8602_SurryCounty_CDLF_GWMReport_DIN26411_20151124

Surry County Closed C&D and Closed MSWLF, Mt. Airy
Mt. Airy, North Carolina
November 2015
Permit Number: 86-02
Semi-Annual Water Quality Monitoring Report
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G15024.0
P.O. Box 97
Garner, NC 27529
License No. C-0281

with Corrective Action Update
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 3
Groundwater Samples Page 3
Surface Water Samples Page 3
Corrective Action Update Page 3
MNA Analysis (AOCs Northern, Southern and MW-11) Page 3
Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern) Page 3
MW-11 AOC Investigations Page 4
Groundwater and Surface Water Characterization Page 4
Findings Page 5
Closing Page 5
FIGURES
Topographic Map with Site Location Figure 1
Potentiometric Map of Uppermost Aquifer w/ VOCs Detected Above 2L Standards Figure 2
Total VOC Concentrations Pre/Post Injection Comparison Figure 3
Bromide Tracer Concentrations Time Series Graph and Table Figure 4
Total Cumulative VOC Concentrations Time Series Graphs/Table Figure 5
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, GWP, 2L, 2B or MCL (Appendix 1) Table 5
Hydrologic Properties at Monitoring Well Locations Table 6
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Parameter Data Sheet(s) Appendix B
April 12, 2016
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report with Corrective Action Update
Surry County Closed C&D and Closed MSWLF, Mount Airy
Permit No. 86-02
MESCO Project No. G15025.0 Event Date(s): November 22-24, 2015
Dear Ms. Drummond:
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Report with Corrective Action Update for the fall 2015 event performed at the Surry
County closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount
Airy. NCDENR Solid Waste Rules 15A NCAC 13B.1632 requires that Surry County provide this report to the NC
Solid Waste Section (SWS) on a semi-annual basis. This report documents the quality of the ground and surface
waters during this monitoring event performed on November 22-24, 2015. Laboratory analytical results indicate
volatile organic compounds (VOCs) in concentrations in excess of SWSL and 2L Standards continue to persist in
samples collected from four wells that monitor the uppermost aquifer. The surface water samples collected from the
local discharge feature remain unimpacted. Corrective action to remediate VOCs in groundwater is ongoing within
all three areas of concern (AOC) as defined in the Corrective Action Plan (CAP) as Northern, Southern and MW-11
with updated information presented herein.
Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North
Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to becoming a C&D landfill
the site operated as a MSW unlined sanitary landfill that consisted of two units. The northern unit was closed prior
to October 1991. The southern unit is comprised of two contiguous portions. The first part stopped receiving waste
prior to October 1991 and the second part stopped receiving waste prior to January 1, 1999. Both portions of the
southern unit were properly closed with a low permeability cohesive cap per the Transition Plan. The top portion
of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly
closed with another cohesive cap in accordance with the Closure Plan. For continuity, both the northern and the
southern units are monitored and reported together.
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available
since 1994. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A
NCAC 13B and as a condition of the post-closure portion of the permit to operate.

As specified within 15A NCAC 13B.1632(j) and the SWS Environmental Monitoring Report Form and SWS issued
memorandums this report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization, and findings. This report also contains a table of detections compared to Standards, field data
results table, groundwater flow directions/rates table, field observations of the monitoring network table, a
potentiometric map of the uppermost aquifer, histograms of historical detections, statistical trend analysis,
laboratory analytical reports with chains-of-custody (C-O-C) and quality assurance/quality control data.
Sampling Procedures
The water quality monitoring program, current as of this event date, includes sampling locations and parameters as
outlined in the Water Quality Sampling and Analysis Plan (SAP) (DIN:18936) dated April 30, 2013 and approved by
the SWS (DIN: 18938) on May 10, 2013. Monitoring locations are shown on the enclosed potentiometric map
(Figure 2). MESCO personnel collected water samples from 20 downgradient groundwater monitoring wells (MW-
3R, MW-4, MW-6 through MW-11, MW-12S, MW-12D, MW-13 through MW-23), one background well (MW-1),
four surface water locations (SW-1, SW-2, SW-3 and SW-4), and the water supply well (SCALEHOUSE) that serves
the facility. Data from two surface water points (SWN-1 and SWN-2) designated in the SAP for the adjacent
Subtitle D Lined MSWLF are presented because this local discharge feature is shared by both permits. Quality
control measures implemented during this event included the quantification of potential artifact contaminants via
equipment (EB), field (FB) and travel (TB) blanks. Samples were not analyzed from the six injection wells (IW-1),
(IW-2/MW-2), (IW-3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5) and (IW-6/MW-8) since they are exempt due to the
presence of injectant residue which would yield unrepresentative water quality results.
A summary of the construction of the water monitoring wells is presented on Table 1. The function and integrity of
all monitoring locations were visually evaluated and no deficiencies identified as documented on Table 2. The
depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation.
Low-flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of three times
the volume of standing water in the well or until dry. Surface water samples were collected from Stoney Creek
discharge feature at previously designated locations. During well purging and surface water sample collection the
required field parameters were recorded. The samples were then placed into laboratory-prepared, pre-preserved
containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC-
certified laboratory under proper C-O-C protocols within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, dissolved oxygen (DO),
temperature, oxidation reduction potential (ORP), specific conductance, total dissolved solids (TDS) and turbidity.
The field parameter data indicates the monitored groundwater is slightly acidic, low DO, with relatively low specific
conductance which is generally consistent relative to each other and congruent with data historically reported. Field
parameter data recorded at the surface water locations were neutral in regard to pH and low specific conductance
which is consistent with uncontaminated water. A summary of the field parameter data is presented in Table 3 and
the field sampling data sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Laboratory (PACE) of Huntersville and Asheville, NC performed the laboratory analysis of
groundwater and surface water samples for the total recoverable constituents listed in 40 CFR Appendix I. Pace
analyzed samples collected from six wells for a monitored natural attenuation (MNA) parameter sulfide.
Additionally, Pace reported bromide levels in samples collected from four wells to assess migration of the tracer
which was previously injected along with the remediation substrates. A sampling and analysis table summarizing
the locations, constituents, and methods is presented on Table 4. Laboratory results and C-O-Cs are contained in
Appendix A.
2
Water samples were analyzed to the laboratory specific Method Detection Limits (MDL), which are quantifiable at or
below the current Solid Waste Section detection limits (SWSL). Table 5 summarizes constituents detected in
groundwater and surface water samples that attain or were above the current SWSL, Groundwater Protection
Standards (GWP), North Carolina Groundwater Standards (2L), the applicable North Carolina Surface Water
Standards (2B) for a class C waterbody, and Maximum Contaminant Levels (MCL) also known as “Federal Primary
Drinking Water Standards”.
Quality Control Samples
Methylene chloride was detected in quality control samples EB and FB thus qualified by the laboratory as “C9”
common laboratory contaminant. Methylene chloride was not detected in any other samples; therefore, the field or
laboratory induced artifact contamination is likely non-consequential.
Groundwater Samples
Total metals continue to be absent in levels above their respective 2L Standards.
One or more VOC(s) were detected in quantifiable concentrations (> SWSL) above their respective 2L Standard in
samples collected from four monitoring wells (MW-9, MW-11, MW-15 and MW-16). The majority of the
monitoring locations that were found to contain VOCs included a mixture of dissolved phase aromatic hydrocarbons
and chlorinated aliphatic hydrocarbons. The only constituents detected above the EPA established maximum
contaminant levels (MCLs) primary “Drinking Water Standards” were vinyl chloride [MW-9 (7.9 ug/L), MW-16 (4.1
ug/L)] and 1,1-dichloroethene in sample MW-15 (12.8 ug/L). A site map depicting the concentrations and estimated
horizontal extent of VOCs that exceeded the 2L Standard during this event is presented on Figure 2.
The on-site water supply well (SCALEHOUSE) continues to lack target detections in exceedance of current
groundwater or drinking water Standards.
Surface Water Samples
Contaminants were not detected above NC 2B Surface Water Standards in any of the surface water samples.
Corrective Action Update
Groundwater remediation continues to be implemented per the approved Corrective Action Plan (CAP) at the three
designated areas of concern (AOC) (Northern, Southern and MW-11). A Corrective Action Evaluation Report
(CAER) (DIN: 19361) was submitted on May 1, 2013 which demonstrated that the plumes continue to decrease and
was approved by the the SWS on July 24, 2013 (DIN:19366). A historical summary of corrective actions performed
to date are briefly presented in the following sections.
MNA Analysis (AOCs Northern, Southern and MW-11)
Semi-annual MNA monitoring of a subset of 12 wells for the full suite of SWS recommended parameters was
initiated on May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A revised
SAP prescribing 7 wells with various targeted MNA constituents was approved by the SWS and initiated during an
event performed in May 2013. MNA monitoring was performed during this event for the parameters and frequency
as listed in the current SAP. Sulfide was the only MNA parameter quantified during this event. Keeping with the
approved SAP MNA monitoring for several parameters will resume during the next event scheduled for May 2016.
Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern)
Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was
initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit
Application and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic
chlorinated hydrocarbons in groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion
with sodium bromide tracer was injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011.
3
Similar substrates were injected into monitoring wells MW-4/IW-4 and MW-8/IW-6 on October 24-25, 2012.
Details of the injection events are provided in the Injection Event Record dated November 4, 2011 and January 10,
2013.
As directed in the UIC Injection Well Permit renewed on April 15, 2013 semi-annual post-injection water quality
monitoring of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13,
MW-14, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient
background well MW-1 was also performed in conjunction with this semi-annual event. Total VOC concentrations
reported during this event were lower at all locations when compared to the respective moving averages of the five
events preceding injection in the selected wells downgradient of the injection points (Figure 3).
Evaluation of injection wells (IW-1, IW-2, IW-3, IW-4, IW-5, IW-6) continues to indicate that a considerable amount
of white highly turbid (>1,000 NTU) viscous residual organic substrate and its byproducts remain in each of these
wells rendering them unsuitable for representative water quality analysis. The viscosity of the water in the injection
wells during this May 2014 event precludes sample collection as either a bailer will not descend or the check valve
fails. IW-1 was verified to not be a viable injection well as less than 3 gallons of substrate was able to be injected
into the low permeable fractured bedrock and injectant levels have remained above static conditions for over a year.
For all intents and purposes IW-1 injection did not occur nor will be possible in the future.
In an attempt to track migration of injectants bromide was targeted at MW-13, MW-15, MW-16 and background
well MW-1. MW-16, located 86 feet downgradient of IW-3, is the only location exhibiting tracer levels which may
potentially indicate injectant communication. Based on the average linear velocity rates of IW-3 and MW-16
reported since injection the injectant was expected to reach MW-16 in May 2012. Bromide concentrations at MW-16
have been variable but remain elevated compared to background levels (Figure 4). Calculations performed
following injection indicates that reported levels of bromide injected was insufficient to provide clear evidence of
migration within the uppermost aquifer.
MW-11 AOC Investigations
The CAP designated MW-11 as an area of concern due to detections of VOCs detected in exceedance of 2L
Standards. MW-11 is located within the compliance boundary near the northern property line which is hydraulically
upgradient of the closed northern landfill. The northern landfill closed before October 1991 which was before
adoption of NC Section .1600 rules that address assessment and corrective action. VOCs have historically been
detected in excess of the 2L Standard at MW-11 which include a mixture of aromatics (fuel hydrocarbons) and
chlorinated hydocarbons (solvents). Over the past 3.5 years (7 semi-annual events) the only constituent detected in
excess of 2L Standard and SWSL was 1,2-dichloropropane. The CAP prescribed MNA and enhanced
biodegredation to remediate MW-11 AOC. MNA has been performed continuously semiannually at MW-11 the past
5.5 years. Enhanced biodegredation has not been initiated at MW-11 AOC since hydrogeologic conditions relative to
the source and property boundaries preclude it as an effective technique. MW-11 is positioned hydraulically
upgradient of the source and is within the review boundary. A well was attempted to be installed at the property line
110 feet north of MW-11 on January 26, 2015 to delineate the extent of contamination. The potentiometric head at
B-11R was expected to be at 25 feet (1132 ft amsl) but the boring encountered very competent rock at 9 ft and
remained dry to 55 ft. (1102 ft amsl) for over 48 hours. Boring B-11R was abandoned and documented per 2C
Rules.
Groundwater and Surface Water Characterization
A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both
saprolite and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Figure 2.
Groundwater flow directions and velocity rates were calculated through modified Darcy's equation as shown on
Table 6. Consistent with previous events the groundwater apparently flows in a general southeasterly direction
towards the tributaries of the Ararat River. The calculated average linear velocity of groundwater indicates an
approximate average of 794 ft/yr in the wells screened in regolith and 340 ft/yr in the wells screened in the bedrock.
The consistent disparity in flow rates between wells is indicative of heterogeneous geologic conditions and/or a
product of the limitations of the linear velocity equation when applied to anisotropic conditions which are
4
Figures
Topographic Map with Site Location
FIGURE 1
Surry County Closed Unlined C&D and Closed Unlined MSWLF, Mt. Airy
237 Landfill Road
Mount Airy, NC 28621
Lat: 36-26-30.065
Long:-80-34-15.314
Northing:983356.18
Easting:1537885.48
Closed Unlined C&D Landfill
Closed Unlined Sanitary Landfill
Active Lined MSW Landfill
Surry Co Property Line
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 3
October 22, 2009 – November 24, 2015
Well ID
INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN
INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S, MW-13 & MW-18
MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100
MW-13 61.00 50.60 74.20 87.30 72.50 69.12 24.10 -45.02 -65
MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0
INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16
MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0
MW-16 137.90 113.60 135.70 121.20 116.30 124.94 59.50 -65.44 -52
INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23
MW-14 15.20 15.60 15.60 8.20 17.00 14.32 0.00 -14.32 -100
MW-21 52.10 50.70 51.38 39.10 32.41 45.14 13.40 -31.74 -70
MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.00 -0.86 -100
INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19
MW-15 96.13 63.89 55.00 78.10 64.06 71.44 65.60 -5.84 -8
MW-19 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0
INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE
Total Cumulative VOC Concentrations Pre/Post Injection Comparison
Oct
2009
(ug/L)
May
2010
(ug/L)
Oct
2010
(ug/L)
May
2011
(ug/L)
Oct
2011
(ug/L)
Average of
first Five
Corrective
Action
Events
(ug/L)
Nov.
2015
(ug/L)
Difference
(ug/L)
Difference
(%)
Statistical Trend*
Between Oct
2009-Nov 2015
«No Trend«
flDownwardfl
«No Trend«
«No Trend«
flDownwardfl
«No Trend«
flDownwardfl
«No Trend«
«No Trend«
«No Trend«
* = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level
11
/
3
/
2
01
1
(
IN
JE
C
T
E
D
)
1 1/
3
/
2
0
11
(I
N
J
E
CT
E
D
)
1 1/
3
/
2
0
11
(I
N
J
E
CT
E D)
1 0/
2
4
/
2
01
3
(I
N
JE
C
T
E
D
)
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 4
Bromide Tracer Concentrations Time Series Graph and Table
February 9, 2012 – November 22, 2015
Date MW-16
2/9/2012 0.038 (j)
5/30/2012 0.130 (j)
8/20/2012 0.260 (j)
10/23/2012 0.280 (j)
5/30/2013 0.140 (j)
10/31/2013 0.110 (j)
5/28/2014 0.220 (j)
10/22/2014 0.350 (j)
5/28/2015 0.290 (j)
11/22/2015 0.220
(j) = The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
* = May 25, 2012 Calculated date injectant expected to reach MW-16 using average flow rates of IW-3 and MW-16 (155 ft/yr) since injection occurred.
0 2 /0 9/1 2
0 5 /3 0/1 2
0 8 /2 0/1 2
1 0 /2 3/1 2
0 5 /3 0/1 3
1 0 /3 1/1 3
0 5 /2 8/1 4
10 /2 2/2
0
14
0 5 /2 8/1 5
1 1/2 2 /1 5
0.00
0.05
0.10
0.15
0.20
0.25
0.30
0.35
Bromide Tracer Levels in MW-16
Located 87 feet Downgradient of IW-3 which was Injected on November 2, 2011
MW-16
Date
mg
/L
Date injectant
expected
to reach
MW-16*
Da
t
e
in
je
c
t
a
n t e
x pe
c
t
e
d

