8002_CelaneseFibers_INDUS_GWMReportMay_DIN26418_20150507

Prepared for:Prepared by:
CNA Holdings LLC AECOM
Dallas, Texas Atlanta, GA
60313404May 2016
Environment
2015 Annual Report
Needmore Road Landfill Facility
Salisbury, North Carolina
Prepared for:Prepared by:
CNA Holdings LLC AECOM
Dallas, Texas Atlanta, GA
60313404May 2016
Environment
2015 Annual Report
Needmore Road Landfill Facility
Salisbury, North Carolina
_________________________________
Prepared By Jing Zhou
Project Engineer
_________________________________
Reviewed By Bryon Dahlgren, PE
Project Director
AECOM Environment
May 2016
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Contents
1.0 Introduction ............................................................................................................... 1-1
1.1 Site Background..........................................................................................................1-1
2.0 Summary of Monitoring Activities ............................................................................ 2-1
3.0 Summary of May 2015 and November 2015 Monitoring Results ............................. 3-1
3.1 Ethylene Glycol ...........................................................................................................3-1
3.2 1,4-Dioxane ................................................................................................................3-2
3.3 DowTherm A™ ...........................................................................................................3-2
3.4 Surface Water Sampling Results .................................................................................3-3
3.5 Phytoremediation System and Landfill Cover Inspections .............................................3-4
4.0 Conclusions .............................................................................................................. 4-1
List of Tables
Table 1 May Groundwater and Surface Water Sampling Plan
Table 2 November Groundwater and Surface Water Sampling Plan
Table 3 Groundwater Analytical Summary
Table 4 Surface Water Analytical Summary
Table 5 Summary of Detected Constituents in Groundwater
Table 6 Time vs. Concentration Plots – Ethylene Glycol
Table 7 Time vs. Concentration Plots – 1,4-Dioxane
Table 8 Time vs. Concentration Plots – Biphenyl Ether
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List of Figures
Figure 1 Site Location Map
Figure 2 Sample Location Map – May 2015
Figure 3 Sample Location Map – November 2015
Figure 4 Groundwater Elevation Data – November 2015
Figure 5 Ethylene Glycol Map – May 2015
Figure 6 Ethylene Glycol Map – November 2015
Figure 7 1,4-Dioxane Map – May 2015
Figure 8 1,4-Dioxane Map – November 2015
Figure 9 1,1-Biphenyl Map – November 2015
Figure 10 Biphenyl Ether Map – November 2015
List of Appendices
Appendix A May 2015 and November 2015 Laboratory Analytical Reports
Appendix B Completed Inspection Forms for Landfill Cap and Phytoremediation System
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P:\ENV\Data\Clients\CNA Holdings\Projects\60313404_Needmore Road Landfill 2014\500-Deliverables\501 Deliverable 1 Annual Reporting\2015 Annual
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List of Acronyms
CAP Corrective Action Plan
mg/L milligrams per liter
MNA monitored natural attenuation
NCDEQ North Carolina Department of Environment and Natural Resources
NPDES National Pollutant Discharge Elimination System
NRLF Needmore Road Landfill Facility
VFA Volatile Fatty Acid
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1.0 Introduction
This annual report has been prepared to present activities completed between May 2015 and April
2016, including the sampling results for the May 2015 and November 2015 monitoring events for the
Needmore Road Landfill Facility (NRLF). This report includes an updated summary of data and
findings at the site. Additionally, this report presents the status of the monitored natural attenuation
(MNA) and phytoremediation programs established in the Corrective Action Plan (CAP).
1.1 Site Background
The Needmore Road Landfill site, located at 345 Messick Farm Road, Salisbury, Rowan County,
North Carolina, was used until 1990 to dispose of by-products of polyester resin manufacturing from
the Hoechst Celanese plant located on U.S. Route 70 near Salisbury, North Carolina. These by-
products primarily included waste materials containing ethylene glycol with some other impurities,
including 1,4-dioxane, 1,1-biphenyl, and biphenyl ether. There were four main disposal areas at this
site and were referred to as Taylor’s Pit, the 14-Acre Site, the 16-Acre Site, and the Secondary Site.
Taylor’s Pit was consolidated into the main part of the landfill prior to final landfill closure. The site
consists of an approximately 243-acre tract of land that is bounded by the South Yadkin River to the
east. The current North Carolina Department of Environment Quality (NCDEQ) status of the site is
“closed.” A site location map is included as Figure 1.
The landfill lies within the central portion of the Charlotte Metamorphic Belt of the Piedmont
Physiographic Province. Bedrock in this area is composed of a complex series of meta-sedimentary,
meta-volcanic, and igneous intrusive rock types. This geologic matrix has undergone repeated cycles
of folding, faulting, metamorphism, and intrusions, which have resulted in regional northeasterly strike
and southeasterly dip directions.
A basic understanding of the geology at the landfill has been established during several phases of
work, during which numerous monitoring and extraction wells were installed. Based on an evaluation
of the subsurface boring logs, the site is underlain by diorite, gabbro, and granite bedrock. Some
localized gneissic and schistose metamorphism has been noted in several of the borings drilled at the
site. These profiles are generally well weathered, and occur in the zone above competent rock.
Remedial activities that were completed at the landfill prior to 2004 included the installation of an
impermeable cover on the landfill, regrading of the surface of the landfill (to improve surface
drainage), and the installation of groundwater extraction wells. Groundwater was extracted and
treated by a UV/peroxide oxidation process and discharged under a National Pollutant Discharge
Elimination System (NPDES) permit. Groundwater extraction was suspended in June 2002.
Soon after the deactivation of the extraction system, a groundwater seep manifested itself as surface
flow traveling from a sump located at the toe of the landfill. The seep area is located at the northeast
end of the landfill and southwest of the South Yadkin River. The surface flow meandered across the
flat area between the landfill and the South Yadkin River and appeared to re-enter the shallow
groundwater near the river bank. This occurrence also coincided with an end to a period of extreme
drought and a return to normal rainfall patterns. The origin of this seep was believed to be associated
with the presence of a drain system at the toe of landfill. During 2004, modifications were made to the
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drain system, including the installation of 40 feet of solid pipe to replace a section of perforated pipe
and the installation of an anti-seepage concrete collar around the drain pipe.
The installation of the collar appeared to eliminate the original seep; however, several weeks after the
drain system modifications were made, a new, lower volume surface water flow was observed coming
out of a culvert pipe further downgradient. After leaving the culvert pipe, the surface water flow
meandered across the cleared area toward the river and infiltrated into the ground prior to reaching
the river. Based on the shallow groundwater elevations in this area, it was interpreted that this surface
water flow was the partial re-establishment of a natural creek that existed prior to the installation of the
extraction system.
In response to the seep, a phytoremediation plan was initiated in 2004. The phytoremediation system
is positioned downgradient of the landfill face before the seep location.
Groundwater monitoring data in the reports submitted semiannually from November 2004 until the
present have demonstrated that the existing groundwater impact has been generally contained and is
not expanding, and biological activity is present in the source areas. Additionally, the levels of impact
in groundwater are not anticipated to exceed surface water quality standards nor pose an
unacceptable risk to the receptors. Based on these data, the reports concluded that MNA with
phytoremediation is a viable remedy. A final CAP was established in 2007 defining a combination of
MNA and phytoremediation as the site remedy.
Biological degradation has been a significant component of natural attenuation of ethylene glycol and
DowTherm A™ components at the site. The original MNA parameters supplemented with the
additional sampling requested by NCDEQ indicate that biological degradation is occurring at the site
to control the ethylene glycol and DowTherm A™ plume. Phytoremediation is currently being utilized
to supplement the MNA in order to treat the 1,4-dioxane plume through evapotranspiration while also
providing additional hydraulic control.
Groundwater and surface water monitoring, as well as regular inspections of the phytoremediation
system and landfill cap, have been ongoing at the site following the schedule detailed in the CAP and
revised in early 2009.
Because the primary constituents at the site have generally remained stable since 2007, and the MNA
and phytoremediation systems have remained effective as designed, AECOM recommended in the
semiannual report submitted to NCDEQ in May 2014 that the groundwater and surface water
monitoring continue to be conducted semiannually in May and November and the reporting frequency
be reduced from semiannual to annual. The NCDEQ approved the reduction of the reporting
frequency in a letter dated on September 10, 2014. Annual report is prepared since May 2015. This
annual report is the second annual report for this site, including the field activities from May 2015 to
April 2016 and analytical results of the May 2015 and November 2015 sampling events
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2.0 Summary of Monitoring Activities
The ongoing MNA/phytoremediation activities for the NRLF include:
· semiannual groundwater and surface water sampling and analyses;
· continued ongoing maintenance and monthly inspection of the landfill cap; and
· continued ongoing maintenance and monthly inspections of the phytoremediation tree farm.
The May 2015 and November 2015 groundwater and surface water sampling events were conducted
using methodologies detailed in the CAP. A reduced scope plan for all May events was approved in
2009, as shown in Table 1. All November events include the full sampling plan shown in Table 2, as
originally presented in the CAP. Replacement of Volatile Fatty Acids (VFAs) with acetic acid analysis
was approved by NCDEQ in 2010.
Sample location maps for the May 2015 and November 2015 sampling events are included as Figure
2 and Figure 3, respectively. During the November 2015 sampling event, wells B-24A and B-24B
could not be sampled due to the high water level at these two locations. These two wells will be
sampled in May 2016 for all the missing analytical parameters in November 2015, and the sampling
results will be included in the next annual report to be submitted in May 2017. Laboratory analytical
reports for groundwater and surface water sampling are included in Appendix A.
Completed monthly inspection forms for the phytoremediation system for May 2015 through April
2016 are included in Appendix B.
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3.0 Summary of May 2015 and November 2015 Monitoring
Results
Nine groundwater monitoring wells along with two surface water locations were sampled during
the May 2015 monitoring event. Surface water location CSW-2 was not sampled because it was
dry. Twelve groundwater monitoring wells along with six surface water locations were sampled
during the November 2015 monitoring event. Wells B-24A and B-24B were not sampled because
the wells could not be approached due to the high water levels in that area. Laboratory analytical
reports for groundwater and surface water sampling are summarized in Tables 3 and 4,
respectively. Parameters detected in at least one sample are included on Tables 3 and 4.
Complete analytical reports are included as Appendix A of this report. Previous reports identified
that the primary constituents in groundwater are ethylene glycol, 1,4-dioxane, 1,1-biphenyl, and
biphenyl ether. Monitoring updates for these constituents are presented in the following sections.
The May 2015 and November 2015 groundwater elevation data are consistent with the groundwater
flow patterns established in the CAP (October 2007), which indicated that groundwater under the site
flows northeast and northwest toward the South Yadkin River. Groundwater elevations collected
during the November 2015 event, combined with historic site data, were used to develop the
potentiometric surface presented on Figure 4. The potentiometric surface indicates that the
groundwater flow patterns underlying the site flow northeast toward the Yadkin River.
3.1 Ethylene Glycol
During the May 2015 sampling event, ethylene glycol was not detected in any wells sampled
(reporting limit was 5.0 milligrams per liter [mg/L]). Similarly, during the November 2015 sampling
event, ethylene glycol was not detected in any wells sampled. It should be noted that the reporting
limits for the November 2015 sampling event was 50 mg/L and 500 mg/L due to the sample dilution.
Ethylene glycol remained below analytical reporting limits (non-detect) in samples collected from 2007
to November 2012. During the 2013 and 2014 sampling events, ethylene glycol was detected in a
few wells including B-01, B-09C, B-10, B-23A, and B-23B, with concentrations ranging from 200 mg/L
to 800 mg/L, greater than the NC 2L groundwater quality standard of 10 mg/L, but most
concentrations were lower than the historic detections in the same wells.
Ethylene glycol concentrations at the site were significantly reduced at the time of the 2007 CAP and
have remained non-detectable during most of the sampling events after 2007. These results support
the ethylene glycol natural attenuation conclusions presented in the 2007 CAP. The landfill cap has
significantly reduced or eliminated the transport of ethylene glycol concentrations from the landfill into
groundwater, and ethylene glycol concentrations, which had entered the groundwater prior to the
installation of the cap, were degraded or attenuated (CAP, 2007). Since ethylene glycol is fully
miscible in water and mobile, it was predicted in the 2007 CAP and subsequent monitoring reports
that additional detections may possibly be observed in future samples. Considering the fact that
ethylene glycol is easily degraded in the water through natural attenuation and the source has been
isolated, the rebound of the ethylene glycol concentration in 2013 and 2014 were temporary, as
expected. Ethylene glycol will continue to be monitored. Additional temporary increases may be
observed in the future, but the landfill cover combined with MNA remains an effective remedy.
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Historic data summaries for ethylene glycol and other site parameters are presented in Table 5.
Select trend plots of ethylene glycol concentrations over time are presented in Table 6. In addition,
ethylene glycol concentrations are included on Figure 5 for the May 2015 sampling event and Figure 6
for the November 2015 sampling event.
3.2 1,4-Dioxane
1,4-Dioxane has been historically detected in wells near all of the four former disposal sites. The
concentration trend plots presented in Table 7 indicate that 1,4-dioxane concentrations in most wells
are generally either stable or declining; however, the 1,4-dioxane concentrations in samples from
three monitoring wells (B-12, B-23A, and B-23B) increased notably during recent sampling events.
The 1,4-dioxane concentration in B-12 increased from 0.132 mg/L in May 2012 to 3.68 mg/L in
November 2012, then remained around 2.5 to 3.5 mg/L during the sampling events in 2013 through
2015, however these results are within the historical range. The 1,4-dioxane concentrations also
increased in B-23A and B-23B during recent sampling events. The 1,4-dioxane concentrations in B-
23A increased from 2.76 mg/L in November 2013 to 3.54 mg/L in November 2014, decreased slightly
in 2015, but still remain above 3.0 mg/L. The 1,4-dioxane concentration in B-23B increased from 2.88
mg/L in November 2013 to above 3.0 mg/L in 2014, and fluctuated in that range during 2015.
The increases noted in 2012 corresponded to a sharp decline in groundwater elevations of 1.5 to 4
feet across the site. Because site conditions are otherwise unchanged, trends of these miscible
compounds were interpreted as response to plume migration impacted by the change in groundwater
elevation. The groundwater elevations have returned to typical levels and the 1,4-dioxane
concentrations have subsequently remained stable to declining. Continued monitoring is expected to
continue demonstration that the on-going cover and phytoremediation system maintenance activities
maintain overall site conditions and are the appropriate selected site remedy.
Data used to generate the plots in Table 7 can be found in Table 5. Plume maps for 1,4-dioxane are
included as Figure 7 for the May 2015 sampling event and Figure 8 for the November 2015 sampling
event. The small area of impact to the southwest of the main area on Figure 7 and Figure 8 indicates
an isolated location of impact continues to exist near the former Taylor’s Pit area.
These results indicate that the release of 1,4-dioxane from the former disposal sites is being controlled
by the landfill cover, and the residual plume has extended toward the downgradient areas. The short-
term trends shown in Table 7 indicate that this long-term process has declined in rate and the site has
become significantly more stable.
3.3 DowTherm A™
1,1-Biphenyl
1,1-Biphenyl results are presented in Table 3, and the 1,1-biphenyl plume map for November 2015 is
shown on Figure 9.
Since 2003, 1,1-biphenyl has only been detected in samples collected from monitoring well B-10. The
result from B-10 was 0.0828 mg/L in May 2015 and 0.192 mg/L in November 2015, similar to the 2014
sampling results. The NC 2L standard for 1,1-biphenyl is 0.40 mg/L. Historic data for 1,1-biphenyl at
B-10 has typically remained below the 0.40 mg/L level but has occasionally exceeded this level. The
historic maximum was 0.461 mg/L reported in 1999.
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Biphenyl Ether
NCDEQ has not developed a 2L standard for biphenyl ether; therefore, the practical quantitation limit
(PQL) has been used as the screening criteria for the presence of this constituent at the site. Biphenyl
ether has been historically detected at several wells located near the former disposal sites and at the
downgradient wells. The May 2015 and November 2015 biphenyl ether data are presented in Table
3. The highest concentration was detected in the sample collected from monitoring well B-10 (2.11
mg/L in November 2015). Biphenyl ether ranged from approximately 1.1 to 4.5 mg/L in recent years,
and has demonstrated a decreasing trend since December 2009.
Biphenyl ether was also detected in samples from monitoring wells B-01, B-09C, and B-22B, with
concentrations below 0.2 mg/L. Biphenyl ether was not detected in the sample from other monitoring
wells sampled. Selected biphenyl ether trends can be observed in Table 8 and on Figure 10.
The data continue to indicate that migration of 1,1-biphenyl and biphenyl ether is being controlled by
the landfill cap and through natural attenuation mechanisms.
3.4 Surface Water Sampling Results
Surface water monitoring was conducted at two surface water locations (CSW-1 and SW-5) during the
May 2015 sampling event, and at six surface water monitoring locations (SW-3, SW-5, SW-7, SW-8,
CSW-1 and CSW-2) during the November 2015 event. The surface water results are summarized in
Table 4. No samples were collected from CSW-2 during the May 2015 sampling event due to this
location being dry. CSW-2 is a monitoring location associated with the surface water seep. This
location has been dry for the majority of sampling events since the phytoremediation program was
initiated. It is located downstream in the creek bed fed by the seep.
Monitoring events prior to the current phytoremediation system indicated concentrations of 1,4-
dioxane at CSW-1 of approximately 0.5 mg/L and lower concentrations at downgradient CSW-2.
When water is present, the concentrations of 1,4-dioxane have declined to less than 50 percent of the
prior concentrations. Results at CSW-1 have varied between approximately 0.08 and 0.25 mg/L. The
1,4-dioxane concentration in CSW-1 was 0.0821 mg/L in May 2015 and 0.014 mg/L in November
2015. The 1,4-dioxane concentration in CSW-2 was 0.0124 mg/L in November 2015. The data
collected when water is present suggest that the phytoremediation is providing control of the 1,4-
dioxane mass in the treatment area.
The May 2015 result is the lowest result reported to date for locations CSW-1. The November 2015
result was nearly an order of magnitude lower, but the site conditions at the time included significant
flooding from the Pacolet River. Locations CSW-1 and CSW-2 were not submerged, but the
concentrations reported may include atypical levels of dilution resulting from inflow of high water.
Concentrations of 1,4-dioxane, ethylene glycol, biphenyl ether, and 1,1-biphenyl at surface water
monitoring locations SW-3, SW-5, SW-7, and SW-8 were below detection levels. Surface water
location SW-05 has been sampled for 1,4-dioxane analysis since 1998. The results for all samples
prior to 2014 were non-detect (<0.010 mg/L). In May 2014 a detection of 0.326 mg/L was reported for
the sample from this location and a much higher concentration was reported in the duplicate sample.
The concentration decreased to non-detect (<0.002 mg/L) in November 2014 and remained non-
detect in 2015. The May 2014 result is therefore considered to be an error resulting from
contamination during the sampling or analytical process.
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3.5 Phytoremediation System and Landfill Cover Inspections
Monthly inspections of the phytoremediation system and landfill cap were conducted for the period of
May 2015 through April 2016 and are presented in Appendix B. Based on these inspections, most of
the trees remained in good health during this reporting period. The willows planted in 2012 are in
good health. During the March 2016 inspection, six trees were found broken due to wind storm. The
broken trees were removed during this inspection event. No other tree losses were reported during
this reporting period, May 2015 through April 2016.
AECOM will review the phytoremediation system and determine if it is appropriate to replace the six
damaged trees and/or any other trees. This assessment will include possibly harvesting other trees
as needed to maintain the remedial performance and hydraulic control.
The landfill cap has been in good condition during this reporting period.
As previously described, the associated surface water sampling has demonstrated that the treatment
system is effective. Groundwater concentrations of 1,4-dioxane in the vicinity of the treatment system
have also remained stable or declining.
The landfill cover has been in place since the early 1990s. The phytoremediation system was first
implemented in 2004 and has been upgraded and maintained consistently since that time.
Groundwater monitoring has consistently demonstrated that these systems remain effective and
combine with MNA to maintain stable to improving conditions as described in the 2007 CAP.
Because the systems have established a long term reliable behavior, we are requesting that the
monthly inspection schedule be reduced to quarterly. The historic data demonstrate that the
conditions are controlled as designed and not changing rapidly. Therefore, quarterly inspections will
continue to provide adequate notice for any maintenance or repairs which may be needed.
Routine mowing and cover service will continue without change in schedule.
Maintenance of the phytoremediation system will also be continued as long as groundwater detections
exceed the 2L standards as described in the CAP. The maintenance will include periodic removal of
trees based on damage, age, or overcrowding and additional trees will be installed as needed to
continue meeting the objectives of the CAP.
.
AECOM Environment
May 2016
4.0 Conclusions
The CAP was submitted in November 2007, and subsequent semiannual reports submitted have
reported declining or stabilized concentrations and extent for the various plumes within the Needmore
Road Landfill Facility. . Per NCDEQ’s approval in a letter dated September 10, 2014, the reporting
frequency was reduced from semiannual to annual. This report is the second annual report including
the field activities from May 2015 to April 2016 and analytical results of the May 2015 and November
2015 sampling events. Semiannual monitoring and regular inspections of the phytoremediation
system were conducted for the period of May 2015 to April 2016
During the May 2015 and November 2015 sampling events, the concentrations of one of the primary
constituents of concern, ethylene glycol, decreased to a non-detect level. Considering the fact that
ethylene glycol is easily degraded in water through natural attenuation and the source has been
isolated, the rebound of the ethylene glycol concentrations in 2013 and 2014 is considered temporary.
1,1-Biphenyl was only detected at monitoring well B-10, and historical data for this well indicate a
decreasing trend since 2008. Biphenyl ether concentrations in the former disposal areas have
decreased or stabilized over time due to the natural attenuation processes. Additionally, although
monitoring well data indicate detectable levels of 1,4-dioxane exceeding the NC 2L standard, in most
wells, concentrations remain well below historical levels observed at the site with generally mostly
stable to declining trends. There are three wells in which the 1,4-dioxane concentrations increased
notably in 2012 but have remained stable to declining since that event.
Based on surface water monitoring data, no site parameters have been observed that could impact
the South Yadkin River.
The phytoremediation systems generally remain in good condition after the maintenance activities
completed during this reporting period. In addition, the landfill cap continues to be in good condition.
We have requested a reduction in inspection frequency to quarterly because the data have
consistently shown stable and effective performance of the current systems.
A review of the phytoremediation system will be completed to determine if tree replacements are
required as a result of the recent loss of six trees. Future maintenance of the phytoremediation
system, including pruning, harvesting and/or installing of new trees will be continued as described in
the CAP.
Groundwater and surface water monitoring will be continued. The next monitoring event is scheduled
for May 2016. The scope of the May 2016 event will be as presented in Table 1. Additionally, wells B-
24A and B-24 will be sampled and analyzed for the parameters that were missed in the November
2015 sampling event. The next full sampling program presented in the CAP will be completed in
November 2016 as shown in Table 2. The May 2016 data and November 2016 data will be presented
in the next annual report to be submitted in May 2017.
AECOM Environment
May 2016
Tables
Table 1
May Groundwater and Surface Water Sampling Plan
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Location 1,4-Dioxane DowTherm A™Ethylene Glycol MNA*
B-01 X X X
B-09C X X X
B-10 X X X X
B-12 X X X
B-17C X X
B-22B X X
B-23A X X X
B-23B X X X
B-24A X X
SW-5 X X X
CSW-1 X
CSW-2 X
Notes:
* MNA: alkalinity, nitrate, phosphate, sulfate, DO, ORP, and ferrous iron
1 of 1 5/4/2016
Table 2
November Groundwater and Surface Water Sampling Plan
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Location 1,4-Dioxane
DowTherm
A™
Ethylene
Glycol VOCs*MNA**
Expanded
MNA***
B-01 X X X X X X
B-09C X X X X X
B-10 X X X X X X
B-12 X X X
B-17B X X X X
B-17C X X X X
B-21B X X
B-22A X X X X X
B-22B X X X X X
B-23A X X X X X X
B-23B X X X X X X
B-24A X X X X
B-24B X X X X
B-32B X X X X X
CSW-1 X
CSW-2 X
SW-3 X X X
SW-5 X X X
SW-7 X X X
SW-8 X X X
Notes:
*** Expanded MNA: TOC, ethane, ethene, methane, carbon dioxide, hydrogen, and volatile fatty acids
** MNA: alkalinity, nitrate, phosphate, sulfate, DO, ORP, and ferrous iron
* VOCs to be analyzed annually (November only - revised from CAP schedule of May only)
1 of 1 5/4/2016
Table 3
Groundwater Analytical Summary
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Chemical Name Unit
NC 2L
Standard
B-01
5/7/2015
B-01
11/11/2015
B-09C
5/6/2015
B-09C
11/10/2015
B-10
5/7/2015
B-10
11/11/2015
B-12
5/6/2015
B-12
11/11/2015
B-17B
11/11/2015
B-17C
5/6/2015
B-17C
11/11/2015
B-21B
11/11/2015
B-22A
11/10/2015
1,1-biphenyl mg/L 0.4 NA <0.01 NA <0.01 0.0828 0.192 <0.01 <0.01 <0.01 NA <0.01 NA <0.01
biphenyl ether mg/L PQL*NA 0.122 NA 0.0106 1.09 2.11 <0.01 <0.01 <0.01 NA <0.01 NA <0.01
ethylene glycol mg/L 10 <5.0 <50 <5.0 <500 <5.0 <50 NA NA NA NA NA NA NA
1,4-dioxane mg/L 0.003 2.89 2.64 0.972 0.909 0.511 0.404 3.09 2.9 0.135 2.9 1.81 0.092 1.69
acetone mg/L 6 NA <1.25 NA 2.66 NA <0.625 NA NA NA NA NA NA <0.025
2-butanone mg/L 4 NA <0.5 NA 0.256 NA <0.25 NA NA NA NA NA NA <0.01
chlorobenzene mg/L 0.05 NA <0.25 NA <0.1 NA <0.125 NA NA NA NA NA NA 0.0075
chloroethane mg/L 3 NA <0.5 NA <0.2 NA <0.25 NA NA NA NA NA NA <0.01
1,1-dichloroethane mg/L 0.006 NA <0.25 NA <0.1 NA <0.125 NA NA NA NA NA NA 0.0065
alkalinity mg/L --1470 1430 2500 2260 664 694 310 313 240 336 329 282 544
nitrate nitrogen mg/L 10 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 0.031 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02
nitrite nitrogen mg/L 1 <0.02 <0.02 0.12 0.073 0.044 0.067 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 0.05
orthophosphate phosphorus mg/L --1.6 0.94 <0.25 0.32 <0.25 0.68 0.13 0.2 0.16 0.21 0.34 0.25 <0.25
sulfate mg/L 250 3.1 28.5 <1 <1 <1 <1 1.3 1.2 2.3 1 1.4 15.1 <1
total organic carbon mg/L --NA 3660 NA NA NA 31.6 NA NA 53.3 NA 61.2 NA 5.5
Field Parameters
dissolved oxygen mg/L --0.41 0.27 0.31 0.3 0.48 0.29 1.17 0.96 1.02 0.44 0.66 1.35 0.72
Ferrous Iron mg/L --NA 6.2 NA 5 NA 1.2 NA 0.2 1.1 NA 0.8 1.4 3.2
groundwater elevation feet MSL --695.74 695.31 673.24 671.1 702.38 701.15 656.94 656.18 659.51 659.54 659.94 661.86 658.94
ORP mV --60.8 -6.4 -74.4 -115.9 -45.4 -87.4 35.9 23.4 -71.2 70.6 57.8 -46.1 -125.9
pH su --5.2 5.1 6.61 6.3 6.49 6.24 6.69 6.29 6.26 6.76 6.39 6.49 6.37
specific conductance umhos/cm --5092 5475 5016 4631 1218 1369 719 714 498 679 688 594 1186
temperature degrees C --16.92 18.6 18.98 15.78 16.86 19.69 18.97 14.45 12.7 16.48 14.69 16.04 17.14
turbidity NTU --4.7 2.1 4.7 4.9 3.7 5.5 7.9 5.8 3.2 3.8 3.9 3.2 5.8
Notes:
PQL ‒ Practical Quantitation Limit
* site-specific target chemical
-- no standard specified under 15A NCAC 2L.0202
mg/L ‒ milligrams per liter
mV ‒ millivolts
su ‒ standard units
umhos/cm ‒ micromhos per centimeter
degrees C ‒ degrees Celsius
feet MSL ‒ feet above mean sea level
NTU ‒ Nephelometric Turbidity Units
NA ‒ Not Analyzed
1 of 2 5/4/2016
Table 3
Groundwater Analytical Summary
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Chemical Name Unit
NC 2L
Standard
1,1-biphenyl mg/L 0.4
biphenyl ether mg/L PQL*
ethylene glycol mg/L 10
1,4-dioxane mg/L 0.003
acetone mg/L 6
2-butanone mg/L 4
chlorobenzene mg/L 0.05
chloroethane mg/L 3
1,1-dichloroethane mg/L 0.006
alkalinity mg/L --
nitrate nitrogen mg/L 10
nitrite nitrogen mg/L 1
orthophosphate phosphorus mg/L --
sulfate mg/L 250
total organic carbon mg/L --
Field Parameters
dissolved oxygen mg/L --
Ferrous Iron mg/L --
groundwater elevation feet MSL --
ORP mV --
pH su --
specific conductance umhos/cm --
temperature degrees C --
turbidity NTU --
Notes:
PQL ‒ Practical Quantitation Limit
* site-specific target chemical
-- no standard specified under 15A NCAC 2L.0202
mg/L ‒ milligrams per liter
mV ‒ millivolts
su ‒ standard units
umhos/cm ‒ micromhos per centimeter
degrees C ‒ degrees Celsius
feet MSL ‒ feet above mean sea level
NTU ‒ Nephelometric Turbidity Units
NA ‒ Not Analyzed
B-22B
5/6/2015
B-22B
11/10/2015
B-22B Dup
11/10/2015
B-23A
5/6/2015
B-23A
11/10/2015
B-23B
5/6/2015
B-23B
11/10/2015
B-24A
5/6/2015
B-24A
11/10/2015
B-24B
11/10/2015
B-32B
11/11/2015
NA <0.01 <0.01 NA <0.1 NA <0.01 NA NA NA <0.01
NA 0.0117 0.0103 NA <0.1 NA <0.01 NA NA NA <0.01
NA NA NA <5.0 <50 <5.0 <50 NA NA NA <50
1.73 1.72 1.61 3.24 3.35 2.78 3.33 0.103 NA NA 0.0183
NA <0.025 <0.025 NA 5.12 NA 5.09 NA NA NA NA
NA <0.01 <0.01 NA 0.483 NA 0.488 NA NA NA NA
NA 0.0089 0.0087 NA <0.1 NA <0.1 NA NA NA NA
NA 0.0118 0.0103 NA <0.2 NA <0.2 NA NA NA NA
NA <0.005 <0.005 NA <0.1 NA <0.1 NA NA NA NA
615 724 615 2490 2540 2160 2250 211 NA NA 194
<0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 NA NA 0.14
0.032 <0.02 0.032 0.035 0.04 0.16 0.12 <0.02 NA NA <0.02
<0.05 0.38 <0.05 0.47 1.3 <0.25 0.96 <0.05 NA NA 0.13
<1 <1 <1 9 7.7 5.3 7.5 2 NA NA <1
NA 6.7 NA NA 2780 NA 2890 NA NA NA 40.8
0.38 0.25 0.38 0.44 0.75 0.39 0.34 1.35 NA NA 1
NA 2.9 NA NA 5.1 NA 1.2 NA NA NA 2
657.89 657.95 657.89 656.88 657.7 657.22 657.88 654.68 NA NA 714.2
-40.3 -93 -40.3 -24 -88.1 -56.8 -84 -76.8 NA NA -98.9
6.72 6.38 6.72 6.29 6.22 6.59 6.14 6.79 NA NA 6.44
1182 1340 1182 5560 5597 4661 5275 466 NA NA 464
18.95 16.19 18.95 20.87 16.22 21.28 16.98 15.72 NA NA 17.65
4.3 4.7 4.3 7.6 7.2 6.9 5 1.1 NA NA 2.1
2 of 2 5/4/2016
Table 4
Surface Water Analytical Summary
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Chemical Name Unit
SW-3
11/10/2015
SW-05
5/6/2015
SW-5
11/10/2015
SW-7
11/10/2015
SW-8
11/10/2015
CSW-1
5/6/2015
CSW-1
11/10/2015
CSW-2
11/10/2015
1,1-biphenyl mg/L <0.01 <0.01 <0.01 <0.01 <0.01 NA NA NA
biphenyl ether mg/L <0.01 <0.01 <0.01 <0.01 <0.01 NA NA NA
turbidity NTU 29.5 <0.002 49.2 70 82.6 4.6 48.6 52.6
1,4-dioxane mg/L <0.002 <0.002 <0.002 <0.002 <0.002 0.0821 0.014 0.0124
ethylene glycol mg/L <50 <5.0 <50 <50 <50 NA NA NA
temperature degrees C 13.76 19.82 14.37 12.19 12.96 17.69 15.62 13.66
ORP mV 61.1 -69.1 31.8 42 99.5 -39.7 31.7 46.5
dissolved oxygen mg/L 7.09 7.49 7.94 10.27 7.71 2.18 6.45 6.27
pH su 6.79 7.81 7.18 7.69 6.55 7.34 6.97 6.87
specific conductance umhos/cm 69 91 63 54 67 347 106 69
Notes:
mg/L ‒ milligrams per liter
NTU ‒ Nephelometric Turbidity Units
degrees C ‒ degrees Celsius
mV ‒ millivolts
su ‒ standard units
umhos/cm ‒ micromhos per centimeter
NA ‒ Not Analyzed
1 of 1 5/4/2016
Table 5
Summary of Detected Constituents in Groundwater
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Parameter
1,1-
Biphenyl 1,4-Dioxane
Biphenyl
Ether
Ethylene
Glycol
Units mg/L mg/L mg/L mg/L
NC 2L Standard 0.4 0.003 PQL 14
B-01
Jun-04 <0.05 4.07 0.0723 <28
Nov-04 <0.01 0.202 0.0211 492
May-05 <2.5 2.93 <2.5 1160
Nov-05 <0.01 3.69 0.02 <70
May-06 <0.02 2.75 0.0419 93.9
Nov-06 <0.01 4.68 0.0446 2000
May-07 <0.01 3.43 0.0716 <140
Nov-07 <0.04 3.01 0.0662 <7
May-08 <0.04 2.15 0.0635 <7
Nov-08 <0.01 3.31 0.0565 <7
May-09 NA 2.26 NA <7
Dec-09 <0.01 3.54 0.0423 <35
May-10 NA 3.56 NA <35
Nov-10 <0.01 3.24 0.0811 <35
May-11 NA 2.15 NA NA
Nov-11 <0.01 3.25 0.083 <35
May-12 NA 3.85 NA NA
Nov-12 <1 3.41 <1 <14
May-13 NA 3.07 NA 254
Nov-13 <0.1 2.74 <0.1 38.5
May-14 NA 1.96 NA 796
Nov-14 <0.01 3.27 0.0858 648
May-15 NA 2.89 NA <5.0
Nov-15 <0.01 2.64 0.122 <50
B-09C
Jun-04 <0.5 0.791 <0.5 <70
Nov-04 <0.05 1.04 0.0545 1420
May-05 <0.2 0.776 <0.2 <70
Nov-05 <0.01 1.31 0.0324 363
May-06 <0.02 0.668 0.0492 85.8
Nov-06 <0.01 1.29 <0.01 2020
May-07 <0.01 1.11 0.0377 <140
Nov-07 <0.01 0.995 0.0352 <7
May-08 <0.01 0.486 0.0312 <7
Nov-08 <0.01 1.11 0.0438 <7
May-09 NA 0.873 NA <7
Dec-09 <0.01 1.15 0.0581 <35
May-10 NA 1.03 NA <35
Nov-10 <0.01 0.951 0.0542 <35
May-11 NA 0.782 NA NA
Nov-11 <0.01 1.1 0.0451 <35
May-12 NA 1.46 NA NA
Nov-12 <0.01 1.15 0.0255 <14
May-13 NA 0.803 NA 448
Nov-13 <0.01 0.766 0.0272 77
May-14 NA 0.86 NA 288
Nov-14 <0.01 0.893 0.029 406
May-15 NA 0.972 NA <5.0
Nov-15 <0.01 0.909 0.0106 <500
1 of 7 5/4/2016
Table 5
Summary of Detected Constituents in Groundwater
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Parameter
1,1-
Biphenyl 1,4-Dioxane
Biphenyl
Ether
Ethylene
Glycol
Units mg/L mg/L mg/L mg/L
NC 2L Standard 0.4 0.003 PQL 14
B-10
Jun-04 <1 0.723 4.63 <28
Nov-04 <0.4 0.592 3.33 354
May-05 0.02 0.419 0.193 647
Nov-05 0.31 0.62 3.62 57.5
May-06 0.29 0.328 3.01 <7
Nov-06 0.28 0.509 3.12 284
May-07 0.28 0.564 3.26 <28
Nov-07 0.31 0.413 3.46 <7
May-08 0.405 0.461 3.22 <7
Nov-08 0.352 0.481 3.12 <7
May-09 0.319 0.412 3.09 <7
Dec-09 0.391 0.649 4.58 <14
May-10 0.288 0.417 2.91 <14
Nov-10 0.25 0.39 2.55 <14
May-11 0.328 0.553 3.34 NA
Nov-11 0.3 0.306 2.53 <14
May-12 0.157 0.484 1.45 NA
Nov-12 0.165 0.546 1.82 <14
May-13 0.106 0.421 1.12 252
Nov-13 0.157 0.47 1.69 <35
May-14 0.0728 0.599 0.73 <10
Nov-14 0.169 0.508 1.84 <10
May-15 0.0828 0.511 1.09 <5.0
Nov-15 0.192 0.404 2.11 <50
B-12
Feb-04 <0.01 0.315 <0.01 <7
May-04 <0.01 0.521 <0.01 <7
Jun-04 <0.01 0.775 0.0102 <7
Nov-04 <0.01 0.942 0.0115 <7
May-05 <0.01 0.222 0.0108 <7
Nov-05 <0.01 0.165 <0.01 <7
May-06 <0.01 0.151 <0.01 NA
Nov-06 <0.01 0.216 <0.01 NA
May-07 <0.01 0.118 <0.01 NA
Nov-07 <0.01 0.169 <0.01 NA
May-08 <0.01 0.121 <0.01 <7
Nov-08 <0.01 0.102 <0.01 NA
May-09 <0.01 0.105 0.0108 NA
Dec-09 <0.01 0.128 0.0119 NA
May-10 <0.01 0.11 <0.01 NA
Nov-10 <0.01 0.0946 <0.01 NA
May-11 <0.01 0.11 <0.01 NA
Nov-11 <0.01 0.0761 <0.01 NA
May-12 <0.01 0.13 <0.01 NA
May-12 <0.01 0.132 <0.01 NA
Nov-12 <0.01 3.68 <0.01 NA
May-13 <0.01 3.44 <0.01 NA
Nov-13 <0.01 3.24 <0.01 NA
May-14 <0.01 2.59 <0.01 NA
Nov-14 <0.01 3.27 <0.01 NA
May-15 <0.01 3.09 <0.01 NA
Nov-15 <0.01 2.9 <0.01 NA
2 of 7 5/4/2016
Table 5
Summary of Detected Constituents in Groundwater
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Parameter
1,1-
Biphenyl 1,4-Dioxane
Biphenyl
Ether
Ethylene
Glycol
Units mg/L mg/L mg/L mg/L
NC 2L Standard 0.4 0.003 PQL 14
B-17B
Feb-04 <0.01 2.98 <0.01 <7
May-04 <0.01 2.33 0.0125 <7
Jun-04 <0.01 4.96 <0.01 <7
Nov-04 <0.01 3.11 <0.01 <7
May-05 <0.01 2.83 0.0102 <7
Nov-05 <0.01 1.87 0.0107 <7
May-06 <0.01 2.42 <0.01 NA
Nov-06 <0.01 2.84 <0.01 NA
May-07 <0.01 2.62 <0.01 NA
Nov-07 <0.01 3.33 <0.01 NA
May-08 <0.01 3.52 <0.01 <7
Nov-08 <0.01 2.35 <0.01 NA
Dec-09 <0.01 2.54 <0.01 NA
Nov-10 <0.01 2.75 <0.01 NA
Nov-11 <0.01 2.59 <0.01 NA
Nov-12 <0.01 0.291 <0.01 NA
Nov-13 <0.01 0.113 <0.01 NA
Nov-14 <0.01 0.271 <0.01 NA
Nov-15 <0.01 0.135 <0.01 NA
B-17C
Feb-04 <0.01 3.29 <0.01 <7
May-04 <0.01 2.21 <0.01 <7
Jun-04 <0.01 3.01 <0.01 <7
Nov-04 <0.01 3.22 0.0117 <7
May-05 <0.01 2.51 <0.01 <8.5
Nov-05 <0.01 2.44 <0.01 <7
May-06 <0.01 2.68 <0.01 NA
Nov-06 <0.01 2.92 <0.01 NA
May-07 <0.01 2.93 <0.01 NA
Nov-07 <0.01 3.06 <0.01 NA
May-08 <0.01 2.90 <0.01 <7
Nov-08 <0.01 2.10 <0.01 NA
Dec-09 <0.01 2.40 <0.01 NA
May-10 NA 1.95 NA NA
Nov-10 <0.01 2.39 <0.01 NA
May-11 NA 2.02 NA NA
Nov-11 <0.01 2.15 <0.01 NA
May-12 NA 2.47 NA NA
Nov-12 <0.01 3.18 <0.01 NA
May-13 NA 3.61 NA NA
Nov-13 <0.01 3.1 <0.01 NA
May-14 NA 3.71 NA NA
Nov-14 <0.01 2.42 <0.01 NA
May-15 NA 2.9 NA NA
Nov-15 <0.01 1.81 <0.01 NA
3 of 7 5/4/2016
Table 5
Summary of Detected Constituents in Groundwater
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Parameter
1,1-
Biphenyl 1,4-Dioxane
Biphenyl
Ether
Ethylene
Glycol
Units mg/L mg/L mg/L mg/L
NC 2L Standard 0.4 0.003 PQL 14
B-21B
Jun-04 <0.01 0.0391 <0.01 <7
Nov-04 <0.01 0.047 <0.01 <7
May-05 <0.01 0.0338 <0.01 <7
Nov-05 <0.01 0.0477 <0.01 <7
May-06 NA 0.0348 NA NA
Nov-06 NA 0.0507 NA NA
May-07 NA 0.0511 NA NA
Nov-07 NA 0.0686 NA NA
May-08 NA 0.0557 NA <7
Nov-08 NA 0.0598 NA NA
Dec-09 NA 0.0698 NA NA
Nov-10 NA 0.0534 NA NA
Nov-11 NA 0.0573 NA NA
Nov-12 NA 0.0811 NA NA
Nov-13 NA 0.0665 NA NA
Nov-14 NA 0.0832 NA NA
Nov-15 NA 0.092 NA NA
B-22A
Feb-04 <0.01 0.67 0.0634 <7
May-04 <0.01 0.322 0.0514 <7
Jun-04 <0.01 1.06 0.0449 <7
Nov-04 <0.01 0.895 0.0427 <7
May-05 <0.01 0.722 0.0284 <7.9
Nov-05 <0.01 0.572 0.0268 <7
May-06 <0.01 0.949 0.025 NA
Nov-06 <0.01 1.12 0.0259 NA
May-07 <0.01 1.13 0.0186 NA
Nov-07 <0.01 1.3 0.0213 NA
May-08 <0.01 1.18 0.0242 <7
Nov-08 <0.01 1.04 0.0214 NA
Dec-09 <0.01 1.25 0.0141 NA
Nov-10 <0.01 1.74 <0.01 NA
Nov-11 <0.01 1.22 <0.01 NA
Nov-12 <0.01 2.05 <0.01 NA
Nov-13 <0.01 1.71 <0.01 NA
Nov-14 <0.01 1.64 <0.01 NA
Nov-15 <0.01 1.69 <0.01 NA
4 of 7 5/4/2016
Table 5
Summary of Detected Constituents in Groundwater
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Parameter
