8606_SurryCounty_MSWLF_GWMReport_DIN26375_20150529

Surry County Subtitle D Lined MSWLF
Mt. Airy, North Carolina
May 2015
Permit Number: 86-06
Semi-Annual Water Quality Monitoring Report
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G15025.0
P.O. Box 97
Garner, NC 27529
License No. C-0281

TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
MW-2 Area Investigations Page 2
MW-6R Area Investigations Page 2
MW-9S Area Investigations Page 2
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 2
Groundwater Samples Page 3
Surface Water Samples Page 3
Leachate Samples Page 3
Groundwater and Surface Water Characterization Page 3
Findings Page 4
Closing Page 4
FIGURES
Topographic Map with Site Location Figure 1
Single Event Potentiometric Map of Uppermost Aquifer Figure 2

TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, GWP, 2L, or 2B (Appendix 1) Table 5
Detections in Leachate Samples above SWSL, GWP or 2L Table 6
Hydrologic Properties at Monitoring Well Locations Table 7
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Data Sheet(s) Appendix B
February 19, 2016
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality
2090 US Highway 70
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report
Surry County Subtitle D Lined MSWLF, Phases 1 & 2
Permit No. 86-06
MESC0 Project No. G15025.0
Sampling Date(s). May 28-29, 2015
Dear Ms Drummond:
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Monitoring Report for an event performed at the Surry County Subtitle D Lined
Municipal Solid Waste Landfill (MSWLF) in the Fall 2014. NCDENR Solid Waste Rules 15A NCAC 13B.1632
requires that Surry County provide this report to the SWS on a semi-annual basis. This report documents the quality
of the ground and surface waters during this monitoring event performed on May 28-29, 2015. Surface water point
SW-4 was re-sampled on July 20, 2015 since the VOC vials collected during the May event were reported by the
laboratory to be broken. The laboratory analytical results indicate that three downgradient wells contained one or
more chlorinated hydrocarbons above NC 2L Groundwater Standards. All contaminants detected above 2L
Standards were not above the Solid Waste Section Reporting Limit (<SWSL/”j-qualified”). All detections were
below Federal “Drinking Water Standards”, contaminants remain low in raw leachate samples and all the surface
water samples continue to appear unimpacted.
Background
The Surry County Subtitle D lined MSWLF, permit #86-06, is located at 237 Landfill Road, Mount Airy, Surry
County, North Carolina. The site location topographic map is depicted in the attached Figure 1. The lined MSWLF
is comprised of contiguous Phases 1 & 2 which are treated as a single unit in this report.
Water quality at this facility has been monitored at least semi-annually since 1998 with historical data available
since 1998. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A
NCAC 13B and as a condition of the permit to operate.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and a recent SWS
memorandum this report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization. Well construction summary table, field observations table, field parameter data table, sampling
and analysis summary table, detections compared to Standards tables, a groundwater flow directions/rates table,
potentiometric map, quality assurance/quality control data, and laboratory analytical data results are enclosed herein.

MW-2 Area Investigations
During this event MESCO investigated the area around MW-2 in an attempt to identify the source of low “j”
qualified concentrations of VOCs detected in samples collected from MW-2. The double lined leachate lagoon
leak detection manhole was observed to be dry, indicating the lagoon has not leaked. Evidence has never been
found to suggest that the lagoon has ever overflowed. There were no detections in a supplemental surface water
sample (SW-A) collected downgradient of MW-2.
MW-6R Area Investigations
During this event MESCO investigated the area around MW-6R in an attempt to identify the source of VOC
detections. MW-6R is located in a ditch that previously conveyed stormwater originating from the lined landfill.
During the construction of Phased 2 in 2009, stormwater originating near the landfill was rerouted so that it no
longer flows adjacent to MW-6R. Landfill gas (LFG) has been detected in migration monitoring probe MGP-5
located less than 75 feet away from MW-6R. Active LFG extraction has been initiated at Lined Phase 1 which
includes vacuum applied at the closest leachate collection system cleanout.. Methane was absent from the adjacent
cleanout during every reading MESCO has taken since it was tied into the active extraction system. There were no
detections in a supplemental surface water sample (SW-B) collected downgradient of MW-6R.
MW-9S Area Investigations
During this event MESCO investigated the area around MW-9S in an attempt to identify the source of VOC
detections. MW-9S is located about 180 feet downgradient of the Phase 2 sump near a previous drainage feature.
Low levels of chlorinated hydrocarbons have consistently been detected in samples collected from MW-9S since
before waste was deposited in Phase 2. VOCs were absent from adjacent deeper cluster well MW-9D.
Sampling Procedure
MESCO personnel performed this sampling event using portable monitoring methodology in general accordance
with the site-specific SAP from the Phase 2 Design Hydrogeologic Study, approved June 13, 2008. Water samples
were collected from 14 downgradient groundwater monitoring wells (MW-2R, MW-3, MW-4S, MW-4D, MW-5,
MW-6R, MW-8, MW-9S, MW-9D, MW-10, MW-11S, MW-11D, MW-12 and MW-13), one background well
(MW-1), four downstream surface water locations (SW-4 , SWN-2, SW-A and SW-B), four upstream surface water
stations (SWN-1, SW-1, SW-2 and SW-3) and a leachate sample (LAGOON). Surface water points SWN-3 and
SWN-4 were not sampled because they were dry. Surface water samples were collected at points directly
downgradient of impacted wells MW-2 and MW-6R named SW-A and SW-B respectively. Quality control
measures included analysis of equipment blanks (EB) field blanks (FB) and trip blanks (TB). Sampling locations
are shown on the potentiometric map (Figure 2).
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and
integrity of all monitoring locations were visually evaluated and no deficiencies identified as documented on Table
2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level
elevation. Low-flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of
three times the volume of standing water in the well or until dry. Surface water samples were collected from Stoney
Creek discharge feature at previously designated locations. During well purging and surface water sample
collection the required field parameters were recorded. The samples were then placed into laboratory-prepared, pre-
preserved containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported
to a NC-certified laboratory under proper C-O-C protocols within the specified hold times for each analysis.
2
Field Parameter Data
Stabilized field parameters were recorded during purging which included pH, specific conductance, temperature,
total dissolved solids (TDS) and visual turbidity. A summary of the field parameter data is presented in Table 3 and
the field sampling data sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Services, Inc. (PACE) of Huntersville and Asheville NC performed the laboratory analysis of the
water and leachate samples. Water samples were analyzed for the current 40 CFR 258 Appendix I list of VOCs and
total recoverable metals. The leachate was tested for the SWS standard leachate specific parameter list which
includes VOCs, total metals, phosphorous, BOD, COD, sulfide and nitrate. A sampling and analysis table
summarizing the locations, constituents and methods is presented as Table 4.
Water samples were analyzed to the laboratory specific Method Detection Limits (MDL), which are quantifiable at
or below the current Solid Waste Section detection limits (SWSL). Table 5 summarizes constituents detected in
groundwater and surface water samples that attain or were above the current SWSL, Groundwater Protection
Standards (GWP), North Carolina Groundwater Standards (2L), the applicable North Carolina Surface Water
Standards (2B) for a class C waterbody, and Maximum Contaminant Levels (MCL) also known as “Federal Primary
Drinking Water Standards”. Table 6 summarizes constituents detected in the leachate lagoon samples. Laboratory
results and C-O-Cs are presented in Appendix A.
Quality Control Samples
Methylene chloride was detected in quality control sample (EB); However, methylene chloride was not detected in
any other samples therefore the field or laboratory induced artifact contamination is non-consequential.
Groundwater Samples
The only metal detected above the SWSL and its respective 2L or GWP Standard during this event was total
chromium in a sample collected from hydraulically upgradient background well MW-1.
Sample collected from MW-6R contained levels of VC (0.8 µg/L) and PCE (0.73 µg/L) which were above their
respective 2L Standards of 0.03 µg/L and 0.7 µg/L but below the SWSL thus “j-qualified”.. PCE continues to be
detected in samples collected from MW-2 at 1.0 µg/L which is above the 2L Standard (0.7µg/L). VC was detected
at a “j-qualified” concentration of 0.67 µg/L in MW-9S for the second consecutive event.
Surface Water Samples
Surface water point SW-4 which consists of potential discharge from both the active lined and closed unlined
landfills contained levels of total copper at 13.7 µg/L which is above the 2B Standard (7 µg/L).
Leachate Samples
Very few contaminants have ever been detected in leachate samples collected at this facility. During this event none
of the parameters detected in groundwater samples above 2L or GWP were detected in the leachate samples. Vinyl
chloride, the lone VOC detected in a groundwater sample above SWSL and 2L Standard, has only been detected in a
leachate sample once over 7 years ago and PCE has never been detected.
Groundwater and Surface Water Characterization
MESCO prepared a potentiometric map of the uppermost aquifer from groundwater elevation data recorded during
this monitoring event (Plate 2). Groundwater flow rates and directions were calculated and are included in the
hydrologic properties table (Table 7). Groundwater flow directions remain generally in a southerly direction
towards the Ararat River with groundwater velocities calculated by modified Darcy's equation varied considerably
due to the anisotropic geologic conditions. Streams located at the designated surface water sampling stations were
observed to be of low volume and flow with low turbidity.
3
Figures
Topographic Map with Site Location
FIGURE 1
Surry County Subtitle D Lined MSWLF, Mt. Airy
237 Landfill Road
Mount Airy, NC 28621
Lat:36-26-30.065
Long:-80-34-15.314
Northing:983356.18
Easting:1537885.48 Closed Unlined C&D Landfill
Closed Unlined Sanitary Landfill
Active Lined MSW Landfill
01 1 MILE
Tables
Surry County Subtitle D MSWLF Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
May 28-29, 2015
Latitude Longitude
(inches)(ft)
MW-1 8/14/98 2 68.5 53.5 15 Rock 1127.02 1124.23 1062.27 64.75 36.434494 -80.577989
MW-2 8/16/98 2 23.5 8.5 15 Rock 936.68 933.91 923.32 13.36 36.430833 -80.571161
MW-3R 12/2/98 2 20 5 15 Rock 930.00 928.15 924.85 5.15 36.430714 -80.571575
MW-4S 8/11/98 2 20 5 15 943.23 940.31 932.16 11.07 36.430853 -80.572400
MW-4D 8/11/98 2 45 35 10 Rock 942.80 940.31 931.17 11.63 36.430853 -80.572400
MW-5 8/18/98 2 47.5 32.5 15 Rock 977.86 971.57 933.59 44.27 36.430356 -80.572961
MW-6R 3/22/99 2 79 64 15 Fractured Rock 1004.75 1001.81 937.74 67.01 36.429958 -80.573508
MW-8 9/1/09 2 70.75 55.75 15 Fractured Rock 971.03 968.35 908.17 62.86 36.429283 -80.573453
MW-9S 6/16/06 2 42.28 27.28 15 Fractured Rock 952.83 949.75 917.87 34.96 36.429314 -80.574464
MW-9D 6/16/06 2 65.54 55.54 10 Competent Rock 952.47 949.49 915.54 36.93 36.429314 -80.574464
MW-10 6/16/06 2 47.13 27.13 20 Fractured Rock 970.24 967.35 938.76 31.48 36.429519 -80.575486
MW-11S 9/3/09 2 46.05 31.05 15 Competent Rock 969.09 965.95 938.12 30.97 36.430197 -80.577131
MW-11D 9/3/09 2 65.31 55.31 10 Competent Rock 965.38 962.38 933.49 31.89 36.430197 -80.577131
MW-12 9/4/09 2 65 50 15 Competent Rock 996.66 993.71 944.80 51.86 36.429831 -80.576750
MW-13 9/3/09 2 36.31 21.31 15 Fractured Rock 983.13 979.83 956.27 26.86 36.430625 -80.578531
MLW-A 8/19/98 2 84 69 15 Competent Rock 1095.51 1092.51 1012.80 82.71 36.432881 -80.573539
P2-6S 6/7/06 2 66.38 51.38 15 Fractured Rock 1040.27 1037.36 983.04 57.23 36.431019 -80.578025
P2-6D 6/7/06 2 93.98 83.98 10 Competent Rock 1040.65 1037.56 974.73 65.92 36.431019 -80.578025
P2-11S 6/16/06 2 50.13 40.13 10 Competent Rock 1021.53 1018.40 971.40 50.13 36.430197 -80.577131
P2-11D 6/16/06 2 65.45 60.45 5 Competent Rock 1021.13 1018.73 970.63 50.50 36.430197 -80.577131
P2-12 6/16/06 2 59.56 44.56 15 Competent Rock 986.61 983.54 933.30 53.31 36.429831 -80.576750
NOTE:
1. Ground, datum and TOR elevations are in units of feet, well diameter are in units of inches.
Monitoring
Well
Date
Installed
Well
Diameter
Total Well
Depth
Top of
Screen Depth
Screen
Length Geology of
Screened Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
Saprolite
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
May 28-29, 2015
Comments
MW-1 Yes Yes Yes Yes Yes Yes
MW-2 Yes Yes Yes Yes Yes ?
MW-3R Yes Yes Yes Yes Yes ?Pad covered by soil
MW-4S Yes Yes Yes Yes Yes ?Pad covered by soil
MW-4D Yes Yes Yes Yes Yes ?Pad covered by soil
MW-5 Yes Yes Yes Yes Yes Yes Repaired by Co. in Sept. 2013 Datum may have changed
MW-6R Yes Yes Yes Yes Yes Yes County improved surface seal in September 2013
MW-8 Yes Yes Yes Yes Yes Yes Path poor
MW-9S Yes Yes Yes Yes Yes Yes
MW-9D Yes Yes Yes Yes Yes Yes
MW-10 Yes Yes Yes Yes Yes Yes
MW-11S Yes Yes Yes Yes Yes Yes Brush cleared around well
MW-11D Yes Yes Yes Yes Yes Yes Slight hydrogen sulfide smell, very slow recharge
MW-12 Yes Yes Yes Yes Yes Yes Slow recharge
MW-13 Yes Yes Yes Yes Yes Yes
SW-1 Yes -----Low gage height & flow
SW-2 Yes -----Low gage height & flow
SW-3 Yes -----Low gage height & flow
SWN-1 Yes -----Low gage height & flow
SWN-2 Yes -----Low gage height & flow
SWN-3 No -----Dry
SWN-4 No -----Dry. Always has been
SW-A Yes -----
SW-B Yes -----
LAGOON Yes Yes Yes Yes Yes Yes
MLW-A Yes Yes Yes Yes Yes ?Pad covered by soil
P2-6S Yes Yes Yes Yes Yes Yes Depth to groundwater only
P2-6D Yes Yes Yes Yes Yes Yes Depth to groundwater only
P2-11S Yes Yes Yes Yes Yes Yes Depth to groundwater only
P2-11D Yes Yes Yes Yes Yes Yes Depth to groundwater only
P2-12 Yes Yes Yes Yes Yes Yes Depth to groundwater only
Any unusual field conditions, observations, or events:
Dual lined leachate lagoon leak detection manhole observed to be dry.
Phase 2 has an earthen berm built w/in liner limits which may reduce any potential for overland flow from Phase 2.
Paths leading to wells and around entire facility have been improved by County recently. All are 4X4 accessible.
Second event that surface water samples collected from points SW-A and SW-B per the SWS verbal request.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked on
Arrival &
Departure
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears
Effective
Pad covered in kudzoo
2nd event per SWS verbal request
2nd event per SWS verbal request
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 3
Field Parameter Data Summary
May 28-29, 2015
Parameter Temp.ORP DO pH TDS
Units C mg/L SU mg/L (%/Vol)Visual
MW-1 64.75 1062.27 1127.02 15.2 NR NR 6.43 120 50 0 Slight
MW-2 13.63 923.05 936.68 14.1 NR NR 5.53 90 40 NR Clear
MW-3R 5.15 924.85 930.00 13.6 NR NR 5.81 390 200 NR Clear
MW-4S 11.07 932.16 943.23 14.8 NR NR 5.12 120 50 NR Slight
MW-4D 11.63 931.17 942.80 14.6 NR NR 6.31 140 80 0 Slight
MW-5 44.27 933.59 977.86 15.0 NR NR 5.77 130 280 0 Clear
MW-6R 67.01 937.74 1004.75 14.8 NR NR 5.03 120 60 0 Clear
MW-8 62.86 908.17 971.03 15.2 NR NR 6.31 50 30 0 Slight
MW-9S 34.96 917.87 952.83 15.9 NR NR 6.57 250 130 NR Clear
MW-9D 36.93 915.54 952.47 16.3 NR NR 7.03 530 260 NR Clear
MW-10 31.48 938.76 970.24 14.9 NR NR 6.81 100 40 NR Clear
MW-11S 30.97 938.12 969.09 14.7 NR NR 5.99 90 30 NR Slight
MW-11D 31.89 933.49 965.38 14.5 NR NR 6.93 190 90 NR Clear
MW-12 51.86 944.80 996.66 14.4 NR NR 6.83 190 80 NR Clear
MW-13 26.86 956.27 983.13 16.9 NR NR 5.81 100 50 NR NR
MLW-A 82.71 1012.80 1095.51 NR NR NR NR NR NR NR NR
P2-6S 57.23 983.04 1040.27 NR NR NR NR NR NR NR NR
P2-6D 65.92 974.73 1040.65 NR NR NR NR NR NR NR NR
P2-11S 50.13 971.40 1021.53 NR NR NR NR NR NR NR NR
P2-11D 50.50 970.63 1021.13 NR NR NR NR NR NR NR NR
P2-12 53.31 933.30 986.61 NR NR NR NR NR NR NR NR
Minimum 5.15 908.17 930.00 13.6 NR NR 5.03 50 30 NR Clear
Average 42.15 949.70 991.85 15.0 NR NR 6.15 174 98 NR Slight
Maximum 82.71 1062.27 1127.02 16.9 NR NR 7.03 530 280 NR Slight
SW-1 ---14.8 NR NR 7.01 290 140 -Clear
SW-2 ---13.4 NR NR 6.97 320 150 -Clear
SW-3 ---14.9 NR NR 7.03 290 140 -Clear
SW-4 ---15.2 NR NR 7.07 310 150 -Clear
SWN-1 ---13.4 NR NR 7.13 90 40 -Clear
SWN-2 ---13.3 NR NR 7.17 180 90 -Clear
SW-A ---15.3 NR NR 7.02 110 50 -Clear
SW-B ---15.2 NR NR 7.07 110 50 -Clear
Minimum ---13.3 NR NR 6.97 90 40 -Clear
Average ---14.4 NR NR 7.06 213 101 -Clear
Maximum ---15.3 NR NR 7.17 320 150 -Clear
NR = No reading attempted
Depth to
Water
Water
Elevation
TOC
Elevation
Specific
Conductance
Methane
Gas in
Headspace
Turbidity of
Metals
Sample
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
btoc = Below top of casing
amsl = Above mean sea level
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 4
Sampling and Analysis Summary
May 28-29, 2015
Field Parameter Leachate
Re
a
s
o
n