t
o

r
e
a
c
h

M
W
-
1
6 *
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 5
Total Cumulative VOC Concentrations Time Series Graphs/Table
October 22, 2009 – November 24, 2015
AOC Well ID
Background MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
Southern
IW-2 (MW-2)105.25 207.00 207.93 159.90 79.10 151.84 NS NS No Trend
IW-3 (MW-3RS)202.90 127.50 127.50 144.00 127.60 145.90 NS NS No Trend
MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
IW-4 (MW-4)27.00 24.20 24.20 27.60 23.50 25.30 NS NS No Trend
IW-5 (MW-5)35.00 46.50 46.50 47.40 34.80 42.04 NS NS No Trend
MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 No Trend
MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-13 61.00 50.60 74.20 87.30 72.50 69.12 24.10 -45.02 -65 Downward
MW-14 15.20 15.60 15.60 8.20 17.00 14.32 0.00 -14.32 -100 Downward
MW-15 96.13 55.00 55.00 78.10 64.06 69.66 65.60 -4.06 -6 No Trend
MW-16 137.90 113.60 135.70 121.20 116.30 124.94 59.50 -65.44 -52 Downward
MW-17 20.34 8.40 8.85 0.00 5.77 8.67 0.00 -8.67 -100 No Trend
MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-19 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-21 52.10 50.70 51.38 39.10 32.41 45.14 13.40 -31.74 -70 Downward
MW-22 28.90 23.80 23.80 11.66 5.20 18.67 0.00 -18.67 -100 Downward
MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.00 -0.86 -100 No Trend
Combined Total 786.02 722.90 770.66 724.46 583.64 717.54 422.20 -295.34 -41 Downward
Northern
MW-6 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-7 7.40 9.40 11.20 9.70 8.80 9.30 1.60 -7.70 -83 No Trend
IW-6 (MW-8)22.00 23.90 16.00 12.30 12.60 17.36 NS NS No Trend
MW-9 23.50 20.40 23.20 25.80 22.90 23.16 28.90 5.74 25 No Trend
MW-20 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
Combined Total 52.90 53.70 50.40 47.80 44.30 49.82 43.10 -6.72 -13 No Trend
MW-11 MW-11 10.10 6.00 6.00 5.44 23.20 10.15 7.07 -3.08 -30 No Trend
SITEWIDE Combined Total 849.02 782.60 827.06 777.70 651.14 777.50 472.37 -305.13 -39 Downward
Oct
2009
(ug/L)
May
2010
(ug/L)
Oct
2010
(ug/L)
May
2011
(ug/L)
Oct
2011
(ug/L)
Average of Preceding
Five
Events
(ug/L)
Nov.
2015
(ug/L)
Difference
(ug/L)
Difference
(%)
Statistical Trend*
Between
Oct 2009 – Nov. 2015
79.10 NS
127.60 NS
18.10 NS
34.80 NS
12.60 NS
NS = Not sampled this event so most recent concentration shown and used in calculations
* = Statistical trend analysis via Sen's Slope Estimator at a 95% Confidence Level
Tables
Surry County Closed C02/26/2016 and Closed MSWLF, Mt. Airy Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
November 22-23, 2015
Monitoring Well Latitude Longitude
(inches)(ft)
MW-1 11/28/89 2 40 30 10 Clay 1134.35 1133.15 1109.39 24.96 36.439211 -80.568133
IW-2 (was MW-2)11/28/89 2 70 60 10 Clay 1068.86 1068.36 1028.98 39.88 36.435833 -80.568894
MW-3R 9/27/94 2 101 86 15 Rock 1017.50 1015.00 975.89 41.61 36.434725 -80.571989
IW-3 (was MW-3RS)5/17/01 2 52 37 15 Rock 1020.57 1018.24 989.29 31.28 36.434656 -80.571858
IW-4 (was MW-4)8/30/94 2 55.4 40.4 15 Rock 1026.26 1025.06 992.38 33.88 36.434686 -80.569200
IW-5 (was MW-5)8/27/94 2 63 48 15 Rock 1080.18 1077.78 <1039.50 >40.68 36.434614 -80.570436
MW-6 9/7/94 2 29.7 14.7 15 Rock 1067.67 1065.61 1045.53 22.14 36.437431 -80.571067
MW-7 8/23/94 2 23 8 15 Rock 1073.50 1071.50 1060.99 12.51 36.438439 -80.570722
IW-6 (was MW-8)8/16/94 2 54 39 15 Rock 1088.45 1086.45 1045.16 43.29 36.439278 -80.570381
MW-9 8/22/94 2 43.8 28.8 15 Rock 1094.07 1092.07 1060.35 33.72 36.439289 -80.571508
MW-11 8/15/94 2 40 25 15 Rock 1151.80 1150.40 1130.09 21.71 36.441589 -80.569558
MW-12S 5/31/01 2 51 11 40 Rock 1025.80 1023.25 1012.82 12.98 36.435942 -80.567972
MW-12D 5/30/01 2 100 90 10 Rock 1027.05 1023.75 1027.05 36.435964 -80.567994
MW-13 5/30/06 2 35.78 20.78 15 1008.48 1005.75 981.35 27.13 36.435036 -80.568183
MW-14 5/30/06 2 48.03 33.03 15 Rock 1018.80 1016.11 976.63 42.17 36.434267 -80.569239
MW-15 6/22/06 2 57 42 15 Rock 1075.96 1073.23 1021.64 54.32 36.433797 -80.570467
MW-16 6/21/06 2 36.3 21.3 15 Rock 999.54 996.67 973.59 25.95 36.434536 -80.572117
MW-17 6/1/07 2 15.32 5.32 10 Rock 965.43 962.26 957.10 8.33 36.433558 -80.572517
MW-18 6/1/07 2 18.15 8.15 10 983.00 980.00 973.80 9.20 36.435453 -80.567050
MW-19 6/1/07 2 17.1 7.1 10 PWR 946.27 942.97 935.47 10.80 36.432231 -80.570556
MW-20 6/1/07 2 25.64 10.64 15 Rock 1082.19 1079.12 1062.40 19.79 36.439025 -80.571650
MW-21 6/1/07 2 15.41 5.41 10 965.36 962.22 959.01 6.35 36.434214 -80.568717
MW-22 6/1/07 2 16.04 6.04 10 953.40 950.23 948.13 5.27 36.432928 -80.571678
MW-23 6/1/07 2 17.1 7.1 10 Sandy Silt 955.31 952.09 948.47 6.84 36.432828 -80.569156
NOTE:
Date
Installed
Well
Diameter
Total Well
Depth
Top of
Screen
Depth
Screen
Length Geology of
Screened Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
Saprolite
Saprolite
Saprolite/PWR
Saprolite
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Table 2
Field Observations of Monitoring Locations
November 22-24, 2015
Location Comments
MW-1 Yes Yes Yes Yes Yes Yes
IW-1 No Yes Yes Yes Yes Yes Fouled since injection 11/2/11.
IW-2 (was MW-2)No Yes Yes Yes Yes Yes Fouled since injection 11/2/11.
MW-3R Yes Yes Yes Yes Yes Yes
IW-3 (was MW-3RS)No Yes Yes Yes Yes Yes Fouled since injection 11/2/11.
IW-4 (was MW-4)No Yes Yes Yes Yes Yes Fouled since injection 10/24/12.
IW-5 (was MW-5)No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. Bailer would not descend
MW-6 Yes Yes Yes Yes Yes Yes
MW-7 Yes Yes Yes Yes Yes Yes
IW-6 (was MW-8)No Yes Yes Yes Yes Yes Fouled since injection 10/24/12.
MW-9 Yes Yes Yes Yes Yes Yes
MW-11 Yes Yes Yes Yes Yes Yes
MW-12S Yes Yes Yes Yes Yes Yes
MW-12D Yes Yes Yes Yes Yes Yes Flowing artesian
MW-13 Yes Yes Yes Yes Yes Yes
MW-14 Yes Yes Yes Yes Yes Yes
MW-15 Yes Yes Yes Yes Yes Yes
MW-16 Yes Yes Yes Yes Yes Yes
MW-17 Yes Yes Yes Yes Yes Yes
MW-18 Yes Yes Yes Yes Yes Yes
MW-19 Yes Yes Yes Yes Yes Yes
MW-20 Yes Yes Yes Yes Yes Yes
MW-21 Yes Yes Yes Yes Yes Yes
MW-22 Yes Yes Yes Yes Yes Yes
MW-23 Yes Yes Yes Yes Yes Yes
SW-1 Yes -----Moderate gage height & flow
SW-2 Yes -----Moderate gage height & flow
SW-3 Yes -----Moderate gage height & flow
SW-4 Yes -----Moderate gage height & flow
SWN-1 Yes -----Moderate gage height & flow
SWN-2 Yes -----Moderate gage height & flow
SCALEHOUSE Yes -----Sample from spigot next to well which is typical
Any unusual field conditions, observations, or events:
Injection wells (IW-1, IW-2, IW-3, IW-4, IW-5 and IW-6) exempt from laboratory analysis as SWS approved on May 10, 2013 (DIN:18938)
Visual markers (10 ft PVC pipes) remain secured to each monitoring well case
Viable
Monitoring Location
Lack of Any
Evidence of Tampering
Locked on
Arrival & Departure
Hinge/Hasp
Operational
Tagged
or Labeled
Concrete Surface Pad
Appears
Effective
Stormwater control improvements performed since May 2012 event.
Surry County Closed C03/30/2016 and Closed MSWLF, Mt. Airy Page 1 of 3
Table 3
Field Parameter Data Summary
November 22-23, 2015
Parameter Temp.ORP DO pH TDS Turbidity
Units C mg/L SU mg/L Visual or NTU
MW-1 24.96 1109.39 1134.35 16.6 199 2.3 6.23 320 150 17.5
IW-2 39.88 1028.98 1068.86 NR NR NR NR NR NR >1000
MW-3R 41.61 975.89 1017.50 15.1 119 0.7 8.21 320 150 18.3
IW-3 31.28 989.29 1020.57 NR NR NR NR NR NR NR
IW-4 33.88 992.38 1026.26 NR NR NR NR NR NR >1000
IW-5 >40.68 <1039.50 1080.18 NR NR NR NR NR NR NR
MW-6 22.14 1045.53 1067.67 14.9 -63 0.8 6.91 410 200 20.1
MW-7 12.51 1060.99 1073.50 16.2 211 0.7 6.53 300 140 Clear
IW-6 43.29 1045.16 1088.45 NR NR NR NR NR NR >1000
MW-9 33.72 1060.35 1094.07 15.7 -21 0.6 5.96 410 200 Clear
MW-11 21.71 1130.09 1151.80 15.4 80 3.4 5.03 110 50 12.1
MW-12S 12.98 1012.82 1025.80 14.8 58 3.3 7.41 510 250 Slight
MW-12D 0.00 1027.05 1027.05 15.2 -83 1.1 7.93 180 70 Slight
MW-13 27.13 981.35 1008.48 14.7 273 0.8 5.91 210 100 Clear
MW-14 42.17 976.63 1018.80 15.1 183 2.3 5.41 110 50 Moderate
MW-15 54.32 1021.64 1075.96 14.7 28 0.6 5.93 150 70 >1000
MW-16 25.95 973.59 999.54 15.1 123 0.5 5.91 410 200 Clear
MW-17 8.33 957.1 965.43 14.9 168 2.1 5.93 430 210 Slight
MW-18 9.2 973.8 983.00 15.3 271 4.6 6.51 10 0 Clear
MW-19 10.8 935.47 946.27 15.1 291 4.5 5.81 10 0 Slight
MW-20 19.79 1062.4 1082.19 15.9 163 1.6 6.41 60 20 Slight
MW-21 6.35 959.01 965.36 15.2 283 3.3 5.91 180 80 Clear
MW-22 5.27 948.13 953.40 14.8 138 0.9 5.93 190 80 Clear
MW-23 6.84 948.47 955.31 15.2 303 3.5 6.41 60 20 Clear
15.1 307 4.6 7.07 810 400 Clear
Minimum 0.00 935.47 946.27 14.7 -83 0.5 5.03 10 0 Clear
Average 23.22 1009.37 1034.58 15.3 152 2.1 6.37 260 122 Slight
Maximum 54.32 1130.09 1151.80 16.6 307 4.6 8.21 810 400 Moderate
SW-1 ---12.3 NR NR 7.03 280 130 Clear
SW-2 ---12.5 NR NR 6.99 300 140 Clear
SW-3 ---12.7 NR NR 6.97 280 130 Clear
SW-4 ---12.4 NR NR 6.99 290 130 Clear
SWN-1 ---12.8 NR NR 7.03 90 40 Clear
SWN-2 ---12.9 NR NR 7.07 90 40 Clear
Minimum ---12.3 NR NR 6.97 90 40 Clear
Average ---12.6 NR NR 7.01 222 102 Clear
Maximum ---12.9 NR NR 7.07 300 140 Clear
NR = No reading attempted
Depth to
Water*
Water
Elevation
TOC
Elevation
Specific
Conductance
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
Scalehouse na na na
btoc = Below top of casing
amsl = Above mean sea level
na = Not available
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Table 4
Sampling and Analysis Summary
November 22-23, 2015
MNA Field Parameter Tracer
To
t
a
l

M
e
t
a
l
s

Al
k
a
l
i
n
i
t
y
Su
l
f
a
t
e
Su
l
f
i
d
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Ch
l
o
r
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d
e
TO
C
CO
D
Ir
o
n
,

D
i
s
s
o
l
v
e
d
Dis
s
o
l
v
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d

O
x
y
g
e
n

(
D
O
)
Ox
i
d
a
t
i
o
n

R
e
d
u
c
t
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n

P
o
t
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n
t
i
a
l

(
O
R
P
)
Te
m
p
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a
t
u
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Co
n
d
u
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t
i
v
i
t
y
To
t
a
l

D
i
s
s
o
l
v
e
d

S
o
l
i
d
s

(
T
D
S
)
pH Tu
r
b
i
d
i
t
y
Br
o
m
i
d
e
La
b

E
P
A

8
2
6
0
B
L
a
b

E
P
A

6
0
0
0
/
7
0
0
0
EP
A

3
1
0
.
2
EP
A

3
0
0
.
0
La
b

S
M
1
8

4
5
0
0
-
S

D
EP
A

3
0
0
.
0
SM

5
3
1
0
B

SM

5
2
2
0
D

La
b

E
P
A

6
0
1
0
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
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Fi
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l
d

M
e
t
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r
Fi
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l
d

M
e
t
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r
Fi
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d

M
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d

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t
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r

o
r

V
i
s
u
a
l
EP
A

3
0
0
.
0
IW-1 Not sampled as injection well exempt x
MW-1 x x x x x x x x x x x
IW-2 Not sampled as injection well exempt x
MW-3R x x x x x x x x x
IW-3 Not sampled as injection well exempt x
IW-4 Not sampled as injection well exempt x
IW-5 Not sampled as injection well exempt x
MW-6 x x x x x x x x x
MW-7 x x x x x x x x x x
IW-6 Not sampled as injection well exempt x
MW-9 x x x x x x x x x x
MW-11 x x x x x x x x x x
MW-12S x x x x x x x x x
MW-12D x x x x x x x x x
MW-13 x x x x x x x x x x
MW-14 x x x x x x x x x x
MW-15 x x x x x x x x x x x
MW-16 x x x x x x x x x x
MW-17 x x x x x x x x x
MW-18 x x x x x x x x x
MW-19 x x x x x x x x x
MW-20 x x x x x x x x x
MW-21 x x x x x x x x x x
MW-22 x x x x x x x x x
MW-23 x x x x x x x x x
x x x x x x x x x
SW-1 x x x x x x x
SW-2 x x x x x x x
SW-3 x x x x x x x
SW-4 x x x x x x x
SWN-1 x x x x x x x
SWN-2 x x x x x x x
EB x x
FB x x
TB x
Injection wells exempt from monitoring except for turbidity and WLR per SWS approved SAP [18936]
App. I
VO
Cs

