Item No 35 - NFA Letter - Indcident No 36355 Morehead Common-OCR

NCDENR
North Caroina Department of Environment and Naturat Resources
Michael Easley Governor
Division of Waste ManagementWilliamRossJiSecretaryUndergroundStorageTankSection Dexter Matthews Director
August 27 2007
Beazer Homes
1300 South Boulevard Suite
Charlotte North Carolina 28203
Attention Jade Eastridge
Re Notice of No Further Action
5A NCAC 2L JJ407d
Risk-based Assessment and Corrective Action
for Petroleum Underground Storage Tanks
Morehead Common Area
1018 Post Street
Mecklenburg County
hicident Number 36355
Risk Classification Low
Dear Mr Eastridge
The Thitial Abatement Action report received by the Underground Storage Tank UST Section
Mooresville Regional Office on August 21 2007 has been reviewed The review indicates that after tank
closure and soil excavation soil contamination does not exceed the lower of the soil-to-groundwater or
residential maximum soil contaminant concentrations MSCCs established in Title 5A NCAC 2L
.04 II
The UST Section determines that no further action is warranted for this incident This
determination shall apply unless the UST Section later finds that the discharge or release poses an
unacceptable risk or potentially unacceptable risk to human health or the environment Pursuant to Title5ANCAC2LM407ayouhavecontinuing obligation
to notify the Department of any changes
that
might affect the risk or land use classifications that have been assigned
This No Further Action determination applies only to the subject incident
for any other incidents
at the subject site the responsible party must continue to address contamination as required
If you have any questions regarding this notice please contact me at 704 235-2172
Sincerely
Hydrogeologist
Mooresville Regional Office
PddiæDf
11.A
INI HAL ASSESSMENT REPORTMOREHEAJCOMMONSITEAREA
1018 POST STREET
CHARLOTTE NORTH 2AROLLNA
INCIDENT NO NOT YET ASSIGNED
ESI PROJECT NO E6-UD42.60.l
Prepared For
NCDENR
UST Section MRO
919 North Main Street
Mooresvillc North Carolina 28115
Prepared By
ESP Associates P.A
P.O Box 7030
Charlotte North Carolina 28241
August 20 2007
ESP Assodates PA August 20 2007
NCDENR
UST Section
Mooresville Regional Office
919 North Main Street
Mooresville North Carolina 28115
Attention Mr Allen Schiff
Reference INITIAL ASSESSMENT REPORT
Morehead Common Site Area
1018 Post Street
Charlotte Meclclenburg County North Carolina
UST Incident No Not Yet Assigned
ESP Project No E6-UD42.601
Dear Mr Schiff
On behalf of the property owner Beazer Homes ESP Associates P.A is pleased to provide the
attached Initial Assessment Report for the closure of the subject propertys petroleum releaseESPrespectivelyrequestsclassificationofthereleaseasLowRiskandissuanceofnofurther
action notice
Thank you for your attention in this matter If you should have any questions please do not
hesitate to contact me at 803 835-0915
Sincerely
ESP Associates P.A
Rog Christop Ward PG
Staff Scientist Environmental Services ManagerNCLicenseNo1600
cc Mr Jade Eastridge Beazer Homes
P.O Box 7030 Charlotte NC 28241
1.800.960.7317 NC 704.583.4949 rax 704.583.4950 SC 803.802.2440 fax [phone]
Www.espassudates.com
Initial Assessment Report
SITE INFORMAI1ON
Site Identification
Date of Report August 20 2007
IJ Facility ID N/A
fl Incident Number Not Yet Assigned
Site Rank Unknown
ri Site Name Morehead Common Site Area
Site Street Address 1018 Post Street
ri City/County/Zip Code Charlotte Mecklenburg County 28278
Description of Geographical Data Point Approximate center of former vault
Location Method Mecklenburg County
Polaris GIS Map
Latitude 352271
Longitude -80.8600
Information about Contacts Associated with the Release
AST Owner Beazer Homes
1300 Blvd Suite Charlotte NC 28203-4265
704.370.7200
AST Operator N/A
Property Owner Same as above
Property Occupant Same as above
Consultant/Contractor ESP Associates P.A Chris Ward PG
PG Box 7030 Charlotte NC 28241
803.835.0915
Analytical Laboratory Prism Laboratories Inc
P0 Box 240543 Charlotte NC 28224-0403
704.529.6364
NC Certification No 402
Information about Release
Date Discovered May 17 2007
Estimated Quantity of Release Unknown
Cause of Release Unknown
ri Source of Release Below ground septic system-type concrete vault
Size and contents of AST or
other containment from which the release occurred NA
Ward Professional Geologist for ESP Associates P.A do certi that thecontainedinthisreportiscorrectandaccuratetothe best of my knowledge
PA is licensed to practice both geology and engineering in North Carolina
certification numbers are Geology C-347 and Engineering C-0587
In lila Assessment Report ESP Project E6-UD42.601
Morehead Conimon Site Area August 20 2007
INTRODUCTION
The undeveloped subject site is located on the north side of Post Street approximately 400 feet
west of its intersection with South Clarkson Street on Tax Parcel No 07325213 in Charlotte
Mecklenburg County North Carolina see Figures and The site had an address of 1018
Post Street and was reportedly once occupied by Ohio Chemical Surgical Equipment but has
been vacant since 1965 The area of the subject release associated with an unearthed septic
tank-type concrete vault has been designated by ESP as Area of the Morehead Common Site
SITE HISTORY AND CHARACTERIZATION
On May 17 2007
ESP responded on behalf of Bearer Homes to an encounter with potentially
impacted soil during mass grading operations
at the subject site Upon arrival at the site ESP
observed soils with slight petroleum odor located beneath an unearthed septic tank-type
concrete vault which had just been excavated by the sites grading contractor As required
following receipt of laboratory results confirming release had occurred ESP emailed
notification of the release discovery to Mr Steve Bograd of the Mooresville Regional Office of
NCDENR on May 30 2007
Release Location
The subject site is located within an urban area of Charlotte which historically included
warehouse and retail structures.The site is currently mass graded and being developed as
mixed-use residential/commercial development see Figures and Based on our review of
the Geologic Map of North Carolina 1985 the subject site is located within the Charlotte Belt
locally comprised of intrusive metamorphosed granitic rocks locally pinkish gray massive to
weakly foliated and containing hornblende Soils encountered in this area are the residual
product of chemical weathering of rock presently underlying the site Soil weathering is more
advanced near the surface grading with depth to less weathered rock and finally bedrock
Initial Assessment Report ESP Project E6-UD42 601
More/iced common Site Area August 20 2007
AST Information
septic system-type concrete vault measuring approximately
ft ft ft deep was
uncovered and unearthed during mass grading operations at the subject site by Gelder Thompson
of Midland North Carolina The roof of the vault had been covered with boards and layer of
soil Piping protruded into the vault at two points but the piping ended within feet outside of the
vault See site photographs in Appendix
Previous Reporting
As required ESP submitted 24-Hour Release Notification by email to the Mooresville
Regional Office of NCDENR on May 30 2007 see Appendix Additionally ESP prepared
20-Day Report which was submitted to the Mooresville Regional Office of NCDENR on July
18 2007
Waste Characterization Sampling
On May 17 2007 using backhoe ESP collected waste characterization soil sample SF-i
from immediately below the recently excavated concrete vault at depth of approximately feet
below land surface BLS representative portion of the soil sample was screened in the field
with an organic vapor analyzer OVA and recorded reading of 10 ppm Soil sample SP-1 was
submitted to Prism Laboratories of Charlotte North Carolina for analysis of total petroleum
hydrocarbons TPH for diesel range organics DRO and gasoline range organics GRO oil
grease OG by EPA Method 9071A volatile organic compounds VOCs by EPA Method
8260B pesticides by EPA Method 8081A PCBs by EPA Method 8082 and for total lead and
chromium by EPA Method 60 lOB Waste characterization soil sample SF-I was collected and
analyzed to document that release had occurred and to characterize contaminant types and
concentrations to aid in the assessment and subsequent off-site permitted disposal/treatment of
impacted soils
InitialAssessrnent Report 51 Project E6-JD42 601
Murehead Common Site Area August 20 2007
As revealed by the laboratory data report for SP-l TPH.-liRO was reported at concentration of
420 mg/Kg OG at 3400 mg/Kg chromium at 22 mg/Kg lead at 51 mg/Kg and the PCB-1260
at 5.1 mg/Kg Results for all remaining analytes were reported to be below reporting limits
BRLs Analytical results for SP-l are summarized on Table B-i See Figure for soil
sample location map See the attached Prism laboratory data report in Appendix
iNITIAL ABATEMENT ACTIVITIES
Soil Excavation and Stockpile Sampling
Following excavation and removal of the concrete vault and the May 17 collection of waste
characterization sample SP-1 approximately two feet of structural fill was placed over the
former vault excavation and surrounding area by the sites grading contractor as part of the sites
mass grading On June 2007 ESP observed the removal of the recently placed non-impacted
structurally placed fill from the concrete vault area until residual soils where encountered ESP
then documented the excavation of 86.25 tons of impacted soils from Area by the sites
grading contractor The excavation was advanced based on OVA readings and evidence of
visible staining The resulting excavation including the non-impacted structural fill measured
approximately 30 ft 50 ft 10 ft deep Neither groundwater bedrock nor free product were
encountered within the tank pit
Non-impacted structure fill was placed to the side while excavated impacted soil was placed on
and covered with plastic awaiting subsequent off-site permitted disposal On June 2007 ESP
collected two composite soil samples from the impacted soil stockpile for laboratory analysis
The soil samples designated and were placed in laboratory provided containers labeled
and hand delivered on ice to Prism Laboratories for compositing and subsequent analysis The
samples were analyzed for TPH-GROIDRO BTEX by EPA Method 8260B TCLP-metals and
TCLP-Total Organic Halides TOX Results of the laboratory analysis summarized on Table
Initial Assessrn en Report ESP Project E6-UD42.601
Morehead Common Site Area August 20 2007
B-2 revealed elevated TPH-DRO and TCLP-TOX concentrations All other analyzed
constituents were BRL
Due to elevated TCLP-TOX results subsequent composite soil sample lab was collected
from the stockpiled soil on July 18 2007 and analyzed for VOC by EPA Method 8260B and for
semi-volatile organic compounds SVOCs by EPA Method 8270C Results of the laboratory
analysis as summarized on Table B-2 revealed elevated concentrations of various SVOCs while
VOCs were all reported to be BRL
On July 31 2007 86.25 tons of previously stockpiled soil from the Area excavation was
transported to the CMS Landfill in Concord North Carolina for permitted disposal see non-
hazardous waste manifest in Appendix
Confirmatory Sampling
On June 2007 following excavation of the vault area Area confirmatory soil samples were
collected at depth of feet BLS from each of the excavations four sidewalls WS-through
WS-4 while one soil sample was collected at depth of 10 feet BLS from the base of the
excavation B-i The five soil samples were hand delivered on ice to Prism Laboratories to be
analyzed for VOCs by EPA Method 8260B SVOCs by EPA Method 8270C pesticides by EPA
Method 8081A PCBs by EPA Method 8082 YPH/EPH by the Massachusetts Department of
Environmental Protection MADEP Method and for total lead and chromium by EPA Method
60 lOB Sample locations and excavation dimensions are depicted on Figure Soil Sample
Location Map Sampling was performed in general accordance with ESPs SOP see
Appendix
Results of the laboratory analysis
of confirmatory soil samples WS-l through WS-4 and B-i
revealed that all analyzed constituents were BRL with the exception of acetone conmion
laboratory contaminant in WS-2 and total lead and chromium is all samples however all
InitialAssessment Report ESP Project E6-UD42 601
Morehead Common Site Area Auguist 20 2007
analyzed constituents were reported to be below their soil-to-groundwater MSCC Laboratory
analytical results for the confirmatory soil samples are summarized on Table B-i The Prism
laboratory data reports are included as Appendix
1500-RADIUS RECEPTOR SURVEY
On July 20 2007
Mr Eddie Rogers of ESP performed receptor survey
to document the
presence or absence of active and/or inactive water supply wells within 1500-foot radius of the
subject release see Figure Receptor Survey Map The receptor survey included interviews
with available site occupants and visual observations for water supply wells and/or municipal
water meters All properties within 500 feet of the site were visited to determine well status
The area within 1000 feet of the subject release consists of commercial and industrial
development with numerous vacant structures No active or inactive water supply wells were
identified within 1000-foot radius of the subject release Municipal water and sewer have
historically been available within the area of the site Additionally no surface water bodies were
idenlifiediwithin 500 feet ofthe release see Figures and
In itial Assessment Report ESP Project E6-UD42.601
Morehead common Site Area August20 2007
however all analyzed constituents were reported to be below their soil-to-groundwater
MSCC
Municipal water and sewer are available in the immediate vicinity of the release
No water supply wells were identified within 1000 feet of the release and
No surface water bodies were identified within 500 feet of the subject release
Based on the documented absence of any analyzed parameter
above North Carolina soil-to-
groundwater MSCCs in site soils ESP recommends that the subject release be issued no further
action notice and the incident closed
Attachments
Table B-i Summary of Soil Sampling Results
Table B-2 Summary of Stockpile Sampling Results
Figure Topographic Site Location Map
Figure 2005 Aerial Photograph
Figure Soil Sample Location Map
Figure 4-Receptor Survey Map
Appendix 24-Hour Release Notification Email
Appendix Non Hazardous Waste Manifests
Appendix Site Photographs
Appendix ESPs SOP
Appendix Prism Laboratory Data Reports
ATTACITMIENTS
TABLES
6/6/07
BRL Below ReportingMSCCmaximumsoil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobile
NA Not Analyzed NL Not Listed
Summary of Soil Sampling ResultsTableB-i
ate 7/26/07 Incident No Not Yet Assigned
AnIytical Method.Ionn
j1.D üt $a iIc7 1ncident
Collected Arci DLpth-Phase
rn/ddv ft BGS
5/17/07
Table B-I
Date 7/26/07 Incident No Not Yet Assigned
An..il tical Method
ætÆfflinaittófCoiictiii
Sample Ddte Source-Sample Inudent
ID Collected Area Depth Phase
Vnste Initialil7/07 1D Abaternen
Summary of Soil Sampling Results
Morehead Common Area No Charlotte North Carolina
601GB 601GB 8270C 826GB 826GB 8260B 826GB
8260B 826GB 826GB
C.iLc
..L
..L
-.o If--o
22 51 NA 0.014 0.0068 0.027 0.021 0.021 0.014 0.014
WS-1 6/6/07 West Pit
Wall
Initial
Abatement 0.63 5.1 BRL 0.013 0.0066 0.026 0.020 0.020 0.013
0.013
WS-2 6/6/07 North Pit
Wall
Initial
Abatement 21 4.4 BRL 0.012 0.0060 0.034 0.018 0.018
0.012 0.012
WS-3 6/6/07 East Pit
Wall
Initial
Abatement 081 5.7 BRL 0.012 0006 0.025 0.018 0.018 0012 0.012
WS-4 6/6/07 South Pit
Wall
Initial
Abatement 0.71 4.1 BRL 0.020 0.0067 0.027 0.020 0.020 0.020 0.020
3.8 BRL 0.013 00063 0.025B-I 6/6/07 PitEloor 10 Initial
Abatement
Soil to GioundwatcrMSCC mg/kg
Resideittial MSCC mg/kg
Indutnal/ominerciaI MSCC mg/kg
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
0.019 0.019 0.013 0.013
27 270 --1.7 0.58 3.3 4.3
47 400 --626 313 1564 626
626 782 782
400 --16350 8176 40880 16350 16350 20440 20440
Sunimary of Soil Sampling Results
82608 82608 8082
0.0068 00068 ERL 5.1
0.0063 0.0063 BRL 0057
4.6 NL
3129 3200 1560 --NL
Table B-I
Date 7/26/07 Incident No Not Yet Assigned
8260B
Sample Date SOUrL Sample Incident
ID Collected Ar Depth PhasemIdd/y ft.BGS
SP1 5/17/07 Wastc Initial
ID Aoatemen
Morehead Common Area No Charlotte North Carolina
8081A
F-
ti
cI
WS-I 6/6/07 West Pit
Wall
Initial
Abatement 0.0 13 0.0066 0.0066 BR 0.061
WS-2 6/6/07 North Pit
Wall
Initial
Abatement 0.012 0.0060 0.0060 BRL 0.058
WS-3 6/6107 East Pit
Wall
Initial
Abatement 0.012 0.0061 0.0061 BRL 0.060
WS-4 6/6/07 South Pit
Wall
Initial
Abatement 0.020 0.0067 0.0067 3RL 0.058
B-i 6/6/07 PiE Floor 10 Initial -0013Abatement
.q
81760
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
82000 40000 NL
FIGURES
FiGURE
TOPOGRAPHIC 7E LOCA liON MAPUSGSCHARLOTTEEASTQUADRANGLE
MCWEHEAD COMMON SI7E
CHARLO17E NORTH CAROLINA $ESP
2005 AERIAL PHOTOGRAPH 10 U.6lUuo7
wL2.6O SHEET FiGURE
ESP 34Th L4kmo.I VkRAHSTyPROJECTMOREHEAOCOMMONSITE
O3-Th-24W tCICHARLOTTENORTHCAROLINA
LEQEND
WS-3
CONF7RMA TORY SOIL SAMPLE
WS-4
WASTE CHARACTER1ZA17ON SAMPLE
WS-2
2O
APPA OX/M SCALE
ws-1
FORMER CONCRETE VAULT
EXCAVATiON DEPTH OF 10 FEET
-PD9426O SHEET TITLE FiGURE At soctalIE1175SOILSAMPLEL0CA7IONMAPAREA.41E 7/ti/al 9ILThdRAIflVürPROJECTMIStThiIEOtED
DM11 MOREHEAD COMMON SITE
CHARLOTTE NORTH CAROLINA
APPENDiX
24-HOUR RELEASE NOTIFICATION EMAIL
Page lof
Chris Ward
From Chris Ward
Sent Wednesday May 30 2007 144 PM
To Steve.BogradncmaiLnet
Cc Jade Eastridge [e-mail] [e-mail]
Sub ject RE 24-Hour Notification Incidents No and
Attachments Incidents Nos and 3pdf
Please see attachment that wcis left off the original email
From ChrIs Ward
Sent Wednesday May 30 2007 140 [e-mail] [e-mail]
Subject 24-Hour Notification Incidents No and
Steve
On behalf of eazer Homes am herein providing 24-Hour Notification of the discovery of
environmentally-impacted soils at two separate locations Incidents Nos and on Beazer
Homes Morehead Commons residential development currently being graded The Morehead
Commons property is located on the south side of West Morehead Street at its intersection
with South Clarkson Street in Charlotte Meckleriburg County North Carolina
Incident No
On May 17 2007 during site grading operations concrete vault-like structure was
encountered on the east side of Post Street Tax Parcel No 07325213 approximately 450 feet
south of ifs intersection with South Clarkson Street see attached 2005 Site Map On May 172007MrChrisWardofESPobservedsoilsthatexhibitedsomeblackstaininghoweverfield
screening with an OVA did riot reveal elevated readings In an attempt to confirm the absence
or presence of potential contaminants on May 17 ESP collected wastecharacterizcjfion soil
sample SP-1 of visibly stained soils from depth of approximately feet The soil sample was
analyzed for volatile organic compounds VOCs by EPA Method 8260B pesticides by EPAMethod8081polychlorinatedbiphenylsPCBsbyEPAMethod8082oilandgreaseOcbyEPAMethod9071for total petroleum hydrocarbons TPH by EPA Methods 3550 arid 5030andfortotalleadandchromiumbyEPAMethod3051PreliminaryresultsoftheanalysisattachedrevealedelevatedlevelsofOcG3100mg/kg TPH-bRO 420 mg/kg and PCB12605.1 mg/kg The parcel was occupied by Air eduction Sales Company arid Ohio Chemicals
Surgical Equipment from 1933 to between 1956 and 1965 before the property occupant waslistedasnolisting
Incident No
On May 29 2007 during site grading operations visibly stained soils with an obvious petroleum
Page of
odor were encountered on the west side of South Clarkson Street approximately 450 feet
south of its intersection with West Morehead Street on Tax Parcel No 07325207 see
thd 2OO Si1 Map The vicinity of The impacted goiI wa onca occupied by
vehicular
service facility with closed LISTs Incidents No 18101 and 9567 buke energy-Worth Keeter
before being demolished On May 29 2007 Mr Chris Ward of ESP observed the
environmentally-impacted soils and directed the collection waste characterization soil sample
SP-3 of visibly impacted soils from depth of approximately feet The soil sample was
submitted to Prism Laboratories to be analyzed for VOCs by EPA Method 8260B pesticides by
EPA Method 8081 PCBs by EPA Method 8082 OG by EPA Method 9071 for TPH by EPA
Methods 3550 and 5030 arid for total lead and chromium by EPA Method 3051
Encident No
Please note that 24-Hour Notification for previously identified area of petroleum-impacted
soils was emailed to your attention on May 16 2007 and is referred as Incident No See
attached Site Map Results of the waste characterization analysis of the Soil sample collected
from this area and designated PS-i revealed elevated concentrations of number of VOCs OG
10000 mg/kg TPH-bRO 3600 mg/kg and TPH-GRO 33 mg/kg See attached Prism
laboratory report
Starting today Incident No us being excavated with impacted soils
stockpiled on site for subsequent off-site disposal
Following receipt of the laboratory results for the waste characterization samples and landfill
disposal authorization ESP will direct the excavation of impacted soils from Incidents Nos
and and their subsequent off-site permitted disposal Confirmatory soil samples will then be
collected from the walls and base of the excavation at Incidents Nos and Assuming
acceptable results initial abatement action reports will then be prepared for submittal to
NCbENR for each incident
The Responsible Party for the property is
Beazer Homes
1300 South Boulevard
Suite
Charlotte North Carolina 28203-4265
Mr Jade Eastridge
704.370.7200
Please call with any questions
Thanks
Chris Ward PG
Environmental Services Manager
E$P Associates P.4
803.835.0915 direct office
803.802.2515 fcix
704.506.7618 mobile
Page of
APPENDIX
NON-IIAZARDOUS WASTE MANIFESTS
on LPI LM4Ur ILL raX/U4Jfl77 Aug 16 2007 1040 P.02
ALLIED WA$TiNDU5RIESiNc
1000 Son2li Ciaæcson Street
Generclos Phone dliP1C 223
Oelder Thompson
16 GENERAIJ CERTIFICAI1ON caitjIth
Printed /IYped Name
17 Transporter Acknowledgement ol Receipt of Materials
Printed Typed Name
lB ltensporter AcknaWledgemejn of Receipt of Materials
Printed Typed Name
Company Name
ORIGINAL RETURN TO GENERATOR
tin uii LMWt-ILL I-ax 1047B221 77 Aug 2007 11341 03
18 GENERATORS ist certify the malerlata described above on thia menifsj ala not eithjuct to federalPrinted1jpedName
17 Transporter AcknowJecJgem0 of Receipt of Materials
Printed /1specf Name
18 Transporter Acknowfedgemenf of Receipt of
Printed 1jped Name
19 Discrepancy 1ndIaatIn Space
ALLIED WA$TINDUSTRIESINC
Mardfes
Qoownent
1000 South CIark Sttet
Charlotte NC 2g231
OMS LàndtHI
5105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Description
ORIGINAL RETURN TO GENERATOR
UI-I CIS LANUILL Fax 1J47B22177 Au 2007 1041 P.04
ALLIED WASTEINDUSTftIE twc
1000 South Cladcsu Jtetchtj8JC231
16 GENERATOft$CERTIFICAyJON cenhty he materials declbed abv an this menU sat are not subject toPittted/Typed Name BeazerjJojng
17 Transporter Acknowledgement at Receipt of Materials
Printed/Typed Name
Transpofter2A kno Jgemant of Receipt of Matertais
PrInted fped Name
19 Discrepancy IndIcation Space
20 FacUlty Owner or OperetorCM$Landtllt
Printed/Type Name
ORIGINAL RETURN TO GENERATOR
ur W4 LMIiIfl-ILL -a 7047B221 77 Aug lii 2007 1041 P.116
j4 G8flItOSPhOflG
Ii Transporter Company
ALLIED WASfEINDU$TRE INC
fizerIoe
1000 South qadcBoa Stteet
chaikij2 NC 223I
18
Printer4fType Name Beacrn
17 Transporir AcknowferJement 01 RecIp at Materials
Printed/Typed Name
Tiansporte-
Printed/Typed Name
Indication Spaca
ORIGINAL RETURN To GENERATOR
APPENDIX
