Item No 36 - NFA Letter - Indcident No 36354 Morehead Common-OCR

NCDENR
North Carolina Department of Environment and Natural Resources
MchaeI Easey Governor Division of Waste ManagementWitUamRossJrSecretaryUndergroundStorageTankSection Dexter Matthews Director
August 27 2007
Beazer Homes
1300 South Boulevard Suite
Charlotte North Carolina 28203-4265
Attention Mr Jade Eastridge
Re Notice of No Further Action
5A NCAC 2L 0407d
Risk-based Assessment and Corrective Action
for Petroleum Underground Storage Tanks
Morehead Common Area
1000 South Clarkson Street Charlotte
Mecklenburg County
Incident Number 36354
Risk Classification Low
Dear Mr Eastridge
The Initial Abatement Action report received by the Underground Storage Tank UST Section
Mooresville RegiOnal Office on August 24 2007 has been reviewed The review indicates that after tank
closure and soil excavation soil contamination does not exceed the lower of the soil-to-groundwater or
residential maximum soil contaminant concentrations MSCCs established in Title iSA NCAC 2L
.0411
The UST Section determines that no further action is warranted for this incident This
determination shall apply unless the UST Section later finds that the discharge or release poses an
unacceptable risk or potentially unacceptable risk to human health or the environment Pursuant to Title
ISA NCAC 2L .0407a you have continuing obligation
to notify the Department of any changes
that
might affect the risk or land use classifications that have been assigned
This No Further Action determination applies only to the subject incident
for any other incidents
at the subject site the responsible party must continue to address contamination as required
If you have any questions regarding
this notice please contact me at the address or telephonenumberlistedbelow
Hydrogeologist
Mooresville Regional Office
Afl5.cvfiMIiftPrct nnsurnr Prr
Prepared For
NCDEN1
USTSection-MRO
919 North Main Street
Mooresville North Carolina 28115
Prepared By
ESP Associates P.A
P.O Box 7030
Charlotte North Carolina 28241
August 23 2007
NCDENR
UST Section
Mooresville Regional Office
919 North Main Street
Mooresville North Carolina 28115
Attention Mr Allen Schiff
INITIAL ABATEMENT ACTION REPORT
Morehead Common Site Area
1000 South Clarkson Street
Charlotte Meeldenburg County North Carolina
UST Incident No No Yet Assigned
ESP Project No E6-UD42601
Dear Mr Schiff
On behalf of the property owner l3eazer Homes ESP Associates P.A is pleased to provide the
attached Initial Abatement Action Report for the closure of the subject propertys petroleum
release ESP respectively requests classification of the release as Low Risk and issuance of no
further action notice
Thank you for your attention in this matter If you should have any questions please do not
hesitate to contact me at 803 835-0915
Sincerely
ESPAssocjafes P.4
Edgar Roge PG
Staff Scientist Environmental Services ManagerNCLicenseNo1600
cc Mr Jade Eastridge Beazer Homes
P.O Box 7030 Charjoue NC 28241
1.800.960.7317 NC 704.583.4949 fax [phone] SC 803.802.2440 fax [phone]
Www.eSpassocjates corn
$ESP
ESP Associates P.A August 23 2007
Reference
Initial Abatement Action Report
SITE INFORMATION
Site Identification
Date of Report August 23 2007
Facility ID NA
UST Incident Number Not Yet Assigned
Site Name Morehead Common Site Area
Site Street Address 1000 South Clarkson Street
City/County/Zip Code Charlotte Mecklenburg County 28278
Description of Geographical Data Point Approximate center of UST
Location Method Mecklenburg County Polaris GIS Map
Latitude 35227104
Longitude -80.858606
Information about Contacts Associated with the Leaking UST SystemUSTOwnerBeazerHomes
1300 Blvd Suite Charlotte NC 28203-4265
704.370.7200
UST Operator N/A
Property Owner Same as above
Property Occupant Same as above
El Consultant/Contractor ESP Associates PA Chris Ward PG
P0 Box 7030 Charlotte NC 28241
803.835.0915
Analytical Laboratory Prism Laboratories Inc
P0 Box 240543 Charlotte NC 28224-0403
704.529.6364
NC Certification No 402
Information about Release
Date Discovered August 2007
Estimated Quantity of Release Unknown
Cause of Release Unknown
Source of Release UST
Size and contents of UST
System from which release occurred 1300-Gallon Diesel UST
Certification
is Ward Professional Geologist for ESP Associates P.A do certify that the
contained in this report is correct and accurate to the best of my knowledge
P.A is licensed to practice both geology and engineering in North Carolina
certification numbers are Geology C-347 and Engineering C-0587
Initial Abatement Action Report ESP Project E6-UD42 601
More/wad common Site Area August 23 2007
iNTRODUCTION
The subject site location of fonner Duke Energy-Worth Keeter facility has an address of 1000
South Clarkson Street in Charlotte Mecklenburg County North Carolina see Figure
Topographic Site Location Map The area of the subject release associated with 1300-gallon
diesel underground storage tank UST uncovered on August 2007 has been designated by
ESP as Area of the Morehead Common site
SITE HISTORY ANT CHARACTERIZATION
On August 2007 ESP responded on behalf of Beazer Homes to an encounter with UST and
impacted soil during mass grading operations at the subject site Upon arriving at the site ESP
observed 1300-gallon steel apparent diesel UST along with soils with petroleum odor located
on the west side of South Clarkson Street approximately 300 feet south of its intersection with
West Morehead Street on Tax Parcel No 07325207 see Figures and As required ESP
emailed notification of the release discovery along
with Release and USTLeak Reporting Form
to Mr Steve Bograd of the Mooresville Regional Office of NCDENR on August 2007
Release Location
The subject site is located within an urban area of Charlotte which historically included
warehouse and commercial structures The site the former location of Duke Energy-Worth
Keeter Inc was recently mass graded and is currently being developed as mixed-use
residential/commercial development see Figures and Previously documented UST
Incidents on the subject parcel include Incidents Nos 18101 9567 and 36331 Locations of
these two previously documented incidents relative to the subject release Area are depicted
on Figure
Initial Abatement Action Report ESP Project E6-UD42.601
Morehead Common Site Area August 23 2007
Based on our review of the Geologic Map of North Carolina 1985 the subject site is located
within the Charlotte Belt locally comprised of intrusive metamorphosed granitic rocks locally
pinkish gray massive to wealdy foliated and containing horublende Soils encountered in this
area are
the residual product of chemical weathering of rock presently underlying
the site Soil
weathering is more advanced near the surface grading with depth to less weathered rock and
finally bedrock
UST Information
Following the August 2007 discovery of 1300-gallon diesel UST AD Environmental and
Industrial Services AD of High Point North Carolina was contacted to remove remaining
product/sludge from the tank following its removal from the excavation On August 2007
AD pumped 77 gallons of product/sludge from the tank for permitted recycling
at their
Archdale North Carolina facility see Product Material Manifest in Appendix Once
removed the tank was transported by AD to the Griffin recycling facility in Greensboro
North Carolina on August 2007 see Tank Disposal Manifest in Appendix See site
photographs in Appendix
PreviousTankInstallationRemovalSizeTankLastTankNoDateDateGallonsDimensionsContentsContents
Unknown 8-1-07 1300 12 ft 4.3 ft Diesel Unknown
completed UST-2 Form is included as Appendix The former location of the above UST is
depicted on Figure
Previous Reporting
ESP ernailed release notification along with 24-Hour Release and UST Leak Reporting Form
to the Mooresville Regional Office of NCDENR on August 2007 see Appendix
Initial Abatement Action Report ESP Project E6-UD42.601
Morehead common Site Area August 23 2007
INITIAL ABATEMENT ACT WITIES
Contaminated Soil Excavation
On August and 2007 ESP documented the excavation of 39i4 tons of impacted soil from
Area by the sites grading contractor Gelder Thompson of Midland North Carolina The
excavation was advanced based on results of OVA field screening and evidence of visible
staining The resulting excavation measured approximately ft 18 ft ft deep The
excavated soil was placed on and covered with plastic awaiting subsequent off-site permitted
disposal Neither groundwater bedrock nor free product were encountered within the tank pit
See site photographs in Appendix
Post-Excavation Confirmatory Sampling
On August 2007 confirmatory soil samples were collected at depth of 3.5 feet BLS from
each of the excavations four sides WS-l through WS-4 while one sample was collected at
depth of feet BLS from the base of the excavation B-i The sidewall samples were collected
at the 3.5 foot depth due to the prevalence of elevated OVA readings at that depth The five soil
samples were hand delivered on ice to Prism Laboratories of Charlotte North Carolina to be
analyzed for risk-based parameters which include volatile organic compounds VOCs by EPA
Method 8260B semi-volatile organic compounds SVOCs by EPA Method 8270C VPHIEPH
by the Massachusetts Department of Environmental Protection MADEP method and for total
lead and chromium by EPA Method 601013 Sample locations and excavation dimensions are
depicted on Figure Soil Sample Location Map Sampling was performed in general
accordance with ESPs SOP see Appendix
Results of the laboratory analysis
of confirmatory samples WS-l through WS-4 and B-i revealed
that all analyzed constituents were either below reporting limits BRLs or below the lowest of
the soil-to-groundwater or residential MSCC Laboratory analytical results for the confirmatory
soil samples are summarized on Table B-i The Prism laboratory data report is included as
Appendix
hitia Abatement Action Report ES Project E6-VD42 601
Morehead Common Site Area August 23 2007
Stockpile Sampling and Soil Disposal
On August 2007 ES collected composite stockpile soil sample for laboratory analysis
The
stockpile soil sample designated lA/lB was placed in laboratory provided containers labeled
and hand delivered on ice to Prism for compositing and subsequent analysis The sample was
analyzed for total petroleum hydrocarbons TPH for gasoline range organics GRO and diesel
range organics DRO by EPA Method 5030/3550 and for BTEX by EPA Method 8260B The
composite sample was collected and analyzed to confirm that release had occurred and to
characterize contaminant types and concentrations for subsequent off-site permitted
disposal/treatment
As revealed by the laboratory analysis of stockpile composite soil sample IA/1B TPH-DRO was
reported at concentration of 710 mg/Kg and TPH-GRO at concentration of 6.9 mg/Kg while
results for the remainder of analytes were BRLs Results of the stockpile sample analyses are
summarized on Table B-2 while the laboratory data report is included as Appendix
On August 16 and 17 2007
39.14 tons of stockpiled soil from the Area excavation was
transported by Gelder Thompson to the CMS Landfill in Concord North Carolina for permitted
disposal see Non-Hazardous Waste Manifest in Appendix
RECEPTOR SURVEY
On July 20 2007 Mr Eddie Rogers of ES performed receptor survey to document the
presence or absence of active and/or inactive water supply wells within 1500-foot radius of the
subject UST release see Figure Receptor Survey Map The receptor survey included
interviews with available site occupants and visual observations for water supply wells and/or
municipal water meters All properties within 500 feet of the site were visited to determine well
status The area within 1000 feet of the subject release consists of commercial and industrial
development with numerous vacant structures No active or inactive water supply wells were
identified within 1000-foot radius of the subject release Municipal water and sewer have
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area August 23 2007
historically been available within the area of the site Additionally no surface water bodies were
identified within 500 feet of the release see Figure
CONCLUSIONS AND RECOMMENDATIONS
The following conclusions have been formulated based on our completion of field activities
including abatement activities receptor survey and our review of laboratory data from the
analysis of collected soil samples
The subject site the location of former Duke Energy-Worth Keeter facility has an
address of 1000 South Clarkson Street Tax Parcel No 07325207 in Charlotte
Mecklenburg County North Carolina
On August 2007 ESP responded on behalf of Beazer Homes to an encounter with
1300-gallon steel apparent diesel UST along with soils with petroleum odor during
mass grading operations
at the subject site
On August and 2007 ESP documented the excavation of 39.14 tons of impacted
soils from the release area The resulting excavation measured approximately ft 18 ft
ft deep
Neither groundwater bedrock nor free product were encountered within the tank pit
On August 2007 confirmatory soil samples were collected at depth of 3.5 feet BLS
from each of the excavations four sides WS-l through WS-4 while one sample was
collected at depth of feet BLS from the base of the excavation B-i
Results of the laboratory analysis of confirmatory samples WS-i through WS-4 and B-i
revealed that all analyzed constituents were either below reporting limits BRLs or
below the lowest of the soil-to-groundwater or residential MSCC
ci On August 2007 ESP collected composite stockpile soil sample designated IA/IB
for laboratory analysis The composite sample was collected and analyzed to confirm
that release had occurred and to characterize contaminant types and concentrations for
subsequent off.site permitted disposal/treatment
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead common Site Area August 23 2007
As revealed by the laboratory analysis of stockpile composite sample 1A/1IB TPH-DRO
was reported at concentration of 710 mg/Kg and TPH-GRO at concentration of 6.9
mg/Kg while results for the remainder of analytes were BRLs
On August 16 and 17 2007
39.14 tons of stockpiled soil from the Area excavation was
transported to the CMS Landfill in Concord North Carolina for permitted disposal
Municipal water and sewer are available in the area of the release
No water supply wells were identified within 1000 feet of the release and
No surface water bodies were identified Within 500 feet of the subject release
Based on the absence of analyzed risk-based soil parameters above the lowest of the North
Carolina soil-to-groundwater or residential MSCCs lack of either groundwater bedrock
or free
product within the tank pit the documented absence of water supply wells within 1000 feet of
the release and the absence of surface water feature within 500 feet of the release ESP
recommends that NCDENR issue notice of no further action for the subject release
Attachments
Table B-i Summary of Soil Sampling Results
Table B-2 Summary of Stockpile Soil Sampling Results
Figure Topographic Site Location Map
Figure 2005 Aerial Photograph
Figure Soil Sample Location Map
Figure 4-Receptor Survey Map
Appendix 24-Hour Release Notification
Appendix UST-2 Form
Appendix Tank Disposal Manifest
Appendix Product Material Manifest
Appendix Site Photographs
Appendix ESPs SOP
Appendix Prism Laboratory Data Reports
Appendix Non-Hazardous Waste Manifests
ATTACHMENTS
TABLES
4-
4-
bO r-
4-0
II IE
C/D 4-
II
Us
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered iirirnobileNANotAnalyzedNL Not Listed
Table B-I
Date 8/20/07
Suirunary of Soil Sampling Results
Incident No Not Yet Assigned Morehead Common Area Charlotte North
Analytical Method 8260B 8260B 8270C 8270C 8270C 8270C 827CC 8270C 8270C 8270C
Contaminant of Concern
I_____..
Collthd rei niple
.Deith
ft EGS
Incident
Phase
8/2/07 South Pit
Wall
Initial
Abatement 00051 0.0051 0.25 0.32J 0.17 0.16 0.161 0.191 0.17 037
8/2/07 West Pit
Wall
Initial
Abatement 00050 0.0050 0.37 0.37 0.37 0.37 0.37 0.37 037 037
8/2/07 North Pzt
Wall
Initial
Abatement 0.0048 0.0048 0.17J O.21J 0.1 0.101 0.37 0.37 0.37 0.25
8/2107 Last Pit
Wall
Initial
Abatement 00144 0.0044 0.28J 0.331 0.141 0.163 0.143 0141 0171 0.361
8/2/07 Pit Floor Initial
Abatement 0.0052 0.0052 0.37 0.37 0.37 0.37 0.37 0.37 0.37 037
MSCC mg/kg 60 290 38 034 0091 12 280
MSCçjnigfkg 3129 200 469 459 88 88 00088 88 620
MSCC mg/kg 81750 82000 12254 12 264 780 078 78 16400
kg
3RL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported hi mg/kg unless otherwise noted
Health based tevel 100%
Considered immobileNANotAnalyzedNL Not Listed
Table B-2
Date 8/20/07
FIGURES
6tJpISHEET177LE F1GURE2ALEN752005AERIALPHOTOGRAPH
AW1 BrDMH PROJECT MOREHEAD COMMON SITEIECICED
CHARLOTTE NORTH CAROLINA
WS-3 B-i
WS-2 ____WS-4
ws-1
LEGEND
DUNBAR STREET
1CONFJRMA TORY SOIL SAMPLE LOCA T1ON
FORMER LOCA flON OF UST
AREA EXCA VA flON DEPTH OF FEET 2tY
APPIOX SCALE
ESP
PDESP
TL4JLI IVUUD4240
ALE NTh
8/27/074MW8TDMH
IEQB2 BYcw
SHEET FiGURE
SCYL SAMPLE LOCA liON MAP AREA
PROJECT MOREHEAD COMMON S17
CHARLOTIE NORTH CAROUNA
APPENDIX
24-HOUR RELEASE NOTIFICATION
UST-61 24Hour Release and UST Leak Reporting Form
For ReIeses This form should be completed and submitted to the UST Sectlons regional office loflowing known or suspected release from
an underground storage tank UST system This form is required to be submiLled within 24 hours of discovery of known or
ka HG suspected release
DWM USE ONLY Suspected ContamInation YIN Facility ID Number 0ic1L13
incident Risk I-IlLU______Conlirmed GW Contamination YIN 1I Date Leak Discovered
Received On Received By Conlirmed Sail Contamination YIN A/Comm/Non-Commercial rciffl
Reported by circle one Phones Fax or Report Free Product YIN 11 Yes Stale Greatest Reg/Men-regulated
Region Thickness
INCIDENT DESCRIPTION
Incident Name
Address /080 5ii/æittd Tt67 County
Regional Office circle one AshevlII1ltŁsvillgFaye1teviIle
CRy/Town Zip COCta Z23 Raleigh WashIngton Wilmington WIitOrFS1em
Latitude Lfitnni i-Longitude f55 Obtained by
BrieRy describe suspected or confirmed release.-including but not ftuiled to nature of release date of release amount GPS
atm/ease amount of Tree product present
and recovery elbrts intl/al responses conducted impacts to receptors
477 c4 %i 8ec-4jL4 /Jd Topographic maphJurEGlSAddressmatching
Other
Unknown-ppp Describe lace Lion1octcce-tHOWRELEASEWAS DICOVERED
Check one
During UST Closure/Removal Cl Water in Tank Surface Water Contamination
Release Detection Equipment or Methods Visual/Odor CI Groundwater Contamination
Li Property Transfer LI Water Supply Well Contamination J4 Other specity1//Ll
SOURCE OF CONTAMINATION
P_riniarv Source of Contamination Primary Contaminant Tvua Location ting
Check one Checkone Checkone
Gasollne/flleseWerosene acility Residential
Continued UST Release Check one below Heating Cli Residence CI Industrial
Dispenser Other Petroleum Products MOther UrbanLineReleaseMSIaiSRuralTankReleaseOtherinorganicsCIliSpHu/OverliR Other OrganicsExactFailureLocationUnknownor
Multiple Failures
Ownership
Municipal Military Unknown 4ale Federal County State
flpemliori Tvne
PublicService AgrIcultural EducaiionlRalig Industrial MIning
USI t-orjnb1 11/05 Page of2
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Welts Affected 1.Yes riri
Number at Water Supply Wells Attested MU-WI7it/IJ
Water Supply Wells Contaminated Include VEers Names Addresses and Phone Numbers Atlach addional.sheet Unessaj
Point of Contact/11W 6reicc
Gly SlateCIZ277a NC
UST SYSTEM OPERATOR
UST
ciperatorlcani7y
StateCity
Aaurass
Zip Code elepnone Number
LANDOWNER AT LOCATIO
Landowner4iWe %-5
CIty ilate
9OFUSTINCIDENT
Address
Zip uone Telephone umoer
Draw Sketch of Area showing two major road intersections or Attach Map
k714llD 4t9
Person Reporting Incident Chr15 1Jai4 Company 5/J ft Telephone Number50hUeAddressODale
LIST Farm 1105
UST SYSTEM OWNER
LIST Ownerlcornpany
Address
v2 fTºIC
Zip Coue Telephone Number
Page of
APPENDIX
UST-2 FORM
APPENDIX
TANK DISPOSAL MANIFEST
APPENDIX
PRODUCT MATERIAL MANIFEST
AO1OIi
4Manifcst Docurient NoMATERIALEnvironmentaland
..-
ivi ANIFEST IndustrialServices Inc of
EMERGENCY PHONE NO POST OFFICE BOX 484 TEl [phone] Job No
800 434 7750
HIGH POINTNC 27261 FAX [phone]
.-GENERATOR INFORMATION
Name ..-USEPA ID No
StreeL Address Phone No
9j-t t4I1 -f_c1jC1C-Cont7y %v
DESCRIPTION OF MATERIALS
USDOT.Proper Shipping Name Hazard UN NA Packing Containers Total Unit
HM Complete Alt Items br Hazardous Materials Class or Div tD No Group Qty Type Quantity WtJ VolL/O4ck-5 1.dAk P4 /V4 .77
-DDITiOPJAL INFORMATION ERG No Profile Code acJtIty Use
L2 5r çL4e jr
3ENERATORS CERTIFiCATION
hisis to certify that the above-described materials are properly classified described packaged marked and labeled and a7i
roper condition for transportation according to the applicable regulations of the Department of Transportation.further certifyhatnoneof the materials described above are hazardous waste as defined by EPA 40 CFR Part 261 or.any applicable
state lawndunlessspecificallyidentifiedabovethematerials contain less than 1000 ppm total halogens and don at contain quantifiableevels2.pprn of PCBs as defined by EPA 40 CFR Parts 279 and 761
rinted Typed Name Signature Mo IDay Y.