Scalehouse
App I = Appendix I List from current 40 CFR 258
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 2
Table 5
Detections in Water Samples above SWSL, 2L, 2B, GWP or MCL (Appendix I)
November 22-24, 2015
Sample ID Result Unit
MW-6 Barium, total 11/22/15 103 2.5 100 700 1300
MW-6 Vanadium, total 11/22/15 13.6 j 2.5 25 NE 0.3 NE
MW-6 Cobalt, total 11/22/15 176 2.5 10 NE 1 NE
MW-7 11/22/15 1.6 0.33 1 6 75
MW-7 Cobalt, total 11/22/15 56.6 2.5 10 NE 1 NE
MW-7 Vanadium, total 11/22/15 9 j 2.5 25 NE 0.3 NE
MW-9 Vinyl chloride 11/22/15 7.9 0.62 1 0.03 2 L &/or LFG
MW-9 Benzene 11/22/15 1.6 0.25 1 1 5 L &/or LFG
MW-9 Zinc, total 11/22/15 36.9 5 10 1000 5000
MW-9 Cobalt, total 11/22/15 180 2.5 10 NE 1 NE
MW-9 11/22/15 5.2 0.33 1 6 75
MW-9 Vanadium, total 11/22/15 13 j 2.5 25 NE 0.3 NE
MW-9 11/22/15 14.2 0.19 5 70 70
MW-11 11/24/15 2 0.27 1 0.6 5 L &/or LFG
MW-11 11/24/15 0.47 j 0.24 1 0.4 5 L &/or LFG
MW-11 11/24/15 4.6 0.33 1 6 75
MW-11 Cobalt, total 11/24/15 12.4 2.5 10 NE 1 NE
MW-13 11/22/15 23.1 0.19 5 70 70
MW-13 Thallium, total 11/22/15 6.5 5 5.5 NE 0.28 2
MW-13 11/22/15 1 0.47 1 3 5
MW-15 Benzene 11/22/15 2.3 0.25 1 1 5 L &/or LFG
MW-15 11/22/15 1 0.46 1 0.07 5 L &/or LFG
MW-15 11/22/15 12.8 0.32 5 6 7 L &/or LFG
MW-15 11/22/15 2.5 0.27 1 0.6 5 L &/or LFG
MW-15 Vinyl chloride 11/22/15 1.7 0.62 1 0.03 2 L &/or LFG
MW-15 11/22/15 2.9 0.47 1 3 5
MW-15 11/22/15 3.3 0.23 3 50 100
MW-15 Zinc, total 11/22/15 11.2 5 10 1000 5000
MW-15 11/22/15 39.1 0.19 5 70 70
MW-16 Vinyl chloride 11/22/15 4.1 0.62 1 0.03 2 L &/or LFG
MW-16 11/22/15 3.2 0.27 1 0.6 5 L &/or LFG
MW-16 Benzene 11/22/15 1.4 0.25 1 1 5 L &/or LFG
MW-16 Barium, total 11/22/15 125 2.5 100 700 1300
MW-16 Cobalt, total 11/22/15 348 2.5 10 NE 1 NE
MW-16 11/22/15 44.1 0.19 5 70 70
MW-16 Vanadium, total 11/22/15 35.6 2.5 25 NE 0.3 NE
MW-16 Zinc, total 11/22/15 12.3 5 10 1000 5000
MW-16 11/22/15 6.7 0.23 3 50 100
MW-17 Cadmium, total 11/22/15 1.6 0.5 1 2 5
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
1,2-Dichloropropane ug/L
1,2-Dichloroethane ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
Trichloroethene ug/L
ug/L
Tetrachloroethene ug/L
1,1-Dichloroethane ug/L
1,2,3-Trichloropropane ug/L
ug/L
Trichloroethene ug/L
Chlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
1,2-Dichloropropane ug/L
ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
Chlorobenzene ug/L
ug/L
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 2 of 2
Sample ID Result UnitParameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
MW-18 Cadmium, total 11/23/15 2 0.5 1 2 5
MW-19 Zinc, total 11/22/15 19.9 5 10 1000 5000
MW-19 Vanadium, total 11/22/15 6.6 j 2.5 25 NE 0.3 NE
MW-20 Cobalt, total 11/22/15 17.9 2.5 10 NE 1 NE
MW-20 Zinc, total 11/22/15 15 5 10 1000 5000
MW-20 Vanadium, total 11/22/15 4 j 2.5 25 NE 0.3 NE
MW-21 11/22/15 13.4 0.19 5 70 70
MW-22 Vanadium, total 11/22/15 4.1 j 2.5 25 NE 0.3 NE
SCALEHOUSEZinc, total 11/23/15 13 5 10 1000 5000
SW-2 Cobalt, total 11/22/15 17.5 2.5 10 270 NE
SW-4 Zinc, total 11/22/15 12.8 5 10 50 5000
EB Methylene Chloride 11/24/15 1.1 (C9)0.97 1 5 NE 5
FB Methylene Chloride 11/24/15 0.99 j (C9)0.97 1 5 NE 5
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
j =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
L = Leachate
LFG = Landfill Gas
(C9) = Flagged by the laboratory as “common laboratory contaminant”
RED BOLD = Concentration > 2L, 2B, GWP or MCL Standard
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Table 6
November 22, 2015
Well (cm/second)(ft/day)(%)(feet/feet)(feet/year)(ft)
MW-1 4.30E-05 0.122 15 0.019 6 S53W 0 24.96 1109.39 Clay
IW-2 4.30E-05 0.122 15 0.163 48 S40E -39.88 1028.98 Clay
MW-7 8.10E-04 2.296 15 0.198 1,106 N60W 704 12.51 1060.99 PWR/Fractured Rock
IW-6 4.40E-04 1.247 15 0.088 267 S47W -43.29 1045.16 PWR/Fractured Rock
MW-9 1.90E-04 0.539 15 0.008 11 S49E 614 33.72 1060.35 Sandy Silt
MW-13 2.06E-04 0.584 23 0.096 89 S27E 1850 27.13 981.35
MW-18 2.04E-03 5.783 15 0.129 S31E 0 9.20 973.80
MW-19 1.10E-03 3.118 3 0.057 2,148 S12W 2663 10.80 935.47 PWR
MW-21 1.28E-03 3.628 3 0.071 3,122 S43E 2041 6.35 959.01
MW-22 9.88E-04 2.801 15 0.144 980 S30W 2506 5.27 948.13
MW-23 3.04E-04 0.862 15 0.077 160 S31E 2610 6.84 948.47 Sandy Silt
Minimum 4.30E-05 0.122 3 0.008 6 -0 5.27 935.47 -
Average 6.77E-04 1.918 14 0.095 794 -1443 20 1004.65 -
Maximum 2.04E-03 5.783 23 0.198 3,122 -2663 43.29 1109.39 -
MW-3R 2.40E-04 0.680 5 1,994 41.61 975.89 Fractured Rock
IW-3 2.40E-05 0.068 5 0.465 231 S11W -31.28 989.29 Fractured Rock
IW-4 1.10E-04 0.312 5 0.149 339 S45E -33.88 992.38 Fractured Rock
IW-5 1.50E-05 0.043 5 ------Fractured Rock
MW-6 1.90E-05 0.054 5 0.184 72 S85W 963 22.14 1045.53 Fractured Rock
MW-11 3.10E-04 0.879 5 0.094 605 S18W 0 21.71 1130.09 Fractured Rock
MW-12S 3 0.108 S19E 0 12.98 1012.82 Fractured Rock
MW-12D 1.30E-06 0.004 5 0 0.00 1027.05 Fractured Rock
MW-14 7.45E-03 21.118 3 0.281 72,156 S75E 2098 42.17 976.63 Fractured Rock
MW-15 7.21E-05 0.204 3 0.078 194 S07E 54.32 1021.64 Fractured Rock
MW-16 2.82E-05 0.080 3 0.054 53 S34W 2089 25.95 973.59 Fractured Rock
MW-17 2.94E-04 0.833 3 0.081 817 S68W 2547 8.33 957.10 Rock
MW-20 1.92E-04 0.544 3 0.062 407 S24E 692 19.79 1062.40 Rock
Minimum 1.30E-06 0.004 3 0.054 53 -0 0.00 957.10 -
Average 1.19E-04 0.336 4 0.156 340 -1154 26.18 1013.70 -
Maximum 3.10E-04 0.879 5 0.465 817 -2547 54.32 1130.09 -
NOTE: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce.
Wells screened entirely in rock were not utilized for flow directions/gradients.
where
Hydrologic Properties at Monitoring Well Locations
Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient
Groundwater
Average
Linear
Velocity Rate
Flow
Direction
Minimum
Distance
From
Upgradient
EOW
Ground
Water
Depth
Groundwater
Potentiometric
Elevation
Screened Interval
Lithology
(feet
btoc)(feet amsl)
Saprolite
na Saprolite
Saprolite/PWR
Saprolite
na na na
na na na
na na na
Hydrologic gradient from water levels recorded on November 22, 2015.
Screens that traverse both rock and regolith assumed flow in regolith dominates.
Hydraulic Conducitivity value and flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum.
na = Not available/applicable
Average Linear Velocity (Q) is defined by modified Darcy's equation:
K= hydraulic conductivity
ne= effective porosity
dh= head difference
dl= horizontal distance
dl
dh
n
KQ
e
-=
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
December 08, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92277673
92277673
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY CLOSED-MT. AIRY (AM)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on November 25, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 24
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Lab ID Sample ID Matrix Date Collected Date Received
92277673001 MW-6 Water 11/22/15 13:35 11/25/15 14:00
92277673002 MW-11 Water 11/24/15 12:00 11/25/15 14:00
92277673003 MW-12D Water 11/23/15 09:50 11/25/15 14:00
92277673004 SCALEHOUSE Water 11/23/15 09:05 11/25/15 14:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92277673001 MW-6 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277673002 MW-11 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 4500-S2D 1 PASI-AMJP
92277673003 MW-12D EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277673004 SCALEHOUSE EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-6 Lab ID:92277673001 Collected:11/22/15 13:35 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 02:51 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 02:51 7440-38-212/01/15 19:0010.0 2.5 1
Barium 103 ug/L 12/05/15 02:51 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 02:51 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 02:51 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 02:51 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt 176 ug/L 12/05/15 02:51 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 02:51 7440-50-812/01/15 19:0010.0 2.5 1
Lead 3.4J ug/L 12/05/15 02:51 7439-92-112/01/15 19:0010.0 2.5 1
Nickel 4.2J ug/L 12/05/15 02:51 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 02:51 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 02:51 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/05/15 02:51 7440-28-012/01/15 19:005.5 5.0 1
Vanadium 13.6J ug/L 12/05/15 02:51 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 02:51 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 03:31 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 03:31 107-13-12001.9 1
Benzene 0.35J ug/L 12/01/15 03:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 03:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 03:31 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 03:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 03:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 03:31 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 03:31 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 03:31 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 03:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 03:31 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 03:31 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 03:31 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 03:31 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 03:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 03:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 03:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 03:31 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 03:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 03:31 110-57-6 M11001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 03:31 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 03:31 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 03:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 03:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 03:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 03:31 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 03:31 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 03:31 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-6 Lab ID:92277673001 Collected:11/22/15 13:35 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 03:31 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 03:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 03:31 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 03:31 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 03:31 108-10-11000.33 1
Styrene ND ug/L 12/01/15 03:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 03:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 03:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 03:31 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 03:31 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 03:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 03:31 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 03:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 03:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 03:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 03:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 03:31 75-01-4 M11.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 03:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %12/01/15 03:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %12/01/15 03:31 17060-07-070-130 1
Toluene-d8 (S)100 %12/01/15 03:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-11 Lab ID:92277673002 Collected:11/24/15 12:00 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 02:57 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 02:57 7440-38-212/01/15 19:0010.0 2.5 1
Barium 34.4J ug/L 12/05/15 02:57 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 02:57 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 02:57 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 02:57 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt 12.4 ug/L 12/05/15 02:57 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 02:57 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 02:57 7439-92-112/01/15 19:0010.0 2.5 1
Nickel 2.8J ug/L 12/05/15 02:57 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 02:57 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 02:57 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 18:12 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 02:57 7440-62-212/01/15 19:0025.0 2.5 1
Zinc 5.1J ug/L 12/05/15 02:57 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 03:48 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 03:48 107-13-12001.9 1
Benzene 0.88J ug/L 12/01/15 03:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 03:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 03:48 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 03:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 03:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 03:48 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 03:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 03:48 56-23-51.0 0.25 1
Chlorobenzene 1.3J ug/L 12/01/15 03:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 03:48 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 03:48 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 03:48 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 03:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 03:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 03:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 03:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 03:48 95-50-15.0 0.30 1
1,4-Dichlorobenzene 4.6 ug/L 12/01/15 03:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 03:48 110-57-61001.0 1
1,1-Dichloroethane 0.85J ug/L 12/01/15 03:48 75-34-35.0 0.32 1
1,2-Dichloroethane 0.47J ug/L 12/01/15 03:48 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 03:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.5J ug/L 12/01/15 03:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 03:48 156-60-55.0 0.49 1
1,2-Dichloropropane 2.0 ug/L 12/01/15 03:48 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 03:48 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 03:48 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-11 Lab ID:92277673002 Collected:11/24/15 12:00 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 03:48 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 03:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 03:48 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 03:48 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 03:48 108-10-11000.33 1
Styrene ND ug/L 12/01/15 03:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 03:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 03:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 03:48 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 03:48 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 03:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 03:48 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 03:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 03:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 03:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 03:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 03:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 03:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %12/01/15 03:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %12/01/15 03:48 17060-07-070-130 1
Toluene-d8 (S)98 %12/01/15 03:48 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/30/15 20:15 18496-25-810001001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-12D Lab ID:92277673003 Collected:11/23/15 09:50 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 03:09 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 03:09 7440-38-212/01/15 19:0010.0 2.5 1
Barium 6.3J ug/L 12/05/15 03:09 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 03:09 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 03:09 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 03:09 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 03:09 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 03:09 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 03:09 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 03:09 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 03:09 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 03:09 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 18:16 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 03:09 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 03:09 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 04:22 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 04:22 107-13-12001.9 1
Benzene ND ug/L 12/01/15 04:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 04:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 04:22 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 04:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 04:22 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 04:22 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 04:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 04:22 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 04:22 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 04:22 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 04:22 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 04:22 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 04:22 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 04:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 04:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 04:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 04:22 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 04:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 04:22 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 04:22 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 04:22 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 04:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 04:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 04:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 04:22 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 04:22 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 04:22 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-12D Lab ID:92277673003 Collected:11/23/15 09:50 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 04:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 04:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 04:22 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 04:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 04:22 108-10-11000.33 1
Styrene ND ug/L 12/01/15 04:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 04:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 04:22 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 04:22 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 04:22 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 04:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 04:22 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 04:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 04:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 04:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 04:22 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 04:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 04:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %12/01/15 04:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/01/15 04:22 17060-07-070-130 1
Toluene-d8 (S)99 %12/01/15 04:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Sample:SCALEHOUSE Lab ID:92277673004 Collected:11/23/15 09:05 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 03:13 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 03:13 7440-38-212/01/15 19:0010.0 2.5 1
Barium 12.7J ug/L 12/05/15 03:13 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 03:13 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 03:13 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 03:13 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 03:13 7440-48-412/01/15 19:0010.0 2.5 1
Copper 3.6J ug/L 12/05/15 03:13 7440-50-812/01/15 19:0010.0 2.5 1
Lead 3.7J ug/L 12/05/15 03:13 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 03:13 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 03:13 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 03:13 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 18:19 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 03:13 7440-62-212/01/15 19:0025.0 2.5 1
Zinc 13.0 ug/L 12/05/15 03:13 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 04:39 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 04:39 107-13-12001.9 1
Benzene ND ug/L 12/01/15 04:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 04:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 04:39 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 04:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 04:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 04:39 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 04:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 04:39 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 04:39 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 04:39 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 04:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 04:39 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 04:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 04:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 04:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 04:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 04:39 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 04:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 04:39 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 04:39 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 04:39 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 04:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 04:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 04:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 04:39 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 04:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 04:39 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
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Page 11 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Sample:SCALEHOUSE Lab ID:92277673004 Collected:11/23/15 09:05 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 04:39 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 04:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 04:39 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 04:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 04:39 108-10-11000.33 1
Styrene ND ug/L 12/01/15 04:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 04:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 04:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 04:39 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 04:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 04:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 04:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 04:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 04:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 04:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 04:39 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 04:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 04:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %12/01/15 04:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %12/01/15 04:39 17060-07-070-130 1
Toluene-d8 (S)99 %12/01/15 04:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
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[phone]
Page 12 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20147
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92277673001, 92277673002, 92277673003, 92277673004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617580
Associated Lab Samples:92277673001, 92277673002, 92277673003, 92277673004
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/05/15 01:553.8
Arsenic ug/L ND 10.0 12/05/15 01:552.5
Barium ug/L ND 100 12/05/15 01:552.5
Beryllium ug/L ND 1.0 12/05/15 01:550.50
Cadmium ug/L ND 1.0 12/05/15 01:550.50
Chromium ug/L ND 10.0 12/05/15 01:552.5
Cobalt ug/L ND 10.0 12/05/15 01:552.5
Copper ug/L ND 10.0 12/05/15 01:552.5
Lead ug/L ND 10.0 12/05/15 01:552.5
Nickel ug/L ND 50.0 12/05/15 01:552.5
Selenium ug/L ND 10.0 12/05/15 01:555.0
Silver ug/L ND 10.0 12/05/15 01:552.5
Thallium ug/L ND 5.5 12/05/15 01:555.0
Vanadium ug/L ND 25.0 12/05/15 01:552.5
Zinc ug/L ND 10.0 12/05/15 01:555.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617581LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 454500 91 80-120
Arsenic ug/L 430500 86 80-120
Barium ug/L 502500 100 80-120
Beryllium ug/L 513500 103 80-120
Cadmium ug/L 466500 93 80-120
Chromium ug/L 494500 99 80-120
Cobalt ug/L 454500 91 80-120
Copper ug/L 479500 96 80-120
Lead ug/L 452500 90 80-120
Nickel ug/L 469500 94 80-120
Selenium ug/L 437500 87 80-120
Silver ug/L 236250 95 80-120
Thallium ug/L 454500 91 80-120
Vanadium ug/L 476500 95 80-120
Zinc ug/L 444500 89 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
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[phone]
Page 13 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1617582MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277330004
1617583
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 87 75-12583 5 25500ND437417
Arsenic ug/L 500 83 75-12579 6 25500ND418395
Barium ug/L 500 97 75-12591 6 2550019.2 503 476
Beryllium ug/L 500 99 75-12594 6 25500ND497468
Cadmium ug/L 500 90 75-12585 5 25500ND448426
Chromium ug/L 500 95 75-12590 6 25500ND475449
Cobalt ug/L 500 87 75-12583 5 25500ND436416
Copper ug/L 500 94 75-12588 6 25500ND468441
Lead ug/L 500 86 75-12582 5 25500ND433411
Nickel ug/L 500 90 75-12585 5 25500ND449427
Selenium ug/L 500 84 75-12580 4 25500ND418401
Silver ug/L 250 91 75-12586 5 25250ND228216
Thallium ug/L 500 87 75-12584 3 255005.2J 438 424
Vanadium ug/L 500 92 75-12587 5 25500ND460436
Zinc ug/L 500 85 75-12581 5 255007.9J 432 411
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34482
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92277673001, 92277673002, 92277673003, 92277673004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616469
Associated Lab Samples:92277673001, 92277673002, 92277673003, 92277673004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/01/15 03:130.33
1,1,1-Trichloroethane ug/L ND 1.0 12/01/15 03:130.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/01/15 03:130.40
1,1,2-Trichloroethane ug/L ND 1.0 12/01/15 03:130.29
1,1-Dichloroethane ug/L ND 5.0 12/01/15 03:130.32
1,1-Dichloroethene ug/L ND 5.0 12/01/15 03:130.56
1,2,3-Trichloropropane ug/L ND 1.0 12/01/15 03:130.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/01/15 03:132.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/01/15 03:130.27
1,2-Dichlorobenzene ug/L ND 5.0 12/01/15 03:130.30
1,2-Dichloroethane ug/L ND 1.0 12/01/15 03:130.24
1,2-Dichloropropane ug/L ND 1.0 12/01/15 03:130.27
1,4-Dichlorobenzene ug/L ND 1.0 12/01/15 03:130.33
2-Butanone (MEK)ug/L ND 100 12/01/15 03:130.96
2-Hexanone ug/L ND 50.0 12/01/15 03:130.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/01/15 03:130.33
Acetone ug/L ND 100 12/01/15 03:1310.0
Acrylonitrile ug/L ND 200 12/01/15 03:131.9
Benzene ug/L ND 1.0 12/01/15 03:130.25
Bromochloromethane ug/L ND 3.0 12/01/15 03:130.17
Bromodichloromethane ug/L ND 1.0 12/01/15 03:130.18
Bromoform ug/L ND 3.0 12/01/15 03:130.26
Bromomethane ug/L ND 10.0 12/01/15 03:130.29
Carbon disulfide ug/L ND 100 12/01/15 03:131.2