1,1-
Biphenyl 1,4-Dioxane
Biphenyl
Ether
Ethylene
Glycol
Units mg/L mg/L mg/L mg/L
NC 2L Standard 0.4 0.003 PQL 14
B-22B
Feb-04 <0.01 2.64 0.0323 <7
May-04 <0.01 1.9 0.0346 <7
Jun-04 <0.01 2.78 0.033 <7
Nov-04 <0.01 2.72 0.0362 <7
May-05 <0.01 2.32 0.0351 <10.8
Nov-05 <0.01 1.22 0.0365 <7
May-06 <0.01 2.46 0.0329 NA
Nov-06 <0.01 2.33 0.028 NA
May-07 <0.01 2.79 0.0284 NA
Nov-07 <0.01 2.62 0.0295 NA
May-08 <0.01 2.42 0.023 <7
Nov-08 <0.01 1.87 0.0236 NA
May-09 NA 2.39 NA NA
Dec-09 <0.01 2.14 0.0265 NA
May-10 NA 2.01 NA NA
Nov-10 <0.01 2.14 0.0316 NA
May-11 NA 1.75 NA NA
Nov-11 <0.01 1.5 0.0251 NA
May-12 NA 1.95 NA NA
Nov-12 <0.01 2.08 0.0243 NA
Nov-12 <0.01 2.2 0.0227 NA
May-13 NA 1.88 NA NA
Nov-13 <0.01 1.69 0.0222 NA
May-14 NA 2.05 NA NA
Nov-14 <0.01 2.8 0.0202 NA
May-15 NA 1.73 NA NA
Nov-15 <0.01 1.72 0.0117 NA
B-23A
Feb-04 <0.01 1.5 0.115 <7
May-04 <0.01 1.21 0.0928 <7
Jun-04 <0.01 2.03 0.0911 <7
Nov-04 <0.01 1.45 0.0769 227
May-05 <0.01 1.41 0.0108 278
Nov-05 <0.01 1.29 0.0919 <70
May-06 <0.01 0.711 0.0823 286
Nov-06 <0.01 2.01 0.0791 255
May-07 <0.01 1.51 0.0768 <70
Nov-07 <0.01 1.45 0.112 <7
May-08 <0.01 1.91 0.0936 NA
Nov-08 <0.01 1.97 0.0711 <7
May-09 NA 1.34 NA <7
Dec-09 <0.01 1.84 0.131 <7
May-10 NA 1.96 NA <7
Nov-10 <0.01 1.81 0.1 <7
May-11 NA 1.3 NA NA
Nov-11 <0.01 2.41 0.0884 <7
May-12 NA 2.45 NA NA
Nov-12 <0.01 3.35 0.0772 <7
May-13 NA 2.82 NA 120
Nov-13 <0.01 2.76 0.0755 146
May-14 NA 3.06 NA <100
Nov-14 <0.01 3.54 0.0708 329
May-15 NA 3.24 NA <5.0
Nov-15 <0.1 3.35 <0.1 <50
5 of 7 5/4/2016
Table 5
Summary of Detected Constituents in Groundwater
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Parameter
1,1-
Biphenyl 1,4-Dioxane
Biphenyl
Ether
Ethylene
Glycol
Units mg/L mg/L mg/L mg/L
NC 2L Standard 0.4 0.003 PQL 14
B-23B
Feb-04 <0.01 1.67 0.124 594
May-04 <0.01 1.14 0.115 <7
Jun-04 <0.01 1.76 0.101 <35
Nov-04 <0.01 1.82 0.0857 393
May-05 <0.2 1.29 <0.2 <35
Nov-05 <0.01 1.33 0.129 <35
May-06 <0.01 0.891 0.116 51.9
Nov-06 <0.02 1.7 0.128 907
May-07 <0.02 2.29 0.0973 <70
Nov-07 <0.01 1.94 0.128 <7
May-08 <0.01 2.31 0.123 <7
Nov-08 <0.01 2.54 0.112 <7
May-09 NA 1.77 NA <7
Dec-09 <0.01 2.46 0.183 <7
May-10 NA 2.14 NA <7
Nov-10 <0.01 2.02 0.0768 <7
May-11 NA 2.15 NA NA
Nov-11 <0.01 2.49 0.0982 <7
May-12 NA 2.39 NA NA
Nov-12 <0.01 3.52 0.0811 <7
May-13 NA 2.72 NA 120
Nov-13 <0.01 2.88 0.0759 82.3
May-14 NA 3.01 NA 381
Nov-14 <0.0111 3.4 0.103 542
May-15 NA 2.78 NA <5.0
Nov-15 <0.01 3.33 <0.01 <50
B-24A
Feb-04 <0.01 0.0548 <0.01 7.8
May-04 <0.01 0.022 <0.01 <7
Jun-04 <0.01 0.0625 <0.01 <7
Nov-04 <0.01 0.0796 <0.01 <7
May-05 <0.01 0.0885 <0.01 <7
Nov-05 <0.01 0.0726 0.0111 <7
May-06 <0.01 0.105 0.0102 NA
Nov-06 <0.01 0.158 0.0126 NA
May-07 <0.01 0.141 <0.01 NA
Nov-07 <0.01 0.161 0.0124 NA
May-08 <0.01 0.159 <0.01 <7
Nov-08 <0.01 0.125 0.0124 NA
May-09 NA 0.113 NA NA
Dec-09 <0.01 0.15 0.0169 NA
May-10 NA 0.135 NA NA
Nov-10 <0.01 0.133 0.01 NA
May-11 NA 0.102 NA NA
Nov-11 <0.01 0.132 0.0118 NA
Nov-12 <0.01 0.218 0.011 NA
May-13 NA 0.126 NA NA
Nov-13 <0.01 0.158 <0.01 NA
May-14 NA 0.189 NA NA
Nov-14 <0.01 0.23 0.0124 NA
May-15 NA 0.103 NA NA
Nov-15 NA NA NA NA
6 of 7 5/4/2016
Table 5
Summary of Detected Constituents in Groundwater
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
Parameter
1,1-
Biphenyl 1,4-Dioxane
Biphenyl
Ether
Ethylene
Glycol
Units mg/L mg/L mg/L mg/L
NC 2L Standard 0.4 0.003 PQL 14
B-24B
Feb-04 <0.01 0.0586 0.0184 <7
May-04 <0.01 0.0439 0.0178 <7
Jun-04 <0.01 0.0892 0.0146 <7
Nov-04 <0.01 0.082 0.0181 <7
May-05 <0.01 0.0722 0.0194 <7
Nov-05 <0.01 0.0591 0.0165 <7
May-06 <0.01 0.0746 0.0178 NA
Nov-06 <0.01 0.101 0.018 NA
May-07 <0.01 0.0962 0.015 NA
Nov-07 <0.01 0.102 0.0158 NA
May-08 <0.01 0.113 0.0151 <7
Nov-08 <0.01 0.0877 0.0178 NA
Dec-09 <0.01 0.0931 0.0226 NA
Nov-10 <0.01 0.0896 0.0151 NA
Nov-11 <0.01 0.0874 0.0144 NA
May-12 NA 0.103 NA NA
Nov-12 <0.01 0.118 0.0136 NA
Nov-13 <0.01 0.0918 <0.01 NA
Nov-14 <0.01 0.103 0.0101 NA
Nov-15 NA NA NA NA
B-32B
Jun-04 <0.01 0.176 0.0577 <28
Nov-04 <0.01 0.198 0.0575 162
May-05 <0.2 0.115 <0.2 <14
Nov-05 <0.01 0.072 0.0416 <14
May-06 <0.01 0.0818 0.0617 27.6
Nov-06 <0.01 0.0996 0.0558 344
May-07 <0.01 0.149 0.0414 <35
Nov-07 <0.01 0.117 0.0816 <7
May-08 <0.01 0.0796 0.0329 <7
Nov-08 <0.01 0.173 0.0816 <7
Dec-09 <0.01 0.104 0.0621 <7
Nov-10 <0.01 0.144 0.0566 <7
Nov-11 <0.01 0.0988 0.0399 <7
Nov-12 <0.01 0.0755 <0.01 <7
Nov-13 <0.01 0.0275 0.0106 <7
Nov-14 <0.01 0.0178 <0.01 <10
Nov-15 <0.01 0.0183 <0.01 <50
Notes:
NA ‒ Not Analyzed
PQL ‒ Practical Quantitation Limit
mg/L ‒ milligrams per liter
7 of 7 5/4/2016
Table 6
Time vs. Concentration Plots ‒ Ethylene Glycol
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
0
500
1000
1500
2000
2500
C o n c e n t r a t i o n (m g /L )
Date
Ethylene Glycol (B-01)
B-01 NC 2L Standard
0
500
1000
1500
2000
2500
C o n c e n t r a t i o n
(m g /L )
Date
Ethylene Glycol (B-09C)
B-09C NC 2L Standard
0
500
1000
1500
2000
2500
C o n c e n t r a t i o n
(m g /L )
Date
Ethylene Glycol (B-10)
B-10 NC 2L Standard
0
500
1000
1500
2000
2500
C o n c e n t r a t i o n (m g /L )
Date
Ethylene Glycol (B-23A)
B-23A NC 2L Standard
0
500
1000
1500
2000
2500
C o n c e n t r a t i o n (m g /L )
Date
Ethylene Glycol (B-23B)
B-23B NC 2L Standard
1 of 1 5/4/2016
Table 7
Time vs. Concentration Plots ‒ 1,4-Dioxane
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
0
1
2
3
4
5
C o n c e n t r a t i o n (m g /L )
Date
1,4-Dioxane (B-01)
B-01 NC 2L Standard
0
1
2
3
4
5
C o n c e n t r a t i o n
(m g /L )
Date
1,4-Dioxane (B-09C)
B-09C NC 2L Standard
0
1
2
3
4
5
C o n c e n t r a t i o n
(m g /L )
Date
1,4-Dioxane (B-10)
B-10 NC 2L Standard
0
1
2
3
4
5
C o n c e n t r a t i o n (m g /L )
Date
1,4-Dioxane (B-17C)
B-17C NC 2L Standard
0
1
2
3
4
5
C o n c e n t r a t i o n
(m g /L )
Date
1,4-Dioxane (B-12)
B-12 NC 2L Standard
0
1
2
3
4
5
C o n c e n t r a t i o n
(m g /L )
Date
1,4-Dioxane (B-22B)
B-22B NC 2L Standard
0
1
2
3
4
5
C o n c e n t r a t i o n (m g /L )
Date
1,4-Dioxane (B-23A)
B-23A NC 2L Standard
0
1
2
3
4
5
C o n c e n t r a t i o n (m g /L )
Date
1,4-Dioxane (B-23B)
B-23B NC 2L Standard
0
0.05
0.1
0.15
0.2
0.25
C o n c e n t r a t i o n (m g /L )
Date
1,4-Dioxane (B-24A)
B-24A NC 2L Standard
1 of 1 5/4/2016
Table 8
Time vs. Concentration Plots ‒ Biphenyl Ether
CNA Holdings LLC ‒ Needmore Road Landfill Facility
AECOM Project No. 60313404
0
1
2
3
4
5
C o n c e n t r a t i o n (m g /L )
Date
Biphenyl Ether (B-10)
B-10 PQL
0
0.005
0.01
0.015
0.02
0.025
0.03
C o n c e n t r a t i o n (m g /L )
Date
Biphenyl Ether (B-12)
B-12 PQL
0
0.1
0.2
0.3
0.4
0.5
C o n c e n t r a t i o n (m g /L )
Date
Biphenyl Ether (B-23A)
B-23A PQL
0
0.1
0.2
0.3
0.4
0.5
C o n c e n t r a t i o n (m g /L )
Date
Biphenyl Ether (B-23B)
B-23B PQL
0
0.1
0.2
0.3
0.4
0.5
C o n c e n t r a t i o n (m g /L )
Date
Biphenyl Ether (B-01)
B-01 PQL
1 of 1 5/4/2016
AECOM Environment
May 2016
Figures
SCALE
4000'2000'0'
N
COOLEEMEE, NC - 1969; REV.1983
SOURCE: USGS 7.5 MIN. QUADRANGLE
FIGURE 1
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
SITE

SITE LOCATION MAP
60313404APRIL 2016
$$D A T E $$
$$D G N $$

T
A
Y
L
O
R
P
I
T
X
X
X
X
X X
X
X
X
X
X
X
X
X
X
660
6
6
0
660
6
6
0
670
6
7
0
6
7
0
670
670
670
680
6 8 0
680
680
690
690
6 9 0
690
690
6 9 0
6 9 0
7 0 0
700
700
7 0 0
700
710
710
710
710
7 1 0
720
720 720
720
7
2
0
730
7 3 0
7
3
0
7
4
0
740
7 4 0
7
4
0
740
750
750
7 5 0
750
7
5
0
760
760
7
6
0
7
6
0
X
X X
X
X X
660
6
70
670
680
680
690
6 9 0
700
7
0
0
7
0
0
700
710
710
7
1 0
7
2
0
7 2 0
720
720
7
3
0
7
3
0
7
3
0
7
3
0
740
740
7
5
0
7 6 0
740770
7
1
0
B-24A
B-22BB-12
B-17C
B-09C
B-10
B-01
B-23A
B-23B
SCALE
800'400'0'
N
BEAVERDAM BRANCH
OF CONFLUENCE WITH
SW-3 SLIGHTLY UPSTREAM
SW-5
CSW-1
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
FIGURE 2
SAMPLE LOCATION MAP
SALISBURY, NORTH CAROLINA
OF COOLEEMEE WEIR
± 1000 FT DOWN STREAM
SW-8
60313404
MAY 2015
APRIL 2016
CSW-2*
LOCATION WAS DRY AND NOT SAMPLED*
SURFACE WATER SAMPLING LOCATIONS
MONITORING WELL LOCATION
LEGEND
$F I L E S $

$D A T E $
T
A
Y
L
O
R
P
I
T
X
X
X
X
X X
X
X
X
X
X
X
X
X
X
660
6
6
0
660
6
6
0
670
6
7
0
6
7
0
670
670
670
680
6 8 0
680
680
690
690
6 9 0
690
690
6 9 0
6 9 0
7 0 0
700
700
7 0 0
700
710
710
710
710
7 1 0
720
720 720
720
7
2
0
730
7 3 0
7
3
0
7
4
0
740
7 4 0
7
4
0
740
750
750
7 5 0
750
7
5
0
760
760
7
6
0
7
6
0
X
X X
X
X X
660
6
70
670
680
680
690
6 9 0
700
7
0
0
7
0
0
700
710
710
7
1 0
7
2
0
7 2 0
720
720
7
3
0
7
3
0
7
3
0
7
3
0
740
740
7
5
0
7 6 0
740770
7
1
0
B-24B*
B-22BB-12
B-17C
B-09C
B-10
B-01
B-23A
B-23B
SCALE
800'400'0'
N
BEAVERDAM BRANCH
OF CONFLUENCE WITH
SW-3 SLIGHTLY UPSTREAM
SW-5
SW-7
CSW-2
CSW-1
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
FIGURE 3
SAMPLE LOCATION MAP
SALISBURY, NORTH CAROLINA
OF COOLEEMEE WEIR
± 1000 FT DOWN STREAM
SW-8
60313404
NOVEMBER 2015
B-17B
B-21B
B-22A
B-24A*
B-32B
B-21B
APRIL 2016
HIGH WATER ELEVATION
* WELLS WERE NOT SAMPLED DUE TO
SURFACE WATER SAMPLING LOCATIONS
MONITORING WELL LOCATION
LEGEND
$F I L E S $

$D A T E $
T
A
Y
L
O
R
P
I
T
X
X
X
X
X X
X
X
X
X
X
X
X
X
X
660
6
6
0
660
6
6
0
670
6
7
0
6
7
0
670
670
670
680
6 8 0
680
680
690
690
6 9 0
690
690
6 9 0
6 9 0
7 0 0
700
700
7 0 0
700
710
710
710
710
7 1 0
720
720 720
720
7
2
0
730
7 3 0
7
3
0
7
4
0
740
7 4 0
7
4
0
740
750
750
7 5 0
750
7
5
0
760
760
7
6
0
7
6
0
X
X X
X
X X
660
6
70
670
680
680
690
6 9 0
700
7
0
0
7
0
0
700
710
710
7
1 0
7
2
0
7 2 0
720
720
7
3
0
7
3
0
7
3
0
7
3
0
740
740
7
5
0
7 6 0
740770
7
1
0
N
B-17C
B-09C
B-12
B-32B
B-10
B-01
B-22A
B-22B
B-23AB-23B
B-24A
B-24B
B-21B
B-17B
FIGURE 4
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
SCALE
800' 400' 0'
710
GROUNDWATER ELEVATION DATA
NOVEMBER 2015
60313404
695.31
671.1
701.15
656.18
659.51
659.94
661.86
658.94
657.7657.88
714.2
based on historical data
(Based on November 2015 data) Inferred dashed lines
POTENTIOMETRIC CONTOUR
EXTRACTION WELL
SAPROLITE MONITORING WELL
LEGEND
APRIL 2016
657.95
DUP 657.89
NA
NA
$F I L E S $

$D A T E $
695
700
705
710
690
6856806756706656
6
0
705
700
6
9
5
6
9
0
6
8
5
6
8
0
6
7
5
6
7
0
6 6 5 6 6 0
655
T
A
Y
L
O
R
P
I
T
X
X
X
X
X X
X
X
X
X
X
X
X
X
X
660
6
6
0
660
6
6
0
670
6
7
0
6
7
0
670
670
670
680
6 8 0
680
680
690
690
6 9 0
690
690
6 9 0
6 9 0
7 0 0
700
700
7 0 0
700
710
710
710
710
7 1 0
720
720 720
720
7
2
0
730
7 3 0
7
3
0
7
4
0
740
7 4 0
7
4
0
740
750
750
7 5 0
750
7
5
0
760
760
7
6
0
7
6
0
X
X X
X
X X
660
6
70
670
680
680
690
6 9 0
700
7
0
0
7
0
0
700
710
710
7
1 0
7
2
0
7 2 0
720
720
7
3
0
7
3
0
7
3
0
7
3
0
740
740
7
5
0
7 6 0
740770
7
1
0
SCALE
800'400'0'
N
B-22BB-12
B-17C
FIGURE 5
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
60313404
NANA
B-24A
B-09C
B-10
B-01
B-23A
B-23B
<5.0
<5.0
<5.0
ETHYLENE GLYCOL MAP
<5.0
<5.0
MAY 2015
APRIL 2016
NA
NA
3. NA - Sample not analyzed for Ethylene Glycol.
2. Wells not sampled are not shown.
1. Concentrations are in milligrams per liter.
NOTES:
PHYTOREMEDIATION SYSTEM
MONITORING WELL
LEGEND
$F I L E S $

$D A T E $
T
A
Y
L
O
R
P
I
T
X
X
X
X
X X
X
X
X
X
X
X
X
X
X
660
6
6
0
660
6
6
0
670
6
7
0
6
7
0
670
670
670
680
6 8 0
680
680
690
690
6 9 0
690
690
6 9 0
6 9 0
7 0 0
700
700
7 0 0
700
710
710
710
710
7 1 0
720
720 720
720
7
2
0
730
7 3 0
7
3
0
7
4
0
740
7 4 0
7
4
0
740
750
750
7 5 0
750
7
5
0
760
760
7
6
0
7
6
0
X
X X
X
X X
660
6
70
670
680
680
690
6 9 0
700
7
0
0
7
0
0
700
710
710
7
1 0
7
2
0
7 2 0
720
720
7
3
0
7
3
0
7
3
0
7
3
0
740
740
7
5
0
7 6 0
740770
7
1
0
SCALE
800'400'0'
N
B-22BB-12
B-17C
FIGURE 6
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
60313404
NA
NA
NA
B-24A*
B-09C
B-10
B-01
B-23A
B-23B
<50
<50
<50
ETHYLENE GLYCOL MAP
B-17B B-22A
B-32B
B-24B*
NA
B-21B
NA
<500
<50
NOVEMBER 2015
<50
APRIL 2016
4. * Sample not collected due to high water elevation.
3. NA - Sample not analyzed for Ethylene Glycol.
2. Wells not sampled are not shown.
1. Concentrations are in milligrams per liter.
NOTES:
PHYTOREMEDIATION SYSTEM
MONITORING WELL
LEGEND
NA
$F I L E S $

$D A T E $
B-17B B-22A
B-32B
B-24B*
B-21B
T
A
Y
L
O
R
P
I
T
X
X
X
X
X X
X
X
X
X
X
X
X
X
X
660
6
6
0
660
6
6
0
670
6
7
0
6
7
0
670
670
670
680
6 8 0
680
680
690
690
6 9 0
690
690
6 9 0
6 9 0
7 0 0
700
700
7 0 0
700
710
710
710
710
7 1 0
720
720 720
720
7
2
0
730
7 3 0
7
3
0
7
4
0
740
7 4 0
7
4
0
740
750
750
7 5 0
750
7
5
0
760
760
7
6
0
7
6
0
X
X X
X
X X
660
6
70
670
680
680
690
6 9 0
700
7
0
0
7
0
0
700
710
710
7
1 0
7
2
0
7 2 0
720
720
7
3
0
7
3
0
7
3
0
7
3
0
740
740
7
5
0
7 6 0
740770
7
1
0
SCALE
800'400'0'
N
B-24A
B-22BB-12
B-17C
B-09C
B-10
B-01
B-23A
B-23B
2.9
2.89
3.24
2.78
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
FIGURE 7
1,4-DIOXANE MAP
SALISBURY, NORTH CAROLINA
2. Wells not sampled are not shown.
1. Concentrations are in milligrams per liter.
NOTES:
PHYTOREMEDIATION SYSTEM
PLUME OF 1,4-DIOXANE
MONITORING WELL
LEGEND
0.103
60313404
3.09
MAY 2015
0.511
1.73
APRIL 2016
0.972
$F I L E S $

$D A T E $
T
A
Y
L
O
R
P
I
T
X
X
X
X
X X
X
X
X
X
X
X
X
X
X
660
6
6
0
660
6
6
0
670
6
7
0
6
7
0
670
670
670
680
6 8 0
680
680
690
690
6 9 0
690
690
6 9 0
6 9 0
7 0 0
700
700
7 0 0
700
710
710
710
710
7 1 0
720
720 720
720
7
2
0
730
7 3 0
7
3
0
7
4
0
740
7 4 0
7
4
0
740
750
750
7 5 0
750
7
5
0
760
760
7
6
0
7
6
0
X
X X
X
X X
660
6
70
670
680
680
690
6 9 0
700
7
0
0
7
0
0
700
710
710
7
1 0
7
2
0
7 2 0
720
720
7
3
0
7
3
0
7
3
0
7
3
0
740
740
7
5
0
7 6 0
740770
7
1
0
SCALE
800'400'0'
N
B-24B*B-24A*
B-21B
B-22A
B-22B
B-32B
B-12
B-17B
B-17C
B-09C
B-10
B-01
B-23A
B-23B
1.81
2.64
3.35
3.33
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
FIGURE 8
1,4-DIOXANE MAP
SALISBURY, NORTH CAROLINA
60313404
2.9
0.404
NOVEMBER 2015
0.909
0.092
0.135
1.72
1.61 DUP
1.69
0.0183
APRIL 2016
Plume contour based on 2014 data.
3. * Sample not collected due to high water level.
2. Wells not sampled are not shown.
1. Concentrations are in milligrams per liter.
NOTES:
PHYTOREMEDIATION SYSTEM
PLUME OF 1,4-DIOXANE
MONITORING WELL
LEGEND
$F I L E S $

$D A T E $
T
A
Y
L
O
R
P
I
T
X
X
X
X
X X
X
X
X
X
X
X
X
X
X
660
6
6
0
660
6
6
0
670
6
7
0
6
7
0
670
670
670
680
6 8 0
680
680
690
690
6 9 0
690
690
6 9 0
6 9 0
7 0 0
700
700
7 0 0
700
710
710
710
710
7 1 0
720
720 720
720
7
2
0
730
7 3 0
7
3
0
7
4
0
740
7 4 0
7
4
0
740
750
750
7 5 0
750
7
5
0
760
760
7
6
0
7
6
0
X
X X
X
X X
660
6
70
670
680
680
690
6 9 0
700
7
0
0
7
0
0
700
710
710
7
1 0
7
2
0
7 2 0
720
720
7
3
0
7
3
0
7
3
0
7
3
0
740
740
7
5
0
7 6 0
740770
7
1
0
SCALE
800'400'0'
N
B-24B*B-24A*
B-22A
B-22B
B-32B
B-12
B-17B
B-17C
B-09C
B-10
B-01
B-23A
B-23B
<0.01
<0.01
<0.01
<0.01
<0.01
FIGURE 9
1,1-BIPHENYL MAP
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
NOVEMBER 2015
60313404
0.192
<0.01 DUP
<0.01
<0.01
<0.01
APRIL 2016
<0.01
<0.1
3. * Sample not collected due to high water level.
2. Wells not sampled are not shown.
1. Concentrations are in milligrams per liter.
NOTES:
PHYTOREMEDIATION SYSTEM
PLUME OF 1,1-BIPHENYL
MONITORING WELL
LEGEND
$F I L E S $

$D A T E $
T
A
Y
L
O
R
P
I
T
X
X
X
X
X X
X
X
X
X
X
X
X
X
X
660
6
6
0
660
6
6
0
670
6
7
0
6
7
0
670
670
670
680
6 8 0
680
680
690
690
6 9 0
690
690
6 9 0
6 9 0
7 0 0
700
700
7 0 0
700
710
710
710
710
7 1 0
720
720 720
720
7
2
0
730
7 3 0
7
3
0
7
4
0
740
7 4 0
7
4
0
740
750
750
7 5 0
750
7
5
0
760
760
7
6
0
7
6
0
X
X X
X
X X
660
6
70
670
680
680
690
6 9 0
700
7
0
0
7
0
0
700
710
710
7
1 0
7
2
0
7 2 0
720
720
7
3
0
7
3
0
7
3
0
7
3
0
740
740
7
5
0
7 6 0
740770
7
1
0
SCALE
800'400'0'
N
B-24B*B-24A*
B-22A
B-22B
B-32B
B-12
B-17B
B-17C
B-09C
B-10
B-01
B-23A
B-23B
<0.01
<0.01
<0.01
0.0106
2.11
<0.01
BIPHENYL ETHER MAP
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
NOVEMBER 2015
60313404
<0.01
FIGURE 10
0.0117
0.0103 DUP
0.122
<0.01
APRIL 2016
<0.1
3. * Sample not collected due to high water level.
2. Wells not sampled are not shown.
1. Concentrations are in milligrams per liter.
NOTES:
PHYTOREMEDIATION SYSTEM
PLUME OF BIPHENYL ETHER
MONITORING WELL
LEGEND
$F I L E S $

$D A T E $
AECOM Environment
May 2016
Appendix A
May 2015 and November 2015
Laboratory Analytical Reports
#=CL#
May 20, 2015
LIMS USE: FR - BRYON DAHLGREN
LIMS OBJECT ID: 92248790
92248790
Project:
Pace Project No.:
RE:
Bryon Dahlgren
AECOM
10 Patewood Drive, Bldg 6
Suite 500
Greenville, SC 29615
NEEDMORE RD. LF
Dear Bryon Dahlgren:
Enclosed are the analytical results for sample(s) received by the laboratory on May 07, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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816 Durst Avenue East
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Page 1 of 34
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074
Indiana Certification #: C-49-06Kansas Certification #:E-10177/ E-10247Kentucky UST Certification #: 0042Kentucky WW Certification #:98019Louisiana/NELAP Certification #: 04076
Ohio VAP Certification #: CL-0065Oklahoma Certification #: 2014-148
Pennsylvania Certification #: 68-05340Texas Certification #: T104704355-15-8West Virginia Certification #: 330Wisconsin Certification #: 999788130USDA Soil Permit #: P330-10-00128
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
Greenwood Certification IDs
816 Durst Avenue East, Greenwood, SC 29649South Carolina Laboratory ID #: 24562North Carolina Divison of Water Resources Certification
number 25
Florida Certification number E87633Virginia VELAP ID: 460250
Asbestos NVLAP accreditation: 101410-0
REPORT OF LABORATORY ANALYSIS
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Page 2 of 34
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92248790001 B-24A EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790002 B-22B EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790003 B-17C EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790004 B-23A EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790005 B-23B EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790006 B-9C EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790007 B-01 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 3 of 34
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790008 B-10 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 8270 8 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790009 B-12 EPA 9056A 1 PASI-GCDC
EPA 8270 8 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790010 SW-99 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 8 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
92248790011 SW-5 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 8 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
92248790012 CSW-1 EPA 8260B Mod.3 PASI-CDLK
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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816 Durst Avenue East
Greenwood, SC 29649
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Page 4 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-24A Lab ID:92248790001 Collected:05/06/15 12:05 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 2.0 mg/L 05/13/15 22:22 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)103 ug/L 05/11/15 22:06 123-91-110.0 5
Surrogates
1,2-Dichloroethane-d4 (S)88 %05/11/15 22:06 17060-07-050-150 5
Toluene-d8 (S)101 %05/11/15 22:06 2037-26-550-150 5
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 211 mg/L 05/11/15 20:195.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:250.020 1
Nitrogen, Nitrite ND mg/L 05/08/15 00:250.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 05/08/15 12:00 M10.050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 5 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-22B Lab ID:92248790002 Collected:05/06/15 15:25 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 05/13/15 22:52 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)1730 ug/L 05/11/15 22:26 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)91 %05/11/15 22:26 17060-07-050-150 50
Toluene-d8 (S)100 %05/11/15 22:26 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 615 mg/L 05/11/15 20:325.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:370.020 1
Nitrogen, Nitrite 0.032 mg/L 05/08/15 00:370.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 05/08/15 12:000.050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 6 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-17C Lab ID:92248790003 Collected:05/06/15 17:35 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 1.0 mg/L 05/13/15 23:23 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2900 ug/L 05/11/15 22:47 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)92 %05/11/15 22:47 17060-07-050-150 50
Toluene-d8 (S)101 %05/11/15 22:47 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 336 mg/L 05/11/15 20:545.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:430.020 1
Nitrogen, Nitrite ND mg/L 05/08/15 00:430.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.21 mg/L 05/08/15 12:000.050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 7 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-23A Lab ID:92248790004 Collected:05/06/15 13:10 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:00 107-21-15.0 1
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 9.0 mg/L 05/13/15 23:53 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)3240 ug/L 05/11/15 23:07 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)96 %05/11/15 23:07 17060-07-050-150 50
Toluene-d8 (S)100 %05/11/15 23:07 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2490 mg/L 05/11/15 21:105.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:300.020 1
Nitrogen, Nitrite 0.035 mg/L 05/08/15 00:300.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.47 mg/L 05/08/15 12:000.25 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 8 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-23B Lab ID:92248790005 Collected:05/06/15 14:20 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:09 107-21-15.0 1
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 5.3 mg/L 05/14/15 01:25 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2780 ug/L 05/11/15 23:28 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)95 %05/11/15 23:28 17060-07-050-150 50
Toluene-d8 (S)100 %05/11/15 23:28 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2160 mg/L 05/11/15 22:105.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:350.020 1
Nitrogen, Nitrite 0.16 mg/L 05/08/15 00:350.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 05/08/15 12:000.25 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 9 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-9C Lab ID:92248790006 Collected:05/06/15 18:45 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:19 107-21-15.0 1
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 05/14/15 01:55 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)972 ug/L 05/11/15 23:48 123-91-120.0 10
Surrogates
1,2-Dichloroethane-d4 (S)99 %05/11/15 23:48 17060-07-050-150 10
Toluene-d8 (S)98 %05/11/15 23:48 2037-26-550-150 10
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2500 mg/L 05/11/15 23:015.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:440.020 1
Nitrogen, Nitrite 0.12 mg/L 05/08/15 00:440.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 05/08/15 12:000.25 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 10 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-01 Lab ID:92248790007 Collected:05/07/15 00:00 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:28 107-21-15.0 1
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 3.1 mg/L 05/14/15 02:26 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2890 ug/L 05/12/15 00:08 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)99 %05/12/15 00:08 17060-07-050-150 50
Toluene-d8 (S)98 %05/12/15 00:08 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 1470 mg/L 05/11/15 23:495.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:450.020 1
Nitrogen, Nitrite ND mg/L 05/08/15 00:450.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 1.6 mg/L 05/08/15 12:000.25 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 11 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-10 Lab ID:92248790008 Collected:05/07/15 09:25 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:38 107-21-15.0 1
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 05/14/15 02:57 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Biphenyl (Diphenyl)82.8 ug/L 05/18/15 12:18 92-52-405/11/15 10:4510.0 1
Diphenyl ether (Phenyl ether)1090 ug/L 05/18/15 14:23 101-84-805/11/15 10:4520020
Surrogates
Nitrobenzene-d5 (S)85 %05/18/15 12:18 4165-60-005/11/15 10:4521-110 1
2-Fluorobiphenyl (S)64 %05/18/15 12:18 321-60-805/11/15 10:4527-110 1
Terphenyl-d14 (S)60 %05/18/15 12:18 1718-51-005/11/15 10:4531-107 1
Phenol-d6 (S)27 %05/18/15 12:18 13127-88-305/11/15 10:4510-110 1
2-Fluorophenol (S)36 %05/18/15 12:18 367-12-405/11/15 10:4512-110 1
2,4,6-Tribromophenol (S)83 %05/18/15 12:18 118-79-605/11/15 10:4527-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)511 ug/L 05/12/15 00:29 123-91-120.0 10
Surrogates
1,2-Dichloroethane-d4 (S)94 %05/12/15 00:29 17060-07-050-150 10
Toluene-d8 (S)99 %05/12/15 00:29 2037-26-550-150 10
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 664 mg/L 05/12/15 16:43 M15.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 22:150.020 1
Nitrogen, Nitrite 0.044 mg/L 05/08/15 22:150.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 05/08/15 12:000.25 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 12 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-12 Lab ID:92248790009 Collected:05/06/15 16:40 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 1.3 mg/L 05/14/15 03:27 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Biphenyl (Diphenyl)ND ug/L 05/18/15 12:50 92-52-405/11/15 10:4510.0 1
Diphenyl ether (Phenyl ether)ND ug/L 05/18/15 12:50 101-84-805/11/15 10:4510.0 1
Surrogates
Nitrobenzene-d5 (S)49 %05/18/15 12:50 4165-60-005/11/15 10:4521-110 1
2-Fluorobiphenyl (S)30 %05/18/15 12:50 321-60-805/11/15 10:4527-110 1
Terphenyl-d14 (S)92 %05/18/15 12:50 1718-51-005/11/15 10:4531-107 1
Phenol-d6 (S)10 %05/18/15 12:50 13127-88-305/11/15 10:4510-110 1
2-Fluorophenol (S)15 %05/18/15 12:50 367-12-405/11/15 10:4512-110 1
2,4,6-Tribromophenol (S)48 %05/18/15 12:50 118-79-605/11/15 10:4527-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)3090 ug/L 05/13/15 01:43 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)94 %05/13/15 01:43 17060-07-050-150 50
Toluene-d8 (S)97 %05/13/15 01:43 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 310 mg/L 05/12/15 17:185.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 0.031 mg/L 05/08/15 22:12 H10.020 1
Nitrogen, Nitrite ND mg/L 05/08/15 22:12 H10.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.13 mg/L 05/08/15 12:000.050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
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[phone]
Page 13 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:SW-99 Lab ID:92248790010 Collected:05/06/15 15:40 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:47 107-21-15.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Biphenyl (Diphenyl)ND ug/L 05/18/15 13:21 92-52-405/11/15 10:4510.0 1
Diphenyl ether (Phenyl ether)ND ug/L 05/18/15 13:21 101-84-805/11/15 10:4510.0 1
Surrogates
Nitrobenzene-d5 (S)111 %05/18/15 13:21 4165-60-0 S305/11/15 10:4521-110 1
2-Fluorobiphenyl (S)71 %05/18/15 13:21 321-60-805/11/15 10:4527-110 1
Terphenyl-d14 (S)109 %05/18/15 13:21 1718-51-0 S305/11/15 10:4531-107 1
Phenol-d6 (S)23 %05/18/15 13:21 13127-88-305/11/15 10:4510-110 1
2-Fluorophenol (S)35 %05/18/15 13:21 367-12-405/11/15 10:4512-110 1
2,4,6-Tribromophenol (S)74 %05/18/15 13:21 118-79-605/11/15 10:4527-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 05/19/15 13:26 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %05/19/15 13:26 17060-07-050-150 1
Toluene-d8 (S)83 %05/19/15 13:26 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 14 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:SW-5 Lab ID:92248790011 Collected:05/06/15 15:45 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:57 107-21-15.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Biphenyl (Diphenyl)ND ug/L 05/18/15 13:52 92-52-405/11/15 10:4510.0 1
Diphenyl ether (Phenyl ether)ND ug/L 05/18/15 13:52 101-84-805/11/15 10:4510.0 1
Surrogates
Nitrobenzene-d5 (S)96 %05/18/15 13:52 4165-60-005/11/15 10:4521-110 1
2-Fluorobiphenyl (S)66 %05/18/15 13:52 321-60-805/11/15 10:4527-110 1
Terphenyl-d14 (S)100 %05/18/15 13:52 1718-51-005/11/15 10:4531-107 1
Phenol-d6 (S)22 %05/18/15 13:52 13127-88-305/11/15 10:4510-110 1
2-Fluorophenol (S)35 %05/18/15 13:52 367-12-405/11/15 10:4512-110 1
2,4,6-Tribromophenol (S)66 %05/18/15 13:52 118-79-605/11/15 10:4527-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 05/18/15 16:06 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)118 %05/18/15 16:06 17060-07-050-150 1
Toluene-d8 (S)98 %05/18/15 16:06 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 15 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:CSW-1 Lab ID:92248790012 Collected:05/06/15 17:55 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)82.1 ug/L 05/18/15 16:27 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)122 %05/18/15 16:27 17060-07-050-150 1
Toluene-d8 (S)98 %05/18/15 16:27 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 16 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/15345
EPA 8015 Alcohol-Glycol
EPA 8015 Alcohol-Glycol
EPA 8015 Modified
Associated Lab Samples:92248790004, 92248790005, 92248790006, 92248790007, 92248790008, 92248790010, 92248790011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1297875
Associated Lab Samples:
Matrix:Water
Analyzed
Ethylene glycol mg/L ND 5.0 05/15/15 14:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1297876LABORATORY CONTROL SAMPLE:
LCSSpike
Ethylene glycol mg/L 23.725 95 79-129
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1297878MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
60193253002
1297879
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Ethylene glycol mg/L R1256867-13386 2325ND17.0 21.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 17 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GWD/2113
EPA 9056A
EPA 9056A
9056 IC Anions, GWD
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007,
92248790008, 92248790009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1456652
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007,
92248790008, 92248790009
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 05/13/15 13:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1456653LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 49.850 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1456654MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248844006
1456655
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 103 90-110103 0500.79J 52.5 52.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1456656MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248790009
1456657
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 100 90-110103 2501.3 51.6 52.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 18 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31574
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92248790001, 92248790002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1455613
Associated Lab Samples:92248790001, 92248790002
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 05/11/15 14:53
1,2-Dichloroethane-d4 (S)%102 50-150 05/11/15 14:53
Toluene-d8 (S)%106 50-150 05/11/15 14:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1455614LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 20.920 104 71-125
1,2-Dichloroethane-d4 (S)%100 50-150
Toluene-d8 (S)%107 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1455615MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92249041008
1455616
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 130 50-150128 220ND26.0 25.6
1,2-Dichloroethane-d4 (S)%102 50-150101
Toluene-d8 (S)%103 50-150102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 19 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31575
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92248790003, 92248790004, 92248790005, 92248790006, 92248790007, 92248790008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1455617
Associated Lab Samples:92248790003, 92248790004, 92248790005, 92248790006, 92248790007, 92248790008
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 05/11/15 14:32
1,2-Dichloroethane-d4 (S)%105 50-150 05/11/15 14:32
Toluene-d8 (S)%106 50-150 05/11/15 14:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1455618LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 21.020 105 71-125
1,2-Dichloroethane-d4 (S)%103 50-150
Toluene-d8 (S)%106 50-150
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 20 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31602
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92248790009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1456598
Associated Lab Samples:92248790009
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 05/12/15 15:29
1,2-Dichloroethane-d4 (S)%88 50-150 05/12/15 15:29
Toluene-d8 (S)%100 50-150 05/12/15 15:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1456599LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 22.320 112 71-125
1,2-Dichloroethane-d4 (S)%84 50-150
Toluene-d8 (S)%100 50-150
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 21 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31702
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92248790011, 92248790012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1461633
Associated Lab Samples:92248790011, 92248790012
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 05/18/15 14:22
1,2-Dichloroethane-d4 (S)%110 50-150 05/18/15 14:22
Toluene-d8 (S)%98 50-150 05/18/15 14:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1461634LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 21.320 107 71-125
1,2-Dichloroethane-d4 (S)%104 50-150
Toluene-d8 (S)%99 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1461635MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92249154001
1461636
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 105 50-150108 220ND21.1 21.6
1,2-Dichloroethane-d4 (S)%123 50-150121
Toluene-d8 (S)%99 50-15099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 22 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31719
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92248790010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1462242
Associated Lab Samples:92248790010
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 05/19/15 12:03
1,2-Dichloroethane-d4 (S)%116 50-150 05/19/15 12:03
Toluene-d8 (S)%85 50-150 05/19/15 12:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1462243LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 18.520 92 71-125
1,2-Dichloroethane-d4 (S)%122 50-150
Toluene-d8 (S)%86 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1462244MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92250030001
1462245
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 96 50-15094 120ND19.1 18.9
1,2-Dichloroethane-d4 (S)%130 50-150131
Toluene-d8 (S)%82 50-15082
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 23 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/34967
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92248790008, 92248790009, 92248790010, 92248790011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1455439
Associated Lab Samples:92248790008, 92248790009, 92248790010, 92248790011
Matrix:Water
Analyzed
Biphenyl (Diphenyl)ug/L ND 10.0 05/18/15 12:19
Diphenyl ether (Phenyl ether)ug/L ND 10.0 05/18/15 12:19
2,4,6-Tribromophenol (S)%72 27-110 05/18/15 12:19
2-Fluorobiphenyl (S)%67 27-110 05/18/15 12:19
2-Fluorophenol (S)%37 12-110 05/18/15 12:19
Nitrobenzene-d5 (S)%88 21-110 05/18/15 12:19
Phenol-d6 (S)%25 10-110 05/18/15 12:19
Terphenyl-d14 (S)%103 31-107 05/18/15 12:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1455440LABORATORY CONTROL SAMPLE:
LCSSpike
Biphenyl (Diphenyl)ug/L 36.650 73 38-120
Diphenyl ether (Phenyl ether)ug/L 36.550 73 51-120
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%71 27-110
2-Fluorophenol (S)%41 12-110
Nitrobenzene-d5 (S)%77 21-110
Phenol-d6 (S)%31 10-110
Terphenyl-d14 (S)%103 31-107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 24 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/37367
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1455260
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 05/11/15 16:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1455261LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 49.250 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1455266MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248924001
1455267
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 98 90-11095 25024.1 73.0 71.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1455268MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92249096001
1455269
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M1508690-11079 35069.8 113 109
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 25 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/37392
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92248790008, 92248790009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1456107
Associated Lab Samples:92248790008, 92248790009
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 05/12/15 16:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1456108LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 47.150 94 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1456109MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248790008
1456110
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M15096090-110944 15066411401140
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1456111MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248377003
1456112
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M1,R1508890-11099 55055.4 99.6 105
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 26 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/22841
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1453829
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 05/08/15 00:04
Nitrogen, Nitrite mg/L ND 0.020 05/08/15 00:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1453830LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 2.52.5 101 90-110
Nitrogen, Nitrite mg/L 1.01 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1453833MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248890002
1453834
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 105 90-110104 02.52.7 5.4 5.3
Nitrogen, Nitrite mg/L 1 102 90-110101 11<0.020 1.0 1.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1453843MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248853002
1453844
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L M1,R12.5 40 90-110108 312.53.6 4.6 6.3
Nitrogen, Nitrite mg/L 1 104 90-110103 110.044 1.1 1.1
REPORT OF LABORATORY ANALYSIS
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Page 27 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/22865
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92248790008, 92248790009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1454963
Associated Lab Samples:92248790008, 92248790009
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 05/08/15 22:04
Nitrogen, Nitrite mg/L ND 0.020 05/08/15 22:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1454964LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 2.62.5 103 90-110
Nitrogen, Nitrite mg/L 1.01 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1454965MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248790008
1454966
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 97 90-11097 02.5ND 2.4 2.4
Nitrogen, Nitrite mg/L 1 97 90-11099 210.044 1.0 1.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1454967MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92249027001
1454968
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 103 90-110104 02.51.2 3.7 3.8
Nitrogen, Nitrite mg/L 1 106 90-110105 110.045 1.1 1.1
REPORT OF LABORATORY ANALYSIS
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Page 28 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/22856
SM 4500-P E
SM 4500-P E
SM4500P-E Phosphorus, Ortho
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007,
92248790008, 92248790009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1454040
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007,
92248790008, 92248790009
Matrix:Water
Analyzed
Orthophosphate as P mg/L ND 0.050 05/08/15 12:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1454041LABORATORY CONTROL SAMPLE:
LCSSpike
Orthophosphate as P mg/L 0.25.25 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1454042MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248790001
1454043
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Orthophosphate as P mg/L M1.25 122 90-110122 0.25ND 0.33 0.33
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - GreenwoodPASI-G
Pace Analytical Services - IndianapolisPASI-I
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples.