SITE PHOTOGRAPHS
MOREHEAD COMMON SITE AREA
VIEW OF CONCRETE VAULT PRIOR TO ITS EXCAVATION VIEW OF AREA NO.2 EXCAVATION -LOOKING SOUTHWITHFOSTSTREETINBACKGROUN
VIEW OF AREA NO.2 EXCAVATION LOOKING SOUTH WITH
POST STREET IN BACKGROUND VIEW OF AREA NO.2 EXCAVATION LOOKING WEST WITHPOSTSTREETTNBACKGROUND
APPENDIX
ESPS SOP
STANbARb OPERATING PRCCEbURE
50P-6
SOIL SAMPLE COLLECTION
ESP Associates P.A Revision bate 3/7/06
This standard operating procedure SOP covers the collection of soil sample for
laboratory analysis Follow these steps when collecting the soil sample unless
otherwise instructed by the project manager
Gather needed field supplies noted below
Confirm lab cooler contains needed sample containers fill cooler with
ice
Upon arriving at site check in with the property owner or company
representative
becontaminate the stainless steel hand auger before and between sample
collection by washing with Alconox soap and scrub brush rinsing with
distilled water and spraying with Isopropyl alcohol Wrap clean sampler
in aluminum foil
Wear disposal latex or nitrile gloves and change into new pair between
samples
buring advancement of the hand auger collect soil samples at regular
intervals for describing lithology Note lithology and other
characteristics of soils in field book relative to depth
If appropriate place representative portion of soil sample into
resealable plastic bag label with boring number and depth interval and
allow to equilibrate Screen soil in bag for volatile organics using an OVA
or Hnu Enter results into field book
Advance hand auger boring to previously specified sampling depth
Collect soil sample from this depth and place in laboratory provided
containers Label containers with boring number and sample depth using
the following sampling scheme i.e B-I ft B-i 10 ft B-2 ft etc
benote boring location in field book relevant to pertinent site features
10 Following collection of The soil samples abandon alt boreholes feet or
greater in depth with cement grout
11 Complete and sign the labs chain-of-custody
12 Keep the sample cooler in secure location until delivered under normal
chain-of-custody procedures to laboratory
5OP-6 Soil Sample Collection Revision bate 3/7/06
E5PAssociates Page of
SUPPUES
SOP-6
Stainless steel hand auger with needed extensions or sampling
spoon
ci OVA orHnu
ci Measuring tape
ci Plastic zip-lock bags
ci Isopropyl alcohol
bistilled water
ci 5-gallon wash bucket scrub brush and Alconox soap
Cement with wheel barrow for mixing
ci Cooler with sample containers and chain-of-custody
tce
ci Permanent marker
bisposable gloves
Knife
ci Field book
Site plan with Site specific sampling instructions
Camera
APPENDiX
PRISM LABORATORY DATA REPORTS
kU JUN 200/
Case NarrativePRISM
LEORATORIES.INC
Date 06119/07 ClIent Project ID Morehead Commons No
Company ESP Associates PA Prism CCC Group No G0607179
Contact Chris Ward Collection Dates 06/06/07
Address P.O Box 7030 Lab Submittal Dates 06/06/07
Charlotte NC 28241
This data package contains the analytical results for the project Identified above and Includes Case Narrative Laboratory Report
and Quality
Control Data totaling 56 pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
No Anomalies Reported
Metals Analysis
Analysis Note for 024176 MS Chromium Matrix Interference is suspected Post-digestion spike recovery 79%is within the
acceptance lImits 75-125%
Analysis Note for 024176 MS Lead Matrix interference Is suspected Post-dlgeslior spike recovery 73%is outside the
acceptance lImits 75-125%
Analysis Note for 024176 MSD Chromium Matrix Interference Is suspected
Analysis Note for 024176 MSD Lead Matrix Interference is suspected
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by Paula Gilleland Project Managec Angela ercash
Signature I1.JL.1tth.3L Signature _________________________
Review Date 06119107 Approval Date 06119/07
Data Qualifiers Key Reference
Compound also detected In the method blank
1k Result outside of the CC limits
DO Compound diluted out
Estimated concentration1 calibration range exceeded
The anaiyte was positively identified but the value Is estimated below the reporting limiL
Estimated concenttatin with high bias
Estimated concentration with law bias
matrix effect is present
Notes This report should not be reproduced1 excepL In Its entirety without the wriLtten consent of Prism Laboratories Inc The results in this
report relate only to the samples submitted for analysis
449 Sprlngbiook Road P.O Box 240543 Charlotte NC 28224-0403
Phone [phone] Toil Free 600/529-6364 Fax [phone]
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 183632
Sample Matrix Soil COO Group 00607179
Time Collected 06/06/07 1400
Time Submitted 06/06107 1640
Percent Solids 82.6 SM2540 0611/07 1700 ibrown
44.DDD
44DDE
44-DDT
44-Methoxychtor
a-SI-IC
bSI-IC
Chiordane
d-BHC
DIeIdrIn
Endosulfan
Endosulfan II
Endosulfan Sulfate
Endrin
Endrtn Aldehyde
Endain Ketone
g-BHC
g-Chlordane
Heptachlor
Heptachior Epoxlde
Toxaphene
BRL pg/kg 2.4 0.74
SRI pg/kg 2.4 0.52
SRI pg/kg 2.4 0.87
BRL pg/kg 4.8 1.7
BRL pg/kg 2.4 0.22
SRI pg/kg 2.4 0.42
BRI pg/kg 2.4 0.48
SRI pg/kg 2.4 0.61
SRL pg/kg 61 14
SRI pg/kg 2.4 0.34
BRI pg/kg 1.2 0.50
BRL pg/kg 2.4 0.43
BRI pg/kg 2.4 0.55
BRL pg/kg 2.4 0.63
SRL pg/kg 2.4 0.73
BRI pg/kg 2.4 0.68
SRI pg/kg 2.4 0.48
BRL pg/kg 2.4 0.28
BRL pg/kg 2.4 0.39
SRI pg/kg 2.4 0.57
BRL pg/kg 2.4 0.45
SRI pg/kg 61 14
06/13/07 2308 jvogel
06/13/07 2308 Jvcgel
06/13/07 2308 Jvogel
08/13/07 2308 Jvogel
06/13/07 2308 ivogal
06/13/07 2308 Ivogal
06/13/07 2308 jvogel
06113/07 2308 Jvcgel
8081A 06/13/07 2308 Jvogel
8081A 06/13/07 2308 Jvogel
024275
024275
024275
024275
024275
024275
024275
024275
024275
Q24275
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1400/529.6384 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 31735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Percent Solids Determination
Organochiot-ine Pesticides by Gas Chromatography
a-Chlordane
Aldrin
06/13/07 2308 Jvogel
08/13/07 2308 jvogel
06/13/07 2308 Jvogei
06113/07 2308 ivogel
06/13/07 2308 Ivogel
05/13/07 2308 Jvogei
06/13/07 2308 Jvogel
024275
024275
024275
024275
024275
024275
024275
BORIA
8081A
8081A
8081A
8081A
8081A
8OBIA
8081A
8081A
BOBIA
8081A
BOBIA
8081A
8081A
BOB1A
8081A
8081A
8081A
8081A
8081A
06/13/07 2308 Jvogel
06113/07 2308 jvogel
06/13/07 2308 jvogei
06/13/07 2308 Jvogel
06/13/07 2308 Jvogel
024275
024275
024275
024275
024275
Page of 45
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06118/07
WS-i
183632
G06071 79
06106107 1400
06106107 1640
Parameter Result Units Report MDL DIIuUon Method Analysis Analyst
Batch
Limit Factor Daternme ID
Volatile Organic Comoouncjs by GCIMS
111 2-Tetrachloroethane
11 1-Trlchloroethane
1122-Tetractdoroetiane
112-Tjichloroethane
11D1chloroethane
11-Dichioroethene
11-Dithioropropene
123-Trlchlorobenzene
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-8364 Fax [phone]
FuJI SrIvn AnJyIIcI IEnkunmubI SIuIIon
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Sample PreparatIon 29.88 10 mL 355DB 06112/07 1000 tipope P18598
Surrogate Recovery Control Limits
Decachiombiphenyl DCB 128 26-204
Tetrachloro-m-xylene TCMX 106 40-162
Polychlorlnated Biphenyls IPCBs by GC-ECD
PCB-1016 BRL
PCB-1221 BRL
PCB-1232 BRL
PCB-1242 BRL
PCB-1 248 BRL
PCB-1254 BRL
PCB-1260 BRL
Sample Preparation
0.061
0.12
0.061
0.061
0.061
0.061
0061
0.011
0.049
0.019
0.021
0.0064
0.021
0.016
8082
8082
8082
8082
8082
8082
6082
06/13/07 2308 JvoseI
06/13/07 2308 jvogel
06/13/07 2308 Jvogel
06/13/07 2308 Jvogel
06/13/07 2308 Ivogel
06/13107 2308 Jvogel
06/13/07 2308 jvogeI
024276
024276
024276
024276
024276
024276
024276
P1859729.88 10 mL 355DB 06/12/07 1000 dpope
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
Surrogate Recovery Control Limits
Decachlorobiphenyl DCB 109 34-182
Tetrachioro-m-xylene TCMX 109 36-182
BRL
ERL
BRL
BRL
BRI
BRL
BRL
BRL
6.6 0.64
6.6 0.37
6.6 0.67
6.6 0.41
6.6 0.47
6.6 0.50
6.6 0.58
13 0.72
82608
8260B
826DB
8260B
826DB
828DB
826DB
826DB
06/08107 1610 ejussell
08/08/07 1610 erussell
06/08/07 1610 enisseil
06/08/07 1610 erussell
06/08/07 1610 erussell
06/08/07 1610 erusselt
06/08/07 1610 erussell
06/08/07 1610 erusseil
024147
024147
024147
024147
024147
024147
024147
024147
Page of 45
Laboratory Report
06/1 8/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 183632
Sample Matrix Soil CCCGroup 00607179
Time Collected 06/06/07 1400
Time Submitted 06/06/07 1640
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrookReactP.O Box 240543 Charlofte NC 28224-0543
Phone [phone] Toll Free Number 1400/5294364 Fax [phone]
NC Certification tio 402
SC Certification No 99012
NC Drinking Water Cart No 37735
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
123-Trichioropropane BRL pg/kg 6.5 0.58 826DB 06108/07 1610 onissell Q24147
124-Trichforobenzene BRL pg/kg 13 0.63 8260B 06/08/07 1610 enissell 024147
124-Tifrnethylbenzene BRL pg/kg 13 050 826DB 0608/07 1610 erussall 024147
12-Dlbromo-3-chloropropane BRL pg/kg 6.6 1.0 82606 06108/07 1610 erussell 024147
12-DlbromoethaneEDB BRL pg/kg 6.6 0.12 8260B 0608/07 1610 enissell 024147
12-Dlchlorobenzene BRL pg/kg 13 0.36 8260B 06/08/07 1610 erussell 024147
12-Dlchloroethane BRL pg/kg 6.6 0.66 82608 0608/07 1610
esusset Q24147
2-Dlchloropropane BRL pg/kg 6.6 0.48 82608 0608/07 1610 enisset 024147
135-Trlmethylbenzene BRL pg/kg 13 0.55 826DB 0608/07 1610 erusseil 024147
3-Dlchlorcbenzene BRL pg/kg 13 0.57 82608 05/08107 1610 erussell 024147
13-Dichioropropane BRL pg/kg 6.6 0.45 826DB 06/08/07 1610 erusselt 024147
14-Dlchiorobenzeno BRL pg/kg 13 0.51 82608 06/08/07 1610 erussell 024147
22-Dichioropropane BRL pg/kg 6.6 0.33 8260B 06/08/07 1610 erusseil 024147
2-Chloroethyi vinyl ether-BRL pg/kg 13 0.49 8260B 06108/07 1610 erussoll 024147
2-Chiorololuene BRL pg/kg 13 0.49 826DB 06108/07 1610 erussefl 024147
2-Hexanone BRL pg/kg 66 0.68 82608 06/08/07 1610 enissell 024147
.4-Chiorotoluene BRL pg/kg 13 0.34 826DB 0608/07 1610 enissell 024147
4-Methyl-2-pentanone MIBK BRL pg/kg 13 0.66 826DB 06/08/07 1610 erussell 024147
Acetone BRL pg/kg 26 2.6 826DB 06/08/07 1610 erusselt Q24147
Benzene BRL pg/kg 3.9 0.53 828DB 06/08/07 1610 erussell 024147
Brornobenzene BRL pg/kg 6.5 0.46 826DB 06/08/07 1610 erussell 024147
Bromochloromethane BRL pg/kg 6.5 0.39 826DB 06/08/07 1610 enisseil 024147
Bromodlchlorometharie BRL pg/kg 6.6 0.58 826DB 06/08/07 1610 enisseR 024147
Bromofomi BRL pg/kg 6.6 0.49 82608 06/08/07 610 erussafl 024147
Bromometharie BRL pg/kg 13 0.76 8260B 06/08/07 1610 anisset 024147
Carbon disutilde BRL pg/kg 13 0.42 8260B 08/08/07 1610 erussell 024147
Carbon tetraohlojde BRL pg/kg 6.6 0.38 826DB 0608/07 1610 erussell 024147
Page of 45
Chlcrobenzene
Chlcrodibromomethane
Chioroethane
Chloroform
Chioromethano
dc-I 2-Dlchloroeth one
cls-I 3-Dichloropropene
Dibromornethane
Dlchlorcdffluoromethane
Ethylbenzene
Hexachlorobutadlene
Isopropyl ether IPE
lsopropylbenzene
mp-Xylenes
Methyl ethyl kelone MEK
Methyl t-butyl ethei-MTBE
Methylene chloride
n-Butylbenzene
n-Propylbenzene
Naphthatene
o-Xylene
p-Isoprcpyltatuene
seo-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachioroethene
Toluene
This repret should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6354 Fax [phone]
NC CertificatIon No.402
SC Certification No 99012
NC Drinking Water Cert No 37735
.ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Parameter
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 183632
Sample Matrix Soil COC Group 30607179
Time Collected 0606/07 1400
Time Submitted 08106/07 1640
Result Units Report MDL Dilution Method Analysis Analyst aatch
Limit Factor Date/Time ID
6.6 0.50BRLpg/kg 826DB 06108/07 1610 erussefl 024147
BRL pg/kg 6.6 0.45 826DB 06/08/07 1610 enissI Q24147
BRL pg/kg 13 0.54 826DB 06/08/07 1610 erusaefl 024147
BRL pg/kg 6.6 0.49 826DB 06/08/07 1610 erusset 024147
BRL pg/kg 13 0.46 82608 06/08/07 1610 erussell 024147
BR pg/kg 6.6 0.29 826DB 06/08/07 1610 erusseil 024147
BR pg/kg 6.6 0.42 826DB 06/08/07 1610 erusseil 024147
BRL pg/kg 6.6 0.49 826DB 06/08/07 1610 erussell 024147
BRL pg/kg 13 1.5 826DB 06/08/07 1610 erussell 024147
BR pg/kg 6.6 0.46 826DB 06/08107 1610 esussell 024147
BRL pg/kg 20 0.82 826DB 06/08/07 1610 erussell 024147
BRL pg/kg 6.6 0.22 826DB 06/08107 1610 enisseil 024147
BRL pg/kg 13 0.53 826DB 06/08107 1610 erussell 024147
BRL pg/kg 13 0.82 826DB 06/08/07 1610 erussell 024147
BRL pg/kg 26 1.8 826DB 06/08/07 1610 erussell 024147
BR pg/kg 6.6 0.38 826DB 06/08/07 1610 erussell 024147
BRL pg/kg 13 0.54 82608 06/08/07 1610 erusselt 024147
BR pg/kg 20 0.53 826DB 06/06/07 1610 erussell 024147
BR pg/kg 13 0.39 82608 06/08/07 1610 erusse 024147
BR pg/kg 6.6 0.76 826DB 06/08/07 1610 erussell 024147
BRL pg/kg 6.6 1.39 826DB 06/08/07 1610 erussell 024147
BRL pg/kg 20 0.54 826DB 06/08107 1610 erusesfl 024147
BRL pg/kg 20 0.43 826DB 06/08/07 1610 enisseil 024147
BR pg/kg 6.6 0.66 82608 06/08/07 1610 erussoll 024147
BRL pg/kg 26 0.41 82608 08/08/07 1610 orusse 024147
BRL pg/kg 13 1.1 82609 06/08/07 1610 erusseil 024147
BRL pg/kg 6.6 0.45 82608 06/08/07 1610 erussell 024147
Page of 45
NC Certification No 402 Laboratory ReportScCertificationNo99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 183632
Sample Matrix Soil coc Group G06071 79
Time Collected 06106107 1400
Time Submitted 06/06/07 1640
Parameter
trans-i2-Dlchloroethene
trans-I 3-Dlchloropropene
Trichioroethene
Trlchiorofluoromethane
Vinyl chloride
5035 06/13/07 000 brown
5035 06/1307 000 brown
5035 0613/07 000 ibrown
Semi-volatile Organic Compounds by GCIMS
I24-Trichlombenzene BRL
12-Dlchiorobenzene BRL
13-Dichjorobenzene ORL
4-Dichlorpbenzene BRL
245-Trichiorophenot BRL
248-Tiichlorophenoi BRL
24-Dlchlorophenol BRL
24-Dimethyiphenol BRL
24-4Jlnltrophenol BRL
24-Dinitrotoluene BRL
26-Dlnltrotoltjene BRL
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543-Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Result Units Report MDL Dilution Method
Limit Factor
Analysis Analyst Batch
Date/Time ID
BRL pg/kg 6.6 0.50 826DB 06/06/07 1610 erusselt Q24147
BRI pg/kg 6.6 0.46 626DB 06/08/07 1610 erussell Q24147
BRL rig/kg 6.6 0.39 826DB 06/08/07 1610 enisseil Q24147
BRL pg/kg 6.6 0.54 826DB 06/08/07 1610 erussefl Q24147
BRL pg/kg 13 0.84 826DB 06/08/07 1610 erussell Q24147
Sample Weight Determination
weight Bisulfate
Weight Blsulfate
Weight Methanol
Surrogate Recovery Control Limits
Bromofluorcbenzene 104 77-128
Dlbromofluoromethane 92 67-143
Toluene-dB 96 81 128
5.02
4.60
4.43
pg/kg 400 39 8270C 08/1107 1117 kcamptotto Q24124
pg/kg 400 29 8270C 06111/07 1117 kcamplgotto Q24124
pg/kg 400 29 8270C 06111/07 1117 kcampigalto Q24124
pg/kg 400 36 8270C 06/11/07 1117 kcamplgotto Q24124
pg/kg 400 41 8270C 06/11/07 1117 kcamplgotto Q24124
pg/kg 400 38 8270C 06/11/07 1117 kcamplgotto Q24124
pg/kg 400 33 8270C 06/11/07 1117 kcamplgotto 024124
pg/kg 400 38 8270C 06111/07 1117 kcamplgollo 024124
pg/kg 400 45 8270C 06/11/07 1117 kcampigotto Q2414
pg/kg 400 23 8270C 06/1 1/07 1117 kcamplQoito 024124
pg/kg 400 42 8270C 06111/07 1117 kcmpIgott 024124
PageS of 45
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 183632
Sample Matrix Soil COG Group G0607179
Time Collected 06/06/07 1400
Time Submitted 06/06/07 1640
This report should net be repmduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6254 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Laboratory Report
06/18/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
2-Chforonaphthafene BRL pg/kg 400 41 827CC 06/11/07 1117 keamplgotto 024124
2-Chiorophenol BRL pg/kg 400 31 82706 00/11/07 1117 kcampigotb Q24124
2-Methyinaphthalene BRL pg/kg 400 32 62706 06/11/07 1117 kcampfgotto 024124
2-Methyiphenol BRL pg/kg 400 37 8270C 06/11/07 1117 kcamplgotto 024124
2-Nitrophenol BRL pg/kg 400 48 82706 05/11/07 1117 kcamplgottu 024124
34-Methyiphenol BRL pg/kg 400 41 827CC 06/11/07 1117 kcamplgotta 024124
33-Dichlorobenzidlne BRL pg/kg 400 25 827CC 06/1107 1117 kcamplgotto 024124
46-Dlnitro-2-methylphenol BRI pg/kg 400 24 8270C 06/11/07 1117 kcamplgotto 024124
4-Bromophenylphenylether BRL pg/kg 400 36 8270C 06/11/07 1117 kcamplgetto 024124
4-Chloro-3-methylpherioi BRL pg/kg 400 29 8270C 0611/07 1117 kcamplgottc 024124
4-Chiorophenyiphenylether BRL pg/kg 400 25 8270C 06/11/07 1117 kcamplgottci 024124
4-Nitrophenol BRL pg/kg 400 26 82706 05/11/07 1117 kcarnplgotto 024124
Acenaphthene BRL pg/kg 400 39 B270C 06/11/07 1117 kcamplgottc 024124
Acenaphthylene BRL pg/kg 400 39 82706 06/11/07 1117 kcamplgotto 024124
Anthracene BRL pg/kg 400 30 62706 06/11/07 1117 kcamplgotto 024124
Benzoaanthracerie BRL pg/kg 400 56 827CC 06/11/07 1117 kcamplgotto 024124
Benzoapyrene BRL pg/kg 400 46 82706 08/11/07 1117 kcamptgotto 024124
Benzobfluomnthene BRL pg/kg 400 18 82706 06/11/07 1117 kcamplgotto 024124
Benzcghjperylene BRL pg/kg 400 19 827CC 06/11/07 1117 kcamplgollo 024124
BenzokIluoranthene BRL pg/kg 400 32 82706 06/1107 1117 kcamplgotlo 024124
Bls2-chloroethoxymethane BRL pg/kg 400 46 62706 06/11107 1117 kcamplgotto 024124
BIs2-chloroethylather BRL pg/kg 400 43 827CC 06/11/07 1117 kcamptgotto 024124
BIs2-chlorolsopropyleuier BRI pg/kg 400 34 8270C 06/11/07 1117 kcarnplgotio 024124
Bis2-ethylliexylphthalate BRL pg/kg 400 20 82706 05/11/07 1117 kcamplgctto 024124
Butylbenzylphthalate BRL pg/kg 400 24 82706 06/11/07 1117 koamplgotto 024124
Chrysene BRL pg/kg 4CC 66 82706 06/11/07 1117 kcamplgotto 024124
DI-n-butylphthaf ate BRL pg/kg 400 18 82706 06/11/07 1117 kcamplotto 024124
Page o145
Dl-n-octylphthalate
Dlbenzoahanthraceno
Dlbenzofuran
Diethylphthalate
Dirnethylphthal3te
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachiorobutadlene
Hexachlorocyclopentadlene
Hexachforoethane
lndeno123-cdpyrene
Isophorone
N-Nltrosodl-n-propylamlne
N-Nltmsodlphenylamlne
Naphihatene
Nltmbenzene
Pentachiomphenot
Phenanthrene
Phenol
Pyrene
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 183632
Sample Matrbc Soil COC Group G0607179
Time Collected 06/06/07 1400
Time Submitted 06106/07 1640
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Ins
449 Spnngbrook Road P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn ChrIs Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datemrne ID
BRL pg/kg 400 30 827CC 06/11/07 1117 koamplgotto 024124
SRI pg/kg 400 40 8270C 06/11/07 1117 kcarnplgotto 024124
BRL pg/kg 400 34 827CC 06/11/07 1117 koaniplgotto 024124
BRL pg/kg 400 24 827CC 06/11/07 1117 kcamplgotto 024124
BRL pg/kg 400 27 827CC 08/11/07 1117 kcamplgolto Q24124
BRL pg/kg 400 27 827CC 08/11/07 1117 kcamplgotto 024124
BR pg/kg 400 24 827CC 06/11/07 1117 kcamplgottc 024124
BRL pg/kg 400 21 827CC 06/11/07 1117 kcamplgollo 024124
BRL pg/kg 400 39 827CC 06/11/07 1117 kcamplgotto 024124
BRL pg/kg 400 42 8270C 06111/07 1117 kcsmplgotto 024124
BRL pg/kg 400 40 827CC 06/11/07 1117 kcamplgotlo 024124
BRL pg/kg 400 41 8270C 06/11/07 1117 kcamplgotto 024124
BRL pg/kg 400 38 827CC 06/11/07 1117 keamplgotto 024124
BRL pg/kg 400 45 827CC 06/11/07 1117 kcamplgotto 024124
BRL pg/kg 400 20 8270C 06/11/07 1117 kcamplgouo 024124
BRL pg/kg 400 43 827CC 08/11/07 1117 kcamplgolth 024124
BRL pg/kg 400 39 827CC 06/11/07 1117 keamplgotto 024124
BRL pg/kg 400 33 827CC 08/11/07 1117 koamplgolto 024124
BRL pg/kg 400 19 827CC 06/11/07 1117 kcamplgollo 024124
BRL pg/kg 400 43 8270C 06/11/07 1117 kcampTgotto 024124
BRL pg/kg 401 27 8270C 06/11107 1117 kcamplgotto 024124
Page 70145
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 06/18/07
FLII5wvko AnIytJcaI EvkonmrnietSatUtirnis
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-1
Attn Chris Ward Prism Sample ID 183632
Box 7030 Sample Matrix Soil COC Group G0607179
Charlotte NC 28241 Time Collected 06/06/07 1400
Time Submitted 06/06/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 30.16 rnL 355GB 06/08/07 700 dpope P18579
Surrogate Recovery Control Limits
246-Tribromophenol 76 25 123
2-Fluoroblphenyl 54 21 -108
2-Fluorophencl 57 14-89
Nltmbenzene-d5 55 14-103
Phenokl5 59 13-95
Terphenyl-d14 84 41-136
Extractable Petroleum Hydrocarbons by GC.FIl
C11-C22Aromatlcs BRL mg/kg 13 6.8 MADEP EPH 0611607 2047 grappaccloli 024301
C19-C3OAllphaUcs BRL mg/kg 13 1.9 MADEP EPH 06116/07 2047 gmppaccloii 024301
C9-C18 Allphatics BRL mg/kg 13 4.0 MADEP EPI-l 06116/07 2047 grappacciot 024301
analysis Note for C11-C22 Aromatics Adjusted value
Sample Preparation 9.62 niL EPH 0613/07 800 dpope P18614
Surrogate Recovery Control Limits
1-Chlora-octadecane 112 40-140
2-Bromonaphthalena 135 40-140
2-Fluoroblphenyl 131 40-140
o-Terphenyl 102 40-140
Metals by ICP
Chromium 0.63 mg/kg 0.30 0.018 601GB 06111/07 2050 mcampbetl 024176
Lead 5.1 mg/kg 0.30 0.025 601DB 06/11/07 2050 mcarnpbeft 024176
Sample PreparatIon 2.03 50 niL 30506 06/11/07 905 Jhoppel P18580
Volatile Petroleum Hydrocarbons by GC-PIDIFU
C5-C8 Aliphatics BRL mg/kg 6.1 1.2 MADEP VPH 06/12/07 2127 hwagner 024220
C9-C10 Aromatics BRL mg/kg 6.1 0.036 MADEP VPH 06/12/07 2127 hwagner 024220
This report should not be reproduced except In Its entirety without the written consent or Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6354.Fax [phone] Page 8o145
Laboratory Report
06/18/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
C9-C12 AtIphatics BRL mg/kg 6.1 1.9 MADEP VPH 06112/07 2127 hwa9ner Q24220
Analysis Note for C5-CB Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
One surrogate recovery
was outside the control limits No target compounds were detected inthissampleNofurtheractionwastaken
Surrogate Recovenj Control Limits
25-Dlbromotoluene-PID 118 70-130
25-Dlbromotoluene-FID 155 70-130
Sample WelghtDetormlnatjon
WeIght 20.05 MADEP VPH 08113/07 000 thrown
WeIght 17.23 MADEP VPH 06/13/07 000 brown
Sample Comments
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report rn/ate only to the samples submitted for analysis and meet state certification requirements of hor thanNELACcertificationexceptforthoseInstances Indicated In the case narrative and/or test comments
All results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except In its entirely without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
NC Certification No 402
SC Certification No 99012
_______
NC Drinking Water Cert No 37735
iIcs AnsIytfaI EmuembSotuthjn
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-1
183632
G0607179
06/06/07 1400
06/06/07 1640
Phone [phone] Toll Free Number 1500/529-6364 Fax [phone] Page of 45
NC CertIfication No.402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 06/18/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 183633
Sample Matrix Soil COG Group G0607179
Time Collected 06/06/07 1415
Time Submitted 06/06/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Percent Solids Determination
44-DDD
44-DDE
44-DDT
44-Methoxychlor
a-BHC
a-Chlordane
Aidrin
b-BIC
Chiordane
d-BHC
Dieldrin
Enclosulfan
Endosuffan II
Endosulfan Sulfate
Endiin
Endrin Aldehyde
Endrin KetOne
g-BHC
g-Chiordane
l-teptchlor
Heptachlor Epoxfde
Toxaphene
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
5M2540 06/11/07 1700 Ibrown
8OBIA
8081A
8081A
8081A
BOBIA
8081A
8OB1A
8081A
8081A
8081A
8061A
8081A
8081A
BOBIA
BOBIA
8081A
8081A
8081A
8081A
8081A
8081A
06/13/07 2350 Jvogel
06/13/07 2350 jvogel
06/13/07 2350 Jvogel
06/13/07 2350 Jvogel
06/13/07 2350 Jvogel
06/13/07 2350 Jvog
05/13/07 2350 Ivogel
06/13/07 2350 Jvoget
06/13/07 2350 Ivogel
06/13/07 2350 VogeI
06/13/07 2350 JYogel
06/13/07 2350 iVogel
08/13/07 2350 Jvogel
06/13/07 2350 Jyogel
08113/07 2350 Jvogel
06/13/07 2350 Ivpgei
06/13/07 2350 Jvogel
06/13/07 2350 Jvoget
06/13/07 2350 Jvogel
06/13/07 2350 JvogeI
06/13/07 2350 Ivogel
Q24275
024275
024275
024275
024275