N
o
t

S
a
m
p
l
e
d
To
t
a
l

M
e
t
a
l
s

Te
m
p
e
r
a
t
u
r
e
Co
n
d
u
c
t
i
v
i
t
y
To
t
a
l

D
i
s
s
o
l
v
e
d

S
o
l
i
d
s

(
T
D
S
)
pH Tu
r
b
i
d
i
t
y
Su
l
f
a
t
e
pH Ph
o
s
p
h
o
r
u
s
BO
D
,

5

d
a
y
CO
D
Ni
t
r
a
t
e
La
b

E
P
A

8
2
6
0
B
L
a
b

E
P
A

6
0
0
0
/
7
0
0
0
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

V
i
s
u
a
l
La
b

E
P
A

3
0
0
.
0
La
b

E
P
A
9
0
4
0
La
b

E
P
A
3
6
5
.
1
La
b

S
M

5
2
1
0
B
La
b

S
M

5
2
2
0
D
La
b

E
P
A

3
5
3
.
2
MW-1 x x x x x x x
MW-2 x x x x x x x
MW-3R x x x x x x x
MW-4S x x x x x x x
MW-4D x x x x x x x
MW-5 x x x x x x x
MW-6R x x x x x x x
MW-8 x x x x x x x
MW-9S x x x x x x x
MW-9D x x x x x x x
MW-10 x x x x x x x
MW-11S x x x x x x x
MW-11D x x x x x x x
MW-12 x x x x x x x
MW-13 x x x x x x x
SWN-1 x x x x x x x
SWN-2 x x x x x x x
SW-1 x x x x x x x
SW-2 x x x x x x x
SW-3 x x x x x x x
SW-4 x x x x x x x
SWN-3 Dry
SWN-4 Dry
SW-A x x x x x x x
SW-B x x x x x x x
LAGOON x x x x x x x x x x
EB x x
FB x x
TB x
Appendix I = List from current 40 CFR 258
App. I
VO
C
s

