0201_AlexanderCountyCDLF_GWMReport_DIN26444_20160107

Alexander County Active C&D and Closed MSWLF
Taylorsville, North Carolina
January 2016
MESCO Project Number: G15003.0
Semi-Annual Water Quality Monitoring Report
with Corrective Action Update
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
Permit Number: 02-01
P.O. Box 97
Garner, NC 27529
P.E. License No. C-0281

TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 2
Groundwater Samples Page 3
Surface Water Samples Page 3
Groundwater and Surface Water Characterization Page 3
Corrective Action Update Page 3
MNA Analysis (AOCs MW-16, MW-24, MW-26) Page 3
Phytoremediation (AOC MW-24) Page 4
Enhanced Bioremediation via Substrate Injection (AOC MW-26) Page 4
Landfill Gas Extraction (AOC MW-1B) Page 4
Findings Page 4
Closing Page 5
FIGURES
Topographic Map with Site Location Figure 1
Potentiometric Map of Uppermost Aquifer w/ VOCs Detected Above 2L Standards Figure 2
Time Series Graph of Groundwater, Precipitation & Tree Size Figure 3
Total VOCs and Benzene Concentrations Pre/Post Injection Comparison in AOC MW-26 Figure 4
Histograms of Dissolved Methane Concentrations Figure 5
Histograms of Total VOC Concentrations Figure 6
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, GWP, 2L, 2B or MCL Table 5
Hydrologic Properties at Monitoring Well Locations Table 6
MNA Parameter Data Summary Table 7
Phytoremediation Tree Measurement Summary Table 8
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Parameter Data Sheet(s) Appendix B
April 12, 2016
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
Division of Waste Management/ NCDEQ
2090 US Highway 70
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report with Corrective Action Update
Alexander County Active C&D and Closed MSWLF
Permit No. 02-01
MESCO Project No. G15003.0 Event Date(s): January 5-8, 2016
Introduction
On behalf of Alexander County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present
this Semi-Annual Water Quality Monitoring Report with Corrective Action Update for an event performed at the
Alexander County active construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)
on January 5-8, 2016. NCDENR Solid Waste Rules 15A NCAC 13B.1632 requires that Alexander County provide
this report to the NC Solid Waste Section (SWS) on a semi-annual basis. Laboratory analytical results indicate one
or more volatile organic compounds (VOCs) continue to persist at levels above the 2L Standard in samples collected
from 8 wells that monitor the uppermost aquifer but concentrations continue to decrease over time and distance.
Surface water samples did not contain contaminant concentrations in excess of the 2B Surface Water Standard.
Corrective action to remediate VOCs in groundwater is ongoing within the four areas of concern (AOC) with
updated information presented herein.
Background
The Alexander County active C&D and closed MSWLF, is located at 2500 Paynes Dairy Road near Taylorsville
North Carolina. The total waste footprint encompasses approximately 24 acres situated on 283 contiguous acres.
The site location topographic map is depicted in the attached Figure 1.
The closed MSWLF ceased operation prior to 1998 and the C&D landfill continues operation owo Assessment and
Corrective Action (ACM) reports dated August 27, 2002 and April 11, 2008. MESCO then developed a Corrective
Action Plan-Revision 1 (CAP-Rev 1) on February 6, 2009. In response to improved water quality and changing
geochemical conditions the originally selected remediation approach was amended by MESCO in a Corrective
Action Plan-Addendum (CAP-Add) dated December 20, 2010. Groundwater remediation efforts have been
implemented at the four distinct areas of concern (AOCs) which are identified as MW-1B, MW-16, MW-24 and
MW-26. Remediation technologies initiated to date with reference to their respective AOC include monitored
natural attenuation (MNA) (MW-16, MW-24, MW-26), phytoremediation (MW-24), enhanced bioremediation via
substrate injection (MW-26) and landfill gas (LFG) extraction (MW-1B). Following establishment of the two year
MNA baseline MESCO completed a Corrective Action Evaluation Report (CAER) (DIN 13596) on March 22, 2011.
Based on improved water quality conditions as demonstrated in the CAER the parameters and frequencies of future
monitoring events were established by the SWS CAER review response (DIN 14150) dated June 16, 2011.

A second CAP-Add was submitted by MESCO dated May 30, 2013 as requested by the SWS in a letter entitled
Compliance Boundary (Relevant Point of Compliance) (DIN 18502) dated February 18, 2013. A Request for
Appendix II Groundwater Monitoring Modification (DIN 20137) was submitted by MESCO dated November 8, 2013
which was subsequently approved by the SWS (DIN 20144) on November 13, 2013.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS
memorandums this report contains sampling procedures, field and laboratory results, corrective action update,
ground/surface water characterization, and findings. Well construction summary table, field observations table, field
parameter data table, sampling and analysis summary table, detections compared to Standards tables, a groundwater
flow directions/rates table, potentiometric map, time-series graph, quality assurance/quality control data, and
laboratory analytical data results are enclosed herein.
Sampling Procedures
MESCO personnel performed this sampling event following the parameters and frequency established by the SWS
review response to the (CAER) (Doc ID 14150) dated June 16, 2011 and the SWS approved Request for Appendix II
Groundwater Monitoring Modification (DIN 20137). The water quality monitoring program includes a combination
of detection, assessment and corrective action monitoring with specifically defined analysis.
Water samples were collected from all monitoring locations outlined in the CAP-Add and CAER with the exception
of MW-1A; which has been chronically dry. Monitoring locations are depicted on the potentiometric map (Figure 2).
Sampling was performed per the protocols outlined in the Groundwater and Surface Water Sampling and Analysis
Plan included as Appendix B of the approved CAP-Add. A summary detailing the construction of the water
monitoring wells is presented on Table 1. The function and integrity of all monitoring locations were visually
evaluated and limited deficiencies identified as documented on Table 2. The depth to water in each well was
electronically gaged prior to purging to quantify the static water level elevation. Low-flow pumping or bailing was
utilized to purge the wells a minimum of three times the volume of standing water in the well or until dry. Surface
water samples were collected from previously designated locations along discharge features. During well purging
and surface water sample collection the required field parameters were recorded. The samples were then placed into
laboratory-prepared, pre-preserved containers via a new disposable polyethylene bailer. Samples were collected, kept
on ice, and transported to a NC-certified laboratory under proper chain of custody (C-O-C) protocols and within the
specified hold times for each analysis.
Field Parameter Data
Field parameters were recorded including depth to water, pH, specific conductance, temperature, dissolved oxygen
(DO), oxidation reduction potential (ORP), total dissolved solids (TDS), and turbidity. A summary of the field
parameter data is presented in Table 3 and the field sampling data sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Services Inc. (PACE) of Huntersville/Asheville, NC performed the laboratory analyses. All water
samples were tested for the constituents listed in 40CFR258 Appendix I. Corrective action monitoring (Appendix I
plus a subset of MNA parameters previously approved by SWS) was also performed on 9 wells (MW-3, MW-5,
MW-6, MW-11, MW-12, MW-12D, MW-24, MW-26 and MW-31). Samples collected from 8 wells were tested for
mercury including both total and dissolved at MW-1B as part of of the approved assessment monitoring program.
Additionally; supplemental samples MW-1 and MW-1B were analyzed for dissolved methane to assess remediation
progress. Quality control measures implemented during this event included submittal and subsequent quantification
of equipment (EB), field (FB), and travel (TB) blanks. A sampling and analysis table summarizing the locations,
laboratory, target analytes and methods is presented as Table 4. Laboratory results and C-O-Cs are presented in
Appendix A.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 5 summarizes App I constituents detected in groundwater and
surface water samples that attain or were above the current SWSL, Groundwater Protection Standards (GWP), North
Carolina Groundwater Standards (2L), the applicable North Carolina Surface Water Standards (2B) for a class C
waterbody and Maximum Contaminant Levels (MCL) also known as “Federal Primary Drinking Water Standards”.
2
Quality Control Samples
Thallium was detected in the quality control blank (EB) above GWP, 2B and MCL Standards. Since thallium was
not detected in any other sample the suspected field/lab induced artifact contamination is effectively non-
consequential.
Groundwater Samples
The only metals detected in exceedance of it's respective NC 2L Standard was total mercury in sample MW-1B and
total chromium in sample MW-13. Further analysis indicates that dissolved mercury was not detected in MW-1B.
The VOCs detected in concentrations exceeding their respective 2L Standard during this event were aromatics
benzene (MW-1, MW-3, MW-4R, MW-5, MW-7, MW-11, MW-12, MW-15 and MW-16) and para-dichlorobenzene
(MW-3, MW-11 and MW-12). Chlorinated hydrocarbons tetrachloroethane and 1,1-dichloroethane were also
detected above their respective 2L Standards in sample MW-16.
Although not applicable for regulatory compliance evaluation all contaminants remain below federally established
primary “Drinking Water Standards” except for benzene in MW-3 and total cadmium in MW-13.
A site map depicting the spatial distribution of VOC concentrations exceeding the 2L Standard during this sampling
event is shown in Figure 2.
Surface Water Samples
None of the targeted constituents were detected in any surface water sample in levels above the NC 2B Surface Water
Standards.
Groundwater and Surface Water Characterization
At the landfill, groundwater flow direction generally mirrors topography, thus flow direction is from higher to lower
elevations as shown on the potentiometric map included as Figure 2. Locally, groundwater flow is expected to be
generally westerly toward the Lower Little River, and southerly toward the Catawba River (Figure 1). Groundwater
linear velocity rates calculated using modified Darcy's equation varied greatly and were slower in the upper bedrock
fracture system than the less prominent regolith (Table 6). Streams at designated monitoring points were visually
observed to be of normal seasonal volume, flow rate and low turbidity. Hydrogeologic parameters appear generally
consistent with historical observations.
Corrective Action Update
Groundwater remediation continues to be implemented at the four AOCs designated in the CAP-Add. Groundwater
remediation per the CAP-Add is expected to continue until the SWS authorizes a change. General background
information and activities performed since the CAER and last semi-annual event are briefly presented in the following
sections.
MNA Analysis (AOCs MW-16, MW-24, MW-26)
Semi-annual MNA monitoring of 14 wells for the full suite of SWS recommended parameters was initiated on June
30, 2009 and performed for four consecutive semi-annual events to establish a baseline per the CAP-Revision 1. The
number of wells requiring MNA analysis was reduced to 10 and the parameters and frequency were also amended per
the SWS CAER review response (DIN 14150) dated June 16, 2011. Establishment of the MNA baseline concluded in
December 2012 at MW-33 and MW-34. MNA data collected during this period is presented on Table 7.
Following the acquisition of a 15.7 acre parcel from Crescent Resources on March 3, 2011, extension of the eastern
relative point of compliance downgradient of AOC MW-16 has been approved with conditions by the SWS on
February 18, 2013 (DIN:18502). Recordation of Survey Plat titled Survey For Notice of Contaminated Site
Alexander County Landfill and A Notice and SWS approved Declaration of Perpetual Land Use Restrictions for this
parcel has remained at the Alexander County Register of Deeds Office since November 13, 2012. The SWS
approved CAP-Add dated May 30, 2013 clarifies that groundwater remediation of AOC MW-16 will remain as only
MNA, rather than any other technologies described in the preceding CAP-Add.
3
Phytoremediation (AOC MW-24)
County personnel planted about 200 hybrid poplar trees over an approximate one acre area between MW-7 and MW-
12 in May 2010 in an effort to phytoremediate groundwater in the MW-24 AOC. The County continued to maintain
the fence-enclosed stand during this semi-annual period which included continuous supplemental watering and
eradication of competing vegetation. MESCO personnel continued quarterly tree growth monitoring by recording
measurements of ten designated sample trees on September 25, 2015 and January 8, 2016. The foliage appeared
more yellow then past Septembers and trees were dormant in January. The average tree has grown considerably
(222” or 584%) over the past 5+ years (Table 8 and Figure 3).
MESCO personnel deployed dedicated pressure transducers in MW-7 and MW-12 on August 12, 2010 to record daily
water levels. Groundwater level fluctuations were downloaded and transducers re-zeroed on September 25, 2015 and
January 6, 2016. In addition, daily precipitation amounts are periodically obtained from the National Weather
Services Cooperative Observer Program Station 318519 database.
A time series-graph depicting the correlation between tree growth, groundwater fluctuation and precipitation since the
stand has been in place is presented on Figure 3. Data continues to suggest both MW-7 and MW-12 water level
variations mirror each other and both respond quickly to precipitation events. Total cumulative VOC concentrations
in AOC MW-24 during this event have have decreased 15% compared to its respective 2 year baseline established in
2010 and statistical trend analysis indicates that an increasing trend is not evident. The phytoremediation zone has not
been established long enough to make a valid assessment of the effectiveness as a remediation measure. The
phytoremediation area will continue to be maintained and monitored on a quarterly basis.
Enhanced Bioremediation via Substrate Injection (AOC MW-26)
In an attempt to remediate benzene as detected in MW-26, Bac-9 was injected 50 ft upgradient in IW-1 on February
17, 2011 following conditions in the Underground Injection Control (UIC) Permit WI0300160. The UIC permit was
renewed on January 31, 2013 and as directed by the UIC post-injection water quality monitoring of MW-3, MW-11,
MW-26, MW-27 and MW-31 is required on a semi-annual basis. During this event VOCs were not detected above
Standards in samples collected from MW-26 or MW-31 located at and beyond the compliance boundary respectively.
Most recent levels of total VOCs compared to the baseline established during the four events prior to injection
exhibited a reduction both upgradient (-52%) and downgradient (-96%) of the injection point. Most recently, total
cumulative VOCs from all samples in AOC MW-26 decreased 62% and benzene concentrations decreased 36%
compared to the baseline averages established during the four events performed over the two years preceding the
injection (Figure 4). Further injections are not planned at this time.
Landfill Gas Extraction (AOC MW-1B)
Three LFG extraction wells (MEW-1, MEW-2, MEW-3) were installed screening the majority of the vadose zone at
the northern border of the closed landfill in the vicinity of the scalehouse. MEW-1 was installed on August 17, 2010
with MEW-2 and MEW-3 installed on October 20, 2010. Well control heads were plumbed to a header pipe by the
County which was connected to a soil vacuum extraction (SVE) unit on July 5, 2012. An active LFG blower system
pilot study was performed by MESCO between June 14, 2012 and July 12, 2012 to evaluate the effectiveness a
vacuum would have on reducing levels of LFG in the soil which may remediate the low level VOCs detected in
groundwater hydraulically upgradient of the landfill. A comparison of LFG concentrations and pressures before and
after vacuum start-up indicated the system is capable of eliminating LFG migration at all locations monitored within
AOC MW-1B. The active LFG Collection Control System (LFGCCS) has been in continuous operation since
November 1, 2012 and been verified and documented by MESCO personnel on at least a quarterly basis to be
eliminating LFG migration through the vadose at all locations monitored beyond the extraction wells. Improvement
in groundwater quality has also been observed in response to implementation of the LFG extraction system.
Dissolved methane levels in groundwater have decreased considerably within MW-1 (-99%) and MW-1B (-97%) in
the 3+ years of operation (Figure 5). During this event total cumulative VOC concentrations within AOC MW-1B
have also exhibited a significant reduction (-82%) and exhibited a statistically significant decreasing trend compared
to the baseline established prior to initiation of remediation via LFG extraction (Figure 6). Levels of benzene have
remained below 2L Standards at MW-1B for two consecutive events following consistent detections the previous 13
years. The LFGCCS is planned to continue operation and will continue to be monitored and assessed on a quarterly
basis.
4
Figures
Topographic Map with Site Location
FIGURE 1
QUADRANGLE LEGEND
Alexander County Active C&D and Closed MSWLF
1/20 1 MILE
LANDFILL PROPERTY
N
2500 Paynes Dairy Road
Taylorsville, NC 28681
Lat:35-15-18.7246
Long:-81-08-51.51.32
Northing:767009.09
Easting:1363506.43
Figure 3
Time-Series Graphs - Groundwater, Precipitation & Tree Size
December 13, 2010 - January 6, 2016
0.505
0.507
0.586
0.602
0.443
0.413
0.532
0.252
0.096
0.096
0.096
0.096
0.338
0.453
0.256
0.368
Data Sources:
GW = Dedicated pressure transducers. Measurements recorded daily.
Precipitation = National Weather Services Cooperative Observer Program Station 318519. Measurements recorded daily.
Tree Size = Field measurements (Height + width + trunk circumference) of 10 designated sample trees. Measurements recorded quarterly.
0
5
10
15
20
25
30
12/4/2010 6/4/2011 12/4/2011 6/4/2012 12/4/2012 6/4/2013 12/4/2013 6/4/2014 12/4/2014 6/4/2015 12/4/2015
0
5
10
15
20
25
30
6/17/2015 7/17/2015 8/17/2015 9/17/2015 10/17/2015 11/17/2015 12/17/2015
MW-7 GW Fluctuation (Ft)
MW-12 GW Fluctuation (Ft)
Precipitation (in)
Average Tree Size (in x 10)
Alexander County Active CD Landfill and Closed MSWLF
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Figure 4
June 30, 2009 – January 9, 2016
Well ID Benzene Benzene Benzene Benzene Benzene Benzene
Up MW-3 61.66 8.10 43.03 7.20 31.50 6.00 37.04 6.10 43.31 6.85 24.30 5.90 -19.01 -0.95 -44 -14
Up MW-11 53.28 5.00 46.25 4.50 40.81 5.90 43.20 4.20 45.89 4.90 24.60 2.90 -21.29 -2.00 -46 -41
Up MW-27 23.70 0.00 20.20 0.00 24.60 0.00 28.00 0.00 24.13 0.00 5.30 0.00 -18.83 0.00 -78 0
138.64 13.10 109.48 11.70 96.91 11.90 108.24 10.30 113.32 11.75 54.20 8.80 -59.12 -2.95 -52 -25
Down MW-26 39.40 1.40 20.00 1.40 39.50 3.20 29.00 1.60 31.98 1.90 1.20 0.00 -30.78 -1.90 -96 -100
Down MW-31 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 0
39.40 1.40 20.00 1.40 39.50 3.20 29.00 1.60 31.98 1.90 1.20 0.00 -30.78 -1.90 -96 -100
Up&Down Gradient Total 178.04 14.50 129.48 13.10 136.41 15.10 137.24 11.90 145.29 13.65 55.40 8.80 -89.89 -4.85 -62 -36
Total VOCs and Benzene Concentrations Pre/Post Injection Comparison in AOC MW-26
Total VOCs & Benzene Concentrations Pre/Post Injection Comparison in AOC MW-26
Hydraulic
Gradient In
Relation to
Injection
Well (IW-1)
June 2009 (ug/L)Dec. 2009 (ug/L)July 2010 (ug/L)Dec. 2010 (ug/L)
Average of Four Events Preceding Injection (ug/L)Jan. 2016 (ug/L)
Difference Between Current and Baseline (ug/L)
Difference Between Current and Baseline (%)
All
VOCs
All
VOCs
All
VOCs
Benzen
e
All
VOCs
Benzen
e All VOCs
All
VOCs
All
VOCs
All
VOCs
Subtotal Upgradient
Subtotal Downgradient
2L
2/
1
7 /2
01
1
2/1
7
/
2
0
1
1
Ba
c
-
9

I
n
j
e
c
t
e
d
Ba
c
-
9

I
n
j
e
c
t
e
d
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Figure 5
Histograms of Dissolved Methane Concentrations
AOC ID WELL ID
DISSOLVED DISSOLVED DISSOLVED DISSOLVED DISSOLVED
METHANE METHANE METHANE METHANE METHANE REDUCTION
Post-Start Up Post-Start Up Post-Start Up Post-Start Up SINCE
06/15/12 06/27/13 06/26/14 06/16/15 01/06/16 START-UP
(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(%)
MW-1B
MW-1 6.78 0.08 0.00153 0.07580 0.0332 -99
MW-1A NS NS NS NS NS NA
MW-1B 1.90 0.69 ND<0.0004 0.099 0.0511 -97
MW-18 NS NS NS NS NS NA
MW-19 NS NS NS NS NS NA
AOC AVG 4.34 0.39 0.0009 0.0873 0.0422 -99
NS = Not sampled since not impacted
Pre-LFGCCS (June 15, 2012) Compared to Post-LFGGCCS (January 6, 2016)
Pre-Start Up
JU
NE 2
0
12 (
Pre)
JU
NE 2
013 (Po
st)
JU
NE 2
0
14 (Po
st)
DEC 2014 (Po
st)
JU
NE 2
015 (Pos
t
)
JA
N
2016 (Pos
t)
0
0.5
11.522.5
3
3.5
4
4.5
5
5.5
6
6.5
7
DISSOLVED METHANE IN GROUNDWATER
MW-1
MW-1B
DATES
m g/
L
Ex
t
r
a
c
t
i
o
n
St
a
r
t
e
d
NOV. 2012
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Figure 6
Histograms of Total VOC Concentrations
Baseline (June 24, 2009-December 9, 2010) Compared to January 2016
AOC ID WELL ID
MW-1B
MW-1 25.22 4.40 -20.82 -83
MW-1A NS NS NA NA
MW-1B 15.66 3.80 -11.86 -76
MW-18 0.00 0.00 0.00 0
MW-19 3.48 0.00 -3.48 -100
AOC AVG 11.09 2.05 -9.04 -82
MW-16
MW-5 18.39 14.40 -3.99 -22
MW-10 2.17 0.00 -2.17 -100
MW-16 44.14 31.50 -12.64 -29
MW-32 0.00 0.00 0.00 0MW-33 0.00 0.00 0.00 0MW-34 0.00 0.00 0.00 0
AOC AVG 10.78 7.65 -3.13 -29
MW-24
MW-7 12.69 3.70 -1.29 -71
MW-12 30.94 20.50 -10.44 -34
MW-12D 0.00 0.00 0.00 0
MW-24 1.56 0.00 -1.56 -100
MW-25 0.30 0.00 -0.30 -100
AOC AVG 9.10 7.75 -1.35 -15
MW-26
MW-3 43.31 24.30 -19.01 -44
MW-11 45.89 24.60 -21.29 -46
MW-26 31.98 1.20 -30.78 -96
MW-27 24.13 5.30 -18.83 -78
MW-31 0.00 0.00 0.00 0
AOC AVG 29.06 11.08 -17.98 -62
MW-2 27.19 0.00 -27.19 -100
MW-4R 25.00 12.00 -13.00 -52
MW-6 0.00 0.00 0.00 0
MW-9 18.51 9.70 -8.81 -48
MW-13 0.00 0.00 0.00 0
MW-14 11.93 8.90 -3.03 -25
MW-15 12.83 10.30 -2.53 -20
MW-17 2.27 0.00 -2.27 -100
MW-20 0.59 0.00 -0.59 -100
MW-21 0.28 0.00 -0.28 -100
MW-22 2.70 0.00 -2.70 -100
MW-23 0.51 0.00 -0.51 -100AOC AVG 8.48 3.41 -5.08 -60ALL WELLS ALL WELLS AVG 12.55 5.46 -7.10 -57
NS = Not sampled since dry
TOTAL VOC(s) BASELINE
AVERAGE
(June 2009-
Dec. 2010)
(ug/l)
TOTAL VOC(s)
LATEST
Jan. 2016
(ug/l)
DIFFERENCE BETWEEN
LATEST AND
BASELINE (ug/L)
DIFFERENCE BETWEEN
LATEST AND
BASELINE
(%)