024275
Q24275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
This report should not be reproducefJ except in its entirety without the written consent of Prism Laboratones Inc449SprlngbrookRoadP.O Box 240543 CharJotte NC 28224.0543
Phone [phone] Toll Free Number 1-800/529.6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Percent Solids 86.4
Organochiorine Pesticides by Gas Chromatography
pg/kg 2.3 0.71
pg/kg 2.3 0.49
pg/kg 2.3 0.83
pg/kg 4.6 1.6
pg/kg 2.3 0.21
pg/kg 2.3 0.40
pg/kg 2.3 0.46
pg/kg 2.3 0.59
pg/kg 58 13
pg/kg 2.3 0.33
pg/kg 1.2 0.48
pg/kg 2.3 0.41
pg/kg 2.3 0.52
pg/kg 2.3 0.60
pg/kg 2.3 0.70
pg/kg 2.3 0.65
pg/kg 2.3 0.46
pg/kg 2.3 0.27
pg/kg 2.3 0.36
pg/kg 2.3 0.55
pg/kg 2.3 0.43
BRL pg/kg 58 13 8081A 06/13/07 2350 Ivogel
Page 10 0145
NC CertIfIcatIon No 402
SC Certification No 99012
NC Drinking Water Cod No 37735
Sample Preparation 29.75 10 mL 3550B 06/12/07 1000 dpape P18598
Polychiorinated Biphenyis 1PCBs by GC-ECD
PCB-1016 BRL
PCB-1221 BRL
PCB-l 232 BRL
PCB-1 242 BRL
PCB-1248 BRL
PCB-1254 BRL
PCB-l 260 BRL
Volatile Oruanic Compounds by GCIMS
111 2-Telrachlaroethane
11 1-Trichloroethane
ii 2.2-Tetrathloroethane
11 2-Trtchloroethane
11-Dldiloroethane
11-Dichiaroethene
11-Dichioropropene
123-Trlchlorobenzene
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories inc
449 Sprlrigbroak Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toil Free Number 1-800/529-6364 Fax [phone]
ESP Assoclat6s PA
AIIm Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/18107
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
183633
G0607179
06/06/07 1415
06106/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
0.058
0.12
0.058
0.058
0.058
0.058
0.058
0.011
0.047
0.019
0.020
0.0080
0.020
0.016
Sample Preparation
Surrogate Recovery Control Limits
Tetrachloro-m-xylene TCMX 103 40 182
Decachiorobiphenyl DCB 121 26 204
8082 06/13/07 2350 Jvogel 024276
8082 06/13/07 2350 Jvogei 024275
8082 06/13/07 2350 lvDgeI 024276
8082 06/13/07 2350 Ivogel 024276
8062 06/13/07 2350 Jvogel 024276
8082 06/13/07 2350 Jvogel 024276
8082 06/13/07 2350 Jvoge 024276
10 mL 355DB 06/12/07 1000 dpope P18597
Surrogate Recovery Control Limits
Decachiorobiphenyl DCB 89 34 -182
Tetrachloro-m-xylene TCMX 101 36 182
mg/kg
mg/kg
mg/hg
mg/kg
mg/kg
mg/kg
mg/kg
119/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
29.76
6.0 0.55
6.0 0.33
6.0 0.61
6.0 0.37
6.0 0.43
6.0 0.45
6.0 0.52
12 0.65
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
826DB
826DB
826DB
826DB
826DB
826DB
826DB
826DB
06/08/07 1642 eru5seU
06/08/07 1642 erussell
06/08/07 1642 erussef
06/08/07 1642 erussell
06/08/07 1642 erussell
06/08/01 1642 ecussalt
06/08/07 1642 etussell
06/06/07 1642 erussell
024147
024147
024147
024147
024147
024147
024147
024147
Page 11 of 45
Laboratory Report
NC Drinking Waler Cert No 37735
Project ID Morehead Commons No Client Sample ID WS-2
PrIsm Sample ID i83633
Sample Matrix Soil COC Group G0607179
Time Collected 06106/07 1415
Time Submitted 06/06107 1640
Parameter
ID
23-Trichloropropane 826oB 024147
24-Trtchlorôbenzene 826DB 024147
124-Trimethylbenzene 826DB 024147
12-Dibromo-3-chloropropane 626DB 024147
12-Dibromoethane EDB 826GB 024147
12-Dichlorobenzene 826DB 024147
12-Dichloroethane 826DB 024147
12-Dichtoropi-opane 626DB 024147
135-TrimŁthylbenzene 826DB 024147
13-Dlchiorobenzene 826DB 024147
13-Dlchloropropane 826GB 024147
4-Dichlorobenzene 626DB 024147
2.2-Dlchioropropane 826DB 024147
2-Chioroethyl vinyl other 826DB Q24 147
2-Chloreloluene 826DB 024147
2-Hexanono 826DB 024147
4-Chlorotoluene 826DB 024147
4-Methyl-2-pentanone MIBK 826GB 024147
Acetone 526DB 024147
Benzene 826DB 024147
Bromobenzene 826DB 024147
Bromochiurornethane BRL 826DB 024147
BromOdlchloromelhane SRI 52603 024147
Bromofomi SRI 826DB 024147
Bromometharig BRL 82603 024147
Carbon disultide BRL 82609 024147
Carbon tetrachlojjda BRL 82609 024147
This report should not be reproduced except In its entirety without the written consent Prism Laboratories Inc
449 Sprlflgbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phono 704/529-5364 Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
06/18/07
Result Units Report MDL Dilution Method
Limit Factor
Analysis Analyst Batch
Date/Time
BRL pg/kg 6.0 0.52
BRL pg/kg 12 0.57
BRL pg/kg 12 0.45
BRL pg/kg 6.0 0.94
BRL pg/kg 6.0 0.11
BRL pg/kg 12 0.32
BRL pg/kg 6.0 0.60
BRL pg/kg 60 0.44
BRL pg/kg 12 0.50
SRI pglkg 12 0.51
BRL pg/kg 6.0 0.4D
BRL pg/kg 12 0.46
BRL pg/kg 6.0 0.30
BRL pg/kg 12 0.44
BRL pg/kg 12 0.44
BRL pg/kg 60 0.62
BRL pg/kg 12 0.31
BRL pg/kg 12 0.60
34 pg/kg 24 2.3
BRL pg/kg 3.6 0.48
BRL pg/kg 6.0 0.42
pg/kg 6.0 0.36
pg/kg 6.0 0.52
pg/kg 6.0 0.44
pg/kg 12 0.69
pg/kg 12 0.38
pg/kg 8.0 0.35
06/08/07 1642 erusseil
06/08/07 1642 erussetl
06/08/07 1642 erussell
06/08107 1642 erussell
06/08/07 1642 erusst
06/08/07 1642 erussell
06108/07 1642 erusseH
06/08/07 1642 erussell
06/08/07 1642 erussejt
06/08/07 1642 orussetl
06/08/07 1642 erussell
06/08/07 1642 erussell
06/08/07 1642 erussell
06/08/07 1642 erussell
06/08/07 1642 erussell
06/08/07 1642 erusselt
06/08/07 1642 erusself
06/08/07 1642 erussell
06/08/07 1642 erusselt
06/08/07 1642 erussell
06/08/07 1642 erusselt
06/08/07 1642 erussetl
06/08107 1642 erusseli
06/08/07 1642 erussejl
06/08/07 1642 erussell
06/08/07 1642 erusselt
06/08/07 1642 erusseli
Page 12 of 45
NC Certification No.402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 06/18107
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 183633
Sample Matrix Soil COG Group G0607179
Time Coliected 06/06/07 1415
Time Submitted 06/06/07 1640
Chtorobenzene
Chlorcdibromomethane
Chioruethane
Chloroform
Chloromethane
cls-12-Dichloroethene
cls-1 3-Dlchloropropene
Dibromomethane
Dlchlorodlfluoromethane
Ethylbenzene
Hexachiorobutadlene
Isopropyl ether IPE
lsopropylbenzene
mp-Xylenes
Methyl ethyl ketone MEK
Methyl t-butyl ether MTBE
Methylene chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p-lsopropyltaluene
sec-Sutylbenzene
Styrene
tert-Butylbenzene
Tetrachioroethene
Toluene
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
SRI
BRL
BRL
BRL
BRL
BRL
BRL
RRL
BRL
BRL
BRL
BRL
BRL
BRL
826GB
826GB
826GB
826DB
826GB
826GB
626GB
826GB
826DB
826GB
826GB
826GB
826GB
8260B
826DB
826GB
826DB
826DB
826DB
826DB
826DB
826DB
826DB
826DB
826GB
826DB
826DB
Analysis Analyst
Date/Time
06108/07 1642 erussell
06/08/07 1642 enisselt
06/08107 1642 erussell
05/08/07 1642 erussejj
06/08107 1642 erussell
05/08/07 1642 erussell
06/08/07 1642 erusseli
06/08/07 1642 erussell
05/08/07 1642 erussall
06/08/07 1642 erusseli
08/08/07 1642 erussell
08/08/07 1642 erussell
06/08/07 1642 erusselt
06/08/07 1642 erussell
06/08/07 1642 erusseli
06/08/07 1642 erussell
06/08/07 1642 erusseff
0608/07 1642 erusselt
06/08/07 1642 erussell
05/08/07 1642 erussell
06/08/07 1642 erusselt
06/08/07 1642 enissell
06/08107 1642 erussett
06/06/07 1642 erussell
06/08/07 1642 erussell
06/08/07 1642 erussell
06/08/07 1642 erusseli
Batch
ID
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method
Limit Factor
jig/kg 6.0 0.45
pg/kg 6.0 0.40
pg/kg 12 0.49
pg/kg 6.0 0.44
jig/kg 12 0.42
pg/kg 6.0 0.26
pg/kg 6.0 038
pg/kg 6.0 0.44
pg/kg 12 1.3
pg/kg 6.0 0.42
pg/kg 18 0.74
pg/kg 6.0 0.20
pg/kg 12 0.48
pg/kg 12 0.83
pg/kg 24 1.7
jig/kg 6.0 0.35
pg/kg 12 0.49
jig/kg 18 0.48
jig/kg 12 0.36
jig/kg 6.0 0.89
jig/kg 6.0 0.36
pg/kg 18 0.49
pg/kg 18 0.39
pg/kg 6.0 0.60
jig/kg 24 0.37
pg/kg 12 1.0
pg/kg 6.0 040
Page 13 o145
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Sample Weight Determination
Weight Blsullate
Weight Blsulfate
Weight Methanol
ESP Associates PA
Atm Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
06118107
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
183633
G06071 79
06106/07 1415
06/06/07 1640
Parameter Result Units Report MDL Dilution Method
trans-i2-Dithloroethene
trans-i .3-Dichioropropene
Trichioroethene
Trichlorofluoromethane
Vinyl chloride
AnalystAnalysis Batch
Limit Factor Date/Time ID
6.0 0.45 826DB 06/08/07 1642 erussell Q24147
6.0 0.42 826DB 06108107 1642 erussell 024147
6.0 0.36 826DB 06/08/07 1642 erussell 024147
6.0 0.49 82608 06/08/07 1642 erusseU Q24147
12 0.76 82608 06/08107 1642 erussell 024147
SRI
BRL
BRL
BRL
BRL
5.08
4.86
4.29
Surrogate Recovery Control Limits
Bromotluorobenzene 106 77-128
Toluene-dB 101 81 128
Dlbromofluoromethane 95 67-143
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
Semi-volatile Organic Compounds by GC/MS
24-Trichkntbenzene BRL
2-DlchlorobØnzene BRL
.3-Dichlorobenzene BRL
4-Dlchlorobenzene BRL
245-Trichiorophenol BRL
246-Trlchlorophenol BRL
24-DkthIorophenol BRL
24-Dimethyiphenol ERL
24-Dinitrophenol BRL
24-Dinltrotoluene BRL
2.6-Dinitrotojuene BRL
2-Chloronaphthalerie BRL
5035
5035
5035
390 38 8270C
390 28 8270C
390 28 82700
390 35 8270C
390 39 82700
390 37 8270C
390 32 8270C
390 37 8270C
390 43 8270C
390 22 8270C
390 41 8270C
390 40 8270C
06/13/07 000
06/13/07 000
06/13/07 000
06/11/07 1209
06/11/07 1209
06/11/07 1209
06/11/07 1209
06/11/07 1209
06/11/07 1209
06111/07 1209
06/11/07 1209
06/11/07 1209
08/11/07 1209
06/11/07 1209
06/11/07 1209
Ibrown
brown
brown
kcarnpigotto
kcamplgotto
kcamplgolto
kcamplgotta
kcamplgctto
kcamplgotto
kcamplgoto
kcamplgotto
kcamplgotto
kcarnplgotto
kcamplgotto
kcamplgotto
024124
024124
024124
024124
024124
024124
Q24124
024124
024124
024124
024124
024124
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 26224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 14 of 45
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cart No 37735 06/18/07
Project ID Morehead Commons No Client Sample ID WS-2
PrIsm Sample ID 183633
Sample Matrix Soil COC Group G0607179
Time Collected 06106107 1415
Time Submitted 06106/07 1640
2-Chiorophenol
2-Methy1naphthaIene
2-MehlphenoI
2-Nitrophenol
34-Methylphenol
33-DlchIorobenldlne
46-Dlnitro-2-methylphenol
4Bromophenylphenylether
4-Chloro-3-methylphenol
4-Chiorophenyiphenylether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Arithracene
Benzoaanthracene
Benzoapyrene
Benzobfiuoranthene
Benzog.hjpenfiene
Benzokfiuoranthene
Bls2-chtoroethoxymethane
61s2-chloroethylether
Bls2-chlorolsopropylether
Bts2-ethylhexylphthatate
Butylbenzylphthalate
Chrysene
Di-n-butylphthatate
Di-n-octytphthaf ate
Analysis
Date/Time
06/11/07 1209 kcamplgotto
06/11/07 1209 kcamplgotto
06/11/07 1209 kcsmplgotto
06/11/07 1203 kcmp1gotto
06/11/07 1209 kcamptgotto
06/11/07 1209 kcamprgotLo
06/11/07 1209 kcamplgotto
06/11/07 1209 kcamptgotto
06/11/07 1209 kcsmplgcitto
06/11/07 1209 kamp1gotto
06/11/07 1209 kcarnplgotto
06/11/07 1209 kcampl9otlo
06/11/07 1209 kcamplgotlo
06/11/07 1209 kcampIgoo
06/11/07 1209 kcamplgorio
06/11/07 1209 kcamplgotto
06/11/07 1209 kcamplgotto
06/11/07 1209 kcamplgotto
08/11/07 1209 hcamplgotta
06/11/07 1209 kcampigotto
06/11/07 1209 kcamplgotto
06/11/07 1209 kcamplgottc
06/1107 1209 kcamplgotlo
06/11/07 1209 kcarnplgoflo
06/11/07 1209 kcamplgouo
06/11/07 1209 kcamplgotb
06/11/07 1209 kcamplgotto
Analyst Batch
ID
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
Q24124
024124
024124
024124
024124
024124
024124
Q24124
024124
024124
This report should not be reproduced except in its entirety withDut the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529.6364 Fax [phone]
F1 Ski An1UaI uvkanmnW Sulins
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 26241
Parameter Result Units Report MDL Dilution Method
Limit Factor
BRL pg/kg 390 30 8270C
BRL pg/kg 390 31 827CC
BRL pg/kg 390 36 827CC
BRL pg/kg 390 46 827CC
BRL pg/kg 390 39 827CC
BRL pg/kg 390 24 827CC
BRL pg/kg 390 23 827CC
BRL pg/kg 390 37 827CC
BRL pg/kg 390 28 827CC
BRL pg/kg 390 24 8270C
BRL pg/kg 390 26 827CC
BRL pg/kg 390 38 827CC
BRL pg/kg 390 38 827CC
BRL pg/kg 390 29 827CC
BRL pg/kg 390 54 827CC
BRL pg/kg 390 45 827CC
BRL pg/kg 390 17 827CC
BRL pg/kg 390 18 827CC
BRL pg/kg 390 31 827CC
BRL pg/kg 390 44 827CC
BRL pg/kg 390 42 827CC
BRI pg/kg 390 33 527CC
BRL pg/kg 390 19 827CC
BRL pg/kg 390 24 8270C
BRL pg/kg 390 64 827CC
BRL pg/kg 390 18 827CC
BRL pg/kg 390 29 827CC
Page 15 of 45
NC Certification No 402 Laboratory ReportSCCrtiIlcatlonNo99012
NC Drinking Water Cert No 37735 0618107
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 183633
Sample Matrix Soil COG Group G0607179
Time Collected 06/06/07 1415
Time Submitted 06/06/07 1640
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Spnngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Olbenzoahanthracene BRL pg/kg 390 39 821CC 06/11/07 1209 kcamplgotto 024124
Dlbenzofijran BRL pg/kg 390 33 827CC 06/11/07 1209 kcamplgotto 024124
DIethyphthalate BRL pg/kg 390 24 827CC 06/11107 1209 kcamplgotto 024124
Dlmethylphthalate BRL pg/kg 390 26 827CC 06/11/07 1209 kcampl9otto 024124
Fluoranthene BRL pg/kg 390 27 827CC 06/11/07 1209 kcamplgotto 024124
Fluorene BRL pg/kg 390 23 827CC 06/11/07 1209 kcamplgDtto 024124
1-lexachlcrobenzena BRL pg/kg 390 20 827CC 06/11/07 1209 kcamplgollo 024124
Flexachlorobutadlene BRL pg/kg 390 37 827CC 06/11/07 1209 kcampigotto 024124
1-lexachiorocyclopentadlene BRL pg/kg 390 41 827CC 06/11/07 1209 kcamplgotto 024124
Rexachioroethane BRL pg/kg 390 39 82706 06/11/07 1209 kcamptgotlo 024124
Indeno123-cdpyrene BRL pg/kg 390 40 82706 06/11/07 1209 kcamptgotto 024124
lsophorone BRL pg/kg 390 34 82706 06/11/07 1209 kcamplgotta 024124
N-Niti-osodl-n-propylamine BRL pg/kg 390 44 82706 06/11/07 1209 kcamplgotlo 024124
N-Nltrosodlpherylarnlne BRL pg/kg 390 20 82706 06/11/07 1209 kcamplgotto 024124
Naphthalene BRL pg/kg 390 42 82706 06/11/07 1209 kcampigolta 024124
Nitrobenzene BRL pg/kg 390 38 827CC 06111/07 1209 kcamplgatto 024124
Pentachlorophenol BRL pg/kg 390 32 827CC 08/11/07 1209 kcamplgolto 024124
Phenanthrene BRL pg/kg 390 19 827CC 06/11/07 1209 kcaniplgotto 024124
Phenol BRL pg/kg 390 42 827CC 06/11107 1209 kcamplgotto 024124
Pene BRL pg/kg 390 26 8270C 06/11/07 1209 kcamplgotto 024124
Page 160145
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
WS-2
183633
G06071 79
06106107 1415
06/06107 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Extractable Petroleum Hydrocarbons by GC-FID
Cl 1-C22 Arornatics BRL mg/kg
C19-C36 Allphatics BRL mg/kg
C9-C18 Atiphatics BRL mg/kg
Analysis Note for Cll-C22 Aromaties
Sample Preparation
Surrogate
1-Chloro-octadecane
2-Bromonaphthalene
2-Fluorobiphenyl
o-Terphenyl
Recovery
95
111
107
98
Control Limits
40-140
40-140
40-140
40-140
2.1 mg/kg
4.4 mg/kg
Sample Preparation
Volatile Petroleum Hydrocarbons by GC-PlD/FID
CS-CS Aliphatics BRL
Cg-C10 Aromatics BRL
0.29 0.017 60108
0.29 0.024 601DB
06111107 2113 mcampbell
06/11/07 2113 mcampbell
024176
024176
Full Srlc Anullkl En nmdut Zolullcn
NC Certification No 402
SC Certification No 99012
NC Drinking Water Ceit No 37735
Laboratory Report
06/18/07
Project 1D Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
Sample Preparation 29.7 mL 35508 06/06/07 700 dpope P16579
Surrogate Recovery Control Limits
2-Fluoroblphenyl 65 21 108
Terphenyl-d14 91 41 136
2-Fluorophenol 49 14-89
Nitrobenzene-d5 57 14 103
246-Tribromophenol 93 25 123
Phenol-d5 58 13-95
12 6.4 MADEP EPII 06/16/07 1123 grappaccloll 024301
12 l.5 MADEP EPH 06/16/07 1123 grappaccloll 024301
12 3.8 MADEP EPH 06/16/07 1123 grappaccloll 024301
Adjusted value
9.73 mL EPH 06/13/07 800 dpope P18614
Metals by ICP
ChromIum
Lead
2.02g 5OmL 30508 06/11/07 905 Jhoppel
mg/kg 5.8 1.1 MAIDEPVPf-f
mg/kg 5.8 0.035 MADEP VPH
This report should not be reproduced except in Its entIrety without the written consent Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
0612/07 2208 bwagner
06/12/07 2208 hwagner
P1 8560
024220
Q24220
Page 17 of 45
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Ceil No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Dateflime ID
BRL mg/kg 5.8 1.8 MADEP VPH 06/12/07 2208 hwagner
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
Two surrogate recoveries were outside of the control limits No target compounds were detectedinthissampleNofurtheractionwastaken
Sample Weight Determination
Weight
Welght2
Sample Comments
BRL Below Reprtlng Uniit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet stale certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on diy-welght basis
Angela Overcash V.P Laboratory Services
misreport should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 CharIotte NC 28224-0543
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
183633
G0607179
06/06/07 1415
06/06/07 1640
C9.C1 Allphatics Q24220
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 183 70-130
25-Dlbrornotoluene.plD 138 70-130
23.18
23.97
MADEP VPH 05/13/07 000 brown
MADEP VPH 06/13/07 000 thrown
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 18 of 45
F...3Q1v1c0 A.............nvIriirnutI Sdijllwi
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Percent Solids Determination
Percent Solids
Organochiorine Pesticides liv Gas Chromatoctraphy
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6354 Fax [phone]
Laboratory Report
06118107
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 183634
Sample Matrix Soil COG Group G0607179
Time Collected 06/0607 1430
Time Submitted 06/06/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
82.9 5M2540 06/11/07 1700 Ibrown
44-DDD BRL pglkg 2.4 0.74 8081A 06/14/07 032 Jvcgel 024275
44-DDE BRI pg/kg 2.4 0.51 BOBIA 05/14/07 032 Ivogel 0.24275
44-DDT BRL pg/kg 2.4 0.87 BOS1A 06/1407 032 Ivogel 024275
44-Methoxycthlor BRL pg/kg 4.8 1.6 8081A 06/1407 032 Ivogel 024275
a-BHC BRL pg/kg 2.4 0.22 8081A 06/14/07 032 Jvogel 024275
a-Chlordane BRL pg/kg 2.4 0.42 8081A 06/14107 032 ivogel 024275
Aidrin BRL pg/kg 2.4 0.48 BOS1A 06/14107 032 Jvogel 024275
b-BHC BRL pg/kg 2.4 0.61 BDBIA 06/1407 032 JvogeI 024275
Chlordane BRL pg/kg 60 14 BOBIA 05/14/07 032 ivogel 0.24275
d-BHC BRL pg/kg 2.4 0.34 8081A 06/14/07 032 Jvogel 024275
Dicldrin BRL pg/kg 1.2 0.50 SOfiA 06/14/07 032 ivogel 024275
Endosullan BRL pg/kg 2.4 0.43 8081A 0614/07 032 Jvogel 024215
Endosullan ii BRL pg/kg 2.4 0.54 8081A 06/14/07 032 Jvo9eI 024275
Endosulfan Sulfate BRL pg/kg 2.4 0.63 8081A 06114107 032 Ivogel 024275
Endrin BRL pg/kg 2.4 0.72 8081A 06/14/07 032 Jvogel 024275
Endrin Aldehyde BRL pg/kg 2.4 0.65 SOfIA 06/14/07 032 Jvogel 024275
Endrin Ketone BRL pg/kg 2.4 0.48 8081A 06/14/07 032 JvogeI 024275
gBHC BRL pg/kg 2.4 0.25 8081A 06/14/07 032 Ivogel 0.24275
g-Chlordane BRL pg/kg 2.4 0.39 BOB1A 06/14/07 032 Jvogel 024275
Heptachior RRL lJ/kg 2.4 0.57 8081A 06/14107 032 Jvogel 024275
HeptabhlorEpoxide BRL pg/kg 2.4 0.44 8081A 06/14/07 032 Ivogel 024275
Toxaphene BRL pg/kg 60 14 8081A 06/14/07 032 Jvoel 024275
Page 19 of 45
iI $i.vI AIytkI Encnmnb1tjIizUan
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-3
183634
G0607179
06/06/07 1430
06/06/07 1640
Volatile Orqanic Compounds by GCMS
11 12-Tetrachloraethane
ljj-Trichioroethane
ii 22-Tetrachloroethane
12-Trlchloroethane
11-Dkhloroethane
11-Dichloroethene
11-Dichloropropene
123-Trichlorobenzene
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 26224-0543
Phone [phone] Toll Free Number 1-800/529.6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
29.1 10 mL 35506 06/12/07 1000 dpope P18598SamplePreparation
Polychiorinated Biphenyls PCBs by GC-ECD
PCB-1015 BRL
PCB-1221 BRL
PCB-1232 BRL
PCB-1 242 BRL
PCB-1 248 BRL
PCB-1254 BRL
PCB-1260 BRL
Sample Preparation
Surrogate Recovery Control Limits
Tetrachloro-m-xylene TCMX 105 40 162
Decachlorobiphenyl 0GB 143 26 204
0.060
0.12
0.060
0.060
0.060
0.060
0.060
0.011
0.049
0.019
0.021
0.0083
0.021
0.016
8082
8082
8082
8052
8082
8082
8082
06/14/07 032
0614/07 032
06/14/07 032
06/14/07 032
06/14/07 032
06/14/07 032
06/14/07 032
JvogeI
JvogaI
Jvogei
jvcget
jvogel
Ivogel
Jvogel
Q24276
024276
024276
024276
024276
024276
024276
P1859729.7 10 mL 355DB 06/12/07 1000 dpope
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
Surrogate Recovery Control Limits
Decachiorobiphenyl DCB 105 34-182
Tetrachloro-m-xylene TCMX 103 36 182
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
6.1 0.60
6.1 0.34
6.1 8.63
6.1 0.35
6.1 0.44
6.1 0.47
6.1 0.54
12 0.67
826DB
826DB
82608
82608
82608
82608
82608
82608
06/08/07 1714 enmseil
06/08/07 1714 erusseil
06/0807 1714 erusseH
06/08/07 1714 erussell
06/08/07 1714 enissell
06/0807 1714 erussell
06/08/07 1714 enisseJi
0608/07 1714 enisseli
024147
024147
024147
024147
024147
024147
024147
024147
Page 20 of 45
F.. .irvu ntàI $hjthrna
ESP Associates PA
Attn Chris Ward
Box 7030
CharloUe NC 28241
This report should not be reproduced except In its enfirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Tall Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water CerL No 37735
Laboratory Report
0618107
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 183634
Sample Matrix Soil COC Group 00607179
Time Collected 06/06/07 1430
Time Submitted 06/06/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/lime ID
123-Trithloropropane BRL pg/kg 6.1 0.54 82606 06/08/07 1714 erussell 024147
124-Trichioroberizene BRL pg/kg 12 0.59 82608 06/08/07 1714 erusset 024147
124-Trimethylbenzene BRL pg/kg 12 0.47 82608 06/09/07 1714 erussell 024147
12-Dlbromo-3-chloropropane BRI pg/kg 6.1 0.97 82608 06/08/07 1714 eruaseil 024147
12-Dibromoethane EDO BRL pg/kg 6.1 0.11 826GB 06/08/07 1714 erussell 024147
12-Dlchlorobonzerie BRL pg/kg 12 0.33 826GB 06/08/07 1714 erussell 024147
12-Dlchloroethane BRL pg/kg 5.1 061 82608 06/08/07 1714 erussell 024147
1.2-Dichioropropane BRL pg/kg 6.1 0.45 8260B 06/08/07 1714 erussell 024147
135-Trimethylbenzene ORL pg/kg 12 0.51 82608 05/08/07 1714 enissell 024147
1.3-Dichlorobenzene BRL pglkg 12 0.53 82608 05/08/07 1714 enissell 024147
13-Dichloroprupane BRL pg/kg 6.1 0.42 82606 06108/07 1714 emssell 024147
14-Dichlorobenzene BRL pg/kg 12 0.48 82608 06/08/07 1714 arussell 024147
22-Dichioropropane BRL pg/kg 6.1 0.31 82608 06/08/07 1714 enissell 024147
2-Chloroethyl vinyl ether BRL pg/kg 12 0.45 82608 06/08/07 1714 enissell 024147
2-Chlorotoluene BRL pg/kg 12 0.45 826GB 06/08/07 1714 erussell 024147
2-Hexanone BRL pg/kg 61 0.64 82608 06/08/07 1714 erussell 024147
4-Chiorotoluene BRL pg/kg 12 0.32 82606 06/08/07 1714 enrnset 024147
4-Methyl-2-pentanoneMIBK BRL pg/kg 12 0.61 826GB 06/0B/07 1714 erussell 024147
Acetone BRL pg/kg 25 2.4 826GB 06/08/07 1714 erussell 024147
Benzene BRL pg/kg 3.7 0.49 826GB 06/08/07 1714 enissetl 024147
Bromobenzene BRL pg/kg 6.1 0.43 82608 06/08/07 1714 erussetl 024147
Bromochioramethane BRL pg/kg 6.1 0.37 826DB 06/08/07 1714 enisseil 024147
Bromodlahloromethane BRL pg/kg 6.1 0.54 826DB 06/08/07 1714 erussell 024147
Bromoform BRL pg/kg 6.1 045 82608 06/08/07 1714 crusseti 024147
Bromometharie BRL pg/kg 12 0.71 82608 06/0807 1714 enisseU 024147
Carbon disulfide BRL pg/kg 12 0.39 82608 08/08107 1714 erussett 024147
Carbon tetractiloride BRL pg/kg 61 0.36 826DB 06/08/07 1714 erussetl 024147
Page 21 of 45
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 183634
Sample Matrix Soil COG Group G0607179
Time Collected 06/06/07 1430
Time Submitted 06/06/07 1640
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 CharIatte NC 282240543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Waler Cert No 37735
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
6.1ChlorobenzeneBRLpg/kg 0.47 8260B 06108107 1714 eruselI Q24147
Chiorodibromomethane BRL pg/kg 8.1 0.42 826DB 06/08/07 1714 enJssell 024147
Chioroethane BRL pg/kg 12 0.50 8260B 06/08/07 1714 erussell 024147
Chloroform BRL pg/kg 6.1 0.45 826DB 06/08/07 1714 erussell 024147
Chloromethane BRL pg/kg 12 0.43 82608 06/08/07 1714 erussell 024147
cls-1.2-Dlchlcroethene BRL pg/kg 6.1 0.27 825DB 06/08/07 1714 erussell 024147
cls-13-Dlchlcropropene BRL pg/kg 5.1 0.39 82608 06/08/07 1714 erussell 024147