Surry County Subtitle D Lined Landfill Page 1 of 2
Table 5
Detections in Water Samples above SWSL, GWP, 2L, or 2B
May 28-29, 2015
Result Unit
MW-1 Copper, total 5/29/15 20.7 2.5 10 1000 1300
MW-1 Vanadium, total 5/29/15 9J 2.5 25 NE 3.5 NE
MW-1 Zinc, total 5/29/15 36.4 5 10 1000 5000
MW-1 Cadmium, total 5/29/15 1 0.5 1 2 5
MW-1 Chromium, total 5/29/15 10.6 2.5 10 10 100 N
MW-2 5/29/15 1 0.46 1 0.7 5 L &/or LFG
MW-4S Zinc, total 5/29/15 12.9 5 10 1000 5000
MW-4S Vanadium, total 5/29/15 7.8J 2.5 25 NE 3.5 NE
MW-5 Zinc, total 5/29/15 12 5 10 1000 5000
MW-5 Copper, total 5/29/15 33.3 2.5 10 1000 1300
MW-6R Vinyl chloride 5/29/15 0.8J 0.62 1 0.03 5 L &/or LFG
MW-6R 5/29/15 0.73J 0.46 1 0.7 5 L &/or LFG
MW-9D Zinc, total 5/29/15 19.2 5 10 1000 5000
MW-9D Copper, total 5/29/15 10.3 2.5 10 1000 1300
MW-9D Vanadium, total 5/29/15 3.7J 2.5 25 NE 3.5 NE
MW-9S Vanadium, total 5/29/15 8.7J 2.5 25 NE 3.5 NE
MW-9S Vinyl chloride 5/29/15 0.67J 0.62 1 0.03 5 L &/or LFG
MW-9S 5/29/15 6.5 0.19 5 70 70
MW-9S Cobalt, total 5/29/15 31.8 2.5 10 NE 70 NE
MW-9S 5/29/15 1.3 0.47 1 3 5
MW-11D Vanadium, total 5/29/15 7.8J 2.5 25 NE 3.5 NE
MW-11D Antimony, total 5/29/15 4.6J 3.8 6 NE 1.4 6
MW-12 Cadmium, total 5/29/15 1.2 0.5 1 2 5
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
ug/L
ug/L
ug/L
ug/L
Tetrachloroethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Tetrachloroethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
Trichloroethene ug/L
ug/L
ug/L
ug/L
Surry County Subtitle D Lined Landfill Page 2 of 2
Result UnitSample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
SW-2 Cobalt, total 5/28/15 22.3 2.5 10 270 NE
SW-4 Zinc, total 5/28/15 118 5 10 50 5000
SW-4 Copper, total 5/28/15 13.7 2.5 10 7 1300 N
EB Methylene Chloride 5/29/15 61.2 0.97 1 4.6 5 Artifact
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
J =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
NE = Not Established
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
L = Leachate
LFG = Landfill Gas
BOLD = Concentration > 2L, 2B or MCL Standard
ug/L
ug/L
ug/L
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 6
Detections in Leachate Samples above SWSL, GWP, 2L or 2B
May 28, 2015
Result Unit
LAGOON Thallium, total 5/28/15 6.9 5 5.5 NE 0.28 2
LAGOON Barium, total 5/28/15 179 2.5 100 700 1300
LAGOON 5/28/15 16.9 0.32 10 NE NE NE
LAGOON Phosphorus 5/28/15 190 25 50 NE NE
LAGOON COD 5/28/15 170000 25000 50000 NE NE
LAGOON BOD, 5 day 5/28/15 54000 2000 2000 NE NE
BOLD = Concentration > 2L, 2B or MCL Standard
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7
ug/L
ug/L
Iodomethane ug/L
ug/L
ug/L
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 7
Hydrogeologic Properties at Monitoring Well Locations
May 29, 2015
Flow Rate
Screened Interval Lithology(cm/second)(%)(feet/feet)(feet/year)
MW-1 2.45E-04 3 0.162 1,372 N54E 64.75 1062.27 Fractured Rock
MW-2 3.20E-04 3 0.064 710 S10E 13.63 923.05 Fractured Rock
MW-3R 3.20E-04 3 0.047 517 S22E 5.15 924.85 Fractured Rock
MW-4S 1.50E-04 3 0.050 261 S29E 11.07 932.16 Sandy Silt & Fractured Rock
MW-4D 1.59E-04 3 --S13E 11.63 931.17 Fractured Rock
MW-5 3.20E-04 3 0.097 1,071 S54E 43.70 933.59 Fractured Rock
MW-6R 3.20E-04 3 0.058 640 S26E 67.01 937.74 Fractured Rock
MW-8 1.08E-03 3 0.102 3,791 S12E 62.86 908.17 Fractured Rock
MW-9S 7.45E-04 3 0.089 2,285 S17E 34.96 917.87 Fractured Rock
MW-9D 1.07E-05 3 --S19E 36.93 915.54 Fractured Rock
MW-10 1.43E-04 3 0.065 320 S00W 31.47 938.77 Fractured Rock
MW-11S 6.19E-05 3 0.118 251 S23W 30.97 938.12 Fractured Rock
MW-11D 3 ---37.35 933.49 Fractured Rock
MW-12 1.91E-06 3 0.173 11 S24W 51.86 944.8 Fractured Rock
MW-13 2.71E-03 3 0.138 12,898 S36W 26.86 956.27 Fractured Rock
P2-12 5.91E-07 3 0.515 10 S19W 53.31 933.3 Fractured Rock
MLW-A 3 0.078 -N39E 82.71 1012.8 Fractured Rock
Minimum 5.91E-07 3 0.047 10 -5.15 908.17 -
Average 4.39E-04 3 0.125 937 -39.19 943.76 -
Maximum 2.71E-03 3 0.515 3,791 -82.71 1062.27 -
NOTE: Hydraulic conductivity and effective porosity values derived from slug tests performed by MESCO.
Flow rate for MW-13 was considered an outlier; therefore not included in the average or maximum.
where
Monitoring
Location
Hydraulic
Conductivity
(cm/sec)
Effective
Porosity
Hydraulic
Gradient Flow
Direction
Depth to
Groundwater
Groundwater
Potentiometric
Elevation
(feet btoc)(feet amsl)
na
na
Hydrologic gradient from water levels recorded on May 29, 2015.
Flow rate (Q) is defined by modified Darcy's equation:
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
dl
dh
n
KQ
e
-=
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
June 18, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92252472
92252472
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY CO LINED MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 46
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 46
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92252472001 MW-1 Water 05/29/15 08:20 06/02/15 16:30
92252472002 MW-2 Water 05/29/15 15:35 06/02/15 16:30
92252472003 MW-3R Water 05/29/15 15:00 06/02/15 16:30
92252472004 MW-4S Water 05/29/15 09:00 06/02/15 16:30
92252472005 MW-4D Water 05/29/15 09:35 06/02/15 16:30
92252472006 MW-5 Water 05/29/15 16:50 06/02/15 16:30
92252472007 MW-6R Water 05/29/15 16:10 06/02/15 16:30
92252472008 MW-8 Water 05/29/15 13:35 06/02/15 16:30
92252472009 MW-9S Water 05/29/15 14:25 06/02/15 16:30
92252472010 MW-9D Water 05/29/15 14:00 06/02/15 16:30
92252472011 MW-10 Water 05/29/15 10:00 06/02/15 16:30
92252472012 MW-11S Water 05/29/15 11:00 06/02/15 16:30
92252472013 MW-11D Water 05/29/15 10:30 06/02/15 16:30
92252472014 MW-12 Water 05/29/15 11:35 06/02/15 16:30
92252472015 MW-13 Water 05/29/15 12:00 06/02/15 16:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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[phone]
Page 3 of 46
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92252472001 MW-1 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472002 MW-2 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472003 MW-3R EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472004 MW-4S EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472005 MW-4D EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472006 MW-5 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472007 MW-6R EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472008 MW-8 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472009 MW-9S EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472010 MW-9D EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472011 MW-10 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472012 MW-11S EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472013 MW-11D EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472014 MW-12 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252472015 MW-13 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-1 Lab ID:92252472001 Collected:05/29/15 08:20 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 17:22 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 17:22 7440-38-206/03/15 17:1510.0 2.5 1
Barium 55.1J ug/L 06/04/15 17:22 7440-39-306/03/15 17:151002.5 1
Beryllium 0.68J ug/L 06/04/15 17:22 7440-41-706/03/15 17:151.0 0.50 1
Cadmium 1.0 ug/L 06/04/15 17:22 7440-43-906/03/15 17:151.0 0.50 1
Chromium 10.6 ug/L 06/04/15 17:22 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt 9.2J ug/L 06/04/15 17:22 7440-48-406/03/15 17:1510.0 2.5 1
Copper 20.7 ug/L 06/04/15 17:22 7440-50-806/03/15 17:1510.0 2.5 1
Lead 4.6J ug/L 06/04/15 17:22 7439-92-106/03/15 17:1510.0 2.5 1
Nickel 17.6J ug/L 06/04/15 17:22 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 17:22 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 17:22 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 17:22 7440-28-006/03/15 17:155.5 5.0 1
Vanadium 9.0J ug/L 06/04/15 17:22 7440-62-206/03/15 17:1525.0 2.5 1
Zinc 36.4 ug/L 06/04/15 17:22 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 00:33 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 00:33 107-13-12001.9 1
Benzene ND ug/L 06/12/15 00:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 00:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 00:33 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 00:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 00:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 00:33 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 00:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 00:33 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 00:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 00:33 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 00:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 00:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 00:33 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 00:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 00:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 00:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 00:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 00:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 00:33 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 00:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 00:33 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 00:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 00:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 00:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 00:33 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 00:33 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 00:33 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-1 Lab ID:92252472001 Collected:05/29/15 08:20 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 00:33 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 00:33 100-41-41.0 0.30 1
2-Hexanone 0.47J ug/L 06/12/15 00:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 00:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 00:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 00:33 108-10-11000.33 1
Styrene ND ug/L 06/12/15 00:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 00:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 00:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 00:33 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 00:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 00:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 00:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 00:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 00:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 00:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 00:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 00:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 00:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %06/12/15 00:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %06/12/15 00:33 17060-07-070-130 1
Toluene-d8 (S)99 %06/12/15 00:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-2 Lab ID:92252472002 Collected:05/29/15 15:35 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 17:26 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 17:26 7440-38-206/03/15 17:1510.0 2.5 1
Barium 31.7J ug/L 06/04/15 17:26 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 17:26 7440-41-706/03/15 17:151.0 0.50 1
Cadmium 0.69J ug/L 06/04/15 17:26 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 17:26 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 17:26 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 17:26 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 17:26 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 17:26 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 17:26 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 17:26 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 17:26 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 17:26 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 17:26 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 00:51 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 00:51 107-13-12001.9 1
Benzene ND ug/L 06/12/15 00:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 00:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 00:51 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 00:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 00:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 00:51 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 00:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 00:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 00:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 00:51 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 00:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 00:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 00:51 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 00:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 00:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 00:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 00:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 00:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 00:51 110-57-61001.0 1
1,1-Dichloroethane 3.8J ug/L 06/12/15 00:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 00:51 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 00:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.4J ug/L 06/12/15 00:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 00:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 00:51 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 00:51 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 00:51 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-2 Lab ID:92252472002 Collected:05/29/15 15:35 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 00:51 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 00:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 00:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 00:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 00:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 00:51 108-10-11000.33 1
Styrene ND ug/L 06/12/15 00:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 00:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 00:51 79-34-53.0 0.40 1
Tetrachloroethene 1.0 ug/L 06/12/15 00:51 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 00:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 00:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 00:51 79-00-51.0 0.29 1
Trichloroethene 0.63J ug/L 06/12/15 00:51 79-01-61.0 0.47 1
Trichlorofluoromethane 0.32J ug/L 06/12/15 00:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 00:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 00:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 00:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 00:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/12/15 00:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %06/12/15 00:51 17060-07-070-130 1
Toluene-d8 (S)100 %06/12/15 00:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-3R Lab ID:92252472003 Collected:05/29/15 15:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 17:29 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 17:29 7440-38-206/03/15 17:1510.0 2.5 1
Barium 50.4J ug/L 06/04/15 17:29 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 17:29 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 17:29 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 17:29 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 17:29 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 17:29 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 17:29 7439-92-106/03/15 17:1510.0 2.5 1
Nickel 2.5J ug/L 06/04/15 17:29 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 17:29 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 17:29 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 17:29 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 17:29 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 17:29 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 01:09 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 01:09 107-13-12001.9 1
Benzene ND ug/L 06/12/15 01:09 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 01:09 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 01:09 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 01:09 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 01:09 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 01:09 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 01:09 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 01:09 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 01:09 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 01:09 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 01:09 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 01:09 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 01:09 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 01:09 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 01:09 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 01:09 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 01:09 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 01:09 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 01:09 110-57-61001.0 1
1,1-Dichloroethane 3.1J ug/L 06/12/15 01:09 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 01:09 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 01:09 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 3.5J ug/L 06/12/15 01:09 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 01:09 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 01:09 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 01:09 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 01:09 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-3R Lab ID:92252472003 Collected:05/29/15 15:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 01:09 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 01:09 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 01:09 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 01:09 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 01:09 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 01:09 108-10-11000.33 1
Styrene ND ug/L 06/12/15 01:09 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 01:09 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 01:09 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 01:09 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 01:09 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 01:09 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 01:09 79-00-51.0 0.29 1
Trichloroethene 0.60J ug/L 06/12/15 01:09 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 01:09 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 01:09 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 01:09 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 01:09 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 01:09 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %06/12/15 01:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %06/12/15 01:09 17060-07-070-130 1
Toluene-d8 (S)100 %06/12/15 01:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-4S Lab ID:92252472004 Collected:05/29/15 09:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 17:32 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 17:32 7440-38-206/03/15 17:1510.0 2.5 1
Barium 88.2J ug/L 06/04/15 17:32 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 17:32 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 17:32 7440-43-906/03/15 17:151.0 0.50 1
Chromium 4.8J ug/L 06/04/15 17:32 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt 8.0J ug/L 06/04/15 17:32 7440-48-406/03/15 17:1510.0 2.5 1
Copper 5.7J ug/L 06/04/15 17:32 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 17:32 7439-92-106/03/15 17:1510.0 2.5 1
Nickel 3.3J ug/L 06/04/15 17:32 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 17:32 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 17:32 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 17:32 7440-28-006/03/15 17:155.5 5.0 1
Vanadium 7.8J ug/L 06/04/15 17:32 7440-62-206/03/15 17:1525.0 2.5 1
Zinc 12.9 ug/L 06/04/15 17:32 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 01:27 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 01:27 107-13-12001.9 1
Benzene ND ug/L 06/12/15 01:27 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 01:27 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 01:27 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 01:27 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 01:27 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 01:27 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 01:27 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 01:27 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 01:27 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 01:27 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 01:27 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 01:27 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 01:27 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 01:27 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 01:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 01:27 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 01:27 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 01:27 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 01:27 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 01:27 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 01:27 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 01:27 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 01:27 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 01:27 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 01:27 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 01:27 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 01:27 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-4S Lab ID:92252472004 Collected:05/29/15 09:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 01:27 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 01:27 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 01:27 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 01:27 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 01:27 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 01:27 108-10-11000.33 1
Styrene ND ug/L 06/12/15 01:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 01:27 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 01:27 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 01:27 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 01:27 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 01:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 01:27 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 01:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 01:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 01:27 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 01:27 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 01:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 01:27 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %06/12/15 01:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %06/12/15 01:27 17060-07-070-130 1
Toluene-d8 (S)99 %06/12/15 01:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-4D Lab ID:92252472005 Collected:05/29/15 09:35 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 17:35 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 17:35 7440-38-206/03/15 17:1510.0 2.5 1
Barium 36.4J ug/L 06/04/15 17:35 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 17:35 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 17:35 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 17:35 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 17:35 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 17:35 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 17:35 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 17:35 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 17:35 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 17:35 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 17:35 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 17:35 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 17:35 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 01:46 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 01:46 107-13-12001.9 1
Benzene ND ug/L 06/12/15 01:46 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 01:46 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 01:46 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 01:46 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 01:46 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 01:46 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 01:46 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 01:46 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 01:46 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 01:46 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 01:46 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 01:46 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 01:46 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 01:46 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 01:46 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 01:46 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 01:46 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 01:46 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 01:46 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 01:46 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 01:46 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 01:46 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 01:46 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 01:46 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 01:46 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 01:46 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 01:46 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-4D Lab ID:92252472005 Collected:05/29/15 09:35 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 01:46 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 01:46 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 01:46 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 01:46 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 01:46 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 01:46 108-10-11000.33 1
Styrene ND ug/L 06/12/15 01:46 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 01:46 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 01:46 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 01:46 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 01:46 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 01:46 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 01:46 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 01:46 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 01:46 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 01:46 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 01:46 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 01:46 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 01:46 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %06/12/15 01:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %06/12/15 01:46 17060-07-070-130 1
Toluene-d8 (S)99 %06/12/15 01:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-5 Lab ID:92252472006 Collected:05/29/15 16:50 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 17:47 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 17:47 7440-38-206/03/15 17:1510.0 2.5 1
Barium 39.3J ug/L 06/04/15 17:47 7440-39-306/03/15 17:151002.5 1
Beryllium 0.56J ug/L 06/04/15 17:47 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 17:47 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 17:47 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 17:47 7440-48-406/03/15 17:1510.0 2.5 1
Copper 33.3 ug/L 06/04/15 17:47 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 17:47 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 17:47 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 17:47 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 17:47 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 17:47 7440-28-006/03/15 17:155.5 5.0 1
Vanadium 2.8J ug/L 06/04/15 17:47 7440-62-206/03/15 17:1525.0 2.5 1
Zinc 12.0 ug/L 06/04/15 17:47 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 02:04 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 02:04 107-13-12001.9 1
Benzene ND ug/L 06/12/15 02:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 02:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 02:04 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 02:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 02:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 02:04 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 02:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 02:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 02:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 02:04 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 02:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 02:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 02:04 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 02:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 02:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 02:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 02:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 02:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 02:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 02:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 02:04 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 02:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.41J ug/L 06/12/15 02:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 02:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 02:04 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 02:04 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 02:04 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-5 Lab ID:92252472006 Collected:05/29/15 16:50 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 02:04 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 02:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 02:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 02:04 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 02:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 02:04 108-10-11000.33 1
