Item No 33 - Initial Assessment Report Morehead Common Site -OCR

Mo res
FN
IR
ret
ixoI
Fe By
Dear Mr Schiff
On behalf of the property owner Beazer Homes ESP Associates P.A is pleased to provide the
attached Initial Assessment Report for the closure of the subject propertys petroleum release
ESP respectively requests classification of the release as Low Risk and issuance of no further
action notice
Thank you for your attention in this matter If you should have any questions please do not
hesitate to contact me at 803 835-0915
Sincerely
ESP Associates P.A
ie Rogers
Staff Scientist
cc Mr Jade Eastridge Beazer Homes
Environmental Services Manager
NC License No 1600
P.O Box 7030 Charlotte NC 28241
1.800.960.7317 NC 7045834949 fax [phone] SC 803.802.2440 fax [phone]
www.espassociates.com
August 20 2007
$ESP
ESP Associates P.A
NCDENR
UST Section
Mooresville Regional Office
919 North Main Street
Mooresville North Carolina 28115
Attention Mr Allen Schiff
Reference INITIAL ASSESSMENT REPORT
Morehead Common Site Area
1018 Post Street
Charlotte Mecklenburg County North Carolina
UST Incident No Not Yet Assigned
ESP Project No E6-UD42.601
PG
Initial Assessment Report
SITE INFORMATION
Site Identification
Date of Report
Facility ID
Incident Number Not Yet Assigned
Site Rank Unknown
Site Name Morehead Common Site Area
Site Street Address 1018 Post Street
City/County/Zip Code Charlotte Mecklenburg County 28278
Description of Geographical Data Point Approximate center of former vault
Location Method Mecklenburg County Polaris GIS Map
Latitude 35.227
Longitude -80.8600
Information about Contacts Associated with the Release
AST Owner Beazer Homes
1300 Blvd Suite Charlotte NC 28203-4265
704.370.7200
N/A
Same as above
ESP Associates P.A Chris Ward PG
P0 Box 7030 Charlotte NC 28241
803.835.0915
Prism Laboratories Inc
P0 Box 240543 Charlotte NC 28224-0403
704.529.6364
NC Certification No 402
Information about Release
f1 Date Discovered May 17 2007
11 Estimated Quantity of Release Unknown
Cause of Release
Source of Release
Size and contents of AST or
other containment from which the release occurred NA
Certification
Ward Professional Geologist for ESP Associates P.A do certify that the
contained in this report is correct and accurate to the best of my knowledge
Associates P.A is licensed to practice both geology and engineering in North Carolina
Associates certification numbers are Geology C-347 and Engineering C-0587
August 20 2007
N/A
AST Operator
Property Owner
Property Occupant
rJ Consultant/Contractor
Analytical Laboratory
Same as above
Unknown
Below ground septic system-type concrete vault
Initial Assessment Report ESP Project E6-UD42 601
Morehead Common Site Area August 20 2007
INTRODUCTION
The undeveloped subject site is located on the north side of Post Street approximately 400 feet
west of its intersection with South Clarkson Street on Tax Parcel No 07325213 in Charlotte
Mecklenburg County North Carolina see Figures and The site had an address of 1018
Post Street and was reportedly once occupied by Ohio Chemical Surgical Equipment but has
been vacant since 1965 The area of the subject release associated with an unearthed septic
tank-type concrete vault has been designated by ESP as Area of the Morehead Common Site
SITE HISTORY AND CHARACTERIZATION
On May 17 2007
ESP responded on behalf of Beazer Homes to an encounter with potentially
impacted soil during mass grading operations at the subject site Upon arrival at the site ESP
observed soils with slight petroleum odor located beneath an unearthed septic tank-type
concrete vault which had just been excavated by the sites grading contractor As required
following receipt of laboratory results confirming release had occurred ESP emailed
notification of the release discovery to Mr Steve Bograd of the Mooresville Regional Office of
NCDENR on May 30 2007
Release Location
The subject site is located within an urban area of Charlotte which historically included
warehouse and retail structures The site is currently mass graded and being developed as
mixed-use residential/commercial development see Figures and Based on our review of
the Geologic Map of North Carolina 1985 the subject site is located within the Charlotte Belt
locally comprised of intrusive metamorphosed granitic rocks locally pinkish gray massive to
weakly foliated and containing hornblende Soils encountered in this area are the residual
product of chemical weathering of rock presently underlying
the site Soil weathering is more
advanced near the surface grading with depth to less weathered rock and finally bedrock
Initial Assessment Report ESP Project E6-UD42 601
MoreheadCoinmon Site Area August 20 2007
AST Information
septic system-type concrete vault measuring approximately
ft ft ft deep was
uncovered and unearthed during mass grading operations
at the subject site by Gelder Thompson
of Midland North Carolina The roof of the vault had been covered with boards and layer of
soil Piping protruded
into the vault at two points but the piping ended within feet outside of the
vault See site photographs in Appendix
Previous Reporting
As required ESP submitted 24-Hour Release Notification by email to the Mooresville
Regional Office of NCDENR on May 30 2007 see Appendix Additionally ESP prepared
20-Day Report which was submitted to the Mooresville Regional Office of NCDENR on July
18 2007
Waste Characterization Sampling
On May 17 2007 using backhoe ESP collected waste characterization soil sample SP-1
from immediately below the recently excavated concrete vault at depth of approximately feet
below land surface BLS representative portion
of the soil sample was screened in the field
with an organic vapor analyzer OVA and recorded reading of 10 ppm Soil sample SP-1 was
submitted to Prism Laboratories of Charlotte North Carolina for analysis of total petroleum
hydrocarbons TPH for diesel range organics DRO and gasoline range organics GRO oil
grease OG by EPA Method 9071A volatile organic compounds VOCs by EPA Method
8260B pesticides by EPA Method 8081A PCBs by EPA Method 8082 and for total lead and
chromium by EPA Method 60 lOB Waste characterization soil sample SP-l was collected and
analyzed to document that release had occurred and to characterize contaminant types and
concentrations to aid in the assessment and subsequent off-site permitted disposal/treatment of
impacted soils
Initial Assessment Report ESP Project E6-UD42 601
Morehead Common Site Area August 20 2007
As revealed by the laboratory data report for SP-l TPH-DRO was reported at concentration of
420 mg/Kg OG at 3400 mg/Kg chromium at 22 mg/Kg lead at 51 mg/Kg and the PCB-l260
at 5.1 mg/Kg Results for all remaining analytes
were reported to be below reporting limits
BRLs Analytical results for SP-1 are summarized on Table B-i See Figure for soil
sample location map See the attached Prism laboratory data report in Appendix
INITIAL ABATEMENT ACTIVITIES
Soil Excavation and Stockpile Sampling
Following excavation and removal of the concrete vault and the May 17 collection of waste
characterization sample SP-approximately two feet of structural fill was placed over the
former vault excavation and surrounding area by the sites grading contractor as part of the sites
mass grading On June 2007 ESP observed the removal of the recently placed non-impacted
structurally placed fill from the concrete vault area until residual soils where encountered ESP
then documented the excavation of 86.25 tons of impacted soils from Area by the sites
grading contractor The excavation was advanced based on OVA readings and evidence of
visible staining The resulting excavation including the non-impacted structural fill measured
approximately 30 ft 50 ft 10 ft deep Neither groundwater bedrock nor free product were
encountered within the tank pit
Non-impacted structure fill was placed to the side while excavated impacted soil was placed on
and covered with plastic awaiting subsequent off-site permitted disposal
On June 2007 ESP
collected two composite soil samples from the impacted soil stockpile for laboratory analysis
The soil samples designated and ib were placed in laboratory provided containers
labeled
and hand delivered on ice to Prism Laboratories for compositing and subsequent analysis The
samples were analyzed for TPH-GRO/DRO BTEX by EPA Method 8260B TCLP-metals and
TCLP-Total Organic Halides TOX Results of the laboratory analysis summarized on Table
Initial Assessment Report ESP Project E6-UD42 601
Morehead Common Site Area August 20 2007
B-2 revealed elevated TPH-DRO and TCLP-TOX concentrations All other analyzed
constituents were BRL
Due to elevated TCLP-TOX results subsequent composite soil sample lab was collected
from the stockpiled soil on July 18 2007 and analyzed for VOC by EPA Method 8260B and for
semi-volatile organic compounds SVOCs by EPA Method 8270C Results of the laboratory
analysis as summarized on Table B-2 revealed elevated concentrations of various SVOCs while
VOCs were all reported to be BRL
On July 31 2007
86.25 tons of previously stockpiled soil from the Area excavation was
transported to the CMS Landfill in Concord North Carolina for permitted disposal see non-
hazardous waste manifest in Appendix
Confirmatory Sampling
On June 2007 following excavation of the vault area Area confirmatory soil samples were
collected at depth of feet BLS from each of the excavations four sidewalls WS-through
WS-4 while one soil sample was collected at depth of 10 feet BLS from the base of the
excavation B-i The five soil samples were hand delivered on ice to Prism Laboratories to be
analyzed for VOçs by EPA Method 8260B SVOCs by EPA Method 8270C pesticides by EPA
Method 8081A PCBs by EPA Method 8082 VPH/EPH by the Massachusetts Department of
Environmental Protection MADEP Method and for total lead and chromium by EPA Method
60 lOB Sample locations and excavation dimensions are depicted on Figure Soil Sample
Location Map Sampling was performed in general accordance with ESPs SOP see
Appendix
Results of the laboratory analysis
of confirmatory soil samples WS-l through WS-4 and B-i
revealed that all analyzed constituents were BRL with the exception of acetone common
laboratory contaminant in WS-2 and total lead and chromium is all samples however all
Initial Assessment Report ESP Project E6-UD42.601
Morehead Common Site Area August 20 2007
analyzed constituents were reported to be below their soil-to-groundwater MSCC Laboratory
analytical results for the confirmatory soil samples are summarized on Table B-i The Prism
laboratory data reports are included as Appendix
1500-RADIUS RECEPTOR SURVEY
On July 20 2007
Mr Eddie Rogers of ESP performed receptor survey to document the
presence or absence of active and/or inactive water supply wells within 1500-foot radius of the
subject release see Figure Receptor Survey Map The receptor survey
included interviews
with available site occupants and visual observations for water supply wells and/or municipal
water meters All properties within 500 feet of the site were visited to determine well status
The area within 1000 feet of the subject release consists of commercial and industrial
development with numerous vacant structures No active or inactive water supply wells were
identified within 1000-foot radius of the subject release Municipal water and sewer have
historically been available within the area of the site Additionally no surface water bodies were
identified within 500 feet of the release see Figures and
Initial Assessment Report ESP Project E6-UD42 601
Morehead Common Site Area August 20 2007
CONCLUSIONS AND RECOMMENDATIONS
The following conclusions have been formulated based on our completion of field activities
including abatement activities receptor survey and our review of laboratory data from the
analysis of collected soil samples
The subject site is located on the north side of Post Street approximately 400 feet west of
its intersection with South Clarkson Street on Tax Parcel No 07325213 in Charlotte
Mecklenburg County North Carolina
ri On May 17 2007
ESP responded on behalf of Beazer Homes to an encounter with
potentially impacted soil during mass grading operations
at the subject site Upon
arriving at the site ESP observed soils with slight petroleum odor located beneath an
unearthed septic tank-type concrete vault which had just been excavated by the sites
grading contractor The vault measured approximately ft ft ft deep
r1 Analysis of waste characterization soil sample SP-1 revealed TPH-DRO at
concentration of 420 mg/Kg OG at 3400 mg/Kg chromium at 22 mg/Kg lead at 51
mg/Kg and the PCB-1260 at 5.1 mg/Kg Results for all remaining analytes were BRLs
On June 2007 ESP documented the excavation of 86.25 tons of impacted soil from
Area No for subsequent permitted disposal
at the CMS Landfill in Concord North
Carolina
The resulting excavation measured approximately 30 ft 50 ft 10 ft deep Neither
groundwater bedrock
nor free product was encountered within the tank pit
ri On June 2007 following excavation of the vault area confirmatory soil samples were
collected at depth of feet BLS from each of the excavations four sidewalls WS-1
through WS-4 while one soil sample was collected at depth of 10 feet BLS from the
base of the excavation B-i
Results of the laboratory analysis of confirmatory soil samples WS-1 through WS-4 and
B-i revealed that all analyzed constituents were BRL with the exception of acetone
common laboratory contaminant in WS-2 and total lead and chromium is all samples
InitialAssessment Report ESP Project E6-UD42.601
Morehead Common Site Area August 20 2007
however all analyzed constituents were reported to be below their soil-to-groundwater
MSCC
Municipal water and sewer are available in the immediate vicinity of the release
No water supply wells were identified within 1000 feet of the release and
No surface water bodies were identified within 500 feet of the subject release
Based on the documented absence of any analyzed parameter
above North Carolina soil-to-
groundwater MSCCs in site soils ESP recommends that the subject release be issued no further
action notice and the incident closed
Attachments
Table B-i Summary of Soil Sampling Results
Table B-2 Summary of Stockpile Sampling Results
Figure Topographic Site Location Map
Figure 2005 Aerial Photograph
Figure Soil Sample Location Map
Figure Receptor Survey Map
Appendix 24-Hour Release Notification Email
Appendix Non Hazardous Waste Manifests
Appendix Site Photographs
Appendix ESPs SOP
Appendix Prism Laboratory Data Reports
ATTACHMENTS
TABLES
Table B-i Summary
Date 7/26/07 Incident No.Not Yet Assigned
8015B
11
of Soil Sampling Results
Morehead_Common Area No Charlotte North Carolina
6/6/07
Soil Groundwater MSCC mg/kg
Residential CC mgikg
In ustral/ommercial MSCC mg/kg
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
8015B MADEP MADEP MADEP MADEP MADEP
MADEP 9071A 9071AEPH EPH EPFI VPH VPH VPH
Considered immobile
NA Not Analyzed NL Not Listed
-I-1.1a1ie I--
Iate 72.U7 Incident No NoL Vet .\ssincd
Analytical Method
Contaminant ol Concern
Sample latc Source Sample Incident
ID Collected Area Depth PhaseddvILUGS
Summary of Soil Sampling Results
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
8260B 8260B 8260B
8081A 8082
Table B-i Summary of Soil Sampling Results
Date 7/26/07 Incident No Not Yet Assigned Morehead_Common Area No 2__Charlotte_North_Carolina ______
AnaLytical Method
_________Contaminant of Concerii
Sample Source Sample lTlij
ID Collected Area Depth Phase
m/dd/yy__1 ft._BGS _______ _______ _______ _______ _______ _______ _______ ________ _______
5/17/07 Waste Initial 0.014 0.0068 0.0068 BRLIDAbatement
E-
-u
.c
C-
5.1
B-i 6/6/07
WS-1 6/6/07 West Pit
Wall
Initial
Abatement 0.013 0.0066 0.0066 BRL 0.061
WS-2 6/6/07 North Pit
Wall
Initial
Abatement 0.0 12 0.0060 0.0060 BRL 0.058
WS-3 6/6/07 East Pit
Wall
Initial
Abatement 0.012 0.0061 0.0061 BRL 0.060
WS-4 6/6/07 South Pit
Wall
Initial
Abatement 0.020 0.0067 0.0067
BRL 0.058
Pit Floor 10
Initial
Abatement 0.013 0.0063 0.0063 BRL 0.057
4.6 NL
3129 3200 1560
--NL
81760 82000 40000
--NL
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobile
NA Not Analyzed NL Not Listed
FIGURES
FiGURE
TOPOGRAPHIC SiTE LOCA 170N MAPUSGSCHARLOTTEEASTQUADRANGLE
MOREHEAD COMMON SiTE
CHARLOTTE NORTH CAROLINA
ESP ESP Assootes PA
P0 7030
CIlIl1p NC 28241
347 Lkrop BldFoMdlSC29708
704 03 4949 NC
801 b02 2440 SC
FIGURE
2005 AERIAL PHOTOGRAPH
MOREHEAD COMMON SiTE
CHARLOTTE NORTH CAROLINA
LEGEND
WS-3
WS-4
CONFIRMA TORY SOIL SAMPLE
WASTE CHARACTERIZA liON SAMPLE
WS-2
20
APPROXIMATE SCALE
IN FEET
ws-l
FORMER CONCRETE VAULT
EXCA VA 770N DEPTH OF 10 FEET
17004260 SHEET 17TLE FIGURE
ate PACALENTSSOILSAMPLELOCATiONMAPAREA
7/11/07
RAM.I BYDMH PROJECT MOREHEAD COMMON ShECHECKED
CHARLOTTE NORTH CAROLINA
tt11k
-1f/
F7CURE
RECEPTOR SURWY MAP
AREA
MOREHEAD COMMON ShE
CHARLOTTE NORTH CAROLINA
ESP Assocotpo P.A
P0 7030
ChorIo0 OC 28241
3475 Lkro BOO
II SC 29708
704 083 4949 19C1
003 802 2440 7C1
APPENDIX
24-HOUR RELEASE NOTIFICATION EMAIL
Page lof3
Chris Ward
From Chris Ward
Sent Wednesday May 30 2007 144 PM
To Steve.Bogradncmau.net
Cc Jade Eastridge [e-mail] [e-mail]
Subject RE 24-Hour Notification Incidents No and
Attachments Incidents Nos and 3.pdf
Please see attachment that was left off the original email
.._____.._
From Chris Ward
Sent Wednesday May 30 2007 140 PMToSteve.Bogradncmail.net
Cc Jade Eastridge [e-mail] [e-mail]
Subject 24-Hour Notification Incidents No and
Steve
On behalf of Beazer Homes am herein providing 24-Hour Notification of the discovery of
environmentally-impacted soils at two separate locations Incidents Nos and on BecizerHomesMoreheadCommonsresidentialdevelopmentcurrentlybeinggradedTheMoreheadCommonspropertyislocatedonthesouthsideofWestMoreheadStreetatitsintersectionwithSouthClarksonStreetinCharlotteMecklenburgCountyNorthCarolina
Incident No
On May 17 2007 during Site grading operations concrete vault-like structure wasencounteredonthe east side of Post Street Tax Parcel No 07325213 approximately 450 feetsouthofitsintersectionwithSouthClarksonStreetseeattached2005SiteMapOnMay172007MrChrisWardofESPobservedsoilsthatexhibitedsomeblackstaininghoweverfield
screening with an OVA did not reveal elevated readings In an attempt to confirm the absenceorpresenceofpotentialcontaminantsonMay17ESPcollectedwastecharacterizationsoilsampleSP-1 of visibly stained soils from depth of approximately feet The soil sample wasanalyzedforvolatileorganiccompoundsVOCsbyEPAMethod8260pesticidesbyEPAMethod8081polychlorinatedbiphenylsPCBsbyEPAMethod8082oilandgreaseOGbyEPAMethod9071fortotalpetroleumhydrocarbonsTPHbyEPAMethods3550 and 5030andfortotalleadandchromiumbyEPAMethod3051PreliminaryresultsoftheanalysisattachedrevealedelevatedlevelsofOcG3100mg/kg TPH-bRO 420 mg/kg and PC12605.1 mg/kg The parcel was occupied by Air Reduction Sales Company and Ohio ChemicalsSurgicalEquipmentfrom1933tobetween1956and1965beforethepropertyoccupantwaslistedasnolisting
Incident No
On May 29 2007 during site grading operations visibly stained soils with an obvious petroleum
Page2 of3
odor were encountered on the west side of South Clarkson Street approximately 450 feet
south of its intersection with West Morehead Street on Tax Parcel No 07325207 see
attached 2005 Site Map The vicinity of the impacted soils was once occupied by vehicular
service facility with closed USTs Incidents Nos 18101 and 9567 buke Energy-Worth Keeter
before being demolished On May 29 2007 Mr Chris Ward of ESP observed the
environmentally-impacted soils and directed the collection waste characterization soil sampleSP-3 of visibly impacted soils from depth of approximately feet The soil sample was
submitted to Prism Laboratories to be analyzed for VOCs by EPA Method 8260B pesticides by
EPA Method 8081 PCBs by EPA Method 8082 OG by EPA Method 9071 for TPH by EPA
Methods 3550 and 5030 and for total lead and chromium by EPA Method 3051
Incident No
Please note that 24-Hour Notification for previously identified area of petroleum-impacted
soils was emailed to your attention on May 16 2007 and is referred as Incident No see
attached Site Map Results of the waste characterization analysis of the soil sample collected
from this area and designated PS-i revealed elevated concentrations of number of VOCs OG
10000 mg/kg TPH-bRO 3600 mg/kg and TPH-GRO 33 mg/kg See attached Prism
laboratory report Starting today Incident No is being excavated with impacted soils
stockpiled on site for subsequent off-site disposal
Following receipt of the laboratory results for the waste characterization samples and landfill
disposal authorization ESP will direct the excavation of impacted soils from Incidents Nos
and and their subsequent off-site permitted disposal Confirmatory soil samples will then be
collected from the walls and base of the excavation at Incidents Nos and Assuming
acceptable results initial abatement action reports will then be prepared for submittal toNCbENRforeachincident
The Responsible Party for the property is
Becizer komes
1300 South Boulevard
Suite
Charlotte North Carolina 28203-4265
Mr Jade Eastridge
704.370.7200
Please call with any questions
Thanks
Chris Ward PG
Environmental Services Manager
ESP Associates
803.835.0915 direct office
803.802.2515 fax
704.506.7618 mobile
Page3of3
APPENDIX
NON-HAZARDOUS WASTE MANIFESTS
BF CMS LADF ILL Fax[phone] Aug 0201J7 1040
ALLIED WA$T$Please print or type
lJ
orm designed tar use on elite 12 pitch typewriterNON-HAZARDOUS Generators US EPA ID No ManifetWASANIFESTDocument No
Generators Name and Mailing Address Beazer Homes
1000 South Clafkson Street
ChdcgjjetJC 221GeneratorsPhone
Transporter Company Name US EPA ID NumberGelderThompson
Transporter Company Name US EPA ID Number
Designated Facility Name and Site Address 10 US EPAID NumberCMSLaridifil
5105 Morehead Rd
Concord NC 28027
ii Waste Shipping Name and Descripti
Petroleum Impacted Soil
16 GENERATORS CERTIFICATION certify the maferials desciiba above on this manifest are not subject to ledersi reguttions for reporting prqper disposal ot Hazardou Waste
Printed Typed Name
Si ature
AntIjj Pay Year
BeazerHojn
17 Transporter Acknowledgement of Receipt of Materials
Printed/Typed Name
Signature
Monthj Cay Year
3elder ii18TransporterAcknowledgementofReceiptpfMaterials
Printed/Typed Name
Signature
Month Cay19DiscrepancyIndicationSpace
20 Facility Owner or Operator Cerhicatlon or receipt of waste materials covered by this manifest except as noted in item 19
CMS Landfill
Printed/Type Name
Signature
AWForm 121ORIGINALRTURNTOGENERATOR
02
ge1
Truck No
Account 100255an9
Transporters Phone
Facilitys Phpne
704 782-2004
12 Containers 14
Total Unit
UtIfyW
EiFI CMS LANDFILL Fax [phone] Aug 16 2007 1041
Generators Phone
Transporter Company Name Ge1d mpson
Transporter Compaime
11 Waste Shipping Name and Description
18 GENERATORS CERTIFICATION certey the materials described above on this manifest are no subject to federal regulations for reporting proper dispqI of
Printed Typed Name
I1ous
17 fransporter Acknowledge of Receipt of Materials
Printed Typed Name
18 Transporter Acknowledgement of Receipt of
Printed Typed Name
19 Discrepancy Indication Space
ALLIED WASTEfet
Document No
1000 South Ctarlcson Sct
c1arJcftsNC 2S2i
Name and Site
OMS Làndf ill
5105 Morehead Rd
Concord NC 28027
ORIGINAL RETURN TO GENERATOR
BFI CMS LANDFILL Fa 70470221 77 Aug 10 2007 1041 04
Accont 10Q255
Additional Descriptions for Matelals Listed Above ________
Handling Codes aste Listed Above
sPealHandinglflstruotionsandAddflonalIIIr
1000 3outh C1ki 8trt
CIw1ctteNC2231
ThNEATORS CERTIFIcATION
ragulafjonsfor reporting properPrintedTypedNameBeazerJoiiies
17 Tr8nsporter Acknowledgement of Receipt of Materials
Printed Typed Name
18 Transpqner Acknowledgement of Receipt of Materials
Printed Typed Name
19 Discrepancy Indication Space
20 Facility Owner or OperatorCMSLandfifl
Printed Type Name
ORIGiNAL RETU8N TO GENERATOR
Generators Phone
ALLiED WASTE ___Please print or type
LIFormdesignedforuseonelite12pitchtypewriter____________________NON-HAZARDOUS 1.Generators US EPA ID No ManifestWASTMANIFST
Generators Name and Mailing Address Beazer Homes
1000 South C1arkou Strett
Genaratot Phone Chadotte NC 2S23
Transporter Company Name
umberOdderThompson
Transporter Company Name EPA ID Number
Designated Facility Name and Site Address 10 US EPA ID Nrnber
5105 Morehead Rd
CMS Landfill
Concord NC 28027
11 Waste Shipping Name and Description
12 Containera 13 14
No Type Quan ity WI1VoI
Additional DeScriptions for Materials Listed Above
Handling Codes for Wastes List Above
F31Y77355
15 SpecIal Handling InstructIons and Additional Information
16 CERTIFIQATION certify the materials described above on this manifest are not subject to fedraJ reuJation fqr reporting proper dispoaj of HazrdusJwaste