....
TRANSPORTER lNFOMATiON
ransporter Ilherebv acknowledge recelpfof the above-described materials or tran5 portENVIRONv.IENTAL AND NDUSTRLAL SERVICES Jfrorn the generator silo listed above
ctdress
718 UWHARR1EROA
RCHDALE NC 27263 __Jlhereby acknowledge tihe above-desÆrlbed materials were received
ru1sporter or Unit No from thi generator site and were transported toihe facil/ty hEed belowPAIDNoNCD986232221/1
ione 336 434-7750
Signature
FACILITY INFORMATION
acuity hereby acknowledge receipt of the materials covered by this manifestENVIRONMENTALANDINDUSTRIAL SERVICES Æxcept for any discrepancy noted blowddress
718 1JWHARRIE ROADtTS.Tf-Signature Receipt DateI%1UJ.IL.j 1.rDIscØpaijciesJ Routing Codes .HindtinMethOd
acility or .L
PA ID No NCD986232221
hone 336 434-7750
ERIC McMANUS
ORIGINAL Facility Retain COPY Return to Generator COPY .-Trnsr4pr PpI.in OV
APPENDIX
SITE PHOTOGRAPHS
MOREHEAD COMMON SITE AREA
VIEW OF 1.300-GALLON DIESEL UST BEING PUMPED OF
REMAINING PRODUCT/SLUDGE
VIEW OF 1.300-GALLON DIESEL UST ON SIDE OF FORMER
TANK PIT LOOKING NORTHEAST
VIEW OF SEVERAL HOLES WITHIN SIDE OF liST
STANbARb OPERATING PROCEbURE
Sop -6
SOIL SAMPLE COLLECTION
ESP Associates P.A Revision bate 3/7/06
This standard operating procedure SOP covers the collection of soil sample for
laboratory analysis
Follow these steps when collecting the soil sample unless
otherwise instructed by the project manager
Gather needed field supplies noted below
Confirm lab cooler contains needed sample containers fill cooler with
ice
Upon arriving at site check in with the property owner or company
representative
Decontaminate the stainless steel hand auger before and between sample
collection by washing with Alconox soap and scrub brush rinsing with
distilled water and spraying with Isopropyl alcohol Wrap clean sampler
in aluminum foil
Wear disposal latex or nitrile gloves and change into new pair between
samples
During advancement of the hand auger collect soil samples at regular
intervals for describing lithology Note lithology and other
characteristics of soils in field book relative to depth
If appropriate place representative portion of soil sample into
resealable plastic buy label with boring number and depth interval and
allow to equilibrate Screen soil in bag for volatile organics using an OVA
or Hnu Enter results into field book
Advance hand auger boring to previously specified sampling depth
Collect soil sample from this depth and place in laboratory provided
containers Label containers with boring number and sample depth using
the following sampling scheme i.e -1 ft -1 10 ft -2 ft etc
benote boring location in field book relevant to pertinent site features
10 Following collection of the soil samples abandon all boreholes feet or
greater in depth with cement grout
11 Complete and sign the labs chain-of-custody12Keepthesamplecoolerinsecurelocation until delivered under normal
chain-of-custody procedures to laboratory
SOP-6 Soil 5amp/e Collection Revision bate 3/7/06
ESP Associates Page of
SUPPLIES
ci SOP-6
Stainless steel hand auger with needed extensions or sampling
spoon
ci OVA orHnu
ci Measuring tape
ci Plastic zip-lock bags
ci Isopropyl alcohol
ci bistilted water
ci 5-gallon wash bucket scrub brush and Alconox soap
ci Cement with wheel barrow for mixing
ci Cooler with sample containers and chain-of-custody
Ice
ci Permanent marker
bisposable gloves
ci Knife
Field book
ci Site plan with site specific sampling instructions
Camera
APPENDIX
PRISM LABORATORY DATA REPORTS
Case NarrativePRISM
E.OflfiTOflIESINC
Date 08/10107 Cftent Project ID Morehead Commons No
Company ESP Associates PA Prism CCC Group No G0807064
Contact Chris Ward Collection Dates 0802107
Address P.O BOX 7030 Lab Submittal Dates 08102/07
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and Quality
Control Data totaling 44 pages chain-of-custody is also attached far the samples submitted to Prism Ear this project
Data qualifiers are flagged individually on each sample key
reference for the data qualifiers appears atthe end of this case narrative Quality
control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
Mo Anomalies Reported
Volatile Analysis
Analysis Note for 025555 MS C9-Cl2AllphaUcs Recovery above the control limits
Analysis Note for Q25565 MSD C9-Cl2Allphatlcs Recovery above the control limits
Metals Analysts
Analysis Note for 025521 MS Chromium MS recovery outside of the conlrol limits Analysis was repealed with similar QC results
Analysis Nate for 025521 MS Lead MS recovery outside of the control limits Analysis was repeated with sImilar CC results
Analysis Note for 025521 MSD Chromium RPD recovery outside of the control limits Analysis was repeated with similar CC
results
Analysis Note for Q25621 MSD Lead MSD recovery RPD were outside of the control ilmits Analysis was repeated with similarCCresults
Wet Lab and Micro Analysis
NJA
Please call if you have any questions relating to this anaiytical report
Date Reviewed by Paula Gilleland Project Manager Mgela Overcash
Signature CA t31JAkS Signature Qa d0 113i1A Olca4I
Review Date 08/10/07 Approval Date 08/1 0/07
Data Qualifiers Key Reference
Compound also detected in the method blank
1k Result outside of the CC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positiveiy friend led but the value is estimated below the reporting limit
Estimated concentration with hIgh bias
Estimated concentration with low bias
matrix effect Is present
Notes This report should not be reproduced except in its entirety without the wriltten consent of Prism Laboratories trio The results iii this
report relate only to the samples submitted for analysis
449 Springbmok Road P.O Box 240543 Chadotto MC 28224-0403
Phone [phone] TDllFme 800/529.6364 Fec 7041525-0409
Percent Solids flelerminatlon
Percent Spflds
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 138652
Sample Matrix Soil COG Group G0807064
Time Collected 08/02/07 915
Time Submitted 03/02107 1325
5.31
5.32
5.73
5035
5035
5035
08110107 00D ibrown
08/10107 000 Ibrown
08110/01 000 lbrown
ESP Associates PA
ttn Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
08/1 0/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
902 SM2540 08/03/07 1555 ddixon
Sanmle Weight Determtnaflog
WeIght Blsu1lte
Weight Bisulfato
Weight Methanol
/olattIa Organic Compounds by GC1MS
111-Trichioroethane BR mg/kg 0.0051 0.00029 8260B 08/03/01 1702 Iwiby 025514
1122.Tstrachlomethane BRL mg/kg 0.0051 0.00052 82609 08/03/07 1702 Iwltjy 025514
112-Trichloroethane BRL mg/kg 0.0051 0.00032 82609 08/03/07 1702 iwitjy 025514
11.Dlohloroothane BR mg/kg 0.0051 0.00037 82609 08/03/07 1702 Iwiby 025514
ITI-DIchIoroeth000 BRL mg/kg 0.0051 000039 82609 08/03/07 1702 Iwiliy 025514
11-Dichioropropene BR mg/kg 0.0051 0.06045 826DB 08/03/07 1702 iwitiy 025514
123-Trlchorobenzone BR mg/kg 0.0051 0.00056 92609 08/03107 1702 Iwitmy 025514
123-Trichioropropane SRI mg/kg 0.0051 0.00045 8260B 08/03/07 1702 Iwliy Q25514
1124-TrithIorobenzene SRI mgkg 0.0051 0.00049 8260B 08/03/07 1102 Iwitiy Q25514
124-Trimnethylbenzene BRL mg/kg 0.0051 0.D0039 8260B 08/03/07 1702 iwlby 025514
12-Dlbromoethane EDB BR mg/kg 0.0031 0.000092 82609 08/03107 1702 Iwitry 025514
12-Dlchtorcbenzene BR mg/kg 0.0051 0.00028 82603 08/03/07 1702 Iwitry 025514
12-Dlchloroettiane BR mg/kg 0.0051 0.00051 8260B 08/03107 1702 IWitI 025514
12-Dichtoropropane BRL mg/kg 0.0051 0.00038 82609 08/03/07 1702 Iwiby 025514
135-Trlrnethyjbenzene 901 xnglkg 0.0051 0.00043 8260B 08/03/07 1702 Iwihry 025514
13-Dlchtorobenzene BRL mg/kg 0.0051 0.00044 8260B 09/03/07 1702 Iwiby 025514
13-Dlchioropropano BR mg/kg 0.0051 0.00035 8260B 08/03107 1702 Iwiby 025514
14-Dlchtorcbenzeno BR mg/kg 0.0051 0.0004 8260B 08/03107 1702 twIll 025514
22-Dlchlorapmpane BRL mg/kg 0.0051 0.00026 82609 08/03/07 1702 Iwtmry 025514
2-Chlorotoluepe BRL mg/kg 0.0051 0.00038 826DB 08/03107 1702 iwllry 025514
This report should not be repmcluced except in Its entirety without the written consent of Prism Laboratories lno
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 26224-0543
Phone[phone].Toll Free Number-1-808/529-0354-Fax [phone] Page of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
This roport should not be repmduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543-Charlotto NC 29224-0543
Phone [phone] Toll Free Number 1400/5294354 Fax [phone]
Laboratory Report
08/10/07
ESP Associates PA Project ID Morehead Commons No Ctient Sample ID WS-i
ttn Chris Ward Prism Sample ID 188652
Box 7030 Sample Matthc Soil coo Group 00307064
Thariotte NC 28241 Time Collected 08102107 915
Time Submitted 08/02/07 1325
ammeter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Umit Factor Date/Time ID
-Hexanone BRI mg/kg 0.051 0.00053
826DB 08/03/07 1702 Iwilry Q25514
1-Chiorotoluene BRL mg/kg 0.0051 0.00027 82609 08/03/07 1702 lwitry Q25514
i-Methyi-2-pentanone MIBK BRI mg/kg 0.051 0.00051 82603 08/03/07 1702 wllry Q25514
tsetone URL mg/kg 0.051 0.0020 826DB 08/03/07 1702 Iwihy 025514
lenzene BRJ.mg/kg 0.0031 0.00041 82609 08/03/07 1702 lwiliy 025514
lromobenzene BRL mg/kg 0.0051 0.00036 82608 08/03/07 1702 lwitiy 025514
romochIoromethane BRL mg/kg 0.0051 0.00031 826DB 08/03/07 1702 twitry 0215514
romod1chloromethane BRL mg/kg 0.0051 0.00045 82603 08/03/07 1702 iwitry 025514
3romoforrn BRL mg/kg 0.0051 0.00038 826DB 08/03/07 1702 lwitry 025514
3mmomethane BRL mg/kg 0.010 DM006 826DB 08103/07 1702 IwlIry 025514
arbon totrachioride BRL mg/kg 0.0051 0.0003 826DB 08/03/07 1702 Iwitxy 025514
hIorobanzene BRL mg/kg 0.0061 0.00039 826DB 08/03/07 1702 why 025514
hlorodlbrornomethane BRI mg/kg 0.0051 0.00035 826DB 08/03/07 1702 lwlliy 025514
hloroethane BRL mg/kg 0010 0.00042 826DB 08/03/07 1702 lwiy 025514
hloroibrm BRL mg/kg 0.0051 0.00038 82608 08/03/07 1702 hwitry 025514
hloromethane BRL mg/kg 0.0051 0.00036 82608 08103/07 1702 Iwitry 025514
is-12-Dlchloroethene BRL mg/kg 0.0051 0.00023 82609 08/03/07 1702 lwitri 025514
1s-13-DIchIompropene BRL mg/kg 0.0051 0.00033 826DB 06/03/07 1702 Iwitri 025514
Dlcliiorodlfluoromethane BRL mg/kg 00051 0.0011 826DB 08/03/07 1702 lwttiy 025514
thyIbenzene URL mg/kg 0.0051 0.00036 82603 08/0307 1702 twftiy 025514
sopropyt ether IPE BRL mg/kg 0.0051 0.00017 82603 08/03/07 1702 iwilry Q25514
sopmpylbenzene BRL mg/kg 00051 0.00041 82603 08/03/07 1702 lwitr 025514
np-Xylanes BRL mg/kg 0010 0.00072 82608 08/03/07 1702 lwihy 025514
Viethyt ethyl ketoneMEK BRL mg/kg 0.10 00014 82609 08103/07 1702 Iwitiy 025514
ViothyI t-butyl ether MTBE BRL mg/kg 0.010 0.0003 826DB 08103/07 1702 Iwilry 025514
Viethylene chloride BRL mg/kg 0.0051 0.00042 82609 03/03/07 1702 IwitrY 025514
-ButyIbenzene BRL mg/kg 0.0051 0.00041 826DB 06/03/07 1702 lwity 025514
Page of 35
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 188652
Sample Matrix Soil COC Group G0807064
Time Collected 08102107 915
Time Submitted 08/02/07 1325
NC Certification No 402
SC Certification 14o 99012
NC Ddnldng Water Cert No 37735
ESP Associates PA
ttn Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
0.0051 0.00031 52605 08/03/07 1702 lwitiy 025514
0.010 0.0006 82605 08103/0 1702 IWlIJY Q25514
0.0051 0.00031 826DB 08103/07 1702 lwltry Q25514
0.0051 0.00042 82606 08103107 1702 witry Q5514
0.0051 0.00034 82606 0810307 1702 lwitJy 025514
0.0051 0.00051 826DB 08/03/07 1702 twftiy 025514
0.0051 0.00032 826DB 08/03107 1702 IwliJy 025514
0.0051 0.00088 826DB 08/03/07 1702 lwiby 025514
0.0051 0.00035 826DB 08103/07 1702 lwftiy 025514
DM051 0.00039 826DB 08103107 1702 Iwitry Q25514
0.0051 0.00036 82605 08/03/07 1702 lwitiy Q25514
0.0051 0.00031 826DB 08/03/07 1702 Iwitry 025514
0.0051 0.00042 826DB 08103/07 1702 Iwitry 025514
0.026 0.0019 826DB 08103/07 1702 Iwitry 025514
0.0051 0.00066 82606 08103/07 1702 lwity 025514
-Pmpylbenzena BRL
Maphthalene BRL
D-Xylene BRL
-Isopmopyltoluene BRL
reoButylbenzene BRL
9tyrene BRL
tert-Butylbenzene BRI.
Tetrachiomethene SRI
Toluone BRL
Lrans-1 2-Oichloroethene BRL
trans-i 3-Dlchloropropene SRI.
Trichiomethens BRL
rrichtoronuommeihane LIRL
Vinyl acetate BRI.