Styrene ND ug/L 06/12/15 02:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 02:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 02:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 02:04 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 02:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 02:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 02:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 02:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 02:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 02:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 02:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 02:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 02:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %06/12/15 02:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %06/12/15 02:04 17060-07-070-130 1
Toluene-d8 (S)101 %06/12/15 02:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-6R Lab ID:92252472007 Collected:05/29/15 16:10 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 17:50 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 17:50 7440-38-206/03/15 17:1510.0 2.5 1
Barium 46.0J ug/L 06/04/15 17:50 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 17:50 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 17:50 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 17:50 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 17:50 7440-48-406/03/15 17:1510.0 2.5 1
Copper 3.4J ug/L 06/04/15 17:50 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 17:50 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 17:50 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 17:50 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 17:50 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 17:50 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 17:50 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 17:50 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 02:22 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 02:22 107-13-12001.9 1
Benzene 0.34J ug/L 06/12/15 02:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 02:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 02:22 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 02:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 02:22 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 02:22 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 02:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 02:22 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 02:22 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 02:22 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 02:22 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 02:22 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 02:22 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 02:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 02:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 02:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 02:22 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 02:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 02:22 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 02:22 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 02:22 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 02:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.5J ug/L 06/12/15 02:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 02:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 02:22 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 02:22 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 02:22 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-6R Lab ID:92252472007 Collected:05/29/15 16:10 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 02:22 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 02:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 02:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 02:22 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 02:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 02:22 108-10-11000.33 1
Styrene ND ug/L 06/12/15 02:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 02:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 02:22 79-34-53.0 0.40 1
Tetrachloroethene 0.73J ug/L 06/12/15 02:22 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 02:22 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 02:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 02:22 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 02:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 02:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 02:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 02:22 108-05-450.0 0.35 1
Vinyl chloride 0.80J ug/L 06/12/15 02:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 02:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/12/15 02:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %06/12/15 02:22 17060-07-070-130 1
Toluene-d8 (S)99 %06/12/15 02:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-8 Lab ID:92252472008 Collected:05/29/15 13:35 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 17:53 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 17:53 7440-38-206/03/15 17:1510.0 2.5 1
Barium 46.1J ug/L 06/04/15 17:53 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 17:53 7440-41-706/03/15 17:151.0 0.50 1
Cadmium 0.59J ug/L 06/04/15 17:53 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 17:53 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 17:53 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 17:53 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 17:53 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 17:53 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 17:53 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 17:53 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 17:53 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 17:53 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 17:53 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 02:40 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 02:40 107-13-12001.9 1
Benzene ND ug/L 06/12/15 02:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 02:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 02:40 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 02:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 02:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 02:40 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 02:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 02:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 02:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 02:40 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 02:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 02:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 02:40 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 02:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 02:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 02:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 02:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 02:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 02:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 02:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 02:40 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 02:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 02:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 02:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 02:40 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 02:40 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 02:40 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-8 Lab ID:92252472008 Collected:05/29/15 13:35 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 02:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 02:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 02:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 02:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 02:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 02:40 108-10-11000.33 1
Styrene ND ug/L 06/12/15 02:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 02:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 02:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 02:40 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 02:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 02:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 02:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 02:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 02:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 02:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 02:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 02:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 02:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/12/15 02:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %06/12/15 02:40 17060-07-070-130 1
Toluene-d8 (S)100 %06/12/15 02:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-9S Lab ID:92252472009 Collected:05/29/15 14:25 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 17:57 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 17:57 7440-38-206/03/15 17:1510.0 2.5 1
Barium 47.0J ug/L 06/04/15 17:57 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 17:57 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 17:57 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 17:57 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt 31.8 ug/L 06/04/15 17:57 7440-48-406/03/15 17:1510.0 2.5 1
Copper 6.7J ug/L 06/04/15 17:57 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 17:57 7439-92-106/03/15 17:1510.0 2.5 1
Nickel 6.3J ug/L 06/04/15 17:57 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 17:57 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 17:57 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 17:57 7440-28-006/03/15 17:155.5 5.0 1
Vanadium 8.7J ug/L 06/04/15 17:57 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 17:57 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 02:58 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 02:58 107-13-12001.9 1
Benzene 0.47J ug/L 06/12/15 02:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 02:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 02:58 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 02:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 02:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 02:58 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 02:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 02:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 02:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 02:58 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 02:58 67-66-35.0 0.14 1
Chloromethane 0.29J ug/L 06/12/15 02:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 02:58 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 02:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 02:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 02:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 02:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 02:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 02:58 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 02:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 02:58 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 02:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 6.5 ug/L 06/12/15 02:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene 0.52J ug/L 06/12/15 02:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 02:58 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 02:58 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 02:58 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-9S Lab ID:92252472009 Collected:05/29/15 14:25 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 02:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 02:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 02:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 02:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 02:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 02:58 108-10-11000.33 1
Styrene ND ug/L 06/12/15 02:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 02:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 02:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 02:58 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 02:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 02:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 02:58 79-00-51.0 0.29 1
Trichloroethene 1.3 ug/L 06/12/15 02:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 02:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 02:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 02:58 108-05-450.0 0.35 1
Vinyl chloride 0.67J ug/L 06/12/15 02:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 02:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/12/15 02:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %06/12/15 02:58 17060-07-070-130 1
Toluene-d8 (S)101 %06/12/15 02:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-9D Lab ID:92252472010 Collected:05/29/15 14:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 18:00 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 18:00 7440-38-206/03/15 17:1510.0 2.5 1
Barium 42.0J ug/L 06/04/15 18:00 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 18:00 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 18:00 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 18:00 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 18:00 7440-48-406/03/15 17:1510.0 2.5 1
Copper 10.3 ug/L 06/04/15 18:00 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 18:00 7439-92-106/03/15 17:1510.0 2.5 1
Nickel 2.6J ug/L 06/04/15 18:00 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 18:00 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 18:00 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 18:00 7440-28-006/03/15 17:155.5 5.0 1
Vanadium 3.7J ug/L 06/04/15 18:00 7440-62-206/03/15 17:1525.0 2.5 1
Zinc 19.2 ug/L 06/04/15 18:00 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 03:16 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 03:16 107-13-12001.9 1
Benzene 0.26J ug/L 06/12/15 03:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 03:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 03:16 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 03:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 03:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 03:16 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 03:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 03:16 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 03:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 03:16 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 03:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 03:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 03:16 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 03:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 03:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 03:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 03:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 03:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 03:16 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 03:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 03:16 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 03:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.8J ug/L 06/12/15 03:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 03:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 03:16 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 03:16 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 03:16 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-9D Lab ID:92252472010 Collected:05/29/15 14:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 03:16 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 03:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 03:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 03:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 03:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 03:16 108-10-11000.33 1
Styrene ND ug/L 06/12/15 03:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 03:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 03:16 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 03:16 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 03:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 03:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 03:16 79-00-51.0 0.29 1
Trichloroethene 0.64J ug/L 06/12/15 03:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 03:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 03:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 03:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 03:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 03:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/12/15 03:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %06/12/15 03:16 17060-07-070-130 1
Toluene-d8 (S)100 %06/12/15 03:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-10 Lab ID:92252472011 Collected:05/29/15 10:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 18:03 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 18:03 7440-38-206/03/15 17:1510.0 2.5 1
Barium 33.1J ug/L 06/04/15 18:03 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 18:03 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 18:03 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 18:03 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 18:03 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 18:03 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 18:03 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 18:03 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 18:03 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 18:03 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 18:03 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 18:03 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 18:03 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 03:35 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 03:35 107-13-12001.9 1
Benzene ND ug/L 06/12/15 03:35 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 03:35 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 03:35 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 03:35 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 03:35 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 03:35 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 03:35 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 03:35 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 03:35 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 03:35 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 03:35 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 03:35 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 03:35 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 03:35 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 03:35 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 03:35 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 03:35 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 03:35 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 03:35 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 03:35 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 03:35 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 03:35 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.26J ug/L 06/12/15 03:35 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 03:35 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 03:35 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 03:35 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 03:35 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-10 Lab ID:92252472011 Collected:05/29/15 10:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 03:35 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 03:35 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 03:35 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 03:35 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 03:35 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 03:35 108-10-11000.33 1
Styrene ND ug/L 06/12/15 03:35 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 03:35 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 03:35 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 03:35 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 03:35 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 03:35 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 03:35 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 03:35 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 03:35 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 03:35 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 03:35 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 03:35 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 03:35 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %06/12/15 03:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %06/12/15 03:35 17060-07-070-130 1
Toluene-d8 (S)100 %06/12/15 03:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-11S Lab ID:92252472012 Collected:05/29/15 11:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 18:06 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 18:06 7440-38-206/03/15 17:1510.0 2.5 1
Barium 11.1J ug/L 06/04/15 18:06 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 18:06 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 18:06 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 18:06 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 18:06 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 18:06 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 18:06 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 18:06 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 18:06 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 18:06 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 18:06 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 18:06 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 18:06 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 03:53 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 03:53 107-13-12001.9 1
Benzene ND ug/L 06/12/15 03:53 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 03:53 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 03:53 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 03:53 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 03:53 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 03:53 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 03:53 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 03:53 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 03:53 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 03:53 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 03:53 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 03:53 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 03:53 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 03:53 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 03:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 03:53 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 03:53 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 03:53 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 03:53 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 03:53 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 03:53 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 03:53 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 03:53 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 03:53 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 03:53 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 03:53 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 03:53 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-11S Lab ID:92252472012 Collected:05/29/15 11:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 03:53 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 03:53 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 03:53 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 03:53 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 03:53 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 03:53 108-10-11000.33 1
Styrene ND ug/L 06/12/15 03:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 03:53 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 03:53 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 03:53 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 03:53 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 03:53 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 03:53 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 03:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 03:53 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 03:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 03:53 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 03:53 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 03:53 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %06/12/15 03:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %06/12/15 03:53 17060-07-070-130 1
Toluene-d8 (S)101 %06/12/15 03:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-11D Lab ID:92252472013 Collected:05/29/15 10:30 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony 4.6J ug/L 06/04/15 18:09 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 18:09 7440-38-206/03/15 17:1510.0 2.5 1
Barium ND ug/L 06/04/15 18:09 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 18:09 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 18:09 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 18:09 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 18:09 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 18:09 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 18:09 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 18:09 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 18:09 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 18:09 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 18:09 7440-28-006/03/15 17:155.5 5.0 1
Vanadium 7.8J ug/L 06/04/15 18:09 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 18:09 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 04:11 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 04:11 107-13-12001.9 1
Benzene ND ug/L 06/12/15 04:11 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 04:11 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 04:11 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 04:11 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 04:11 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 04:11 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 04:11 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 04:11 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 04:11 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 04:11 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 04:11 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 04:11 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 04:11 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 04:11 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 04:11 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 04:11 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 04:11 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 04:11 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 04:11 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 04:11 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 04:11 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 04:11 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 04:11 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 04:11 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 04:11 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 04:11 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 04:11 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-11D Lab ID:92252472013 Collected:05/29/15 10:30 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 04:11 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 04:11 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 04:11 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 04:11 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 04:11 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 04:11 108-10-11000.33 1
Styrene ND ug/L 06/12/15 04:11 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 04:11 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 04:11 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 04:11 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 04:11 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 04:11 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 04:11 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 04:11 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 04:11 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 04:11 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 04:11 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 04:11 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 04:11 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/12/15 04:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %06/12/15 04:11 17060-07-070-130 1
Toluene-d8 (S)101 %06/12/15 04:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-12 Lab ID:92252472014 Collected:05/29/15 11:35 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 18:12 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 18:12 7440-38-206/03/15 17:1510.0 2.5 1
Barium 14.7J ug/L 06/04/15 18:12 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 18:12 7440-41-706/03/15 17:151.0 0.50 1
Cadmium 1.2 ug/L 06/04/15 18:12 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 18:12 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 18:12 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 18:12 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 18:12 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 18:12 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 18:12 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 18:12 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 18:12 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 18:12 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 18:12 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 04:30 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 04:30 107-13-12001.9 1