Printed/Typed Name
Si ture Menth Lay Yew
e-17 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name
Signature
MQnfh Dan Year
3/18 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name
Signature
Mane Pa YearDiscrepancyIndicationSpace
20 FacIlity Owner or Operator Cerificati of reqelpf of Waste materials covered by this manifest eceptas óted in item 19.
CMS Landfill
Printed/Type Name
Signature Mon
AWl FormiORIGINALRETURNTOGENERATOR
BFI CMS LANDFILL Fax7 Aug 113 20117 11141
Accot 100255
05
1131...o
981Li 12648
TrUpkNo
anspo
Transrr Phone
Facif dys Phone
704 78-O04
Petroleum hnpacted Soil
fl
APPENDIX
SITE PHOTOGRAPHS
APPENDIX
ESPS SOP
STANbARb OPERATING PROCEbURE
SOP-6
SOIL SAMPLE COLLECTION
ESP Associates P.A Revision bate 3/7/06
This standard operating procedure SOP covers the collection of soil sample for
laboratory analysis
Follow these steps when collecting the soil sample unless
otherwise instructed by the project manager
Gather needed field supplies noted below
Confirm lab cooler contains needed sample containers fill cooler with
ice
Upon arriving at site check in with the property owner or company
representative
becontaminate the stainless steel hand auger before and between sample
collection by washing with Alconox soap and scrub brush rinsing with
distilled water and spraying with Isopropyl alcohol Wrap clean sampler
in aluminum foil
Wear disposal latex or nitrile gloves and change into new pair between
samples
buring advancement of the hand auger collect soil samples at regular
intervals for describing lithology Note lithology and other
characteristics of soils in field book relative to depth
If appropriate place representative portion of soil sample into
resealable plastic bag label with boring number and depth interval and
allow to equilibrate Screen soil in bag for volatile organics using art OVA
or 1-mu Enter results into field book
Advance hand auger boring to previously specified sampling depth
Collect soil sample from this depth and place in laboratory provided
containers Label containers with boring number and sample depth using
the following sampling scheme i.e B-i ft B-i 10 ft B-2 ft etc
benote boring location in field book relevant to pertinent site features
10 Following collection of the soil samples abandon all boreholes feet or
greater in depth with cement grout
ii Complete and sign the labs chain-of-custody
12 Keep the sample cooler in secure location until delivered under normal
chain-of-custody procedures to laboratory
SOP-6 Soil Sampk Collection fevision bate 3/7/06
ESP Associates Page of
SUPPLIES
SOP-6
Stainless steel hand auger with needed extensions or sampling
spoon
OVA orHnu
11 Measuring tape
Plastic zip-lock bags
Isopropyl alcohol
bistilled water
5-gallon wash bucket scrub brush and Alcortox soap
Cement with wheel barrow for mixing
Cooler with sample containers and chain-of-custody
Ice
Permanent marker
bisposable gloves
Knife
Field book
Site plan with site specific sampling instructions
Camera
APPENDIX
PRISM LABORATORY DATA REPORTS
iU JUN ZO/
Case NarrativePRISM
LABORATORIES INC
Date 06119/07 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COC Group No G0607179
Contact Chris Ward Collection Dates 06106/07
Address Box 7030 Lab Submittal Dates 06/06/07
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrave Laboratory Report and Quality
Control Data totaling 56 pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Qualitycontrolstatementsand/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
No Anomalies Reported
Metals Analysis
Analysis Note for Q24176 MS Chromium Matrix interference is suspected Post-digestion spike recovery 79%is within the
acceptance limits 75-125%
Analysis Note for Q24176 MS Lead Matrix interference is suspected Post-digestion spike recovery 73%is outside the
acceptance limits 75-125%
Analysis Note for Q24176 MSD Chromium Matrix interference is suspected
Analysis Note for Q24176 MSD Lead Matrix interference is suspected
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by Paula Gilleland Project Manager
Signature i3Jtf2k.Signature
Review Date 06/19/07 Approval Date -___________________________
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect is present
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories Inc The results in thisreportrelateonlytothesamplessubmittedforanalysis
449 Springbrook Road P.O Box 240543 chaolle NC 28224-0403
Phone [phone] Toll Free 800/529-6364 Fax [phone]Q
SC CUfifiOfl No 99012 Laboratory Report
NC Dnnking Water Cert No 37735 06/18/07
Wi SeMce Analyticat Environmnntal Solutions
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-1
ttn Chris Ward Prism Sample ID 183632
Box 7030 Sample Matrix Soil COC Group G06071 79
charlotte NC 28241 Time Collected 06/06/07 1400
Time Submitted 06/06/07 1640
iarameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
ercent Solids Determination
Percent Solids 82.6 SM2540 06111/07 1700 brown
rganochlorine Pesticides by Gas ChromatociraDhy
44-DDD BRL pg/kg 2.4 0.74 8081A 06/13/07 2308 ivogel 024275
14-DDE BRL pg/kg 2.4 0.52 8081A 06/13/07 2308 jvogel Q24275
44-DDT BRL pg/kg 2.4 0.87 8081A 06/13/07 2308 jvogel Q24275
4-Methoxychlor BRL pg/kg 4.8 1.7 8081A 06/13/07 2308 ivogel Q24275
a-BHC BRI pg/kg 2.4 0.22 8081A 06/13/07 2308 jvogel Q24275
i-Chlordane BRL pg/kg 2.4 0.42 8081A 06/13/07 2308 ivogel Q24275
Jdrin BRL pg/kg 2.4 0.48 8081A 06/13/07 2308 ivogel 024275
b-BHC BRL pg/kg 2.4 0.61 8081A 06/13/07 2308 ivogel 024275
hlordane BRL pg/kg 61 14 8081A 06/13/07 2308 jvogel Q24275
d-BHC BRL pg/kg 2.4 0.34 8081A 06/13/07 2308 ivogel Q24275
ietdrin BRL pg/kg 1.2 0.50 8081A 06/13/07 2308 ivogel Q24275
Endosulfan BRL pg/kg 2.4 0.43 8081A 06/13/07 2308 ivogel 024275
Endosulfan II BRL pg/kg 2.4 0.55 8081A 06/13/07 2308 jvogel Q24275
Endosulfan Sulfate BRL pg/kg 2.4 0.63 8081A 06/13/07 2308 ivogel 024275
Endrin BRL pg/kg 2.4 0.73 8081A 06/13/07 2308 ivogel 024275
Endrin Aldehyde BRL pg/kg 2.4 0.68 8081A 06/13/07 2308 ivogel 024275
Endrin Ketone BRI pg/kg 2.4 0.48 8081A 06/13/07 2308 Jvogel Q24275
-BHC BRL pg/kg 2.4 0.28 8081A 06/13/07 2308 ivogel Q24275
g-Chlordane BRL pg/kg 2.4 0.39 8081A 06/13/07 2308 Jvogel Q24275
Heptachlor BRL pg/kg 2.4 0.57 8081A 06/13/07 2308 jvoget Q24275
Heptachor Epoxide BRL pg/kg 2.4 0.45 8081A 06/13/07 2308 ivogel Q24275
Toxaphene BRL pg/kg 61 14 8081A 06/13/07 2308 ivogel Q24275
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page of 45
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Laboratory Report
06/18/07
SP Associates PA Project ID Morehead Commons No Client Sample ID WS-1
ttn Chris Ward Prism Sample ID 183632
Box 7030 Sample Matrix Soil COG Group G0607179
harlofte NC 28241 Time Collected 06/06/07 1400
Time Submitted 06/06/07 1640
Result Units Report MDL
Limit
Dilution
Factor
Method
Sample Preparation 29.88 10 mL 3550B 06/12107 1000 dpope P18598
Analysis
Date/Time
Analyst Batch
ID
Surrogate Recovery Control Limits
Decachiorobiphenyl DCB 128 26 204
Tetrachloro-m-xylene TCMX 106 40 162
0.061
0.12
0.061
0.061
0.061
0.061
0.061
0.011
0.049
0.019
0.021
0.0084
0.021
0.016
8082
8082
8082
8082
8082
8082
8082
06/13/07
06/13/07
06/1 3107
06/13/07
06/13/07
06113/07
06/13/07
2308 jvogeI
2308 jvogel
2308 jvoge
2308 jvoge
2308 jvogel
2308 jvogel
2308 jvogel
Polychlorinated Biphenyls PCBs by GC-ECD
7CB-1 016 BRL
CB-1 221 BRL
CB-1 232 BRL
3CB-1242 BRL
PCB-1 248 BRL
CB-1 254 BRL
PCB-1260 BRL
Sample Preparation
Iolatile Organic Compounds by GC/MS
111 2-Teti-achloroethane BRL
11 1-Trichloroethane BRL
11 22-Tetrachloroethane BRL
11 2-Trichloroethane BRL
1-Dichloroethane BRL
1-Dichloroethene BRL
Ji 1-Dichloropropene BRL
23-Trichlorobenzene BRL
Q24276
Q24276
Q24276
Q24276
Q24276
024276
024276
P1859729.88 10 mL 3550B 06/12/07 1000 dpope
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
Surrogate Recovery Control Limits
Decachlorobiphenyl DCB 109 34 182
Tetrachloro-m-xylene TCMX 109 36 182
6.6 0.64
6.6 0.37
6.6 0.67
6.6 0.41
6.6 0.47
6.6 0.50
6.6 0.58
13 0.72
8260B
8260B
8260B
8260B
8260B
8260B
82603
8260B
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
1610 erussell
1610 erussell
1610 erussell
1610 erussell
1610 erussell
1610 erussell
1610 erussell
1610 erusseH
024147
024147
Q24147
024147
024147
Q24147
Q241 47
024147
Page of 45
SP Associates PA
ttn Chris Ward
P.O Box 7030
1.harlotte NC 28241
Laboratory Report
06/18/07
Ws-1
183632
G0607179
06/06/07
06/06/07
Parameter
23-Trichloropropane
24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromo-3-chloropropane
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichlorobenzene
22-Dichioropropane
-Chloroethyl vinyl ether
2-ChIorotoIuene
.-Hexanone
1-Chiorotoluene
4-Methyl-2-pentanone MIBK
\cetone
Benzene
romobenzene
Bromochioromethane
romodichIoromethane
omoform
3romomethane
carbon disulfide
carbon tetrachloride
BRL pg/kg 6.6 0.58
BRL pg/kg 13 0.63
BRL pg/kg 13 0.50
BRL pg/kg 6.6 1.0
BRL pg/kg 6.6 0.12
BRL pg/kg 13 0.36
BRL pg/kg 6.6 0.66
BRL pg/kg 6.6 0.49
BRL pg/kg 13 0.55
BRL pg/kg 13 0.57
BRL pg/kg 6.6 0.45
BRL pg/kg 13 0.51
BRL pg/kg 6.6 0.33
BRL pg/kg 13 0.49
BRL pg/kg 13 0.49
BRL pg/kg 66 0.68
BRL pg/kg 13 0.34
BRL pg/kg 13 0.66
BRL pg/kg 26 2.6
BRL pg/kg 3.9 0.53
BRL pg/kg 6.6 0.46
BRL pg/kg 6.6 0.39
BRL pg/kg 6.6 0.58
BRL pg/kg 6.6 0.49
BRL pg/kg 13 0.76
BRL pg/kg 13 0.42
BRL pg/kg 6.6 0.38
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
Analyst Batch
ID
Q24147
Q241 47
024147
024147
024147
Q24147
024147
024147
Q24147
024147
Q24147
024147
024147
024147
024147
024147
024147
024147
024147
Q24147
024147
024147
Q241 47
Q24147
024147
Q24147
024147
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
lt Service Analytical Environmental Solutions
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1400
1640
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
G6/08/G7 1610 erussell
06/08/07 1610 erussefl
06/08/07 1610 erussetl
06/08/07 1610 erussell
06/08/07 1610 erussell
06/08/07 1610 erussell
G6/G8/G7 1610 erussell
G6/G8/G7 1610 erussell
G6/G8/G7 16IG erussell
06/08/07 16IG erussell
06/08/07 1610 erussell
G6/G8/G7 16IG erussell
G6/G8/G7 1610 erussell
06/08/07 1610 erusseH
G6/G8/G7 16IG erussell
06/08/07 1610 erussell
06/08/07 1610 erussell
G6/G8/G7 1610 erussetl
06/08/07 1610 erussell
06/08/07 1610 erussell
G6/G8/G7 1610 erussetl
06/08/07 16IG erusselt
G6/G8/G7 1610 erussell
06/08/07 1610 erussell
06/08/07 1610 erussell
06/08/07 1610 erusselt
06/08/07 1610 erusset
Page of 45
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ll Service Analytical Environmental Solutions
SP Associates PA
kttn Chris Ward
.0 Box 7030
rharlotte NC 28241
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Laboratory Report
06/18/07
iarameter
Project ID Morehead Commons No Cflent Sample ID WS-1
Prism Sample ID 183632
Sample Matrix Soil COC Group G0607179
Time Collected 06/06/07 1400
Time Submitted 06/06/07 1640
Result Units Report MDL Dilution
Limit
Method
Factor
Analysis Analyst
Batch
Date/Time ID
Thlorobenzene BRL pg/kg 6.6 0.50 826GB 06/08/07 1610 erussefl Q24147
Chiorodibromomethane BRL pg/kg 6.6 0.45 8260B 06/08/07 1610 erussell 024147
Thioroethane BRL pg/kg 13 0.54 826GB 06/08/07 1610 erussell 024147
Chloroform BRL pg/kg 6.6 0.49 826GB 06/08/07 1610 erusseli 024147
hloromethane BRL pg/kg 13 0.46 826GB 06/08/07 1610 erusseA Q24147
ds-1 2-Dichloroethene BRL pg/kg 6.6 0.29 8260B 06/08/07 1610 erussell 024147
is-1 3-Dichloropropene BRL pg/kg 6.6 0.42 826GB 06/08/07 1610 erussefl Q24147
ibromomethane BRL pg/kg 6.6 0.49 826GB 06/08/07 1610 erussefl Q24147
Dichlorodifluoromethane BRL pg/kg 13 1.5 8260B 06/08/07 1610 erussell 024147
Ethylbenzene BRL pg/kg 6.6 0.46 826GB 06/08/07 1610 erussell 024147
Hexachlorobutadiene BRL pg/kg 20 0.82 826GB 06/08/07 1610 erussetl 024147
sopropyl ether IPE BRL pg/kg 6.6 0.22 8260B 06/08/07 1610 erussell 024147
Isopropylbenzene BRL pg/kg 13 0.53 826GB 06/08/07 1610 erussell 024147
np-Xylenes BRL pg/kg 13 0.92 826GB 06/08/07 1610 erussell Q24147
Methyl ethyl ketoneMEK BRL pg/kg 26 1.8 826GB 06/08/07 1610 erussefl 024147
AethyI t-butyl ether MTBE BRL pg/kg 6.6 0.38 826GB 06/08/07 1610 erussell Q24147
ylethylene chloride BRL pg/kg 13 0.54 826GB 06/08/07 1610 erussell 024147
n-Butylbenzene BRL pg/kg 20 0.53 826GB 06/08/07 1610 erussell 024147
-Propylbenzene BRL pg/kg 13 0.39 8260B 06/08/07 1610 erusseH 024147
Naphthalene BRL pg/kg 6.6 0.76 826GB 06/08/07 1610 erussell 024147
-Xylene BRL pg/kg 6.6 0.39 826GB 06/08/07 1610 erussell Q24147
p-Isopropyltoluene BRL pg/kg 20 0.54 826GB 06/08/07 1610 erussell 024147
BRL pg/kg 20 0.43 826GB 06/08/07 1610 erussell Q24147
5tyrene BRL pg/kg 6.6 0.66 8260B 06/08/07 1610 erussell 024147
4ert-Butylbenzene BRL pg/kg 26 0.41 826GB 06/08/07 1610 erussell 024147
BRL pg/kg 13 1.1 826GB 06/08/07 1610 erussell 024147
Toluene BRL pg/kg 6.6 0.45 8260B 06/08/07 1610 erussell 024147
Page of 45
3ample Weight Determination
Neight Bisulfate
Weight Bisulfate
Neight Methanol
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Laboratory Report
06/18/07
all Service Analytical Environmental Solutionn
ESP Associates PA
ttn Chris Ward
O.Box7030
Charlotte NC 28241
parameter
rans-1 2-Dichloroethene
trans-I 3-Dichloropropene
richloroethene
Trichlorofluoromethane
/inyl chloride
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 183632
Sample Matrix Soil COC Group G06071 79
Time Collected 06/06/07 1400
Time Submitted 06/06/07 1640
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
6.6 0.50 8260B 06/08/07 1610 erussell Q24147
6.6 0.46 8260B 06/08/07 1610 erusselt Q24147
6.6 0.39 8260B 06/08/07 1610 erussell 024147
6.6 0.54 8260B 06/08/07 1610 erussell 024147
13 0.84 8260B 06108/07 1610 erussell 024147
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
5.02
4.60
4.43
Surrogate Recovery Control Limits
Bromofluorobenzene 104 77 128
Dibromofluoromethane 92 67 143
Toluene-d8 96 131 128
06/13/07 000
06/13/07 000
06/13/07 000
brown
brown
brown
emi-volatile Organic ComDounds by GCIMS
24-Trichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
45-TrichIorophenol BRL
246-Trichlorophenol BRL
24-Dichlorophenol BRL
4-Dimethylphenol BRL
24-Dinitrophenoj BRL
4-DinitrotoIuene BRL
26-Dinitrotoluene BRL
06/11/07
06/11/07
1117 kcampigotto
1117 kcampigotto
5035
5035
5035
39 8270C
29 8270C
29 8270C
36 8270C
41 8270C
38 8270C
33 8270C
38 8270C
45 8270C
23 8270C
42 8270C
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
400
400
400
400
400
400
400
400
400
400
400
06/11/07 1117
06/11/07 1117
06/11/07 1117
06/11/07 1117
06/11/07 1117
06/11/07 1117
06/11/07 1117
06/11/07 1117
06/11/07 1117
024124
024124
024124
Q24124
024124
024124
024124
024124
024124
024124
024124
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
Page of 45
uIl Service Anatylical Environmental Solutions
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-1
183632
G06071 79
06/06/07 1400
06/06/07 1640
arameter
-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
34-Methylphenol
33-Dichlorobenzidine
46-Dinitro-2-methylphenol
4-Bromophenylphenylether
4-Chloro-3-methylphenol
4-Chiorophenylphenylether
4-Nitrophenol
cenaphthene
cenaphthylene
-Anthracene
-enzoaanthracene
3enzoapyrene
Benzobfluoranthene
Benzoghiperylene
Benzokfluoranthene
Bis2-chloroethoxymethane
Bis2-chloroethylether
Sis2-chloroisopropylether
Bis2-ethylhexylphthalate
utyIbenzylphthalate
hrysene
Di-n-butylphthalate
Limit
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRI pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRI pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
Factor
41
31
32
37
48
41
25
24
38
29
25
26
39
39
30
56
46
18
19
32
46
43
34
20
24
66
18
Batch
ID
024124
024124
024124
024124
024124
Q24124
Q24124
Q24124
024124
024124
024124
Q24124
Q24124
024124
024124
Q24124
Q24124
024124
024124
024124
024124
024124
Q24124
Q24124
024124
024124
024124
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Result Units Report MDL Dilution Method Analysis Analyst
Date/Time
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270G 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
8270C 06/11/07 1117 kcampigotto
Page of 45
iarameter
i-n-octylphthalate
Dibenzoahanthracene
ibenzofuran
Diethylphthalate
imethylphthalate
luoranthene
luorene
IexachIorobenzene
Hexachiorobutadiene
lexachlorocyclopentadiene
Hexachioroethane
ldeno1 23-cdpyrene
isophorone
-Nitrosodi-n-propylamine
.-Nitrosodiphenylamine
laphthaIene
litrobenzene
Pentachiorophenol
henanthrene
Phenol
tyrene
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
ll Service Analytical Environmental Solutions
Laboratory Report
06/18/07
FSP Associates PA Project ID Morehead Commons No Client Sample ID WS-1
ttn Chris Ward Prism Sample ID 183632
Box 7030 Sample Matrix Soil COC Group G06071 79
rharlotte NC 28241 Time Collected 06/06/07 1400
Time Submitted 06/06/07 1640
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
BRL pg/kg 400 30 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 40 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 34 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 24 8270C 06/11/07 1117 kcampigotto 024124
BRI pg/kg 400 27 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 27 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 24 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 21 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 39 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 42 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 40 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 41 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 36 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 45 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 20 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 43 8270C 06/11/07 1117 kcampigotto 024124
BRL pglkg 400 39 8270C 06111/07 1117 kcampigotto Q24124
BRL pg/kg 400 33 8270C 06/11/07 1117 kcampigotto 024124
BRI pg/kg 400 19 8270C 06/11/07 1117 kcampigotto 024124
BRL pg/kg 400 43 8270C 06/11/07 1117 kcampigotto Q24124
BRL pg/kg 400 27 8270C 06/11/07 1117 kcampigotto 024124
Page of 45
$IIi 99012 Laboratory Report
NC Dnnking Water Cert No 37735 06/18/07
4itl Service Analytical Environmental Solutions
SP Associates PA Project ID Morehead Commons No Client Sample ID WS-1
ttn Chris Ward Prism Sample ID 183632
Box 7030 Sample Matrix Soil COG Group G0607179
harlotte NC 28241 Time Collected 06/06/07 1400
Time Submitted 06/06/07 1640
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 30.16 mL 3550B 06/08/07 700 dpope P18579
Surrogate Recovery Control Limits
246-Tribromophenol 76 25 123
2-Fluorobiphenyl 54 21 108
2-Fluorophenol 57 14 89
Nitrobenzene-d5 55 14-103
Phenol-d5 59 13-95
Terphenyl-d14 84 41 136
xtractable Petroleum Hydrocarbons by GC-FID
C11-C22 Aromatics BRL mg/kg 13 6.8 MADEP EPH 06/16/07 2047 grappaccioli Q24301
9-C36 Aliphatics BRL mg/kg 13 1.9 MADEP EPH 06/16/07 2047 grappaccioli 024301
C9-C18 Aliphatics BRL mg/kg 13 4.0 MADEP EPH 06/16/07 2047 grappaccioli 024301
Analysis Note for Cll-C22 Aromatics Adjusted value
Sample Preparation 9.62 mL EPH 06/13/07 800 dpope P18614
Surrogate Recovery Control Limits
-Chloro-octadecane 112 40 140
2-Bromonaphthalene 135 40 140
2-Fluorobiphenyl 131 40-140
o-Terphenyl 102 40 140
iAetals by ICP
chromium 0.63 mg/kg 0.30 0.018 6010B 06/11/07 2050 mcampbefl Q24176
.ead 5.1 mg/kg 0.30 0.025 6010B 06/11/07 2050 mcampbell 024176
Sample Preparation 2.03 50 mL 3050B 06/11/07 905 ihoppel P18580
iolatile Petroleum Hydrocarbons by GC-PID/FID
C5-C8 Aliphatics BRL mg/kg 6.1 1.2 MADEP VPH 06/12/07 2127 hwagner 024220
9-C10 Aromatics BRL mg/kg 6.1 0.036 MADEP VPH 06/12/07 2127 hwagner 024220
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 45
uS Service Analytical Envtrenmvntal Solutions
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
BRL mg/kg 6.1 1.9 MADEP VPH 06/12/07 2127 hwagner
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-Cl2 Aliphatics Adjusted value
One surrogate recovery was outside the control limits No target compounds were detected inthissampleNofurtheractionwastaken
Surrogate Recovery Control Limits
SamIe Weight Determination
Weight 20.05
Weight 17.23
25-Dibromotoluene-PID 118 70 130
25-Dibromotoluene-FID 155 70-130
Sample Comments
SRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthoseinstances indicated in the case narrative and/or test comments
AIl results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
Parameter
wS-1
183632
G0607179
06/06/07
06/06/07
9-C12 Aliphatics
1400
1640
Q24220
MADEP VPH 06/13/07 000 brown
MADEP VPH 06/13/07 000 brown
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 45
Full Service Analytical Environmental Solutions
Laboratory Report
06/18/07
ESP Associates PA
Attn Chris
Ward
Box 7030
Charlotte NC 28241
WS-2
183633
G06071 79
06/06/07
06/06/07
Parameter
Percent Solids Determination
Percent Solids
Analyst Batch
ID
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1415
1640
Result Units Report MDL Dilution Method
Limit Factor
Analysis
Date/Time
86.4 SM25400 06/11/07 1700 brown
Organochlorine Pesticides by Gas Chromatography
44-DDD BRL pg/kg 2.3 0.71 8081A 06/13/07 2350 Jvogel 024275
44-DDE BRL pg/kg 2.3 0.49 8081A 06/13/07 2350 Jvogel Q24275
44-DDT BRL pg/kg 2.3 0.83 8081A 06/13/07 2350 Ivogel 024275
44-Methoxychlor BRL pg/kg 4.6 1.6 8081A 06/13/07 2350 jvogel 024275
a-BHC BRL pg/kg 2.3 0.21 8081A 06/13/07 2350 Jvogel 024275
a-Chlordane BRL pg/kg 2.3 0.40 8081A 06/13/07 2350 ivogel 024275
Aldrin BRL pg/kg 2.3 0.46 8081A 06/13/07 2350 Jvogel 024275
b-BHC BRL pg/kg 2.3 0.59 8081A 06/13/07 2350 Jvogel 024275
Chlordane BRL pg/kg 58 13 8081A 06/13/07 2350 ivogel 024275
d-BHC BRL pg/kg 2.3 0.33 8081A 06/13/07 2350 Jvogel 024275
Dieldrin BRL pg/kg 1.2 0.48 8081A 06/13/07 2350 Jvogel 024275
Endosulfan BRL pg/kg 2.3 0.41 8081A 06/13/07 2350 Jvogel 024275
Endosulfan II BRL pg/kg 2.3 0.52 8081A 06/13/07 2350 ivogel 024275
Endosulfan Sulfate BRL pg/kg 2.3 0.60 8081A 06/13/07 2350 ivogel 024275
Endrin BRL pg/kg 2.3 0.70 8081A 06/13/07 2350 ivogel 024275
Endrin Aldehyde BRL pg/kg 2.3 0.65 8081A 06/13/07 2350 ivogel 024275
Endrin Ketone BRL pg/kg 2.3 0.46 8081A 06/13/07 2350 Jvogel 024275
g-BHC BRL pg/kg 2.3 0.27 8081A 06/13/07 2350 ivogel 024275
g-Chlordane BRL pg/kg 2.3 0.38 8081A 06/13/07 2350 jvogel 024275
Heptachior BRL pg/kg 2.3 0.55 8081A 06/13/07 2350 Ivogel 024275
Heptachlor Epoxide BRL pg/kg 2.3 0.43 8081A 06/13/07 2350 ivogel 024275
Toxaphene BRL pg/kg 58 13 8081A 06/13/07 2350 jvogel 024275
Page 10 of 45
Full Service Analytical
Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
WS-2
183633
G06071 79
06/06/07 1415
06/06/07 1640
Analysis Analyst Batch
Date/Time ID
This report should not
be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter
Sample Preparation
Result Units Report MDL
Limit
Dilution
Factor
Method
29.76 10 mL 3550B 06/12/07 1000 dpope
Surrogate Recovery
Tetrachloro-m-xylene TCMX 103
Decachlorobiphenyl DCB 121
P18598
Control Limits
40-162
26 204
Polychlorinated Biphenyls PCBs by GC-ECD
PCB-1016 BRL mg/kg 0.058 0.011 8082 06/13/07 2350 ivogel 024276
PCB-1221 BRL mg/kg 0.12 0.047 8082 06/13/07 2350 Jvogel Q24276
PCB-1232 BRL mg/kg 0.058 0.019 8082 06/13/07 2350 Jvogel Q24276
PCB-1242 BRL mg/kg 0.058 0.020 8082 06/13/07 2350 Jvogel Q24276
PCB-1248 BRL mg/kg 0.058 0.0080 8082 06/13/07 2350 Jvogel Q24276
PCB-1254 BRL mg/kg 0.058 0.020
8082 06/13/07 2350 jvogel 024276
PCB-1260 BRL mg/kg 0.058 0.016
8082 06/13/07 2350 Jvogel Q24276
29.76 10 mL 3550B 06/12/07 1000 dpope P18597SamplePreparation
Volatile Organic Compounds by GCIMS
111 2-Tetrachloroethane
111 -Trichloroethane