Dlbromomethane BRL pg/kg 6.1 0.45 82608 06108/07 1714 arussetl 024147
Dlchlorodifluoromethaae BRL pg/kg 12 1.4 826DB 06/08/07 1714 erussell 024147
Ethylbenzene BRL pg/kg 6.1 0.43 8260B 06/08/07 1714 erusset 024147
Hexachlorobutadlene BRL pg/kg 18 0.76 826GB 06/08/07 1714 erussell 024147
IsopropyletherIPE BRL pg/kg 6.1 0.21 826GB 06/08/07 1714 erussell 024147
lsopropylbenzene BRL pg/kg 12 0.49 82608 06/08/07 1714 enissell 024147
mp-Xylenes BRL pg/kg 12 0.86 826GB 06/08/07 1714 enisset 024147
Methyl ethyl ketoneMEK BRL pg/kg 25 1.7 826GB 06/08/07 1714 ezussI 024147
Methyl t-butyt ether MTBE BRL pg/kg 6.1 0.36 82608 06/08/07 1714 erussell 024147
Methylene chloride BRL pg/kg 12 0.50 826GB 06/08/07 1714 euse1I 024147
n-Butylbenzene BRL pg/kg 18 0.49 82608 06/08/07 1714 erussell 024147
n-Prapylbenzene BRL pg/kg 12 0.37 826GB 06/08/07 1714 erussetl 024147
Naphthalene BRL pg/kg 5.1 0.71 8260B 06/08/07 1714 erussell 024147
oXylene BRL pg/kg 6.1 0.37 826GB 06/08/07 1714 enissell 024147
p-Isopropyltoluene BRL pg/kg 18 0.50 826DB 06/08/07 1714 erussell Q24147
sec-Butylberizene BRL pg/kg 18 0.40 826DB 06/08/07 1714 erussell 024147
Styrene BRL pg/kg 6.1 0.61 826DB 06/08/07 1714 enissell 024147
tert-Butylbenzene BRL pg/kg 25 0.38 82608 06/08/07 1714 enissell 024147
Tetrachioroethene BRL pg/kg 12 1.1 82608 06/08/07 1714 erussell 024147
Toluene BRL pg/kg 8.1 0.42 826GB 06/08/07 1714 ewssell 024147
Page 22 of 45
Laboratory Report
06/18107
Project ID Morehead Commons No Client Sample ID WS3
Prism Sample ID 183634
Sample Matrix Soil ccc Group G0607179
Time Collected 06/06/07 1430
Time Submitted 06106107 1640
trans-i .2-Dichloroethene
trans-i .3-Dichioropropene
TrlchloroØthene
Trichlorofluoromethane
Vinyl chloride
826DB
82608
826DB
826DB
626DB
5035
5035
5035
06/08/07 1714 erussell
06/08107 1714 erussell
06/08107 1714 erussell
06/08/07 1714 enissell
06/06/07 1714 enissell
06/13/07 000 Ibrown
05/13107 000 brown
05/13/07 000 Ibrown
024147
024147
024147
024147
024147
Semi-volatile Organic Compounds by GC/MS
124.TrIchlorobenzene BRL jig/kg 400 39 82700 06/11/07 1300 kcamplgotto 024124
12-Dlchlorobenzene BRL pg/kg 400 29 82700 00/11/07 1300 kcamplgotto 024124
3-Dlchlorobenzene BRL pg/kg 400 29 82700 06/11/07 1300 kcamplgotto 024124
14-Dlchlorobenzene BRL pg/kg 400 36 62700 06/11/07 1300 kcamplgotto 024124
245-Trichlorophenol BRL pg/kg 400 41 82700 06/11/07 1300 kcampfgotto 024124
246-Trlchlorophenol BRL pg/kg 400 38 82700 08/11/07 1300 kcamplgouo 024124
24-Dichiorophonol BRL pg/kg 400 33 8270C 08/11/07 1300 kcamplgotlo 024124
24-Dimethyiphonol BRL pg/kg 400 38 82700 06/11/07 1300 kcamplgotto 024124
24-Dinitrophenol BRL pg/kg 400 45 6270C 06/11/07 1300 Iccamplgotto Q24124
24-Dinitrotoluene ERL pg/kg 400 23 82700 06/11/07 1300 kcamplgotto 024124
26-Dinitrotoluene BRL pg/kg 400 42 82700 06/11/07 1300 kcamplgotto 024124
2-Chlororiaphthalene RRL pg/kg 400 41 82700 06/11/07 1300 kcampgotb 024124
This report should net be reproduced except In its entirety without the written consent or Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 23 of 45
NC Certification No 402
SC Certification No 990i
NC Drinking Water Cert No 37735
ESP Associates PA
Atm Chris Ward
Box 7030
Charlotte MC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
BRL pg/kg 6.1 0.47
BRL pg/kg 6.1 0.43
BRL pg/kg 6.1 0.37
BRL pg/kg 6.1 0.50
BRL pg/kg 12 0.78
Surrogate
Sample Weight Determination
Weight Blsulfate
Weight Bisulfate
Weight Methanol
Recovery Control Limits
Bromofluorobenzene 103 77 128
Toluene-d8 97 81 128
Dibromofluoromeihane g2 67 -143
5.13
492
4.91
Fill Sw Miali1ll EnvnmrtISip
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRI
BRL
BRL
BRL
pg/kg 400 31
pg/kg 400 32
pg/kg 400 37
pg/kg 400 48
pg/kg 400 41
pg/kg 400 25
pg/kg 400 24
pg/kg 400 38
pg/kg 400 29
pg/kg 400 25
pg/kg 400 26
pg/kg 400 39
pg/kg 400 40
pg/kg 400 30
pg/kg 400 58
pg/kg 400 46
pg/kg 400 18
pg/kg 400 19
pg/kg 400 32
pg/kg 400 46
pg/kg 400 43
pg/kg 400 34
pg/kg 400 20
pg/kg 400 24
pg/kg 400 66
pg/kg 400 18
pg/kg 400 30
82700
8270C
82700
82700
8270C
82700
8270C
8270C
82700
8270C
82700
82700
82700
82700
8270C
8270C
8270C
8270C
82700
8270C
82700
82700
82700
82700
82700
82700
82700
06/11/07 1300 kamp1gollo 024124
06/11/07 1300 kcamplgotto 024124
06/11/07 1300 kcampgotc 024124
06/11/07 1300 kcamplgolto 024124
06/11/07 1300 kcamplgotto 024124
06/11/07 1300 kcampigotto 024124
06/11/07 1300 kcampigotlo 024124
06/11/07 1300 kcampigouo 024124
06/11/07 1300 kcampigolio 024124
06/11/07 1300 kcamplgotb 024124
0611/07 1300 kcamplgotto 024124
06/11/07 1300 kcampigotio 024124
06/11/07 1300 kcamplgotto 024124
06/11/07 1300 kcarnplgotto 024124
06/11/07 1300 kcmpigotto 024124
06/11/07 1300 kcamplgotto 024124
06/11/07 1300 kcampigauo 024124
06/11/07 1300 kcamplgotto 024124
06/11/07 1300 kcamplgouo 024124
06/11/07 1300 kcampl9otto 024124
06/11/07 1300 kcamplollo 024124
06/11/07 1300 kcamplgotto 024124
06/11/07 1300 kcamplgottQ Q24124
06/11/07 1300 kcamplgolto 024124
06/11/07 1300 kcampigotio 024124
06/11/07 1300 kcamplgotto 024124
06/11/07 1300 kcamplgotiu 024124
This report should not be reproducecJ except in Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-B00I529-6364 Fax [phone]
NO Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 183634
Sample Matrix Soil COC Group G0607179
Time Collected 06/06/07 1430
Time Submitted 06/06/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/TIme ID
2-Chlorophenol
2-Methylnaphthalene
2-Methyiphenol
2-Nitrophenol
34-Mathyiphenoi
33-Dichlorobenzidine
46-Dlnltro-2-methylphenol
4-Bromophenyiphenylether
4-Chloro-3-methylphenol
4-Chiorophenyiphenylether
4-Nltrophenai
Acenaphthene
Acenaphthylene
Anthracene
Benzoaanthracene
Benzoapyrene
Benzobfluoranlhene
Benzoghjperylene
Benzokfluoranthene
BIs2-chloroethoxymethane
Bls2-chloroethylother
Bls2-chloroisopropylether
BIs2-ethylhexyiphthalate
Butylbenzylphthalata
Chrysene
Dl-n-butyiphthalate
Di-n-octylphthalate
Page 24 of 45
Laboratory Report
06/18/07
WS-3
183634
G06071 79
06/06/07 1430
06/06107 1640
This report should not be reproduced1 except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte1 NC 28224-0543
Phone [phone] Toll Free Number 1-8001529.8384 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Fufl5eAnIyUcI
ESP Associates PA
Attn ChrIs Ward
Box 7030
Charlotte MC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
Dibenzoahanthracene BRL pg/kg 400 40 8270C 06/11/07 1300 kcampigolto 024124
DibenzofUran BRL pg/kg 400 34 8270C 06/11/07 1300 kcamplgotto 024124
Diethylphthaiate BRL pg/kg 400 24 8270C 06/11/07 1300 kcampigotto 024124
Dlmethylphthalate BRL pg/kg 400 27 8270C 06/11/07 1300 kcampfgoUo 024124
Fluoranthena BRL pg/kg 400 27 8270C 06/11/07 1300 kcampigoUo 024124
Fluorene BRL pg/kg 400 24 827CC 06/11/07 1300 kcampigotto 024124
Hexachlorobenzene BRL pg/kg 400 21 8270G 06/11/07 1300 kcamplgotto 024124
Hexachiorobutadicrie BRL pg/kg 400 39 827CC 06/11/07 1300 kcarnpigouo 024124
Hexachlomoyclopentacliene BRL jig/kg 400 42 8270C 06/11/07 1300 kcamplgotlo 024124
Hexachloroethane BRL pg/kg 400 40 8270C 00/11/07 1300 hcampigotlo 024124
lndeno123-cdpyrene BRL jig/kg 400 41 827CC 06/11/07 1300 kcampigotto 024124
lsophorone BRL pg/kg 400 36 8270C 06/11/07 1300 kcamplgotto Q24124
N-Nitrosodl-n-propyiamine BRL jig/kg 400 45 8270C 06/11/07 1300 kcampigotio 024124
N-Nitrosodiphenylamine BRL pg/kg 400 20 827CC 06/11107 1300 kcamplgoun 024124
Naphthalene BRL pg/kg 400 43 827CC 06/11/07 1300 kcamplgotto 024124
Nitrobenzene BRL jig/kg 400 39 827CC 06/11/07 1300 kcamplgotlo 024124
Pentachlorophenol BRL pg/kg 400 33 827CC 06/11/07 1300 kcamptgotto 024124
Phenanthrene BRL jig/kg 400 19 8270C 0611/07 1300 kcamplgolto 024124
Phenol BRL pg/kg 400 43 827CC 06/11/07 1300 kcamplgotto 024124
Pyrene BRL pg/kg 400 27 827CC 06/11/07 1300 kcamplgotto 024124
Page 25 of 45
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time II
Extractable Petroleum Hydrocarbons by GC-FID
C11-C22 Aromatics BRL mg/kg
C19-C36 Aliphatics BRL mg/kg
C9-C1 Aliphatics BRL mglkg
Analysis Note for C11-C22 Aromnatics
Sample Preparation
Metals by ICP
Chromium
Lead
Sample Preparation
Volatile Petroleum Hydrocarbons by GC-PID/FID
CS-Ca Aliphatics BRL
C9-C10 Aromätlcs BRL
Adjusted value
9.55 mL EPH 06113/07 800 dpope
Laboratory Report
06/18/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-3
Attn Chris Ward Prism Sample ID 183634
Box 7030
Sample Matrix SOB COC Group G0607179
Charlotte NC 28241 Time Collected 06/06/07 1430
Time Submitted 06106/07 1640
Sample Preparation 30.03 mL 35506 06/0607 700 dpope P18579
Surrogate Recovery Control Limits
Terphenyl-d14 88 41 136
246-Tribromophenol 86 25-123
Phenol-d5 65 13-95
2-Fluomphenol 63 14 89
2-Fiucroblphenyl 75 21 108
Nitrobenzene-d5 69 14-103
13 6.8 MADEP EPH 06/17/07 950 grappaccloli 024301
13 1.9 MADEP EPI-I 06117/07 950 grappaccloll 024301
13 4.0 MADEP EPH 06/17/07 950 grappacctoll 024301
P18614
Surrogate Recovery Control Limits
1-Chloro-octadecane 138 40 140
2-Fluoroblphenyl 128 40-140
o-Terphenyl 114 40-140
2-Bromonaphthalene 132 40-140
0.81 mg/kg
5.7 mg/kg
0.29 0.018
0.29 0.025
60106
601DB
2.05g SOmL
06/11/07 2121 mcampbelt
06/11/07 2121 mcampbelt
mg/kg
mg/kg
024176
024176
6.0 1.2
6.0 0.036
30506 0811/07 905 Jhoppei P18580
MADEP VPH 0612/07 2249 hwagnnr 024220
MADEP VPH 06/12/07 2249 hwagner 024220
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240843 Charlotte NC 28224-0543
Phone [phone] Toll Free Numbec 1-800/529-6364 Fax [phone] Page 26 of 45
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
C9-Gl2Allphatics BRL mg/kg 6.0 t9 MADEP VPII 06/12/07 2249 hwagner 024220
Pnalysis Note for C5-C8 Aliphatics Adjusted value
inalysis Note for C9-C12 Aliphatics Adjusted value
One surrogate recovery
was outside the control limits No target compounds were detected inthissampleNofurtheractionwastaken
Surrogate Recovery Control Limits
25-Dlbromotoluene-FID 165 70 130
25Dibromotoluene-PID 129 70 130
Sample Weight Determination
Weight 20.39 MADEP VPH 06/13/07 000 ibrown
Weight 21.94 MADEP VPH 06/13/07 000 brown
Sample Comments
RL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced1 except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte1 NC 28224-0543
Laboratory Report
06/18/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-3
Attn Chris Ward Prism Sample ID 183634
P.O Box 7030 Sample Matrix Soil COG Group G0607179
Charlotte NC 28241 Time Collected 06/06/07 1430
Time Submitted 06/06/07 1640
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 27 ot45
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 183635
Sample Matrix Soil coc Gup G0607179
Time Collected 06/06107 1445
Time Submitted 06/06/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Percent Solids Determination
86.5 SM2540 06/11/07 1700 brown
gnochiorjne Pesticides by Gas Chromatography
44LDDO
44-DDE
44-DOT
4.4-Methoxychlor
aBHC
a-Chlordane
Aidrin
b-BHC
Chlordane
d-BHC
Dleldrln
Endosulfan
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin Aldehyde
Endrin Ketone
g-BlIC
g-Chlordane
1-leptachlor
Heptachlor Epoxide
Toxaphene
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number l-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
06/18/07
Percent Solids
BRL pg/kg 2.3 0.71 8081A 06/14/07 114 Jvogel 024275
BRL pg/kg 2.3 0.49 8081A 06/14/07 114 Jvogel 024275
BRL pg/kg 2.3 0.83 8081A 06/14/07 114 Jvogel 024275
BRL pg/kg 4.6 1.6 BOB1A 06/14/07 114 Jvogel 024275
BRL pg/kg 2.3 0.21 BOR1A 06/14/07 114 Jvogel 024275
BRL pg/kg 2.3 0.40 8081A 06/14/07 114 Jvogel 024275
BRL pg/kg 2.3 0.46 8081A 06/14/07 114 JvogeI 024275
BRL pg/kg 2.3 0.58 BOB1A 06/14/07 114 Ivogel 024275
BRL pg/kg 58 13 8081A 06/14/07 114 jvogel 024275
BRL pg/kg 2.3 0.33 8081A 06/14/07 114 jvogel 024275
BRL pg/kg 1.2 0.48 BOBIA 06/14/07 114 Ivogel 024275
BRL pg/kg 2.3 0.41 8081A 06/14/07 114 Jvogel 024275
BRL pg/kg 2.3 0.52 8081A 06/14/07 114 Jvogel 024275
BRL pg/kg 2.3 0.60 8081A 06/14/07 114 Jvogel Q24275
BRL pg/kg 2.3 0.69 BOB1A 06/14/07 114 Jvngal 024275
BRL pg/kg 2.3 065 8081A 06/14/07 114 Jvogel 024275
BRL pg/kg 2.3 0.46 OOBIA 06/14/07 114 ivogel 024275
BRL pg/kg 2.3 0.27 BOBIA 06/14/07 114 ivogel 024275
BRL pg/kg 2.3 0.38 8081A 06/14/07 114 Jvogel 024275
URL pg/kg 2.3 0.55 80IA 06/14/07 114 Jvogel 024275
BRL pg/kg 2.3 0.43 8081A 0814/07 114 Jvogel 024275
BRL pg/kg 58 13 BOO1A 06/14/07 114 Jvogel 024275
Pge 28 of 45
NC Certification No 402 Laboratory ReportSCCertificationNo99012
if NC Drinking Water Cert No 37735 0618/07
Fu Swk.AwIyIJcI EiiwumntI Saruucri
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-4
Attn Chris Ward PrIsm Sample ID 183635
Box 7030 Sample Matrix Soil GOC Group G0607179
Charlotte NC 28241 Time Collected 06/06/07 1445
Time Submitted 06/06/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample PreparatIon 29.55 10 mL 355GB 06/12/07 1000 dpope P18598
Surrogate Recovery Control Limits
Decachiorobiphenyl DCB 124 26-204
Tetrathloro-m-xylene TCMX 109 40-162
Polychiorinated Biphenyls 1PCBs by GC-ECD
PCB-1016 BRL mg/kg 0.058 0.011 8082 06/14/07 114 JvoeI 024276
PCB-1221 BRL mg/kg 0.12 0.047 8082 06/14/07 114 Ivogel 024276
FCB-1232 BRL mg/kg 0.058 0.018 8082 0614/07 114 Jvoet 024276
PCB-1242 BRL mg/kg 0.058 0.020 8082 06/14/07 114 Jvogsl 024276
PCB-1248 BRL mg/kg 0.058 0.0080 8082 06/14/07 114 ivD951 024276
PCB-1254 BRL mg/kg 0.058 0.020 8052 0614/07 114 JvoeI 024276
PCB-1260 BRL mg/kg 0.058 0.015 6082 06/14/07 114 jvogel 024276
Sample Preparation 29.55 10 mL 355GB 06/12/07 1000 dpope P18597
Surrogate Recovery Control Limits
Decachiorobiphenyl DCB 90 34-182
Tetrachloro-m-xylene TCMX 98 36-182
Volatile Organic Compounds by GCIMS
1112-Tetrachloroethane BRL pg/kg 6.7 0.66 826GB 06/08/07 1747 erussell 024147
111-Trichioroethane BRL pg/kg 6.7 0.38 826DB 06/08/07 1747 erussell 024147
1122-Tetrachloroethane BRL pg/kg 6.7 0.69 82805 06/08/07 1747 erussell 024147
112-Trtchloroethane BRL pg/kg 6.7 0.42 82606 06/08/07 1747 erussell 024147
11-Dichioroethane BRL pg/kg 6.7 0.49 826GB 06/08/07 1747 enissetl 024147
11-Dichloroetheno BRL pg/kg 6.7 0.51 826GB 06/08/07 1747 erusseti 024147
11-Dlchloropropene BRL pg/kg 5.7 0.59 82608 08/08/07 1747 erussell 024147
123-Trlchlorobenzene BRL pg/kg 13 0.74 826DB 06/08/07 1747 enissell 024147
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page 29 oM5
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 06/18/07
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 183635
Sample Matrix Soil COC Group G0607179
Time Collected 06/06/07 1445
Time Submitted 06/06/07 1640
This report should not be reproduced except lii its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toil Free Number 1400/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Limit Factor Datelflme ID
Batch
323-Trlchloropropane BRL pg/kg 6.7 0.59 826DB 06/08/07 1747 erussell 024147
124-Trichlorobenzene BRL pg/kg 13 0.65 82608 06108/07 1747 erussell 024147
124-Trimethylbenzene BRL pg/kg 13 0.51 826DB 06/0807 1747 erusseU 024147
12-Dlbrorno-3-chloropropane BRL pg/kg 6.7 1.1 826DB 0608/07 1747
erussell 024147
12-DlbromoethaneEDB BRL pg/kg 6.7 0.12 826DB 06/08/07 1747 erusseO 024147
12-Dlchlorobenzene BRL pg/kg 13 0.36 826DB 06/08/07 1747 erussell 024147
12-Dichloroethane BRL pg/kg 6.7 0.57 826DB 06108/07 1747 erussell 024147
12-Dichloropropane BRL pg/kg 6.7 0.50 826DB 06/08/07 1747 erussell 024147
t35-Trimethylbenzene BRL pg/kg 13 0.57 826DB 06/08/07 1747 erussell 024147
13-Dichlorobenzene BRL pg/kg 13 0.58 826DB 06/08/07 1747 erusset 024147
13-Dichioropropane BRL pg/kg 6.7 0.46 82608 060807 1747 erussell 024147
14-Dlchlorobenzerie BRL pg/kg 13 0.53 826DB 06108/07 1747 eru5sell 024147
22-Dichioropropane BRL pg/kg 6.7 0.34 826DB 06/08/07 1747 erusselt 024147
2-Chioroethyl vinyl ether BRL pg/kg 13 0.50 826DB 0610807 1747 erussell 024147
2-Chiorotoluene BRL pg/kg 13 0.50 826DB 0610807 1747 erusseli 024147
2-Hexanone BRI pg/kg 67 0.70 8260B 06/08/07 1747 erussell 024147
4-Chlorotoluene BRL pg/kg 13 0.35 82608 06/08/07 1747 erussell 024147
4-Methyl-2-pentanone MIBK BRL pg/kg 13 0.67 626DB 06/0807 1747
erussolt 024147
Acetone BRL pg/kg 27 26 826DB 06/08/07 1747 erusselt 024147
Benzeno BRL pg/kg 4.0 0.54 826DB 0608/07 1747 enissell 024147
Bromobenzene BRL pg/kg 6.7 0.47 826DB 06/08/07 1747 erussell 024147
Bromochioromethane BRL pg/kg 6.7 0.40 82608 06/08/07 1747 erussefl 024147
Bromodithioromethane BRL pg/kg 6.7 0.59 826DB 05/08/07 1747 erussell 024147
Bromoform BRL pg/kg 6.7 0.50 82608 06/08/07 1747 erussell Q24147
Brornomethane BRL pg/kg 13 0.78 82608 06/08/07 1747 ezussell 024147
Carbon dlsulfide BRL pg/kg 13 0.43 8260B 06/08107 1747 eiusselt Q24147
Carbon tetrachloride BRL pg/kg 6.7 0.39 826DB 00/08/07 1747 enjssell 024147
Page 30 of 45
NC Cettlficatlon No 402
SC Certification No 90012 Laboratory Report
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 183635
Sample Matrix Soil COC Group G0607179
Time Collected 06106/07 1445
Time Submitted 06/06/07 1640
Chlorobenzene
Chiorodibromomathane
Chloroethane
Chloroform
Chioromethane
cis-1 2-Dlchloroethene
cls-1 3-Dlchloropropene
Dibromomethane
Dichiorodifluoromethane
Ethylbenzene
Hexachiorobutadlene
Isopropyl ether IPE
tsopropytbenzene
mp-Xylenes
Methyl ethyl ketone MEK
Methyl t-butyl ether MTBE
Mothylene chloride
n-Butylbenzene
n-Propylbenzene
Naphthalone
o-Xylene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrathlcroethene
Toluene
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ORL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
826DB
826DB
826DB
82608
826DB
826DB
826DB
826DB
82508
826DB
82608
826DB
826DB
826DB
82608
826DB
82608
826DB
826DB
82608
82600
626GB
826GB
826DB
826DB
8260B
82608
06/08/07 1747 erussell
06/08/07 1747 erussetl
06/08/07 1747 erussell
06/08/07 1747 enissell
06/08/07 1747 erussell
06/08/07 1747 erusselt
06/08/07 1747 enissell
06/08/07 1747 erusselt
06/08/07 1747 enissell
06/08/07 1747 eiussell
06/0801 1747 erussell
06/08/07 1747 erussell
06/08/07 1747 erussell
06/08/07 1747 enisseli
06/08/07 1741 erussell
06/08/07 1747 erusseU
06/08/07 1747 erussell
06/08/07 1747 erussell
06/08/07 1747 erussell
06/08/07 1747 enissell
06/08/07 1747 erussell
06/08/07 1747 erusselt
06/08/07 1747 erussell
06/08/07 1747 erussell
06/08/07 1747 elussell
06/08/07 1747 erussell
06/06/07 1747 erussell
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
Q24147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
Q24147
024147
024147
024147
024147
This report should riot be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Full SpMc AnulyUl munlul SdutiunE
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
0618/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
pg/kg 6.7 0.51
pg/kg 5.7 0.46
pg/kg 13 0.55
pg/kg 6.7 0.50
pg/kg 13 0.47
pg/kg 6.7 0.30
pg/kg 6.7 0.43
pg/kg 6.7 0.50
pg/kg 13 1.5
pg/kg 6.7 0.47
pg/kg 20 0.84
pg/kg 6.7 0.23
pg/kg 13 0.54
pg/kg 13 0.94
pg/kg 27 1.9
pg/kg 6.7 0.39
pg/kg 13 0.55
pg/kg 20 0.54
pg/kg 13 0.40
pg/kg 6.7 0.78
pg/kg 6.7 0.40
pg/kg 20 055
pg/kg 20 0.44
pg/kg 6.7 0.67
pg/kg 27 0.42
pg/kg 13 1.2
pg/kg 6.7 0.46
Page 31 of 45
wInmunt SoUiIoM
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Sample Weight Determination
Weight Bisullate
Weight Bisulfate
Weight Methanol
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18107
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 183635
Sample Matrix Soil coc Group 00607179
Time Collected 06/06/07 1445
Time SubmItted 06/06/07 1640
Parameter Result Units MDL
trans-I 2-Dlchtoroethene
trans-I 3-Dlchloropropene
Trichioroethene
Trlchlorofluoromethane
Vinyl chloride
Method AnalystReportDilutionAnalysis Batch
Limit Factor Date/Time ID
6.7 0.51
05/08/07 1747 erussell 024147
6.7 0.47 06/08/07 1747 crussetl 024147
6.7 0.40 0610B107 1747 erusseti 024147
6.7 055 06/08/07 1747 erussell 024147
13 0.86 06/08/07 1747 eruasetl 024147
826DB
8260B
8260B
82008
8260B
BRL
BRL
BRL
BRL
BRL
4.51
4.29
4.58
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
Surrogate Recovery Control Limits
Toluene.d8 101 81-128
Bromofluorobenzene 106 77-128
Dibromofluoromethane 62 67-143
06/13/07
06/13/07
06/13/07
000
000
000
SemI-volatile Organic Compounds by GMS
124-Trichlorobenzene BRL
2-Dlthlorobenzene BRL
13-Dlchlorobenzene BRI
4-Dichlorobenzene BRL
245-Trichiorophenol BRL
246-Trichlorophenol BRL
24-Dichiorophenol BRL
24-Dimethyiphenol ERL
2.4-Dlnltrophenol BRL
24-Dinitrotoluerie BRL
20-Dinltrotoluene BRL
2-Chlororiaphthalene BRL
5035
5035
5035
pg/kg 380 38 8270C
pg/kg 380 28 821CC
pg/kg 380 27 8270C
pg/kg 380 34 8270C
pg/kg 380 39 827CC
pg/kg 380 36 827CC
pg/kg 380 32 827CC
pg/kg 380 37 8270C
pg/kg 380 43 827CC
pg/kg 380 21 827CC
pg/kg 380 40 8270C
pg/kg 380 39 827CC
Ibrown
thrown
thrown
kcampigotto
kcamplgotto
kcampigotto
kcamptgotto
kcamplgotto
kcemplgotto
kcamplgotto
kcamplgotlo
kcamplgotto
kcamplgotto
kcampigottc
kcampigolth
06/11/07 1352
06/11/07 1352
06/11/07 1352
06/11/07 1352
00/11/07 1352
06/11/07 1352
06/11/07 1352
00111/07 1352
06/11/07 1352
00111/07 1352
06/11/07 1352
06/11107 1352
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
This report should not be reproduced except In Its enUrBty without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page 32 of 45
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 06/1 8/07
Project ID Morehead Commons No Client Sample ID WS4
Prism Sample ID 183635
Sample Matrix Soil coc Group G0607179
Time Collected 06106/07 1445
Time Submitted 06/06/07 1640
This report should not be reproduced except in Its entirety without the written consent oF Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800l529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
2-Chiorophanol BRL iig/kg 380 30 827CC 06111/07 1352 kcampigotto 024124
2..Methyinaphthalerie BRL pg/kg 380 30 827CC 06111107 1352 kcamplgo8o 024124
2-Methylphenol BRL pg/kg 380 36 827CC 06/11/07 1352 kcamplgouo Q24124
2-Nitrophenol BRL pg/kg 380 45 827CC 06111/07 1352 kcamplgolto Q24124
34-Methylphenol BRL pg/kg 380 39 8270C 06/11/07 1352 kcamplgotto 024124
33-Dichiorobenzidine BRL pg/kg 380 24 827CC 06/11/07 1352 kcmpgotto 024124
46-Dlnltro-2-rnethylphenol BRL pg/kg 380 23 827CC 06/11/07 1352 kcamplgoLo 024124
4-Bromophenylphenyielher BRL pg/kg 380 36 827CC 06/11/07 1352 kcampIoIto 024124
4-Chioro-3-methylphenol BRL pg/kg 380 28 827CC 08/11/07 1352 kcampgDtto 024124
4-Chlorophenylphenylether BRL pg/kg 380 23 827CC 06I11/07 1352 kcarnplgollo 024124
4-Nitrophenol BRL pg/kg 380 25 827CC 06/11/07 1352 kcamplgouo 024124
Acenaphihene BRL pg/kg 380 37 827CC 06/11/07 1352 kcamplgouo 024124
Acenaphthylene BRL pg/kg 380 38 8270C 06/11/07 1352 hcamplgctto 024124
Anthracene BRL pg/kg 380 29 827CC 06111/07 1352 kcampigottn 024124
Benzoaanthracene BRL pg/kg 380 53 827CC 06/11/07 1352 kcamplgotto 024124
Benzoapyrene BRL pg/kg 380 44 827CC 06/11/07 1352 kcainplgofto 024124
Benzobfluoranthene BRL pg/kg 380 17 8270C 06/11/07 1352 kcamplgotto 024124
Benzaghiperylene BRL pg/kg 360 18 827CC 06/11/07 1352 kcamplgottu 024124
Benzokfiuoranthene BRL pg/kg 380 31 827CC 06/11/07 1352 kcamplgOtlo 024124
BIs2-chloroethoxymethane BRL pg/kg 380 44 827CC 06/11/07 1352 kcamplgottu 024124
BIs2-chloroethylethor BRI pg/kg 380 41 8270C 06/11/07 1352 kcomplgotto 024124
Bis2-chlorolsopropylether BRL pg/kg 380 32 8270C 06/11107 1352 kcamplgotto 024124
BIs2-ethylhexylphthalate BRL pg/kg 380 19 827CC 06/11/07 1352 kcamplgDttc 024124
Butylbenzylphthalate BRL pg/kg 380 23 8270C 06/11/07 1352 kcamplgoto 024124
Chrysene BRL pg/kg 380 63 827CC 06/11/07 1352 kcampigOtI 024124
Di-n-butyIphthaIate BRL pg/kg 360 17 827CC 06/11/07 1352 kcamplgotto 024124
Di-n-octyIphthaite BRL pg/kg 380 28 827CC 06/11/07 1352 kcampigctto Q24124
Page 33 of 45
NC Certification No.402