Results unaffected by high bias.S3
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92248790004 GCSV/15345B-23A EPA 8015 Alcohol-Glycol
92248790005 GCSV/15345B-23B EPA 8015 Alcohol-Glycol
92248790006 GCSV/15345B-9C EPA 8015 Alcohol-Glycol
92248790007 GCSV/15345B-01 EPA 8015 Alcohol-Glycol
92248790008 GCSV/15345B-10 EPA 8015 Alcohol-Glycol
92248790010 GCSV/15345SW-99 EPA 8015 Alcohol-Glycol
92248790011 GCSV/15345SW-5 EPA 8015 Alcohol-Glycol
92248790001 GWD/2113B-24A EPA 9056A
92248790002 GWD/2113B-22B EPA 9056A
92248790003 GWD/2113B-17C EPA 9056A
92248790004 GWD/2113B-23A EPA 9056A
92248790005 GWD/2113B-23B EPA 9056A
92248790006 GWD/2113B-9C EPA 9056A
92248790007 GWD/2113B-01 EPA 9056A
92248790008 GWD/2113B-10 EPA 9056A
92248790009 GWD/2113B-12 EPA 9056A
92248790008 OEXT/34967 MSSV/10681B-10 EPA 3510 EPA 8270
92248790009 OEXT/34967 MSSV/10681B-12 EPA 3510 EPA 8270
92248790010 OEXT/34967 MSSV/10681SW-99 EPA 3510 EPA 8270
92248790011 OEXT/34967 MSSV/10681SW-5 EPA 3510 EPA 8270
92248790001 MSV/31574B-24A EPA 8260B Mod.
92248790002 MSV/31574B-22B EPA 8260B Mod.
92248790003 MSV/31575B-17C EPA 8260B Mod.
92248790004 MSV/31575B-23A EPA 8260B Mod.
92248790005 MSV/31575B-23B EPA 8260B Mod.
92248790006 MSV/31575B-9C EPA 8260B Mod.
92248790007 MSV/31575B-01 EPA 8260B Mod.
92248790008 MSV/31575B-10 EPA 8260B Mod.
92248790009 MSV/31602B-12 EPA 8260B Mod.
92248790010 MSV/31719SW-99 EPA 8260B Mod.
92248790011 MSV/31702SW-5 EPA 8260B Mod.
92248790012 MSV/31702CSW-1 EPA 8260B Mod.
92248790001 WET/37367B-24A SM 2320B
92248790002 WET/37367B-22B SM 2320B
92248790003 WET/37367B-17C SM 2320B
92248790004 WET/37367B-23A SM 2320B
92248790005 WET/37367B-23B SM 2320B
92248790006 WET/37367B-9C SM 2320B
92248790007 WET/37367B-01 SM 2320B
92248790008 WET/37392B-10 SM 2320B
92248790009 WET/37392B-12 SM 2320B
92248790001 WETA/22841B-24A EPA 353.2
92248790002 WETA/22841B-22B EPA 353.2
92248790003 WETA/22841B-17C EPA 353.2
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92248790004 WETA/22841B-23A EPA 353.2
92248790005 WETA/22841B-23B EPA 353.2
92248790006 WETA/22841B-9C EPA 353.2
92248790007 WETA/22841B-01 EPA 353.2
92248790008 WETA/22865B-10 EPA 353.2
92248790009 WETA/22865B-12 EPA 353.2
92248790001 WETA/22856B-24A SM 4500-P E
92248790002 WETA/22856B-22B SM 4500-P E
92248790003 WETA/22856B-17C SM 4500-P E
92248790004 WETA/22856B-23A SM 4500-P E
92248790005 WETA/22856B-23B SM 4500-P E
92248790006 WETA/22856B-9C SM 4500-P E
92248790007 WETA/22856B-01 SM 4500-P E
92248790008 WETA/22856B-10 SM 4500-P E
92248790009 WETA/22856B-12 SM 4500-P E
REPORT OF LABORATORY ANALYSIS
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Page 32 of 34
Page 33 of 34
Page 34 of 34
#=CL#
November 21, 2015
LIMS USE: FR - BRYON DAHLGREN
LIMS OBJECT ID: 92275754
92275754
Project:
Pace Project No.:
RE:
Bryon Dahlgren
AECOM
10 Patewood Drive, Bldg 6
Suite 500
Greenville, SC 29615
CNA/NRLF
Dear Bryon Dahlgren:
Enclosed are the analytical results for sample(s) received by the laboratory on November 11, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 1 of 69
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92275754
CNA/NRLF
Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074
Indiana Certification #: C-49-06Kansas Certification #:E-10177Kentucky UST Certification #: 0042Kentucky WW Certification #:98019Louisiana Certification #: 04076
Ohio VAP Certification #: CL-0065Oklahoma Certification #: 2014-148
Texas Certification #: T104704355-15-9West Virginia Certification #: 330Wisconsin Certification #: 999788130USDA Soil Permit #: P330-10-00128
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
Greenwood Certification IDs
816 Durst Avenue East, Greenwood, SC 29649South Carolina Laboratory ID #: 24562North Carolina Divison of Water Resources Certification
number 25
Florida Certification number E87633Virginia VELAP ID: 460250
Asbestos NVLAP accreditation: 101410-0
REPORT OF LABORATORY ANALYSIS
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Page 2 of 69
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92275754
CNA/NRLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92275754001 B-23A EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CRES
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ABRJ
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275754002 B-23B EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CBPJ
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ABRJ
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275754003 B-22A EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CBPJ
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ABRJ
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275754004 B-22B EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CBPJ
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ABRJ
SM 4500-P E 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92275754
CNA/NRLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 9060A 5 PASI-AMDW
92275754005 B-99B EPA 8270 3 PASI-CBPJ
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
92275754006 SW-7 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 3 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
92275754007 SW-5 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 3 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
92275754008 CSW-2 EPA 8260B Mod.3 PASI-CDLK
92275754009 CSW-1 EPA 8260B Mod.3 PASI-CDLK
92275754010 SW-3 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 3 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
92275754011 SW-8 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 3 PASI-CRES
EPA 8260B Mod.3 PASI-CDLK
92275754012 B-09C EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CBPJ
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ABRJ
SM 4500-P E 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
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Page 4 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-23A Lab ID:92275754001 Collected:11/10/15 10:25 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:03 107-21-1 D350.0 10
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 7.7 mg/L 11/19/15 02:12 14808-79-8 M11.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/16/15 19:53 92-52-411/12/15 15:3910010
Diphenyl ether (Phenyl ether)ND ug/L 11/16/15 19:53 101-84-811/12/15 15:3910010
Surrogates
2-Fluorobiphenyl (S)0 %11/16/15 19:53 321-60-8 D3,S411/12/15 15:3927-110 10
Analytical Method: EPA 82608260 MSV
Acetone 5120 ug/L 11/18/15 17:05 67-64-150020
Benzene ND ug/L 11/18/15 17:05 71-43-210020
Bromochloromethane ND ug/L 11/18/15 17:05 74-97-5 L310020
Bromodichloromethane ND ug/L 11/18/15 17:05 75-27-410020
Bromoform ND ug/L 11/18/15 17:05 75-25-210020
Bromomethane ND ug/L 11/18/15 17:05 74-83-920020
2-Butanone (MEK)483 ug/L 11/18/15 17:05 78-93-320020
Carbon disulfide ND ug/L 11/18/15 17:05 75-15-020020
Carbon tetrachloride ND ug/L 11/18/15 17:05 56-23-510020
Chlorobenzene ND ug/L 11/18/15 17:05 108-90-710020
Chloroethane ND ug/L 11/18/15 17:05 75-00-320020
Chloroform ND ug/L 11/18/15 17:05 67-66-310020
Chloromethane ND ug/L 11/18/15 17:05 74-87-310020
Cyclohexane ND ug/L 11/18/15 17:05 110-82-710020
1,2-Dibromo-3-chloropropane ND ug/L 11/18/15 17:05 96-12-840.0 20
Dibromochloromethane ND ug/L 11/18/15 17:05 124-48-110020
1,2-Dibromoethane (EDB)ND ug/L 11/18/15 17:05 106-93-410020
1,2-Dichlorobenzene ND ug/L 11/18/15 17:05 95-50-110020
1,3-Dichlorobenzene ND ug/L 11/18/15 17:05 541-73-110020
1,4-Dichlorobenzene ND ug/L 11/18/15 17:05 106-46-710020
Dichlorodifluoromethane ND ug/L 11/18/15 17:05 75-71-810020
1,1-Dichloroethane ND ug/L 11/18/15 17:05 75-34-310020
1,2-Dichloroethane ND ug/L 11/18/15 17:05 107-06-210020
1,1-Dichloroethene ND ug/L 11/18/15 17:05 75-35-410020
cis-1,2-Dichloroethene ND ug/L 11/18/15 17:05 156-59-210020
trans-1,2-Dichloroethene ND ug/L 11/18/15 17:05 156-60-510020
1,2-Dichloropropane ND ug/L 11/18/15 17:05 78-87-510020
cis-1,3-Dichloropropene ND ug/L 11/18/15 17:05 10061-01-510020
trans-1,3-Dichloropropene ND ug/L 11/18/15 17:05 10061-02-610020
Ethylbenzene ND ug/L 11/18/15 17:05 100-41-410020
2-Hexanone ND ug/L 11/18/15 17:05 591-78-620020
Isopropylbenzene (Cumene)ND ug/L 11/18/15 17:05 98-82-810020
Methyl acetate ND ug/L 11/18/15 17:05 79-20-920020
Methylcyclohexane ND ug/L 11/18/15 17:05 108-87-220020
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-23A Lab ID:92275754001 Collected:11/10/15 10:25 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Methylene Chloride ND ug/L 11/18/15 17:05 75-09-210020
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/15 17:05 108-10-120020
Methyl-tert-butyl ether ND ug/L 11/18/15 17:05 1634-04-410020
Styrene ND ug/L 11/18/15 17:05 100-42-510020
1,1,2,2-Tetrachloroethane ND ug/L 11/18/15 17:05 79-34-510020
Tetrachloroethene ND ug/L 11/18/15 17:05 127-18-410020
Toluene ND ug/L 11/18/15 17:05 108-88-310020
1,2,3-Trichlorobenzene ND ug/L 11/18/15 17:05 87-61-610020
1,2,4-Trichlorobenzene ND ug/L 11/18/15 17:05 120-82-110020
1,1,1-Trichloroethane ND ug/L 11/18/15 17:05 71-55-610020
1,1,2-Trichloroethane ND ug/L 11/18/15 17:05 79-00-510020
Trichloroethene ND ug/L 11/18/15 17:05 79-01-610020
Trichlorofluoromethane ND ug/L 11/18/15 17:05 75-69-420020
1,1,2-Trichlorotrifluoroethane ND ug/L 11/18/15 17:05 76-13-110020
Vinyl chloride ND ug/L 11/18/15 17:05 75-01-410020
Xylene (Total)ND ug/L 11/18/15 17:05 1330-20-720020
Surrogates
4-Bromofluorobenzene (S)106 %11/18/15 17:05 460-00-470-130 20
1,2-Dichloroethane-d4 (S)99 %11/18/15 17:05 17060-07-070-130 20
Toluene-d8 (S)108 %11/18/15 17:05 2037-26-570-130 20
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)3350 ug/L 11/12/15 18:28 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)105 %11/12/15 18:28 17060-07-050-150 50
Toluene-d8 (S)97 %11/12/15 18:28 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2540 mg/L 11/19/15 10:035.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 07:040.020 1
Nitrogen, Nitrite 0.040 mg/L 11/12/15 07:04 M10.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 1.3 mg/L 11/11/15 22:20 M60.20 4
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 2750 mg/L 11/16/15 17:00 7440-44-0 M6100100
Total Organic Carbon 2690 mg/L 11/16/15 17:00 7440-44-0 M6100100
Total Organic Carbon 2780 mg/L 11/16/15 17:00 7440-44-0 M6100100
Total Organic Carbon 2770 mg/L 11/16/15 17:00 7440-44-0 M6100100
Mean Total Organic Carbon 2750 mg/L 11/16/15 17:00 7440-44-0 M6100100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 6 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-23B Lab ID:92275754002 Collected:11/10/15 11:15 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:13 107-21-1 D350.0 10
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 7.5 mg/L 11/19/15 03:26 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 21:43 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/13/15 21:43 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)69 %11/13/15 21:43 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 82608260 MSV
Acetone 5090 ug/L 11/18/15 17:21 67-64-150020
Benzene ND ug/L 11/18/15 17:21 71-43-210020
Bromochloromethane ND ug/L 11/18/15 17:21 74-97-5 L310020
Bromodichloromethane ND ug/L 11/18/15 17:21 75-27-410020
Bromoform ND ug/L 11/18/15 17:21 75-25-210020
Bromomethane ND ug/L 11/18/15 17:21 74-83-920020
2-Butanone (MEK)488 ug/L 11/18/15 17:21 78-93-320020
Carbon disulfide ND ug/L 11/18/15 17:21 75-15-020020
Carbon tetrachloride ND ug/L 11/18/15 17:21 56-23-510020
Chlorobenzene ND ug/L 11/18/15 17:21 108-90-710020
Chloroethane ND ug/L 11/18/15 17:21 75-00-320020
Chloroform ND ug/L 11/18/15 17:21 67-66-310020
Chloromethane ND ug/L 11/18/15 17:21 74-87-310020
Cyclohexane ND ug/L 11/18/15 17:21 110-82-710020
1,2-Dibromo-3-chloropropane ND ug/L 11/18/15 17:21 96-12-840.0 20
Dibromochloromethane ND ug/L 11/18/15 17:21 124-48-110020
1,2-Dibromoethane (EDB)ND ug/L 11/18/15 17:21 106-93-410020
1,2-Dichlorobenzene ND ug/L 11/18/15 17:21 95-50-110020
1,3-Dichlorobenzene ND ug/L 11/18/15 17:21 541-73-110020
1,4-Dichlorobenzene ND ug/L 11/18/15 17:21 106-46-710020
Dichlorodifluoromethane ND ug/L 11/18/15 17:21 75-71-810020
1,1-Dichloroethane ND ug/L 11/18/15 17:21 75-34-310020
1,2-Dichloroethane ND ug/L 11/18/15 17:21 107-06-210020
1,1-Dichloroethene ND ug/L 11/18/15 17:21 75-35-410020
cis-1,2-Dichloroethene ND ug/L 11/18/15 17:21 156-59-210020
trans-1,2-Dichloroethene ND ug/L 11/18/15 17:21 156-60-510020
1,2-Dichloropropane ND ug/L 11/18/15 17:21 78-87-510020
cis-1,3-Dichloropropene ND ug/L 11/18/15 17:21 10061-01-510020
trans-1,3-Dichloropropene ND ug/L 11/18/15 17:21 10061-02-610020
Ethylbenzene ND ug/L 11/18/15 17:21 100-41-410020
2-Hexanone ND ug/L 11/18/15 17:21 591-78-620020
Isopropylbenzene (Cumene)ND ug/L 11/18/15 17:21 98-82-810020
Methyl acetate ND ug/L 11/18/15 17:21 79-20-920020
Methylcyclohexane ND ug/L 11/18/15 17:21 108-87-220020
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 7 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-23B Lab ID:92275754002 Collected:11/10/15 11:15 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Methylene Chloride ND ug/L 11/18/15 17:21 75-09-210020
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/15 17:21 108-10-120020
Methyl-tert-butyl ether ND ug/L 11/18/15 17:21 1634-04-410020
Styrene ND ug/L 11/18/15 17:21 100-42-510020
1,1,2,2-Tetrachloroethane ND ug/L 11/18/15 17:21 79-34-510020
Tetrachloroethene ND ug/L 11/18/15 17:21 127-18-410020
Toluene ND ug/L 11/18/15 17:21 108-88-310020
1,2,3-Trichlorobenzene ND ug/L 11/18/15 17:21 87-61-610020
1,2,4-Trichlorobenzene ND ug/L 11/18/15 17:21 120-82-110020
1,1,1-Trichloroethane ND ug/L 11/18/15 17:21 71-55-610020
1,1,2-Trichloroethane ND ug/L 11/18/15 17:21 79-00-510020
Trichloroethene ND ug/L 11/18/15 17:21 79-01-610020
Trichlorofluoromethane ND ug/L 11/18/15 17:21 75-69-420020
1,1,2-Trichlorotrifluoroethane ND ug/L 11/18/15 17:21 76-13-110020
Vinyl chloride ND ug/L 11/18/15 17:21 75-01-410020
Xylene (Total)ND ug/L 11/18/15 17:21 1330-20-720020
Surrogates
4-Bromofluorobenzene (S)106 %11/18/15 17:21 460-00-470-130 20
1,2-Dichloroethane-d4 (S)98 %11/18/15 17:21 17060-07-070-130 20
Toluene-d8 (S)108 %11/18/15 17:21 2037-26-570-130 20
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)3330 ug/L 11/12/15 18:49 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)107 %11/12/15 18:49 17060-07-050-150 50
Toluene-d8 (S)99 %11/12/15 18:49 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2250 mg/L 11/19/15 11:055.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 07:100.020 1
Nitrogen, Nitrite 0.12 mg/L 11/12/15 07:100.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.96 mg/L 11/11/15 22:200.20 4
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 2600 mg/L 11/16/15 14:30 7440-44-0100100
Total Organic Carbon 2880 mg/L 11/16/15 14:30 7440-44-0100100
Total Organic Carbon 2890 mg/L 11/16/15 14:30 7440-44-0100100
Total Organic Carbon 2890 mg/L 11/16/15 14:30 7440-44-0100100
Mean Total Organic Carbon 2810 mg/L 11/16/15 14:30 7440-44-0100100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 8 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-22A Lab ID:92275754003 Collected:11/10/15 14:20 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 11/19/15 04:39 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 22:09 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/13/15 22:09 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)73 %11/13/15 22:09 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 82608260 MSV
Acetone ND ug/L 11/18/15 17:38 67-64-125.0 1
Benzene ND ug/L 11/18/15 17:38 71-43-25.0 1
Bromochloromethane ND ug/L 11/18/15 17:38 74-97-5 L35.0 1
Bromodichloromethane ND ug/L 11/18/15 17:38 75-27-45.0 1
Bromoform ND ug/L 11/18/15 17:38 75-25-25.0 1
Bromomethane ND ug/L 11/18/15 17:38 74-83-910.0 1
2-Butanone (MEK)ND ug/L 11/18/15 17:38 78-93-310.0 1
Carbon disulfide ND ug/L 11/18/15 17:38 75-15-010.0 1
Carbon tetrachloride ND ug/L 11/18/15 17:38 56-23-55.0 1
Chlorobenzene 7.5 ug/L 11/18/15 17:38 108-90-75.0 1
Chloroethane ND ug/L 11/18/15 17:38 75-00-3 M110.0 1
Chloroform ND ug/L 11/18/15 17:38 67-66-35.0 1
Chloromethane ND ug/L 11/18/15 17:38 74-87-35.0 1
Cyclohexane ND ug/L 11/18/15 17:38 110-82-75.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/18/15 17:38 96-12-82.0 1
Dibromochloromethane ND ug/L 11/18/15 17:38 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/18/15 17:38 106-93-45.0 1
1,2-Dichlorobenzene ND ug/L 11/18/15 17:38 95-50-15.0 1
1,3-Dichlorobenzene ND ug/L 11/18/15 17:38 541-73-15.0 1
1,4-Dichlorobenzene ND ug/L 11/18/15 17:38 106-46-75.0 1
Dichlorodifluoromethane ND ug/L 11/18/15 17:38 75-71-85.0 1
1,1-Dichloroethane 6.5 ug/L 11/18/15 17:38 75-34-35.0 1
1,2-Dichloroethane ND ug/L 11/18/15 17:38 107-06-25.0 1
1,1-Dichloroethene ND ug/L 11/18/15 17:38 75-35-45.0 1
cis-1,2-Dichloroethene ND ug/L 11/18/15 17:38 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/L 11/18/15 17:38 156-60-55.0 1
1,2-Dichloropropane ND ug/L 11/18/15 17:38 78-87-55.0 1
cis-1,3-Dichloropropene ND ug/L 11/18/15 17:38 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/L 11/18/15 17:38 10061-02-65.0 1
Ethylbenzene ND ug/L 11/18/15 17:38 100-41-45.0 1
2-Hexanone ND ug/L 11/18/15 17:38 591-78-610.0 1
Isopropylbenzene (Cumene)ND ug/L 11/18/15 17:38 98-82-85.0 1
Methyl acetate ND ug/L 11/18/15 17:38 79-20-910.0 1
Methylcyclohexane ND ug/L 11/18/15 17:38 108-87-210.0 1
Methylene Chloride ND ug/L 11/18/15 17:38 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/15 17:38 108-10-110.0 1
Methyl-tert-butyl ether ND ug/L 11/18/15 17:38 1634-04-45.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 9 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-22A Lab ID:92275754003 Collected:11/10/15 14:20 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Styrene ND ug/L 11/18/15 17:38 100-42-55.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/18/15 17:38 79-34-55.0 1
Tetrachloroethene ND ug/L 11/18/15 17:38 127-18-45.0 1
Toluene ND ug/L 11/18/15 17:38 108-88-35.0 1
1,2,3-Trichlorobenzene ND ug/L 11/18/15 17:38 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/L 11/18/15 17:38 120-82-15.0 1
1,1,1-Trichloroethane ND ug/L 11/18/15 17:38 71-55-65.0 1
1,1,2-Trichloroethane ND ug/L 11/18/15 17:38 79-00-55.0 1
Trichloroethene ND ug/L 11/18/15 17:38 79-01-65.0 1
Trichlorofluoromethane ND ug/L 11/18/15 17:38 75-69-410.0 1
1,1,2-Trichlorotrifluoroethane ND ug/L 11/18/15 17:38 76-13-15.0 1
Vinyl chloride ND ug/L 11/18/15 17:38 75-01-45.0 1
Xylene (Total)ND ug/L 11/18/15 17:38 1330-20-710.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/18/15 17:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %11/18/15 17:38 17060-07-070-130 1
Toluene-d8 (S)109 %11/18/15 17:38 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)1690 ug/L 11/12/15 19:09 123-91-150.0 25
Surrogates
1,2-Dichloroethane-d4 (S)103 %11/12/15 19:09 17060-07-050-150 25
Toluene-d8 (S)97 %11/12/15 19:09 2037-26-550-150 25
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 544 mg/L 11/18/15 18:195.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 07:110.020 1
Nitrogen, Nitrite 0.050 mg/L 11/12/15 07:110.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 11/11/15 22:200.25 5
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 5.0 mg/L 11/16/15 17:24 7440-44-05.0 5
Total Organic Carbon 5.5 mg/L 11/16/15 17:24 7440-44-05.0 5
Total Organic Carbon 5.2 mg/L 11/16/15 17:24 7440-44-05.0 5
Total Organic Carbon 5.3 mg/L 11/16/15 17:24 7440-44-05.0 5
Mean Total Organic Carbon 5.2 mg/L 11/16/15 17:24 7440-44-05.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 10 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-22B Lab ID:92275754004 Collected:11/10/15 15:05 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 11/19/15 05:03 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 22:34 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)11.7 ug/L 11/13/15 22:34 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)43 %11/13/15 22:34 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 82608260 MSV
Acetone ND ug/L 11/18/15 17:55 67-64-125.0 1
Benzene ND ug/L 11/18/15 17:55 71-43-25.0 1
Bromochloromethane ND ug/L 11/18/15 17:55 74-97-5 L35.0 1
Bromodichloromethane ND ug/L 11/18/15 17:55 75-27-45.0 1
Bromoform ND ug/L 11/18/15 17:55 75-25-25.0 1
Bromomethane ND ug/L 11/18/15 17:55 74-83-910.0 1
2-Butanone (MEK)ND ug/L 11/18/15 17:55 78-93-310.0 1
Carbon disulfide ND ug/L 11/18/15 17:55 75-15-010.0 1
Carbon tetrachloride ND ug/L 11/18/15 17:55 56-23-55.0 1
Chlorobenzene 8.9 ug/L 11/18/15 17:55 108-90-75.0 1
Chloroethane 11.8 ug/L 11/18/15 17:55 75-00-310.0 1
Chloroform ND ug/L 11/18/15 17:55 67-66-35.0 1
Chloromethane ND ug/L 11/18/15 17:55 74-87-35.0 1
Cyclohexane ND ug/L 11/18/15 17:55 110-82-75.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/18/15 17:55 96-12-82.0 1
Dibromochloromethane ND ug/L 11/18/15 17:55 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/18/15 17:55 106-93-45.0 1
1,2-Dichlorobenzene ND ug/L 11/18/15 17:55 95-50-15.0 1
1,3-Dichlorobenzene ND ug/L 11/18/15 17:55 541-73-15.0 1
1,4-Dichlorobenzene ND ug/L 11/18/15 17:55 106-46-75.0 1
Dichlorodifluoromethane ND ug/L 11/18/15 17:55 75-71-85.0 1
1,1-Dichloroethane ND ug/L 11/18/15 17:55 75-34-35.0 1
1,2-Dichloroethane ND ug/L 11/18/15 17:55 107-06-25.0 1
1,1-Dichloroethene ND ug/L 11/18/15 17:55 75-35-45.0 1
cis-1,2-Dichloroethene ND ug/L 11/18/15 17:55 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/L 11/18/15 17:55 156-60-55.0 1
1,2-Dichloropropane ND ug/L 11/18/15 17:55 78-87-55.0 1
cis-1,3-Dichloropropene ND ug/L 11/18/15 17:55 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/L 11/18/15 17:55 10061-02-65.0 1
Ethylbenzene ND ug/L 11/18/15 17:55 100-41-45.0 1
2-Hexanone ND ug/L 11/18/15 17:55 591-78-610.0 1
Isopropylbenzene (Cumene)ND ug/L 11/18/15 17:55 98-82-85.0 1
Methyl acetate ND ug/L 11/18/15 17:55 79-20-910.0 1
Methylcyclohexane ND ug/L 11/18/15 17:55 108-87-210.0 1
Methylene Chloride ND ug/L 11/18/15 17:55 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/15 17:55 108-10-110.0 1
Methyl-tert-butyl ether ND ug/L 11/18/15 17:55 1634-04-45.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 11 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-22B Lab ID:92275754004 Collected:11/10/15 15:05 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Styrene ND ug/L 11/18/15 17:55 100-42-55.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/18/15 17:55 79-34-55.0 1
Tetrachloroethene ND ug/L 11/18/15 17:55 127-18-45.0 1
Toluene ND ug/L 11/18/15 17:55 108-88-35.0 1
1,2,3-Trichlorobenzene ND ug/L 11/18/15 17:55 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/L 11/18/15 17:55 120-82-15.0 1
1,1,1-Trichloroethane ND ug/L 11/18/15 17:55 71-55-65.0 1
1,1,2-Trichloroethane ND ug/L 11/18/15 17:55 79-00-55.0 1
Trichloroethene ND ug/L 11/18/15 17:55 79-01-65.0 1
Trichlorofluoromethane ND ug/L 11/18/15 17:55 75-69-410.0 1
1,1,2-Trichlorotrifluoroethane ND ug/L 11/18/15 17:55 76-13-15.0 1
Vinyl chloride ND ug/L 11/18/15 17:55 75-01-45.0 1
Xylene (Total)ND ug/L 11/18/15 17:55 1330-20-710.0 1
Surrogates
4-Bromofluorobenzene (S)105 %11/18/15 17:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/18/15 17:55 17060-07-070-130 1
Toluene-d8 (S)108 %11/18/15 17:55 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)1720 ug/L 11/12/15 19:29 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)103 %11/12/15 19:29 17060-07-050-150 50
Toluene-d8 (S)98 %11/12/15 19:29 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 724 mg/L 11/18/15 18:455.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 07:150.020 1
Nitrogen, Nitrite ND mg/L 11/12/15 07:150.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.38 mg/L 11/11/15 22:200.050 1
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 6.6 mg/L 11/16/15 17:55 7440-44-05.0 5
Total Organic Carbon 6.6 mg/L 11/16/15 17:55 7440-44-05.0 5
Total Organic Carbon 6.7 mg/L 11/16/15 17:55 7440-44-05.0 5
Total Organic Carbon 6.5 mg/L 11/16/15 17:55 7440-44-05.0 5
Mean Total Organic Carbon 6.6 mg/L 11/16/15 17:55 7440-44-05.0 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
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[phone]
Page 12 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-99B Lab ID:92275754005 Collected:11/10/15 15:10 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 23:00 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)10.3 ug/L 11/13/15 23:00 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)61 %11/13/15 23:00 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 82608260 MSV
Acetone ND ug/L 11/18/15 18:29 67-64-125.0 1
Benzene ND ug/L 11/18/15 18:29 71-43-25.0 1
Bromochloromethane ND ug/L 11/18/15 18:29 74-97-5 L35.0 1
Bromodichloromethane ND ug/L 11/18/15 18:29 75-27-45.0 1
Bromoform ND ug/L 11/18/15 18:29 75-25-25.0 1
Bromomethane ND ug/L 11/18/15 18:29 74-83-910.0 1
2-Butanone (MEK)ND ug/L 11/18/15 18:29 78-93-310.0 1
Carbon disulfide ND ug/L 11/18/15 18:29 75-15-010.0 1
Carbon tetrachloride ND ug/L 11/18/15 18:29 56-23-55.0 1
Chlorobenzene 8.7 ug/L 11/18/15 18:29 108-90-75.0 1
Chloroethane 10.3 ug/L 11/18/15 18:29 75-00-310.0 1
Chloroform ND ug/L 11/18/15 18:29 67-66-35.0 1
Chloromethane ND ug/L 11/18/15 18:29 74-87-35.0 1
Cyclohexane ND ug/L 11/18/15 18:29 110-82-75.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/18/15 18:29 96-12-82.0 1
Dibromochloromethane ND ug/L 11/18/15 18:29 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/18/15 18:29 106-93-45.0 1
1,2-Dichlorobenzene ND ug/L 11/18/15 18:29 95-50-15.0 1
1,3-Dichlorobenzene ND ug/L 11/18/15 18:29 541-73-15.0 1
1,4-Dichlorobenzene ND ug/L 11/18/15 18:29 106-46-75.0 1
Dichlorodifluoromethane ND ug/L 11/18/15 18:29 75-71-85.0 1
1,1-Dichloroethane ND ug/L 11/18/15 18:29 75-34-35.0 1
1,2-Dichloroethane ND ug/L 11/18/15 18:29 107-06-25.0 1
1,1-Dichloroethene ND ug/L 11/18/15 18:29 75-35-45.0 1
cis-1,2-Dichloroethene ND ug/L 11/18/15 18:29 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/L 11/18/15 18:29 156-60-55.0 1
1,2-Dichloropropane ND ug/L 11/18/15 18:29 78-87-55.0 1
cis-1,3-Dichloropropene ND ug/L 11/18/15 18:29 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/L 11/18/15 18:29 10061-02-65.0 1
Ethylbenzene ND ug/L 11/18/15 18:29 100-41-45.0 1
2-Hexanone ND ug/L 11/18/15 18:29 591-78-610.0 1
Isopropylbenzene (Cumene)ND ug/L 11/18/15 18:29 98-82-85.0 1
Methyl acetate ND ug/L 11/18/15 18:29 79-20-910.0 1
Methylcyclohexane ND ug/L 11/18/15 18:29 108-87-210.0 1
Methylene Chloride ND ug/L 11/18/15 18:29 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/15 18:29 108-10-110.0 1
Methyl-tert-butyl ether ND ug/L 11/18/15 18:29 1634-04-45.0 1
Styrene ND ug/L 11/18/15 18:29 100-42-55.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/18/15 18:29 79-34-55.0 1
Tetrachloroethene ND ug/L 11/18/15 18:29 127-18-45.0 1
Toluene ND ug/L 11/18/15 18:29 108-88-35.0 1
REPORT OF LABORATORY ANALYSIS
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Page 13 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-99B Lab ID:92275754005 Collected:11/10/15 15:10 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
1,2,3-Trichlorobenzene ND ug/L 11/18/15 18:29 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/L 11/18/15 18:29 120-82-15.0 1
1,1,1-Trichloroethane ND ug/L 11/18/15 18:29 71-55-65.0 1
1,1,2-Trichloroethane ND ug/L 11/18/15 18:29 79-00-55.0 1
Trichloroethene ND ug/L 11/18/15 18:29 79-01-65.0 1
Trichlorofluoromethane ND ug/L 11/18/15 18:29 75-69-410.0 1
1,1,2-Trichlorotrifluoroethane ND ug/L 11/18/15 18:29 76-13-15.0 1
Vinyl chloride ND ug/L 11/18/15 18:29 75-01-45.0 1
Xylene (Total)ND ug/L 11/18/15 18:29 1330-20-710.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/18/15 18:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/18/15 18:29 17060-07-070-130 1
Toluene-d8 (S)107 %11/18/15 18:29 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)1610 ug/L 11/12/15 19:49 123-91-150.0 25
Surrogates
1,2-Dichloroethane-d4 (S)102 %11/12/15 19:49 17060-07-050-150 25
Toluene-d8 (S)98 %11/12/15 19:49 2037-26-550-150 25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 14 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:SW-7 Lab ID:92275754006 Collected:11/10/15 13:10 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:32 107-21-1 D350.0 10
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 23:26 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/13/15 23:26 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)72 %11/13/15 23:26 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/12/15 20:09 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %11/12/15 20:09 17060-07-050-150 1
Toluene-d8 (S)97 %11/12/15 20:09 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 15 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:SW-5 Lab ID:92275754007 Collected:11/10/15 15:45 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:41 107-21-1 D350.0 10
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 23:52 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/13/15 23:52 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)48 %11/13/15 23:52 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/12/15 21:10 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %11/12/15 21:10 17060-07-050-150 1
Toluene-d8 (S)99 %11/12/15 21:10 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
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Page 16 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:CSW-2 Lab ID:92275754008 Collected:11/10/15 15:55 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)12.4 ug/L 11/12/15 21:30 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %11/12/15 21:30 17060-07-050-150 1
Toluene-d8 (S)96 %11/12/15 21:30 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 17 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:CSW-1 Lab ID:92275754009 Collected:11/10/15 16:05 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)14.0 ug/L 11/12/15 21:51 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %11/12/15 21:51 17060-07-050-150 1
Toluene-d8 (S)97 %11/12/15 21:51 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 18 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:SW-3 Lab ID:92275754010 Collected:11/10/15 16:20 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:53 107-21-1 D350.0 10
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/14/15 00:18 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/14/15 00:18 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)76 %11/14/15 00:18 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/12/15 22:11 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %11/12/15 22:11 17060-07-050-150 1
Toluene-d8 (S)97 %11/12/15 22:11 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 19 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:SW-8 Lab ID:92275754011 Collected:11/10/15 16:45 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 14:02 107-21-1 D350.0 10
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/18/15 13:50 92-52-411/17/15 09:3010.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/18/15 13:50 101-84-811/17/15 09:3010.0 1