11 22-Tetrachloroethane
11 2-Trichloroethane
1-Dichloroethane
1-Dichloroethene
11 -Dichloropropene
23-Trichlorobenzene
Surrogate Recovery Control Limits
Decachiorobiphenyl DCB 89 34 182
Tetrachloro-m-xylene TCMX 101 36-182
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
6.0 0.58
6.0 0.33
6.0 0.61
6.0 0.37
6.0 0.43
6.0 0.45
6.0 0.52
12 0.65
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
1642
1642
1642
1642
1642
1642
1642
1642
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
024147
024147
Q24147
024147
024147
024147
024147
024147
Page 11 of 45
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Laboratory Report
06/18/07
WS-2
183633
G06071 79
06/06/07
06/06/07
Acetone
Benzene
Bromomethane
Carbon disulfide
erusseli
erussell
erussell
erussefi
erussell
erussell
erusseli
erusseil
erussell
erusseil
erussefi
erusseli
erussefl
erusseli
erussell
erusseH
erusseH
erusseil
erusseii
erusseil
erusseil
erusseil
erussell
erusseli
erusseli
erusseli
erusseil
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] ToH Free Number 1-800/529-6364 Fax [phone]
024147
024147
024147
024147
024147
Q24147
Q24147
024147
024147
024147
Q24147
024147
024147
024147
024147
024147
024147
Q24147
024147
024147
Q24147
024147
024147
Q24147
024147
024147
024147
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter
11415
1640
Analyst Batch
ID
23-Trichloropropane
24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromo-3-chloropropane
12-Dibromoethane EDB
2-Dichlorobenzene
2-Dichloroethane
2-Dichloropropane
35-Trimethyibenzene
3-Dichiorobenzene
3Dichloropropane
4-Dichlorobenzene
22-Dichloropropane
2-Chloroethyl vinyl ether
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone MIBK
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
BRL pg/kg 6.0 0.52
8260B 06/08/07 1642
BRL pg/kg 12 0.57 8260B 06/08/07 1642
BRL pg/kg 12 0.45 8260B 06/08/07 1642
BRL pg/kg 6.0 0.94 8260B 06/08/07 1642
BRL pg/kg 6.0 0.11 8260B 06/08/07 1642
BRL pg/kg 12 0.32 8260B 06/08/07 1642
BRL pg/kg 6.0 0.60 8260B 06/08/07 1642
BRL pg/kg 6.0 0.44 8260B 06/08/07 1642
BRL pg/kg 12 0.50 8260B 06/08/07 1642
BRL pg/kg 12 0.51 8260B 06/08/07 1642
BRL pg/kg 6.0 0.40 8260B 06/08/07 1642
BRL pg/kg 12 0.46 8260B 06/08/07 1642
BRL pg/kg 6.0 0.30 8260B 06/08/07 1642
BRL pg/kg 12 0.44 8260B 06108/07 1642
BRL pg/kg 12 0.44 8260B 06/08/07 1642
BRL pg/kg 60 0.62 8260B 06/08/07 1642
BRL pg/kg 12 0.31 8260B 06/05/07 1642
BRL pg/kg 12 0.60 8260B 06/08/07 1642
34 pg/kg 24 2.3 8260B 06/08/07 1642
BRL pg/kg 3.6 0.48 8260B 06/08/07 1642
BRL pg/kg 6.0 0.42 8260B 06/08/07 1642
BRL pg/kg 6.0 0.36 8260B 06/08/07 1642
BRL pg/kg 6.0 0.52 8260B 06/08/07 1642
BRL pg/kg 6.0 0.44 8260B 06/08/07 1642
BRL pg/kg 12 0.69 8260B 06/08/07 1642
BRL pg/kg 12 0.38 8260B 06/08/07 1642
BRL pg/kg 6.0 0.35 8260B 06/08/07 1642
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Carbon tetrachloride
Page 12 of 45
Project ID Morehead Commons No CHent Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
183633
G06071 79
06/06/07 1415
06/06/07 1640
Parameter
Chlorobenzene
Chlorodibromomethane
Chioroethane
Chloroform
Chloromethane
cis-1 2-Dichloroethene
cis-1 3-Dichloropropene
Dibromomethane
Dichlorodifluoromethane
Ethylbenzene
Hexachiorobutadiene
Isopropyl ether IPE
lsopropylbenzerie
mp-Xylenes
Methyl ethyl ketone MEK
Methyl t-butyl ether MTBE
Methylene chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p-lsopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachioroethene
Toluene
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
ESP Associates PA
Am Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
BRL pg/kg 6.0 0.45 82606 06/08/07 1642 erussell 024147
BRL pg/kg 6.0 0.40 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 12 0.49 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 6.0 0.44 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 12 0.42 8260B 06/08/07 1642 erusseI 024147
BRL pg/kg 6.0 0.26 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 6.0 0.38 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 6.0 0.44 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 12 1.3 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 6.0 0.42 82606 06/08/07 1642 erussell 024147
BRL pg/kg 18 0.74 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 6.0 0.20 82606 06/08/07 1642 ewssell 024147
BRL pg/kg 12 0.48 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 12 0.83 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 24 1.7 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 6.0 0.35 82606 06/08/07 1642 erussell 024147
BRL pg/kg 12 0.49 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 18 0.48 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 12 0.36 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 6.0 0.69 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 6.0 0.36 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 18 0.49 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 18 0.39 8260B 06/08/07 1642 erussell Q24147
BRL pg/kg 6.0 0.60 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 24 0.37 8260B 06/08/07 1642 erussell 024147
BRL pg/kg 12 1.0 82606 06/08/07 1642 erussell 024147
BRL pg/kg 6.0 0.40 8260B 06/08/07 1642 erussell 024147
Page 13of45
Laboratory Report
06/18/07
WS-2
183633
G06071 79
06/06/07
06/06/07
5035
5035
5035
38 827CC
28 827CC
28 827CC
35 827CC
39 827CC
37 827CC
32 827CC
37 827CC
43 827CC
22 827CC
41 827CC
40 827CC
06/13/07 000 Ibrown
06/13/07 000 brown
06/13/07 000 brown
06/11/07 1209 kcampigotto
06/11/07 1209 kcampigotto
C6/1 1/07 1209 kcampigotto
06/11/07 1209 kcampigotto
06/11/07 1209 kcampigotto
06/11/07 1209 kcampigotto
06/11/07 1209 kcampigotto
06/11/07 1209 kcampigotto
06/11/C7 1209 kcampigotto
06/11/07 1209 kcampigotto
C6/11/C7 1209 kcampigotto
C6111/07 1209 kcampigotto
024124
024124
024124
024124
024124
Q24124
024124
Q24124
Q24124
024124
024124
024124
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method
Limit Factor
1415
1640
Analyst Batch
ID
6.0 0.45
6.0 0.42
6.0 0.36
6.0 0.49
12 0.76
826CB
8260B
8260B
826CB
826CB
Analysis
Date/Time
06/08/07 1642
06/08/07 1642
06/08/07 1642
06/08/07 1642
06/08/07 1642
erussell
erussell
erussell
erussell
erussefl
024147
024147
024147
024147
024147
Surrogate Recovery Control Limits
Bromofluorobenzene 106 77 128
Toluene-d8 101 81 128
Dibromofluoromethane 95 67 143
trans-i 2-Dichloroethene BRL
trans-13-Dichloropropene BRL
Trichloroethene BRL
Trichlorofluoromethane BRL
Vinyl chloride BRL
Sample Weight Determination
Weight Bisulfate 5.08
Weight Bisulfate 4.86
Weight Methanol 4.29
Semi-volatile Organic Compounds by GCMS
24-Trichlorobenzene BRL
12-Dichlorobenzene BRL
13-Dichlorobenzene BRL
4-Dichlorobenzene BRL
245-Trichlorophenol BRL
246-Trichiorophenol BRL
24-Dichlorophenol BRL
24-Dimethylphenol BRL
24-Dinitrophenol BRL
24-Dinitrotoluene BRL
26-Dinitrotoluene BRL
2-Chloronaphthalene BRL
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
390
390
390
390
390
390
390
390
390
390
390
390
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 14of45
Full Sornice Analybcal Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
WS-2
183633
G06071 79
06/06/07
06/06/07
This report shoud not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road PO Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method
1415
1640
Analyst Batch
ID
Analysis
Limit Factor Date/Time
2-Chlorophenol BRL pg/kg 390 30
8270C 06/11/07 1209 kcampigottci 024124
2-Methylnaphthalene BRL pg/kg 390 31 8270C 06/11/07 1209 kcampigottc 024124
Methylphenol BRL pg/kg 390 36 8270C 06/11/07 1209 kcamplgotto 024124
2-Nitrophenol BRL pg/kg 390 46
8270C 06/11/07 1209 kcampigotto 024124
34-Methylphenol BRL pg/kg 390 39
8270C 06/11/07 1209 kcampgotto Q24124
33-DichIorobenzidine BRL pg/kg 390 24
8270C 06/11/07 1209 kcampigottci 024124
46-Dinitro-2-methylphenol BRL pg/kg 390 23 8270C 06/11/07 1209 kcampigottci 024124
4-Bromophenylphenylether BRL pg/kg 390 37 8270C 06/11/07 1209 kcampigottci 024124
4-Chloro-3-methylphenol BRL pg/kg 390 28
8270C 06/11/07 1209 kcampgottci 024124
4-Chiorophenyiphenylether BRL pg/kg 390 24
8270C 06/11/07 1209 kcampigottci 024124
4-Nitrophenol BRL pg/kg 390 26
8270C 06/11/07 1209 kcampigottci Q24124
Acenaphthene BRL pg/kg 390 38 8270C 06/11/07 1209 kcampigotto 024124
Acenaphthylene BRL pg/kg 390 38
8270C 06/11/07 1209 kcampigottci 024124
Anthracene BRL pg/kg 390 29 8270C 06/11/07 1209 kcampigotto 024124
Benzoaanthracene BRL pg/kg 390 54
8270C 06/11/07 1209 kcampigotto 024124
Benzoapyrene BRL pg/kg 390 45 8270C 06/11/07 1209 kcampigollo 024124
Benzobfluoranthene BRL pg/kg 390 17 8270C 06/11/07 1209 kcampigollo 024124
Benzoghiperylene BRL pg/kg 390 18 8270C 06/11/07 1209 kcampigotto 024124
Benzokfluoranthene BRL pg/kg 390 31 8270C 06/11/07 1209 kcampigottci 024124
Bis2-chloroethoxymethane BRL pg/kg 390 44 8270C 06/11/07 1209 kcampigotto 024124
Bis2-chloroethylether BRL pg/kg 390 42 8270C 06/11/07 1209 kcampigotto 024124
Bis2-chloroisopropylether BRL pg/kg 390 33 8270C 06/11/07 1209 kcampigotto 024124
Bis2-ethylhexylphthalate BRL pg/kg 390 19 8270C 06/11/07 1209 kcampigotto Q24124
Butylbenzylphthalate BRL pg/kg 390 24 8270C 06/11/07 1209 kcampigottci 024124
Chrysene BRL pg/kg 390 64 8270C 06/11/07 1209 kcampigotto 024124
Di-n-butylphthalate BRL pg/kg 390 18 8270C 06/11/07 1209 kcampigotto 024124
Di-n-octylphthalate BRL pg/kg 390 29 8270C 06/11/07 1209 kcampigctto Q24124
Page 15 of 45
Full Servico Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
183633
G0607179
06/06/07 l415
06/06/07 1640
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
Analyst Batch
ID
Parameter
Dibenzoahanthracene BRL pg/kg 390 39 8270C 06/11/07 1209 kcampigotto 024124
Dibenzofuran BRL pg/kg 390 33 8270C 06/11/07 1209 kcampigotto 024124
Diethylphthalate BRL pg/kg 390 24 82700 06/11/07 1209 kcampigotto 024124
Dimethylphthalate BRL pg/kg 390 26 8270C 06/11/07 1209 kcampigotto 024124
Fluoranthene BRL pg/kg 390 27 82700 06/11/07 1209 kcampigotto 024124
Fluorene BRL pg/kg 390 23 82700 06/11/07 1209 kcampigotto 024124
Hexachlorobenzene BRL pg/kg 390 20 8270C 06/11/07 1209 kcarnpigotto 024124
Hexachlorobutadiene BRL pg/kg 390 37 8270C 06/11/07 1209 kcampigotto 024124
Hexachlorocyclopentadiene BRL pg/kg 390 41 82700 06/11/07 1209 kcampigotto 024124
Hexachloroethane BRL pg/kg 390 39 8270C 06/11/07 1209 kcampigotto 024124
lndeno123-cdpyrene BRL pg/kg 390 40 8270C 06/11/07 1209 kcampigotto Q24124
Isophorone BRL pg/kg 390 34 8270C 06/11/07 1209 kcampigotto 024124
NNitrosodi-n-propylamine BRL pg/kg 390 44 82700 06/11/07 1209 kcampigotto 024124
N-Nitrosodiphenylamine BRL pg/kg 390 20 82700 06/11/07 1209 kcampigotto 024124
Naphthalene BRL pg/kg 390 42 82700 06/11/07 1209 kcampigotto 024124
Nitrobenzene BRL pg/kg 390 38 8270C 06/11/07 1209 kcampigotto 024124
Pentachlorophenol BRL pg/kg 390 32 82700 06/11/07 1209 kcarrlpigotto 024124
Phenanthrene BRL pg/kg 390 19 8270C 06/11/07 1209 kcampigotto 024124
Phenol BRL pg/kg 390 42 82700 06/11/07 1209 kcampigotto 024124
Pyrene BRL pg/kg 390 26 82700 06/11/07 1209 kcampigotto 024124
Page 16of45
Fu Service Analyhcal
Environmental Solutions
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
183633
G0607179
06/06/07 1415
06/06107 1640
Parameter Result Units Report MDL
Limit
Dilution Method
Factor
Analysis Analyst
Batch
Date/Time ID
Sample Preparation 29.7 mL 35508 06/08/07 700 dpope P18579
Extractable Petroleum Hydrocarbons by GC-FID
C11-C22 Aromatics BRL mg/kg
C19-C36 Aliphatics BRL mg/kg
C9-C18 Aliphatics BRL mg/kg
Analysis Note for Cl1C22 Aromatics
Sample Preparation
2.1 mg/kg
4.4 mg/kg
0.29 0.017 6010B
0.29 0.024 6010B
06/11/07 2113 mcampbell
06/11/07 2113 mcampbell
024176
024176
Sample Preparation
Volatile Petroleum Hydrocarbons by GC-PID/FID
C5-C8 Aliphatics BRL
C9-C10 Aromatics BRL
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Surrogate Recovery Control Limits
2-Fluorobiphenyl 65 21 108
Terphenyl-d14 91 41 136
2-Fluorophenol 49 14 89
Nitrobenzerie-d5 57 14 103
246-Tribromophenol 93 25 123
Phenol-d5 58 13-95
12 6.4 MADEP EPH 06/16/07 1123 grappaccioli 024301
12 1.8 MADEP EPH 06/16/07 1123 grappaccioli 024301
12 3.8 MADEP EPH 06/16/07 1123 grappaccioli 024301
Adjusted value
9.73 mL EPH 06/13/07 800 dpope 18614
Metals by ICP
Chromium
Lead
Surrogate Recovery Control Limits
-Chloro-octadecane 95 40 140
2-Bromonaphthalene 111 40-140
2-Fluorobiphenyl 107 40 140
o-Terphenyl 98 40 140
2.02 50 mL 3050B 06/11/07 905 jhoppel P18580
mg/kg 5.8 1.1 MADEP VPH 06/12/07 2208 hwagner 024220
mg/kg 5.8 0.035 MADEP VPH 06/12/07 2208 hwagner 024220
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 17of45
Full Service Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time
C9-C12 Aliphatics BRL mg/kg 5.8 1.8 MADEP VPH 06/12/07 2208 hwagner
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
Two surrogate recoveries were outside of the control limits No target compounds were detected
in this sample No further action was taken
Sample Comments
BRL Below Reporting Limit
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 183 70-130
25-Dibromotoluene-PID 138 70 130
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthoseinstances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
WS-2
183633
G06071 79
06/06/07
06/06/07
1415
1640
Q24220
SampVe Weight Determination
Weight 23.18
Weight 23.97
MADEP VPH 06/13/07 000 brown
MADEP VPH 06/13/07 000 brown
Angela Overcash V.P Laboratory Services
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 18of45
SM
Full Service Anulyticat Environmental Solutions
ESP Associates PA
Attn Chris Ward
O.Box7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-3
183634
G06071 79
06/06/07
06/06/07
Parameter
Percent Solids Determination
Percent Solids
Report MDL Dilution Method
Limit Factor
Analyst Batch
ID
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Result Units
1430
1640
82.9
Analysis
Date/Time
SM2540 06/11/07 1700 brown
Organochiorine Pesticides by Gas Chromatography
44-DDD BRL pg/kg 2.4 0.74 8081A 06/14/07 032 Jvogel Q24275
DDE BRL pg/kg 24 51 8081A 06/14/07 32 jvogel 024275
44-DDT BRL pg/kg 2.4 0.87 8081A 06/14/07 032 Jvoge 024275
44-Methoxychlor BRL pg/kg 4.8 1.6 8081A 06/14/07 032 Jvoge 024275
a-BHC BRL pg/kg 2.4 0.22 8081A 06/14/07 032 ivogel Q24275
a-Chlordane BRL pg/kg 2.4 0.42 8081A 06/14/07 032 Jvogel Q24275
Aidrin BRL pg/kg 2.4 0.48 8081A 06/14/07 032 Jvogel 024275
b-BHC BRL pg/kg 2.4 0.61 8081A 06/14/07 032 Jvogel Q24275
Chlordane BRL pg/kg 60 14 8081A 06/14/07 032 jvogel 024275
d-BHC BRL pg/kg 24 0.34 8081A 06/14/07 032 jvoge 024275
Dieldrin BRL pg/kg 1.2 0.50 8081A 06/14/07 032 ivogel Q24275
Endosulfan BRL pg/kg 2.4 0.43 8081A 06/14/07 032 ivogel 024275
Endosulfan II BRL pg/kg 2.4 0.54 8081A 06/14/07 032 ivogel 024275
Endosulfan Sulfate BRL pg/kg 2.4 0.63 8081A 06/14/07 032 jvogel Q24275
Endrin BRL pg/kg 2.4 0.72 8081A 06/14/07 032 ivog 024275
Endrin Aldehyde BRL pg/kg 2.4 0.68 8081A 06/14/07 032 ivogel 024275
Endrin Ketone BRL pg/kg 2.4 0.48 8081A 06/14/07 032 jvoge 024275
g-BHC BRL pg/kg 2.4 0.28 8081A 06/14/07 032 jvogel 024275
g-Chlordane BRL pg/kg 2.4 0.39 8081A 06/14/07 032 jvogel 024275
Heptachlor BRL pg/kg 2.4 0.57 8081A 06/14/07 032 ivogel 024275
HeptachlorEpoxide BRL pg/kg 2.4 0.44 8081A 06/14/07 032 jvogel 024275
Toxaphene BRL pg/kg 60 14 8081A 06/14/07 032 Jvogel 024275
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 19of45
kRISM
Full Service Analytical Environmental Solulion
ESP Associates PA
Attn Chris Ward
O.Box7030
Charlotte NC 28241
Laboratory Report
06/18/07
WS-3
183634
G06071 79
06/06/07 1430
06/06/07 1640
Result Units Report MDL
Limit
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
Parameter Dilution Method
Factor
Analysis
Date/Time
Analyst Batch
ID
29.7 10 mL 3550B 06/12/07 1000 dpope P18598
Surrogate Recovery Control Limits
Tetrachloro-m-xylene TCMX 105 40 162
Decachiorobiphenyl DCB 143 26 204
0.060
0.12
0.060
0.060
0.060
0.060
0.060
0.011
0.049
0.019
0.021
0.0083
0.021
0.016
8082
8082
8082
8082
8082
8082
8082
Sample Preparation
Polychiorinated Biphenyls PCBs byGC-ECD
PCB-1016 BRL
PCB-1221 BRL
PCB-1232 BRL
PCB-1242 BRL
PCB-1248 BRL
PCB 1254 BRL
PCB-1 260 BRL
Sample Preparation
Volatile Organic Compounds by GC/MS
111 2-Tetrachloroethane BRL
111-Trichloroethane BRL
11 22-Tetrachloroethane BRL
11 2-Trichloroethane BRL
11 -Dichloroethane BRL
11-Dichloroethene BRL
1-Dichloropropene BRL
23-Trichlorobenzene BRL
06/14/07 032
06/14/07 032
06/14/07 032
06/14/07 032
06/14/07 032
06/14/07 032
06/14/07 032
jvogel
jvogel
ivogel
jvogel
jvogel
jvogel
jvogel
Q24276
024276
024276
024276
024276
024276
024276
P1859729.7 10 mL 3550B 06/12/07 1000 dpope
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
Surrogate Recovery Control Limits
Decachiorobiphenyl DCB 105 34-182
Tetrachloro-m-xylene TCMX 103 36 182
6.1 0.60
6.1 0.34
6.1 0.63
6.1 0.38
6.1 0.44
6.1 0.47
6.1 0.54
12 0.67
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
1714 erussell
1714 erussell
1714 erussell
1714 erusseH
1714 erussell
1714 erussell
1714 erussell
1714 erussell
024147
024147
024147
024147
024147
Q24147
024147
024147
Page 20 of 45
Full Service Analytical
Environmental Solutions
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Atm Chris Ward
P.O Box7030
Charlotte NC 28241
Parameter
23-Trichloropropane
24-Trichlorobenzene
24-Trim ethylbenzene
2-Dibromo-3-chloropropane
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichlorobenzene
22-Dichioropropane
2-Chloroethyl vinyl ether
2-Chiorotoluene
2-Hexanone
4-Chiorotoluene
4-Methyl-2-pentanone MIBK
Acetone
Benzene
Bromobenzene
Bromochioromethane
Bromodichioromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachioride
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
Limit Factor
6.1 0.54
12 0.59
12 0.47
6.1 0.97
6.1 0.11
12 0.33
6.1 0.61
6.1 0.45
12 0.51
12 0.53
6.1 0.42
12 0.48
6.1 0.31
12 0.45
12 0.45
61 0.64
12 0.32
12 0.61
25 2.4
3.7 0.49
6.1 0.43
6.1 0.37
6.1 0.54
6.1 0.45
12 0.71
12 0.39
6.1 0.36
024147
024147
024147
024147
Q24147
024147
024147
024147
024147
024147
024147
024147
024147
Q24147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 183634
Sample Matrix Soil COG Group G0607179
Time Collected 06/06/07 1430
Time Submitted 06/06/07 1640
Result Units Report MDL Dilution Batch
ID
Method Analysis Analyst
Date/Time
8260B 06/08/07 1714 erussell
8260B 06/08/07 1714 erussell
8260B 06/08/07 1714 erussell
8260B 06/08/07 1714 erussell
8260B 06/08/07 1714 erusseH
8260B 06/08/07 1714 ewssell
8260B 06/08/07 1714 erussel
8260B 06/08/07 1714 erussel
8260B 06/08/07 1714 erussell
826DB 06/08/07 1714 erussell
826DB 06/08/07 1714 erussell
8260B 06/08/07 1714 erussel
826DB 06/08/07 1714 erussell
8260B 06/08/07 1714 erussell
8260B 06/08/07 1714 erussell
8260B 06/08/07 1714 ewssel
8260B 06/08/07 1714 erussell
8260B 06/08/07 1714 erussell
826DB 06/08/07 1714 erussell
8260B 06/08/07 1714 erussel
8260B 06/08/07 1714 erussell
826DB 06/08/07 1714 erussell
826DB 06/08/07 1714 erussell
826DB 06/08/07 1714 erussell
826DB 06/08/07 1714 erussell
826DB 06/08/07 1714 erussell
826DB 06/08/07 1714 erussell
Page 21 of 45
Laboratory Report
06/18/07
Full Service Analytical Environmental Solutions
ESP Associates PA WS-3
Attn Chris Ward 183634
Box 7030 G0607179
Charlotte NC 28241 06/06/07
06/06/07
Parameter
Chlorobenzene erussell 024147
Chlorodibromomethane erusseU Q241 47
Chloroethane erusselt Q24147
Chloroform erussefl 024147
Chloromethane erussell 024147
cis-1 2-Dichloroethene ewssell 024147
cis-1 3-Dichloropropene erussell 024147
Dibromomethane erussell Q24147
Dichiorodifluoromethane erussell Q24147
Ethylbenzene erussell 024147
Hexachiorobutadiene erussell 024147
Isopropyl ether IPE erussell 024147
lsopropylbenzene erussell 024147
mp-Xylenes erussell 024147
Methyl ethyl ketone MEK erusseH 024147
Methyl t-butyl ether MTBE erusseH 024147
Methylene chloride erusselt Q24147
n-Butylbenzene erussell 024147
n-Propylbenzene erussell 024147
Naphthalene erusset 024147
o-Xylene erusset 024147
p-lsopropyltoluene erussell 024147
sec-Butylbenzene erussefl 024147
Styrene erussell 024147
tert-Butylbenzene erusselt 024147
Tetrachloroethene erussell Q24147
Toluene erussell 024147
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1430
1640
Analyst Batch
ID
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
BRL pg/kg 6.1 0.47 8260B 06/08/07 1714
BRL pg/kg 6.1 0.42 8260B 06/08/07 1714
BRL pg/kg 12 0.50 8260B 06/08/07 1714
BRL pg/kg 6.1 0.45 8260B 06/08/07 1714
BRL pg/kg 12 0.43 8260B 06/08/07 1714
BRL pg/kg 6.1 0.27 8260B 06/08/07 1714
BRL pg/kg 6.1 0.39 8260B 06/08/07 1714
BRL pg/kg 6.1 0.45 8260B 06/08/07 1714
BRL pg/kg 12 1.4 8260B 06/08/07 1714
BRL pg/kg 6.1 0.43 8260B 06/08/07 1714
BRL pg/kg 18 0.76 8260B 06/08/07 1714
BRL pg/kg 6.1 0.21 8260B 06/08/07 1714
BRL pg/kg 12 0.49 8260B 06/08/07 1714
BRL pg/kg 12 0.86 8260B 06/08/07 1714
BRL pg/kg 25 1.7 8260B 06/08/07 1714
BRL pg/kg 6.1 0.36 8260B 06/08/07 1714
BRL pg/kg 12 0.50 8260B 06/08/07 1714
BRL pg/kg 18 0.49 8260B 06/08/07 1714
BRL pg/kg 12 0.37 8260B 06/08/07 1714
BRL pg/kg 6.1 0.71 8260B 06/08/07 1714
BRL pg/kg 6.1 0.37 8260B 06/08/07 1714
BRL pg/kg 18 0.50 8260B 06/08/07 1714
BRL pg/kg 18 0.40 8260B 06/08/07 1714
BRL pg/kg 6.1 0.61 8260B 06/08/07 1714
BRL pg/kg 25 0.38 8260B 06/08/07 1714
BRL pg/kg 12 1.1 8260B 06/08/07 1714
BRL pg/kg 6.1 0.42 8260B 06/08/07 1714
Page 22 of 45
RISM
IN
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
WS-3
183634
G0607179
06/06/07 1430
06/06/07 1640
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter
trans-i 2-Dichloroethene
trans-i 3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Result Units Report MDL Dilution Method
Limit Factor
Analyst Batch
ID
6.1 0.47
6.1 0.43
6.1 0.37
6.1 0.50
12 0.78
8260B
8260B
8260B
8260B
8260B
Analysis
Date/Time
06/08/07 1714
06/08/07 1714
06/08/07 1714
06/08/07 1714
06/08/07 1714
erussell
erusseil
erussell
erussell
erussell
BRL
BRL
BRL
BRL
BRL
5.13
4.92
4.91
024147
024147
Q24147
024147
024147
Surrogate Recovery Control Limits
Bromofluorobenzene 103 77 128
Toluene-d8 97 81 128
Dibromofluoromethane 92 67 143
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
Semi-volatile Organic Compounds by GC/MS
124-Trichlorobenzene BRL
2-Dichlorobenzene BRL
i3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
245-Trichlorophenol BRL
246-Trichiorophenol BRL
24-Dichiorophenol BRL
24-Dimethyiphenol BRL
24-Dinitrophenol BRL
24-Dinitrotoluene BRL
26-Dinitrotoluene BRL
2-Chloronaphthalene BRL
5035
5035
5035
39 8270G
29 8270C
29 8270C
36 8270C
41 8270C
38 8270C
33 827CC
38 827CC
45 8270C
23 827CC
42 8270C
41 827CC
400
400
400
400
400
400
400
400
400
400
400
400
06/13/07
06/13/07
06/13/07
06/11/07
06/11/07
06/11/07
06/11/07
06/11/07
06/11/07
06/11/07
06/11/07
06/11/07
06/11/07
06/11/07
06/11/07
000
000
000
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
brown
brown
brown
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampgotto
024124
024124
024124
024124
024124
024124
024124
Q24i24
024124
024124
024124
024124
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 23 of 45
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
O.Box7030
Charlotte NC 28241
Laboratory Report
06/18/07
WS-3
183634
G06071 79
06/06/07
06/06/07
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method
1430
1640
Limit Factor
Analyst Batch
ID
Analysis
Date/Time
2-ChlorophenoI BRL pg/kg 400 31 8270C 06/11/07 1300 kcampigottcl 024124
2-Methylnaphthalene BRL pg/kg 400 32 8270C 06/11/07 1300 kcampigottci 024124
2-Methylphenol BRL pg/kg 400 37 8270C 06/11/07 1300 kcampigottci 024124
2-Nitrophenol BRL pg/kg 400 48 8270C 06/11/07 1300 kcampigottci 024124
