.575.0
Toluene 108-88-3 8260B ND 1ug/L0.241.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.241.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.221.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.161.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.741.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 32
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
SW-2
RD21041-005
04/20/2016 1140
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/26/2016 1220 RAG 11786
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.351.0
Vinyl acetate 108-05-4 8260B ND 1ug/L1.05.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.501.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.321.0
m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.191.0
o - Xylenes 95-47-6 8260B ND 1ug/L0.141.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Bromofluorobenzene 98 70-130
Toluene-d8 100 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 32
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Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Smith Gardner, Inc.
SW-2
RD21041-005
04/20/2016 1140
04/21/2016
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 04/25/2016 1625 BNW 04/22/2016 0841 11519
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020A 0.24 J 1ug/L0.171.0
Arsenic 7440-38-2 6020A ND 1ug/L0.261.0
Barium 7440-39-3 6020A 12 1ug/L0.535.0
Beryllium 7440-41-7 6020A ND 1ug/L0.120.40
Cadmium 7440-43-9 6020A 0.044 J 1ug/L0.0440.10
Chromium 7440-47-3 6020A ND 1ug/L0.635.0
Cobalt 7440-48-4 6020A 0.67 J 1ug/L0.265.0
Copper 7440-50-8 6020A 0.65 BJ 1ug/L0.151.0
Lead 7439-92-1 6020A ND 1ug/L0.151.0
Nickel 7440-02-0 6020A ND 1ug/L0.635.0
Selenium 7782-49-2 6020A ND 1ug/L0.951.0
Silver 7440-22-4 6020A ND 1ug/L0.171.0
Thallium 7440-28-0 6020A 0.15 J 1ug/L0.0750.50
Vanadium 7440-62-2 6020A 1.2 J 1ug/L1.05.0
Zinc 7440-66-6 6020A 1.7 J 1ug/L1.610
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 32
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QC Summary
Page: 20 of 32
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ11786-001
11786 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 04/26/2016 1020201.6 ug/L1
Acrylonitrile ND 04/26/2016 1020200.62 ug/L1
Benzene ND 04/26/2016 10201.0 0.21 ug/L1
Bromochloromethane ND 04/26/2016 10201.0 0.45 ug/L1
Bromodichloromethane ND 04/26/2016 10201.0 0.23 ug/L1
Bromoform ND 04/26/2016 10201.0 0.35 ug/L1
Bromomethane (Methyl bromide)ND 04/26/2016 10202.0 0.19 ug/L1
2-Butanone (MEK)ND 04/26/2016 1020101.8 ug/L1
Carbon disulfide ND 04/26/2016 10201.0 0.45 ug/L1
Carbon tetrachloride ND 04/26/2016 10201.0 0.31 ug/L1
Chlorobenzene ND 04/26/2016 10201.0 0.20 ug/L1
Chloroethane ND 04/26/2016 10202.0 0.28 ug/L1
Chloroform ND 04/26/2016 10201.0 0.21 ug/L1
Chloromethane (Methyl chloride)ND 04/26/2016 10201.0 0.19 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 04/26/2016 10201.0 0.57 ug/L1
Dibromochloromethane ND 04/26/2016 10201.0 0.23 ug/L1
1,2-Dibromoethane (EDB)ND 04/26/2016 10201.0 0.17 ug/L1
Dibromomethane (Methylene bromide)ND 04/26/2016 10201.0 0.26 ug/L1
trans-1,4-Dichloro-2-butene ND 04/26/2016 10202.0 1.4 ug/L1
1,2-Dichlorobenzene ND 04/26/2016 10201.0 0.46 ug/L1
1,4-Dichlorobenzene ND 04/26/2016 10201.0 0.19 ug/L1
1,1-Dichloroethane ND 04/26/2016 10201.0 0.19 ug/L1
1,2-Dichloroethane ND 04/26/2016 10201.0 0.23 ug/L1
1,1-Dichloroethene ND 04/26/2016 10201.0 0.31 ug/L1
cis-1,2-Dichloroethene ND 04/26/2016 10201.0 0.20 ug/L1