Carbon tetrachloride ug/L ND 1.0 12/01/15 03:130.25
Chlorobenzene ug/L ND 3.0 12/01/15 03:130.23
Chloroethane ug/L ND 10.0 12/01/15 03:130.54
Chloroform ug/L ND 5.0 12/01/15 03:130.14
Chloromethane ug/L ND 1.0 12/01/15 03:130.11
cis-1,2-Dichloroethene ug/L ND 5.0 12/01/15 03:130.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/01/15 03:130.13
Dibromochloromethane ug/L ND 3.0 12/01/15 03:130.21
Dibromomethane ug/L ND 10.0 12/01/15 03:130.21
Ethylbenzene ug/L ND 1.0 12/01/15 03:130.30
Iodomethane ug/L ND 10.0 12/01/15 03:130.32
Methylene Chloride ug/L ND 1.0 12/01/15 03:130.97
Styrene ug/L ND 1.0 12/01/15 03:130.26
Tetrachloroethene ug/L ND 1.0 12/01/15 03:130.46
Toluene ug/L ND 1.0 12/01/15 03:130.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/01/15 03:130.49
trans-1,3-Dichloropropene ug/L ND 1.0 12/01/15 03:130.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616469
Associated Lab Samples:92277673001, 92277673002, 92277673003, 92277673004
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 12/01/15 03:131.0
Trichloroethene ug/L ND 1.0 12/01/15 03:130.47
Trichlorofluoromethane ug/L ND 1.0 12/01/15 03:130.20
Vinyl acetate ug/L ND 50.0 12/01/15 03:130.35
Vinyl chloride ug/L ND 1.0 12/01/15 03:130.62
Xylene (Total)ug/L ND 5.0 12/01/15 03:130.66
1,2-Dichloroethane-d4 (S)%97 70-130 12/01/15 03:13
4-Bromofluorobenzene (S)%103 70-130 12/01/15 03:13
Toluene-d8 (S)%100 70-130 12/01/15 03:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616470LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.050 88 80-125
1,1,1-Trichloroethane ug/L 47.550 95 71-129
1,1,2,2-Tetrachloroethane ug/L 41.950 84 79-124
1,1,2-Trichloroethane ug/L 46.050 92 85-125
1,1-Dichloroethane ug/L 49.050 98 73-126
1,1-Dichloroethene ug/L 51.650 103 66-135
1,2,3-Trichloropropane ug/L 44.150 88 75-130
1,2-Dibromo-3-chloropropane ug/L 39.550 79 71-133
1,2-Dibromoethane (EDB)ug/L 45.150 90 83-124
1,2-Dichlorobenzene ug/L 47.050 94 80-133
1,2-Dichloroethane ug/L 45.650 91 67-128
1,2-Dichloropropane ug/L 46.150 92 75-132
1,4-Dichlorobenzene ug/L 46.950 94 78-130
2-Butanone (MEK)ug/L 95.3J100 95 61-144
2-Hexanone ug/L 82.2100 82 68-143
4-Methyl-2-pentanone (MIBK)ug/L 93.9J100 94 72-135
Acetone ug/L 92.9J100 93 48-146
Acrylonitrile ug/L 239250 95 40-160
Benzene ug/L 48.850 98 80-125
Bromochloromethane ug/L 52.650 105 71-125
Bromodichloromethane ug/L 44.750 89 78-124
Bromoform ug/L 39.350 79 71-128
Bromomethane ug/L 46.150 92 40-160
Carbon disulfide ug/L 48.4J50 97 50-160
Carbon tetrachloride ug/L 48.750 97 69-131
Chlorobenzene ug/L 43.850 88 81-122
Chloroethane ug/L 50.250 100 39-148
Chloroform ug/L 49.050 98 73-127
Chloromethane ug/L 47.850 96 44-146
cis-1,2-Dichloroethene ug/L 50.950 102 74-124
cis-1,3-Dichloropropene ug/L 44.550 89 72-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616470LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 41.450 83 78-125
Dibromomethane ug/L 50.250 100 82-120
Ethylbenzene ug/L 44.550 89 79-121
Iodomethane ug/L 94.2100 94 39-154
Methylene Chloride ug/L 51.050 102 64-133
Styrene ug/L 45.950 92 84-126
Tetrachloroethene ug/L 46.350 93 78-122
Toluene ug/L 47.450 95 80-121
trans-1,2-Dichloroethene ug/L 50.850 102 71-127
trans-1,3-Dichloropropene ug/L 44.650 89 69-141
trans-1,4-Dichloro-2-butene ug/L 34.0J50 68 40-160
Trichloroethene ug/L 46.550 93 78-122
Trichlorofluoromethane ug/L 54.150 108 53-137
Vinyl acetate ug/L 95.3100 95 40-160
Vinyl chloride ug/L 55.550 111 58-137
Xylene (Total)ug/L 132150 88 81-126
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1616471MATRIX SPIKE SAMPLE:
MSSpike
Result
92277673001
1,1,1,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,1-Trichloroethane ug/L 22.120 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.520 92 70-130ND
1,1,2-Trichloroethane ug/L 21.020 105 70-130ND
1,1-Dichloroethane ug/L 22.620 113 70-130ND
1,1-Dichloroethene ug/L 24.720 123 70-166ND
1,2,3-Trichloropropane ug/L 19.220 96 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.820 84 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.820 104 70-130ND
1,2-Dichlorobenzene ug/L 21.120 105 70-130ND
1,2-Dichloroethane ug/L 20.620 103 70-130ND
1,2-Dichloropropane ug/L 20.920 105 70-130ND
1,4-Dichlorobenzene ug/L 20.820 103 70-130ND
2-Butanone (MEK)ug/L 41.8J40 105 70-130ND
2-Hexanone ug/L 36.1J40 90 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 41.1J40 103 70-130ND
Acetone ug/L 44.0J40 104 70-130ND
Acrylonitrile ug/L 106J100 106 70-130ND
Benzene ug/L 23.220 114 70-1480.35J
Bromochloromethane ug/L 25.020 125 70-130ND
Bromodichloromethane ug/L 19.220 96 70-130ND
Bromoform ug/L 16.520 83 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 04:18 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
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Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1616471MATRIX SPIKE SAMPLE:
MSSpike
Result
92277673001
Bromomethane ug/L 21.920 109 70-130ND
Carbon disulfide ug/L 22.6J20 113 70-130ND
Carbon tetrachloride ug/L 22.720 114 70-130ND
Chlorobenzene ug/L 20.920 104 70-146ND
Chloroethane ug/L 23.820 119 70-130ND
Chloroform ug/L 22.920 114 70-130ND
Chloromethane ug/L 23.520 117 70-130ND
cis-1,2-Dichloroethene ug/L 24.120 120 70-130ND
cis-1,3-Dichloropropene ug/L 19.620 98 70-130ND
Dibromochloromethane ug/L 18.620 93 70-130ND
Dibromomethane ug/L 22.720 113 70-130ND
Ethylbenzene ug/L 20.520 102 70-130ND
Iodomethane ug/L 37.440 93 70-130ND
Methylene Chloride ug/L 23.620 118 70-130ND
Styrene ug/L 20.220 101 70-130ND
Tetrachloroethene ug/L 21.620 108 70-130ND
Toluene ug/L 21.620 108 70-155ND
trans-1,2-Dichloroethene ug/L 24.220 121 70-130ND
trans-1,3-Dichloropropene ug/L 19.520 97 70-130ND
trans-1,4-Dichloro-2-butene ug/L 13.0J M1206570-130ND
Trichloroethene ug/L 20.720 104 69-151ND
Trichlorofluoromethane ug/L 25.720 129 70-130ND
Vinyl acetate ug/L 35.1J40 88 70-130ND
Vinyl chloride ug/L 27.3 M12013770-130ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277673002
1616472SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.94J 300.85J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L 0.47J 300.47J
1,2-Dichloropropane ug/L 1.9 7 302.0
1,4-Dichlorobenzene ug/L 4.4 5 304.6
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 18 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277673002
1616472SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.88J 300.88J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 1.3J 7 301.3J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 2.6J 5 302.5J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%99 297
4-Bromofluorobenzene (S)%105 0104
Toluene-d8 (S)%99 198
REPORT OF LABORATORY ANALYSIS
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Page 19 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41653
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92277673002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616619
Associated Lab Samples:92277673002
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 11/30/15 20:15100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616620LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 497J500 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616621MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277680001
1616622
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L H15009590-11095 0 10500ND473J473J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616623MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277687001
1616624
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M1500090-1100 10500NDNDND
REPORT OF LABORATORY ANALYSIS
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Page 20 of 24
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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Page 21 of 24
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92277673
SURRY CLOSED-MT. AIRY (AM)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92277673001 MPRP/20147 ICP/18175MW-6 EPA 3010 EPA 6010
92277673002 MPRP/20147 ICP/18175MW-11 EPA 3010 EPA 6010
92277673003 MPRP/20147 ICP/18175MW-12D EPA 3010 EPA 6010
92277673004 MPRP/20147 ICP/18175SCALEHOUSEEPA 3010 EPA 6010
92277673001 MSV/34482MW-6 EPA 8260
92277673002 MSV/34482MW-11 EPA 8260
92277673003 MSV/34482MW-12D EPA 8260
92277673004 MSV/34482SCALEHOUSEEPA 8260
92277673002 WET/41653MW-11 SM 4500-S2D
REPORT OF LABORATORY ANALYSIS
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Page 22 of 24
Page 23 of 24
Page 24 of 24
#=CL#
February 19, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92277680
92277680
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY CLOSED-MT. AIRY (UIC)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on November 25, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Dale Ingram for
[e-mail]
Project Manager
Kevin Godwin
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 55
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
Asheville Certification IDs2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 55
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID Matrix Date Collected Date Received
92277680001 MW-1 Water 11/22/15 15:30 11/25/15 15:55
92277680002 MW-7 Water 11/22/15 13:05 11/25/15 15:55
92277680003 MW-9 Water 11/22/15 17:00 11/25/15 15:55
92277680004 MW-14 Water 11/22/15 11:50 11/25/15 15:55
92277680005 MW-15 Water 11/22/15 12:20 11/25/15 15:55
92277680006 MW-21 Water 11/22/15 10:50 11/25/15 15:55
92277680007 MW-3R Water 11/22/15 14:30 11/25/15 15:55
92277680008 MW-12S Water 11/23/15 10:10 11/25/15 15:55
92277680009 MW-13 Water 11/22/15 11:15 11/25/15 15:55
92277680010 MW-16 Water 11/22/15 15:50 11/25/15 15:55
92277680011 MW-17 Water 11/22/15 08:30 11/25/15 15:55
92277680012 MW-18 Water 11/23/15 10:35 11/25/15 15:55
92277680013 MW-19 Water 11/22/15 16:30 11/25/15 15:55
92277680014 MW-20 Water 11/22/15 17:15 11/25/15 15:55
92277680015 MW-22 Water 11/22/15 09:00 11/25/15 15:55
92277680016 MW-23 Water 11/22/15 10:05 11/25/15 15:55
REPORT OF LABORATORY ANALYSIS
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Page 3 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92277680001 MW-1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 4500-S2D 1 PASI-AMJP
92277680002 MW-7 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 4500-S2D 1 PASI-AMJP
92277680003 MW-9 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 4500-S2D 1 PASI-AMJP
92277680004 MW-14 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 4500-S2D 1 PASI-AMJP
92277680005 MW-15 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 4500-S2D 1 PASI-AMJP
92277680006 MW-21 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
SM 4500-S2D 1 PASI-AMJP
92277680007 MW-3R EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277680008 MW-12S EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277680009 MW-13 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277680010 MW-16 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277680011 MW-17 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277680012 MW-18 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277680013 MW-19 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277680014 MW-20 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277680015 MW-22 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277680016 MW-23 EPA 6010 15 PASI-ACDF
REPORT OF LABORATORY ANALYSIS
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Page 4 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260 50 PASI-CNB
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 5 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-1 Lab ID:92277680001 Collected:11/22/15 15:30 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 04:36 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 04:36 7440-38-212/01/15 19:0010.0 2.5 1
Barium 26.2J ug/L 12/05/15 04:36 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 19:39 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 04:36 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 04:36 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 04:36 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 04:36 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 04:36 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 04:36 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 04:36 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 04:36 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 19:39 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 04:36 7440-62-212/01/15 19:0025.0 2.5 1
Zinc 7.1J ug/L 12/05/15 04:36 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 06:04 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 06:04 107-13-12001.9 1
Benzene ND ug/L 12/06/15 06:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 06:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 06:04 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 06:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 06:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 06:04 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 06:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 06:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/06/15 06:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 06:04 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 06:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 06:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 06:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 06:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 06:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 06:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 06:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 06:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 06:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/06/15 06:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 06:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 06:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/06/15 06:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 06:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 06:04 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 06:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 06:04 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-1 Lab ID:92277680001 Collected:11/22/15 15:30 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 06:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 06:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 06:04 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 06:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 06:04 108-10-11000.33 1
Styrene ND ug/L 12/06/15 06:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 06:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 06:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 06:04 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 06:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 06:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 06:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 06:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 06:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 06:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 06:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 06:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 06:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %12/06/15 06:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/06/15 06:04 17060-07-070-130 1
Toluene-d8 (S)97 %12/06/15 06:04 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/30/15 20:15 18496-25-8 H310001001
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-7 Lab ID:92277680002 Collected:11/22/15 13:05 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 04:39 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 04:39 7440-38-212/01/15 19:0010.0 2.5 1
Barium 64.1J ug/L 12/05/15 04:39 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 19:42 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 04:39 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 04:39 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt 56.6 ug/L 12/05/15 04:39 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 04:39 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 04:39 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 04:39 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 04:39 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 04:39 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 19:42 7440-28-012/01/15 19:005.5 5.0 1
Vanadium 9.0J ug/L 12/05/15 04:39 7440-62-212/01/15 19:0025.0 2.5 1
Zinc 8.1J ug/L 12/05/15 04:39 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 06:22 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 06:22 107-13-12001.9 1
Benzene ND ug/L 12/06/15 06:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 06:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 06:22 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 06:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 06:22 74-83-9 M110.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 06:22 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 06:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 06:22 56-23-51.0 0.25 1
Chlorobenzene 2.6J ug/L 12/06/15 06:22 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 06:22 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 06:22 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 06:22 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 06:22 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 06:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 06:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 06:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 06:22 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.6 ug/L 12/06/15 06:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 06:22 110-57-6 M11001.0 1
1,1-Dichloroethane ND ug/L 12/06/15 06:22 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 06:22 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 06:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/06/15 06:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 06:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 06:22 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 06:22 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 06:22 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-7 Lab ID:92277680002 Collected:11/22/15 13:05 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 06:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 06:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 06:22 74-88-4 M110.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 06:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 06:22 108-10-11000.33 1
Styrene ND ug/L 12/06/15 06:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 06:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 06:22 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 06:22 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 06:22 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 06:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 06:22 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 06:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 06:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 06:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 06:22 108-05-4 M150.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 06:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 06:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %12/06/15 06:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/06/15 06:22 17060-07-070-130 1
Toluene-d8 (S)96 %12/06/15 06:22 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/30/15 20:15 18496-25-8 H310001001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-9 Lab ID:92277680003 Collected:11/22/15 17:00 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 04:42 7440-36-012/01/15 19:006.0 3.8 1
Arsenic 2.9J ug/L 12/05/15 04:42 7440-38-212/01/15 19:0010.0 2.5 1
Barium 45.3J ug/L 12/05/15 04:42 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 19:45 7440-41-712/01/15 19:001.0 0.50 1
Cadmium 0.95J ug/L 12/05/15 04:42 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 04:42 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt 180 ug/L 12/05/15 04:42 7440-48-412/01/15 19:0010.0 2.5 1
Copper 2.9J ug/L 12/05/15 04:42 7440-50-812/01/15 19:0010.0 2.5 1
Lead 2.5J ug/L 12/05/15 04:42 7439-92-112/01/15 19:0010.0 2.5 1
Nickel 6.3J ug/L 12/05/15 04:42 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 04:42 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 04:42 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 19:45 7440-28-012/01/15 19:005.5 5.0 1
Vanadium 13.0J ug/L 12/05/15 04:42 7440-62-212/01/15 19:0025.0 2.5 1
Zinc 36.9 ug/L 12/05/15 04:42 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 06:39 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 06:39 107-13-12001.9 1
Benzene 1.6 ug/L 12/06/15 06:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 06:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 06:39 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 06:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 06:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 06:39 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 06:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 06:39 56-23-51.0 0.25 1
Chlorobenzene 1.8J ug/L 12/06/15 06:39 108-90-73.0 0.23 1
Chloroethane 1.6J ug/L 12/06/15 06:39 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 06:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 06:39 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 06:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 06:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 06:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 06:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene 1.0J ug/L 12/06/15 06:39 95-50-15.0 0.30 1
1,4-Dichlorobenzene 5.2 ug/L 12/06/15 06:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 06:39 110-57-61001.0 1
1,1-Dichloroethane 2.1J ug/L 12/06/15 06:39 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 06:39 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 06:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 14.2 ug/L 12/06/15 06:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 06:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 06:39 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 06:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 06:39 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-9 Lab ID:92277680003 Collected:11/22/15 17:00 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 06:39 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 06:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 06:39 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 06:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 06:39 108-10-11000.33 1
Styrene ND ug/L 12/06/15 06:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 06:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 06:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 06:39 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 06:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 06:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 06:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 06:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 06:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 06:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 06:39 108-05-450.0 0.35 1
Vinyl chloride 7.9 ug/L 12/06/15 06:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 06:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %12/06/15 06:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/06/15 06:39 17060-07-070-130 1
Toluene-d8 (S)95 %12/06/15 06:39 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/30/15 20:15 18496-25-8 H310001001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-14 Lab ID:92277680004 Collected:11/22/15 11:50 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 04:45 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 04:45 7440-38-212/01/15 19:0010.0 2.5 1
Barium 25.1J ug/L 12/05/15 04:45 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 19:58 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 04:45 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 04:45 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 04:45 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 04:45 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 04:45 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 04:45 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 04:45 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 04:45 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 19:58 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 04:45 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 04:45 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 07:15 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 07:15 107-13-12001.9 1
Benzene ND ug/L 12/06/15 07:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 07:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 07:15 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 07:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 07:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 07:15 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 07:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 07:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/06/15 07:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 07:15 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 07:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 07:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 07:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 07:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 07:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 07:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 07:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 07:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 07:15 110-57-61001.0 1
1,1-Dichloroethane 3.5J ug/L 12/06/15 07:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 07:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 07:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 4.8J ug/L 12/06/15 07:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 07:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 07:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 07:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 07:15 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-14 Lab ID:92277680004 Collected:11/22/15 11:50 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 07:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 07:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 07:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 07:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 07:15 108-10-11000.33 1
Styrene ND ug/L 12/06/15 07:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 07:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 07:15 79-34-53.0 0.40 1
Tetrachloroethene 0.64J ug/L 12/06/15 07:15 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 07:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 07:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 07:15 79-00-51.0 0.29 1
Trichloroethene 0.79J ug/L 12/06/15 07:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 07:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 07:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 07:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 07:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 07:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %12/06/15 07:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/06/15 07:15 17060-07-070-130 1