Benzene ND ug/L 06/12/15 04:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 04:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 04:30 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 04:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 04:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 04:30 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 04:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 04:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 04:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 04:30 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 04:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 04:30 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 04:30 96-12-8 L113.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 04:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 04:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 04:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 04:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 04:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 04:30 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 04:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 04:30 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 04:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 04:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 04:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 04:30 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 04:30 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 04:30 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-12 Lab ID:92252472014 Collected:05/29/15 11:35 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 04:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 04:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 04:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 04:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 04:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 04:30 108-10-11000.33 1
Styrene ND ug/L 06/12/15 04:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 04:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 04:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 04:30 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 04:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 04:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 04:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 04:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 04:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 04:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 04:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 04:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 04:30 1330-20-7 LS5.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/12/15 04:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %06/12/15 04:30 17060-07-070-130 1
Toluene-d8 (S)100 %06/12/15 04:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-13 Lab ID:92252472015 Collected:05/29/15 12:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 18:15 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 18:15 7440-38-206/03/15 17:1510.0 2.5 1
Barium 25.3J ug/L 06/04/15 18:15 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 18:15 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 18:15 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 18:15 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 18:15 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 18:15 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 18:15 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 18:15 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 18:15 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 18:15 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 18:15 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 18:15 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 18:15 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 05:06 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 05:06 107-13-12001.9 1
Benzene ND ug/L 06/12/15 05:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 05:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 05:06 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 05:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 05:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 05:06 78-93-3 M11000.96 1
Carbon disulfide ND ug/L 06/12/15 05:06 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 05:06 56-23-5 M11.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 05:06 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 05:06 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 05:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 05:06 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 05:06 96-12-8 L1,M013.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 05:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 05:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 05:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 05:06 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 05:06 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 05:06 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 05:06 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 05:06 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 05:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 05:06 156-59-2 M15.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 05:06 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 05:06 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 05:06 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 05:06 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
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Page 33 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Sample:MW-13 Lab ID:92252472015 Collected:05/29/15 12:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 05:06 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 05:06 100-41-4 M11.0 0.30 1
2-Hexanone ND ug/L 06/12/15 05:06 591-78-6 M150.0 0.46 1
Iodomethane ND ug/L 06/12/15 05:06 74-88-4 M110.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 05:06 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 05:06 108-10-11000.33 1
Styrene ND ug/L 06/12/15 05:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 05:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 05:06 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 05:06 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 05:06 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 05:06 71-55-6 M11.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 05:06 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 05:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 05:06 75-69-4 M11.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 05:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 05:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 05:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 05:06 1330-20-7 LS,MS5.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/12/15 05:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %06/12/15 05:06 17060-07-070-130 1
Toluene-d8 (S)99 %06/12/15 05:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18607
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92252472001, 92252472002, 92252472003, 92252472004, 92252472005, 92252472006, 92252472007,
92252472008, 92252472009, 92252472010, 92252472011, 92252472012, 92252472013, 92252472014,
92252472015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1474278
Associated Lab Samples:92252472001, 92252472002, 92252472003, 92252472004, 92252472005, 92252472006, 92252472007,
92252472008, 92252472009, 92252472010, 92252472011, 92252472012, 92252472013, 92252472014,
92252472015
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 06/04/15 17:08
Arsenic ug/L ND 10.0 06/04/15 17:08
Barium ug/L ND 100 06/04/15 17:08
Beryllium ug/L ND 1.0 06/04/15 17:08
Cadmium ug/L ND 1.0 06/04/15 17:08
Chromium ug/L ND 10.0 06/04/15 17:08
Cobalt ug/L ND 10.0 06/04/15 17:08
Copper ug/L ND 10.0 06/04/15 17:08
Lead ug/L ND 10.0 06/04/15 17:08
Nickel ug/L ND 50.0 06/04/15 17:08
Selenium ug/L ND 10.0 06/04/15 17:08
Silver ug/L ND 10.0 06/04/15 17:08
Thallium ug/L ND 5.5 06/04/15 17:08
Vanadium ug/L ND 25.0 06/04/15 17:08
Zinc ug/L ND 10.0 06/04/15 17:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1474279LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 479500 96 80-120
Arsenic ug/L 456500 91 80-120
Barium ug/L 448500 90 80-120
Beryllium ug/L 450500 90 80-120
Cadmium ug/L 454500 91 80-120
Chromium ug/L 440500 88 80-120
Cobalt ug/L 451500 90 80-120
Copper ug/L 440500 88 80-120
Lead ug/L 447500 89 80-120
Nickel ug/L 451500 90 80-120
Selenium ug/L 432500 86 80-120
Silver ug/L 224250 90 80-120
Thallium ug/L 460500 92 80-120
Vanadium ug/L 435500 87 80-120
Zinc ug/L 449500 90 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1474280MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92251954001
1474281
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 95 75-12596 1 25500ND478483
Arsenic ug/L 500 91 75-12592 1 25500ND458461
Barium ug/L 500 90 75-12591 1 2550048.4 498 504
Beryllium ug/L 500 91 75-12592 1 25500ND456461
Cadmium ug/L 500 91 75-12592 1 25500ND453458
Chromium ug/L 500 89 75-12589 1 25500ND443447
Cobalt ug/L 500 89 75-12590 1 25500ND446450
Copper ug/L 500 88 75-12589 1 2550011.6 450 454
Lead ug/L 500 88 75-12589 1 25500ND441447
Nickel ug/L 500 89 75-12590 1 255002.7J 448 452
Selenium ug/L 500 85 75-12586 0 25500ND429431
Silver ug/L 250 89 75-12590 1 25250ND223225
Thallium ug/L 500 90 75-12591 1 25500ND451456
Vanadium ug/L 500 87 75-12589 2 25500ND438445
Zinc ug/L 500 89 75-12590 1 2550028.6 473 477
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32101
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92252472001, 92252472002, 92252472003, 92252472004, 92252472005, 92252472006, 92252472007,
92252472008, 92252472009, 92252472010, 92252472011, 92252472012, 92252472013, 92252472014,
92252472015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1482649
Associated Lab Samples:92252472001, 92252472002, 92252472003, 92252472004, 92252472005, 92252472006, 92252472007,
92252472008, 92252472009, 92252472010, 92252472011, 92252472012, 92252472013, 92252472014,
92252472015
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/12/15 00:14
1,1,1-Trichloroethane ug/L ND 1.0 06/12/15 00:14
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/12/15 00:14
1,1,2-Trichloroethane ug/L ND 1.0 06/12/15 00:14
1,1-Dichloroethane ug/L ND 5.0 06/12/15 00:14
1,1-Dichloroethene ug/L ND 5.0 06/12/15 00:14
1,2,3-Trichloropropane ug/L ND 1.0 06/12/15 00:14
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/12/15 00:14
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/12/15 00:14
1,2-Dichlorobenzene ug/L ND 5.0 06/12/15 00:14
1,2-Dichloroethane ug/L ND 1.0 06/12/15 00:14
1,2-Dichloropropane ug/L ND 1.0 06/12/15 00:14
1,3-Dichloropropane ug/L ND 1.0 06/12/15 00:14
1,4-Dichlorobenzene ug/L ND 1.0 06/12/15 00:14
2-Butanone (MEK)ug/L ND 100 06/12/15 00:14
2-Hexanone ug/L ND 50.0 06/12/15 00:14
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/12/15 00:14
Acetone ug/L ND 100 06/12/15 00:14
Acrylonitrile ug/L ND 200 06/12/15 00:14
Benzene ug/L ND 1.0 06/12/15 00:14
Bromochloromethane ug/L ND 3.0 06/12/15 00:14
Bromodichloromethane ug/L ND 1.0 06/12/15 00:14
Bromoform ug/L ND 3.0 06/12/15 00:14
Bromomethane ug/L ND 10.0 06/12/15 00:14
Carbon disulfide ug/L ND 100 06/12/15 00:14
Carbon tetrachloride ug/L ND 1.0 06/12/15 00:14
Chlorobenzene ug/L ND 3.0 06/12/15 00:14
Chloroethane ug/L ND 10.0 06/12/15 00:14
Chloroform ug/L ND 5.0 06/12/15 00:14
Chloromethane ug/L ND 1.0 06/12/15 00:14
cis-1,2-Dichloroethene ug/L ND 5.0 06/12/15 00:14
cis-1,3-Dichloropropene ug/L ND 1.0 06/12/15 00:14
Dibromochloromethane ug/L ND 3.0 06/12/15 00:14
Dibromomethane ug/L ND 10.0 06/12/15 00:14
Ethylbenzene ug/L ND 1.0 06/12/15 00:14
Iodomethane ug/L ND 10.0 06/12/15 00:14
Methylene Chloride ug/L ND 1.0 06/12/15 00:14
Styrene ug/L ND 1.0 06/12/15 00:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1482649
Associated Lab Samples:92252472001, 92252472002, 92252472003, 92252472004, 92252472005, 92252472006, 92252472007,
92252472008, 92252472009, 92252472010, 92252472011, 92252472012, 92252472013, 92252472014,
92252472015
Matrix:Water
Analyzed
Tetrachloroethene ug/L ND 1.0 06/12/15 00:14
Toluene ug/L ND 1.0 06/12/15 00:14
trans-1,2-Dichloroethene ug/L ND 5.0 06/12/15 00:14
trans-1,3-Dichloropropene ug/L ND 1.0 06/12/15 00:14
trans-1,4-Dichloro-2-butene ug/L ND 100 06/12/15 00:14
Trichloroethene ug/L ND 1.0 06/12/15 00:14
Trichlorofluoromethane ug/L ND 1.0 06/12/15 00:14
Vinyl acetate ug/L ND 50.0 06/12/15 00:14
Vinyl chloride ug/L ND 1.0 06/12/15 00:14
Xylene (Total)ug/L ND 5.0 06/12/15 00:14
1,2-Dichloroethane-d4 (S)%111 70-130 06/12/15 00:14
4-Bromofluorobenzene (S)%101 70-130 06/12/15 00:14
Toluene-d8 (S)%105 70-130 06/12/15 00:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1482650LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 58.650 117 80-125
1,1,1-Trichloroethane ug/L 61.250 122 71-129
1,1,2,2-Tetrachloroethane ug/L 58.950 118 79-124
1,1,2-Trichloroethane ug/L 59.150 118 85-125
1,1-Dichloroethane ug/L 59.250 118 73-126
1,1-Dichloroethene ug/L 54.150 108 66-135
1,2,3-Trichloropropane ug/L 61.450 123 75-130
1,2-Dibromo-3-chloropropane ug/L 67.1 L05013471-133
1,2-Dibromoethane (EDB)ug/L 61.050 122 83-124
1,2-Dichlorobenzene ug/L 58.650 117 80-133
1,2-Dichloroethane ug/L 58.250 116 67-128
1,2-Dichloropropane ug/L 59.150 118 75-132
1,3-Dichloropropane ug/L 61.450 123 76-131
1,4-Dichlorobenzene ug/L 57.450 115 78-130
2-Butanone (MEK)ug/L 119100 119 61-144
2-Hexanone ug/L 137100 137 68-143
4-Methyl-2-pentanone (MIBK)ug/L 119100 119 72-135
Acetone ug/L 127100 127 48-146
Acrylonitrile ug/L 308250 123 40-160
Benzene ug/L 60.150 120 80-125
Bromochloromethane ug/L 57.650 115 71-125
Bromodichloromethane ug/L 54.150 108 78-124
Bromoform ug/L 53.550 107 71-128
Bromomethane ug/L 56.750 113 40-160
Carbon disulfide ug/L 59.8J50 120 50-160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1482650LABORATORY CONTROL SAMPLE:
LCSSpike
Carbon tetrachloride ug/L 59.150 118 69-131
Chlorobenzene ug/L 60.350 121 81-122
Chloroethane ug/L 50.550 101 39-148
Chloroform ug/L 54.750 109 73-127
Chloromethane ug/L 49.050 98 44-146
cis-1,2-Dichloroethene ug/L 60.450 121 74-124
cis-1,3-Dichloropropene ug/L 59.650 119 72-132
Dibromochloromethane ug/L 53.050 106 78-125
Dibromomethane ug/L 58.750 117 82-120
Ethylbenzene ug/L 59.450 119 79-121
Iodomethane ug/L 105100 105 39-154
Methylene Chloride ug/L 65.650 131 64-133
Styrene ug/L 61.850 124 84-126
Tetrachloroethene ug/L 55.550 111 78-122
Toluene ug/L 57.750 115 80-121
trans-1,2-Dichloroethene ug/L 59.950 120 71-127
trans-1,3-Dichloropropene ug/L 60.850 122 69-141
trans-1,4-Dichloro-2-butene ug/L 61.7J50 123 40-160
Trichloroethene ug/L 56.350 113 78-122
Trichlorofluoromethane ug/L 53.750 107 53-137
Vinyl acetate ug/L 120100 120 40-160
Vinyl chloride ug/L 57.150 114 58-137
Xylene (Total)ug/L 190 LS15012781-126
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1482652MATRIX SPIKE SAMPLE:
MSSpike
Result
92252472015
1,1,1,2-Tetrachloroethane ug/L 25.020 125 70-130ND
1,1,1-Trichloroethane ug/L 27.4 M12013770-130ND
1,1,2,2-Tetrachloroethane ug/L 24.120 121 70-130ND
1,1,2-Trichloroethane ug/L 23.820 119 70-130ND
1,1-Dichloroethane ug/L 26.120 130 70-130ND
1,1-Dichloroethene ug/L 25.320 126 70-166ND
1,2,3-Trichloropropane ug/L 25.320 126 70-130ND
1,2-Dibromo-3-chloropropane ug/L 26.2 M02013170-130ND
1,2-Dibromoethane (EDB)ug/L 24.820 124 70-130ND
1,2-Dichlorobenzene ug/L 24.720 123 70-130ND
1,2-Dichloroethane ug/L 25.520 128 70-130ND
1,2-Dichloropropane ug/L 23.920 120 70-130ND
1,3-Dichloropropane ug/L 25.320 126 70-130ND
1,4-Dichlorobenzene ug/L 24.620 123 70-130ND
2-Butanone (MEK)ug/L 52.3J M14013170-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1482652MATRIX SPIKE SAMPLE:
MSSpike
Result
92252472015
2-Hexanone ug/L 53.6 M14013470-130ND
4-Methyl-2-pentanone (MIBK)ug/L 49.4J40 124 70-130ND
Acetone ug/L 54.3J40 128 70-130ND
Acrylonitrile ug/L 118J100 118 70-130ND
Benzene ug/L 26.020 130 70-148ND
Bromochloromethane ug/L 25.320 127 70-130ND
Bromodichloromethane ug/L 23.220 116 70-130ND
Bromoform ug/L 21.420 107 70-130ND
Bromomethane ug/L 17.320 86 70-130ND
Carbon disulfide ug/L 24.2J20 121 70-130ND
Carbon tetrachloride ug/L 28.9 M12014470-130ND
Chlorobenzene ug/L 26.020 130 70-146ND
Chloroethane ug/L 23.820 119 70-130ND
Chloroform ug/L 24.220 121 70-130ND
Chloromethane ug/L 21.120 106 70-130ND
cis-1,2-Dichloroethene ug/L 26.6 M12013370-130ND
cis-1,3-Dichloropropene ug/L 23.920 119 70-130ND
Dibromochloromethane ug/L 21.720 108 70-130ND
Dibromomethane ug/L 23.820 119 70-130ND
Ethylbenzene ug/L 26.2 M12013170-130ND
Iodomethane ug/L 26.0 M1406570-130ND
Methylene Chloride ug/L 25.820 129 70-130ND
Styrene ug/L 25.020 125 70-130ND
Tetrachloroethene ug/L 25.220 126 70-130ND
Toluene ug/L 24.720 123 70-155ND
trans-1,2-Dichloroethene ug/L 26.120 130 70-130ND
trans-1,3-Dichloropropene ug/L 24.720 123 70-130ND
trans-1,4-Dichloro-2-butene ug/L 24.3J20 121 70-130ND
Trichloroethene ug/L 24.920 124 69-151ND
Trichlorofluoromethane ug/L 27.8 M12013970-130ND
Vinyl acetate ug/L 39.3J40 98 70-130ND
Vinyl chloride ug/L 24.420 122 70-130ND
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92252472014
1482651SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
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Page 40 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92252472014
1482651SAMPLE DUPLICATE:
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%113 3109
4-Bromofluorobenzene (S)%100 4103
Toluene-d8 (S)%100 1100
REPORT OF LABORATORY ANALYSIS
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Page 41 of 46
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was outside QC limits for one or more of the constituent analytes
used in the calculated result.LS
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
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Page 42 of 46
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92252472
SURRY CO LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92252472001 MPRP/18607 ICP/16689MW-1 EPA 3010 EPA 6010
92252472002 MPRP/18607 ICP/16689MW-2 EPA 3010 EPA 6010
92252472003 MPRP/18607 ICP/16689MW-3R EPA 3010 EPA 6010
92252472004 MPRP/18607 ICP/16689MW-4S EPA 3010 EPA 6010
92252472005 MPRP/18607 ICP/16689MW-4D EPA 3010 EPA 6010
92252472006 MPRP/18607 ICP/16689MW-5 EPA 3010 EPA 6010
92252472007 MPRP/18607 ICP/16689MW-6R EPA 3010 EPA 6010
92252472008 MPRP/18607 ICP/16689MW-8 EPA 3010 EPA 6010
92252472009 MPRP/18607 ICP/16689MW-9S EPA 3010 EPA 6010
92252472010 MPRP/18607 ICP/16689MW-9D EPA 3010 EPA 6010
92252472011 MPRP/18607 ICP/16689MW-10 EPA 3010 EPA 6010
92252472012 MPRP/18607 ICP/16689MW-11S EPA 3010 EPA 6010
92252472013 MPRP/18607 ICP/16689MW-11D EPA 3010 EPA 6010
92252472014 MPRP/18607 ICP/16689MW-12 EPA 3010 EPA 6010
92252472015 MPRP/18607 ICP/16689MW-13 EPA 3010 EPA 6010
92252472001 MSV/32101MW-1 EPA 8260
92252472002 MSV/32101MW-2 EPA 8260
92252472003 MSV/32101MW-3R EPA 8260
92252472004 MSV/32101MW-4S EPA 8260
92252472005 MSV/32101MW-4D EPA 8260
92252472006 MSV/32101MW-5 EPA 8260
92252472007 MSV/32101MW-6R EPA 8260
92252472008 MSV/32101MW-8 EPA 8260
92252472009 MSV/32101MW-9S EPA 8260
92252472010 MSV/32101MW-9D EPA 8260
92252472011 MSV/32101MW-10 EPA 8260
92252472012 MSV/32101MW-11S EPA 8260
92252472013 MSV/32101MW-11D EPA 8260
92252472014 MSV/32101MW-12 EPA 8260
92252472015 MSV/32101MW-13 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/18/2015 05:44 PM
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Page 43 of 46
Page 44 of 46
Page 45 of 46
Page 46 of 46
#=CL#
June 12, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92252038
92252038
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY CO LINED
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92252038
SURRY CO LINED
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 23
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92252038
SURRY CO LINED
Lab ID Sample ID Matrix Date Collected Date Received
92252038001 LAGOON Water 05/28/15 18:20 05/29/15 13:00
REPORT OF LABORATORY ANALYSIS
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Page 3 of 23
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92252038
SURRY CO LINED
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92252038001 LAGOON EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
SM 5210B 1 PASI-ABRJ
EPA 9040 1 PASI-AMLS
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-ADMN
EPA 365.1 1 PASI-AJDA
SM 5220D 1 PASI-AMAB
REPORT OF LABORATORY ANALYSIS
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Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252038
SURRY CO LINED
Sample:LAGOON Lab ID:92252038001 Collected:05/28/15 18:20 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 23:50 7440-36-006/02/15 23:306.0 3.8 1
Arsenic ND ug/L 06/04/15 23:50 7440-38-206/02/15 23:3010.0 2.5 1
Barium 179 ug/L 06/04/15 23:50 7440-39-306/02/15 23:301002.5 1
Beryllium ND ug/L 06/04/15 23:50 7440-41-706/02/15 23:301.0 0.50 1
Cadmium ND ug/L 06/04/15 23:50 7440-43-906/02/15 23:301.0 0.50 1
Chromium 3.8J ug/L 06/04/15 23:50 7440-47-306/02/15 23:3010.0 2.5 1
Cobalt 9.0J ug/L 06/04/15 23:50 7440-48-406/02/15 23:3010.0 2.5 1
Copper ND ug/L 06/04/15 23:50 7440-50-806/02/15 23:3010.0 2.5 1
Lead 4.7J ug/L 06/04/15 23:50 7439-92-106/02/15 23:3010.0 2.5 1
Nickel 3.3J ug/L 06/04/15 23:50 7440-02-006/02/15 23:3050.0 2.5 1
Selenium ND ug/L 06/04/15 23:50 7782-49-206/02/15 23:3010.0 5.0 1
Silver 4.7J ug/L 06/04/15 23:50 7440-22-406/02/15 23:3010.0 2.5 1
Thallium 6.9 ug/L 06/04/15 23:50 7440-28-006/02/15 23:305.5 5.0 1
Vanadium 21.0J ug/L 06/04/15 23:50 7440-62-206/02/15 23:3025.0 2.5 1
Zinc 6.5J ug/L 06/04/15 23:50 7440-66-606/02/15 23:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 12.5J ug/L 06/04/15 19:44 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/15 19:44 107-13-12001.9 1
Benzene ND ug/L 06/04/15 19:44 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/15 19:44 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/15 19:44 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/15 19:44 75-25-2 L23.0 0.26 1
Bromomethane 1.1J ug/L 06/04/15 19:44 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/15 19:44 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/15 19:44 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/15 19:44 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/15 19:44 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/15 19:44 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/15 19:44 67-66-35.0 0.14 1
Chloromethane 0.21J ug/L 06/04/15 19:44 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/15 19:44 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/15 19:44 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/15 19:44 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/15 19:44 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/15 19:44 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/15 19:44 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/15 19:44 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/15 19:44 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/15 19:44 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/04/15 19:44 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/15 19:44 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/15 19:44 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/15 19:44 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/15 19:44 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/04/15 19:44 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252038
SURRY CO LINED
Sample:LAGOON Lab ID:92252038001 Collected:05/28/15 18:20 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/04/15 19:44 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/15 19:44 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/15 19:44 591-78-650.0 0.46 1
Iodomethane 16.9 ug/L 06/04/15 19:44 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/15 19:44 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/15 19:44 108-10-11000.33 1
Styrene ND ug/L 06/04/15 19:44 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/15 19:44 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/15 19:44 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/15 19:44 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/15 19:44 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/15 19:44 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/15 19:44 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/15 19:44 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/15 19:44 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/15 19:44 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/15 19:44 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/15 19:44 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/15 19:44 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %06/04/15 19:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %06/04/15 19:44 17060-07-070-130 1
Toluene-d8 (S)100 %06/04/15 19:44 2037-26-570-130 1
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 54000 ug/L 06/04/15 16:32 B2,D605/30/15 12:36200020001
Analytical Method: EPA 90409040 pH
pH 7.1 Std. Units 05/31/15 16:20 H60.10 0.10 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 28500J ug/L 06/05/15 23:04 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 61700J ug/L 05/29/15 23:2620000020020
Analytical Method: EPA 365.1365.1 Phosphorus, Total
Phosphorus 190 ug/L 06/09/15 12:22 7723-14-050.0 25.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 170000 ug/L 06/02/15 09:5050000250002
REPORT OF LABORATORY ANALYSIS
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Page 6 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18601
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92252038001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1473363
Associated Lab Samples:92252038001
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 06/04/15 22:53
Arsenic ug/L ND 10.0 06/04/15 22:53
Barium ug/L ND 100 06/04/15 22:53
Beryllium ug/L ND 1.0 06/04/15 22:53
Cadmium ug/L ND 1.0 06/04/15 22:53
Chromium ug/L ND 10.0 06/04/15 22:53
Cobalt ug/L ND 10.0 06/04/15 22:53
Copper ug/L ND 10.0 06/05/15 16:24
Lead ug/L ND 10.0 06/05/15 16:24
Nickel ug/L ND 50.0 06/04/15 22:53
Selenium ug/L ND 10.0 06/04/15 22:53
Silver ug/L ND 10.0 06/04/15 22:53
Thallium ug/L ND 5.5 06/04/15 22:53
Vanadium ug/L ND 25.0 06/04/15 22:53
Zinc ug/L ND 10.0 06/05/15 16:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1473364LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 472500 94 80-120
Arsenic ug/L 458500 92 80-120
Barium ug/L 459500 92 80-120
Beryllium ug/L 460500 92 80-120
Cadmium ug/L 457500 91 80-120
Chromium ug/L 458500 92 80-120
Cobalt ug/L 461500 92 80-120
Copper ug/L 458500 92 80-120
Lead ug/L 455500 91 80-120
Nickel ug/L 458500 92 80-120
Selenium ug/L 434500 87 80-120
Silver ug/L 224250 90 80-120
Thallium ug/L 460500 92 80-120
Vanadium ug/L 451500 90 80-120
Zinc ug/L 453500 91 80-120
REPORT OF LABORATORY ANALYSIS
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Page 7 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1473365MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92252036001
1473366
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 93 75-125103 10 25500ND464514
Arsenic ug/L 500 90 75-125100 10 25500ND452499
Barium ug/L 500 91 75-125100 8 25500144597644
Beryllium ug/L 500 91 75-125101 10 25500ND457503
Cadmium ug/L 500 90 75-12599 10 25500ND449496
Chromium ug/L 500 90 75-12599 9 255005.2 458 501
Cobalt ug/L 500 90 75-12598 10 25500ND448492
Copper ug/L 500 100 75-125100 0 255008.7 508 507
Lead ug/L 500 89 75-12597 9 25500ND444485
Nickel ug/L 500 89 75-12598 9 25500ND446490
Selenium ug/L 500 85 75-12595 11 25500ND429477
Silver ug/L 250 88 75-12597 10 25250ND220243
Thallium ug/L 500 89 75-12598 10 25500ND446493
Vanadium ug/L 500 89 75-12597 9 255004.0J 448 491
Zinc ug/L 500 93 75-12597 3 2550011.4 478 495
REPORT OF LABORATORY ANALYSIS
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Page 8 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32002
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92252038001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1475797
Associated Lab Samples:92252038001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/15 16:39
1,1,1-Trichloroethane ug/L ND 1.0 06/04/15 16:39
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/15 16:39
1,1,2-Trichloroethane ug/L ND 1.0 06/04/15 16:39
1,1-Dichloroethane ug/L ND 5.0 06/04/15 16:39
1,1-Dichloroethene ug/L ND 5.0 06/04/15 16:39
1,2,3-Trichloropropane ug/L ND 1.0 06/04/15 16:39
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/15 16:39
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/15 16:39
1,2-Dichlorobenzene ug/L ND 5.0 06/04/15 16:39
1,2-Dichloroethane ug/L ND 1.0 06/04/15 16:39
1,2-Dichloropropane ug/L ND 1.0 06/04/15 16:39
1,3-Dichloropropane ug/L ND 1.0 06/04/15 16:39
1,4-Dichlorobenzene ug/L ND 1.0 06/04/15 16:39
2-Butanone (MEK)ug/L ND 100 06/04/15 16:39
2-Hexanone ug/L ND 50.0 06/04/15 16:39
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/15 16:39
Acetone ug/L ND 100 06/04/15 16:39
Acrylonitrile ug/L ND 200 06/04/15 16:39
Benzene ug/L ND 1.0 06/04/15 16:39
Bromochloromethane ug/L ND 3.0 06/04/15 16:39
Bromodichloromethane ug/L ND 1.0 06/04/15 16:39
Bromoform ug/L ND 3.0 06/04/15 16:39
Bromomethane ug/L ND 10.0 06/04/15 16:39
Carbon disulfide ug/L ND 100 06/04/15 16:39
Carbon tetrachloride ug/L ND 1.0 06/04/15 16:39
Chlorobenzene ug/L ND 3.0 06/04/15 16:39
Chloroethane ug/L ND 10.0 06/04/15 16:39
Chloroform ug/L ND 5.0 06/04/15 16:39
Chloromethane ug/L ND 1.0 06/04/15 16:39
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/15 16:39
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/15 16:39
Dibromochloromethane ug/L ND 3.0 06/04/15 16:39
Dibromomethane ug/L ND 10.0 06/04/15 16:39
Ethylbenzene ug/L ND 1.0 06/04/15 16:39
Iodomethane ug/L ND 10.0 06/04/15 16:39
Methylene Chloride ug/L ND 1.0 06/04/15 16:39
Styrene ug/L ND 1.0 06/04/15 16:39
Tetrachloroethene ug/L ND 1.0 06/04/15 16:39
Toluene ug/L ND 1.0 06/04/15 16:39
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/15 16:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1475797
Associated Lab Samples:92252038001
Matrix:Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/15 16:39
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/15 16:39