SC Certification No 99012
NC Drinking Water Cart No 37735
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-6001529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-4
183635
G0607179
06106/07 1445
06/06/07 1640
Parameter Result Units Report MDL Dilution Method Batch
ID
Analysis Analyst
Limit Factor Date/Time
Dibenzoahanthracene BRL pg/kg 380 38 827DC 06/11/01 1352 kcamplgctlo 024124
Dibenzofuran BRL pg/kg 380 33 8270C 06/11/07 1352 kcamplgotto 024124
Dlethylphthalate BRL pg/kg 380 23 8270C 06/11107 1352 kcarnplgotto 024124
Dlmethyiphthalate BRL pg/kg 380 26 8270C 06/11/07 1352 kcamplgotta 024124
Fluorantherie BRL pg/kg 380 26 8270C 06/11/07 1352 kcamplgotlo 024124
Fluorene BRL pg/kg 380 23 8270C 06/11/07 1352 kcamplgotto 024124
Hexachlorobenzene BRL pg/kg 380 20 6270C 06/11/07 1352 kcamplgotto 024124
Hexachlorobutacllene BRL pg/kg 380 37 827CC 06/11/07 1352 kcarnplgotto 024124
Hexachlarocyclopentadierie BRL pg/kg 380 40 827CC 06/11/07 1352 kcamplgotto 024124
Hexachloroethane BRL pg/kg 380 39 8270C 06/11/07 1352 kcampfgoIo 024124
lrideno1 23-cdpyrerie BRL pg/kg 380 39 8270C 06/11/07 1352 kcamplgotto 024124
Isophorone BRL pg/kg 380 34 8270C 06/11/07 1352 kcamplgotto 024124
N-Nltrosodi-n-propylamtne BRL pg/kg 380 43 8270C 06/11/07 1352 kcamplgotto 024124
N-Nltrosodlphenylamine BRL pg/kg 380 19 8270C 06/11/07 1352 kcamplgottc 024124
Naphthalene BRL pg/kg 380 41 827CC 08/11/07 1352 kcamplgotto 024124
Nitrobenzene BRI pg/kg 380 37 827CC 06/11/07 1352 kcamplgotto Q24124
Pentachioropheriot BRE pg/kg 380 32 8270C 06/11/07 1352 kcamplgottci 024124
Phenanthrene BRL pg/kg 380 19 827CC 06/11/07 1352 kcaniplgoflo 024124
Phenol BRL pg/kg 380 41 827CC 06/11/07 1352 kcamplgotlo 024124
Pyrene BRL pg/kg 380 26 8270C 06/11/07 1352 kcamptgoto Q24124
Page 34 of 45
.óvk AwVU Envbwmbt.......Jrn
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Cflent Sample ID
PrIsm Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-4
183635
G0607 179
0610607 1445
06106/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 30.17 mL 3550B 05/08/07 700 dpope P18579
Extractable Petroleum Hydrocarbons by GC-FID
C11-C22 Aromatics BRL mg/kg
Cl 9-C36 Aliphatics BRL mglkg
C9-C18 Aliphatics BRL mg/kg
Analysis Note for C1l-C22 Aromatics
Sample Preparation
Sample Preparation
Volatile Petroleum Hydrocarbons by GC-PIDIFID
C5-C8 Alipha tics BRL
C9-C10 Aromatics BRL
NC Certification No 402
SC Certification No 99012
NC Drinking Waler Cert No 37735
Laboratory Report
06/18/07
Surrogate Recovery Control Limits
2-Fluorophenol 60 14-89
2-Fluoroblphenyl 73 21 108
Phenol-d5 62 13-95
246-Trlbromophenol 83 25 123
Nirobenzene-d5 53 14-103
Terphenyl-d14 86 41 136
12 6.5 MADEPEPI-I
12 1.8 MADEPEPH
12 3.8 MADEPEPH
Adjusted value
9.64g 2mL EPH
06/15/07 939
06/15107 939
06/16/07 939
gappaccIoIt
giappaccolI
grappacci oil
024301
024301
024301
P1861406/13/07 800 dpope
Metals by ICP
Chromium
Lead
Surrogate Recovery Control LImits
2-Fluorobiphenyl 126 40 -140
1-Chloro-octadecane 106 40-140
o-Terphenyl 105 40-140
2-Bromonaphthalene 129 40-140
0.71 mg/kg
4.1 mg/kg
0.28 0.017
0.28 0.024
6010B 06/11/07 2129 mcampbeit 024176
6010B 06/11/07 2129 mcampbll 024176
2.OGg 50 mL
mg/kg
mg/kg
30508 06111/07 905 Jhoppel
5.8 1.1
5.8 0.035
MADEPVPH
MADEPVPI-I
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800529-6364 Fax [phone]
06/12/07 2330 hwagner
06/12/07 2330 hwagner
P1 8580
024220
024220
Page 35 of 45
NC Certification No 402 Laboratory ReportSCCertificationNo98012
NC Drinking Water Cert No 37735 06118107
Project ID Morehead Commons No Client Sample ID WS-4
PrIsm Sample ID 183635
Sample Matrix Soil COC Group G0607179
Time Collected 06/06/07 1445
Time Submitted 06/06/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
C9-Cl2Allphatlcs BRL mg/kg 5.8 1.8 MADEPVPII 06/12/07 2330 hwagner 024220
Analysis Note for CS-C9 Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
One surrogate recovery
was outside the control limits No target compounds were detected inthissampleNofurtheractionwastaken
Sample Weight Determination
Weight
Weight
Sample Comments
SAL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The resulls In this report relate only fri the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated In the case narrative arid/or test comments
All results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Surrogate Recovery Control Limits
25-Dibromotoluerte-PID 118 70 130
25-Dibrornotoluane-FID 176 70-130
19.14
18.65
MADEP VPH 06/13/07 000 Ibrown
MADEP VPH 06/13107 000 Ibrown
Phone [phone] Toll Free Number 1-800/529.6364 Fax [phone] Page 36 of 45
SC Gerttilcatlan No 99012 Laboratoiy Report
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID B-i
Prism Sample ID 183636
Sample Matrix Soil COG Group 00607179
Time Collected 06/06/07 1500
Time Submitted 06106/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Percent Solids Determination
884 SM2540 06/11/07 1700 ibrown
BOB1A 06/14/07 156 Jvogel Q24275
ROBIA 06/14/07 156 jvogei 024275
8081A 06/14/07 156 Jvogel 024275
8081A 06/14/07 156 JvogeI 024275
BOB1A 06/14/07 156 Jvogel 024275
BOBIA 06/14/07 156 Jvogei 024275
8081A 06/14/07 156 ivogel 024275
8081A 06114/07 156 JvogeI 024275
6081A 06/14/07 156 JvogeI 024275
BOBIA 06/14/07 156 Jvogel 024275
6081A 06/14/07 158 Jvagel 024275
BOB1A 06/14107 156 Jvogel 024275
8081A 06/14/07 156 Jvogel 024275
6051A 08/14/UT 156 IvogEt 024275
8081A 06/14/07 156 jvogel 024275
BOB1A 06/14/07 156 Ivogel 024275
BOBIA 06/14/07 156 Jvogel 024275
BOBIA 06/14107 156 Ivogel 024275
BOB1A 06/14/07 156 Jvogel 024275
8081A 06/14/07 156 Jvogel 024275
8081A 06/14/07 156 jvog 024275
8081A 06/14/07 156 Jvogei 024275
This report should not be reproduced except in Its entirety without the written consent of Prism LabOratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7O4/529634 Toll Free Number 1-800/529-63M Fax [phone]
Fu1 ..wIcs AnatkàI EnvkvnInr4ÆjDtidIDfl
ESP Associates PA
Attn Chris Ward
Box 7030
Chatlotte NC 28241
06/18/07
Percent SolIds
Organochiorine Pesticides by Gas Chromatography
44-DDD BRL pg/kg 2.3 0.69
44-DDE BRL pg/kg 2.3 0.48
44-DDT BRL pg/kg 2.3 0.81
44-Methoxychlor BRL pg/kg 4.5 1.5
a-BHC BRL pg/kg 2.3 0.20
aCh1oidane BRL pg/kg 2.3 0.39
Alcirin BRL pg/kg 2.3 0.45
b.BHC BRL pg/kg 2.3 0.57
Chiordane BRL pg/kg 57 13
d-BHC BRL pg/kg 23 0.32
Dieldrin BRL pg/kg 1.1 0.47
Endosulfan BRL pg/kg 2.3 0.40
Endosulfan II BRL pg/kg 2.3 0.51
Endosutfan Sulfate BRL pg/kg 2.3 0.59
Endrin BRL pg/kg 2.3 0.68
Endrin AidØhyde BRL pg/kg 2.3 0.63
Endrin Ketone BRL pg/kg 2.3 0.45
g-RHC BRL pg/kg 2.3 0.26
g-Chlordane BRL pg/kg 2.3 0.37
Hepfachlor BRL pg/kg 2.3 0.53
Heptachlor Epoxide BRL pg/hg 2.3 0.42
Toxaphene BRL pg/kg 57 13
Page 37 cf45
NC CertlflcaUon No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Sample Preparation 29.71 10 mL 35508 06112/07 1000 dpope P18598
Volatile Organic Comnounds by GC/MS
11 j2-Tetrachloroethane
11 1-Trichloroethene
ii 2.2-Tetrachloroethane
11 .2-Trichloroethane
11-Dichioroethane
1-Dlchforoethene
1-Diohioropropene
23-Trtchlojobemene
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6354 Fax [phone]
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
0618/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soft COG Group
Time Collected
Time Submitted
B-i
183636
G0607179
06106/07 1500
06/86/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Surrogate Recovery Control Limits
Decachloroblphenyl DCB 136 26 204
Tetrachloro-m-xylene TCMX 108 40-162
Polychiorinated Biphenyls PCBs by GC-ECD
PCB-i016 BRL
PCB-1221 BRL
PCB-1 232 BRL
PCB-1242 BRL
PCB-1248 BRL
PCB-1254 BRL
PCB-1260 BRL
Sample Preparation
0.057
0.11
0.057
0.057
0.057
0.057
0.057
0.010
0.046
0.018
0.020
0.0078
0.020
0.015
8062
8082
8082
8052
8082
8082
8082
06/14/07 156
06/14/07 156
06/14/07 156
06/14/07 156
06/14/07 156
06/1407 156
06/14/07 156
JYog
Jvogel
Ivogel
JYogel
Jvogel
JvogeI
JvogeI
024276
024276
024276
024276
024276
Q24276
024276
P1859729.71 10 mL 355DB 06/12/07 1000 dpope
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
pg/kg
pg/kg
jig/kg
pg/kg
jig/kg
pg/kg
pg/kg
pg/kg
Surrogate Recovery Control Limits
Decachiorobiphenyt DCB 96 34 182
Tetrachloro-m-xylene TCMX 106 36 182
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
6.3 0.62
6.3 0.36
6.3 0.65
6.3 0.39
6.3 0.46
6.3 0.48
6.3 0.56
13 0.70
826GB
82608
8260B
82606
82606
826GB
826GB
826GB
0610807 1820 ezussell
06/0807 1820 erussell
06/08/07 1820 eussl
06/06/07 1820 erussell
06/08/07 1820 enisselt
06/08/07 1820 erusset
06/08/07 1820 erussell
06/08/07 120 erussell
024147
Q24147
024147
024147
024147
024147
024147
024147
Page 38 of 45
Laboratory Report
0618/07
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID 183636
Sample Matrix Soil COC Group G0607179
Time Collected 06/06/07 1500
Time Submitted 06/06/07 1640
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 25224-0543
Phone [phone] Toll Iree Number 1-800529.6364 Fax [phone]
NC CertIfication No 402
SC Certification No 99012
NC Drinking Water Cart No 37736
Fult ..urva AnuIyIIcuI EnvhumtinaI Sóhiflu
ESP Associates PA
Attri Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datemme ID
.23-Trichloropropane BRL pg/kg 6.3 0.56 826DB 06/08/07 1820 erussell 024147
124-Trichlorobenene BRL pg/kg 13 0.51 826GB 06/08107 1820 erussell 024147
124-Trirnethylbenzene BRL pg/kg 13 0.48 826DB 06/08/07 1820 eruzsI 024147
1.2Dlbromo-3-chloropropane BRL pg/kg 6.3 10 826DB 0608/07 1820 erussell 024147
12-Dlbromoethane EDB BRL pg/kg 63 0.11 826DB 06/08/07 1820 erusseH 024147
12-Dichlorobenzene BRL pg/kg 13 0.34 82608 06/08/07 1820 erussell 024147
12-Dichloroethane BRL pg/kg 6.3 0.63 52608 06/08/07 1820 erussell 024147
12-Dlchlcrropropane BRL pg/kg 6.3 0.47 826GB 06/08/07 1820 erussell 024147
13.5-Trimathylbenzene BRL pg/kg 13 0.53 826GB 06/08/07 1520 erussell 024147
13-Dlthtorobenzene BRL pg/kg 13 0.55 826GB 06/08/07 1820 enisseIl 024147
13-Dichioropropane BRL pg/kg 6.3 0.43 826GB 06/08/07 1820 enissetl 024147
14-Dichiorobeuzene BRL pg/kg 13 0.49 826GB 06/06/07 1820 erussell 024147
22-Dichioropropane BRL pg/kg 6.3 0.32 826GB 06/0807 1820 erusedi 024147
2-Chloroethyi vinyl ether BRL pg/kg 13 0.47 82608 06/08/07 1820 erussell 024147
2-Chlarotoluene BRL pg/kg 13 0.47 826GB 06/0807 1820 erussell 024147
2-Hexanone BRL pg/kg 63 066 82508 06/0807 1820 erusselt 024147
4-Chiorotoluene BRL jig/kg 13 0.33 82608 06/08/07 1820 erussell 024147
4-Methyl-2-pentanone MIBK BRL pg/kg 13 0.63 826GB 06/08/07 1820 erussell 024147
Acetone BRL pg/kg 25 2.5 82608 06/08/07 1820 erussell 024147
Benzane BRL pg/kg 3.8 0.51 826DB 06/06/07 1820 erussell 024147
Bromobenzene BRL pg/kg 6.3 0.44 826GB 06/08/07 1820 enissefl 024147
Bromochloromethane BRL pg/kg 6.3 0.38 8260B 06/08/07 1820 erussell 024147
Bromodichloromethane BRL pg/kg 6.3 0.56 82608 06/08/07 1820 enissell 024147
Bromofomi BRL pg/kg 6.3 0.47 826GB 06/08/07 1820 erussefl 024147
Bromomethane BRL pg/kg 13 0.74 826DB 06/08/07 1820 erussetl 024147
Carbon disullide BRL pg/kg 13 0.41 82608 06/08/07 1820 eruessfl 024147
Carbon tetrachloride BRL pg/kg 6.3 0.37 826GB 06/0807 1820 erussell 024147
Page 39 of 45
Laboratory ReportSCCertificationNo99012
NC Drinking Water Cart No 37735 06/18/07
Project ID Morehead Commons No Client Sample ID B-i
Prism Sample ID 183636
Sample Matrix Soil coc Gmup 60607179
Time Collected 06106/07 1500
Time Submitted 06106107 1640
This report should not be reproduced except in Its entirety without the written consent Prism LaboratorIes Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Chlorobenzene BRL pg/kg 6.3 0.48 826DB 06/08/07 1820 arussell 024147
Chlorodibromomehane BRL pg/kg 6.3 0.43 826DB 06108/07 120 erussell 024147
Chioroethane BRL pg/kg 13 0.52 826DB 06/08107 1820 erussell 024147
Chloroform BRL pg/kg 6.3 0.47 826DB 06/08107 1820 erussell 024147
Chioromethane BRL pg/kg 13 0.44 82608 06/08107 1820 erussell 024147
cis-12-Dichloroethene BRL pg/kg 6.3 0.28 826DB 06/08/07 1820 erussell 024147
cls-i3-Dlchloropropene BRL pg/kg 6.3 0.41 826DB 06/08/07 1820 enisseH 024147
Dibrornometharie BRL pg/kg 6.3 0.47 826DB 05/08/07 1820 erusseli 024147
Dlchlorodifiuorornetharre BRL pg/kg 13 1.4 826DB 06/08/07 1820 eiussell 024147
Ethylbenzene BRL pg/kg 6.3 0.44 826DB 06/08/07 1820 erussell 024147
Hexachlorobutadlene SRI pg/kg 19 0.79 826DB 06/08/07 1820 enissell 024147
Isopropyl ether IPE BRL pg/kg 6.3 0.22 828DB 06/08107 1820 erussell 024147
Isopropyibenzene BRL pg/kg 13 0.51 82606 06/08/07 1820 enissell 024147
mp-Xylenes BRL pg/kg 13 0.89 826GB 06/08/07 1820 eiuszell 024147
Methyl ethyl ketone MEK BRL pg/kg 25 18 826DB 05/08/07 1820 erussell 024147
Methyl t-butyi ether MTBE BRL pg/kg 6.3 0.37 86DB 06/08/07 .1820 erussef 024147
Methylene chloride SRI pg/kg 13 0.52 826DB 06/0807 1820
erusseil 024147
n-Butylbenzene BRL pg/kg 19 0.51 826DB 06/08/07 1820 erussell 024147
n-Propylbenzene BRL pg/kg 13 0.38 826GB 06/06/07 1820 erussell 024147
Naphthalene BRL pg/kg 6.3 074 826DB 06/08/07 1820 erussell 024147
o-Xylene SRI pg/kg 6.3 0.38 826DB 06/08/07 1820 erusseli 024147
p-lsopropyltoluene SRI pg/kg 19 0.52 82609 06/08/07 1820 erusseH 024147
sec-Butylbenzene BRL pg/kg 19 0.42 82608 06/08/07 1820 erusseil 024147
Styrene BRL pg/kg 6.3 0.63 826DB 06/08/07 1820 erussell 024147
tert-Butylbenzene BRL pg/kg 25 0.39 826DB 06/08/07 1820 erussell 024147
Tetrachioroethene BRL pg/kg 13 1.1 826DB 06/08/07 1820 erussell 024147
Toluerre BRL pg/kg 6.3 0.43 826DB 06/08/07 1820 erusseil 024147
Page 40 of 45
..1 SrvciArntytkLI EiImnmnbI SolutJon3
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
trans-i 2-Dlchloroethene
trans-i .3-Dichioropropene
Trichioroethene
Trichiorofluaromothane
Vinyl chloride
Analysis
Date/Time
06/08/07 1820 erussell
06/08/07 1820 erussell
06108107 1820 erussell
06/08/07 1620 erussell
06/08107 1820 erussell
5035
5035
5035
06/13/07 000 brown
05/13/07 000 brown
06/13/07 000 Ibrown
Semi-volatile Organic Compounds by CC/MS
124-Trichlorobenzene BRL pg/kg 380 37 8270C 05/11/07 1442 kcamplgotto 024124
2-Dichlorobenzene BRL pg/kg 380 28 B270C 06/11/07 1442 kcamplgbllo 024124
13-Dlchiorobenzene BRL pg/kg 350 27 827CC 06/11/07 1442 kcamplgotto 024124
4-Dlchlorobenzene BRL pg/kg 380 34 827CC 06/11/07 1442 kcamplgotlo 024124
245-Trlchlorophenol BRL pg/kg 380 39 8270C 06/11/07 1442 keamplgotto 024124
246-Trichiorophenol BRL pg/kg 380 36 827CC 06/11/07 1442 kcamplgotto 024124
24-Dichlorophenol BRL pg/kg 380 32 827CC 06/11/07 1442 kcamptgotto 024124
24-Dimethyiphenol BRL pg/kg 380 36 8270C 06/11/07 1442 kcamplgotto 024124
24-Dinitrophenol BRL pg/kg 380 42 827CC 06/11/07 1442 kcamplgotlc 024124
24-Dlnitrotoluene BRL pg/kg 380 21 827CC 06/11/07 1442 kcamplgotta 024124
26-Dlnitrotoluene BRL pg/kg 380 40 827CC 06/11/07 1442 kcamplgotto Q24124
2-Chloronaphthalene BRL pg/kg 380 39 827CC 06/11/07 1442 kcamplgofto 024124
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 282244543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC DrinkIng Water Cert No 37735
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID B-i
PrIsm Sample ID 183636
Sample Matrix Soil COG Group G0607179
Time Collected 06/06/07 1500
Time Submitted 06/06/07 1640
Parameter Result Units Report MDL Dilution Method
Limit Factor
BRL pg/kg 5.3 0.48 82608
BRL pg/kg 8.3 0.44 82603
BRL pg/kg 6.3 0.38 82603
BRL pg/kg 5.3 0.52 82603
BRL pg/kg 13 0.61 826GB
Analyst Batch
ID
024147
024147
024147
024147
024147
Samole Weight Determination
WeIght Bisulfate 4.36
Weight Bisulfate 446
Weight Methanol 4.07
Surrogate Recovery Control Limits
Bromofluorobenzene 106 77 128
Toluene-dB 101 81-128
Dlbromofluoromethane 92 67-143
Page 41 of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID
Sample Matrix Soil
Laboratory Report
06/18107
Morehead Commons No Client Sample ID B-I
Prism Sample ID 163636
COC Group G0607179
Time Collected 06/06107 1500
Time Submitted 06/06/07 1640
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Date/Time IDLimitFactor
2-Chiorophenol BRL pg/kg 380 30 827CC 06/11/07 1442 kcamplgotto 024124
2-Methylnaphthalene BRL pg/kg 380 30 827CC 06/11/07 1442 kcamplgotlo 024124
2-Methylphenol BRL pg/kg 380 35 827CC 06/11/07 1442 kcampigouo 024124
2-Nitrophenol BRL pg/kg 380 45 8270C 06/11/07 1442 kcarnplgotto 024124
34-Methyiphenol BRL pg/kg 380 39 827CC 06/11/07 1442 kcamplgouo 024124
33-Dlclilorobenzidine BRL pg/kg 380 24 827CC 06/11/07 1442 kcarnplgouo 024124
46-Dinitro-2-methylphenol BRL pg/kg 380 23 827CC 06/11/07 1442 kcamplgotto 024124
4-Bromophenyiphenylether BRL pg/kg 380 36 827CC 06/11/07 1442 kcampigotto 024124
4-Chloro-3-methyiphenoi BRL pg/kg 390 28 827CC 06/11/07 1442 kcamplgotto 024124
4-Chlorophenyiphenylether BRL pg/kg 380 23 827CC 06/11/07 1442 kcamplgotto 024124
4-Nitrophenol BRL pg/kg 380 25 827CC 06/11/07 1442 kcamplgolto 024124
Acenaphthene BRL pg/kg 380 37 827CC 06/11/07 1442 kcampgotto 024124
Accnaphthylene BRL pg/kg 380 38 827CC 06/11/07 1442 kcampigotto 024124
Anthracene BRL pg/kg 380 29 827CC 06/11/07 1442 kcampigotto 024124
Benzoaanthracere BRL pg/kg 380 53 827CC 06/11/07 1442 kcamplgoito 024124
Benzoapyrene BRL pg/kg 380 44 827CC 06/11/07 1442 kcamplgotto 024124
Berizobfiuoranthene BRL pg/kg 380 17 827CC 06/11/07 1442 kcamplgoLlo 024124
Benzoghjpetyiene BRL pg/kg 380 18 827CC 06/11/07 1442 kcampigottd 024124
Benzokfiuoranthene BRL pg/kg 380 31 827CC 06/11/07 1442 kcamplgotlo 024124
BIs2-chloroethaxymethane BRL pg/kg 380 43 8270C 06/11/07 1442 kcampgotla 024124
Hls2-chioroethylether BRL pg/kg 380 41 827CC 06/11/07 1442 kcamplgoLto 024124
Bls2-chloroisopropyiether BRL pg/kg 380 32 827CC 06/11/07 1442 kcamplgotto 024124
BIs2-ethylhexylphthalate BRL pg/kg 380 19 827CC 06/11/07 1442 kcampigottc 024124
Butylbenzyiphthaiate BRL pg/kg 380 23 827CC 06/11/07 1442 kcampIotto 024124
Chrysene BRL pg/kg 380 63 8270C 06/11/07 1442 kcampIotto 024124
Dl-n-butylphthalate BRL pg/kg 380 17 827CC 06/11/07 1442 kcamplgotto 024124
Di-n-octyiphthaiate BRL pg/kg 380 28 827CC 06/11/07 1442 kcamplgotto 024124
Page 42 ot45
FutycnAntytJcI EwbnSilws
ESP Associates PA
ALtn Chris Ward
P.O Bdx 7030
Charlotte NC 28241
ThIs report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 CharIotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6354 Fax [phone]
NC Certification No.402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID B-i
Prism Sample ID 163636
Sample Matrix Soil COG Group G0607179
Time Collected 06/06/07 1500
Time Submllled 06/06/07 1640
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
Dibenzoahanthracene BRL pg/kg 380 38 82706 06111107 1442 kcamplgotto 024124
Dibenzofuran BRL pg/kg 380 32 827CC 06/11/07 1442 kcampigolto Q24124
Dlethylphthalate BRL pg/kg 380 23 827CC 06/11/07 1442 kcamplgotlo 024124
Dlmethylphthalate BRL pg/kg 380 26 827CC 06/11/07 1442 kcampIgoto 024124
Fluoranthene BRL pg/kg 380 26 627CC 06/11/07 1442 kcamprgotlo 024124
Fluorene BRL pg/kg 380 22 8270C 06/11/07 1442 kcarnplgoLto 024124
Hexachlorobenzene BRL pg/kg 380 20 8270C 06/11/07 1442 kcamplgotto 024124
Hexachiorobutadlene BRL pg/kg 380 37 827CC 06/11/07 1442 kcamplgollo 024124
Hexachlorocyclopentadjena BRI pg/kg 380 40 827CC 06/11/07 1442 kcamplgolto 024124
Hexachicroethane BRL pg/kg 380 38 82706 06/11/07 1442 kcarnplgotto 024124
lndeno12.3-cdpyrene BRL pg/kg 380 39 827CC 06/11/07 1442 kcamplgotto 024124
Isophorone BRL pg/kg 380 34 827CC 06/11/07 1442 kcanlgoUo 024124
N-Nltrasodl-n-propylamlne BRL pg/kg 380 43 827CC 06/11/07 1442 kcamprgotto 024124
N-Nltrosodlphenylamjne BRL pg/kg 380 19 82706 06/11/07 1442 kcamplgotto 024124
Naphthalene BRL pg/kg 380 41 82706 06/11/07 1442 kcamplgotto 024124
Nitrobeazene BRL pg/kg 360 37 82706 06/11/07 1442 kcarnplgolto 024124
Pentachiorophenol BRL pg/kg 380 32 82706 06111/07 1442 kampIgoto 024124
Phenanthrene BRL pg/kg 380 18 827CC 06/11/07 1442 kcarnplgotto 024124
Phenol BRL pg/kg 380 41 82706 06/11107 1442 kcamptgotto 024124
Pyrene BRL pg/kg 360 26 827CC 06/11/07 1442 kcampIotto 024124
Page 43 of 45
Laboratory Report
06/18/07
Project ID Morehoad Commons No Client Sample ID B-I
PrIsm Sample ID 183636
Sample Matrix Soil COC Group G0607179
Time Collected 06/06/07 1500
Time Submitted 06/06/07 1640
Extractable Petroleum Hydrocarbons by GC-FID
Cl 1.022 Aromatics BRL mg/kg
C19-036 Atlphatics ERL mg/kg
C9-C18 Aliphatics BRL mg/kg
Analysis Note for Cll-C22 Aromatics
Sample Preparation
MtalsbylCP
Chromium
Lead
Sample Preparation
Volatile Petroleum Hydrocarbons by GC-PlD/FID
Cs-Ca Aliphatics BRL
CO-ClO Aromatics BRL
Adjusted value
I0.04g 2mL
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Sample Preparation
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Daternme ID
29.64 mL 355DB 06/08/07 700 dpope P18579
Surrogate Recovery Control Limits
246-Tribromophenol 82 26-123
2-Fluoroblphenyl 83 21 -108
2-Fluorophenol 60 14-89
Nltrobenzene-d5 71 14 103
Phenoki5 69 13-95
Terphenyl-d14 89 41 136
11 6.1 MADEPEPI-I
11 1.7 MADEPEPH
11 3.6 MADEP EPH
06/16/07 1031
06/16/07 1031
0611607 1031
grappacdoll
greppacciall
grappaccioll
EPH
024301
024301
024301
P1861406/13/07 800 dpope
Surrogate Recovery Control Limits
2-Fluoroblphenyl 132 40 140
1-Chloro-ocladocane 105 40 140
o-Torphenyl 103 40-140
2-Bromonaphthalene 136 40 140
1.0 mg/kg 0.28 0.017 801DB 06/11107 2137 mcampbelt 024176
3$mg/kg 0.28 0.024 60108 06/11/07 2137 mcampbet 024176
50 mL 30508 06/11/07 905 lhoppel P18580
mg/kg 5.7 1.1 MADEP VPH 06113107 012 hwagner 024220
mg/kg 5.7 0.034 MADEP VPH 06/13/07 012 hwagner Q24220
This report should not be reproduced except In its entirety without the written consent of Prim Laboratories Inc
449 Spdngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 44 of 45
NC Certification No 402 Laboratory ReportScCertificationNo99012
NC Drinking Water Cert No 37735 06118107
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
C9-C12 Aliphalics BRL mg/kg 5.7 1.7 MADEP VPH 06113107 012 liwagner 024220
Analysis Note for C5-CB Aliphatics Adjusted value
Analysis Note for C9-C12 A.iphatics Adjusted value
One surrogate recovery was outside the control limits No target compounds were detected inthissampleNofurtheractionwastaken
Sample Weight Determination
Weight
Weight
19.38
26.09
MADEP VPH 06/13/07 000 brown
MADEP VPH 06/13/07 000 Ibrown
Sample Comments
BRL Below Reporting Umit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certilication requirements other thanNELACcertificationexceptforthose instances indicated In the case narrative and/or test comments
Al/results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in Its entirely without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 24054 Charlotte NC 2B224-0543
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 26241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
B-I
183636
G0607179
06/06107 1500
06/06/07 1640
Surrogate Recovery Control Limits
25-Dibromotoluerie-FID 145 70-130
25-Dibromotoluene-PJD 102 70-130
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page 45 of 45
NC CertflicaUon No 402 Level Ii QC ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 6/19/07
ESP Associates PA Project ID Morehoad Commons No COC GrOUp Number 00607179
Attrt Chris Ward Date/Time Submitted 6/6/07 1640
Box 7030
Charlotte NC 28241
Snmt.nkfll flrnnb tnm....rn.h IIRII 7fl...SJSflIfl IIJCIIIJU
Method Blank QC Batch
Result RL Control Umit Unfla ID
124-TnchIoroberizeje ND 330 185 pg/kg 024124
2-Dlchlorobenzene ND 330 165 pg/kg 024124
13-Dlchlorobenzene ND 330 165 pg/kg 024124
14-Dlchicrobenzene ND 330 165 pg/kg 024124
245-Ttlchlorophenol ND 330 155 pg/kg 024124
246-Trichiorophenot ND 330 165 hg/kg 024124
24-Dichloropheriul ND 330 165 hg/kg 024124
24-Dimethyiphenol ND 330 165 hO/kg 024124
24-Dinitrophenol MD 330 165 pg/kg 024124
24-Dlnltmtoiuene ND 330 165 pg/kg 024124