Vinyl chloride BRL
Semi-volatile Oroanic Comnounds by CC/MS
1.24-Tdchlorobenzene BRL
12-Dlthlorobenzene BRL
1.3-Dichlorobenzene BRL
14-Dlchlorobenzene BRL
2.45TrlchlorophenoI BRL
2.46-Trtchlorophenol SRI
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Toluene-dB 97 81 -128
Dlbromofluommethane 90 67-143
Bmmafiuombenzene 110 77-128
0.37
0.37
0.37
0.37
0.37
0.37
0.035
0.027
0.026
0.033
0.037
0.035
82700
82700
82700
82700
82700
52700
08107/07 1402 kcamplgotto
08/01/07 1402 kcamp1otto
08/07/01 1402 kcamp1otto
08/07/07 1402 kcaniplotto
08/07/01 1402 kcamplgotto
08/07/07 1402 kcamplgotb
Q25550
025550
Q25550
Q25550
025550
025550
This report should not be reproduced except In It entirety wthout the written consent or Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone[phone] Toll Free Number l-800/529.5364 Fax [phone] Page of 35
NC Certification No 402
SC Certification No g9012
NC Drinking Water Cart No 37735
vlci An1tIcI Lnvhnmcn5I Sthiicns
ESP Associates PA
\ttn Chris Ward
.0 Box 7030
harlotte NC 2824i
This report should not be reproduced exoept in Its entireLy without the written conseritof Prism Labomtortes Inc
449 Spilngbrook Road P.O Box 240543 Charlotte1 NC 29224-0543
Phone [phone] Toll Free Number 1400/529-6354 Fax[phone]
Laboratory Report
08/10/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 188652
Sample Matrix Soil coc Group G0807064
Time Collected 05/02107 915
Time Submitted 0802107 13-25
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Datefflme ID
DIchkimphenc$BRL mg/kg 0.37 0.031 827CC 08/07/07 1402 kcamplgoflo 025550
4-D1methyIphenol BRL mg/kg 0.37 0.035 827CC 08107/07 1402 kcamptgotto Q25550
4-Dlnhtrophenol BRL mg/kg tB 0.041 8270C 08/07107 1402 kcmpIotto 025550
4-DInItroto1uene SRI mg/kg 0.37 0.021 827CC 08107/07 1402 kcamp1otto Q25550
5Dinitrotoluene BRL mg/kg 0.37 0.039 827CC 08/07107 1402 kampgotto 025550
-ChIcmnaphthaIene SRI mg/kg 0.37 0.038 827CC 08107107 1402 kcamplgatto 025550
-Chorophenol BRL mg/kg 0.37 0.029 827CC 08/07/37 1402 kcampotto 025550
-Methylnaphtha1one BRL mg/kg 0.37 0.029 827CC 08/07/07 1402 Iccamplgotto Q2555
-Methylphenol SRI mg/kg 0.37 0.034 827CC 08/07/07 1402 kcampIotto Q2555Q
-NItmphenoI SRI mg/kg 0.37 0.044 8270C 08/07/07 1402 kcamplgotto Q25550
l4-Methylphenol BRL mg/kg 0.37 0.037 8270C 08107/07 1402 kcamplgotto 025550
33-Dichloroben2idlne BRL mg/kg 0.73 0.023 8270C 08/07107 1402 kcamphotto 025550
l.6-DlnIlro-2-methytpheno BRL mg/kg 1.8 0.022 8270C 08107107 1402 kcenplgolto 025550
1-Bromophenyiphenylether SRI mg/kg 0.37 0.035 827CC 0807/07 1402 hcarnpIgotto 025550
t-Chloro-3-methylphenol SRI mg/kg 0.73 0.027 827CC 03/07/07 1402 kcampiotto 025550
t-Chloroanlllne SRI mg/kg 0.37 0.047 827CC 08/07/07 1402 kcampIgotto 025550
l-Chlompheriylphenylether SRI mg/kg 0.37 0.023 82700 08107/07 1402 kcamphouo 025550
1-Nitrophenol SRI mg/kg 1.8 0.024 8270C 08/07/07 1402 hvamplgotto 025550
cenaphIhene SRI mg/kg 0.37 0.035 8270C 08/07/07 1402 kcamplgotto 025550
cenaphthylene SRI mg/kg 0.37 1.036 8270C 08/07/07 1402 hcanphotto 025550
nthracene BRL mg/kg 0.37 0.028 827CC 08/07/07 1402 kcamplgotto 025550
.zobenzene BRL mg/kg 1.8 0034 8270C 08/07/07 1402 kcampigotto Q25550
3enzoaanthracene 0.16 .i mg/kg 0.37 0.051 827CC 08/07/07 1402 kcamplgotto 025550
3enzoapyrene 0.18 mg/kg 0.37 0.042 8270C 08/07/07 1402 kcamplgotto Q25550
3enzobfiunranlhene 0.19.1 mg/kg 0.37 0.016 827CC 08/07/07 1402 kcampIotto 025550
3enzog.hjpe4ene BRL mg/kg 0.37 0.017 82700 08/07107 1402 keamplgotto 025550
3enzokfiucranthene 0.17 mg/kg 0.37 0.030 82700 0807/01 1402 kcamplgolto 025550
Page of 35
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 188652
Sample Matrix Soil COC Group G0807064
Time Collected 08102/07 915
Time Submitted 08102107 1325
SRI
SRI
BRI
SRi
SRI
SRI
BRI
0.17
BRL
BR
BRL
I3RL
ERL
BRL
0.37
aRt
BR
BRL
BRL
BRL
SRL
BRL
BRL
BRL
BRL
BRL
BR
mg/kg 1.8 0.16
mg/kg 0.73 0.039
mg/kg 0.37 0.042
mg/kg 0.37 0.040
mg/kg 0.37 0.031
my/kg 0.37 0.018
mg/kg 0.37 0.022
mg/kg 0.37 0881
mg/kg 0.37 0.017
mg/kg 0.37 0.027
mg/kg 1.37 0.037
mg/kg 0.37 0.031
mg/kg 0.37 0023
mg/kg 0.37 0.025
my/kg 0.37 0.025
mg/kg 0.37 0.022
mg/kg 0.37 0.019
mg/kg 0.37 0.036
mg/kg 1.37 0.039
mg/kg 0.37 0.037
mg/kg 037 0.038
mg/kg 0.37 0.033
mg/kg 0.37 1.042
mg/kg 0.31 0.019
mg/kg 0.37 0.040
mg/kg 0.37 0.036
mg/kg 1.8 0.031
8270C
827CC
827CC
8270C
827CC
827CC
82700
82700
82700
827CC
82700
82700
82700
82700
82700
82700
827CC
82700
82700
82700
82700
82700
821CC
82700
82700
827CC
827CC
08/07/07 1402 kcamplgolto 025550
08/07/07 1402 kcarnpigotlo 025550
08/07/07 1402 kcampigotlo 025550
08/07/07 1402 kcarnpiotto Q25550
08/07/07 1402 kcamptgotto 025550
08/07/07 1402 kcamplgofln 025550
08/07/07 1402 kcamplgotto 025550
08/07/07 1402 kcamplgotlo 025550
08107/07 1402 kcampIotto 025550
08/01/07 1402 kcampiofto 025558
08107107 1402 kcainptgotio Q25550
08/07/07 1402 kcamplgolto 025550
08107/07 1402 kcamplgotto 025550
08107/07 1402 kcampIatta Q25550
08/07/07 1402 kcamplgotto 025550
08/07/07 1402 kcamplgotto 025550
08/07/07 1402 kcampigotto 025551
08/07/07 1402 kcamplootto 025550
08/07/07 1402 kcampiotto 025550
08/07/07 1402 kcampigotb 025550
08/07/07 1402 kcatnptgotto 025550
08/07/07 1402 kcsmplaotlo 025550
08/07/07 1402 kcamploLto 025550
08/07/07 1402 koamplgotto 025550
08/07107 1402 kcampigctio 025550
08/07107 1402 kcampigotto 025550
08/07/07 1402 kcamplgotto 025550
This report should not be reproduced except In ha entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Chadotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529.8384 Fax [phone]
NC Certilicalion No 402
SC Certlflcation No 99012
NC Drinking Water Cart No 37735
SP Associates PA
ttn Chjis Ward
.0 Box 7030
hartotte NC 28241
Laboratory Report
0810107
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Daternme ID
3erizolo acid
3enzyl alcohol
31s2-thloroethoxymethane
3is2-chtoroethdether
31s2-chbroisopropylether
31s2-ethylhexylphthalate
3utylbenyIphthalate
Chtysene
D1-n-butylphthatate
Dl-n-ootyiphthalate
lbenzoahanlhracene
Dlbenzoluran
Dlothylphthalate
Dlmethytphthalate
Fluoranthene
Fluorene
-lexachlorobenzeno
1exachlorobutad1ene
tiexathlorocycicpentadlene
Ilexathloruelhone
Indeno1 23-cdpyrene
sophorone
t1-Mtrosodl-n.propyamjne
M-Nhtrosodlphenylarnino
Naphthalene
titrobenzene
Pentachlcrophenol
Page 35
henanthrerle
henol
yrene
Extractable Petroleum Hydrocarbons
by GC-Fll
1-C22 Asomatics ORL mg/kg
Analysis NoIe for CU-C22 Aromatica
19-C36AflphaUcs BRL mg/kg
9-C18 Aliphatics BRL mg/kg
Sample Preparation
MDI IDilulion
Factor
29.Og ImL 35509
08/07/07 1402 kcasnpigoilo
08/07/07 1402 kcampigotto
08/07/07 1402 keampigotto
08/04/07 900 pbaw
025550
025550
025550
P19082
Surrogate Recovery Control Limits
Terphenyl-d14 80 41 136
Phenol-d5 89 13-95
Nitrobennene-d5 75 14-103
2-Fluomphancl 80 14-89
2-Fluombiphenyl 76 21 -108
246-Trlbromophenol 87 25-123
21 mg/kg 027 0.015 6010B
110 mg/kg 0.27 0.018 60109
This report should not be reproduced except in Its entirety ydthout the written consent of Pilam Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 2B224-0543
Phone [phone] Toil Free Number 1-800/529.8364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
SP AssociateS PA
ttn Chris Ward
.0 Box 7030
hartotte NC 28241
Laboratory Report
08/10/07
Project ID Morehead Commons No Client Sample ID
PrIsm Sample ID
Sample Matrix Soil COG Group
Time Collected
lime SubmItted
arameter Result Units
wS-I
1B8652
G0807064
06/02/07 915
08102/07 1325
Method Analysis Analyst Batch
Datamme IDReport
Limit
0.37
0.37
0.25
BRL
0.32
mg/kg
mg/kg
mg/kg
0.018
0.040
0.37 0.025
Sample PreparaUom
8270C
827CC
82700
11 5.9
AdjuBIed value
Ii 1.6
11 3.5
MADEP EPI-I 08/07/07 2107 grappacrioll 025548
MADEP EPH
MADEP EPH
08/07/07 2107 grappaccioli
08/07107 2107 grappaccioli
10.14 mL EPH 08103/07 700 pbarr
025548
025548
P19081
1etals by ICP
hromIum
ead
Surrogate Recovery Control Limits
o-Terphenyl 82 40-140
2-Fkrorobiphenyl 84 40-140
2-Bmmonaphthalefle 90 40-140
1-Gb oro-octadecane 57 40-140
08/03/07 1959 mcampbefl
08/03107 1959 mcampbeil
Q25521
025521
Page Cr35
Laboratory Report
08/10/07
wS-1
188652
00807064
08102/07 915
08/02107 1325
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample PreparatIon 2.02 50 mL 30503 08/03107 745 ddixon P19078
ilolatlle Petroleum Hydrocarbons
by 3C-PIOIFID
5-C8 Atiphatics BRL mg/kg 5.5 1.1 MADEP VPH 08107107 431 hwagner Q25565
analysis Note for C5-C8 Aliphatioa Adjusted value
9-C10 Aromatics BR.mg/kg 5.5 0.033 MADEP VPK 08107/07 431 hwagner Q25565
C9.Cl2AllphatJcs ERL mg/kg 5.5 1.7 MADEPVPH 08107/07 431 hwagnar Q25565
xialysis Note for C9-C12 AliphaticS Adjusted value
Surrogate Recovery Control Limits
25-Dlbromotoluene-PID 102 70-130
25-Dlbromotoluene-flD 109 70-130
3amplo Weight Detennnaton
Nelght 21.79 MADEP VP1-l 08/08/07 000 Ibrown
P/eight 20.04 MADEP VPI-I 08/08/07 000 Ibrown
sample Comments
3R1 Below Reporting Limit
I-Estimated value between the Reporting Umit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certlflcathn requirements other than
VELAC certification except for those Instances Indicated in the case nanativo ancYor lest comments
4ff results are reported on dy-wefght basis
This report should not be reproduced except In Its entirety without the written consent ci Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Char7otte NC 28224-0543
NC Certilication No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
ESP Associates PA
4.ttn Chris Ward
Box 7030
hartotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
ngeIa Overcash
V.P Laboratory Services
Phone [phone] Toll Free Numban 1-800/529-6384 Fax [phone] Page of 35
percent Solids Determination
percent Solids
NC Certification No 402
SC Certification No 90012
NC Drinking Water Cert Un 37735
5.60
5.78
5.59
5035
5035
5035
0811007 000 lbrcari
08110/07 000
08/10107 000
rolatile Organic Compounds by GCMS
11-Tdchloroethane
22.Tetrachtoroethane
l2-Trichioroethane
I..Dlchloroethanu
1-Dlchloraethene
1-Dlchloropropene
23-TrIthlorobenzene
23-Tilchloroprcpane
24-Trichlorobenzene
24-Trimethy1benzene
2-Dibromoethane EDB
2-Dlchlorobenzene
2-Dlchloroothane
2-Dlchloropropano
35-Trtmethylbenzene
.3-Dlchtorobenzerie
3-Dlcbloropropane
4-Dlchiorobenzcne
2-Dlchtoropropana
-Chiorotoiuene
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
826DB
82608
82608
826GB
82608
82609
82603
82608
82608
82608
82608
826GB
826DB
82608
82609
62609
826GB
826GB
826GB
82608
08/03/07 17A5 Iwitiy
08/03/07 1745 twity
08/03/07 1745 lwitiy
08103/07 1745 Iwby
08103/07 1745 IwlIzy
08/03/07 1745 IW1IIY
08103/01 1745 1MIty
08/03/07 1745 wIlly
08/03107 1745 wiry
08/03/07 1745 Iwilly
08/03/07 1745 lwitiy
08/03/07 1745 willy
08/03/07 1745 willy
08/03107 1745 wiry
08/03107 1745 twitry
08103107 1745 MW
08/03/07 1745 lwitiy
08/03/07 1745 Iwitry
08/03/07 1745 wIlly
08/03/07 1745 lwilry
025514
025514
025514
Q25514
025514
Q25514
025514
025514
Q25514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
ESP Associates PA
ttn Chris Ward
Box 7030
Tharlotte NC 28241
Laboratory Report
08110/07
ProJ9ct ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrbc Soil COC Group
Time Collected
Time Submitted
WS4
188853
30807064
08102107 930
0802107 1325
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
88.8
amnie Weight Determination
Veight Blsulfte
Veight BisuUte
Veight Methanol
SM2540 08103/07 1555 ridlxon
Ibrown
brown
0.0050
0.0050
000028
0.00051
0.0050 0.00031
0.0050 0.00038
0.0050 000038
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRL
BRL
BRL
URL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.00044
0.00055
0.00044
0.00048
0.00038
0.00009
0.00027
0.0005
0.00037
000042
0.00043
0.0050 0.00034
0.0050 0.00039
0.0050 0.00025
00050 0.00037
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories
Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 282.24-0543
Phone [phone] Toll Free Number 1-8110/529-6354 fax [phone] Page8of35
ESP Associates PA
Atm Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
Project ID Morehead Commons No Client Sample ID WS-2
PrIsm Sample ID 188653
Sample Matnx Soil COC Group G0807064
lime Collected 08102107 930
Time Submitted 08102/07 1325
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] ToU lreo Numbec 1-8001529-0364 Eax 7041525-0409
NC Certification No 402
SC CerLificatlon No 99012
NC DrInking Water Cert No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.050 0.00052
826DB 08103107 1745 lw/ky Q25514
4-Chlarotaluene BRL mg/kg 0.0050 0.00026
826DB 08103/07 1745 Iwliry 025514
4-Methyt.2-pentanoneMIBK BRL mg/kg 0.050 0.0005
82608 08103/01 1745 IwlIiy 025514
Acetone BR mg/kg 0.050 0.0020
825DB 08/03/07 1745 IWiLiy 025514
Benzene BRL mg/kg 0.0030 0.0004 825DB 08103/07 1745 lwitnr 025514
Bromobenzene BRL mg/kg 00050 000035 82609 08/03/07 1745 Iwitry 025514
Bromochloromethane BRL mg/kg 0.0050 0.0003
826DB 08/03/07 1745 1w/ky 025514
Bmmodlchlororuethana BR mg/kg 0.0050 0.00044
82608 08/03107 1745 lw/ky Q25514
Bromoform BRL mg/kg 0.0050 0.00037 826DB 05/03107 1745 lwltzy 025514
Bromomethane BRL mg/kg 0.010 0.00058 826DB 08/03/07 1745 lw/ky Q25514
Carbon tetrachioride BRL mg/kg 0.0050 0.00029
82608 08/03/07 1745 lw/ky 025514
Chlorobenzene SRI mg/kg 0.0050 0.00038
826DB 08/03/07 1745 1w/ky Q25514
Chtorodibromomothane BRL mg/kg 0.0050 0.00034 82608 08/03/01 1745 lw/ky 025514
Chioroethane BR mg/kg 0.010 0.00041
82603 08/03/01 1745 lw/ky 125514
Chloroform BRL mg/kg 0.0050 0.00037
826DB 08/03107 1745 lw/ky 125514
Chioromethane BRL rug/kg 0.0050 0.00035
82603 08/03/07 1745 IwIby 025514
ds-12-DIchoroethene SRI mg/kg 0.0050 0.00022
82608 08/03107 1745 lwitiy 025514
cls-13-Dlchloropropene BRL mg/kg 0.0050 0.00032 826DB 08/03/07 1745 IWILTY 125514
Dlchlorodifluoromethane BRL mg/kg 0.0050 0.0011
826DB 08103/07 1145 lw/kY 025514
EthyIbenene BR mg/kg 0.0050 000035 826DB 08/03/07 1745 1W/ky 125514
Isopropyl ether IPE BRL mg/kg 0.0050 0.00017 826DB 08/03/07 1745 lw/ky 025514
Isopropylbenzene BR.mg/kg 0.0050 0.0004 826DB 08/03/07 1745 lW/ky 025514
mp-Xyteries BR.mg/kg 0.010 0.0007 826GB 08/03/07 1745 lwllr 125514
Methyl ethyl ketone MEK BRL mg/kg 0.10 0.0014 826DB 08/03/07 1745 lw/ky 025514
Methyl ether MTBE SRI mg/kg 0.010 000029 626DB 00/03107 1745 lw/ky 125514
MethyleneohtorTde SRI mg/kg 0.0050 0.00041
826GB 08103107 1745 lw/ky 025514
n-Butylbonzene BRL mg/kg 0.0050 0.0004 826DB 08/03107 1745 lw/ky 025514
Page of 35
ESP Associates PA
ttn Chris Ward
0.Box7030
harloUe NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coo Group
Time Collected
Time Submitted
WS-2
188653
G0807064
08102/07 930
18/02/07 1325
This report should not be reproduced except In its entirety 4thout the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte1 NC 28224-0543
Phone[phone] Toll Free Number 1-800/529-6384 Fax [phone]
NC CertificatIon No.402
SC Certification No 99012
NC Drinking Water CerL No 37735
Laboratory Report
08/1007
-I
Parameter Result Units Report MDL Dilution
Limit
Method
Factor
-Prcpylbenzene
JaphthaIene
-Xylene
u-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butyibenzene
retrachtoroethens
Toluene
tmns-1 2-Dlchloroethene
trans-I 13-Dlchloropropene
Frichioroethene
rricblorofiuoromethano
Vinyl acetate
Vinyl chloride
BRL
BRL
BRL
I3RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
URL
BRL
BRL
BRL
0.0050 0.0003
0.010 0.00058
0.0050 0.0003
0.0050 0.00041
00050 0.00033
0.0050 0.0005
0.0050 0.00031
0.0050 0.00086
0.0050 0.00034
0.0050 0.00038
0.0050 0.00035
0.0050 0.0003
0.0050 0.00041
0.025 0.0018
0.0050 0.00064
Analysis Analyst Batch
Date/lime ID
826DB 08103/07 1745 iwitry Q25514
82606 08103107 1745 twitry 025514
826DB 08/03/07 1745 lwiliy Q25514
826DB 08/03/01 1745 lwitxy 025514
026DB 08103107 1745 iwitry 025514
828DB 08/03/07 1745 Iwitry 025514
826DB 08/03/07 1745 Iwitry 025514
82503 00/03/07 1745 Iwitry 026514
82503 08/03/07 1745 Iwitry 025514
826DB 08/03/07 1745 Iwitry 025514
626DB 08103/07 1745 Iwitry 025514
82608 08/03/07 1745 lwitry 025514
82603 08103107 1745 IWitry 025514
82608 08/03/07 1745 twitry 025514