Toluene-d8 (S)96 %12/06/15 07:15 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/30/15 20:15 18496-25-8 H310001001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-15 Lab ID:92277680005 Collected:11/22/15 12:20 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 04:49 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 04:49 7440-38-212/01/15 19:0010.0 2.5 1
Barium 53.8J ug/L 12/05/15 04:49 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 20:01 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 04:49 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 04:49 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 04:49 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 04:49 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 04:49 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 04:49 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 04:49 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 04:49 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 20:01 7440-28-012/01/15 19:005.5 5.0 1
Vanadium 2.8J ug/L 12/05/15 04:49 7440-62-212/01/15 19:0025.0 2.5 1
Zinc 11.2 ug/L 12/05/15 04:49 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 07:33 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 07:33 107-13-12001.9 1
Benzene 2.3 ug/L 12/06/15 07:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 07:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 07:33 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 07:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 07:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 07:33 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 07:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 07:33 56-23-51.0 0.25 1
Chlorobenzene 3.3 ug/L 12/06/15 07:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 07:33 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 07:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 07:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 07:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 07:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 07:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 07:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 07:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 07:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 07:33 110-57-61001.0 1
1,1-Dichloroethane 12.8 ug/L 12/06/15 07:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 07:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 07:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 39.1 ug/L 12/06/15 07:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 07:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 07:33 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 07:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 07:33 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-15 Lab ID:92277680005 Collected:11/22/15 12:20 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 07:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 07:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 07:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 07:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 07:33 108-10-11000.33 1
Styrene ND ug/L 12/06/15 07:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 07:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 07:33 79-34-53.0 0.40 1
Tetrachloroethene 1.0 ug/L 12/06/15 07:33 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 07:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 07:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 07:33 79-00-51.0 0.29 1
Trichloroethene 2.9 ug/L 12/06/15 07:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 07:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane 2.5 ug/L 12/06/15 07:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 07:33 108-05-450.0 0.35 1
Vinyl chloride 1.7 ug/L 12/06/15 07:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 07:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %12/06/15 07:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %12/06/15 07:33 17060-07-070-130 1
Toluene-d8 (S)96 %12/06/15 07:33 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/30/15 20:15 18496-25-8 H310001001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-21 Lab ID:92277680006 Collected:11/22/15 10:50 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 04:52 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 04:52 7440-38-212/01/15 19:0010.0 2.5 1
Barium 57.6J ug/L 12/05/15 04:52 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 20:04 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 04:52 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 04:52 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt 3.6J ug/L 12/05/15 04:52 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 04:52 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 04:52 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 04:52 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 04:52 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 04:52 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 20:04 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 04:52 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 04:52 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 07:50 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 07:50 107-13-12001.9 1
Benzene ND ug/L 12/06/15 07:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 07:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 07:50 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 07:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 07:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 07:50 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 07:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 07:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/06/15 07:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 07:50 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 07:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 07:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 07:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 07:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 07:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 07:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 07:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 07:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 07:50 110-57-61001.0 1
1,1-Dichloroethane 3.5J ug/L 12/06/15 07:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 07:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 07:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 13.4 ug/L 12/06/15 07:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 07:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 07:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 07:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 07:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-21 Lab ID:92277680006 Collected:11/22/15 10:50 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 07:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 07:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 07:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 07:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 07:50 108-10-11000.33 1
Styrene ND ug/L 12/06/15 07:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 07:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 07:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 07:50 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 07:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 07:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 07:50 79-00-51.0 0.29 1
Trichloroethene 0.87J ug/L 12/06/15 07:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 07:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 07:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 07:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 07:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 07:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %12/06/15 07:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/06/15 07:50 17060-07-070-130 1
Toluene-d8 (S)96 %12/06/15 07:50 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/30/15 20:15 18496-25-8 H310001001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-3R Lab ID:92277680007 Collected:11/22/15 14:30 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 04:55 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 04:55 7440-38-212/01/15 19:0010.0 2.5 1
Barium 5.9J ug/L 12/05/15 04:55 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 20:07 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 04:55 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 04:55 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 04:55 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 04:55 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 04:55 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 04:55 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 04:55 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 04:55 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 20:07 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 04:55 7440-62-212/01/15 19:0025.0 2.5 1
Zinc 9.2J ug/L 12/05/15 04:55 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 08:08 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 08:08 107-13-12001.9 1
Benzene ND ug/L 12/06/15 08:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 08:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 08:08 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 08:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 08:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 08:08 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 08:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 08:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/06/15 08:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 08:08 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 08:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 08:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 08:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 08:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 08:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 08:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 08:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 08:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 08:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/06/15 08:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 08:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 08:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/06/15 08:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 08:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 08:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 08:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 08:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-3R Lab ID:92277680007 Collected:11/22/15 14:30 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 08:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 08:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 08:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 08:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 08:08 108-10-11000.33 1
Styrene ND ug/L 12/06/15 08:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 08:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 08:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 08:08 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 08:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 08:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 08:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 08:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 08:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 08:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 08:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 08:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 08:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %12/06/15 08:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/06/15 08:08 17060-07-070-130 1
Toluene-d8 (S)95 %12/06/15 08:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-12S Lab ID:92277680008 Collected:11/23/15 10:10 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 04:58 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 04:58 7440-38-212/01/15 19:0010.0 2.5 1
Barium 17.5J ug/L 12/05/15 04:58 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 20:10 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 04:58 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 04:58 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 04:58 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 04:58 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 04:58 7439-92-112/01/15 19:0010.0 2.5 1
Nickel 3.7J ug/L 12/05/15 04:58 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 04:58 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 04:58 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 20:10 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 04:58 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 04:58 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 08:27 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 08:27 107-13-12001.9 1
Benzene ND ug/L 12/06/15 08:27 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 08:27 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 08:27 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 08:27 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 08:27 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 08:27 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 08:27 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 08:27 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/06/15 08:27 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 08:27 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 08:27 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 08:27 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 08:27 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 08:27 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 08:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 08:27 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 08:27 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 08:27 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 08:27 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/06/15 08:27 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 08:27 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 08:27 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/06/15 08:27 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 08:27 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 08:27 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 08:27 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 08:27 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-12S Lab ID:92277680008 Collected:11/23/15 10:10 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 08:27 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 08:27 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 08:27 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 08:27 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 08:27 108-10-11000.33 1
Styrene ND ug/L 12/06/15 08:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 08:27 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 08:27 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 08:27 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 08:27 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 08:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 08:27 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 08:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 08:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 08:27 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 08:27 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 08:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 08:27 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %12/06/15 08:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/06/15 08:27 17060-07-070-130 1
Toluene-d8 (S)95 %12/06/15 08:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-13 Lab ID:92277680009 Collected:11/22/15 11:15 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 05:23 7440-36-012/03/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 05:23 7440-38-212/03/15 19:0010.0 2.5 1
Barium 20.4J ug/L 12/05/15 05:23 7440-39-312/03/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 05:23 7440-41-712/03/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 05:23 7440-43-912/03/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 05:23 7440-47-312/03/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 05:23 7440-48-412/03/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 05:23 7440-50-812/03/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 05:23 7439-92-112/03/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 05:23 7440-02-012/03/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 05:23 7782-49-212/03/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 05:23 7440-22-412/03/15 19:0010.0 2.5 1
Thallium 6.5 ug/L 12/07/15 20:23 7440-28-012/03/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 05:23 7440-62-212/03/15 19:0025.0 2.5 1
Zinc 7.3J ug/L 12/05/15 05:23 7440-66-612/03/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 08:44 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 08:44 107-13-12001.9 1
Benzene ND ug/L 12/06/15 08:44 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 08:44 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 08:44 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 08:44 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 08:44 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 08:44 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 08:44 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 08:44 56-23-51.0 0.25 1
Chlorobenzene 0.65J ug/L 12/06/15 08:44 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 08:44 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 08:44 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 08:44 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 08:44 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 08:44 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 08:44 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 08:44 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 08:44 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 08:44 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 08:44 110-57-61001.0 1
1,1-Dichloroethane 4.3J ug/L 12/06/15 08:44 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 08:44 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 08:44 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 23.1 ug/L 12/06/15 08:44 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 08:44 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 08:44 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 08:44 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 08:44 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-13 Lab ID:92277680009 Collected:11/22/15 11:15 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 08:44 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 08:44 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 08:44 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 08:44 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 08:44 108-10-11000.33 1
Styrene ND ug/L 12/06/15 08:44 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 08:44 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 08:44 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 08:44 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 08:44 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 08:44 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 08:44 79-00-51.0 0.29 1
Trichloroethene 1.0 ug/L 12/06/15 08:44 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 08:44 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 08:44 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 08:44 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 08:44 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 08:44 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %12/06/15 08:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %12/06/15 08:44 17060-07-070-130 1
Toluene-d8 (S)96 %12/06/15 08:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-16 Lab ID:92277680010 Collected:11/22/15 15:50 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 05:10 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 05:10 7440-38-212/01/15 19:0010.0 2.5 1
Barium 125 ug/L 12/05/15 05:10 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 20:13 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 05:10 7440-43-912/01/15 19:001.0 0.50 1
Chromium 4.9J ug/L 12/05/15 05:10 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt 348 ug/L 12/05/15 05:10 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 05:10 7440-50-812/01/15 19:0010.0 2.5 1
Lead 4.4J ug/L 12/05/15 05:10 7439-92-112/01/15 19:0010.0 2.5 1
Nickel 20.3J ug/L 12/05/15 05:10 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 05:10 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 05:10 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 20:13 7440-28-012/01/15 19:005.5 5.0 1
Vanadium 35.6 ug/L 12/05/15 05:10 7440-62-212/01/15 19:0025.0 2.5 1
Zinc 12.3 ug/L 12/05/15 05:10 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 09:02 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 09:02 107-13-12001.9 1
Benzene 1.4 ug/L 12/06/15 09:02 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 09:02 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 09:02 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 09:02 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 09:02 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 09:02 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 09:02 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 09:02 56-23-51.0 0.25 1
Chlorobenzene 6.7 ug/L 12/06/15 09:02 108-90-73.0 0.23 1
Chloroethane 0.66J ug/L 12/06/15 09:02 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 09:02 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 09:02 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 09:02 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 09:02 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 09:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 09:02 74-95-310.0 0.21 1
1,2-Dichlorobenzene 1.8J ug/L 12/06/15 09:02 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 09:02 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 09:02 110-57-61001.0 1
1,1-Dichloroethane 1.9J ug/L 12/06/15 09:02 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 09:02 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 09:02 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 44.1 ug/L 12/06/15 09:02 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 09:02 156-60-55.0 0.49 1
1,2-Dichloropropane 3.2 ug/L 12/06/15 09:02 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 09:02 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 09:02 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-16 Lab ID:92277680010 Collected:11/22/15 15:50 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 09:02 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 09:02 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 09:02 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 09:02 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 09:02 108-10-11000.33 1
Styrene ND ug/L 12/06/15 09:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 09:02 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 09:02 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 09:02 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 09:02 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 09:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 09:02 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 09:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 09:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 09:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 09:02 108-05-450.0 0.35 1
Vinyl chloride 4.1 ug/L 12/06/15 09:02 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 09:02 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %12/06/15 09:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/06/15 09:02 17060-07-070-130 1
Toluene-d8 (S)95 %12/06/15 09:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-17 Lab ID:92277680011 Collected:11/22/15 08:30 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 05:32 7440-36-012/03/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 05:32 7440-38-212/03/15 19:0010.0 2.5 1
Barium 52.2J ug/L 12/05/15 05:32 7440-39-312/03/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 05:32 7440-41-712/03/15 19:001.0 0.50 1
Cadmium 1.6 ug/L 12/05/15 05:32 7440-43-912/03/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 05:32 7440-47-312/03/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 05:32 7440-48-412/03/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 05:32 7440-50-812/03/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 05:32 7439-92-112/03/15 19:0010.0 2.5 1
Nickel 2.7J ug/L 12/05/15 05:32 7440-02-012/03/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 05:32 7782-49-212/03/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 05:32 7440-22-412/03/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 20:41 7440-28-012/03/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 05:32 7440-62-212/03/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 05:32 7440-66-612/03/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 09:21 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 09:21 107-13-12001.9 1
Benzene ND ug/L 12/06/15 09:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 09:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 09:21 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 09:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 09:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 09:21 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 09:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 09:21 56-23-51.0 0.25 1
Chlorobenzene 1.3J ug/L 12/06/15 09:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 09:21 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 09:21 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 09:21 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 09:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 09:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 09:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 09:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.83J ug/L 12/06/15 09:21 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 09:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 09:21 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/06/15 09:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 09:21 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 09:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.83J ug/L 12/06/15 09:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 09:21 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 09:21 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 09:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 09:21 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-17 Lab ID:92277680011 Collected:11/22/15 08:30 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 09:21 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 09:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 09:21 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 09:21 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 09:21 108-10-11000.33 1