Surrogates
2-Fluorobiphenyl (S)64 %11/18/15 13:50 321-60-811/17/15 09:3027-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/12/15 22:31 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %11/12/15 22:31 17060-07-050-150 1
Toluene-d8 (S)97 %11/12/15 22:31 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 20 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-09C Lab ID:92275754012 Collected:11/10/15 17:35 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:22 107-21-1 D3500100
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 11/19/15 05:28 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/14/15 00:43 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)10.6 ug/L 11/14/15 00:43 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)82 %11/14/15 00:43 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 82608260 MSV
Acetone 2660 ug/L 11/17/15 19:18 67-64-150020
Benzene ND ug/L 11/17/15 19:18 71-43-210020
Bromochloromethane ND ug/L 11/17/15 19:18 74-97-510020
Bromodichloromethane ND ug/L 11/17/15 19:18 75-27-410020
Bromoform ND ug/L 11/17/15 19:18 75-25-210020
Bromomethane ND ug/L 11/17/15 19:18 74-83-920020
2-Butanone (MEK)256 ug/L 11/17/15 19:18 78-93-320020
Carbon disulfide ND ug/L 11/17/15 19:18 75-15-020020
Carbon tetrachloride ND ug/L 11/17/15 19:18 56-23-510020
Chlorobenzene ND ug/L 11/17/15 19:18 108-90-710020
Chloroethane ND ug/L 11/17/15 19:18 75-00-320020
Chloroform ND ug/L 11/17/15 19:18 67-66-310020
Chloromethane ND ug/L 11/17/15 19:18 74-87-310020
Cyclohexane ND ug/L 11/17/15 19:18 110-82-710020
1,2-Dibromo-3-chloropropane ND ug/L 11/17/15 19:18 96-12-840.0 20
Dibromochloromethane ND ug/L 11/17/15 19:18 124-48-110020
1,2-Dibromoethane (EDB)ND ug/L 11/17/15 19:18 106-93-410020
1,2-Dichlorobenzene ND ug/L 11/17/15 19:18 95-50-110020
1,3-Dichlorobenzene ND ug/L 11/17/15 19:18 541-73-110020
1,4-Dichlorobenzene ND ug/L 11/17/15 19:18 106-46-710020
Dichlorodifluoromethane ND ug/L 11/17/15 19:18 75-71-810020
1,1-Dichloroethane ND ug/L 11/17/15 19:18 75-34-310020
1,2-Dichloroethane ND ug/L 11/17/15 19:18 107-06-210020
1,1-Dichloroethene ND ug/L 11/17/15 19:18 75-35-410020
cis-1,2-Dichloroethene ND ug/L 11/17/15 19:18 156-59-210020
trans-1,2-Dichloroethene ND ug/L 11/17/15 19:18 156-60-510020
1,2-Dichloropropane ND ug/L 11/17/15 19:18 78-87-510020
cis-1,3-Dichloropropene ND ug/L 11/17/15 19:18 10061-01-510020
trans-1,3-Dichloropropene ND ug/L 11/17/15 19:18 10061-02-610020
Ethylbenzene ND ug/L 11/17/15 19:18 100-41-410020
2-Hexanone ND ug/L 11/17/15 19:18 591-78-620020
Isopropylbenzene (Cumene)ND ug/L 11/17/15 19:18 98-82-810020
Methyl acetate ND ug/L 11/17/15 19:18 79-20-920020
Methylcyclohexane ND ug/L 11/17/15 19:18 108-87-220020
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
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Page 21 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-09C Lab ID:92275754012 Collected:11/10/15 17:35 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Methylene Chloride ND ug/L 11/17/15 19:18 75-09-210020
4-Methyl-2-pentanone (MIBK)ND ug/L 11/17/15 19:18 108-10-120020
Methyl-tert-butyl ether ND ug/L 11/17/15 19:18 1634-04-410020
Styrene ND ug/L 11/17/15 19:18 100-42-510020
1,1,2,2-Tetrachloroethane ND ug/L 11/17/15 19:18 79-34-510020
Tetrachloroethene ND ug/L 11/17/15 19:18 127-18-410020
Toluene ND ug/L 11/17/15 19:18 108-88-310020
1,2,3-Trichlorobenzene ND ug/L 11/17/15 19:18 87-61-610020
1,2,4-Trichlorobenzene ND ug/L 11/17/15 19:18 120-82-110020
1,1,1-Trichloroethane ND ug/L 11/17/15 19:18 71-55-610020
1,1,2-Trichloroethane ND ug/L 11/17/15 19:18 79-00-510020
Trichloroethene ND ug/L 11/17/15 19:18 79-01-610020
Trichlorofluoromethane ND ug/L 11/17/15 19:18 75-69-420020
1,1,2-Trichlorotrifluoroethane ND ug/L 11/17/15 19:18 76-13-110020
Vinyl chloride ND ug/L 11/17/15 19:18 75-01-410020
Xylene (Total)ND ug/L 11/17/15 19:18 1330-20-720020
Surrogates
4-Bromofluorobenzene (S)100 %11/17/15 19:18 460-00-470-130 20
1,2-Dichloroethane-d4 (S)100 %11/17/15 19:18 17060-07-070-130 20
Toluene-d8 (S)101 %11/17/15 19:18 2037-26-570-130 20
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)909 ug/L 11/12/15 22:51 123-91-120.0 10
Surrogates
1,2-Dichloroethane-d4 (S)108 %11/12/15 22:51 17060-07-050-150 10
Toluene-d8 (S)96 %11/12/15 22:51 2037-26-550-150 10
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2260 mg/L 11/19/15 12:045.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 07:160.020 1
Nitrogen, Nitrite 0.073 mg/L 11/12/15 07:160.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.32 mg/L 11/11/15 22:200.25 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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Page 22 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/17520
EPA 8015 Alcohol-Glycol
EPA 8015 Alcohol-Glycol
EPA 8015 Modified
Associated Lab Samples:92275754001, 92275754002, 92275754006, 92275754007, 92275754010, 92275754011, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1426234
Associated Lab Samples:
Matrix:Water
Analyzed
Ethylene glycol mg/L ND 5.0 11/17/15 12:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1426235LABORATORY CONTROL SAMPLE:
LCSSpike
Ethylene glycol mg/L 22.425 89 79-129
REPORT OF LABORATORY ANALYSIS
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816 Durst Avenue East
Greenwood, SC 29649
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Page 23 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GWD/2671
EPA 9056A
EPA 9056A
9056 IC Anions, GWD
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609962
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 11/19/15 01:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609963LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 48.850 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1609964MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754001
1609965
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L M1507990-11082 3507.7 47.3 48.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 24 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34316
EPA 8260
EPA 8260
8260 MSV
Associated Lab Samples:92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608047
Associated Lab Samples:92275754012
Matrix:Water
Analyzed
1,1,1-Trichloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2,2-Tetrachloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2-Trichloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2-Trichlorotrifluoroethane ug/L ND 5.0 11/17/15 14:29
1,1-Dichloroethane ug/L ND 5.0 11/17/15 14:29
1,1-Dichloroethene ug/L ND 5.0 11/17/15 14:29
1,2,3-Trichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2,4-Trichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/17/15 14:29
1,2-Dibromoethane (EDB)ug/L ND 5.0 11/17/15 14:29
1,2-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2-Dichloroethane ug/L ND 5.0 11/17/15 14:29
1,2-Dichloropropane ug/L ND 5.0 11/17/15 14:29
1,3-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,4-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
2-Butanone (MEK)ug/L ND 10.0 11/17/15 14:29
2-Hexanone ug/L ND 10.0 11/17/15 14:29
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 11/17/15 14:29
Acetone ug/L ND 25.0 11/17/15 14:29
Benzene ug/L ND 5.0 11/17/15 14:29
Bromochloromethane ug/L ND 5.0 11/17/15 14:29
Bromodichloromethane ug/L ND 5.0 11/17/15 14:29
Bromoform ug/L ND 5.0 11/17/15 14:29
Bromomethane ug/L ND 10.0 11/17/15 14:29
Carbon disulfide ug/L ND 10.0 11/17/15 14:29
Carbon tetrachloride ug/L ND 5.0 11/17/15 14:29
Chlorobenzene ug/L ND 5.0 11/17/15 14:29
Chloroethane ug/L ND 10.0 11/17/15 14:29
Chloroform ug/L ND 5.0 11/17/15 14:29
Chloromethane ug/L ND 5.0 11/17/15 14:29
cis-1,2-Dichloroethene ug/L ND 5.0 11/17/15 14:29
cis-1,3-Dichloropropene ug/L ND 5.0 11/17/15 14:29
Cyclohexane ug/L ND 5.0 11/17/15 14:29
Dibromochloromethane ug/L ND 5.0 11/17/15 14:29
Dichlorodifluoromethane ug/L ND 5.0 11/17/15 14:29
Ethylbenzene ug/L ND 5.0 11/17/15 14:29
Isopropylbenzene (Cumene)ug/L ND 5.0 11/17/15 14:29
Methyl acetate ug/L ND 10.0 11/17/15 14:29
Methyl-tert-butyl ether ug/L ND 5.0 11/17/15 14:29
Methylcyclohexane ug/L ND 10.0 11/17/15 14:29
Methylene Chloride ug/L ND 5.0 11/17/15 14:29
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 25 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608047
Associated Lab Samples:92275754012
Matrix:Water
Analyzed
Styrene ug/L ND 5.0 11/17/15 14:29
Tetrachloroethene ug/L ND 5.0 11/17/15 14:29
Toluene ug/L ND 5.0 11/17/15 14:29
trans-1,2-Dichloroethene ug/L ND 5.0 11/17/15 14:29
trans-1,3-Dichloropropene ug/L ND 5.0 11/17/15 14:29
Trichloroethene ug/L ND 5.0 11/17/15 14:29
Trichlorofluoromethane ug/L ND 10.0 11/17/15 14:29
Vinyl chloride ug/L ND 5.0 11/17/15 14:29
Xylene (Total)ug/L ND 10.0 11/17/15 14:29
1,2-Dichloroethane-d4 (S)%99 70-130 11/17/15 14:29
4-Bromofluorobenzene (S)%100 70-130 11/17/15 14:29
Toluene-d8 (S)%102 70-130 11/17/15 14:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608048LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 44.950 90 71-129
1,1,2,2-Tetrachloroethane ug/L 47.250 94 79-124
1,1,2-Trichloroethane ug/L 44.450 89 85-125
1,1,2-Trichlorotrifluoroethane ug/L 47.950 96 71-142
1,1-Dichloroethane ug/L 43.150 86 73-126
1,1-Dichloroethene ug/L 48.550 97 66-135
1,2,3-Trichlorobenzene ug/L 49.750 99 73-135
1,2,4-Trichlorobenzene ug/L 48.150 96 75-134
1,2-Dibromo-3-chloropropane ug/L 48.750 97 71-133
1,2-Dibromoethane (EDB)ug/L 53.050 106 83-124
1,2-Dichlorobenzene ug/L 50.450 101 80-133
1,2-Dichloroethane ug/L 47.450 95 67-128
1,2-Dichloropropane ug/L 46.250 92 75-132
1,3-Dichlorobenzene ug/L 50.450 101 77-130
1,4-Dichlorobenzene ug/L 49.450 99 78-130
2-Butanone (MEK)ug/L 98.2100 98 61-144
2-Hexanone ug/L 98.2100 98 68-143
4-Methyl-2-pentanone (MIBK)ug/L 90.9100 91 72-135
Acetone ug/L 89.8100 90 48-146
Benzene ug/L 48.150 96 80-125
Bromochloromethane ug/L 57.150 114 71-125
Bromodichloromethane ug/L 44.550 89 78-124
Bromoform ug/L 47.150 94 71-128
Bromomethane ug/L 53.950 108 40-160
Carbon disulfide ug/L 47.650 95 50-160
Carbon tetrachloride ug/L 46.850 94 69-131
Chlorobenzene ug/L 47.850 96 81-122
Chloroethane ug/L 50.550 101 39-148
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 26 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608048LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroform ug/L 50.150 100 73-127
Chloromethane ug/L 49.050 98 44-146
cis-1,2-Dichloroethene ug/L 50.450 101 74-124
cis-1,3-Dichloropropene ug/L 48.050 96 72-132
Cyclohexane ug/L 47.550 95 62-145
Dibromochloromethane ug/L 51.550 103 78-125
Dichlorodifluoromethane ug/L 51.350 103 34-157
Ethylbenzene ug/L 48.050 96 79-121
Isopropylbenzene (Cumene)ug/L 53.050 106 81-132
Methyl acetate ug/L 59.150 118 58-128
Methyl-tert-butyl ether ug/L 50.650 101 74-131
Methylcyclohexane ug/L 47.550 95 65-144
Methylene Chloride ug/L 50.150 100 64-133
Styrene ug/L 49.950 100 84-126
Tetrachloroethene ug/L 49.850 100 78-122
Toluene ug/L 42.050 84 80-121
trans-1,2-Dichloroethene ug/L 46.750 93 71-127
trans-1,3-Dichloropropene ug/L 46.950 94 69-141
Trichloroethene ug/L 45.950 92 78-122
Trichlorofluoromethane ug/L 47.550 95 53-137
Vinyl chloride ug/L 50.150 100 58-137
Xylene (Total)ug/L 146150 97 81-126
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%93 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1608049MATRIX SPIKE SAMPLE:
MSSpike
Result
92275933004
1,1,1-Trichloroethane ug/L 18.120 90 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.820 99 70-130ND
1,1,2-Trichloroethane ug/L 16.720 84 70-130ND
1,1,2-Trichlorotrifluoroethane ug/L 17.720 89 70-130ND
1,1-Dichloroethane ug/L 17.220 86 70-130ND
1,1-Dichloroethene ug/L 18.620 93 65-160ND
1,2,3-Trichlorobenzene ug/L 19.220 96 70-130ND
1,2,4-Trichlorobenzene ug/L 18.820 94 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.220 106 60-139ND
1,2-Dichlorobenzene ug/L 21.120 106 70-130ND
1,2-Dichloroethane ug/L 16.420 82 70-130ND
1,2-Dichloropropane ug/L 18.120 91 70-130ND
1,3-Dichlorobenzene ug/L 21.420 107 70-130ND
1,4-Dichlorobenzene ug/L 20.920 104 70-130ND
2-Butanone (MEK)ug/L 35.040 88 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 27 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1608049MATRIX SPIKE SAMPLE:
MSSpike
Result
92275933004
2-Hexanone ug/L 40.640 101 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 34.640 87 70-130ND
Acetone ug/L 37.4 M1404670-13019.1J
Benzene ug/L 22.920 96 58-1623.8J
Bromochloromethane ug/L 18.620 93 70-130ND
Bromodichloromethane ug/L 17.920 89 70-130ND
Bromoform ug/L 16.320 81 70-130ND
Bromomethane ug/L 12.3 M1206170-130ND
Carbon disulfide ug/L 17.220 86 70-130ND
Carbon tetrachloride ug/L 19.220 96 70-130ND
Chlorobenzene ug/L 21.520 107 70-138ND
Chloroethane ug/L 16.220 81 70-130ND
Chloroform ug/L 18.320 92 70-130ND
Chloromethane ug/L 18.220 91 70-130ND
cis-1,2-Dichloroethene ug/L 17.920 89 70-130ND
cis-1,3-Dichloropropene ug/L 17.320 86 70-130ND
Cyclohexane ug/L 19.620 86 70-1302.4J
Dibromochloromethane ug/L 19.620 98 70-130ND
Dichlorodifluoromethane ug/L 17.520 88 70-130ND
Ethylbenzene ug/L 20.920 100 22-189ND
Isopropylbenzene (Cumene)ug/L 27.820 105 70-1306.8
Methyl acetate ug/L 16.120 81 70-130ND
Methyl-tert-butyl ether ug/L 18.120 86 37-169ND
Methylcyclohexane ug/L 18.420 83 70-130ND
Methylene Chloride ug/L 15.620 78 70-130ND
Styrene ug/L 20.720 104 70-130ND
Tetrachloroethene ug/L 21.420 107 70-130ND
Toluene ug/L 17.020 85 65-152ND
trans-1,2-Dichloroethene ug/L 17.720 89 70-130ND
trans-1,3-Dichloropropene ug/L 16.820 84 70-130ND
Trichloroethene ug/L 17.620 88 70-142ND
Trichlorofluoromethane ug/L 18.520 92 70-130ND
Vinyl chloride ug/L 18.420 92 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1,2-Trichlorotrifluoroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 28 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
1,1-Dichloroethene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L ND22.5J
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Cyclohexane ug/L NDND
Dibromochloromethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Isopropylbenzene (Cumene)ug/L NDND
Methyl acetate ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylcyclohexane ug/L NDND
Methylene Chloride ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%99 199
4-Bromofluorobenzene (S)%99 297
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 29 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
Toluene-d8 (S)%103 1103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 30 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34335
EPA 8260
EPA 8260
8260 MSV
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609255
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005
Matrix:Water
Analyzed
1,1,1-Trichloroethane ug/L ND 5.0 11/18/15 16:13
1,1,2,2-Tetrachloroethane ug/L ND 5.0 11/18/15 16:13
1,1,2-Trichloroethane ug/L ND 5.0 11/18/15 16:13
1,1,2-Trichlorotrifluoroethane ug/L ND 5.0 11/18/15 16:13
1,1-Dichloroethane ug/L ND 5.0 11/18/15 16:13
1,1-Dichloroethene ug/L ND 5.0 11/18/15 16:13
1,2,3-Trichlorobenzene ug/L ND 5.0 11/18/15 16:13
1,2,4-Trichlorobenzene ug/L ND 5.0 11/18/15 16:13
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/18/15 16:13
1,2-Dibromoethane (EDB)ug/L ND 5.0 11/18/15 16:13
1,2-Dichlorobenzene ug/L ND 5.0 11/18/15 16:13
1,2-Dichloroethane ug/L ND 5.0 11/18/15 16:13
1,2-Dichloropropane ug/L ND 5.0 11/18/15 16:13
1,3-Dichlorobenzene ug/L ND 5.0 11/18/15 16:13
1,4-Dichlorobenzene ug/L ND 5.0 11/18/15 16:13
2-Butanone (MEK)ug/L ND 10.0 11/18/15 16:13
2-Hexanone ug/L ND 10.0 11/18/15 16:13
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 11/18/15 16:13
Acetone ug/L ND 25.0 11/18/15 16:13
Benzene ug/L ND 5.0 11/18/15 16:13
Bromochloromethane ug/L ND 5.0 11/18/15 16:13
Bromodichloromethane ug/L ND 5.0 11/18/15 16:13
Bromoform ug/L ND 5.0 11/18/15 16:13
Bromomethane ug/L ND 10.0 11/18/15 16:13
Carbon disulfide ug/L ND 10.0 11/18/15 16:13
Carbon tetrachloride ug/L ND 5.0 11/18/15 16:13
Chlorobenzene ug/L ND 5.0 11/18/15 16:13
Chloroethane ug/L ND 10.0 11/18/15 16:13
Chloroform ug/L ND 5.0 11/18/15 16:13
Chloromethane ug/L ND 5.0 11/18/15 16:13
cis-1,2-Dichloroethene ug/L ND 5.0 11/18/15 16:13
cis-1,3-Dichloropropene ug/L ND 5.0 11/18/15 16:13
Cyclohexane ug/L ND 5.0 11/18/15 16:13
Dibromochloromethane ug/L ND 5.0 11/18/15 16:13
Dichlorodifluoromethane ug/L ND 5.0 11/18/15 16:13
Ethylbenzene ug/L ND 5.0 11/18/15 16:13
Isopropylbenzene (Cumene)ug/L ND 5.0 11/18/15 16:13
Methyl acetate ug/L ND 10.0 11/18/15 16:13
Methyl-tert-butyl ether ug/L ND 5.0 11/18/15 16:13
Methylcyclohexane ug/L ND 10.0 11/18/15 16:13
Methylene Chloride ug/L ND 5.0 11/18/15 16:13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 31 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609255
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005
Matrix:Water
Analyzed
Styrene ug/L ND 5.0 11/18/15 16:13
Tetrachloroethene ug/L ND 5.0 11/18/15 16:13
Toluene ug/L ND 5.0 11/18/15 16:13
trans-1,2-Dichloroethene ug/L ND 5.0 11/18/15 16:13
trans-1,3-Dichloropropene ug/L ND 5.0 11/18/15 16:13
Trichloroethene ug/L ND 5.0 11/18/15 16:13
Trichlorofluoromethane ug/L ND 10.0 11/18/15 16:13
Vinyl chloride ug/L ND 5.0 11/18/15 16:13
Xylene (Total)ug/L ND 10.0 11/18/15 16:13
1,2-Dichloroethane-d4 (S)%95 70-130 11/18/15 16:13
4-Bromofluorobenzene (S)%105 70-130 11/18/15 16:13
Toluene-d8 (S)%107 70-130 11/18/15 16:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609256LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 52.250 104 71-129
1,1,2,2-Tetrachloroethane ug/L 49.950 100 79-124
1,1,2-Trichloroethane ug/L 52.350 105 85-125
1,1,2-Trichlorotrifluoroethane ug/L 52.050 104 71-142
1,1-Dichloroethane ug/L 49.550 99 73-126
1,1-Dichloroethene ug/L 56.150 112 66-135
1,2,3-Trichlorobenzene ug/L 52.050 104 73-135
1,2,4-Trichlorobenzene ug/L 49.450 99 75-134
1,2-Dibromo-3-chloropropane ug/L 50.450 101 71-133
1,2-Dibromoethane (EDB)ug/L 56.050 112 83-124
1,2-Dichlorobenzene ug/L 50.550 101 80-133
1,2-Dichloroethane ug/L 45.850 92 67-128
1,2-Dichloropropane ug/L 51.250 102 75-132
1,3-Dichlorobenzene ug/L 50.950 102 77-130
1,4-Dichlorobenzene ug/L 50.050 100 78-130
2-Butanone (MEK)ug/L 114100 114 61-144
2-Hexanone ug/L 105100 105 68-143
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 72-135
Acetone ug/L 103100 103 48-146
Benzene ug/L 54.250 108 80-125
Bromochloromethane ug/L 63.0 L05012671-125
Bromodichloromethane ug/L 49.550 99 78-124
Bromoform ug/L 49.650 99 71-128
Bromomethane ug/L 79.250 158 40-160
Carbon disulfide ug/L 57.850 116 50-160
Carbon tetrachloride ug/L 50.750 101 69-131
Chlorobenzene ug/L 49.250 98 81-122
Chloroethane ug/L 50.850 102 39-148
REPORT OF LABORATORY ANALYSIS
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Greenwood, SC 29649
[phone]
Page 32 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609256LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroform ug/L 49.650 99 73-127
Chloromethane ug/L 56.250 112 44-146
cis-1,2-Dichloroethene ug/L 50.350 101 74-124
cis-1,3-Dichloropropene ug/L 53.550 107 72-132
Cyclohexane ug/L 53.350 107 62-145
Dibromochloromethane ug/L 49.950 100 78-125
Dichlorodifluoromethane ug/L 55.550 111 34-157
Ethylbenzene ug/L 48.250 96 79-121
Isopropylbenzene (Cumene)ug/L 52.450 105 81-132
Methyl acetate ug/L 59.350 119 58-128
Methyl-tert-butyl ether ug/L 59.750 119 74-131
Methylcyclohexane ug/L 51.150 102 65-144
Methylene Chloride ug/L 53.850 108 64-133
Styrene ug/L 48.550 97 84-126
Tetrachloroethene ug/L 50.550 101 78-122
Toluene ug/L 48.850 98 80-121
trans-1,2-Dichloroethene ug/L 53.750 107 71-127
trans-1,3-Dichloropropene ug/L 54.650 109 69-141
Trichloroethene ug/L 50.950 102 78-122
Trichlorofluoromethane ug/L 50.750 101 53-137
Vinyl chloride ug/L 60.450 121 58-137
Xylene (Total)ug/L 143150 96 81-126
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1609436MATRIX SPIKE SAMPLE:
MSSpike
Result
92275754003
1,1,1-Trichloroethane ug/L 23.320 117 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,2-Trichloroethane ug/L 21.420 107 70-130ND
1,1,2-Trichlorotrifluoroethane ug/L 23.220 116 70-130ND
1,1-Dichloroethane ug/L 29.120 113 70-1306.5
1,1-Dichloroethene ug/L 26.220 127 65-160ND
1,2,3-Trichlorobenzene ug/L 20.020 100 70-130ND
1,2,4-Trichlorobenzene ug/L 20.020 100 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.220 96 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.920 110 60-139ND
1,2-Dichlorobenzene ug/L 21.620 103 70-130ND
1,2-Dichloroethane ug/L 20.820 101 70-130ND
1,2-Dichloropropane ug/L 22.820 114 70-130ND
1,3-Dichlorobenzene ug/L 21.320 106 70-130ND
1,4-Dichlorobenzene ug/L 21.020 104 70-130ND
2-Butanone (MEK)ug/L 46.340 116 70-130ND
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 33 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1609436MATRIX SPIKE SAMPLE:
MSSpike
Result
92275754003
2-Hexanone ug/L 40.840 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 41.140 103 70-130ND
Acetone ug/L 50.440 96 70-130ND
Benzene ug/L 24.320 122 58-162ND
Bromochloromethane ug/L 25.820 129 70-130ND
Bromodichloromethane ug/L 21.820 109 70-130ND
Bromoform ug/L 17.320 87 70-130ND
Bromomethane ug/L 22.220 111 70-130ND
Carbon disulfide ug/L 25.320 127 70-130ND
Carbon tetrachloride ug/L 23.720 119 70-130ND
Chlorobenzene ug/L 29.520 110 70-1387.5
Chloroethane ug/L 28.9 M12013670-130ND
Chloroform ug/L 22.320 112 70-130ND
Chloromethane ug/L 17.620 88 70-130ND
cis-1,2-Dichloroethene ug/L 23.120 116 70-130ND
cis-1,3-Dichloropropene ug/L 21.520 107 70-130ND
Cyclohexane ug/L 23.620 118 70-130ND
Dibromochloromethane ug/L 18.820 94 70-130ND
Dichlorodifluoromethane ug/L 18.220 91 70-130ND
Ethylbenzene ug/L 21.220 106 22-189ND
Isopropylbenzene (Cumene)ug/L 23.220 116 70-130ND
Methyl acetate ug/L 22.520 112 70-130ND
Methyl-tert-butyl ether ug/L 23.520 117 37-169ND
Methylcyclohexane ug/L 21.920 109 70-130ND
Methylene Chloride ug/L 24.320 121 70-130ND
Styrene ug/L 21.720 108 70-130ND
Tetrachloroethene ug/L 21.620 108 70-130ND
Toluene ug/L 22.220 111 65-152ND
trans-1,2-Dichloroethene ug/L 24.220 121 70-130ND
trans-1,3-Dichloropropene ug/L 21.320 106 70-130ND
Trichloroethene ug/L 23.120 116 70-142ND
Trichlorofluoromethane ug/L 22.720 114 70-130ND
Vinyl chloride ug/L 27.720 128 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92275754004
1609437SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1,2-Trichlorotrifluoroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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Page 34 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275754004
1609437SAMPLE DUPLICATE:
1,1-Dichloroethene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L 8.3 68.9
Chloroethane ug/L 10.2 1411.8
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Cyclohexane ug/L NDND
Dibromochloromethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Isopropylbenzene (Cumene)ug/L NDND
Methyl acetate ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylcyclohexane ug/L NDND
Methylene Chloride ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%98 2100
4-Bromofluorobenzene (S)%101 3105
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 35 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275754004
1609437SAMPLE DUPLICATE:
Toluene-d8 (S)%107 1108
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 36 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34257
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005, 92275754006, 92275754007,
92275754008, 92275754009, 92275754010, 92275754011, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1604959
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005, 92275754006, 92275754007,
92275754008, 92275754009, 92275754010, 92275754011, 92275754012
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/12/15 18:08
1,2-Dichloroethane-d4 (S)%100 50-150 11/12/15 18:08
Toluene-d8 (S)%99 50-150 11/12/15 18:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1604960LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 20.620 103 71-125
1,2-Dichloroethane-d4 (S)%103 50-150
Toluene-d8 (S)%97 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1604961MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754006
1604962
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 97 50-150100 320ND21.0 21.6
1,2-Dichloroethane-d4 (S)%107 50-150106
Toluene-d8 (S)%98 50-15098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 37 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39029
EPA 3510
EPA 8270
8270 Water MSSV HVI
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005, 92275754006, 92275754007,
92275754010, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1605123
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005, 92275754006, 92275754007,
92275754010, 92275754012
Matrix:Water
Analyzed
Biphenyl (Diphenyl)ug/L ND 10.0 11/13/15 14:56
Diphenyl ether (Phenyl ether)ug/L ND 10.0 11/13/15 14:56
2,4,6-Tribromophenol (S)%39 27-110 11/13/15 14:56
2-Fluorobiphenyl (S)%69 27-110 11/13/15 14:56
2-Fluorophenol (S)%34 12-110 11/13/15 14:56
Nitrobenzene-d5 (S)%73 21-110 11/13/15 14:56
Phenol-d6 (S)%29 10-110 11/13/15 14:56
Terphenyl-d14 (S)%82 31-107 11/13/15 14:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1605124LABORATORY CONTROL SAMPLE:
LCSSpike
Biphenyl (Diphenyl)ug/L 33.450 67 38-120
Diphenyl ether (Phenyl ether)ug/L 33.750 67 51-120
2,4,6-Tribromophenol (S)%95 27-110
2-Fluorobiphenyl (S)%69 27-110
2-Fluorophenol (S)%37 12-110
Nitrobenzene-d5 (S)%77 21-110
Phenol-d6 (S)%25 10-110
Terphenyl-d14 (S)%99 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1605125MATRIX SPIKE SAMPLE:
MSSpike
Result
92275067003
Biphenyl (Diphenyl)ug/L 41.650 83 50-150ND
Diphenyl ether (Phenyl ether)ug/L 41.450 83 50-150ND
2,4,6-Tribromophenol (S)%S012127-110
2-Fluorobiphenyl (S)%91 27-110
2-Fluorophenol (S)%52 12-110
Nitrobenzene-d5 (S)%93 21-110
Phenol-d6 (S)%38 10-110
Terphenyl-d14 (S)%81 31-107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 38 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275067004
1605126SAMPLE DUPLICATE:
Biphenyl (Diphenyl)ug/L NDND
Diphenyl ether (Phenyl ether)ug/L NDND
2,4,6-Tribromophenol (S)%54 552
2-Fluorobiphenyl (S)%70 1279
2-Fluorophenol (S)%41 1038
Nitrobenzene-d5 (S)%73 375
Phenol-d6 (S)%34 1529
Terphenyl-d14 (S)%94 887
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 39 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39091
EPA 3510
EPA 8270
8270 Water MSSV HVI
Associated Lab Samples:92275754011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608030
Associated Lab Samples:92275754011
Matrix:Water
Analyzed
Biphenyl (Diphenyl)ug/L ND 10.0 11/17/15 13:51
Diphenyl ether (Phenyl ether)ug/L ND 10.0 11/17/15 13:51
2,4,6-Tribromophenol (S)%64 27-110 11/17/15 13:51
2-Fluorobiphenyl (S)%82 27-110 11/17/15 13:51
2-Fluorophenol (S)%44 12-110 11/17/15 13:51
Nitrobenzene-d5 (S)%76 21-110 11/17/15 13:51
Phenol-d6 (S)%35 10-110 11/17/15 13:51
Terphenyl-d14 (S)%80 31-107 11/17/15 13:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608031LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1608032
Biphenyl (Diphenyl)ug/L 38.350 77 38-1207839.2 2 30
Diphenyl ether (Phenyl ether)ug/L 34.450 69 51-1207437.1 7 30
2,4,6-Tribromophenol (S)%88 27-11082
2-Fluorobiphenyl (S)%84 27-11079
2-Fluorophenol (S)%47 12-11046
Nitrobenzene-d5 (S)%82 21-11080
Phenol-d6 (S)%31 10-11034
Terphenyl-d14 (S)%92 31-10785
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 40 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41436
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608082
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 11/18/15 16:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608083LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 49.750 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1608084MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275067004
1608085
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 100 90-110100 0506.0 56.2 56.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1608086MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275794004
1608087
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M1509090-11088 150102147146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 41 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25365
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1604426
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 11/12/15 07:01
Nitrogen, Nitrite mg/L ND 0.020 11/12/15 07:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1604427LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 2.52.5 98 90-110
Nitrogen, Nitrite mg/L 1.01 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1604428MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754001
1604429
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 91 90-11090 02.5ND 2.3 2.3
Nitrogen, Nitrite mg/L M117790-11077 010.040 0.81 0.81
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 42 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25364
SM 4500-P E
SM 4500-P E
SM4500P-E Phosphorus, Ortho
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1604413
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Matrix:Water
Analyzed
Orthophosphate as P mg/L ND 0.050 11/11/15 22:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1604414LABORATORY CONTROL SAMPLE:
LCSSpike
Orthophosphate as P mg/L 0.27.25 108 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1604415MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754001
1604416
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Orthophosphate as P mg/L M625390-11053 021.3 2.4 2.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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Greenwood, SC 29649
[phone]
Page 43 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25407
EPA 9060A
EPA 9060A
9060 TOC, AVL
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1607246
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004
Matrix:Water
Analyzed
Mean Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1607247LABORATORY CONTROL SAMPLE:
LCSSpike
Mean Total Organic Carbon mg/L 24.025 96 75-125
Total Organic Carbon mg/L 23.925 96 75-125
Total Organic Carbon mg/L 24.025 96 75-125
Total Organic Carbon mg/L 23.825 95 75-125
Total Organic Carbon mg/L 24.125 96 75-125
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1607248MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754001
1607249
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mean Total Organic Carbon mg/L M625-76 75-1250 125275027302750
Total Organic Carbon mg/L M62523675-125596 325269027502840
Total Organic Carbon mg/L M625-196 75-12596 325277027202800
Total Organic Carbon mg/L M625-116 75-125280 425275027202820
Total Organic Carbon mg/L M625-220 75-125-964 725278027202540
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92275754
CNA/NRLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - GreenwoodPASI-G
Pace Analytical Services - IndianapolisPASI-I
Pace Analytical Services - GreenwoodPASI-W
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 45 of 69
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92275754
CNA/NRLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92275754001 GCSV/17520B-23A EPA 8015 Alcohol-Glycol