826DB 08/03/07 1745 iwitiy 025514
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Toluene-d8 99 81 128
Dibromoltuoromethane 92 67-143
Bromofiuorobenzene 108 77-128
SemI-volatIle Organic Compounds by GC/MS
1Z4-Tflchtorobenzene BRL
12-Dlchlorobenzene BRL
13-Dlchlorobenzene BRL
t4-Plchlorobenzene BRL
a41.Trlchlorophenol BRL
2416-Trlchlorophenol BRL
0.37
0.37
0.37
0.37
0.37
0.37
0038
0.027
0027
0.033
0.038
0.035
82700
6270C
82700
8210C
827QC
82700
00107/07 1451
00/07/07 1457
08/07/07 1457
08/07/07 1457
08/07/07 1457
08/07/07 1457
kcampIotto
kcaniplotto
kcamplgotto
kcamptgotto
kcainplgotto
kcamplgotto
025550
025550
025550
025550
025550
Q25550
Page 10 of 35
This report should not be reproduced except In its entirety without the wtitten consent of Prism Laboratories Inc
449 Sprlrigbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Pt
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
/\ttn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
08110107
Project ID Morehead Commons No Client Sample ID WS.2
PrIsm Sample ID 188653
Sample Matrix Soil COC Group 30807064
Time Collected 08/02107 930
Time Submitted 08/02107 3.25
Parameter Result Units Report MDL DIluliort Method Analysis Analyst
Batch
Limit Factor Date/Time II
4-DichIorophenoI BR mg/kg 0.37 0031 82706 08107/07 1457 kcampleattD Q25550
24.Dlmethylphenol BR.mg/kg 0.37 0.035 8270C 08107/07 1457 kcampluolio 025550
24-Dinitrophenol URL mg/kg 1.8 0.041 82706 08/07/07 1457 kcainplgotto 025550
24-Dlnltrotoluene BRL mg/kg D.37 0.021
82706 08107/07 1457 kcainplgottu 025550
8-DlnItmtoluene BR.mg/kg 0.37 0.039 82706 08/07101 1457 kcarnplgollo Q25550
a.Chloronaphthatene BR mg/kg 0.37 0.038 82706 08/07/07 1457 kcamplgotto 025550
a-Chlorophenol BRL mg/kg 0.37 0.029 8270C 08/07/07 1457 hcarnplgotto 025550
..MethylnaphthaIene BRL mg/kg 0.37 0.029 82700 08/07/07 1457 kcamplgotto Q25550
-Metbytphenol BRL mg/kg 037 0.034 82706 08107/07 1457 kcamplgotto Q2555Q
a-Nurophanal BRL mg/kg 0.37 0.044 82100 08/07/07 1457 hcamplotto 025550
34-Methylphenol BRL mg/kg 0.37 0.038 82706 08107/07 1457 kcarnp1oUo 025550
33-Dlchlorobonzldlne I3RL mg/kg 0.74 0.023 82700 08/07/01 1457 kcarnplgotto 025550
16-Dlnltro--2-methylphenol BRL mg/kg 15 0.022 82700 08/07/07 1457 kcamplgotto 025550
1-Bromophenylphanylether BRL mg/kg 0.37 0.035 8270C 08107/07 1457 kcamplgotto 025550
i-Chloro-3-rnethylphenol BRL mg/kg 0.74 0.027 82706 08107/07 1457 kcamplgotto 025550
1-Chioroaniline BRL mg/kg 0.37 0.047 82700 08/07/07 1457 kcampigotto 025550
1-Chlomphenytphenylether BRL mg/kg 0.37 0.023 82700 08/07/07 1457 kcamplgotto 025550
1-Nltrophenol BRL mg/kg 1.8 0.024 82706 08/07/01 1457 kcamplgotto 025550
cenaphthene BRL mg/kg 0.37 0.036 82700 08107/01 1457 kcamplgotto 025550
oenaphlhylene BRL mg/kg 0.37 0.037 82700 08/07/07 1457 kcamptgotto 025550
nthmcene BR.mg/kg 0.37 0.028 82700 08107/07 1457 koamplgotto 025550
4zobenzene BRL mg/kg 1.8 0034 82700 08/07/07 1457 kcamplgotto 025550
3enzoaanthracene BR mg/kg 0.37 0.051 82706 08/07/07 1457 kcamplgo%to Q25550
3erzoapyrene BRL mg/kg 037 0.042 82700 08/07/01 1457 kcarnplpotto 025550
3enzobfluoranthene BRL mg/kg 0.37 0.015 82700 08/07/07 1457 koarupigotto 025550
3erizog.hIperylene BR mg/kg 0.37 0.017 82700 08/07/07 1457 kcamplotto 025550
3enzoktluoranthene BRL mg/kg 0.37 0.030 82700 08107/07 1457 kcarnp1otb 025550
Page 11 ci 35
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Spdngbrook Read P.O Box 240543-Charlotte NC 26224-0543
Phone [phone] ToIl Free Number 1-8001529.6364 Fax [phone]
SOC cation No 99012 Laboratory Report
NC Drinking Water Cert No 37735 06/10/07
Ii
SP Associates PA Project ID Morehead Commons No Client Sample ID WS-2
\thi Chris Ward Prism Sample ID 188653
Box 7030
Sample Matrix Soil COC Group G0807064
harIotte NC 28241 TIme Collected 08102/07 930
Time Submitted 08102107 1325
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Daternme ID
1.8 0.163enzolc acid
BRL mg/kg 82700 08/07107 1457 kcamplgottn 025550
3enzyl alcohol BRL mg/kg 0.74 0.039 827CC 08/07/01 1457 kcamplgotto 025550
31s2-chioroethoxymethane BRL mg/kg 0.37 0.042 827CC 08/07107 1457 kcamplatto 025550
3ls2-chloroethylether BRL mg/kg 0.37 0.040 82700 08/07/07 1457 kcamplgotto 025550
31s2.chloroiscpropylether SRI mg/kg 0.37 0.031 82700 08/07/07 1457 keampigouo 025550
31s2-ethyihexylphthalate BRL mg/kg 0.37 0.018 82700 08/07/07 1451 kcamplgotto Q25550
3utylbenzylphthaiate SRI mg/kg 0.37 0.023 82700 08/07/07 1457 kcamplgotto 025550
Thrysene BRL mg/kg 0.37 0.061 827CC 08101/07 1457 kcamplgotto 025550
l-n-butylphthalate BRL mg/kg 0.37 0.017 82700 08/07/07 1451 kcamplgotto 025550
J..n.octylphthoiate SRI mg/kg 0.37 0.027 827CC 08/07/07 1457 kcamplgotto 025550
Ibenzoahanthracene URL mg/kg 0.37 0.037 827CC 08/07/07 1451 kcarnpigolto 025550
Ibenzofuran BRI mg/kg 0.37 0.032 821CC 08107/07 1457 kcarnplgotto 025550
lethylphthalate SRI mg/kg 0.37 0.023 8270C 08/07/07 1457 kcamplgctto Q25550
imethyiphthalata BRL mg/kg 0.37 0.025 827CC 08107/07 1457 koampigotic 025550
Iuoranthone BRL mg/kg 0.37 0.025 82700 08/07/07 1457 keamplgotto 025550
luorene BRL mg/kg 0.37 0.022 8270C 08107/07 1457 kcamplgotlo 025550
lexachlorobenzene BRL mg/kg 0.37 0.019 821CC 08107/01 1457 kamipigotto 025550
lexachtorobutadlerie BRL mg/kg 0.37 0.036 827CC 08/07/07 1457 Iccamplgotto 025550
iexachlorocyclopentadlene BRL mg/kg 0.37 0.039 82700 08/07107 1457 kcamplgolto 025550
exachloroethane SRI mg/kg 0.31 0.037 827CC 08/07/07 1457 kcamplgoth1 025550
ndeno123-cdpyrene SRI mg/kg 0.37 0.038 82700 0807/07 1467 kcamplgotto 025550
sophorone SRI mg/kg 037 0.033 82700 08107101 1457 kcarnpigolto 025550
1-Nltrosodl-n-propylamino SRI mg/kg 0.37 0.042 82700 08107107 1457 kcampigotto 025550
I-NltrosodIphenyIamIne SRI mg/kg 0.37 0.019 827CC 08/07/07 1457 kcampigclio 025550
daphthalene BRL mg/kg 0.37 0.040 82700 0807/07 1457 kcampigofto 025550
4itrobenzene BRL mg/kg 0.37 0.035 827CC 0807/07 1457 kcainplgotto 025550
entachlorophenoi BRL mg/kg 1.8 0.031 82700 0807107 1457 kcamplgotto 025550
Page 12 of 35
0.1
_.UcaI EwIzornunIMO31i
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil CCC Group
Time Collected
Time Submitted
WS-2
188653
G0807064
08102/07 930
08/02/07 325
Parameter
Phenanthrene
Phenol
Pyrene
Report
Limit
0.37
0.37
0.37
Analysis
Date/lime
C810707 1457 Kcamplgollo
08/07107 1457 kcamplotto
08/01/07 1457 kcamplgotto
08104/07 900 pbarr
025550
Q25550
Q25550
P19082
Surrogate
Terphenyl.ii14
Phenol-d5
Nlirobenzened5
2-Fluorophenol
2-Phiorobiphenyl
24.Tribromophenol
Recovery
74
62
63
57
75
72
Control Limits
41-136
13-95
14-103
14-89
21-1013
25-123
Extractable Petroleum Hydrocarbons by GC-FID
C11-C22 Aromalics
Analysis Note or
C19-C36 Aliphalics
CD-Cia Aliphatics
18 mgkg
58 mg/kg
11 13.0
Aduted value
11 1.7
11 3.6
This report should not be reproduced except In Its entirety1 without the written consent of Prism Laboratories trio
449 Sprlngbrook Road P.O Box 240543 Charlotte1 NC 28224-0543
Phone [phone] Toil Free Number 14001529.6364 Fax [phone]
NC Cartlflcatlon No 402
SC Certifloatlon No 99012
NC Drinking Water Cert No 37735
Laboratory Report
08110107
Result Units Analyst Batch
IDMDLMethod
saL
BRL
BRL
mglkg
mg/kg
mglkg
Dilution
Factor
0.018
0.040
0.025
Sample Preparation
82700
82700
82700
30.32 mt 355013
BRL mg/kg
Cl1-C22 7romatics
DRL mglkg
BRL mg/kg
Sample Preparation
MADEP EPH 08107107 2251 grappaccloll 025548
MADEP EPH 08/07/07 2251 grappaccloll 025545
MADEP EPH 08107/07 251 grappaccioli 025548
10.1 niL EPH 08/03107 700 pbarr P19081
Metals bVICP
Chromium
Lead
Surrogate Recovery Control Limits
o-Terphenyt 87 40-140
2-Fluorobiphenyl 96 40-140
2-Bromonaphthalene 99 40-140
1-Chloro-octadecana 80 40-140
0.28 0.016 601DB 08/03107 2022 mcampbsll 025521
0.28 0.018 601DB 08/03/07 2022 mcampbelt 025521
Page 13 of 35
NC Certification No 402 Laboratory Report
SC Certification No 99012
NC Drinking Water Ceit No 37135 08/1007
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-2
AUn Chris Ward Prism Sample ID 188653
P.O Box 7030 Sample Matrix Soil COC Group 00807064
Charlotte NC 28241 lime Collected 08/02/07 930
Time Submitted 08/02/07 1325
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 2.01 50 ml-305GB 08/03/07 745 ddixon P19078
Volatile Petroleum Hydrocarbons by
GC-P1D1FID
CS-CS AQphatics SRI mg/kg 5.6 1.1 MADEP VFH 08/07/07 515 hwaner Q25565
na1ysis fate for C5-C8 Aliphatics Idjusted
value
C9-C10 Aroniatfcs BRL mg/kg 56 0.034 MADEP VPH 08/07/07 516 hwagner Q25565
C9.Cl2AIlphatlcs BRL mg/kg 6.6 1.7 MADEP VPH
08/07107 515 hwaner 025565
7na1ysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dlbromotoluene-PID 99 70-130
25.Dlbromotaluene-FID 102 70-131
Sample Woiaht Doterminpflon
Weight 22.04 MADEP VPH
08/08107 000 Ibrown
WeIght2 18.22 MADEPVPH 08108107 000 Ibrown
Sample Comments
BRL BelowReporung Limit
J-Estimated value between the Reposting Limit end the MDL
The results hp Ms report relate only to the samples submitted for analysis and meet
state cerllllcallon requirements other than
NELAC certiffcation except for those instances indicated In the case nanativo and/or
test comments
All results are reportedon drj-weght
basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories
Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone[phone] Toll Free Number 1-8001520.6364 Fax [phone] Page 14 ci 35
ES Associates PA
Atth Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
0811007
Project ID Morehead Cornnions No Client Sample ID WS.3
Prism Sample ID 188654
Sample Matrix Soil coc Gup 30807064
Time Collected 08/02/07 945
Time Submitted 08/02/07 1325
Percent Solids Determination
Percent Solids
5035
5035
5035
08/10/07 000 ibrcwn
06/10/07 000 Ibrown
08110107 000 Ibrown
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Datelflme ID
88.2 SM2540 06/03/07 1555 ddkon
Samnie Weloht Determination
Weight Bisuliete 5.88
Weight Blsulmte 5.79
Weight Methanol 5.23
Volatile Organic Compounds byGC/MS
111-Trtchloroathane BRL mg/kg 0.0048 0.00027
62608 06/03/07 1829 twity 025514
1122-Tetrachloroethane BRL mglkg 0.0048 0.00049 826DB 08/03107 1829 Iwby 025514
112-Trlchloroathane BRL mg/kg 0.0048 0.0003
826DB 08/03/07 1029 Iwitry 025514
tl-Dlchloroethana BRL mg/kg 0.0048 0.00035
826DB 08103/07 1829 lwitry Q25514
11-Dichloroethene SRI mg/kg 0.0048 0.00037 82608 08/03107 1829 twhy Q25514
lj-Dlthlompmpene BRL mg/kg 0.0048 0.00042
826DB 08/03107 1829 Iwitry Q25514
123-Trichlorobenzene BRL mg/kg 0.0048 0.00053 826DB 08/03107 1029 IWhy 025514
123-Trlobloropropane SRI mg/kg 0.0048 0.00042 826DB 08/03/07 1829 lwhy 025514
124-Tiichlorobenzeno SRI mg/kg 0.0048 0.00046 826DB 08/03101 1829 twilly 025514
12.4-Trimethylbenzene BRL mg/kg 0.0048 000031 826DB 08/03/07 1829 Iwitry 025514
12-Dibromoethane EDB BRL mg/kg 0.0048 0.000087 826DB 0803/07 1829 Iwlby Q25514
12-Dlchtorobenzene BR.mg/kg 0.0048 000026 826DB 06/03107 1829 lwitiy 025514
12-Blchloroethane BIlL mg/kg 0.0048 0.00048
826DB 08/03/07 1829 lwiIiy Q25514
12-Dichloroprupane BIlL mg/kg 0.0043 0.00036 82609 08/03/07 129 Iwitry Q25514
135-Trlmathylbenzene BRL mg/kg 0.0048 0.0004 826DB 0803/07 1829 IWIIIY Q25514
13-Dtchlorobanzene SRI mg/kg 0.0048 0.00041 826DB 08/03/07 1829 iwitry Q25514
3-Dlchloropropane BRL mg/kg 0.0048 0.00033 826DB 0803/07 1829 Iwitry 025514
14-Dlchlorobenzene SRI mg/kg 0.0048 0.00038 82609 08/03I07 1829 Iwiby 025514
22-Dichioropropane SRI mg/kg 0.0048 0.00024 82608 08/03/07 i29 twlhii 025514
2-Chiorotoiuene BR.mg/kg 0.0048 0.00036 826DB 08/03/07 1829 lwttry 025514
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Spdngbrook Road P.O Box 240543-Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page 15 o135
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] ToIl Free Numben 1-8001529-8394 Fax [phone]
.1
.9
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Laboratory Report
08/10/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-3
ttn Chris Ward Prism Sample ID 188654
Box 7030
Sample Matrix Soil CCC Group G0807064
har1otte NC 28241 Time Collected 08/02/07 945
Time Submitted 08102/07 1325
aremeter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/lime
-Hexanone BRL mg/kg 0.048 0.0005
828GB 08/03107 1829 wiIrr 025514
-Chiorotoluene BRL mg/kg 0.0048 0.00025
82608 08/03107 1829 Iwltiy 025514
-Methyl-2-pentanone MIBK BR mg/kg 0.048 0.00048 526GB 08103/07 1829 Iwltry 025514
BR mg/kg 0.048 0.0019
82608 08103/07 1829 iwlIry
Ienzene BR mg/kg 0.0029 0.00039 826GB 08/03/07 1829 IWIry 026514
Irumcbenzene ORL mg/kg 0.0048 0.00034 82608 08103107 1629 Iwitc Q25514
trornochloromethane BR mg/kg 0.0048 0.00029
826GB 08/03/07 1829 Iwttry 025514
lromodlchlommethane BRL mg/kg 0.0048 0.00042 826GB 08103/07 1829 Iwttry 025514
lramoforrn BRI mg/kg 0.0048 0.00036
82608 08103/07 1829 twltiy 025514
tromoruethane BR mg/kg 0.0096 0.00056
82608 08/03/07 1829 Iwiry 025514
athon tetiachlorlde BRL mg/kg 0.0048 0.00028 82608 08/03/07 1829 Iwby 025514
hlorobenzene BRL mg/kg 00048 0.00037 826GB 08/03/07 1829 tstty 025514
htorodIbromomothane BR mg/kg 0.0048 000033 82605 08/03/07 1829 twhy 025514
hloroathane BR1 mg/kg 0.0096 0.0004 82600 08/03107 1829 Iwitry 025514
thloroIrm BRI mg/kg 0.0048 0.00036
8260B 08/03/07 129 lwity 025514
hloromethane BRL mg/kg 0.0048 0.00034 82608 08/03/07 1829 hæIry 025514
is-I 2.Dlchloroethene BRL mg/kg 0.0048 0.00021 826GB 0810307 1829 IwihY 025514
Is-13-Dlchloropropene BRI mg/kg 0.0048 0.00031 82608 08/0307 1829 Iwby 025514
tlchlorodifluommethane BRL mg/kg 0.0048 0.0011 826GB 08/03/07 129 twItry 025514
ilhylbenzane BR mg/kg 0.0048 0.00034 82608 08/03107 129 lwitiy 025514
ether IPE BR mg/kg 0.0048 0.00016 826GB 08/03107 1829 twitry Q25514
3opropylbenzene BR mg/kg 0.0048 0.00039 8260B 08/03/07 129 IwitiY 025514
ip-Xylenes 881 mg/kg 0.0096 0.00067 82608 08103107 1829 IWihy 025514
4ethyl ethyl ketone MEK BRL mg/kg 0.096 0.0013 82608 08/03/07 1829 Iwtty 025514
tethyl t-bu ether MTBE BRL mg/kg 0.0096 0.00028 826GB 08/03/07 129 twitiy 025514
4ethylane chloride BRL mg/kg 0.0048 0.0004 82608 08/03107 1829 lwltY 025514
-Butylbenzena SRI mg/kg 0.0048 0.00039 826DB 08/03107 1829 lwity 025514
Page 16 of 35
This report should not be reproduced except In Its entirety without the written consent or Prism Laboratories Inc
449 Sprlngbroak Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800I529.6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
ttn Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
lime Submitted
WS-3
188654
00807064
08/02/07 945
08/02/07 1325
Parameter Result Units Report MDL Dilution Method
Limit
Analyst
n-.Pmpylbenzene
Naphthalene
o-Xylene
p-lsopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzcne
Tetrachioroethene
Toluene
trans-12-Dlchloroethene
trans-13-Dlchlompropene
Trlchlaroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
BRL
DRL
BRL
BRL
SRI
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
DRL
0.0048 000029
0.0096 0.00056
0.0048 0.00029
0.0048 0.0004
0.0048 0.00032
00048 0.00048
0.0048 0.0003
0.0048 0.00083
0.0048 0.00033
0.0048 0.00031
0.0040 0.00034
0.0048 0.00029
0.0048 0.0004
0.024 00017
0.0048 0.00062
Factor
Analysis
Dateflime
08103/07 1829 lwItiy
08103107 1829 lwiLty
09/03/07 1829 IWitly
08103/07 1829 Iwhy
08103/07 1829 Iwitry
0803/07 1829 lwhy
08/03107 18.29 Iwiby
09/03/07 1829 IwIby
08/03/07 1829 twitiy
08103/07 1829 twIIiy
08/03/CT 1829 twitiy
08/0307 1829 iwby
08103/07 1829 Iwitry
08/03107 1829 Iwitry
08/03/07 1829 lwitry
82608
82608
82608
82608
826GB
826GB
825GB
526DB
82600
82608
826GB
826GB
82608
826GB
82608
Batch
ID
Q25514
025514
Q25514
025514
025514
025514
Q25514
Q25514
025514
025514
025514
025514
025514
025514
Q25514
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rng/lcg
mg/kg
Surrogate Recovery Control LImits
Toluene-dU 91 81 -128
Dltimmolluoromethana 91 67-143
Bromofluombonzene 108 77-128
Semi-volatIle Organic Compounds by GCIMS
124-Trichlambenzene BRL
12-Dlchlorobenzene SRI
13-Dlchloroboozene BRL
14-Dlchlorobenzene SRI
245-Trichiomphenol SRI
2.48-Trtchlomphenaj SRI.