26-Dlnttmtoiuene ND 330 165 pg/kg 024124
2-Chloronaphthaiene ND 330 165 pg/kg 024124
2-Chtorophenol ND 330 165 pg/kg 024124
2-Methylnaphthalene MD 330 165 pg/kg 024124
2-Methyiphenot ND 330 165 pg/kg 024124
2-Nllrophenoi ND 330 165 pg/kg 024124
34-Methylphenol ND 330 155 pg/kg 024124
33Dichlorobenzidlne ND 330 165 pg/kg 024124
4.6-Dlnltro-2-methytphenol ND 330 165 pg/kg Q24124
4-Bromophertyiphenylether ND 330 165 ig/kg 024124
4-Chioro-3-methylphenot ND 330 165 pg/kg 024124
4-Chiorophenyiphenylether ND 330 165 pg/kg 024124
4-Nltmphenol ND 330 165 pg/kg 024124
Acenaphthene ND 330 165 pg/kg Q24124
Acenaphthylene ND 330 165 pg/kg 024124
Anthracene ND 330 165 pg/kg 024124
Benzoaanlhracene MD 330 165 pg/kg 024124
Benzoapyrene ND 330 165 pglkg 024124
Benzobfiuoranthene ND 330 165 pg/kg 024124
Benzoghlpeylene ND 330 165 pg/kg 024124
Benzokfiuoranhene ND 330 165 pg/kg 024124
Bis2-chloroethoxymcthane ND 330 165 pg/kg 024124
Bls2-chioroethylether Nt 330 165 pg/kg 024124
BIs2-chlorolsopropylether ND 330 165 pg/kg 024124
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SprinybrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone[phone] IoU Free Numben 1-80W529-6354 Fax [phone] Page oflO
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6119/07
Project ID Morehead Commons No COG Group Number G0607179
Date/Time SubmItted 6/6107 1640
Method Blank OC Batch
Result RL Control Umit Untla ID
BIs2-ethylhexytphthalate ND 330 165 pg/kg 024124
Butylbeuzyiphthalate ND 330 165 pg/kg 024124
Chrysene ND 330 165 pg/kg 024124
DI-n-butylphthalate ND 330 165 pg/kg 024124
DI-n.octylphthalate ND 330 165 pg/kg 024124
Dibenzoajiaflthracene ND 330 165 pg/kg 024124
Dlbenzoftjran ND 330 165 pg/kg 024124
Dlethylphthalate ND 330 165 pg/kg 024124
Dlmethylphthalate ND 330 165 pg/kg 024124
Fluoranthene ND 330 165 pg/kg 024124
Fluorene ND 330 165 pg/kg 024124
Hexathlorobertzene ND 330 165 pg/kg 024124
1-foxachiorobutacitene ND 330 165 pg/kg 024124
Hexachiorocyclopentadlene NI 330 165 pg/kg 024124
Hexachloroethane ND 330 165 pg/kg 024124
lndeno123-cdpyrene ND 330 165 pg/kg 024124
Isophorone ND 330 165 pg/kg 024124
N-Nltrosodl-n-propylamlne ND 330 165 pg/kg 024124
N-Nttrosodlphenylamine ND 330 165 pg/kg Q24124
Naphthalene ND 330 165 pg/kg Q24124
Nltrobenzene ND 330 165 pg/kg 024124
Pentachiorophenol ND 330 165 pg/kg 024124
Phenanthrene ND 330 165 pg/kg 024124
Phenol ND 330 165 pg/kg 024124
Pyrene NI 330 165 p9/kg 024124
Laboratory Control Sample Recovey QC BelchResultSpIkeAnwuntJoltsID
124-Trtchlorobenzene 1293.98 1663.1 pg/kg 78 39-99 Q24124
14-Dichlorobenzene 1228.79 1663.1 pg/kg 74 37-95 024124
24-Dlnitrotoluene 1502.15 1663.1 pg/kg 90 56-128 024124
2-Chlorophenol 1187.56 16631 pg/kg 71 37-98 024124
4-Chloro-3-methylphenol 1360.15 1663.1 pg/kg 82 45-111 024124
4-Nitrophenol 1595.27 1663.1 pg/kg 96 20-157 024124
Acenaphthene 1335.55 1663.1 pg/kg 80 44-110 024124
N-Nitrosodl-n.propylamine 1382.10 1663.1 p9/kg 83 38-101 024124
Peritachiorophenol 1774.55 16631 pg/kg 107 53-127 024124
ThIs report should not be reproduced except In Its entirely without the written censent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-800/529-6364 Fax [phone]j40g Page of 10
NC CerllflcaUon No 402 Level II QC ReportSCCertifIcatIonNo99012
NC Drinking Water Cart No 37735 6119107
ESP Associates PA Project ID Morehead Commons No COG Group Number G0607179
Atm Chris Ward Date/TIme Submitted 6/6/07 1640
Box 7030
Charlotte NC 28241
Laboratory Control Sample Recovejy RecoveY
CIC Eatch
Result Spike Amount Units Ii
Phenol 1249.41 1663.1 pg/kg 75 34-102 024124
Pyrene 1525.44 1663.1 pg/kg 92 54-131 024124
Matrix Spike Reunvey
Ranges QCEaICh
Sample 10 Result Spike Amount Urea ID
183523 124-Trictiiorobenzene 1401.93 1665.3 pg/kg 84 26-97 024124
14-Dlchlorobenzene 1292.04 1665.3 pg/kg 78 23-92 024124
24-Dlnltrotoluene 1659.67 1665.3 pg/kg ICC 45-127 024124
2-Chlorophenol 1225.77 1665.3 pg/kg 74 25-94 024124
4-Chloro-3-melhylphenol 1382.95 1665.3 pg/kg 83 31-113 024124
4-Nllrophenoi 1736.26 1665.3 pg/kg 104 17-150 024124
Acenaphthene 1423.90 1665.3 pg/kg 86 36-107 024124
N-Nltrosodl-n-propylarnlne 1427.57 1665.3 pg/kg 86 22-105 024124
Pentachlorophenol 1823.17 1665.3 pg/kg 109 39-137 024124
Phenol 1305.69 1665.3 pg/kg 78 23-97 024124
Pyrene 1547.45 1665.3 pg/kg 93 45-133 024124
Matrix Spike Duplicate Recovery Ravery RPD
Ranges RPO Range OS BatchSampleIDReSUltSpikeAmountUnitsID
183523 24-Trichtorobenzene 1166.55 1662.5 pg/kg 7Q 26-97 18 0-37 024124
14-Dlchlorobenzene 1196.47 1662.5 pg/kg 72 23-92 0-36 024124
24-DInjtntoluene 1824.33 1562.5 pg/kg 98 45-127 0-29 024124
2-Chiorophenol 1144.28 1662.5 pg/kg 69 25-94 0-37 024124
4-Chloro-3-methylphenol 1250 1662.5 pg/kg 75 31-113 10 0-32 024124
4-Nltrophonol 1670.21 1662.5 pg/kg 100 17-150 0-32 024124
Acenaphthene 1376.99 1682.5 pg/kg 83 36-lOT 0-32 024124
N.NlthsodI-n.propylamlne 1309.17 1662.5 pg/kg 79 22-105 0-37 024124
Pentachlorophenol 1867.35 1662.5 pg/kg 112 39-137 0-27 024124
Phenol 1190.15 1662.5 pg/kg 72 23-97 0-42 024124
Pyrene 1564.16 1562.5 pg/kg 94 45-133 0-27 024124
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-8001529-6364 Fax [phone] Page of 10
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking WaLer Cert No 37735
11-Trlchloroe
1.1 22-Tetrachloroethane
11 2-Trlchloroethane
1-Dlchloroethane
1-Dichloroethene
11-Dlchloropropene
23-Tdchlorobenzene
.2.3-Trichioropropane
24-TrjchIorrbenzene
124-Trimethylbenzene
2-Djbromoethane EDB
12-Dichiorobeozene
12-Dichioroethane
.2-Dichioropropane
.35-Trimethylbenzene
3-DlchIorobnen
3-Dlchloropropane
.4-Dlchtcrobenzene
2.2-Dichloropropane
2-Chiorotoluene
2-Hexanone
4-ChlorotOluene
4-MeIhyI-2-pentanone Ml8K
Acetone
Berizene
Bromobenzene
Brcnlociijoromethane
Bromodichioromethane
Bromotbim
Bromomefliane
Carbon tetrachioride
Chlomberjzene
Chiorodibromomethane
Chioroetharie
tvkaAn.iI ewmIsQ.
Level II QC Report
6/19/07
Project ID Morehead Commons No COC Group Number G0607179
Date/Time Submitted 6/6107 1640
VoIatll flrninu rnmnniinI by CC/MS
Method Blank
OCResultRIConircILimitUnits ID
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.0D5 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg Q24t47
ND 0.005 0.0025 mg/kg 024147
ND 0005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg Q24147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.05 0.025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147
ND 0.05 0.025 mg/kg 024147
ND 0.05 0.025 mg/kg 024147
ND 0.003 0.0015 mg/kg 024147
ND 0.005 0.0025 mg/kg Q24147
ND 0.005 0.0025 mg/kg Q24147
ND 0005 0.0025 mg/kg 024147ND0.005 0.0025 mg/kg 024147
ND 0.01 0.005 mg/kg 024147ND0.005 0.0025 mg/kg 024147
ND 0.005 0.0025 mg/kg 024147ND0.005 0.0025 mg/kg 024147ND0.01 0.005 mg/kg 024147
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1400/529-5364 Fax [phone] Page of 10
NC CertificatIon No.402 Level II QC ReportScCettifloallonNo99012
6119107NCDrinkingWaterCertNo37735
ESP Associates PA Project ID Morehead Commons No COG Group Number 30607179
Attn Chris Ward Date/Time Submitted 6/6/07 1640P.O Box 7030
Charlotte NC 28241
Method Blank cc Saith
Result RL Conloi LimiL tints ID
Chlorotbrm ND 0.005 0.0025 mg/kg 024147
Chioromethane ND 0.005 0.0025 mg/kg 024147
cls-12-Dlchloroethene ND 0.005 0.0025 mg/kg 024147
cls-13..Dlchloropropene ND 0.005 0.0025 mg/kg 4j47
Dichiorodifluorornethane ND 0.005 0.0025 mg/kg 024147
Ethylbenzene ND 0.005 0.0025 mg/kg Q24147
Isopropyl ether IPE ND 0.005 0.0025 mg/kg 024147
Isopropylbenzene ND 0.005 0.0025 mg/kg 024147
mp-Xylenes ND 0.01 0.005 mg/kg 024147
Methyl ethyl ketone ME1 ND 0.1 0.05 mg/kg 024147
Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg 024147
Methylane chloride ND 0.005 0.0025 mg/kg 024147
n-Butylbenzene ND 0.005 0.0025 mg/kg 024147
n-Propylbenzene ND 0.005 0.0025 mg/kg 024147
Naphthalene ND 0.01 0.005 mg/kg 024147
oXylene ND 0.005 0.0025 mg/kg 024147
plsopmpyltoIuene ND 0.005 0.0025 mg/kg 024147
seo-Butylbenzene Nfl 0.005 0.0025 mg/kg 024147
Styrene ND 0.005 0.0025 mg/kg 024147
tert-Butylbenzane ND 0.005 0.0025 mg/kg Q24147
Tetrachioroethene Nt 0.005 0.0025 mg/kg 024147
Toluene ND 0.005 0.0025 mg/kg 024147
trans-i2-Dithloroethene Ni 0.005 0.0025 mg/kg 024147
trans-i 3-DlchIompropene ND 0.005 0.0025 mg/kg 024147
Tiichloroethene ND 0.005 0.0025 mg/kg 024147
Tlichlorofluoromethane ND 0.005 0.0025 mg/kg 024147
Vinyl acetate ND 0.025 0.0125 mg/kg 024147
Vinyl chibrido ND 0.005 0.0025 mg/kg 024147
Laboratory Control Sample
Recovery ac BntcIResultSpikeAmountUniID
11-Dichlcroethene 0.04482 0.05 mg/kg 91 57-122 024147
Benzene 0.05086 0.05 mg/kg 102 62-119 Q24147
Chlorobenzene 0.05259 0.05 mg/kg 105 61-124 024147
Toluene 0.05299 0.05 mg/kg 106 57-122 024147
Trlctiloroethene 0.05365 0.05 mg/kg 107 69-129 024147
This report should not be repmduced except In Its entirety without the written consent of Prism Laboratories Inc449SprIngbrooRoadP.O Box 240543 Charlotte NC 28224.0543Phone[phone] Toll Free Number 1-800/529-6364 Fax[phone] Page of 10
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
This report should not be reproduced except in its enUrety without the wiitten consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] ToIl Free Numbec 1-800/529.6364 Fax [phone]
NC CertificatIon No.402
SC Cerilficalion No 99012
NC Drinking Water Cert No 37735
Level II QC Report
619/07
Project ID Morehead Commons No COC Group Numbec G0607179
Date/Time SubmItted 6/6107 1640
Matrix Spike Recovoy Rocovesy
Sample ID Result Spike Miount Units ngas QC Batch
ID
183205 11-Dichloroethene 0.04446 0.05 mg/kg 89 44-140 024147
Benzene 0.0476 0.05 mg/kg 95 46-136 024147
Chlorobenzene 0.04586 0.05 mg/kg 92 47-135 024147
Toluene 0.0476 0.05 mg/kg 95 47-136 024147
Trlchloroethene 0.04859 0.05 mg/kg 97 45-141 024147
Matrix Spike Duplicate Recovwy Recove RPD
Sample to ReSUlt SpIke Amount Units gas RPD iitange OC Batch
183205 11-Dlchtoroethene .04499 005 mg/kg 90 44-140 0-23 024147
Renzene 0.04937 0.05 mg/kg 99 46-136 0-22 024147
Chlorobenzene 0.0472 0.05 mg/kg 94 47-1 35 0-22 024147
Toluee 0.04972 0.05 mg/kg 99 47-136 -22 024147
Trichloroethene 0.05061 0.05 mg/kg 101 45-1 41 0-23 024147
Metals by ICP method 6010BBlan
00 BatchResultRIControlUmitUnItsto
Chromium 0.0513 0.25 0.125 mg/kg 024176
Lead 0.0553 0.25 0.125 mg/kg 024178
Laboratory Control Sample Recovwy Recovery
Result Spike Amount Units
00 Batch
ID
Chromium 22.4412 25 mg/kg 90 80-120 024176
Lead 21.4504 25 mg/kg 86 80-120 024176
Matrix Spike
Recovery ReCOVCfY
Sample ID Result SpIke Amount Units Rarees 00 Batch
II
183632 Chromium 16.5648 24.875 mg/kg 65 78-125 024176
Lead 20.5958 24875 mg/kg 66 //75-125 024176
Matrix Spike Duplicate Recovery Recovery RPD
Sntjle Ilk Result Spike Amount Units
RPD Range 00 Batch
ID
183632 Chromium
Lead
16.0388
18.9135
24.630
24.630
mg/kg 63 //75-125 0-20 024178
mg/kg 60 //75-125 0-20 024176
Page of 10
ESP Associates PA
Attn Chris Ward
Box 7030
Chariotte NC 28241
This report should not be reproduced except in Its entirety without the written Consent ci Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1.8001529.6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Level Ii QC Report
6/1 9/07
Project ID Morehead Commons No COC Group Number G0607179
Daterflrne SubmItted 6/6/07 1640
%hIHI De.....t.....U......method MADPP VPHtSSJI4IfJIYIMIJI.flI UIJI ia UV
Method Blank
ac BatchResultRtCorrtmiLimitUnitsto
C5-C8 Allphatics ND 2.5 mg/kg 024220
CS-Cl Arcmatlcs ND 2.5 mg/kg 024220
C9-C12 Aliphatics ND 2.5 mg/kg 024220
Laboratory Control Sample Rocoveiy Recovery
Rarges QCBalCliResultSpikeAmountUnitsID
C5-C8Aliphatics 14.906 15 mg/kg 99 70-130 024220
C9-C10 Aromatics 3.909 mg/kg 78 70.130 024220
C9-Cl2Allphatics 9.460 10 mg/kg 95 70-130 024220
Matrix Spike Recovery
Ranges DC BatchSampleioRemitSpikeAmountUnitsID
183632 CS-CS Allphatics 11.352 15 mg/kg 76 70-130 024220
C9-Cj0Ammatjcs 3.501 mg/kg 70 70-130 024220
C9-Cl2AIlphatlcs 7.313 10 mg/kg 73 70-130 024220
Matrix Spike Duplicate Recove Recovery RPD
Ranges RPD Range ESResult Spike Amount UnitsSamptelo
183632 C5-CSAIiphatIcs 12.679 15 mg/kg 85 70-130 11 0-25 024220
CO-Cia Aromatlcs 3.573 mg/kg 71 70-1 30 -25 024220
C9-C12 Aiiphatics 7.963 10 mg/kg 80 70-130 0-25 024220
Page of 10
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
44-DDD
44-DDE
44-DDT
44-MethoxychIor
a-BHC
a-Chlordane
Aidrin
b-BHC
Chlordane
d-BHC
Oleldrin
Endosulfan
Endosulfan II
Endosullan Sulfate
Endrin
Enddn Aldehyde
Endrin Ketona
g-BHC
g-Chlordane
Heptathlor
Heptachior Epoxide
Toxaphene
Laboratory Control Sample
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND 51 25 pg/kg
ND pg/kg
ND 0.5 pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND pg/kg
ND 50 25 pg/kg
33.4 33
26.0 33
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
024275
024275
024275
Q24275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
024275
QC Satcii
ID
024275
024275
024275
024275
024275
00 Belch
ID
103 75-141
105 66-132
105 72-1 36
103 74-147
100 72-134
Reve
84 56-163 024275
101 57-137 024275
79 60-141 024275
NC CertificatIon No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6/19/07
Project ID Morehead Commons No COC Group Number G06071 79
Date/Time Submitted 6/6/07 1640
flrn1nnhlnrtnA DÆaIb.ld-......S.JtII flflIflttPLlI Oilily ulctiuuu
Method Blank
OC BatchResistRLContrctUrrdtunitsID
Recovey Recavejy
Result Spike Amount Units Ranges
44tDDT 33.83 33
Aidrin 3473 33
DleldrIn 34.69 33
Efldrln 34.14 33
Heptachlor 32.89 33
Matrix Spike
Sample ID Result SpIke Amount
183801 444-DDT 27.6 33
Aidrin
Oleidrin
Unite
pg/kg
pg/kg
pg/kg
This report should not be reproduced except in Its entirety without the wuitten consent of Prism Laboratories Inc449SprtngbrookRoadP.O Box 240543 Chartotte NC 28224-0543Phone[phone] Toll Free Number 1-800/529-6354 Fax [phone] Page of 10
ESP Associates PA
Attn Chiis Ward
Box 7030
Charlotte NC 28241
Matrix Spike Recovery
Ranges OCRatch
Sample ID
Result Spike Anrctmt Units ID
183801 Endrln 28.0 33 pg/kg 85 65-164 Q24275
lIeptathlor 27.2 33 pg/kg 82 63-142 024275
Matrix Spike Duplicate Recovery Recovery RPD CatchRangesRHRangeSampleIDResultSpikeAmountUnits
183801 44-DDT 31.1 33 pg/kg 94 56-163 12 0-38 024275
Aldriri 35.8 33 pg/kg 108 57-137 0-29 024275
Dleldrin 28.9 33 pg/kg 88 60-1 41 11 0-30 024275
Endrin 30.9 33 pg/kg 94 65-164 10 0-21 Q24275
Heptadilor 29.7 33 pg/kg 90 63-142 0-27 024275
Polychioririated Biphenyls PCBs by GC-ECD method 9082
Method Blank DC Batch
Result RI Control Limit Units ID
PCB-1016 ND 0.05 0.025 mg/kg 024276
PCB-1221 ND 0.1 0.05 mg/kg 024276
PCB1232 ND 0.05 0.025 mg/kg 024276
PCB-1242 ND 0.05 0.025 mg/kg 024276
PCB-1248 ND 0.05 0.025 mg/kg 024276
PCB-1254 ND 0.05 0.025 mg/kg 024276
PCB-1260 ND 0.05 0.025 mg/kg 024276
Laboratory Control Sample Recovery Recovery
Ranges DC Batch
Result SpIke Mieurit Units ID
P00-1016 0.308 0.333 mg/kg 92 64-151 024276
PCB.1260 0.306 0.333 mg/kg 92 45-166 024276
Matrix Spike gecovey Recovery
Ranges CC BatchSSmpIaIDResult Spike Amount Units ID
183632 PCB-1016 0.325 0.333 mg/kg 98 14192 024276
PCB-1260 0.337 0.333 mg/kg 101 10-192 024276
Matrix Spike Duplicate RSCOV Recovery RPD
Ranges RPD Range DC BatchSampleIDResultSpikeAmountUnitsID
183632 PCB-1016 0.290 0.333 mg/kg 87 14-192 11 0-40 024276
PCB-1 260 0.298 0.333 mg/kg 39 10-192 12 0-40 024276
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O BOx 240543 Charlotte NC 28224.0543Phone[phone] Toll Free Number 14001529-6334 Fax [phone]
NC Certification No 402
SC CertificatIon No.99012
NC Drinking Water Cart No 37735
Level II QC Report
6/19/07
Project ID Morehead Commons No COG Group Number G0607179
Date/TIme Submitted 6/6/07 1640
Page of 10
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification Na 99012
NC lrinklng Water Cert No 37735
Level II QC Report
6/19/07
Project ID Morehead Commons No COC Group Numbcr G0607179
Date/Time Submitted 6/6107 1640
vhI MAflP FPH...yt.JeW SJUIJ icuuu
Method Blank UC Batch
Result RL Ccnlroi limit Units
C11-C22Amrnatics ND 10 mg/kg 024301
C19-C36Aliphatics ND 10 fig/kg 024301
C9-.C1 Aliphatics ND 10 mg/kg 024301
Laboratory Control Sample Recovery Recovery
Ranges 00 Batch
Result Spike Amount Units ID
C11-C22Aromafics 168.1 170 mg/kg 99 40-140 024301
C19-C36AlIphatlcs 76.7 80 mg/kg 96 40-140 024301
C9-C18 Allphatics 44.3 60 mg/kg 74 40-140 024301
Matrix Spike Recovery Recovery cc Batch
Sample ID Result Spike Amount Units ID
183819 C11-C22 Aromatics 15668 170 mg/kg 92 40-140 Q243D1
C19-C36 Allphatics 74.04 90 mg/kg 93 40-140 024301
C9-ClBAllphatIcs 43.36 60 mg/kg 72 40-140 024301
Matrix SpIke Duplicate Recovery Recovery RPD
dlRangesRPDRangeOCBat
Sample ID Result Spike Amount Units ID
183819 C11-C22 Aromatics
C19-C36 Aliphatics
C9-C18 Afiphafics
4-See Case Narrative
164.44 170 mg/kg 97 40-140 -50 024301
75.54 80 mg/kg 94 40-1 40 0-50 Q24301
44.22 60 mg/kg 74 40-140 0-50 Q24301
Page 100110
Full Seivloo Mlytlaal EnvlranmBntai Satutlona
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704l529.634 Fax 704I5254y
Client Company Name_______________________
Report To/Contact Name
Reporting Address ____________________________
Phone Fax Yes No
Email Yes No Email Address
EDD Type PDF_Exce _Ohor1
Site Location Name /LfO/t4d41f/P1o9
Site Location Physical Address ____________________
ERÔE9 usel7
TO BE FILLED IN BY CUENT/SAMPLING PERSONNEL
Certification NELAC_.USACE_FL____NC_L_
SC_OTHER _____N/A_____
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES NO
CHAIN OF CUSTODY RECORD
PACE OF_.L QUOT TO NSURE PR ER aIL.LING
M....1Lt11i IiL.7.t
Short Hold Analysis Yes No USI Project Yes No
please ATTACH any
provisions and/or
Invoice To
project pacific
Rmegts
reporting QC LEVE Ill III IV
Address I4
Purchase Order NoJBiIIing Reference1
equesled Due Data Cl Day Days
04 Pa Days
44WorIcing Days 06-9 Days Sta1d 10 days pproveJ
Samples receIved after 1500 will be processed next bu5lrress day
Turnaräund lime Is based an
busIness days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITiONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CUENTI
CLIENT
SAMPLE DESCRIPTION
1i5bs-1341q
DATE
COLLECTED
çL
TIME
COLLECTED
MILITARY
HOURS
j_cjc
/ir
/gqf5
MATRIX SAMPLE CONTAINERSOiL
WATER OR
TYPE
SLUDGE SEE BELOW NO SIZE
fl../Cio
PRESERVA-
lIVES
ANALYSES REQUESTEDAO%j D/Li /0
//
17 liiiIJ_
LJ
.L
REMARKS PS5M
ID NO
35
lB3b3
annqurane ay uignaiure
.-
Samplers Signature /rjf7 Sampled By Print Name I2t Je Atfihlatlo
Upon relinquIshing this Cn of ciody is your authorization for Prism to proceed with the anaIysas requested above AnysubmittedinwritingtothePrismProjectManagerTherewillbechargesforanychangesafteranalyseshave been Initialized
/P
changes must be
rieceweo ay raignature Dale
RellnquI5hod 8y Sinalure
5A FLES ARE
Fad Ex UPS tnnd-deItvered
Received By SI nature
TAP TO Th LABoRATORYACCEPTED AND VERIFIED AGAINST COD UNTIL RECEIVED AT ThE LABORATORY
Cl Pdsm FIeld ServIce Cl Oilier
Data
SP1
MItllaryfrIOurs Additional Comments
NPDES UflT GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHERNCcscINNCDSCONCDSC ONC DSC ONC QSC ONO OSC ONC 050 ONC OSC UNC
OSC____O___JO _Io _______lo ______lo________________
SEE REVERSEFORTERMSCONDITIONS
Full Swe Analyilcal nvlrocimantal SolUUon
CLIENT ESP 4Ssk P14
A1TN JVi Ward
PRISM COC GROUP
Please fill In the Site Location information on the attached VPH and/or EPH Forms
I\NaSO1\FOLDCOMMON\FbRMS\H EPHSjte Location for Cllentdac
VPH AliphaticslAromatics Laboratory Reporting Form
Client Name ESP Associates PA Laboratory Name Prism Laboratories Inc
Project Name Morehead Commons No NC Certification Lab 402
Site Location ______________________________Sample Matrix Soil
Sample Information and Analytical Results
Method for Ranges MADEP VPH
VPH Surrogate Standards Aliphatic 25-Dibromotoluene Aromatic 25-Dibromotoluene
rr rkf .JIth Iii 1t
Sample Identification iIP -i1r 183632 183633 183634 183835 183636
Collection Option for soil
iJlf
Date Collected 6/612007 ______________________________ __________
Date Received .Qiii4 fli 6/612007 __________ __________ _____________________
Date Extracted ii 8/12/2007 __________ ____________________ __________
Date Analyzed tit1 612/2007 __________ ____________________ __________
Dry Solids 82.6 _________ _________ _________ _________
Dilution Factor __________ ____________________ __________
Hydrocarbon Ranges In mg/kg ilbh Sample Results __________ ____________________ __________
CS_CS Aliphatics _________ _________ _________ _________
C9_Cl Aliphatics ______________________________ __________C9 Cl Aromatlcs __________ ____________________ __________
Blank C5 C8 Aliphatrcs i._______________________________ __________C9 C12 Aliphatics
__________C9-C1 0_Aromatics ___________ _______________________ ____________RL C5 CS Aliphatics ____________________ __________C9-C12 Aliphatics h_i __________________ _________
_________C9-C1 Aromatics ______________________________ __________MDL C5-C8 Aliphatics
C9-C12 Alrphatics __________ ______________________________
________C9-C10 Aroniatics
Surrogate Acceptance Ranee Blank 70-130 70-130 70-130 70-130 70-130
Aliphatic Surrogate Rec FID 116
Aromatic Surrogate Rec PID 91
6.1
Si
6.1
5.0
5.0
5.0
6.1
6.1
6.1
1.2
1.9
0.036
55
118
6/6/2007
6/6/2007
6/1 2/2007
61212007
86.4
Sample Results
5.8
5.8
5.8
5.0
5.0
5.0
5.6
5.8
5.8
1.1
1.8
0.035
163
138
6/6/2007
6/6/2007
6/1 2/2007
6I12I2007
82.9
Sample Results
6.0
6.0
6.050
5.0
5.0
6.0
6.0
6.0
1.2
1.9
0.036
65
129
6/6/2007
6/6/2007
6/1212007
8/12/2007
88.5
Sample Results
5.8
5.8
5.8
5.0
5.0
5.0
5.8
5.8
5.8
1.1
1.8
0.035
176
118
6/6/2007
6/6/2007
6/13/2007
6/13/2007
88.4
Sample Results
5.7
5.7
5.7
5.0
5.0
5.0
5.7
5.7
5.7
1.1
1.7
0.034
145
102
OptIon Established fill line on vial
Option Sampling
device indicate brand e.g EnCore TM
Option Field weight of soil
--Unadjusted value should exclude the concentration of any surrogates Internal standards and/or
concentrations of other ranges that elute within the specified range
---Adjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank or Trip Blank
whichever Is higher indicate typeWereallperformance/acceptance standards for required OAIQC
procedures achieved YES No Details Attached
Were any significant modifications to the VPH method made NO Yes Details Attached
Comments VPH trip blank was not submitted to the laboratory
Result outside of the QC limits
Page of VPI-I Sell
EPH AliphatlcslAromatics Laboratory Reporting Form
Client Name
Project Name
Site Location
ESP Associates PA
Morehead Commons No
Laboratory Name
NC Certification Lab
Sample Matrix
Prism Laboratories Inc
402
Soil
Sample Information and Analytical Results
EPH Fractionation Surrogates
Sample Identification
Date Collected
Date Received
Date Extracted
Date Analyzed
Dry Solids
Dilution Factor
Hydrocarbon Ranges in mg/kg
C9-C1B Aliphatics
CI 9-C36 Aliphatics
Cl 1-C22 Aromatics
Blank C9-C18 Aliphatics
019-036 Aliphatics
_________Cl 1-C22 Aromatics
RL C9-C18 Aliphatics
Cl 9-C36 Aliphatics
_________011-022 Aromatics
C9-C18 Aliphatics
019-036 Aiiphatics
________Cl 1-C22 Aromatics
Surrogate Acceptance Range
Atiphatic Surrogate Rec
Aromatic Surrogate Rec
Fractionation Surrogate Accep Range
Frac Surrogate D/Rec
Frac Surrogate Rec
6/17/2007 6/16/2007
82.9 86.5
Method for Ranges MADEP EPH
EPH Surrogate Standards Aliphatic 1-Chioro-octadecane Aromatic o-Terphenvl
183633
6/6/2007
6/6/2007
6/13/2007
183634 183635 183636
6/8/2007 6/62007 6/6/2007
6/6/2007 6/62007 6/6/2007
6/13/2007 6/13/2007 6113/2007
6/16/2007
88.4
2-Bromonaphthalene Fluoroblohen
tI 183632 _________
6/612007 _________ML 6/6/2007 _________
lit.6/13/2007 ___________i1 616/2007 6/16/2007
jriiE 82.6 86.4
Sample Results ____________
iiliit
___________________________
I.