92275754002 GCSV/17520B-23B EPA 8015 Alcohol-Glycol
92275754006 GCSV/17520SW-7 EPA 8015 Alcohol-Glycol
92275754007 GCSV/17520SW-5 EPA 8015 Alcohol-Glycol
92275754010 GCSV/17520SW-3 EPA 8015 Alcohol-Glycol
92275754011 GCSV/17520SW-8 EPA 8015 Alcohol-Glycol
92275754012 GCSV/17520B-09C EPA 8015 Alcohol-Glycol
92275754001 GWD/2671B-23A EPA 9056A
92275754002 GWD/2671B-23B EPA 9056A
92275754003 GWD/2671B-22A EPA 9056A
92275754004 GWD/2671B-22B EPA 9056A
92275754012 GWD/2671B-09C EPA 9056A
92275754001 OEXT/39029 MSSV/11519B-23A EPA 3510 EPA 8270
92275754002 OEXT/39029 MSSV/11519B-23B EPA 3510 EPA 8270
92275754003 OEXT/39029 MSSV/11519B-22A EPA 3510 EPA 8270
92275754004 OEXT/39029 MSSV/11519B-22B EPA 3510 EPA 8270
92275754005 OEXT/39029 MSSV/11519B-99B EPA 3510 EPA 8270
92275754006 OEXT/39029 MSSV/11519SW-7 EPA 3510 EPA 8270
92275754007 OEXT/39029 MSSV/11519SW-5 EPA 3510 EPA 8270
92275754010 OEXT/39029 MSSV/11519SW-3 EPA 3510 EPA 8270
92275754011 OEXT/39091 MSSV/11531SW-8 EPA 3510 EPA 8270
92275754012 OEXT/39029 MSSV/11519B-09C EPA 3510 EPA 8270
92275754001 MSV/34335B-23A EPA 8260
92275754002 MSV/34335B-23B EPA 8260
92275754003 MSV/34335B-22A EPA 8260
92275754004 MSV/34335B-22B EPA 8260
92275754005 MSV/34335B-99B EPA 8260
92275754012 MSV/34316B-09C EPA 8260
92275754001 MSV/34257B-23A EPA 8260B Mod.
92275754002 MSV/34257B-23B EPA 8260B Mod.
92275754003 MSV/34257B-22A EPA 8260B Mod.
92275754004 MSV/34257B-22B EPA 8260B Mod.
92275754005 MSV/34257B-99B EPA 8260B Mod.
92275754006 MSV/34257SW-7 EPA 8260B Mod.
92275754007 MSV/34257SW-5 EPA 8260B Mod.
92275754008 MSV/34257CSW-2 EPA 8260B Mod.
92275754009 MSV/34257CSW-1 EPA 8260B Mod.
92275754010 MSV/34257SW-3 EPA 8260B Mod.
92275754011 MSV/34257SW-8 EPA 8260B Mod.
92275754012 MSV/34257B-09C EPA 8260B Mod.
92275754001 WET/41436B-23A SM 2320B
92275754002 WET/41436B-23B SM 2320B
92275754003 WET/41436B-22A SM 2320B
92275754004 WET/41436B-22B SM 2320B
92275754012 WET/41436B-09C SM 2320B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92275754
CNA/NRLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92275754001 WETA/25365B-23A EPA 353.2
92275754002 WETA/25365B-23B EPA 353.2
92275754003 WETA/25365B-22A EPA 353.2
92275754004 WETA/25365B-22B EPA 353.2
92275754012 WETA/25365B-09C EPA 353.2
92275754001 WETA/25364B-23A SM 4500-P E
92275754002 WETA/25364B-23B SM 4500-P E
92275754003 WETA/25364B-22A SM 4500-P E
92275754004 WETA/25364B-22B SM 4500-P E
92275754012 WETA/25364B-09C SM 4500-P E
92275754001 WETA/25407B-23A EPA 9060A
92275754002 WETA/25407B-23B EPA 9060A
92275754003 WETA/25407B-22A EPA 9060A
92275754004 WETA/25407B-22B EPA 9060A
REPORT OF LABORATORY ANALYSIS
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#=CL#
November 25, 2015
LIMS USE: FR - BRYON DAHLGREN
LIMS OBJECT ID: 92275972
92275972
Project:
Pace Project No.:
RE:
Bryon Dahlgren
AECOM
10 Patewood Drive, Bldg 6
Suite 500
Greenville, SC 29615
CNA/NRLF
Dear Bryon Dahlgren:
Enclosed are the analytical results for sample(s) received by the laboratory on November 12, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 1 of 55
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92275972
CNA/NRLF
Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074
Indiana Certification #: C-49-06Kansas Certification #:E-10177Kentucky UST Certification #: 0042Kentucky WW Certification #:98019Louisiana Certification #: 04076
Ohio VAP Certification #: CL-0065Oklahoma Certification #: 2014-148
Texas Certification #: T104704355-15-9West Virginia Certification #: 330Wisconsin Certification #: 999788130USDA Soil Permit #: P330-10-00128
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
Greenwood Certification IDs
816 Durst Avenue East, Greenwood, SC 29649South Carolina Laboratory ID #: 24562North Carolina Divison of Water Resources Certification
number 25
Florida Certification number E87633Virginia VELAP ID: 460250
Asbestos NVLAP accreditation: 101410-0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92275972
CNA/NRLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92275972001 B-17C EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 8 PASI-CRES
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275972002 B-17B EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 8 PASI-CRES
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275972003 B-01 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CRES
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275972004 B-10 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CRES
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275972005 B-32B EPA 8015 Alcohol-Glycol 1 PASI-IBJW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Greenwood, SC 29649
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Page 3 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92275972
CNA/NRLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CRES
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275972006 B-12 EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CRES
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
92275972007 B-21B EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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816 Durst Avenue East
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Page 4 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-17C Lab ID:92275972001 Collected:11/11/15 08:25 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 1.4 mg/L 11/19/15 18:50 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/19/15 13:46 92-52-4 M111/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/19/15 13:46 101-84-8 M111/18/15 13:3010.0 1
Surrogates
Nitrobenzene-d5 (S)33 %11/19/15 13:46 4165-60-011/18/15 13:3021-110 1
2-Fluorobiphenyl (S)31 %11/19/15 13:46 321-60-811/18/15 13:3027-110 1
Terphenyl-d14 (S)46 %11/19/15 13:46 1718-51-011/18/15 13:3031-107 1
Phenol-d6 (S)13 %11/19/15 13:46 13127-88-311/18/15 13:3010-110 1
2-Fluorophenol (S)17 %11/19/15 13:46 367-12-411/18/15 13:3012-110 1
2,4,6-Tribromophenol (S)27 %11/19/15 13:46 118-79-611/18/15 13:3027-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)1810 ug/L 11/13/15 15:53 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/13/15 15:53 17060-07-050-150 50
Toluene-d8 (S)91 %11/13/15 15:53 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 329 mg/L 11/22/15 13:315.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 23:490.020 1
Nitrogen, Nitrite ND mg/L 11/12/15 23:490.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.34 mg/L 11/12/15 23:05 M10.050 1
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 61.2 mg/L 11/16/15 18:07 7440-44-02.0 2
Total Organic Carbon 58.4 mg/L 11/16/15 18:07 7440-44-02.0 2
Total Organic Carbon 59.1 mg/L 11/16/15 18:07 7440-44-02.0 2
Total Organic Carbon 59.8 mg/L 11/16/15 18:07 7440-44-02.0 2
Mean Total Organic Carbon 59.6 mg/L 11/16/15 18:07 7440-44-02.0 2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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Greenwood, SC 29649
[phone]
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-17B Lab ID:92275972002 Collected:11/11/15 09:30 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 2.3 mg/L 11/19/15 20:03 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/19/15 15:00 92-52-411/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/19/15 15:00 101-84-811/18/15 13:3010.0 1
Surrogates
Nitrobenzene-d5 (S)67 %11/19/15 15:00 4165-60-011/18/15 13:3021-110 1
2-Fluorobiphenyl (S)67 %11/19/15 15:00 321-60-811/18/15 13:3027-110 1
Terphenyl-d14 (S)57 %11/19/15 15:00 1718-51-011/18/15 13:3031-107 1
Phenol-d6 (S)13 %11/19/15 15:00 13127-88-311/18/15 13:3010-110 1
2-Fluorophenol (S)7 %11/19/15 15:00 367-12-4 S211/18/15 13:3012-110 1
2,4,6-Tribromophenol (S)12 %11/19/15 15:00 118-79-6 S211/18/15 13:3027-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)135 ug/L 11/13/15 16:14 123-91-110.0 5
Surrogates
1,2-Dichloroethane-d4 (S)100 %11/13/15 16:14 17060-07-050-150 5
Toluene-d8 (S)91 %11/13/15 16:14 2037-26-550-150 5
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 240 mg/L 11/22/15 13:485.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 23:590.020 1
Nitrogen, Nitrite ND mg/L 11/12/15 23:590.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.16 mg/L 11/12/15 23:050.050 1
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 53.3 mg/L 11/16/15 18:20 7440-44-02.0 2
Total Organic Carbon 52.5 mg/L 11/16/15 18:20 7440-44-02.0 2
Total Organic Carbon 53.1 mg/L 11/16/15 18:20 7440-44-02.0 2
Total Organic Carbon 53.0 mg/L 11/16/15 18:20 7440-44-02.0 2
Mean Total Organic Carbon 53.0 mg/L 11/16/15 18:20 7440-44-02.0 2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 6 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-01 Lab ID:92275972003 Collected:11/11/15 14:05 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 16:18 107-21-1 D350.0 10
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 28.5 mg/L 11/19/15 21:17 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/19/15 15:50 92-52-411/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)122 ug/L 11/19/15 15:50 101-84-811/18/15 13:3010.0 1
Surrogates
2-Fluorobiphenyl (S)162 %11/19/15 15:50 321-60-8 S511/18/15 13:3027-110 1
Analytical Method: EPA 82608260 MSV
Acetone ND ug/L 11/17/15 19:35 67-64-1125050
Benzene ND ug/L 11/17/15 19:35 71-43-225050
Bromochloromethane ND ug/L 11/17/15 19:35 74-97-525050
Bromodichloromethane ND ug/L 11/17/15 19:35 75-27-425050
Bromoform ND ug/L 11/17/15 19:35 75-25-225050
Bromomethane ND ug/L 11/17/15 19:35 74-83-950050
2-Butanone (MEK)ND ug/L 11/17/15 19:35 78-93-350050
Carbon disulfide ND ug/L 11/17/15 19:35 75-15-050050
Carbon tetrachloride ND ug/L 11/17/15 19:35 56-23-525050
Chlorobenzene ND ug/L 11/17/15 19:35 108-90-725050
Chloroethane ND ug/L 11/17/15 19:35 75-00-350050
Chloroform ND ug/L 11/17/15 19:35 67-66-325050
Chloromethane ND ug/L 11/17/15 19:35 74-87-325050
Cyclohexane ND ug/L 11/17/15 19:35 110-82-725050
1,2-Dibromo-3-chloropropane ND ug/L 11/17/15 19:35 96-12-810050
Dibromochloromethane ND ug/L 11/17/15 19:35 124-48-125050
1,2-Dibromoethane (EDB)ND ug/L 11/17/15 19:35 106-93-425050
1,2-Dichlorobenzene ND ug/L 11/17/15 19:35 95-50-125050
1,3-Dichlorobenzene ND ug/L 11/17/15 19:35 541-73-125050
1,4-Dichlorobenzene ND ug/L 11/17/15 19:35 106-46-725050
Dichlorodifluoromethane ND ug/L 11/17/15 19:35 75-71-825050
1,1-Dichloroethane ND ug/L 11/17/15 19:35 75-34-325050
1,2-Dichloroethane ND ug/L 11/17/15 19:35 107-06-225050
1,1-Dichloroethene ND ug/L 11/17/15 19:35 75-35-425050
cis-1,2-Dichloroethene ND ug/L 11/17/15 19:35 156-59-225050
trans-1,2-Dichloroethene ND ug/L 11/17/15 19:35 156-60-525050
1,2-Dichloropropane ND ug/L 11/17/15 19:35 78-87-525050
cis-1,3-Dichloropropene ND ug/L 11/17/15 19:35 10061-01-525050
trans-1,3-Dichloropropene ND ug/L 11/17/15 19:35 10061-02-625050
Ethylbenzene ND ug/L 11/17/15 19:35 100-41-425050
2-Hexanone ND ug/L 11/17/15 19:35 591-78-650050
Isopropylbenzene (Cumene)ND ug/L 11/17/15 19:35 98-82-825050
Methyl acetate ND ug/L 11/17/15 19:35 79-20-950050
Methylcyclohexane ND ug/L 11/17/15 19:35 108-87-250050
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 7 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-01 Lab ID:92275972003 Collected:11/11/15 14:05 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Methylene Chloride ND ug/L 11/17/15 19:35 75-09-225050
4-Methyl-2-pentanone (MIBK)ND ug/L 11/17/15 19:35 108-10-150050
Methyl-tert-butyl ether ND ug/L 11/17/15 19:35 1634-04-425050
Styrene ND ug/L 11/17/15 19:35 100-42-525050
1,1,2,2-Tetrachloroethane ND ug/L 11/17/15 19:35 79-34-525050
Tetrachloroethene ND ug/L 11/17/15 19:35 127-18-425050
Toluene ND ug/L 11/17/15 19:35 108-88-325050
1,2,3-Trichlorobenzene ND ug/L 11/17/15 19:35 87-61-625050
1,2,4-Trichlorobenzene ND ug/L 11/17/15 19:35 120-82-125050
1,1,1-Trichloroethane ND ug/L 11/17/15 19:35 71-55-625050
1,1,2-Trichloroethane ND ug/L 11/17/15 19:35 79-00-525050
Trichloroethene ND ug/L 11/17/15 19:35 79-01-625050
Trichlorofluoromethane ND ug/L 11/17/15 19:35 75-69-450050
1,1,2-Trichlorotrifluoroethane ND ug/L 11/17/15 19:35 76-13-125050
Vinyl chloride ND ug/L 11/17/15 19:35 75-01-425050
Xylene (Total)ND ug/L 11/17/15 19:35 1330-20-750050
Surrogates
4-Bromofluorobenzene (S)99 %11/17/15 19:35 460-00-4 D370-130 50
1,2-Dichloroethane-d4 (S)104 %11/17/15 19:35 17060-07-070-130 50
Toluene-d8 (S)102 %11/17/15 19:35 2037-26-570-130 50
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2640 ug/L 11/13/15 16:34 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)109 %11/13/15 16:34 17060-07-050-150 50
Toluene-d8 (S)90 %11/13/15 16:34 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 1430 mg/L 11/23/15 02:125.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/13/15 00:170.020 1
Nitrogen, Nitrite ND mg/L 11/13/15 00:170.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.94 mg/L 11/12/15 23:050.25 5
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 3620 mg/L 11/16/15 15:59 7440-44-0100100
Total Organic Carbon 3660 mg/L 11/16/15 15:59 7440-44-0100100
Total Organic Carbon 3640 mg/L 11/16/15 15:59 7440-44-0100100
Total Organic Carbon 3290 mg/L 11/16/15 15:59 7440-44-0100100
Mean Total Organic Carbon 3550 mg/L 11/16/15 15:59 7440-44-0100100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 8 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-10 Lab ID:92275972004 Collected:11/11/15 15:50 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 16:28 107-21-1 D350.0 10
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 11/19/15 21:41 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)192 ug/L 11/19/15 16:15 92-52-411/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)2110 ug/L 11/20/15 11:11 101-84-811/18/15 13:3010010
Surrogates
2-Fluorobiphenyl (S)79 %11/19/15 16:15 321-60-811/18/15 13:3027-110 1
Analytical Method: EPA 82608260 MSV
Acetone ND ug/L 11/17/15 19:52 67-64-162525
Benzene ND ug/L 11/17/15 19:52 71-43-212525
Bromochloromethane ND ug/L 11/17/15 19:52 74-97-512525
Bromodichloromethane ND ug/L 11/17/15 19:52 75-27-412525
Bromoform ND ug/L 11/17/15 19:52 75-25-212525
Bromomethane ND ug/L 11/17/15 19:52 74-83-925025
2-Butanone (MEK)ND ug/L 11/17/15 19:52 78-93-325025
Carbon disulfide ND ug/L 11/17/15 19:52 75-15-025025
Carbon tetrachloride ND ug/L 11/17/15 19:52 56-23-512525
Chlorobenzene ND ug/L 11/17/15 19:52 108-90-712525
Chloroethane ND ug/L 11/17/15 19:52 75-00-325025
Chloroform ND ug/L 11/17/15 19:52 67-66-312525
Chloromethane ND ug/L 11/17/15 19:52 74-87-312525
Cyclohexane ND ug/L 11/17/15 19:52 110-82-712525
1,2-Dibromo-3-chloropropane ND ug/L 11/17/15 19:52 96-12-850.0 25
Dibromochloromethane ND ug/L 11/17/15 19:52 124-48-112525
1,2-Dibromoethane (EDB)ND ug/L 11/17/15 19:52 106-93-412525
1,2-Dichlorobenzene ND ug/L 11/17/15 19:52 95-50-112525
1,3-Dichlorobenzene ND ug/L 11/17/15 19:52 541-73-112525
1,4-Dichlorobenzene ND ug/L 11/17/15 19:52 106-46-712525
Dichlorodifluoromethane ND ug/L 11/17/15 19:52 75-71-812525
1,1-Dichloroethane ND ug/L 11/17/15 19:52 75-34-312525
1,2-Dichloroethane ND ug/L 11/17/15 19:52 107-06-212525
1,1-Dichloroethene ND ug/L 11/17/15 19:52 75-35-412525
cis-1,2-Dichloroethene ND ug/L 11/17/15 19:52 156-59-212525
trans-1,2-Dichloroethene ND ug/L 11/17/15 19:52 156-60-512525
1,2-Dichloropropane ND ug/L 11/17/15 19:52 78-87-512525
cis-1,3-Dichloropropene ND ug/L 11/17/15 19:52 10061-01-512525
trans-1,3-Dichloropropene ND ug/L 11/17/15 19:52 10061-02-612525
Ethylbenzene ND ug/L 11/17/15 19:52 100-41-412525
2-Hexanone ND ug/L 11/17/15 19:52 591-78-625025
Isopropylbenzene (Cumene)ND ug/L 11/17/15 19:52 98-82-812525
Methyl acetate ND ug/L 11/17/15 19:52 79-20-925025
Methylcyclohexane ND ug/L 11/17/15 19:52 108-87-225025
REPORT OF LABORATORY ANALYSIS
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Greenwood, SC 29649
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Page 9 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-10 Lab ID:92275972004 Collected:11/11/15 15:50 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Methylene Chloride ND ug/L 11/17/15 19:52 75-09-212525
4-Methyl-2-pentanone (MIBK)ND ug/L 11/17/15 19:52 108-10-125025
Methyl-tert-butyl ether ND ug/L 11/17/15 19:52 1634-04-412525
Styrene ND ug/L 11/17/15 19:52 100-42-512525
1,1,2,2-Tetrachloroethane ND ug/L 11/17/15 19:52 79-34-512525
Tetrachloroethene ND ug/L 11/17/15 19:52 127-18-412525
Toluene ND ug/L 11/17/15 19:52 108-88-312525
1,2,3-Trichlorobenzene ND ug/L 11/17/15 19:52 87-61-612525
1,2,4-Trichlorobenzene ND ug/L 11/17/15 19:52 120-82-112525
1,1,1-Trichloroethane ND ug/L 11/17/15 19:52 71-55-612525
1,1,2-Trichloroethane ND ug/L 11/17/15 19:52 79-00-512525
Trichloroethene ND ug/L 11/17/15 19:52 79-01-612525
Trichlorofluoromethane ND ug/L 11/17/15 19:52 75-69-425025
1,1,2-Trichlorotrifluoroethane ND ug/L 11/17/15 19:52 76-13-112525
Vinyl chloride ND ug/L 11/17/15 19:52 75-01-412525
Xylene (Total)ND ug/L 11/17/15 19:52 1330-20-725025
Surrogates
4-Bromofluorobenzene (S)99 %11/17/15 19:52 460-00-4 D370-130 25
1,2-Dichloroethane-d4 (S)101 %11/17/15 19:52 17060-07-070-130 25
Toluene-d8 (S)101 %11/17/15 19:52 2037-26-570-130 25
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)404 ug/L 11/13/15 16:54 123-91-120.0 10
Surrogates
1,2-Dichloroethane-d4 (S)104 %11/13/15 16:54 17060-07-050-150 10
Toluene-d8 (S)92 %11/13/15 16:54 2037-26-550-150 10
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 694 mg/L 11/22/15 15:355.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/13/15 00:390.020 1
Nitrogen, Nitrite 0.067 mg/L 11/13/15 00:390.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.68 mg/L 11/12/15 23:050.20 4
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 31.6 mg/L 11/16/15 18:45 7440-44-02.0 2
Total Organic Carbon 29.7 mg/L 11/16/15 18:45 7440-44-02.0 2
Total Organic Carbon 30.9 mg/L 11/16/15 18:45 7440-44-02.0 2
Total Organic Carbon 30.7 mg/L 11/16/15 18:45 7440-44-02.0 2
Mean Total Organic Carbon 30.7 mg/L 11/16/15 18:45 7440-44-02.0 2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 10 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-32B Lab ID:92275972005 Collected:11/11/15 12:30 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 16:37 107-21-1 D350.0 10
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 11/19/15 22:05 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/19/15 16:40 92-52-411/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/19/15 16:40 101-84-811/18/15 13:3010.0 1
Surrogates
2-Fluorobiphenyl (S)74 %11/19/15 16:40 321-60-811/18/15 13:3027-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)18.3 ug/L 11/13/15 17:14 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %11/13/15 17:14 17060-07-050-150 1
Toluene-d8 (S)89 %11/13/15 17:14 2037-26-550-150 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 194 mg/L 11/22/15 16:255.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 0.14 mg/L 11/13/15 00:140.020 1
Nitrogen, Nitrite ND mg/L 11/13/15 00:140.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.13 mg/L 11/12/15 23:050.050 1
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 40.8 mg/L 11/16/15 18:58 7440-44-02.0 2
Total Organic Carbon 39.1 mg/L 11/16/15 18:58 7440-44-02.0 2
Total Organic Carbon 39.8 mg/L 11/16/15 18:58 7440-44-02.0 2
Total Organic Carbon 40.2 mg/L 11/16/15 18:58 7440-44-02.0 2
Mean Total Organic Carbon 40.0 mg/L 11/16/15 18:58 7440-44-02.0 2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 11 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-12 Lab ID:92275972006 Collected:11/11/15 10:20 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 1.2 mg/L 11/19/15 22:30 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/19/15 17:05 92-52-411/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/19/15 17:05 101-84-811/18/15 13:3010.0 1
Surrogates
2-Fluorobiphenyl (S)83 %11/19/15 17:05 321-60-811/18/15 13:3027-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2900 ug/L 11/13/15 17:34 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/13/15 17:34 17060-07-050-150 50
Toluene-d8 (S)90 %11/13/15 17:34 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 313 mg/L 11/22/15 16:405.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/13/15 00:000.020 1
Nitrogen, Nitrite ND mg/L 11/13/15 00:000.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.20 mg/L 11/12/15 23:050.050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 12 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-21B Lab ID:92275972007 Collected:11/11/15 11:20 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 15.1 mg/L 11/19/15 22:54 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)92.0 ug/L 11/13/15 17:54 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %11/13/15 17:54 17060-07-050-150 1
Toluene-d8 (S)89 %11/13/15 17:54 2037-26-550-150 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 282 mg/L 11/22/15 16:565.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/13/15 00:030.020 1
Nitrogen, Nitrite ND mg/L 11/13/15 00:030.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.25 mg/L 11/12/15 23:050.050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 13 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/17520
EPA 8015 Alcohol-Glycol
EPA 8015 Alcohol-Glycol
EPA 8015 Modified
Associated Lab Samples:92275972003, 92275972004, 92275972005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1426234
Associated Lab Samples:
Matrix:Water
Analyzed
Ethylene glycol mg/L ND 5.0 11/17/15 12:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1426235LABORATORY CONTROL SAMPLE:
LCSSpike
Ethylene glycol mg/L 22.425 89 79-129
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 14 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GWD/2674
EPA 9056A
EPA 9056A
9056 IC Anions, GWD
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1610278
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 11/19/15 10:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1610279LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 49.050 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1610280MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275972001
1610281
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 95 90-11096 0501.4 49.1 49.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 15 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34316
EPA 8260
EPA 8260
8260 MSV
Associated Lab Samples:92275972003, 92275972004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608047
Associated Lab Samples:92275972003, 92275972004
Matrix:Water
Analyzed
1,1,1-Trichloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2,2-Tetrachloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2-Trichloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2-Trichlorotrifluoroethane ug/L ND 5.0 11/17/15 14:29
1,1-Dichloroethane ug/L ND 5.0 11/17/15 14:29
1,1-Dichloroethene ug/L ND 5.0 11/17/15 14:29
1,2,3-Trichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2,4-Trichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/17/15 14:29
1,2-Dibromoethane (EDB)ug/L ND 5.0 11/17/15 14:29
1,2-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2-Dichloroethane ug/L ND 5.0 11/17/15 14:29
1,2-Dichloropropane ug/L ND 5.0 11/17/15 14:29
1,3-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,4-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
2-Butanone (MEK)ug/L ND 10.0 11/17/15 14:29
2-Hexanone ug/L ND 10.0 11/17/15 14:29
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 11/17/15 14:29
Acetone ug/L ND 25.0 11/17/15 14:29
Benzene ug/L ND 5.0 11/17/15 14:29
Bromochloromethane ug/L ND 5.0 11/17/15 14:29
Bromodichloromethane ug/L ND 5.0 11/17/15 14:29
Bromoform ug/L ND 5.0 11/17/15 14:29
Bromomethane ug/L ND 10.0 11/17/15 14:29
Carbon disulfide ug/L ND 10.0 11/17/15 14:29
Carbon tetrachloride ug/L ND 5.0 11/17/15 14:29
Chlorobenzene ug/L ND 5.0 11/17/15 14:29
Chloroethane ug/L ND 10.0 11/17/15 14:29
Chloroform ug/L ND 5.0 11/17/15 14:29
Chloromethane ug/L ND 5.0 11/17/15 14:29
cis-1,2-Dichloroethene ug/L ND 5.0 11/17/15 14:29
cis-1,3-Dichloropropene ug/L ND 5.0 11/17/15 14:29
Cyclohexane ug/L ND 5.0 11/17/15 14:29
Dibromochloromethane ug/L ND 5.0 11/17/15 14:29
Dichlorodifluoromethane ug/L ND 5.0 11/17/15 14:29
Ethylbenzene ug/L ND 5.0 11/17/15 14:29
Isopropylbenzene (Cumene)ug/L ND 5.0 11/17/15 14:29
Methyl acetate ug/L ND 10.0 11/17/15 14:29
Methyl-tert-butyl ether ug/L ND 5.0 11/17/15 14:29
Methylcyclohexane ug/L ND 10.0 11/17/15 14:29
Methylene Chloride ug/L ND 5.0 11/17/15 14:29
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 16 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608047
Associated Lab Samples:92275972003, 92275972004
Matrix:Water
Analyzed
Styrene ug/L ND 5.0 11/17/15 14:29
Tetrachloroethene ug/L ND 5.0 11/17/15 14:29
Toluene ug/L ND 5.0 11/17/15 14:29
trans-1,2-Dichloroethene ug/L ND 5.0 11/17/15 14:29
trans-1,3-Dichloropropene ug/L ND 5.0 11/17/15 14:29
Trichloroethene ug/L ND 5.0 11/17/15 14:29
Trichlorofluoromethane ug/L ND 10.0 11/17/15 14:29
Vinyl chloride ug/L ND 5.0 11/17/15 14:29
Xylene (Total)ug/L ND 10.0 11/17/15 14:29
1,2-Dichloroethane-d4 (S)%99 70-130 11/17/15 14:29
4-Bromofluorobenzene (S)%100 70-130 11/17/15 14:29
Toluene-d8 (S)%102 70-130 11/17/15 14:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608048LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 44.950 90 71-129
1,1,2,2-Tetrachloroethane ug/L 47.250 94 79-124
1,1,2-Trichloroethane ug/L 44.450 89 85-125
1,1,2-Trichlorotrifluoroethane ug/L 47.950 96 71-142
1,1-Dichloroethane ug/L 43.150 86 73-126
1,1-Dichloroethene ug/L 48.550 97 66-135
1,2,3-Trichlorobenzene ug/L 49.750 99 73-135
1,2,4-Trichlorobenzene ug/L 48.150 96 75-134
1,2-Dibromo-3-chloropropane ug/L 48.750 97 71-133
1,2-Dibromoethane (EDB)ug/L 53.050 106 83-124
1,2-Dichlorobenzene ug/L 50.450 101 80-133
1,2-Dichloroethane ug/L 47.450 95 67-128
1,2-Dichloropropane ug/L 46.250 92 75-132
1,3-Dichlorobenzene ug/L 50.450 101 77-130
1,4-Dichlorobenzene ug/L 49.450 99 78-130
2-Butanone (MEK)ug/L 98.2100 98 61-144
2-Hexanone ug/L 98.2100 98 68-143
4-Methyl-2-pentanone (MIBK)ug/L 90.9100 91 72-135
Acetone ug/L 89.8100 90 48-146
Benzene ug/L 48.150 96 80-125
Bromochloromethane ug/L 57.150 114 71-125
Bromodichloromethane ug/L 44.550 89 78-124
Bromoform ug/L 47.150 94 71-128
Bromomethane ug/L 53.950 108 40-160
Carbon disulfide ug/L 47.650 95 50-160
Carbon tetrachloride ug/L 46.850 94 69-131
Chlorobenzene ug/L 47.850 96 81-122
Chloroethane ug/L 50.550 101 39-148
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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[phone]
Page 17 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608048LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroform ug/L 50.150 100 73-127
Chloromethane ug/L 49.050 98 44-146
cis-1,2-Dichloroethene ug/L 50.450 101 74-124
cis-1,3-Dichloropropene ug/L 48.050 96 72-132
Cyclohexane ug/L 47.550 95 62-145
Dibromochloromethane ug/L 51.550 103 78-125
Dichlorodifluoromethane ug/L 51.350 103 34-157
Ethylbenzene ug/L 48.050 96 79-121
Isopropylbenzene (Cumene)ug/L 53.050 106 81-132
Methyl acetate ug/L 59.150 118 58-128
Methyl-tert-butyl ether ug/L 50.650 101 74-131
Methylcyclohexane ug/L 47.550 95 65-144
Methylene Chloride ug/L 50.150 100 64-133
Styrene ug/L 49.950 100 84-126
Tetrachloroethene ug/L 49.850 100 78-122
Toluene ug/L 42.050 84 80-121
trans-1,2-Dichloroethene ug/L 46.750 93 71-127
trans-1,3-Dichloropropene ug/L 46.950 94 69-141
Trichloroethene ug/L 45.950 92 78-122
Trichlorofluoromethane ug/L 47.550 95 53-137
Vinyl chloride ug/L 50.150 100 58-137
Xylene (Total)ug/L 146150 97 81-126
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%93 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1608049MATRIX SPIKE SAMPLE:
MSSpike
Result
92275933004
1,1,1-Trichloroethane ug/L 18.120 90 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.820 99 70-130ND
1,1,2-Trichloroethane ug/L 16.720 84 70-130ND
1,1,2-Trichlorotrifluoroethane ug/L 17.720 89 70-130ND
1,1-Dichloroethane ug/L 17.220 86 70-130ND
1,1-Dichloroethene ug/L 18.620 93 65-160ND
1,2,3-Trichlorobenzene ug/L 19.220 96 70-130ND
1,2,4-Trichlorobenzene ug/L 18.820 94 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.220 106 60-139ND
1,2-Dichlorobenzene ug/L 21.120 106 70-130ND
1,2-Dichloroethane ug/L 16.420 82 70-130ND
1,2-Dichloropropane ug/L 18.120 91 70-130ND
1,3-Dichlorobenzene ug/L 21.420 107 70-130ND
1,4-Dichlorobenzene ug/L 20.920 104 70-130ND
2-Butanone (MEK)ug/L 35.040 88 70-130ND
REPORT OF LABORATORY ANALYSIS
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Page 18 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1608049MATRIX SPIKE SAMPLE:
MSSpike
Result
92275933004
2-Hexanone ug/L 40.640 101 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 34.640 87 70-130ND
Acetone ug/L 37.4 M1404670-13019.1J
Benzene ug/L 22.920 96 58-1623.8J
Bromochloromethane ug/L 18.620 93 70-130ND
Bromodichloromethane ug/L 17.920 89 70-130ND
Bromoform ug/L 16.320 81 70-130ND
Bromomethane ug/L 12.3 M1206170-130ND
Carbon disulfide ug/L 17.220 86 70-130ND
Carbon tetrachloride ug/L 19.220 96 70-130ND
Chlorobenzene ug/L 21.520 107 70-138ND
Chloroethane ug/L 16.220 81 70-130ND
Chloroform ug/L 18.320 92 70-130ND
Chloromethane ug/L 18.220 91 70-130ND
cis-1,2-Dichloroethene ug/L 17.920 89 70-130ND
cis-1,3-Dichloropropene ug/L 17.320 86 70-130ND
Cyclohexane ug/L 19.620 86 70-1302.4J
Dibromochloromethane ug/L 19.620 98 70-130ND
Dichlorodifluoromethane ug/L 17.520 88 70-130ND
Ethylbenzene ug/L 20.920 100 22-189ND
Isopropylbenzene (Cumene)ug/L 27.820 105 70-1306.8
Methyl acetate ug/L 16.120 81 70-130ND
Methyl-tert-butyl ether ug/L 18.120 86 37-169ND
Methylcyclohexane ug/L 18.420 83 70-130ND
Methylene Chloride ug/L 15.620 78 70-130ND
Styrene ug/L 20.720 104 70-130ND
Tetrachloroethene ug/L 21.420 107 70-130ND
Toluene ug/L 17.020 85 65-152ND
trans-1,2-Dichloroethene ug/L 17.720 89 70-130ND
trans-1,3-Dichloropropene ug/L 16.820 84 70-130ND
Trichloroethene ug/L 17.620 88 70-142ND
Trichlorofluoromethane ug/L 18.520 92 70-130ND
Vinyl chloride ug/L 18.420 92 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1,2-Trichlorotrifluoroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 19 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
1,1-Dichloroethene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L ND22.5J
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Cyclohexane ug/L NDND
Dibromochloromethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Isopropylbenzene (Cumene)ug/L NDND
Methyl acetate ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylcyclohexane ug/L NDND
Methylene Chloride ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%99 199
4-Bromofluorobenzene (S)%99 297
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 20 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
Toluene-d8 (S)%103 1103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 21 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34275
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1606378
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/13/15 15:33
1,2-Dichloroethane-d4 (S)%100 50-150 11/13/15 15:33
Toluene-d8 (S)%91 50-150 11/13/15 15:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1606379LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 22.320 111 71-125
1,2-Dichloroethane-d4 (S)%100 50-150
Toluene-d8 (S)%92 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1606380MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276008003
1606381
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 101 50-150106 620ND20.1 21.3
1,2-Dichloroethane-d4 (S)%102 50-150102
Toluene-d8 (S)%89 50-15088
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 22 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39138
EPA 3510
EPA 8270
8270 Water MSSV HVI
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609395
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006
Matrix:Water
Analyzed
Biphenyl (Diphenyl)ug/L ND 10.0 11/19/15 11:17
Diphenyl ether (Phenyl ether)ug/L ND 10.0 11/19/15 11:17
2,4,6-Tribromophenol (S)%57 27-110 11/19/15 11:17
2-Fluorobiphenyl (S)%78 27-110 11/19/15 11:17
2-Fluorophenol (S)%42 12-110 11/19/15 11:17
Nitrobenzene-d5 (S)%77 21-110 11/19/15 11:17
Phenol-d6 (S)%35 10-110 11/19/15 11:17
Terphenyl-d14 (S)%69 31-107 11/19/15 11:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609396LABORATORY CONTROL SAMPLE:
LCSSpike
Biphenyl (Diphenyl)ug/L 30.150 60 38-120
Diphenyl ether (Phenyl ether)ug/L 27.050 54 51-120
2,4,6-Tribromophenol (S)%69 27-110
2-Fluorobiphenyl (S)%63 27-110
2-Fluorophenol (S)%41 12-110
Nitrobenzene-d5 (S)%66 21-110
Phenol-d6 (S)%31 10-110
Terphenyl-d14 (S)%64 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1609397MATRIX SPIKE SAMPLE:
MSSpike
Result
92275972001
Biphenyl (Diphenyl)ug/L 15.2 M1503050-150ND
Diphenyl ether (Phenyl ether)ug/L 13.3 M1502750-150ND
2,4,6-Tribromophenol (S)%62 27-110
2-Fluorobiphenyl (S)%31 27-110
2-Fluorophenol (S)%19 12-110
Nitrobenzene-d5 (S)%33 21-110
Phenol-d6 (S)%12 10-110
Terphenyl-d14 (S)%55 31-107
Parameter Units
Dup
Result QualifiersRPDResult
92275972002
1609398SAMPLE DUPLICATE:
Biphenyl (Diphenyl)ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 23 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275972002
1609398SAMPLE DUPLICATE:
Diphenyl ether (Phenyl ether)ug/L 6JND
2,4,6-Tribromophenol (S)%13 S0612
2-Fluorobiphenyl (S)%58 1567
2-Fluorophenol (S)%11 S0487
Nitrobenzene-d5 (S)%60 1067
Phenol-d6 (S)%20 4213
Terphenyl-d14 (S)%53 957
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 24 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41532
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1612032
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 11/22/15 12:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612033LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 48.450 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1612034MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276163001
1612035
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M1508990-11079 250206251245
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1612036MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276011002
1612037
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 98 90-11096 350ND49.2 47.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 25 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25376
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972005, 92275972006, 92275972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1605650
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972005, 92275972006, 92275972007
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 11/12/15 23:38
Nitrogen, Nitrite mg/L ND 0.020 11/12/15 23:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1605651LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 2.52.5 98 90-110
Nitrogen, Nitrite mg/L 1.01 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1605652MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275827002
1605653
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 97 90-11096 12.50.95 3.4 3.3
Nitrogen, Nitrite mg/L 1 106 90-110106 01ND1.1 1.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1605654MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275962003
1605655
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 93 90-110107 32.58.5 10.8 11.1
Nitrogen, Nitrite mg/L 1 101 90-110102 01ND1.0 1.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 26 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25377
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92275972004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1605656
Associated Lab Samples:92275972004
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 11/13/15 00:24
Nitrogen, Nitrite mg/L ND 0.020 11/13/15 00:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1605657LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 2.52.5 101 90-110
Nitrogen, Nitrite mg/L 1.01 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1605658MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276004003
1605659
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 96 90-11096 02.50.030 2.4 2.4
Nitrogen, Nitrite mg/L 1 100 90-11099 11ND1.0 0.99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 27 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25381
SM 4500-P E
SM 4500-P E
SM4500P-E Phosphorus, Ortho
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1605684
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Matrix:Water
Analyzed
Orthophosphate as P mg/L ND 0.050 11/12/15 23:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1605685LABORATORY CONTROL SAMPLE:
LCSSpike
Orthophosphate as P mg/L 0.26.25 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1605686MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275972001
1605687
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Orthophosphate as P mg/L M1.5 29 90-11029 0.50.34 0.49 0.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 28 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25407
EPA 9060A
EPA 9060A
9060 TOC, AVL
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1607246
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005
Matrix:Water
Analyzed
Mean Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1607247LABORATORY CONTROL SAMPLE:
LCSSpike
Mean Total Organic Carbon mg/L 24.025 96 75-125
Total Organic Carbon mg/L 23.925 96 75-125
Total Organic Carbon mg/L 24.025 96 75-125
Total Organic Carbon mg/L 23.825 95 75-125
Total Organic Carbon mg/L 24.125 96 75-125
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1607248MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754001
1607249
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mean Total Organic Carbon mg/L M625-76 75-1250 125275027302750
Total Organic Carbon mg/L M62523675-125596 325269027502840
Total Organic Carbon mg/L M625-196 75-12596 325277027202800
Total Organic Carbon mg/L M625-116 75-125280 425275027202820
Total Organic Carbon mg/L M625-220 75-125-964 725278027202540
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 29 of 55
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92275972
CNA/NRLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - GreenwoodPASI-G
Pace Analytical Services - IndianapolisPASI-I
Pace Analytical Services - GreenwoodPASI-W
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 30 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92275972
CNA/NRLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92275972003 GCSV/17520B-01 EPA 8015 Alcohol-Glycol
92275972004 GCSV/17520B-10 EPA 8015 Alcohol-Glycol
92275972005 GCSV/17520B-32B EPA 8015 Alcohol-Glycol
92275972001 GWD/2674B-17C EPA 9056A
92275972002 GWD/2674B-17B EPA 9056A
92275972003 GWD/2674B-01 EPA 9056A
92275972004 GWD/2674B-10 EPA 9056A
92275972005 GWD/2674B-32B EPA 9056A
92275972006 GWD/2674B-12 EPA 9056A
92275972007 GWD/2674B-21B EPA 9056A
92275972001 OEXT/39138 MSSV/11545B-17C EPA 3510 EPA 8270
92275972002 OEXT/39138 MSSV/11545B-17B EPA 3510 EPA 8270
92275972003 OEXT/39138 MSSV/11545B-01 EPA 3510 EPA 8270
92275972004 OEXT/39138 MSSV/11545B-10 EPA 3510 EPA 8270
92275972005 OEXT/39138 MSSV/11545B-32B EPA 3510 EPA 8270
92275972006 OEXT/39138 MSSV/11545B-12 EPA 3510 EPA 8270
92275972003 MSV/34316B-01 EPA 8260
92275972004 MSV/34316B-10 EPA 8260
92275972001 MSV/34275B-17C EPA 8260B Mod.
92275972002 MSV/34275B-17B EPA 8260B Mod.
92275972003 MSV/34275B-01 EPA 8260B Mod.
92275972004 MSV/34275B-10 EPA 8260B Mod.
92275972005 MSV/34275B-32B EPA 8260B Mod.
92275972006 MSV/34275B-12 EPA 8260B Mod.
92275972007 MSV/34275B-21B EPA 8260B Mod.
92275972001 WET/41532B-17C SM 2320B
92275972002 WET/41532B-17B SM 2320B
92275972003 WET/41532B-01 SM 2320B
92275972004 WET/41532B-10 SM 2320B
92275972005 WET/41532B-32B SM 2320B
92275972006 WET/41532B-12 SM 2320B
92275972007 WET/41532B-21B SM 2320B
92275972001 WETA/25376B-17C EPA 353.2
92275972002 WETA/25376B-17B EPA 353.2
92275972003 WETA/25376B-01 EPA 353.2
92275972004 WETA/25377B-10 EPA 353.2
92275972005 WETA/25376B-32B EPA 353.2
92275972006 WETA/25376B-12 EPA 353.2
92275972007 WETA/25376B-21B EPA 353.2
92275972001 WETA/25381B-17C SM 4500-P E
92275972002 WETA/25381B-17B SM 4500-P E
92275972003 WETA/25381B-01 SM 4500-P E
92275972004 WETA/25381B-10 SM 4500-P E
92275972005 WETA/25381B-32B SM 4500-P E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 31 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92275972
CNA/NRLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92275972006 WETA/25381B-12 SM 4500-P E
92275972007 WETA/25381B-21B SM 4500-P E
92275972001 WETA/25407B-17C EPA 9060A
92275972002 WETA/25407B-17B EPA 9060A
92275972003 WETA/25407B-01 EPA 9060A
92275972004 WETA/25407B-10 EPA 9060A
92275972005 WETA/25407B-32B EPA 9060A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 32 of 55
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Page 55 of 55
AECOM Environment
May 2016
Appendix B
Completed Inspection Forms
for Landfill Cap and
Phytoremediation System
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:rain
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T1 R13T8
30.5 45.25 22.75 6.25
30'+30'+20'+15'
full canopy full canopy full canopy full canopy
Other Observations:Willows from last planting are thriving
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
(attach additional
pages if needed)
0 .2/.9
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
5/29/2015
5/1/2015 5/8/2015 5/15/2015 5/22,29/2015
0 0
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:seasonal mowing
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:rain
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T1 R13T8
30.75 45.5 22.75 6.25
30'+30'+20'+15'
full canopy full canopy full canopy full canopy
Other Observations:
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
(attach additional
pages if needed)
0 0.9
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
6/26/2015
6/5/2015 6/12/2015 6/19/2015 6/26/2015
1.2 0.8
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:seasonal mowing
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:clear
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T1 R13T8
30.75 45.75 22.75 6.25
30'+30'+20'+15'
full canopy full canopy full canopy full canopy
Other Observations:
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
(attach additional
pages if needed)
0.5 0.8,0
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
7/31/2015
7/3/2015 7/10/2015 7/17/2015 7/24,31/2015
0 0.8
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:seasonal mowing
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:rain
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T1 R13T8
30.75 46 22.75 6.25
30'+30'+20'+15'
full canopy full canopy full canopy full canopy
Other Observations:
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
(attach additional
pages if needed)
1 1.4
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
8/28/2015
8/7/2015 8/14/2015 8/21/2015 8/28/2015
0.1 0
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:seasonal mowing
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:rain
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T1 R13T8
30.75 46.25 22.75 6.25
30'+30'+20'+15'
full canopy full canopy full canopy full canopy
Other Observations:Leaves turning to Fall color
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
(attach additional
pages if needed)
0 1.5
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
9/25/2015
9/4/2015 9/11/2015 9/18/2015 9/25/2015
0 0.2
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:seasonal mowing
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:rain
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T1 R13T8
30.75 46.5 22.75 6.25
30'+30'+20'+15'
full canopy full canopy full canopy full canopy
Other Observations:Leaves have fallen
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
(attach additional
pages if needed)
0 0,1.3
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
10/30/2015
10/2/2015 10/9/2015 10/16/2015 10/23,30/2015
2.5 0.4
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:seasonal mowing
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:clear
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T1 R13T8
30.75 46.75 22.75 6.25
30'+30'+20'+15'
N/A N/A N/A N/A
Other Observations:Leaves have fallen
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
(attach additional
pages if needed)
1.3 0
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
11/27/2015
11/6/2015 11/13/2015 11/20/2015 11/27/2015
2.4 1.9
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:none
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:rain
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T1 R13T8
30.75 47 22.75 6.25
30'+30'+20'+15'
N/A N/A N/A N/A
Other Observations:None
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
(attach additional
pages if needed)
1 2.1
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
12/26/2015
12/4/2015 12/11/2015 12/18/2015 12/26/2015
1.9 0
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:none
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:clear
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T1 R13T8
30.75 47 22.75 6.25
30'+30'+20'+15'
N/A N/A N/A N/A
Other Observations:None
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
1/2/2016 1/8/2016 1/15/2016 1/22,29/2016
1.8 0.3
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
(attach additional
pages if needed)
1.2 .4/0
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
1/29/2016
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:none
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:rain
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T1 R13T8
30.75 47 22.75 6.25
30'+30'+20'+15'
N/A N/A N/A N/A
Other Observations:None
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
2/5/2016 2/12/2016 2/19/2016 2/26/2016
0.7 0
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
(attach additional
pages if needed)
0.5 1.1
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
2/26/2016
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:none
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:rain
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):storm/wind broke 6 trees
Tree Status: R2T3 R6T4 R9T1 R13T8
31 47.5 N/A 6.5
30'+30'+20'+15'
N/A N/A N/A N/A
Other Observations:Broken trees: 1 in row 5, 1 in row 8, 2 in row 9 including monitor, 2 row 13.
R9T1 monitor gone - removed all broken trees
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
3/4/2016 3/11/2016 3/18/2016 3/25/2016
0.1 0
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
(attach additional
pages if needed)
0.1 0.2
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
3/25/2016
x
x
x
x
xx
x
x
x x
x
x
x
x
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:Seasonal mowing, removed additional trees from gravel road from
wind event.
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
PAGE 1 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:L.Brooks
General Site Conditions
Site Conditions:Dry Wet Weather:rain
Water Flow From Culvert:Yes X No
Rain Gauge Readings (unit in inches)
Date
Reading
Tree Farm Inspection
Tree Observation:Change in Tree Health Observed: Improving/Positive Declining No Change
Area of Declining Health (if any):None observed
Tree Status: R2T3 R6T4 R9T6 R13T8
31 47.5 8 6.5
30'+30'+15'15'
N/A N/A N/A N/A
Other Observations:Row 9 monitor changed to tree 6 - a willow
Tree Farm Maintenance
Grass Seeding:Yes No
Grass Mowing:Yes No
Fertilize the Tree:Yes No
Site Irrigation:Yes No
Apply Herbicide:Yes No
Tree Prune:Yes No
Fence Condition:Intact Damaged Repaired
Evidence of Grazing:Yes No
Photos Taken:Yes No
Tree Growth Audit by Others:Yes No
(attach additional
pages if needed)
0.1 .2/.7
Trunk Size (inches circ.)