0.37
0.37
0.37
0.37
0.37
0.37
0037
0.027
0.027
0.034
0038
0.036
827CC
827CC
82700
82700
82700
82700
0807/01 1834 kcamplgolto
08107/UT 1834 kcmptgcIto
08107107 1834 kcamplgolto
0807/07 1834 kcamplgolto
08/01107 1834 kcamp1olIo
08/01107 1834 kcamplgotto
Q25550
025550
025550
025550
025550
025550
Page 17 of 35
........I....k....P.IJ
ESP Associates PA
Qtn Chris Ward
P.O Box 7030
3hadotte MC 28241
NC Certillcallon No.402
Sc Certilicalion No 99012
NC Drinking Water CaL No 37735
Laboratory Report 11
08110/07
Pt
-t
24-Dlchlorophenol
24-Dirnethyiphenol
2Dlnitrophenot
24-Dlnllrotoluene
28-Dlnitrotoluene
Z-Chloronaphthalene
2-Chiorophenol
2-Methylnaphihalene
2-Methyiphenol
2-Nilrophenol
34-Methylphenol
33-Dlthlorobenzldlne
46-DinIlro-2-methylphenol
4-Bromophenylphenylether
l-Chlom-3-methylphenol
4-Chioroaniline
4-Chlorophenylphenylether
4-Nitrophenol
Acenephthene
Aoenaphthytene
Anthracene
Azoberizene
Benzoaanthracene
Benzoapyrene
BenzobIluoranthene
Benzoghlperylene
Benzokfluoranthene
This report should not be repmduced except In its entirety without the written consent of Prism Laboratories Inc
449 Spylngbrook Road P.O Box 240543 Charlotte NC 282240543
Phone [phone] Toll Free Number 1-800/529-6384 Pat 704/525-0409
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 188654
Sample Matrbc Soil CCC Group 00807064
Time Collected 08/02/07 945
Time Submitted 08/02/07 1325
Parameter Result Units Report MDL DilutIon Method Analysis Analyst Batch
Limit Factor Date/Time It
82700 00/07/07 1834 koamplgotto 025550BRLmg/kg 0.37 0.031
BRL mg/kg 0.37 0.036 82700 08/07/07 1834 kcamplgotlo 025550
ain mg/kg 1.9 0042 8270C 08/07/07 1834 kcainplgotto 025550
SRI mg/kg 0.37 0.021 8270C 08107/07 1834 kcamplgoilo 025550
SRI mg/kg 0.37 0.040 82700 08/07/07 1834 kcamplgotto 025550
BR mg/kg 0.37 0038 82700 08107/07 1834 kcampigotto 025550
BR mg/kg 0.37 0.029 82700 08107/07 1834 kcamplgotto 025550
BR mg/kg 0.37 0.030 82700 08107/07 1834 kcampigotto 025550
BR mg/kg 0.37 0.035 82700 08107/07 1834 kcampigotto 025559
BR mg/kg 0.37 0.045 82700 08107/07 1824 kcampigotto 025550
BR mg/kg 0.31 0.038 82700 08107/07 1834 kcamplgoito 025550
BRL mg/kg 0.75 0.023 82700 08/07/07 1834 keamplgatto 025550
BR mg/kg 1.9 0.023 82700 08/07/07 1834 kcetnplgotto 025550
SRL mg/kg 0.37 0.035 82700 08/07107 1834 kcamplgotto 025550
BRL mg/kg 0.75 0.027 82700 08/07/07 1834 kcamplgotto 025550
BR mg/kg 0.37 0.048 82700 08/07/07 1834 kcamplgotto 025550
BRL mg/kg 0.37 0.023 82700 08/07/07 1834 kcamplgotto 025550
BR mg/kg 1.9 0.025 827CC 08/07/07 1834 kcampigotto 025550
URL mg/kg 0.37 0.037 82700 08/07/07 1834 keamplgotto 025550
SRI mg/kg 0.37 0.037 82700 08/07/07 1834 kcamplgotto 025550
SRI mg/kg 0.37 0.028 82700 08/07/07 1834 keamplgotto 025550
BR mg/kg 1.9 0.035 82700 08/07/07 1834 kcaznpigotto 025550
0.10.1 mg/kg 0.37 0.052 82700 08/07/07 1834 kcanwtootto 025550
BR mg/kg 0.37 0.043 82700 08/07/07 1834 kcamplgotto 025550
BR mg/kg 0.37 0.017 82700 08/01/07 1834 kcamplgotto 025550
BR mg/kg 0.37 0.018 82700 08/01/07 1834 kcamplgolb 025550
BR mg/kg 0.37 0.030 82700 08107/07 1834 kCatTIpIgDUO 025550
Page 18 of 35
ESP Associates PA
ttn Chris Ward
Box 7030
harlotte NC 28241
Laboratory Report
08110107
Project ID Morehead Commons No Client Sample 1D WS-3
Prism Sample ID 188654
Sample Matrix Soil COC Group 60807064
lime Collected 08102/07 945
Time Submitted 08/02/07 1325
BRL
BRL
BRI
BRL
BRL
8RL
BRL
0.11
URL
BRL
URL
BRL
BRL
BRL
025
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRL
SRI
SRI
BRL
mg/kg 1.9 0.16
mg/kg 0.75 0.039
mg/kg 0.37 0.043
mg/kg 0.37 0.041
mg/kg 0.37 0.032
mg/kg 0.37 0.018
mg/kg 0.37 0.023
mg/kg 0.37 0.062
mg/kg 037 0.017
mg/kg 0.37 0.028
mg/kg 0.37 0.037
mg/kg 0.37 0.032
mg/kg 0.37 0.023
mg/kg 0.37 0.025
mg/kg 037 0026
mg/kg 0.37 0.022
mg/kg 0.37 0.019
mg/kg 0.37 0.036
mg/kg 0.37 0.039
mg/kg 0.37 0.039
mg/kg 0.31 0.038
mg/kg 037 0.033
mg/kg 0.37 0.042
mg/kg 037 0.019
mg/kg 0.31 0.041
mg/kg 037 0.036
mg/kg 1.9 0.031
8270C
82700
82700
82700
8270C
82700
82700
8270C
82700
827CC
82700
82706
82706
82700
827CC
8270C
82700
82700
82700
82700
827CC
82706
82700
8270C
82700
82706
82100
08/07/07 1834 kcamplgotto 025550
08/07/07 1834 koampigotto 025550
08/07/07 1834 kcamplgouo 025550
08/07/07 1834 koamplgolto 025550
08/07/07 834 kcamplgolto 025550
08/07/07 1834 kcamplgotto 025550
08/0707 1834 kcainplgotto 025550
08/07/07 1834 kcamplgottn 025550
08/07/07 1834 kcamplgotto 025550
08/07/07 1834 koamplgotto Q2555D
08107107 1834 kcamplgolto 025550
08/07/07 1834 kcamplgotto 025550
08/07/07 1834 kcamptgotlo 025550
08/07/07 1834 kcamplgotto 025550
08/07107 1834 kcamplgotto Q25550
08/07/07 1834 kcamplgolto 025550
08107/07 1834 kcamplgotto 025550
08/07/07 1834 kcamplgotto 025550
08/07/07 1834 koamplgotto 025550
08107/07 1834 kcampigotto Q25550
08/07107 1834 kcamptgotto 025550
08107/07 1834 kcamplgntto 025550
08/07/07 1834 kcamplgotb 025550
08/07/07 1934 kcampfgotto 025550
08107/01 1834 kcampigotto 025550
08/07/07 1834 koampigolto 025550
08/07/07 1834 kcarnplgotto 025550
This report should not be repnduced except inks entirely without the written consentof Prism Laboratories Inc
449 Spilngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Numbon 1400/529-6364 Fax [phone] Page 19 of 35
.1
NC Certitication No 402
SC Ceitlilcatlon No 99012
NC Drinking Water Cat No 37735
aranieter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
ii
3enzolc acid
3enzyl alcohol
31s2-chlomethoxymethano
31s2-cbloroethylother
31s2-chioroisopropylether
31s2-athylhexylphthalate
utylbenz1phthalate
hrysene
I-n.butylphthalate
31-n-octylphthalate
Ibenzoahanlhracene
ibenzoftiran
Diethyiphihalate
Dlmethylphthaiate
Fluoranlhene
Fluorono
hfexachiorobenrene
F-Iexachlorobutadlene
l-iexachlorooyclopentadlene
Hexachioroethane
Indeno1 23-cdpyrene
Isophomne
N-Nitrosodl-n-propylamlre
N-Nltrosodlphenylamlne
Naphihalerte
Nltrobenzene
Pentachlorophenol
ESP Associates PA
\ttn Chris Ward
.0 Box 7030
harlotte NC 28241
Laboratory Report
08/1 0/07
WS-3
163654
00807064
08/02/07 945
08/02/07 1325
henanthrene
henol
yrene
MDL Dilution
Factor
Method
30.08 mL 35508
Analysis
Date/lime
08107/07 1834 keamplgotlo
08107107 1834 keampfgotlo
08107/07 1834 kcampigotb
08104/07 900 pbarr
025550
025550
025550
ixtractablc Petroleum Hydrocarbons by
GC-FlD
1-C22 Aromatlcs BRL mg/kg
Ina1ysis Note for 011-022 Jromatics
9-C36 Aliphatics BRL mg/kg
9-C18 Aliphatics BRL mg/kg
Sample Preparation 9.89g 2mL EPI-1 0810307 700 pbarr P19081
This report should not
be reproduced except in its entirety without the written consent or Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1400/529-6384 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil Coc c3roup
Time Collected
Time Submitted
arameter Result Units Analyst Batch
IDReport
Limit
0.37
0.37
0.17J
URL
0.21
mg/kg
mg/kg
mg/kg
0.018
0.041
0.37 0.025
Sample Preparation
8270C
8210C
8270C
P19082
Surrogate Recovery Control Limits
Terphenyl-d14 78 41 -136
Phenol-d5 59 13-95
Nltrobonzened5 63 14-103
2-Fluómphenol 61 14-89
2-Fluoroblphenyl 75 21 -100
246-Tiibromophenal 81 25-123
11 6.2 MADEP EPI-I 08/08/07 035 grappacclofl Q25548
Adjusted value
11 1.1 MADEP EPH 08108/01 035 grappeectoll 025548
11 3.7 MADEP EPI-I 0808/07 035 greppacclolt 025548
Surrogate Recovery Control Limits
o-Teiphen4 94 40-140
Intajs bviCp
hromium
.ead
2-Fluorobiphenyl 90 40-140
2-Bmmonaphthatene 95 40-141
1-Chloro-octadecarro 90 40-140
19 mg/kg 0.28 0.016 60108 08/03/07 2029 mcampbell Q25521
100 mg/kg 028 0.010 ODIOB 08/03/07 2029 mcampbell 025521
Page 20 ci 35
Sample Comments
BRL Below Reporting Urn
J-Estimated value between the Reporting Limit and the MDL
The results In this report relate only to the samples submitted lbr analysis and meet state certification requirements other than
NELAC certification eccept forthose Instances Indicated in the case narrative and/or test comments
Al results are reported on dry-weight basis
Angela ft Overcash V.P Laboratory Services
Ths report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone[phone] Toll Free Number 1400529-6364 Fax [phone]
.4
SP Associates PA
ttn Chris Ward
Box 7030
NC CertificatIon No 402
Sc Certification No 99012
NC Drinking Water Cart No 37735
Project ID Morehead Commons No
Sample Matrix Soil
hartotte NC 26241
Laboratory Report
06110107
Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
WS-3
108654
30807064
08102/07 945
08/02/07 1325
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/lime ID
Sample PreparatIon 1.99 50 mL 30509 08/03/07 745 ddIXO3l P19078
llolatile Petroleum Hydrocarbons by GC-PIDJ Fin
l5-C8 ilphat1cs BRL mg/kg 5.7 1.1 MADEP VPI-I 08107/07 55B hwagnar 025565
Analysis Note for CS-Cli Aliphatics Aajusted value
C9-C10 Ammalics BRL mg/kg 5.7 0.034 MADEP VPI-I 08107/07 558 hwagnar 025565
09-Cl2AllphaIIcs BRL mg/kg 5.7 1.7 MADEP VPH 08/07107 558 tiwagner 025565
Analysis Note for C9-C12 Miphatics Adjusted value
Surrogate Recovery Control LImits
25-Dibromotofuene-PID 97 70-130
25-Dlbromotoluene-FID 104 70-130
Sample Weight Determination
Weight 21.95 MADEP VPH 08108107 000 thrown
Weight 16.95 MADEP VPI-l 0808/07 001 thrown
Page 21 of 35
ESP Associates PA
ttn Chris Ward
Box 7030
har1otte NC 28241
Laboratory Report
08110107
Project ID Morehead Commons No Client Sampla ID WS4
Prism Sample ID 188655
Sample Matrix Soil COO Group G0507064
Time Collected 08/02/01 1000
Time Submitted 08/02/07 25
Fercent Solids Determination
ercent Solids
5.91
6.42
5.51
5035 05110107 000
5035 05/10107 000
5035 08/10/07 000
brown
Ibrown
Ibrown
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Datefllme ID
SLT SM2540 08/03/07 1555 ddixon
2rn Die Weight Determination
Weight Bisulfate
Weight Bisulfata
Weight Methanol
Ifttlptile Organic Compounds by GCIMS
I1i-Trichloroethane BRL mg/kg 0.0044 0.00025 82605 05/03/07 1912 Witty 025514
L122-Tetrachloroethane BRL mg/kg 0.0044 0.00045 826DB 08103/07 1912 IWiby 025514
I12-Ttichloroethane BRL mg/kg 0.0044 000027 82603 05103/07 1912 IwlIry 025514
11-Dichioroothana BRI mg/kg 0.0044 000032 826DB 08/03107 1912 Iwflty 025514
lj-Dlchioroethene RRL mg/kg 0.0044 0.00034 826DB 08/03/07 1912 twltry 025514
1-Dlthloropropene URL mg/kg 0.0044 0.00039 82603 08/03/07 1912 iwlIjy 025514
123-Trichlorobenzene BRL mg/kg 0.0044 000049 826DB 08/03107 1912 twitty Q25514
l23-Trlchloropropane BRL mg/kg 0.0044 0.00039 826DB 03/03107 1912 twiby Q25514
l.24-Trichlorobenzene BRL mg/kg 0.0044 0.00042 82608 08/03107 1912 Iwfby 025514
124-Trimethylbenzene BRL mg/kg 0.0044 0.00034 82608 08103/07 1912 LwIUy 025514
12-Dibromoethane EDB 8RL mg/kg 0.0044 0.00008 82608 08/03/07 1912 tWitry 025514
t.2-Dlchlorobenzene BRL mg/kg 0.0044 0.00024 82608 08103/07 1912 iwitty 025514
t2-Dlchloroethane EIRL mg/kg 0.0044 0.00044 826DB 08103/07 1912 iwitry Q2551
12-Dichioroprapane BRL mg/kg 0.0044 0.00033 826DB 08103/07 1912 Iwib 025514
l3.5-Trimethylbenzene BRL mg/kg 0.0044 0.00037 826DB 08/03/07 1912 IWitty 026514
l3-Dichlarobenzene ERL mg/kg 0.0044 0.00038 82608 08103107 1912 IwItry Q25514
13-Dichioropropane BRL mg/kg 0.0044 0.0003 826DB 08/03/07 1912 iwiliy 025514
l4-Dlchlorobenzene BRL mg/kg 0.0044 0.00034 82608 08/03/07 1912 iwltry 025514
2-DIchIoropropane BRL mg/kg 0.0044 0.00022 82603 08/03/07 1912 Iwitty 025514
-Chtorotoiueno URL mg/kg 0.0044 0.00033 82608 08/03/07 1912 IWitty Q25514
This report should not be reproduced except in Its entirety without the written consent or Prism Laboratories Inc
449 Sprlngbroolc Read P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-0364 Fax [phone] Page 22 of 35
NC Certification No 402
SC Certification No 99012
NC DrinkIng Water Cert No 37735
This report should not be reproduced except In Its entirety without the written consent of PrIsm Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll 1ree Number 1-8081529-6364 Fax [phone]
Laboratory Report
08/10/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-4
ttn Chris Ward Prism Sample ID 188655
P.O Box 7030
Sample Matrix Soil coc Gmup 00807064
Chadotte NC 28241 Time Collected 08/02/07 1000
Time Submitted 08102/07 1325
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.044 0.00046 826GB 08/03107 1912 lwltW 025514
4-Chiorotolueno URL mg/kg 0.0044 000023 826DB 08/03/07 1912 Iwiliy 025514
4-MethyI-2-pentanone MIBK BRI mg/kg 0.044 0.00044
826GB 08103107 1912 IWkIy 025514
cetone BRL mg/kg 0.044 0.0017 826DB 08103107 1912 IWltry 025514
Benzene BRL mg/kg 0.0027 0.00035 826DB 08/03/07 1912 Lwitry 025514
Brornobenzene BR.mg/kg 0.0044 0.00031 626GB 08/03/07 1912 lwitty 025514
Bromochtommethane BRL mg/kg 0.0044 0.00027 82608 08/0307 1912 IwlIry 025514
Bromodlchloromethane BRL mg/kg 0.0044 0.00039
82606 08103/07 1912 twitrY 025514
Bronioform BRL mg/kg 0.0044 0.00033 82606 08103107 1912 Iwitry 025514
Brornomethane BRL mg/kg 0.0088 0.00051 825GB 08103/07 1912 Iwitry 025514
Carbon tetrachiodde BRL mg/kg 0.0044 0.00026 826GB 08/0307
1912 Iwitry 025514
Chloivbenzene BRL mg/kg 0.0044 0.00034 826DB 08103/07 1912 IwItry 025514
Chlorodlbmmomelhano BRL mg/kg 0.0044 0.0003 826DB 08/03/07 1912 Iwiby 025514
Chtoroethane BRL mg/kg 0.0088 0.00036 82608 08/03107 1912 IwIby 025514
Chloroform BRL mg/kg 0.0044 0.00033 826DB 08/03/07 1912 twltry 025514
Chloromethane BR mg/kg 0.0044 0.00031 82608 08/03107 1912 wRry 025514
cls-12-Dlchlcmethene BRL mg/kg 0.0044 0.00019 826GB 0803/07 1912 lwitry 025514
cls-13.Dlchloroprcpene BRL mg/kg 0.0044 0.00028 826DB 08/03/07 1912 twitlY 025514
Dlchlorodlfluoromethane BRL mg/kg 0.0044 0.00099 82808 08/03/07 1912 Iwitry 025514
Ethylbenzene BRL mg/kg 0.0044 0.00031 825DB 08/03/07 1912 wiry 025514
leopropyl ether IPE BRL mg/kg 0.0044 0.00015 82606 08/03/07 1912 IWILIY 025514
lsopropylbenzene BRL mg/kg 0.0044 0.00035 826DB 08/03/07 1912 lwitry 025514
mp-Xylenes BRL mg/kg 0.0088 0.00062 82608 08/03/07 1912 Iwilsy 025514
Methyl ethyl ketone MK BRL mg/kg 0088 0.0012 826GB 08/03/07 1912 IwiUy 025514
Methyl t-butyl other MTBE BRL mg/kg 0.0088 0.00026 62603 08/03/07 1912 LWIJY 025514
Methylene chloride BRL mg/kg 0.0044 0.00036 826DB 08103/07 1912 Iwitry Q25514
n-Butylbenzene BRL mg/kg 0.0044 0.00035 82606 08/03/07 1912 iwiry 025514
Page 23 of 36
ESP Associates PA
Athi Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morohead Commons No Client Sample ID
Prism Sample ID
Sample Matrbc Soil coo Group
Time Collected
Time Submitted
WS-4
188655
00807064
08/02107 1000
08/02/07 1325
This report should not be reproduced except In Ils entirety without the written consent ci Prism labaratorles Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 2B2244543
Phone [phone] Toll Free Number 1-800/529-8364 Fax [phone]
NC Certification No 402
SC Certification Nc 99012
NC Drinking Water Cert No 31735
.1
Laboratory Report
08/10/07
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Untit Factor Date/Time ID
0.0044 0.00027 8260B 08/03/07 1912 Iwitsy Q25514
0.0088 0.00051 82608 08/03/07 1912 iwilry 025514
0.0044 000027 82608 08/03/07 1912 lwilty 025514
0.0044 0.00036 82605 08/03/07 1912 iwltry 025514
0.0044 0.00029 B260B 08/03/07 1912 lwilzy Q25514
0.0044 0.00044 8260B 08/03/07 1912 twitiy 025514
00044 0.00027 82608 08/03/07 1912 lwltty Q25514
0.0044 0.00076 8260B 08/03/07 1912 Iwitfy 025514
0.0044 0.0003 82608 08/03/07 1912 IwIky Q25514
00044 0.00034 8260B 08/03/07 1912 Iwitry 025514
0.0044 0.00031 8260B 08/03/01 1912 Iwitry 025514
0.0044 0.00027 8260B 08/03/07 1912 Iwitry Q25514
0.0044 0.00036 82608 08103107 1912 witiy 025514
0.022 0.0016 8260B 08/03/07 1912 Iwitry 025514
0.0044 0.00057 82608 08/03/07 1912 Iwitry 025514
n-Propylbenzene SRI
Naphihalene BRL
o-X4ene BRL
p-isopropyltoluene BRL
soc-Butylbenzsna BRL
Styrene BRL
tert-Butylbenzene BRL
Tetzachloroethene BRL
Toluene SRI
trans-I 2-Dlchforcethene BRL
trans-I .3-Dichioropropeno SRI
Irichioroethene BRI
rdchtorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Seml-votatffB Orcanta Compounds by GC/MS
l24-Trlchlorobenzerte SRI
l2-Dlchlorobenzene SRI
l3-Dlchlorobenzena BRL
14-Dlchlorobeazene SRI
M45-Trlthlorophenol SRI
a46-Trlchlorophenol BRI
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Sunogate Recovery Control Limits
Toluene-d8 97 81 -128
Dlbromofluommethane 93 67-143
Bromofluorobenzerie 109 77-128
0.37
0.37
0.37
0.37
0.31
0.37
0.037
0.027
0.027
0.033
0.038
0.035
82700
82700
82700
82100
8270C
8270C
08/07/07 1553 kcampigatto
08107/07 1553 kcanipFgntio
08/07/07 1553 kcamplgolio
08101/07 1553 kcampJotto
08/07/07 1553 kcamplgolto
08/07/07 1553 kcamplaoita
025550
025550
025650
026550
025550
025550
Page 24 of 35
ESP Associates PA
ttn Chris Ward
Box 7030
harlotte NC 28241
Laboratory Report
08/10107
Project ID Morehead Commons No Client Sample ID WS4
Prism Sample ID 88655
Sample Matrbc Soil COO Group 00807064
Time Collected 08/02107 1000
Time Submitted 08102/07 1325
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
aRt mg/kg
BRL mg/kg
BRI mg/kg
BRI mg/kg
BRI.mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
Bat mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRI mg/kg
BRt mg/kg
0.16 mg/kg
0.14 mg/kg
0.14 mg/kg
BRL mg/kg
0.17 mg/kg
Limit Factor
0.37 0.031 82700
82700
82100
82700
82700
82700
82700
82700
82700
82700
82100
82700
82700
82700
82700
82700
82700
82700
82700
82700
82700
8270C
8270C
8270C
8270C
82700
82700
0.37 0.036
1.8 0042
0.37 0.021
0.37 0.039
0.37 0.038
037 0.029
0.37 0.029
0.37 0.035
0.37 0.044
0.31 0.038
0.74 0.023
1.8 0.022
0.37 0.035
0.74 0.027
0.37 0.047
0.31 0.023
1.8 0.025
0.37 0.036
0.37 0.037
0.37 0.028
1.8 0.034
0.37 0.052
0.37 0.043
0.37 0.017
0.37 0.018
0.37 0.030
Analysis Artayst Batch
Date/Time ID
08/07/Ui 1553 kcamptsotto 025550
08/07107 1553 kcamplgoflO 025550
08/07/07 1553 kcamplgoUD 025550
08/07/01 1653 kcainpigofto 025550
08107107 1553 keamplgotto Q25550
08/01/07 1553 kcamplgutto 025550
08/07/07 1553 kcampigotto 025550
08/07/07 1553 kcamplgoflo 025550
08/07/07 1553 kcamplgolto Q25550
08/07/07 1553 kcsmplgotto 025550
08/07/07 1553 kcamplgotto Q25550
08107/07 1553 kip1go 025550
08107107 1553 kcamplgotto 025550
08/07107 1553 kcamplgotto 025550
08/07107 1563 kcamplgotto 025550
08/0107 1553 kcamplgaltc 025550
08/01/07 1553 kvamptgotto 025550
08/07/07 1553 kcampigotto 025550
08101/07 1553 kcamplgotto 025550
0810707 1553 kcamplgoUo 025550
08/07/07 1553 kcamplgotiz 025550
08/07/07 1553 kcamplgotto Q25550
08/07101 1553 koamplgotto fl2555Q
08/07/07 1553 kcarnplgotti3 025550
08107/07 1553 kcampigotto 025550
08/01/07 1553 kcamplaoLto Q25550
08/07107 i553 kcampgotto 026550
This report should not
be reproduced except In its entirety without the
written consent of Prism l.aboratoæes
Inc
449 Spiingbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1.800/529.8364 Fax[phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
if
Result Units Report MDL Dilution Method
Parameter
24.DlChlo1OPh8nOl
24-DimethyipheROl
24-Dlnltrophefloi
24-UlnItrotolUSne
26-DlnItrotoIURfle
2-ChloronaphUlaisfle
2-ChloropheflOl
2-Methylnaphthaleflo
2-Methyiphoflol
2-NitrophenOl
34.Methylphenol
33-DIchlorobefl7idiflB
46.DinILro-2-methylPheflOI
4.BromophenylpheflYlether
4-Chloro-3-methYlPhenOl
4-Chioroanlilne
4.Chlorophenylphenylothor
4-Nltrophenol
Acenaphtbene
Acenaphthylena
Mthracene
Azobenzerte
Benzoaanthracefle
Benzoapyrene
Benzobfluoranthene
Benzoghtperyiene
Benzokfluoranthene
Page 26 of 35
ESP Associates PA
tth Chris Ward
Box 7030
charlotte1 NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-4
188655
G0807064
08/02/07 1000
08/02/07 1325
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Spdngbrooh Road P.O Box 240543 Cherlotte NC 25224-0543
Phone [phone] Toll Free Number 1-8001529-8364 Fax [phone]
NC CertIfication No 402
SC Cerlllloation No 99012
NC Drinking Water Cert No 37735
Laboratory Report
08/10/07
Parameter Result Units Report MDL DliuUon Method
Umlt Factor
18
AnalystAnalysis Batch
Date/lime ID
Benzolc acid BRL mg/kg 0.16 82700 08107/01 1553 hcamplgolio 025550
8enzyt alcohol BRI mg/kg 074 0.039 8270C 0807/07 1553 kcampigotto Q25550
Bis2-thloroethoxymethafle ORL mg/kg 037 0.042 8270C 08/01/07 1553 kcampigotto Q25550
Sls2-chloroethytether SRI mg/kg 0.37 0.040 82700 08/07/07 1553 kcainplgotio 025550
Bls2-chlomlsopropyiether BRL mg/kg 0.37 0.032 8270C 08/07107 1553 kcampigotlo 025550
Bls2-ethylhexylphthalate SRI mg/kg 037 0.018 8270C 08/07/07 1553 kcamplgotio 025550
Butylbenzylphthaiate SRI mg/kg 037 0.023 8270C 08/07/07 1553 kcmp1tto 025550
lhrysene 0.14 mg/kg 0.37 0051 8270C 08107/07 1553 kcamplgotto 025550
D1-n-butylphthalate BR.mg/kg 0.37 0.017 827CC 08/07/07 1553 kcamplgctto 025550
Dl-n-octylphthalate SRI mg/kg 0.37 0.028 82700 08107/01 1553 kcamplgotto 025550
Dibenzoahanthracene BR.mg/kg 0.37 0.037 82700 08/07107 1553 kcamptgotta Q25550
DlbenzoIuran BRL mg/kg 0.37 0032 82700 08107/07 1553 kcamplgotto 025550
Dlelhytphthalate BRL mg/kg 0.37 0023 82700 08/07/07 1553 kcampiotto 025550
Dlmethylphthalato ERL mg/kg 0.37 0.025 82700 08/07/07 1553 kcamplgotto 025550
Fluoranthene 036 mg/kg 0.37 0.025 82700 08/07/07 1553 kcampigotto 025550
Fluorene BR mg/kg 0.37 0.022 82700 08107/07 1553 kcamplgotto 025550
-Iexachlorobenzene BRL mg/kg 0.37 0019 82700 08107/07 1553 kCaJflplgotto 025550
llexachlorobutadlene BRL mg/kg 0.37 0.036 82100 08107/07 1553 lccarnphouo 025550
riexaclilorocyclopentadlene SRI mg/kg 0.37 0.039 82700 09/07/07 1553 kCampIgOtiO 025550
Hexachioroethana BRL mg/kg 0.37 0.038 821CC 08107/07 1553 kcamplgotlo 025550
Indenol23-cdpyrene BRI mg/kg 0.37 0.036 82700 08/07/07 1553 Iccamplgoflo 025550
lsophoione SRI mg/kg 0.37 0.033 827CC 08/07/07 1553 kcarnplgotio Q555Q
NJ-Nltrosodi-n-propylamlne SRI mg/kg 0.37 0.042 827CC 08107/07 1553 kcamploUo 025550
N-Nllrosodlphenyiamlne BR.mg/kg 0.37 0.019 827CC 08107/07 1553 kcaznplgotto 025550
Naphthalene BRI mg/kg 0.31 0.040 82700 08/07/07 1553 kcamplgatto 025550
Mltrobenzene SRI mg/kg 0.37 0.036 8270C 08107107 1553 kcampigotto 025550
Penlachloroplienol BRI mg/kg 1.8 0.031 62700 08/07/07 1553 kcampigouo 025550
Page 26 of 35
NC Certification No 402
SC Certification No 99012
NC DrInking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID WS.4
Prism Sample ID 188655
Sample Matrix Soil COC Group 00807064
Time Collected 08102107 1000
Time Submitted 08/02/07 1325
-1
Phenanthrene
Phenol
Pyrene
Sample Preparatlom
23 mg/kg
150 mg/kg
Report
Limit
0.37
0.37
0.37
l0.18g 2rnL
0.28 0.016 60106
0.28 0.018 6010B
Anaysis
Date/lime
08/07/07 1553 Iccamplgotto
08/07/07 1553 kcampgattQ
08/07/07 1553 kcamplgollo
08/04/07 900 pbarr
EPH 08/03/07 700 pbwr
08/03/07 2036 mcampbeli
08103/07 2036 mcarnpbell
Q26550
Q25550
Q25550
P19082
P19081
Q25521
Q25521
This report should not be repmduced except In Its entirety without the written consent or Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] ToIl Free Number 1400/529.8364 Fax [phone]
jII BioAisIyIkaJ
ESP Associates PA
Attr Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
Parameter Result Units MDL MethodDiluSon
Factor
0.OIB
0.040
0.025
Analyst Batch
ID
8270C
8270C
82TOC
30.22 mL 35508
Surrogate Recovery Control Limits
Terphenykll4 82 41 -136
Phenol-d5 56 13-95
Nitrobanzene-d5 65 14-103
2-Aucrophenol 69 14-89
2-Fluombiphenyl 70 21 -108
2.46-Tdbromophenol 81 25-123
0.28 mg/kg
BRL mg/kg
0.33J mg/kg
Sample Preparation
Extractable Petroleum Hg1rocarbons by 3C-FID
C11-C22Aromatics 15 mg/kg
na1ysis Note for Cl1-C22 1rornatics
C19.C36 Aliphatics BRL mg/kg
C9-Ci8AllphaUcs BRL mg/Kg
Metals bv
Chromium
Lead
11 6.0
Adjusted value.