34-Methylphenol BRL pg/kg 400 41 8270C 06/11/07 1300 kcampigotto Q24124
33-Dichlorobenzidine BRL pg/kg 400 25 8270C 06/11/07 1300 kcampigottci 024124
146-Dinitro-2-methylphenol BRL pg/kg 400 24 8270C 06/11/07 1300 kcampigottci Q24124
4-BromophenylphenyIether BRL pg/kg 400 38 8270C 06/11/07 1300 kcampigottci 024124
--4-Chloro-3-methylphenol BRL pg/kg 400 29 8270C 06/11/07 1300 kcampigotto 024124
4-Chlorophenyiphenylether BRL pg/kg 400 25 8270C 06/11/07 1300 kcampigottci 024124
4-Nitrophenol BRL pg/kg 400 26 8270C 06/11/07 1300 kcampigottci 024124
Acenaphthene BRL pg/kg 400 39 8270C 06/11/07 1300 kcampigottci 024124
Acenaphthylene BRL pg/kg 400 40 8270C 06/11/07 1300 kcampigotto 024124
Anthracene BRL pg/kg 400 30 8270C 06/11/07 1300 kcampigottci 024124
Benzoaanthracene BRL pg/kg 400 56 8270C 06/11/07 1300 kcampigotto 024124
Benzoapyrene BRL pg/kg 400 46 8270C 06/11/07 1300 kcampigotto 024124
Benzobfluoranthene BRL pg/kg 400 18 8270C 06/11/07 1300 kcampigotto 024124
Benzoghiperylene BRL pg/kg 400 19 8270C 06/11/07 1300 kcampgotto 024124
Benzokfluoranthene BRL pg/kg 400 32 8270C 06/11/07 1300 keampigotto 024124
Bis2-chloroethoxymethane BRL pg/kg 400 46 8270C 06/11/07 1300 kcampigottci 024124
Bis2-chloroethylether BRL pg/kg 400 43 8270C 06/11/07 1300 kcampigotto 024124
Bis2-chloroisopropylether BRL pg/kg 400 34 8270C 06/11/07 1300 kcampigotto 024124
Bis2-ethylhexylphthalate BRL pg/kg 400 20 82700 06/11/07 1300 kcampigotto 024124
Butylbenzylphthalate BRL pg/kg 400 24 8270C 06/11/07 1300 kcampigotto 024124
Chrysene BRL pg/kg 400 66 82700 06/11/07 1300 kcampigotto 024124
Di-n-butylphthalate BRL pg/kg 400 18 82700 06/11/07 1300 kcampigotto Q24124
Di-n-octylphthalate BRL pg/kg 400 30 8270C 06/11/07 1300 kcampigofta 024124
Page 24 of 45
Fufi SeMce Analytcal Environmentul Solutiono
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Laboratory Report
06/18/07
WS-3
183634
00607179
06/06/07
06/06/07
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1430
1640
Result Units Report MDL Dilution Method
Limit Factor
Analysis
Date/Time
Analysit Batch
ID
Parameter
Dibenzoahanthracene BRL pg/kg 400 40 827CC 06/11/07 1300 kcampgotto 024124
Dibenzofuran BRL pg/kg 400 34 827CC 06/11/07 1300 kcarnpigotto 024124
Diethyphthalate BRL pg/kg 400 24 827CC 06/11/07 1300 kcampigotto 024124
Dimethylphthalate BRL pg/kg 400 27 8270C 06/11/07 1300 kcampigotto Q24124
Fluoranthene BRL pg/kg 400 27 827CC 06/11/07 1300 kcampigotto 024124
Fluorene BRL pg/kg 400 24 8270C 06/11/07 1300 kcampigotto 024124
Hexachlorobenzene BRL pg/kg 400 21 827CC 06/11/07 1300 kcampigotto 024124
Hexachiorobutadiene BRL pg/kg 400 39 827CC 06/11/07 1300 kcampigotto 024124
Hexachiorocyclopentadiene BRL pg/kg 400 42 827CC 06/11/07 1300 kcampgotto 024124
Hexachioroethane BRL pg/kg 400 40 8270C 06/11/07 1300 kcampigotto 024124
lndeno123-cdpyrene BRL pg/kg 400 41 827CC 06/11/07 1300 kcampigotto 024124
Isophorone BRL pg/kg 400 36 827CC 06/11/07 1300 kcampigotto 024124
N-Nitrosodi-n-propylamine BRL pg/kg 400 45 827CC 06/11/07 1300 kcampgotto 024124
N-Nitrosodiphenylamine BRL pg/kg 400 20 827CC 06/11/07 1300 kcampigotto 024124
Naphthalene BRL pg/kg 400 43 8270C 06/11/07 1300 kcampigotto 024124
Nitrobenzene BRL pg/kg 400 39 8270C 06/11/07 1300 kcampigotto 024124
Pentachiorophenol BRL pg/kg 400 33 827CC 06/11/07 1300 kcampigotto 024124
Phenanthrene BRL pg/kg 400 19 827CC 06/11/07 1300 kcampigotto 024124
Phenol BRL pg/kg 400 43 827CC 06/11/07 1300 kcampigotto 024124
Pyrene BRL pg/kg 400 27 8270C 06/11/07 1300 kcampigotto 024124
Page 25 of 45
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 30.03 mL 3550B 06/08/07 700 dpope
Extractable Petroleum Hydrocarbons by GC-FID
Ci1-C22 Aromatics BRL mg/kg
C19-C36 Aliphatics BRL mg/kg
C9-C18 Aliphatics BRL mg/kg
Analysis Note for Cll-C22 Aromatics
Sample Preparation
Metals by ICP
Chromium
Adjusted value
9.55g 2mL EPH
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 183634
Sample Matrix Soil COC Group G0607179
Time Collected 06/06/07
Time Submitted 06/06/07
430
1640
P18579
Surrogate Recovery Control Limits
Terphenyl-d14 88 41 136
246-Tribromophenol 86 25 123
Phenol-d5 65 13-95
2-Fluorophenol 63 14 89
2-Fluorobiphenyl 75 21 108
Nitrobenzene-d5 69 14-103
13 6.8 MADEPEPH
13 1.9 MADEPEPH
13 4.0 MADEPEPH
06/17/07
06/17/07
06/17/07
950
950
950
grappaccioli
grappaccioli
grappaccioli
dpope
024301
024301
024301
1861406/13/07 800
Lead
Surrogate Recovery Control Limits
1-Chloro-octadecane 138 40-140
2-Fluorobiphenyl 128 40 140
o-Terphenyl 114 40-140
2-Bromonaphthalene 132 40 140
Sample Preparation 2.05 50 mL
0.81 mg/kg 0.29 0.018 6010B 06/11/07 2121 mcampbell 024176
5.7 mg/kg 0.29 0.025 6010B 06/11/07 2121 mcampbell 024176
Volatile Petroleum Hydrocarbons by GC-PID/FID
C5-C8 Aliphatics BRL mg/kg 6.0 1.2 MADEP VPH 06/12/07 2249 hwagner Q24220
C9-C10 Aromatics BRL mg/kg 6.0 0.036 MADEP VPH 06/12/07 2249 hwagner 024220
3050B 06/11/07 905 jhoppel P18580
Page 26 of 45
Full SeMca Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
C9-C12 Aliphatics BRL mg/kg 6.0 1.9 MADEP VPH 06/12/07 2249 hwagner
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-Cl2 Aliphatics Adjusted value
One surrogate recovery was outside the control limits Nc target compounds were detected in
this sample No further action was taken
Sample Weight Determination
Weight 20.39
Weight 21.94
Sample Comments
MADEP VPH 06/13/07 000 brown
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated/n the case narrative and/or test comments
All results are reported on thy-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
WS-3
183634
G06071 79
06/06/07
06/06/07
1430
1640
Q24220
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 165 70 130
25-Dibromotoluene-PID 129 70 130
MADEP VPH 06/13/07 000 brown
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 27 of 45
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 183635
Sample Matrix Soil COC Group 00607179
Time Collected 06/06/07 1445
Time Submitted 06/06/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Percent Solids Determination
Percent Solids 86.5
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402PR1SMSCCertificationNo99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
SM2540 06/11/07 1700 brown
Organochlorine Pesticides by Gas Chromatography
44-DDD BRL pg/kg 2.3 0.71 8081A 06/14/07 114 jvogel Q24275
DDE BRL pg/kg 49 8081A 06/14/07 14 jvogel Q24275
44-DDT BRL pg/kg 2.3 0.83 8081A 06/14/07 114 ivogel 024275
44-Methoxychlor BRL pg/kg 4.6 1.6 8081A 06/14/07 114 ivogel 024275
a-BHC BRL pg/kg 2.3 0.21 8081A 06/14/07 114 ivogel 024275
a-Chlordane BRL pg/kg 2.3 0.40 8081A 06/14/07 114 Jvogel 024275
Aldrin BRL pg/kg 2.3 0.46 8081A 06/14/07 114 ivogel 024275
b-BHC BRL pg/kg 2.3 0.58 8081A 06/14/07 114 Ivogel 024275
Chiordane BRL pg/kg 58 13 8081A 06/14/07 114 ivogel 024275
d-BHC BRL pg/kg 2.3 0.33 8081A 06/14/07 114 Jvogel 024275
Dieldrin BRL pg/kg 1.2 0.48 8081A 06/14/07 114 jvogel 024275
Endosulfan BRL pg/kg 2.3 0.41 8081A 06/14/07 114 Jvogel 024275
Endosulfan II BRL pg/kg 2.3 0.52 8081A 06/14/07 114 ivogel 024275
Endosulfari Sulfate BRL pg/kg 2.3 0.60 8081A 06/14/07 114 Jvogel 024275
Endrin BRL pg/kg 2.3 0.69 8081A 06/14/07 114 jvogel 024275
Endrin Aldehyde BRL pg/kg 2.3 0.65 8081A 06/14/07 114 ivogel 024275
Endrin Ketone BRL pg/kg 2.3 0.46 8081A 06/14/07 114 jvogel 024275
g-BHC BRL pg/kg 2.3 0.27 8081A 06/14/07 114 jvoge 024275
g-Chlordane BRL pg/kg 2.3 0.38 8081A 06/14/07 114 ivogel 024275
Heptachior BRL pg/kg 2.3 0.55 8081A 06/14/07 114 ivogel Q24275
Heptachior Epoxide BRL pg/kg 2.3 0.43 8081A 06/14/07 114 Ivogel 024275
Toxaphene BRL pg/kg 58 13 8081A 06/14/07 114 ivogel 024275
Page 28 of 45
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
WS-4
183635
00607179
06/06/07
06/06/07
Parameter Result Units Report MDL
Limit
Dilution Method
Factor
Analysis Analyst
Batch
Date/Time ID
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1445
1640
29.55 10 mL 3550B 06/12/07 1000 dpope P1 8598
Surrogate Recovery Coitrol Limits
Decachlorobiphenyl DCB 124 26-204
Tetrachloro-m-xylene TCMX 109 40 162
Sample Preparation
Polychiorinated Biphenyls PCBs by GC-ECD
PCB-1016 BRL
PCB-1221 BRL
PCB-1232 BRL
PCB-1242 BRL
PCB-1248 BRL
PCB 1254 BRL
PCB-1260 BRL
Sample Preparation
Volatile Organic Compounds by GC/MS
111 2-Tetrachloroethane BRL
11 1-Trichloroethane BRL
11 22-Tetrachloroethane BRL
11 2-Trichloroethane BRL
1-Dichloroethane BRL
11-Dichloroethene BRL
11-Dichloropropene BRL
123-Trichlorobenzene BRL
0.058 0.011 8082 06/14/07 114 jvogel Q24276
0.12 0.047 8082 06/14/07 114 jvogel 024276
0.058 0.018 8082 06/14/07 114 jvogel Q24276
0.058 0.020 8082 06/14/07 114 jvogel 024276
0.058 0.0080 8082 06/14/07 114 jvogel 024276
0.058 0.020 8082 06/14/07 114 jvogel Q24276
0.058 0.015 8082 06/14/07 114 jvogel Q24276
29.55 10 mL 355DB 06/12/07 1000 dpope
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
P18597
Surrogate Recovery Control Limits
Decachlorobiphenyl DCB 90 34 182
Tetrachloro-m-xylene TCMX 98 36 182
6.7 0.66
6.7 0.38
6.7 0.69
6.7 0.42
6.7 0.49
6.7 0.51
6.7 0.59
13 0.74
826DB
8260B
82608
8260B
8260B
82608
826DB
826DB
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
06/08/07
1747
1747
1747
1747
1747
1747
1747
1747
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erusseD
024147
024147
024147
024147
Q24147
Q241 47
024147
024147
Page 29 of 45
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 183635
Sample Matrix Soil COC Group G0607179
Time Collected 06/06/07 1445
Time Submitted 06/06/07 1640
Parameter
23-Trichloropropane
24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromo-3-chloropropane
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichlorobenzene
22-Dichloropropane
2-Chloroethyl vinyl ether
2-Chiorotoluene
2-Hexanone
4-Chiorotoluene
4-Methyl-2-pentanone MIBK
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichioromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Result Units Report MDL Dilution
Limit
BRL pg/kg 6.7 0.59
BRL pg/kg 13 0.65
BRL pg/kg 13 0.51
BRL pg/kg 6.7 1.1
BRL pg/kg 6.7 0.12
BRL pg/kg 13 0.36
BRL pg/kg 6.7 0.67
BRL pg/kg 6.7 0.50
BRL pg/kg 13 0.57
BRL pg/kg 13 0.58
BRL pg/kg 6.7 0.46
BRL pg/kg 13 0.53
BRL pg/kg 6.7 0.34
BRL pg/kg 13 0.50
BRL pg/kg 13 0.50
BRL pg/kg 67 0.70
BRL pg/kg 13 0.35
BRL pg/kg 13 0.67
BRL pg/kg 27 2.6
BRL pg/kg 4.0 0.54
BRL pg/kg 6.7 0.47
BRL pg/kg 6.7 0.40
BRL pg/kg 6.7 0.59
BRL pg/kg 6.7 0.50
BRL pg/kg 13 0.78
BRL pg/kg 13 0.43
BRL pg/kg 6.7 0.39
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussetl
8260B 06/08/07 1747 erussefi
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erusset
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erusseU
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erusseU
8260B 06/08/07 1747 erussell
8260B 06/08/07 1747 erussell
Batch
ID
Q24147
024147
024147
024147
Q24147
024147
Q24147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
024147
Q24147
024147
024147
024147
024147
024147
024147
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical EnvironmntaI Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Factor Date/Time
Method Analysis Analyst
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 30 of 45
Fall Service Analytical
Environmental Solutions
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Laboratory Report
06/18/07
WS-4
183635
G06071 79
06/06/07 1445
06/06/07 1640
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
AnalysiL Batch
ID
Chlorobenzene BRL pg/kg 6.7 0.51 8260B 06/08/07 1747 erussell 024147
Chlorodibromomethane BRL pg/kg 6.7 0.46 8260B 06/08/07 1747 erussell 024147
Chioroethane BRL pg/kg 13 0.55 8260B 06/08/07 1747 erussell 024147
Chloroform BRL pg/kg 6.7 0.50 8260B 06/08/07 1747 erussell Q24147
Chloromethane BRL pg/kg 13 0.47 8260B 06/08/07 1747 erussell 024147
cis-12-Dichloroethene BRL pg/kg 6.7 0.30 8260B 06/08/07 1747 erussell Q24147
cis-13-Dichloropropene BRL pg/kg 6.7 0.43 8260B 06/08/07 1747 erussell 024147
Dbromomethane BRL pg/kg 6.7 0.50 8260B 06/08/07 1747 erussell 024147
Dchlorodifluoromethane BRL pg/kg 13 1.5 8260B 06/08/07 1747 erussell Q24147
Ethylbenzene BRL pg/kg 6.7 0.47 8260B 06/08/07 1747 ewssell 024147
Hexachlorobutadiene BRL pg/kg 20 0.84 8260B 06/08/07 1747 erussell 024147
lsopropyl ether IPE BRL pg/kg 6.7 0.23 8260B 06/08/07 1747 erusselt 024147
Isopropylbenzerie BRL pg/kg 13 0.54 8260B 06/08/07 1747 erussell 024147
mp-Xylenes BRL pg/kg 13 0.94 8260B 06/08/07 1747 erussett Q24147
Methyl ethyl ketone MEK BRL pg/kg 27 1.9 826GB 06/08/07 1747 erussell 024147
Methyl t-butyl ether MTBE BRL pg/kg 6.7 0.39 826GB 06/08/07 1747 erusselt 024147
Methylene chloride BRL pg/kg 13 0.55 8260B 06/08/07 1747 erussell 024147
n-Butylbenzene BRL pg/kg 20 0.54 826GB 06/08/07 1747 erussell 024147
n-Propylbenzene BRL pg/kg 13 0.40 8260B 06/08/07 1747 erusselt 024147
Naphthalene BRL pg/kg 6.7 0.78 826GB 06/08/07 1747 erussell 024147
o-Xylene BRL pg/kg 6.7 0.40 8260B 06/08/07 1747 erusset Q24147
p-lsopropyltoluene BRL pg/kg 20 0.55 8260B 06/08/07 1747 erusselt 024147
sec-Butylbenzerie BRL pg/kg 20 0.44 8260B 06/08/07 1747 erusselt 024147
Styrene BRL pg/kg 6.7 0.67 826GB 06/08/07 1747 erussel 024147
tert-Butylbenzene BRL pg/kg 27 0.42 8260B 06/08/07 1747 erussell 024147
Tetrachloroethene BRL pg/kg 13 1.2 826GB 06/08/07 1747 erussell Q24147
Toluene BRL pg/kg 6.7 0.46 8260B 06/08/07 1747 erusselt 024147
Page 31 of 45
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Project ID Morehead Commons No CJient Sample ID WS-4
Prism Sample ID 183635SampleMatrixSoilCOCGroupG0607179
Time Collected 06/06/07 1445
Time Submitted 06/06/07 1640
BRL
BRL
BRL
BRL
pg/kg
pg/kg
pg/kg
pg/kg
6.7 0.47
6.7 0.40
6.7 0.55
13 0.86
8260B
8260B
8260B
8260B
06/08/07 1747 erusseji
06/08/07 1747 erussell
06/08/07 1747 erussell
06/08/07 1747 erussell
024147
024147
Q24147
024147
ÆH
Full SeMcn An lytcaI roum Ia lub
ESP Associates PA
Atth Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
ltrans-12-Dichoroethene BRL pg/kg 6.7 0.51 8260B 06/08/07 1747 erussell Q24147
trans-i 3-Dichloropropene
Trichioroethene
Trichlorofluorom ethane
Vinyl chloride
Surrogate Recovery Control Limits
Toluene-d8 101 81 128
Bromofluorobenzene 106 77-128
Dibromofluoromethane 92 67 143
--Sample Weight Determination
Weight Bisulfate 4.51 5035 06/13/07 000 Ibrown
Weight Bisulfate 4.29 5035 06/13/07 000 brown
Weight Methanol 4.58 5035 06/13/07 000 brown
Semi-volatile Organic Compounds by GC/MS
l24-Trichlorobenzene BRL pg/kg 380 38 8270C 06/11/07 1352 kcampigotto 024124
12-Dichlorobenzene BRL pg/kg 380 28 8270C 06/11/07 1352 kcampigotto Q24124
13-Dichlorobenzene BRL pg/kg 380 27 8270C 06/11/07 1352 kcampigotto Q24124
14-Dichlorobenzene BRL pg/kg 380 34 8270C 06/11/07 1352 kcampigotto 024124
245-Trichiorophenol BRL pg/kg 380 39 8270C 06/11/07 1352 kcampigouo 024124
246-Trichlorophenol BRL pg/kg 380 36 8270C 06/11/07 1352 kcampigotto 024124
24-Dichloropheriol BRL pg/kg 380 32 8270C 06/11/07 1352 kcampigotto Q24124
24-Dimethyiphenol BRL pg/kg 380 37 8270C 06/11/07 1352 kcampigotto 024124
24-Dinitrophenol BRL pg/kg 380 43 8270C 06/11/07 1352 kcampigotto Q24124
24-Dinitrotoluene BRL pg/kg 380 21 8270C 06/11/07 1352 kcampigotto 024124
26-Dinitrotojuene BRL pg/kg 380 40 8270C 06/11/07 1352 kcampigotto Q24124
2-Chloronaphthalene BRL pg/kg 380 39 8270C 06/11/07 1352 kcampigotto Q24124
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 32 of 45
Full Service Analytical
Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
0611 8/07
WS-4
183635
G06071 79
06/06/07
06/06/07
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1445
1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
2-Chlorophenol BRL pg/kg 380 30
8270C 06/11/07 1352 kcampigotto 024124
2-Methylnaphthalene BRL pg/kg 380 30
8270C 06/11/07 1352 kcampigotto 024124
2-Methyiphenol BRL pg/kg 380 36 8270C 06/11/07 1352 kcampigottci 024124
2-Nitrophenol BRL pg/kg 380 45 8270C 06/11/07 1352 kcampigotto 024124
34-Methyphenol BRL pg/kg 380 39 8270C 06/11/07 1352 kcampigotto 024124
33-Dichlorobenzidine BRL pg/kg 380 24 8270C 06/11/07 1352 kcampigotto 024124
46-Dinitro-2-methylphenol BRL pg/kg 380 23 8270C 06/11/07 1352 kcampigottct Q24124
4-Bromophenyiphenylether BRL pg/kg 380 36 8270C 06/11/07 1352 kcampigottcl 024124
4-Chloro-3-methylphenol BRL pg/kg 380 28 8270C 06/11/07 1352 kcampigotto 024124
4-Chiorophenyiphenylether BRL pg/kg 380 23
8270C 06/11/07 1352 kcampigotto 024124
4-Nitropheriol BRL pg/kg 380 25 8270C 06/11/07 1352 kcampigotto 024124
Acenaphthene BRL pg/kg 380 37 8270C 06/11/07 1352 kcampigotto 024124
Acenaphthylene BRL pg/kg 380 38 8270C 06/11/07 1352 kcampigotto 024124
Anthracene BRL pg/kg 380 29 8270C 06/11/07 1352 kcampgotto 024124
Benzoaanthracene BRL pg/kg 380 53 8270C 06/11/07 1352 kcampigotto 024124
Benzoapyrene BRL pg/kg 380 44 8270C 06/11/07 1352 kcampigotto 024124
Benzobfluoranthene BRL pg/kg 380 17 8270C 06/11/07 1352 kcampigotto 024124
Benzoghiperylene BRL pg/kg 380 18 8270C 06/11/07 1352 kcampigotto Q24124
Benzokfluoranthene BRL pg/kg 380 31 8270C 06/11/07 1352 kcampigotto 024124
Bis2-chloroethoxymethane BRL pg/kg 380 44 8270C 06/11/07 1352 kcampigotto 024124
Bis2-chloroethylether BRL pg/kg 380 41 8270C 06/11/07 1352 kcampigotto 024124
Bis2-chloroisopropylether BRL pg/kg 380 32 8270C 06/11/07 1352 kcampigotto 024124
Bis2-ethylhexylphthalate BRL pg/kg 380 19 8270C 06/11/07 1352 kcampigotto 024124
Butylbenzylphthalate BRL pg/kg 380 23 8270C 06/11/07 1352 kcampigotto 024124
Chrysene BRL pg/kg 380 63 8270C 06/11/07 1352 kcampigotto 024124
Di-n-butylphthalate BRL pg/kg 380 17 8270C 06/11/07 1352 kcampigotto 024124
Di-n-octylphthalate BRL pg/kg 380 28 8270C 06/11/07 1352 kcampigotto 024124
Page 33 of 45
ESP Associates PA
Attn Chris Ward
Box7030
Charlotte NC 28241
Laboratory Report
06/18/07
WS-4
183635
G06071 79
06/06/07
06/06/07
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Survice Anulytical Environmental Solutions
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method
Limit Factor
1445
1640
Analyst Batch
ID
Analysis
Date/Time
Dibenzoahanthracene BRL pg/kg 380 38 8270C 06/11/07 1352 kcampigotto 024124
Dibenzofuran BRL pg/kg 380 33
8270C 06/11/07 1352 kcampigotto 024124
Diethylphthalate BRL pg/kg 380 23
8270C 06/11/07 1352 kcampigotto 024124
Dimethylphthalate BRL pg/kg 380 26 8270C 06/11/07 1352 kcampigotto 024124
Fluoranthene BRL pg/kg 380 26 8270C 06/11/07 1352 kcampigotto 024124
Fluorene BRL pg/kg 380 23 8270C 06/11/07 1352 kcampigotto 024124
Hexachlorobenzene BRL pg/kg 380 20 8270C 06/11/07 1352 kcampigotto Q24124
Hexachlorobutadiene BRL pg/kg 380 37 8270C 06/11/07 1352 kcampigotto 024124
Hexachlorocyclopentadiene BRL pg/kg 380 40 8270C 06/11/07 1352 kcampigotto 024124
Hexachloroethane BRL pg/kg 380 39 8270C 06/11/07 1352 kcampigotto 024124
lrideno1 23-cdpyrene BRL pg/kg 380 39 8270C 06/11/07 1352 kcampigotto 024124
Isophorone BRL pg/kg 380 34 8270C 06/11/07 1352 kcampigotto 024124
N-Nitrosodi-n-propylamine BRL pg/kg 380 43 8270C 06/11/07 1352 kcampigotto Q24124
N-Nitrosodiphenylarnine BRL pg/kg 380 19 8270C 06/11/07 1352 kcampigotto 024124
Naphthalene BRL pg/kg 380 41 8270C 06/11/07 1352 kcampigotto 024124
Nitrobenzene BRL pg/kg 380 37 8270C 06/11/07 1352 kcampigotto Q24124
Pentachlorophenol BRL pg/kg 380 32 8270C 06/11/07 1352 kcampigotto Q24124
Phenanthrene BRL pg/kg 380 19 8270C 06/11/07 1352 kcampigotto 024124
Phenol BRL pg/kg 380 41 8270C 0/11/07 1352 kcampigotto Q24124
Pyrene BRL pg/kg 380 26 8270C 06/11/07 1352 kcamplgotto 024124
Page 34 of 45
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
O.Box7030
Charlotte NC 28241
WS-4
183635
G06071 79
06/06/07 1445
06/06/07 1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 30.17 mL 3550B 06/08/07 700 dpope P18579
Extractable Petroleum Hydrocarbons by
GC-FID
Cli -022 Aromatics BRL
C19-C36 Aliphatics BRL
C9-C18 Aliphatics BRL
Analysis Note for CllC22 Aromatics
Sample Preparation
Adjusted value
9.64g mL EPH
Sample Preparation
Volatile Petroleum Hydrocarbons by GC-PID/FID
C5-C8 Aliphatics BRL
C9-C10 Aromatics BRL
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Surrogate Recovery Control Limits
2-Fluorophenol 60 14 89
2-Fluorobiphenyl 73 21 108
Phenol-d5 62 13-95
246-Tribromophenol 83 25-123
Nitrobenzene-d5 53 14 103
Terphenyl-d14 86 41 136
mg/kg
mg/kg
mg/kg
12 6.5 MADEPEPH
12 1.8 MADEPEPH
12 3.8 MADEPEPH
06/16/07
06/16/07
06/16/07
939
939
939
grappaccioli
grappaccioli
grappacciofli
dpope
024301
Q24301
024301
P1861406/13/07 800
Metals by ICP
Chromium
Lead
Surrogate Recovery Control Limits
2-Fluorobiphenyl 126 40 140
1-Chloro-octadecane 106 40 140
o-Terphenyl 105 40-140
2-Bromonaphthalene 129 40 140
0.71 mg/kg 0.28 0.017 601DB 06/11/07 2129 mcampbell 024176
4.1 mg/kg 0.28 0.024 601DB 06/11/07 2129 mcampbell 024176
2.06 50 mL 305DB 06/11/07 905 jhoppel P18580
mg/kg 5.8 1.1 MADEPVPH 06/12/07 2330 hwagner Q24220
mg/kg 5.8 0.035 MADEP VPH 06/12/07 2330 hwagner 024220
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 35 of 45
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-4
183635
G06071 79
06/06/07 1445
06/06/07 1640
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
Analyst Batch
ID
BRL mg/kg 5.8 1.8
MADEPVPH 06/12/07 2330 hwagner Q24220
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-Cl2 Aliphatics Adjusted value
One surrogate recovery
was outside the control limits No target compounds were detected in
this sample No further action was taken
Surrogate Recovery Control Limits
Sample Weight Determination
Weight 19.14
Weight 18.65
25-Dibromotoluene-PID 118 70-130
25-Dibromotoluene-FID 176 70 130
MADEP VPH 06/13/07 000 brown
MADEP VPH 06/13/07 000 brown
Sample Comments
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical
Environmental Solutions
Laboratory Report
06/18/07
Parameter
C9-C12 Aliphatics
Angela Overcash V.P Laboratory Services
Page 36 of 45
Full Service Analytmal Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
183636
G06071 79
06/06/07 1500
06/06/07 1640
Parameter Result Units Report MDL
Percent Solids Determination
Percent Solids
88.4
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/18/07
Limit
Dilution Method
Factor
Analysis
Date/Time
Analyst Batch
ID
SM2540 06/11/07 1700 Ibrown
Organochlorine Pesticides by Gas Chromatography
44-DDD BRL pg/kg 2.3 0.69 8081A 06/14/07 156 Jvogel 024275
44-DDE BRL pg/kg 2.3 0.48 8081A 06/14/07 156 jvogel 024275
44-DDT BRL pg/kg 2.3 0.81 8081A 06/14/07 156 jvogel 024275
44-Methoxychlor BRL pg/kg 4.5 1.5 8081A 06/14/07 156 jvogel Q24275
a-BHC BRL pg/kg 2.3 0.20 8081A 06/14/07 156 jvogel 024275
a-Chlordane BRL pg/kg 2.3 0.39 8081A 06/14/07 156 Jvogel Q24275
Aldrin BRL pg/kg 2.3 0.45 8081A 06/14/07 156 jvogel 024275
b-BHC BRL pg/kg 2.3 0.57 8081A 06/14/07 156 Jvogel 024275
Chiordane BRL pg/kg 57 13 8081A 06/14/07 156 ivogel 024275
d-BHC BRL pg/kg 2.3 0.32 8081A 06/14/07 156 jvogel 024275
Dieldrin BRL pg/kg 1.1 0.47 8081A 06/14/07 156 Jvogel 024275
Endosulfan BRL pg/kg 2.3 0.40
8081A 06/14/07 156 jvogel 024275
Endosulfan II BRL pg/kg 2.3 0.51
8081A 06/14/07 156 jvogel Q24275
Endosulfan Sulfate BRL pg/kg 2.3 0.59 8081A 06/14/07 156 Ivogel 024275
Endrin BRL pg/kg 2.3 0.68 8081A 06/14/07 156 Jvogel 024275
Endrin Aldehyde BRL pg/kg 2.3 0.63
8081A 06/14/07 156 ivogel 024275
Endrin Ketone BRL pg/kg 2.3 0.45 8081A 06/14/07 156 jvogel 024275
g-BHC BRL pg/kg 2.3 0.26 8081A 06/14/07 156 ivogel 024275
g-Chlordane BRL pg/kg 2.3 0.37
8081A 06/14/07 156 jvogel 024275
Heptachlor BRL pg/kg 2.3 0.53 8081A 06/14/07 156 Jvogel 024275
HeptachlorEpoxide BRL pg/kg 2.3 0.42 8081A 06/14/07 156 jvogel 024275
Toxaphene BRL pg/kg 57 13 8081A 06/14/07 56 jvogel 024275
Page 37 of 45
_....