1II
ttflt4 tI.t
Blank ____________________128
107 __________________
MDL
c13
13
13
10
10
10
13
13
13
4.0
1.9
6.8
40-1 40
Sample Results
12
12
12
10
10
10
12
12
12
3.8
1.8
6.4
40-1 40
Sample Results Sample Results Sample Results
13 12 11
13 12 Ii
13 12 11
10 10 10
10 10 10
10 10 10
13 12 11
13 12 11
13 12 11
4.0 3.8 3.6
1.9 1.8 1.7
6.8 6.5 6.1
40-140 40-140%40-140
112
102
95
Blank
134
132
98
138
40-1 40
135
131
114
106
40-140
111
107
105
105 103
40-140 40-140 40-140
132 129 136
128 126 132
Unadjusted value should exclude the concentration of any surrogates internal standards and/or
concentrations of other ranges that elute within the specified range
Adjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank
Wore all performance/acceptance standards for required QAIQC
procedures achieved
Was blank correction applied as significant modification of the method
Were any significant modifications to the EPH method made
Comments
No Details Attached
Yes NO
NO Yes Details Attached
Page of EPI-Sell
RtU Ut4
Case NarrativePRISM.44 LABORATORJES114C
Date 06/15/07 Client Project ID Morettead Commons No.2
Company ESP Associates PA Prism COC Group No G0607193
Contact Chris Ward Collection Dates 06/07/07AddressBox 7030 Lab Submittal Dates 06/07107
Chariotte NC 28241
This data package contains the analytical results for the project Identified above and includes Case Narrative Laboratory Report QualityControlandSubcontractedLaboratoryReportwithcorresponding Chain-cl-Custody totaling 22 pages chain-of-custody is also attached forthesamplessubmittedtoPrismfor this projecL
Data qualifiers are flagged individually on each sample key
reference for the data quafifiers appears at the end of this case narrative Qualitycontrolstatements and/or sample specific remarks are Included in the sample comments section of the laboratory report for each sampleaffected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
Analysts Note for 024193 MSD Ethylbenzene Recovery below the control lImits
Analysis Note for 024193 MSD m.p-Xylenes RPD value outside the control limits
Analysis Note for 024193 MSO o-Xylene RPD value outside the control limits
Metals Analysis
Analysis Note for 024208 MS Barium Matrix Interference is suspected
Analysis Note for 024208 MSD Barium Matrix Interference is suspected
Wet Lab and Micro Analysis
Total Halogens analysis subcontracted to GCAL Laboratory report Is attached
Please call if you have any questions relating to this analytical report
Date Reviewed by Rabbi Jones Project Manager _____________________________
Signature Io-_.e-i.-Signature ____________________________
Review Date 7i5/07 Approval Date __________________________
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound dIluted out
EsUmated concentrallon calibration range exceedert
The analyte was positively Identified but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect Is present
Notes This report should not be reproduced except In its entirety without the writtten consent of Prism Laboratories Inc The results in thisreportrelateonlytothesamplessubmittedforanalysis
449 Springbroak Road P.O Box 240543 Charlotte NC 28224-0403
Phone [phone] To Free 800/529.6364 Fax [phone]
Angela D6cashJ/
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06115/07
ESP Msociates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
1b-234 Comp
183685
G0607193
06/07/07 1315
06/07/07 1400
ercent Solids Determination
Percent Solids
Volatile Organic Compounds by GCMS
Benzene
Ethylbenzene
mp-Xylenes
o-Xylene
Tolu ens
BRL pg/kg 3.5 0.46 5260B 06/13/07 012 erussell
BRL pg/kg 5.8 0.41 82608 06/13/07 012 erussell
BRL pg/kg 12 0.81 826GB 06/13/07 012 erussell
BRL pg/kg 5.8 0.35 8260B 06/13/07 012 erussell
BRL pg/kg 5.8 0.39 826GB 06/13/07 012 erussell
Q24193
Q24193
Q24193
Q24193
024193
Diesel Range Organics DRO by GC-FID
Diesel Range Organics DRO
Sample Preparation
Gasoline Range Organics tGRO by GC.FID
Gasoline Range Organics GRO BRL
TCLP Extraction for Metals
TCLP Extraction
98 mg/kg 7.7 1.9
49.78
mg/kg 1.1 0.070
Complete
Surrogate Recovery Control Limits
Toluene-d8 104 81-128
Bromofluorobenzene 111 77-128
Dlbromofluoromethane 106 67-143
80158 06/11/07 2347 Jvogel Q24213
mL 35505 08/1107 900 dpope P1860Y
Surrogate Recovery Control Limits
o-Terphenyl 107 48-130
80158 06/13/07 1359 hwayner 024199
Surrogate Recovery Control Limits
aaa-TFT 89 55-129
1311 06/11/07 1340 Ihoppel
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
91.5 SM2540 06/12/07 1640 ithao
Phone [phone] Toll Free Number l-800/52983M Fax [phone] Page of
5rvkMIyl EnvlwmtmI Sk5an
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
TCLP Leachable Mercury by CVAA
Mercury BRL mg/L 0.010 0.000042 7470A 06/13/07 1231 Ihoppel 024234
Sample Preparation 20 mL 30 mL 7470A 06/13107 735 Ihoppel P18612
TCLP Leachable Metals by ICP
Arsenic BRL mg/L 0.050 0.0029 601GB 06/13/07 015 rncampbetl Q24208
Barium 0.61 mg/L 5.0 0.0019 6010B 08/13/07 015 mcampbeft 024208
CadmIum 0.0006 mg/L 0.025 0.00034 6010B 06/13/07 015 mcampbell 024208
Chromium 0.0083 mgIL 0.25 0.0006 601GB 06/13/07 015 mcampbell 024203
Lead 0.011 mg/L 0.050 0.0021 60108 06/13/07 015 mcampbell 024208
Selenium BRL mgIL 0.050 0.0035 601GB 06/13/07 015 mcampbelt 024208
Silver RRL mg/L 0.25 0.00025 601DB 06/13/07 015 mcarnpbeli 024208
Sample Preparation so mL 50 mL 3010A 06/12/07 715 Jhoppel P18602
Total Halogen by Method 9076
Subcontract Report See 9076
Attached
Analysis Note for Subcontract Report Analysis subcontracted to NC certified lab 618
Sample Comments
BRL Below Reporting Umit
Estimated value between the Reporting Limit and the MDL
The results in 1/ifs report relate only to the samples submitted lbr analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrathe and/or test comments
All results are reported on thy-weight basis
This report should not be reproduced except In its entirety wIthout the Written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529.6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Laboratory Report
06/15/07
Prolect ID Morehead Commons No Client Sample ID lb-234 Camp
Prism Sample ID 183685
Sample Matrix Soil COC Group G0607193
Time Collected 06/07/07 1315
Time Submitted 06/07107 1400
Angela Overcash V.P Laboratory Services
Page of
ESP Associates PA
Atm Chris Ward
Box 7030
Charlotte NC 28241
NC CertIfication No.402
SC Certification No 99012
NC Drinking Water Cert No 37135
Project ID Morehead Commons No
Level QC Report
6/15/07
COG Group Number G0607193
Date/Time Submitted 611/07 1400
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-800I529.54 Fax [phone]
Volatile --by IR 8260B..MSJIJWO .annn.3 cti.uu
Method Blank UC Batch
ReSUU RL Contnol Umtt Units ID
Benzene ND 0.003 0.0015 mg/kg 024193
Ethylbenzene ND 0.005 0.0025 mg/kg 024193
mp-Xylenes ND 0.01 0.005 mg/kg 024193
o-Xylene ND 0.005 0.0025 mg/kg Q24193
Toluene ND 0.005 0.0025 mg/kg 024193
Laboratory Control Sample Recovery
RecuR Spike Miount Units Ranges OC Batch
ID
Benzene 0.0473 0.05 mg/kg 95 62-119 024193
Ethylbenzene 0.04943 0.05 mg/kg 99 57-128 024193
mp-Xyterjes 0.10007 0.1 mg/kg 100 54-132 024193
o-Xylene 0.05009 0.05 mg/kg 100 57-131 024193
Toluene 0.04451 0.05 mg/kg 90 57-122 024193
Matrix Spike Recovery
Sample Eli Result Spike Miount Units sages DC Batch
ID
183910 Benzene 0.04076 0.05 mg/kg 82 46-136 024193
Ethylbenzene 0.03384 0.05 mg/kg 68 51-135 Q24193
mp-Xylenes 0.07635 0.1 mg/kg 76 51-135 024193
o-Xylene 0.04017 0.05 mg/kg 80 49-137 024193
Toluene 0.03654 0.05 mg/kg 73 47-138 024193
Matrix Spike Duplicate necy Recovery RPD
Sample 1D RecuR Spike Mount Units RPD Range OCicts
183910 Benzene 0.03704 0.05 mg/kg 74 46-136 10 0-22 024193
Ethylbeozene 0.02507 0.05 mg/kg 50 51-1 35 30 0-23 024193
mp-Xylenes 0.05752 0.1 mg/kg 58 51-138 28 0-20 024193
o-Xylene 0.03177 0.05 mg/kg 64 49-1 37 23 0-22 024193
Toluene 0.03077 0.05 mg/kg 62 47-136 17 0-22 024193
Page of4
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No.37735
Level II QC Report
6/15/07
ESP Associates PA
Attn Chris Ward
Box 7030
Project ID Morehead Commons No COC Group Numbec G06071 93
DateITime Submitted 6/7107 1400
Charlotte NC 28241
tconlln Pann flrni by ---Oft4
Method Blank
cc
Result RL Control UmIt Uolfs ID
Gasoline Range Organics GRO ND 0.5 nigkg 024199
Laboratory Control Sample Recovery Recovery
Ranges DC BatchResultSpikeAmountUnitsID
Gasoline Range Organics GRO 2.055 mgfkg 103 64-124 024199
Matrix Spike ReC0VGJ Recovery
RangesSampleResultSpikeAmountUnits
183776 Gasoline Range Organlcs ORG 1.385 mgllrg 69 37-126 024199
Matrix Spike Duplicate Recovery RPD
Ranges RPD Range OC Batch
Sample ID Result Spike Amount Units ID
183776 Gasoline Range Organlcs GRO 1.442 mkg 72 37-125 0-34 024199
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories It449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-8001529-8394.Fax [phone]
Cadmium
Chromium
Lead
NC Certification No 402
SC Certification No 99012
NC Drinking Water CerL No 37735
mg/I 76 75-125 0-20 024208
mg/I 77 75-125 0-20 024208
mg/L 75 75-125 0-20 024208
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
TCIP Imaihnht Mmtln by ICP
riuthnI 6010B
Level II QC Report
6115/07
Project ID Morehead Commons No COC Group Number 00607193
Date/Time Submitted 6/7107 1400
Method Blank 00 Batch
Result RI ContmI Umit Units ID
ArsenIc 0.0016 0.05 0.025 mg/I 024208
Barium -0.0012 2.5 mg/I 024208
Cadmium -0.0016 0.025 0.0125 mg/I 024208
Chromium 0.0035 0.25 0.125 mg/I 024208
Lead 0.0064 0.05 0.025 mg/I 024208
Selenium -0.0005 0.05 0.025 mg/L 024208
Silver 0.0002 0.25 0.125 mg/I 024206
Laboratory Control Sample Rcoveiy R8COVOtY
Ranges Batch
Result Spike Amount Units 3k ID
Arsenic 0.2555 0.25 mpJL 102 80-120 024208
Barium 0.2298 0.25 mg/I 92 80-120 024208
Cadmium 0.2408 0.25 mgIL 96 80-120 024208
Chromium 0.2262 0.25 mg/I 90 80-120 024208
Lead 0.2276 0.25 mg/I 91 80-120 024208
Selenium 0.2475 0.25 mg/I-99 60-120 024208
SlIver 0.2393 0.25 mg/I 96 80-120 024208
Matrix Spike ReCOVS Reovej
Ranges 00 eatch
Sample iD Flasull Spike Amount Units ID
183684 Arsenic 0.2149 0.25 mg/I-90 75-125 024208
Barium 0.8706 0.25 mg/I 72 75-125 024208
CadmIum 0.1885 0.25 mg/I 75 75-125 024208
Chromium 0199 0.25 mg/I 77 75-125 024208
Lead 0.1996 0.25 mg/I 75 75-125 024208
Selenium 0.1899 0.25 mg/I 88 75-125 024208
SlIver 0.2304 0.25 mg/I 93 75-125 024208
Matrix Spike Duplicate RaCOV RPJ
Sample Result Spike Amnt Ranges RPI QC Batch
3k 3k ID
183684 ArsenIc
Barium
0.2148 0.25
0.8661 0.25
0.1911
0.2006
0.2001
mg/I 90 75-125
mg/I 71 75-125
Selenium
Silver
0.25
025
0.25
0-20 024208
0-20 024208
0.1891 0.25
0.2321 025
mg/I 85 75-125
mg/I 93 75-1 25
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories In449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-8001529-6364 Fac 7041525-0409
0-20 Q2420P
0-20
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 09012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Level II QC Report
6/15/07
COC Group Number G0607193
Date/Time Submitted 6/7107 1400
flincrvl P2nnn flrnmni lflPflt GC.FD method SOISB
Method Blank
Result RL Control Urntt Units IL
Diesel Range Organlcs DRO ND 3.5 mglkg Q24213
Laboratory Control Sample Recovery Recovery
Ranges
iiResult Spike Miounl Unite 1k
Diesel Range OrganlcsDRO 41.4 40 mg/kg 104 53-118 024213
Matrix Spike Recovery Recovery
RangesSample10ResultSpikeMrounUnttc Ii
183671 DIesel Range Organics DRO 47.0 40 mg/kg 118 52-119 024213
Matrix Spike Duplicate Recovery Recovely RPD
Ranges HP RangesampleResultSplicefunountUnits1k
183671 DieselRangeOrganlcsDRO 39.9 40 mg/kg 100 52-119 16 0-25 024213
TCLP Leachable Mercury by CVAA method 7470A
Method Blank
QC BatchResultHIControlUrnSUniteii
Mercury -0.00007 0.01 0.005 mg/I 024234
Laboratory Control Sample Recovery Recovery
itanges CC BatchResultSpikevnountUnits11
Mercury 0.00973 0.0093 mg/I 104 80-120 024234
Matrix Spike
Recovery Recovery
Ranges CC BatCh
Sample ID Result Spike hnaunt Unite tic ID
183685 Mercury 0.00928 0.0093 mg/I 100 80-120 024234
Matrix SpIke Duplicate
Recovery Recovery RPD
Ranges RPD RangeSample10ResultSpliceAmountUnits
183685 Mercury 0.00939 0.0093 mg/I 101 80-120 0-20 024234
-See Case Narrative
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449Spdngbrook Road P.O BOx 240543 Charlotte NC 28224-0543
Phone[phone] Toll Free Number 1-8001529-6354 Fax [phone] Page of
ACCESS
ANALYrICAL Iwc
ANALYTICAL REPORT
CLIENT
Prism Laboratories Inc
P0 BOX 240543
Charlotte NC 28224
ATTENTION
Angie Overcash
PROJECT ID
Prism Lab-G06071 93
LABORATORY REPORT NUMBER
207060924
DATE
06/1 4/2007
Primary Data Review By Secondary Data Review By
_____
Curtis Ekker Ashley AmickDataValidationManagerGCALProjectManager Access Analytical
aamickaccessanalytrcalinc corn
PLEASE NOTE
Unless otherwise noted all analysis on this report performed at Gulf Coast Analytical Labs GCAL 7979 GSRIRdBatonRougeLA70820
GCAL ISSCDHEC certified laboratory 73006 NCDENR certified lab 618 GA certified lab LA-01955 NELAPcertifiedlaboratory01955
Local support services for this project are provided by Access Analytical1 Inc.Access Analytical is representative ofGCALservingclientsintheSC/NC/GA areas All questions regarding this report should be directed to your local AccessAnalyticalrepresentativeat803.7814243 or toll free at 888.315.4243
CASE NARRATIVE
Client Prism Laboratories Inc Report 207060924
Gulf Coast Analytical Laboratories received and analyzed the samples listed
on the sample cross-reference page of this report Receipt of the samples is documented
by the attached chain of custody This applies only to the samples listed in this reportNosampleintegrityorqualitycontrolexceptionswereidentifiedunlessnotedbelow
No anomalies were found for the analyzed samples
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by
the
Environmental Protection Agency or other recognized agencies
The samples and their corresponding
extracts will be maintained for period of 30 days unless otherwise arranged Following this retention
period the samples will be disposed in accordance with GCALs Standard Operating Procedures
Common Abbreviations Utilized in this Report
ND Indicates the result was Not Detected at the specified RDLDOIndicatestheresultwasDilutedOut
Ml Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC indicates the analysis was Sub-Contracted
ELD Indicates the analysis was performed In the Field
PQL Practical Quantitation Limit
MDL Method Detection Limit
RDL Reporting Detection Limit
0000 Reported as time equivalent to 1200 AM
Reporting Flags Utilized in this Report
Indicates an estimated value
Indicates the compound was analyzed for but not detected
ORGANICS Indicates the analyte was detected in the associated Method Blank
INORGANICS Indicates the result is between the RDL and MDL
Sample receipt at GCAL is documented through the attached chain of custody In accordance with ISOGuide25 and NELAC this report shall be reproduced only in full and with the written permission of GCALTheresultscontainedwithinthisreportrelateonlytothesamplesreportedThedocumentedresultsare
presented within this report
This report pertains only to the samples listed in the Report Sample Summary and should be retainedas
permanent record thereof The results contained within this report are intended for the use of the clientAnyunauthorizeduseofthe information contained In this report Is prohibited
certify that this data package Is in compliance with the terms and conditions of the contract andStatementofWorkbothtechnicallyandforcompletenessforotherthantheconditionsInthecasenarrativeReleaseofthedatacontainedInthishardcopy data package and In the computer-readabledatasubmittedhasbeenauthorizedbytheQualityAssuranceManagerorhis/her designee as verified bythefollowingsignature
CURTIS EKKER
DATA VALIDATION MANAGERGCALREPORT207060924
THIS REPORT CONTAINS ______PAGES
Report Sample Summary
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
20706092401 103684 Solid 06/07/2007 1300 06/09/2007 0825
20706092402 183685 Solid 06/07/2007 1315 06/09/2007 0925
GCAL Report 207060924
Summary of Compounds Detected
rGcAL ID Client ID Matrix Collect Date/Time Receive DaIe/Tirnf
20706092401 183684 SolId 36/0712007 1300 06/09/20070925
SW-846 9056 Organic Halides
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 39.IB 46.0 19.9 mg/kg
GCAL ID Client ID Matrix Collect Date/Time Receive Dateflimi
20706092i02 183685 Solid 06/07/2007 13 15 06/09/20070925
SW-846 9056 Organic Halides
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 50.8 48.4 209 mg/kg
GCAL Report 207050924
SM 2540G Dry Weight
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
06111/2007 1350 JEM 350931
CAS Parameter Result RDI MDL Units
WET-037 Total MoIsture 13.0 0.010 0.010
RESULTS REPORTED ON DRY WEIGHT BASIS
GCAL Report 207060924
SW-846 9056 Organic Halides
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
06111/2007 0900 350917 SW-846 5050 06111/2007 1348 AEL 350918
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 39.1B 46.0 19.9 mg/kg
RESULTS REPORTED ON DRY WEIGHT BASIS
GCAL Report 207060924
SM 2540G Dry Weight
Prep Date Prep Batch
CAS
WET-037
Parameter
Total MoIsture
Prep Method Dilution Analyzed By Analytical Batch
06111/2007 1350 JEM 350931
RESULTS REPORTED ON DRY WEIGHT BASIS
Result RDL MDL Units
17.4 0.010 0.010
GCAL Report 207060924
RESULTS REPORTED ON DRY WEIGHT BASIS
SW-846 9056 Organic Halides
Prep Date Prep Batch
06111/2007 0900 350917
CAS
59473-04-U Total Organic Halides
Parameter
Prep Method DIlutIoN Analyzed By Anaytlcal Batch
SW-846 500 05111/2007 1405 AEI a50919
Result RDL MDL
50.8 48.4 20.9
Units
mglkg
GCAL Report 207060024
General Chemistry Quality Control Summary
naIyticaL Batch 350931 CHant ID
Prep patch N/A GCALID
Sample Type
Analytical Date
Matrix
CONTAMINATED SOIL
20706066501
SAMPLE
O11/2007 15C
Solid
495491 DUP
495912
DUP
0611112007 1360
Solid
SM 25400 Dry Weight Units
Result RDL
RPDResultRPDLimit
20.8 207 25WET-037 Total MoIsture 16.9 0.010
QCAL Report 207060924
General Chemistry Quality Control Summary
nalytical Batch 350918
Prep Batch 350917
Prep Method SW-845 5050
Client ID
GCAL 10
Sample Type
Prep Date
Analytical Date
Matrix
MB350917
495874
Method Blank
0611112007 0900
08111/2007 1203
Solid
LCS350917
495875
ICS
06/11/2007 0900
05/11/2007 1220
Solid
SW-846 9056 Organic Halides Units mg/kg
Result
Spike
Rlided
ControlRasult
Limits
59473-04-0 Total Organic Flalides 17.3U 17.3 2000 1990 80 120
nalytical Batch 350916
Prep Batch 350917
Prep Method SW-845 5050
Client ID
GCAL ID
Sample Typo
Prep Date
Analytical Date
Matrix
183690
20706092301
SAMPLE
06/11/2007 0900
06/11/2007 1238
Solid
4956921DLJP
495076
DUP
06/11/2007 0900
06/11/20071255
Solid
SW-846 9056 OrganIc Halides Units mg/kg
Result RDL
RPDResultRPDLimit
113 2559473-04-0 Total Organic HalIdes 108 17.3
Analytical Batch 351004
Prep Batch 351003
Prep Method SW-845 5050
ClIent ID
GCAL ID
Sample Type
Prop Date
Analytical Date
Matrix
MB351003
496190
Method Blank
00/11/2007 1100
08/11/2007 1450
Solid
LCS351003
496191
LOS
06/11/2007 1100
08/11/2007 1516
Soild
ControlResultLimits
SW-846 9056 Inorganic Anions UnIts mg/kg
Result
Spike
RUded
16837-00-6 ChlorIde
16984-48-8 FluorIde
24959-67-9 Bromide
WET-036 Total HalIdes
2.50U 2.50
2.401 2.40
5.40U 5.40
17U 17
500
500
1000
2000
474
501
1020
1990
94.8
100
102
99.6
80 120
80 120
00 120
80 120
GCAL Repoit 207060924
General Chemistry Quality Control Summary
naIytical Batch 351004
Prep Batch 351003
Prep Method SW-846 5050
Client ID
GCAL ID
Sample Typo
Prep Date
Analytical Date
Matrix
163690
20706092301
SAMPLE
0611112007 1100
06/1112007 1533
Solid
495892M9
496193
MS
06/11/2007 1100
05/11/2007 1608
Solid
SW-846 9056 Inorganic Anions UnIts mg/kg
Result
Spike
Rl1ded Result Control
Limits
16881-00-6 Chloride
16984-48-B Fluoride
2495957-9 Bromide
WET-036 Tolal Halides
43.0 2.50
74.0 2.40
0.000 5.40
117 17
500
500
1000
2000
542
574
1020
2140
99.8
100
102
101
75 125
75 125
75 125
75 125
thalytical Batch 351004
Prep Batch 351003
Prep Method SW-846 5050
Client ID
GCAL.ID
Sample Type
Prep Date
Analytical Date
Matrix
183690
20706092301
SAMPLE
08/11/2007 1100
05/11/2007 1533
Solid
495692DL1P
496192
DLIP
06/11/2007 1100
06/11/2007 1551
Solid
SW-846 9056 Inorganic Anions Result RPD
16887-00-6 Chloride
16984-48-8 Fluoride