11 1.7
ii 3.5
MADEP EPI-I 08/08101 403 grappaccloll Q25548
MADEP EPH
MADEP EPH
08/08/07 403
08/08/07 403
9rappaccloll
9rappaccioll
Q2i1548
Q26548
Surrogate Recovery Control Limits
o-Terphenyt 102 40-140
2-Fluoroblphenyl 97 40-140
2-Bromonaphthalene 102 40-140
1-Chioro-octadecane 85 40-140
Page 27 of 35
Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
WS-4
188655
G0807064
08/02/07 1000
08/02/07 1325
Parameter Result Units Report MDL Dution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 2.02 50 mL 305DB 08103/07 745 ddbon P19078
Volatile Petroleum Hydrocarbons by GC-PIDJFID
CS-Ca Allphatca BRL mg/kg 5.6 1.1 MADEP VPI-I 09107701 641 hwagnor Q25555
Pnalysis Note for C5-C8 AUphatics Adjusted value
09-ClOAromatics BRL mg/kg 5.6 0.034 MADEP VPH 08/07107 641 hwagner Q25555
C9-Cl2Aliphatlcs BRL rngikg 56 1.7 MADEPVPH 08/07/07 641 hwegner Q25565
Analysis Note for C9-C12 Aliphatics Adjustzed value
Surrogate Recovery Control Limits
Z5-Dlbromotoluene-PID 82 70-130
25-Dlbromotoluane-FID 94 70-130
SamDla Weight Datermhiatlors
Weight 16.74 MADEP VPH 08/08/07 000 brown
WeIght 20.11 MADEP WH 08108/07 000 brown
Sample Comments
BR Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results In this report relate only to the samples submiltod for analysis and meet state certiticatlon requirements other thanWELACcartificatknexceptforthose instances Indicated In the case narrative and/or test comments
4/1 results are ropoitodon di -weight be s/s
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in Its entirety without the wTitteri consent of Prism Laboratories Inc
449 Sprinbrook Road P.O Box 240543 Charlotte NC 29224-0543
Phone [phone] Toil Free Number 1-800/529-6364 Fax [phone]
NC CerllflcatJon No 402
SC Certification No.99012
NC Drinking Water Cert No 37735
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
Project ID Morehead Commons No
Sample Matrix Soil
Page 28 of 35
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 08/10/07
Full sMaAulyUta mlmmuntal SMutiuns
ESP AssocIates PA Project ID Morehead Commons No Client Sample 1D B-I
fQtn Chris Ward Prism Sample ID 188656
Box 7030 Sample Matrix Soil COG Group G0807064
Charlotte NC 28241 Time Collected 08/02107 1015
Time Submitted 08/02107 1325
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Daternma ID
Percent Solids Determination
ement Solids 89.9 SM2540 08/03/07 1555 ddixort
Sample Weiqht Determination
Neight Bisulfate 5.31 5035 08/10/07 000 ibrown
Neight Bisulfate 5.57 5035 0810107 000 brown
Iveight Methanol 4.91 5035 0810/07 000 Lbruwn
Volatile Orianlc Compounds by GCIMS
1.tl-Trlchloroethane BR rag/kg 0.0052 0.00029 8260B 0803/07 1955 lwhy Q25514
I122-Tetrachloroethane BRL mg/kg 0.0052 0.00053 82608 08/03/07 1955 Iwitry 025514
l.12-Thchtoroethane BRL mg/kg 0.0052 0.00032 82608 08/03/07 1955 lwltnt 025514
1.1-Dichiomethane BRL mg/kg 0.0052 0.00031 826DB 08/03/07 1955 Iwlhy 025514
l1-Dlchtomethene BR mg/kg 0.0052 0.00039 8260B 08/03/07 1955 lwitry Q25514
1.1-Dichlomproperie BRL mg/kg 0.0052 0.00045 826DB 08/03/OT 1955 lefty 025514
I23-Tdchloroberizene BRL mg/kg 0.0052 0.00057 826DB 08/03/07 1955 iwitry Q25514
123.Trlthloropropane BR mg/kg 0.0052 0.00045 826DB 08/03/07 1955 lwflry 025514
124-Trichlorobenzene BRL mg/kg 0.0052 0.00049 82608 08/03/07 1955 iwilry 025514
124-Trirriethylberizene BRL mg/kg 0.0052 0.00039 826DB 08/03/07 1955 Iwiby Q25514
12-Dibromoathane 5DB BRL rug/kg 0.0052 0.000093 826DB 08/03/07 1955 lefty 025514
l2-Dlchlorobenzene BR mg/kg 0.0052 0.00028 82608 08/03/07 1955 iwitiy 025514
12-Dichlomethane BRL mg/kg 0.0052 0.00052 82608 08103/07 1955 iwitry 025514
l2-Dichlcropropane BRI mg/kg 0.0052 0.00038 826DB 08/03/07 1955 Iwitry 025514
l.35-Tritnethylbenzene BRL mg/kg 00052 0.00043 82603 08/03107 1955 Lwitiy 025514
13-Diohlorebeuzene BR.mg/kg 00052 0.00044 826DB 08103/07 1955 iwitty 025514
13-Dichloropropane BRL mg/kg 0.0052 0.00035 82608 08/03/07 1955 Iwitiy 025514
l4-Dlchlowbenzena BRL mg/kg 0.0052 0.0004 826DB 08/03/07 1955 twitly 025514
a2-Dlchlompropane BR mg/kg 0.0052 0.00026 826DB 08103/07 1955 twthy 025514
a-Chlorotoiuene BRL mg/kg 0.0052 0.00038 8260B 08/03107 1955 twfty 025514
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 2822.4-0543
Phone [phone] Toll Free Number 1.800/529-6384 Fax [phone] Pags 29 of 35
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories lnc
449 Sprlngbroak Road P.O Box 240543 Charlotte NC 28224-0543
Phone 104I529.43$4 Toll Free Number 1.8001529-6384 Fax [phone]
NC Certification No 402
SC Certification Wa 99012
NC Drinking Water Cert No 37735
Laboratory Report
08110107
ESP Associates PA Project ID Morehead Commons No Client Sample ID B-I
\ttn Chris Ward Prism Sample ID 188665
Box 7030 Sample Matrix Soil COC Group 30807064
harlotte NC 28241 Time Collected 08/02107 1015
Time Submitted 08/02/07 1325
arameter Result Units Report MDL Dilutton Method Analysis Analyst
Batch
Date/lime IDLimitFactor
-Hexanone BRL mg/kg 0052 0.00054 8260B 08103/07 1955 Iwitiy 025514
1-ChIorutoluene BRL mg/kg 0.0052 0.00027 826GB 08/03/07 1955 lWItJy 025514
t-Methyl-2-pentanone MIBK BRL mg/kg 0.052 0.00052 826GB 08/03/07 1955 iwiby 025514
\cetone BRL mg/kg 0.052 0.0020 826GB 08/03/07 1955 Iwifry 025514
3enzena BRL mg/kg 0.0031 0.00041 82603 0803/07 1955 IwIhy 025514
3romoberizene J3RL mg/kg 0.0052 0.00036 826DB 08103/07 1955 Iwihy 025514
3romochloromelbane BRL mg/kg 0.0052 0.00031 826013 08103/07 1955 IWI1IY 025514
3mrnodlchloromethane BRL mg/kg 0.0152 0.00045 826013 08/03107 1955 lwilry Q25514
3romofbrm BRI mg/kg 0.0052 0.00038 826013 08/03107 1955 IWitry 025514
roniomethane BRL mg/kg 0.010 0.0006 826DB 08/03/07 1955 Iwlhy Q25514
arbon tetrachlortde BRL mg/kg 0.0052 0.0003 826DB 08/03/07 1955 IwlIy 025514
hlorobanzene BRL mg/kg 0.0052 0.00039 826DB 08/03/07 1955 lWIuiy 025514
Thlorodlbromomsthane DPi mg/kg 0.0052 0.00035 82608 08103/07 1955 IWIhy 025514
h1oreethane BRL mg/kg 0.010 0.00042 826DB 08/03/07 1955 Iwihy 025514
hlorofbrm BRL mg/kg 0.0052 0.00038 826DB 08103107 1955 iwiliy 025514
htoromethane BRL mg/kg 0.0052 0.00036 826DB 08103/01 1955 Iwitw 025514
ts-12-Dlchloroethene DPI mg/kg 0.0052 0.00023 826DB 08/03/07 19.55 Iwitsy 025514
1s-13.Dlchlaropropene BRI mg/kg 0.0052 0.00033 82603 08/03/07 1955 Iwitw Q25514
Ichlorodlfluommethane BRL mg/kg 0.0052 0.0012 826GB 08/03/01 1955 lwitiy 025514
thylbenzene BRL mg/kg 0.0052 0.00036 82603 08103107 1955 lwilry 025514
sopropyl ether IPE SRI mg/kg 0.0052 0.00018 826013 08/03/07 1955 lwiIri 025514
sopropylbenzeno BRL mg/kg 0.0052 0.00141 82608 08/03/07 1955 IwitrY 025514
up-Xyienes BRL mg/kg 0.010 0.00072 82603 08/03/07 1955 Iwitry 025514
ethyl ethyl ketone ME1 BRL mg/kg 0.10 0.0014 626GB 08/03/07 1955 Iwiby 025514
ilethy1 t-butyl ether MTBE BRI mg/kg 0.010 0.0003 82603 08/03/07 1955 lwitiy Q25514
1ethy1ene chloride BRL mg/kg 0.0052 0.00042 826DB 08103/07 1955 Iwitty 025514
i-Butylbenzeno BRL mg/kg 00052 0.00041 82608 08/03/07 1955 iwiIr 025514
Page 30 of 35
ESP Associates PA
LUn Chris Ward
Box 7030
TharJotte NC 28241
Laboratory Report
08/10107
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample 1D 188656
Sample Matrix Soil COC Group G0807064
Time Collected 08/02/07 1015
Time SubmItted 08/02/07 1325
NC CerlfficaUon No 402
SC Certiftoation No 99012
NC Drtnklng Water Cert No 37735
arameter Result Units Report MDL Dilution Method Analyst
i-Propyibenzene
iaphthaiene
-Xytene
-lSopmpyitOlUene
ec-Butylbenzena
5tyrene
ert-Rutylbenzene
retrathloroelhane
foluene
rans-1 .2-Dichioroethene
ians-13-Dlcliloropropene
rriclnoroethene
rorofluoromethne
dlnyl acetate
/inyl chloride
BRL
BRL
BRI
BRL
BRI
BRL
BRL
BR.
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Analysis Batch
Limit Factor Date/Time ID
0.0052 000031 8260B 08/03/07 1955 lwllq Q25514
0.010 0.0005 8260B 08/03107 1955 lwity Q25514
0.0052 0.00031 82608 08/03101 1955 Iwihy 025514
0.0052 0.00042 8260B 08/03/07 1955 lwitiy 025514
00052 0.00034 8260B 0803/07 1955 Iwiliy 025514
00052 0.00052 82609 08/03/07 1955 Iwitry 025514
0.0052 0.00032 82508 08/03/07 1955 Lwitiy 025514
0.0052 0.00089 8260B 08103/07 1955 IwIky 025514
0.0052 0.00035 8260B 08/03/07 1955 Iwtry 025514
0.0052 0.00039 8260B 08/03107 1955 iwItry Q25514
0.0052 0.00036 82608 08/03/07 1955 iwiby 025514
0.0052 000031 8260B 08/03/07 1955 iwitry Q25514
0.0052 0.00042 8260B 08103/07 1955 Iwilty 025514
0.026 0.0019 82608 08103/07 1955 Iwiliy 02551
0.0052 000066 82608 08103/07 1955 twitry 025514
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rug/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Toluene-18 95 81 -128
Dlbmmofluoromelhane 94 67-143
Bromofluorobarrzene 103 77-128
eml.votaflle Organic Compounds by 13C/MS
l2.4-Trichlombanzeno BRL
I2-Dlthlorobenzene BRL
L3-Dlchtarebanzene BR.