STATISTICAL
TREND*
Between June
2009 – Jan.
2016
flDownwardfl
«No Trend«
flDownwardfl
«No Trend«
«No Trend«
flDownwardfl
«No Trend«
«No Trend«
«No Trend«
«No Trend«
«No Trend«
«No Trend«
«No Trend«
«No Trend«
flDownwardfl
«No Trend«
«No Trend«
«No Trend«
«No Trend«
flDownwardfl
flDownwardfl
«No Trend«
flDownwardfl
«No Trend«
flDownwardfl
Undesignated
(No
Remediation)
flDownwardfl
flDownwardfl
«No Trend«
flDownwardfl
«No Trend«
«No Trend«
«No Trend«
«No Trend«
«No Trend«
«No Trend«
«No Trend«
«No Trend«
flDownwardfl
flDownwardfl
* = Statistical trend analysis of all events between June 2009 and January 2016 via Sen's Slope Estimator at both a 90% or 95% Confidence Level
MW-1B MW-16 MW-26 MW-24 UNDESIGNATED SITEWIDE
0
2.5
5
7.5
10
12.5
15
17.5
20
22.5
25
27.5
30
TOTAL VOC(s) BASELINE AVERAGE COMPARED TO JAN. 2016
BASELINE AVERAGE
JAN 2015
AREA OF CONCERN
ug
/L
Tables
Alexander County Active C04/06/2016 and Closed MSWLF Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
January 5-8, 2016
Latitude Longitude
(inches)(ft)
MW-1 9/14/90 2 40.00 25.00 15 Soil & Rock 1080.54 1077.98 1045.75 34.79 35.8389 -81.1478
MW-1A 9/30/94 2 47.50 32.50 15 Soil & Rock 1085.32 1083.28 <1035.78 Dry (>49.54)35.8389 -81.1478
MW-1B 5/21/03 2 61.00 46.00 15 Rock 1082.56 1079.56 1041.01 41.55 35.8391 -81.1478
MW-2 9/6/90 2 30.00 15.00 15 Soil 1004.48 1002.28 985.64 18.84 35.8376 -81.1524
MW-3 9/19/90 2 33.00 13.00 20 Soil & Rock 1024.73 1024.23 998.85 25.88 35.8365 -81.1503
MW-4R 9/30/94 2 20.50 5.50 15 Soil & Rock 1012.64 1008.54 998.49 14.15 35.8366 -81.1479
MW-5 9/16/94 2 48.80 33.80 15 Soil & Rock 1051.26 1049.01 1012.30 38.96 35.8373 -81.1465
MW-6 9/29/94 2 41.00 26.00 15 Rock 1010.79 1008.29 989.07 21.72 35.8369 -81.1364
MW-7 9/29/94 2 53.00 38.00 15 Rock 1009.24 1005.84 970.36 38.88 35.8364 -81.1522
MW-9 10/24/00 2 31.50 16.50 15 Rock 996.27 993.76 986.22 10.05 35.8361 -81.1481
MW-10 10/25/00 2 91.00 76.00 15 Rock 1040.80 1037.83 1004.59 36.21 35.8366 -81.1469
MW-11 10/24/00 2 56.00 41.00 15 Rock 1011.96 1008.98 978.93 33.03 35.8359 -81.1505
MW-12 10/23/00 2 66.50 51.50 15 Soil 1007.35 1004.46 955.85 51.50 35.3577 -81.1525
MW-12D 6/9/00 2 100.00 90.00 10 Rock 1008.46 1006.03 949.91 58.55 35.3577 -81.1525
MW-13 10/25/00 2 60.50 45.50 15 Rock 1004.56 1001.63 973.05 31.51 35.8368 -81.1532
MW-14 10/26/00 2 40.50 25.50 15 Soil & Rock 997.44 994.06 965.60 31.84 35.8376 -81.1525
MW-15 10/25/00 2 35.00 20.00 15 Soil & Rock 1023.44 1020.81 1002.29 21.15 35.8385 -81.1508
MW-16 12/20/07 2 40.25 25.25 15 Rock 1037.56 1034.94 1008.88 28.68 35.8371 -81.1465
MW-17 6/10/03 2 22.30 7.30 15 Rock 991.16 988.36 975.96 15.20 35.8386 -81.1511
MW-18 12/19/07 2 56.70 41.70 15 Rock 1084.33 1081.52 1031.89 52.44 35.8392 -81.1467
MW-19 12/20/07 2 63.92 48.92 15 Rock 1071.48 1068.67 1019.33 52.15 35.8391 -81.1487
MW-20 12/20/07 2 63.55 48.55 15 Rock 1046.92 1044.19 1006.54 40.38 35.8391 -81.1502
MW-21 12/19/07 2 41.05 26.05 15 Rock 990.00 987.08 962.29 27.71 35.8386 -81.1514
MW-22 12/19/07 2 18.12 8.12 10 Rock 958.97 956.21 943.94 15.03 35.8381 -81.1524
MW-23 12/19/07 2 21.54 6.54 15 Soil 950.48 947.83 934.76 15.72 35.8376 -81.1529
MW-24 12/20/07 2 35.35 20.35 15 Soil 974.04 971.29 944.65 29.39 35.8356 -81.1533
MW-25 12/19/07 2 44.48 29.48 15 Rock 981.93 979.93 955.74 26.19 35.8353 -81.1528
MW-26 12/20/07 2 49.80 34.80 15 Rock 990.69 988.08 976.55 14.14 35.8354 -81.1504
MW-27 12/20/07 2 49.82 34.82 15 Rock 992.19 989.19 980.37 11.82 35.8356 -81.1493
MW-31 8/16/10 2 32.56 17.56 15 Soil 985.42 982.42 975.07 10.35 35.8348 -81.1506
MW-32 8/16/10 2 42.70 27.7 15 Rock 1025.26 1022.26 994.41 30.85 35.8361 -81.1469
MW-33 4/27/13 2 21.38 6.38 15 PWR 1007.40 1004.40 994.71 12.69 35.8367 -81.1462
MW-34 4/27/13 2 21.19 6.19 15 PWR 1014.60 1011.60 1006.67 7.93 35.8373 -81.1459
IW-1 2/14/11 4 52.44 37.44 15 Rock 990.44 987.44 NR NR 35.8356 -81.1504
NOTE:
PWR = partially weathered rock
Monitoring
Well
Date
Installed
Well
Diameter
Total Well
Depth
Top of
Screen
Depth
Screen
Length Geology of Screened
Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
January 5-7, 2016
Locked Comments
MW-1 Yes Yes Yes Yes Yes Yes
MW-1A No Yes Yes Yes Yes Yes Dry which is typical
MW-1B Yes Yes Yes Yes Yes Yes
MW-2 Yes Yes Yes Yes Yes ?Surface pad covered with soil
MW-3 Yes Yes Yes Yes Yes Yes Slow recharge
MW-4R Yes Yes Yes Yes Yes Yes Purge water has sulfur smell.
MW-5 Yes Yes Yes Yes Yes ?Surface pad covered with soil
MW-6 Yes Yes Yes Yes Yes Yes
MW-7 Yes Yes Yes Yes Yes Yes
MW-9 Yes Yes Yes Yes Yes Yes Not able to purge dry which is atypical
MW-10 Yes Yes Yes Yes Yes Yes Purge water has sulfur smell. Very slow recharge
MW-11 Yes Yes Yes Yes Yes Yes
MW-12 Yes Yes Yes Yes Yes Yes
MW-12D Yes Yes Yes Yes Yes Yes
MW-13 Yes Yes Yes Yes Yes Yes
MW-14 Yes Yes Yes Yes Yes ?Surface pad cracked
MW-15 Yes Yes Yes Yes Yes Yes
MW-16 Yes Yes Yes Yes Yes ?Surface pad covered with soil
MW-17 Yes Yes Yes Yes Yes Yes
MW-18 Yes Yes Yes Yes Yes Yes
MW-19 Yes Yes Yes Yes Yes Yes
MW-20 Yes Yes Yes Yes Yes Yes
MW-21 Yes Yes Yes Yes Yes Yes
MW-22 Yes Yes Yes Yes Yes Yes
MW-23 Yes Yes Yes Yes Yes Yes
MW-24 Yes Yes Yes Yes Yes Yes
MW-25 Yes Yes Yes Yes Yes Yes
MW-26 Yes Yes Yes Yes Yes Yes
MW-27 Yes Yes Yes Yes Yes Yes
MW-31 Yes Yes Yes Yes Yes Yes
MW-32 Yes Yes Yes Yes Yes Yes
MW-33 Yes Yes Yes Yes Yes Yes
MW-34 Yes Yes Yes Yes Yes Yes Path to well recently improved by County
IW-1 Yes Yes Yes Yes Yes Yes Injection well. Not sampled this event.
SW-3 Yes -----Low gage height and flow rate
SW-4R Yes -----Low gage height and flow rate
SW-5 Yes -----Low gage height and flow rate
SW-6 Yes -----Low gage height and flow rate
Any unusual field conditions, observations, or events:
LFG extraction system operating in AOC MW-1B which is typical.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface
Pad
Effective
Phytoremediation transducer data downloaded
Phytoremediation transducer data downloaded
Alexander County Active C02/26/2016 and Closed MSWLF Page 1 of 1
Table 3
Field Parameter Data Summary
January 5-7, 2016
Parameter Temp.ORP DO pH TDS
Units C mg/L SU mg/L % Vol.Visual or NTU
MW-1 34.79 1045.75 1080.54 16.7 -93 0.3 6.03 440 210 NR Clear
MW-1B 41.55 1041.01 1082.56 16.6 NR NR 5.19 80 30 NR Clear
MW-2 18.84 985.64 1004.48 16.9 NR NR 5.83 410 200 NR 307
MW-3 25.88 998.85 1024.73 16.9 -38 0.1 6.01 420 210 NR Clear
MW-4R 14.15 998.49 1012.64 16.1 NR NR 5.91 70 30 NR Clear
MW-5 38.96 1012.30 1051.26 15.8 181 0.3 6.97 80 30 NR 39.1
MW-6 21.72 989.07 1010.79 15.9 189 0.9 6.93 440 220 NR 19.2
MW-7 38.88 970.36 1009.24 15.5 31.0 0.3 6.03 80.0 40.0 NR Clear
MW-9 10.05 986.22 996.27 15.4 51 0.3 6.41 710 350 NR Clear
MW-10 36.21 1004.59 1040.80 15.5 39 0.5 6.81 40 20 NR Clear
MW-11 33.03 978.93 1011.96 13.3 112 0.8 6.14 410 200 NR Clear
MW-12 51.50 955.85 1007.35 10.7 89 0.9 5.99 230 110 NR 18.1
MW-12D 58.55 949.91 1008.46 10.8 111 1.4 6.97 70 30 NR 10.4
MW-13 31.51 973.05 1004.56 11.2 123 1.6 6.91 210 100 NR 13.3
MW-14 31.84 965.60 997.44 10.8 9 0.7 6.97 90 40 NR Slight
MW-15 21.15 1002.29 1023.44 15.4 191 0.3 6.26 460 230 NR Clear
MW-16 28.68 1008.88 1037.56 12.7 273 0.4 5.99 80 30 NR 109
MW-17 15.20 975.96 991.16 13.8 210 0.9 5.63 60 20 NR Clear
MW-18 52.44 1031.89 1084.33 17.1 301 2.1 6.83 40 20 NR 157
MW-19 52.15 1019.33 1071.48 17.8 239 2.5 6.93 80 30 NR Clear
MW-20 40.38 1006.54 1046.92 13.9 82 1.5 6.32 90 40 NR Slight
MW-21 27.71 962.29 990.00 13.3 201 2.1 5.63 620 300 NR Clear
MW-22 15.03 943.94 958.97 14.1 210 3.9 6.51 820 400 NR Slight
MW-23 15.72 934.76 950.48 15.1 201 5.1 6.91 90 40 NR Slight
MW-24 29.39 944.65 974.04 12.2 281 0.5 5.99 190 90 NR Slight
MW-25 26.19 955.74 981.93 14.3 227 0.6 5.87 80 40 NR Clear
MW-26 14.14 976.55 990.69 15.1 105 0.5 5.73 400 190 NR Clear
MW-27 11.82 980.37 992.19 13.9 271 3.1 6.6 180 90 NR Clear
MW-31 10.35 975.07 985.42 14.6 214 0.9 5.28 110 50 NR Moderate
MW-32 30.85 994.41 1025.26 14.2 212 1.2 6.91 280 130 NR Slight
MW-33 12.69 994.71 1007.40 15.1 192 4.2 6.89 80 40 NR Moderate
MW-34 7.93 1006.67 1014.60 15.2 147 4.4 6.81 80 40 NR Moderate
Minimum 7.93 934.76 950.48 10.7 -93 0.1 5.19 40 20 NR Clear
Average 28.10 986.55 1014.65 14.6 150 1.5 6.32 235 113 NR Slight
Maximum 58.55 1045.75 1084.33 17.8 301 5.1 6.97 820 400 NR Moderate
SW-3 ---7.3 41 6.1 7.02 80 30 NR Clear
SW-4R ---7.4 29 6.3 7.01 80 40 NR Clear
SW-5 ---7.1 38 6.2 6.98 80 40 NR Clear
SW-6 ---6.9 42 6.1 7.01 80 40 NR Clear
Minimum ---6.9 29 6.1 6.98 80 30 NR Clear
Average ---7.2 38 6.2 7.01 80 38 NR Clear
Maximum ---7.4 42 6.3 7.02 80 40 NR Clear
NR = No Reading Attempted
Water
Depth
Water
Elevation
TOC
Elevation
Specific
Conductance
Methane Gas in
Headspace
Turbidity of
Metal Sample
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 4
Sampling and Analysis Summary
January 5-8, 2016
MNA
Constituent To
t
a
l

M
e
t
a
l
s
Me
r
c
u
r
y
,

t
o
t
a
l
Me
r
c
u
r
y
,

d
i
s
s
o
l
v
e
d
VF
A
Hy
d
r
o
g
e
n
Me
t
h
a
n
e
,

D
i
s
s
o
l
v
e
d
Ca
r
b
o
n

D
i
o
x
i
d
e
Al
k
a
l
i
n
i
t
y
Su
l
f
a
t
e
Su
l
f
i
d
e
Ch
l
o
r
i
d
e
TO
C
CO
D
BO
D
Ir
o
n
,

D
i
s
s
o
l
v
e
d
Ni
t
r
a
t
e
Laboratory PA
C
E
PA
C
E
PA
C
E
PA
C
E
PA
C
E
PA
C
E
PA
C
E
PA
C
E
FI
E
L
D
PA
C
E
PA
C
E
PA
C
E
PA
C
E
PA
C
E
PA
C
E
PA
C
E
PA
C
E
PA
C
E
Method La
b

E
P
A

8
2
6
0
B
L
a
b

E
P
A

6
0
0
0
/
7
0
0
0
L
a
b

E
P
A

7
4
7
0
L
a
b

E
P
A

7
4
7
0
AM
2
3
G
AM
2
0
G
A
X
RS
K
1
7
5
AM
2
0
G
A
X
La
b

S
M

2
3
2
0
B
EP
A

3
0
0
.
0
La
b

S
M
1
8

4
5
0
0
-
S

D
SM

5
3
1
0
B
SM

5
2
2
0
D
SM
5
2
1
0
B
La
b

E
P
A

6
0
1
0
La
b

3
5
3
.
2
MW-1 x x x x
MW-1A Dry so not sampled which is typical
MW-1B x x x x x
MW-2 x x x
MW-3 x x x x x x x x
MW-4R x x
MW-5 x x x x x x x x x x x
MW-6 x x x x x x x x x x x x
MW-7 x x
MW-9 x x
MW-10 x x
MW-11 x x x x x x x x x x x
MW-12 x x x x x x x x x x x
MW-12D x x x x x x x x x x x
MW-13 x x
MW-14 x x
MW-15 x x x
MW-16 x x
MW-17 x x x
MW-18 x x x x
MW-19 x x
MW-20 x x
MW-21 x x x
MW-22 x x
MW-23 x x
MW-24 x x x x x x x x x x x
MW-25 x x x
MW-26 x x x x x x x x x x x
MW-27 x x
MW-31 x x x x x x x x x x x
MW-32 x x
MW-33 x x
MW-34 x x
SW-3 x x
SW-4R x x
SW-5 x x
SW-6 x x
EB x x x
TB x
FB x x x
App. I App II
VO
C
s
Et
h
e
ne
/E th
a
ne
H ac
h
K it
L ab
SM