QORi l$
Fell Srice AnaIytic3l 5mironmental SolutirnTh
ESP Associates PA
Attn Chris
Ward
Box7030
Charlotte NC 28241
Laboratory Report
06/18/07
B-I
183636
G06071 79
06/06/07
06/06/07
Result Units Report MDL Dilution Method
Limit Factor
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories
Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter
1500
1640
Analysis
Date/Time
29.71 10 mL
Analyst Batch
ID
3550B 06/12/07 1000 dpope
Surrogate
Decachlorobiphenyl DCB
Tetrachloro-m-xylene TCMX
Recovery
136
108
P18598
Control Limits
26 204
40-162
mg/kg 0.057 0.010 8082 06/14/07 156 jvogel 024276
mg/kg 0.11 0.046 8082 06/14/07 156 jvogel 024276
mg/kg 0.057 0.018 8082 06/14/07 156 jvogel 024276
mg/kg 0.057 0.020
8082 06/14/07 156 jvogel Q24276
mg/kg 0.057 0.0078 8082 06/14/07 156 jvogel 024276
mg/kg 0.057 0.020 8082 06/14/07 156 jvogel 024276
mg/kg 0.057 0.015
8082 06/14/07 156 Jvogei 024276
Sample Preparation
Polychiorinated Biphenyls PCBs by GC-ECD
PCB1016 BRL
.1pCB-1221 BRL
.PCB-1232 BRL
PCB-1242 BRL
PCB-1248 BRL
PCB 1254 BRL
PCB-1260 BRL
Sample Preparation
Volatile Organic Compounds by CC/MS
1112-Tetrachloroethane BRL pg/kg
111-Trichioroethane BRL pg/kg
11 22-Tetrachloroethane BRL pg/kg
112-Trichloroethane BRL pg/kg
11-Dichioroethane BRL pg/kg
11 -Dichloroethene BRL pg/kg
11-Dichloropropene BRL pg/kg
123-Trichlorobenzene BRL pg/kg
29.71 10 mL 3550B 06/12/07 1000 dpope P18597
Surrogate Recovery Control Limits
Decachlorobiphenyl DCB 98 34-182
Tetrachloro-m-xylene TCMX 106 36 182
6.3 0.62
6.3 0.36
6.3 0.65
6.3 0.39
6.3 0.46
6.3 0.48
6.3 0.56
13 0.70
8260B
8260B
8260B
82606
8260B
82606
8260B
8260B
06/08/07 1820
06/08/07 1820
06/08/07 1820
06/08/07 1820
06/08/07 1820
06/08/07 1820
06/08/07 1820
06/08/07 1820
erussell
erussell
erussell
erussell
erussell
erussell
erusseH
erussell
024147
024147
Q24147
024147
024147
024147
024147
024147
Page 38 of 45
Foil Seroice Anulytical EnvIronmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
B-I
183636
G06071 79
06/06/07 1500
06/06/07 1640
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories
Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
123-Trichioropropane BRL pg/kg 6.3 0.56 826GB 06/08/07 1820 erussell 024147
124-Trichlorobenzene BRL pg/kg 13 0.61 826GB 06/08/07 1820 erussell 024147
124-Trimethylbenzene BRL pg/kg 13 0.48 826GB 06/08/07 1820 erussell 024147
12-Dibromo-3-chloropropane BRL pg/kg 6.3 1.0 8260B 06/08/07 1820 erussell 024147
12-DibromoethaneEDB BRL pg/kg 6.3 0.11 826GB 06/08/07 1820 erussell 024147
12-Dichlorobenzene BRL pg/kg 13 0.34 826GB 06/08/07 1820 erussell 024147
12-Dichioroethane BRL pg/kg 6.3 0.63
826GB 06/08/07 1820 erussell 024147
12-Dichloropropane BRL pg/kg 6.3 0.47
826GB 06/08/07 1820 erussell 024147
135-Trimethylbenzene BRL pg/kg 13 0.53 826GB 06/08/07 1820 erussell 024147
13-Dichlorobenzene BRL pg/kg 13 0.55 826GB 06/08/07 1820 erussell 024147
13-Dichioropropane BRL pg/kg 6.3 0.43 826GB 06/08/07 1820 erusset 024147
14-Dichlorobenzene BRL pg/kg 13 0.49 826GB 06/08/07 1820 erusselt 024147
22-Dichioropropane BRL pg/kg 6.3 0.32
826GB 06/08/07 1820 erussell 024147
2.-Chloroethyl vinyl ether BRL pg/kg 13 0.47 826GB 06/08/07 1820 erussell 024147
2-Chiorotoluene BRL pg/kg 13 0.47 826GB 06/08/07 1820 ewssell 024147
2-Hexanone BRL pg/kg 63 0.66 826GB 06/08/07 1820 erussell 024147
4-Chiorotoluene BRL pg/kg 13 0.33 826GB G6/08/07 1820 erussell 024147
4-Methyl-2-pentanone MIBK BRL pg/kg 13 0.63 826GB 06/08/07 1820 ewssell 024147
Acetone BRL pg/kg 25 2.5 826GB 06/08/07 1820 erussell 024147
Benzene BRL pg/kg 3.8 0.51
826GB 06/08/07 1820 erussell 024147
Bromobenzene BRL pg/kg 6.3 0.44
826GB G6/G8/G7 1820 erussell 024147
Bromochioromethane BRL pg/kg 6.3 0.38
8260B 06/08/07 1820 erussell 024147
Bromodichloromethane BRL pg/kg 6.3 0.56
826GB 06/08/07 1820 erussell 024147
Bromoform BRL pg/kg 6.3 0.47 826GB 06/08/07 1820 erussell 024147
Bromometharte BRL pg/kg 13 0.74 826GB 06/08/07 1820 erussell 024147
Carbon disulfide BRL pg/kg 13 G.41 826GB 06/08/07 1820 erussell 024147
---Carbon tetrachloride BRL pg/kg 6.3 0.37
826GB 06/08/07 1820 ewssell 024147
Page 39 of 45
....
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Parameter
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chioromethane
cis-1 2-Dichloroethene
cis-1 3-Dichloroproperie
Dibromomethane
Dichiorodifluorometharie
Ethylbenzerie
Hexachiorobutadiene
Isopropyl ether IPE
lsopropylbenzene
p-Xylenes
Methyl ethyl ketone MEK
Methyl t-butyl ether MTBE
Methylene chloride
ri-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p.isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ulI Service Anelytical
Environmental Solations
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID 183636
Sample Matrix Soil COG Group G0607179
Time Collected 06/06/07 1500
Time Submitted 06/06/07 1640
Result Units Report MDL Dilution Method
Limit Factor
Analysis
Date/Time
Analyst Batch
ID
BRL pg/kg 6.3 0.48
8260B 06/08/07 1820 erussell 024147
BRL pg/kg 6.3 0.43
8260B 06/08/07 1820 erussell 024147
BRL pg/kg 13 0.52 8260B 06/08/07 1820 erussell 024147
BRL pg/kg 6.3 0.47
8260B 06/08/07 1820 erussell 024147
BRL pg/kg 13 0.44 8260B 06/08/07 1820 erussell Q24147
BRL pg/kg 6.3 0.28
8260B 06/08/07 1820 erussell 024147
BRL pg/kg 6.3 0.41
8260B 06/08/07 1820 erussell Q24147
BRL pg/kg 6.3 0.47 8260B 06/08/07 1820 erussell 024147
BRL pg/kg 13 1.4 8260B 06/08/07 1820 erussell 024147
BRL pg/kg 6.3 0.44
8260B 06/08/07 1820 erussell 024147
BRL pg/kg 19 0.79 8260B 06/08/07 1820 erussell 024147
BRL pg/kg 6.3 0.22
8260B 06/08/07 1820 erussell 024147
BRL pg/kg 13 0.51 826DB 06/08/07 1820 erussell 024147
BRL pg/kg 13 0.89 8260B 06/08/07 1820 erussell 024147
BRL pg/kg 25 1.8 8260B 06/08/07 1820 erussell 024147
BRL pg/kg 6.3 0.37 826DB 06/08/07 .1820 erussetl Q24147
BRL pg/kg 13 0.52 826DB 06/08/07 1820 erussell Q24147
BRL pg/kg 19 0.51 826DB 06/08/07 1820 erussell 024147
BRL pg/kg 13 0.38 826DB 06/08/07 1820 erussell 024147
BRL pg/kg 6.3 0.74 826DB 06/08/07 1820 erussell 024147
BRL pg/kg 6.3 0.38 826DB 06/08/07 1820 erussell 024147
BRL pg/kg 19 0.52 826DB 06/08/07 1820 erussell 024147
BRL pg/kg 19 0.42 826DB 06/08/07 1820 erussell 024147
BRL pg/kg 6.3 0.63
826DB 06/08/07 1820 erussell 024147
BRL pg/kg 25 0.39 826DB 06/08/07 1820 erussell 024147
BRL pg/kg 13 1.1 826DB 06/08/07 1820 erussell 024147
BRL pg/kg 6.3 0.43
826DB 06/08/07 1820 erussell Q24147
Page 40 of 45
Full Suruice Anelytical
Enuironnentol Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
B-i
183636
G06071 79
06/06/07
06/06/07
Parameter
trans-i 2-Dichloroethene
trans-i 3-Dichloropropene
Trichioroethene
Trichiorofluoromethane
Vinyl chloride
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
MDL Dilution Method
Limit Factor
6.3 0.48
8260B
6.3 0.44 8260B
6.3 0.38 8260B
6.3 0.52
8260B
13 0.81 82606
Date/Time
06/08/07 1820
06/08/07 1820
06/08/07 1820
06/08/07 1820
06/08/07 1820
Analysis Analyst Batch
ID
ertissell Q24i 47
erussefl 024147
erussell Q24i47
erussell Q24i 47
erussell Q24i 47
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Result Units Report
1500
1640
BRL
BRL
BRL
BRL
BRL
4.36
4.46
4.07
Surrogate Recovery Control Limits
Bromofluorobenzene 106 77 128
Toluene-d8 101 81 128
Dibromofluoromethane 92 67 143
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
06/13/07 000
06/13107 000
06/13/07 000
Semi-volatile Organic Compounds by GC/MS
124-Trichlorobenzene BRL
12-Dichlorobenzene BRL
13-Dichlorobenzene BRL
4-Dichlorobenzene BRL
245-Trichlorophenol BRL
246-Trichlorophenol BRL
24-Dichiorophenol BRL
24-Dimethylphenol BRL
24-Dinitrophenol BRL
24-Dinitrotoluene BRL
26-Dinitrotoluene BRL
2-Chloronaphthalene BRL
5035
5035
5035
37 8270C
28 8270C
27 8270C
34 8270C
39 8270C
36 8270C
32 8270C
36 8270C
42 8270C
21 8270C
40 8270C
39 8270C
380
380
380
380
380
380
380
380
380
380
380
380
brown
Ibrown
brown
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcarnpigotto
kcampigotto
kcampigolio
kcampigotto
08/11/07
06/11/07
06/11/07
06/i 1/07
06/11/07
06/11/07
06/11/07
06/11/07
06/11/07
06/11/07
06/i 1/07
06/11/07
1442
1442
1442
1442
1442
1442
1442
1442
1442
1442
1442
1442
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
024124
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 41 of 45
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full SoMce Anulylical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter
Laboratory Report
06/18/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
B-i
183636
G06071 79
06/06/07 1500
06/06/07 1640
Analyst Batch
IDResultUnitsReportMDLDilutionMethod
Limit Factor
Analysis
Date/Time
2-Chiorophenol BRL pg/kg 380 30 8270C 06/11/07 1442 kcampigotto Q24124
2-Methylnaphthalene BRL pg/kg 380 30
8270C 06/11/07 1442 kcampigotto 024124
2-Methyiphenol BRL pg/kg 380 35
8270C 06/11/07 1442 kcampigotto 024124
2-Nitrophenol BRL pg/kg 380 45
8270C 06/11/07 1442 kcampigotto Q24i24
34-Methylphenol BRL pg/kg 380 39
8270C 06/11/07 1442 kcampigotto 024124
33-Dichlorobenzidine BRL pg/kg 380 24 8270C 06/11/07 1442 kcampigotto 024124
46-Dinitro-2-methylphenol BRL pg/kg 380 23
8270C 06/11/07 1442 kcampigotto 024124
4-Bromophenyiphenylether BRL pg/kg 380 36 8270C 06/11/07 1442 kcampigotto Q24124
4-Chloro-3-methylphenol BRL pg/kg 380 28
8270C 06/11/07 1442 kcampigotto 024124
4-Chiorophenylphenylether BRL pg/kg 380 23 8270C 06/11/07 1442 kcampigotto 024124
4-Nitrophenol BRL pg/kg 380 25
8270C 06/11/07 1442 kcampigotto 024124
Acenaphthene BRL pg/kg 380 37
8270C 06/11/07 1442 kcampigotto 024124
Acenaphthylene BRL pg/kg 380 38
8270C 06/11/07 1442 kcampigotto 024124
Anthracene BRL pg/kg 380 29
8270C 06/11/07 1442 kcampigotto 024124
Benzoaanthracene BRL pg/kg 380 53
8270C 06/11/07 1442 kcampigotto 024124
Benzoapyrene BRL pg/kg 380 44 8270C 06/11/07 1442 kcampigotto 024124
Benzobfluoranthene BRL pg/kg 380 17 8270C 06/11/07 1442 kcampigotto 024124
Benzoghiperylene BRL pg/kg 380 18 8270C 06/11/07 1442 kcampigotto 024124
Benzokfluoranthene BRL pg/kg 380 31 8270C 06/11/07 1442 kcampgofto 024124
Bis2-chloroethoxymethane BRL pg/kg 380 43
8270C 06/11/07 1442 kcampigotto 024124
Bis2-chloroethylether BRL pg/kg 380 41 8270C 06/11/07 1442 kcampigotto 024124
Bis2-chloroisopropylether BRL pg/kg 380 32
8270C 06/11/07 1442 kcampigotto 024124
Bis2-ethylhexylphthalate BRL pg/kg 380 19 8270C 06/11/07 1442 kcampigotto 024124
Butylbenzylphthalate BRL pg/kg 380 23 8270C 06/11/07 1442 kcampigoflo 024124
Chrysene BRL pg/kg 380 63
8270C 06/11/07 1442 kcampigotto 024124
Di-n-butylphthalate BRL pg/kg 380 17 8270C 06/11/07 1442 kcampigotto 024124
Di-n-octylphthalate BRL pg/kg 380 28 8270C 06/11/07 1442 kcampigotto 024124
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories
Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 42 of 45
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/18/07
B-I
183636
G06071 79
06/06/07
06/06/07
This report should not be reproduced except in its entirety without the
written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1500
1640
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Dibenzoahanthracene BRL pg/kg 380 38 8270C 06/11/07 1442 kcampigotto 024124
Dibenzofurari BRL pg/kg 380 32 8270C 06/11/07 1442 kcampigotto 024124
Diethylphthalate BRL pg/kg 380 23
8270C 06/11/07 1442 kcampigotto 024124
Dimethylphthalate BRL pg/kg 380 26
8270C 06/11/07 1442 kcampigotto Q24124
Fluàranthene BRL pg/kg 380 26
8270C 06/11/07 1442 kcampigotto Q24124
Fluorene BRL pg/kg 380 22 8270C 06/11/07 1442 kcampigotto Q24124
Flexachlorobenzene BRL pg/kg 380 20 8270C 06/11/07 1442 kcampigotto 024124
Hexachlorobutadiene BRL pg/kg 380 37
8270C 06/11/07 1442 kcampigotto 024124
Hexachiorocyclopentadiene BRL pg/kg 380 40
8270C 06/11/07 1442 kcampigotto 024124
Hexachioroethane BRL pg/kg 380 38
8270C 06/11/07 1442 kcampigotto 024124
Indeno123-cdpyrene BRL pg/kg 380 39 8270C 06/11/07 1442 kcampigotto 024124
Isophorone BRL pg/kg 380 34 8270C 06/11/07 1442 kcampigotto 024124
NNitrosodi-n-propylamine BRL pg/kg 380 43 8270C 06/11/07 1442 kcampigotto 024124
NNitrosodiphenylamine BRL pg/kg 380 19 8270C 06/11/07 1442 keampigotto Q24124
Naphthalene BRL pg/kg 380 41 8270C 06/11/07 1442 kcampigotto Q24124
Nitrobenzene BRL pg/kg 380 37
8270C 06/11/07 1442 kcampigotto 024124
Pentachlorophenol BRL pg/kg 380 32 8270C 06/11/07 1442 kcampigotto 024124
Phenanthrene BRL pg/kg 380 18 8270C 06/11/07 1442 kcampigotto 024124
Phenol BRL pg/kg 380 41 8270C 06/11/07 1442 kcampigotto 024124
Pyrene BRL pg/kg 380 26
8270C 06111/07 1442 kcampigotto 024124
Page 43 of 45
RISMLIESlNC
Full Service AnalyticOl
Environmental Solutions
ESP Associates PA
Attn Chris
Ward
P.O Box7030
Charlotte NC 28241
Laboratory Report
06/18/07
B-i
183636
G06071 79
06/06/07
06/06/07
Extractable Petroleum Hydrocarbons
by GC-FID
Ci 1-C22 Aromatics BRL mg/kg
C19-C36 Aliphatics BRL mg/kg
C9-C18 Aliphatics BRL mg/kg
Analysis Note for Cll-C22 Aromatics
Sample Preparation
Analyst Batch
ID
Recovery
82
83
60
71
69
89
Control Limits
25-123
21 -108
14-89
14-103
13 -95
41 -136
Surrogate Recovery Control Limits
2-Fluorobiphenyl 132 40 140
1-Chloro-octadecane 105 40 140
o-Terphenyl 103 40 140
2-Bromonaphthalene 136 40 140
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Parameter
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Sample Preparation
Result Units Report
Limit
1500
1640
MDL Dilution
Factor
Method Analysis
Date/Time
29.64 mL 3550B 06/08/07 700 dpope P18579
Surrogate
246-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-di
11 6.1 MADEP EPH 06/16/07 1031 grappaccioli 024301
11 1.7 MADEP EPH 06/16/07 1031 rappaccioli 024301
11 3.6 MADEP EPH 06/16/07 1031 grappaccioli 024301
Adjusted value
10.04 mL EPH
06/13/07 800 dpope P18614
Metals by
ICP
Chromium
Lead
1.0 mg/kg 0.28 0.017 6010B 06/11/07 2137 mcampbet 024176
3.8 mg/kg 0.28 0.024 6010B 06/11/07 2137 mcampbell 024176
Sample Preparation 50 mL 3050B 06/11/07 905 jhoppel P18580
Volatile Petroleum Hydrocarbons by
GC-PIDIFID
C5-C8 Aliphatics BRL mg/kg 5.7 1.1 MADEP VPH 06/13/07 012 hwagner 024220
C9-C10 Aromatics BRL mg/kg 5.7 0.034 MADEP VPH 06/13/07 012 hwagner 024220
Page 44 of 45
...... .......... ......