I4-Dlchlorobenzene BRL
4.5-Tr1thIorcphenol BR1
46-TrIchlorophenol BRL
0.37
0.37
0.37
0.37
0.37
0.37
0.037
0.027
0.027
0.033
0.038
0.036
82700
82700
82700
82700
82700
827CC
08/07/07 1307 keamplgono
08/07/07 1307 kcamplgotto
08/07/07 1307 kcamplgotto
08/07/07 1307 kcamplgotto
08/07/07 1307 kcampigalto
08107/07 1307 kcampToIto
025550
025550
025550
025550
025550
025550
This report should not be reproduced except In its entirety wilhout the written consent Pijam Laboratories lnc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Numben 1-800/529.5364 Fax [phone] Page 31 o35
FuO 8one MaytI4 En
ES Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte1 NC 28241
Laboratory Report
08/10107
This report should not be reproduced except In Its entirety without the written consent at Prism Laboratories Inc
448 $prlngbrook Road P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1409/529.6354 Fax[phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID B..1
Prism Sample ID 188656
Sample Mahix Soil COC Group 60807064
Time Collected 08/02/07 1015
Time Submitted 08/02/07 13.25
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
24-Dlthlorophenol BR1.mg/kg 0.37 0.031 8270C 08/07/07 1307 kcampigoftc Q25350
24-Dimethyiphenof BRL mg/kg 0.37 0.036 827CC 08107101 1307 kcamplgotto Q25550
24-Dlnitmphenol BRL mg/kg 19 0.042 827CC 08107107 1307 kcanipigotto 025550
24-Dlnltrotoluene BRL mg/kg 037 0.021 82700 08/01/07 1307 kcassplgtilto 025550
26-Dlnltmtoluene BRL mg/kg 0.37 0.039 82700 08/07/07 1307 kcampigotto 025550
2-Chloronaphthalene BRL mg/kg 0.37 0.038 8270C 08/07/07 1307 kcamptgotto Q25550
2-Chiorophenol BRL mg/kg 0.37 0.029 8270C 08/07107 1307 kcamplgotto 025550
2-Methylnaphthalene BRL mg/kg 0.37 0.030 827CC 08/07/07 1307 kcamplgotto 025550
2-Methphenof BRL mg/kg 0.37 0.035 8270C 08/07/07 13 kcampintto 025550
2-Nitrophenol BRL mg/kg 0.37 0.044 0270C 08/07/07 1307 kcampigotto 025551
34-Methylphenoi BRL mg/kg 0.37 0.035 827CC 08/07/07 1307 kcamplgotto 025550
33Dith1orohenzidIne ERL mg/kg 0.74 0.023 827CC 08107/07 1307 kcampigotto 025550
46-Of nhtro-2-m ethf phenol BRI mg/kg 1.9 0.023 827CC 08/07107 1307 hcampiQotto Q25550
4-Bromophenylpheriylether BRL mg/kg 0.37 0.035 8270C 08/01/07 1307 kcampigotto 025550
4-Chloro-3-methyiphenol BRL rug/kg 0.74 0.027 8270C 08/07/07 1307 kcaznpieotto Q25550
4-Chiomaniline BR mg/kg 0.37 0.047 827CC 08107107 1307 kcainplgotto 025550
4-Chiorophenyiphenylether ORL mg/kg 0.37 0.023 827CC 08107/07 1307 hcamplgoilo 025550
4.Nltrophenol BR1 mg/kg 1.9 0.025 8210C 08/07/07 1307 kcamplgntto 025550
Acenaphthene URL mg/kg 0.37 0.036 827CC 05/07/07 1307 kc2mpigotto 025551
Acenaphthyiene BRI.mg/kg 0.37 0.037 82700 08/07/07 1307 kcamplgotb 025550
Anthracene BRL mg/kg 1.37 0.028 827CC 08/07/07 1307 kcamplgotto 025550
Azobenzene BRL mg/kg 1.9 0.034 827CC 08/07/07 1307 keampitiotto 025550
Bonzoaanthracene BRI mg/kg 0.37 0.052 827CC 08/07/07 1307 kcampigotio 025550
Benzoapyrene BRI mg/kg 0.31 0.043 827CC 09/07/07 1307 kcamplgotlo Q25550
Benzobfluoranthene BRL mg/kg 0.37 0.017 827CC 08/07/07 1307 kcampfgotto 025550
Benzog.hlpeylene BRL mg/kg 0.37 0.018 82700 08/07/01 1307 kcampigotto Q25550
8enzokfluoranthene BR mg/kg 0.37 0.030 82700 08/07/07 1307 kcampigQtto 025550
Page 32 of 35
ESP Associates PA
ttn Chris Ward
P.O Box 7030
charlotte NC 28241
onz0Ic acid
Bunayl alcohol
31s2-chioroethoxymetharie
31s2-chloroethylether
3Is2-chlorolsopropylether
Bls2-ethylhex1phthalate
3utylbenzylphthalate
ChEysene
DI-n-butylphthatate
DI-n-octylphthatate
Dlbenzoahanthracene
flbenzofiiran
Dlethylphthalate
Dimethylphihalate
Pluoranthene
Fluorene
lexachtorobenzene
loxachlorobutadiene
Rexathlorocyclopentacjjene
Rexachiomethane
ndeno123-cdpyrene
sophorono
Z-NUrosodl-n-pmpyJamtne
N/-Nltrosodlphenylamlne
Nlaphthalene
llrobenzene
Pentachiomphent
mg/kg 1.9 0.16
mg/kg 0.74 0.039
mg/kg 0.37 0.043
mg/kg 0.37 0.040
mg/kg 0.37 0.032
mg/kg 0.37 0.018
mg/kg 0.37 0.023
mg/kg 0.37 0.062
mg/kg 0.37 0.017
mg/kg 0.37 0.028
mg/kg 0.37 0.037
mg/kg 0.37 0.032
mg/kg 0.37 0.023
mg/kg 0.37 0.025
mg/kg 0.37 0.026
mg/kg 0.37 0.022
mg/kg 0.37 0.019
mg/kg 0.37 0.036
mg/kg 0.37 0.039
mg/kg 0.37 0.038
mg/kg 0.37 0.038
mg/kg 0.37 0.033
mg/kg 0.37 0042
mg/kg 0.37 0.019
mg/kg 0.37 0.040
mg/kg 037 0.036
mg/kg 1.8 0.031
82706
327CC
82700
8270C
827CC
827CC
827CC
82706
82700
827CC
82700
B2706
82700
827CC
82700
8270C
82706
8270C
8270C
82700
827CC
827CC
82700
827CC
827CC
827CC
82706
This report should not be repnxfuced except In Its entirety without the sltten consent of Prism Laboiatmies Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1400/529-6364 Fax [phone]
NC CertifIcation No.402
SC Certification No 9812
NC Drinking Water CerL No 37735
Laboratory Report
08/10/07
Project ID Morehead Commons No Client Sample ID 8.-i
Prism Sample ID 188656
Sample Matrix Soil coc ou 00807064
Time Collected 08102/07 1015
Time Submitted 08/02/07 1325
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
LI mit Factor Date/lime ID
BR
BR
BRL
BR
BRL
BR
BRL
URL
BRL
BR
BR
BRL
BRL
BR
BRL
BRL
BR
ER
BR
BRL
BR
BRL
ORL
BR
BR
BR
BR
08101/CT 1307 kcampgotiu Q5t
08/07/07 1307 kcamplijofto Q25550
08/07/07 1307 kcampigotto 025550
08107/07 1307 kcamplgotto 025550
08/07/07 1301 kcamplutta 025550
08/07/07 1307 kcamptgulto 025550
08107/07 1307 kcamplgotlo 025550
08/07107 1307 koamplgotto 025550
08/07107 1307 kcamplgotk 025550
08/07/07 1307 kcamplgotto 025550
08/07/07 1307 kcamplgotto 025550
08/07/07 1307 kcamplgotto 025550
08107/07 1307 kcamplgotto Q25550
08/07/07 1307 kcamptgolta 025550
08/07/07 1307 koampigotto 026550
08/07/07 1307 koamplgotto 025550
08/07/07 1307 kcamplgotto 025550
08/07/01 1307 kcamptgotto 025550
08/07/07 1307 kcamptgotto 025550
08107/07 1307 kcampigotto 025550
08/07/01 1307 kcampfgofto 025550
08/07/07 1307 kcamplgoflo 025550
08/07/07 1307 kcaniplgotto 025550
08/07/07 1307 kcamptgolto 025550
08107/07 1307 Iccamplgotto 025550
08/07/07 1307 kcamplgotto 025560
08/07/07 1307 kcamplgotto 025550
Page 33 of 35
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID 168656
Sample Matrix SoU COG Group G0807064
Time Collected 08/02107 1015
Time SubmItted 08/02/07 1325
Sample Preparation
Sample Preparation
30g lmL 35506
10.Olg 2mL
08/04/07 900 pt3arr
EPH 08103107 700 pbarr
P19062
P19081
This report should not be repsoduced except In its entirety without the Written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O 8ox 240543-CharIotte NC 28224.0543
Phone [phone] Toll Free Number 1-808/529.6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
SP Associates PA
\ttn Chris Ward
Box 7030
Tharbtte NC 28241
Laboratory Report
08110/07
ii
arameter Result Units MDL MethodReport
Limit
0.37
0.37
0.37
Dilution
Factor
0.018
0.040
0.025
Analyst Batch
ID
821013
827013
827013
Analysis
DatelTime
08/07/07 1307 kcamplgotto
08/07/07 1307 kcampiotto
08/07/07 1307 kcamplolte
025550
025550
025550
Surrogate Recovery Control LimIts
Terphenyl-d14 76 41 136
Phenol-d5 70 13-95
Nltrobenzene-d5 72 14-103
2-Fkiomphenol 78 14-89
2-Fluomblphenyl 73 21 108
246-Tdbromaphenol 86 25-123
henanthrene BRL mg/kg
Thenol BRL mg/kg
yrene BRL mg/kg
xtractabIa PEtroleum Hydrocarbons by GC-FID
C11-C22AromaIfcs BRL mg/kg
Analysis Note for Cll-C22 romatics
C19-C36Aliphatics URL mg/kg
C9-Ci8 Mphatics BRL mg/kg
Metals by ICP
ChromIum
Lead
11 6.0
Adjusted value
11 1.7
11 3.6
MADEP EPH 08/08107 547 grappoccloll 025548
MADEP EPH 08/08/07 547
MADEP EPH 08/08/0 547
giappacclotl
grappacctot
025548
025548
Surrogate Recovery Control Limits
o-Terphenyt 73 40-140
2-Fluomblphenyl 81 40-140
2-Bromcnaphthalene 84 40-140
i-Chfom-octadecane 76 40-140
24 mg/kg 0.28 0.016 BQIOB 08/08/07 2044 mcampbell 025521
98 mg/kg 028 0.018 6010B 08/03/07 2044 mcampbell 025521
Page 34 of 35
ESP Associates PA
ttn Chris Ward
Box 7030
Tharlotte NC 28241
Laboratory Report
08110/07
Client Sample ID B-f
Prism Sample ID
COC Group
Time Collected
Time Submitted
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 1.98 50 mL 305DB 08/03/07 745 ddlxon P19078
Jolatile Petroleum Hydrocarbons by GC-PIDIFID
5-C8 Aliphatics BRL mg/kg 5.6 1.1 MADEP VPH 08/07/07 7.24 hwanrr 025565
Analysis Note for C5-C8 Aliphatics Adjusted value
9C10 Aromalics BRL mg/kg 5.6 0.034 MADEP VPH OBIO7R7 724 hwaener 025565
9-C12 Aliphallcs BRL mg/kg 5.6 1.7 MADEP VPH 08/07/07 724 hwagner Q25565
Analysis Note for C9-C12 Aliphatics Adjusted value.
Surrogate Recovery Control Limits
25-Dibromotolusne-PID 96 70-130
25-Dibmmototuene-FID 104 70-130
ampio WeIght Determination
Nelght 21.79 MADEP VPH 08/08/07 000 tbrown
Neight 20.04 MADEP VPH 08/08107 000 brcan
3ample Comments
3FtL Below Repelling Limit
Estimated value between the Reporting Limit and the MDL
The results In this report iIata only to the samples submitted for analysts and meet slate certilication requirements other thanVELACcerllficatlonexceptforThoseInstancesIndicatedInthecasenan-alive andlor test comments
41/results are reported on thy-weight basis
ngeia Overcash V.P Laboratoty Services
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbroopc Road.P.O Box 240543 Charlotte NC 28224-0543
ut AnaIdica3 m$imet.I 8uluIbn
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Project ID Morehead Commons No
Sample Matrix Soil
188656
G0B07064
08/02107 1015
08/02/07 1325
Phone[phone] Toll Free Number 1-800/529-6354 Fax [phone] Page 35 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte1 NC 28241
Level II QC Report
8110107
Project ID Morehead Commons No COC Group Number 130807064
Date/Time Submitted 8/2107 1325
Volatile Organic Cornnaunds by GC/MS method 8260B
Method J3Iank QO Ba/eli
Result RI on/mi Umit UnIts ID
1111-Tdchloroethana
11 22-Tetmchtcroethana
12-Trichtomethane
11-Dichloroethane
1-Dlchloroethene
11-Dichloropmpene
Z3-Tdchlorobenzene
23-Tdchlompropane
24-TrichIombenzene
24-lrhnethyibenzene
12-Qlbromoethane EDB
I2-Dlchlorobenzene
i2-Dichloroethane
112-Dichioropropane
1315-Trlmethylbenzene
113-Dithlorobenzene
113-Dlthioropropane
i4-Dlchtorobenzene
212-Dlchloropropane
2-Chiorotohiene
2-Ilexanone
4-Chiorotolueno
4-Methyl.2-pentanone MIBK
Acetone
Benzene
Brornobanzene
Bromochiorornethane
Bromodlchtoromethane
Bromoform
Bromomothane
Carbon tetrachioddB
Chtorobenzena
Chlorodlbrornomethane
Chioroulliane
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0026
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.05 0.025
ND 0.005 0.0025
ND 0.05 0.025
Nt 0.05 0.025
ND 0.003 0.0015
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.01 0.005
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.01 0.005
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/hg
mg/kg
mg/kg
Q25514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
Q25514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc440SprlngbrookRoad-P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] ToIl Free Number 1-800/529.6364 Fax [phone] Page 101
Level II QC Report
8/10107
SP Associates PA
Attn Chris Ward
Box 7030
Charlotte1 NC 28241
Project ID Morehead Commons No coc Group Number G0607064
Dateffime Submitted 812107 1325
Method Blank cc
Result RL CnloI Umft Unlie tO
Chloroform ND 0005 0.0026 mg/kg 025514
Chioromethano ND 0.005 0.0025 mg/kg 025514
dc-I 2-Dlchloroethene ND 0005 0.0025 mg/kg 025514
cls.13.Dlchloropropene ND 0.005 0.0025 mg/kg 025514
Dicidorodlfluoromethane ND 0.005 0.0025 mg/kg 025514
Ethytbenzene ND 0005 0.0025 mg/kg 025514
Isopropki ether IPE ND 0.005 0.0025 mglkg 025514
lsopmpyibenzene ND 0005 0.0025 mg/kg 025514
mp-Xylenes ND 0.01 0.005 mo/kg 025514
Methyl ethyl ketone MEK NI 0.1 0.05 mg/kg 025514
Methyl t.butyl ether MTBE ND 0.01 0.005 mo/kg 025514
Methylene chloride ND 0.005 0.0025 mg/kg 025514
n-Butylbenzone Nt 0.005 0.0025 mg/kg 025514
n-Propylbenzene ND 0.005 0.0025 mg/kg 025514
Naphthalene ND 0.01 0.005 mg/kg 025514
o-Xylene ND 0.005 0.0025 mg/kg 025514
p.Jsopropyltoluene ND 0.005 0.0025 mg/kg 025514
seoButytherizene ND 0.005 0.0025 mg/kg 025514
Styrene ND 0.005 0.0025 mg/kg 025514
tert-Butylbenzene ND 0.005 0.0025 mg/kg 025514
Tetmehioroethene ND 0.005 0.0025 mg/kg 025514
Toluene ND 0.005 0.0025 mg/kg 025514
trans-12-Dlchloinethene ND 0.005 0.0025 mg/kg 025514
trans-i3-Dlchloropropene Nt 0.005 0.0025 mg/kg 025514
Trichioroethens ND 0.005 0.0025 mg/kg 025514
Trichtorofluoromethare ND 0.005 0.0025 mg/kg 025514
Viny acetate ND 0.025 0.D125 mg/kg 025514
VInyl chloride ND 0.005 0.0025 mg/kg 025514
Laboratory Confrot Sample RJ3carwy
Result Spike AmaunL Unib .2 1D
111-Dlthloroethene 0051 19 0.05 mg/kg 102 57-122 Q25514
Berizene 0.044 0.05 mg/kg 86 62-119 Q25514
Chlorobenzene 0.0478 005 mg/kg 96 61-124 Q25514
Totuena 0.05135 0.05 mg/kg 103 57-122 025514
Triclitorcelheno 0.0605 0.05 mg/kg 121 59-129 028514
This report should not be reproduced1 except In Its entirety without the written consent of Prism Laboratories Ino449SprlngbrcokRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-5001523.6334 Fax [phone]
NC Certiflcalion No 402
SC Certification No 99012
NC Drinking Water Cork No 37735
Page of
Level II QC Report
8110/07
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte1 NC 28241
186652 ChromIum
Lead
Project ID Morehead Commons No COG Group Number 30807064
Date/Time Submitted 8/2/07 1325
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc449SpflngbrookRoadP.O Box 240543 Chaliotte NC 28224-0543
PhonB 7041529-6364 Toll Free Number 1400/529-6354 Fax [phone]
NC Certification No.402
SC Certification No 99012
NC Drinking Water Cert No 37735
Matrix Spike RBCOVS
1L1 Result SpfltaAsmunt Units ID
188597 11-Dichtoroethone 0.05093 0.05 mg/kg 102 44-140 025514
Benzena 0.04675 0.05 mg/kg 94 46-135 025514
Chlombenzene 0.04795 0.05 mg/kg 95 47-135 025514
Toluene 0.04701 0.05 mg/kg 94 47-136 Q25514
Trlchloroelherie 0.0499 0.05 mg/kg 100 45-141 025514
Matrix Spike Duplicate Rvey Recovwy RPD an usiri
rnpla in Result Spike Amount Unils
188597 11.-Dlchioroethene 0.04928 0.05 mg/kg 99 44-140 0-23 025514
Benzane 0.04467 0.05 mg/kg 89 46-136 0-22 025514
Chlorobeazene 0.04666 0.05 mg/kg 93 47-135 0-22 025514
Toluene 0.04496 0.05 mg/kg 90 47-I 36 0-22 025514
Trichloroethena 0.04651 0.05 mg/kg 93 45-141 -23 025514
Metals by ICP method 601i38
Method Blank OCBSI
Result RL Conlesi limit Unite ID
Chromium 0.0186 0.25 0.125 mg/hg 025521
Lead 00268 0.25 0.125 mg/kg 025521
Laboratory Control Sample pjy 0V5
Result Spike Minuet Units ID
Chromium 22.4199 25 mg/kg 90 80-120 025521
Lead 22.7376 25 mg/kg 91 80-120 025521
Matrix Splice Recovay RsCaVuSy QCBatth
Ssrnpk ILl Result Spike Amount Units ID
188652 ChromIum 31.0259 25380 mg/kg 46 75-125 025521
Lead 132.172 25.380 mg/kg 142 75-125 025521
Matrix Spike Duplicate Renuvary RaCCVmy RPD
phiD Result SpikoMiount Units
Ibi Rano 10
40.6402 24.630 mg/kg 87 75-125 27 0-20 025521
969916 24.630 mg/kg 75-125 31 //0-20 025521
Page of
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Level QC Report
8/10107
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 26241
Project ID Morehead Commons No COG Group Number G0807064
Daternme Submitted 8/2107 1325
This report should not be repmduced1 except In Its entirely without the written consent of Prism Laboratories Inc449Spdngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toli Free Number 14001529-6354 Fax [phone] Page of
FnUSeMcMssI$IeslAEiivfranmepW Lm1$
by -F1D AFrIlICUIMUivittijcr
Method Blank
Result RL Confrot Limit Unite II
C11-C22Aromatlcs ND 10 mg/kg Q25548
C19-C36Aliphatics ND 10 mg/kg Q25548
C9-C18 Mphatlcs MD 10 mg/kg Q25548
I..aboratory Control Sample Recovasy Recovac
Ranges QC Batch
Result Spike Amourt Unite
C11-C22Ammatlcs 140.38 170 mg/kg 83 40-140 Q25548
G19-C36AlIphatics 54.74 80 mg/kg 55 40.440 Q25548
C9-C18 Aliphatlce 30.28 60 mg/kg 50 40-140 025545
Matrix SpIke Recovey cc Batch
sampleio Result SplkoAmounl Units ID
188424 C11-C22AromaIics 131.86 170 mg/kg 75 40-140 Q25548
C19-C3SAIIphaUcs 69.66 80 mgllcg 87 40-140 Q25548
C9-C18 Aliphatics 37.14 60 mg/kg 62 40-140 Q25548
Matrix Spike Duplicate Recovery Recovery
Ranges RPD RangeSampleioResultSpikeAmountUnits
188424 Cl 1-022 Aromatlcs 124.02 170 mg/kg 73 40-140 0-50 Q25548
C19-C3SAIIphatlcs 51.52 80 mg/kg 64 40-140 30 0-50 Q25548
C9-C18 Aliphatics 28.66 60 mg/kg 48 40-140 26 -50 Q25548
.1
-I
ESP Associates PA
Attn Chris Ward
Hox 7030
Chartotte NC 28241
SemivolaIIIe Organic Compounds by GC/MS method B270C
Method Blank 00 Baldi
Rasut RI Can%n4 Iitr1I UnRs ID
l24-Tzichlorcbeiizene
112-Dicblorobanzeno
3-Dichlorobenzene
14-Dichlombenzene
Z45-ThchIorophenoI
246.Trlthlorophenol
24-DcMorophenoI
24-D1methyiphenoI
2.4Dinitiophenol
24-D1n1ttoluene
26-Dinlimtoluene
2-ChioRInaphthalene
2-Chioropheriol
2-Methyinaphthalena
2-Methyiphenol
2-Nitrophenol
34-Methyiphenol
33-Dlchiorobenzldine
4BDinhIro-2-methylphenol
4-Bromophen4phenylether
4-Chloro-3-methylphenol
4-Chioroanilirie
4-Chlorophonylphenylether
4.Nltrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzoaanthracene
Benzoapyrene
Oenzobfluoranhene
Benzogh.tperylcne
Uenzokliuoranthene
Benzolsacjd
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 1.55 0.825 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/hg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.155 mg/kg
ND 0.33 0.165 mg/kg
ND 0.66 0.33 mg/hg
ND 1.65 0.825 mg/kg
ND 0.33 0.165 mg/kg
ND 0.66 0.33 mg/kg
ND 0.33 0.165 mg/hg
ND 0.33 0.165 mg/kg
ND 1.65 0.825 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
NI 0.33 0.165 mg/kg
ND 165 0.825 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 1.65 0825 mg/kg
025550
025550
025550
025550
Q25550
025550
025550
025550
025550
025550
025550
Q25550
025550
025550
025550
025550
Q25550
025550
025550
025550
025550
025550
025550
025550
025550
025550
Q25550
025550
025550
025550
025550
025550
025550
025550
NC Cerilhication No 402
SC CorUScation No 99012
NC Drinking Water Cert No 37735
Level II QC Report
8/10/07
Project ID Morehead Commons No COG Group Number 30807064
Date/TIme Submitted 8/2/07 1325
This report should not be reproduced except In Its entirety without the written cansent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone[phone] Toll Free Number l-800529.6364 Fax [phone] Page of