trans-1,2-Dichloroethene ND 04/26/2016 10201.0 0.33 ug/L1
1,2-Dichloropropane ND 04/26/2016 10201.0 0.29 ug/L1
cis-1,3-Dichloropropene ND 04/26/2016 10201.0 0.30 ug/L1
trans-1,3-Dichloropropene ND 04/26/2016 10201.0 0.22 ug/L1
Ethylbenzene ND 04/26/2016 10201.0 0.21 ug/L1
2-Hexanone ND 04/26/2016 1020100.26 ug/L1
Methyl iodide (Iodomethane)ND 04/26/2016 10205.0 0.28 ug/L1
4-Methyl-2-pentanone ND 04/26/2016 1020100.29 ug/L1
Methylene chloride ND 04/26/2016 10201.0 0.42 ug/L1
Styrene ND 04/26/2016 10201.0 0.13 ug/L1
1,1,1,2-Tetrachloroethane ND 04/26/2016 10201.0 0.19 ug/L1
1,1,2,2-Tetrachloroethane ND 04/26/2016 10201.0 0.13 ug/L1
Tetrachloroethene ND 04/26/2016 10201.0 0.22 ug/L1
Tetrahydrofuran ND 04/26/2016 10205.0 0.57 ug/L1
Toluene ND 04/26/2016 10201.0 0.24 ug/L1
1,1,1-Trichloroethane ND 04/26/2016 10201.0 0.24 ug/L1
1,1,2-Trichloroethane ND 04/26/2016 10201.0 0.22 ug/L1
Trichloroethene ND 04/26/2016 10201.0 0.16 ug/L1
Trichlorofluoromethane ND 04/26/2016 10201.0 0.74 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 21 of 32
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ11786-001
11786 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
1,2,3-Trichloropropane ND 04/26/2016 10201.0 0.35 ug/L1
Vinyl acetate ND 04/26/2016 10205.0 1.0 ug/L1
Vinyl chloride ND 04/26/2016 10201.0 0.50 ug/L1
m+p - Xylenes ND 04/26/2016 10201.0 0.19 ug/L1
o - Xylenes ND 04/26/2016 10201.0 0.14 ug/L1
Xylenes (total)ND 04/26/2016 10201.0 0.32 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 22 of 32
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ11786-002
11786 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 67 04/26/2016 08476710060-1401
Acrylonitrile 99 04/26/2016 08479910070-1301
Benzene 48 04/26/2016 0847975070-1301
Bromochloromethane 52 04/26/2016 08471055070-1301
Bromodichloromethane 52 04/26/2016 08471035070-1301
Bromoform 49 04/26/2016 0847975070-1301
Bromomethane (Methyl bromide)52 04/26/2016 08471045060-1401
2-Butanone (MEK)85 04/26/2016 08478510060-1401
Carbon disulfide 54 04/26/2016 08471085060-1401
Carbon tetrachloride 57 04/26/2016 08471135070-1301
Chlorobenzene 49 04/26/2016 0847975070-1301
Chloroethane 53 04/26/2016 08471055060-1401
Chloroform 52 04/26/2016 08471035070-1301
Chloromethane (Methyl chloride)46 04/26/2016 0847925060-1401
1,2-Dibromo-3-chloropropane (DBCP)41 04/26/2016 0847825070-1301
Dibromochloromethane 51 04/26/2016 08471025070-1301
1,2-Dibromoethane (EDB)47 04/26/2016 0847935070-1301
Dibromomethane (Methylene bromide)49 04/26/2016 0847975070-1301
trans-1,4-Dichloro-2-butene 57 04/26/2016 08471145034-1421
1,2-Dichlorobenzene 49 04/26/2016 0847985070-1301
1,4-Dichlorobenzene 46 04/26/2016 0847935070-1301
1,1-Dichloroethane 53 04/26/2016 08471065070-1301
1,2-Dichloroethane 48 04/26/2016 0847975070-1301
1,1-Dichloroethene 53 04/26/2016 08471055070-1301
cis-1,2-Dichloroethene 50 04/26/2016 0847995070-1301
trans-1,2-Dichloroethene 51 04/26/2016 08471035070-1301
1,2-Dichloropropane 49 04/26/2016 0847985070-1301
cis-1,3-Dichloropropene 51 04/26/2016 08471035070-1301
trans-1,3-Dichloropropene 50 04/26/2016 08471005070-1301
Ethylbenzene 49 04/26/2016 0847985070-1301
2-Hexanone 99 04/26/2016 08479910060-1401
Methyl iodide (Iodomethane)50 04/26/2016 08471015070-1301
4-Methyl-2-pentanone 96 04/26/2016 08479610060-1401
Methylene chloride 52 04/26/2016 08471035070-1301
Styrene 50 04/26/2016 08471005070-1301
1,1,1,2-Tetrachloroethane 51 04/26/2016 08471025070-1301
1,1,2,2-Tetrachloroethane 45 04/26/2016 0847905060-1401