4
5
0 0 -C
l -E
App I & II = Appendix I Listed in current 40 CFR 258
Alexander Co. Active CDLF over MSW Page 1 of 3
Table 5
Detections in Water Samples Above Established SWSL, GWP, 2L, 2B, or MCL
January 5-8, 2016
Result Unit
MW-1 Zinc, total 1/06/16 42.6 5 10 1000 5000
MW-1 Benzene 1/06/16 1.6 0.25 1 1 5 LFG
MW-1 Cobalt, total 1/06/16 10.9(B)2.5 10 NE 1 NE
MW-1 1/06/16 2.8 0.33 1 6 75
MW-1B Zinc, total 1/06/16 18 5 10 1000 5000
MW-1B Cobalt, total 1/06/16 111 2.5 10 NE 1 NE
MW-1B Mercury, total 1/06/16 1.1 0.1 0.2 1 2 N S
MW-1B Mercury, dissolved 1/06/16 ND<0.2 0.2 0.2 1 2
MW-1B 1/06/16 3.8 0.33 1 6 75
MW-2 Cobalt, total 1/07/16 195 2.5 10 NE 1 NE
MW-2 Zinc, total 1/07/16 10.6 5 10 1000 5000
MW-2 Cadmium, total 1/07/16 1.1 0.5 1 2 5
MW-3 1/06/16 1.2 0.3 1 600 NE
MW-3 1/06/16 10.6 0.33 1 6 75 L &/or LFG
MW-3 Cobalt, total 1/06/16 19.3(B)2.5 10 NE 1 NE
MW-3 1/06/16 6.6 0.19 5 70 70
MW-3 Benzene 1/06/16 5.9 0.25 1 1 5 L &/or LFG
MW-4R 1/05/16 8.2 0.19 5 70 70
MW-4R Cobalt, total 1/05/16 160 2.5 10 NE 1 NE
MW-4R Benzene 1/05/16 1.1 0.25 1 1 5 L &/or LFG
MW-4R 1/05/16 2.7 0.33 1 6 75
MW-4R Barium, total 1/05/16 119 2.5 100 700 1300
MW-5 Benzene 1/05/16 2.6 0.25 1 1 5 L &/or LFG
MW-5 Zinc, total 1/05/16 13.9 5 10 1000 5000
MW-5 1/05/16 1.6 0.33 1 6 75
MW-5 Cobalt, total 1/05/16 7.1J 2.5 10 NE 1 NE
MW-5 Vanadium, total 1/05/16 3.3J 2.5 25 NE 0.3 NE
MW-5 1/05/16 10.2 0.19 5 70 70
MW-6 Cadmium, total 1/05/16 1.1 0.5 1 2 5
MW-6 Cobalt, total 1/05/16 16.5 2.5 10 NE 1 NE
MW-6 Mercury, total 1/05/16 0.26 0.1 0.2 1 2
MW-6 Zinc, total 1/05/16 15.8 5 10 1000 5000
MW-7 1/07/16 1.5 0.33 1 6 75
MW-7 Benzene 1/07/16 2.2 0.25 1 1 5 L &/or LFG
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
Ethylbenzene ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
Alexander Co. Active CDLF over MSW Page 2 of 3
Result UnitSample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
MW-9 Cobalt, total 1/05/16 18.1 2.5 10 NE 1 NE
MW-9 1/05/16 9.7 0.19 5 70 70
MW-9 Barium, total 1/05/16 107 2.5 100 700 1300
MW-11 1/06/16 7.5 0.33 1 6 75 L &/or LFG
MW-11 1/06/16 14.2 0.19 5 70 70
MW-11 Cobalt, total 1/06/16 143 2.5 10 NE 1 NE
MW-11 Barium, total 1/06/16 138 2.5 100 700 1300
MW-11 Benzene 1/06/16 2.9 0.25 1 1 5 L &/or LFG
MW-12 1/06/16 1.6 0.47 1 3 5
MW-12 Zinc, total 1/06/16 277 5 10 1000 5000
MW-12 Cobalt, total 1/06/16 75.3 2.5 10 NE 1 NE
MW-12 Benzene 1/06/16 1.2 0.25 1 1 5 L &/or LFG
MW-12 1/06/16 7.3 0.33 1 6 75 L &/or LFG
MW-12 Barium, total 1/06/16 115 2.5 100 700 1300
MW-12 1/06/16 10.4 0.19 5 70 70
MW-12D Zinc, total 1/06/16 19.1 5 10 1000 5000
MW-13 Cadmium, total 1/05/16 12.1 0.5 1 2 5 N
MW-13 Zinc, total 1/05/16 39.9 5 10 1000 5000
MW-14 Cobalt, total 1/07/16 8.2J 2.5 10 NE 1 NE
MW-15 Benzene 1/07/16 2.6 0.25 1 1 5 L &/or LFG
MW-15 1/07/16 7.7 0.19 5 70 70
MW-16 Methylene Chloride 1/05/16 1.1(C9)0.97 1 5 5
MW-16 Benzene 1/05/16 2.3 0.25 1 1 5 L &/or LFG
MW-16 1/05/16 16.5 0.19 5 70 70
MW-16 1/05/16 6.3 0.32 5 6 7 L &/or LFG
MW-16 1/05/16 1.5 0.46 1 0.7 5 L &/or LFG
MW-16 1/05/16 1.8 0.47 1 3 5
MW-16 1/05/16 2 0.33 1 6 75
MW-16 Cobalt, total 1/05/16 57.4 2.5 10 NE 1 NE
MW-17 Mercury, total 1/05/16 0.27 0.1 0.2 1 2
MW-17 Cobalt, total 1/05/16 14 2.5 10 NE 1 NE
MW-18 Zinc, total 1/06/16 24 5 10 1000 5000
MW-18 Mercury, total 1/06/16 0.37 0.1 0.2 1 2
MW-18 Vanadium, total 1/06/16 3.1J 2.5 25 NE 0.3 NE
MW-18 Cobalt, total 1/06/16 26.1(B)2.5 10 NE 1 NE
MW-18 Copper, total 1/06/16 29.1 2.5 10 1000 NE
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
1,4-Dichlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
Trichloroethene ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
1,1-Dichloroethane ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Alexander Co. Active CDLF over MSW Page 3 of 3
Result UnitSample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
MW-21 Mercury, total 1/05/16 0.16J 0.1 0.2 1 2
MW-21 Cobalt, total 1/05/16 8.8J 2.5 10 NE 1 NE
MW-22 Zinc, total 1/05/16 10.2 5 10 1000 5000
MW-22 Vanadium, total 1/05/16 3.2J 2.5 25 NE 0.3 NE
MW-22 Cobalt, total 1/05/16 6.5J 2.5 10 NE 1 NE
MW-24 Cobalt, total 1/06/16 21.4 2.5 10 NE 1 NE
MW-24 Zinc, total 1/06/16 13.4 5 10 1000 5000
MW-25 Zinc, total 1/07/16 15.7 5 10 1000 5000
MW-26 Cobalt, total 1/06/16 104 2.5 10 NE 1 NE
MW-26 1/06/16 1.2 0.33 1 6 75
MW-26 Zinc, total 1/06/16 23.5 5 10 1000 5000
MW-27 Zinc, total 1/06/16 15.4 5 10 1000 5000
MW-27 1/06/16 5.3 0.19 5 70 70
MW-27 Cadmium, total 1/06/16 1.7 0.5 1 2 5
MW-31 Cobalt, total 1/06/16 6J (B)2.5 10 NE 1 NE
MW-33 Cobalt, total 1/06/16 10.5 2.5 10 NE 1 NE
SW-5 Cobalt, total 1/06/16 20.1 2.5 10 270 NE
EB Thallium, total 1/08/16 17.8 5 5.5 NE 0.47 0.28 2
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
J=The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
(B) = Also detected in associated method Blank and flagged by the laboratory as such. Likely false positive or high bias originating in the laboratory.
(C9) = Common laboratory contaminant and flagged by the laboratory as such. Used in lab extraction process and common cross contaminant via air.
NE = Not Established
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
L = Leachate
LFG = Landfill Gas
S = Sediment in sample container as evidenced by absence in lab filtered dissolved sample
Concentration > 2L, 2B, GWP or MCL Standard
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
BOLD =
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 6
January 5-7, 2016
MW-2 3.70E-06 28 0.806 11 N54W 18.84 985.64 UC
MW-12 n/a 28 0.108 n/a N58W 51.50 955.85 UC
MW-16 8.72E-04 17 0.037 198 S07E 28.68 1008.88 UC
MW-17 n/a 17 0.311 n/a N42W 15.20 975.96 UC
MW-21 3.77E-03 28 0.176 2454 N54W 27.71 962.29 UC
MW-22 6.04E-04 28 0.303 676 N51W 15.03 943.94 UC
MW-23 9.83E-04 28 0.349 1269 N41W 15.72 934.76 UC
MW-24 1.33E-02 28 0.106 5194 N63W 29.39 944.65 UC
MW-31 n/a 28 0.184 n/a S48W 10.35 975.07 UC
MW-33 n/a 28 0.096 n/a S32E 12.69 994.71 UC
MW-34 n/a 28 0.145 n/a S27E 7.93 1006.67 UC
Minimum 3.70E-006 17 0.037 11 -7.93 934.76 -
Average 3.26E-003 26 0.238 1634 -21.19 971.67 -
Maximum 1.33E-002 28 0.806 5194 -51.5 1008.88 -
MW-1 5.60E-05 10 0.096 56 N47W 34.79 1045.75 UC/UBR
MW-3 3.90E-06 10 0.018 1 S08W 25.88 998.85 UC/UBR
MW-4R 4.90E-04 10 0.047 239 S21W 14.15 998.49 UC/UBR
MW-5 6.40E-05 28 0.038 9 S06E 38.96 1012.30 UC/UBR
MW-14 n/a 10 0.880 n/a N58W 31.84 965.60 UC/UBR
MW-15 n/a 10 0.229 n/a N47W 21.15 1002.29 UC/UBR
Minimum 3.90E-06 10 0.018 1 -14.15 965.6 -
Average 1.53E-04 13 0.218 76 -27.80 1003.88 -
Maximum 4.90E-04 28 0.880 239 -38.96 1045.75 -
MW-1B n/a 10 0.072 n/a N02E 41.55 1041.01 UBR
MW-6 2.40E-05 10 0.432 107 N78W 26.27 989.07 UBR
MW-7 1.60E-06 10 0.016 0 S24W 38.88 970.36 UBR
MW-9 n/a 10 0.057 n/a S04W 10.05 986.22 UBR
MW-11 n/a 10 0.097 n/a S27W 33.03 978.93 UBR
MW-13 n/a 10 0.203 n/a S82W 31.51 973.05 UBR
MW-19 1.92E-06 10 0.042 1 N30W 52.15 1019.33 UBR
MW-20 5.49E-05 10 0.030 17 N67W 40.38 1006.54 UBR
MW-25 5.41E-05 10 0.125 70 N70W 26.19 955.74 UBR
MW-26 1.16E-04 10 0.211 254 S27W 14.14 976.55 UBR
MW-27 2.83E-05 10 0.031 9 S08E 11.82 980.37 UBR
MW-32 n/a 10 0.147 n/a S14E 30.85 994.41 UBR
Minimum 1.60E-06 10 0.016 0 -10.05 955.74 -
Average 4.01E-05 10 0.122 65 -29.74 989.30 -
Maximum 1.16E-04 10 0.432 254 -52.15 1041.01 -
MW-10 n/a 10 0.109 n/a n/a 36.21 1004.59 LBR
MW-12D n/a 10 0.075 n/a n/a 58.55 949.91 LBR
MW-18 1.19E-04 10 0.270 n/a n/a 52.44 1031.89 LBR
Minimum 1.19E-04 10 0.075 --36.21 949.91 -
Average 1.19E-04 10 0.151 --49.07 995.46 -
Maximum 1.19E-04 10 0.270 --58.55 1031.89 -
NOTE:Values for hydraulic conductivity obtained from GAI Consultants Sampling Report (April, 1995) & MESCO ACM Report (2008).
Average Linear Groundwater Velocities calculated only for UC & UBR wells with hydraulic conductivity values.
Wells screened in LBR not utilized for flow directions/gradients.
Flow rate (Q) calculated via modified Darcy's equation:
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well
Hydraulic
Conductivity
(cm/sec)
Effective
Porosity
(%)
Hydraulic
Gradient
(ft/ft)
Average Linear
Velocity Rate
(ft/yr)
Flow
Direction
Depth to
Groundwater
(ft btoc)
Groundwater
Potentiometric
Elevation (ft amsl)
Screened Interval
Lithology
K= hydraulic conductivity
UC = Unconfined/saprolite; UBR = Upper Bedrock fracture system; LBR = Lower Bedrock fracture system.ne = effective porosity
dh= head difference
Hydrologic Gradient taken from water elevations recorded between January 5-7, 2016.dl= horizontal distancedl
dh
n
KQ
e
-=
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 7
MNA Parameter Data Summary
January 5-7, 2016
Parameters Method MDL*Units MW-18 MW-3 MW-5 MW-6 MW-7 MW-11 MW-12 MW-12D MW-16 MW-24 MW-25 MW-26 MW-27 MW-31 MW-33 MW-34
1/06/16 1/06/16 1/05/16 1/05/16 1/07/16 1/06/16 1/06/16 1/06/16 1/05/16 1/06/16 1/07/16 1/06/16 1/06/16 1/06/16 1/06/16 1/06/16
VFA – Acetic Acid AM23G NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
AM23G NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
VFA – Lactic Acid AM23G NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
AM23G NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
AM23G NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Hydrogen AM20GAX NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Methane AM20GAX NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
AM20GAX NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Ethane AM20GAX NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
CO2-Dissolved Field HACH Kit NS mg/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Alkalinity SM 2320B 1000 NS 96900 NS NS NS 202000 123000 345000 NS 31000 NS 113000 NS 18000 NS NS
Sulfate EPA 300.0 1000 NS <1000 NS NS NS 2870j 4920j 1230j NS 2460j NS 4240j NS 1980j NS NS
Sulfide SM 4500-S2D 100 NS NS NS NS NS <100 <100 <100 NS <100 NS <100 NS <100 NS NS
Chloride SM 4500-Cl-E 1000 NS 21800 NS NS NS 36900 11900 58600 NS 21700 NS 15400 NS 8980 NS NS
TOC SM 5310B 500 NS 4980 NS NS NS 3120 1390 2800 NS 5020 NS 1470 NS 1780 NS NS
COD SM 5220D 12500 NS 30000 NS NS NS 41000 25000 23000j NS 14000j NS 23000j NS <12500 NS NS
BOD SM5210B NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Iron (total-dissolved)EPA 6010 25 <25 NS NS NS NS 48900 35500 262j NS 103j NS 17600 NS <25 NS NS
Nitrate EPA 353.2 10 NS NS NS NS NS <10 <10 59.6j NS 315j NS <10 NS 1060j NS NS
Temperature Field Instrument 0 C 17.1 16.9 15.8 15.9 15.5 13.3 10.7 10.8 12.7 12.2 14.3 15.1 13.9 14.6 15.1 15.2
ORP Field Instrument -900 301 -38 181 189 31 112 89 111 273 281 227 105 271 214 192 147
DO Field Instrument 0 mg/L 2.1 0.1 0.3 0.9 0.3 0.8 0.9 1.4 0.4 0.5 0.6 0.5 3.1 0.9 4.2 4.4
pH Field Instrument 0 SU 6.83 6.01 6.97 6.93 6.03 6.14 5.99 6.97 5.99 5.99 5.87 5.73 6.61 5.28 6.89 6.81
Sp. Conductance Field Instrument 0 us/cm 40 420 80 440 80 410 230 70 80 190 80 400 180 110 80 80
Turbidity Field Instrument 0 NTU 157 NS 39.1 19.2 NS NS 18.1 10.4 109 NS NS NS NS NS NS NS
Notes:
VFA = Volatile Fatty Acids
MDL* = Lab Method Detection Limit or lowest field measurement possible
< = Not Detected above MDL value
MNA monitoring not required for MW-31 by SWS but recorded per NC Underground Injection Control (UIC) Permit requirement
NS = Not Sampled since not required during this specific event
ug/L
VFA – Butyric Acid ug/L
ug/L
VFA – Propionic Acid ug/L
VFA – Pyruvic Acid ug/L
nM
ug/L
Ethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mV
Alexander County Active C&D and Closed MSWLF Page 1 of 1
Table 8
January 8, 2016
September 25, 2015 January 8, 2016 Sept. 25, 2015 compared to Jan. 8, 2016
Notes Notes
1 5/25/10 243 195 16.8 455 80% yellow 5/25/10 244 195 16.8 456 Dormant 1 0 0.0 1
2 5/22/13 86 68 3.4 157 0% yellow 5/22/13 87 68 3.5 159 Dormant 1 0 0.1 1
3 5/25/10 199 133 8.4 340 80% yellow 5/25/10 199 133 8.4 340 Dormant 0 0 0.0 0
4 5/25/10 218 85 7.9 311 20% yellow 5/25/10 221 86 7.9 315 Dormant 3 1 0.0 4
5 5/25/10 158 72 6.3 236 70% yellow 5/25/10 159 72 6.3 237 Dormant 1 0 0.0 1
6 5/25/10 135 61 5.2 201 10% yellow 5/25/10 136 61 5.2 202 Dormant 1 0 0.0 1
7 5/25/10 132 87 4.6 224 60% yellow 5/25/10 133 87 4.6 225 Dormant 1 0 0.0 1
8 5/25/10 188 71 6.8 266 60% yellow 5/25/10 191 71 6.8 269 Dormant 3 0 0.0 3
9 5/25/10 163 75 4.9 243 40% yellow 5/25/10 172 75 4.9 252 Dormant 9 0 0.0 9
10 5/22/13 91 49 3.5 144 0% yellow 5/22/13 91 50 3.5 145 Dormant 0 1 0.0 1
Min.-86 49 3.4 144 --87 50 3.5 145 -0 0 0.0 0
Avg.-161 90 6.8 258 --163 90 6.8 260 -2 0 0.0 2
Max.-243 195 16.8 455 --244 195 16.8 456 -9 1 0.1 9
NOTES:
All trees except for those replaced in 2013 exhibited increasing yellowing of foliage between June and September.
Phytoremediation Tree Measurement Summary
Tree
ID
Date
Planted
Date
Planted
Height
(in)
Width
Middle
(in)
Trunk
Circ.
(in)
Total (Ht +
Width +
Circ.)
(in)
Height
(in)
Width
Middle
(in)
Trunk
Circ.
(in)
Total (Ht
+ Width +
Circ.) (in)
Height
(in)
Width
Middle
(in)
Trunk Circ.
(in)
Total (Ht +
Width + Circ.)
(in)
12/13/10 03/08/11 06/18/11 12/08/11 09/27/12 12/13/12 09/27/12 12/13/12 03/29/13 06/28/13 09/18/13 12/18/13 03/27/14 06/24/14 10/08/14 12/05/14 03/16/15 06/17/15 09/25/15 01/08/16
0
25
50
75
100
125
150
175
200
225
250
275
Average Tree Size
Average Tree Size (Inches)Date
I n ch
e s
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
January 21, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92282266
92282266
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Alexander LF-SWS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between January 07,
2016 and January 08, 2016. The results relate only to the samples included in this report. Results
reported herein conform to the most current TNI standards and the laboratory's Quality Assurance
Manual, where applicable, unless otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Dale Ingram
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 110
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 110
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Lab ID Sample ID Matrix Date Collected Date Received
92282266001 MW-1 Water 01/06/16 17:00 01/07/16 10:30
92282266002 MW-1B Water 01/06/16 17:45 01/07/16 10:30
92282266003 MW-4R Water 01/05/16 15:00 01/07/16 10:30
92282266004 MW-5 Water 01/05/16 15:40 01/07/16 10:30
92282266005 MW-9 Water 01/05/16 14:35 01/07/16 10:30
92282266006 MW-10 Water 01/05/16 17:30 01/07/16 10:30
92282266007 MW-13 Water 01/05/16 14:10 01/07/16 10:30
92282266008 MW-16 Water 01/05/16 17:00 01/07/16 10:30
92282266009 MW-22 Water 01/05/16 12:15 01/07/16 10:30
92282266010 MW-23 Water 01/05/16 12:50 01/07/16 10:30
92282266011 MW-32 Water 01/05/16 13:40 01/07/16 10:30
92282266012 MW-33 Water 01/06/16 10:20 01/07/16 10:30
92282266013 MW-34 Water 01/06/16 09:30 01/07/16 10:30
92282266014 SW-3 Water 01/06/16 08:10 01/07/16 10:30
92282266015 SW-4R Water 01/05/16 13:05 01/07/16 10:30
92282266016 SW-5 Water 01/06/16 08:30 01/07/16 10:30
92282266017 SW-6 Water 01/06/16 09:10 01/07/16 10:30
92282266018 MW-6 Water 01/05/16 16:10 01/07/16 10:30
92282266019 MW-17 Water 01/05/16 11:15 01/07/16 10:30
92282266020 MW-21 Water 01/05/16 11:40 01/07/16 10:30
92282266021 MW-12 Water 01/06/16 15:35 01/07/16 10:30
92282266022 MW-12D Water 01/06/16 15:15 01/07/16 10:30
92282266023 MW-24 Water 01/06/16 13:45 01/07/16 10:30
92282266024 MW-2 Water 01/07/16 10:05 01/08/16 08:06
92282266025 MW-14 Water 01/07/16 09:30 01/08/16 08:06
92282266026 MW-15 Water 01/07/16 11:40 01/08/16 08:06
92282266027 MW-19 Water 01/07/16 10:55 01/08/16 08:06
92282266028 MW-20 Water 01/07/16 14:30 01/08/16 08:06
92282266029 MW-25 Water 01/07/16 16:00 01/08/16 08:06
92282266030 MW-7 Water 01/07/16 13:35 01/08/16 08:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 110
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92282266001 MW-1 EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 50 PASI-CNB
92282266002 MW-1B EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 50 PASI-CNB
92282266003 MW-4R EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266004 MW-5 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266005 MW-9 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266006 MW-10 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266007 MW-13 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266008 MW-16 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266009 MW-22 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266010 MW-23 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266011 MW-32 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266012 MW-33 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266013 MW-34 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266014 SW-3 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266015 SW-4R EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266016 SW-5 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266017 SW-6 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266018 MW-6 EPA 6010 15 PASI-ACDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 110
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470 1 PASI-ASH1
EPA 8260 50 PASI-CNB
92282266019 MW-17 EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 50 PASI-CNB
92282266020 MW-21 EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 50 PASI-CNB
92282266021 MW-12 EPA 6010 15 PASI-ACDF
EPA 6010 1 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-AEWS
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92282266022 MW-12D EPA 6010 15 PASI-ACDF
EPA 6010 1 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 4500-S2D 1 PASI-ASAM
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-AEWS
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92282266023 MW-24 EPA 6010 15 PASI-ACDF
EPA 6010 1 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-AEWS
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 110
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 5310B 1 PASI-AMDW
92282266024 MW-2 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266025 MW-14 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266026 MW-15 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266027 MW-19 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266028 MW-20 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266029 MW-25 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92282266030 MW-7 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-1 Lab ID:92282266001 Collected:01/06/16 17:00 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/11/16 18:04 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/11/16 18:04 7440-38-201/08/16 18:0010.0 2.5 1
Barium 30.9J ug/L 01/11/16 18:04 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/11/16 18:04 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/11/16 18:04 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/11/16 18:04 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 10.9 ug/L 01/11/16 18:04 7440-48-4 B01/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/11/16 18:04 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/11/16 18:04 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 10.2J ug/L 01/11/16 18:04 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/11/16 18:04 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/11/16 18:04 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 14:12 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/11/16 18:04 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 42.6 ug/L 01/11/16 18:04 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/14/16 11:55 7439-97-601/08/16 21:300.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 18:42 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 18:42 107-13-12001.9 1
Benzene 1.6 ug/L 01/11/16 18:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 18:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 18:42 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 18:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 18:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 18:42 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 18:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 18:42 56-23-51.0 0.25 1
Chlorobenzene 0.27J ug/L 01/11/16 18:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 18:42 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 18:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 18:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 18:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 18:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 18:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 18:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 18:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.8 ug/L 01/11/16 18:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 18:42 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 18:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 18:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 18:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.0J ug/L 01/11/16 18:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 18:42 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
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Page 7 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-1 Lab ID:92282266001 Collected:01/06/16 17:00 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 18:42 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 18:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 18:42 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 18:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 18:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 18:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 18:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 18:42 108-10-11000.33 1
Styrene ND ug/L 01/11/16 18:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 18:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 18:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 18:42 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 18:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 18:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 18:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 18:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 18:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 18:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 18:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 18:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 18:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)110 %01/11/16 18:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/11/16 18:42 17060-07-070-130 1
Toluene-d8 (S)99 %01/11/16 18:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 8 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-1B Lab ID:92282266002 Collected:01/06/16 17:45 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/11/16 18:07 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/11/16 18:07 7440-38-201/08/16 18:0010.0 2.5 1
Barium 78.6J ug/L 01/11/16 18:07 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/11/16 18:07 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/11/16 18:07 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/11/16 18:07 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 111 ug/L 01/11/16 18:07 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/11/16 18:07 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/11/16 18:07 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 8.8J ug/L 01/11/16 18:07 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/11/16 18:07 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/11/16 18:07 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 14:15 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/11/16 18:07 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 18.0 ug/L 01/11/16 18:07 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 1.1 ug/L 01/14/16 11:57 7439-97-601/08/16 21:300.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 18:59 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 18:59 107-13-12001.9 1
Benzene ND ug/L 01/11/16 18:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 18:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 18:59 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 18:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 18:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 18:59 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 18:59 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 18:59 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 18:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 18:59 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 18:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 18:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 18:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 18:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 18:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 18:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 18:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene 3.8 ug/L 01/11/16 18:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 18:59 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 18:59 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 18:59 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 18:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.4J ug/L 01/11/16 18:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 18:59 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-1B Lab ID:92282266002 Collected:01/06/16 17:45 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 18:59 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 18:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 18:59 10061-02-61.0 0.26 1
Ethylbenzene 0.39J ug/L 01/11/16 18:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 18:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 18:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 18:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 18:59 108-10-11000.33 1
Styrene ND ug/L 01/11/16 18:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 18:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 18:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 18:59 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 18:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 18:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 18:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 18:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 18:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 18:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 18:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 18:59 75-01-41.0 0.62 1
Xylene (Total)1.4J ug/L 01/11/16 18:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)109 %01/11/16 18:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %01/11/16 18:59 17060-07-070-130 1
Toluene-d8 (S)99 %01/11/16 18:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-4R Lab ID:92282266003 Collected:01/05/16 15:00 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/11/16 18:20 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/11/16 18:20 7440-38-201/08/16 18:0010.0 2.5 1
Barium 119 ug/L 01/11/16 18:20 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/11/16 18:20 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/11/16 18:20 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/11/16 18:20 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 160 ug/L 01/11/16 18:20 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/11/16 18:20 7440-50-801/08/16 18:0010.0 2.5 1
Lead 4.4J ug/L 01/11/16 18:20 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 6.3J ug/L 01/11/16 18:20 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/11/16 18:20 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/11/16 18:20 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 14:27 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/11/16 18:20 7440-62-201/08/16 18:0025.0 2.5 1
Zinc ND ug/L 01/11/16 18:20 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 19:16 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 19:16 107-13-12001.9 1
Benzene 1.1 ug/L 01/11/16 19:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 19:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 19:16 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 19:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 19:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 19:16 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 19:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 19:16 56-23-51.0 0.25 1
Chlorobenzene 1.3J ug/L 01/11/16 19:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 19:16 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 19:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 19:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 19:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 19:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 19:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 19:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 19:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.7 ug/L 01/11/16 19:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 19:16 110-57-61001.0 1
1,1-Dichloroethane 0.98J ug/L 01/11/16 19:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 19:16 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 19:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 8.2 ug/L 01/11/16 19:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 19:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 19:16 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 19:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 19:16 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-4R Lab ID:92282266003 Collected:01/05/16 15:00 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 19:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 19:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 19:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 19:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 19:16 108-10-11000.33 1
Styrene ND ug/L 01/11/16 19:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 19:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 19:16 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 19:16 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 19:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 19:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 19:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 19:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 19:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 19:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 19:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 19:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 19:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)111 %01/11/16 19:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %01/11/16 19:16 17060-07-070-130 1
Toluene-d8 (S)99 %01/11/16 19:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-5 Lab ID:92282266004 Collected:01/05/16 15:40 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:03 7440-36-001/08/16 18:006.0 3.8 1
Arsenic 2.6J ug/L 01/12/16 02:03 7440-38-201/08/16 18:0010.0 2.5 1
Barium 46.0J ug/L 01/12/16 02:03 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:03 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:03 7440-43-901/08/16 18:001.0 0.50 1
Chromium 3.9J ug/L 01/12/16 02:03 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 7.1J ug/L 01/12/16 02:03 7440-48-401/08/16 18:0010.0 2.5 1
Copper 2.8J ug/L 01/12/16 02:03 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:03 7439-92-101/08/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 02:03 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:03 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:03 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 15:35 7440-28-001/08/16 18:005.5 5.0 1
Vanadium 3.3J ug/L 01/12/16 02:03 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 13.9 ug/L 01/12/16 02:03 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 16.7J ug/L 01/11/16 19:33 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 19:33 107-13-12001.9 1
Benzene 2.6 ug/L 01/11/16 19:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 19:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 19:33 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 19:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 19:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 19:33 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 19:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 19:33 56-23-51.0 0.25 1
Chlorobenzene 0.55J ug/L 01/11/16 19:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 19:33 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 19:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 19:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 19:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 19:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 19:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 19:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 19:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.6 ug/L 01/11/16 19:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 19:33 110-57-61001.0 1
1,1-Dichloroethane 3.6J ug/L 01/11/16 19:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 19:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 19:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 10.2 ug/L 01/11/16 19:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 19:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 19:33 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 19:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 19:33 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
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Page 13 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-5 Lab ID:92282266004 Collected:01/05/16 15:40 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 19:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 19:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 19:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 19:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 19:33 108-10-11000.33 1
Styrene ND ug/L 01/11/16 19:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 19:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 19:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 19:33 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 19:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 19:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 19:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 19:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 19:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 19:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 19:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 19:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 19:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)108 %01/11/16 19:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/11/16 19:33 17060-07-070-130 1
Toluene-d8 (S)99 %01/11/16 19:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 14 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-9 Lab ID:92282266005 Collected:01/05/16 14:35 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:12 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 02:12 7440-38-201/08/16 18:0010.0 2.5 1
Barium 107 ug/L 01/12/16 02:12 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:12 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:12 7440-43-901/08/16 18:001.0 0.50 1
Chromium 3.9J ug/L 01/12/16 02:12 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 18.1 ug/L 01/12/16 02:12 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 02:12 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:12 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 36.8J ug/L 01/12/16 02:12 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:12 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:12 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 16:02 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 02:12 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 6.7J ug/L 01/12/16 02:12 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 19:50 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 19:50 107-13-12001.9 1
Benzene ND ug/L 01/11/16 19:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 19:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 19:50 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 19:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 19:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 19:50 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 19:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 19:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 19:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 19:50 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 19:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 19:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 19:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 19:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 19:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 19:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 19:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.45J ug/L 01/11/16 19:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 19:50 110-57-61001.0 1
1,1-Dichloroethane 0.57J ug/L 01/11/16 19:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 19:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 19:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 9.7 ug/L 01/11/16 19:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 19:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 19:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 19:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 19:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-9 Lab ID:92282266005 Collected:01/05/16 14:35 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 19:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 19:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 19:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 19:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 19:50 108-10-11000.33 1
Styrene ND ug/L 01/11/16 19:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 19:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 19:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 19:50 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 19:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 19:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 19:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 19:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 19:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 19:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 19:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 19:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 19:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)108 %01/11/16 19:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/11/16 19:50 17060-07-070-130 1
Toluene-d8 (S)99 %01/11/16 19:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 16 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-10 Lab ID:92282266006 Collected:01/05/16 17:30 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:24 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 02:24 7440-38-201/08/16 18:0010.0 2.5 1
Barium 26.0J ug/L 01/12/16 02:24 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:24 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:24 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 02:24 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 02:24 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 02:24 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:24 7439-92-101/08/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 02:24 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:24 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:24 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 02:24 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 02:24 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 5.7J ug/L 01/12/16 02:24 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 20:08 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 20:08 107-13-12001.9 1
Benzene ND ug/L 01/11/16 20:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 20:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 20:08 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 20:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 20:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 20:08 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 20:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 20:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 20:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 20:08 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 20:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 20:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 20:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 20:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 20:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 20:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 20:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 20:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 20:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 20:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 20:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 20:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.61J ug/L 01/11/16 20:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 20:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 20:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 20:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 20:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-10 Lab ID:92282266006 Collected:01/05/16 17:30 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 20:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 20:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 20:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 20:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 20:08 108-10-11000.33 1
Styrene ND ug/L 01/11/16 20:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 20:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 20:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 20:08 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 20:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 20:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 20:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 20:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 20:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 20:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 20:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 20:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 20:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)108 %01/11/16 20:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/11/16 20:08 17060-07-070-130 1
Toluene-d8 (S)100 %01/11/16 20:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-13 Lab ID:92282266007 Collected:01/05/16 14:10 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:27 7440-36-001/08/16 18:006.0 3.8 1
Arsenic 2.7J ug/L 01/12/16 02:27 7440-38-201/08/16 18:0010.0 2.5 1
Barium 14.1J ug/L 01/12/16 02:27 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:27 7440-41-701/08/16 18:001.0 0.50 1
Cadmium 12.1 ug/L 01/12/16 02:27 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 02:27 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 02:27 7440-48-401/08/16 18:0010.0 2.5 1
Copper 6.5J ug/L 01/12/16 02:27 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:27 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 7.0J ug/L 01/12/16 02:27 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:27 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:27 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 02:27 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 02:27 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 39.9 ug/L 01/12/16 02:27 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 20:25 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 20:25 107-13-12001.9 1
Benzene ND ug/L 01/11/16 20:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 20:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 20:25 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 20:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 20:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 20:25 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 20:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 20:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 20:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 20:25 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 20:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 20:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 20:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 20:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 20:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 20:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 20:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 20:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 20:25 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 20:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 20:25 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 20:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 20:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 20:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 20:25 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 20:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 20:25 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-13 Lab ID:92282266007 Collected:01/05/16 14:10 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 20:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 20:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 20:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 20:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 20:25 108-10-11000.33 1