ESP Associates PA
Atta Chris Ward
O.Box7030
Charlotte NC 28241
NC CertificatIon No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
8/10/07
Project ID Morehead Commons No CCC Group Number G0807064
Date/Time SubmItted 8/2107 1325
Method Blank
Hesuft RL Conm Llmt Unus
Henzyl alcohol ND 0.65 0.33 mg/kg 025550
Bf52-chtoroethoxymethane ND 0.33 0.165 mg/kg 025550
Bls2-chtoroethylether ND 0.33 0.155 mg/kg 025550
BIs2-chlorclsopropylether ND 0.33 0.165 mg/hg 025550
Bls2.ethythexylphthalate ND 0.33 0.165 mg/kg 025550
Butythenzylphthalate ND 033 0.165 mg/kg 025550
Chrysene ND 0.33 0.165 mg/kg 025550
DI-n.butytphthalate ND 0.33 0165 mg/kg 025550
Di-n.octylphthalate ND 0.33 0.165 mg/kg 025550
Dthenzoahanthracene ND 0.33 0.165 mg/kg 025550
Dtherizofuran ND 0.33 0.165 mg/kg 025550
Diethylphthalate ND 0.33 0.165 mg/kg 025550
Dtmethylphthalate ND 0.33 0.165 mg/kg 025550
Fluoranthene ND 0.33 0.165 mg/kg 025550
Fluorerie ND 0.33 0.165 mg/kg 025550
Hexachlorobenzene ND 0.33 0.165 mg/kg 025550
Hexachlorobutadilene ND 033 0.165 mg/kg 025550
Hexachlorocyctopenfadlene ND 033 0.165 mg/kg Q25550
Hexachloroelhane ND 0.33 0.165 mg/kg 025550
Indeno123-cdpyrene ND 0.33 0.165 mg/kg 025550
Isophorone ND 0.33 0.165 mg/kg 025550
N-NsodI.n-propylamne ND 0.33 0.165 mg/kg Q25550
NNltrosodlphenytanijne ND 0.33 0.165 mg/kg Q2555D
Naphthatene ND 0.33 0.165 mg/kg 025550
Njtmbenzene NI 0.33 0.165 mg/kg 025550
Pentashlorophenol ND 1.65 0.825 mg/kg 025550
Phenonthrege ND 0.33 0.165 mg/kg Q25550
Phenol ND 0.33 0.165 mg/kg 025550
Pyrene ND 033 0.165 mg/kg 025550
Laboratory Control Sample Rocovesy
Resuft SpkeAmount Units If
lZ4-Trichlorobenzene 1308.84 1669.7 mg/kg 73 39.98 025550
14-Dlctitorobgnzene 1239.73 1669.7 mg/kg 74 37..95 025550
24-Dinltmtclueng 1505.17 1659.7 mg/kg 90 56-128 025550
2-Chtorophenol 1236.39 1669.7 mg/kg 74 37-98 025530
4-Chloro-3-rnethylpherrnl 1440.40 1669.7 mg/kg 86 45.411 025550
ThIs report should riot be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone]TollFreeNumber1-5001529-0334 Fax [phone] Page of
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
MEcamaISoIitIcn
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be repioduced except In Its entirety without the wiitten consent of Prism Laboratories Inc449SprlngbrooicRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529.6354 Fax [phone]
Level II QC Report
8110/07
Project ID Morehead Commons No COG Group Number 00807064
Date/Time Submitted 8/2/07 1325
Laboratory Control Sample Recovery Badi
ResUlt Spike Mount Units
Nltrophenol 1206.34 1669.7 mg/kg 72 20-157 025550
Acenaphthena 1351.25 1669.7 mg/kg 81 44-110 Q25550
N-Nltrosodl-n-propylamlne 1246.41 1669.7 mg/kg 75 38-101 025550
Pentachlorophenol 1687.14 1669.7 mg/kg 101 53-127 Q25550
Phenol 1279.13 1669.7 mglkg 77 34-102 025550
Pyrene 1379.96 1669.7 mg/kg 83 54-131 025550
Matrix Spike Recey QO Baldi
Sample Result Spike /4flW4fll Unite ID
188424 1124-Trjchlorobenzeno 1171.66 1667 mg/kg 71J 26-97 025550
14-Dichlorobenzene 1110.33 1667 mg/kg 67 23-92 025550
24-Dlnltmtoluene 1409.66 1661 mg/kg 85 45-127 025550
2-Chlorophenci 114966 1687 mg/kg 69 25-94 025550
4-Chloro-3-methylphenol 1299.33 1667 mg/kg 78 31-1 13 Q25550
4-Nltrophenci 1172.66 1667 mg/kg 70 17-150 025550
Acenaphthene 1238.33 1667 mg/kg 74 36-107 Q25550
N-Nitrosodl-n-propylamlne 1121 1667 mg/kg 67 22-105 025550
Pentachlorophenol 178966 1667 mg/kg 107 39-137 025550
Phenol 111933 1667 mg/kg 67 23-97 026550
Pyrene 1603.66 1667 mg/hg 98 45-133 025550
Matrix Spike Duplicate Recovery RPD Range C20551th
Sample ID Result Spike Amount outs ranges ID
188424 124-Trlchlorobenzene 103233 1667 mg/kg 62 26.91 13 0-37 025550
14-Dlchlorobenzene 1017 1667 mg/kg 61 23-92 0-36 Q25550
24-Olnhtmtoluene 1453.33 1667 mg/kg 87 45-127 0-29 025550
2-Chlorophenol 1098.33 1667 mg/hg 68 25.94 -37 025550
4-Chlora-3-methylphonol 1268 1687 mg/kg 76 31.-I 13 0-32 Q2555C
4-Nltrophenol 1219.66 1657 mg/kg 73 17-150 0-32 025560
Acenaphthene 1221.33 1667 mg/kg 73 36.417 0-32 025550
N-Nltrosodl.n.propylamjne 1081.66 1657 mg/kg 65 22-105 -37 025550
Penlachiomphenol 1709.66 1667 mg/kg 103 39-137 0-27 025550
Phenol 1062 1667 mg/kg 64 23.97 0-42 025550
Pyreno 1440 1651 mg/kg 88 45-133 11 0-27 025550
Page 7018
188652 CS-CS AJiphalics
cs-cio Ammatics
C9-C12 Aliphatics
-See Case Narrative
This report should not be reproduced except In Its entirety without the written consent of Prism laboratories Inc449SprlngbrookRoadP.O Box 240543 CharIo1te NC 28224-0543Phone[phone] Toll Free Nunibem 1-800529-5394 Fax [phone] Page of
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
8/10/07
ESP Associates PA Project ID Mcrehead Commons No COG Group Number G0807064
Atm Chris Ward Daterflme Submitted 8/2107
Box 7030
Chariolte NC 28241
vnkut1r DAh-.Insin Mssr1rnrn4rnn GC-PIDIPID mthnd MADP VPH
1325
Method Blank QCBa1thRtRLConimi Umit Units ID
C5-C8.4ilphatlcs ND 2.5 mg/hg Q25565
C9-C10 Aromatics ND 2.5 mg/kg 25565
C6-C12 Atiphatics ND 2.5 mg/kg Q25565
Laboratoiy Control Sample P.ecovey
Result SplkaAniount Units
C5-C8Allphatlcs 17165 18 mg/kg 114 70.130 026565
C9-C10 Aromatics 4.924 mg/hg 98 70-130 025565
C9-Cl2AIiphaflcs 10.981 10 mo/kg 110 70-130 025565
Matrix Spike Rs Recoveiy
Result SplkeMicunt Unils
188652 CS-CR Allphatlcs 17.575 15 mg/kg 117 70-130 Q25565
C9-CiD Aromatics 5.116 mg/kg 102 70.130 Q25565
C9-ClZAliphatics 21.085 10 mg/kg 211 70-130 Q25565
Matrix Spike Duplicate Revovnsy Rvsry
SeinplalD Result SpllraMount Units ID
18.442 15 mg/kg 123 70-130 0-25 Q25565
5.259 mg/kg 105 70-130 0-25 025565
22.641 10 mg/kg 226 70-130 0-25 Q25565
RA1-ornesrnc
FuilSeMoMel1Icai Environmental Solutions
449 $prlngbrook Road P.O Box 240543 Charloflo1 NC 25224-0543
Phone [phone] Fax 7041
Client Company Name _5 /o
Report To/Contact Name .4he
Reporting Address ______________________________
Phone Fax Yes No_
Email Yes No Email Address_____________________EDD Type PDF_ExceL....Othe
P1 ..i
PAaE4_._orj__QUOTE TO ENSU P54 FR BILLING
Project Name jq1L-J
Short Hold Analysis Yes No UST Proeot Yes No
please ATTACH any project specific reportIri QO LEVEL ii III IV
provisions and/or QO Require5ds
Invoice To
Samplers Signature /d Sampled By Print Name AWiliation_tiP
RelinquIshad By Sigriaturo Received By S1natUre3
Relinquished By
Muihou 01 OniprnonU NErLI BA OOL.BRS SHOULD SE TAPED SHUT WIT4 CUSTODY SEALS FOR TRANSPORTAnON
TO ThE LABORATORY
EAMpI5 ARE NOTAGOEPTED AND VERIFIED AGAINS iCUN11L RECEIVED ATTHE LABORATORY
Ci Fed Es ClUes nml.dIvarsd Ci Pdsm Field ServIce Other
CO Group No
44
NPDES Ur GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OThER
ONO CiSCiNC 050 ONC CiSC ONC CiSC ONC DSC ONC CiSC ONC CISC ONC CISC CINC
CiSC
CONTAINER TYPE CODES Amber Clear Glass Plastic TL Tenon-LIned Cap VOA Volatile Organics Analysis Zero Head Space
CHAIN OF CUSTODY RECORD
Sta Location Name
Site Location PhysIo
jr-.4I1.-4-I4 Jhra4
purchase Order No./Rilling Reference 1J 00
Requested Due Date 01 Day 02 Days 03 Days 04 Days It Days
WorkIng Days 06-9 Days Standard 10 days U5I Be
Samples received altor 15OO Will be procassod
next business day
Turnaround time Is based on
busIness days excluding weekends and holidays
BEE REVERSE FQRERMS CONDITIONS REGARDINS SERVICES
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CUSTDD SEALS INTACT
VOLATILES rocd W/OJT I-IEADSPACE
PROPER CQWIAINERS used
To BE IILLED IN BY GUENT/SAMPUNG PERSONNEL
Certification NELAQ..JJSACE_FL NGL..
SC OTHER
__N/A _____
Water Chlorinated YES......NO_
Sample Iced Upon Collection YES ________
CUENT
SAMPLE DESCRIPTION
DAIS
COLLECTED
TIME
COLLECTED
MiLITARY
MATRIX
SOIL
WATER OR
SAMPLE CONTAINER PRESERVA-
flVES
/0 4/çj//AY 7/REMARKSJ-ID NO
SEE BELOW NO SIZEt_____J_--I4
HeiunqvEflDtl uy iuignaursj ecsivea ay lolenaluw
Upon rellnqulshhig this Ctin of Custoy is your authorization for Prism to proceed with the onalyseSis requested above Ai
submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been
Initialized
changes must be
Ode Additional Comments
PRtSM USE ONLY
Arrival Time
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SEE REVEFISE FORTERMSCONDITIONS
OB%G1NA1
VA
pflr AUG 13 2007
Case NarrativePRISM
LABDRATORIESINC
Date 08/09/07 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COG Group No G0807065
Contact Chris Ward Collection Dates 08/02107
Address Box 7030 Lab Submittal Dates 08/02/07
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and Quality
Control Data totaling pages chain-of-custody is also attached for the samples submitted to Prism for this projecL
Data qualifiers are flagged individually on each sample key
reference for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are Included In the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
No Anomalies Reported
Metals Analysis
N/A
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by Paula Gilleland Project Manager qela Overcash
Signature auQa..Jt-QuD_Signature 344 OvJAc-L
Review Date 080907 Approval Date 08/09/07
Data Qualifiers Key Reference
Compound also detected In the method blank
ResUlt outside of the QC limits
DO Compound diluted out
Estimated concentration calIbration range exceeded
The analyte was positively Identified but the value Is estimated below the reporting limit
Estimated concentration with hIgh bIas
Estimated concentration with low bias
matrtx effect is presenL
Notes This report should not be reproduced except
in its entirety without the writtten consent of Prism Laboratories Inc The results In this
report relate only to the samples submitted for analysis
449 Sprtngbrook Road P.O Box 240543 Chadotte NC 28224-0403
Phone [phone] ToO Free 800/529-6364 Fax [phone]
SP Associates PA
Un Chris Ward
Box 7030
harlotte NC 28241
lA/lB COMPOSITE
188657
00807065
08/02/07 1030
08/02/07 1325
ercent Solids Determination
ercent Solids
lesel Range Organlcs DR0 by GC-FID
lesel Range Organics DRO
Sample Preparation
asoline Range Organics GROI by GC-FID
asoline Range Organlcs GRO 6.9
Surrogate Recovery Control Limits
Toluene-d8 99 81 128
Dibromofluoromethane 109 67-143
Bromofiuorobenzene 105 77 128
710 mg/kg 200 4.9 80156 08/07107 2314 ivogel 025614
25.OBg mL 3545 08106/07 1650 wconder P19099
Surrogate Recovery Control Limits
o-Terphenyl 49 124
mg/kg 6.7 3.6 50 6015B 08/08107 030 hwagner 025589
Surrogate
aaa-TFT
Recovery
90
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Control Urnits
55-129
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
08/09/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
ammeter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
89.2 5M2540 08/03/07 1555 ddfxon
olatile Organic Comeounds by GCIMS
enzene BRL pg/kg 3.3 0.44 82606 06/08/07 2202 Iwitry 025514
thylbenzene BRL pg/kg 5.5 0.38 82606 08/08/07 2202 lwitry 025514
p-Xylenes 4.3 pg/kg 11 0.77 82606 08108/07 2202 Iwltry 025514
Xylene 3.7 pg/kg 5.5 0.33 82606 08/08/07 2202 IwiIJy 025514
otuene BRL pglkg 5.5 0.37 82606 08/08/07 2202 Iwitsy 025514
Pagel of2
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
08109107
SP Associates PA
ttn Chris Ward
.O.Box 7030
harfolle NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
IA/lB COMPOSITE
188657
G0807065
08/02/07 1030
08/02/07 1325
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
ample Comments
RL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
he msuits In this report relate only to the samples submitted for analysis and meet state certification requirements other than
ELAC certification except for those instances
indicated In the case narrative and/or test comments
II results are reported on dry-weight basis
ngela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
It SatvksAulydcat EiwIrnmntI Itc1utJon
Phone [phone]M Toil Free Number 1-8001529-6364 Fax [phone] Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehoad Commons No
Level II QC Report
8/9/07
COC Group Number G0807065
Daternme Submitted 8/2/07 1325
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlolte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
bv 8260B.PIMflI In Jtfl11 IJJIJII.I --.JIWI%St fln.tIItnJ
Method Blank 00 Batch
Result RI Control Limit Units ID
Benzerie ND 0.003 0.0015 mg/kg 025514
Ethylbenzene ND 0.005 0.0025 mg/kg 025514
mp-Xylenes ND 0.01 0.005 mg/kg 025514
o-Xyiene ND 0.005 0.0025 mg/kg Q25514
Toluene ND 0.005 0.0025 mg/kg 025514
Laboratory Control Sample Recovgxy Recovery
Pines OC Batch
IDResultSpikeAmountUnits
Benzene 0.044 0.05 mg/kg 88 62-119 025514
Ethylbenzene 0.04939 0.05 mg/kg 99 57-128 025514
mp-Xylenes 0.09958 0.1 mg/kg 100 54-132 025514
o-Xytene 0.04956 0.05 mg/kg 99 57-131 025514
Toluene 0.051 35 0.05 mg/kg 103 57-122 025514
Matrix Spike Recovery Recovery
Ranges QCBaICI1
sampia ID Result Spike Amount Units ID
188597 Benzene 0.04675 0.05 mg/kg 94 46-136 Q25514
Ethyibanzene 0.05109 0.05 mg/kg 102 51-135 025514
mp-Xylenes 0.10369 0.1 mg/kg 104 51-136 025514
o-Xylene 0.051 62 0.05 mg/kg 103 49-137 025514
Toluerie 0.04701 0.05 mg/kg 94 47-136 025514
Matrix Spike Duplicate Recov Recovery RPD
Ranges RPD Range 00 Batch
Sample Result Spike Amount Units
188597 Beozene 0.04467 0.05 mg/kg 89 46-136 0-22 025514
Ethylbenzene 0.04982 0.05 mg/kg 100 51-1 35 0-23 025514
mp-Xylenes 0.09579 0.1 mg/kg 96 51-136 0-20 025514
o-Xyiene 0.05082 0.05 mg/kg 102 49-137 0-22 025514
Toluene 0.04496 0.05 mg/kg 90 47-1 36 0-22 025514
Page of
Rifi Sov AnstyUcal Envlmemgntal Soielipns
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level QC Report
8/9/07
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No COC Group Number 30807065
Date/Time Submitted 8/2/07 1325
D.........i..aflt htr .PIfl ......I.aaatJl.c SSOhI%.ffl It4fllfl %IStfl IIPCIIJUU PU .2tJ
Method Blank OC Batch
Result RI Conlrci Umit Units ID
Gasoline Range Organics ND 0.5 mg/kg 025589CR0
Laboratory Control Sample Recovery Recovery ac atclRangesResultSpikeAmountUnitsID
Gasoline Range Organlcs 2.050 mg/kg 103 64-124 Q25589GRO
Matrix Spike Recovery Recovery QC BatchRanges
Sample Result Spike Amount Units 1k ID
188906 Gasoline Range Organics 1.948 mg/kg 97 37-1 26 025589GRO
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range QC Batch
Sample ID Result Spike Amount Units ii
188906 Gasoline Range Organics 2.075 mg/kg 104 37-126 0-34 025589CR0
Diesel Range Orcianics IDRO by CC-AD method 801 SB
Method Blank
QCBaIch
Result Rt Control Umtr Units ID
Diesel Range Organics DRO ND 35 mg/kg 025614
Laboratory Control Sample Recovery overy
Ranges QC Batch
IDResultSpikeAmountUnits1k
Diesel Range Organics DRO 85.1 80 mg/kg 106 55-109 025614
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample ID Result Spike Amount Units 1k 3D
188240 DIesel Range Orgartlcs DRO 72.9 80 mg/kg 91 50-117 025614
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPI Range OC Batch
Sempie ID Result Spike Amount Units 1k ID
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Chai1otte NC 28224-0543
Phone[phone] Toll Free Number 1-8001529-5364 Fax [phone]
188240 Diesel Range Organlcs DRO 68.1
-See Case Narrative
80 mg/kg 85 50-117 0-24 025614
Page of
Full Service Malytlcai Environmental Solutions
440 Springbrook Road P.O Box 240543 Charlotte1 NC 28224-0543
Phone [phone] Fax [phone]
Client Company Name _________________________
Report To/Contact Name lilt
Reporting Address _______________________________
Phone _______________Fax Yes No
Email Yes No Email Address______________________
EDI Type PDF_Excel Othpr
Site Location Name ____________________________
I1MII UI UIJT I1%Ul1U
PAGE...L OFJ....QUOTE TO PROPER BIWNG
Project Name -k
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reporting QC LEVEL 111111 lv
provisions and/ar QC Re9i.iyemen
invoice To JLH
Addres
Purchase Order NoJBiIllng Refere 1IiLi OO
Requested Due Date ci Day 02 Days 03 Days 04 Days Days
WorkIng Days ci 6-9 Days El Standard 10 days u3h Work MdU5t Be
Samples received after 1600 will be processed next business day
Turnaround time Is based on buslnes5 days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIENT
.....L
PRCPR CONTA ESUaad L___L
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_LJSACE._.._FL____NCj2
SC_OTHER ______N/A _____
Water Chlorinated YES_NO
Sample Iced Upon Collection YES
Samplers Signature Sampled By Print Name e-Affiliation
Upon relInquishing this am of Oust is your authorization for Prismto proceed with the analy es as requested
above Any changes must be
submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been Initialized
iieiinqutsnea by bfl51UD Fecovs5 by Signature Dale MlIitatyMOL$tS
Relinquished Dy Stgnature Received By 5irwlure Darn
ReIlnquJ5hed By Signature flec For Pile boralorles By-__
MeWed of Shipment .fi.ltSxMF GaOI.ERS SHOULD SE TAPED SHU1WITI1CUsTODY SEALS FOR TRANSPORTA11ON ThE LAe0RATDHY
SArPLES ARE NOT ACCEPTED AND VERIFIED AGAINST Q9UNTIL RECEIVED AT THE LABORATORY
Fed Ex UPS lfand.dsllvere$Pilem Fleki Seivice Other
eli
mup No
leId.ieci Fee
Site Location Physical Address
MiwtIMTTnnarreIir/f
SAMPLE DESCRIPTION
CLIENT
COLLECTEDDATE
TIME
MILITARY
COLLECTED
HOURS
MATRIX
WATER OR
SOIL
SLUDGE
SAMPLE CONTAINER
TIVES
PRESERVA-
ANALYSES REQUESTED
////REMARKS LAB
PRISM
ID NOTYPE
SEE BELOW NO SIZE
/_31/12
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Additional Comments
NPDES GROUNDWATER DRiNKiNG WATER SOLID WASTE RCRA CERCLA LANDFILL OTHER
NC SCC SC NC SC NC El SC NC USC NC SC NC El SC NC SC NC SC___io ____________________________ci ___
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SEE REVERSE FORTERMSCONDITIONS
ORIGINAL
APPENDIX
NON-HAZARDOUS WASTE MANIFESTS
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flJGINAI.RTURNTO GENERATOR
...... .....7ff .-ES Associates
Corporate Office
MailingP0Box 7030
Charlotte North carolina 28241
Phswa
3475 LalemontI3ailevaid
Fort Mill SC 29708
8038022440
Raleigh Wibnznglon Concord14001ViestonParkway2120-B Capital Dnve 4601 Corporate Drive NWSuite100WilmingtonNorthCarolina28405Suite165CaryNorth Carolina 27513 910 313 6648 Concord North Carolina 28027
704 793 9855
800 960 7317
PPU e4pussocufes con