Approx Tree Height
Tree Identification:
4/29/2016
4/1/2016 4/8/2016 4/15/2016 4/22,29/2016
0.7 0.5
Foliage Condition
Notes: (Please provide the chemical brand name
when applicable)
x
x
x
x
xx
x
x
x
x
x
xx
x
x
x
x
Rev. 11/15/2007
PAGE 2 of 2
PROJECT:Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER:AECOM - 60135443
LOCATION:Salisbury, NC DATE:
CLIENT:CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation:good condition
Landfill Cap Maintenance Activities:none
Other Activities
Form Reviewed By:
Date:
Rev. 11/15/2007
Notification Table
Results Exceeding 2L Standards for Needmore Road Landfill
May and November 2015 Values in mg/L
Chemical_name sys_loc_code Sample_Date NC 2L 2010 amount
1,1-dichloroethane B-22A 11/10/2015 0.006 0.0065
1,4-dioxane B-01 5/7/2015 0.003 2.89
1,4-dioxane B-01 11/11/2015 0.003 2.64
1,4-dioxane B-09C 5/6/2015 0.003 0.972
1,4-dioxane B-09C 11/10/2015 0.003 0.909
1,4-dioxane B-10 5/7/2015 0.003 0.511
1,4-dioxane B-10 11/11/2015 0.003 0.404
1,4-dioxane B-12 5/6/2015 0.003 3.09
1,4-dioxane B-12 11/11/2015 0.003 2.9
1,4-dioxane B-17B 11/11/2015 0.003 0.135
1,4-dioxane B-17C 5/6/2015 0.003 2.9
1,4-dioxane B-17C 11/11/2015 0.003 1.81
1,4-dioxane B-21B 11/11/2015 0.003 0.092
1,4-dioxane B-22A 11/10/2015 0.003 1.69
1,4-dioxane B-22B 5/6/2015 0.003 1.73
1,4-dioxane B-22B 11/10/2015 0.003 1.72
1,4-dioxane B-22B 11/10/2015 0.003 1.61
1,4-dioxane B-23A 5/6/2015 0.003 3.24
1,4-dioxane B-23A 11/10/2015 0.003 3.35
1,4-dioxane B-23B 5/6/2015 0.003 2.78
1,4-dioxane B-23B 11/10/2015 0.003 3.33
1,4-dioxane B-24A 5/6/2015 0.003 0.103
1,4-dioxane B-32B 11/11/2015 0.003 0.0183
#=CL#
May 20, 2015
LIMS USE: FR - BRYON DAHLGREN
LIMS OBJECT ID: 92248790
92248790
Project:
Pace Project No.:
RE:
Bryon Dahlgren
AECOM
10 Patewood Drive, Bldg 6
Suite 500
Greenville, SC 29615
NEEDMORE RD. LF
Dear Bryon Dahlgren:
Enclosed are the analytical results for sample(s) received by the laboratory on May 07, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 1 of 34
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074
Indiana Certification #: C-49-06Kansas Certification #:E-10177/ E-10247Kentucky UST Certification #: 0042Kentucky WW Certification #:98019Louisiana/NELAP Certification #: 04076
Ohio VAP Certification #: CL-0065Oklahoma Certification #: 2014-148
Pennsylvania Certification #: 68-05340Texas Certification #: T104704355-15-8West Virginia Certification #: 330Wisconsin Certification #: 999788130USDA Soil Permit #: P330-10-00128
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
Greenwood Certification IDs
816 Durst Avenue East, Greenwood, SC 29649South Carolina Laboratory ID #: 24562North Carolina Divison of Water Resources Certification
number 25
Florida Certification number E87633Virginia VELAP ID: 460250
Asbestos NVLAP accreditation: 101410-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 2 of 34
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92248790001 B-24A EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790002 B-22B EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790003 B-17C EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790004 B-23A EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790005 B-23B EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790006 B-9C EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790007 B-01 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 3 of 34
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790008 B-10 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 8270 8 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790009 B-12 EPA 9056A 1 PASI-GCDC
EPA 8270 8 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ADMN
SM 4500-P E 1 PASI-AMAB
92248790010 SW-99 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 8 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
92248790011 SW-5 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 8 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
92248790012 CSW-1 EPA 8260B Mod.3 PASI-CDLK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 4 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-24A Lab ID:92248790001 Collected:05/06/15 12:05 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 2.0 mg/L 05/13/15 22:22 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)103 ug/L 05/11/15 22:06 123-91-110.0 5
Surrogates
1,2-Dichloroethane-d4 (S)88 %05/11/15 22:06 17060-07-050-150 5
Toluene-d8 (S)101 %05/11/15 22:06 2037-26-550-150 5
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 211 mg/L 05/11/15 20:195.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:250.020 1
Nitrogen, Nitrite ND mg/L 05/08/15 00:250.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 05/08/15 12:00 M10.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 5 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-22B Lab ID:92248790002 Collected:05/06/15 15:25 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 05/13/15 22:52 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)1730 ug/L 05/11/15 22:26 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)91 %05/11/15 22:26 17060-07-050-150 50
Toluene-d8 (S)100 %05/11/15 22:26 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 615 mg/L 05/11/15 20:325.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:370.020 1
Nitrogen, Nitrite 0.032 mg/L 05/08/15 00:370.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 05/08/15 12:000.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 6 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-17C Lab ID:92248790003 Collected:05/06/15 17:35 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 1.0 mg/L 05/13/15 23:23 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2900 ug/L 05/11/15 22:47 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)92 %05/11/15 22:47 17060-07-050-150 50
Toluene-d8 (S)101 %05/11/15 22:47 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 336 mg/L 05/11/15 20:545.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:430.020 1
Nitrogen, Nitrite ND mg/L 05/08/15 00:430.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.21 mg/L 05/08/15 12:000.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 7 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-23A Lab ID:92248790004 Collected:05/06/15 13:10 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:00 107-21-15.0 1
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 9.0 mg/L 05/13/15 23:53 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)3240 ug/L 05/11/15 23:07 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)96 %05/11/15 23:07 17060-07-050-150 50
Toluene-d8 (S)100 %05/11/15 23:07 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2490 mg/L 05/11/15 21:105.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:300.020 1
Nitrogen, Nitrite 0.035 mg/L 05/08/15 00:300.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.47 mg/L 05/08/15 12:000.25 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 8 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-23B Lab ID:92248790005 Collected:05/06/15 14:20 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:09 107-21-15.0 1
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 5.3 mg/L 05/14/15 01:25 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2780 ug/L 05/11/15 23:28 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)95 %05/11/15 23:28 17060-07-050-150 50
Toluene-d8 (S)100 %05/11/15 23:28 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2160 mg/L 05/11/15 22:105.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:350.020 1
Nitrogen, Nitrite 0.16 mg/L 05/08/15 00:350.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 05/08/15 12:000.25 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 9 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-9C Lab ID:92248790006 Collected:05/06/15 18:45 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:19 107-21-15.0 1
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 05/14/15 01:55 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)972 ug/L 05/11/15 23:48 123-91-120.0 10
Surrogates
1,2-Dichloroethane-d4 (S)99 %05/11/15 23:48 17060-07-050-150 10
Toluene-d8 (S)98 %05/11/15 23:48 2037-26-550-150 10
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2500 mg/L 05/11/15 23:015.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:440.020 1
Nitrogen, Nitrite 0.12 mg/L 05/08/15 00:440.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 05/08/15 12:000.25 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 10 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-01 Lab ID:92248790007 Collected:05/07/15 00:00 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:28 107-21-15.0 1
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 3.1 mg/L 05/14/15 02:26 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2890 ug/L 05/12/15 00:08 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)99 %05/12/15 00:08 17060-07-050-150 50
Toluene-d8 (S)98 %05/12/15 00:08 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 1470 mg/L 05/11/15 23:495.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 00:450.020 1
Nitrogen, Nitrite ND mg/L 05/08/15 00:450.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 1.6 mg/L 05/08/15 12:000.25 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 11 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-10 Lab ID:92248790008 Collected:05/07/15 09:25 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:38 107-21-15.0 1
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 05/14/15 02:57 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Biphenyl (Diphenyl)82.8 ug/L 05/18/15 12:18 92-52-405/11/15 10:4510.0 1
Diphenyl ether (Phenyl ether)1090 ug/L 05/18/15 14:23 101-84-805/11/15 10:4520020
Surrogates
Nitrobenzene-d5 (S)85 %05/18/15 12:18 4165-60-005/11/15 10:4521-110 1
2-Fluorobiphenyl (S)64 %05/18/15 12:18 321-60-805/11/15 10:4527-110 1
Terphenyl-d14 (S)60 %05/18/15 12:18 1718-51-005/11/15 10:4531-107 1
Phenol-d6 (S)27 %05/18/15 12:18 13127-88-305/11/15 10:4510-110 1
2-Fluorophenol (S)36 %05/18/15 12:18 367-12-405/11/15 10:4512-110 1
2,4,6-Tribromophenol (S)83 %05/18/15 12:18 118-79-605/11/15 10:4527-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)511 ug/L 05/12/15 00:29 123-91-120.0 10
Surrogates
1,2-Dichloroethane-d4 (S)94 %05/12/15 00:29 17060-07-050-150 10
Toluene-d8 (S)99 %05/12/15 00:29 2037-26-550-150 10
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 664 mg/L 05/12/15 16:43 M15.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 05/08/15 22:150.020 1
Nitrogen, Nitrite 0.044 mg/L 05/08/15 22:150.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 05/08/15 12:000.25 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 12 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:B-12 Lab ID:92248790009 Collected:05/06/15 16:40 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 1.3 mg/L 05/14/15 03:27 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Biphenyl (Diphenyl)ND ug/L 05/18/15 12:50 92-52-405/11/15 10:4510.0 1
Diphenyl ether (Phenyl ether)ND ug/L 05/18/15 12:50 101-84-805/11/15 10:4510.0 1
Surrogates
Nitrobenzene-d5 (S)49 %05/18/15 12:50 4165-60-005/11/15 10:4521-110 1
2-Fluorobiphenyl (S)30 %05/18/15 12:50 321-60-805/11/15 10:4527-110 1
Terphenyl-d14 (S)92 %05/18/15 12:50 1718-51-005/11/15 10:4531-107 1
Phenol-d6 (S)10 %05/18/15 12:50 13127-88-305/11/15 10:4510-110 1
2-Fluorophenol (S)15 %05/18/15 12:50 367-12-405/11/15 10:4512-110 1
2,4,6-Tribromophenol (S)48 %05/18/15 12:50 118-79-605/11/15 10:4527-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)3090 ug/L 05/13/15 01:43 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)94 %05/13/15 01:43 17060-07-050-150 50
Toluene-d8 (S)97 %05/13/15 01:43 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 310 mg/L 05/12/15 17:185.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 0.031 mg/L 05/08/15 22:12 H10.020 1
Nitrogen, Nitrite ND mg/L 05/08/15 22:12 H10.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.13 mg/L 05/08/15 12:000.050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 13 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:SW-99 Lab ID:92248790010 Collected:05/06/15 15:40 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:47 107-21-15.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Biphenyl (Diphenyl)ND ug/L 05/18/15 13:21 92-52-405/11/15 10:4510.0 1
Diphenyl ether (Phenyl ether)ND ug/L 05/18/15 13:21 101-84-805/11/15 10:4510.0 1
Surrogates
Nitrobenzene-d5 (S)111 %05/18/15 13:21 4165-60-0 S305/11/15 10:4521-110 1
2-Fluorobiphenyl (S)71 %05/18/15 13:21 321-60-805/11/15 10:4527-110 1
Terphenyl-d14 (S)109 %05/18/15 13:21 1718-51-0 S305/11/15 10:4531-107 1
Phenol-d6 (S)23 %05/18/15 13:21 13127-88-305/11/15 10:4510-110 1
2-Fluorophenol (S)35 %05/18/15 13:21 367-12-405/11/15 10:4512-110 1
2,4,6-Tribromophenol (S)74 %05/18/15 13:21 118-79-605/11/15 10:4527-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 05/19/15 13:26 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %05/19/15 13:26 17060-07-050-150 1
Toluene-d8 (S)83 %05/19/15 13:26 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 14 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:SW-5 Lab ID:92248790011 Collected:05/06/15 15:45 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 05/15/15 16:57 107-21-15.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Biphenyl (Diphenyl)ND ug/L 05/18/15 13:52 92-52-405/11/15 10:4510.0 1
Diphenyl ether (Phenyl ether)ND ug/L 05/18/15 13:52 101-84-805/11/15 10:4510.0 1
Surrogates
Nitrobenzene-d5 (S)96 %05/18/15 13:52 4165-60-005/11/15 10:4521-110 1
2-Fluorobiphenyl (S)66 %05/18/15 13:52 321-60-805/11/15 10:4527-110 1
Terphenyl-d14 (S)100 %05/18/15 13:52 1718-51-005/11/15 10:4531-107 1
Phenol-d6 (S)22 %05/18/15 13:52 13127-88-305/11/15 10:4510-110 1
2-Fluorophenol (S)35 %05/18/15 13:52 367-12-405/11/15 10:4512-110 1
2,4,6-Tribromophenol (S)66 %05/18/15 13:52 118-79-605/11/15 10:4527-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 05/18/15 16:06 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)118 %05/18/15 16:06 17060-07-050-150 1
Toluene-d8 (S)98 %05/18/15 16:06 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 15 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Sample:CSW-1 Lab ID:92248790012 Collected:05/06/15 17:55 Received:05/07/15 10:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)82.1 ug/L 05/18/15 16:27 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)122 %05/18/15 16:27 17060-07-050-150 1
Toluene-d8 (S)98 %05/18/15 16:27 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 16 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/15345
EPA 8015 Alcohol-Glycol
EPA 8015 Alcohol-Glycol
EPA 8015 Modified
Associated Lab Samples:92248790004, 92248790005, 92248790006, 92248790007, 92248790008, 92248790010, 92248790011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1297875
Associated Lab Samples:
Matrix:Water
Analyzed
Ethylene glycol mg/L ND 5.0 05/15/15 14:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1297876LABORATORY CONTROL SAMPLE:
LCSSpike
Ethylene glycol mg/L 23.725 95 79-129
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1297878MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
60193253002
1297879
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Ethylene glycol mg/L R1256867-13386 2325ND17.0 21.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 17 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GWD/2113
EPA 9056A
EPA 9056A
9056 IC Anions, GWD
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007,
92248790008, 92248790009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1456652
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007,
92248790008, 92248790009
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 05/13/15 13:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1456653LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 49.850 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1456654MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248844006
1456655
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 103 90-110103 0500.79J 52.5 52.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1456656MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248790009
1456657
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 100 90-110103 2501.3 51.6 52.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 18 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31574
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92248790001, 92248790002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1455613
Associated Lab Samples:92248790001, 92248790002
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 05/11/15 14:53
1,2-Dichloroethane-d4 (S)%102 50-150 05/11/15 14:53
Toluene-d8 (S)%106 50-150 05/11/15 14:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1455614LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 20.920 104 71-125
1,2-Dichloroethane-d4 (S)%100 50-150
Toluene-d8 (S)%107 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1455615MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92249041008
1455616
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 130 50-150128 220ND26.0 25.6
1,2-Dichloroethane-d4 (S)%102 50-150101
Toluene-d8 (S)%103 50-150102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 19 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31575
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92248790003, 92248790004, 92248790005, 92248790006, 92248790007, 92248790008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1455617
Associated Lab Samples:92248790003, 92248790004, 92248790005, 92248790006, 92248790007, 92248790008
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 05/11/15 14:32
1,2-Dichloroethane-d4 (S)%105 50-150 05/11/15 14:32
Toluene-d8 (S)%106 50-150 05/11/15 14:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1455618LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 21.020 105 71-125
1,2-Dichloroethane-d4 (S)%103 50-150
Toluene-d8 (S)%106 50-150
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 20 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31602
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92248790009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1456598
Associated Lab Samples:92248790009
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 05/12/15 15:29
1,2-Dichloroethane-d4 (S)%88 50-150 05/12/15 15:29
Toluene-d8 (S)%100 50-150 05/12/15 15:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1456599LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 22.320 112 71-125
1,2-Dichloroethane-d4 (S)%84 50-150
Toluene-d8 (S)%100 50-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 21 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31702
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92248790011, 92248790012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1461633
Associated Lab Samples:92248790011, 92248790012
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 05/18/15 14:22
1,2-Dichloroethane-d4 (S)%110 50-150 05/18/15 14:22
Toluene-d8 (S)%98 50-150 05/18/15 14:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1461634LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 21.320 107 71-125
1,2-Dichloroethane-d4 (S)%104 50-150
Toluene-d8 (S)%99 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1461635MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92249154001
1461636
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 105 50-150108 220ND21.1 21.6
1,2-Dichloroethane-d4 (S)%123 50-150121
Toluene-d8 (S)%99 50-15099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 22 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31719
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92248790010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1462242
Associated Lab Samples:92248790010
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 05/19/15 12:03
1,2-Dichloroethane-d4 (S)%116 50-150 05/19/15 12:03
Toluene-d8 (S)%85 50-150 05/19/15 12:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1462243LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 18.520 92 71-125
1,2-Dichloroethane-d4 (S)%122 50-150
Toluene-d8 (S)%86 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1462244MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92250030001
1462245
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 96 50-15094 120ND19.1 18.9
1,2-Dichloroethane-d4 (S)%130 50-150131
Toluene-d8 (S)%82 50-15082
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
Greenwood, SC 29649
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Page 23 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/34967
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92248790008, 92248790009, 92248790010, 92248790011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1455439
Associated Lab Samples:92248790008, 92248790009, 92248790010, 92248790011
Matrix:Water
Analyzed
Biphenyl (Diphenyl)ug/L ND 10.0 05/18/15 12:19
Diphenyl ether (Phenyl ether)ug/L ND 10.0 05/18/15 12:19
2,4,6-Tribromophenol (S)%72 27-110 05/18/15 12:19
2-Fluorobiphenyl (S)%67 27-110 05/18/15 12:19
2-Fluorophenol (S)%37 12-110 05/18/15 12:19
Nitrobenzene-d5 (S)%88 21-110 05/18/15 12:19
Phenol-d6 (S)%25 10-110 05/18/15 12:19
Terphenyl-d14 (S)%103 31-107 05/18/15 12:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1455440LABORATORY CONTROL SAMPLE:
LCSSpike
Biphenyl (Diphenyl)ug/L 36.650 73 38-120
Diphenyl ether (Phenyl ether)ug/L 36.550 73 51-120
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%71 27-110
2-Fluorophenol (S)%41 12-110
Nitrobenzene-d5 (S)%77 21-110
Phenol-d6 (S)%31 10-110
Terphenyl-d14 (S)%103 31-107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/20/2015 06:36 PM
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816 Durst Avenue East
Greenwood, SC 29649
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Page 24 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/37367
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1455260
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 05/11/15 16:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1455261LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 49.250 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1455266MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248924001
1455267
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 98 90-11095 25024.1 73.0 71.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1455268MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92249096001
1455269
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M1508690-11079 35069.8 113 109
REPORT OF LABORATORY ANALYSIS
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Greenwood, SC 29649
[phone]
Page 25 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/37392
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92248790008, 92248790009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1456107
Associated Lab Samples:92248790008, 92248790009
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 05/12/15 16:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1456108LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 47.150 94 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1456109MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248790008
1456110
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M15096090-110944 15066411401140
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1456111MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248377003
1456112
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M1,R1508890-11099 55055.4 99.6 105
REPORT OF LABORATORY ANALYSIS
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Greenwood, SC 29649
[phone]
Page 26 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/22841
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1453829
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 05/08/15 00:04
Nitrogen, Nitrite mg/L ND 0.020 05/08/15 00:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1453830LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 2.52.5 101 90-110
Nitrogen, Nitrite mg/L 1.01 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1453833MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248890002
1453834
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 105 90-110104 02.52.7 5.4 5.3
Nitrogen, Nitrite mg/L 1 102 90-110101 11<0.020 1.0 1.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1453843MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248853002
1453844
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L M1,R12.5 40 90-110108 312.53.6 4.6 6.3
Nitrogen, Nitrite mg/L 1 104 90-110103 110.044 1.1 1.1
REPORT OF LABORATORY ANALYSIS
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Greenwood, SC 29649
[phone]
Page 27 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/22865
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92248790008, 92248790009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1454963
Associated Lab Samples:92248790008, 92248790009
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 05/08/15 22:04
Nitrogen, Nitrite mg/L ND 0.020 05/08/15 22:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1454964LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 2.62.5 103 90-110
Nitrogen, Nitrite mg/L 1.01 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1454965MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248790008
1454966
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 97 90-11097 02.5ND 2.4 2.4
Nitrogen, Nitrite mg/L 1 97 90-11099 210.044 1.0 1.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1454967MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92249027001
1454968
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 103 90-110104 02.51.2 3.7 3.8
Nitrogen, Nitrite mg/L 1 106 90-110105 110.045 1.1 1.1
REPORT OF LABORATORY ANALYSIS
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Greenwood, SC 29649
[phone]
Page 28 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/22856
SM 4500-P E
SM 4500-P E
SM4500P-E Phosphorus, Ortho
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007,
92248790008, 92248790009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1454040
Associated Lab Samples:92248790001, 92248790002, 92248790003, 92248790004, 92248790005, 92248790006, 92248790007,
92248790008, 92248790009
Matrix:Water
Analyzed
Orthophosphate as P mg/L ND 0.050 05/08/15 12:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1454041LABORATORY CONTROL SAMPLE:
LCSSpike
Orthophosphate as P mg/L 0.25.25 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1454042MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92248790001
1454043
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Orthophosphate as P mg/L M1.25 122 90-110122 0.25ND 0.33 0.33
REPORT OF LABORATORY ANALYSIS
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Page 29 of 34
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - GreenwoodPASI-G
Pace Analytical Services - IndianapolisPASI-I
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples.
Results unaffected by high bias.S3
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 30 of 34
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92248790004 GCSV/15345B-23A EPA 8015 Alcohol-Glycol
92248790005 GCSV/15345B-23B EPA 8015 Alcohol-Glycol
92248790006 GCSV/15345B-9C EPA 8015 Alcohol-Glycol
92248790007 GCSV/15345B-01 EPA 8015 Alcohol-Glycol
92248790008 GCSV/15345B-10 EPA 8015 Alcohol-Glycol
92248790010 GCSV/15345SW-99 EPA 8015 Alcohol-Glycol
92248790011 GCSV/15345SW-5 EPA 8015 Alcohol-Glycol
92248790001 GWD/2113B-24A EPA 9056A
92248790002 GWD/2113B-22B EPA 9056A
92248790003 GWD/2113B-17C EPA 9056A
92248790004 GWD/2113B-23A EPA 9056A
92248790005 GWD/2113B-23B EPA 9056A
92248790006 GWD/2113B-9C EPA 9056A
92248790007 GWD/2113B-01 EPA 9056A
92248790008 GWD/2113B-10 EPA 9056A
92248790009 GWD/2113B-12 EPA 9056A
92248790008 OEXT/34967 MSSV/10681B-10 EPA 3510 EPA 8270
92248790009 OEXT/34967 MSSV/10681B-12 EPA 3510 EPA 8270
92248790010 OEXT/34967 MSSV/10681SW-99 EPA 3510 EPA 8270
92248790011 OEXT/34967 MSSV/10681SW-5 EPA 3510 EPA 8270
92248790001 MSV/31574B-24A EPA 8260B Mod.
92248790002 MSV/31574B-22B EPA 8260B Mod.
92248790003 MSV/31575B-17C EPA 8260B Mod.
92248790004 MSV/31575B-23A EPA 8260B Mod.
92248790005 MSV/31575B-23B EPA 8260B Mod.
92248790006 MSV/31575B-9C EPA 8260B Mod.
92248790007 MSV/31575B-01 EPA 8260B Mod.
92248790008 MSV/31575B-10 EPA 8260B Mod.
92248790009 MSV/31602B-12 EPA 8260B Mod.
92248790010 MSV/31719SW-99 EPA 8260B Mod.
92248790011 MSV/31702SW-5 EPA 8260B Mod.
92248790012 MSV/31702CSW-1 EPA 8260B Mod.
92248790001 WET/37367B-24A SM 2320B
92248790002 WET/37367B-22B SM 2320B
92248790003 WET/37367B-17C SM 2320B
92248790004 WET/37367B-23A SM 2320B
92248790005 WET/37367B-23B SM 2320B
92248790006 WET/37367B-9C SM 2320B
92248790007 WET/37367B-01 SM 2320B
92248790008 WET/37392B-10 SM 2320B
92248790009 WET/37392B-12 SM 2320B
92248790001 WETA/22841B-24A EPA 353.2
92248790002 WETA/22841B-22B EPA 353.2
92248790003 WETA/22841B-17C EPA 353.2
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92248790
NEEDMORE RD. LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92248790004 WETA/22841B-23A EPA 353.2
92248790005 WETA/22841B-23B EPA 353.2
92248790006 WETA/22841B-9C EPA 353.2
92248790007 WETA/22841B-01 EPA 353.2
92248790008 WETA/22865B-10 EPA 353.2
92248790009 WETA/22865B-12 EPA 353.2
92248790001 WETA/22856B-24A SM 4500-P E
92248790002 WETA/22856B-22B SM 4500-P E
92248790003 WETA/22856B-17C SM 4500-P E
92248790004 WETA/22856B-23A SM 4500-P E
92248790005 WETA/22856B-23B SM 4500-P E
92248790006 WETA/22856B-9C SM 4500-P E
92248790007 WETA/22856B-01 SM 4500-P E
92248790008 WETA/22856B-10 SM 4500-P E
92248790009 WETA/22856B-12 SM 4500-P E
REPORT OF LABORATORY ANALYSIS
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Page 32 of 34
Page 33 of 34
Page 34 of 34
#=CL#
November 21, 2015
LIMS USE: FR - BRYON DAHLGREN
LIMS OBJECT ID: 92275754
92275754
Project:
Pace Project No.:
RE:
Bryon Dahlgren
AECOM
10 Patewood Drive, Bldg 6
Suite 500
Greenville, SC 29615
CNA/NRLF
Dear Bryon Dahlgren:
Enclosed are the analytical results for sample(s) received by the laboratory on November 11, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 69
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92275754
CNA/NRLF
Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074
Indiana Certification #: C-49-06Kansas Certification #:E-10177Kentucky UST Certification #: 0042Kentucky WW Certification #:98019Louisiana Certification #: 04076
Ohio VAP Certification #: CL-0065Oklahoma Certification #: 2014-148
Texas Certification #: T104704355-15-9West Virginia Certification #: 330Wisconsin Certification #: 999788130USDA Soil Permit #: P330-10-00128
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
Greenwood Certification IDs
816 Durst Avenue East, Greenwood, SC 29649South Carolina Laboratory ID #: 24562North Carolina Divison of Water Resources Certification
number 25
Florida Certification number E87633Virginia VELAP ID: 460250
Asbestos NVLAP accreditation: 101410-0
REPORT OF LABORATORY ANALYSIS
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Page 2 of 69
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92275754
CNA/NRLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92275754001 B-23A EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CRES
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ABRJ
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275754002 B-23B EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CBPJ
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ABRJ
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275754003 B-22A EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CBPJ
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ABRJ
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275754004 B-22B EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CBPJ
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ABRJ
SM 4500-P E 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Greenwood, SC 29649
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Page 3 of 69
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92275754
CNA/NRLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 9060A 5 PASI-AMDW
92275754005 B-99B EPA 8270 3 PASI-CBPJ
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
92275754006 SW-7 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 3 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
92275754007 SW-5 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 3 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
92275754008 CSW-2 EPA 8260B Mod.3 PASI-CDLK
92275754009 CSW-1 EPA 8260B Mod.3 PASI-CDLK
92275754010 SW-3 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 3 PASI-CBPJ
EPA 8260B Mod.3 PASI-CDLK
92275754011 SW-8 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 8270 3 PASI-CRES
EPA 8260B Mod.3 PASI-CDLK
92275754012 B-09C EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CBPJ
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ABRJ
SM 4500-P E 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 4 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-23A Lab ID:92275754001 Collected:11/10/15 10:25 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:03 107-21-1 D350.0 10
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 7.7 mg/L 11/19/15 02:12 14808-79-8 M11.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/16/15 19:53 92-52-411/12/15 15:3910010
Diphenyl ether (Phenyl ether)ND ug/L 11/16/15 19:53 101-84-811/12/15 15:3910010
Surrogates
2-Fluorobiphenyl (S)0 %11/16/15 19:53 321-60-8 D3,S411/12/15 15:3927-110 10
Analytical Method: EPA 82608260 MSV
Acetone 5120 ug/L 11/18/15 17:05 67-64-150020
Benzene ND ug/L 11/18/15 17:05 71-43-210020
Bromochloromethane ND ug/L 11/18/15 17:05 74-97-5 L310020
Bromodichloromethane ND ug/L 11/18/15 17:05 75-27-410020
Bromoform ND ug/L 11/18/15 17:05 75-25-210020
Bromomethane ND ug/L 11/18/15 17:05 74-83-920020
2-Butanone (MEK)483 ug/L 11/18/15 17:05 78-93-320020
Carbon disulfide ND ug/L 11/18/15 17:05 75-15-020020
Carbon tetrachloride ND ug/L 11/18/15 17:05 56-23-510020
Chlorobenzene ND ug/L 11/18/15 17:05 108-90-710020
Chloroethane ND ug/L 11/18/15 17:05 75-00-320020
Chloroform ND ug/L 11/18/15 17:05 67-66-310020
Chloromethane ND ug/L 11/18/15 17:05 74-87-310020
Cyclohexane ND ug/L 11/18/15 17:05 110-82-710020
1,2-Dibromo-3-chloropropane ND ug/L 11/18/15 17:05 96-12-840.0 20
Dibromochloromethane ND ug/L 11/18/15 17:05 124-48-110020
1,2-Dibromoethane (EDB)ND ug/L 11/18/15 17:05 106-93-410020
1,2-Dichlorobenzene ND ug/L 11/18/15 17:05 95-50-110020
1,3-Dichlorobenzene ND ug/L 11/18/15 17:05 541-73-110020
1,4-Dichlorobenzene ND ug/L 11/18/15 17:05 106-46-710020
Dichlorodifluoromethane ND ug/L 11/18/15 17:05 75-71-810020
1,1-Dichloroethane ND ug/L 11/18/15 17:05 75-34-310020
1,2-Dichloroethane ND ug/L 11/18/15 17:05 107-06-210020
1,1-Dichloroethene ND ug/L 11/18/15 17:05 75-35-410020
cis-1,2-Dichloroethene ND ug/L 11/18/15 17:05 156-59-210020
trans-1,2-Dichloroethene ND ug/L 11/18/15 17:05 156-60-510020
1,2-Dichloropropane ND ug/L 11/18/15 17:05 78-87-510020
cis-1,3-Dichloropropene ND ug/L 11/18/15 17:05 10061-01-510020
trans-1,3-Dichloropropene ND ug/L 11/18/15 17:05 10061-02-610020
Ethylbenzene ND ug/L 11/18/15 17:05 100-41-410020
2-Hexanone ND ug/L 11/18/15 17:05 591-78-620020
Isopropylbenzene (Cumene)ND ug/L 11/18/15 17:05 98-82-810020
Methyl acetate ND ug/L 11/18/15 17:05 79-20-920020
Methylcyclohexane ND ug/L 11/18/15 17:05 108-87-220020
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 5 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-23A Lab ID:92275754001 Collected:11/10/15 10:25 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Methylene Chloride ND ug/L 11/18/15 17:05 75-09-210020
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/15 17:05 108-10-120020
Methyl-tert-butyl ether ND ug/L 11/18/15 17:05 1634-04-410020
Styrene ND ug/L 11/18/15 17:05 100-42-510020
1,1,2,2-Tetrachloroethane ND ug/L 11/18/15 17:05 79-34-510020
Tetrachloroethene ND ug/L 11/18/15 17:05 127-18-410020
Toluene ND ug/L 11/18/15 17:05 108-88-310020
1,2,3-Trichlorobenzene ND ug/L 11/18/15 17:05 87-61-610020
1,2,4-Trichlorobenzene ND ug/L 11/18/15 17:05 120-82-110020
1,1,1-Trichloroethane ND ug/L 11/18/15 17:05 71-55-610020
1,1,2-Trichloroethane ND ug/L 11/18/15 17:05 79-00-510020
Trichloroethene ND ug/L 11/18/15 17:05 79-01-610020
Trichlorofluoromethane ND ug/L 11/18/15 17:05 75-69-420020
1,1,2-Trichlorotrifluoroethane ND ug/L 11/18/15 17:05 76-13-110020
Vinyl chloride ND ug/L 11/18/15 17:05 75-01-410020
Xylene (Total)ND ug/L 11/18/15 17:05 1330-20-720020
Surrogates
4-Bromofluorobenzene (S)106 %11/18/15 17:05 460-00-470-130 20
1,2-Dichloroethane-d4 (S)99 %11/18/15 17:05 17060-07-070-130 20
Toluene-d8 (S)108 %11/18/15 17:05 2037-26-570-130 20
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)3350 ug/L 11/12/15 18:28 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)105 %11/12/15 18:28 17060-07-050-150 50
Toluene-d8 (S)97 %11/12/15 18:28 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2540 mg/L 11/19/15 10:035.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 07:040.020 1
Nitrogen, Nitrite 0.040 mg/L 11/12/15 07:04 M10.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 1.3 mg/L 11/11/15 22:20 M60.20 4
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 2750 mg/L 11/16/15 17:00 7440-44-0 M6100100
Total Organic Carbon 2690 mg/L 11/16/15 17:00 7440-44-0 M6100100
Total Organic Carbon 2780 mg/L 11/16/15 17:00 7440-44-0 M6100100
Total Organic Carbon 2770 mg/L 11/16/15 17:00 7440-44-0 M6100100
Mean Total Organic Carbon 2750 mg/L 11/16/15 17:00 7440-44-0 M6100100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 6 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-23B Lab ID:92275754002 Collected:11/10/15 11:15 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:13 107-21-1 D350.0 10
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 7.5 mg/L 11/19/15 03:26 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 21:43 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/13/15 21:43 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)69 %11/13/15 21:43 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 82608260 MSV
Acetone 5090 ug/L 11/18/15 17:21 67-64-150020
Benzene ND ug/L 11/18/15 17:21 71-43-210020
Bromochloromethane ND ug/L 11/18/15 17:21 74-97-5 L310020
Bromodichloromethane ND ug/L 11/18/15 17:21 75-27-410020
Bromoform ND ug/L 11/18/15 17:21 75-25-210020
Bromomethane ND ug/L 11/18/15 17:21 74-83-920020
2-Butanone (MEK)488 ug/L 11/18/15 17:21 78-93-320020
Carbon disulfide ND ug/L 11/18/15 17:21 75-15-020020
Carbon tetrachloride ND ug/L 11/18/15 17:21 56-23-510020
Chlorobenzene ND ug/L 11/18/15 17:21 108-90-710020
Chloroethane ND ug/L 11/18/15 17:21 75-00-320020
Chloroform ND ug/L 11/18/15 17:21 67-66-310020
Chloromethane ND ug/L 11/18/15 17:21 74-87-310020
Cyclohexane ND ug/L 11/18/15 17:21 110-82-710020
1,2-Dibromo-3-chloropropane ND ug/L 11/18/15 17:21 96-12-840.0 20
Dibromochloromethane ND ug/L 11/18/15 17:21 124-48-110020
1,2-Dibromoethane (EDB)ND ug/L 11/18/15 17:21 106-93-410020
1,2-Dichlorobenzene ND ug/L 11/18/15 17:21 95-50-110020
1,3-Dichlorobenzene ND ug/L 11/18/15 17:21 541-73-110020
1,4-Dichlorobenzene ND ug/L 11/18/15 17:21 106-46-710020
Dichlorodifluoromethane ND ug/L 11/18/15 17:21 75-71-810020
1,1-Dichloroethane ND ug/L 11/18/15 17:21 75-34-310020
1,2-Dichloroethane ND ug/L 11/18/15 17:21 107-06-210020
1,1-Dichloroethene ND ug/L 11/18/15 17:21 75-35-410020
cis-1,2-Dichloroethene ND ug/L 11/18/15 17:21 156-59-210020
trans-1,2-Dichloroethene ND ug/L 11/18/15 17:21 156-60-510020
1,2-Dichloropropane ND ug/L 11/18/15 17:21 78-87-510020
cis-1,3-Dichloropropene ND ug/L 11/18/15 17:21 10061-01-510020
trans-1,3-Dichloropropene ND ug/L 11/18/15 17:21 10061-02-610020
Ethylbenzene ND ug/L 11/18/15 17:21 100-41-410020
2-Hexanone ND ug/L 11/18/15 17:21 591-78-620020
Isopropylbenzene (Cumene)ND ug/L 11/18/15 17:21 98-82-810020
Methyl acetate ND ug/L 11/18/15 17:21 79-20-920020
Methylcyclohexane ND ug/L 11/18/15 17:21 108-87-220020
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 7 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-23B Lab ID:92275754002 Collected:11/10/15 11:15 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Methylene Chloride ND ug/L 11/18/15 17:21 75-09-210020
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/15 17:21 108-10-120020
Methyl-tert-butyl ether ND ug/L 11/18/15 17:21 1634-04-410020
Styrene ND ug/L 11/18/15 17:21 100-42-510020
1,1,2,2-Tetrachloroethane ND ug/L 11/18/15 17:21 79-34-510020
Tetrachloroethene ND ug/L 11/18/15 17:21 127-18-410020
Toluene ND ug/L 11/18/15 17:21 108-88-310020
1,2,3-Trichlorobenzene ND ug/L 11/18/15 17:21 87-61-610020
1,2,4-Trichlorobenzene ND ug/L 11/18/15 17:21 120-82-110020
1,1,1-Trichloroethane ND ug/L 11/18/15 17:21 71-55-610020
1,1,2-Trichloroethane ND ug/L 11/18/15 17:21 79-00-510020
Trichloroethene ND ug/L 11/18/15 17:21 79-01-610020
Trichlorofluoromethane ND ug/L 11/18/15 17:21 75-69-420020
1,1,2-Trichlorotrifluoroethane ND ug/L 11/18/15 17:21 76-13-110020
Vinyl chloride ND ug/L 11/18/15 17:21 75-01-410020
Xylene (Total)ND ug/L 11/18/15 17:21 1330-20-720020
Surrogates
4-Bromofluorobenzene (S)106 %11/18/15 17:21 460-00-470-130 20
1,2-Dichloroethane-d4 (S)98 %11/18/15 17:21 17060-07-070-130 20
Toluene-d8 (S)108 %11/18/15 17:21 2037-26-570-130 20
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)3330 ug/L 11/12/15 18:49 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)107 %11/12/15 18:49 17060-07-050-150 50
Toluene-d8 (S)99 %11/12/15 18:49 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2250 mg/L 11/19/15 11:055.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 07:100.020 1
Nitrogen, Nitrite 0.12 mg/L 11/12/15 07:100.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.96 mg/L 11/11/15 22:200.20 4
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 2600 mg/L 11/16/15 14:30 7440-44-0100100
Total Organic Carbon 2880 mg/L 11/16/15 14:30 7440-44-0100100
Total Organic Carbon 2890 mg/L 11/16/15 14:30 7440-44-0100100
Total Organic Carbon 2890 mg/L 11/16/15 14:30 7440-44-0100100
Mean Total Organic Carbon 2810 mg/L 11/16/15 14:30 7440-44-0100100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 8 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-22A Lab ID:92275754003 Collected:11/10/15 14:20 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 11/19/15 04:39 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 22:09 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/13/15 22:09 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)73 %11/13/15 22:09 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 82608260 MSV
Acetone ND ug/L 11/18/15 17:38 67-64-125.0 1
Benzene ND ug/L 11/18/15 17:38 71-43-25.0 1
Bromochloromethane ND ug/L 11/18/15 17:38 74-97-5 L35.0 1
Bromodichloromethane ND ug/L 11/18/15 17:38 75-27-45.0 1
Bromoform ND ug/L 11/18/15 17:38 75-25-25.0 1
Bromomethane ND ug/L 11/18/15 17:38 74-83-910.0 1
2-Butanone (MEK)ND ug/L 11/18/15 17:38 78-93-310.0 1
Carbon disulfide ND ug/L 11/18/15 17:38 75-15-010.0 1
Carbon tetrachloride ND ug/L 11/18/15 17:38 56-23-55.0 1
Chlorobenzene 7.5 ug/L 11/18/15 17:38 108-90-75.0 1
Chloroethane ND ug/L 11/18/15 17:38 75-00-3 M110.0 1
Chloroform ND ug/L 11/18/15 17:38 67-66-35.0 1
Chloromethane ND ug/L 11/18/15 17:38 74-87-35.0 1
Cyclohexane ND ug/L 11/18/15 17:38 110-82-75.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/18/15 17:38 96-12-82.0 1
Dibromochloromethane ND ug/L 11/18/15 17:38 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/18/15 17:38 106-93-45.0 1
1,2-Dichlorobenzene ND ug/L 11/18/15 17:38 95-50-15.0 1
1,3-Dichlorobenzene ND ug/L 11/18/15 17:38 541-73-15.0 1
1,4-Dichlorobenzene ND ug/L 11/18/15 17:38 106-46-75.0 1
Dichlorodifluoromethane ND ug/L 11/18/15 17:38 75-71-85.0 1
1,1-Dichloroethane 6.5 ug/L 11/18/15 17:38 75-34-35.0 1
1,2-Dichloroethane ND ug/L 11/18/15 17:38 107-06-25.0 1
1,1-Dichloroethene ND ug/L 11/18/15 17:38 75-35-45.0 1
cis-1,2-Dichloroethene ND ug/L 11/18/15 17:38 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/L 11/18/15 17:38 156-60-55.0 1
1,2-Dichloropropane ND ug/L 11/18/15 17:38 78-87-55.0 1
cis-1,3-Dichloropropene ND ug/L 11/18/15 17:38 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/L 11/18/15 17:38 10061-02-65.0 1
Ethylbenzene ND ug/L 11/18/15 17:38 100-41-45.0 1
2-Hexanone ND ug/L 11/18/15 17:38 591-78-610.0 1
Isopropylbenzene (Cumene)ND ug/L 11/18/15 17:38 98-82-85.0 1
Methyl acetate ND ug/L 11/18/15 17:38 79-20-910.0 1
Methylcyclohexane ND ug/L 11/18/15 17:38 108-87-210.0 1