Styrene ND ug/L 12/06/15 09:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 09:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 09:21 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 09:21 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 09:21 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 09:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 09:21 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 09:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 09:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 09:21 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 09:21 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 09:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 09:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %12/06/15 09:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/06/15 09:21 17060-07-070-130 1
Toluene-d8 (S)95 %12/06/15 09:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-18 Lab ID:92277680012 Collected:11/23/15 10:35 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 05:35 7440-36-012/03/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 05:35 7440-38-212/03/15 19:0010.0 2.5 1
Barium 11.1J ug/L 12/05/15 05:35 7440-39-312/03/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 05:35 7440-41-712/03/15 19:001.0 0.50 1
Cadmium 2.0 ug/L 12/05/15 05:35 7440-43-912/03/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 05:35 7440-47-312/03/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 05:35 7440-48-412/03/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 05:35 7440-50-812/03/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 05:35 7439-92-112/03/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 05:35 7440-02-012/03/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 05:35 7782-49-212/03/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 05:35 7440-22-412/03/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 20:44 7440-28-012/03/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 05:35 7440-62-212/03/15 19:0025.0 2.5 1
Zinc 6.9J ug/L 12/05/15 05:35 7440-66-612/03/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 09:38 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 09:38 107-13-12001.9 1
Benzene ND ug/L 12/06/15 09:38 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 09:38 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 09:38 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 09:38 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 09:38 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 09:38 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 09:38 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 09:38 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/06/15 09:38 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 09:38 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 09:38 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 09:38 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 09:38 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 09:38 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 09:38 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 09:38 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 09:38 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 09:38 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 09:38 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/06/15 09:38 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 09:38 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 09:38 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/06/15 09:38 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 09:38 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 09:38 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 09:38 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 09:38 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-18 Lab ID:92277680012 Collected:11/23/15 10:35 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 09:38 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 09:38 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 09:38 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 09:38 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 09:38 108-10-11000.33 1
Styrene ND ug/L 12/06/15 09:38 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 09:38 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 09:38 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 09:38 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 09:38 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 09:38 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 09:38 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 09:38 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 09:38 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 09:38 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 09:38 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 09:38 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 09:38 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %12/06/15 09:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/06/15 09:38 17060-07-070-130 1
Toluene-d8 (S)97 %12/06/15 09:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-19 Lab ID:92277680013 Collected:11/22/15 16:30 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 05:38 7440-36-012/03/15 19:006.0 3.8 1
Arsenic 2.7J ug/L 12/05/15 05:38 7440-38-212/03/15 19:0010.0 2.5 1
Barium 72.9J ug/L 12/05/15 05:38 7440-39-312/03/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 05:38 7440-41-712/03/15 19:001.0 0.50 1
Cadmium 0.93J ug/L 12/05/15 05:38 7440-43-912/03/15 19:001.0 0.50 1
Chromium 4.9J ug/L 12/05/15 05:38 7440-47-312/03/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 05:38 7440-48-412/03/15 19:0010.0 2.5 1
Copper 3.1J ug/L 12/05/15 05:38 7440-50-812/03/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 05:38 7439-92-112/03/15 19:0010.0 2.5 1
Nickel 3.1J ug/L 12/05/15 05:38 7440-02-012/03/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 05:38 7782-49-212/03/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 05:38 7440-22-412/03/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 20:47 7440-28-012/03/15 19:005.5 5.0 1
Vanadium 6.6J ug/L 12/05/15 05:38 7440-62-212/03/15 19:0025.0 2.5 1
Zinc 19.9 ug/L 12/05/15 05:38 7440-66-612/03/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 09:56 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 09:56 107-13-12001.9 1
Benzene ND ug/L 12/06/15 09:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 09:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 09:56 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 09:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 09:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 09:56 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 09:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 09:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/06/15 09:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 09:56 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 09:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 09:56 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 09:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 09:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 09:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 09:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 09:56 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 09:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 09:56 110-57-61001.0 1
1,1-Dichloroethane 1.1J ug/L 12/06/15 09:56 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 09:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 09:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.4J ug/L 12/06/15 09:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 09:56 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 09:56 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 09:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 09:56 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-19 Lab ID:92277680013 Collected:11/22/15 16:30 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 09:56 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 09:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 09:56 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 09:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 09:56 108-10-11000.33 1
Styrene ND ug/L 12/06/15 09:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 09:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 09:56 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 09:56 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 09:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 09:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 09:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 09:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 09:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 09:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 09:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 09:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 09:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %12/06/15 09:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %12/06/15 09:56 17060-07-070-130 1
Toluene-d8 (S)98 %12/06/15 09:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-20 Lab ID:92277680014 Collected:11/22/15 17:15 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 05:50 7440-36-012/03/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 05:50 7440-38-212/03/15 19:0010.0 2.5 1
Barium 31.4J ug/L 12/05/15 05:50 7440-39-312/03/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 05:50 7440-41-712/03/15 19:001.0 0.50 1
Cadmium 0.83J ug/L 12/05/15 05:50 7440-43-912/03/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 05:50 7440-47-312/03/15 19:0010.0 2.5 1
Cobalt 17.9 ug/L 12/05/15 05:50 7440-48-412/03/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 05:50 7440-50-812/03/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 05:50 7439-92-112/03/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 05:50 7440-02-012/03/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 05:50 7782-49-212/03/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 05:50 7440-22-412/03/15 19:0010.0 2.5 1
Thallium ND ug/L 12/05/15 05:50 7440-28-012/03/15 19:005.5 5.0 1
Vanadium 4.0J ug/L 12/05/15 05:50 7440-62-212/03/15 19:0025.0 2.5 1
Zinc 15.0 ug/L 12/05/15 05:50 7440-66-612/03/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 10:14 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 10:14 107-13-12001.9 1
Benzene ND ug/L 12/06/15 10:14 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 10:14 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 10:14 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 10:14 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 10:14 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 10:14 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 10:14 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 10:14 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/06/15 10:14 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 10:14 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 10:14 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 10:14 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 10:14 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 10:14 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 10:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 10:14 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 10:14 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 10:14 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 10:14 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/06/15 10:14 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 10:14 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 10:14 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.63J ug/L 12/06/15 10:14 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 10:14 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 10:14 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 10:14 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 10:14 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-20 Lab ID:92277680014 Collected:11/22/15 17:15 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 10:14 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 10:14 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 10:14 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 10:14 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 10:14 108-10-11000.33 1
Styrene ND ug/L 12/06/15 10:14 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 10:14 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 10:14 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 10:14 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 10:14 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 10:14 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 10:14 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 10:14 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 10:14 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 10:14 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 10:14 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 10:14 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 10:14 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %12/06/15 10:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/06/15 10:14 17060-07-070-130 1
Toluene-d8 (S)97 %12/06/15 10:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-22 Lab ID:92277680015 Collected:11/22/15 09:00 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 05:53 7440-36-012/03/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 05:53 7440-38-212/03/15 19:0010.0 2.5 1
Barium 72.9J ug/L 12/05/15 05:53 7440-39-312/03/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 05:53 7440-41-712/03/15 19:001.0 0.50 1
Cadmium 0.89J ug/L 12/05/15 05:53 7440-43-912/03/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 05:53 7440-47-312/03/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 05:53 7440-48-412/03/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 05:53 7440-50-812/03/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 05:53 7439-92-112/03/15 19:0010.0 2.5 1
Nickel 4.8J ug/L 12/05/15 05:53 7440-02-012/03/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 05:53 7782-49-212/03/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 05:53 7440-22-412/03/15 19:0010.0 2.5 1
Thallium ND ug/L 12/05/15 05:53 7440-28-012/03/15 19:005.5 5.0 1
Vanadium 4.1J ug/L 12/05/15 05:53 7440-62-212/03/15 19:0025.0 2.5 1
Zinc 9.8J ug/L 12/05/15 05:53 7440-66-612/03/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 10:31 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 10:31 107-13-12001.9 1
Benzene ND ug/L 12/06/15 10:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 10:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 10:31 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 10:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 10:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 10:31 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 10:31 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 10:31 56-23-51.0 0.25 1
Chlorobenzene 0.45J ug/L 12/06/15 10:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 10:31 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 10:31 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 10:31 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 10:31 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 10:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 10:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 10:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 10:31 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 10:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 10:31 110-57-61001.0 1
1,1-Dichloroethane 0.61J ug/L 12/06/15 10:31 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 10:31 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 10:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.0J ug/L 12/06/15 10:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 10:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 10:31 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 10:31 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 10:31 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-22 Lab ID:92277680015 Collected:11/22/15 09:00 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 10:31 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 10:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 10:31 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 10:31 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 10:31 108-10-11000.33 1
Styrene ND ug/L 12/06/15 10:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 10:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 10:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 10:31 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 10:31 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 10:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 10:31 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 10:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 10:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 10:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 10:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 10:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 10:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %12/06/15 10:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %12/06/15 10:31 17060-07-070-130 1
Toluene-d8 (S)97 %12/06/15 10:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-23 Lab ID:92277680016 Collected:11/22/15 10:05 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/05/15 05:57 7440-36-012/03/15 19:006.0 3.8 1
Arsenic 2.6J ug/L 12/05/15 05:57 7440-38-212/03/15 19:0010.0 2.5 1
Barium 20.3J ug/L 12/05/15 05:57 7440-39-312/03/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 05:57 7440-41-712/03/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 05:57 7440-43-912/03/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 05:57 7440-47-312/03/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 05:57 7440-48-412/03/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 05:57 7440-50-812/03/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 05:57 7439-92-112/03/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 05:57 7440-02-012/03/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 05:57 7782-49-212/03/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 05:57 7440-22-412/03/15 19:0010.0 2.5 1
Thallium ND ug/L 12/05/15 05:57 7440-28-012/03/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 05:57 7440-62-212/03/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 05:57 7440-66-612/03/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/06/15 10:49 67-64-110010.0 1
Acrylonitrile ND ug/L 12/06/15 10:49 107-13-12001.9 1
Benzene ND ug/L 12/06/15 10:49 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/06/15 10:49 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/06/15 10:49 75-27-41.0 0.18 1
Bromoform ND ug/L 12/06/15 10:49 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/06/15 10:49 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/06/15 10:49 78-93-31000.96 1
Carbon disulfide ND ug/L 12/06/15 10:49 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/06/15 10:49 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/06/15 10:49 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/06/15 10:49 75-00-310.0 0.54 1
Chloroform ND ug/L 12/06/15 10:49 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/06/15 10:49 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/15 10:49 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/06/15 10:49 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/15 10:49 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/06/15 10:49 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/06/15 10:49 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/06/15 10:49 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/06/15 10:49 110-57-61001.0 1
1,1-Dichloroethane 0.43J ug/L 12/06/15 10:49 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/06/15 10:49 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/06/15 10:49 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/06/15 10:49 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/06/15 10:49 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/06/15 10:49 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/06/15 10:49 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/06/15 10:49 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-23 Lab ID:92277680016 Collected:11/22/15 10:05 Received:11/25/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/06/15 10:49 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/06/15 10:49 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/06/15 10:49 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/06/15 10:49 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/15 10:49 108-10-11000.33 1
Styrene ND ug/L 12/06/15 10:49 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/15 10:49 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/15 10:49 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/06/15 10:49 127-18-41.0 0.46 1
Toluene ND ug/L 12/06/15 10:49 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/06/15 10:49 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/06/15 10:49 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/06/15 10:49 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/06/15 10:49 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/06/15 10:49 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/06/15 10:49 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/06/15 10:49 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/06/15 10:49 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %12/06/15 10:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %12/06/15 10:49 17060-07-070-130 1
Toluene-d8 (S)97 %12/06/15 10:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 37 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20148
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92277680001, 92277680002, 92277680003, 92277680004, 92277680005, 92277680006, 92277680007,
92277680008, 92277680010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617591
Associated Lab Samples:92277680001, 92277680002, 92277680003, 92277680004, 92277680005, 92277680006, 92277680007,
92277680008, 92277680010
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/05/15 03:313.8
Arsenic ug/L ND 10.0 12/05/15 03:312.5
Barium ug/L ND 100 12/05/15 03:312.5
Beryllium ug/L ND 1.0 12/07/15 18:440.50
Cadmium ug/L ND 1.0 12/05/15 03:310.50
Chromium ug/L ND 10.0 12/05/15 03:312.5
Cobalt ug/L ND 10.0 12/05/15 03:312.5
Copper ug/L ND 10.0 12/05/15 03:312.5
Lead ug/L ND 10.0 12/05/15 03:312.5
Nickel ug/L ND 50.0 12/05/15 03:312.5
Selenium ug/L ND 10.0 12/05/15 03:315.0
Silver ug/L ND 10.0 12/05/15 03:312.5
Thallium ug/L ND 5.5 12/07/15 18:445.0
Vanadium ug/L ND 25.0 12/05/15 03:312.5
Zinc ug/L ND 10.0 12/05/15 03:315.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617592LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 433500 87 80-120
Arsenic ug/L 412500 82 80-120
Barium ug/L 415500 83 80-120
Beryllium ug/L 409500 82 80-120
Cadmium ug/L 421500 84 80-120
Chromium ug/L 415500 83 80-120
Cobalt ug/L 422500 84 80-120
Copper ug/L 426500 85 80-120
Lead ug/L 418500 84 80-120
Nickel ug/L 422500 84 80-120
Selenium ug/L 417500 83 80-120
Silver ug/L 209250 84 80-120
Thallium ug/L 411500 82 80-120
Vanadium ug/L 416500 83 80-120
Zinc ug/L 415500 83 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1617593MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277674005
1617594
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 91 75-12585 7 25500ND456424
Arsenic ug/L 500 87 75-12581 7 25500ND436405
Barium ug/L 500 99 75-12593 6 2550020.5J 515 485
Beryllium ug/L 500 95 75-12590 5 25500ND473449
Cadmium ug/L 500 93 75-12587 7 25500ND465433
Chromium ug/L 500 98 75-12592 6 25500ND488459
Cobalt ug/L 500 91 75-12584 7 25500ND453421
Copper ug/L 500 96 75-12590 6 25500ND480451
Lead ug/L 500 90 75-12584 7 25500ND448419
Nickel ug/L 500 93 75-12587 7 25500ND466435
Selenium ug/L 500 88 75-12582 8 25500ND440408
Silver ug/L 250 95 75-12589 7 25250ND237222
Thallium ug/L 500 95 75-12591 4 25500ND480461
Vanadium ug/L 500 95 75-12589 7 25500ND477445
Zinc ug/L 500 89 75-12583 7 25500ND444415
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20158
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92277680009, 92277680011, 92277680012, 92277680013, 92277680014, 92277680015, 92277680016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1618611
Associated Lab Samples:92277680009, 92277680011, 92277680012, 92277680013, 92277680014, 92277680015, 92277680016
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/05/15 05:173.8
Arsenic ug/L ND 10.0 12/05/15 05:172.5
Barium ug/L ND 100 12/05/15 05:172.5
Beryllium ug/L ND 1.0 12/05/15 05:170.50
Cadmium ug/L ND 1.0 12/05/15 05:170.50
Chromium ug/L ND 10.0 12/05/15 05:172.5
Cobalt ug/L ND 10.0 12/05/15 05:172.5
Copper ug/L ND 10.0 12/05/15 05:172.5
Lead ug/L ND 10.0 12/05/15 05:172.5
Nickel ug/L ND 50.0 12/05/15 05:172.5
Selenium ug/L ND 10.0 12/05/15 05:175.0
Silver ug/L ND 10.0 12/05/15 05:172.5
Thallium ug/L ND 5.5 12/07/15 20:165.0
Vanadium ug/L ND 25.0 12/05/15 05:172.5
Zinc ug/L ND 10.0 12/05/15 05:175.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1618612LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 463500 93 80-120
Arsenic ug/L 447500 89 80-120
Barium ug/L 517500 103 80-120
Beryllium ug/L 529500 106 80-120
Cadmium ug/L 482500 96 80-120
Chromium ug/L 503500 101 80-120
Cobalt ug/L 467500 93 80-120
Copper ug/L 496500 99 80-120
Lead ug/L 467500 93 80-120
Nickel ug/L 482500 96 80-120
Selenium ug/L 454500 91 80-120
Silver ug/L 240250 96 80-120
Thallium ug/L 502500 100 80-120
Vanadium ug/L 489500 98 80-120
Zinc ug/L 459500 92 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1618613MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277680009
1618614
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12590 9 25500ND493452
Arsenic ug/L 500 94 75-12587 8 25500ND474440
Barium ug/L 500 110 75-125102 8 2550020.4J 570 529
Beryllium ug/L 500 113 75-125105 7 25500ND564524
Cadmium ug/L 500 103 75-12595 8 25500ND514473
Chromium ug/L 500 108 75-125100 8 25500ND542501
Cobalt ug/L 500 100 75-12592 8 25500ND498460
Copper ug/L 500 106 75-12598 8 25500ND531491
Lead ug/L 500 99 75-12591 8 25500ND495457
Nickel ug/L 500 103 75-12595 8 25500ND514475
Selenium ug/L 500 97 75-12589 8 25500ND486447
Silver ug/L 250 102 75-12595 7 25250ND255237
Thallium ug/L 500 105 75-12596 9 255006.5 531 488
Vanadium ug/L 500 105 75-12597 8 25500ND527487
Zinc ug/L 500 98 75-12590 8 255007.3J 497 460
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34557