Styrene ND ug/L 01/11/16 20:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 20:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 20:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 20:25 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 20:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 20:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 20:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 20:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 20:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 20:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 20:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 20:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 20:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)111 %01/11/16 20:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %01/11/16 20:25 17060-07-070-130 1
Toluene-d8 (S)99 %01/11/16 20:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 20 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-16 Lab ID:92282266008 Collected:01/05/16 17:00 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:31 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 02:31 7440-38-201/08/16 18:0010.0 2.5 1
Barium 52.6J ug/L 01/12/16 02:31 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:31 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:31 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 02:31 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 57.4 ug/L 01/12/16 02:31 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 02:31 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:31 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 6.2J ug/L 01/12/16 02:31 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:31 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:31 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 02:31 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 02:31 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 9.3J ug/L 01/12/16 02:31 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 20:42 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 20:42 107-13-12001.9 1
Benzene 2.3 ug/L 01/11/16 20:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 20:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 20:42 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 20:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 20:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 20:42 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 20:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 20:42 56-23-51.0 0.25 1
Chlorobenzene 0.52J ug/L 01/11/16 20:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 20:42 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 20:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 20:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 20:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 20:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 20:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 20:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 20:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.0 ug/L 01/11/16 20:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 20:42 110-57-61001.0 1
1,1-Dichloroethane 6.3 ug/L 01/11/16 20:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 20:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 20:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 16.5 ug/L 01/11/16 20:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 20:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 20:42 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 20:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 20:42 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-16 Lab ID:92282266008 Collected:01/05/16 17:00 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 20:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 20:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 20:42 74-88-410.0 0.32 1
Methylene Chloride 1.1 ug/L 01/11/16 20:42 75-09-2 C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 20:42 108-10-11000.33 1
Styrene ND ug/L 01/11/16 20:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 20:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 20:42 79-34-53.0 0.40 1
Tetrachloroethene 1.5 ug/L 01/11/16 20:42 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 20:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 20:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 20:42 79-00-51.0 0.29 1
Trichloroethene 1.8 ug/L 01/11/16 20:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 20:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 20:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 20:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 20:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 20:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)109 %01/11/16 20:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/11/16 20:42 17060-07-070-130 1
Toluene-d8 (S)99 %01/11/16 20:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-22 Lab ID:92282266009 Collected:01/05/16 12:15 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:34 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 02:34 7440-38-201/08/16 18:0010.0 2.5 1
Barium 64.2J ug/L 01/12/16 02:34 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:34 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:34 7440-43-901/08/16 18:001.0 0.50 1
Chromium 3.8J ug/L 01/12/16 02:34 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 6.5J ug/L 01/12/16 02:34 7440-48-401/08/16 18:0010.0 2.5 1
Copper 3.4J ug/L 01/12/16 02:34 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:34 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 3.1J ug/L 01/12/16 02:34 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:34 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:34 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 02:34 7440-28-001/08/16 18:005.5 5.0 1
Vanadium 3.2J ug/L 01/12/16 02:34 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 10.2 ug/L 01/12/16 02:34 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 20:59 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 20:59 107-13-12001.9 1
Benzene ND ug/L 01/11/16 20:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 20:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 20:59 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 20:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 20:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 20:59 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 20:59 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 20:59 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 20:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 20:59 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 20:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 20:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 20:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 20:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 20:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 20:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 20:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 20:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 20:59 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 20:59 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 20:59 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 20:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 20:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 20:59 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 20:59 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 20:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 20:59 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-22 Lab ID:92282266009 Collected:01/05/16 12:15 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 20:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 20:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 20:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 20:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 20:59 108-10-11000.33 1
Styrene ND ug/L 01/11/16 20:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 20:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 20:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 20:59 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 20:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 20:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 20:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 20:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 20:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 20:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 20:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 20:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 20:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)110 %01/11/16 20:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %01/11/16 20:59 17060-07-070-130 1
Toluene-d8 (S)101 %01/11/16 20:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-23 Lab ID:92282266010 Collected:01/05/16 12:50 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:37 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 02:37 7440-38-201/08/16 18:0010.0 2.5 1
Barium 21.9J ug/L 01/12/16 02:37 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:37 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:37 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 02:37 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 02:37 7440-48-401/08/16 18:0010.0 2.5 1
Copper 3.9J ug/L 01/12/16 02:37 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:37 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 3.4J ug/L 01/12/16 02:37 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:37 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:37 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 02:37 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 02:37 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 5.5J ug/L 01/12/16 02:37 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 16:47 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 16:47 107-13-12001.9 1
Benzene ND ug/L 01/11/16 16:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 16:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 16:47 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 16:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 16:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 16:47 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 16:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 16:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 16:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 16:47 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 16:47 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 16:47 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 16:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 16:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 16:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 16:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 16:47 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 16:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 16:47 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 16:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 16:47 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 16:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 16:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 16:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 16:47 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 16:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 16:47 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-23 Lab ID:92282266010 Collected:01/05/16 12:50 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 16:47 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 16:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 16:47 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 16:47 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 16:47 108-10-11000.33 1
Styrene ND ug/L 01/11/16 16:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 16:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 16:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 16:47 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 16:47 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 16:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 16:47 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 16:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 16:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 16:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 16:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 16:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 16:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/11/16 16:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %01/11/16 16:47 17060-07-070-130 1
Toluene-d8 (S)103 %01/11/16 16:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-32 Lab ID:92282266011 Collected:01/05/16 13:40 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:40 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 02:40 7440-38-201/08/16 18:0010.0 2.5 1
Barium 10.6J ug/L 01/12/16 02:40 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:40 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:40 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 02:40 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 02:40 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 02:40 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:40 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 9.8J ug/L 01/12/16 02:40 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:40 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:40 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 02:40 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 02:40 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 6.0J ug/L 01/12/16 02:40 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 17:04 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 17:04 107-13-12001.9 1
Benzene ND ug/L 01/11/16 17:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 17:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 17:04 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 17:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 17:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 17:04 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 17:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 17:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 17:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 17:04 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 17:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 17:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 17:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 17:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 17:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 17:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 17:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 17:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 17:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 17:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 17:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 17:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 17:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 17:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 17:04 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 17:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 17:04 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-32 Lab ID:92282266011 Collected:01/05/16 13:40 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 17:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 17:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 17:04 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 17:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 17:04 108-10-11000.33 1
Styrene ND ug/L 01/11/16 17:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 17:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 17:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 17:04 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 17:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 17:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 17:04 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 17:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 17:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 17:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 17:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 17:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 17:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %01/11/16 17:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %01/11/16 17:04 17060-07-070-130 1
Toluene-d8 (S)106 %01/11/16 17:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 28 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-33 Lab ID:92282266012 Collected:01/06/16 10:20 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:43 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 02:43 7440-38-201/08/16 18:0010.0 2.5 1
Barium 26.4J ug/L 01/12/16 02:43 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:43 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:43 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 02:43 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 10.5 ug/L 01/12/16 02:43 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 02:43 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:43 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 4.4J ug/L 01/12/16 02:43 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:43 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:43 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 02:43 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 02:43 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 7.7J ug/L 01/12/16 02:43 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 17:21 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 17:21 107-13-12001.9 1
Benzene ND ug/L 01/11/16 17:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 17:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 17:21 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 17:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 17:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 17:21 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 17:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 17:21 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 17:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 17:21 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 17:21 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 17:21 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 17:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 17:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 17:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 17:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 17:21 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 17:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 17:21 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 17:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 17:21 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 17:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 17:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 17:21 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 17:21 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 17:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 17:21 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-33 Lab ID:92282266012 Collected:01/06/16 10:20 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 17:21 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 17:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 17:21 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 17:21 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 17:21 108-10-11000.33 1
Styrene ND ug/L 01/11/16 17:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 17:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 17:21 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 17:21 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 17:21 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 17:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 17:21 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 17:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 17:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 17:21 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 17:21 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 17:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 17:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %01/11/16 17:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %01/11/16 17:21 17060-07-070-130 1
Toluene-d8 (S)103 %01/11/16 17:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-34 Lab ID:92282266013 Collected:01/06/16 09:30 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:46 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 02:46 7440-38-201/08/16 18:0010.0 2.5 1
Barium 20.0J ug/L 01/12/16 02:46 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:46 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:46 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 02:46 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 02:46 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 02:46 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:46 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 2.7J ug/L 01/12/16 02:46 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:46 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:46 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 02:46 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 02:46 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 6.9J ug/L 01/12/16 02:46 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 17:39 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 17:39 107-13-12001.9 1
Benzene ND ug/L 01/11/16 17:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 17:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 17:39 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 17:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 17:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 17:39 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 17:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 17:39 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 17:39 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 17:39 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 17:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 17:39 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 17:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 17:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 17:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 17:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 17:39 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 17:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 17:39 110-57-61001.0 1
1,1-Dichloroethane 0.39J ug/L 01/11/16 17:39 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 17:39 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 17:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 17:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 17:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 17:39 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 17:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 17:39 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-34 Lab ID:92282266013 Collected:01/06/16 09:30 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 17:39 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 17:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 17:39 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 17:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 17:39 108-10-11000.33 1
Styrene ND ug/L 01/11/16 17:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 17:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 17:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 17:39 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 17:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 17:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 17:39 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 17:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 17:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 17:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 17:39 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 17:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 17:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %01/11/16 17:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %01/11/16 17:39 17060-07-070-130 1
Toluene-d8 (S)103 %01/11/16 17:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:SW-3 Lab ID:92282266014 Collected:01/06/16 08:10 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:49 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 02:49 7440-38-201/08/16 18:0010.0 2.5 1
Barium 34.4J ug/L 01/12/16 02:49 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:49 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:49 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 02:49 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 02:49 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 02:49 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:49 7439-92-101/08/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 02:49 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:49 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:49 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 02:49 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 02:49 7440-62-201/08/16 18:0025.0 2.5 1
Zinc ND ug/L 01/12/16 02:49 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 17:56 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 17:56 107-13-12001.9 1
Benzene ND ug/L 01/11/16 17:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 17:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 17:56 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 17:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 17:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 17:56 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 17:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 17:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 17:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 17:56 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 17:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 17:56 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 17:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 17:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 17:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 17:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 17:56 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 17:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 17:56 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 17:56 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 17:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 17:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 17:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 17:56 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 17:56 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 17:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 17:56 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
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Page 33 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:SW-3 Lab ID:92282266014 Collected:01/06/16 08:10 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 17:56 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 17:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 17:56 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 17:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 17:56 108-10-11000.33 1
Styrene ND ug/L 01/11/16 17:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 17:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 17:56 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 17:56 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 17:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 17:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 17:56 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 17:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 17:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 17:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 17:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 17:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 17:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/11/16 17:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %01/11/16 17:56 17060-07-070-130 1
Toluene-d8 (S)103 %01/11/16 17:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:SW-4R Lab ID:92282266015 Collected:01/05/16 13:05 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 02:52 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 02:52 7440-38-201/08/16 18:0010.0 2.5 1
Barium 35.5J ug/L 01/12/16 02:52 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 02:52 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 02:52 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 02:52 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 02:52 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 02:52 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 02:52 7439-92-101/08/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 02:52 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 02:52 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 02:52 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 02:52 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 02:52 7440-62-201/08/16 18:0025.0 2.5 1
Zinc ND ug/L 01/12/16 02:52 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 18:13 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 18:13 107-13-12001.9 1
Benzene ND ug/L 01/11/16 18:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 18:13 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 18:13 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 18:13 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 18:13 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 18:13 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 18:13 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 18:13 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 18:13 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 18:13 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 18:13 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 18:13 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 18:13 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 18:13 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 18:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 18:13 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 18:13 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 18:13 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 18:13 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 18:13 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 18:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 18:13 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 18:13 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 18:13 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 18:13 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 18:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 18:13 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:SW-4R Lab ID:92282266015 Collected:01/05/16 13:05 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 18:13 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 18:13 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 18:13 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 18:13 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 18:13 108-10-11000.33 1
Styrene ND ug/L 01/11/16 18:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 18:13 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 18:13 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 18:13 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 18:13 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 18:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 18:13 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 18:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 18:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 18:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 18:13 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 18:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 18:13 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %01/11/16 18:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %01/11/16 18:13 17060-07-070-130 1
Toluene-d8 (S)104 %01/11/16 18:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:SW-5 Lab ID:92282266016 Collected:01/06/16 08:30 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 03:05 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 03:05 7440-38-201/08/16 18:0010.0 2.5 1
Barium 25.4J ug/L 01/12/16 03:05 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 03:05 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 03:05 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 03:05 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 20.1 ug/L 01/12/16 03:05 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 03:05 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 03:05 7439-92-101/08/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 03:05 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 03:05 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 03:05 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 03:05 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 03:05 7440-62-201/08/16 18:0025.0 2.5 1
Zinc ND ug/L 01/12/16 03:05 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 18:31 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 18:31 107-13-12001.9 1
Benzene ND ug/L 01/11/16 18:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 18:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 18:31 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 18:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 18:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 18:31 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 18:31 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 18:31 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 18:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 18:31 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 18:31 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 18:31 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 18:31 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 18:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 18:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 18:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 18:31 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 18:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 18:31 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 18:31 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 18:31 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 18:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 18:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 18:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 18:31 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 18:31 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 18:31 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:SW-5 Lab ID:92282266016 Collected:01/06/16 08:30 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 18:31 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 18:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 18:31 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 18:31 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 18:31 108-10-11000.33 1
Styrene ND ug/L 01/11/16 18:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 18:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 18:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 18:31 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 18:31 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 18:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 18:31 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 18:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 18:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 18:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 18:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 18:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 18:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %01/11/16 18:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %01/11/16 18:31 17060-07-070-130 1
Toluene-d8 (S)104 %01/11/16 18:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:SW-6 Lab ID:92282266017 Collected:01/06/16 09:10 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 03:08 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 03:08 7440-38-201/08/16 18:0010.0 2.5 1
Barium 18.5J ug/L 01/12/16 03:08 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 03:08 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 03:08 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 03:08 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 03:08 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 03:08 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 03:08 7439-92-101/08/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 03:08 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 03:08 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 03:08 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 03:08 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 03:08 7440-62-201/08/16 18:0025.0 2.5 1
Zinc ND ug/L 01/12/16 03:08 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 18:48 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 18:48 107-13-12001.9 1
Benzene ND ug/L 01/11/16 18:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 18:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 18:48 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 18:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 18:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 18:48 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 18:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 18:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 18:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 18:48 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 18:48 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 18:48 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 18:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 18:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 18:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 18:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 18:48 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 18:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 18:48 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 18:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 18:48 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 18:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 18:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 18:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 18:48 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 18:48 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 18:48 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 39 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:SW-6 Lab ID:92282266017 Collected:01/06/16 09:10 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 18:48 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 18:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 18:48 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 18:48 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 18:48 108-10-11000.33 1
Styrene ND ug/L 01/11/16 18:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 18:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 18:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 18:48 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 18:48 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 18:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 18:48 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 18:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 18:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 18:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 18:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 18:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 18:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/11/16 18:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %01/11/16 18:48 17060-07-070-130 1
Toluene-d8 (S)102 %01/11/16 18:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-6 Lab ID:92282266018 Collected:01/05/16 16:10 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 03:11 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 03:11 7440-38-201/08/16 18:0010.0 2.5 1
Barium 43.2J ug/L 01/12/16 03:11 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 03:11 7440-41-701/08/16 18:001.0 0.50 1
Cadmium 1.1 ug/L 01/12/16 03:11 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 03:11 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 16.5 ug/L 01/12/16 03:11 7440-48-401/08/16 18:0010.0 2.5 1
Copper 3.5J ug/L 01/12/16 03:11 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 03:11 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 4.5J ug/L 01/12/16 03:11 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 03:11 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 03:11 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 03:11 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 03:11 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 15.8 ug/L 01/12/16 03:11 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.26 ug/L 01/14/16 12:00 7439-97-601/08/16 21:300.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 19:06 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 19:06 107-13-12001.9 1
Benzene ND ug/L 01/11/16 19:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 19:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 19:06 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 19:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 19:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 19:06 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 19:06 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 19:06 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 19:06 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 19:06 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 19:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 19:06 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 19:06 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 19:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 19:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 19:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 19:06 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 19:06 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 19:06 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 19:06 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 19:06 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 19:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 19:06 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 19:06 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-6 Lab ID:92282266018 Collected:01/05/16 16:10 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 19:06 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 19:06 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 19:06 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 19:06 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 19:06 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 19:06 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 19:06 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 19:06 108-10-11000.33 1
Styrene ND ug/L 01/11/16 19:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 19:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 19:06 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 19:06 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 19:06 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 19:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 19:06 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 19:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 19:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 19:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 19:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 19:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 19:06 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %01/11/16 19:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %01/11/16 19:06 17060-07-070-130 1