iiusM
Full Service Analyticul
Environmental Solutions
ESP Associates PA
Attn Chris Ward
O.Box7030
Charlotte NC 28241
Laboratory Report
Client Sample ID B-I
Prism Sample ID
COC Group
Time Collected
Time Submitted
06/18/07
Parameter Result Units Report MDL Dilution
Limit Factor
BRL mg/kg 5.7 1.7 MADEPVPH 06/13/07 012 hwagner
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-Cl2 Aliphatics Adjusted value
One surrogate recovery was outside the control limits No target compounds were detected in
this sample No further action was taken
Sample Weight Determination
Weight
Weight
Sample Comments
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances
indicated/n the case narrative and/or test comments
All results are reported on dry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Sample Matrix Soil
CO-Cl Aliphatics
183636
G06071 79
06/06/07
06/06/07
1500
1640
Method Analysis
Date/Time
Analyst Batch
ID
Q24220
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 145 70 130
25-Dibromotoluene-PID 102 70-130
19.38
26.09
MADEP VPH
06/13/07 000 brown
MADEP VPH 06/13/07 000 brown
Angela Overcash V.P Laboratory Services
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 45 of 45
NC Certification No 402 Level II QC Report
Sc Certification No 99012 6/19/07NCDrinkingWaterCertNo37735
Project ID Morehead Commons No COC Group Number G06071 79
Date/Time Submitted 6/6/07 1640
Semi-volatile Organic Compounds by GC/MS method 8270C
Method Blank CC Batch
Result RL Control Limit Units ID
24-Trichlorobenzene ND 330 165 pg/kg 024124
12-Dichlorobenzene ND 330 165 pg/kg 024124
13-Dichlorobenzene ND 330 165 pg/kg 024124
14-Dichlorobenzene ND 330 165 pg/kg 024124
245-Trichlorophenol ND 330 165 pg/kg 024124
246-Trichiorophenol ND 330 165 pg/kg 024124
24-Dichiorophenol ND 330 165 pg/kg 024124
24-Dimethyiphenol ND 330 165 pg/kg 024124
24-Dinitrophenol ND 330 165 pg/kg 024124
24-Dinitrotoluene ND 330 165 pg/kg 024124
26-Dinitrotoluene ND 330 165 pg/kg Q24124
2-Chloronaphthalene ND 330 165 pg/kg 024124
2-Chiorophenol ND 330 165 pg/kg 024124
2-Methylnaphthalene ND 330 165 pg/kg 024124
2-Methyiphenol ND 330 165 pg/kg 024124
2-Nitrophenol ND 330 165 pg/kg 024124
34-Methylphenol ND 330 165 pg/kg 024124
33-Dichlorobenzidine ND 330 165 pg/kg 024124
46-Dinitro-2-methylphenol ND 330 165 pg/kg 024124
4-Bromophenyiphenylether ND 330 165 pg/kg 024124
4-Chloro-3-methylphenol ND 330 165 pg/kg 024124
4-Chiorophenylphenylether ND 330 165 pg/kg Q241 24
4-Nitrophenol ND 330 165 pg/kg 024124
Acenaphthene ND 330 165 pg/kg 024124
Acenaphthylene ND 330 165 pg/kg 024124
Anthracene ND 330 165 pg/kg 024124
Benzoaanthracene ND 330 165 pg/kg 024124
Benzoapyrene ND 330 165 pg/kg 024124
Benzobfluoranthene ND 330 165 pg/kg 024124
Benzoghiperylene ND 330 165 pg/kg 024124
Benzokfluoranthene ND 330 165 pg/kg 024124
Bis2-chloroethoxymethane ND 330 165 pg/kg 024124
Bis2-chloroethylether ND 330 165 pg/kg 024124
Bis2-chloroisopropylether ND 330 165 pg/kg 024124
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris
Ward
Box 7030
Charlotte NC 28241
Page oflO
NC Certification No 402 Level II QC Report
Sc Certification No 99012
NC Drinking Water Cert No 37735 6/19/07
tervice Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COC Group Number G0607179
Attn Chris Ward Date/Time Submitted 6/6/07 1640
Box 7030
Charlotte NC 28241
Method Blank QC Batch
Result RL Control Limit Units ID
Bis2-ethylhexylphthalate ND 330 165 pg/kg Q24124
Butylbenzylphthalate ND 330 165 pg/kg Q24124
Chrysene ND 330 165 pg/kg 024124
Di-n-butylphthalate ND 330 165 pg/kg 024124
Di-n-octylphthalate ND 330 165 pg/kg Q24124
Dibenzoahanthracene ND 330 165 pg/kg 024124
Dibenzofuran ND 330 165 pg/kg 024124
Diethylphthalate ND 330 165 pg/kg 024124
Dimethylphthalate ND 330 165 pg/kg 024124
Fluoranthene ND 330 165 pg/kg Q24124
Fluorene ND 330 165 pg/kg 024124
Hexachlorobenzene ND 330 165 pg/kg 024124
Hexachiorobutadiene ND 330 165 pg/kg 024124
Hexachiorocyclopentadiene ND 330 165 pg/kg 024124
Hexachioroethane ND 330 165 pg/kg 024124
lndeno123-cdpyrene ND 330 165 pg/kg 024124
Isophorone ND 330 165 pg/kg 024124
N-Nitrosodi-n-propylamine ND 330 165 pg/kg 024124
N-Nitrosodiphenylamine ND 330 165 pg/kg 024124
Naphthalene ND 330 165 pg/kg 024124
Nitrobenzene ND 330 165 pglkg 024124
Pentachlorophenol ND 330 165 pg/kg Q24124
Phenanthrene ND 330 165 pg/kg 024124
Phenol ND 330 165 pg/kg 024124
Pyrene ND 330 165 pg/kg 024124
Laboratory Control Sample Recovery Recovery
Panges QC Batch
Result Spike
Amount Units ID
24-Trichlorobenzene 1293.98 1663.1 pg/kg 78 39-98 024124
4-Dichlorobenzene 1228.79 1663.1 pg/kg 74 37-95 024124
24-Dinitrotoluene 1502.16 1663.1 pg/kg 90 56-128 024124
2-Chlorophenol 1187.56 1663.1 pg/kg 71 37-98 024124
4-Chloro-3-methylphenol 1360.15 1663.1 pg/kg 82 45-111 024124
4-Nitrophenol 1595.27 1663.1 pg/kg 96 20-157 024124
Acenaphthene 1335.55 1663.1 pg/kg 80 44-110 024124
N-Nitrosodi-n-propylamine 1382.10 1663.1 pg/kg 83 38-101 024124
Pentachlorophenol 1774.85 1663.1 pg/kg 107 53-127 Q24124
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 10
NO 99012
Level II QC Report
NC Drinking Water Cert No 37735 6/19/07
FLIP Srj AnalrIimI Environmnti SoIuSois
ESP Associates PA Project ID Morehead Commons No COG Group Number G0607179
Attn Chris
Ward Date/Time Submitted 6/6/07 1640
Box 7030
Charlotte NC 28241
Recovery CC BatchLaboratoryControlSampleRecoveryRangesIDResult Spike Amount Units
Phenol 1249.41 1663.1 pg/kg 75 34.102 024124
Pyrene 1525.44 1663.1 pg/kg 92 54-131 024124
Recovery CIC BatchMatrixSpikeRecoveryRanges
Result Spike Amount UnitsSampleID
183523 24-Trichlorobenzene 1401.93 1665.3 pg/kg 84 26-97 024124
4-Dichlorobenzene 1292.04 1665.3 pg/kg 78 23-92 Q241 24
24-Dinitrotoluene 1659.67 1665.3 pg/kg 100 45-127 Q24124
2-Chlorophenol 1225.77 1665.3 pg/kg 74 25-94 024124
4-Chloro-3-methylphenol 1382.95 1665.3 pg/kg 83 31-113 024124
4-Nitrophenol 1736.26 1665.3 pg/kg 104 17-150 Q24124
Acenaphthene 1423.90 1665.3 pg/kg 86 36-107 024124
N-Nitrosodi-n-propylamine 1427.57 1665.3 pg/kg 86 22-105 024124
Pentachlorophenol 1823.17 1665.3 pg/kg 109 39-137 024124
Phenol 1305.69 1665.3 pg/kg 78 23-97 024124
Pyrene 1547.45 1665.3 pg/kg 93 45-133 024124
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range CC Batch
Sample ID Result Spike Amount Units ID
183523 124-Trichlorobenzene 1166.55 1662.5 pg/kg 70 26-97 18 0-37 024124
14-Dichlorobenzene 1196.47 1662.5 pg/kg 72 23-92 0-36 024124
24-Dinitrotoluene 1624.33 1662.5 pg/kg 98 45-127 0-29 024124
2-Chlorophenol 1144.28 1662.5 pg/kg 69 25-94 0-37 024124
4-Chloro-3-methytphenol 1250 1662.5 pg/kg 75 31-113 10 0-32 Q24124
4-Nitrophenol 1670.21 1662.5 pg/kg 100 17-150 0-32 024124
Acenaphthene 1376.99 1662.5 pg/kg 83 36-107 0-32 024124
N-Nitrosodi-n-propylamine 1309.17 1662.5 pg/kg 79 22-105 37 024124
Pentachlorophenol 1867.35 1662.5 pg/kg 112 39-137 0-27 024124
Phenol 1190.15 1662.5 pg/kg 72 23-97 0-42 024124
Pyrene 1564.16 1662.5 pg/kg 94 45-133 0-27 024124
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 10
NC Certification No 402 Level II QC Report
Sc Certification No 99012
NC Drinking Water Cert No 37735 6/19/07
Project ID Morehead Commons No COC Group Number G0607179
Date/Time Submitted 6/6/07 1640
hw rgIMq mifhrid 9lflR
Method Blank QC Batch
Result RI Control Limit Units ID
111-Trichioroethane ND 0.005 0.0025 mg/kg 024147
11 22-Tetrachloroethane ND 0.005 0.0025 mg/kg 024147
11 2-Trichloroethane ND 0.005 0.0025 mg/kg 024147
1-Dichloroethane ND 0.005 0.0025 mg/kg 024147
1-Dichloroethene ND 0.005 0.0025 mg/kg 024147
11-Dichioropropene ND 0.005 0.0025 mg/kg Q24147
23-Trichlorobenzene ND 0.005 0.0025 mg/kg 024147
23-Trichloropropane ND 0.005 0.0025 mg/kg 024147
24-Trichlorobenzene ND 0.005 0.0025 mg/kg 024147
24-Trimethylbenzene ND 0.005 0.0025 mg/kg 024147
2-Dibromoethane EDB ND 0.005 0.0025 mg/kg 024147
2-Dichlorobenzene ND 0.005 0.0025 mg/kg 024147
2-Dichloroethane ND 0.005 0.0025 mg/kg 024147
2-Dichloropropane ND 0.005 0.0025 mg/kg 024147
35-Trimethylbenzene ND 0.005 0.0025 mg/kg 024147
3-Dichlorobenzene ND 0.005 0.0025 mg/kg 024147
3-Dichloropropane ND 0.005 0.0025 mg/kg 024147
4-Dichlorobenzene ND 0.005 0.0025 mg/kg 024147
22-Dichloropropane ND 0.005 0.0025 mg/kg 024147
2-Chlorotoluene ND 0.005 0.0025 mg/kg 024147
2-Hexanone ND 0.05 0.025 mg/kg 024147
4-Chlorotoluene ND 0.005 0.0025 mg/kg 024147
4-Methyl-2-pentanone MIBK ND 0.05 0.025 mg/kg 024147
Acetone ND 0.05 0.025 mg/kg 024147
Benzene ND 0.003 0.0015 mg/kg 024147
Bromobenzene ND 0.005 0.0025 mg/kg 024147
Bromochioromethane ND 0.005 0.0025 mg/kg 024147
Bromodichioromethane ND 0.005 0.0025 mg/kg 024147
Bromofomi ND 0.005 0.0025 mg/kg 024147
Bromomethane ND 0.01 0.005 mg/kg 024147
Carbon tetrachloride ND 0.005 0.0025 mg/kg 024147
Chlorobenzene ND 0.005 0.0025 mg/kg Q24147
Chlorodibromomethane ND 0.005 0.0025 mg/kg Q24147
Chloroethane ND 0.01 0.005 mg/kg 024147
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Page of 10
NC Certification No 402 Level II QC Renort
Sc Certification No 99012
NC Drinking Water Cert No 37735 6/19/07
SeMen Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COC Group Number 00607179
Attn Chris Ward Date/Time Submitted 6/6/07 1640
Box 7030
Charlotte NC 28241
Method Blank QC Batch
Result RL Control Umit Units ID
Chloroform ND 0.005 0.0025 mg/kg 024147
Chioromethane ND 0.005 0.0025 mg/kg Q24147
cis-1 2-Dichloroethene ND 0.005 0.0025 mg/kg 024147
cis-1 3-Dichloropropene ND 0.005 0.0025 mg/kg Q24 147
Dichiorodifluoromethane ND 0.005 0.0025 mg/kg 024147
Ethylbenzene ND 0.005 0.0025 mg/kg Q24147
lsopropyl ether IPE ND 0.005 0.0025 mg/kg 024147
lsopropylbenzene ND 0.005 0.0025 mg/kg 024147
mp-Xylenes ND 0.01 0.005 mg/kg 024147
Methyl ethyl ketone MEK ND 0.1 0.05 mg/kg 024147
Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg 024147
Methylene chloride ND 0.005 0.0025 mg/kg Q24147
n-Butylbenzene ND 0.005 0.0025 mg/kg 024147
n-Propylbenzene ND 0.005 0.0025 mg/kg 024147
Naphthalene ND 0.01 0.005 mg/kg 024147
o-Xylene ND 0.005 0.0025 mg/kg 024147
p-Isopropyltoluene ND 0.005 0.0025 mg/kg 024147
sec-Butylbenzene ND 0.005 0.0025 mg/kg 024147
Styrene ND 0.005 0.0025 mg/kg C124147
tert-Butylbenzene ND 0.005 0.0025 mg/kg Q24147
Tetrachloroethene ND 0.005 0.0025 mg/kg 024147
Toluene ND 0.005 0.0025 mg/kg 024147
trans-I 2-Dichloroethene ND 0.005 0.0025 mg/kg 024147
trans-I 3-Dichloropropene ND 0.005 0.0025 mg/kg 024147
Trichioroethene ND 0.005 0.0025 mg/kg 024147
Trichlorofluoromethane ND 0.005 0.0025 mg/kg 024147
Vinyl acetate ND 0.025 0.0125 mg/kg 024147
Vinyl chloride ND 0.005 0.0025 mg/kg 024147
Laboratory Control Sample Recovery Recovery QC Batch
Result Spike Amount Units ID
II-Dichloroethene 0.04482 0.05 mg/kg 90 57-122 024147
Benzene 0.05086 0.05 mg/kg 102 62-119 024147
Chlorobenzene 0.05259 0.05 mg/kg 105 61-124 Q24147
Toluene 0.05299 0.05 mg/kg 106 57-1 22 024147
Trichloroethene 0.05366 0.05 mg/kg 107 59-129 024147
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] TeD Free Number 1-800/529-6364 Fax [phone] Page of 10
99012
Level II QC Report
NC Drinking Water Cert No 37735 6/19/07
Full Survice Analytical
Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COC Group Number G0607179
Attn Chris Ward Date/Time Submitted 6/6/07 1640
Box 7030
Charlotte NC 28241
RecoveryatrxSpikeRecoveryRanges CC Batch
IDResult Spike Amount Units YeSampleID
183205 11
-Dichloroethene 0.04446 0.05 mg/kg 89 44-1 40 Q24147
Benzene 0.0476 0.05 mg/kg 95 46-136 024147
Chlorobenzene 0.04586 0.05 mg/kg 92 47-135 024147
Toluene 0.0476 0.05 mg/kg 95 47-136 024147
Trichloroethene 0.04859 0.05 mg/kg 97 45-141 Q24147
Recovery RPDMatrixSpikeDuplicateRecoveryRangesRPDRange CC Batch
Result Spike Amount Units iD
Sample ID
183205 11-Dichloroethene .04499 0.05 mg/kg 90 44-140 0-23 024147
Benzene 0.04937 0.05 mg/kg 99 46-1 36 -22 024147
Chlorobenzene 0.0472 0.05 mg/kg 94 47-135 -22 024147
Toluene 0.04972 0.05 mg/kg 99 47-1 36 0-22 024147
Trichloroethene 0.05061 0.05 mg/kg 101 45-141
0-23 024147
Metals by ICP method 6010B
Method Blank oc Batch
Result RL Control Limit Units iD
Chromium 0.0513 0.25 0.125 mg/kg 024176
Lead 0.0663 0.25 0.125 mg/kg 024176
Laboratory Control Sample Recovery Recovery CC BatchRanges
Result Spike Amount Units Jo ID
Chromium 22.4412 25 mg/kg 90 80-1 20 024176
Lead 21.4504 25 mg/kg 86 80-120 024176
Matrix Spike Recovery Recovery
Ranges CC Batch
IDResult Spike Amount UnitsSampleID
183632 Chromium 16.5648 24.875 mg/kg 65 75-1 25 Q24176
Lead 20.5958 24.875 mg/kg 66 75-125 024176
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range CC Batch
Sample ID Result Spike Amount Units ID
183632 Chromium 16.0388 24.630 mg/kg 63 75-125 0-20 024176
Lead 18.9135 24630 mg/kg 60 75-1 25 20 024176
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704I59-6364 Toll Free Number 1-8001529-6364 Frnr 704155-0409 Page of 10
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
tnrvlce Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6/19/07
Project ID Morehead Commons No COC Group Number G0607179
Date/Time Submitted 6/6/07 1640
OL..i..411 .bons by GC-PID/FID mgshnd MAflEP VPH.JIaIIc roll otain 10111 ...._
Method Blank CC
Result RI Control Umit Units ID
C5-C8 4AJiphatics ND 2.5 mg/kg Q24220
C9-C10 Aromatics ND 2.5 mg/kg Q24220
C9-Cl2Aliphatics ND 2.5 mg/kg Q24220
Laboratory Control Sample Recovery Recovery
Ranges CIC Batch
Result Spike Amount Units ID
C5-C8 Aliphatics 14.906 15 mg/kg 99 70-1 30 Q24220
C9-Cl0Aromatics 3.909 mg/kg 78 70-130 Q24220
C9-C12 Aliphatics 9.460 10 mg/kg 95 70-1 30 Q24220
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample ID Result Spike Amount Units ID
183632 C5-C8 Aliphatics 11.352 15 mg/kg 76 70-130 Q24220
C9-C10 Aromatics 3.501 mg/kg 70 70-1 30 Q24220
C9-Cl2Aliphatics 7.313 10 mg/kg 73 70-130 Q24220
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range
Sample ID Result Spike Amount Units
OC
31atch
183632 C5-C8 Aliphatics 12.679 15 mg/kg 85 70-130 11 -25 Q24220
C9-C10 Aromatics 3.573 mg/kg 71
70-1 30 -25 Q24220
C9-Cl2Aliphaflcs 7.963 10 mg/kg 80 70-130 0-25 Q24220
Page of 10
ESP Associates PA
Attn Chris
Ward
Box7030
Charlotte NC 28241
Q24275
024275
Q24275
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Full Service Analytical
Environmental
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6/19/07
Project ID Morehead Commons No COC Group Number G0607179
Date/Time Submitted 6/6/07 1640
by Gas hr Ianrrahn niafhntl 8081A.ji gal iuuui.r lul ..
Method Blank QC Batch
Result RL Control Limit Units
ID
44-DDD ND pg/kg Q24275
44-DDE ND pg/kg 024275
44-DDT ND pg/kg Q24275
44-Methoxychlor ND pg/kg 024275
a-BHC ND pg/kg 024275
a-Chlordane ND pg/kg 024275
Aldrin ND pg/kg 024275
b-BHC ND pg/kg 024275
Chlordane ND 50 25 pg/kg 024275
d-BHC ND pg/kg Q24275
Dieldrin ND 0.5 pg/kg Q24275
Endosulfan ND pg/kg 024275
Endosulfan II ND pg/kg 024275
Endosulfan Sulfate ND pg/kg 024275
Endrin ND pg/kg 024275
Endrin Aldehyde ND pg/kg 024275
Endrin Ketone ND pg/kg 024275
g-BHC ND pg/kg 024275
g-Chlordane ND pg/kg 024275
Heptachlor ND pg/kg 024275
Heptachlor Epoxide ND pg/kg 024275
Toxaphene ND 50 25 pg/kg 024275
Laboratory Control Sample Recovery Recovery
Ranges QC Batch
Result Spike Amount Units U/ID
44-DDT 33.83 33 pg/kg 103 75-141 024275
AIdrin 34.73 33 pg/kg 105 66-132 024275
Dieldrin 34.69 33 pg/kg 105 72-136 024275
Endrin 34.14 33 pg/kg 103 74-147 024275
Heptachlor 32.89 33 pg/kg 100 72-134 024275
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample ID Result Spike Amount Units u/v ID
183801 44-DDT 27.6 33 pg/kg 84 56-163
Aldrin 33.4 33 pg/kg 101 57-137
Dieldrin 26.0 33 pg/kg 79 60-141
Page8oflO
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
.ervice Analytical Environmeni_.._.__ons
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories lnc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax 704I525-0409
Level QC Report
6/19/07
Project ID Morehead Commons No COG Group Number G0607179
Date/Time Submitted 616/07 1640
Matrix Spike Recovery Recovery
Ranges OC Batch
IDResult Spike Amount UnitsSamplelD
183801 Endrin 28.0 33 pg/kg 85 65-164 024275
Heptachlor 27.2 33 pg/kg 82 63-142 Q24275
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range QC Batch
sample l0 Result Spike Amount Units c/c ID
183801 44-DDT 31.1 33 pg/kg 94 56-163 12 0-38 Q24275
Aldrin 35.8 33 pg/kg 108 57-1 37 -29 Q24275
Dieldrin 28.9 33 pg/kg 88 60-1 41 11 30 024275
Endrin 30.9 33 pg/kg 94 65-1 64 10 0-21 024275
Heptachlor 29.7 33 pg/kg 90 63-1 42 0-27 024275
Povchlorinated Biphenvis PCBs by GC-ECD method 8082
Method Blank oc natch
Result RL Control Limit Units it
PCB-1016 ND 0.05 0.025 mg/kg 024276
PCB-1221 ND 0.1 0.05 mg/kg 024276
PCB-1 232 ND 0.05 0.025 mg/kg 024276
PCB-1242 ND 0.05 0.025 mg/kg 024276
PCB-1248 ND 0.05 0.025 mg/kg Q24276
PCB-1254 ND 0.05 0.025 mg/kg 024276
PCB-1 260 ND 0.05 0.025 mg/kg Q24276
Laboratory Control Sample Recovery Recovery
Ranges QC Batch
Result Spike Amount Units ID
PCB-1 016 0.308 0.333 mg/kg 92 64-1 51 024276
PCB-1260 0.306 0.333 mg/kg 92 45-166 Q24276
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample_ID Result Spike
Amount Units Ya ID
183632 PCB-1016
0.325 0.333 mg/kg 98 14-1 92 Q24276
PCB-1 260 0.337 0.333 mg/kg 101
10-1 92 Q24276
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range QC Batch
Sample ID Result Spike
Amount Units ID
183632 PCB-1016
0.290 0.333 mg/kg 87 14-1 92 11 0-40 024276
PCB-1260 0.298 0.333 mg/kg 89 10-1 92 12 0-40 024276
Page of 10
-See Case Narrative
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Level II QC Report
6/19/07
Project ID Morehead Commons No COC Group Number G0607179
Date/Time Submitted 616/07 1640
lvr4hl ----by GC-FID m.hn1 MADEP EPHeUVIUIIIVul-_
Method Blank QC Batch
Result RL Control Limit Units ID
C11-C22 Aromatics ND 10 mg/kg Q24301
C19-C36 Aliphatics ND 10 mg/kg 024301
C9-Cl8Aliphatics ND 10 mg/kg Q24301
Laboratory Control Sample Recovery Recovery BatchRanges
Result Spike Amount Units ID
C11-C22Aromatics 168.1 170 mg/kg 99 40-140 024301
C19-C36Aliphatics 76.7 80 mg/kg 96 40-140 024301
C9-C18 Aliphatics 44.3 60 mg/kg 74 40-140 024301
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample ID Result Spike Amount Units ID
183819 C11-C22 Aromatics 156.68 170 mg/kg 92 40-140 Q24301
C19-C36Aliphatics 74.04 80 mg/kg 93 40-140 024301
C9-C18 Aliphatics 43.36 60 mg/kg 72 40-1 40 024301
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range DC Batch
Sample ID Result Spike
Amount Units ID
183819 C11-C22
Aromatics 164.44 170 mg/kg 97 40-140 0-50 024301
C19-C36 Aliphatics 75.54 80 mg/kg 94 40-1 40 0-50 024301
C9-Cl8Aliphatics 44.22 60 mg/kg 74 40-140 0-50 024301
Page 10 of 10
Full Service Analytical Environmental Solutions
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Fax 704/525-
Client Company Name
Report To/Contact Name
Reporting Address
Phone _______________Fax Yes No
Email Yes No Email Address
EDD Type PDF_Exce
Site Location Name
Site LocatEon Physical Address
Project Name
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reporting OC LEVEL III III IV
provisions and/or OC Re9ujr1mets
Invoice To 41J_Yt
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE__FL ____NC.j
SC_OTHER _____N/A_
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES iL NO
CHAIN OF CUSTODY RECORD
PAGE OF .J_QUOT TO NSURE PR ER BILLINGLLIJIL..