Tetrachloroethene 51 04/26/2016 08471035070-1301
Tetrahydrofuran 44 04/26/2016 0847895070-1301
Toluene 50 04/26/2016 08471005070-1301
1,1,1-Trichloroethane 53 04/26/2016 08471065070-1301
1,1,2-Trichloroethane 46 04/26/2016 0847925070-1301
Trichloroethene 49 04/26/2016 0847995070-1301
Trichlorofluoromethane 57 04/26/2016 08471145070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 23 of 32
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ11786-002
11786 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,2,3-Trichloropropane 45 04/26/2016 0847895070-1301
Vinyl acetate 49 04/26/2016 0847985060-1401
Vinyl chloride 57 04/26/2016 08471135070-1301
m+p - Xylenes 52 04/26/2016 08471045070-1301
o - Xylenes 50 04/26/2016 08471015070-1301
Xylenes (total)100 04/26/2016 084710210070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 24 of 32
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Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:RD21041-001DU
11786 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)
Acetone ND 04/26/2016 18480.00 20ND1
Acrylonitrile ND 04/26/2016 18480.00 20ND1
Benzene 0.43 04/26/2016 1848J10200.48 1
Bromochloromethane ND 04/26/2016 18480.00 20ND1
Bromodichloromethane ND 04/26/2016 18480.00 20ND1
Bromoform ND 04/26/2016 18480.00 20ND1
Bromomethane (Methyl bromide)ND 04/26/2016 18480.00 20ND1
2-Butanone (MEK)ND 04/26/2016 18480.00 20ND1
Carbon disulfide ND 04/26/2016 18480.00 20ND1
Carbon tetrachloride ND 04/26/2016 18480.00 20ND1
Chlorobenzene 0.21 04/26/2016 1848J15200.25 1
Chloroethane ND 04/26/2016 18480.00 20ND1
Chloroform ND 04/26/2016 18480.00 20ND1
Chloromethane (Methyl chloride)ND 04/26/2016 18480.00 20ND1
1,2-Dibromo-3-chloropropane (DBCP)ND 04/26/2016 18480.00 20ND1
Dibromochloromethane ND 04/26/2016 18480.00 20ND1
1,2-Dibromoethane (EDB)ND 04/26/2016 18480.00 20ND1
Dibromomethane (Methylene bromide)ND 04/26/2016 18480.00 20ND1
trans-1,4-Dichloro-2-butene ND 04/26/2016 18480.00 20ND1
1,2-Dichlorobenzene ND 04/26/2016 18480.00 20ND1
1,4-Dichlorobenzene 1.0 04/26/2016 18488.0 201.1 1
1,1-Dichloroethane ND 04/26/2016 18480.00 20ND1
1,2-Dichloroethane ND 04/26/2016 18480.00 20ND1
1,1-Dichloroethene ND 04/26/2016 18480.00 20ND1
cis-1,2-Dichloroethene 0.63 04/26/2016 1848J7.6 200.58 1
trans-1,2-Dichloroethene ND 04/26/2016 18480.00 20ND1
1,2-Dichloropropane ND 04/26/2016 18480.00 20ND1
cis-1,3-Dichloropropene ND 04/26/2016 18480.00 20ND1
trans-1,3-Dichloropropene ND 04/26/2016 18480.00 20ND1
Ethylbenzene ND 04/26/2016 18480.00 20ND1
2-Hexanone ND 04/26/2016 18480.00 20ND1
Methyl iodide (Iodomethane)ND 04/26/2016 18480.00 20ND1
4-Methyl-2-pentanone ND 04/26/2016 18480.00 20ND1
Methylene chloride ND 04/26/2016 18480.00 20ND1
Styrene ND 04/26/2016 18480.00 20ND1
1,1,1,2-Tetrachloroethane ND 04/26/2016 18480.00 20ND1
1,1,2,2-Tetrachloroethane ND 04/26/2016 18480.00 20ND1
Tetrachloroethene ND 04/26/2016 18480.00 20ND1
Tetrahydrofuran ND 04/26/2016 18480.00 20ND1
Toluene ND 04/26/2016 18480.00 20ND1
1,1,1-Trichloroethane ND 04/26/2016 18480.00 20ND1
1,1,2-Trichloroethane ND 04/26/2016 18480.00 20ND1
Trichloroethene ND 04/26/2016 18480.00 20ND1
Trichlorofluoromethane ND 04/26/2016 18480.00 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 25 of 32
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:RD21041-001DU
11786 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)
1,2,3-Trichloropropane ND 04/26/2016 18480.00 20ND1
Vinyl acetate ND 04/26/2016 18480.00 20ND1