Toluene-d8 (S)103 %01/11/16 19:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-17 Lab ID:92282266019 Collected:01/05/16 11:15 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 03:14 7440-36-001/08/16 18:006.0 3.8 1
Arsenic 3.0J ug/L 01/12/16 03:14 7440-38-201/08/16 18:0010.0 2.5 1
Barium 56.3J ug/L 01/12/16 03:14 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 03:14 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 03:14 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 03:14 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 14.0 ug/L 01/12/16 03:14 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 03:14 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 03:14 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 3.1J ug/L 01/12/16 03:14 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 03:14 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 03:14 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 03:14 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 03:14 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 6.1J ug/L 01/12/16 03:14 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.27 ug/L 01/14/16 12:40 7439-97-601/08/16 21:300.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 19:23 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 19:23 107-13-12001.9 1
Benzene 0.56J ug/L 01/11/16 19:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 19:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 19:23 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 19:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 19:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 19:23 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 19:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 19:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 19:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 19:23 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 19:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 19:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 19:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 19:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 19:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 19:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 19:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 19:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 19:23 110-57-61001.0 1
1,1-Dichloroethane 0.66J ug/L 01/11/16 19:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 19:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 19:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.6J ug/L 01/11/16 19:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 19:23 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-17 Lab ID:92282266019 Collected:01/05/16 11:15 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 19:23 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 19:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 19:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 19:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 19:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 19:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 19:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 19:23 108-10-11000.33 1
Styrene ND ug/L 01/11/16 19:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 19:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 19:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 19:23 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 19:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 19:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 19:23 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 19:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 19:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 19:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 19:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 19:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 19:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/11/16 19:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %01/11/16 19:23 17060-07-070-130 1
Toluene-d8 (S)102 %01/11/16 19:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-21 Lab ID:92282266020 Collected:01/05/16 11:40 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 03:18 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 03:18 7440-38-201/08/16 18:0010.0 2.5 1
Barium 46.8J ug/L 01/12/16 03:18 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 03:18 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 03:18 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 03:18 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 8.8J ug/L 01/12/16 03:18 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 03:18 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 03:18 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 4.7J ug/L 01/12/16 03:18 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 03:18 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 03:18 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 03:18 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 03:18 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 5.3J ug/L 01/12/16 03:18 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.16J ug/L 01/14/16 12:42 7439-97-601/08/16 21:300.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 19:41 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 19:41 107-13-12001.9 1
Benzene ND ug/L 01/11/16 19:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 19:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 19:41 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 19:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 19:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 19:41 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 19:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 19:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 19:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 19:41 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 19:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 19:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 19:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 19:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 19:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 19:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 19:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 19:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 19:41 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 19:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 19:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 19:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.55J ug/L 01/11/16 19:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 19:41 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
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Page 45 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-21 Lab ID:92282266020 Collected:01/05/16 11:40 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 19:41 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 19:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 19:41 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 19:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 19:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 19:41 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 19:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 19:41 108-10-11000.33 1
Styrene ND ug/L 01/11/16 19:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 19:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 19:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 19:41 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 19:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 19:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 19:41 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 19:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 19:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 19:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 19:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 19:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 19:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/11/16 19:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %01/11/16 19:41 17060-07-070-130 1
Toluene-d8 (S)103 %01/11/16 19:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 46 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-12 Lab ID:92282266021 Collected:01/06/16 15:35 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 16:06 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 16:06 7440-38-201/08/16 18:0010.0 2.5 1
Barium 115 ug/L 01/12/16 16:06 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 16:06 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 16:06 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 16:06 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 75.3 ug/L 01/12/16 16:06 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 16:06 7440-50-801/08/16 18:0010.0 2.5 1
Lead 2.5J ug/L 01/12/16 16:06 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 7.4J ug/L 01/12/16 16:06 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 16:06 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 16:06 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 16:06 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 16:06 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 277 ug/L 01/12/16 16:06 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Dissolved
Iron, Dissolved 35500 ug/L 01/13/16 21:06 7439-89-6 M101/12/16 20:3750.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 19:58 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 19:58 107-13-12001.9 1
Benzene 1.2 ug/L 01/11/16 19:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 19:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 19:58 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 19:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 19:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 19:58 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 19:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 19:58 56-23-51.0 0.25 1
Chlorobenzene 2.4J ug/L 01/11/16 19:58 108-90-73.0 0.23 1
Chloroethane 1.4J ug/L 01/11/16 19:58 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 19:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 19:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 19:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 19:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 19:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 19:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 19:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene 7.3 ug/L 01/11/16 19:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 19:58 110-57-61001.0 1
1,1-Dichloroethane 1.3J ug/L 01/11/16 19:58 75-34-35.0 0.32 1
1,2-Dichloroethane 0.32J ug/L 01/11/16 19:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 19:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 10.4 ug/L 01/11/16 19:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 19:58 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-12 Lab ID:92282266021 Collected:01/06/16 15:35 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 19:58 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 19:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 19:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 19:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 19:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 19:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 19:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 19:58 108-10-11000.33 1
Styrene ND ug/L 01/11/16 19:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 19:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 19:58 79-34-53.0 0.40 1
Tetrachloroethene 0.58J ug/L 01/11/16 19:58 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 19:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 19:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 19:58 79-00-5 L21.0 0.29 1
Trichloroethene 1.6 ug/L 01/11/16 19:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 19:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 19:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 19:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 19:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 19:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/11/16 19:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %01/11/16 19:58 17060-07-070-130 1
Toluene-d8 (S)106 %01/11/16 19:58 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 123000 ug/L 01/19/16 17:46500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/08/16 15:00 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 4920J ug/L 01/13/16 20:32 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 01/08/16 10:491000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 11900 ug/L 01/12/16 21:04 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 25000 ug/L 01/12/16 15:3025000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-12 Lab ID:92282266021 Collected:01/06/16 15:35 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1390 ug/L 01/11/16 18:15 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-12D Lab ID:92282266022 Collected:01/06/16 15:15 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 03:24 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 03:24 7440-38-201/08/16 18:0010.0 2.5 1
Barium 17.1J ug/L 01/12/16 03:24 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 03:24 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 03:24 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 03:24 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 03:24 7440-48-401/08/16 18:0010.0 2.5 1
Copper 2.7J ug/L 01/12/16 03:24 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 03:24 7439-92-101/08/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 03:24 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 03:24 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 03:24 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 03:24 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 03:24 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 19.1 ug/L 01/12/16 03:24 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Dissolved
Iron, Dissolved 262 ug/L 01/13/16 21:24 7439-89-601/12/16 20:3750.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 20:15 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 20:15 107-13-12001.9 1
Benzene ND ug/L 01/11/16 20:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 20:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 20:15 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 20:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 20:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 20:15 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 20:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 20:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 20:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 20:15 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 20:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 20:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 20:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 20:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 20:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 20:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 20:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 20:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 20:15 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 20:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 20:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 20:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.58J ug/L 01/11/16 20:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 20:15 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-12D Lab ID:92282266022 Collected:01/06/16 15:15 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 20:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 20:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 20:15 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 20:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 20:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 20:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 20:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 20:15 108-10-11000.33 1
Styrene ND ug/L 01/11/16 20:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 20:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 20:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 20:15 127-18-41.0 0.46 1
Toluene 0.35J ug/L 01/11/16 20:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 20:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 20:15 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 20:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 20:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 20:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 20:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 20:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 20:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %01/11/16 20:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %01/11/16 20:15 17060-07-070-130 1
Toluene-d8 (S)101 %01/11/16 20:15 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 345000 ug/L 01/19/16 17:59500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/10/16 11:30 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1230J ug/L 01/13/16 20:45 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 59.6J ug/L 01/08/16 10:481000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 58600 ug/L 01/12/16 21:05 16887-00-6200010002
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 23000J ug/L 01/12/16 15:3025000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-12D Lab ID:92282266022 Collected:01/06/16 15:15 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2800 ug/L 01/11/16 18:25 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 52 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-24 Lab ID:92282266023 Collected:01/06/16 13:45 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 03:27 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 03:27 7440-38-201/08/16 18:0010.0 2.5 1
Barium 80.3J ug/L 01/12/16 03:27 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 03:27 7440-41-701/08/16 18:001.0 0.50 1
Cadmium 0.82J ug/L 01/12/16 03:27 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 03:27 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 21.4 ug/L 01/12/16 03:27 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 03:27 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 03:27 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 2.8J ug/L 01/12/16 03:27 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 03:27 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 03:27 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 03:27 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 03:27 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 13.4 ug/L 01/12/16 03:27 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Dissolved
Iron, Dissolved 103 ug/L 01/13/16 21:27 7439-89-601/12/16 20:3750.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 20:33 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 20:33 107-13-12001.9 1
Benzene ND ug/L 01/11/16 20:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 20:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 20:33 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 20:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 20:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 20:33 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 20:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 20:33 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 20:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 20:33 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 20:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 20:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 20:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 20:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 20:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 20:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 20:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.56J ug/L 01/11/16 20:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 20:33 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 20:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 20:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 20:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.1J ug/L 01/11/16 20:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 20:33 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 53 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-24 Lab ID:92282266023 Collected:01/06/16 13:45 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 20:33 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 20:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 20:33 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 20:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 20:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 20:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 20:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 20:33 108-10-11000.33 1
Styrene ND ug/L 01/11/16 20:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 20:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 20:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 20:33 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 20:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 20:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 20:33 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 20:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 20:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 20:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 20:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 20:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 20:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/11/16 20:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %01/11/16 20:33 17060-07-070-130 1
Toluene-d8 (S)102 %01/11/16 20:33 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 31000 ug/L 01/19/16 18:50500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/08/16 15:00 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2460J ug/L 01/13/16 20:59 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 315J ug/L 01/08/16 10:441000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 21700 ug/L 01/12/16 21:09 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 14000J ug/L 01/12/16 15:3025000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-24 Lab ID:92282266023 Collected:01/06/16 13:45 Received:01/07/16 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 5020 ug/L 01/12/16 09:25 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-2 Lab ID:92282266024 Collected:01/07/16 10:05 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 21:56 7440-36-001/11/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 21:56 7440-38-201/11/16 18:0010.0 2.5 1
Barium 24.8J ug/L 01/12/16 21:56 7440-39-301/11/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 21:56 7440-41-701/11/16 18:001.0 0.50 1
Cadmium 1.1 ug/L 01/12/16 21:56 7440-43-901/11/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 21:56 7440-47-301/11/16 18:0010.0 2.5 1
Cobalt 195 ug/L 01/12/16 21:56 7440-48-401/11/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 21:56 7440-50-801/11/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 21:56 7439-92-101/11/16 18:0010.0 2.5 1
Nickel 4.5J ug/L 01/12/16 21:56 7440-02-001/11/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 21:56 7782-49-201/11/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 21:56 7440-22-401/11/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 21:56 7440-28-001/11/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 21:56 7440-62-201/11/16 18:0025.0 2.5 1
Zinc 10.6 ug/L 01/12/16 21:56 7440-66-601/11/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 20:50 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 20:50 107-13-12001.9 1
Benzene 0.46J ug/L 01/11/16 20:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 20:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 20:50 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 20:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 20:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 20:50 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 20:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 20:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 20:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 20:50 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 20:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 20:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 20:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 20:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 20:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 20:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 20:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.56J ug/L 01/11/16 20:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 20:50 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 20:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 20:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 20:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.9J ug/L 01/11/16 20:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 20:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 20:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 20:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 20:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-2 Lab ID:92282266024 Collected:01/07/16 10:05 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 20:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 20:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 20:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 20:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 20:50 108-10-11000.33 1
Styrene ND ug/L 01/11/16 20:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 20:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 20:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 20:50 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 20:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 20:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 20:50 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 20:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 20:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 20:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 20:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 20:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 20:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %01/11/16 20:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %01/11/16 20:50 17060-07-070-130 1
Toluene-d8 (S)101 %01/11/16 20:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-14 Lab ID:92282266025 Collected:01/07/16 09:30 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 22:00 7440-36-001/11/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 22:00 7440-38-201/11/16 18:0010.0 2.5 1
Barium 30.4J ug/L 01/12/16 22:00 7440-39-301/11/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 22:00 7440-41-701/11/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 22:00 7440-43-901/11/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 22:00 7440-47-301/11/16 18:0010.0 2.5 1
Cobalt 8.2J ug/L 01/12/16 22:00 7440-48-401/11/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 22:00 7440-50-801/11/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 22:00 7439-92-101/11/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 22:00 7440-02-001/11/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 22:00 7782-49-201/11/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 22:00 7440-22-401/11/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 22:00 7440-28-001/11/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 22:00 7440-62-201/11/16 18:0025.0 2.5 1
Zinc ND ug/L 01/12/16 22:00 7440-66-601/11/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 21:08 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 21:08 107-13-12001.9 1
Benzene ND ug/L 01/11/16 21:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 21:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 21:08 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 21:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 21:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 21:08 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 21:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 21:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 21:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 21:08 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 21:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 21:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 21:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 21:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 21:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 21:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 21:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 21:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 21:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 21:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 21:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 21:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 21:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 21:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 21:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 21:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 21:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-14 Lab ID:92282266025 Collected:01/07/16 09:30 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 21:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 21:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 21:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 21:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 21:08 108-10-11000.33 1
Styrene ND ug/L 01/11/16 21:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 21:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 21:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 21:08 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 21:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 21:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 21:08 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 21:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 21:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 21:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 21:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 21:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 21:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %01/11/16 21:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %01/11/16 21:08 17060-07-070-130 1
Toluene-d8 (S)102 %01/11/16 21:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-15 Lab ID:92282266026 Collected:01/07/16 11:40 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 22:03 7440-36-001/11/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 22:03 7440-38-201/11/16 18:0010.0 2.5 1
Barium 14.3J ug/L 01/12/16 22:03 7440-39-301/11/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 22:03 7440-41-701/11/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 22:03 7440-43-901/11/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 22:03 7440-47-301/11/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 22:03 7440-48-401/11/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 22:03 7440-50-801/11/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 22:03 7439-92-101/11/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 22:03 7440-02-001/11/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 22:03 7782-49-201/11/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 22:03 7440-22-401/11/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 22:03 7440-28-001/11/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 22:03 7440-62-201/11/16 18:0025.0 2.5 1
Zinc ND ug/L 01/12/16 22:03 7440-66-601/11/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 21:25 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 21:25 107-13-12001.9 1
Benzene 2.6 ug/L 01/11/16 21:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 21:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 21:25 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 21:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 21:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 21:25 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 21:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 21:25 56-23-51.0 0.25 1
Chlorobenzene 0.48J ug/L 01/11/16 21:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 21:25 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 21:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 21:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 21:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 21:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 21:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 21:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 21:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.64J ug/L 01/11/16 21:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 21:25 110-57-61001.0 1
1,1-Dichloroethane 1.2J ug/L 01/11/16 21:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 21:25 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 21:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 7.7 ug/L 01/11/16 21:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 21:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 21:25 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 21:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 21:25 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-15 Lab ID:92282266026 Collected:01/07/16 11:40 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 21:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 21:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 21:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 21:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 21:25 108-10-11000.33 1
Styrene ND ug/L 01/11/16 21:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 21:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 21:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 21:25 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 21:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 21:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 21:25 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 21:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 21:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 21:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 21:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 21:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 21:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/11/16 21:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %01/11/16 21:25 17060-07-070-130 1
Toluene-d8 (S)100 %01/11/16 21:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-19 Lab ID:92282266027 Collected:01/07/16 10:55 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 22:06 7440-36-001/11/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 22:06 7440-38-201/11/16 18:0010.0 2.5 1
Barium 21.7J ug/L 01/12/16 22:06 7440-39-301/11/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 22:06 7440-41-701/11/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 22:06 7440-43-901/11/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 22:06 7440-47-301/11/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 22:06 7440-48-401/11/16 18:0010.0 2.5 1
Copper 2.6J ug/L 01/12/16 22:06 7440-50-801/11/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 22:06 7439-92-101/11/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 22:06 7440-02-001/11/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 22:06 7782-49-201/11/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 22:06 7440-22-401/11/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 22:06 7440-28-001/11/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 22:06 7440-62-201/11/16 18:0025.0 2.5 1
Zinc ND ug/L 01/12/16 22:06 7440-66-601/11/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 22:00 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 22:00 107-13-12001.9 1
Benzene ND ug/L 01/11/16 22:00 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 22:00 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 22:00 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 22:00 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 22:00 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 22:00 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 22:00 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 22:00 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 22:00 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 22:00 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 22:00 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 22:00 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 22:00 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 22:00 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 22:00 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 22:00 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 22:00 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 22:00 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 22:00 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 22:00 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 22:00 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 22:00 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 22:00 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 22:00 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 22:00 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 22:00 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 22:00 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-19 Lab ID:92282266027 Collected:01/07/16 10:55 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 22:00 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 22:00 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 22:00 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 22:00 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 22:00 108-10-11000.33 1
Styrene ND ug/L 01/11/16 22:00 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 22:00 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 22:00 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 22:00 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 22:00 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 22:00 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 22:00 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 22:00 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 22:00 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 22:00 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 22:00 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 22:00 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 22:00 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/11/16 22:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %01/11/16 22:00 17060-07-070-130 1
Toluene-d8 (S)102 %01/11/16 22:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-20 Lab ID:92282266028 Collected:01/07/16 14:30 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 22:09 7440-36-001/11/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 22:09 7440-38-201/11/16 18:0010.0 2.5 1
Barium 42.6J ug/L 01/12/16 22:09 7440-39-301/11/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 22:09 7440-41-701/11/16 18:001.0 0.50 1
Cadmium 0.83J ug/L 01/12/16 22:09 7440-43-901/11/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 22:09 7440-47-301/11/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 22:09 7440-48-401/11/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 22:09 7440-50-801/11/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 22:09 7439-92-101/11/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 22:09 7440-02-001/11/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 22:09 7782-49-201/11/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 22:09 7440-22-401/11/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 22:09 7440-28-001/11/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 22:09 7440-62-201/11/16 18:0025.0 2.5 1
Zinc ND ug/L 01/12/16 22:09 7440-66-601/11/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 22:17 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 22:17 107-13-12001.9 1
Benzene ND ug/L 01/11/16 22:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 22:17 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 22:17 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 22:17 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 22:17 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 22:17 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 22:17 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 22:17 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 22:17 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 22:17 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 22:17 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 22:17 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 22:17 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 22:17 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 22:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 22:17 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 22:17 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 22:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 22:17 110-57-61001.0 1
1,1-Dichloroethane 0.37J ug/L 01/11/16 22:17 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 22:17 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 22:17 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 22:17 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 22:17 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 22:17 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 22:17 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 22:17 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-20 Lab ID:92282266028 Collected:01/07/16 14:30 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 22:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 22:17 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 22:17 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 22:17 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 22:17 108-10-11000.33 1
Styrene ND ug/L 01/11/16 22:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 22:17 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 22:17 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 22:17 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 22:17 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 22:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 22:17 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 22:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 22:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 22:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 22:17 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 22:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 22:17 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %01/11/16 22:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %01/11/16 22:17 17060-07-070-130 1
Toluene-d8 (S)104 %01/11/16 22:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-25 Lab ID:92282266029 Collected:01/07/16 16:00 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 22:12 7440-36-001/11/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 22:12 7440-38-201/11/16 18:0010.0 2.5 1
Barium 70.0J ug/L 01/12/16 22:12 7440-39-301/11/16 18:001002.5 1
Beryllium ND ug/L 01/12/16 22:12 7440-41-701/11/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 22:12 7440-43-901/11/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 22:12 7440-47-301/11/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 22:12 7440-48-401/11/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 22:12 7440-50-801/11/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 22:12 7439-92-101/11/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 22:12 7440-02-001/11/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 22:12 7782-49-201/11/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 22:12 7440-22-401/11/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 22:12 7440-28-001/11/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 22:12 7440-62-201/11/16 18:0025.0 2.5 1
Zinc 15.7 ug/L 01/12/16 22:12 7440-66-601/11/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 22:35 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 22:35 107-13-12001.9 1