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92277680001, 92277680002, 92277680003, 92277680004, 92277680005, 92277680006, 92277680007,
92277680008, 92277680009, 92277680010, 92277680011, 92277680012, 92277680013, 92277680014,
92277680015, 92277680016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1621073
Associated Lab Samples:92277680001, 92277680002, 92277680003, 92277680004, 92277680005, 92277680006, 92277680007,
92277680008, 92277680009, 92277680010, 92277680011, 92277680012, 92277680013, 92277680014,
92277680015, 92277680016
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/06/15 04:540.33
1,1,1-Trichloroethane ug/L ND 1.0 12/06/15 04:540.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/06/15 04:540.40
1,1,2-Trichloroethane ug/L ND 1.0 12/06/15 04:540.29
1,1-Dichloroethane ug/L ND 5.0 12/06/15 04:540.32
1,1-Dichloroethene ug/L ND 5.0 12/06/15 04:540.56
1,2,3-Trichloropropane ug/L ND 1.0 12/06/15 04:540.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/06/15 04:542.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/06/15 04:540.27
1,2-Dichlorobenzene ug/L ND 5.0 12/06/15 04:540.30
1,2-Dichloroethane ug/L ND 1.0 12/06/15 04:540.24
1,2-Dichloropropane ug/L ND 1.0 12/06/15 04:540.27
1,4-Dichlorobenzene ug/L ND 1.0 12/06/15 04:540.33
2-Butanone (MEK)ug/L ND 100 12/06/15 04:540.96
2-Hexanone ug/L ND 50.0 12/06/15 04:540.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/06/15 04:540.33
Acetone ug/L ND 100 12/06/15 04:5410.0
Acrylonitrile ug/L ND 200 12/06/15 04:541.9
Benzene ug/L ND 1.0 12/06/15 04:540.25
Bromochloromethane ug/L ND 3.0 12/06/15 04:540.17
Bromodichloromethane ug/L ND 1.0 12/06/15 04:540.18
Bromoform ug/L ND 3.0 12/06/15 04:540.26
Bromomethane ug/L ND 10.0 12/06/15 04:540.29
Carbon disulfide ug/L ND 100 12/06/15 04:541.2
Carbon tetrachloride ug/L ND 1.0 12/06/15 04:540.25
Chlorobenzene ug/L ND 3.0 12/06/15 04:540.23
Chloroethane ug/L ND 10.0 12/06/15 04:540.54
Chloroform ug/L ND 5.0 12/06/15 04:540.14
Chloromethane ug/L ND 1.0 12/06/15 04:540.11
cis-1,2-Dichloroethene ug/L ND 5.0 12/06/15 04:540.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/06/15 04:540.13
Dibromochloromethane ug/L ND 3.0 12/06/15 04:540.21
Dibromomethane ug/L ND 10.0 12/06/15 04:540.21
Ethylbenzene ug/L ND 1.0 12/06/15 04:540.30
Iodomethane ug/L ND 10.0 12/06/15 04:540.32
Methylene Chloride ug/L 1.0 1.0 C912/06/15 04:540.97
Styrene ug/L ND 1.0 12/06/15 04:540.26
Tetrachloroethene ug/L ND 1.0 12/06/15 04:540.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1621073
Associated Lab Samples:92277680001, 92277680002, 92277680003, 92277680004, 92277680005, 92277680006, 92277680007,
92277680008, 92277680009, 92277680010, 92277680011, 92277680012, 92277680013, 92277680014,
92277680015, 92277680016
Matrix:Water
AnalyzedMDL
Toluene ug/L ND 1.0 12/06/15 04:540.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/06/15 04:540.49
trans-1,3-Dichloropropene ug/L ND 1.0 12/06/15 04:540.26
trans-1,4-Dichloro-2-butene ug/L ND 100 12/06/15 04:541.0
Trichloroethene ug/L ND 1.0 12/06/15 04:540.47
Trichlorofluoromethane ug/L ND 1.0 12/06/15 04:540.20
Vinyl acetate ug/L ND 50.0 12/06/15 04:540.35
Vinyl chloride ug/L ND 1.0 12/06/15 04:540.62
Xylene (Total)ug/L ND 5.0 12/06/15 04:540.66
1,2-Dichloroethane-d4 (S)%95 70-130 12/06/15 04:54
4-Bromofluorobenzene (S)%99 70-130 12/06/15 04:54
Toluene-d8 (S)%97 70-130 12/06/15 04:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1621074LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.750 93 80-125
1,1,1-Trichloroethane ug/L 43.950 88 71-129
1,1,2,2-Tetrachloroethane ug/L 45.150 90 79-124
1,1,2-Trichloroethane ug/L 42.650 85 85-125
1,1-Dichloroethane ug/L 44.150 88 73-126
1,1-Dichloroethene ug/L 46.650 93 66-135
1,2,3-Trichloropropane ug/L 49.150 98 75-130
1,2-Dibromo-3-chloropropane ug/L 44.350 89 71-133
1,2-Dibromoethane (EDB)ug/L 47.950 96 83-124
1,2-Dichlorobenzene ug/L 52.250 104 80-133
1,2-Dichloroethane ug/L 42.350 85 67-128
1,2-Dichloropropane ug/L 45.050 90 75-132
1,4-Dichlorobenzene ug/L 51.250 102 78-130
2-Butanone (MEK)ug/L 92.5J100 92 61-144
2-Hexanone ug/L 97.5100 97 68-143
4-Methyl-2-pentanone (MIBK)ug/L 100100 100 72-135
Acetone ug/L 92.7J100 93 48-146
Acrylonitrile ug/L 232250 93 40-160
Benzene ug/L 48.550 97 80-125
Bromochloromethane ug/L 44.850 90 71-125
Bromodichloromethane ug/L 42.650 85 78-124
Bromoform ug/L 39.750 79 71-128
Bromomethane ug/L 29.550 59 40-160
Carbon disulfide ug/L 41.8J50 84 50-160
Carbon tetrachloride ug/L 47.150 94 69-131
Chlorobenzene ug/L 48.450 97 81-122
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1621074LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroethane ug/L 39.450 79 39-148
Chloroform ug/L 44.850 90 73-127
Chloromethane ug/L 45.250 90 44-146
cis-1,2-Dichloroethene ug/L 47.050 94 74-124
cis-1,3-Dichloropropene ug/L 43.450 87 72-132
Dibromochloromethane ug/L 42.950 86 78-125
Dibromomethane ug/L 50.750 101 82-120
Ethylbenzene ug/L 48.150 96 79-121
Iodomethane ug/L 84.8100 85 39-154
Methylene Chloride ug/L 43.050 86 64-133
Styrene ug/L 48.950 98 84-126
Tetrachloroethene ug/L 51.550 103 78-122
Toluene ug/L 46.550 93 80-121
trans-1,2-Dichloroethene ug/L 47.850 96 71-127
trans-1,3-Dichloropropene ug/L 42.250 84 69-141
trans-1,4-Dichloro-2-butene ug/L 40.1J50 80 40-160
Trichloroethene ug/L 45.850 92 78-122
Trichlorofluoromethane ug/L 48.450 97 53-137
Vinyl acetate ug/L 86.5100 86 40-160
Vinyl chloride ug/L 48.450 97 58-137
Xylene (Total)ug/L 143150 95 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1621075MATRIX SPIKE SAMPLE:
MSSpike
Result
92277680002
1,1,1,2-Tetrachloroethane ug/L 20.920 104 70-130ND
1,1,1-Trichloroethane ug/L 19.320 97 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.820 94 70-130ND
1,1,2-Trichloroethane ug/L 18.220 91 70-130ND
1,1-Dichloroethane ug/L 18.920 95 70-130ND
1,1-Dichloroethene ug/L 19.420 97 70-166ND
1,2,3-Trichloropropane ug/L 21.020 105 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.520 92 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.620 103 70-130ND
1,2-Dichlorobenzene ug/L 22.620 112 70-130ND
1,2-Dichloroethane ug/L 17.820 89 70-130ND
1,2-Dichloropropane ug/L 19.320 96 70-130ND
1,4-Dichlorobenzene ug/L 23.920 111 70-1301.6
2-Butanone (MEK)ug/L 40.0J40 100 70-130ND
2-Hexanone ug/L 43.1J40 108 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.4J40 106 70-130ND
Acetone ug/L 42.6J40 106 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1621075MATRIX SPIKE SAMPLE:
MSSpike
Result
92277680002
Acrylonitrile ug/L 94.3J100 94 70-130ND
Benzene ug/L 21.520 108 70-148ND
Bromochloromethane ug/L 19.020 95 70-130ND
Bromodichloromethane ug/L 18.720 94 70-130ND
Bromoform ug/L 16.820 84 70-130ND
Bromomethane ug/L 6.8J M1203470-130ND
Carbon disulfide ug/L 16.7J20 83 70-130ND
Carbon tetrachloride ug/L 21.120 105 70-130ND
Chlorobenzene ug/L 23.320 104 70-1462.6J
Chloroethane ug/L 16.520 82 70-130ND
Chloroform ug/L 19.420 97 70-130ND
Chloromethane ug/L 17.920 90 70-130ND
cis-1,2-Dichloroethene ug/L 19.720 99 70-130ND
cis-1,3-Dichloropropene ug/L 17.120 85 70-130ND
Dibromochloromethane ug/L 17.920 90 70-130ND
Dibromomethane ug/L 22.320 111 70-130ND
Ethylbenzene ug/L 20.820 104 70-130ND
Iodomethane ug/L 20.1 M1405070-130ND
Methylene Chloride ug/L 17.720 89 70-130ND
Styrene ug/L 21.420 107 70-130ND
Tetrachloroethene ug/L 22.220 111 70-130ND
Toluene ug/L 20.820 104 70-155ND
trans-1,2-Dichloroethene ug/L 19.320 97 70-130ND
trans-1,3-Dichloropropene ug/L 16.720 84 70-130ND
trans-1,4-Dichloro-2-butene ug/L 12.7J M1206470-130ND
Trichloroethene ug/L 19.820 99 69-151ND
Trichlorofluoromethane ug/L 21.020 105 70-130ND
Vinyl acetate ug/L 21.9J M1405570-130ND
Vinyl chloride ug/L 19.520 97 70-130ND
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1621078MATRIX SPIKE SAMPLE:
MSSpike
Result
92278313002
1,1,1,2-Tetrachloroethane ug/L 22.620 113 70-130ND
1,1,1-Trichloroethane ug/L 20.320 101 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,2-Trichloroethane ug/L 19.620 98 70-130ND
1,1-Dichloroethane ug/L 20.720 102 70-1300.34J
1,1-Dichloroethene ug/L 20.220 101 70-166ND
1,2,3-Trichloropropane ug/L 22.920 115 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.320 107 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.020 110 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1621078MATRIX SPIKE SAMPLE:
MSSpike
Result
92278313002
1,2-Dichlorobenzene ug/L 24.820 124 70-130ND
1,2-Dichloroethane ug/L 19.220 96 70-130ND
1,2-Dichloropropane ug/L 20.720 104 70-130ND
1,4-Dichlorobenzene ug/L 24.820 124 70-130ND
2-Butanone (MEK)ug/L 41.9J40 105 70-130ND
2-Hexanone ug/L 47.4J40 118 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 46.4J40 116 70-130ND
Acetone ug/L 46.0J40 115 70-130ND
Acrylonitrile ug/L 100J100 100 70-130ND
Benzene ug/L 22.520 113 70-148ND
Bromochloromethane ug/L 21.120 106 70-130ND
Bromodichloromethane ug/L 20.420 102 70-130ND
Bromoform ug/L 18.620 93 70-130ND
Bromomethane ug/L 6.0J M1203070-130ND
Carbon disulfide ug/L 18.0J20 90 70-130ND
Carbon tetrachloride ug/L 21.320 107 70-130ND
Chlorobenzene ug/L 22.920 113 70-1460.35J
Chloroethane ug/L 18.020 90 70-130ND
Chloroform ug/L 21.220 106 70-130ND
Chloromethane ug/L 20.320 101 70-130ND
cis-1,2-Dichloroethene ug/L 21.220 106 70-130ND
cis-1,3-Dichloropropene ug/L 18.120 91 70-130ND
Dibromochloromethane ug/L 19.320 96 70-130ND
Dibromomethane ug/L 23.820 119 70-130ND
Ethylbenzene ug/L 22.420 112 70-130ND
Iodomethane ug/L 22.8 M1405770-130ND
Methylene Chloride ug/L 18.420 92 70-130ND
Styrene ug/L 22.720 114 70-130ND
Tetrachloroethene ug/L 25.120 125 70-130ND
Toluene ug/L 22.320 111 70-155ND
trans-1,2-Dichloroethene ug/L 20.720 103 70-130ND
trans-1,3-Dichloropropene ug/L 17.520 88 70-130ND
trans-1,4-Dichloro-2-butene ug/L 14.7J20 74 70-130ND
Trichloroethene ug/L 21.620 108 69-151ND
Trichlorofluoromethane ug/L 22.120 111 70-130ND
Vinyl acetate ug/L 21.3J M1405370-130ND
Vinyl chloride ug/L 21.320 106 70-130ND
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277680003
1621076SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277680003
1621076SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 2.0J 7 302.1J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L 0.82J 301.0J
1,2-Dichloroethane ug/L 0.27J 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 5.0 3 305.2
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 1.5 9 301.6
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 1.6J 14 301.8J
Chloroethane ug/L 1.3J 16 301.6J
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 16.3 13 3014.2
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 7.1 11 307.9
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%97 294
REPORT OF LABORATORY ANALYSIS
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Page 47 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277680003
1621076SAMPLE DUPLICATE:
4-Bromofluorobenzene (S)%99 2101
Toluene-d8 (S)%96 295
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92278313001
1621077SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.34J 300.43J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 2.2J 6 302.4
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.97J 300.89J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 48 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92278313001
1621077SAMPLE DUPLICATE:
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 0.70J 300.70J
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%94 193
4-Bromofluorobenzene (S)%103 3101
Toluene-d8 (S)%97 097
REPORT OF LABORATORY ANALYSIS
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Page 49 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/41653
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92277680001, 92277680002, 92277680003, 92277680004, 92277680005, 92277680006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616619
Associated Lab Samples:92277680001, 92277680002, 92277680003, 92277680004, 92277680005, 92277680006
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 11/30/15 20:15100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616620LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 497J500 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616621MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277680001
1616622
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L H15009590-11095 0 10500ND473J473J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616623MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277687001
1616624
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M1500090-1100 10500NDNDND
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Analysis conducted outside the EPA method holding time.H1
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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Page 51 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92277680
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92277680001 MPRP/20148 ICP/18176MW-1 EPA 3010A EPA 6010
92277680002 MPRP/20148 ICP/18176MW-7 EPA 3010A EPA 6010
92277680003 MPRP/20148 ICP/18176MW-9 EPA 3010A EPA 6010
92277680004 MPRP/20148 ICP/18176MW-14 EPA 3010A EPA 6010
92277680005 MPRP/20148 ICP/18176MW-15 EPA 3010A EPA 6010
92277680006 MPRP/20148 ICP/18176MW-21 EPA 3010A EPA 6010
92277680007 MPRP/20148 ICP/18176MW-3R EPA 3010A EPA 6010
92277680008 MPRP/20148 ICP/18176MW-12S EPA 3010A EPA 6010
92277680009 MPRP/20158 ICP/18189MW-13 EPA 3010A EPA 6010
92277680010 MPRP/20148 ICP/18176MW-16 EPA 3010A EPA 6010
92277680011 MPRP/20158 ICP/18189MW-17 EPA 3010A EPA 6010
92277680012 MPRP/20158 ICP/18189MW-18 EPA 3010A EPA 6010
92277680013 MPRP/20158 ICP/18189MW-19 EPA 3010A EPA 6010
92277680014 MPRP/20158 ICP/18189MW-20 EPA 3010A EPA 6010
92277680015 MPRP/20158 ICP/18189MW-22 EPA 3010A EPA 6010
92277680016 MPRP/20158 ICP/18189MW-23 EPA 3010A EPA 6010
92277680001 MSV/34557MW-1 EPA 8260
92277680002 MSV/34557MW-7 EPA 8260
92277680003 MSV/34557MW-9 EPA 8260
92277680004 MSV/34557MW-14 EPA 8260
92277680005 MSV/34557MW-15 EPA 8260
92277680006 MSV/34557MW-21 EPA 8260
92277680007 MSV/34557MW-3R EPA 8260
92277680008 MSV/34557MW-12S EPA 8260
92277680009 MSV/34557MW-13 EPA 8260
92277680010 MSV/34557MW-16 EPA 8260
92277680011 MSV/34557MW-17 EPA 8260
92277680012 MSV/34557MW-18 EPA 8260
92277680013 MSV/34557MW-19 EPA 8260
92277680014 MSV/34557MW-20 EPA 8260
92277680015 MSV/34557MW-22 EPA 8260
92277680016 MSV/34557MW-23 EPA 8260
92277680001 WET/41653MW-1 SM 4500-S2D
92277680002 WET/41653MW-7 SM 4500-S2D
92277680003 WET/41653MW-9 SM 4500-S2D
92277680004 WET/41653MW-14 SM 4500-S2D
92277680005 WET/41653MW-15 SM 4500-S2D
92277680006 WET/41653MW-21 SM 4500-S2D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/19/2016 09:33 AM
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Page 52 of 55
Page 53 of 55
Page 54 of 55
Page 55 of 55
#=CL#
December 08, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92277674
92277674
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY MSWLF SWs
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on November 25, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 33
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Lab ID Sample ID Matrix Date Collected Date Received
92277674001 SW-1 Water 11/23/15 10:50 11/25/15 14:00
92277674002 SW-2 Water 11/22/15 17:30 11/25/15 14:00
92277674003 SW-3 Water 11/22/15 15:00 11/25/15 14:00
92277674004 SW-4 Water 11/22/15 16:00 11/25/15 14:00
92277674005 SWN-1 Water 11/23/15 11:45 11/25/15 14:00
92277674006 SWN-2 Water 11/23/15 12:10 11/25/15 14:00
92277674007 SW-A Water 11/23/15 11:05 11/25/15 14:00
92277674008 SW-B Water 11/23/15 11:30 11/25/15 14:00
REPORT OF LABORATORY ANALYSIS
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Page 3 of 33
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92277674001 SW-1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277674002 SW-2 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277674003 SW-3 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277674004 SW-4 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277674005 SWN-1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277674006 SWN-2 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277674007 SW-A EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92277674008 SW-B EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-1 Lab ID:92277674001 Collected:11/23/15 10:50 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 03:16 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 03:16 7440-38-212/01/15 19:0010.0 2.5 1
Barium 21.8J ug/L 12/05/15 03:16 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 03:16 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 03:16 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 03:16 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 03:16 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 03:16 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 03:16 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 03:16 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 03:16 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 03:16 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 18:22 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 03:16 7440-62-212/01/15 19:0025.0 2.5 1
Zinc 6.7J ug/L 12/05/15 03:16 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 04:56 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 04:56 107-13-12001.9 1
Benzene ND ug/L 12/01/15 04:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 04:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 04:56 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 04:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 04:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 04:56 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 04:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 04:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 04:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 04:56 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 04:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 04:56 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 04:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 04:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 04:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 04:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 04:56 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 04:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 04:56 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 04:56 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 04:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 04:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 04:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 04:56 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 04:56 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 04:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 04:56 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-1 Lab ID:92277674001 Collected:11/23/15 10:50 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 04:56 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 04:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 04:56 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 04:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 04:56 108-10-11000.33 1
Styrene ND ug/L 12/01/15 04:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 04:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 04:56 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 04:56 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 04:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 04:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 04:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 04:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 04:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 04:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 04:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 04:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 04:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %12/01/15 04:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %12/01/15 04:56 17060-07-070-130 1
Toluene-d8 (S)102 %12/01/15 04:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-2 Lab ID:92277674002 Collected:11/22/15 17:30 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 03:19 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 03:19 7440-38-212/01/15 19:0010.0 2.5 1
Barium 16.5J ug/L 12/05/15 03:19 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 03:19 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 03:19 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 03:19 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt 17.5 ug/L 12/05/15 03:19 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 03:19 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 03:19 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 03:19 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 03:19 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 03:19 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 18:25 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 03:19 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 03:19 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 05:13 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 05:13 107-13-12001.9 1
Benzene ND ug/L 12/01/15 05:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 05:13 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 05:13 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 05:13 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 05:13 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 05:13 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 05:13 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 05:13 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 05:13 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 05:13 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 05:13 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 05:13 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 05:13 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 05:13 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 05:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 05:13 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 05:13 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 05:13 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 05:13 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 05:13 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 05:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 05:13 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.58J ug/L 12/01/15 05:13 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 05:13 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 05:13 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 05:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 05:13 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-2 Lab ID:92277674002 Collected:11/22/15 17:30 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 05:13 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 05:13 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 05:13 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 05:13 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 05:13 108-10-11000.33 1
Styrene ND ug/L 12/01/15 05:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 05:13 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 05:13 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 05:13 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 05:13 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 05:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 05:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 05:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 05:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 05:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 05:13 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 05:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 05:13 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %12/01/15 05:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/01/15 05:13 17060-07-070-130 1
Toluene-d8 (S)100 %12/01/15 05:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-3 Lab ID:92277674003 Collected:11/22/15 15:00 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 03:22 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 03:22 7440-38-212/01/15 19:0010.0 2.5 1
Barium 15.8J ug/L 12/05/15 03:22 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 03:22 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 03:22 7440-43-912/01/15 19:001.0 0.50 1
Chromium 3.0J ug/L 12/05/15 03:22 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 03:22 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 03:22 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 03:22 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 03:22 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 03:22 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 03:22 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 18:37 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 03:22 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 03:22 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 05:30 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 05:30 107-13-12001.9 1
Benzene ND ug/L 12/01/15 05:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 05:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 05:30 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 05:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 05:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 05:30 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 05:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 05:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 05:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 05:30 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 05:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 05:30 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 05:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 05:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 05:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 05:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 05:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 05:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 05:30 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 05:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 05:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 05:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 05:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 05:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 05:30 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 05:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 05:30 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-3 Lab ID:92277674003 Collected:11/22/15 15:00 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 05:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 05:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 05:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 05:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 05:30 108-10-11000.33 1
Styrene ND ug/L 12/01/15 05:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 05:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 05:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 05:30 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 05:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 05:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 05:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 05:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 05:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 05:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 05:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 05:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 05:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %12/01/15 05:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %12/01/15 05:30 17060-07-070-130 1