Trichloroethene ug/L ND 1.0 06/04/15 16:39
Trichlorofluoromethane ug/L ND 1.0 06/04/15 16:39
Vinyl acetate ug/L ND 50.0 06/04/15 16:39
Vinyl chloride ug/L ND 1.0 06/04/15 16:39
Xylene (Total)ug/L ND 5.0 06/04/15 16:39
1,2-Dichloroethane-d4 (S)%98 70-130 06/04/15 16:39
4-Bromofluorobenzene (S)%99 70-130 06/04/15 16:39
Toluene-d8 (S)%100 70-130 06/04/15 16:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1475798LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.650 103 80-125
1,1,1-Trichloroethane ug/L 47.950 96 71-129
1,1,2,2-Tetrachloroethane ug/L 51.850 104 79-124
1,1,2-Trichloroethane ug/L 50.150 100 85-125
1,1-Dichloroethane ug/L 48.450 97 73-126
1,1-Dichloroethene ug/L 48.350 97 66-135
1,2,3-Trichloropropane ug/L 53.150 106 75-130
1,2-Dibromo-3-chloropropane ug/L 49.450 99 71-133
1,2-Dibromoethane (EDB)ug/L 53.450 107 83-124
1,2-Dichlorobenzene ug/L 57.750 115 80-133
1,2-Dichloroethane ug/L 48.650 97 67-128
1,2-Dichloropropane ug/L 49.850 100 75-132
1,3-Dichloropropane ug/L 54.050 108 76-131
1,4-Dichlorobenzene ug/L 55.650 111 78-130
2-Butanone (MEK)ug/L 99.9J100 100 61-144
2-Hexanone ug/L 109100 109 68-143
4-Methyl-2-pentanone (MIBK)ug/L 99.4J100 99 72-135
Acetone ug/L 105100 105 48-146
Acrylonitrile ug/L 241250 96 40-160
Benzene ug/L 51.050 102 80-125
Bromochloromethane ug/L 50.050 100 71-125
Bromodichloromethane ug/L 43.750 87 78-124
Bromoform ug/L 33.9 L0506871-128
Bromomethane ug/L 62.350 125 40-160
Carbon disulfide ug/L 41.7J50 83 50-160
Carbon tetrachloride ug/L 47.150 94 69-131
Chlorobenzene ug/L 54.050 108 81-122
Chloroethane ug/L 46.250 92 39-148
Chloroform ug/L 45.350 91 73-127
Chloromethane ug/L 50.750 101 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1475798LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 50.550 101 74-124
cis-1,3-Dichloropropene ug/L 49.750 99 72-132
Dibromochloromethane ug/L 42.850 86 78-125
Dibromomethane ug/L 50.350 101 82-120
Ethylbenzene ug/L 53.350 107 79-121
Iodomethane ug/L 113100 113 39-154
Methylene Chloride ug/L 55.050 110 64-133
Styrene ug/L 57.150 114 84-126
Tetrachloroethene ug/L 55.050 110 78-122
Toluene ug/L 49.950 100 80-121
trans-1,2-Dichloroethene ug/L 49.050 98 71-127
trans-1,3-Dichloropropene ug/L 50.950 102 69-141
trans-1,4-Dichloro-2-butene ug/L 41.0J50 82 40-160
Trichloroethene ug/L 48.650 97 78-122
Trichlorofluoromethane ug/L 50.150 100 53-137
Vinyl acetate ug/L 106100 106 40-160
Vinyl chloride ug/L 54.550 109 58-137
Xylene (Total)ug/L 161150 107 81-126
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1475800MATRIX SPIKE SAMPLE:
MSSpike
Result
92252070006
1,1,1,2-Tetrachloroethane ug/L 15.220 76 70-130ND
1,1,1-Trichloroethane ug/L 17.720 88 70-130ND
1,1,2,2-Tetrachloroethane ug/L 16.620 83 70-130ND
1,1,2-Trichloroethane ug/L 17.420 87 70-130ND
1,1-Dichloroethane ug/L 18.520 92 70-130ND
1,1-Dichloroethene ug/L 19.320 97 70-166ND
1,2,3-Trichloropropane ug/L 16.820 84 70-130ND
1,2-Dibromo-3-chloropropane ug/L 15.020 75 70-130ND
1,2-Dibromoethane (EDB)ug/L 17.120 85 70-130ND
1,2-Dichlorobenzene ug/L 18.520 92 70-130ND
1,2-Dichloroethane ug/L 17.820 89 70-130ND
1,2-Dichloropropane ug/L 18.120 90 70-130ND
1,3-Dichloropropane ug/L 17.520 88 70-130ND
1,4-Dichlorobenzene ug/L 17.420 87 70-130ND
2-Butanone (MEK)ug/L 37.9J40 95 70-130ND
2-Hexanone ug/L 35.9J40 90 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 35.5J40 89 70-130ND
Acetone ug/L 37.0J40 89 70-130ND
Acrylonitrile ug/L 85.7J100 86 70-130ND
Benzene ug/L 18.720 94 70-148ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1475800MATRIX SPIKE SAMPLE:
MSSpike
Result
92252070006
Bromochloromethane ug/L 18.920 95 70-130ND
Bromodichloromethane ug/L 14.020 70 70-130ND
Bromoform ug/L 11.8 M0205970-130ND
Bromomethane ug/L 18.820 94 70-130ND
Carbon disulfide ug/L 15.6J20 78 70-130ND
Carbon tetrachloride ug/L 15.620 78 70-130ND
Chlorobenzene ug/L 18.620 93 70-146ND
Chloroethane ug/L 19.720 98 70-130ND
Chloroform ug/L 16.320 81 70-130ND
Chloromethane ug/L 21.820 109 70-130ND
cis-1,2-Dichloroethene ug/L 18.920 95 70-130ND
cis-1,3-Dichloropropene ug/L 15.920 79 70-130ND
Dibromochloromethane ug/L 11.5 M1205870-130ND
Dibromomethane ug/L 17.420 87 70-130ND
Ethylbenzene ug/L 18.220 91 70-130ND
Iodomethane ug/L 41.340 103 70-130ND
Methylene Chloride ug/L 19.820 99 70-130ND
Styrene ug/L 18.820 94 70-130ND
Tetrachloroethene ug/L 18.520 92 70-130ND
Toluene ug/L 18.020 90 70-155ND
trans-1,2-Dichloroethene ug/L 19.120 96 70-130ND
trans-1,3-Dichloropropene ug/L 15.420 77 70-130ND
trans-1,4-Dichloro-2-butene ug/L 14.2J20 71 70-130ND
Trichloroethene ug/L 18.420 92 69-151ND
Trichlorofluoromethane ug/L 19.520 97 70-130ND
Vinyl acetate ug/L 33.2J40 83 70-130ND
Vinyl chloride ug/L 19.720 98 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92252070005
1475799SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.46J 300.46J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L 0.13J 300.14J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92252070005
1475799SAMPLE DUPLICATE:
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 0.44J 300.42J
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.72J 300.74J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%104 0104
4-Bromofluorobenzene (S)%97 197
Toluene-d8 (S)%102 1102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/37780
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92252038001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1471458
Associated Lab Samples:92252038001
Matrix:Water
Analyzed
BOD, 5 day ug/L ND 2000 06/04/15 16:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1471459LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 169000198000 85 84.6-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92252038001
1471460SAMPLE DUPLICATE:
BOD, 5 day ug/L 66000 B2,D6201054000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/37784
EPA 9040
EPA 9040
9040 pH
Associated Lab Samples:92252038001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92251844001
1471546SAMPLE DUPLICATE:
pH Std. Units 6.6 H6196.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23162
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92252038001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1475158
Associated Lab Samples:92252038001
Matrix:Water
Analyzed
Sulfate ug/L ND 250000 06/05/15 19:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1475159LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 20000J20000 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1475160MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92252271001
1475161
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 102 90-110102 0 1020000ND20300J20300J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1475162MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92252055001
1475163
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 106 90-110106 0 102000012000J33100J33200J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23094
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92252038001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1471384
Associated Lab Samples:92252038001
Matrix:Water
Analyzed
Nitrogen, Nitrate ug/L ND 20.0 05/29/15 22:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1471385LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24902500 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1471386MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92251926002
1471387
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 93 90-11093 0 102500ND23302320
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1471388MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92251926003
1471389
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 92 90-11094 2 1025000.30 mg/L 2600 2650
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23191
EPA 365.1
EPA 365.1
365.1 Phosphorus, Total
Associated Lab Samples:92252038001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1478233
Associated Lab Samples:92252038001
Matrix:Water
Analyzed
Phosphorus ug/L ND 50.0 06/09/15 12:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1478234LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus ug/L 27302500 109 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1478235MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92252721001
1478236
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 100 90-110104 1 1025006.1 mg/L 8640 8750
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1478237MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92252345001
1478238
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 103 90-110102 1 1025000.11 mg/L 2690 2660
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252038
SURRY CO LINED
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23115
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92252038001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1471738
Associated Lab Samples:92252038001
Matrix:Water
Analyzed
Chemical Oxygen Demand ug/L ND 25000 06/02/15 09:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1471739LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 785000750000 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1471740MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92251288003
1471741
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 103 90-110103 0 3750000ND778000778000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1471742MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92251814001
1471743
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 101 90-110101 0 3750000ND756000756000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92252038
SURRY CO LINED
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.B2
The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6
Analysis initiated outside of the 15 minute EPA recommended holding time.H6
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92252038
SURRY CO LINED
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92252038001 MPRP/18601 ICP/16683LAGOONEPA 3010 EPA 6010
92252038001 MSV/32002LAGOONEPA 8260
92252038001 WET/37780 WET/37782LAGOONSM 5210B SM 5210B
92252038001 WET/37784LAGOONEPA 9040
92252038001 WETA/23162LAGOONEPA 300.0
92252038001 WETA/23094LAGOONEPA 353.2
92252038001 WETA/23191LAGOONEPA 365.1
92252038001 WETA/23115LAGOONSM 5220D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/12/2015 07:50 PM
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Huntersville, NC 28078
[phone]
Page 21 of 23
Page 22 of 23
Page 23 of 23
#=CL#
July 28, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92260076
92260076
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY CO MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on July 23, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 1 of 13
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92260076
SURRY CO MSWLF
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 2 of 13
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92260076
SURRY CO MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92260076001 SW-4 Water 07/20/15 17:00 07/23/15 13:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 3 of 13
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92260076
SURRY CO MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92260076001 SW-4 EPA 8260 51 PASI-CSNP
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 4 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260076
SURRY CO MSWLF
Sample:SW-4 Lab ID:92260076001 Collected:07/20/15 17:00 Received:07/23/15 13:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 24.2J ug/L 07/28/15 09:27 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 09:27 107-13-12001.9 1
Benzene ND ug/L 07/28/15 09:27 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 09:27 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 09:27 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 09:27 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 09:27 74-83-910.0 0.29 1
2-Butanone (MEK)13.0J ug/L 07/28/15 09:27 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 09:27 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 09:27 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 09:27 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 09:27 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 09:27 67-66-35.0 0.14 1
Chloromethane 0.15J ug/L 07/28/15 09:27 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 09:27 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 09:27 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 09:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 09:27 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 09:27 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 09:27 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 09:27 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 09:27 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 09:27 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 09:27 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 09:27 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 09:27 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 09:27 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 09:27 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 09:27 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/28/15 09:27 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 09:27 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 09:27 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 09:27 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 09:27 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 09:27 108-10-11000.33 1
Styrene ND ug/L 07/28/15 09:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 09:27 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 09:27 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 09:27 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 09:27 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 09:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 09:27 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 09:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 09:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 09:27 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 09:27 108-05-450.0 0.35 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/28/2015 06:14 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260076
SURRY CO MSWLF
Sample:SW-4 Lab ID:92260076001 Collected:07/20/15 17:00 Received:07/23/15 13:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride ND ug/L 07/28/15 09:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 09:27 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %07/28/15 09:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %07/28/15 09:27 17060-07-070-130 1
Toluene-d8 (S)100 %07/28/15 09:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/28/2015 06:14 PM
Pace Analytical Services, Inc.
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[phone]
Page 6 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260076
SURRY CO MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32722
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92260076001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519232
Associated Lab Samples:92260076001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/28/15 04:10
1,1,1-Trichloroethane ug/L ND 1.0 07/28/15 04:10
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/28/15 04:10
1,1,2-Trichloroethane ug/L ND 1.0 07/28/15 04:10
1,1-Dichloroethane ug/L ND 5.0 07/28/15 04:10
1,1-Dichloroethene ug/L ND 5.0 07/28/15 04:10
1,2,3-Trichloropropane ug/L ND 1.0 07/28/15 04:10
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/28/15 04:10
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/28/15 04:10
1,2-Dichlorobenzene ug/L ND 5.0 07/28/15 04:10
1,2-Dichloroethane ug/L ND 1.0 07/28/15 04:10
1,2-Dichloropropane ug/L ND 1.0 07/28/15 04:10
1,3-Dichloropropane ug/L ND 1.0 07/28/15 04:10
1,4-Dichlorobenzene ug/L ND 1.0 07/28/15 04:10
2-Butanone (MEK)ug/L ND 100 07/28/15 04:10
2-Hexanone ug/L ND 50.0 07/28/15 04:10
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/28/15 04:10
Acetone ug/L ND 100 07/28/15 04:10
Acrylonitrile ug/L ND 200 07/28/15 04:10
Benzene ug/L ND 1.0 07/28/15 04:10
Bromochloromethane ug/L ND 3.0 07/28/15 04:10
Bromodichloromethane ug/L ND 1.0 07/28/15 04:10
Bromoform ug/L ND 3.0 07/28/15 04:10
Bromomethane ug/L ND 10.0 07/28/15 04:10
Carbon disulfide ug/L ND 100 07/28/15 04:10
Carbon tetrachloride ug/L ND 1.0 07/28/15 04:10
Chlorobenzene ug/L ND 3.0 07/28/15 04:10
Chloroethane ug/L ND 10.0 07/28/15 04:10
Chloroform ug/L ND 5.0 07/28/15 04:10
Chloromethane ug/L ND 1.0 07/28/15 04:10
cis-1,2-Dichloroethene ug/L ND 5.0 07/28/15 04:10
cis-1,3-Dichloropropene ug/L ND 1.0 07/28/15 04:10
Dibromochloromethane ug/L ND 3.0 07/28/15 04:10
Dibromomethane ug/L ND 10.0 07/28/15 04:10
Ethylbenzene ug/L ND 1.0 07/28/15 04:10
Iodomethane ug/L ND 10.0 07/28/15 04:10
Methylene Chloride ug/L ND 1.0 07/28/15 04:10
Styrene ug/L ND 1.0 07/28/15 04:10
Tetrachloroethene ug/L ND 1.0 07/28/15 04:10
Toluene ug/L ND 1.0 07/28/15 04:10
trans-1,2-Dichloroethene ug/L ND 5.0 07/28/15 04:10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/28/2015 06:14 PM
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Huntersville, NC 28078
[phone]
Page 7 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260076
SURRY CO MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519232
Associated Lab Samples:92260076001
Matrix:Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 07/28/15 04:10
trans-1,4-Dichloro-2-butene ug/L ND 100 07/28/15 04:10
Trichloroethene ug/L ND 1.0 07/28/15 04:10
Trichlorofluoromethane ug/L ND 1.0 07/28/15 04:10
Vinyl acetate ug/L ND 50.0 07/28/15 04:10
Vinyl chloride ug/L ND 1.0 07/28/15 04:10
Xylene (Total)ug/L ND 5.0 07/28/15 04:10
1,2-Dichloroethane-d4 (S)%105 70-130 07/28/15 04:10
4-Bromofluorobenzene (S)%100 70-130 07/28/15 04:10
Toluene-d8 (S)%99 70-130 07/28/15 04:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519233LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.450 101 80-125
1,1,1-Trichloroethane ug/L 52.150 104 71-129
1,1,2,2-Tetrachloroethane ug/L 54.450 109 79-124
1,1,2-Trichloroethane ug/L 52.350 105 85-125
1,1-Dichloroethane ug/L 48.750 97 73-126
1,1-Dichloroethene ug/L 51.150 102 66-135
1,2,3-Trichloropropane ug/L 55.150 110 75-130
1,2-Dibromo-3-chloropropane ug/L 52.150 104 71-133
1,2-Dibromoethane (EDB)ug/L 53.250 106 83-124
1,2-Dichlorobenzene ug/L 54.050 108 80-133
1,2-Dichloroethane ug/L 48.750 97 67-128
1,2-Dichloropropane ug/L 50.150 100 75-132
1,3-Dichloropropane ug/L 52.150 104 76-131
1,4-Dichlorobenzene ug/L 52.550 105 78-130
2-Butanone (MEK)ug/L 100100 100 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 110100 110 72-135
Acetone ug/L 101100 101 48-146
Acrylonitrile ug/L 239250 96 40-160
Benzene ug/L 51.550 103 80-125
Bromochloromethane ug/L 54.350 109 71-125
Bromodichloromethane ug/L 54.550 109 78-124
Bromoform ug/L 49.450 99 71-128
Bromomethane ug/L 43.550 87 40-160
Carbon disulfide ug/L 45.8J50 92 50-160
Carbon tetrachloride ug/L 54.750 109 69-131
Chlorobenzene ug/L 51.050 102 81-122
Chloroethane ug/L 46.050 92 39-148
Chloroform ug/L 51.750 103 73-127
Chloromethane ug/L 43.750 87 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/28/2015 06:14 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 8 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260076
SURRY CO MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519233LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 50.150 100 74-124
cis-1,3-Dichloropropene ug/L 51.450 103 72-132
Dibromochloromethane ug/L 52.650 105 78-125
Dibromomethane ug/L 55.250 110 82-120
Ethylbenzene ug/L 51.450 103 79-121
Iodomethane ug/L 89.1100 89 39-154
Methylene Chloride ug/L 51.050 102 64-133
Styrene ug/L 50.850 102 84-126
Tetrachloroethene ug/L 50.350 101 78-122
Toluene ug/L 52.850 106 80-121
trans-1,2-Dichloroethene ug/L 47.950 96 71-127
trans-1,3-Dichloropropene ug/L 51.050 102 69-141
trans-1,4-Dichloro-2-butene ug/L 53.1J50 106 40-160
Trichloroethene ug/L 49.450 99 78-122
Trichlorofluoromethane ug/L 50.850 102 53-137
Vinyl acetate ug/L 99.2100 99 40-160
Vinyl chloride ug/L 46.350 93 58-137
Xylene (Total)ug/L 152150 101 81-126
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/28/2015 06:14 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 9 of 13
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92260076
SURRY CO MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/28/2015 06:14 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 13
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92260076
SURRY CO MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92260076001 MSV/32722SW-4 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/28/2015 06:14 PM
Pace Analytical Services, Inc.
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[phone]
Page 11 of 13
Page 12 of 13
Page 13 of 13
#=CL#
June 24, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92252037
92252037
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY SWs
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 30
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92252037
SURRY SWs
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 30
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92252037
SURRY SWs
Lab ID Sample ID Matrix Date Collected Date Received
92252037001 SW-1 Water 05/28/15 11:10 05/29/15 13:00
92252037002 SW-2 Water 05/28/15 15:35 05/29/15 13:00
92252037003 SW-3 Water 05/28/15 20:50 05/29/15 13:00
92252037004 SW-4 Water 05/28/15 18:10 05/29/15 13:00
92252037005 SW-A Water 05/28/15 17:35 05/29/15 13:00
92252037006 SW-B Water 05/28/15 17:50 05/29/15 13:00
92252037007 SWN-1 Water 05/28/15 17:20 05/29/15 13:00
92252037008 SWN-2 Water 05/28/15 16:20 05/29/15 13:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 30
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92252037
SURRY SWs
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92252037001 SW-1 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252037002 SW-2 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252037003 SW-3 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252037004 SW-4 EPA 6010 15 PASI-AJMW
92252037005 SW-A EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252037006 SW-B EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252037007 SWN-1 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252037008 SWN-2 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-1 Lab ID:92252037001 Collected:05/28/15 11:10 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 23:16 7440-36-006/02/15 23:306.0 3.8 1
Arsenic ND ug/L 06/04/15 23:16 7440-38-206/02/15 23:3010.0 2.5 1
Barium 20.3J ug/L 06/04/15 23:16 7440-39-306/02/15 23:301002.5 1
Beryllium ND ug/L 06/04/15 23:16 7440-41-706/02/15 23:301.0 0.50 1
Cadmium ND ug/L 06/04/15 23:16 7440-43-906/02/15 23:301.0 0.50 1
Chromium ND ug/L 06/04/15 23:16 7440-47-306/02/15 23:3010.0 2.5 1
Cobalt ND ug/L 06/04/15 23:16 7440-48-406/02/15 23:3010.0 2.5 1
Copper ND ug/L 06/04/15 23:16 7440-50-806/02/15 23:3010.0 2.5 1
Lead ND ug/L 06/04/15 23:16 7439-92-106/02/15 23:3010.0 2.5 1
Nickel ND ug/L 06/04/15 23:16 7440-02-006/02/15 23:3050.0 2.5 1
Selenium ND ug/L 06/04/15 23:16 7782-49-206/02/15 23:3010.0 5.0 1
Silver ND ug/L 06/04/15 23:16 7440-22-406/02/15 23:3010.0 2.5 1
Thallium ND ug/L 06/04/15 23:16 7440-28-006/02/15 23:305.5 5.0 1
Vanadium ND ug/L 06/04/15 23:16 7440-62-206/02/15 23:3025.0 2.5 1
Zinc ND ug/L 06/04/15 23:16 7440-66-606/02/15 23:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/15 17:46 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/15 17:46 107-13-12001.9 1
Benzene ND ug/L 06/04/15 17:46 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/15 17:46 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/15 17:46 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/15 17:46 75-25-2 L23.0 0.26 1
Bromomethane 0.78J ug/L 06/04/15 17:46 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/15 17:46 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/15 17:46 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/15 17:46 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/15 17:46 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/15 17:46 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/15 17:46 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/15 17:46 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/15 17:46 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/15 17:46 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/15 17:46 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/15 17:46 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/15 17:46 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/15 17:46 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/15 17:46 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/15 17:46 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/15 17:46 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/04/15 17:46 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/15 17:46 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/15 17:46 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/15 17:46 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/15 17:46 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/04/15 17:46 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-1 Lab ID:92252037001 Collected:05/28/15 11:10 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/04/15 17:46 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/15 17:46 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/15 17:46 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/15 17:46 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/15 17:46 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/15 17:46 108-10-11000.33 1
Styrene ND ug/L 06/04/15 17:46 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/15 17:46 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/15 17:46 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/15 17:46 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/15 17:46 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/15 17:46 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/15 17:46 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/15 17:46 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/15 17:46 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/15 17:46 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/15 17:46 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/15 17:46 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/15 17:46 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %06/04/15 17:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %06/04/15 17:46 17060-07-070-130 1
Toluene-d8 (S)101 %06/04/15 17:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-2 Lab ID:92252037002 Collected:05/28/15 15:35 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 23:19 7440-36-006/02/15 23:306.0 3.8 1
Arsenic ND ug/L 06/04/15 23:19 7440-38-206/02/15 23:3010.0 2.5 1
Barium 15.6J ug/L 06/04/15 23:19 7440-39-306/02/15 23:301002.5 1
Beryllium ND ug/L 06/04/15 23:19 7440-41-706/02/15 23:301.0 0.50 1
Cadmium ND ug/L 06/04/15 23:19 7440-43-906/02/15 23:301.0 0.50 1
Chromium ND ug/L 06/04/15 23:19 7440-47-306/02/15 23:3010.0 2.5 1
Cobalt 22.3 ug/L 06/04/15 23:19 7440-48-406/02/15 23:3010.0 2.5 1
Copper ND ug/L 06/04/15 23:19 7440-50-806/02/15 23:3010.0 2.5 1
Lead ND ug/L 06/04/15 23:19 7439-92-106/02/15 23:3010.0 2.5 1
Nickel ND ug/L 06/04/15 23:19 7440-02-006/02/15 23:3050.0 2.5 1
Selenium ND ug/L 06/04/15 23:19 7782-49-206/02/15 23:3010.0 5.0 1
Silver ND ug/L 06/04/15 23:19 7440-22-406/02/15 23:3010.0 2.5 1
Thallium ND ug/L 06/04/15 23:19 7440-28-006/02/15 23:305.5 5.0 1
Vanadium ND ug/L 06/04/15 23:19 7440-62-206/02/15 23:3025.0 2.5 1
Zinc ND ug/L 06/04/15 23:19 7440-66-606/02/15 23:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/15 18:03 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/15 18:03 107-13-12001.9 1
Benzene ND ug/L 06/04/15 18:03 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/15 18:03 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/15 18:03 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/15 18:03 75-25-2 L23.0 0.26 1
Bromomethane ND ug/L 06/04/15 18:03 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/15 18:03 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/15 18:03 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/15 18:03 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/15 18:03 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/15 18:03 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/15 18:03 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/15 18:03 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/15 18:03 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/15 18:03 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/15 18:03 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/15 18:03 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/15 18:03 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/15 18:03 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/15 18:03 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/15 18:03 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/15 18:03 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/04/15 18:03 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.76J ug/L 06/04/15 18:03 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/15 18:03 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/15 18:03 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/15 18:03 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/04/15 18:03 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-2 Lab ID:92252037002 Collected:05/28/15 15:35 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/04/15 18:03 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/15 18:03 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/15 18:03 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/15 18:03 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/15 18:03 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/15 18:03 108-10-11000.33 1
Styrene ND ug/L 06/04/15 18:03 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/15 18:03 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/15 18:03 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/15 18:03 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/15 18:03 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/15 18:03 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/15 18:03 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/15 18:03 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/15 18:03 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/15 18:03 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/15 18:03 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/15 18:03 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/15 18:03 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %06/04/15 18:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %06/04/15 18:03 17060-07-070-130 1