Benzene ND ug/L 01/11/16 22:35 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 22:35 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 22:35 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 22:35 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 22:35 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 22:35 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 22:35 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 22:35 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 22:35 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 22:35 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 22:35 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 22:35 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 22:35 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 22:35 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 22:35 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 22:35 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 22:35 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 22:35 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 22:35 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 22:35 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 22:35 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 22:35 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 22:35 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 22:35 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 22:35 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 22:35 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 22:35 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
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Page 66 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-25 Lab ID:92282266029 Collected:01/07/16 16:00 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 22:35 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 22:35 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 22:35 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 22:35 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 22:35 108-10-11000.33 1
Styrene ND ug/L 01/11/16 22:35 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 22:35 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 22:35 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 22:35 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 22:35 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 22:35 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 22:35 79-00-5 L21.0 0.29 1
Trichloroethene ND ug/L 01/11/16 22:35 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 22:35 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 22:35 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 22:35 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 22:35 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 22:35 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %01/11/16 22:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %01/11/16 22:35 17060-07-070-130 1
Toluene-d8 (S)103 %01/11/16 22:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
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Page 67 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-7 Lab ID:92282266030 Collected:01/07/16 13:35 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/12/16 22:15 7440-36-001/11/16 18:006.0 3.8 1
Arsenic ND ug/L 01/12/16 22:15 7440-38-201/11/16 18:0010.0 2.5 1
Barium 5.7J ug/L 01/12/16 22:15 7440-39-301/11/16 18:001002.5 1
Beryllium 0.52J ug/L 01/12/16 22:15 7440-41-701/11/16 18:001.0 0.50 1
Cadmium ND ug/L 01/12/16 22:15 7440-43-901/11/16 18:001.0 0.50 1
Chromium ND ug/L 01/12/16 22:15 7440-47-301/11/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/12/16 22:15 7440-48-401/11/16 18:0010.0 2.5 1
Copper ND ug/L 01/12/16 22:15 7440-50-801/11/16 18:0010.0 2.5 1
Lead ND ug/L 01/12/16 22:15 7439-92-101/11/16 18:0010.0 2.5 1
Nickel ND ug/L 01/12/16 22:15 7440-02-001/11/16 18:0050.0 2.5 1
Selenium ND ug/L 01/12/16 22:15 7782-49-201/11/16 18:0010.0 5.0 1
Silver ND ug/L 01/12/16 22:15 7440-22-401/11/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 22:15 7440-28-001/11/16 18:005.5 5.0 1
Vanadium ND ug/L 01/12/16 22:15 7440-62-201/11/16 18:0025.0 2.5 1
Zinc ND ug/L 01/12/16 22:15 7440-66-601/11/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/12/16 03:50 67-64-110010.0 1
Acrylonitrile ND ug/L 01/12/16 03:50 107-13-12001.9 1
Benzene 2.2 ug/L 01/12/16 03:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/12/16 03:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/12/16 03:50 75-27-41.0 0.18 1
Bromoform ND ug/L 01/12/16 03:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/12/16 03:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/12/16 03:50 78-93-31000.96 1
Carbon disulfide ND ug/L 01/12/16 03:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/12/16 03:50 56-23-51.0 0.25 1
Chlorobenzene 1.0J ug/L 01/12/16 03:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/12/16 03:50 75-00-310.0 0.54 1
Chloroform ND ug/L 01/12/16 03:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/12/16 03:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/12/16 03:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/12/16 03:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/12/16 03:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/12/16 03:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/12/16 03:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.5 ug/L 01/12/16 03:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/12/16 03:50 110-57-61001.0 1
1,1-Dichloroethane 1.2J ug/L 01/12/16 03:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/12/16 03:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/12/16 03:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 4.9J ug/L 01/12/16 03:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/12/16 03:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/12/16 03:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/12/16 03:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/12/16 03:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 110
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Sample:MW-7 Lab ID:92282266030 Collected:01/07/16 13:35 Received:01/08/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/12/16 03:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/12/16 03:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/12/16 03:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/12/16 03:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/12/16 03:50 108-10-11000.33 1
Styrene ND ug/L 01/12/16 03:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/12/16 03:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/12/16 03:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/12/16 03:50 127-18-41.0 0.46 1
Toluene ND ug/L 01/12/16 03:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/12/16 03:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/12/16 03:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/12/16 03:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/12/16 03:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/12/16 03:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/12/16 03:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/12/16 03:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/12/16 03:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %01/12/16 03:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %01/12/16 03:50 17060-07-070-130 1
Toluene-d8 (S)100 %01/12/16 03:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 69 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/8850
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92282266001, 92282266002, 92282266018, 92282266019, 92282266020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1643395
Associated Lab Samples:92282266001, 92282266002, 92282266018, 92282266019, 92282266020
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 01/14/16 11:100.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1643396LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643397MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281698007
1643398
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 92 75-12593 1 252.5ND 2.4 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
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Page 70 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20439
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92282266001, 92282266002, 92282266003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1643941
Associated Lab Samples:92282266001, 92282266002, 92282266003
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/11/16 16:393.8
Arsenic ug/L ND 10.0 01/11/16 16:392.5
Barium ug/L ND 100 01/11/16 16:392.5
Beryllium ug/L ND 1.0 01/11/16 16:390.50
Cadmium ug/L ND 1.0 01/11/16 16:390.50
Chromium ug/L ND 10.0 01/11/16 16:392.5
Cobalt ug/L 5.0J 10.0 01/11/16 16:392.5
Copper ug/L ND 10.0 01/11/16 16:392.5
Lead ug/L ND 10.0 01/11/16 16:392.5
Nickel ug/L ND 50.0 01/11/16 16:392.5
Selenium ug/L ND 10.0 01/11/16 16:395.0
Silver ug/L ND 10.0 01/11/16 16:392.5
Thallium ug/L ND 5.5 01/11/16 16:395.0
Vanadium ug/L ND 25.0 01/11/16 16:392.5
Zinc ug/L ND 10.0 01/11/16 16:395.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1643942LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 466500 93 80-120
Barium ug/L 457500 91 80-120
Beryllium ug/L 452500 90 80-120
Cadmium ug/L 467500 93 80-120
Chromium ug/L 454500 91 80-120
Cobalt ug/L 473500 95 80-120
Copper ug/L 463500 93 80-120
Lead ug/L 467500 93 80-120
Nickel ug/L 468500 94 80-120
Selenium ug/L 467500 93 80-120
Silver ug/L 236250 94 80-120
Thallium ug/L 450500 90 80-120
Vanadium ug/L 458500 92 80-120
Zinc ug/L 467500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643943MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282072001
1643944
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125104 0 25500ND520521
Arsenic ug/L 500 99 75-12599 0 25500ND498497
Barium ug/L 500 97 75-12595 1 25500140623617
Beryllium ug/L 500 96 75-12596 1 25500ND482478
Cadmium ug/L 500 98 75-12598 0 25500ND490491
Chromium ug/L 500 95 75-12595 0 25500ND477477
Cobalt ug/L 500 96 75-12596 0 25500ND480481
Copper ug/L 500 99 75-12598 0 25500ND494492
Lead ug/L 500 93 75-12593 0 25500ND464465
Nickel ug/L 500 95 75-12595 0 25500ND476477
Selenium ug/L 500 98 75-12598 0 25500ND490491
Silver ug/L 250 100 75-125100 0 25250ND250250
Thallium ug/L 500 86 75-12589 3 255006.2 438 450
Vanadium ug/L 500 98 75-12599 0 25500ND492493
Zinc ug/L 500 97 75-12597 0 2550011.3 497 497
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20440
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92282266004, 92282266005, 92282266006, 92282266007, 92282266008, 92282266009, 92282266010,
92282266011, 92282266012, 92282266013, 92282266014, 92282266015, 92282266016, 92282266017,
92282266018, 92282266019, 92282266020, 92282266021, 92282266022, 92282266023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1643956
Associated Lab Samples:92282266004, 92282266005, 92282266006, 92282266007, 92282266008, 92282266009, 92282266010,
92282266011, 92282266012, 92282266013, 92282266014, 92282266015, 92282266016, 92282266017,
92282266018, 92282266019, 92282266020, 92282266021, 92282266022, 92282266023
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/12/16 01:573.8
Arsenic ug/L ND 10.0 01/12/16 01:572.5
Barium ug/L ND 100 01/12/16 01:572.5
Beryllium ug/L ND 1.0 01/12/16 01:570.50
Cadmium ug/L ND 1.0 01/12/16 01:570.50
Chromium ug/L ND 10.0 01/12/16 01:572.5
Cobalt ug/L ND 10.0 01/12/16 01:572.5
Copper ug/L ND 10.0 01/12/16 01:572.5
Lead ug/L ND 10.0 01/12/16 01:572.5
Nickel ug/L ND 50.0 01/12/16 01:572.5
Selenium ug/L ND 10.0 01/12/16 01:575.0
Silver ug/L ND 10.0 01/12/16 01:572.5
Thallium ug/L ND 5.5 01/12/16 15:295.0
Vanadium ug/L ND 25.0 01/12/16 01:572.5
Zinc ug/L ND 10.0 01/12/16 01:575.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1643957LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 504500 101 80-120
Arsenic ug/L 468500 94 80-120
Barium ug/L 487500 97 80-120
Beryllium ug/L 482500 96 80-120
Cadmium ug/L 483500 97 80-120
Chromium ug/L 480500 96 80-120
Cobalt ug/L 485500 97 80-120
Copper ug/L 484500 97 80-120
Lead ug/L 480500 96 80-120
Nickel ug/L 487500 97 80-120
Selenium ug/L 474500 95 80-120
Silver ug/L 244250 98 80-120
Thallium ug/L 433500 87 80-120
Vanadium ug/L 482500 96 80-120
Zinc ug/L 480500 96 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643958MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282266004
1643959
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 101 75-125101 1 25500ND506503
Arsenic ug/L 500 95 75-12594 1 255002.6J 478 472
Barium ug/L 500 98 75-12597 1 2550046.0J 535 530
Beryllium ug/L 500 98 75-12597 1 25500ND488484
Cadmium ug/L 500 97 75-12596 1 25500ND486481
Chromium ug/L 500 96 75-12596 0 255003.9J 483 482
Cobalt ug/L 500 96 75-12595 2 255007.1J 489 480
Copper ug/L 500 99 75-12598 1 255002.8J 496 493
Lead ug/L 500 95 75-12594 1 25500ND477470
Nickel ug/L 500 96 75-12596 1 25500ND483480
Selenium ug/L 500 93 75-12592 1 25500ND464460
Silver ug/L 250 99 75-12598 1 25250ND247245
Thallium ug/L 500 86 75-12588 2 25500ND432439
Vanadium ug/L 500 97 75-12597 0 255003.3J 489 487
Zinc ug/L 500 97 75-12594 3 2550013.9 500 484
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20449
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92282266024, 92282266025, 92282266026, 92282266027, 92282266028, 92282266029, 92282266030
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644706
Associated Lab Samples:92282266024, 92282266025, 92282266026, 92282266027, 92282266028, 92282266029, 92282266030
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/12/16 21:263.8
Arsenic ug/L ND 10.0 01/12/16 21:262.5
Barium ug/L ND 100 01/12/16 21:262.5
Beryllium ug/L ND 1.0 01/12/16 21:260.50
Cadmium ug/L ND 1.0 01/12/16 21:260.50
Chromium ug/L ND 10.0 01/12/16 21:262.5
Cobalt ug/L ND 10.0 01/12/16 21:262.5
Copper ug/L ND 10.0 01/12/16 21:262.5
Lead ug/L ND 10.0 01/12/16 21:262.5
Nickel ug/L ND 50.0 01/12/16 21:262.5
Selenium ug/L ND 10.0 01/12/16 21:265.0
Silver ug/L ND 10.0 01/12/16 21:262.5
Thallium ug/L ND 5.5 01/12/16 21:265.0
Vanadium ug/L ND 25.0 01/12/16 21:262.5
Zinc ug/L ND 10.0 01/12/16 21:265.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644707LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 497500 99 80-120
Arsenic ug/L 470500 94 80-120
Barium ug/L 460500 92 80-120
Beryllium ug/L 452500 90 80-120
Cadmium ug/L 454500 91 80-120
Chromium ug/L 424500 85 80-120
Cobalt ug/L 464500 93 80-120
Copper ug/L 452500 90 80-120
Lead ug/L 459500 92 80-120
Nickel ug/L 452500 90 80-120
Selenium ug/L 468500 94 80-120
Silver ug/L 233250 93 80-120
Thallium ug/L 442500 88 80-120
Vanadium ug/L 439500 88 80-120
Zinc ug/L 468500 94 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282291001
1644709
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 107 75-125103 3 25500ND536520
Arsenic ug/L 500 102 75-12599 3 25500ND512495
Barium ug/L 500 99 75-12596 2 25500105599584
Beryllium ug/L 500 97 75-12595 3 25500ND487474
Cadmium ug/L 500 98 75-12595 3 2550067.2 558 540
Chromium ug/L 500 89 75-12587 2 25500ND447437
Cobalt ug/L 500 98 75-12594 4 25500ND489472
Copper ug/L 500 96 75-12594 3 25500ND484470
Lead ug/L 500 96 75-12593 3 25500ND482466
Nickel ug/L 500 95 75-12592 3 25500156631614
Selenium ug/L 500 100 75-12596 3 25500ND499483
Silver ug/L 250 98 75-12596 3 25250ND246240
Thallium ug/L 500 92 75-12589 3 25500ND462448
Vanadium ug/L 500 95 75-12592 3 25500ND475460
Zinc ug/L 500 100 75-12595 2 2550073512401210
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20453
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Associated Lab Samples:92282266021, 92282266022, 92282266023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644723
Associated Lab Samples:92282266021, 92282266022, 92282266023
Matrix:Water
AnalyzedMDL
Iron, Dissolved ug/L ND 50.0 01/13/16 21:0025.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644724LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Dissolved ug/L 49705000 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644725MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282266021
1644726
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Iron, Dissolved ug/L M150007475-12586 1 205000355003920039800
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35119
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92282266001, 92282266002, 92282266003, 92282266004, 92282266005, 92282266006, 92282266007,
92282266008, 92282266009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644503
Associated Lab Samples:92282266001, 92282266002, 92282266003, 92282266004, 92282266005, 92282266006, 92282266007,
92282266008, 92282266009
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/11/16 10:420.33
1,1,1-Trichloroethane ug/L ND 1.0 01/11/16 10:420.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/11/16 10:420.40
1,1,2-Trichloroethane ug/L ND 1.0 01/11/16 10:420.29
1,1-Dichloroethane ug/L ND 5.0 01/11/16 10:420.32
1,1-Dichloroethene ug/L ND 5.0 01/11/16 10:420.56
1,2,3-Trichloropropane ug/L ND 1.0 01/11/16 10:420.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/11/16 10:422.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/11/16 10:420.27
1,2-Dichlorobenzene ug/L ND 5.0 01/11/16 10:420.30
1,2-Dichloroethane ug/L ND 1.0 01/11/16 10:420.24
1,2-Dichloropropane ug/L ND 1.0 01/11/16 10:420.27
1,4-Dichlorobenzene ug/L ND 1.0 01/11/16 10:420.33
2-Butanone (MEK)ug/L ND 100 01/11/16 10:420.96
2-Hexanone ug/L ND 50.0 01/11/16 10:420.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/11/16 10:420.33
Acetone ug/L ND 100 01/11/16 10:4210.0
Acrylonitrile ug/L ND 200 01/11/16 10:421.9
Benzene ug/L ND 1.0 01/11/16 10:420.25
Bromochloromethane ug/L ND 3.0 01/11/16 10:420.17
Bromodichloromethane ug/L ND 1.0 01/11/16 10:420.18
Bromoform ug/L ND 3.0 01/11/16 10:420.26
Bromomethane ug/L ND 10.0 01/11/16 10:420.29
Carbon disulfide ug/L ND 100 01/11/16 10:421.2
Carbon tetrachloride ug/L ND 1.0 01/11/16 10:420.25
Chlorobenzene ug/L ND 3.0 01/11/16 10:420.23
Chloroethane ug/L ND 10.0 01/11/16 10:420.54
Chloroform ug/L ND 5.0 01/11/16 10:420.14
Chloromethane ug/L ND 1.0 01/11/16 10:420.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/11/16 10:420.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/11/16 10:420.13
Dibromochloromethane ug/L ND 3.0 01/11/16 10:420.21
Dibromomethane ug/L ND 10.0 01/11/16 10:420.21
Ethylbenzene ug/L ND 1.0 01/11/16 10:420.30
Iodomethane ug/L ND 10.0 01/11/16 10:420.32
Methylene Chloride ug/L ND 1.0 01/11/16 10:420.97
Styrene ug/L ND 1.0 01/11/16 10:420.26
Tetrachloroethene ug/L ND 1.0 01/11/16 10:420.46
Toluene ug/L ND 1.0 01/11/16 10:420.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/11/16 10:420.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644503
Associated Lab Samples:92282266001, 92282266002, 92282266003, 92282266004, 92282266005, 92282266006, 92282266007,
92282266008, 92282266009
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 01/11/16 10:420.26
trans-1,4-Dichloro-2-butene ug/L ND 100 01/11/16 10:421.0
Trichloroethene ug/L ND 1.0 01/11/16 10:420.47
Trichlorofluoromethane ug/L ND 1.0 01/11/16 10:420.20
Vinyl acetate ug/L ND 50.0 01/11/16 10:420.35
Vinyl chloride ug/L ND 1.0 01/11/16 10:420.62
Xylene (Total)ug/L ND 5.0 01/11/16 10:420.66
1,2-Dichloroethane-d4 (S)%99 70-130 01/11/16 10:42
4-Bromofluorobenzene (S)%108 70-130 01/11/16 10:42
Toluene-d8 (S)%101 70-130 01/11/16 10:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644504LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.350 97 80-125
1,1,1-Trichloroethane ug/L 48.850 98 71-129
1,1,2,2-Tetrachloroethane ug/L 49.650 99 79-124
1,1,2-Trichloroethane ug/L 47.850 96 85-125
1,1-Dichloroethane ug/L 48.250 96 73-126
1,1-Dichloroethene ug/L 48.050 96 66-135
1,2,3-Trichloropropane ug/L 49.250 98 75-130
1,2-Dibromo-3-chloropropane ug/L 48.550 97 71-133
1,2-Dibromoethane (EDB)ug/L 49.150 98 83-124
1,2-Dichlorobenzene ug/L 48.350 97 80-133
1,2-Dichloroethane ug/L 45.250 90 67-128
1,2-Dichloropropane ug/L 46.450 93 75-132
1,4-Dichlorobenzene ug/L 50.150 100 78-130
2-Butanone (MEK)ug/L 97.0J100 97 61-144
2-Hexanone ug/L 98.5100 99 68-143
4-Methyl-2-pentanone (MIBK)ug/L 98.8J100 99 72-135
Acetone ug/L 105100 105 48-146
Acrylonitrile ug/L 248250 99 40-160
Benzene ug/L 48.650 97 80-125
Bromochloromethane ug/L 50.650 101 71-125
Bromodichloromethane ug/L 49.650 99 78-124
Bromoform ug/L 44.050 88 71-128
Bromomethane ug/L 46.050 92 40-160
Carbon disulfide ug/L 53.8J50 108 50-160
Carbon tetrachloride ug/L 50.250 100 69-131
Chlorobenzene ug/L 48.150 96 81-122
Chloroethane ug/L 42.850 86 39-148
Chloroform ug/L 47.850 96 73-127
Chloromethane ug/L 45.450 91 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644504LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 46.950 94 74-124
cis-1,3-Dichloropropene ug/L 48.750 97 72-132
Dibromochloromethane ug/L 49.850 100 78-125
Dibromomethane ug/L 50.450 101 82-120
Ethylbenzene ug/L 47.550 95 79-121
Iodomethane ug/L 72.8100 73 39-154
Methylene Chloride ug/L 43.150 86 64-133
Styrene ug/L 49.350 99 84-126
Tetrachloroethene ug/L 48.350 97 78-122
Toluene ug/L 47.850 96 80-121
trans-1,2-Dichloroethene ug/L 47.250 94 71-127
trans-1,3-Dichloropropene ug/L 50.250 100 69-141
trans-1,4-Dichloro-2-butene ug/L 52.4J50 105 40-160
Trichloroethene ug/L 48.450 97 78-122
Trichlorofluoromethane ug/L 48.150 96 53-137
Vinyl acetate ug/L 99.5100 100 40-160
Vinyl chloride ug/L 49.950 100 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1644505MATRIX SPIKE SAMPLE:
MSSpike
Result
92282265001
1,1,1,2-Tetrachloroethane ug/L 21.720 109 70-130ND
1,1,1-Trichloroethane ug/L 22.820 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.220 101 70-130ND
1,1,2-Trichloroethane ug/L 20.720 104 70-130ND
1,1-Dichloroethane ug/L 22.020 110 70-130ND
1,1-Dichloroethene ug/L 22.620 113 70-166ND
1,2,3-Trichloropropane ug/L 21.420 107 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.720 103 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.620 108 70-130ND
1,2-Dichlorobenzene ug/L 21.820 105 70-1300.74J
1,2-Dichloroethane ug/L 22.020 108 70-1300.30J
1,2-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 32.020 107 70-13010.6
2-Butanone (MEK)ug/L 42.6J40 106 70-130ND
2-Hexanone ug/L 44.3J40 111 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 47.0J40 118 70-130ND
Acetone ug/L 77.0J M14019270-130ND
Acrylonitrile ug/L 110J100 110 70-130ND
Benzene ug/L 27.820 109 70-1485.9
Bromochloromethane ug/L 21.720 108 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1644505MATRIX SPIKE SAMPLE:
MSSpike
Result
92282265001
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 19.120 96 70-130ND
Bromomethane ug/L 21.120 106 70-130ND
Carbon disulfide ug/L 21.2J20 106 70-130ND
Carbon tetrachloride ug/L 25.520 127 70-130ND
Chlorobenzene ug/L 22.620 106 70-1461.4J
Chloroethane ug/L 20.620 103 70-130ND
Chloroform ug/L 22.120 110 70-130ND
Chloromethane ug/L 23.720 118 70-130ND
cis-1,2-Dichloroethene ug/L 28.420 109 70-1306.6
cis-1,3-Dichloropropene ug/L 20.220 101 70-130ND
Dibromochloromethane ug/L 20.420 102 70-130ND
Dibromomethane ug/L 22.420 112 70-130ND
Ethylbenzene ug/L 22.820 108 70-1301.2
Iodomethane ug/L 33.040 82 70-130ND
Methylene Chloride ug/L 21.920 109 70-130ND
Styrene ug/L 21.320 107 70-130ND
Tetrachloroethene ug/L 23.120 115 70-130ND
Toluene ug/L 22.020 108 70-1550.43J
trans-1,2-Dichloroethene ug/L 22.220 111 70-130ND
trans-1,3-Dichloropropene ug/L 22.020 110 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.8J20 99 70-130ND
Trichloroethene ug/L 22.620 109 69-1510.72J
Trichlorofluoromethane ug/L 24.520 123 70-130ND
Vinyl acetate ug/L 39.2J40 98 70-130ND
Vinyl chloride ug/L 23.220 114 70-130ND
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%109 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282265002
1644506SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L 0.42J 300.44J
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282265002
1644506SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L 7.6 2 307.5
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 2.9 3 302.9
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 2.1J 8 301.9J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 14.3 1 3014.2
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%110 0110
4-Bromofluorobenzene (S)%113 2110
Toluene-d8 (S)%100 0100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35120
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92282266010, 92282266011, 92282266012, 92282266013, 92282266014, 92282266015, 92282266016,
92282266017, 92282266018, 92282266019, 92282266020, 92282266021, 92282266022, 92282266023,
92282266024, 92282266025, 92282266026, 92282266027, 92282266028, 92282266029
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644536
Associated Lab Samples:92282266010, 92282266011, 92282266012, 92282266013, 92282266014, 92282266015, 92282266016,
92282266017, 92282266018, 92282266019, 92282266020, 92282266021, 92282266022, 92282266023,
92282266024, 92282266025, 92282266026, 92282266027, 92282266028, 92282266029
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/11/16 16:290.33
1,1,1-Trichloroethane ug/L ND 1.0 01/11/16 16:290.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/11/16 16:290.40
1,1,2-Trichloroethane ug/L ND 1.0 01/11/16 16:290.29
1,1-Dichloroethane ug/L ND 5.0 01/11/16 16:290.32
1,1-Dichloroethene ug/L ND 5.0 01/11/16 16:290.56
1,2,3-Trichloropropane ug/L ND 1.0 01/11/16 16:290.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/11/16 16:292.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/11/16 16:290.27
1,2-Dichlorobenzene ug/L ND 5.0 01/11/16 16:290.30
1,2-Dichloroethane ug/L ND 1.0 01/11/16 16:290.24
1,2-Dichloropropane ug/L ND 1.0 01/11/16 16:290.27
1,4-Dichlorobenzene ug/L ND 1.0 01/11/16 16:290.33
2-Butanone (MEK)ug/L ND 100 01/11/16 16:290.96
2-Hexanone ug/L ND 50.0 01/11/16 16:290.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/11/16 16:290.33
Acetone ug/L ND 100 01/11/16 16:2910.0
Acrylonitrile ug/L ND 200 01/11/16 16:291.9
Benzene ug/L ND 1.0 01/11/16 16:290.25
Bromochloromethane ug/L ND 3.0 01/11/16 16:290.17
Bromodichloromethane ug/L ND 1.0 01/11/16 16:290.18
Bromoform ug/L ND 3.0 01/11/16 16:290.26
Bromomethane ug/L ND 10.0 01/11/16 16:290.29
Carbon disulfide ug/L ND 100 01/11/16 16:291.2
Carbon tetrachloride ug/L ND 1.0 01/11/16 16:290.25
Chlorobenzene ug/L ND 3.0 01/11/16 16:290.23
Chloroethane ug/L ND 10.0 01/11/16 16:290.54
Chloroform ug/L ND 5.0 01/11/16 16:290.14
Chloromethane ug/L ND 1.0 01/11/16 16:290.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/11/16 16:290.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/11/16 16:290.13
Dibromochloromethane ug/L ND 3.0 01/11/16 16:290.21
Dibromomethane ug/L ND 10.0 01/11/16 16:290.21
Ethylbenzene ug/L ND 1.0 01/11/16 16:290.30
Iodomethane ug/L ND 10.0 01/11/16 16:290.32
Methylene Chloride ug/L ND 1.0 01/11/16 16:290.97
Styrene ug/L ND 1.0 01/11/16 16:290.26
Tetrachloroethene ug/L ND 1.0 01/11/16 16:290.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644536
Associated Lab Samples:92282266010, 92282266011, 92282266012, 92282266013, 92282266014, 92282266015, 92282266016,
92282266017, 92282266018, 92282266019, 92282266020, 92282266021, 92282266022, 92282266023,
92282266024, 92282266025, 92282266026, 92282266027, 92282266028, 92282266029
Matrix:Water
AnalyzedMDL
Toluene ug/L ND 1.0 01/11/16 16:290.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/11/16 16:290.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/11/16 16:290.26
trans-1,4-Dichloro-2-butene ug/L ND 100 01/11/16 16:291.0
Trichloroethene ug/L ND 1.0 01/11/16 16:290.47
Trichlorofluoromethane ug/L ND 1.0 01/11/16 16:290.20
Vinyl acetate ug/L ND 50.0 01/11/16 16:290.35
Vinyl chloride ug/L ND 1.0 01/11/16 16:290.62
Xylene (Total)ug/L ND 5.0 01/11/16 16:290.66
1,2-Dichloroethane-d4 (S)%98 70-130 01/11/16 16:29
4-Bromofluorobenzene (S)%99 70-130 01/11/16 16:29
Toluene-d8 (S)%101 70-130 01/11/16 16:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644537LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.350 89 80-125
1,1,1-Trichloroethane ug/L 46.550 93 71-129
1,1,2,2-Tetrachloroethane ug/L 44.350 89 79-124
1,1,2-Trichloroethane ug/L 41.8 L0508485-125
1,1-Dichloroethane ug/L 45.350 91 73-126
1,1-Dichloroethene ug/L 46.650 93 66-135
1,2,3-Trichloropropane ug/L 45.150 90 75-130
1,2-Dibromo-3-chloropropane ug/L 49.550 99 71-133
1,2-Dibromoethane (EDB)ug/L 48.050 96 83-124
1,2-Dichlorobenzene ug/L 44.350 89 80-133
1,2-Dichloroethane ug/L 43.150 86 67-128
1,2-Dichloropropane ug/L 43.750 87 75-132
1,4-Dichlorobenzene ug/L 44.750 89 78-130
2-Butanone (MEK)ug/L 94.1J100 94 61-144
2-Hexanone ug/L 94.8100 95 68-143
4-Methyl-2-pentanone (MIBK)ug/L 97.8J100 98 72-135
Acetone ug/L 116100 116 48-146
Acrylonitrile ug/L 240250 96 40-160
Benzene ug/L 44.650 89 80-125
Bromochloromethane ug/L 45.750 91 71-125
Bromodichloromethane ug/L 44.050 88 78-124
Bromoform ug/L 44.150 88 71-128
Bromomethane ug/L 52.750 105 40-160
Carbon disulfide ug/L 49.1J50 98 50-160
Carbon tetrachloride ug/L 45.450 91 69-131
Chlorobenzene ug/L 42.750 85 81-122
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644537LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroethane ug/L 44.950 90 39-148
Chloroform ug/L 42.450 85 73-127
Chloromethane ug/L 52.750 105 44-146
cis-1,2-Dichloroethene ug/L 44.650 89 74-124
cis-1,3-Dichloropropene ug/L 45.950 92 72-132
Dibromochloromethane ug/L 43.850 88 78-125
Dibromomethane ug/L 44.550 89 82-120
Ethylbenzene ug/L 43.150 86 79-121
Iodomethane ug/L 86.2100 86 39-154
Methylene Chloride ug/L 47.950 96 64-133
Styrene ug/L 43.250 86 84-126
Tetrachloroethene ug/L 44.450 89 78-122
Toluene ug/L 43.750 87 80-121
trans-1,2-Dichloroethene ug/L 45.450 91 71-127
trans-1,3-Dichloropropene ug/L 46.450 93 69-141
trans-1,4-Dichloro-2-butene ug/L 46.0J50 92 40-160
Trichloroethene ug/L 43.350 87 78-122
Trichlorofluoromethane ug/L 45.450 91 53-137
Vinyl acetate ug/L 99.5100 99 40-160
Vinyl chloride ug/L 51.650 103 58-137
Xylene (Total)ug/L 128150 86 81-126
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1644538MATRIX SPIKE SAMPLE:
MSSpike
Result
92282266025
1,1,1,2-Tetrachloroethane ug/L 20.220 101 70-130ND
1,1,1-Trichloroethane ug/L 21.220 106 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.720 93 70-130ND
1,1,2-Trichloroethane ug/L 18.620 93 70-130ND
1,1-Dichloroethane ug/L 19.920 99 70-130ND
1,1-Dichloroethene ug/L 21.620 108 70-166ND
1,2,3-Trichloropropane ug/L 20.120 100 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.620 103 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.520 103 70-130ND
1,2-Dichlorobenzene ug/L 19.120 96 70-130ND
1,2-Dichloroethane ug/L 18.720 94 70-130ND
1,2-Dichloropropane ug/L 20.120 101 70-130ND
1,4-Dichlorobenzene ug/L 19.220 96 70-130ND
2-Butanone (MEK)ug/L 42.7J40 107 70-130ND
2-Hexanone ug/L 39.8J40 100 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 40.6J40 102 70-130ND
Acetone ug/L 45.8J40 115 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1644538MATRIX SPIKE SAMPLE:
MSSpike
Result
92282266025
Acrylonitrile ug/L 101J100 101 70-130ND
Benzene ug/L 20.720 103 70-148ND
Bromochloromethane ug/L 20.520 102 70-130ND
Bromodichloromethane ug/L 19.620 98 70-130ND
Bromoform ug/L 18.020 90 70-130ND
Bromomethane ug/L 19.220 96 70-130ND
Carbon disulfide ug/L 21.7J20 109 70-130ND
Carbon tetrachloride ug/L 20.620 103 70-130ND
Chlorobenzene ug/L 19.720 98 70-146ND
Chloroethane ug/L 20.320 102 70-130ND
Chloroform ug/L 19.220 96 70-130ND
Chloromethane ug/L 24.520 123 70-130ND
cis-1,2-Dichloroethene ug/L 20.320 102 70-130ND
cis-1,3-Dichloropropene ug/L 20.020 100 70-130ND
Dibromochloromethane ug/L 19.220 96 70-130ND
Dibromomethane ug/L 19.720 99 70-130ND
Ethylbenzene ug/L 20.020 100 70-130ND
Iodomethane ug/L 30.740 77 70-130ND
Methylene Chloride ug/L 20.120 100 70-130ND
Styrene ug/L 19.120 96 70-130ND
Tetrachloroethene ug/L 20.320 101 70-130ND
Toluene ug/L 19.820 99 70-155ND
trans-1,2-Dichloroethene ug/L 19.520 98 70-130ND
trans-1,3-Dichloropropene ug/L 19.320 97 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.4J20 97 70-130ND
Trichloroethene ug/L 20.620 103 69-151ND
Trichlorofluoromethane ug/L 21.020 105 70-130ND
Vinyl acetate ug/L 34.5J40 86 70-130ND
Vinyl chloride ug/L 22.720 114 70-130ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282266026
1644539SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 1.1J 9 301.2J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282266026
1644539SAMPLE DUPLICATE:
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 0.63J 300.64J
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 2.3 11 302.6
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 0.45J 300.48J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 7.4 5 307.7
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%99 297
4-Bromofluorobenzene (S)%100 1100
Toluene-d8 (S)%101 1100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35121
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92282266030
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644541
Associated Lab Samples:92282266030
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/12/16 02:420.33
1,1,1-Trichloroethane ug/L ND 1.0 01/12/16 02:420.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/12/16 02:420.40
1,1,2-Trichloroethane ug/L ND 1.0 01/12/16 02:420.29
1,1-Dichloroethane ug/L ND 5.0 01/12/16 02:420.32
1,1-Dichloroethene ug/L ND 5.0 01/12/16 02:420.56
1,2,3-Trichloropropane ug/L ND 1.0 01/12/16 02:420.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/12/16 02:422.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/12/16 02:420.27
1,2-Dichlorobenzene ug/L ND 5.0 01/12/16 02:420.30
1,2-Dichloroethane ug/L ND 1.0 01/12/16 02:420.24
1,2-Dichloropropane ug/L ND 1.0 01/12/16 02:420.27
1,4-Dichlorobenzene ug/L ND 1.0 01/12/16 02:420.33
2-Butanone (MEK)ug/L ND 100 01/12/16 02:420.96
2-Hexanone ug/L ND 50.0 01/12/16 02:420.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/12/16 02:420.33
Acetone ug/L ND 100 01/12/16 02:4210.0
Acrylonitrile ug/L ND 200 01/12/16 02:421.9
Benzene ug/L ND 1.0 01/12/16 02:420.25
Bromochloromethane ug/L ND 3.0 01/12/16 02:420.17
Bromodichloromethane ug/L ND 1.0 01/12/16 02:420.18
Bromoform ug/L ND 3.0 01/12/16 02:420.26
Bromomethane ug/L ND 10.0 01/12/16 02:420.29
Carbon disulfide ug/L ND 100 01/12/16 02:421.2
Carbon tetrachloride ug/L ND 1.0 01/12/16 02:420.25
Chlorobenzene ug/L ND 3.0 01/12/16 02:420.23
Chloroethane ug/L ND 10.0 01/12/16 02:420.54
Chloroform ug/L ND 5.0 01/12/16 02:420.14
Chloromethane ug/L ND 1.0 01/12/16 02:420.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/12/16 02:420.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/12/16 02:420.13
Dibromochloromethane ug/L ND 3.0 01/12/16 02:420.21
Dibromomethane ug/L ND 10.0 01/12/16 02:420.21
Ethylbenzene ug/L ND 1.0 01/12/16 02:420.30
Iodomethane ug/L ND 10.0 01/12/16 02:420.32
Methylene Chloride ug/L ND 1.0 01/12/16 02:420.97
Styrene ug/L ND 1.0 01/12/16 02:420.26
Tetrachloroethene ug/L ND 1.0 01/12/16 02:420.46
Toluene ug/L ND 1.0 01/12/16 02:420.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/12/16 02:420.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/12/16 02:420.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644541
Associated Lab Samples:92282266030
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 01/12/16 02:421.0
Trichloroethene ug/L ND 1.0 01/12/16 02:420.47
Trichlorofluoromethane ug/L ND 1.0 01/12/16 02:420.20
Vinyl acetate ug/L ND 50.0 01/12/16 02:420.35
Vinyl chloride ug/L ND 1.0 01/12/16 02:420.62
Xylene (Total)ug/L ND 5.0 01/12/16 02:420.66
1,2-Dichloroethane-d4 (S)%97 70-130 01/12/16 02:42
4-Bromofluorobenzene (S)%102 70-130 01/12/16 02:42
Toluene-d8 (S)%99 70-130 01/12/16 02:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644542LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.750 97 80-125
1,1,1-Trichloroethane ug/L 50.250 100 71-129
1,1,2,2-Tetrachloroethane ug/L 47.150 94 79-124
1,1,2-Trichloroethane ug/L 47.450 95 85-125
1,1-Dichloroethane ug/L 48.850 98 73-126
1,1-Dichloroethene ug/L 52.850 106 66-135
1,2,3-Trichloropropane ug/L 47.750 95 75-130
1,2-Dibromo-3-chloropropane ug/L 49.350 99 71-133
1,2-Dibromoethane (EDB)ug/L 50.850 102 83-124
1,2-Dichlorobenzene ug/L 48.350 97 80-133
1,2-Dichloroethane ug/L 44.050 88 67-128
1,2-Dichloropropane ug/L 49.450 99 75-132
1,4-Dichlorobenzene ug/L 48.150 96 78-130
2-Butanone (MEK)ug/L 103100 103 61-144
2-Hexanone ug/L 93.9100 94 68-143
4-Methyl-2-pentanone (MIBK)ug/L 95.4J100 95 72-135
Acetone ug/L 111100 111 48-146
Acrylonitrile ug/L 245250 98 40-160
Benzene ug/L 50.350 101 80-125
Bromochloromethane ug/L 56.650 113 71-125
Bromodichloromethane ug/L 49.250 98 78-124
Bromoform ug/L 43.350 87 71-128
Bromomethane ug/L 54.050 108 40-160
Carbon disulfide ug/L 58.1J50 116 50-160
Carbon tetrachloride ug/L 50.250 100 69-131
Chlorobenzene ug/L 48.050 96 81-122
Chloroethane ug/L 52.650 105 39-148
Chloroform ug/L 49.250 98 73-127
Chloromethane ug/L 56.250 112 44-146
cis-1,2-Dichloroethene ug/L 49.550 99 74-124
cis-1,3-Dichloropropene ug/L 50.250 100 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644542LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 47.250 94 78-125
Dibromomethane ug/L 49.850 100 82-120
Ethylbenzene ug/L 48.450 97 79-121
Iodomethane ug/L 99.1100 99 39-154
Methylene Chloride ug/L 52.050 104 64-133
Styrene ug/L 49.450 99 84-126
Tetrachloroethene ug/L 49.050 98 78-122
Toluene ug/L 49.650 99 80-121
trans-1,2-Dichloroethene ug/L 49.350 99 71-127
trans-1,3-Dichloropropene ug/L 50.050 100 69-141
trans-1,4-Dichloro-2-butene ug/L 46.3J50 93 40-160
Trichloroethene ug/L 48.150 96 78-122
Trichlorofluoromethane ug/L 50.250 100 53-137
Vinyl acetate ug/L 100100 100 40-160
Vinyl chloride ug/L 58.950 118 58-137
Xylene (Total)ug/L 145150 97 81-126
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1644543MATRIX SPIKE SAMPLE:
MSSpike
Result
92282365007
1,1,1,2-Tetrachloroethane ug/L 18.720 93 70-130ND
1,1,1-Trichloroethane ug/L 20.820 104 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.020 90 70-130ND
1,1,2-Trichloroethane ug/L 17.920 90 70-130ND
1,1-Dichloroethane ug/L 21.520 98 70-1301.9J
1,1-Dichloroethene ug/L 21.720 109 70-166ND
1,2,3-Trichloropropane ug/L 19.420 97 70-130ND
1,2-Dibromo-3-chloropropane ug/L 17.620 88 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.520 97 70-130ND
1,2-Dichlorobenzene ug/L 18.920 94 70-130ND
1,2-Dichloroethane ug/L 18.020 88 70-1300.43J
1,2-Dichloropropane ug/L 19.120 96 70-130ND
1,4-Dichlorobenzene ug/L 19.220 94 70-1300.44J
2-Butanone (MEK)ug/L 39.0J40 97 70-130ND
2-Hexanone ug/L 36.9J40 92 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 37.5J40 94 70-130ND
Acetone ug/L 40.3J40 101 70-130ND
Acrylonitrile ug/L 97.3J100 97 70-130ND
Benzene ug/L 19.320 97 70-148ND
Bromochloromethane ug/L 20.520 103 70-130ND
Bromodichloromethane ug/L 19.020 95 70-130ND
Bromoform ug/L 15.820 79 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1644543MATRIX SPIKE SAMPLE:
MSSpike
Result
92282365007
Bromomethane ug/L 17.620 88 70-130ND
Carbon disulfide ug/L 20.4J20 102 70-130ND
Carbon tetrachloride ug/L 21.720 109 70-130ND
Chlorobenzene ug/L 18.720 94 70-146ND
Chloroethane ug/L 19.720 98 70-130ND
Chloroform ug/L 19.320 97 70-130ND
Chloromethane ug/L 22.320 111 70-130ND
cis-1,2-Dichloroethene ug/L 22.320 97 70-1303.0J
cis-1,3-Dichloropropene ug/L 18.520 92 70-130ND
Dibromochloromethane ug/L 16.820 84 70-130ND
Dibromomethane ug/L 18.420 92 70-130ND
Ethylbenzene ug/L 19.220 96 70-130ND
Iodomethane ug/L 24.0 M1406070-130ND
Methylene Chloride ug/L 19.720 98 70-130ND
Styrene ug/L 18.720 93 70-130ND
Tetrachloroethene ug/L 22.220 98 70-1302.7
Toluene ug/L 19.020 95 70-155ND
trans-1,2-Dichloroethene ug/L 19.920 99 70-130ND
trans-1,3-Dichloropropene ug/L 17.820 89 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.4J20 87 70-130ND
Trichloroethene ug/L 22.220 93 69-1513.6
Trichlorofluoromethane ug/L 21.320 107 70-130ND
Vinyl acetate ug/L 25.7J M1406470-130ND
Vinyl chloride ug/L 22.620 113 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282365008
1644544SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 3.6J 1 303.7J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282365008
1644544SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 8.6 1 308.5
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L 2.7 1 302.7
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 2.0 4 301.9
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%101 0101
4-Bromofluorobenzene (S)%104 1105
Toluene-d8 (S)%100 1100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/42528
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92282266021, 92282266022, 92282266023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1648483
Associated Lab Samples:92282266021, 92282266022, 92282266023
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 01/19/16 14:501000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1648484LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4830050000 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1648485MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92283086031
1648486
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 87 80-12088 1 2550000ND4870049100
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1648487MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282266022
1648488
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 99 80-12090 1 2550000345000394000390000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/42369
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92282266021, 92282266023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1643330
Associated Lab Samples:92282266021, 92282266023
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 01/08/16 15:00100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1643331LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 496J500 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643332MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282265002
1643333
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L H3,M150011690-110116 0 10500ND582J582J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643334MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282184017
1643335
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 91 90-11091 0 10500ND456J456J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/42392
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92282266022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644382
Associated Lab Samples:92282266022
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 01/10/16 11:30100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644383LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 501J500 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644384MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282355022
1644385
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M15005890-11058 0 10500ND291J291J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/26031
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92282266021, 92282266022, 92282266023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644924
Associated Lab Samples:92282266021, 92282266022, 92282266023
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 01/13/16 14:251000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644925LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 18900J20000 94 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644926MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282346001
1644927
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M620000-50 90-11021 1 10200001250 mg/L 1240000
J
1250000
J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644928MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281822001
1644929
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 98 90-11096 1 102000021.9 mg/L 41400J 41000J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/26019
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92282266021, 92282266022, 92282266023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1643436
Associated Lab Samples:92282266021, 92282266022, 92282266023
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 01/08/16 10:3410.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1643437LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24902500 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643438MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282265003
1643439
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L M125008990-11088 0 102500ND22102210
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/26042
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92282266021, 92282266022, 92282266023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1645084
Associated Lab Samples:92282266021, 92282266022, 92282266023
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 01/12/16 20:36500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1645085LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2020020000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645086MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281796001
1645087
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M65000000-4 90-110-4 1 1050000001600 mg/L 1430000 1410000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645088MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282075002
1645089
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 40000 99 90-11099 0 104000012.5 mg/L 51900 52000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/26044
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92282266021, 92282266022, 92282266023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1645129