24959-67-9 Bromide
WET-038 Total Halides
43.0 2.50
74.0 2.40
0000 5.40
117 17
44.0
74.0
0.000
118
2.3
0.65
25
25
25
25
GCAL Report 207060924
CHAIN OF CUSTODY RECORD
PAGE _L 0F.L QU ENSU PER BILLINGu_______________
Project Name 41 W..1...c
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reportçig OC LEVEL 111111 IV
provisions and/or OC Re rnpnts
Invoice To //4v
Address 4I7
Purchase Order No./SliIing Reference 1/D
Requested Due Data 01 Day 02 Days Days Days
OiDays
WorkIng Days 5-5 Days Standard 10 days 0ust Be
Samples received after 1500 will be processed next business dayTurnaroundtimeIsbasedonbusinessdaysexcludingweekends and holIdaysSEEREVERSEFOR TERMS CONDITIONS REGARDING SERVICESRENDERED BY PRISM LABORATORIES INC TO CUENT
Samplers Signature Sampled By Print Name Arfillatlon
Upon relInquishing this 9ftiii of Cs dy Is your authorlzaUon for Prism to proceed with the andIyses as requested above Any changes must besubmittedInwriting to the Prism Project Manager There will be charges for any changes after analyses have been initialized
Relinquished Ey SlnuIure ttgnewreJ
ReunqlJlaheis By Sllnalure Recveu by Siglialure elu
Relinquished Dy SIgnature el ad or us Lsbaratorie By/iMethodofShlprneiftSAMPLECDEISSHOULDSETAPED SH CUSTODY SEALS FOR TRANSPORTATION TO ThE LABORAYORYSAMLESARE NOT ACCEPTED AND VERIFIED AGAINST COG UNTIL RECEIVED AT ThE LABORATORY
lFadEx DUPS and-delivered 0PdsmFleidSrvfe ClOther
DaIj
/7ba
rctip No
Full Service Analytical Environmental SolutIons
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543Phone[phone] Fax [phone]
lient Company Name
leport To/Contact Name Li Vi
Leporting Address ______________________
hone _Fax Yes No
mail Yes No Email Address______________________DD Type PDF_Excel _Opler
ite Location Name J1f
ife Location Physical Address J-r1 .g
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
CertIfication NELAC USACE FL____NC
OThER _____N/A_____
Water Chlorinated YES_NO
Sample iced Upon Collection YES.jNO_
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
SOILWATER OR
SLUDGE
SAMPLE CONTAINER
PRESERVA-TIVES
ANALYSES REQUESTED4k4VAJY REMARKS PSBM
ID NO
TYPE
SEE BELOW Np SIZE-I
--
-7-
/io
jjj
MLrr______
___
vj $L
I83e
3183
usia VIflyOVUD Additional Comments
JPDES US GROUNDWATER DRINKING WATER
I-
SOLID WASTE RCRA CRCLA LANDFILL OTHERNCESCW1CQSC1ONCZISC1DNCUSCUNçUM.USCJ ONC DSCfDNC USC UNC USC
SEE flEVEUSE FOR
REtt1
Case NarrativePRISM
LA5ORAT0AE5.INC
Date 07126/07 ClIent Project ID Morehead Commons No.2
Company ESP Associates PA Prism CCC Group No 00707487
Contact Chris Ward Collection Dates 07/18/07
Address P.O Box 7030 Lab Submittal Dates 07/18/01
Charlotte NC 28241
This data package contains the analytical results for the project identified above and Includes Case Narrative Laboratory Report
and Quality
Control Data totaling 13 pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case naælive Quality
control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
aftected
Semi Volatile Analysis
Analysis Note for 025204 MSD 24-Trlchlorobenzene RPD value outside the control limits
Analysis Note for 025204 MSD 4-Dlclilorobenzene RPD value outside the control limits
Analysis Note for 025204 MSD 2Chlorophenoi RPD value outside the control limits
Analysis Note for 025204 MSD N-Nltrosodl-n-propylamlne RPD value outside the control limits
Analysis Note for 025204 MSD Phenol RPL value outside the control limits
Analysis Note for 025204 MSD Pyrene RPD value outsIde the control limits
Volatile Analysis
No Anomalies Reported
Metals Analysis
N/A
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by Paula Glileland Project Managec
Signature t.SL tIm.iL Signature
Review Date 07/26/07 Approval Date
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The anaiyte was positively Idenlified but the value is estimated below the reporting lImit
I-I Estimated concentration with high bias
Estimated concentration with law bias
matrix effoct is present
Angela Overcash
/0
Notes This report should not be reproduced except In its entirety without the writuen consent of Prism Laboratories1 Inc The results in thisreportrelateonlytothesamplessubmittedforanalysis
449 Sprtngbmak Road P.O Box 240543 Ghaztotte NC 28224-0403
Phone7Ol529-6354 ToVFree800/529.6384 Fax[phone]
.4
FuH$iAnaytkat EdmnmntaI5atuUon
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
This report should not be reproduced except In its entirety without the wiliten consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-9364 Fax [phone]
__
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Laboratory Report
07126/07
Sample Matrix Soil
Project ID Morehead Commons No Client Sample ID Camp of lal-S and
1b2-4
Prism Sample ID 187383
COC Group G0707487
Time Collected 07/18/07 1600
Time Submitted 07/18/07 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datefflme ID
Bls2-chloroethylether BRI pg/kg 370 40 821CC 07/25/07 1815 kcamplgouo 025204
Bls2-chloroisoprcpylether BRL pg/kg 370 31 8270C 07/25/07 1815 kcamplgoUo 025204
Bls2-ethylhexylphthalate BRI pg/kg 370 18 827CC 07/25/07 1815 kcamplgatto 025204
Butylbeny1phIhaJate SRI pg/kg 370 22 827CC 07/25107 1815 kcamplgouo 025204
Chrysene 640 pg/kg 370 61 8270C 07/25/07 1815 kcamplgotjo 025204
0I-n-butylphthajate BRL pg/kg 370 17 827CC 07/25/07 1815 kcamplgotto 025204
DI-n-octylphthalate SRI pg/kg 370 27 8270C 07/25/07 1815 kcamplgotlo 025204
Dlbenzoahanthracene BRL pg/kg 370 37 821CC 07/25/07 1815 kcsmplgotto 025204
Dlbenzofuran BRL pg/kg 370 31 8270C 07/25/07 1815 kcamptgoUo 025204
Dlethylphthalate BRL pg/kg 370 23 827cC 07/25/07 1815 kcamplgottu 025204
Dlmethylphthalate BRL pg/kg 370 25 827CC 07/2507 1815 kcarnplgotto 025204
Fluoranthene 2300 pg/kg 370 25 827CC 07/25/07 1815 kcarnplotto 025204
Fluorene BRL pg/kg 370 22 827CC 07/25/07 1815 kcamplgotto 025204
Hexachlorobenzene SRI pg/kg 370 19 827CC 07/25/07 1815 koamplgotto 025204
Hexachiorobutadlene BR.pg/kg 370 36 82700 07125/07 1815 keampigotto 025204
Hexachlorocyclopantadlene BRL pg/kg 370 39 827CC 07/25/07 1815 koaniplgoflo 025204
Hexachioroethane BRL pg/kg 370 37 8270C 07/25/07 1815 kcamptgotto 025204
lndeno123-cclpyrene BR.pg/kg 370 38 8270C 07/25/07 1815 kcarnplgotto Q25204
Isophorone SRI pg/kg 370 33 827CC 07/2507 1815 kcampIotIo 025204
N-Nltrosodl-n-propylamlne BRL pg/kg 370 42 8270C 07/25/07 1815 koamplgotto 025204
N-Nltrosodlphenytamjne BRL pg/kg 370 19 82700 07/25/07 1815 kcamplgotto 025204
Naphthalene BR.pg/kg 370 40 827CC 07/25/07 1815 koamplgotto 025204
Nitrobenzene BRL pg/kg 370 36 827CC 07/25/07 1815 kcamplgotto Q25204
Pentaclilorophenol SRI pg/kg 370 31 82700 07/25/07 1815 kcampigotto 025204
Phenanthrene 1200 pg/kg 370 18 82700 07/25/07 1815 kcamplgotto 025204
Phenol BRL pg/kg 370 40 82700 07/25/07 1815 kcamplgotto 025204
Pyrene 2100 pg/kg 370 25 82700 07/25/07 1815 kcamplgotto 025204
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
EnvkcnmenolSuiglon
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cart No 37735
Level II QC Report
7/26/07
Project ID Morehead Commons No COG GmUp Number G0707487
Date/Time Submitted 7/18/07 1635
InIett flm..nT 1.r.r.Ims ------826DB...-..y IIU2LIIUU
Method Blank
00 BatchResultFtControlLiniltUnttsto
11 1-Trichloroelhane ND 0.005 0.0025 mg/kg 025185
122-Tetrachloroethane ND 0.005 0.0025 mglkg 025155
12-Thchloroethane ND 0.005 0.0025 mg/kg 025185
111-Dlchloroefhane ND 0.005 0.0025 mg/kg 025185
11-DichloroeUierie ND 0.005 0.0025 mg/kg 025185
11-Dichloropropene ND 0.005 0.0025 mg/kg 025185
23-Thchlorobeazene ND 0.005 0.0025 mg/kg 025185
123-Trictilompropane ND 0.005 0.0025 mg/kg 025185
24-Trichlorobenzene ND 0.005 0.0025 mg/kg 025185
124-Trlmethyibenzene ND 0.005 0.0025 mg/kg 025185
2-Dlbromoethane EDB ND 0.005 0.0025 mg/kg 025185
12-Dlchlorobenzene ND 0.005 0.0025 mg/kg 025185
12-Dlchiornethane ND 0.005 0.0025 mg/kg Q25185
1.2-Dichioropropane ND 0.005 0.0025 mg/kg Q25185
135-Trimethylbeozene ND 0.005 0.0025 mg/kg 025185
13-Dlchiorobenzene ND 0.005 0.0025 mg/kg 025185
13-Dichioroprupane ND 0.005 0.0025 mg/kg Q25185
14-Dtchlorobenzene ND 0.005 0.0025 mg/kg 025185
22-Dichioropropane ND 0.005 0.0025 mg/kg 025185
2-Chiorototusne ND 0.005 0.0025 mg/kg 025185
2-1-lexanone ND 0.05 0.025 mg/kg 025185
4-Chtorotoluene MD 0.005 0.0025 mg/kg 025185
4-Methyi-2-pentanone MlBK ND 0.05 0.025 mg/kg 025185
Acetone ND 0.05 0.025 mg/kg Q251 85
Benzene NI 0.003 0.0015 mg/kg 025185
Bromobenene ND 0.005 0.0025 mg/kg 025185
Bromochiommethane ND 0.005 0.0025 mg/kg 025185
Bromodjchforomethane ND 0.005 0.0025 mg/kg 025185
Brorooform ND 0.005 0.0025 mg/kg 025185
Bramomethane ND 0.01 0.005 mg/kg 025185
Carbon tetrachjojkle ND 0.005 0.0025 mg/kg 025185
Chlorobenzene ND 0.005 0.0025 mg/kg 025185
Chlorocfibromomethane ND 0.005 0.0025 mg/kg 025185
ChIonethgne ND 0.01 0.005 mg/kg Q25185
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc449SpringbrooicRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number l-8001529-6364 Fax [phone] Pagel of6
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except In its entirety without the written consent of Prism LaboratorIes Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone[phone] Tell Free Number 1-800/529.6364 Fax[phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water CerL No 37735
Level II QC Report
7/26/07
Project ID Morehead Commons No COG Group Number G0707487
Datefflme Submitted 7/18/07 1635
Method Blank QC Batth
Result RI CoroUmlt Unils ID
Chloroform ND 0.005 0.0025 mg/kg 025185
Chioromethane ND 0.005 0.0025 mg/kg 025185
cls-1 2-Dichlorcetherte ND 0.005 0.0025 mg/kg 025185
ole-I .3-Dichioropropene ND 0.005 0.0025 mg/kg 0251 85
Dichlorodifluoromethane ND 0.005 0.0025 mg/kg 025185
Ethyibenzene ND 0.005 0.0025 mg/kg 025185
Isopropyl ether IPE ND 0.005 0.0025 mg/kg 025185
lsopropylbenzene ND 0.005 0.0025 mg/kg Q251 85
mp-Xylenes ND 0.01 0.005 mg/kg 0251 85
Methyl ethyl ketone MEK ND 0.1 0.05 mg/kg 025185
Methyl ether MTBE ND 0.01 0.005 mg/kg Q25185
Methylene chloride ND 0.005 0.0025 mg/kg 025185
n-Butylberizerte ND 0.005 0.0025 mg/kg 025185
n-Propylhenzene ND 0.005 0.0025 mg/kg 025185
Naphthalene NI 0.01 0.005 mg/kg 025185
o-Xylene ND 0.005 0.0025 mg/kg 025185
p-lscpropyltoluene ND 0.005 0.0025 mu/kg 025185
sec-Butylbenzene ND 0.005 0.0025 mg/kg 025185
Styrene ND 0.005 0.0025 mg/kg 025185
tert-Butylbenzene ND 0.005 0.0025 mg/kg 025185
Tetrachloroethene ND 0.005 0.0025 mg/kg 025185
Toluerie ND 0.005 0.0025 mg/kg 025185
trans-I 2-Dichloroethene ND 0.005 0.0025 mg/kg 025185
trans-I .3-DichiorOpropene ND 0.005 0.0025 mg/kg 025185
Trichioroetbene ND 0.005 00025 mg/kg 025185
Trichlorofluoromethane ND 0.005 0.0025 mg/kg 025185
Vinyl acetate ND 0.025 0.0125 mg/kg 025185
Vinyl chloride Nt 0.005 0.0025 mg/kg 025185
Laboratory Control Sample pyy ove
Result SplknArnount Unfis to
.1-Dfchloroelhene 0.05615 0.05 mg/kg 112 57-122 025185
Benzene 0.0506 0.05 mg/kg 101 62-119 025185
Chtombenzene 0.05235 0.05 mg/kg 105 61-124 025185
Toluerte 0.05132 0.05 mg/kg 103 57-122 025185
Trichloroetliene 0.05338 0.05 mg/ks 107 59-129 025185
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in lb entirely without the written consent of Prism LaboratorIes Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-8001529.6364 Fax 704I525-ui4o
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cerl No 37735
Level 11 QC Repori
7/26/07
Project ID Morehead Commons No COC Group Number G0707487
Date/Time Submitted 7/18/07 1635
Matrix Spike Recovery Recovery
RangesSampleIDResultSpikeMiountUnits ID
187298 11-Dlchloroethene 0.05573 0.05 mg/kg 111 44-140 025185
Benzene 0.05019 0.05 mg/kg 100 46-136 025185
Chlorobenzene 0.05013 0.05 mg/kg 100 47-135 025185
Toluene 0.0514 0.05 mg/kg 103 47-136 025185
Tricliloroethene 0.05146 0.05 mg/kg 103 45-141 025185
Matrix Spike Duplicate Rvery Recovery RPD
Ranges RPD Range 00 BSIdlSample ID Result Spike Miount Untie ID
187298 1-Dlchlorcethene 0.05476 0.05 mg/kg 110 44-140 0-23 Q25185
Benzene 0.05001 0.05 mg/kg 100 46-136 0-22 025185
Chlcrabenzerie 0.05017 0.05 mg/kg 100 47-135 0-22 025185
Toluene 0.05054 0.05 mg/kg 101 47-1 36 0-22 025185
Trichloroethene 0.05102 0.05 mg/kg 102 45-1 41 0-23 025185
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
24-Trichiorobenzene
.2-Dlchiorcbenzene
3-Dlthlorobenzene
4Dlchtorobenzene
245-Tiiclilorophenol
246-Itichiorophenol
24-Dichiorophenol
24-Dlmethylplienol
2.4Dinitrophenol
24-Dlnilrotoluene
26-Dinitrotoluene
2-Chloronaphthaene
2-Chlorcphenol
2-Methyinaphthaiene
2-Methyiphenol
2-Nitrophenol
34-Methylphenol
S3-Dlchlorobenzldlrie
4.6-Dinitro-2methyiphenoI
4Bronlophenylphenylether
4-Chlom-3-methyipheno
4-Chloroanillne
4-Chtorophenylphenylether
4Nitrophenol
Acenaphthene
Acenaphthytene
Anthracene
Azobenzene
Benzoaanthracano
Benzoapyrene
Benzobfluoranlliene
Benzoghipejylene
Benzoklluuranthene
Benzolc acid
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
7126107
Project ID Morehead Commons No COC Group Number 00707487
DatelTime Submitted 7/18/07 1635
SemI-voI2fltP flminir Cnmnnrn IIIMO .k....l aYsnf
Method Blank
OCBatciiResultRIControltJmkUnitsin
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg Q25204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 1.65 0.825 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.66 0.33 mg/kg 025204
ND 1.65 0.825 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.66 0.33 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 1.65 0.825 mg/kg 025204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.155 mg/kg 025204ND0.33 0.165 mg/kg 025204ND1.65 0.825 mg/kg 025204
ND 0.33 0.155 mg/kg 025204
ND 0.33 0.165 mg/kg Q25204
ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204ND0.33 0.165 mg/kg 025204ND1.65 0.825 mg/kg 025204
This report should not be reproduced except In Its entirety without the written censent of Prism Laboratories Inc449SpringhrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-800/529.6354 Far 7041526-0409 Page of
Charlotte NC 28241
NC Certification No 402 Level II QC ReportSCCertificationNo99012
NC Drinking Water Cerl No 37735
Project ID Moreheaci Commons No COC Group Number 30707487
Date/Time Submitted 7/18107 1635
Method Blank
00 BatchResuLRLControlUmitlinUs
Benayl alcohol
Bls2-chforoelhoxymethane
BIs2-chloroethylether
BIs2-chlorolsopropylether
Bis2-ethylhexylphthalate
Butylbenzylphthalate
Chrysena
Di-n-butylphthalate
D1-n-octyfphthalate
Dlbenzoa.hanthracene
DIbenofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachiorobeazene
HexaÆhjorobutadjene
Hexachlorocycloperitadiene
Hexacliloroethane
lndeno123-cdpyrene
Isophorone
N-Nltmsodl-n-pmpylamine
N-Nltiosodlphenylarnlna
Naphthalene
Nltrobenzerte
Pentachiorophenot
Phenanlhrene
Phenol
Pyrena
14-Dkilorobenzene
24-Dinltrotoluene
2-Chiomphenol
4-Chloro..3-methylphenol
ND 0.66 0.33 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.105 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
ND 1.65 0.625 mg/kg
ND 0.33 0.165 mg/kg
ND 0.33 0.165 mg/kg
Nt 0.33 0.165 mg/kg
121800 1.6929
1.19566 1.6929
1.49255 16929
1.29891 1.6929
1.37000 1.6929
025204
025204
025204
025204
025204
025204
025204
025204
025204
025204
025204
Q25204
025204
025204
025204
025204
025204
Q25204
025204
025204
025204
025204
025204
025204
025204
025204
025204
Q25204
025204
025204
Q25204
025204
025204
025204
ESP Associates PA
Attn Chris Ward
Box 7030
7126/07
Laboratory Control Sample
Recovery Rery ac BatrhResultSpikeAmauntLinUsID
l24-Trlchiorobenzene mg/kg 72 39-98
mg/kg 71 37-95
mg/kg 88 56.128
mg/kg 77 37-98
mg/kg 81 45-111
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone].Toll Free Number 1-800/529-6364 Fax [phone] Page of
NC CertifIcation No.402 Level II QC ReportScCertificationNo99012
NC Drinking Water Celt No 37735
Project ID Morehead Commons No COG Group Number G0707487
Daternme Submitted 7/18/07 1635
4-DIchJorobenzne
24-Dlnlhntoluene
2-Chlomphenol
4-Chloro-3-methylphenol
4-Nltrophenol
Acenaphihene
N-Nltrosodi-n-propylamine
PentathlOrophonol
Phenol
Pyrene
0.66433 1.667
0.61333 1.667
1.38933 1.667
0.72933 1.667
1.14633 1.667
1.52533 1.667
1.24933 1.667
0.95666 1.667
1.50033 1.667
0.71933 1.667
1.54568 1.667
mg/kg 40 26-97
mg/kg 37 23-92
mg/kg B3 45-127
mg/kg 44 25-94
mg/kg 69 31-113
mg/kg 92 17-150
mg/kg 75 36-107
mg/hg 57 22-105
mg/kg 90 39-131
mg/kg 43 23-97
mg/kg 93 45-133
63 0-37 025204
66 0-36 025204
10 0-29 025204
62 0-37 025204
21 0-32 Q25204
0-32 025204
0-32 025204
40 0-37 025204
0-27 025204
61 0-42 Q25204
32 0-27 Q25204
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte1 NC 28224-0543Phone[phone] Toll Free Number 1-800/5294364 Fax[phone]
ESP Associates PA
Attti Chris Ward
P.O Box 7030
Charlotte NC 28241
7/26/07
Laboratoiy Control Sample Recovery QC Batth
Result Spike Miount ID
4-Nitrophenol 1.64014 1.6929 mg/kg 97 20-157 025204
Acenaphthene 1.32159 1.6929 mg/kg 78 44-110 025204
N-Nltmsodl-n-propylamjrie 1.28672 1.6929 mg/kg 76 38-101 025204
Pentachlorophenol 1.65132 1.6929 mg/kg 98 53-127 025204
Phenol 1.41299 1.6929 mg/kg 83 34-102 025204
Pyrene 1.81482 1.6929 mg/kg 107 54-131 025204
Matrix Spike Pcovery Recoveiy OC Bich
Sample ID Result Spike Miount Units ID
187298 124-Trichjorobenzene 1.27366 1.667 mg/kg 76 26-97 025204
1.4-Dichlorobenzene 1.22065 1.667 mg/kg 73 23-92 025204
24-Dlnitrotoluene 1.53066 1.667 mg/kg 92 45-127 025204
2-Chlomphenol 1.383 1.667 mg/kg 83 25-94 025204
4-Chloro-3-methylphenol 1.42233 1.667 mg/kg 85 31-113 025204
4-Nitmpllanol 1.633 1.667 mg/kg 98 17-150 025204
Acenaphthene 1299 1.667 mg/kg 78 36-107 025204
N-Nltrosodl.n-propylamine 1.43266 1.667 mg/kg 86 22-105 025204
Penlachlorcphenol 1.61033 1.667 mg/kg 97 39-137 025204
Phenol 1.34865 1.667 mg/kg 81 23-97 025204
Pyrene 2.1 3833 1.657 mg/kg 128 45-133 025204
Matrix Spike Duplicate
Recovery Ruveni ppi OC BatchSampleI/k Resull Spike ount ID
187298 124-Trjchlorobenzene
5-See Case Narrative
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449 Springbrook Road P.O Box 2405431 Charlotte NO 282241543Phone[phone] Fax 7042E-09
Client Company Name Aaij
Report Te/Contact Name 44.Y
Reporting Address ______________________________
Fax Yes No
CHAIN OF CUSTODY RECORD
PAGE.J.0F...L QUOTE EN ROPER B1LUN0
Project Name Jr
Short Hold Analysis Yes No UST Projeot Yes No
eplease ATFACH any project specific reporting QC LEVEL 11111 IV
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Invoice To Lh
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Email Yes No Email Address_____________________
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Site Location Name ______________________________
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Ip.t n.s4-l s.i
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NoJBillin Reference
Requested Due Date Day 02 Days 03 Days Ci DaYS Days
Working Days 69 Days Standard 10 days SL Be
Samples received after 1500 wfli he processed next busIness day
Turnaround time Is based on busIness days excluding weekends arid hodays
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FOR TERMS CONDITIONS REGARDING SERVICESRENDERED BY PRISM LABORATORIES INC TO CUENfl
TO BE FILLED IN BY CLIENT/SAMPUNGPRSONNEL
Certification NELACJJSACE_FL____NC.jL
SC_OTHER _____N/A _____
Water Chlorinated YES NO
Sample Iced Upon Collection YES...N0_
CUENT
SAMPLE DESCRIPTION
DATECOLLECTED
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MILITARY
MATRIX
SOILWATER OR
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSES REQUESTED
REMARKS
PRISM
ID NOSEEBELOWNOSiZE
%-4TI/-7
z-g
7/
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L/
/oo$
/C/Diiizô
/2c ___
TL
CI
cpic
Samplers Signature Sampled By Print Name AffilIatIon
Upon relinquIshIng thIaln of C.t dy Is your authorization for Prism to proceed with the analyses as requested above Any changes
must besubmittedlnwritingtothePrismProjectManagerTherewillbechargesforanychangesafteranalyseshave been
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cliciriwie North cci vIlija 28241
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Raleigh Wilmington Concord14001 Weston Parkway 2120-fl CapitaiDrive 4601 Corporate Drive NWSuite100WilmingtonNon/i camihia 28/05 Suite 165aiMart/i Camlina 27513 910.3/3.6648 Concord North Carolina 28027919.678.1070 704 793.9855
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