NO N/A
Samples INTACT upon arrival
Received ON WET lCE Temp
PROPER PRESERVATIVES indicated .rI ._
eceived THIN l4OLDl TIMES
CL.4STODY SEALS INTACV
VQl1tecd W/OUT HADPJAQE
ROPONTAINEf ued
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
Purchase Order No./Billing Reference1
Requested Due Date LI Day LI Days LI Da Days
Working Days LI 6-9 Days LI Sta ard 10 days LI pproved Be
Samples received after 1500 will be processed
next business day
Turnaround time is based on business days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY
PRISM LABORATORIES INC TO CLIENT -______________
TIME
COLLECTED
MILITARY
HOURS
MATRIX
SOILWATER OR
SLUDGE
SAMPLE CONTAINER
EaZ
Lf
SEE BELOW
i4ôz
NO
TL /1DP
SIZE
PRESERVA
TIVES
ANALYSES REQUESTED/óÆ42ii
icoo
VI
REMARKS
PRISM
LAB
ID NO
-i3
335
a3
-tennqusnea by Signature
Samplers Signature Sampled By
Print Name Affiliation
Upon relinquishing this .1cain of tody is your authorization for Prism to proceed with the analy as requested
above Any changes must be
submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been initialized
Date Military/HoursReceivedBySignature
Relinnuished By Signature
Relinquished
Method of Shipment NOtALL SAMPL
SA PLES
ARE OLERS SHOULD BE
ACCEPTED AND VERIF
Received By Sjnature
Receiv4rIBY
TAPED SHUT WITH GUST EALS FOR TRANSPORTATION
TO THE LABORATORY
lED AGAINST COG UNTIL RECEIVED AT THE
LABORATORY
Group No
Fed Ex LI UPS 1and-delivered Prism Field Service LI Other
Additional Comments
NPDES
ONC USC
UT GROUNDWATERNCUSCUNC USC
DRINKING WATER
ONC USC
SOLID WASTE
UNC USC
RCRA CERCLA
UNC USC UNC
USC
LANDFILL
UNC USC
OTHER
UNC USC
U____
SEE REVERSE FORTERMSCONDITIONS
PllNA
FuI ervce AnayticaI Envirnmental Solulions
CLIENT 5P ssks P4
A1IN Q1riS Wa-rd
PRISM COC GROUP
Pease fill in the Site Location information on the attached VPH and/or EPH Forms
\NasO1\FOLD\CoMMo\FoMs\vp EPH Site Location for CiienLdoc
VPH Aliphatics/Aromatics Laboratory Reporting Form
Client Name
Project Name
Site Location
ESP Associates PA
Morehead Commons No _____Laboratory Name
_____NC Certification Lab
Sample Matrix
Prism Laboratories Inc
402
Soil
Blank C5-C8 Aliphatics
C9-C12 Aliphatics
C9-C10 Aromatics
RL C5-C8 Aliphatics
C9-C12 Aliphatics
C9-C10_Aromatics
MDL C5-C8 Aliphatics
C9-C12 Aliphatics
C9-C1 Aromatics
Comments VPH trip blank was not submitted to the laboratory
Result outside of the QC limits
______-Sample Information and Analytical Results
Method for Ranges MADEP VPH
Sample Identification
Collection Option for soil
Date Collected
5-Dibrom
Date Received
Date Extracted
1.3
Date Analyzed
Dry Solids
If
183635
Dilution Factor
6/6/2007 6/6/2007
6/6/2007 6/6/2007
6/6/2007 6/6/2007 6/6/2007
183636
Hydrocarbon Ranges in mg/kg
C5-C8 Aliphatics
6/6/2007
C9-C12 Aliphatics
616/2007 6/6/2007
C9-C10 Aromatics
6/12/2007 6/12/2007 6/12/2007 6/12/2007 6/13/2007
6/12/2007 6/12/2007 6/12/2007 6/12/2007 6/13/2007
82.6 86.4 82.9 86.5 88.4
Sample Results Sample Results Sample Results Sample Results Sample Results
6.1 5.8 6.0 5.8
5.7
6.1 5.8 6.0 5.8 5.7
6.1 5.8 6.0
5.8 5.7
5.0 5.0 5.0 5.0 50
5.0 5.0
5.0 5.0 5.0
5.0 5.0 5.0 5.0 5.0
6.1 5.8 6.0 5.8 5.7
6.1 5.8 6.0 5.8 5.7
6.1 5.8 6.0 5.8 5.7
1.2 1.1 1.2 1.1 1.1
1.9 1.8 1.9 1.8 1.7
0.036 0.035 0.036 0.035 0.034
Surrogate Acceptance Range Blank 70-130%70-130%70-130 70-130% 70-130%
AliphaticSurrogate%Rec.-FID 116 155 183 165
176 145
Aromatic Surrogate Rec PID 91 118 1381 129 118 102
Option Established fill line on vial
Option Sampling
device indicate brand e.g EnCore TM
Option Field weight of soil
Unadjusted value should exclude the concentration of any surrogates internal standards and/or
concentrations of other ranges that elute within the specified range
Adjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank or Trip Blank
whichever is higher indicate type
Were all performance/acceptance standards for required QA/QC
procedures achieved YES No Details Attached
Were any significant modifications to the VPH method made NO Yes Details Attached
Page of VPH Soil
EPH Aliphatics/AromatiCS Laboratory Reporting Form
Client Name
Project Name
Site Location
Laboratory Name
NC Certification Lab
Sample Matrix
402
Soil
ESP Associates PA
Morehead Commons No.2
Prism Laboratories
Inc
Sample Information and Analytical Results
Method for Ranges MADEP EPH
EPH Surrogate Standards Aliphatic 1-Chloro-octadecane Aromatic o-Terphenyl
EPH Fractionation Surrogates nonaph 2-Fluorobiphenyl
Sample Identification 183633 183634
183635 183636
Date Collected 6/6/2007 6/6/2007 6/6/2007 6/6/2007
Date Received 6/6/2007 6/6/2007 6/6/2007 6/6/2007
Date Extracted 6/13/2007 6/13/2007
6/13/2007 6/13/2007
Date Analyzed 6/16/2007 6/17/2007 6/16/2007 6/16/2007
Dry Solids 86.4 82.9 86.5 88.4
Dilution Factor
Hydrocarbon Ranges in mg/kg Sample Results Sample Results Sample Results Sample Results Sample Results
C9C18AIiphatics 12 13 12 11
C19C36Aliphatics 12 13 12
11
C11C22Aromatics 12 13 12 11
Blank C9-Cl8Aliphatics 10 10 10 10_
C19-C36Aliphatics 10 10 10 10
C11-C22Aromatics 10 10 10 10
RL C9-Cl8Aliphatics 12 13 12 11_
C19-C36Aliphatics 12 13 12 11
C11-C22Aromatics 12 13 12 11
MDL C9-C18 Aliphatics 3.8 4.0 3.8 3.6_
C19-C36Aliphatics 1.8 1.9 1.8 1.7
Cl 1-C22 Aromatics
6.4 6.8 6.5 6.1
Surrogate Acceptance Range 40-1 40 40-1 40 40-1 40 40-140%
Aliphatic Surrogate Rec 128 112 95 138 106 105
Aromatic Surrogate Rec 107 102 98 114 105 103
Fractionation Surrogate Accep Range Blank 40-1 40 40-140 40-1 40 40-1 40 40-1 40
Frac Surrogate %Rec 134 135 111 132 129 136
Frac Surrogate Rec 132 131 107 128 126 132
Unadjusted value should exclude the concentration
of any surrogates internal standards and/or
concentrations of other ranges that elute within the specified range
Adjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank
Were all performance/acceptance standards for required QNQC
procedures achieved
Was blank correction applied as significant modification of the method
Were any significant modifications to the EPH method made
Comments
YES No Details Attached
Yes NO
NO Yes Details Attached
Page of EPH Soil
UN 2.Oftl
Case Narrative
PRISM
LABORATORIES INC
Date 06/15/07
Client Project ID Morehead Commons No
Company ESP Associates PA Prism COG Group No G0607193
Contact Chris Ward Collection Dates 06/07/07
Address Box 7030
Lab Submittal Dates 06/07/07
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory
Report Quality
Control and Subcontracted Laboratory Report with corresponding Chain-of-Custody totaling 22 pages chain-of-custody is also attached
for
the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key
reference for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
Analysis Note for Q24193 MSD Ethylbenzene Recovery below the control limits
\nalysis Note for Q24193 MSD mp-Xylenes RPD value outside the control limits
Analysis Note for Q241 93 MSD o-Xylene RPD value outside
the control limits
Metals Analysis
Analysis Note for Q24208 MS Barium Matrix interference is suspected
Analysis Note for Q24208 MSD Barium Matrix interference is suspected
Wet Lab and Micro Analysis
Total Halogens analysis subcontracted to GCAL Laboratory report is attached
Please call if you have any questions relating to this analycal report
Date Reviewed by Robbi Jones Project Manager Angela Q6vercash
Signature 4-1--1i Signature
Review Date 06/15/07 Approval Date 06/15/07
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentrafon
calibration range exceeded
The analyte was positively identified but the
value is estimated below the reporting limit
Estimated concentration
with high bias
Estimated concentraon with low bias
matrix effect is present
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories
Inc The results in this
report relate only to the samples submitted for analysis
449 Spngbrook Road P.O Box 240543
Chedotte NC 28224-0403
Phone [phone] Toll Free 800/529-6364 Fax [phone]
gall Service Analytical Environmental Solations
ESP Associates PA
Attn Chris
Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/15/07
la-123 Comp
183684
G06071 93
06/07107 1300
06/07/07 1400
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Percent Solids Determination
Percent Solids
Diesel Range Organics DRO by GC-FID
Diesel Range Organics DRO
Sample Preparation
Gasoline Range Organics GRO by GC-FID
Gasoline Range Organics GRO BRL
TCLP Extraction for Metals
TCLP Extraction Complete
Surrogate Recovery Control Limits
Dibromofluoromethane 106 67 143
Bromofluorobenzene 114 77-128
Toluene-d8 104 81 128
86 mg/kg 7.7 1.9 8015B 06/12/07 024 jvogel
49.6 mL 3550B 06/11/07 900 dpope
Q24213
P18609
Surrogate %Recovery Control Limits
o-Terphenyl 121 48 130
mg/kg 1.1 0.070 8015B 06/13/07 1328 hwagner Q24199
Surrogate Recovery Control Limits
aaa-TFT 103 55-129
1311 06/11/07 1340 jhoppel
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cent No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
90.5 SM2540 06/12/07 1640 Ithao
VolatiIe Organic Compounds by GC/MS
Benzene BRL pg/kg 3.4 0.46 8260B 06/12/07 2329 erusselt Q24193
Ethylbenzene BRL pg/kg 5.7 0.40 8260B 06/12/07 2329 erussell 024193
mp-Xylenes BRL pg/kg 11 0.80 8260B 06/12/07 2329 erussetl 024193
o-Xylene BRL pg/kg 5.7 0.34 8260B 06/12/07 2329 erussetl 024193
Totuene BRL pg/kg 5.7 0.39 8260B 06/12/07 2329 erussell 024193
Page of
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation
Total Halogen by Method 9076
Subcontract Report
5OmL 5OmL 3010A 06/12/07 715 jhoppel
Analysis Note for Subcontract Report Analysis subcontracted to NC certified lab It 618
Sample Comments
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
Full Service Anulyticol
Environmental Solutions
Laboratory Report
06/15/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID la-123 Comp
Attn Chris Ward Prism Sample ID 183684
Box 7030
Sample Matrix Soil coc Group G0607193
Charlotte NC 28241 Time Collected 06/07/07 1300
Time Submitted 06/07/07 1400
LCLP Leachable Mercury by CVAA
Mercury
Sample Preparation
TCLP Leachable Metals by ICP
Arsenic
BRL mg/L 0.010 0.000042
2OmL 3OmL
7470A 06/13/07 1257 jhoppel
7470A 06/13/07 735 jhoppel
Q24234
P18612
BRL mg/L 0.050 0.0029 6010B 06/12/07 2355 mcampbell 024208
Barium 0.69J mg/L 5.0 0.0019 601DB 06/12/07 2355 mcampbell Q24208
Cadmium 0.0010 mg/L 0.025 0.00034 60106 06/12/07 2355 mcampbell Q24208
Chromium 0.0074J mg/L 0.25 0.0006 60106 06/12/07 2355 mcampbell 024208
Lead 0.012 mg/L 0.050 0.0021 601DB 06/12/07 2355 mcampbell 024208
Selenium BRL mg/L 0.050 0.0035 601DB 06/12/07 2355 mcampbell 024208
Silver BRL mg/L 0.25 0.00025 6010B 06/12/07 2355 mcampbell Q24208
See
Attached
9076
P18602
Angela Overcash V.P Laboratory Services
Full Soruice Avulytical
Environmental Solutions
ESP Associates PA
Attn Chris Ward
O.Box7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
lb-234 Comp
183685
G06071 93
06/07/07 1315
06/07/07 1400
Result Units Report MDL Dilution
Limit Factor
91.5
Diesel Range Organics DRO by GC-FID
Diesel Range Organics DRO
Sample Preparation
Control Limits
81 -128
Bromofluorobenzene 111 77-128
Dibromofluoromethane 106 67 143
Surrogate Recovery Control Limits
o-Terphenyl 107 48 130
Surrogate Recovery Control Limits
aaa-TFT 89 55-129
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/15/07
Parameter
Percent Solids Determination
Percent Solids
Method Analysis Analyst
Batch
Date/Time ID
SM2540 06/12/07 1640 lthao
Volatile Organic Compounds by GC/MS
Benzene BRL pg/kg 3.5 0.46 8260B 06/13/07 012 erussell 024193
Ethylbenzene BRL pg/kg 5.8 0.41 8260B 06/13/07 012 erussell Q24193
mp-Xylenes BRL pg/kg 12 0.81 8260B 06/13/07 012 erussell 024193
o-Xylene BRL pg/kg 5.8 0.35 8260B 06/13/07 012 erussell 024193
Toluene BRL pg/kg 5.8 0.39 8260B 06/13/07 012 erussell 024193
Surrogate
Toluene-d8
Recovery
104
98 mg/kg 7.7 1.9 8015B 06/11/07 2347 ivogel 024213
49.76 mL 3550B 06/11/07 900 dpope P1 8609
Gasoline Range Organics GRO by GC-FID
Gasoline Range Organics GRO BRL
TCLP Extraction for Metals
TCLP Extraction Complete
mg/kg 1.1 0.070 8015B 06/13/07 1359 hwagner 024199
1311 06/11/07 1340 jhoppel
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Analysis
Date/Time
b-234 Comp
183685
G06071 93
06/07/07 1315
06/07/07 1400
Sample Preparation 50 mL 50 mL
Total Halogen by Method 9076
Subcontract Report
Sample Comments
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requfrements other thanNELACcertificationexceptforthoseinstances indicated in the case narrative and/or test comments
All results are reported on dnj-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
Laboratory Report
06/15/07
Parameter Result Units Report MDL Dilution
Limit
Method
Factor
TCLP Leachable Mercury by CVAA
Mercury
Sample Preparation
TCLP Leachable Metals by ICP
Arsenic
Analyst Batch
ID
BRL mg/L 0.010 0.000042 7470A 06/13/07 1231 ihoppel Q24234
20 mL 30 mL 7470A 06/13/07 735 jhoppel P18612
BRL mg/L 0.050 0.0029 6010B 06/13/07 015 mcampbelt Q24208
Barium 0.61 mg/L 5.0 0.0019 6010B 06/13/07 015 mcampbell Q24208
Cadmium 0.0006J mg/L 0.025 0.00034 6010B 06/13/07 015 mcampbell Q242o8
Chromium 0.0083J mg/L 0.25 0.0006 6010B 06/13/07 015 mcampbell Q24208
Lead 0.011 mg/L 0.050 0.0021 6010B 06/13/07 015 mcampbell 024208
Selenium BRL mg/L 0.050 0.0035 6010B 06/13/07 015 mcampbell 024208
Silver BRL mg/L 0.25 0.00025 6010B 06/13/07 015 mcampbell 024208
See
Attached
Analysis Note or Subcontract Report Analysis subcontracted
9076
P1 8602
3010A 06/12/07 715 jhoppel
to NC certified lab It 618
Page 4of
NC Certification No 402 Level II QC ReportSCCertificationNo99012
6/15/07NCDnnkingWaterCertNo37735
Full Service Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COG Group Number G0607193
Attn Chris Ward Date/Time Submitted 6/7/07 1400
O.Box7030
Charlotte NC 28241
Volatile Organic Compounds by GC/MS method 8260B
Method Blank
OC Batch
Result RL Control Limit Units ID
Benzene ND 0.003 0.0015 mg/kg 024193
Ethylbenzene ND 0.005 0.0025 mg/kg 024193
mp-Xylenes ND 0.01 0.005 mg/kg Q24193
o-Xylene ND 0.005 0.0025 mg/kg 024193
Toluene ND 0.005 0.0025 mg/kg Q24193
Laboratory Control Sample Recovery Recovery QC Batch
Result Spike Amount Units ID
Benzene 0.0473 0.05 mg/kg 95 62-119 024193
Ethylbenzene 0.04943 0.05 mg/kg 99 57-128 Q24193
mp-Xylenes 0.10007 0.1 mg/kg 100 54-132 Q24193
o-Xylene 0.05009 0.05 mg/kg 100 57-131 Q24193
Toluene 0.04481 0.05 mg/kg 90 57-122 Q24193
Matrix Spike Recovery Recovry
Sample ID Result Spike Amount Units ID
183910 Benzene 0.04076 0.05 mg/kg 82 46-136 024193
Ethylbenzene 0.03384 0.05 mg/kg 68 51-135 Q24193
mp-Xylenes 0.07635 0.1 mgkg 76 51-136 024193
o-Xylene 0.04017 0.05 mg/kg 80 49-1 37 024193
Toluene 0.03654 0.05 mg/kg 73 47-136 Q24193
Matrix Spike Duplicate Recovery Recovery RPD Range BatchSampleIDResultSpikeAmountUnitsID
183910 Benzene 0.03704 0.05 mg/kg 74 46-136 10 0-22 024193
Ethylbenzene 0.02507 0.05 mg/kg 50 51-1 35 30 -23 024193
mp-Xylenes 0.05752 0.1 mg/kg 58 51-136 28 20 024193
o-Xylene 0.031 77 0.05 mg/kg 64 49-1 37 23 0-22 Q24193
Toluene 0.03077 0.05 mg/kg 62 47-136 17 0-22 024193
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of4
RjSM 99012
Level II QC Report
Tcl 11.5 NC Drinking Water Cert No 37735 6/15/07
Full Scrsico Analytical
Enviruninonlal Solutoris
ESP Associates PA Project ID Morehead Commons No COC Group Number G0607193
Attn Chris Ward Date/Time Submitted 6/7/07 1400
P.O Box7030
Charlotte NC 28241
by GC-F1 mahrsrl 3015BS.a5UIu IC flOl ILIC MtI II
Method Blank OC Batch
Result RL Control Limit Units ID
Gasoline Range Organics GRO ND 0.5 mg/kg 024199
Laboratory Control Sample Recovery Recovery
Ranges QC Batch
Result Spike Amount Units Yo ID
Gasoline Range Organics GRO 2.055 mg/kg 103 64-124 024199
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample ID Result Spike Amount Units ID
183776 Gasoline Range Organics GRO 1.385 mg/kg 69 37-1 26 024199
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range QC
Sample ID Result Spike Amount Units
atch
183776 Gasoline Range Organics GRO 1.442 mg/kg 72 37-126 0-34 024199
This report should not be reproduced except in its entirety without the wiitten consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
NC Certification No 402 Level II QC Report
SC Certification No.99012 6/15/07NCDrinkingWaterCertNo37735
Full Sereice Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No Group Number G0607193
Attn Chris
Ward Date/Time Submitted 6/7/07 1400
Box 7030
Charlotte NC 28241
IQLP Leachable Metals by ICP method 6010B
Method Blank QC Batch
Result RL Control Limit Units ID
Arsenic 0.0016 0.05 0.025 mg/L 024208
Barium -0.0012 2.5 mg/L Q24208
Cadmium -0.0016 0.025 0.0125 mg/L 024208
Chromium 0.0035 0.25 0.125 mg/L 024208
Lead 0.0064 0.05 0.025 mg/L 024208
Selenium -0.0005 0.05 0.025 mg/L 024208
Silver 0.0002 0.25 0.125 mg/L 024208
Laboratory Control Sample Recovery Recovery OC Batch
Result Spike
Amount Units Yn ID
Arsenic 0.2555 0.25 mg/L 102 80-120 Q24208
Barium 0.2298 0.25 mg/L 92 80-1 20 024208
Cadmium 0.2408 0.25 mg/L 96 80-1 20 024208
Chromium 0.2262 0.25 mg/L 90 80-1 20 Q24208
Lead 0.2276 0.25 mg/L 91 80-120 024208
Selenium 0.2475 0.25 mg/I 99 80-1 20 024208
Silver 0.2393 0.25 mg/L 96 80-1 20 024208
Matrix Spike Recovery Recovery QC Batch
Sample ID Result Spike
Amount Units 5/
ID
183684 Arsenic 0.2149 0.25 mg/L 90 75-125 024208
Barium 0.8706 0.25 mg/L 72 75-1 25 024208
Cadmium 0.1885 0.25 mg/L 75 75-125 024208
Chromium 0.199 0.25 mgIL 77 75-1 25 Q24208
Lead 0.1996 0.25 mg/L 75 75-1 25 Q24208
Selenium 0.1899 0.25 mgIL 86 75-125 024208
Silver 0.2304 0.25 mg/L 93 75-125 Q24208
Matrix Spike Duplicate Recovery Recovery RPD RRae QC Batch
Sample ID Result Spike
Amount Units ID
183684 Arsenic 0.2148 0.25 mg/L 90 75-125 0-20 024208
Barium 0.8661 0.25 mg/L 71 75-125 0-20 024208
Cadmium 0.1911 0.25 mg/I 76 75-1 25 0-20 024208
Chromium 0.2006 0.25 mg/L 77 75-1 25 -20 Q24208
Lead 0.2001 0.25 mgIL 75 75-1 25 -20 024208
Selenium 0.1891 0.25 mg/L 85 75-125 -20 024208
Silver 0.2321 0.25 mg/L 93 75-1 25 -20 024208
This report should not be reproduced except in its entirety without the
written consent of Prism Laboratories
Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Fall Serice naiytical Environmental SolutIons
ESP Associates PA Project ID
Attn Chris Ward
Box 7030
Charlotte NC 28241
Level II QC Report
6/15/07
Morehead Commons No COG Group Number G0607193
Date/Time Submitted 6/7/07 1400
Irinn keGC.FID nimfhnd i%fl1BijieeirdIIL1 .J.lmm..o w.s ....
Method Blank QC Batch
Result RL Control Limit Units ID
Diesel Range Organics DRO ND 3.5 mg/kg 024213
Laboratory Control Sample eryCBatch
Result Spike
Amount Units 0/
ID
Diesel Range Organics DRO 41.4 40 mg/kg 104 53-1 18 024213
Matrix Spike Recovery Recovry OC Batch
Sample ID Result Spike Amount Units 0/
ID
1831371 Diesel Range Organics DRO 47.0 40 mg/kg 118 52-119 024213
Matrix Spike Duplicate Recovery Recovry RPD QC Batch
Sample ID Result Spike Amount Units ID
183671 Diesel Range Organics DRO 39.9 40 mg/kg 100 52-119 16 -25 024213
TCLP Leachable Nleràury by CVAA method 7470A
Method Blank OC Batch
Result RL Control Limit Units ID
MercUry -0.00007 0.01
0.005 mg/I 024234
Laboratory Control Sample Recovery Recovry OC Batch
Result Spike
Amount Units Yo ID
Mercury 0.00973 0.0093 mg/L 104 80-120 024234
Matrix Spike Recovery Recovery
Ranges
Sample ID Result Spike Amount Units /n ID
183685 Mercury 0.00928 0.0093 mg/I 100 80-120 024234
Matrix Spike Duplicate Recovery Recovery RPID DCRangesRPDRange ac
Sample ID Result Spike Amount Units Ye ID
183685 Mercury 0.00939 0.0093 mg/L 101 80-1 20 -20 Q24234
-See Case Narrative
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 4of4
AccEss
ANALY11CAL 1Nc
ANALYTICAL REPORT
CLIENT
Prism Laboratories Inc
P0 BOX 240543
Charlotte NC 28224
ATTENTION
Angie Overcash
PROJECT ID
Prism Lab-G06071 93
LABORATORY REPORT NUMBER
207060924
DATE
06/14/2007
Primary Data Review By
Curtis Ekker
Data Validation Manager GCAL
Secondary Data Review By
Ashley Amick
Project Manager Access Analytical
[e-mail]
Unless otherwise noted all analysis on this report performed at Gulf Coast Analytical Labs GCAL 7979 GSRIRdBatonRougeLA 70820
GCAL isSCDHEC certified laboratory 73006 NCDENR certified lab 618 GA certified lab LA-01955 NELAP
certified laboratory 01955
Local support services for this project are provided by Access Analytical Inc.Access Analytical is representative ofGCALservingclientsintheSC/NC/GA areas All questions regarding this report should be directed to your local Access
Analytical representative at 803.781.4243 or toll free at 888.315.4243
PLEASE NOTE
CASE NARRATIVE
Client Prism Laboratories Inc Report 207060924
Gulf Coast Analytical Laboratories received and analyzed the samples listed
on the sample cross-reference page of this report Receipt of the samples is documented
by the attached chain of custody This applies only to the samples listed in this report
No sample integrity or quality control exceptions were identified unless noted below
No anomalies were found for the analyzed samples
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by
the
Environmental Protection Agency or other recognized agencies The samples and their corresponding
extracts will be maintained for period of 30 days unless otherwise arranged Following this retention
period the samples will be disposed in accordance with GCALs Standard Operating Procedures
Common Abbreviations Utilized in this Report
ND Indicates the result was Not Detected at the specified RDL
DO Indicates the result was Diluted Out
Ml Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub-Contracted
FLD Indicates the analysis was performed in the Field
PQL Practical Quantitation Limit
MDL Method Detection Limit
RDL Reporting Detection Limit
0000 Reported as time equivalent to 1200 AM
Reporting Flags Utilized in this Report
Indicates an estimated value
Indicates the compound was analyzed for but not detected
ORGANICS Indicates the analyte was detected in the associated Method Blank
INORGANICS Indicates the result is between the RDL and MDL
Sample receipt at GOAL is documented through the attached chain of custody In accordance with ISO
Guide 25 and NELAC this report shall be reproduced only in full and with the written permission of GOAL
The results contained within this report relate only to the samples reported The documented results are
presented within this report
This report pertains only
to the samples listed in the Report Sample Summary and should be retained as
permanent record thereof The results contained within this report are intended for the use of the client
Any unauthorized use of the information contained in this report is prohibited
certify that this data package is in compliance with the terms and conditions of the contract and
Statement of Work both technically and for completeness for other than the conditions in the case
narrative Release of the data contained in this hardcopy data package and in the computer-readabedatasubmittedhasbeenauthorizedbytheQualityAssuranceManagerorhis/her designee as verified bythefollowingsignature
CURTIS EKKER
DATA VALIDATION MANAGER
GCAL REPORT 207060924
THIS REPORT CONTAINS PAGES
Report Sample Summary
GOAL ID Client ID Matrix Collect Date/Time Receive Date/Time
20706092401 183684 Solid 06/07/2007 1300 06/09/2007 0925
20706092402 183685 Solid 06/07/2007 1315 06/09/2007 0925
GCAL Report 207060924
Summary of Compounds Detected
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
20706092401 183684 Solid 06/07/2007 1300 06/09/2007 0925
SW-846 9056 Organic Halides
CAS Parameter
59473-04-0 Total Organic Halides
SW-846 9056 Organic Halides
CAS Parameter
59473-04-0 Total Organic Halides
Result RDL MDL Units
39.IB 46.0 19.9 mg/kg
Result RDL MDL Units
50.8 48.4 20.9 mg/kg
GCAL Report 207060924
CAS Parameter
WET-037 Total Moisture
RESULTS REPORTED ON DRY WEIGHT BASIS
SM 2540G Dry Weight
Prep Date Prep Batch Prep Method Dilution Analyzed By
06/11/2007 1350 JEM
Result RDL
13.0 0.010
Analytical Batch
350931
MDL
0.010
Units
GCAL Report 207060924
SW-846 9056 Organic Halides
Prep Date Prep Batch
06/11/2007 0900 350917
CAS Parameter
59473-04-0 Total Organic Halides
RESULTS REPORTED ON
DRY WEIGHT BASIS
Prep Method
SW-846 5050
Dilution Analyzed By
06/11/2007 1348 AEL
Result RDL
39.IB 46.0
Analytical Batch
350918
MDL
9.9
Units
mg/kg
GCAL Report 207060924
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
20706092402 183685 Solid 06/07/2007 1315 06/09/2007 0925
SM 2540G Dry Weight
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
06/11/2007 1350 JEM 350931
CAS Parameter Result RDL MDL Units
WET-037 Total Moisture 17.4 0.010 0.010
RESULTS REPORTED
ON DRY WEIGHT BASIS
GCAL Report 207060924
SW-846 9056 Organic Halides
Prep Date Prep Batch
06111/2007 0900 350917
CAS Parameter
59473-04.0 Total Organic Halides
Dilution Analyzed By
06/11/2007 1406 AEL
Result RDL
50.8 48.4
RESULTS REPORTED ON DRY WEIGHT BASIS
Prep Method
SW-846 5050
Analytical Batch
350918
MDL
20.9
Units
mglkg
GCAL Report 207060924
General Chemistry Quality Control Summary
Analytical Batch 350931 Client ID
Prep Batch N/A GCAL ID
Sample Type
Analytical Date
Matrix
CONTAMINATED SOIL
20706086501
SAMPLE
06/11/2007 1350
Solid
495491 DUP
495912
DUP
06/11/2007 1350
Solid
SM 2540G Dry Weight Units
Result RDL
RPDResultRPDLimit
WET-037 Total Moisture 169 0.010 20.8 20.7 25
GCAL Report 207060924
General Chemistry Quality Control Summary
Analytical Batch 350918 Client ID MB350917
495875PrepBatch350917GCALID495874
LCSPrepMethod SW-846 5050 Sample Type
Method Blank
06/11/2007 0900PrepDate06/11/2007 0900
06/11/2007 1220AnalyticalDate06/11/2007 1203
SolidMatrixSolid
Control
SW-846 9056 Organic Halides Units mg/kg Spike
Result Rded Result %R
1990 99.6
Limits%R_J
80 120
59473-04-0 Total Organic Halides 17.3U 17.3 2000
nalytical Batch 350918 Client ID 183690 495692DUP
495876PrepBatch350917OCALID20706092301
Prep Method SW-846
5050 Sample Type
SAMPLE
06/11/2007 0900PrepDate06/11/2007 0900
06/11/2007 1255AnalyticalDate06/11/2007 1238