Associated Lab Samples:92282266021, 92282266022, 92282266023
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 01/12/16 15:3012500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1645130LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 762000750000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645131MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281851003
1645132
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 3000000 95 90-11095 0 33000000696 mg/L 3540000 3540000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645133MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281854005
1645134
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 96 90-11096 0 375000034.0 mg/L 755000 755000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 110
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/26026
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92282266021, 92282266022, 92282266023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644476
Associated Lab Samples:92282266021, 92282266022, 92282266023
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 01/11/16 14:56500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644477LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2390025000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644478MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281496001
1644479
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 95 90-11096 0 525000ND2420024300
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644509MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282266022
1644510
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 98 90-11098 0 52500028002720027200
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 110
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92282266
Alexander LF-SWS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
Sample was received or analysis requested beyond the recognized method holding time.H3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 110
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92282266001 MPRP/20439 ICP/18443MW-1 EPA 3010A EPA 6010
92282266002 MPRP/20439 ICP/18443MW-1B EPA 3010A EPA 6010
92282266003 MPRP/20439 ICP/18443MW-4R EPA 3010A EPA 6010
92282266004 MPRP/20440 ICP/18442MW-5 EPA 3010A EPA 6010
92282266005 MPRP/20440 ICP/18442MW-9 EPA 3010A EPA 6010
92282266006 MPRP/20440 ICP/18442MW-10 EPA 3010A EPA 6010
92282266007 MPRP/20440 ICP/18442MW-13 EPA 3010A EPA 6010
92282266008 MPRP/20440 ICP/18442MW-16 EPA 3010A EPA 6010
92282266009 MPRP/20440 ICP/18442MW-22 EPA 3010A EPA 6010
92282266010 MPRP/20440 ICP/18442MW-23 EPA 3010A EPA 6010
92282266011 MPRP/20440 ICP/18442MW-32 EPA 3010A EPA 6010
92282266012 MPRP/20440 ICP/18442MW-33 EPA 3010A EPA 6010
92282266013 MPRP/20440 ICP/18442MW-34 EPA 3010A EPA 6010
92282266014 MPRP/20440 ICP/18442SW-3 EPA 3010A EPA 6010
92282266015 MPRP/20440 ICP/18442SW-4R EPA 3010A EPA 6010
92282266016 MPRP/20440 ICP/18442SW-5 EPA 3010A EPA 6010
92282266017 MPRP/20440 ICP/18442SW-6 EPA 3010A EPA 6010
92282266018 MPRP/20440 ICP/18442MW-6 EPA 3010A EPA 6010
92282266019 MPRP/20440 ICP/18442MW-17 EPA 3010A EPA 6010
92282266020 MPRP/20440 ICP/18442MW-21 EPA 3010A EPA 6010
92282266021 MPRP/20440 ICP/18442MW-12 EPA 3010A EPA 6010
92282266022 MPRP/20440 ICP/18442MW-12D EPA 3010A EPA 6010
92282266023 MPRP/20440 ICP/18442MW-24 EPA 3010A EPA 6010
92282266024 MPRP/20449 ICP/18451MW-2 EPA 3010A EPA 6010
92282266025 MPRP/20449 ICP/18451MW-14 EPA 3010A EPA 6010
92282266026 MPRP/20449 ICP/18451MW-15 EPA 3010A EPA 6010
92282266027 MPRP/20449 ICP/18451MW-19 EPA 3010A EPA 6010
92282266028 MPRP/20449 ICP/18451MW-20 EPA 3010A EPA 6010
92282266029 MPRP/20449 ICP/18451MW-25 EPA 3010A EPA 6010
92282266030 MPRP/20449 ICP/18451MW-7 EPA 3010A EPA 6010
92282266021 MPRP/20453 ICP/18456MW-12 EPA 3010 EPA 6010
92282266022 MPRP/20453 ICP/18456MW-12D EPA 3010 EPA 6010
92282266023 MPRP/20453 ICP/18456MW-24 EPA 3010 EPA 6010
92282266001 MERP/8850 MERC/8499MW-1 EPA 7470 EPA 7470
92282266002 MERP/8850 MERC/8499MW-1B EPA 7470 EPA 7470
92282266018 MERP/8850 MERC/8499MW-6 EPA 7470 EPA 7470
92282266019 MERP/8850 MERC/8499MW-17 EPA 7470 EPA 7470
92282266020 MERP/8850 MERC/8499MW-21 EPA 7470 EPA 7470
92282266001 MSV/35119MW-1 EPA 8260
92282266002 MSV/35119MW-1B EPA 8260
92282266003 MSV/35119MW-4R EPA 8260
92282266004 MSV/35119MW-5 EPA 8260
92282266005 MSV/35119MW-9 EPA 8260
92282266006 MSV/35119MW-10 EPA 8260
92282266007 MSV/35119MW-13 EPA 8260
92282266008 MSV/35119MW-16 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 110
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92282266
Alexander LF-SWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92282266009 MSV/35119MW-22 EPA 8260
92282266010 MSV/35120MW-23 EPA 8260
92282266011 MSV/35120MW-32 EPA 8260
92282266012 MSV/35120MW-33 EPA 8260
92282266013 MSV/35120MW-34 EPA 8260
92282266014 MSV/35120SW-3 EPA 8260
92282266015 MSV/35120SW-4R EPA 8260
92282266016 MSV/35120SW-5 EPA 8260
92282266017 MSV/35120SW-6 EPA 8260
92282266018 MSV/35120MW-6 EPA 8260
92282266019 MSV/35120MW-17 EPA 8260
92282266020 MSV/35120MW-21 EPA 8260
92282266021 MSV/35120MW-12 EPA 8260
92282266022 MSV/35120MW-12D EPA 8260
92282266023 MSV/35120MW-24 EPA 8260
92282266024 MSV/35120MW-2 EPA 8260
92282266025 MSV/35120MW-14 EPA 8260
92282266026 MSV/35120MW-15 EPA 8260
92282266027 MSV/35120MW-19 EPA 8260
92282266028 MSV/35120MW-20 EPA 8260
92282266029 MSV/35120MW-25 EPA 8260
92282266030 MSV/35121MW-7 EPA 8260
92282266021 WET/42528MW-12 SM 2320B
92282266022 WET/42528MW-12D SM 2320B
92282266023 WET/42528MW-24 SM 2320B
92282266021 WET/42369MW-12 SM 4500-S2D
92282266022 WET/42392MW-12D SM 4500-S2D
92282266023 WET/42369MW-24 SM 4500-S2D
92282266021 WETA/26031MW-12 EPA 300.0
92282266022 WETA/26031MW-12D EPA 300.0
92282266023 WETA/26031MW-24 EPA 300.0
92282266021 WETA/26019MW-12 EPA 353.2
92282266022 WETA/26019MW-12D EPA 353.2
92282266023 WETA/26019MW-24 EPA 353.2
92282266021 WETA/26042MW-12 SM 4500-Cl-E
92282266022 WETA/26042MW-12D SM 4500-Cl-E
92282266023 WETA/26042MW-24 SM 4500-Cl-E
92282266021 WETA/26044MW-12 SM 5220D
92282266022 WETA/26044MW-12D SM 5220D
92282266023 WETA/26044MW-24 SM 5220D
92282266021 WETA/26026MW-12 SM 5310B
92282266022 WETA/26026MW-12D SM 5310B
92282266023 WETA/26026MW-24 SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/21/2016 03:15 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 110
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#=CL#
January 18, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92282265
92282265
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
ALEXANDER LF (SWS & UIC)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on January 07, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Dale Ingram
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 40
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 40
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Lab ID Sample ID Matrix Date Collected Date Received
92282265001 MW-3 Water 01/06/16 14:15 01/07/16 10:25
92282265002 MW-11 Water 01/06/16 16:05 01/07/16 10:25
92282265003 MW-26 Water 01/06/16 11:30 01/07/16 10:25
92282265004 MW-31 Water 01/06/16 12:10 01/07/16 10:25
92282265005 MW-18 Water 01/06/16 18:30 01/07/16 10:25
92282265006 MW-27 Water 01/06/16 13:15 01/07/16 10:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 40
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92282265001 MW-3 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 2320B 1 PASI-AMLS
EPA 300.0 1 PASI-AMDW
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92282265002 MW-11 EPA 6010 15 PASI-ACDF
EPA 6010 1 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-AEWS
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92282265003 MW-26 EPA 6010 15 PASI-ACDF
EPA 6010 1 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-AEWS
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
92282265004 MW-31 EPA 6010 15 PASI-ACDF
EPA 6010 1 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 2320B 1 PASI-AMLS
SM 4500-S2D 1 PASI-AMJP
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-AEWS
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AWRC
SM 5310B 1 PASI-AMDW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 40
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92282265005 MW-18 EPA 6010 15 PASI-ACDF
EPA 6010 1 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 50 PASI-CNB
92282265006 MW-27 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-3 Lab ID:92282265001 Collected:01/06/16 14:15 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/11/16 17:45 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/11/16 17:45 7440-38-201/08/16 18:0010.0 2.5 1
Barium 42.3J ug/L 01/11/16 17:45 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/11/16 17:45 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/11/16 17:45 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/11/16 17:45 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 19.3 ug/L 01/11/16 17:45 7440-48-4 B01/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/11/16 17:45 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/11/16 17:45 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 8.3J ug/L 01/11/16 17:45 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/11/16 17:45 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/11/16 17:45 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 13:53 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/11/16 17:45 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 9.9J ug/L 01/11/16 17:45 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 16:42 67-64-1 M110010.0 1
Acrylonitrile ND ug/L 01/11/16 16:42 107-13-12001.9 1
Benzene 5.9 ug/L 01/11/16 16:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 16:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 16:42 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 16:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 16:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 16:42 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 16:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 16:42 56-23-51.0 0.25 1
Chlorobenzene 1.4J ug/L 01/11/16 16:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 16:42 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 16:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 16:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 16:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 16:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 16:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 16:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.74J ug/L 01/11/16 16:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene 10.6 ug/L 01/11/16 16:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 16:42 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 16:42 75-34-35.0 0.32 1
1,2-Dichloroethane 0.30J ug/L 01/11/16 16:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 16:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 6.6 ug/L 01/11/16 16:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 16:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 16:42 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 16:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 16:42 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Huntersville, NC 28078
[phone]
Page 6 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-3 Lab ID:92282265001 Collected:01/06/16 14:15 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene 1.2 ug/L 01/11/16 16:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 16:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 16:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 16:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 16:42 108-10-11000.33 1
Styrene ND ug/L 01/11/16 16:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 16:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 16:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 16:42 127-18-41.0 0.46 1
Toluene 0.43J ug/L 01/11/16 16:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 16:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 16:42 79-00-51.0 0.29 1
Trichloroethene 0.72J ug/L 01/11/16 16:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 16:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 16:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 16:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 16:42 75-01-41.0 0.62 1
Xylene (Total)2.6J ug/L 01/11/16 16:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)110 %01/11/16 16:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %01/11/16 16:42 17060-07-070-130 1
Toluene-d8 (S)100 %01/11/16 16:42 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 96900 ug/L 01/14/16 00:08500010001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate ND ug/L 01/13/16 19:10 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 21800 ug/L 01/12/16 21:01 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 30000 ug/L 01/12/16 15:3025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 4980 ug/L 01/11/16 17:25 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Page 7 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-11 Lab ID:92282265002 Collected:01/06/16 16:05 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/11/16 17:48 7440-36-001/08/16 18:006.0 3.8 1
Arsenic 2.6J ug/L 01/11/16 17:48 7440-38-201/08/16 18:0010.0 2.5 1
Barium 138 ug/L 01/11/16 17:48 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/11/16 17:48 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/11/16 17:48 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/11/16 17:48 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 143 ug/L 01/11/16 17:48 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/11/16 17:48 7440-50-801/08/16 18:0010.0 2.5 1
Lead 4.3J ug/L 01/11/16 17:48 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 11.1J ug/L 01/11/16 17:48 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/11/16 17:48 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/11/16 17:48 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 13:56 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/11/16 17:48 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 7.0J ug/L 01/11/16 17:48 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 48900 ug/L 01/13/16 22:43 7439-89-6 M101/12/16 20:4350.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 16:59 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 16:59 107-13-12001.9 1
Benzene 2.9 ug/L 01/11/16 16:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 16:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 16:59 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 16:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 16:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 16:59 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 16:59 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 16:59 56-23-51.0 0.25 1
Chlorobenzene 1.9J ug/L 01/11/16 16:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 16:59 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 16:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 16:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 16:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 16:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 16:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 16:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.44J ug/L 01/11/16 16:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene 7.5 ug/L 01/11/16 16:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 16:59 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 16:59 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 16:59 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 16:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 14.2 ug/L 01/11/16 16:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 16:59 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Page 8 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-11 Lab ID:92282265002 Collected:01/06/16 16:05 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 16:59 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 16:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 16:59 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 16:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 16:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 16:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 16:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 16:59 108-10-11000.33 1
Styrene ND ug/L 01/11/16 16:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 16:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 16:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 16:59 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 16:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 16:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 16:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 16:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 16:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 16:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 16:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 16:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 16:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)110 %01/11/16 16:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %01/11/16 16:59 17060-07-070-130 1
Toluene-d8 (S)100 %01/11/16 16:59 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 202000 ug/L 01/14/16 00:21500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/08/16 15:00 18496-25-8 M110001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2870J ug/L 01/13/16 19:51 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 01/08/16 10:501000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 36900 ug/L 01/12/16 21:02 16887-00-6200010002
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 41000 ug/L 01/12/16 15:3025000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-11 Lab ID:92282265002 Collected:01/06/16 16:05 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 3120 ug/L 01/11/16 17:35 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-26 Lab ID:92282265003 Collected:01/06/16 11:30 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/11/16 17:52 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/11/16 17:52 7440-38-201/08/16 18:0010.0 2.5 1
Barium 82.0J ug/L 01/11/16 17:52 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/11/16 17:52 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/11/16 17:52 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/11/16 17:52 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 104 ug/L 01/11/16 17:52 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/11/16 17:52 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/11/16 17:52 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 10J ug/L 01/11/16 17:52 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/11/16 17:52 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/11/16 17:52 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 13:59 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/11/16 17:52 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 23.5 ug/L 01/11/16 17:52 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 17600 ug/L 01/13/16 22:52 7439-89-601/12/16 20:4350.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 17:33 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 17:33 107-13-12001.9 1
Benzene ND ug/L 01/11/16 17:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 17:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 17:33 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 17:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 17:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 17:33 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 17:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 17:33 56-23-51.0 0.25 1
Chlorobenzene 0.25J ug/L 01/11/16 17:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 17:33 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 17:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 17:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 17:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 17:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 17:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 17:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 17:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.2 ug/L 01/11/16 17:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 17:33 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 17:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 17:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 17:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 4.0J ug/L 01/11/16 17:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 17:33 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-26 Lab ID:92282265003 Collected:01/06/16 11:30 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 17:33 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 17:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 17:33 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 17:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 17:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 17:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 17:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 17:33 108-10-11000.33 1
Styrene ND ug/L 01/11/16 17:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 17:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 17:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 17:33 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 17:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 17:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 17:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 17:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 17:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 17:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 17:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 17:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 17:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)108 %01/11/16 17:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %01/11/16 17:33 17060-07-070-130 1
Toluene-d8 (S)98 %01/11/16 17:33 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 113000 ug/L 01/14/16 00:35500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/08/16 15:00 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 4240J ug/L 01/13/16 20:05 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 01/08/16 10:37 M11000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 15400 ug/L 01/12/16 21:03 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 23000J ug/L 01/12/16 15:3025000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-26 Lab ID:92282265003 Collected:01/06/16 11:30 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1470 ug/L 01/11/16 17:48 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-31 Lab ID:92282265004 Collected:01/06/16 12:10 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/11/16 17:55 7440-36-001/08/16 18:006.0 3.8 1
Arsenic ND ug/L 01/11/16 17:55 7440-38-201/08/16 18:0010.0 2.5 1
Barium 50.8J ug/L 01/11/16 17:55 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/11/16 17:55 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/11/16 17:55 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/11/16 17:55 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 6.0J ug/L 01/11/16 17:55 7440-48-4 B01/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/11/16 17:55 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/11/16 17:55 7439-92-101/08/16 18:0010.0 2.5 1
Nickel ND ug/L 01/11/16 17:55 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/11/16 17:55 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/11/16 17:55 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 14:03 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/11/16 17:55 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 5.7J ug/L 01/11/16 17:55 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved ND ug/L 01/13/16 22:55 7439-89-601/12/16 20:4350.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 17:50 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 17:50 107-13-12001.9 1
Benzene ND ug/L 01/11/16 17:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 17:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 17:50 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 17:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 17:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 17:50 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 17:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 17:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 17:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 17:50 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 17:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 17:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 17:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 17:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 17:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 17:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 17:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 17:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 17:50 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 17:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 17:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 17:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.1J ug/L 01/11/16 17:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 17:50 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-31 Lab ID:92282265004 Collected:01/06/16 12:10 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/11/16 17:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 17:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 17:50 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 17:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 17:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 17:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 17:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 17:50 108-10-11000.33 1
Styrene ND ug/L 01/11/16 17:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 17:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 17:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 17:50 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 17:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 17:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 17:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 17:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 17:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 17:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 17:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 17:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 17:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)107 %01/11/16 17:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %01/11/16 17:50 17060-07-070-130 1
Toluene-d8 (S)99 %01/11/16 17:50 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 18000 ug/L 01/14/16 00:48500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/08/16 15:00 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1980J ug/L 01/13/16 20:18 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 1060J ug/L 01/08/16 10:421000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 8980 ug/L 01/12/16 21:03 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 01/12/16 15:3025000125001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Page 15 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-31 Lab ID:92282265004 Collected:01/06/16 12:10 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1780 ug/L 01/11/16 18:03 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Page 16 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-18 Lab ID:92282265005 Collected:01/06/16 18:30 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/11/16 17:58 7440-36-001/08/16 18:006.0 3.8 1
Arsenic 2.8J ug/L 01/11/16 17:58 7440-38-201/08/16 18:0010.0 2.5 1
Barium 23.3J ug/L 01/11/16 17:58 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/11/16 17:58 7440-41-701/08/16 18:001.0 0.50 1
Cadmium ND ug/L 01/11/16 17:58 7440-43-901/08/16 18:001.0 0.50 1
Chromium 2.6J ug/L 01/11/16 17:58 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt 26.1 ug/L 01/11/16 17:58 7440-48-4 B01/08/16 18:0010.0 2.5 1
Copper 29.1 ug/L 01/11/16 17:58 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/11/16 17:58 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 25.6J ug/L 01/11/16 17:58 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/11/16 17:58 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/11/16 17:58 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 14:06 7440-28-001/08/16 18:005.5 5.0 1
Vanadium 3.1J ug/L 01/11/16 17:58 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 24.0 ug/L 01/11/16 17:58 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved ND ug/L 01/13/16 22:58 7439-89-601/12/16 20:4350.0 25.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.37 ug/L 01/14/16 12:37 7439-97-601/08/16 21:300.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 18:07 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 18:07 107-13-12001.9 1
Benzene ND ug/L 01/11/16 18:07 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 18:07 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 18:07 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 18:07 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 18:07 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 18:07 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 18:07 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 18:07 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 18:07 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 18:07 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 18:07 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 18:07 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 18:07 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 18:07 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 18:07 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 18:07 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 18:07 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 18:07 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 18:07 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 18:07 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 18:07 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Page 17 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-18 Lab ID:92282265005 Collected:01/06/16 18:30 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 01/11/16 18:07 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/11/16 18:07 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 18:07 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 18:07 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 18:07 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 18:07 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/11/16 18:07 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 18:07 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 18:07 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 18:07 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 18:07 108-10-11000.33 1
Styrene ND ug/L 01/11/16 18:07 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 18:07 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 18:07 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 18:07 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 18:07 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 18:07 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 18:07 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 18:07 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 18:07 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 18:07 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 18:07 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 18:07 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 18:07 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)109 %01/11/16 18:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/11/16 18:07 17060-07-070-130 1
Toluene-d8 (S)99 %01/11/16 18:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Page 18 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-27 Lab ID:92282265006 Collected:01/06/16 13:15 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/11/16 18:01 7440-36-001/08/16 18:006.0 3.8 1
Arsenic 2.6J ug/L 01/11/16 18:01 7440-38-201/08/16 18:0010.0 2.5 1
Barium 25.6J ug/L 01/11/16 18:01 7440-39-301/08/16 18:001002.5 1
Beryllium ND ug/L 01/11/16 18:01 7440-41-701/08/16 18:001.0 0.50 1
Cadmium 1.7 ug/L 01/11/16 18:01 7440-43-901/08/16 18:001.0 0.50 1
Chromium ND ug/L 01/11/16 18:01 7440-47-301/08/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/11/16 18:01 7440-48-401/08/16 18:0010.0 2.5 1
Copper ND ug/L 01/11/16 18:01 7440-50-801/08/16 18:0010.0 2.5 1
Lead ND ug/L 01/11/16 18:01 7439-92-101/08/16 18:0010.0 2.5 1
Nickel 4.8J ug/L 01/11/16 18:01 7440-02-001/08/16 18:0050.0 2.5 1
Selenium ND ug/L 01/11/16 18:01 7782-49-201/08/16 18:0010.0 5.0 1
Silver ND ug/L 01/11/16 18:01 7440-22-401/08/16 18:0010.0 2.5 1
Thallium ND ug/L 01/12/16 14:09 7440-28-001/08/16 18:005.5 5.0 1
Vanadium ND ug/L 01/11/16 18:01 7440-62-201/08/16 18:0025.0 2.5 1
Zinc 15.4 ug/L 01/11/16 18:01 7440-66-601/08/16 18:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/11/16 18:25 67-64-110010.0 1
Acrylonitrile ND ug/L 01/11/16 18:25 107-13-12001.9 1
Benzene ND ug/L 01/11/16 18:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/11/16 18:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/11/16 18:25 75-27-41.0 0.18 1
Bromoform ND ug/L 01/11/16 18:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/11/16 18:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/11/16 18:25 78-93-31000.96 1
Carbon disulfide ND ug/L 01/11/16 18:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/11/16 18:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/11/16 18:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/11/16 18:25 75-00-310.0 0.54 1
Chloroform ND ug/L 01/11/16 18:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/11/16 18:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/11/16 18:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/11/16 18:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/11/16 18:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/11/16 18:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/11/16 18:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/11/16 18:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/11/16 18:25 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/11/16 18:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/11/16 18:25 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/11/16 18:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 5.3 ug/L 01/11/16 18:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/11/16 18:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/11/16 18:25 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/11/16 18:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/11/16 18:25 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Sample:MW-27 Lab ID:92282265006 Collected:01/06/16 13:15 Received:01/07/16 10:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/11/16 18:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/11/16 18:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/11/16 18:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/11/16 18:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/11/16 18:25 108-10-11000.33 1
Styrene ND ug/L 01/11/16 18:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/11/16 18:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/11/16 18:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/11/16 18:25 127-18-41.0 0.46 1
Toluene ND ug/L 01/11/16 18:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/11/16 18:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/11/16 18:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/11/16 18:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/11/16 18:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/11/16 18:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/11/16 18:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/11/16 18:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/11/16 18:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)109 %01/11/16 18:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %01/11/16 18:25 17060-07-070-130 1
Toluene-d8 (S)98 %01/11/16 18:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Page 20 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/8850
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92282265005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1643395
Associated Lab Samples:92282265005
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 01/14/16 11:100.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1643396LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643397MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281698007
1643398
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 92 75-12593 1 252.5ND 2.4 2.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Page 21 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20439
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004, 92282265005, 92282265006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1643941
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004, 92282265005, 92282265006
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/11/16 16:393.8
Arsenic ug/L ND 10.0 01/11/16 16:392.5
Barium ug/L ND 100 01/11/16 16:392.5
Beryllium ug/L ND 1.0 01/11/16 16:390.50
Cadmium ug/L ND 1.0 01/11/16 16:390.50
Chromium ug/L ND 10.0 01/11/16 16:392.5
Cobalt ug/L 5.0J 10.0 01/11/16 16:392.5
Copper ug/L ND 10.0 01/11/16 16:392.5
Lead ug/L ND 10.0 01/11/16 16:392.5
Nickel ug/L ND 50.0 01/11/16 16:392.5
Selenium ug/L ND 10.0 01/11/16 16:395.0
Silver ug/L ND 10.0 01/11/16 16:392.5
Thallium ug/L ND 5.5 01/11/16 16:395.0
Vanadium ug/L ND 25.0 01/11/16 16:392.5
Zinc ug/L ND 10.0 01/11/16 16:395.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1643942LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 466500 93 80-120
Barium ug/L 457500 91 80-120
Beryllium ug/L 452500 90 80-120
Cadmium ug/L 467500 93 80-120
Chromium ug/L 454500 91 80-120
Cobalt ug/L 473500 95 80-120
Copper ug/L 463500 93 80-120
Lead ug/L 467500 93 80-120
Nickel ug/L 468500 94 80-120
Selenium ug/L 467500 93 80-120
Silver ug/L 236250 94 80-120
Thallium ug/L 450500 90 80-120
Vanadium ug/L 458500 92 80-120
Zinc ug/L 467500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Page 22 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643943MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282072001
1643944
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125104 0 25500ND520521
Arsenic ug/L 500 99 75-12599 0 25500ND498497
Barium ug/L 500 97 75-12595 1 25500140623617
Beryllium ug/L 500 96 75-12596 1 25500ND482478
Cadmium ug/L 500 98 75-12598 0 25500ND490491
Chromium ug/L 500 95 75-12595 0 25500ND477477
Cobalt ug/L 500 96 75-12596 0 25500ND480481
Copper ug/L 500 99 75-12598 0 25500ND494492
Lead ug/L 500 93 75-12593 0 25500ND464465
Nickel ug/L 500 95 75-12595 0 25500ND476477
Selenium ug/L 500 98 75-12598 0 25500ND490491
Silver ug/L 250 100 75-125100 0 25250ND250250
Thallium ug/L 500 86 75-12589 3 255006.2 438 450
Vanadium ug/L 500 98 75-12599 0 25500ND492493
Zinc ug/L 500 97 75-12597 0 2550011.3 497 497
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20458
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Associated Lab Samples:92282265002, 92282265003, 92282265004, 92282265005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1645752
Associated Lab Samples:92282265002, 92282265003, 92282265004, 92282265005
Matrix:Water
AnalyzedMDL
Iron, Dissolved ug/L ND 50.0 01/13/16 22:2825.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1645753LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Dissolved ug/L 45305000 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645754MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282265002
1645755
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Iron, Dissolved ug/L M150007975-12558 2 205000489005290051800
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35119
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004, 92282265005, 92282265006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644503
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004, 92282265005, 92282265006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/11/16 10:420.33
1,1,1-Trichloroethane ug/L ND 1.0 01/11/16 10:420.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/11/16 10:420.40
1,1,2-Trichloroethane ug/L ND 1.0 01/11/16 10:420.29
1,1-Dichloroethane ug/L ND 5.0 01/11/16 10:420.32
1,1-Dichloroethene ug/L ND 5.0 01/11/16 10:420.56
1,2,3-Trichloropropane ug/L ND 1.0 01/11/16 10:420.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/11/16 10:422.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/11/16 10:420.27
1,2-Dichlorobenzene ug/L ND 5.0 01/11/16 10:420.30
1,2-Dichloroethane ug/L ND 1.0 01/11/16 10:420.24
1,2-Dichloropropane ug/L ND 1.0 01/11/16 10:420.27
1,4-Dichlorobenzene ug/L ND 1.0 01/11/16 10:420.33
2-Butanone (MEK)ug/L ND 100 01/11/16 10:420.96
2-Hexanone ug/L ND 50.0 01/11/16 10:420.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/11/16 10:420.33
Acetone ug/L ND 100 01/11/16 10:4210.0
Acrylonitrile ug/L ND 200 01/11/16 10:421.9
Benzene ug/L ND 1.0 01/11/16 10:420.25
Bromochloromethane ug/L ND 3.0 01/11/16 10:420.17
Bromodichloromethane ug/L ND 1.0 01/11/16 10:420.18
Bromoform ug/L ND 3.0 01/11/16 10:420.26
Bromomethane ug/L ND 10.0 01/11/16 10:420.29
Carbon disulfide ug/L ND 100 01/11/16 10:421.2
Carbon tetrachloride ug/L ND 1.0 01/11/16 10:420.25
Chlorobenzene ug/L ND 3.0 01/11/16 10:420.23
Chloroethane ug/L ND 10.0 01/11/16 10:420.54
Chloroform ug/L ND 5.0 01/11/16 10:420.14
Chloromethane ug/L ND 1.0 01/11/16 10:420.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/11/16 10:420.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/11/16 10:420.13
Dibromochloromethane ug/L ND 3.0 01/11/16 10:420.21
Dibromomethane ug/L ND 10.0 01/11/16 10:420.21
Ethylbenzene ug/L ND 1.0 01/11/16 10:420.30
Iodomethane ug/L ND 10.0 01/11/16 10:420.32
Methylene Chloride ug/L ND 1.0 01/11/16 10:420.97
Styrene ug/L ND 1.0 01/11/16 10:420.26
Tetrachloroethene ug/L ND 1.0 01/11/16 10:420.46
Toluene ug/L ND 1.0 01/11/16 10:420.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/11/16 10:420.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/11/16 10:420.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644503
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004, 92282265005, 92282265006
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 01/11/16 10:421.0
Trichloroethene ug/L ND 1.0 01/11/16 10:420.47
Trichlorofluoromethane ug/L ND 1.0 01/11/16 10:420.20
Vinyl acetate ug/L ND 50.0 01/11/16 10:420.35
Vinyl chloride ug/L ND 1.0 01/11/16 10:420.62
Xylene (Total)ug/L ND 5.0 01/11/16 10:420.66
1,2-Dichloroethane-d4 (S)%99 70-130 01/11/16 10:42
4-Bromofluorobenzene (S)%108 70-130 01/11/16 10:42
Toluene-d8 (S)%101 70-130 01/11/16 10:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644504LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.350 97 80-125
1,1,1-Trichloroethane ug/L 48.850 98 71-129
1,1,2,2-Tetrachloroethane ug/L 49.650 99 79-124
1,1,2-Trichloroethane ug/L 47.850 96 85-125
1,1-Dichloroethane ug/L 48.250 96 73-126
1,1-Dichloroethene ug/L 48.050 96 66-135
1,2,3-Trichloropropane ug/L 49.250 98 75-130
1,2-Dibromo-3-chloropropane ug/L 48.550 97 71-133
1,2-Dibromoethane (EDB)ug/L 49.150 98 83-124
1,2-Dichlorobenzene ug/L 48.350 97 80-133
1,2-Dichloroethane ug/L 45.250 90 67-128
1,2-Dichloropropane ug/L 46.450 93 75-132
1,4-Dichlorobenzene ug/L 50.150 100 78-130
2-Butanone (MEK)ug/L 97.0J100 97 61-144
2-Hexanone ug/L 98.5100 99 68-143
4-Methyl-2-pentanone (MIBK)ug/L 98.8J100 99 72-135
Acetone ug/L 105100 105 48-146
Acrylonitrile ug/L 248250 99 40-160
Benzene ug/L 48.650 97 80-125
Bromochloromethane ug/L 50.650 101 71-125
Bromodichloromethane ug/L 49.650 99 78-124
Bromoform ug/L 44.050 88 71-128
Bromomethane ug/L 46.050 92 40-160
Carbon disulfide ug/L 53.8J50 108 50-160
Carbon tetrachloride ug/L 50.250 100 69-131
Chlorobenzene ug/L 48.150 96 81-122
Chloroethane ug/L 42.850 86 39-148
Chloroform ug/L 47.850 96 73-127
Chloromethane ug/L 45.450 91 44-146
cis-1,2-Dichloroethene ug/L 46.950 94 74-124
cis-1,3-Dichloropropene ug/L 48.750 97 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644504LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 49.850 100 78-125
Dibromomethane ug/L 50.450 101 82-120
Ethylbenzene ug/L 47.550 95 79-121
Iodomethane ug/L 72.8100 73 39-154
Methylene Chloride ug/L 43.150 86 64-133
Styrene ug/L 49.350 99 84-126
Tetrachloroethene ug/L 48.350 97 78-122
Toluene ug/L 47.850 96 80-121
trans-1,2-Dichloroethene ug/L 47.250 94 71-127
trans-1,3-Dichloropropene ug/L 50.250 100 69-141
trans-1,4-Dichloro-2-butene ug/L 52.4J50 105 40-160
Trichloroethene ug/L 48.450 97 78-122
Trichlorofluoromethane ug/L 48.150 96 53-137
Vinyl acetate ug/L 99.5100 100 40-160
Vinyl chloride ug/L 49.950 100 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1644505MATRIX SPIKE SAMPLE:
MSSpike
Result
92282265001
1,1,1,2-Tetrachloroethane ug/L 21.720 109 70-130ND