Toluene-d8 (S)101 %06/04/15 18:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-3 Lab ID:92252037003 Collected:05/28/15 20:50 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 23:23 7440-36-006/02/15 23:306.0 3.8 1
Arsenic ND ug/L 06/04/15 23:23 7440-38-206/02/15 23:3010.0 2.5 1
Barium 21.0J ug/L 06/04/15 23:23 7440-39-306/02/15 23:301002.5 1
Beryllium ND ug/L 06/04/15 23:23 7440-41-706/02/15 23:301.0 0.50 1
Cadmium ND ug/L 06/04/15 23:23 7440-43-906/02/15 23:301.0 0.50 1
Chromium ND ug/L 06/04/15 23:23 7440-47-306/02/15 23:3010.0 2.5 1
Cobalt 8.8J ug/L 06/04/15 23:23 7440-48-406/02/15 23:3010.0 2.5 1
Copper ND ug/L 06/04/15 23:23 7440-50-806/02/15 23:3010.0 2.5 1
Lead ND ug/L 06/04/15 23:23 7439-92-106/02/15 23:3010.0 2.5 1
Nickel ND ug/L 06/04/15 23:23 7440-02-006/02/15 23:3050.0 2.5 1
Selenium ND ug/L 06/04/15 23:23 7782-49-206/02/15 23:3010.0 5.0 1
Silver ND ug/L 06/04/15 23:23 7440-22-406/02/15 23:3010.0 2.5 1
Thallium ND ug/L 06/04/15 23:23 7440-28-006/02/15 23:305.5 5.0 1
Vanadium 2.6J ug/L 06/04/15 23:23 7440-62-206/02/15 23:3025.0 2.5 1
Zinc ND ug/L 06/04/15 23:23 7440-66-606/02/15 23:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/15 18:19 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/15 18:19 107-13-12001.9 1
Benzene ND ug/L 06/04/15 18:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/15 18:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/15 18:19 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/15 18:19 75-25-2 L23.0 0.26 1
Bromomethane 0.79J ug/L 06/04/15 18:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/15 18:19 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/15 18:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/15 18:19 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/15 18:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/15 18:19 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/15 18:19 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/15 18:19 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/15 18:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/15 18:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/15 18:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/15 18:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/15 18:19 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/15 18:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/15 18:19 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/15 18:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/15 18:19 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/04/15 18:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/15 18:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/15 18:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/15 18:19 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/15 18:19 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/04/15 18:19 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 9 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-3 Lab ID:92252037003 Collected:05/28/15 20:50 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/04/15 18:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/15 18:19 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/15 18:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/15 18:19 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/15 18:19 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/15 18:19 108-10-11000.33 1
Styrene ND ug/L 06/04/15 18:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/15 18:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/15 18:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/15 18:19 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/15 18:19 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/15 18:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/15 18:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/15 18:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/15 18:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/15 18:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/15 18:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/15 18:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/15 18:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/04/15 18:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %06/04/15 18:19 17060-07-070-130 1
Toluene-d8 (S)103 %06/04/15 18:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 10 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-4 Lab ID:92252037004 Collected:05/28/15 18:10 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 23:26 7440-36-006/02/15 23:306.0 3.8 1
Arsenic ND ug/L 06/04/15 23:26 7440-38-206/02/15 23:3010.0 2.5 1
Barium 4.4J ug/L 06/04/15 23:26 7440-39-306/02/15 23:301002.5 1
Beryllium ND ug/L 06/04/15 23:26 7440-41-706/02/15 23:301.0 0.50 1
Cadmium ND ug/L 06/04/15 23:26 7440-43-906/02/15 23:301.0 0.50 1
Chromium ND ug/L 06/04/15 23:26 7440-47-306/02/15 23:3010.0 2.5 1
Cobalt ND ug/L 06/04/15 23:26 7440-48-406/02/15 23:3010.0 2.5 1
Copper 13.7 ug/L 06/05/15 16:27 7440-50-806/02/15 23:3010.0 2.5 1
Lead ND ug/L 06/05/15 16:27 7439-92-106/02/15 23:3010.0 2.5 1
Nickel 3.7J ug/L 06/04/15 23:26 7440-02-006/02/15 23:3050.0 2.5 1
Selenium ND ug/L 06/04/15 23:26 7782-49-206/02/15 23:3010.0 5.0 1
Silver ND ug/L 06/04/15 23:26 7440-22-406/02/15 23:3010.0 2.5 1
Thallium ND ug/L 06/04/15 23:26 7440-28-006/02/15 23:305.5 5.0 1
Vanadium ND ug/L 06/04/15 23:26 7440-62-206/02/15 23:3025.0 2.5 1
Zinc 118 ug/L 06/05/15 16:27 7440-66-606/02/15 23:3010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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9800 Kincey Ave. Suite 100
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Page 11 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-A Lab ID:92252037005 Collected:05/28/15 17:35 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 23:29 7440-36-006/02/15 23:306.0 3.8 1
Arsenic ND ug/L 06/04/15 23:29 7440-38-206/02/15 23:3010.0 2.5 1
Barium 12.9J ug/L 06/04/15 23:29 7440-39-306/02/15 23:301002.5 1
Beryllium ND ug/L 06/04/15 23:29 7440-41-706/02/15 23:301.0 0.50 1
Cadmium ND ug/L 06/04/15 23:29 7440-43-906/02/15 23:301.0 0.50 1
Chromium ND ug/L 06/04/15 23:29 7440-47-306/02/15 23:3010.0 2.5 1
Cobalt ND ug/L 06/04/15 23:29 7440-48-406/02/15 23:3010.0 2.5 1
Copper ND ug/L 06/04/15 23:29 7440-50-806/02/15 23:3010.0 2.5 1
Lead ND ug/L 06/04/15 23:29 7439-92-106/02/15 23:3010.0 2.5 1
Nickel ND ug/L 06/04/15 23:29 7440-02-006/02/15 23:3050.0 2.5 1
Selenium ND ug/L 06/04/15 23:29 7782-49-206/02/15 23:3010.0 5.0 1
Silver ND ug/L 06/04/15 23:29 7440-22-406/02/15 23:3010.0 2.5 1
Thallium ND ug/L 06/04/15 23:29 7440-28-006/02/15 23:305.5 5.0 1
Vanadium ND ug/L 06/04/15 23:29 7440-62-206/02/15 23:3025.0 2.5 1
Zinc ND ug/L 06/04/15 23:29 7440-66-606/02/15 23:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/15 18:36 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/15 18:36 107-13-12001.9 1
Benzene ND ug/L 06/04/15 18:36 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/15 18:36 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/15 18:36 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/15 18:36 75-25-2 L23.0 0.26 1
Bromomethane ND ug/L 06/04/15 18:36 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/15 18:36 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/15 18:36 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/15 18:36 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/15 18:36 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/15 18:36 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/15 18:36 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/15 18:36 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/15 18:36 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/15 18:36 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/15 18:36 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/15 18:36 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/15 18:36 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/15 18:36 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/15 18:36 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/15 18:36 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/15 18:36 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/04/15 18:36 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/15 18:36 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/15 18:36 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/15 18:36 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/15 18:36 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/04/15 18:36 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-A Lab ID:92252037005 Collected:05/28/15 17:35 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/04/15 18:36 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/15 18:36 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/15 18:36 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/15 18:36 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/15 18:36 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/15 18:36 108-10-11000.33 1
Styrene ND ug/L 06/04/15 18:36 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/15 18:36 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/15 18:36 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/15 18:36 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/15 18:36 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/15 18:36 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/15 18:36 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/15 18:36 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/15 18:36 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/15 18:36 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/15 18:36 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/15 18:36 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/15 18:36 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/04/15 18:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %06/04/15 18:36 17060-07-070-130 1
Toluene-d8 (S)101 %06/04/15 18:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-B Lab ID:92252037006 Collected:05/28/15 17:50 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 23:32 7440-36-006/02/15 23:306.0 3.8 1
Arsenic ND ug/L 06/04/15 23:32 7440-38-206/02/15 23:3010.0 2.5 1
Barium 13.6J ug/L 06/04/15 23:32 7440-39-306/02/15 23:301002.5 1
Beryllium ND ug/L 06/04/15 23:32 7440-41-706/02/15 23:301.0 0.50 1
Cadmium ND ug/L 06/04/15 23:32 7440-43-906/02/15 23:301.0 0.50 1
Chromium ND ug/L 06/04/15 23:32 7440-47-306/02/15 23:3010.0 2.5 1
Cobalt ND ug/L 06/04/15 23:32 7440-48-406/02/15 23:3010.0 2.5 1
Copper ND ug/L 06/04/15 23:32 7440-50-806/02/15 23:3010.0 2.5 1
Lead ND ug/L 06/04/15 23:32 7439-92-106/02/15 23:3010.0 2.5 1
Nickel ND ug/L 06/04/15 23:32 7440-02-006/02/15 23:3050.0 2.5 1
Selenium ND ug/L 06/04/15 23:32 7782-49-206/02/15 23:3010.0 5.0 1
Silver ND ug/L 06/04/15 23:32 7440-22-406/02/15 23:3010.0 2.5 1
Thallium ND ug/L 06/04/15 23:32 7440-28-006/02/15 23:305.5 5.0 1
Vanadium ND ug/L 06/04/15 23:32 7440-62-206/02/15 23:3025.0 2.5 1
Zinc ND ug/L 06/04/15 23:32 7440-66-606/02/15 23:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/15 18:53 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/15 18:53 107-13-12001.9 1
Benzene ND ug/L 06/04/15 18:53 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/15 18:53 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/15 18:53 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/15 18:53 75-25-2 L23.0 0.26 1
Bromomethane ND ug/L 06/04/15 18:53 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/15 18:53 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/15 18:53 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/15 18:53 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/15 18:53 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/15 18:53 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/15 18:53 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/15 18:53 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/15 18:53 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/15 18:53 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/15 18:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/15 18:53 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/15 18:53 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/15 18:53 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/15 18:53 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/15 18:53 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/15 18:53 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/04/15 18:53 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/15 18:53 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/15 18:53 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/15 18:53 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/15 18:53 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/04/15 18:53 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SW-B Lab ID:92252037006 Collected:05/28/15 17:50 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/04/15 18:53 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/15 18:53 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/15 18:53 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/15 18:53 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/15 18:53 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/15 18:53 108-10-11000.33 1
Styrene ND ug/L 06/04/15 18:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/15 18:53 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/15 18:53 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/15 18:53 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/15 18:53 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/15 18:53 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/15 18:53 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/15 18:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/15 18:53 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/15 18:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/15 18:53 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/15 18:53 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/15 18:53 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/04/15 18:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %06/04/15 18:53 17060-07-070-130 1
Toluene-d8 (S)100 %06/04/15 18:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SWN-1 Lab ID:92252037007 Collected:05/28/15 17:20 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 23:44 7440-36-006/02/15 23:306.0 3.8 1
Arsenic ND ug/L 06/04/15 23:44 7440-38-206/02/15 23:3010.0 2.5 1
Barium 13.1J ug/L 06/04/15 23:44 7440-39-306/02/15 23:301002.5 1
Beryllium ND ug/L 06/04/15 23:44 7440-41-706/02/15 23:301.0 0.50 1
Cadmium ND ug/L 06/04/15 23:44 7440-43-906/02/15 23:301.0 0.50 1
Chromium ND ug/L 06/04/15 23:44 7440-47-306/02/15 23:3010.0 2.5 1
Cobalt ND ug/L 06/04/15 23:44 7440-48-406/02/15 23:3010.0 2.5 1
Copper ND ug/L 06/04/15 23:44 7440-50-806/02/15 23:3010.0 2.5 1
Lead ND ug/L 06/04/15 23:44 7439-92-106/02/15 23:3010.0 2.5 1
Nickel ND ug/L 06/04/15 23:44 7440-02-006/02/15 23:3050.0 2.5 1
Selenium ND ug/L 06/04/15 23:44 7782-49-206/02/15 23:3010.0 5.0 1
Silver ND ug/L 06/04/15 23:44 7440-22-406/02/15 23:3010.0 2.5 1
Thallium ND ug/L 06/04/15 23:44 7440-28-006/02/15 23:305.5 5.0 1
Vanadium ND ug/L 06/04/15 23:44 7440-62-206/02/15 23:3025.0 2.5 1
Zinc ND ug/L 06/04/15 23:44 7440-66-606/02/15 23:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/15 19:10 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/15 19:10 107-13-12001.9 1
Benzene ND ug/L 06/04/15 19:10 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/15 19:10 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/15 19:10 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/15 19:10 75-25-2 L23.0 0.26 1
Bromomethane ND ug/L 06/04/15 19:10 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/15 19:10 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/15 19:10 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/15 19:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/15 19:10 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/15 19:10 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/15 19:10 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/15 19:10 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/15 19:10 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/15 19:10 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/15 19:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/15 19:10 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/15 19:10 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/15 19:10 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/15 19:10 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/15 19:10 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/15 19:10 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/04/15 19:10 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/15 19:10 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/15 19:10 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/15 19:10 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/15 19:10 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/04/15 19:10 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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Page 16 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SWN-1 Lab ID:92252037007 Collected:05/28/15 17:20 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/04/15 19:10 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/15 19:10 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/15 19:10 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/15 19:10 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/15 19:10 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/15 19:10 108-10-11000.33 1
Styrene ND ug/L 06/04/15 19:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/15 19:10 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/15 19:10 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/15 19:10 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/15 19:10 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/15 19:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/15 19:10 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/15 19:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/15 19:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/15 19:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/15 19:10 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/15 19:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/15 19:10 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/04/15 19:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %06/04/15 19:10 17060-07-070-130 1
Toluene-d8 (S)101 %06/04/15 19:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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Page 17 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SWN-2 Lab ID:92252037008 Collected:05/28/15 16:20 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 23:47 7440-36-006/02/15 23:306.0 3.8 1
Arsenic ND ug/L 06/04/15 23:47 7440-38-206/02/15 23:3010.0 2.5 1
Barium 12.7J ug/L 06/04/15 23:47 7440-39-306/02/15 23:301002.5 1
Beryllium ND ug/L 06/04/15 23:47 7440-41-706/02/15 23:301.0 0.50 1
Cadmium ND ug/L 06/04/15 23:47 7440-43-906/02/15 23:301.0 0.50 1
Chromium ND ug/L 06/04/15 23:47 7440-47-306/02/15 23:3010.0 2.5 1
Cobalt ND ug/L 06/04/15 23:47 7440-48-406/02/15 23:3010.0 2.5 1
Copper ND ug/L 06/04/15 23:47 7440-50-806/02/15 23:3010.0 2.5 1
Lead ND ug/L 06/04/15 23:47 7439-92-106/02/15 23:3010.0 2.5 1
Nickel ND ug/L 06/04/15 23:47 7440-02-006/02/15 23:3050.0 2.5 1
Selenium ND ug/L 06/04/15 23:47 7782-49-206/02/15 23:3010.0 5.0 1
Silver ND ug/L 06/04/15 23:47 7440-22-406/02/15 23:3010.0 2.5 1
Thallium ND ug/L 06/04/15 23:47 7440-28-006/02/15 23:305.5 5.0 1
Vanadium ND ug/L 06/04/15 23:47 7440-62-206/02/15 23:3025.0 2.5 1
Zinc ND ug/L 06/04/15 23:47 7440-66-606/02/15 23:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/15 19:27 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/15 19:27 107-13-12001.9 1
Benzene ND ug/L 06/04/15 19:27 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/15 19:27 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/15 19:27 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/15 19:27 75-25-2 L23.0 0.26 1
Bromomethane ND ug/L 06/04/15 19:27 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/15 19:27 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/15 19:27 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/15 19:27 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/15 19:27 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/15 19:27 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/15 19:27 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/15 19:27 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/15 19:27 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/15 19:27 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/15 19:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/15 19:27 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/15 19:27 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/15 19:27 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/15 19:27 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/15 19:27 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/15 19:27 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/04/15 19:27 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/15 19:27 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/15 19:27 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/15 19:27 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/15 19:27 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/04/15 19:27 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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Page 18 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252037
SURRY SWs
Sample:SWN-2 Lab ID:92252037008 Collected:05/28/15 16:20 Received:05/29/15 13:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/04/15 19:27 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/15 19:27 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/15 19:27 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/15 19:27 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/15 19:27 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/15 19:27 108-10-11000.33 1
Styrene ND ug/L 06/04/15 19:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/15 19:27 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/15 19:27 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/15 19:27 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/15 19:27 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/15 19:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/15 19:27 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/15 19:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/15 19:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/15 19:27 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/15 19:27 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/15 19:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/15 19:27 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/04/15 19:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/04/15 19:27 17060-07-070-130 1
Toluene-d8 (S)101 %06/04/15 19:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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Page 19 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252037
SURRY SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18601
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92252037001, 92252037002, 92252037003, 92252037004, 92252037005, 92252037006, 92252037007,
92252037008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1473363
Associated Lab Samples:92252037001, 92252037002, 92252037003, 92252037004, 92252037005, 92252037006, 92252037007,
92252037008
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 06/04/15 22:53
Arsenic ug/L ND 10.0 06/04/15 22:53
Barium ug/L ND 100 06/04/15 22:53
Beryllium ug/L ND 1.0 06/04/15 22:53
Cadmium ug/L ND 1.0 06/04/15 22:53
Chromium ug/L ND 10.0 06/04/15 22:53
Cobalt ug/L ND 10.0 06/04/15 22:53
Copper ug/L ND 10.0 06/05/15 16:24
Lead ug/L ND 10.0 06/05/15 16:24
Nickel ug/L ND 50.0 06/04/15 22:53
Selenium ug/L ND 10.0 06/04/15 22:53
Silver ug/L ND 10.0 06/04/15 22:53
Thallium ug/L ND 5.5 06/04/15 22:53
Vanadium ug/L ND 25.0 06/04/15 22:53
Zinc ug/L ND 10.0 06/05/15 16:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1473364LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 472500 94 80-120
Arsenic ug/L 458500 92 80-120
Barium ug/L 459500 92 80-120
Beryllium ug/L 460500 92 80-120
Cadmium ug/L 457500 91 80-120
Chromium ug/L 458500 92 80-120
Cobalt ug/L 461500 92 80-120
Copper ug/L 458500 92 80-120
Lead ug/L 455500 91 80-120
Nickel ug/L 458500 92 80-120
Selenium ug/L 434500 87 80-120
Silver ug/L 224250 90 80-120
Thallium ug/L 460500 92 80-120
Vanadium ug/L 451500 90 80-120
Zinc ug/L 453500 91 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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Huntersville, NC 28078
[phone]
Page 20 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252037
SURRY SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1473365MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92252036001
1473366
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 93 75-125103 10 25500ND464514
Arsenic ug/L 500 90 75-125100 10 25500ND452499
Barium ug/L 500 91 75-125100 8 25500144597644
Beryllium ug/L 500 91 75-125101 10 25500ND457503
Cadmium ug/L 500 90 75-12599 10 25500ND449496
Chromium ug/L 500 90 75-12599 9 255005.2 458 501
Cobalt ug/L 500 90 75-12598 10 25500ND448492
Copper ug/L 500 100 75-125100 0 255008.7 508 507
Lead ug/L 500 89 75-12597 9 25500ND444485
Nickel ug/L 500 89 75-12598 9 25500ND446490
Selenium ug/L 500 85 75-12595 11 25500ND429477
Silver ug/L 250 88 75-12597 10 25250ND220243
Thallium ug/L 500 89 75-12598 10 25500ND446493
Vanadium ug/L 500 89 75-12597 9 255004.0J 448 491
Zinc ug/L 500 93 75-12597 3 2550011.4 478 495
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 21 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252037
SURRY SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32002
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92252037001, 92252037002, 92252037003, 92252037005, 92252037006, 92252037007, 92252037008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1475797
Associated Lab Samples:92252037001, 92252037002, 92252037003, 92252037005, 92252037006, 92252037007, 92252037008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/15 16:39
1,1,1-Trichloroethane ug/L ND 1.0 06/04/15 16:39
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/15 16:39
1,1,2-Trichloroethane ug/L ND 1.0 06/04/15 16:39
1,1-Dichloroethane ug/L ND 5.0 06/04/15 16:39
1,1-Dichloroethene ug/L ND 5.0 06/04/15 16:39
1,2,3-Trichloropropane ug/L ND 1.0 06/04/15 16:39
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/15 16:39
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/15 16:39
1,2-Dichlorobenzene ug/L ND 5.0 06/04/15 16:39
1,2-Dichloroethane ug/L ND 1.0 06/04/15 16:39
1,2-Dichloropropane ug/L ND 1.0 06/04/15 16:39
1,3-Dichloropropane ug/L ND 1.0 06/04/15 16:39
1,4-Dichlorobenzene ug/L ND 1.0 06/04/15 16:39
2-Butanone (MEK)ug/L ND 100 06/04/15 16:39
2-Hexanone ug/L ND 50.0 06/04/15 16:39
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/15 16:39
Acetone ug/L ND 100 06/04/15 16:39
Acrylonitrile ug/L ND 200 06/04/15 16:39
Benzene ug/L ND 1.0 06/04/15 16:39
Bromochloromethane ug/L ND 3.0 06/04/15 16:39
Bromodichloromethane ug/L ND 1.0 06/04/15 16:39
Bromoform ug/L ND 3.0 06/04/15 16:39
Bromomethane ug/L ND 10.0 06/04/15 16:39
Carbon disulfide ug/L ND 100 06/04/15 16:39
Carbon tetrachloride ug/L ND 1.0 06/04/15 16:39
Chlorobenzene ug/L ND 3.0 06/04/15 16:39
Chloroethane ug/L ND 10.0 06/04/15 16:39
Chloroform ug/L ND 5.0 06/04/15 16:39
Chloromethane ug/L ND 1.0 06/04/15 16:39
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/15 16:39
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/15 16:39
Dibromochloromethane ug/L ND 3.0 06/04/15 16:39
Dibromomethane ug/L ND 10.0 06/04/15 16:39
Ethylbenzene ug/L ND 1.0 06/04/15 16:39
Iodomethane ug/L ND 10.0 06/04/15 16:39
Methylene Chloride ug/L ND 1.0 06/04/15 16:39
Styrene ug/L ND 1.0 06/04/15 16:39
Tetrachloroethene ug/L ND 1.0 06/04/15 16:39
Toluene ug/L ND 1.0 06/04/15 16:39
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/15 16:39
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252037
SURRY SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1475797
Associated Lab Samples:92252037001, 92252037002, 92252037003, 92252037005, 92252037006, 92252037007, 92252037008
Matrix:Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/15 16:39
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/15 16:39
Trichloroethene ug/L ND 1.0 06/04/15 16:39
Trichlorofluoromethane ug/L ND 1.0 06/04/15 16:39
Vinyl acetate ug/L ND 50.0 06/04/15 16:39
Vinyl chloride ug/L ND 1.0 06/04/15 16:39
Xylene (Total)ug/L ND 5.0 06/04/15 16:39
1,2-Dichloroethane-d4 (S)%98 70-130 06/04/15 16:39
4-Bromofluorobenzene (S)%99 70-130 06/04/15 16:39
Toluene-d8 (S)%100 70-130 06/04/15 16:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1475798LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.650 103 80-125
1,1,1-Trichloroethane ug/L 47.950 96 71-129
1,1,2,2-Tetrachloroethane ug/L 51.850 104 79-124
1,1,2-Trichloroethane ug/L 50.150 100 85-125
1,1-Dichloroethane ug/L 48.450 97 73-126
1,1-Dichloroethene ug/L 48.350 97 66-135
1,2,3-Trichloropropane ug/L 53.150 106 75-130
1,2-Dibromo-3-chloropropane ug/L 49.450 99 71-133
1,2-Dibromoethane (EDB)ug/L 53.450 107 83-124
1,2-Dichlorobenzene ug/L 57.750 115 80-133
1,2-Dichloroethane ug/L 48.650 97 67-128
1,2-Dichloropropane ug/L 49.850 100 75-132
1,3-Dichloropropane ug/L 54.050 108 76-131
1,4-Dichlorobenzene ug/L 55.650 111 78-130
2-Butanone (MEK)ug/L 99.9J100 100 61-144
2-Hexanone ug/L 109100 109 68-143
4-Methyl-2-pentanone (MIBK)ug/L 99.4J100 99 72-135
Acetone ug/L 105100 105 48-146