Vinyl chloride ND 04/26/2016 18480.00 20ND1
Xylenes (total)ND 04/26/2016 18480.00 20ND1
m+p - Xylenes ND 04/26/2016 18480.00 20ND1
o - Xylenes ND 04/26/2016 18480.00 20ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 104 70-130
Bromofluorobenzene 100 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 26 of 32
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:RD21041-002MS
11786 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Acetone 120 04/26/2016 191112110060-140ND1
Acrylonitrile 110 04/26/2016 191110610070-122ND1
Benzene 50 04/26/2016 19111005072-127ND1
Bromochloromethane 53 04/26/2016 19111065070-130ND1
Bromodichloromethane 52 04/26/2016 19111035071-143ND1
Bromoform 49 04/26/2016 1911995065-131ND1
Bromomethane (Methyl bromide)52 04/26/2016 19111055036-168ND1
2-Butanone (MEK)100 04/26/2016 191110210060-140ND1
Carbon disulfide 57 04/26/2016 19111155060-140ND1
Carbon tetrachloride 59 04/26/2016 19111185037-166ND1
Chlorobenzene 49 04/26/2016 1911975078-129ND1
Chloroethane 55 04/26/2016 19111105060-140ND1
Chloroform 53 04/26/2016 19111055063-123ND1
Chloromethane (Methyl chloride)49 04/26/2016 1911985020-158ND1
1,2-Dibromo-3-chloropropane (DBCP)40 04/26/2016 1911815070-130ND1
Dibromochloromethane 50 04/26/2016 19111015074-134ND1
1,2-Dibromoethane (EDB)48 04/26/2016 1911965070-130ND1
Dibromomethane (Methylene bromide)49 04/26/2016 1911985070-130ND1
trans-1,4-Dichloro-2-butene 46 04/26/2016 1911915034-142ND1
1,2-Dichlorobenzene 47 04/26/2016 1911945070-130ND1
1,4-Dichlorobenzene 44 04/26/2016 1911895070-130ND1
1,1-Dichloroethane 55 04/26/2016 19111095069-132ND1
1,2-Dichloroethane 49 04/26/2016 1911975059-143ND1
1,1-Dichloroethene 57 04/26/2016 19111155050-132ND1
cis-1,2-Dichloroethene 50 04/26/2016 19111015070-130ND1
trans-1,2-Dichloroethene 54 04/26/2016 19111085067-141ND1
1,2-Dichloropropane 50 04/26/2016 1911995071-126ND1
cis-1,3-Dichloropropene 48 04/26/2016 1911965069-130ND1
trans-1,3-Dichloropropene 47 04/26/2016 1911935073-131ND1
Ethylbenzene 49 04/26/2016 1911995079-132ND1
2-Hexanone 110 04/26/2016 191111210060-140ND1
Methyl iodide (Iodomethane)52 04/26/2016 19111045070-130ND1
4-Methyl-2-pentanone 100 04/26/2016 191110510060-140ND1
Methylene chloride 53 04/26/2016 19111075069-129ND1
Styrene 48 04/26/2016 1911975070-130ND1
1,1,1,2-Tetrachloroethane 50 04/26/2016 19111015070-130ND1
1,1,2,2-Tetrachloroethane 46 04/26/2016 1911925060-155ND1
Tetrachloroethene 52 04/26/2016 19111055070-130ND1
Tetrahydrofuran 52 04/26/2016 19111045070-130ND1
Toluene 50 04/26/2016 19111005075-125ND1
1,1,1-Trichloroethane 55 04/26/2016 19111105077-132ND1
1,1,2-Trichloroethane 48 04/26/2016 1911965077-132ND1
Trichloroethene 51 04/26/2016 19111025073-124ND1
Trichlorofluoromethane 55 04/26/2016 19111095041-173ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 27 of 32
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:RD21041-002MS
11786 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
1,2,3-Trichloropropane 46 04/26/2016 1911925070-130ND1
Vinyl acetate 41 04/26/2016 1911825060-140ND1
Vinyl chloride 59 04/26/2016 19111195029-159ND1
Xylenes (total)100 04/26/2016 191110210070-130ND1
m+p - Xylenes 52 04/26/2016 19111045070-130ND1
o - Xylenes 50 04/26/2016 19111005070-130ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 100 70-130
Bromofluorobenzene 98 70-130
Toluene-d8 103 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 28 of 32
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Shealy Environmental Services, Inc.