Methylene Chloride ND ug/L 11/18/15 17:38 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/15 17:38 108-10-110.0 1
Methyl-tert-butyl ether ND ug/L 11/18/15 17:38 1634-04-45.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 9 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-22A Lab ID:92275754003 Collected:11/10/15 14:20 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Styrene ND ug/L 11/18/15 17:38 100-42-55.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/18/15 17:38 79-34-55.0 1
Tetrachloroethene ND ug/L 11/18/15 17:38 127-18-45.0 1
Toluene ND ug/L 11/18/15 17:38 108-88-35.0 1
1,2,3-Trichlorobenzene ND ug/L 11/18/15 17:38 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/L 11/18/15 17:38 120-82-15.0 1
1,1,1-Trichloroethane ND ug/L 11/18/15 17:38 71-55-65.0 1
1,1,2-Trichloroethane ND ug/L 11/18/15 17:38 79-00-55.0 1
Trichloroethene ND ug/L 11/18/15 17:38 79-01-65.0 1
Trichlorofluoromethane ND ug/L 11/18/15 17:38 75-69-410.0 1
1,1,2-Trichlorotrifluoroethane ND ug/L 11/18/15 17:38 76-13-15.0 1
Vinyl chloride ND ug/L 11/18/15 17:38 75-01-45.0 1
Xylene (Total)ND ug/L 11/18/15 17:38 1330-20-710.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/18/15 17:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %11/18/15 17:38 17060-07-070-130 1
Toluene-d8 (S)109 %11/18/15 17:38 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)1690 ug/L 11/12/15 19:09 123-91-150.0 25
Surrogates
1,2-Dichloroethane-d4 (S)103 %11/12/15 19:09 17060-07-050-150 25
Toluene-d8 (S)97 %11/12/15 19:09 2037-26-550-150 25
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 544 mg/L 11/18/15 18:195.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 07:110.020 1
Nitrogen, Nitrite 0.050 mg/L 11/12/15 07:110.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P ND mg/L 11/11/15 22:200.25 5
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 5.0 mg/L 11/16/15 17:24 7440-44-05.0 5
Total Organic Carbon 5.5 mg/L 11/16/15 17:24 7440-44-05.0 5
Total Organic Carbon 5.2 mg/L 11/16/15 17:24 7440-44-05.0 5
Total Organic Carbon 5.3 mg/L 11/16/15 17:24 7440-44-05.0 5
Mean Total Organic Carbon 5.2 mg/L 11/16/15 17:24 7440-44-05.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 10 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-22B Lab ID:92275754004 Collected:11/10/15 15:05 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 11/19/15 05:03 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 22:34 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)11.7 ug/L 11/13/15 22:34 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)43 %11/13/15 22:34 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 82608260 MSV
Acetone ND ug/L 11/18/15 17:55 67-64-125.0 1
Benzene ND ug/L 11/18/15 17:55 71-43-25.0 1
Bromochloromethane ND ug/L 11/18/15 17:55 74-97-5 L35.0 1
Bromodichloromethane ND ug/L 11/18/15 17:55 75-27-45.0 1
Bromoform ND ug/L 11/18/15 17:55 75-25-25.0 1
Bromomethane ND ug/L 11/18/15 17:55 74-83-910.0 1
2-Butanone (MEK)ND ug/L 11/18/15 17:55 78-93-310.0 1
Carbon disulfide ND ug/L 11/18/15 17:55 75-15-010.0 1
Carbon tetrachloride ND ug/L 11/18/15 17:55 56-23-55.0 1
Chlorobenzene 8.9 ug/L 11/18/15 17:55 108-90-75.0 1
Chloroethane 11.8 ug/L 11/18/15 17:55 75-00-310.0 1
Chloroform ND ug/L 11/18/15 17:55 67-66-35.0 1
Chloromethane ND ug/L 11/18/15 17:55 74-87-35.0 1
Cyclohexane ND ug/L 11/18/15 17:55 110-82-75.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/18/15 17:55 96-12-82.0 1
Dibromochloromethane ND ug/L 11/18/15 17:55 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/18/15 17:55 106-93-45.0 1
1,2-Dichlorobenzene ND ug/L 11/18/15 17:55 95-50-15.0 1
1,3-Dichlorobenzene ND ug/L 11/18/15 17:55 541-73-15.0 1
1,4-Dichlorobenzene ND ug/L 11/18/15 17:55 106-46-75.0 1
Dichlorodifluoromethane ND ug/L 11/18/15 17:55 75-71-85.0 1
1,1-Dichloroethane ND ug/L 11/18/15 17:55 75-34-35.0 1
1,2-Dichloroethane ND ug/L 11/18/15 17:55 107-06-25.0 1
1,1-Dichloroethene ND ug/L 11/18/15 17:55 75-35-45.0 1
cis-1,2-Dichloroethene ND ug/L 11/18/15 17:55 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/L 11/18/15 17:55 156-60-55.0 1
1,2-Dichloropropane ND ug/L 11/18/15 17:55 78-87-55.0 1
cis-1,3-Dichloropropene ND ug/L 11/18/15 17:55 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/L 11/18/15 17:55 10061-02-65.0 1
Ethylbenzene ND ug/L 11/18/15 17:55 100-41-45.0 1
2-Hexanone ND ug/L 11/18/15 17:55 591-78-610.0 1
Isopropylbenzene (Cumene)ND ug/L 11/18/15 17:55 98-82-85.0 1
Methyl acetate ND ug/L 11/18/15 17:55 79-20-910.0 1
Methylcyclohexane ND ug/L 11/18/15 17:55 108-87-210.0 1
Methylene Chloride ND ug/L 11/18/15 17:55 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/15 17:55 108-10-110.0 1
Methyl-tert-butyl ether ND ug/L 11/18/15 17:55 1634-04-45.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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Page 11 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-22B Lab ID:92275754004 Collected:11/10/15 15:05 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Styrene ND ug/L 11/18/15 17:55 100-42-55.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/18/15 17:55 79-34-55.0 1
Tetrachloroethene ND ug/L 11/18/15 17:55 127-18-45.0 1
Toluene ND ug/L 11/18/15 17:55 108-88-35.0 1
1,2,3-Trichlorobenzene ND ug/L 11/18/15 17:55 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/L 11/18/15 17:55 120-82-15.0 1
1,1,1-Trichloroethane ND ug/L 11/18/15 17:55 71-55-65.0 1
1,1,2-Trichloroethane ND ug/L 11/18/15 17:55 79-00-55.0 1
Trichloroethene ND ug/L 11/18/15 17:55 79-01-65.0 1
Trichlorofluoromethane ND ug/L 11/18/15 17:55 75-69-410.0 1
1,1,2-Trichlorotrifluoroethane ND ug/L 11/18/15 17:55 76-13-15.0 1
Vinyl chloride ND ug/L 11/18/15 17:55 75-01-45.0 1
Xylene (Total)ND ug/L 11/18/15 17:55 1330-20-710.0 1
Surrogates
4-Bromofluorobenzene (S)105 %11/18/15 17:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/18/15 17:55 17060-07-070-130 1
Toluene-d8 (S)108 %11/18/15 17:55 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)1720 ug/L 11/12/15 19:29 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)103 %11/12/15 19:29 17060-07-050-150 50
Toluene-d8 (S)98 %11/12/15 19:29 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 724 mg/L 11/18/15 18:455.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 07:150.020 1
Nitrogen, Nitrite ND mg/L 11/12/15 07:150.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.38 mg/L 11/11/15 22:200.050 1
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 6.6 mg/L 11/16/15 17:55 7440-44-05.0 5
Total Organic Carbon 6.6 mg/L 11/16/15 17:55 7440-44-05.0 5
Total Organic Carbon 6.7 mg/L 11/16/15 17:55 7440-44-05.0 5
Total Organic Carbon 6.5 mg/L 11/16/15 17:55 7440-44-05.0 5
Mean Total Organic Carbon 6.6 mg/L 11/16/15 17:55 7440-44-05.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 12 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-99B Lab ID:92275754005 Collected:11/10/15 15:10 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 23:00 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)10.3 ug/L 11/13/15 23:00 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)61 %11/13/15 23:00 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 82608260 MSV
Acetone ND ug/L 11/18/15 18:29 67-64-125.0 1
Benzene ND ug/L 11/18/15 18:29 71-43-25.0 1
Bromochloromethane ND ug/L 11/18/15 18:29 74-97-5 L35.0 1
Bromodichloromethane ND ug/L 11/18/15 18:29 75-27-45.0 1
Bromoform ND ug/L 11/18/15 18:29 75-25-25.0 1
Bromomethane ND ug/L 11/18/15 18:29 74-83-910.0 1
2-Butanone (MEK)ND ug/L 11/18/15 18:29 78-93-310.0 1
Carbon disulfide ND ug/L 11/18/15 18:29 75-15-010.0 1
Carbon tetrachloride ND ug/L 11/18/15 18:29 56-23-55.0 1
Chlorobenzene 8.7 ug/L 11/18/15 18:29 108-90-75.0 1
Chloroethane 10.3 ug/L 11/18/15 18:29 75-00-310.0 1
Chloroform ND ug/L 11/18/15 18:29 67-66-35.0 1
Chloromethane ND ug/L 11/18/15 18:29 74-87-35.0 1
Cyclohexane ND ug/L 11/18/15 18:29 110-82-75.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/18/15 18:29 96-12-82.0 1
Dibromochloromethane ND ug/L 11/18/15 18:29 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/18/15 18:29 106-93-45.0 1
1,2-Dichlorobenzene ND ug/L 11/18/15 18:29 95-50-15.0 1
1,3-Dichlorobenzene ND ug/L 11/18/15 18:29 541-73-15.0 1
1,4-Dichlorobenzene ND ug/L 11/18/15 18:29 106-46-75.0 1
Dichlorodifluoromethane ND ug/L 11/18/15 18:29 75-71-85.0 1
1,1-Dichloroethane ND ug/L 11/18/15 18:29 75-34-35.0 1
1,2-Dichloroethane ND ug/L 11/18/15 18:29 107-06-25.0 1
1,1-Dichloroethene ND ug/L 11/18/15 18:29 75-35-45.0 1
cis-1,2-Dichloroethene ND ug/L 11/18/15 18:29 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/L 11/18/15 18:29 156-60-55.0 1
1,2-Dichloropropane ND ug/L 11/18/15 18:29 78-87-55.0 1
cis-1,3-Dichloropropene ND ug/L 11/18/15 18:29 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/L 11/18/15 18:29 10061-02-65.0 1
Ethylbenzene ND ug/L 11/18/15 18:29 100-41-45.0 1
2-Hexanone ND ug/L 11/18/15 18:29 591-78-610.0 1
Isopropylbenzene (Cumene)ND ug/L 11/18/15 18:29 98-82-85.0 1
Methyl acetate ND ug/L 11/18/15 18:29 79-20-910.0 1
Methylcyclohexane ND ug/L 11/18/15 18:29 108-87-210.0 1
Methylene Chloride ND ug/L 11/18/15 18:29 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/15 18:29 108-10-110.0 1
Methyl-tert-butyl ether ND ug/L 11/18/15 18:29 1634-04-45.0 1
Styrene ND ug/L 11/18/15 18:29 100-42-55.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/18/15 18:29 79-34-55.0 1
Tetrachloroethene ND ug/L 11/18/15 18:29 127-18-45.0 1
Toluene ND ug/L 11/18/15 18:29 108-88-35.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 13 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-99B Lab ID:92275754005 Collected:11/10/15 15:10 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
1,2,3-Trichlorobenzene ND ug/L 11/18/15 18:29 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/L 11/18/15 18:29 120-82-15.0 1
1,1,1-Trichloroethane ND ug/L 11/18/15 18:29 71-55-65.0 1
1,1,2-Trichloroethane ND ug/L 11/18/15 18:29 79-00-55.0 1
Trichloroethene ND ug/L 11/18/15 18:29 79-01-65.0 1
Trichlorofluoromethane ND ug/L 11/18/15 18:29 75-69-410.0 1
1,1,2-Trichlorotrifluoroethane ND ug/L 11/18/15 18:29 76-13-15.0 1
Vinyl chloride ND ug/L 11/18/15 18:29 75-01-45.0 1
Xylene (Total)ND ug/L 11/18/15 18:29 1330-20-710.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/18/15 18:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/18/15 18:29 17060-07-070-130 1
Toluene-d8 (S)107 %11/18/15 18:29 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)1610 ug/L 11/12/15 19:49 123-91-150.0 25
Surrogates
1,2-Dichloroethane-d4 (S)102 %11/12/15 19:49 17060-07-050-150 25
Toluene-d8 (S)98 %11/12/15 19:49 2037-26-550-150 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 14 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:SW-7 Lab ID:92275754006 Collected:11/10/15 13:10 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:32 107-21-1 D350.0 10
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 23:26 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/13/15 23:26 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)72 %11/13/15 23:26 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/12/15 20:09 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %11/12/15 20:09 17060-07-050-150 1
Toluene-d8 (S)97 %11/12/15 20:09 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 15 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:SW-5 Lab ID:92275754007 Collected:11/10/15 15:45 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:41 107-21-1 D350.0 10
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/13/15 23:52 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/13/15 23:52 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)48 %11/13/15 23:52 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/12/15 21:10 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %11/12/15 21:10 17060-07-050-150 1
Toluene-d8 (S)99 %11/12/15 21:10 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 16 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:CSW-2 Lab ID:92275754008 Collected:11/10/15 15:55 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)12.4 ug/L 11/12/15 21:30 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %11/12/15 21:30 17060-07-050-150 1
Toluene-d8 (S)96 %11/12/15 21:30 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 17 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:CSW-1 Lab ID:92275754009 Collected:11/10/15 16:05 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)14.0 ug/L 11/12/15 21:51 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %11/12/15 21:51 17060-07-050-150 1
Toluene-d8 (S)97 %11/12/15 21:51 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 18 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:SW-3 Lab ID:92275754010 Collected:11/10/15 16:20 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:53 107-21-1 D350.0 10
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/14/15 00:18 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/14/15 00:18 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)76 %11/14/15 00:18 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/12/15 22:11 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %11/12/15 22:11 17060-07-050-150 1
Toluene-d8 (S)97 %11/12/15 22:11 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 19 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:SW-8 Lab ID:92275754011 Collected:11/10/15 16:45 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 14:02 107-21-1 D350.0 10
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/18/15 13:50 92-52-411/17/15 09:3010.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/18/15 13:50 101-84-811/17/15 09:3010.0 1
Surrogates
2-Fluorobiphenyl (S)64 %11/18/15 13:50 321-60-811/17/15 09:3027-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/12/15 22:31 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %11/12/15 22:31 17060-07-050-150 1
Toluene-d8 (S)97 %11/12/15 22:31 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 20 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-09C Lab ID:92275754012 Collected:11/10/15 17:35 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 13:22 107-21-1 D3500100
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 11/19/15 05:28 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/14/15 00:43 92-52-411/12/15 15:3910.0 1
Diphenyl ether (Phenyl ether)10.6 ug/L 11/14/15 00:43 101-84-811/12/15 15:3910.0 1
Surrogates
2-Fluorobiphenyl (S)82 %11/14/15 00:43 321-60-811/12/15 15:3927-110 1
Analytical Method: EPA 82608260 MSV
Acetone 2660 ug/L 11/17/15 19:18 67-64-150020
Benzene ND ug/L 11/17/15 19:18 71-43-210020
Bromochloromethane ND ug/L 11/17/15 19:18 74-97-510020
Bromodichloromethane ND ug/L 11/17/15 19:18 75-27-410020
Bromoform ND ug/L 11/17/15 19:18 75-25-210020
Bromomethane ND ug/L 11/17/15 19:18 74-83-920020
2-Butanone (MEK)256 ug/L 11/17/15 19:18 78-93-320020
Carbon disulfide ND ug/L 11/17/15 19:18 75-15-020020
Carbon tetrachloride ND ug/L 11/17/15 19:18 56-23-510020
Chlorobenzene ND ug/L 11/17/15 19:18 108-90-710020
Chloroethane ND ug/L 11/17/15 19:18 75-00-320020
Chloroform ND ug/L 11/17/15 19:18 67-66-310020
Chloromethane ND ug/L 11/17/15 19:18 74-87-310020
Cyclohexane ND ug/L 11/17/15 19:18 110-82-710020
1,2-Dibromo-3-chloropropane ND ug/L 11/17/15 19:18 96-12-840.0 20
Dibromochloromethane ND ug/L 11/17/15 19:18 124-48-110020
1,2-Dibromoethane (EDB)ND ug/L 11/17/15 19:18 106-93-410020
1,2-Dichlorobenzene ND ug/L 11/17/15 19:18 95-50-110020
1,3-Dichlorobenzene ND ug/L 11/17/15 19:18 541-73-110020
1,4-Dichlorobenzene ND ug/L 11/17/15 19:18 106-46-710020
Dichlorodifluoromethane ND ug/L 11/17/15 19:18 75-71-810020
1,1-Dichloroethane ND ug/L 11/17/15 19:18 75-34-310020
1,2-Dichloroethane ND ug/L 11/17/15 19:18 107-06-210020
1,1-Dichloroethene ND ug/L 11/17/15 19:18 75-35-410020
cis-1,2-Dichloroethene ND ug/L 11/17/15 19:18 156-59-210020
trans-1,2-Dichloroethene ND ug/L 11/17/15 19:18 156-60-510020
1,2-Dichloropropane ND ug/L 11/17/15 19:18 78-87-510020
cis-1,3-Dichloropropene ND ug/L 11/17/15 19:18 10061-01-510020
trans-1,3-Dichloropropene ND ug/L 11/17/15 19:18 10061-02-610020
Ethylbenzene ND ug/L 11/17/15 19:18 100-41-410020
2-Hexanone ND ug/L 11/17/15 19:18 591-78-620020
Isopropylbenzene (Cumene)ND ug/L 11/17/15 19:18 98-82-810020
Methyl acetate ND ug/L 11/17/15 19:18 79-20-920020
Methylcyclohexane ND ug/L 11/17/15 19:18 108-87-220020
REPORT OF LABORATORY ANALYSIS
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Page 21 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275754
CNA/NRLF
Sample:B-09C Lab ID:92275754012 Collected:11/10/15 17:35 Received:11/11/15 05:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Methylene Chloride ND ug/L 11/17/15 19:18 75-09-210020
4-Methyl-2-pentanone (MIBK)ND ug/L 11/17/15 19:18 108-10-120020
Methyl-tert-butyl ether ND ug/L 11/17/15 19:18 1634-04-410020
Styrene ND ug/L 11/17/15 19:18 100-42-510020
1,1,2,2-Tetrachloroethane ND ug/L 11/17/15 19:18 79-34-510020
Tetrachloroethene ND ug/L 11/17/15 19:18 127-18-410020
Toluene ND ug/L 11/17/15 19:18 108-88-310020
1,2,3-Trichlorobenzene ND ug/L 11/17/15 19:18 87-61-610020
1,2,4-Trichlorobenzene ND ug/L 11/17/15 19:18 120-82-110020
1,1,1-Trichloroethane ND ug/L 11/17/15 19:18 71-55-610020
1,1,2-Trichloroethane ND ug/L 11/17/15 19:18 79-00-510020
Trichloroethene ND ug/L 11/17/15 19:18 79-01-610020
Trichlorofluoromethane ND ug/L 11/17/15 19:18 75-69-420020
1,1,2-Trichlorotrifluoroethane ND ug/L 11/17/15 19:18 76-13-110020
Vinyl chloride ND ug/L 11/17/15 19:18 75-01-410020
Xylene (Total)ND ug/L 11/17/15 19:18 1330-20-720020
Surrogates
4-Bromofluorobenzene (S)100 %11/17/15 19:18 460-00-470-130 20
1,2-Dichloroethane-d4 (S)100 %11/17/15 19:18 17060-07-070-130 20
Toluene-d8 (S)101 %11/17/15 19:18 2037-26-570-130 20
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)909 ug/L 11/12/15 22:51 123-91-120.0 10
Surrogates
1,2-Dichloroethane-d4 (S)108 %11/12/15 22:51 17060-07-050-150 10
Toluene-d8 (S)96 %11/12/15 22:51 2037-26-550-150 10
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 2260 mg/L 11/19/15 12:045.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 07:160.020 1
Nitrogen, Nitrite 0.073 mg/L 11/12/15 07:160.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.32 mg/L 11/11/15 22:200.25 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
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Page 22 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/17520
EPA 8015 Alcohol-Glycol
EPA 8015 Alcohol-Glycol
EPA 8015 Modified
Associated Lab Samples:92275754001, 92275754002, 92275754006, 92275754007, 92275754010, 92275754011, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1426234
Associated Lab Samples:
Matrix:Water
Analyzed
Ethylene glycol mg/L ND 5.0 11/17/15 12:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1426235LABORATORY CONTROL SAMPLE:
LCSSpike
Ethylene glycol mg/L 22.425 89 79-129
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 23 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GWD/2671
EPA 9056A
EPA 9056A
9056 IC Anions, GWD
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609962
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 11/19/15 01:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609963LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 48.850 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1609964MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754001
1609965
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L M1507990-11082 3507.7 47.3 48.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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Greenwood, SC 29649
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Page 24 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34316
EPA 8260
EPA 8260
8260 MSV
Associated Lab Samples:92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608047
Associated Lab Samples:92275754012
Matrix:Water
Analyzed
1,1,1-Trichloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2,2-Tetrachloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2-Trichloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2-Trichlorotrifluoroethane ug/L ND 5.0 11/17/15 14:29
1,1-Dichloroethane ug/L ND 5.0 11/17/15 14:29
1,1-Dichloroethene ug/L ND 5.0 11/17/15 14:29
1,2,3-Trichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2,4-Trichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/17/15 14:29
1,2-Dibromoethane (EDB)ug/L ND 5.0 11/17/15 14:29
1,2-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2-Dichloroethane ug/L ND 5.0 11/17/15 14:29
1,2-Dichloropropane ug/L ND 5.0 11/17/15 14:29
1,3-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,4-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
2-Butanone (MEK)ug/L ND 10.0 11/17/15 14:29
2-Hexanone ug/L ND 10.0 11/17/15 14:29
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 11/17/15 14:29
Acetone ug/L ND 25.0 11/17/15 14:29
Benzene ug/L ND 5.0 11/17/15 14:29
Bromochloromethane ug/L ND 5.0 11/17/15 14:29
Bromodichloromethane ug/L ND 5.0 11/17/15 14:29
Bromoform ug/L ND 5.0 11/17/15 14:29
Bromomethane ug/L ND 10.0 11/17/15 14:29
Carbon disulfide ug/L ND 10.0 11/17/15 14:29
Carbon tetrachloride ug/L ND 5.0 11/17/15 14:29
Chlorobenzene ug/L ND 5.0 11/17/15 14:29
Chloroethane ug/L ND 10.0 11/17/15 14:29
Chloroform ug/L ND 5.0 11/17/15 14:29
Chloromethane ug/L ND 5.0 11/17/15 14:29
cis-1,2-Dichloroethene ug/L ND 5.0 11/17/15 14:29
cis-1,3-Dichloropropene ug/L ND 5.0 11/17/15 14:29
Cyclohexane ug/L ND 5.0 11/17/15 14:29
Dibromochloromethane ug/L ND 5.0 11/17/15 14:29
Dichlorodifluoromethane ug/L ND 5.0 11/17/15 14:29
Ethylbenzene ug/L ND 5.0 11/17/15 14:29
Isopropylbenzene (Cumene)ug/L ND 5.0 11/17/15 14:29
Methyl acetate ug/L ND 10.0 11/17/15 14:29
Methyl-tert-butyl ether ug/L ND 5.0 11/17/15 14:29
Methylcyclohexane ug/L ND 10.0 11/17/15 14:29
Methylene Chloride ug/L ND 5.0 11/17/15 14:29
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 25 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608047
Associated Lab Samples:92275754012
Matrix:Water
Analyzed
Styrene ug/L ND 5.0 11/17/15 14:29
Tetrachloroethene ug/L ND 5.0 11/17/15 14:29
Toluene ug/L ND 5.0 11/17/15 14:29
trans-1,2-Dichloroethene ug/L ND 5.0 11/17/15 14:29
trans-1,3-Dichloropropene ug/L ND 5.0 11/17/15 14:29
Trichloroethene ug/L ND 5.0 11/17/15 14:29
Trichlorofluoromethane ug/L ND 10.0 11/17/15 14:29
Vinyl chloride ug/L ND 5.0 11/17/15 14:29
Xylene (Total)ug/L ND 10.0 11/17/15 14:29
1,2-Dichloroethane-d4 (S)%99 70-130 11/17/15 14:29
4-Bromofluorobenzene (S)%100 70-130 11/17/15 14:29
Toluene-d8 (S)%102 70-130 11/17/15 14:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608048LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 44.950 90 71-129
1,1,2,2-Tetrachloroethane ug/L 47.250 94 79-124
1,1,2-Trichloroethane ug/L 44.450 89 85-125
1,1,2-Trichlorotrifluoroethane ug/L 47.950 96 71-142
1,1-Dichloroethane ug/L 43.150 86 73-126
1,1-Dichloroethene ug/L 48.550 97 66-135
1,2,3-Trichlorobenzene ug/L 49.750 99 73-135
1,2,4-Trichlorobenzene ug/L 48.150 96 75-134
1,2-Dibromo-3-chloropropane ug/L 48.750 97 71-133
1,2-Dibromoethane (EDB)ug/L 53.050 106 83-124
1,2-Dichlorobenzene ug/L 50.450 101 80-133
1,2-Dichloroethane ug/L 47.450 95 67-128
1,2-Dichloropropane ug/L 46.250 92 75-132
1,3-Dichlorobenzene ug/L 50.450 101 77-130
1,4-Dichlorobenzene ug/L 49.450 99 78-130
2-Butanone (MEK)ug/L 98.2100 98 61-144
2-Hexanone ug/L 98.2100 98 68-143
4-Methyl-2-pentanone (MIBK)ug/L 90.9100 91 72-135
Acetone ug/L 89.8100 90 48-146
Benzene ug/L 48.150 96 80-125
Bromochloromethane ug/L 57.150 114 71-125
Bromodichloromethane ug/L 44.550 89 78-124
Bromoform ug/L 47.150 94 71-128
Bromomethane ug/L 53.950 108 40-160
Carbon disulfide ug/L 47.650 95 50-160
Carbon tetrachloride ug/L 46.850 94 69-131
Chlorobenzene ug/L 47.850 96 81-122
Chloroethane ug/L 50.550 101 39-148
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
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[phone]
Page 26 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608048LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroform ug/L 50.150 100 73-127
Chloromethane ug/L 49.050 98 44-146
cis-1,2-Dichloroethene ug/L 50.450 101 74-124
cis-1,3-Dichloropropene ug/L 48.050 96 72-132
Cyclohexane ug/L 47.550 95 62-145
Dibromochloromethane ug/L 51.550 103 78-125
Dichlorodifluoromethane ug/L 51.350 103 34-157
Ethylbenzene ug/L 48.050 96 79-121
Isopropylbenzene (Cumene)ug/L 53.050 106 81-132
Methyl acetate ug/L 59.150 118 58-128
Methyl-tert-butyl ether ug/L 50.650 101 74-131
Methylcyclohexane ug/L 47.550 95 65-144
Methylene Chloride ug/L 50.150 100 64-133
Styrene ug/L 49.950 100 84-126
Tetrachloroethene ug/L 49.850 100 78-122
Toluene ug/L 42.050 84 80-121
trans-1,2-Dichloroethene ug/L 46.750 93 71-127
trans-1,3-Dichloropropene ug/L 46.950 94 69-141
Trichloroethene ug/L 45.950 92 78-122
Trichlorofluoromethane ug/L 47.550 95 53-137
Vinyl chloride ug/L 50.150 100 58-137
Xylene (Total)ug/L 146150 97 81-126
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%93 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1608049MATRIX SPIKE SAMPLE:
MSSpike
Result
92275933004
1,1,1-Trichloroethane ug/L 18.120 90 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.820 99 70-130ND
1,1,2-Trichloroethane ug/L 16.720 84 70-130ND
1,1,2-Trichlorotrifluoroethane ug/L 17.720 89 70-130ND
1,1-Dichloroethane ug/L 17.220 86 70-130ND
1,1-Dichloroethene ug/L 18.620 93 65-160ND
1,2,3-Trichlorobenzene ug/L 19.220 96 70-130ND
1,2,4-Trichlorobenzene ug/L 18.820 94 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.220 106 60-139ND
1,2-Dichlorobenzene ug/L 21.120 106 70-130ND
1,2-Dichloroethane ug/L 16.420 82 70-130ND
1,2-Dichloropropane ug/L 18.120 91 70-130ND
1,3-Dichlorobenzene ug/L 21.420 107 70-130ND
1,4-Dichlorobenzene ug/L 20.920 104 70-130ND
2-Butanone (MEK)ug/L 35.040 88 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
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Page 27 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1608049MATRIX SPIKE SAMPLE:
MSSpike
Result
92275933004
2-Hexanone ug/L 40.640 101 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 34.640 87 70-130ND
Acetone ug/L 37.4 M1404670-13019.1J
Benzene ug/L 22.920 96 58-1623.8J
Bromochloromethane ug/L 18.620 93 70-130ND
Bromodichloromethane ug/L 17.920 89 70-130ND
Bromoform ug/L 16.320 81 70-130ND
Bromomethane ug/L 12.3 M1206170-130ND
Carbon disulfide ug/L 17.220 86 70-130ND
Carbon tetrachloride ug/L 19.220 96 70-130ND
Chlorobenzene ug/L 21.520 107 70-138ND
Chloroethane ug/L 16.220 81 70-130ND
Chloroform ug/L 18.320 92 70-130ND
Chloromethane ug/L 18.220 91 70-130ND
cis-1,2-Dichloroethene ug/L 17.920 89 70-130ND
cis-1,3-Dichloropropene ug/L 17.320 86 70-130ND
Cyclohexane ug/L 19.620 86 70-1302.4J
Dibromochloromethane ug/L 19.620 98 70-130ND
Dichlorodifluoromethane ug/L 17.520 88 70-130ND
Ethylbenzene ug/L 20.920 100 22-189ND
Isopropylbenzene (Cumene)ug/L 27.820 105 70-1306.8
Methyl acetate ug/L 16.120 81 70-130ND
Methyl-tert-butyl ether ug/L 18.120 86 37-169ND
Methylcyclohexane ug/L 18.420 83 70-130ND
Methylene Chloride ug/L 15.620 78 70-130ND
Styrene ug/L 20.720 104 70-130ND
Tetrachloroethene ug/L 21.420 107 70-130ND
Toluene ug/L 17.020 85 65-152ND
trans-1,2-Dichloroethene ug/L 17.720 89 70-130ND
trans-1,3-Dichloropropene ug/L 16.820 84 70-130ND
Trichloroethene ug/L 17.620 88 70-142ND
Trichlorofluoromethane ug/L 18.520 92 70-130ND
Vinyl chloride ug/L 18.420 92 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1,2-Trichlorotrifluoroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
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Page 28 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
1,1-Dichloroethene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L ND22.5J
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Cyclohexane ug/L NDND
Dibromochloromethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Isopropylbenzene (Cumene)ug/L NDND
Methyl acetate ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylcyclohexane ug/L NDND
Methylene Chloride ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%99 199
4-Bromofluorobenzene (S)%99 297
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 29 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
Toluene-d8 (S)%103 1103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 30 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34335
EPA 8260
EPA 8260
8260 MSV
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609255
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005
Matrix:Water
Analyzed
1,1,1-Trichloroethane ug/L ND 5.0 11/18/15 16:13
1,1,2,2-Tetrachloroethane ug/L ND 5.0 11/18/15 16:13
1,1,2-Trichloroethane ug/L ND 5.0 11/18/15 16:13
1,1,2-Trichlorotrifluoroethane ug/L ND 5.0 11/18/15 16:13
1,1-Dichloroethane ug/L ND 5.0 11/18/15 16:13
1,1-Dichloroethene ug/L ND 5.0 11/18/15 16:13
1,2,3-Trichlorobenzene ug/L ND 5.0 11/18/15 16:13
1,2,4-Trichlorobenzene ug/L ND 5.0 11/18/15 16:13
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/18/15 16:13
1,2-Dibromoethane (EDB)ug/L ND 5.0 11/18/15 16:13
1,2-Dichlorobenzene ug/L ND 5.0 11/18/15 16:13
1,2-Dichloroethane ug/L ND 5.0 11/18/15 16:13
1,2-Dichloropropane ug/L ND 5.0 11/18/15 16:13
1,3-Dichlorobenzene ug/L ND 5.0 11/18/15 16:13
1,4-Dichlorobenzene ug/L ND 5.0 11/18/15 16:13
2-Butanone (MEK)ug/L ND 10.0 11/18/15 16:13
2-Hexanone ug/L ND 10.0 11/18/15 16:13
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 11/18/15 16:13
Acetone ug/L ND 25.0 11/18/15 16:13
Benzene ug/L ND 5.0 11/18/15 16:13
Bromochloromethane ug/L ND 5.0 11/18/15 16:13
Bromodichloromethane ug/L ND 5.0 11/18/15 16:13
Bromoform ug/L ND 5.0 11/18/15 16:13
Bromomethane ug/L ND 10.0 11/18/15 16:13
Carbon disulfide ug/L ND 10.0 11/18/15 16:13
Carbon tetrachloride ug/L ND 5.0 11/18/15 16:13
Chlorobenzene ug/L ND 5.0 11/18/15 16:13
Chloroethane ug/L ND 10.0 11/18/15 16:13
Chloroform ug/L ND 5.0 11/18/15 16:13
Chloromethane ug/L ND 5.0 11/18/15 16:13
cis-1,2-Dichloroethene ug/L ND 5.0 11/18/15 16:13
cis-1,3-Dichloropropene ug/L ND 5.0 11/18/15 16:13
Cyclohexane ug/L ND 5.0 11/18/15 16:13
Dibromochloromethane ug/L ND 5.0 11/18/15 16:13
Dichlorodifluoromethane ug/L ND 5.0 11/18/15 16:13
Ethylbenzene ug/L ND 5.0 11/18/15 16:13
Isopropylbenzene (Cumene)ug/L ND 5.0 11/18/15 16:13
Methyl acetate ug/L ND 10.0 11/18/15 16:13
Methyl-tert-butyl ether ug/L ND 5.0 11/18/15 16:13
Methylcyclohexane ug/L ND 10.0 11/18/15 16:13
Methylene Chloride ug/L ND 5.0 11/18/15 16:13
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 31 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609255
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005
Matrix:Water
Analyzed
Styrene ug/L ND 5.0 11/18/15 16:13
Tetrachloroethene ug/L ND 5.0 11/18/15 16:13
Toluene ug/L ND 5.0 11/18/15 16:13
trans-1,2-Dichloroethene ug/L ND 5.0 11/18/15 16:13
trans-1,3-Dichloropropene ug/L ND 5.0 11/18/15 16:13
Trichloroethene ug/L ND 5.0 11/18/15 16:13
Trichlorofluoromethane ug/L ND 10.0 11/18/15 16:13
Vinyl chloride ug/L ND 5.0 11/18/15 16:13
Xylene (Total)ug/L ND 10.0 11/18/15 16:13
1,2-Dichloroethane-d4 (S)%95 70-130 11/18/15 16:13
4-Bromofluorobenzene (S)%105 70-130 11/18/15 16:13
Toluene-d8 (S)%107 70-130 11/18/15 16:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609256LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 52.250 104 71-129
1,1,2,2-Tetrachloroethane ug/L 49.950 100 79-124
1,1,2-Trichloroethane ug/L 52.350 105 85-125
1,1,2-Trichlorotrifluoroethane ug/L 52.050 104 71-142
1,1-Dichloroethane ug/L 49.550 99 73-126
1,1-Dichloroethene ug/L 56.150 112 66-135
1,2,3-Trichlorobenzene ug/L 52.050 104 73-135
1,2,4-Trichlorobenzene ug/L 49.450 99 75-134
1,2-Dibromo-3-chloropropane ug/L 50.450 101 71-133
1,2-Dibromoethane (EDB)ug/L 56.050 112 83-124
1,2-Dichlorobenzene ug/L 50.550 101 80-133
1,2-Dichloroethane ug/L 45.850 92 67-128
1,2-Dichloropropane ug/L 51.250 102 75-132
1,3-Dichlorobenzene ug/L 50.950 102 77-130
1,4-Dichlorobenzene ug/L 50.050 100 78-130
2-Butanone (MEK)ug/L 114100 114 61-144
2-Hexanone ug/L 105100 105 68-143
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 72-135
Acetone ug/L 103100 103 48-146
Benzene ug/L 54.250 108 80-125
Bromochloromethane ug/L 63.0 L05012671-125
Bromodichloromethane ug/L 49.550 99 78-124
Bromoform ug/L 49.650 99 71-128
Bromomethane ug/L 79.250 158 40-160
Carbon disulfide ug/L 57.850 116 50-160
Carbon tetrachloride ug/L 50.750 101 69-131
Chlorobenzene ug/L 49.250 98 81-122
Chloroethane ug/L 50.850 102 39-148
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 32 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609256LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroform ug/L 49.650 99 73-127
Chloromethane ug/L 56.250 112 44-146
cis-1,2-Dichloroethene ug/L 50.350 101 74-124
cis-1,3-Dichloropropene ug/L 53.550 107 72-132
Cyclohexane ug/L 53.350 107 62-145
Dibromochloromethane ug/L 49.950 100 78-125
Dichlorodifluoromethane ug/L 55.550 111 34-157
Ethylbenzene ug/L 48.250 96 79-121
Isopropylbenzene (Cumene)ug/L 52.450 105 81-132
Methyl acetate ug/L 59.350 119 58-128
Methyl-tert-butyl ether ug/L 59.750 119 74-131
Methylcyclohexane ug/L 51.150 102 65-144
Methylene Chloride ug/L 53.850 108 64-133
Styrene ug/L 48.550 97 84-126
Tetrachloroethene ug/L 50.550 101 78-122
Toluene ug/L 48.850 98 80-121
trans-1,2-Dichloroethene ug/L 53.750 107 71-127
trans-1,3-Dichloropropene ug/L 54.650 109 69-141
Trichloroethene ug/L 50.950 102 78-122
Trichlorofluoromethane ug/L 50.750 101 53-137
Vinyl chloride ug/L 60.450 121 58-137
Xylene (Total)ug/L 143150 96 81-126
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1609436MATRIX SPIKE SAMPLE:
MSSpike
Result
92275754003
1,1,1-Trichloroethane ug/L 23.320 117 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,2-Trichloroethane ug/L 21.420 107 70-130ND
1,1,2-Trichlorotrifluoroethane ug/L 23.220 116 70-130ND
1,1-Dichloroethane ug/L 29.120 113 70-1306.5
1,1-Dichloroethene ug/L 26.220 127 65-160ND
1,2,3-Trichlorobenzene ug/L 20.020 100 70-130ND
1,2,4-Trichlorobenzene ug/L 20.020 100 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.220 96 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.920 110 60-139ND
1,2-Dichlorobenzene ug/L 21.620 103 70-130ND
1,2-Dichloroethane ug/L 20.820 101 70-130ND
1,2-Dichloropropane ug/L 22.820 114 70-130ND
1,3-Dichlorobenzene ug/L 21.320 106 70-130ND
1,4-Dichlorobenzene ug/L 21.020 104 70-130ND
2-Butanone (MEK)ug/L 46.340 116 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 33 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1609436MATRIX SPIKE SAMPLE:
MSSpike
Result
92275754003
2-Hexanone ug/L 40.840 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 41.140 103 70-130ND
Acetone ug/L 50.440 96 70-130ND
Benzene ug/L 24.320 122 58-162ND
Bromochloromethane ug/L 25.820 129 70-130ND
Bromodichloromethane ug/L 21.820 109 70-130ND
Bromoform ug/L 17.320 87 70-130ND
Bromomethane ug/L 22.220 111 70-130ND
Carbon disulfide ug/L 25.320 127 70-130ND
Carbon tetrachloride ug/L 23.720 119 70-130ND
Chlorobenzene ug/L 29.520 110 70-1387.5
Chloroethane ug/L 28.9 M12013670-130ND
Chloroform ug/L 22.320 112 70-130ND
Chloromethane ug/L 17.620 88 70-130ND
cis-1,2-Dichloroethene ug/L 23.120 116 70-130ND
cis-1,3-Dichloropropene ug/L 21.520 107 70-130ND
Cyclohexane ug/L 23.620 118 70-130ND
Dibromochloromethane ug/L 18.820 94 70-130ND
Dichlorodifluoromethane ug/L 18.220 91 70-130ND
Ethylbenzene ug/L 21.220 106 22-189ND
Isopropylbenzene (Cumene)ug/L 23.220 116 70-130ND
Methyl acetate ug/L 22.520 112 70-130ND
Methyl-tert-butyl ether ug/L 23.520 117 37-169ND
Methylcyclohexane ug/L 21.920 109 70-130ND
Methylene Chloride ug/L 24.320 121 70-130ND
Styrene ug/L 21.720 108 70-130ND
Tetrachloroethene ug/L 21.620 108 70-130ND
Toluene ug/L 22.220 111 65-152ND
trans-1,2-Dichloroethene ug/L 24.220 121 70-130ND
trans-1,3-Dichloropropene ug/L 21.320 106 70-130ND
Trichloroethene ug/L 23.120 116 70-142ND
Trichlorofluoromethane ug/L 22.720 114 70-130ND
Vinyl chloride ug/L 27.720 128 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92275754004
1609437SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1,2-Trichlorotrifluoroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 34 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275754004
1609437SAMPLE DUPLICATE:
1,1-Dichloroethene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L 8.3 68.9
Chloroethane ug/L 10.2 1411.8
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Cyclohexane ug/L NDND
Dibromochloromethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Isopropylbenzene (Cumene)ug/L NDND
Methyl acetate ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylcyclohexane ug/L NDND
Methylene Chloride ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%98 2100
4-Bromofluorobenzene (S)%101 3105
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 35 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275754004
1609437SAMPLE DUPLICATE:
Toluene-d8 (S)%107 1108
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 36 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34257
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005, 92275754006, 92275754007,
92275754008, 92275754009, 92275754010, 92275754011, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1604959
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005, 92275754006, 92275754007,
92275754008, 92275754009, 92275754010, 92275754011, 92275754012
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/12/15 18:08
1,2-Dichloroethane-d4 (S)%100 50-150 11/12/15 18:08
Toluene-d8 (S)%99 50-150 11/12/15 18:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1604960LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 20.620 103 71-125
1,2-Dichloroethane-d4 (S)%103 50-150
Toluene-d8 (S)%97 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1604961MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754006
1604962
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 97 50-150100 320ND21.0 21.6
1,2-Dichloroethane-d4 (S)%107 50-150106
Toluene-d8 (S)%98 50-15098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 37 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39029
EPA 3510
EPA 8270
8270 Water MSSV HVI
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005, 92275754006, 92275754007,
92275754010, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1605123
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754005, 92275754006, 92275754007,
92275754010, 92275754012
Matrix:Water
Analyzed
Biphenyl (Diphenyl)ug/L ND 10.0 11/13/15 14:56
Diphenyl ether (Phenyl ether)ug/L ND 10.0 11/13/15 14:56
2,4,6-Tribromophenol (S)%39 27-110 11/13/15 14:56
2-Fluorobiphenyl (S)%69 27-110 11/13/15 14:56
2-Fluorophenol (S)%34 12-110 11/13/15 14:56
Nitrobenzene-d5 (S)%73 21-110 11/13/15 14:56
Phenol-d6 (S)%29 10-110 11/13/15 14:56
Terphenyl-d14 (S)%82 31-107 11/13/15 14:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1605124LABORATORY CONTROL SAMPLE:
LCSSpike
Biphenyl (Diphenyl)ug/L 33.450 67 38-120
Diphenyl ether (Phenyl ether)ug/L 33.750 67 51-120
2,4,6-Tribromophenol (S)%95 27-110
2-Fluorobiphenyl (S)%69 27-110
2-Fluorophenol (S)%37 12-110
Nitrobenzene-d5 (S)%77 21-110
Phenol-d6 (S)%25 10-110
Terphenyl-d14 (S)%99 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1605125MATRIX SPIKE SAMPLE:
MSSpike
Result
92275067003
Biphenyl (Diphenyl)ug/L 41.650 83 50-150ND
Diphenyl ether (Phenyl ether)ug/L 41.450 83 50-150ND
2,4,6-Tribromophenol (S)%S012127-110
2-Fluorobiphenyl (S)%91 27-110
2-Fluorophenol (S)%52 12-110
Nitrobenzene-d5 (S)%93 21-110
Phenol-d6 (S)%38 10-110
Terphenyl-d14 (S)%81 31-107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 38 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275067004
1605126SAMPLE DUPLICATE:
Biphenyl (Diphenyl)ug/L NDND
Diphenyl ether (Phenyl ether)ug/L NDND
2,4,6-Tribromophenol (S)%54 552
2-Fluorobiphenyl (S)%70 1279
2-Fluorophenol (S)%41 1038
Nitrobenzene-d5 (S)%73 375
Phenol-d6 (S)%34 1529
Terphenyl-d14 (S)%94 887
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 12:29 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 39 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39091
EPA 3510
EPA 8270
8270 Water MSSV HVI
Associated Lab Samples:92275754011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608030
Associated Lab Samples:92275754011
Matrix:Water
Analyzed
Biphenyl (Diphenyl)ug/L ND 10.0 11/17/15 13:51
Diphenyl ether (Phenyl ether)ug/L ND 10.0 11/17/15 13:51
2,4,6-Tribromophenol (S)%64 27-110 11/17/15 13:51
2-Fluorobiphenyl (S)%82 27-110 11/17/15 13:51
2-Fluorophenol (S)%44 12-110 11/17/15 13:51
Nitrobenzene-d5 (S)%76 21-110 11/17/15 13:51
Phenol-d6 (S)%35 10-110 11/17/15 13:51
Terphenyl-d14 (S)%80 31-107 11/17/15 13:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608031LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1608032
Biphenyl (Diphenyl)ug/L 38.350 77 38-1207839.2 2 30
Diphenyl ether (Phenyl ether)ug/L 34.450 69 51-1207437.1 7 30
2,4,6-Tribromophenol (S)%88 27-11082
2-Fluorobiphenyl (S)%84 27-11079
2-Fluorophenol (S)%47 12-11046
Nitrobenzene-d5 (S)%82 21-11080
Phenol-d6 (S)%31 10-11034
Terphenyl-d14 (S)%92 31-10785
REPORT OF LABORATORY ANALYSIS
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Page 40 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41436
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608082
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 11/18/15 16:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608083LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 49.750 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1608084MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275067004
1608085
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 100 90-110100 0506.0 56.2 56.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1608086MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275794004
1608087
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M1509090-11088 150102147146
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 41 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25365
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1604426
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 11/12/15 07:01
Nitrogen, Nitrite mg/L ND 0.020 11/12/15 07:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1604427LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 2.52.5 98 90-110
Nitrogen, Nitrite mg/L 1.01 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1604428MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754001
1604429
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 91 90-11090 02.5ND 2.3 2.3
Nitrogen, Nitrite mg/L M117790-11077 010.040 0.81 0.81
REPORT OF LABORATORY ANALYSIS
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Page 42 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25364
SM 4500-P E
SM 4500-P E
SM4500P-E Phosphorus, Ortho
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1604413
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004, 92275754012
Matrix:Water
Analyzed
Orthophosphate as P mg/L ND 0.050 11/11/15 22:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1604414LABORATORY CONTROL SAMPLE:
LCSSpike
Orthophosphate as P mg/L 0.27.25 108 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1604415MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754001
1604416
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Orthophosphate as P mg/L M625390-11053 021.3 2.4 2.4
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275754
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25407
EPA 9060A
EPA 9060A
9060 TOC, AVL
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1607246
Associated Lab Samples:92275754001, 92275754002, 92275754003, 92275754004
Matrix:Water
Analyzed
Mean Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1607247LABORATORY CONTROL SAMPLE:
LCSSpike
Mean Total Organic Carbon mg/L 24.025 96 75-125
Total Organic Carbon mg/L 23.925 96 75-125
Total Organic Carbon mg/L 24.025 96 75-125
Total Organic Carbon mg/L 23.825 95 75-125
Total Organic Carbon mg/L 24.125 96 75-125
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1607248MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754001
1607249
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mean Total Organic Carbon mg/L M625-76 75-1250 125275027302750
Total Organic Carbon mg/L M62523675-125596 325269027502840
Total Organic Carbon mg/L M625-196 75-12596 325277027202800
Total Organic Carbon mg/L M625-116 75-125280 425275027202820
Total Organic Carbon mg/L M625-220 75-125-964 725278027202540
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92275754
CNA/NRLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - GreenwoodPASI-G
Pace Analytical Services - IndianapolisPASI-I
Pace Analytical Services - GreenwoodPASI-W
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92275754
CNA/NRLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92275754001 GCSV/17520B-23A EPA 8015 Alcohol-Glycol