Acrylonitrile ug/L 241250 96 40-160
Benzene ug/L 51.050 102 80-125
Bromochloromethane ug/L 50.050 100 71-125
Bromodichloromethane ug/L 43.750 87 78-124
Bromoform ug/L 33.9 L0506871-128
Bromomethane ug/L 62.350 125 40-160
Carbon disulfide ug/L 41.7J50 83 50-160
Carbon tetrachloride ug/L 47.150 94 69-131
Chlorobenzene ug/L 54.050 108 81-122
Chloroethane ug/L 46.250 92 39-148
Chloroform ug/L 45.350 91 73-127
Chloromethane ug/L 50.750 101 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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[phone]
Page 23 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252037
SURRY SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1475798LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 50.550 101 74-124
cis-1,3-Dichloropropene ug/L 49.750 99 72-132
Dibromochloromethane ug/L 42.850 86 78-125
Dibromomethane ug/L 50.350 101 82-120
Ethylbenzene ug/L 53.350 107 79-121
Iodomethane ug/L 113100 113 39-154
Methylene Chloride ug/L 55.050 110 64-133
Styrene ug/L 57.150 114 84-126
Tetrachloroethene ug/L 55.050 110 78-122
Toluene ug/L 49.950 100 80-121
trans-1,2-Dichloroethene ug/L 49.050 98 71-127
trans-1,3-Dichloropropene ug/L 50.950 102 69-141
trans-1,4-Dichloro-2-butene ug/L 41.0J50 82 40-160
Trichloroethene ug/L 48.650 97 78-122
Trichlorofluoromethane ug/L 50.150 100 53-137
Vinyl acetate ug/L 106100 106 40-160
Vinyl chloride ug/L 54.550 109 58-137
Xylene (Total)ug/L 161150 107 81-126
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1475800MATRIX SPIKE SAMPLE:
MSSpike
Result
92252070006
1,1,1,2-Tetrachloroethane ug/L 15.220 76 70-130ND
1,1,1-Trichloroethane ug/L 17.720 88 70-130ND
1,1,2,2-Tetrachloroethane ug/L 16.620 83 70-130ND
1,1,2-Trichloroethane ug/L 17.420 87 70-130ND
1,1-Dichloroethane ug/L 18.520 92 70-130ND
1,1-Dichloroethene ug/L 19.320 97 70-166ND
1,2,3-Trichloropropane ug/L 16.820 84 70-130ND
1,2-Dibromo-3-chloropropane ug/L 15.020 75 70-130ND
1,2-Dibromoethane (EDB)ug/L 17.120 85 70-130ND
1,2-Dichlorobenzene ug/L 18.520 92 70-130ND
1,2-Dichloroethane ug/L 17.820 89 70-130ND
1,2-Dichloropropane ug/L 18.120 90 70-130ND
1,3-Dichloropropane ug/L 17.520 88 70-130ND
1,4-Dichlorobenzene ug/L 17.420 87 70-130ND
2-Butanone (MEK)ug/L 37.9J40 95 70-130ND
2-Hexanone ug/L 35.9J40 90 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 35.5J40 89 70-130ND
Acetone ug/L 37.0J40 89 70-130ND
Acrylonitrile ug/L 85.7J100 86 70-130ND
Benzene ug/L 18.720 94 70-148ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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Page 24 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252037
SURRY SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1475800MATRIX SPIKE SAMPLE:
MSSpike
Result
92252070006
Bromochloromethane ug/L 18.920 95 70-130ND
Bromodichloromethane ug/L 14.020 70 70-130ND
Bromoform ug/L 11.8 M0205970-130ND
Bromomethane ug/L 18.820 94 70-130ND
Carbon disulfide ug/L 15.6J20 78 70-130ND
Carbon tetrachloride ug/L 15.620 78 70-130ND
Chlorobenzene ug/L 18.620 93 70-146ND
Chloroethane ug/L 19.720 98 70-130ND
Chloroform ug/L 16.320 81 70-130ND
Chloromethane ug/L 21.820 109 70-130ND
cis-1,2-Dichloroethene ug/L 18.920 95 70-130ND
cis-1,3-Dichloropropene ug/L 15.920 79 70-130ND
Dibromochloromethane ug/L 11.5 M1205870-130ND
Dibromomethane ug/L 17.420 87 70-130ND
Ethylbenzene ug/L 18.220 91 70-130ND
Iodomethane ug/L 41.340 103 70-130ND
Methylene Chloride ug/L 19.820 99 70-130ND
Styrene ug/L 18.820 94 70-130ND
Tetrachloroethene ug/L 18.520 92 70-130ND
Toluene ug/L 18.020 90 70-155ND
trans-1,2-Dichloroethene ug/L 19.120 96 70-130ND
trans-1,3-Dichloropropene ug/L 15.420 77 70-130ND
trans-1,4-Dichloro-2-butene ug/L 14.2J20 71 70-130ND
Trichloroethene ug/L 18.420 92 69-151ND
Trichlorofluoromethane ug/L 19.520 97 70-130ND
Vinyl acetate ug/L 33.2J40 83 70-130ND
Vinyl chloride ug/L 19.720 98 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92252070005
1475799SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.46J 300.46J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L 0.13J 300.14J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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Page 25 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252037
SURRY SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92252070005
1475799SAMPLE DUPLICATE:
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 0.44J 300.42J
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.72J 300.74J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%104 0104
4-Bromofluorobenzene (S)%97 197
Toluene-d8 (S)%102 1102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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Page 26 of 30
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92252037
SURRY SWs
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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[phone]
Page 27 of 30
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92252037
SURRY SWs
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92252037001 MPRP/18601 ICP/16683SW-1 EPA 3010 EPA 6010
92252037002 MPRP/18601 ICP/16683SW-2 EPA 3010 EPA 6010
92252037003 MPRP/18601 ICP/16683SW-3 EPA 3010 EPA 6010
92252037004 MPRP/18601 ICP/16683SW-4 EPA 3010 EPA 6010
92252037005 MPRP/18601 ICP/16683SW-A EPA 3010 EPA 6010
92252037006 MPRP/18601 ICP/16683SW-B EPA 3010 EPA 6010
92252037007 MPRP/18601 ICP/16683SWN-1 EPA 3010 EPA 6010
92252037008 MPRP/18601 ICP/16683SWN-2 EPA 3010 EPA 6010
92252037001 MSV/32002SW-1 EPA 8260
92252037002 MSV/32002SW-2 EPA 8260
92252037003 MSV/32002SW-3 EPA 8260
92252037005 MSV/32002SW-A EPA 8260
92252037006 MSV/32002SW-B EPA 8260
92252037007 MSV/32002SWN-1 EPA 8260
92252037008 MSV/32002SWN-2 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2015 09:12 AM
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Page 28 of 30
Page 29 of 30
Page 30 of 30
#=CL#
June 15, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92252475
92252475
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY BLANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 1 of 20
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92252475
SURRY BLANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 20
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92252475
SURRY BLANKS
Lab ID Sample ID Matrix Date Collected Date Received
92252475001 EB Water 05/29/15 17:55 06/02/15 16:30
92252475002 FB Water 05/29/15 18:00 06/02/15 16:30
92252475003 TB Water 05/29/15 00:00 06/02/15 16:30
REPORT OF LABORATORY ANALYSIS
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Page 3 of 20
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92252475
SURRY BLANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92252475001 EB EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252475002 FB EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW
92252475003 TB EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 4 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252475
SURRY BLANKS
Sample:EB Lab ID:92252475001 Collected:05/29/15 17:55 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 18:28 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 18:28 7440-38-206/03/15 17:1510.0 2.5 1
Barium ND ug/L 06/04/15 18:28 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 18:28 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 18:28 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 18:28 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 18:28 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 18:28 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 18:28 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 18:28 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 18:28 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 18:28 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 18:28 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 18:28 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 18:28 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 16:47 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 16:47 107-13-12001.9 1
Benzene ND ug/L 06/12/15 16:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 16:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 16:47 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 16:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 16:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 16:47 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 16:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 16:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 16:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 16:47 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 16:47 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 16:47 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 16:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 16:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 16:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 16:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 16:47 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 16:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 16:47 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 16:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 16:47 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 16:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 16:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 16:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 16:47 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 16:47 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 16:47 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252475
SURRY BLANKS
Sample:EB Lab ID:92252475001 Collected:05/29/15 17:55 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 16:47 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 16:47 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 16:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 16:47 74-88-410.0 0.32 1
Methylene Chloride 61.2 ug/L 06/12/15 16:47 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 16:47 108-10-11000.33 1
Styrene ND ug/L 06/12/15 16:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 16:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 16:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 16:47 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 16:47 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 16:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 16:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 16:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 16:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 16:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 16:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 16:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 16:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)92 %06/12/15 16:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %06/12/15 16:47 17060-07-070-130 1
Toluene-d8 (S)99 %06/12/15 16:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
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Page 6 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252475
SURRY BLANKS
Sample:FB Lab ID:92252475002 Collected:05/29/15 18:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 06/04/15 18:31 7440-36-006/03/15 17:156.0 3.8 1
Arsenic ND ug/L 06/04/15 18:31 7440-38-206/03/15 17:1510.0 2.5 1
Barium ND ug/L 06/04/15 18:31 7440-39-306/03/15 17:151002.5 1
Beryllium ND ug/L 06/04/15 18:31 7440-41-706/03/15 17:151.0 0.50 1
Cadmium ND ug/L 06/04/15 18:31 7440-43-906/03/15 17:151.0 0.50 1
Chromium ND ug/L 06/04/15 18:31 7440-47-306/03/15 17:1510.0 2.5 1
Cobalt ND ug/L 06/04/15 18:31 7440-48-406/03/15 17:1510.0 2.5 1
Copper ND ug/L 06/04/15 18:31 7440-50-806/03/15 17:1510.0 2.5 1
Lead ND ug/L 06/04/15 18:31 7439-92-106/03/15 17:1510.0 2.5 1
Nickel ND ug/L 06/04/15 18:31 7440-02-006/03/15 17:1550.0 2.5 1
Selenium ND ug/L 06/04/15 18:31 7782-49-206/03/15 17:1510.0 5.0 1
Silver ND ug/L 06/04/15 18:31 7440-22-406/03/15 17:1510.0 2.5 1
Thallium ND ug/L 06/04/15 18:31 7440-28-006/03/15 17:155.5 5.0 1
Vanadium ND ug/L 06/04/15 18:31 7440-62-206/03/15 17:1525.0 2.5 1
Zinc ND ug/L 06/04/15 18:31 7440-66-606/03/15 17:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 17:03 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 17:03 107-13-12001.9 1
Benzene ND ug/L 06/12/15 17:03 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 17:03 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 17:03 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 17:03 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 17:03 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 17:03 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 17:03 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 17:03 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 17:03 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 17:03 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 17:03 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 17:03 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 17:03 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 17:03 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 17:03 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 17:03 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 17:03 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 17:03 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 17:03 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 17:03 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 17:03 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 17:03 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 17:03 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 17:03 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 17:03 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 17:03 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 17:03 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
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Page 7 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252475
SURRY BLANKS
Sample:FB Lab ID:92252475002 Collected:05/29/15 18:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 06/12/15 17:03 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 17:03 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 17:03 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 17:03 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 17:03 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 17:03 108-10-11000.33 1
Styrene ND ug/L 06/12/15 17:03 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 17:03 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 17:03 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 17:03 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 17:03 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 17:03 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 17:03 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 17:03 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 17:03 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 17:03 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 17:03 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/12/15 17:03 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 17:03 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)90 %06/12/15 17:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %06/12/15 17:03 17060-07-070-130 1
Toluene-d8 (S)99 %06/12/15 17:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
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Page 8 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252475
SURRY BLANKS
Sample:TB Lab ID:92252475003 Collected:05/29/15 00:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/12/15 17:19 67-64-110010.0 1
Acrylonitrile ND ug/L 06/12/15 17:19 107-13-12001.9 1
Benzene ND ug/L 06/12/15 17:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/12/15 17:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/12/15 17:19 75-27-41.0 0.18 1
Bromoform ND ug/L 06/12/15 17:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/12/15 17:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/12/15 17:19 78-93-31000.96 1
Carbon disulfide ND ug/L 06/12/15 17:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/12/15 17:19 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/12/15 17:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/12/15 17:19 75-00-310.0 0.54 1
Chloroform ND ug/L 06/12/15 17:19 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/12/15 17:19 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/15 17:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/12/15 17:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/15 17:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/12/15 17:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/12/15 17:19 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/12/15 17:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/12/15 17:19 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/12/15 17:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/12/15 17:19 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 06/12/15 17:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/12/15 17:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/12/15 17:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/12/15 17:19 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/12/15 17:19 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 06/12/15 17:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/12/15 17:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/12/15 17:19 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/12/15 17:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/12/15 17:19 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/12/15 17:19 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/12/15 17:19 108-10-11000.33 1
Styrene ND ug/L 06/12/15 17:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/15 17:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/15 17:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/12/15 17:19 127-18-41.0 0.46 1
Toluene ND ug/L 06/12/15 17:19 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/12/15 17:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/12/15 17:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/12/15 17:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/12/15 17:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/12/15 17:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/12/15 17:19 108-05-450.0 0.35 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
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Page 9 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92252475
SURRY BLANKS
Sample:TB Lab ID:92252475003 Collected:05/29/15 00:00 Received:06/02/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride ND ug/L 06/12/15 17:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/12/15 17:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)89 %06/12/15 17:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %06/12/15 17:19 17060-07-070-130 1
Toluene-d8 (S)97 %06/12/15 17:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252475
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18607
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92252475001, 92252475002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1474278
Associated Lab Samples:92252475001, 92252475002
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 06/04/15 17:08
Arsenic ug/L ND 10.0 06/04/15 17:08
Barium ug/L ND 100 06/04/15 17:08
Beryllium ug/L ND 1.0 06/04/15 17:08
Cadmium ug/L ND 1.0 06/04/15 17:08
Chromium ug/L ND 10.0 06/04/15 17:08
Cobalt ug/L ND 10.0 06/04/15 17:08
Copper ug/L ND 10.0 06/04/15 17:08
Lead ug/L ND 10.0 06/04/15 17:08
Nickel ug/L ND 50.0 06/04/15 17:08
Selenium ug/L ND 10.0 06/04/15 17:08
Silver ug/L ND 10.0 06/04/15 17:08
Thallium ug/L ND 5.5 06/04/15 17:08
Vanadium ug/L ND 25.0 06/04/15 17:08
Zinc ug/L ND 10.0 06/04/15 17:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1474279LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 479500 96 80-120
Arsenic ug/L 456500 91 80-120
Barium ug/L 448500 90 80-120
Beryllium ug/L 450500 90 80-120
Cadmium ug/L 454500 91 80-120
Chromium ug/L 440500 88 80-120
Cobalt ug/L 451500 90 80-120
Copper ug/L 440500 88 80-120
Lead ug/L 447500 89 80-120
Nickel ug/L 451500 90 80-120
Selenium ug/L 432500 86 80-120
Silver ug/L 224250 90 80-120
Thallium ug/L 460500 92 80-120
Vanadium ug/L 435500 87 80-120
Zinc ug/L 449500 90 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252475
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1474280MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92251954001
1474281
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 95 75-12596 1 25500ND478483
Arsenic ug/L 500 91 75-12592 1 25500ND458461
Barium ug/L 500 90 75-12591 1 2550048.4 498 504
Beryllium ug/L 500 91 75-12592 1 25500ND456461
Cadmium ug/L 500 91 75-12592 1 25500ND453458
Chromium ug/L 500 89 75-12589 1 25500ND443447
Cobalt ug/L 500 89 75-12590 1 25500ND446450
Copper ug/L 500 88 75-12589 1 2550011.6 450 454
Lead ug/L 500 88 75-12589 1 25500ND441447
Nickel ug/L 500 89 75-12590 1 255002.7J 448 452
Selenium ug/L 500 85 75-12586 0 25500ND429431
Silver ug/L 250 89 75-12590 1 25250ND223225
Thallium ug/L 500 90 75-12591 1 25500ND451456
Vanadium ug/L 500 87 75-12589 2 25500ND438445
Zinc ug/L 500 89 75-12590 1 2550028.6 473 477
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252475
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32119
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92252475001, 92252475002, 92252475003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1484008
Associated Lab Samples:92252475001, 92252475002, 92252475003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/12/15 14:41
1,1,1-Trichloroethane ug/L ND 1.0 06/12/15 14:41
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/12/15 14:41
1,1,2-Trichloroethane ug/L ND 1.0 06/12/15 14:41
1,1-Dichloroethane ug/L ND 5.0 06/12/15 14:41
1,1-Dichloroethene ug/L ND 5.0 06/12/15 14:41
1,2,3-Trichloropropane ug/L ND 1.0 06/12/15 14:41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/12/15 14:41
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/12/15 14:41
1,2-Dichlorobenzene ug/L ND 5.0 06/12/15 14:41
1,2-Dichloroethane ug/L ND 1.0 06/12/15 14:41
1,2-Dichloropropane ug/L ND 1.0 06/12/15 14:41
1,3-Dichloropropane ug/L ND 1.0 06/12/15 14:41
1,4-Dichlorobenzene ug/L ND 1.0 06/12/15 14:41
2-Butanone (MEK)ug/L ND 100 06/12/15 14:41
2-Hexanone ug/L ND 50.0 06/12/15 14:41
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/12/15 14:41
Acetone ug/L ND 100 06/12/15 14:41
Acrylonitrile ug/L ND 200 06/12/15 14:41
Benzene ug/L ND 1.0 06/12/15 14:41
Bromochloromethane ug/L ND 3.0 06/12/15 14:41
Bromodichloromethane ug/L ND 1.0 06/12/15 14:41
Bromoform ug/L ND 3.0 06/12/15 14:41
Bromomethane ug/L ND 10.0 06/12/15 14:41
Carbon disulfide ug/L ND 100 06/12/15 14:41
Carbon tetrachloride ug/L ND 1.0 06/12/15 14:41
Chlorobenzene ug/L ND 3.0 06/12/15 14:41
Chloroethane ug/L ND 10.0 06/12/15 14:41
Chloroform ug/L ND 5.0 06/12/15 14:41
Chloromethane ug/L ND 1.0 06/12/15 14:41
cis-1,2-Dichloroethene ug/L ND 5.0 06/12/15 14:41
cis-1,3-Dichloropropene ug/L ND 1.0 06/12/15 14:41
Dibromochloromethane ug/L ND 3.0 06/12/15 14:41
Dibromomethane ug/L ND 10.0 06/12/15 14:41
Ethylbenzene ug/L ND 1.0 06/12/15 14:41
Iodomethane ug/L ND 10.0 06/12/15 14:41
Methylene Chloride ug/L ND 1.0 06/12/15 14:41
Styrene ug/L ND 1.0 06/12/15 14:41
Tetrachloroethene ug/L ND 1.0 06/12/15 14:41
Toluene ug/L ND 1.0 06/12/15 14:41
trans-1,2-Dichloroethene ug/L ND 5.0 06/12/15 14:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252475
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1484008
Associated Lab Samples:92252475001, 92252475002, 92252475003
Matrix:Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 06/12/15 14:41
trans-1,4-Dichloro-2-butene ug/L ND 100 06/12/15 14:41
Trichloroethene ug/L ND 1.0 06/12/15 14:41
Trichlorofluoromethane ug/L ND 1.0 06/12/15 14:41
Vinyl acetate ug/L ND 50.0 06/12/15 14:41
Vinyl chloride ug/L ND 1.0 06/12/15 14:41
Xylene (Total)ug/L ND 5.0 06/12/15 14:41
1,2-Dichloroethane-d4 (S)%91 70-130 06/12/15 14:41
4-Bromofluorobenzene (S)%91 70-130 06/12/15 14:41
Toluene-d8 (S)%98 70-130 06/12/15 14:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1484009LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.850 110 80-125
1,1,1-Trichloroethane ug/L 61.050 122 71-129
1,1,2,2-Tetrachloroethane ug/L 53.750 107 79-124
1,1,2-Trichloroethane ug/L 53.250 106 85-125
1,1-Dichloroethane ug/L 57.450 115 73-126
1,1-Dichloroethene ug/L 57.050 114 66-135
1,2,3-Trichloropropane ug/L 52.350 105 75-130
1,2-Dibromo-3-chloropropane ug/L 51.550 103 71-133
1,2-Dibromoethane (EDB)ug/L 55.150 110 83-124
1,2-Dichlorobenzene ug/L 54.450 109 80-133
1,2-Dichloroethane ug/L 54.650 109 67-128
1,2-Dichloropropane ug/L 55.850 112 75-132
1,3-Dichloropropane ug/L 54.350 109 76-131
1,4-Dichlorobenzene ug/L 54.150 108 78-130
2-Butanone (MEK)ug/L 113100 113 61-144
2-Hexanone ug/L 100100 100 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 115100 115 48-146
Acrylonitrile ug/L 291250 116 40-160
Benzene ug/L 56.950 114 80-125
Bromochloromethane ug/L 60.650 121 71-125
Bromodichloromethane ug/L 51.150 102 78-124
Bromoform ug/L 49.650 99 71-128
Bromomethane ug/L 54.150 108 40-160
Carbon disulfide ug/L 53.6J50 107 50-160
Carbon tetrachloride ug/L 58.550 117 69-131
Chlorobenzene ug/L 54.350 109 81-122
Chloroethane ug/L 45.650 91 39-148
Chloroform ug/L 52.350 105 73-127
Chloromethane ug/L 51.250 102 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
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9800 Kincey Ave. Suite 100
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Page 14 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252475
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1484009LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 61.550 123 74-124
cis-1,3-Dichloropropene ug/L 54.950 110 72-132
Dibromochloromethane ug/L 48.350 97 78-125
Dibromomethane ug/L 53.550 107 82-120
Ethylbenzene ug/L 53.650 107 79-121
Iodomethane ug/L 104100 104 39-154
Methylene Chloride ug/L 63.250 126 64-133
Styrene ug/L 55.250 110 84-126
Tetrachloroethene ug/L 55.250 110 78-122
Toluene ug/L 54.450 109 80-121
trans-1,2-Dichloroethene ug/L 58.650 117 71-127
trans-1,3-Dichloropropene ug/L 55.650 111 69-141
trans-1,4-Dichloro-2-butene ug/L 55.1J50 110 40-160
Trichloroethene ug/L 53.350 107 78-122
Trichlorofluoromethane ug/L 49.250 98 53-137
Vinyl acetate ug/L 110100 110 40-160
Vinyl chloride ug/L 55.250 110 58-137
Xylene (Total)ug/L 160150 107 81-126
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1484010MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92252725003
1484011
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 107 70-130115 7 3020ND21.4 23.0
1,1,1-Trichloroethane ug/L M12011970-130131 9 3020ND23.9 26.1
1,1,2,2-Tetrachloroethane ug/L 20 100 70-130104 4 3020ND19.9 20.8
1,1,2-Trichloroethane ug/L 20 109 70-130114 4 3020ND21.8 22.7
1,1-Dichloroethane ug/L 20 116 70-130120 4 30200.40J 23.6 24.4
1,1-Dichloroethene ug/L 20 129 70-166135 4 3020ND25.8 27.0
1,2,3-Trichloropropane ug/L 20 106 70-130106 0 3020ND21.2 21.3
1,2-Dibromo-3-
chloropropane ug/L 20 92 70-130102 10 3020ND18.4 20.5
1,2-Dibromoethane (EDB)ug/L 20 113 70-130119 6 3020ND22.5 23.8
1,2-Dichlorobenzene ug/L 20 115 70-130118 3 3020ND23.1 23.7
1,2-Dichloroethane ug/L 20 96 70-130100 3 30200.80J 20.1 20.8
1,2-Dichloropropane ug/L 20 120 70-130123 2 30200.74J 24.8 25.3
1,3-Dichloropropane ug/L 20 109 70-130115 5 3020ND21.8 23.0
1,4-Dichlorobenzene ug/L 20 117 70-130118 0 30203.1 26.6 26.7
2-Butanone (MEK)ug/L 40 95 70-130101 6 3040ND38.0J 40.4J
2-Hexanone ug/L 40 101 70-130107 7 3040ND40.2J 43.0J
4-Methyl-2-pentanone
(MIBK)ug/L 40 100 70-130108 8 3040ND39.9J 43.1J
Acetone ug/L 40 95 70-130103 7 3040ND41.6J 44.8J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92252475
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1484010MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92252725003
1484011
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acrylonitrile ug/L 100 108 70-130113 5 30100ND109J114J
Benzene ug/L 20 121 70-148130 7 30200.83J 25.1 26.8
Bromochloromethane ug/L M12012570-130131 5 3020ND25.0 26.2
Bromodichloromethane ug/L 20 104 70-130105 1 3020ND20.9 21.0
Bromoform ug/L 20 89 70-13094 6 3020ND17.7 18.8
Bromomethane ug/L 20 122 70-130109 11 3020ND24.4 21.9
Carbon disulfide ug/L 20 128 70-130126 2 3020ND25.7J 25.2J
Carbon tetrachloride ug/L 20 125 70-130130 5 3020ND24.9 26.1
Chlorobenzene ug/L 20 117 70-146121 3 30202.9 26.3 27.2
Chloroethane ug/L M12013170-130138 5 3020ND26.2 27.5
Chloroform ug/L 20 106 70-130111 4 3020ND21.3 22.2
Chloromethane ug/L 20 110 70-130115 4 30200.22J 22.3 23.1
cis-1,2-Dichloroethene ug/L 20 119 70-130129 7 30205.6 29.4 31.4
cis-1,3-Dichloropropene ug/L 20 117 70-130121 4 3020ND23.3 24.2
Dibromochloromethane ug/L 20 93 70-13098 6 3020ND18.5 19.6
Dibromomethane ug/L 20 112 70-130114 1 3020ND22.5 22.7
Ethylbenzene ug/L 20 112 70-130117 5 3020ND22.3 23.4
Iodomethane ug/L 40 84 70-130105 22 3040ND33.7 42.2
Methylene Chloride ug/L 20 103 70-130109 5 3020ND20.6 21.7
Styrene ug/L 20 116 70-130118 2 3020ND23.1 23.6
Tetrachloroethene ug/L 20 123 70-130129 5 3020ND24.6 25.8
Toluene ug/L 20 115 70-155119 3 3020ND23.1 23.7
trans-1,2-Dichloroethene ug/L 20 118 70-130123 4 3020ND23.6 24.6
trans-1,3-Dichloropropene ug/L 20 105 70-130110 5 3020ND20.9 22.1
trans-1,4-Dichloro-2-butene ug/L 20 98 70-130102 4 3020ND19.6J 20.3J
Trichloroethene ug/L 20 123 69-151129 5 3020ND24.9 26.1
Trichlorofluoromethane ug/L 20 122 70-130124 2 3020ND24.5 24.9
Vinyl acetate ug/L 40 92 70-13094 2 3040ND36.6J 37.5J
Vinyl chloride ug/L M12013170-130139 6 30201.2 27.4 29.0
1,2-Dichloroethane-d4 (S)%89 70-13096
4-Bromofluorobenzene (S)%93 70-13093
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 20
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92252475
SURRY BLANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 20
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92252475
SURRY BLANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92252475001 MPRP/18607 ICP/16689EBEPA 3010 EPA 6010
92252475002 MPRP/18607 ICP/16689FBEPA 3010 EPA 6010
92252475001 MSV/32119EBEPA 8260
92252475002 MSV/32119FBEPA 8260
92252475003 MSV/32119TBEPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/15/2015 02:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 20
Page 19 of 20
Page 20 of 20
Appendix B
Field Sampling Parameter Data Sheet(s)