ICP-MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:RQ11519-001
11519 3005A
04/22/2016 841Analytical Method:6020A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Antimony ND 04/25/2016 15161.0 0.17 ug/L1
Arsenic ND 04/25/2016 15161.0 0.26 ug/L1
Barium ND 04/25/2016 15165.0 0.53 ug/L1
Beryllium ND 04/25/2016 15160.40 0.12 ug/L1
Cadmium ND 04/25/2016 15160.10 0.044 ug/L1
Chromium ND 04/25/2016 15165.0 0.63 ug/L1
Cobalt ND 04/25/2016 15165.0 0.26 ug/L1
Copper 0.25 04/25/2016 1516J1.0 0.15 ug/L1
Lead ND 04/25/2016 15161.0 0.15 ug/L1
Nickel ND 04/25/2016 15165.0 0.63 ug/L1
Selenium ND 04/25/2016 15161.0 0.95 ug/L1
Silver ND 04/25/2016 15161.0 0.17 ug/L1
Thallium ND 04/25/2016 15160.50 0.075 ug/L1
Vanadium ND 04/25/2016 15165.0 1.0 ug/L1
Zinc ND 04/25/2016 1516101.6 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 29 of 32
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Shealy Environmental Services, Inc.

ICP-MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:RQ11519-002
11519 3005A
04/22/2016 841Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Antimony 100 04/25/2016 152210010080-1201
Arsenic 100 04/25/2016 152210110080-1201
Barium 100 04/25/2016 152210310080-1201
Beryllium 100 04/25/2016 152210210080-1201
Cadmium 99 04/25/2016 15229910080-1201
Chromium 99 04/25/2016 15229910080-1201
Cobalt 100 04/25/2016 152210110080-1201
Copper 100 04/25/2016 152210210080-1201
Lead 100 04/25/2016 152210110080-1201
Nickel 100 04/25/2016 152210010080-1201
Selenium 100 04/25/2016 152210510080-1201
Silver 100 04/25/2016 152210410080-1201
Thallium 100 04/25/2016 152210210080-1201
Vanadium 99 04/25/2016 15229910080-1201
Zinc 100 04/25/2016 152210110080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 30 of 32
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Shealy Environmental Services, Inc.

ICP-MS - MS
Batch:Prep Method:
Prep Date:
Sample ID:RD21041-001MS
11519 3005A
04/22/2016 841Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Antimony 100 04/25/2016 153210410070-1300.23 1
Arsenic 100 04/25/2016 153210210070-130ND1
Barium 230 04/25/2016 153210410070-1301301
Beryllium 100 04/25/2016 153210210070-130ND1
Cadmium 100 04/25/2016 153210010070-1300.43 1
Chromium 100 04/25/2016 153210110070-130ND1
Cobalt 120 04/25/2016 153210210070-130151
Copper 100 04/25/2016 153210410070-1300.32 1
Lead 100 04/25/2016 153210410070-130ND1
Nickel 110 04/25/2016 153210210070-1304.0 1
Selenium 100 04/25/2016 153210410070-130ND1
Silver 100 04/25/2016 153210410070-130ND1
Thallium 100 04/25/2016 153210410070-1300.086 1
Vanadium 100 04/25/2016 153210110070-130ND1
Zinc 120 04/25/2016 15329910070-130171
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 31 of 32
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Shealy Environmental Services, Inc.

ICP-MS - MSD
Batch:Prep Method:
Prep Date:
Sample ID:RD21041-001MD
11519 3005A
04/22/2016 841Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Antimony 100 04/25/2016 153710010070-1303.1 200.23 1
Arsenic 98 04/25/2016 15379810070-1304.4 20ND1
Barium 230 04/25/2016 153710110070-1301.3 201301
Beryllium 100 04/25/2016 153710210070-1300.49 20ND1
Cadmium 97 04/25/2016 15379610070-1303.8 200.43 1
Chromium 98 04/25/2016 15379810070-1303.1 20ND1
Cobalt 110 04/25/2016 15379910070-1302.9 20151
Copper 100 04/25/2016 153710010070-1304.5 200.32 1
Lead 100 04/25/2016 153710110070-1302.8 20ND1
Nickel 100 04/25/2016 15379910070-1302.5 204.0 1
Selenium 100 04/25/2016 153710110070-1302.2 20ND1
Silver 100 04/25/2016 153710110070-1302.4 20ND1
Thallium 100 04/25/2016 153710210070-1302.5 200.086 1
Vanadium 99 04/25/2016 15379910070-1302.8 20ND1
Zinc 110 04/25/2016 15379610070-1302.5 20171
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 32 of 32
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Shealy Environmental Services, Inc.

Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.