92275754002 GCSV/17520B-23B EPA 8015 Alcohol-Glycol
92275754006 GCSV/17520SW-7 EPA 8015 Alcohol-Glycol
92275754007 GCSV/17520SW-5 EPA 8015 Alcohol-Glycol
92275754010 GCSV/17520SW-3 EPA 8015 Alcohol-Glycol
92275754011 GCSV/17520SW-8 EPA 8015 Alcohol-Glycol
92275754012 GCSV/17520B-09C EPA 8015 Alcohol-Glycol
92275754001 GWD/2671B-23A EPA 9056A
92275754002 GWD/2671B-23B EPA 9056A
92275754003 GWD/2671B-22A EPA 9056A
92275754004 GWD/2671B-22B EPA 9056A
92275754012 GWD/2671B-09C EPA 9056A
92275754001 OEXT/39029 MSSV/11519B-23A EPA 3510 EPA 8270
92275754002 OEXT/39029 MSSV/11519B-23B EPA 3510 EPA 8270
92275754003 OEXT/39029 MSSV/11519B-22A EPA 3510 EPA 8270
92275754004 OEXT/39029 MSSV/11519B-22B EPA 3510 EPA 8270
92275754005 OEXT/39029 MSSV/11519B-99B EPA 3510 EPA 8270
92275754006 OEXT/39029 MSSV/11519SW-7 EPA 3510 EPA 8270
92275754007 OEXT/39029 MSSV/11519SW-5 EPA 3510 EPA 8270
92275754010 OEXT/39029 MSSV/11519SW-3 EPA 3510 EPA 8270
92275754011 OEXT/39091 MSSV/11531SW-8 EPA 3510 EPA 8270
92275754012 OEXT/39029 MSSV/11519B-09C EPA 3510 EPA 8270
92275754001 MSV/34335B-23A EPA 8260
92275754002 MSV/34335B-23B EPA 8260
92275754003 MSV/34335B-22A EPA 8260
92275754004 MSV/34335B-22B EPA 8260
92275754005 MSV/34335B-99B EPA 8260
92275754012 MSV/34316B-09C EPA 8260
92275754001 MSV/34257B-23A EPA 8260B Mod.
92275754002 MSV/34257B-23B EPA 8260B Mod.
92275754003 MSV/34257B-22A EPA 8260B Mod.
92275754004 MSV/34257B-22B EPA 8260B Mod.
92275754005 MSV/34257B-99B EPA 8260B Mod.
92275754006 MSV/34257SW-7 EPA 8260B Mod.
92275754007 MSV/34257SW-5 EPA 8260B Mod.
92275754008 MSV/34257CSW-2 EPA 8260B Mod.
92275754009 MSV/34257CSW-1 EPA 8260B Mod.
92275754010 MSV/34257SW-3 EPA 8260B Mod.
92275754011 MSV/34257SW-8 EPA 8260B Mod.
92275754012 MSV/34257B-09C EPA 8260B Mod.
92275754001 WET/41436B-23A SM 2320B
92275754002 WET/41436B-23B SM 2320B
92275754003 WET/41436B-22A SM 2320B
92275754004 WET/41436B-22B SM 2320B
92275754012 WET/41436B-09C SM 2320B
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92275754
CNA/NRLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92275754001 WETA/25365B-23A EPA 353.2
92275754002 WETA/25365B-23B EPA 353.2
92275754003 WETA/25365B-22A EPA 353.2
92275754004 WETA/25365B-22B EPA 353.2
92275754012 WETA/25365B-09C EPA 353.2
92275754001 WETA/25364B-23A SM 4500-P E
92275754002 WETA/25364B-23B SM 4500-P E
92275754003 WETA/25364B-22A SM 4500-P E
92275754004 WETA/25364B-22B SM 4500-P E
92275754012 WETA/25364B-09C SM 4500-P E
92275754001 WETA/25407B-23A EPA 9060A
92275754002 WETA/25407B-23B EPA 9060A
92275754003 WETA/25407B-22A EPA 9060A
92275754004 WETA/25407B-22B EPA 9060A
REPORT OF LABORATORY ANALYSIS
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#=CL#
November 25, 2015
LIMS USE: FR - BRYON DAHLGREN
LIMS OBJECT ID: 92275972
92275972
Project:
Pace Project No.:
RE:
Bryon Dahlgren
AECOM
10 Patewood Drive, Bldg 6
Suite 500
Greenville, SC 29615
CNA/NRLF
Dear Bryon Dahlgren:
Enclosed are the analytical results for sample(s) received by the laboratory on November 12, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 55
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92275972
CNA/NRLF
Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074
Indiana Certification #: C-49-06Kansas Certification #:E-10177Kentucky UST Certification #: 0042Kentucky WW Certification #:98019Louisiana Certification #: 04076
Ohio VAP Certification #: CL-0065Oklahoma Certification #: 2014-148
Texas Certification #: T104704355-15-9West Virginia Certification #: 330Wisconsin Certification #: 999788130USDA Soil Permit #: P330-10-00128
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
Greenwood Certification IDs
816 Durst Avenue East, Greenwood, SC 29649South Carolina Laboratory ID #: 24562North Carolina Divison of Water Resources Certification
number 25
Florida Certification number E87633Virginia VELAP ID: 460250
Asbestos NVLAP accreditation: 101410-0
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92275972
CNA/NRLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92275972001 B-17C EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 8 PASI-CRES
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275972002 B-17B EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 8 PASI-CRES
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275972003 B-01 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CRES
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275972004 B-10 EPA 8015 Alcohol-Glycol 1 PASI-IBJW
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CRES
EPA 8260 53 PASI-CCCL
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275972005 B-32B EPA 8015 Alcohol-Glycol 1 PASI-IBJW
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92275972
CNA/NRLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CRES
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
EPA 9060A 5 PASI-AMDW
92275972006 B-12 EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8270 3 PASI-CRES
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
92275972007 B-21B EPA 9056A 1 PASI-GCDC
EPA 9056A 1 PASI-WCDC
EPA 8260B Mod.3 PASI-CDLK
SM 2320B 1 PASI-AMLS
EPA 353.2 2 PASI-ASER
SM 4500-P E 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-17C Lab ID:92275972001 Collected:11/11/15 08:25 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 1.4 mg/L 11/19/15 18:50 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/19/15 13:46 92-52-4 M111/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/19/15 13:46 101-84-8 M111/18/15 13:3010.0 1
Surrogates
Nitrobenzene-d5 (S)33 %11/19/15 13:46 4165-60-011/18/15 13:3021-110 1
2-Fluorobiphenyl (S)31 %11/19/15 13:46 321-60-811/18/15 13:3027-110 1
Terphenyl-d14 (S)46 %11/19/15 13:46 1718-51-011/18/15 13:3031-107 1
Phenol-d6 (S)13 %11/19/15 13:46 13127-88-311/18/15 13:3010-110 1
2-Fluorophenol (S)17 %11/19/15 13:46 367-12-411/18/15 13:3012-110 1
2,4,6-Tribromophenol (S)27 %11/19/15 13:46 118-79-611/18/15 13:3027-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)1810 ug/L 11/13/15 15:53 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/13/15 15:53 17060-07-050-150 50
Toluene-d8 (S)91 %11/13/15 15:53 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 329 mg/L 11/22/15 13:315.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 23:490.020 1
Nitrogen, Nitrite ND mg/L 11/12/15 23:490.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.34 mg/L 11/12/15 23:05 M10.050 1
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 61.2 mg/L 11/16/15 18:07 7440-44-02.0 2
Total Organic Carbon 58.4 mg/L 11/16/15 18:07 7440-44-02.0 2
Total Organic Carbon 59.1 mg/L 11/16/15 18:07 7440-44-02.0 2
Total Organic Carbon 59.8 mg/L 11/16/15 18:07 7440-44-02.0 2
Mean Total Organic Carbon 59.6 mg/L 11/16/15 18:07 7440-44-02.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 5 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-17B Lab ID:92275972002 Collected:11/11/15 09:30 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 2.3 mg/L 11/19/15 20:03 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/19/15 15:00 92-52-411/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/19/15 15:00 101-84-811/18/15 13:3010.0 1
Surrogates
Nitrobenzene-d5 (S)67 %11/19/15 15:00 4165-60-011/18/15 13:3021-110 1
2-Fluorobiphenyl (S)67 %11/19/15 15:00 321-60-811/18/15 13:3027-110 1
Terphenyl-d14 (S)57 %11/19/15 15:00 1718-51-011/18/15 13:3031-107 1
Phenol-d6 (S)13 %11/19/15 15:00 13127-88-311/18/15 13:3010-110 1
2-Fluorophenol (S)7 %11/19/15 15:00 367-12-4 S211/18/15 13:3012-110 1
2,4,6-Tribromophenol (S)12 %11/19/15 15:00 118-79-6 S211/18/15 13:3027-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)135 ug/L 11/13/15 16:14 123-91-110.0 5
Surrogates
1,2-Dichloroethane-d4 (S)100 %11/13/15 16:14 17060-07-050-150 5
Toluene-d8 (S)91 %11/13/15 16:14 2037-26-550-150 5
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 240 mg/L 11/22/15 13:485.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/12/15 23:590.020 1
Nitrogen, Nitrite ND mg/L 11/12/15 23:590.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.16 mg/L 11/12/15 23:050.050 1
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 53.3 mg/L 11/16/15 18:20 7440-44-02.0 2
Total Organic Carbon 52.5 mg/L 11/16/15 18:20 7440-44-02.0 2
Total Organic Carbon 53.1 mg/L 11/16/15 18:20 7440-44-02.0 2
Total Organic Carbon 53.0 mg/L 11/16/15 18:20 7440-44-02.0 2
Mean Total Organic Carbon 53.0 mg/L 11/16/15 18:20 7440-44-02.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 6 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-01 Lab ID:92275972003 Collected:11/11/15 14:05 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 16:18 107-21-1 D350.0 10
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 28.5 mg/L 11/19/15 21:17 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/19/15 15:50 92-52-411/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)122 ug/L 11/19/15 15:50 101-84-811/18/15 13:3010.0 1
Surrogates
2-Fluorobiphenyl (S)162 %11/19/15 15:50 321-60-8 S511/18/15 13:3027-110 1
Analytical Method: EPA 82608260 MSV
Acetone ND ug/L 11/17/15 19:35 67-64-1125050
Benzene ND ug/L 11/17/15 19:35 71-43-225050
Bromochloromethane ND ug/L 11/17/15 19:35 74-97-525050
Bromodichloromethane ND ug/L 11/17/15 19:35 75-27-425050
Bromoform ND ug/L 11/17/15 19:35 75-25-225050
Bromomethane ND ug/L 11/17/15 19:35 74-83-950050
2-Butanone (MEK)ND ug/L 11/17/15 19:35 78-93-350050
Carbon disulfide ND ug/L 11/17/15 19:35 75-15-050050
Carbon tetrachloride ND ug/L 11/17/15 19:35 56-23-525050
Chlorobenzene ND ug/L 11/17/15 19:35 108-90-725050
Chloroethane ND ug/L 11/17/15 19:35 75-00-350050
Chloroform ND ug/L 11/17/15 19:35 67-66-325050
Chloromethane ND ug/L 11/17/15 19:35 74-87-325050
Cyclohexane ND ug/L 11/17/15 19:35 110-82-725050
1,2-Dibromo-3-chloropropane ND ug/L 11/17/15 19:35 96-12-810050
Dibromochloromethane ND ug/L 11/17/15 19:35 124-48-125050
1,2-Dibromoethane (EDB)ND ug/L 11/17/15 19:35 106-93-425050
1,2-Dichlorobenzene ND ug/L 11/17/15 19:35 95-50-125050
1,3-Dichlorobenzene ND ug/L 11/17/15 19:35 541-73-125050
1,4-Dichlorobenzene ND ug/L 11/17/15 19:35 106-46-725050
Dichlorodifluoromethane ND ug/L 11/17/15 19:35 75-71-825050
1,1-Dichloroethane ND ug/L 11/17/15 19:35 75-34-325050
1,2-Dichloroethane ND ug/L 11/17/15 19:35 107-06-225050
1,1-Dichloroethene ND ug/L 11/17/15 19:35 75-35-425050
cis-1,2-Dichloroethene ND ug/L 11/17/15 19:35 156-59-225050
trans-1,2-Dichloroethene ND ug/L 11/17/15 19:35 156-60-525050
1,2-Dichloropropane ND ug/L 11/17/15 19:35 78-87-525050
cis-1,3-Dichloropropene ND ug/L 11/17/15 19:35 10061-01-525050
trans-1,3-Dichloropropene ND ug/L 11/17/15 19:35 10061-02-625050
Ethylbenzene ND ug/L 11/17/15 19:35 100-41-425050
2-Hexanone ND ug/L 11/17/15 19:35 591-78-650050
Isopropylbenzene (Cumene)ND ug/L 11/17/15 19:35 98-82-825050
Methyl acetate ND ug/L 11/17/15 19:35 79-20-950050
Methylcyclohexane ND ug/L 11/17/15 19:35 108-87-250050
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 7 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-01 Lab ID:92275972003 Collected:11/11/15 14:05 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Methylene Chloride ND ug/L 11/17/15 19:35 75-09-225050
4-Methyl-2-pentanone (MIBK)ND ug/L 11/17/15 19:35 108-10-150050
Methyl-tert-butyl ether ND ug/L 11/17/15 19:35 1634-04-425050
Styrene ND ug/L 11/17/15 19:35 100-42-525050
1,1,2,2-Tetrachloroethane ND ug/L 11/17/15 19:35 79-34-525050
Tetrachloroethene ND ug/L 11/17/15 19:35 127-18-425050
Toluene ND ug/L 11/17/15 19:35 108-88-325050
1,2,3-Trichlorobenzene ND ug/L 11/17/15 19:35 87-61-625050
1,2,4-Trichlorobenzene ND ug/L 11/17/15 19:35 120-82-125050
1,1,1-Trichloroethane ND ug/L 11/17/15 19:35 71-55-625050
1,1,2-Trichloroethane ND ug/L 11/17/15 19:35 79-00-525050
Trichloroethene ND ug/L 11/17/15 19:35 79-01-625050
Trichlorofluoromethane ND ug/L 11/17/15 19:35 75-69-450050
1,1,2-Trichlorotrifluoroethane ND ug/L 11/17/15 19:35 76-13-125050
Vinyl chloride ND ug/L 11/17/15 19:35 75-01-425050
Xylene (Total)ND ug/L 11/17/15 19:35 1330-20-750050
Surrogates
4-Bromofluorobenzene (S)99 %11/17/15 19:35 460-00-4 D370-130 50
1,2-Dichloroethane-d4 (S)104 %11/17/15 19:35 17060-07-070-130 50
Toluene-d8 (S)102 %11/17/15 19:35 2037-26-570-130 50
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2640 ug/L 11/13/15 16:34 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)109 %11/13/15 16:34 17060-07-050-150 50
Toluene-d8 (S)90 %11/13/15 16:34 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 1430 mg/L 11/23/15 02:125.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/13/15 00:170.020 1
Nitrogen, Nitrite ND mg/L 11/13/15 00:170.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.94 mg/L 11/12/15 23:050.25 5
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 3620 mg/L 11/16/15 15:59 7440-44-0100100
Total Organic Carbon 3660 mg/L 11/16/15 15:59 7440-44-0100100
Total Organic Carbon 3640 mg/L 11/16/15 15:59 7440-44-0100100
Total Organic Carbon 3290 mg/L 11/16/15 15:59 7440-44-0100100
Mean Total Organic Carbon 3550 mg/L 11/16/15 15:59 7440-44-0100100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 8 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-10 Lab ID:92275972004 Collected:11/11/15 15:50 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 16:28 107-21-1 D350.0 10
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 11/19/15 21:41 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)192 ug/L 11/19/15 16:15 92-52-411/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)2110 ug/L 11/20/15 11:11 101-84-811/18/15 13:3010010
Surrogates
2-Fluorobiphenyl (S)79 %11/19/15 16:15 321-60-811/18/15 13:3027-110 1
Analytical Method: EPA 82608260 MSV
Acetone ND ug/L 11/17/15 19:52 67-64-162525
Benzene ND ug/L 11/17/15 19:52 71-43-212525
Bromochloromethane ND ug/L 11/17/15 19:52 74-97-512525
Bromodichloromethane ND ug/L 11/17/15 19:52 75-27-412525
Bromoform ND ug/L 11/17/15 19:52 75-25-212525
Bromomethane ND ug/L 11/17/15 19:52 74-83-925025
2-Butanone (MEK)ND ug/L 11/17/15 19:52 78-93-325025
Carbon disulfide ND ug/L 11/17/15 19:52 75-15-025025
Carbon tetrachloride ND ug/L 11/17/15 19:52 56-23-512525
Chlorobenzene ND ug/L 11/17/15 19:52 108-90-712525
Chloroethane ND ug/L 11/17/15 19:52 75-00-325025
Chloroform ND ug/L 11/17/15 19:52 67-66-312525
Chloromethane ND ug/L 11/17/15 19:52 74-87-312525
Cyclohexane ND ug/L 11/17/15 19:52 110-82-712525
1,2-Dibromo-3-chloropropane ND ug/L 11/17/15 19:52 96-12-850.0 25
Dibromochloromethane ND ug/L 11/17/15 19:52 124-48-112525
1,2-Dibromoethane (EDB)ND ug/L 11/17/15 19:52 106-93-412525
1,2-Dichlorobenzene ND ug/L 11/17/15 19:52 95-50-112525
1,3-Dichlorobenzene ND ug/L 11/17/15 19:52 541-73-112525
1,4-Dichlorobenzene ND ug/L 11/17/15 19:52 106-46-712525
Dichlorodifluoromethane ND ug/L 11/17/15 19:52 75-71-812525
1,1-Dichloroethane ND ug/L 11/17/15 19:52 75-34-312525
1,2-Dichloroethane ND ug/L 11/17/15 19:52 107-06-212525
1,1-Dichloroethene ND ug/L 11/17/15 19:52 75-35-412525
cis-1,2-Dichloroethene ND ug/L 11/17/15 19:52 156-59-212525
trans-1,2-Dichloroethene ND ug/L 11/17/15 19:52 156-60-512525
1,2-Dichloropropane ND ug/L 11/17/15 19:52 78-87-512525
cis-1,3-Dichloropropene ND ug/L 11/17/15 19:52 10061-01-512525
trans-1,3-Dichloropropene ND ug/L 11/17/15 19:52 10061-02-612525
Ethylbenzene ND ug/L 11/17/15 19:52 100-41-412525
2-Hexanone ND ug/L 11/17/15 19:52 591-78-625025
Isopropylbenzene (Cumene)ND ug/L 11/17/15 19:52 98-82-812525
Methyl acetate ND ug/L 11/17/15 19:52 79-20-925025
Methylcyclohexane ND ug/L 11/17/15 19:52 108-87-225025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 9 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-10 Lab ID:92275972004 Collected:11/11/15 15:50 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV
Methylene Chloride ND ug/L 11/17/15 19:52 75-09-212525
4-Methyl-2-pentanone (MIBK)ND ug/L 11/17/15 19:52 108-10-125025
Methyl-tert-butyl ether ND ug/L 11/17/15 19:52 1634-04-412525
Styrene ND ug/L 11/17/15 19:52 100-42-512525
1,1,2,2-Tetrachloroethane ND ug/L 11/17/15 19:52 79-34-512525
Tetrachloroethene ND ug/L 11/17/15 19:52 127-18-412525
Toluene ND ug/L 11/17/15 19:52 108-88-312525
1,2,3-Trichlorobenzene ND ug/L 11/17/15 19:52 87-61-612525
1,2,4-Trichlorobenzene ND ug/L 11/17/15 19:52 120-82-112525
1,1,1-Trichloroethane ND ug/L 11/17/15 19:52 71-55-612525
1,1,2-Trichloroethane ND ug/L 11/17/15 19:52 79-00-512525
Trichloroethene ND ug/L 11/17/15 19:52 79-01-612525
Trichlorofluoromethane ND ug/L 11/17/15 19:52 75-69-425025
1,1,2-Trichlorotrifluoroethane ND ug/L 11/17/15 19:52 76-13-112525
Vinyl chloride ND ug/L 11/17/15 19:52 75-01-412525
Xylene (Total)ND ug/L 11/17/15 19:52 1330-20-725025
Surrogates
4-Bromofluorobenzene (S)99 %11/17/15 19:52 460-00-4 D370-130 25
1,2-Dichloroethane-d4 (S)101 %11/17/15 19:52 17060-07-070-130 25
Toluene-d8 (S)101 %11/17/15 19:52 2037-26-570-130 25
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)404 ug/L 11/13/15 16:54 123-91-120.0 10
Surrogates
1,2-Dichloroethane-d4 (S)104 %11/13/15 16:54 17060-07-050-150 10
Toluene-d8 (S)92 %11/13/15 16:54 2037-26-550-150 10
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 694 mg/L 11/22/15 15:355.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/13/15 00:390.020 1
Nitrogen, Nitrite 0.067 mg/L 11/13/15 00:390.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.68 mg/L 11/12/15 23:050.20 4
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 31.6 mg/L 11/16/15 18:45 7440-44-02.0 2
Total Organic Carbon 29.7 mg/L 11/16/15 18:45 7440-44-02.0 2
Total Organic Carbon 30.9 mg/L 11/16/15 18:45 7440-44-02.0 2
Total Organic Carbon 30.7 mg/L 11/16/15 18:45 7440-44-02.0 2
Mean Total Organic Carbon 30.7 mg/L 11/16/15 18:45 7440-44-02.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 10 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-32B Lab ID:92275972005 Collected:11/11/15 12:30 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Alcohol-Glycol8015M Glycols in water
Ethylene glycol ND mg/L 11/17/15 16:37 107-21-1 D350.0 10
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate ND mg/L 11/19/15 22:05 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/19/15 16:40 92-52-411/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/19/15 16:40 101-84-811/18/15 13:3010.0 1
Surrogates
2-Fluorobiphenyl (S)74 %11/19/15 16:40 321-60-811/18/15 13:3027-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)18.3 ug/L 11/13/15 17:14 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %11/13/15 17:14 17060-07-050-150 1
Toluene-d8 (S)89 %11/13/15 17:14 2037-26-550-150 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 194 mg/L 11/22/15 16:255.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 0.14 mg/L 11/13/15 00:140.020 1
Nitrogen, Nitrite ND mg/L 11/13/15 00:140.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.13 mg/L 11/12/15 23:050.050 1
Analytical Method: EPA 9060ATotal Organic Carbon,Asheville
Total Organic Carbon 40.8 mg/L 11/16/15 18:58 7440-44-02.0 2
Total Organic Carbon 39.1 mg/L 11/16/15 18:58 7440-44-02.0 2
Total Organic Carbon 39.8 mg/L 11/16/15 18:58 7440-44-02.0 2
Total Organic Carbon 40.2 mg/L 11/16/15 18:58 7440-44-02.0 2
Mean Total Organic Carbon 40.0 mg/L 11/16/15 18:58 7440-44-02.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 11 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-12 Lab ID:92275972006 Collected:11/11/15 10:20 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 1.2 mg/L 11/19/15 22:30 14808-79-81.0 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV HVI Semivol Organic
Biphenyl (Diphenyl)ND ug/L 11/19/15 17:05 92-52-411/18/15 13:3010.0 1
Diphenyl ether (Phenyl ether)ND ug/L 11/19/15 17:05 101-84-811/18/15 13:3010.0 1
Surrogates
2-Fluorobiphenyl (S)83 %11/19/15 17:05 321-60-811/18/15 13:3027-110 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2900 ug/L 11/13/15 17:34 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/13/15 17:34 17060-07-050-150 50
Toluene-d8 (S)90 %11/13/15 17:34 2037-26-550-150 50
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 313 mg/L 11/22/15 16:405.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/13/15 00:000.020 1
Nitrogen, Nitrite ND mg/L 11/13/15 00:000.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.20 mg/L 11/12/15 23:050.050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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Greenwood, SC 29649
[phone]
Page 12 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275972
CNA/NRLF
Sample:B-21B Lab ID:92275972007 Collected:11/11/15 11:20 Received:11/12/15 06:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Sulfate 15.1 mg/L 11/19/15 22:54 14808-79-81.0 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)92.0 ug/L 11/13/15 17:54 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %11/13/15 17:54 17060-07-050-150 1
Toluene-d8 (S)89 %11/13/15 17:54 2037-26-550-150 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 282 mg/L 11/22/15 16:565.0 1
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND mg/L 11/13/15 00:030.020 1
Nitrogen, Nitrite ND mg/L 11/13/15 00:030.020 1
Analytical Method: SM 4500-P ESM4500P-E, Phosphate, Ortho
Orthophosphate as P 0.25 mg/L 11/12/15 23:050.050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 13 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/17520
EPA 8015 Alcohol-Glycol
EPA 8015 Alcohol-Glycol
EPA 8015 Modified
Associated Lab Samples:92275972003, 92275972004, 92275972005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1426234
Associated Lab Samples:
Matrix:Water
Analyzed
Ethylene glycol mg/L ND 5.0 11/17/15 12:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1426235LABORATORY CONTROL SAMPLE:
LCSSpike
Ethylene glycol mg/L 22.425 89 79-129
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 14 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GWD/2674
EPA 9056A
EPA 9056A
9056 IC Anions, GWD
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1610278
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 11/19/15 10:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1610279LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 49.050 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1610280MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275972001
1610281
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 95 90-11096 0501.4 49.1 49.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 15 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34316
EPA 8260
EPA 8260
8260 MSV
Associated Lab Samples:92275972003, 92275972004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608047
Associated Lab Samples:92275972003, 92275972004
Matrix:Water
Analyzed
1,1,1-Trichloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2,2-Tetrachloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2-Trichloroethane ug/L ND 5.0 11/17/15 14:29
1,1,2-Trichlorotrifluoroethane ug/L ND 5.0 11/17/15 14:29
1,1-Dichloroethane ug/L ND 5.0 11/17/15 14:29
1,1-Dichloroethene ug/L ND 5.0 11/17/15 14:29
1,2,3-Trichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2,4-Trichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/17/15 14:29
1,2-Dibromoethane (EDB)ug/L ND 5.0 11/17/15 14:29
1,2-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,2-Dichloroethane ug/L ND 5.0 11/17/15 14:29
1,2-Dichloropropane ug/L ND 5.0 11/17/15 14:29
1,3-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
1,4-Dichlorobenzene ug/L ND 5.0 11/17/15 14:29
2-Butanone (MEK)ug/L ND 10.0 11/17/15 14:29
2-Hexanone ug/L ND 10.0 11/17/15 14:29
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 11/17/15 14:29
Acetone ug/L ND 25.0 11/17/15 14:29
Benzene ug/L ND 5.0 11/17/15 14:29
Bromochloromethane ug/L ND 5.0 11/17/15 14:29
Bromodichloromethane ug/L ND 5.0 11/17/15 14:29
Bromoform ug/L ND 5.0 11/17/15 14:29
Bromomethane ug/L ND 10.0 11/17/15 14:29
Carbon disulfide ug/L ND 10.0 11/17/15 14:29
Carbon tetrachloride ug/L ND 5.0 11/17/15 14:29
Chlorobenzene ug/L ND 5.0 11/17/15 14:29
Chloroethane ug/L ND 10.0 11/17/15 14:29
Chloroform ug/L ND 5.0 11/17/15 14:29
Chloromethane ug/L ND 5.0 11/17/15 14:29
cis-1,2-Dichloroethene ug/L ND 5.0 11/17/15 14:29
cis-1,3-Dichloropropene ug/L ND 5.0 11/17/15 14:29
Cyclohexane ug/L ND 5.0 11/17/15 14:29
Dibromochloromethane ug/L ND 5.0 11/17/15 14:29
Dichlorodifluoromethane ug/L ND 5.0 11/17/15 14:29
Ethylbenzene ug/L ND 5.0 11/17/15 14:29
Isopropylbenzene (Cumene)ug/L ND 5.0 11/17/15 14:29
Methyl acetate ug/L ND 10.0 11/17/15 14:29
Methyl-tert-butyl ether ug/L ND 5.0 11/17/15 14:29
Methylcyclohexane ug/L ND 10.0 11/17/15 14:29
Methylene Chloride ug/L ND 5.0 11/17/15 14:29
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 16 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608047
Associated Lab Samples:92275972003, 92275972004
Matrix:Water
Analyzed
Styrene ug/L ND 5.0 11/17/15 14:29
Tetrachloroethene ug/L ND 5.0 11/17/15 14:29
Toluene ug/L ND 5.0 11/17/15 14:29
trans-1,2-Dichloroethene ug/L ND 5.0 11/17/15 14:29
trans-1,3-Dichloropropene ug/L ND 5.0 11/17/15 14:29
Trichloroethene ug/L ND 5.0 11/17/15 14:29
Trichlorofluoromethane ug/L ND 10.0 11/17/15 14:29
Vinyl chloride ug/L ND 5.0 11/17/15 14:29
Xylene (Total)ug/L ND 10.0 11/17/15 14:29
1,2-Dichloroethane-d4 (S)%99 70-130 11/17/15 14:29
4-Bromofluorobenzene (S)%100 70-130 11/17/15 14:29
Toluene-d8 (S)%102 70-130 11/17/15 14:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608048LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 44.950 90 71-129
1,1,2,2-Tetrachloroethane ug/L 47.250 94 79-124
1,1,2-Trichloroethane ug/L 44.450 89 85-125
1,1,2-Trichlorotrifluoroethane ug/L 47.950 96 71-142
1,1-Dichloroethane ug/L 43.150 86 73-126
1,1-Dichloroethene ug/L 48.550 97 66-135
1,2,3-Trichlorobenzene ug/L 49.750 99 73-135
1,2,4-Trichlorobenzene ug/L 48.150 96 75-134
1,2-Dibromo-3-chloropropane ug/L 48.750 97 71-133
1,2-Dibromoethane (EDB)ug/L 53.050 106 83-124
1,2-Dichlorobenzene ug/L 50.450 101 80-133
1,2-Dichloroethane ug/L 47.450 95 67-128
1,2-Dichloropropane ug/L 46.250 92 75-132
1,3-Dichlorobenzene ug/L 50.450 101 77-130
1,4-Dichlorobenzene ug/L 49.450 99 78-130
2-Butanone (MEK)ug/L 98.2100 98 61-144
2-Hexanone ug/L 98.2100 98 68-143
4-Methyl-2-pentanone (MIBK)ug/L 90.9100 91 72-135
Acetone ug/L 89.8100 90 48-146
Benzene ug/L 48.150 96 80-125
Bromochloromethane ug/L 57.150 114 71-125
Bromodichloromethane ug/L 44.550 89 78-124
Bromoform ug/L 47.150 94 71-128
Bromomethane ug/L 53.950 108 40-160
Carbon disulfide ug/L 47.650 95 50-160
Carbon tetrachloride ug/L 46.850 94 69-131
Chlorobenzene ug/L 47.850 96 81-122
Chloroethane ug/L 50.550 101 39-148
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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Greenwood, SC 29649
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Page 17 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608048LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroform ug/L 50.150 100 73-127
Chloromethane ug/L 49.050 98 44-146
cis-1,2-Dichloroethene ug/L 50.450 101 74-124
cis-1,3-Dichloropropene ug/L 48.050 96 72-132
Cyclohexane ug/L 47.550 95 62-145
Dibromochloromethane ug/L 51.550 103 78-125
Dichlorodifluoromethane ug/L 51.350 103 34-157
Ethylbenzene ug/L 48.050 96 79-121
Isopropylbenzene (Cumene)ug/L 53.050 106 81-132
Methyl acetate ug/L 59.150 118 58-128
Methyl-tert-butyl ether ug/L 50.650 101 74-131
Methylcyclohexane ug/L 47.550 95 65-144
Methylene Chloride ug/L 50.150 100 64-133
Styrene ug/L 49.950 100 84-126
Tetrachloroethene ug/L 49.850 100 78-122
Toluene ug/L 42.050 84 80-121
trans-1,2-Dichloroethene ug/L 46.750 93 71-127
trans-1,3-Dichloropropene ug/L 46.950 94 69-141
Trichloroethene ug/L 45.950 92 78-122
Trichlorofluoromethane ug/L 47.550 95 53-137
Vinyl chloride ug/L 50.150 100 58-137
Xylene (Total)ug/L 146150 97 81-126
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%93 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1608049MATRIX SPIKE SAMPLE:
MSSpike
Result
92275933004
1,1,1-Trichloroethane ug/L 18.120 90 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.820 99 70-130ND
1,1,2-Trichloroethane ug/L 16.720 84 70-130ND
1,1,2-Trichlorotrifluoroethane ug/L 17.720 89 70-130ND
1,1-Dichloroethane ug/L 17.220 86 70-130ND
1,1-Dichloroethene ug/L 18.620 93 65-160ND
1,2,3-Trichlorobenzene ug/L 19.220 96 70-130ND
1,2,4-Trichlorobenzene ug/L 18.820 94 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.220 106 60-139ND
1,2-Dichlorobenzene ug/L 21.120 106 70-130ND
1,2-Dichloroethane ug/L 16.420 82 70-130ND
1,2-Dichloropropane ug/L 18.120 91 70-130ND
1,3-Dichlorobenzene ug/L 21.420 107 70-130ND
1,4-Dichlorobenzene ug/L 20.920 104 70-130ND
2-Butanone (MEK)ug/L 35.040 88 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
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Page 18 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1608049MATRIX SPIKE SAMPLE:
MSSpike
Result
92275933004
2-Hexanone ug/L 40.640 101 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 34.640 87 70-130ND
Acetone ug/L 37.4 M1404670-13019.1J
Benzene ug/L 22.920 96 58-1623.8J
Bromochloromethane ug/L 18.620 93 70-130ND
Bromodichloromethane ug/L 17.920 89 70-130ND
Bromoform ug/L 16.320 81 70-130ND
Bromomethane ug/L 12.3 M1206170-130ND
Carbon disulfide ug/L 17.220 86 70-130ND
Carbon tetrachloride ug/L 19.220 96 70-130ND
Chlorobenzene ug/L 21.520 107 70-138ND
Chloroethane ug/L 16.220 81 70-130ND
Chloroform ug/L 18.320 92 70-130ND
Chloromethane ug/L 18.220 91 70-130ND
cis-1,2-Dichloroethene ug/L 17.920 89 70-130ND
cis-1,3-Dichloropropene ug/L 17.320 86 70-130ND
Cyclohexane ug/L 19.620 86 70-1302.4J
Dibromochloromethane ug/L 19.620 98 70-130ND
Dichlorodifluoromethane ug/L 17.520 88 70-130ND
Ethylbenzene ug/L 20.920 100 22-189ND
Isopropylbenzene (Cumene)ug/L 27.820 105 70-1306.8
Methyl acetate ug/L 16.120 81 70-130ND
Methyl-tert-butyl ether ug/L 18.120 86 37-169ND
Methylcyclohexane ug/L 18.420 83 70-130ND
Methylene Chloride ug/L 15.620 78 70-130ND
Styrene ug/L 20.720 104 70-130ND
Tetrachloroethene ug/L 21.420 107 70-130ND
Toluene ug/L 17.020 85 65-152ND
trans-1,2-Dichloroethene ug/L 17.720 89 70-130ND
trans-1,3-Dichloropropene ug/L 16.820 84 70-130ND
Trichloroethene ug/L 17.620 88 70-142ND
Trichlorofluoromethane ug/L 18.520 92 70-130ND
Vinyl chloride ug/L 18.420 92 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1,2-Trichlorotrifluoroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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Greenwood, SC 29649
[phone]
Page 19 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
1,1-Dichloroethene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L ND22.5J
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Cyclohexane ug/L NDND
Dibromochloromethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Isopropylbenzene (Cumene)ug/L NDND
Methyl acetate ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylcyclohexane ug/L NDND
Methylene Chloride ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%99 199
4-Bromofluorobenzene (S)%99 297
REPORT OF LABORATORY ANALYSIS
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Greenwood, SC 29649
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Page 20 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275933005
1608050SAMPLE DUPLICATE:
Toluene-d8 (S)%103 1103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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Greenwood, SC 29649
[phone]
Page 21 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34275
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1606378
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/13/15 15:33
1,2-Dichloroethane-d4 (S)%100 50-150 11/13/15 15:33
Toluene-d8 (S)%91 50-150 11/13/15 15:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1606379LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 22.320 111 71-125
1,2-Dichloroethane-d4 (S)%100 50-150
Toluene-d8 (S)%92 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1606380MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276008003
1606381
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 101 50-150106 620ND20.1 21.3
1,2-Dichloroethane-d4 (S)%102 50-150102
Toluene-d8 (S)%89 50-15088
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 22 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39138
EPA 3510
EPA 8270
8270 Water MSSV HVI
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1609395
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006
Matrix:Water
Analyzed
Biphenyl (Diphenyl)ug/L ND 10.0 11/19/15 11:17
Diphenyl ether (Phenyl ether)ug/L ND 10.0 11/19/15 11:17
2,4,6-Tribromophenol (S)%57 27-110 11/19/15 11:17
2-Fluorobiphenyl (S)%78 27-110 11/19/15 11:17
2-Fluorophenol (S)%42 12-110 11/19/15 11:17
Nitrobenzene-d5 (S)%77 21-110 11/19/15 11:17
Phenol-d6 (S)%35 10-110 11/19/15 11:17
Terphenyl-d14 (S)%69 31-107 11/19/15 11:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1609396LABORATORY CONTROL SAMPLE:
LCSSpike
Biphenyl (Diphenyl)ug/L 30.150 60 38-120
Diphenyl ether (Phenyl ether)ug/L 27.050 54 51-120
2,4,6-Tribromophenol (S)%69 27-110
2-Fluorobiphenyl (S)%63 27-110
2-Fluorophenol (S)%41 12-110
Nitrobenzene-d5 (S)%66 21-110
Phenol-d6 (S)%31 10-110
Terphenyl-d14 (S)%64 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1609397MATRIX SPIKE SAMPLE:
MSSpike
Result
92275972001
Biphenyl (Diphenyl)ug/L 15.2 M1503050-150ND
Diphenyl ether (Phenyl ether)ug/L 13.3 M1502750-150ND
2,4,6-Tribromophenol (S)%62 27-110
2-Fluorobiphenyl (S)%31 27-110
2-Fluorophenol (S)%19 12-110
Nitrobenzene-d5 (S)%33 21-110
Phenol-d6 (S)%12 10-110
Terphenyl-d14 (S)%55 31-107
Parameter Units
Dup
Result QualifiersRPDResult
92275972002
1609398SAMPLE DUPLICATE:
Biphenyl (Diphenyl)ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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Page 23 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92275972002
1609398SAMPLE DUPLICATE:
Diphenyl ether (Phenyl ether)ug/L 6JND
2,4,6-Tribromophenol (S)%13 S0612
2-Fluorobiphenyl (S)%58 1567
2-Fluorophenol (S)%11 S0487
Nitrobenzene-d5 (S)%60 1067
Phenol-d6 (S)%20 4213
Terphenyl-d14 (S)%53 957
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 24 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41532
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1612032
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 11/22/15 12:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1612033LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 48.450 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1612034MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276163001
1612035
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L M1508990-11079 250206251245
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1612036MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276011002
1612037
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 98 90-11096 350ND49.2 47.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 25 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25376
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972005, 92275972006, 92275972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1605650
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972005, 92275972006, 92275972007
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 11/12/15 23:38
Nitrogen, Nitrite mg/L ND 0.020 11/12/15 23:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1605651LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 2.52.5 98 90-110
Nitrogen, Nitrite mg/L 1.01 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1605652MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275827002
1605653
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 97 90-11096 12.50.95 3.4 3.3
Nitrogen, Nitrite mg/L 1 106 90-110106 01ND1.1 1.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1605654MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275962003
1605655
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 93 90-110107 32.58.5 10.8 11.1
Nitrogen, Nitrite mg/L 1 101 90-110102 01ND1.0 1.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 26 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25377
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92275972004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1605656
Associated Lab Samples:92275972004
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 11/13/15 00:24
Nitrogen, Nitrite mg/L ND 0.020 11/13/15 00:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1605657LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 2.52.5 101 90-110
Nitrogen, Nitrite mg/L 1.01 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1605658MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276004003
1605659
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 2.5 96 90-11096 02.50.030 2.4 2.4
Nitrogen, Nitrite mg/L 1 100 90-11099 11ND1.0 0.99
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 27 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25381
SM 4500-P E
SM 4500-P E
SM4500P-E Phosphorus, Ortho
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1605684
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005, 92275972006, 92275972007
Matrix:Water
Analyzed
Orthophosphate as P mg/L ND 0.050 11/12/15 23:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1605685LABORATORY CONTROL SAMPLE:
LCSSpike
Orthophosphate as P mg/L 0.26.25 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1605686MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275972001
1605687
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Orthophosphate as P mg/L M1.5 29 90-11029 0.50.34 0.49 0.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
Pace Analytical Services, Inc.
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 28 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275972
CNA/NRLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/25407
EPA 9060A
EPA 9060A
9060 TOC, AVL
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1607246
Associated Lab Samples:92275972001, 92275972002, 92275972003, 92275972004, 92275972005
Matrix:Water
Analyzed
Mean Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Total Organic Carbon mg/L ND 1.0 11/16/15 12:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1607247LABORATORY CONTROL SAMPLE:
LCSSpike
Mean Total Organic Carbon mg/L 24.025 96 75-125
Total Organic Carbon mg/L 23.925 96 75-125
Total Organic Carbon mg/L 24.025 96 75-125
Total Organic Carbon mg/L 23.825 95 75-125
Total Organic Carbon mg/L 24.125 96 75-125
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1607248MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275754001
1607249
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mean Total Organic Carbon mg/L M625-76 75-1250 125275027302750
Total Organic Carbon mg/L M62523675-125596 325269027502840
Total Organic Carbon mg/L M625-196 75-12596 325277027202800
Total Organic Carbon mg/L M625-116 75-125280 425275027202820
Total Organic Carbon mg/L M625-220 75-125-964 725278027202540
REPORT OF LABORATORY ANALYSIS
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816 Durst Avenue East
Greenwood, SC 29649
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Page 29 of 55
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92275972
CNA/NRLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - GreenwoodPASI-G
Pace Analytical Services - IndianapolisPASI-I
Pace Analytical Services - GreenwoodPASI-W
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
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Greenwood, SC 29649
[phone]
Page 30 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92275972
CNA/NRLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92275972003 GCSV/17520B-01 EPA 8015 Alcohol-Glycol
92275972004 GCSV/17520B-10 EPA 8015 Alcohol-Glycol
92275972005 GCSV/17520B-32B EPA 8015 Alcohol-Glycol
92275972001 GWD/2674B-17C EPA 9056A
92275972002 GWD/2674B-17B EPA 9056A
92275972003 GWD/2674B-01 EPA 9056A
92275972004 GWD/2674B-10 EPA 9056A
92275972005 GWD/2674B-32B EPA 9056A
92275972006 GWD/2674B-12 EPA 9056A
92275972007 GWD/2674B-21B EPA 9056A
92275972001 OEXT/39138 MSSV/11545B-17C EPA 3510 EPA 8270
92275972002 OEXT/39138 MSSV/11545B-17B EPA 3510 EPA 8270
92275972003 OEXT/39138 MSSV/11545B-01 EPA 3510 EPA 8270
92275972004 OEXT/39138 MSSV/11545B-10 EPA 3510 EPA 8270
92275972005 OEXT/39138 MSSV/11545B-32B EPA 3510 EPA 8270
92275972006 OEXT/39138 MSSV/11545B-12 EPA 3510 EPA 8270
92275972003 MSV/34316B-01 EPA 8260
92275972004 MSV/34316B-10 EPA 8260
92275972001 MSV/34275B-17C EPA 8260B Mod.
92275972002 MSV/34275B-17B EPA 8260B Mod.
92275972003 MSV/34275B-01 EPA 8260B Mod.
92275972004 MSV/34275B-10 EPA 8260B Mod.
92275972005 MSV/34275B-32B EPA 8260B Mod.
92275972006 MSV/34275B-12 EPA 8260B Mod.
92275972007 MSV/34275B-21B EPA 8260B Mod.
92275972001 WET/41532B-17C SM 2320B
92275972002 WET/41532B-17B SM 2320B
92275972003 WET/41532B-01 SM 2320B
92275972004 WET/41532B-10 SM 2320B
92275972005 WET/41532B-32B SM 2320B
92275972006 WET/41532B-12 SM 2320B
92275972007 WET/41532B-21B SM 2320B
92275972001 WETA/25376B-17C EPA 353.2
92275972002 WETA/25376B-17B EPA 353.2
92275972003 WETA/25376B-01 EPA 353.2
92275972004 WETA/25377B-10 EPA 353.2
92275972005 WETA/25376B-32B EPA 353.2
92275972006 WETA/25376B-12 EPA 353.2
92275972007 WETA/25376B-21B EPA 353.2
92275972001 WETA/25381B-17C SM 4500-P E
92275972002 WETA/25381B-17B SM 4500-P E
92275972003 WETA/25381B-01 SM 4500-P E
92275972004 WETA/25381B-10 SM 4500-P E
92275972005 WETA/25381B-32B SM 4500-P E
REPORT OF LABORATORY ANALYSIS
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Greenwood, SC 29649
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Page 31 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92275972
CNA/NRLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92275972006 WETA/25381B-12 SM 4500-P E
92275972007 WETA/25381B-21B SM 4500-P E
92275972001 WETA/25407B-17C EPA 9060A
92275972002 WETA/25407B-17B EPA 9060A
92275972003 WETA/25407B-01 EPA 9060A
92275972004 WETA/25407B-10 EPA 9060A
92275972005 WETA/25407B-32B EPA 9060A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/25/2015 02:00 PM
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
Page 32 of 55
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