SolidMatrix Solid RPD
SW-846 9056 Organic Halides Units
Result
mg/kg
RDL
113 4.5
Result RPD Limit
59473-04-0 Total Organic Halides 108 17.3
Analytical Batch 351004 Client ID MB351003 LCS351 003
496191PrepBatch351003GCALID496190LCSPrepMethod SW-846 Sample Type Method Blank
06/11/2007 1100
5050
Prep Date 06/11/2007 1100
06/11/2007 1516AnalyticalDate06/11/2007 1458
SolidMatrix Solid
Control
SW-846 9056 Inorganic Anions Units mg/kg
Result
Spike
R.kIded
Result Limits
16887-00-6 Chloride 2.SOU
16984-48-8 Fluoride 2.40U 2.40
24959-67-9 Bromide 5.40U 5.40
WET-036 Total Halides
17U 17
500
500
1000
2000
474
501
1020
1990
94.8
100
102
99.6
80
80
80
80
120
120
120
120
GCAL Report 207060924
General Chemistry Quality Control Summary
.nalytical Batch 351004
Prep Batch 351003
Prep Method SW-846 5050
Client ID
GCAL ID
Sample Type
Prep Date
Analytical Date
Matrix
183690
20706092301
SAMPLE
06/11/2007 1100
06/11/2007 1533
Solid
496193
MS
06/11/20071100
06/11/2007 1608
Solid
Control
SW-846 9056 Inorganic Anions Units mg/kg
Result
Spike
Rtlded Result
99.8
Limits
75 12516887-00-6 Chloride
16984-48-8 Fluoride
24959-67-9 Bromide
WET-036 Total Halides
43.0 2.50
74.0 2.40
0.000 5.40
117 17
500
500
1000
2000
574
1020
2140
100
102
101
75 125
75 125
75 125
Analytical Batch 351004
Prep Batch 351003
Prep Method SW-846 5050
Client ID
GCALID
Sample Type
Prep Date
Analytical Date
Matrix
183690
20706092301
SAMPLE
06/11/2007 1100
06/11/2007 1533
Solid
496192
DUP
06/11/2007 1100
06/11/2007 1551
Solid
SW-846 9056 Inorganic Anions Result RPD
2516887-00-6 Chloride
16984-48-8 Fluoride
24959-67-9 Bromide
WET-036 Total Halides
43.0 2.50
74.0 2.40
0.000 5.40
117 17
44.0
74.0
0.000
118
2.3
0.85
25
25
25
GCAL Report 207060924
FL j44
4t 6Tk-
hone _______________Fax Yes No
maiI Yes No Email Address______________________
DD Type PDF Excel ._OJier
ite Location Name fitsJto1
ite Location Physical Address .fri
CHAIN OF CUSTODY RECORD
PAGE _L OF .L QU TE TO ENSU
PER BILLING
11
Project Name
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reportipg QC LEVEL 111111 IV
provisions and/or QC Re mpnts1
Invoice To PI1.1 A/
Address /f1l.-3 a--i
PRISM
LABORATORIES INC
Full Service Analytical Environmental Solutions
449 Springbrook Road P.O
Box 240543 Charlotte NC 28224-0543
Phone [phone] Fax [phone]
lient Company Name fri
eport To/Contact Name
eporting Address A/
Purchase Order NoiBilling Reference /P g2i.OO
Requested Due Date LI Day LI Days LI Days Days
Days
Working Days 6-9 Days LI Standard 10 days us Work Pust Be
Samples received after 1500 will be processed next business day
Turnaround time is based on
business days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIENT _________________
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE__FL____NC
SC_OTHER _____NIA _____
Water Chlorinated YES._NO_
Sample Iced Upon Collection YES ..L NO _________
CLIENT
SAMPLE DESCRIPTION
ja-/a-2
DATE
COLLECTED
6-7-O7
TIME MATRIX
COLLECTED SOIL
MILITARY WATER OR
HOURS SLUDGE
JbO/3
/1o
/3/5iO
J_ii
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSES REQUESTED
AcA\15e\h REMARKS
p$aiQj__j_T
-__
PRISM
ID NO
13L
TYPE
SEE BELOW
.2TL
-.__
NO SIZE
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must be
submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been initialized
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SEE REVERSE FORTERMSCONDITIONS
007
JUL 31 27 Case Narrative
PRISM
LABORATORIESINC
Date 07/26/07 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COC Group No G0707487
Contact Chris Ward Collection Dates 07/18/07
Address Box 7030 Lab Submittal Dates 07/18/07
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and Quality
Control Data totaling 13 pages chain-of-custody is also attached
for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
Analysis Note for 025204 MSD 24-Trichlorobenzene RPD value outside the control limits
Analysis Note for 025204 MSD 4-Dichlorobenzene RPD value outside the control limits
Analysis Note for 025204 MSD 2-Chlorophenol RPD value outside the
control limits
Analysis Note for 025204 MSD N-Nitrosodi-n-propylamine RPD value outside the control limits
Analysis Note for 025204 MSD Phenol RPD value outside the
control limits
Analysis Note for 025204 MSD Pyrene RPD value outside the
control limits
Volatile Analysis
No Anomalies Reported
Metals Analysis
N/A
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analycal report
Date Reviewed by Paula Gilleland Project Manager Angela Overcash
Signature cccL ..A Signature iDôt4 DVJ2tC0I
Review Date 07/26/07 Approval Date 07/26/07
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentraon calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
El Estimated concentration with high bias
Estimated concentraon with low bias
matx effect is present
Notes This report should not be reproduced except
in its entirety without the writtten consent of Prism Laboratories Inc The results in this
report relate only to the samples submitted for analysis
449 Spiingbrook Road P.O Box 240543 chadotte NC 28224-0403
Phone [phone] Toll Free 800/529-6364 Fax [phone]
Laboratory Report
07/26/07
Project ID Morehead Commons No Client Sample ID Comp of lal-3 and
b2-4
187383
G0707487
07/18107 1100
07/18/07 1635
Prism Sample ID
COC Group
Time Collected
Time Submitted
3-Dichlorobenzene
4-Dichlorobenzene
245-Trichlorophenol
36 8270C
27 8270C
26 8270C
33 8270C
38 8270C
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07125/07 1815 kcanipigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
025204
Q25204
Q25204
025204
025204
NC Certification No 402FRISMSCCertificationNo99012
NC Drinking Water Cert No 37735
all Service Analytical
Environmental Solutions
ESP Associates PA
\ttn Chris Ward
P.O Box7030
charlotte NC 28241
Sample Matrix Soil
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Viethylene chloride BRI pg/kg 11 0.44 826GB 07/21/07 243 erussell Q25185
n-Butylbenzene BRL pg/kg 16 0.43 8260B 07/21/07 243 erussell 025185
i-Propylbenzene BRL pg/kg 11 0.32 826GB 07/21/07 243 erusssH 025185
iaphthaIene BRL pg/kg 5.4 0.63 8260B 0721/07 243 erussell Q25185
1-Xylene BRL pg/kg 5.4 0.32 826GB 07/21/07 243 erussell Q25185
p-lsopropyltoluene BRL pg/kg 16 0.44 826GB 07/21/07 243 erussell Q25185
sec-Butylbenzene BRL pg/kg 16 0.36 826GB 07/21/07 243 erussell Q25185
3tyrene BRL pg/kg 5.4 0.54 826GB 07/21/07 243 erussell 025185
tert-Butylbenzene BRL pg/kg 22 0.34 826GB 07/21/07 243 erussell 025185
Ietrachloroethene BRL pg/kg 11 0.93 826GB 07/21/07 243 erussell 025185
Toluene BRI pg/kg 5.4 0.37
8260B 07/21/07 243 erussell 025185
rans-1 2-Dichloroethene BRL pg/kg 5.4 0.41
826GB 07/21/07 243 erussell 025185
trans-I 3..Dichloropropene BRL pg/kg 5.4 0.38
8260B 07/21/07 243 erussell 025185
Trichloroethene BRI pg/kg 5.4 0.32
826GB 07/21/07 243 erusseH 025185
frichlorofluoromethane BRL pg/kg 5.4 0.44
826GB 07/21/07 243 erussell 025185
Vinyl chloride BRL pg/kg 11 0.69 8260B 07/21/07 243 erussell Q25185
Surrogate
Toluene-d8
Recovery Control Limits
102 81-128
Semi-volatile Organic Compounds by GC/MS
24-Trichlorobenzene BRL
2-Dichlorobenzene BRL
BRL
BRL
BRL
Dibromofluoromethane 110 67-143
Bromofluorobenzene 113 77 128
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
370
370
370
370
370
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
ill Sorvice Anslytical
Environmental Solutions
ESP Associates PA
%ttn Chris Ward
i-Box 7030
harlotte NC 28241
Laboratory Report
07/26/07
Prism Sample ID
COG Group
Time Collected
Time Submitted
46-Trichlorophenol
24-Dichlorophenol
4-Dimethylphenol
24-Dinitrophenol
4-Dinitrotoluene
6-Dinitrotouene
2-Chloronaphthalene
-Chlorophenol
2-Methylnaphthalene
-Methyiphenol
2-Nitrophenol
4-Methylphenol
3-DichIorobenzidine
6-Dinitro-2-methylphenol
-Bromophenyiphenylether
4-Chloro-3-methylphenol
-Chiorophenyiphenylether
4-Nitrophenol
cenaphthene
Acenaphthylene
nthracene
3enzoaanthracene
enzoapyrene
enzobfluoranthene
Renzoghiperylene
enzokfluoranthene
Bis2-chloroethoxymethane
35 8270C
31 8270C
35 8270C
41 8270C
21 8270C
39 8270C
38 8270C
29 8270C
29 8270C
34 8270C
44 8270C
38 8270C
23 8270C
22 8270C
35 8270C
27 8270C
23 8270C
24 8270C
36 8270C
36 8270C
28 8270C
51 8270C
42 8270C
16 8270C
17 8270C
30 8270C
42 8270C
Analysis
Date/Time
07/25/07 1815 kcampigottO
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 keampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 keampigotto
07/25/07 1815 kcampigotto
07125/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
07/25/07 1815 kcampigotto
025204
025204
Q25204
025204
Q25204
025204
025204
Q25204
025204
025204
025204
025204
Q25204
025204
Q25204
025204
025204
Q25204
025204
025204
025204
025204
025204
025204
025204
025204
025204
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Sample Matrix Soil
Project ID Morehead Commons No Client Sample ID Comp of 1a1-3 and
b2-4
187383
G0707487
07/18/07 1600
07/18/07 1635
.arameter Result Units Report MDL Dilution Method Analyst Batch
Limit Factor ID
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRI pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRL pg/kg 370
BRI pg/kg 370
BRL pg/kg 370
BRI pg/kg 370
220 pg/kg 370
630 pg/kg 370
380 pg/kg 370
910 pg/kg 370
BRL pg/kg 370
510 pg/kg 370
BRL pg/kg 370
Page of
-oil Service Analytical Environmentfll Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
07/26/07
Prism Sample ID
COC Group
Time Collected
Time Submitted
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Sample Matrix Soil
Project ID Morehead Commons No Client Sample ID Comp of lal-3 and
b2-4
187383
G0707487
07/18/07 1600
07/18/07 1635
Parameter Result Units Report MDL Dilution Method Batch
Limit Factor ID
AnalystAnalysis
Date/Time
Bis2-chloroethylether BRL pg/kg 370 40
8270C 07/25/07 1815 kcampigotto 025204
Bis2-chloroisopropylether BRL pg/kg 370 31 8270C 07/25/07 1815 kcampigotto Q25204
Bis2-ethylhexylphthalate BRL pg/kg 370 18 8270C 07/25/07 1815 kcampigotto Q25204
ButyIbenzylphthalate BRL pg/kg 370 22
8270C 07/25/07 1815 kcampigotto 025204
Chrysene 640 pg/kg 370 61 8270C 07/25/07 1815 kcampigotto 025204
Di-n-butylphthalate BRL pg/kg 370 17
8270C 07/25/07 1815 kcampigotto 025204
Di-n-octylphthalate BRL pg/kg 370 27
8270C 07/25/07 1815 kcampigotto 025204
Dibenzoahanthracene BRL pg/kg 370 37
8270C 07/25/07 1815 kcampigotto 025204
Dibenzofuran BRL pg/kg 370 31 8270C 07/25/07 1815 kcampigotto Q25204
Diethylphthalate BRL pg/kg 370 23
8270C 07/25/07 1815 kcarnpigotto 025204
Dimethylphthalate BRL pg/kg 370 25
8270C 07/25/07 1815 kcampigotto Q25204
Fluoranthene 2300 pg/kg 370 25
8270C 07/25/07 1815 kcampigotto 025204
FtLJorene BRL pg/kg 370 22
8270C 07125/07 1815 kcampigotto 025204
Hexachlorobenzene BRL pg/kg 370 19 8270C 07/25/07 1815 kcampigotto 025204
HexachIorobutadiene BRL pglkg 370 36 8270C 07/25/07 1815 kcampigotto 025204
Hexachiorocyclopentadiene BRL pg/kg 370 39 8270C 07/25/07 1815 kcampigotto 025204
Hexachloroethane BRL pg/kg 370 37 8270C 07/25/07 1815 kcampigotto 025204
lndeno1 23-cdpyrene
BRL pg/kg 370 38 8270C 07/25/07 1815 kcampigotto 025204
Isophorone BRL pg/kg 370 33
8270C 07/25/07 1815 kcampigotto Q25204
N-Nitrosodi-n-propylamine BRL pg/kg 370 42
8270C 07/25/07 1815 kcampigotto 025204
N-Nitrosodiphenylamine BRL pg/kg 370 19
8270C 07/25/07 1815 kcampigotto 025204
Naphthalene BRL pg/kg 370 40 8270C 07/25/07 1815 kcampigotto Q25204
HNlitrobenzene BRI pg/kg 370 36
8270C 07/25/07 1815 kcampigotto 025204
PenthchIorophenoI BRL pg/kg 370 31 8270C 07/25/07 1815 kcampigotto Q25204
Phenanthrene 1200 pg/kg 370 18 8270C 07/25/07 1815 kcampigotto Q25204
Phenol BRL pg/kg 370 40 8270C 07/25/07 1815 kcampigotto 025204
Pyrene 2100 pg/kg 370 25
8270C 07/25/07 1815 kcampigotto Q25204
Page of
99012 Laboratory Report
NC Drinking Water Cert No 37735 07/26/07
Il Service Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No Client Sample ID Comp of lal-3 and
ttn Chris Ward b2-4
Box 7030 Sample Matrix Soil Prism Sample ID 187383
charlotte NC 28241
COC Group G0707487
Time Collected 07/18/07 1600
Time Submitted 07/18/07 1635
1arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 29.79 mL 355GB 07/23/07 800 dpope P18956
Surrogate Recovery Control Limits
Terphenyl-d14 96 41 136
Phenol-d5 68 13-95
Nitrobenzene-d5 75 14 103
2-Fluorophenol 63 14 89
2-Fluorobiphenyl 72 21 108
246-Tribromophenol 103 25 123
Sample Comments
3RL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
IVELAC certification except for those instances indicated in the case narrative and/or test comments
ll results are reported on dry-weight basis
ngela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the wiitten consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
NC Certification No 402 Level II QC Report
SC Certification No 99012
NC Drinking Water Cert No 37735 7/26/07
Full Service Analytical
Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COC Group Number 00707487
Attn Chris Ward Date/Time Submitted 7/18/07 1635
Box 7030
Charlotte NC 28241
s1..i..rs....rn.4m ts I/M mshnd R9RORvuauicJIL4aIuIs....
Method Blank OC Batch
Result RL Control Umit Units ID
111-Trichloroethane ND 0.005 0.0025 mg/kg 025185
1122-Tetrachloroethane ND 0.005 0.0025 mg/kg 025185
11 2-Trichloroethane ND 0.005 0.0025 mg/kg 025185
11-Dichioroethane ND 0.005 0.0025 mg/kg Q25185
11-Dichloroethene ND 0.005 0.0025 mg/kg 025185
11 -Dichloropropene ND 0.005 0.0025 mg/kg 025185
23-Trichlorobenzene ND 0.005 0.0025 mg/kg Q251 85
23-Trichloropropane ND 0.005 0.0025 mg/kg 025185
24-Trichlorobenzene ND 0.005 0.0025 mg/kg 025185
24-Trimethylbenzene ND 0.005 0.0025 mg/kg 025185
12-Dibromoethane EDB ND 0.005 0.0025 mg/kg 025185
2-Dichlorobenzene ND 0.005 0.0025 mg/kg 025185
2-Dichloroethane ND 0.005 0.0025 mg/kg 025185
2-Dichloropropane ND 0.005 0.0025 mg/kg 025185
35-Trimethylbenzene ND 0.005 0.0025 mg/kg 025185
3-Dichlorobenzene ND 0.005 0.0025 mg/kg 025185
3-Dichloropropane ND 0.005 0.0025 mg/kg 025185
4-Dichlorobenzene ND 0.005 0.0025 mg/kg 025185
22-Dichloropropane ND 0.005 0.0025 mg/kg 025185
2-Chlorotoluene ND 0.005 0.0025 mg/kg Q25185
2-Hexanone ND 0.05 0.025 mg/kg 025185
4-Chlorotoluene ND 0.005 0.0025 mg/kg 025185
4-Methyl-2-pentanone MIBK ND 0.05 0.025 mg/kg 025185
Acetone ND 0.05 0.025 mg/kg Q25185
Benzene ND 0.003 0.0015 mg/kg 025185
Bromobenzene ND 0.005 0.0025 mg/kg 025185
Bromochloromethane ND 0.005 0.0025 mg/kg 025185
Bromodichioromethane ND 0.005 0.0025 mg/kg 025185
Bromoform ND 0.005 0.0025 mg/kg 025185
Bromomethane ND 0.01 0.005 mg/kg Q25185
Carbon tetrachioride ND 0.005 0.0025 mg/kg 025185
Chlorobenzene ND 0.005 0.0025 mg/kg Q25185
Chlorodibromomethane ND 0.005 0.0025 mg/kg 025185
Chioroethane ND 0.01 0.005 mg/kg 025185
This report should not
be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page of
NC Certification No 402 Level II QC Report4IRiiSj\A1j SC Certification No 99012
NC Drinking Water Cert No 37735 7/26/07
Full Service Analytical
Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COG Group Number 00707487
Attn Chris Ward Date/Time Submitted 7/18/07 1635
Box 7030
Charlotte NC 28241
Method Blank QC Batch
Result RL Control Limit Units ID
Chloroform ND 0.005 0.0025 mg/kg 025185
Chloromethane ND 0.005 0.0025 mg/kg 025185
cis-1 2-Dichloroethene ND 0.005 0.0025 mg/kg Q251 85
cis-1 3-Dichloropropene ND 0.005 0.0025 mg/kg Q25185
Dichlorodifluoromethane ND 0.005 0.0025 mg/kg 025185
Ethylbenzene ND 0.005 0.0025 mg/kg 025185
Isopropyl ether IPE ND 0.005 0.0025 mg/kg Q25185
Isopropylbenzene ND 0.005 0.0025 mg/kg 025185
mp-Xylenes ND 0.01 0.005 mg/kg 025185
Methyl ethyl ketone MEK ND 0.1 0.05 mg/kg 025185
Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg 025185
Methyleno chloride ND 0.005 0.0025 mg/kg 025185
n-Butylbenzene ND 0.005 0.0025 mg/kg Q25185
n-Propylbenzene ND 0.005 0.0025 mg/kg Q25185
Naphthalene ND 0.01 0.005 mg/kg 025185
o-Xylene ND 0.005 0.0025 mg/kg Q25185
p-Isopropyltoluene ND 0.005 0.0025 mg/kg 025185
sec-Butylbenzene ND 0.005 0.0025 mg/kg Q25185
Styrene ND 0.005 0.0025 mg/kg 025185
tert-Butylbenzene ND 0.005 0.0025 mg/kg 025185
Tetrachioroethene ND 0.005 0.0025 mg/kg 025185
Toluene ND 0.005 0.0025 mg/kg 025185
trans-I 2-Dichloroethene ND 0.005 0.0025 mg/kg 025185
trans-I 3-Dichloropropene ND 0.005 0.0025 mg/kg 025185
Trichloroethene ND 0.005 0.0025 mg/kg 025185
Trichiorofluoromethane ND 0.005 0.0025 mg/kg 025185
Vinyl acetate ND 0.025 0.0125 mg/kg 025185
Vinyl chloride ND 0.005 0.0025 mg/kg 025185
Laboratory Control Sample Recovery Recovry OC Batch
Result Spike Amount Units
11-Dichloroethene 0.05615 0.05 mg/kg 112 57-122 025185
Benzene 0.0506 0.05 mg/kg 101 62-119 025185
Chlorobenzene 0.05235 0.05 mg/kg 105 61-124 025185
Toluene 0.05132 0.05 mg/kg 103 57-122 025185
Tiichloroethene 0.05338 0.05 mg/kg 107 59-129 025185
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprinybrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page of
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris
Ward
Box 7030
Charlotte NC 28241
Level II QC Report
7/26/07
Project ID Morehead Commons No COC Group Number G0707487
Date/Time Submitted 7/18/07 1635
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample ID Result Spike
Amount Units ID
187298 11-Dichloroethene 0.05573 0.05 mg/kg 111
44.140 025185
Benzene 0.05019 905 mg/kg 100 46-136 Q25185
Chlorobenzene 005013 0.05 mg/kg 100 47-135 025185
Toluene 0.0514 0.05 mg/kg 103 47-136 Q25185
Trichloroethene 0.05146 0.05 mg/kg 103
45-141 025185
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range DC Batch
Sample ID
Result Spike Amount Units ID
187298 11-Dichloroethene 0.05476 0.05 mg/kg 110
44-140 0-23 025185
Benzene 0.05001 0.05 mg/kg 100 46-136 0-22 025185
Chlorobenzene 0.05017 0.05 mg/kg 100 47-1 35 0-22 025185
Toluene 0.05054 0.05 mg/kg 101 47-1 36 0-22 Q25185
Trichloroethene 0.051 02 0.05 mg/kg 102 45-141 0-23 025185
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
Full ..ervlce Analytical
Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
7/26/07
Project ID Morehead Commons No COC Group Number G0707487
Date/Time Submitted 7/18/07 1635
Semi-volatile -...-l nhn.l 8270CJigalin....juuiinun..a lay
Method Blank OC Batch
Result RL Control Limit Units ID
24-Trichlorobenzene ND 0.33 0.165 mg/kg Q25204
2-Dichlorobenzene ND 0.33 0.165 mg/kg 025204
13-Dichlorobenzene ND 0.33 0.165 mg/kg 025204
4-Dichlorobenzene ND 0.33 0.165 mg/kg Q25204
245-Trichlorophenol ND 0.33 0.165 mg/kg 025204
246-Trichlorophenol ND 0.33 0.165 mg/kg 025204
24-Dichlorophenol ND 0.33 0.165 mg/kg 025204
24-Dimethylphenol ND 0.33 0.165 mg/kg Q25204
24-Dinitrophenol ND 1.65 0.825 mg/kg 025204
24-Dinitrotoluene ND 0.33 0.165 mg/kg Q25204
26-Dinitrotoluene ND 0.33 0.165 mg/kg 025204
2-Chloronaphthalene ND 0.33 0.165 mg/kg Q25204
2-Chlorophenol ND 0.33 0.165 mg/kg 025204
2-Methylnaphthalene ND 0.33 0.165 mg/kg 025204
2-Methyiphenol ND 0.33 0.165 mg/kg 025204
2-Nitrophenol ND 0.33 0.165 mg/kg 025204
34-Methylphenol ND 0.33 0.165 mg/kg Q25204
33-Dichlorobenzidine ND 0.66 0.33 mg/kg 025204
46-Dinitro-2-methylphenol ND 1.65 0.825 mg/kg 025204
4-Bromophenylphenylether ND 0.33 0.165 mg/kg Q25204
4-Chloro-3-methyphenol ND 0.66 0.33 mg/kg 025204
4-Chioroaniline ND 0.33 0.165 mg/kg Q25204
4-Chlorophenylphenylether ND 0.33 0.165 mg/kg 025204
4-Nitrophenol ND 1.65 0.825 mg/kg Q25204
Acenaphthene ND 0.33 0.165 mg/kg 025204
Acenaphthylene ND 0.33 0.165 mg/kg 025204
Anthracene ND 0.33 0.165 mg/kg 025204
Azobenzene ND 1.65 0.825 mg/kg 025204
Benzoaanthracene ND 0.33 0.165 mg/kg 025204
Benzoapyrene ND 0.33 0.165 mg/kg 025204
Benzobfluoranthene ND 0.33 0.165 mg/kg 025204
Benzoghiperylene ND 0.33 0.165 mg/kg 025204
Benzokfluoranthene ND 0.33 0.165 mg/kg 025204
Benzoic acid ND 1.65 0.825 mg/kg 025204
Page of
INO
Fu5 Service Analytical Cnvironmental Solutions
ESP Associates PA
Attn Chris
Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
7/26/07
Method Blank
Project ID Morehead Commons No COC Group Number G0707487
Date/Time Submitted 7/18/07 1635
Result RL Control Limit Units
CC Batch
ID
Benzyl alcohol ND 0.66 0.33 mg/kg 025204
Bis2-chloroethoxymethane ND 0.33 0.165 mg/kg 025204
Bis2-chloroethylether ND 0.33 0.165 mg/kg 025204
BIs2-chloroisopropylether ND 0.33 0.165 mg/kg 025204
Bis2-othylhexylphthalate ND 0.33 0.165 mg/kg 025204
Butylbenzylphthalate ND 0.33 0.165 mg/kg 025204
Chrysene ND 0.33 0.165 mg/kg 025204
Di-n-butylphthalate ND 0.33 0.165 mg/kg 025204
Di-n-octylphthalate ND 0.33 0.165 mg/kg Q25204
Dibenzoahanthracene ND 0.33 0.165 mg/kg 025204
Dibenzofuran ND 0.33 0.165 mg/kg 025204
Diethylphthalate ND 0.33 0.165 mg/kg 025204
Dimethylphthalate ND 0.33 0.165 mg/kg 025204
Fluoranthene ND 0.33 0.165 mg/kg 025204
Fluorene ND 0.33 0.165 mg/kg 025204
Hexachlorobenzene ND 0.33 0.165 mg/kg Q25204
Hexachiorobutadiene ND 0.33 0.165 mg/kg 025204
Hexachlorocyclopentadiene ND 0.33 0.165 mg/kg 025204
Hexachloroethane ND 0.33 0.165 mg/kg 025204
lndeno123-cdpyrene ND 0.33 0.165 mg/kg 025204
Isophorone ND 0.33 0.165 mg/kg 025204
N-Nitrosodi-n-propylamine ND 0.33 0.165 mg/kg Q25204
N-Nitrosodiphenylamine ND 0.33 0.165 mg/kg 025204
Naphthalene ND 0.33 0.165 mg/kg 025204
Nitrobenzene ND 0.33 0.165 mg/kg 025204
Pentachlorophenol ND 1.65 0.825 mg/kg 025204
Phenanthrene ND 0.33 0.165 mg/kg 025204
Phenol ND 0.33 0.165 mg/kg 025204
ND 0.33 0.165 mg/kg 025204Pyrene
Laboratory Control Sample Recovery Recovery
Result Spike Amount Units
Ranges CC Batch
ID
24-Trichlorobenzene 1.21800 1.6929 mg/kg 72 39-98 025204
14-Dichlorobenzene 1.19566 1.6929 mg/kg 71 37-95 025204
24-Dinitrotoluene 1.49255 1.6929 mg/kg 88 56-128 025204
2-Chlorophenol 1.29891 1.6929 mg/kg 77 37-98 025204
4-Chloro-3-methylphenol 1.37000 1.6929 mg/kg 81 45-111 025204
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
NC Certification No 402 Level II QC Renort
SC Certification No 99012
NC Drinking Water Cert No 37735 7/26/07
Full Service AnaIytict
Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COC Group Number G0707487
Attn Chris
Ward Date/Time Submitted 7/18/07 1635
Box 7030
Charlotte NC 28241
Recovery DC BatchLaboratoryControlSampleRecoveryRangesIDResultSpikeAmountUnits0/
4-Nitrophenol 1.64014 1.6929 mg/kg 97 20-157 025204
Acenaphthene 1.32159 1.6929 mg/kg 78 44-110 Q25204
N-Nitrosodi-n-propylamine 1.28672 1.6929 mg/kg 76 38-101 025204
Pentachlorophenol 1.65132 1.6929 mg/kg 98 53-127 Q25204
Phenol 1.41299 1.6929 mg/kg 83 34-102 025204
Pyrene 1.81482 1.6929 mg/kg 107 54-131 025204
Recovery DC BatchMatrixSpikeRecoveryRangesIDResult Spike
Amount UnitsSampleID
187298 24-Trichlorobenzene 1.27366 1.667 mg/kg 76 26-97 025204
4-Dichlorobenzene 1.22066 1.667 mg/kg 73 23-92 Q25204
24-Dinitrotoluene 1.53066 1.667 mg/kg 92 45-1 27 Q25204
2-Chlorophenol 1.383 1.667 mg/kg 83 25-94 025204
4-Chloro-3-methylphenol 1.42233 1.667 mg/kg 85 31-113 Q25204
4-Nitrophenol 1.633 1.667 mg/kg 98 17-150 025204
Acenaphthene 1.299 1.667 mg/kg 78 36-107 025204
N-Nitrosodi-n-propytamine 1.43266 1.667 mg/kg 86 22-105 025204
Pentachlorophenol 1.61033 1.667 mg/kg 97 39-137 025204
Phenol 1.34866 1.667 mg/kg 81
23-97 025204
Pyrene 2.13833 1.667 mg/kg 128 45-133 025204
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range DC Batch
Sample ID Result Spike Amount Units /0 0/
ID
187298 124-Trichlorobenzene 0.66433 1.667 mg/kg 40 26-97 63 0-37 025204
14-Dichlorobenzene 0.61333 1.667 mg/kg 37 23-92 66 0-36 025204
24-Dinitrotoluene 1.38933 1.667 mg/kg 83 45-127 10 0-29 Q25204
2-Chlorophenol 0.72933 1.667 mg/kg 44 25-94 62 0-37 025204
4-Chloro-3-methylphenol 1.14633 1.667 mg/kg 69 31-113 21 0-32 025204
4-Nitrophenol 1.52533 1.667 mg/kg 92 17-150 0-32 025204
Acenaphthene 1.24933 1.667 mg/kg 75 36-107 0-32 025204
N-Nitrosodi-n-propylamine 0.95666 1.667 mg/kg 57 22-105 40 0-37 025204
Pentachlorophenol 1.50033 1.667 mg/kg 90 39-137 0-27 025204
Phenol 0.71 933 1.667 mg/kg 43 23-97 61 0-42 025204
Pyrene 1.54566 1.667 mg/kg 93 45-133 32 0-27 Q25204
-See Case Narrative
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
Full Service Analytical Environmental Solutions
449 Springbrook Road P.O Box
240543 Charlotte NC 28224-0543
Phone [phone] Fax 7046-49
Client Company Name
Report TofContact Name IyY
Reporting Address
Phone _______________Fax Yes No
Email Yes No Email Address
EDD Type PDF_Excel _er4//7SiteLocationName
Site Location Physical Address r-
CHAIN OF CUSTODY RECORD
PAGE _J_OF QUOTE ENS 7ROPER BILLING
Project Name
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reporting QC LEVEL 111111 IV
irementprovisionsand/or
Invoice To
Address
Purchase Order NoJBiIling Referenc
Requested Due Date Day Days Days
04 Days Days
Rush Work Must Be
Working Days 6-9 Days Standard 10 days Pre-Approved
Samples received after 1500 will be processed next business day
Turnaround time is based on
business days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIENT
SAMPLE CONTAINER
TYPE NO SiZE
SEE BELOW
By .ure__________Method of Sf4megW NOTELL SAMPLE COOLERS SHOULL ut TRANSPORTAI IUN
SAMI5LES ARE NOT ACCEPTED
AND VERIFIED AGAIN UNTIL RECEIVED AT THE LABORATORY
and-delivered
NPDES
EINC
CERCLA LANDFILL OTHER
LJNC USC lUNG OSC lUNG USC
SEE REVERSE FOR
TERMS CONDITIONS
Samples INTACT upon arrival
NO N/A
Received ON WET ICE Temp ii
PROP ER PRESERVATIVES indicated ..L __4
-Received.WITFIIN HOLDING TIMES
CUSTODY SEALS INTACT
VOLATILES recd W/OUT HEADSPACE
PROPER CONTAINERS used
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE____-_
SC__OTHER _N/A
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES NO
TIME
COLLECTED
MILITARY
HOURS
MATRIX
SOILWATER OR
SLUDGE
PRESERVA
TIVES
.YSES
Comments
ORIGINAL
Corporate Office
MailingP0Box 7030
Charlotte North Carolina 28241
Physical
3475 Lakemont Boulevard
Fort Mill SC 29708
803802.2440
Raleigh
14001 Weston Parkway
Suite 100
Cary North Carolina 27513
919.678.1070
Wilmington
2120-B Capital Drive
Wilmington North Carolina 28405
910.313.6648
800.960.7317
Concord
4601 Corporate Drive NW
Suite 165
Concord North Carolina 28027
704 793.9855
ESP Associates PA
www.espassociates.com