1,1,1-Trichloroethane ug/L 22.820 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.220 101 70-130ND
1,1,2-Trichloroethane ug/L 20.720 104 70-130ND
1,1-Dichloroethane ug/L 22.020 110 70-130ND
1,1-Dichloroethene ug/L 22.620 113 70-166ND
1,2,3-Trichloropropane ug/L 21.420 107 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.720 103 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.620 108 70-130ND
1,2-Dichlorobenzene ug/L 21.820 105 70-1300.74J
1,2-Dichloroethane ug/L 22.020 108 70-1300.30J
1,2-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 32.020 107 70-13010.6
2-Butanone (MEK)ug/L 42.6J40 106 70-130ND
2-Hexanone ug/L 44.3J40 111 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 47.0J40 118 70-130ND
Acetone ug/L 77.0J M14019270-130ND
Acrylonitrile ug/L 110J100 110 70-130ND
Benzene ug/L 27.820 109 70-1485.9
Bromochloromethane ug/L 21.720 108 70-130ND
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 19.120 96 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1644505MATRIX SPIKE SAMPLE:
MSSpike
Result
92282265001
Bromomethane ug/L 21.120 106 70-130ND
Carbon disulfide ug/L 21.2J20 106 70-130ND
Carbon tetrachloride ug/L 25.520 127 70-130ND
Chlorobenzene ug/L 22.620 106 70-1461.4J
Chloroethane ug/L 20.620 103 70-130ND
Chloroform ug/L 22.120 110 70-130ND
Chloromethane ug/L 23.720 118 70-130ND
cis-1,2-Dichloroethene ug/L 28.420 109 70-1306.6
cis-1,3-Dichloropropene ug/L 20.220 101 70-130ND
Dibromochloromethane ug/L 20.420 102 70-130ND
Dibromomethane ug/L 22.420 112 70-130ND
Ethylbenzene ug/L 22.820 108 70-1301.2
Iodomethane ug/L 33.040 82 70-130ND
Methylene Chloride ug/L 21.920 109 70-130ND
Styrene ug/L 21.320 107 70-130ND
Tetrachloroethene ug/L 23.120 115 70-130ND
Toluene ug/L 22.020 108 70-1550.43J
trans-1,2-Dichloroethene ug/L 22.220 111 70-130ND
trans-1,3-Dichloropropene ug/L 22.020 110 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.8J20 99 70-130ND
Trichloroethene ug/L 22.620 109 69-1510.72J
Trichlorofluoromethane ug/L 24.520 123 70-130ND
Vinyl acetate ug/L 39.2J40 98 70-130ND
Vinyl chloride ug/L 23.220 114 70-130ND
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%109 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282265002
1644506SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L 0.42J 300.44J
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 7.6 2 307.5
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282265002
1644506SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 2.9 3 302.9
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 2.1J 8 301.9J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 14.3 1 3014.2
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%110 0110
4-Bromofluorobenzene (S)%113 2110
Toluene-d8 (S)%100 0100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/42440
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1645805
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 01/13/16 19:371000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1645806LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4740050000 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645807MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282551003
1645808
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 82 80-12082 0 2550000ND4100040900
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645809MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281885002
1645810
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 95 80-12089 2 2550000107 mg/L 154000 151000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/42369
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92282265002, 92282265003, 92282265004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1643330
Associated Lab Samples:92282265002, 92282265003, 92282265004
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 01/08/16 15:00100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1643331LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 496J500 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643332MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282265002
1643333
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L H3,M150011690-110116 0 10500ND582J582J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643334MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282184017
1643335
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 91 90-11091 0 10500ND456J456J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/26031
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644924
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 01/13/16 14:251000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644925LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 18900J20000 94 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644926MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282346001
1644927
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M620000-50 90-11021 1 10200001250 mg/L 1240000
J
1250000
J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644928MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281822001
1644929
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 98 90-11096 1 102000021.9 mg/L 41400J 41000J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/26019
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92282265002, 92282265003, 92282265004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1643436
Associated Lab Samples:92282265002, 92282265003, 92282265004
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 01/08/16 10:3410.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1643437LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24902500 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1643438MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282265003
1643439
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L M125008990-11088 0 102500ND22102210
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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[phone]
Page 33 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/26042
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1645084
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 01/12/16 20:36500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1645085LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2020020000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645086MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281796001
1645087
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M65000000-4 90-110-4 1 1050000001600 mg/L 1430000 1410000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645088MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282075002
1645089
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 40000 99 90-11099 0 104000012.5 mg/L 51900 52000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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[phone]
Page 34 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/26044
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1645129
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 01/12/16 15:3012500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1645130LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 762000750000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645131MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281851003
1645132
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 3000000 95 90-11095 0 33000000696 mg/L 3540000 3540000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645133MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281854005
1645134
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 96 90-11096 0 375000034.0 mg/L 755000 755000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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[phone]
Page 35 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/26026
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644476
Associated Lab Samples:92282265001, 92282265002, 92282265003, 92282265004
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 01/11/16 14:56500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644477LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2390025000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644478MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92281496001
1644479
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 95 90-11096 0 525000ND2420024300
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1644509MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282266022
1644510
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 98 90-11098 0 52500028002720027200
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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[phone]
Page 36 of 40
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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[phone]
Page 37 of 40
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92282265
ALEXANDER LF (SWS & UIC)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92282265001 MPRP/20439 ICP/18443MW-3 EPA 3010A EPA 6010
92282265002 MPRP/20439 ICP/18443MW-11 EPA 3010A EPA 6010
92282265003 MPRP/20439 ICP/18443MW-26 EPA 3010A EPA 6010
92282265004 MPRP/20439 ICP/18443MW-31 EPA 3010A EPA 6010
92282265005 MPRP/20439 ICP/18443MW-18 EPA 3010A EPA 6010
92282265006 MPRP/20439 ICP/18443MW-27 EPA 3010A EPA 6010
92282265002 MPRP/20458 ICP/18459MW-11 EPA 3010 EPA 6010
92282265003 MPRP/20458 ICP/18459MW-26 EPA 3010 EPA 6010
92282265004 MPRP/20458 ICP/18459MW-31 EPA 3010 EPA 6010
92282265005 MPRP/20458 ICP/18459MW-18 EPA 3010 EPA 6010
92282265005 MERP/8850 MERC/8499MW-18 EPA 7470 EPA 7470
92282265001 MSV/35119MW-3 EPA 8260
92282265002 MSV/35119MW-11 EPA 8260
92282265003 MSV/35119MW-26 EPA 8260
92282265004 MSV/35119MW-31 EPA 8260
92282265005 MSV/35119MW-18 EPA 8260
92282265006 MSV/35119MW-27 EPA 8260
92282265001 WET/42440MW-3 SM 2320B
92282265002 WET/42440MW-11 SM 2320B
92282265003 WET/42440MW-26 SM 2320B
92282265004 WET/42440MW-31 SM 2320B
92282265002 WET/42369MW-11 SM 4500-S2D
92282265003 WET/42369MW-26 SM 4500-S2D
92282265004 WET/42369MW-31 SM 4500-S2D
92282265001 WETA/26031MW-3 EPA 300.0
92282265002 WETA/26031MW-11 EPA 300.0
92282265003 WETA/26031MW-26 EPA 300.0
92282265004 WETA/26031MW-31 EPA 300.0
92282265002 WETA/26019MW-11 EPA 353.2
92282265003 WETA/26019MW-26 EPA 353.2
92282265004 WETA/26019MW-31 EPA 353.2
92282265001 WETA/26042MW-3 SM 4500-Cl-E
92282265002 WETA/26042MW-11 SM 4500-Cl-E
92282265003 WETA/26042MW-26 SM 4500-Cl-E
92282265004 WETA/26042MW-31 SM 4500-Cl-E
92282265001 WETA/26044MW-3 SM 5220D
92282265002 WETA/26044MW-11 SM 5220D
92282265003 WETA/26044MW-26 SM 5220D
92282265004 WETA/26044MW-31 SM 5220D
92282265001 WETA/26026MW-3 SM 5310B
92282265002 WETA/26026MW-11 SM 5310B
92282265003 WETA/26026MW-26 SM 5310B
92282265004 WETA/26026MW-31 SM 5310B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/18/2016 11:03 AM
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Page 38 of 40
Page 39 of 40
Page 40 of 40
#=CL#
February 19, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92286894
92286894
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
ALEXANDER LF- MW-1B
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on February 17, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Dale Ingram
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 10
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92286894
ALEXANDER LF- MW-1B
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 2 of 10
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92286894
ALEXANDER LF- MW-1B
Lab ID Sample ID Matrix Date Collected Date Received
92286894001 MW-1B Water 01/06/16 05:45 02/17/16 09:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 3 of 10
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92286894
ALEXANDER LF- MW-1B
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92286894001 MW-1B EPA 7470 1 PASI-AHVK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 4 of 10
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92286894
ALEXANDER LF- MW-1B
Sample:MW-1B Lab ID:92286894001 Collected:01/06/16 05:45 Received:02/17/16 09:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury, Lab Filtered
Mercury, Dissolved ND ug/L 02/18/16 15:20 7439-97-6 H302/18/16 12:250.20 0.090 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 03:04 PM
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Page 5 of 10
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92286894
ALEXANDER LF- MW-1B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/8970
EPA 7470
EPA 7470
7470 Mercury Dissolved
Associated Lab Samples:92286894001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1668730
Associated Lab Samples:92286894001
Matrix:Water
AnalyzedMDL
Mercury, Dissolved ug/L ND 0.20 02/18/16 15:150.090
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1668731LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.22.5 90 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1668732MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92286900009
1668733
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2.5 94 75-12592 3 252.5ND 2.4 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 03:04 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 6 of 10
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92286894
ALEXANDER LF- MW-1B
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
ANALYTE QUALIFIERS
Sample was received or analysis requested beyond the recognized method holding time.H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 03:04 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 10
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92286894
ALEXANDER LF- MW-1B
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92286894001 MERP/8970 MERC/8618MW-1B EPA 7470 EPA 7470
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 03:04 PM
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[phone]
Page 8 of 10
Page 9 of 10
Page 10 of 10
#=CL#
January 12, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92282252
92282252
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
ALEXANDER LF- METHANE
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on January 07, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 1 of 11
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92282252
ALEXANDER LF- METHANE
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN 55414525 N 8th Street, Salina, KS 67401
A2LA Certification #: 2926.01Alaska Certification #: UST-078Alaska Certification #MN00064
Alabama Certification #40770Arizona Certification #: AZ-0014
Arkansas Certification #: 88-0680California Certification #: 01155CAColorado Certification #Pace
Connecticut Certification #: PH-0256EPA Region 8 Certification #: 8TMS-L
Florida/NELAP Certification #: E87605Guam Certification #:14-008rGeorgia Certification #: 959
Georgia EPD #: PaceIdaho Certification #: MN00064
Hawaii Certification #MN00064Illinois Certification #: 200011Indiana Certification#C-MN-01
Iowa Certification #: 368Kansas Certification #: E-10167
Kentucky Dept of Envi. Protection - DW #90062Kentucky Dept of Envi. Protection - WW #:90062Louisiana DEQ Certification #: 3086
Louisiana DHH #: LA140001Maine Certification #: 2013011
Maryland Certification #: 322Michigan DEPH Certification #: 9909
Minnesota Certification #: 027-053-137Mississippi Certification #: Pace
Montana Certification #: MT0092Nevada Certification #: MN_00064Nebraska Certification #: Pace
New Jersey Certification #: MN-002New York Certification #: 11647
North Carolina Certification #: 530North Carolina State Public Health #: 27700North Dakota Certification #: R-036
Ohio EPA #: 4150Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507Oregon Certification #: MN200001Oregon Certification #: MN300001
Pennsylvania Certification #: 68-00563Puerto Rico Certification
Saipan (CNMI) #:MP0003South Carolina #:74003001Texas Certification #: T104704192
Tennessee Certification #: 02818Utah Certification #: MN000642013-4
Virginia DGS Certification #: 251Virginia/VELAP Certification #: PaceWashington Certification #: C486
West Virginia Certification #: 382West Virginia DHHR #:9952C
Wisconsin Certification #: 999407970
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 11
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92282252
ALEXANDER LF- METHANE
Lab ID Sample ID Matrix Date Collected Date Received
92282252001 MW-1 Water 01/06/16 17:00 01/07/16 10:35
92282252002 MW-1B Water 01/06/16 17:45 01/07/16 10:35
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 3 of 11
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92282252
ALEXANDER LF- METHANE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92282252001 MW-1 RSK 175 1 PASI-MDR1
92282252002 MW-1B RSK 175 1 PASI-MDR1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 4 of 11
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282252
ALEXANDER LF- METHANE
Sample:MW-1 Lab ID:92282252001 Collected:01/06/16 17:00 Received:01/07/16 10:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175RSK 175 AIR Headspace
Methane 33.2 ug/L 01/11/16 18:53 74-82-810.0 0.63 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/12/2016 12:28 PM
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Huntersville, NC 28078
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Page 5 of 11
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282252
ALEXANDER LF- METHANE
Sample:MW-1B Lab ID:92282252002 Collected:01/06/16 17:45 Received:01/07/16 10:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175RSK 175 AIR Headspace
Methane 51.1 ug/L 01/11/16 19:01 74-82-810.0 0.63 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/12/2016 12:28 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 6 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282252
ALEXANDER LF- METHANE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
AIR/25002
RSK 175
RSK 175
RSK 175 AIR HEADSPACE
Associated Lab Samples:92282252001, 92282252002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2173091
Associated Lab Samples:92282252001, 92282252002
Matrix:Water
AnalyzedMDL
Methane ug/L 1.9J 10.0 01/11/16 17:550.63
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2173092LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2173093
Methane ug/L 58.860.7 97 85-1159859.4 1 20
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282355023
2173516SAMPLE DUPLICATE:
Methane ug/L 1.6J 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282350004
2173517SAMPLE DUPLICATE:
Methane ug/L 3.0J 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/12/2016 12:28 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 7 of 11
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92282252
ALEXANDER LF- METHANE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/12/2016 12:28 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 11
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92282252
ALEXANDER LF- METHANE
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92282252001 AIR/25002MW-1 RSK 175
92282252002 AIR/25002MW-1B RSK 175
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/12/2016 12:28 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 9 of 11
Page 10 of 11
Page 11 of 11
#=CL#
January 19, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92282367
92282367
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
BLANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on January 08, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Dale Ingram
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 1 of 22
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92282367
BLANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 22
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92282367
BLANKS
Lab ID Sample ID Matrix Date Collected Date Received
92282367001 EB Water 01/08/16 11:51 01/08/16 11:53
92282367002 FB Water 01/08/16 11:53 01/08/16 11:53
92282367003 TB Water 01/08/16 00:00 01/08/16 11:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 3 of 22
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92282367
BLANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92282367001 EB EPA 6010 16 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 50 PASI-CNB
92282367002 FB EPA 6010 16 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 50 PASI-CNB
92282367003 TB EPA 8260 50 PASI-CNB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 4 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282367
BLANKS
Sample:EB Lab ID:92282367001 Collected:01/08/16 11:51 Received:01/08/16 11:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/19/16 11:32 7440-36-001/15/16 18:006.0 3.8 1
Arsenic ND ug/L 01/19/16 11:32 7440-38-201/15/16 18:0010.0 2.5 1
Barium ND ug/L 01/19/16 11:32 7440-39-301/15/16 18:001002.5 1
Beryllium ND ug/L 01/19/16 11:32 7440-41-701/15/16 18:001.0 0.50 1
Cadmium ND ug/L 01/19/16 11:32 7440-43-901/15/16 18:001.0 0.50 1
Chromium ND ug/L 01/19/16 11:32 7440-47-301/15/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/19/16 11:32 7440-48-401/15/16 18:0010.0 2.5 1
Copper ND ug/L 01/19/16 11:32 7440-50-801/15/16 18:0010.0 2.5 1
Lead ND ug/L 01/19/16 11:32 7439-92-101/15/16 18:0010.0 2.5 1
Nickel ND ug/L 01/19/16 11:32 7440-02-001/15/16 18:0050.0 2.5 1
Selenium ND ug/L 01/19/16 11:32 7782-49-201/15/16 18:0010.0 5.0 1
Silver ND ug/L 01/19/16 11:32 7440-22-401/15/16 18:0010.0 2.5 1
Thallium 17.8 ug/L 01/19/16 11:32 7440-28-001/15/16 18:005.5 5.0 1
Tin ND ug/L 01/19/16 11:32 7440-31-501/15/16 18:001002.5 1
Vanadium ND ug/L 01/19/16 11:32 7440-62-201/15/16 18:0025.0 2.5 1
Zinc ND ug/L 01/19/16 11:32 7440-66-601/15/16 18:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/14/16 15:04 7439-97-601/14/16 09:400.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/12/16 07:34 67-64-110010.0 1
Acrylonitrile ND ug/L 01/12/16 07:34 107-13-12001.9 1
Benzene ND ug/L 01/12/16 07:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/12/16 07:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/12/16 07:34 75-27-41.0 0.18 1
Bromoform ND ug/L 01/12/16 07:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/12/16 07:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/12/16 07:34 78-93-31000.96 1
Carbon disulfide ND ug/L 01/12/16 07:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/12/16 07:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/12/16 07:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/12/16 07:34 75-00-310.0 0.54 1
Chloroform ND ug/L 01/12/16 07:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/12/16 07:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/12/16 07:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/12/16 07:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/12/16 07:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/12/16 07:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/12/16 07:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/12/16 07:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/12/16 07:34 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/12/16 07:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/12/16 07:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/12/16 07:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/12/16 07:34 156-59-25.0 0.19 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
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Page 5 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282367
BLANKS
Sample:EB Lab ID:92282367001 Collected:01/08/16 11:51 Received:01/08/16 11:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,2-Dichloroethene ND ug/L 01/12/16 07:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/12/16 07:34 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/12/16 07:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/12/16 07:34 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/12/16 07:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/12/16 07:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/12/16 07:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/12/16 07:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/12/16 07:34 108-10-11000.33 1
Styrene ND ug/L 01/12/16 07:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/12/16 07:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/12/16 07:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/12/16 07:34 127-18-41.0 0.46 1
Toluene ND ug/L 01/12/16 07:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/12/16 07:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/12/16 07:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/12/16 07:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/12/16 07:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/12/16 07:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/12/16 07:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/12/16 07:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/12/16 07:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)109 %01/12/16 07:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %01/12/16 07:34 17060-07-070-130 1
Toluene-d8 (S)100 %01/12/16 07:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
Pace Analytical Services, Inc.
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Page 6 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282367
BLANKS
Sample:FB Lab ID:92282367002 Collected:01/08/16 11:53 Received:01/08/16 11:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/19/16 11:35 7440-36-001/15/16 18:006.0 3.8 1
Arsenic ND ug/L 01/19/16 11:35 7440-38-201/15/16 18:0010.0 2.5 1
Barium ND ug/L 01/19/16 11:35 7440-39-301/15/16 18:001002.5 1
Beryllium ND ug/L 01/19/16 11:35 7440-41-701/15/16 18:001.0 0.50 1
Cadmium ND ug/L 01/19/16 11:35 7440-43-901/15/16 18:001.0 0.50 1
Chromium ND ug/L 01/19/16 11:35 7440-47-301/15/16 18:0010.0 2.5 1
Cobalt ND ug/L 01/19/16 11:35 7440-48-401/15/16 18:0010.0 2.5 1
Copper ND ug/L 01/19/16 11:35 7440-50-801/15/16 18:0010.0 2.5 1
Lead ND ug/L 01/19/16 11:35 7439-92-101/15/16 18:0010.0 2.5 1
Nickel ND ug/L 01/19/16 11:35 7440-02-001/15/16 18:0050.0 2.5 1
Selenium ND ug/L 01/19/16 11:35 7782-49-201/15/16 18:0010.0 5.0 1
Silver ND ug/L 01/19/16 11:35 7440-22-401/15/16 18:0010.0 2.5 1
Thallium ND ug/L 01/19/16 11:35 7440-28-001/15/16 18:005.5 5.0 1
Tin ND ug/L 01/19/16 11:35 7440-31-501/15/16 18:001002.5 1
Vanadium ND ug/L 01/19/16 11:35 7440-62-201/15/16 18:0025.0 2.5 1
Zinc ND ug/L 01/19/16 11:35 7440-66-601/15/16 18:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/14/16 15:07 7439-97-601/14/16 09:400.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/12/16 07:51 67-64-110010.0 1
Acrylonitrile ND ug/L 01/12/16 07:51 107-13-12001.9 1
Benzene ND ug/L 01/12/16 07:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/12/16 07:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/12/16 07:51 75-27-41.0 0.18 1
Bromoform ND ug/L 01/12/16 07:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/12/16 07:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/12/16 07:51 78-93-31000.96 1
Carbon disulfide ND ug/L 01/12/16 07:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/12/16 07:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/12/16 07:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/12/16 07:51 75-00-310.0 0.54 1
Chloroform ND ug/L 01/12/16 07:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/12/16 07:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/12/16 07:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/12/16 07:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/12/16 07:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/12/16 07:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/12/16 07:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/12/16 07:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/12/16 07:51 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/12/16 07:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/12/16 07:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/12/16 07:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/12/16 07:51 156-59-25.0 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
Pace Analytical Services, Inc.
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Page 7 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282367
BLANKS
Sample:FB Lab ID:92282367002 Collected:01/08/16 11:53 Received:01/08/16 11:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,2-Dichloroethene ND ug/L 01/12/16 07:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/12/16 07:51 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/12/16 07:51 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/12/16 07:51 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/12/16 07:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/12/16 07:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/12/16 07:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/12/16 07:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/12/16 07:51 108-10-11000.33 1
Styrene ND ug/L 01/12/16 07:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/12/16 07:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/12/16 07:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/12/16 07:51 127-18-41.0 0.46 1
Toluene ND ug/L 01/12/16 07:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/12/16 07:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/12/16 07:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/12/16 07:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/12/16 07:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/12/16 07:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/12/16 07:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/12/16 07:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/12/16 07:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %01/12/16 07:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %01/12/16 07:51 17060-07-070-130 1
Toluene-d8 (S)100 %01/12/16 07:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282367
BLANKS
Sample:TB Lab ID:92282367003 Collected:01/08/16 00:00 Received:01/08/16 11:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/12/16 08:08 67-64-110010.0 1
Acrylonitrile ND ug/L 01/12/16 08:08 107-13-12001.9 1
Benzene ND ug/L 01/12/16 08:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/12/16 08:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/12/16 08:08 75-27-41.0 0.18 1
Bromoform ND ug/L 01/12/16 08:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/12/16 08:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/12/16 08:08 78-93-31000.96 1
Carbon disulfide ND ug/L 01/12/16 08:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/12/16 08:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/12/16 08:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/12/16 08:08 75-00-310.0 0.54 1
Chloroform ND ug/L 01/12/16 08:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/12/16 08:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/12/16 08:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/12/16 08:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/12/16 08:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/12/16 08:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/12/16 08:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/12/16 08:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/12/16 08:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/12/16 08:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/12/16 08:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/12/16 08:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/12/16 08:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/12/16 08:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/12/16 08:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/12/16 08:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/12/16 08:08 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/12/16 08:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/12/16 08:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/12/16 08:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/12/16 08:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/12/16 08:08 108-10-11000.33 1
Styrene ND ug/L 01/12/16 08:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/12/16 08:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/12/16 08:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/12/16 08:08 127-18-41.0 0.46 1
Toluene ND ug/L 01/12/16 08:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/12/16 08:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/12/16 08:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/12/16 08:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/12/16 08:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/12/16 08:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/12/16 08:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/12/16 08:08 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
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Page 9 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92282367
BLANKS
Sample:TB Lab ID:92282367003 Collected:01/08/16 00:00 Received:01/08/16 11:53 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 01/12/16 08:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %01/12/16 08:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %01/12/16 08:08 17060-07-070-130 1
Toluene-d8 (S)102 %01/12/16 08:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
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Page 10 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282367
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/8861
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92282367001, 92282367002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1645879
Associated Lab Samples:92282367001, 92282367002
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 01/14/16 14:030.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1645880LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1645881MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92282276001
1645882
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 88 75-12585 3 252.5ND 2.4 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282367
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20488
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92282367001, 92282367002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1648385
Associated Lab Samples:92282367001, 92282367002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/19/16 11:173.8
Arsenic ug/L ND 10.0 01/19/16 11:172.5
Barium ug/L ND 100 01/19/16 11:172.5
Beryllium ug/L ND 1.0 01/19/16 11:170.50
Cadmium ug/L ND 1.0 01/19/16 11:170.50
Chromium ug/L ND 10.0 01/19/16 11:172.5
Cobalt ug/L ND 10.0 01/19/16 11:172.5
Copper ug/L ND 10.0 01/19/16 11:172.5
Lead ug/L ND 10.0 01/19/16 11:172.5
Nickel ug/L ND 50.0 01/19/16 11:172.5
Selenium ug/L ND 10.0 01/19/16 11:175.0
Silver ug/L ND 10.0 01/19/16 11:172.5
Thallium ug/L ND 5.5 01/19/16 11:175.0
Tin ug/L ND 100 01/19/16 11:172.5
Vanadium ug/L ND 25.0 01/19/16 11:172.5
Zinc ug/L ND 10.0 01/19/16 11:175.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1648386LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 514500 103 80-120
Arsenic ug/L 510500 102 80-120
Barium ug/L 513500 103 80-120
Beryllium ug/L 509500 102 80-120
Cadmium ug/L 515500 103 80-120
Chromium ug/L 502500 100 80-120
Cobalt ug/L 514500 103 80-120
Copper ug/L 524500 105 80-120
Lead ug/L 509500 102 80-120
Nickel ug/L 513500 103 80-120
Selenium ug/L 510500 102 80-120
Silver ug/L 252250 101 80-120
Thallium ug/L 519500 104 80-120
Tin ug/L 510500 102 80-120
Vanadium ug/L 507500 101 80-120
Zinc ug/L 503500 101 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
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Huntersville, NC 28078
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Page 12 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282367
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1648387MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277140008
1648388
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 106 75-125109 3 255009.4 537 552
Arsenic ug/L 500 107 75-125111 3 25500ND542559
Barium ug/L 500 101 75-125104 2 25500318822838
Beryllium ug/L 500 102 75-125104 2 25500ND510522
Cadmium ug/L 500 105 75-125108 2 25500ND525538
Chromium ug/L 500 99 75-125101 2 255007.9 504 515
Cobalt ug/L 500 97 75-125100 3 25500ND484500
Copper ug/L 500 106 75-125109 3 25500ND528543
Lead ug/L 500 95 75-12598 3 25500ND475488
Nickel ug/L 500 96 75-12599 3 255006.0 484 499
Selenium ug/L 500 104 75-125107 3 25500ND527542
Silver ug/L 250 105 75-125107 2 25250ND263269
Thallium ug/L 500 91 75-12598 7 2550012.8 468 500
Tin ug/L 500 98 75-125101 3 25500ND492507
Vanadium ug/L 500 103 75-125106 3 25500ND516533
Zinc ug/L 500 96 75-12599 3 2550048.8 529 544
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282367
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35121
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92282367001, 92282367002, 92282367003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644541
Associated Lab Samples:92282367001, 92282367002, 92282367003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/12/16 02:420.33
1,1,1-Trichloroethane ug/L ND 1.0 01/12/16 02:420.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/12/16 02:420.40
1,1,2-Trichloroethane ug/L ND 1.0 01/12/16 02:420.29
1,1-Dichloroethane ug/L ND 5.0 01/12/16 02:420.32
1,1-Dichloroethene ug/L ND 5.0 01/12/16 02:420.56
1,2,3-Trichloropropane ug/L ND 1.0 01/12/16 02:420.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/12/16 02:422.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/12/16 02:420.27
1,2-Dichlorobenzene ug/L ND 5.0 01/12/16 02:420.30
1,2-Dichloroethane ug/L ND 1.0 01/12/16 02:420.24
1,2-Dichloropropane ug/L ND 1.0 01/12/16 02:420.27
1,4-Dichlorobenzene ug/L ND 1.0 01/12/16 02:420.33
2-Butanone (MEK)ug/L ND 100 01/12/16 02:420.96
2-Hexanone ug/L ND 50.0 01/12/16 02:420.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/12/16 02:420.33
Acetone ug/L ND 100 01/12/16 02:4210.0
Acrylonitrile ug/L ND 200 01/12/16 02:421.9
Benzene ug/L ND 1.0 01/12/16 02:420.25
Bromochloromethane ug/L ND 3.0 01/12/16 02:420.17
Bromodichloromethane ug/L ND 1.0 01/12/16 02:420.18
Bromoform ug/L ND 3.0 01/12/16 02:420.26
Bromomethane ug/L ND 10.0 01/12/16 02:420.29
Carbon disulfide ug/L ND 100 01/12/16 02:421.2
Carbon tetrachloride ug/L ND 1.0 01/12/16 02:420.25
Chlorobenzene ug/L ND 3.0 01/12/16 02:420.23
Chloroethane ug/L ND 10.0 01/12/16 02:420.54
Chloroform ug/L ND 5.0 01/12/16 02:420.14
Chloromethane ug/L ND 1.0 01/12/16 02:420.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/12/16 02:420.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/12/16 02:420.13
Dibromochloromethane ug/L ND 3.0 01/12/16 02:420.21
Dibromomethane ug/L ND 10.0 01/12/16 02:420.21
Ethylbenzene ug/L ND 1.0 01/12/16 02:420.30
Iodomethane ug/L ND 10.0 01/12/16 02:420.32
Methylene Chloride ug/L ND 1.0 01/12/16 02:420.97
Styrene ug/L ND 1.0 01/12/16 02:420.26
Tetrachloroethene ug/L ND 1.0 01/12/16 02:420.46
Toluene ug/L ND 1.0 01/12/16 02:420.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/12/16 02:420.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/12/16 02:420.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282367
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1644541
Associated Lab Samples:92282367001, 92282367002, 92282367003
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 01/12/16 02:421.0
Trichloroethene ug/L ND 1.0 01/12/16 02:420.47
Trichlorofluoromethane ug/L ND 1.0 01/12/16 02:420.20
Vinyl acetate ug/L ND 50.0 01/12/16 02:420.35
Vinyl chloride ug/L ND 1.0 01/12/16 02:420.62
Xylene (Total)ug/L ND 5.0 01/12/16 02:420.66
1,2-Dichloroethane-d4 (S)%97 70-130 01/12/16 02:42
4-Bromofluorobenzene (S)%102 70-130 01/12/16 02:42
Toluene-d8 (S)%99 70-130 01/12/16 02:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644542LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.750 97 80-125
1,1,1-Trichloroethane ug/L 50.250 100 71-129
1,1,2,2-Tetrachloroethane ug/L 47.150 94 79-124
1,1,2-Trichloroethane ug/L 47.450 95 85-125
1,1-Dichloroethane ug/L 48.850 98 73-126
1,1-Dichloroethene ug/L 52.850 106 66-135
1,2,3-Trichloropropane ug/L 47.750 95 75-130
1,2-Dibromo-3-chloropropane ug/L 49.350 99 71-133
1,2-Dibromoethane (EDB)ug/L 50.850 102 83-124
1,2-Dichlorobenzene ug/L 48.350 97 80-133
1,2-Dichloroethane ug/L 44.050 88 67-128
1,2-Dichloropropane ug/L 49.450 99 75-132
1,4-Dichlorobenzene ug/L 48.150 96 78-130
2-Butanone (MEK)ug/L 103100 103 61-144
2-Hexanone ug/L 93.9100 94 68-143
4-Methyl-2-pentanone (MIBK)ug/L 95.4J100 95 72-135
Acetone ug/L 111100 111 48-146
Acrylonitrile ug/L 245250 98 40-160
Benzene ug/L 50.350 101 80-125
Bromochloromethane ug/L 56.650 113 71-125
Bromodichloromethane ug/L 49.250 98 78-124
Bromoform ug/L 43.350 87 71-128
Bromomethane ug/L 54.050 108 40-160
Carbon disulfide ug/L 58.1J50 116 50-160
Carbon tetrachloride ug/L 50.250 100 69-131
Chlorobenzene ug/L 48.050 96 81-122
Chloroethane ug/L 52.650 105 39-148
Chloroform ug/L 49.250 98 73-127
Chloromethane ug/L 56.250 112 44-146
cis-1,2-Dichloroethene ug/L 49.550 99 74-124
cis-1,3-Dichloropropene ug/L 50.250 100 72-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
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[phone]
Page 15 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282367
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1644542LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 47.250 94 78-125
Dibromomethane ug/L 49.850 100 82-120
Ethylbenzene ug/L 48.450 97 79-121
Iodomethane ug/L 99.1100 99 39-154
Methylene Chloride ug/L 52.050 104 64-133
Styrene ug/L 49.450 99 84-126
Tetrachloroethene ug/L 49.050 98 78-122
Toluene ug/L 49.650 99 80-121
trans-1,2-Dichloroethene ug/L 49.350 99 71-127
trans-1,3-Dichloropropene ug/L 50.050 100 69-141
trans-1,4-Dichloro-2-butene ug/L 46.3J50 93 40-160
Trichloroethene ug/L 48.150 96 78-122
Trichlorofluoromethane ug/L 50.250 100 53-137
Vinyl acetate ug/L 100100 100 40-160
Vinyl chloride ug/L 58.950 118 58-137
Xylene (Total)ug/L 145150 97 81-126
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1644543MATRIX SPIKE SAMPLE:
MSSpike
Result
92282365007
1,1,1,2-Tetrachloroethane ug/L 18.720 93 70-130ND
1,1,1-Trichloroethane ug/L 20.820 104 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.020 90 70-130ND
1,1,2-Trichloroethane ug/L 17.920 90 70-130ND
1,1-Dichloroethane ug/L 21.520 98 70-1301.9J
1,1-Dichloroethene ug/L 21.720 109 70-166ND
1,2,3-Trichloropropane ug/L 19.420 97 70-130ND
1,2-Dibromo-3-chloropropane ug/L 17.620 88 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.520 97 70-130ND
1,2-Dichlorobenzene ug/L 18.920 94 70-130ND
1,2-Dichloroethane ug/L 18.020 88 70-1300.43J
1,2-Dichloropropane ug/L 19.120 96 70-130ND
1,4-Dichlorobenzene ug/L 19.220 94 70-1300.44J
2-Butanone (MEK)ug/L 39.0J40 97 70-130ND
2-Hexanone ug/L 36.9J40 92 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 37.5J40 94 70-130ND
Acetone ug/L 40.3J40 101 70-130ND
Acrylonitrile ug/L 97.3J100 97 70-130ND
Benzene ug/L 19.320 97 70-148ND
Bromochloromethane ug/L 20.520 103 70-130ND
Bromodichloromethane ug/L 19.020 95 70-130ND
Bromoform ug/L 15.820 79 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
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Page 16 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282367
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1644543MATRIX SPIKE SAMPLE:
MSSpike
Result
92282365007
Bromomethane ug/L 17.620 88 70-130ND
Carbon disulfide ug/L 20.4J20 102 70-130ND
Carbon tetrachloride ug/L 21.720 109 70-130ND
Chlorobenzene ug/L 18.720 94 70-146ND
Chloroethane ug/L 19.720 98 70-130ND
Chloroform ug/L 19.320 97 70-130ND
Chloromethane ug/L 22.320 111 70-130ND
cis-1,2-Dichloroethene ug/L 22.320 97 70-1303.0J
cis-1,3-Dichloropropene ug/L 18.520 92 70-130ND
Dibromochloromethane ug/L 16.820 84 70-130ND
Dibromomethane ug/L 18.420 92 70-130ND
Ethylbenzene ug/L 19.220 96 70-130ND
Iodomethane ug/L 24.0 M1406070-130ND
Methylene Chloride ug/L 19.720 98 70-130ND
Styrene ug/L 18.720 93 70-130ND
Tetrachloroethene ug/L 22.220 98 70-1302.7
Toluene ug/L 19.020 95 70-155ND
trans-1,2-Dichloroethene ug/L 19.920 99 70-130ND
trans-1,3-Dichloropropene ug/L 17.820 89 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.4J20 87 70-130ND
Trichloroethene ug/L 22.220 93 69-1513.6
Trichlorofluoromethane ug/L 21.320 107 70-130ND
Vinyl acetate ug/L 25.7J M1406470-130ND
Vinyl chloride ug/L 22.620 113 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282365008
1644544SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 3.6J 1 303.7J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92282367
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92282365008
1644544SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 8.6 1 308.5
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L 2.7 1 302.7
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 2.0 4 301.9
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%101 0101
4-Bromofluorobenzene (S)%104 1105
Toluene-d8 (S)%100 1100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 22
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92282367
BLANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 22
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92282367
BLANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92282367001 MPRP/20488 ICP/18487EBEPA 3010A EPA 6010
92282367002 MPRP/20488 ICP/18487FBEPA 3010A EPA 6010
92282367001 MERP/8861 MERC/8514EBEPA 7470 EPA 7470
92282367002 MERP/8861 MERC/8514FBEPA 7470 EPA 7470
92282367001 MSV/35121EBEPA 8260
92282367002 MSV/35121FBEPA 8260
92282367003 MSV/35121TBEPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/19/2016 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 22
Page 21 of 22
Page 22 of 22
Appendix B
Field Sampling Parameter Data Sheet(s)