Toluene-d8 (S)99 %12/01/15 05:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-4 Lab ID:92277674004 Collected:11/22/15 16:00 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 03:25 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 03:25 7440-38-212/01/15 19:0010.0 2.5 1
Barium 16.4J ug/L 12/05/15 03:25 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 03:25 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 03:25 7440-43-912/01/15 19:001.0 0.50 1
Chromium 7.7J ug/L 12/05/15 03:25 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 03:25 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 03:25 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 03:25 7439-92-112/01/15 19:0010.0 2.5 1
Nickel 3.8J ug/L 12/05/15 03:25 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 03:25 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 03:25 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 18:40 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 03:25 7440-62-212/01/15 19:0025.0 2.5 1
Zinc 12.8 ug/L 12/05/15 03:25 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 05:47 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 05:47 107-13-12001.9 1
Benzene ND ug/L 12/01/15 05:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 05:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 05:47 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 05:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 05:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 05:47 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 05:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 05:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 05:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 05:47 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 05:47 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 05:47 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 05:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 05:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 05:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 05:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 05:47 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 05:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 05:47 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 05:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 05:47 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 05:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 05:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 05:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 05:47 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 05:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 05:47 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-4 Lab ID:92277674004 Collected:11/22/15 16:00 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 05:47 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 05:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 05:47 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 05:47 75-09-2 C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 05:47 108-10-11000.33 1
Styrene ND ug/L 12/01/15 05:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 05:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 05:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 05:47 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 05:47 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 05:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 05:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 05:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 05:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 05:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 05:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 05:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 05:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %12/01/15 05:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %12/01/15 05:47 17060-07-070-130 1
Toluene-d8 (S)100 %12/01/15 05:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SWN-1 Lab ID:92277674005 Collected:11/23/15 11:45 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 03:37 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 03:37 7440-38-212/01/15 19:0010.0 2.5 1
Barium 20.5J ug/L 12/05/15 03:37 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 18:50 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 03:37 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 03:37 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 03:37 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 03:37 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 03:37 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 03:37 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 03:37 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 03:37 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 18:50 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 03:37 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 03:37 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 06:05 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 06:05 107-13-12001.9 1
Benzene ND ug/L 12/01/15 06:05 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 06:05 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 06:05 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 06:05 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 06:05 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 06:05 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 06:05 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 06:05 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 06:05 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 06:05 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 06:05 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 06:05 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 06:05 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 06:05 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 06:05 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 06:05 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 06:05 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 06:05 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 06:05 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 06:05 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 06:05 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 06:05 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 06:05 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 06:05 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 06:05 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 06:05 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 06:05 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SWN-1 Lab ID:92277674005 Collected:11/23/15 11:45 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 06:05 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 06:05 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 06:05 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 06:05 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 06:05 108-10-11000.33 1
Styrene ND ug/L 12/01/15 06:05 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 06:05 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 06:05 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 06:05 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 06:05 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 06:05 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 06:05 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 06:05 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 06:05 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 06:05 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 06:05 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 06:05 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 06:05 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %12/01/15 06:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/01/15 06:05 17060-07-070-130 1
Toluene-d8 (S)101 %12/01/15 06:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SWN-2 Lab ID:92277674006 Collected:11/23/15 12:10 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 03:55 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 03:55 7440-38-212/01/15 19:0010.0 2.5 1
Barium 19.7J ug/L 12/05/15 03:55 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 18:58 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 03:55 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 03:55 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 03:55 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 03:55 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 03:55 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 03:55 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 03:55 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 03:55 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 18:58 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 03:55 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 03:55 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 06:22 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 06:22 107-13-12001.9 1
Benzene ND ug/L 12/01/15 06:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 06:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 06:22 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 06:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 06:22 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 06:22 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 06:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 06:22 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 06:22 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 06:22 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 06:22 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 06:22 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 06:22 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 06:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 06:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 06:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 06:22 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 06:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 06:22 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 06:22 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 06:22 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 06:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 06:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 06:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 06:22 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 06:22 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 06:22 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SWN-2 Lab ID:92277674006 Collected:11/23/15 12:10 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 06:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 06:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 06:22 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 06:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 06:22 108-10-11000.33 1
Styrene ND ug/L 12/01/15 06:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 06:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 06:22 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 06:22 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 06:22 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 06:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 06:22 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 06:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 06:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 06:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 06:22 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 06:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 06:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %12/01/15 06:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %12/01/15 06:22 17060-07-070-130 1
Toluene-d8 (S)100 %12/01/15 06:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-A Lab ID:92277674007 Collected:11/23/15 11:05 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 03:59 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 03:59 7440-38-212/01/15 19:0010.0 2.5 1
Barium 21.5J ug/L 12/05/15 03:59 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 19:02 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 03:59 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 03:59 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 03:59 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 03:59 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 03:59 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 03:59 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 03:59 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 03:59 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 19:02 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 03:59 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 03:59 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 06:39 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 06:39 107-13-12001.9 1
Benzene ND ug/L 12/01/15 06:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 06:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 06:39 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 06:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 06:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 06:39 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 06:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 06:39 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 06:39 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 06:39 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 06:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 06:39 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 06:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 06:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 06:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 06:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 06:39 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 06:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 06:39 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 06:39 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 06:39 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 06:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 06:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 06:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 06:39 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 06:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 06:39 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-A Lab ID:92277674007 Collected:11/23/15 11:05 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 06:39 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 06:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 06:39 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 06:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 06:39 108-10-11000.33 1
Styrene ND ug/L 12/01/15 06:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 06:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 06:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 06:39 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 06:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 06:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 06:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 06:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 06:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 06:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 06:39 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 06:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 06:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %12/01/15 06:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %12/01/15 06:39 17060-07-070-130 1
Toluene-d8 (S)101 %12/01/15 06:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-B Lab ID:92277674008 Collected:11/23/15 11:30 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 04:02 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 04:02 7440-38-212/01/15 19:0010.0 2.5 1
Barium 21.7J ug/L 12/05/15 04:02 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/07/15 19:05 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 04:02 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 04:02 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 04:02 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 04:02 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 04:02 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 04:02 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 04:02 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 04:02 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 19:05 7440-28-012/01/15 19:005.5 5.0 1
Vanadium ND ug/L 12/05/15 04:02 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 04:02 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 06:56 67-64-110010.0 1
Acrylonitrile ND ug/L 12/01/15 06:56 107-13-12001.9 1
Benzene ND ug/L 12/01/15 06:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 06:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 06:56 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 06:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 06:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 06:56 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 06:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 06:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 06:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 06:56 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 06:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 06:56 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 06:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 06:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 06:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 06:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 06:56 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/01/15 06:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 06:56 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/01/15 06:56 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 06:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 06:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 06:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 06:56 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 06:56 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 06:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 06:56 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
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Page 19 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Sample:SW-B Lab ID:92277674008 Collected:11/23/15 11:30 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/01/15 06:56 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/01/15 06:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 06:56 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/01/15 06:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 06:56 108-10-11000.33 1
Styrene ND ug/L 12/01/15 06:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 06:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 06:56 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 06:56 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 06:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/01/15 06:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 06:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 06:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 06:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 06:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 06:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 06:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 06:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %12/01/15 06:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/01/15 06:56 17060-07-070-130 1
Toluene-d8 (S)100 %12/01/15 06:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
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Page 20 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20147
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92277674001, 92277674002, 92277674003, 92277674004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617580
Associated Lab Samples:92277674001, 92277674002, 92277674003, 92277674004
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/05/15 01:553.8
Arsenic ug/L ND 10.0 12/05/15 01:552.5
Barium ug/L ND 100 12/05/15 01:552.5
Beryllium ug/L ND 1.0 12/05/15 01:550.50
Cadmium ug/L ND 1.0 12/05/15 01:550.50
Chromium ug/L ND 10.0 12/05/15 01:552.5
Cobalt ug/L ND 10.0 12/05/15 01:552.5
Copper ug/L ND 10.0 12/05/15 01:552.5
Lead ug/L ND 10.0 12/05/15 01:552.5
Nickel ug/L ND 50.0 12/05/15 01:552.5
Selenium ug/L ND 10.0 12/05/15 01:555.0
Silver ug/L ND 10.0 12/05/15 01:552.5
Thallium ug/L ND 5.5 12/05/15 01:555.0
Vanadium ug/L ND 25.0 12/05/15 01:552.5
Zinc ug/L ND 10.0 12/05/15 01:555.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617581LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 454500 91 80-120
Arsenic ug/L 430500 86 80-120
Barium ug/L 502500 100 80-120
Beryllium ug/L 513500 103 80-120
Cadmium ug/L 466500 93 80-120
Chromium ug/L 494500 99 80-120
Cobalt ug/L 454500 91 80-120
Copper ug/L 479500 96 80-120
Lead ug/L 452500 90 80-120
Nickel ug/L 469500 94 80-120
Selenium ug/L 437500 87 80-120
Silver ug/L 236250 95 80-120
Thallium ug/L 454500 91 80-120
Vanadium ug/L 476500 95 80-120
Zinc ug/L 444500 89 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
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Huntersville, NC 28078
[phone]
Page 21 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1617582MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277330004
1617583
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 87 75-12583 5 25500ND437417
Arsenic ug/L 500 83 75-12579 6 25500ND418395
Barium ug/L 500 97 75-12591 6 2550019.2 503 476
Beryllium ug/L 500 99 75-12594 6 25500ND497468
Cadmium ug/L 500 90 75-12585 5 25500ND448426
Chromium ug/L 500 95 75-12590 6 25500ND475449
Cobalt ug/L 500 87 75-12583 5 25500ND436416
Copper ug/L 500 94 75-12588 6 25500ND468441
Lead ug/L 500 86 75-12582 5 25500ND433411
Nickel ug/L 500 90 75-12585 5 25500ND449427
Selenium ug/L 500 84 75-12580 4 25500ND418401
Silver ug/L 250 91 75-12586 5 25250ND228216
Thallium ug/L 500 87 75-12584 3 255005.2J 438 424
Vanadium ug/L 500 92 75-12587 5 25500ND460436
Zinc ug/L 500 85 75-12581 5 255007.9J 432 411
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20148
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92277674005, 92277674006, 92277674007, 92277674008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617591
Associated Lab Samples:92277674005, 92277674006, 92277674007, 92277674008
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/05/15 03:313.8
Arsenic ug/L ND 10.0 12/05/15 03:312.5
Barium ug/L ND 100 12/05/15 03:312.5
Beryllium ug/L ND 1.0 12/07/15 18:440.50
Cadmium ug/L ND 1.0 12/05/15 03:310.50
Chromium ug/L ND 10.0 12/05/15 03:312.5
Cobalt ug/L ND 10.0 12/05/15 03:312.5
Copper ug/L ND 10.0 12/05/15 03:312.5
Lead ug/L ND 10.0 12/05/15 03:312.5
Nickel ug/L ND 50.0 12/05/15 03:312.5
Selenium ug/L ND 10.0 12/05/15 03:315.0
Silver ug/L ND 10.0 12/05/15 03:312.5
Thallium ug/L ND 5.5 12/07/15 18:445.0
Vanadium ug/L ND 25.0 12/05/15 03:312.5
Zinc ug/L ND 10.0 12/05/15 03:315.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617592LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 433500 87 80-120
Arsenic ug/L 412500 82 80-120
Barium ug/L 415500 83 80-120
Beryllium ug/L 409500 82 80-120
Cadmium ug/L 421500 84 80-120
Chromium ug/L 415500 83 80-120
Cobalt ug/L 422500 84 80-120
Copper ug/L 426500 85 80-120
Lead ug/L 418500 84 80-120
Nickel ug/L 422500 84 80-120
Selenium ug/L 417500 83 80-120
Silver ug/L 209250 84 80-120
Thallium ug/L 411500 82 80-120
Vanadium ug/L 416500 83 80-120
Zinc ug/L 415500 83 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1617593MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277674005
1617594
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 91 75-12585 7 25500ND456424
Arsenic ug/L 500 87 75-12581 7 25500ND436405
Barium ug/L 500 99 75-12593 6 2550020.5J 515 485
Beryllium ug/L 500 95 75-12590 5 25500ND473449
Cadmium ug/L 500 93 75-12587 7 25500ND465433
Chromium ug/L 500 98 75-12592 6 25500ND488459
Cobalt ug/L 500 91 75-12584 7 25500ND453421
Copper ug/L 500 96 75-12590 6 25500ND480451
Lead ug/L 500 90 75-12584 7 25500ND448419
Nickel ug/L 500 93 75-12587 7 25500ND466435
Selenium ug/L 500 88 75-12582 8 25500ND440408
Silver ug/L 250 95 75-12589 7 25250ND237222
Thallium ug/L 500 95 75-12591 4 25500ND480461
Vanadium ug/L 500 95 75-12589 7 25500ND477445
Zinc ug/L 500 89 75-12583 7 25500ND444415
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34482
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92277674001, 92277674002, 92277674003, 92277674004, 92277674005, 92277674006, 92277674007,
92277674008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616469
Associated Lab Samples:92277674001, 92277674002, 92277674003, 92277674004, 92277674005, 92277674006, 92277674007,
92277674008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/01/15 03:130.33
1,1,1-Trichloroethane ug/L ND 1.0 12/01/15 03:130.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/01/15 03:130.40
1,1,2-Trichloroethane ug/L ND 1.0 12/01/15 03:130.29
1,1-Dichloroethane ug/L ND 5.0 12/01/15 03:130.32
1,1-Dichloroethene ug/L ND 5.0 12/01/15 03:130.56
1,2,3-Trichloropropane ug/L ND 1.0 12/01/15 03:130.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/01/15 03:132.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/01/15 03:130.27
1,2-Dichlorobenzene ug/L ND 5.0 12/01/15 03:130.30
1,2-Dichloroethane ug/L ND 1.0 12/01/15 03:130.24
1,2-Dichloropropane ug/L ND 1.0 12/01/15 03:130.27
1,4-Dichlorobenzene ug/L ND 1.0 12/01/15 03:130.33
2-Butanone (MEK)ug/L ND 100 12/01/15 03:130.96
2-Hexanone ug/L ND 50.0 12/01/15 03:130.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/01/15 03:130.33
Acetone ug/L ND 100 12/01/15 03:1310.0
Acrylonitrile ug/L ND 200 12/01/15 03:131.9
Benzene ug/L ND 1.0 12/01/15 03:130.25
Bromochloromethane ug/L ND 3.0 12/01/15 03:130.17
Bromodichloromethane ug/L ND 1.0 12/01/15 03:130.18
Bromoform ug/L ND 3.0 12/01/15 03:130.26
Bromomethane ug/L ND 10.0 12/01/15 03:130.29
Carbon disulfide ug/L ND 100 12/01/15 03:131.2
Carbon tetrachloride ug/L ND 1.0 12/01/15 03:130.25
Chlorobenzene ug/L ND 3.0 12/01/15 03:130.23
Chloroethane ug/L ND 10.0 12/01/15 03:130.54
Chloroform ug/L ND 5.0 12/01/15 03:130.14
Chloromethane ug/L ND 1.0 12/01/15 03:130.11
cis-1,2-Dichloroethene ug/L ND 5.0 12/01/15 03:130.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/01/15 03:130.13
Dibromochloromethane ug/L ND 3.0 12/01/15 03:130.21
Dibromomethane ug/L ND 10.0 12/01/15 03:130.21
Ethylbenzene ug/L ND 1.0 12/01/15 03:130.30
Iodomethane ug/L ND 10.0 12/01/15 03:130.32
Methylene Chloride ug/L ND 1.0 12/01/15 03:130.97
Styrene ug/L ND 1.0 12/01/15 03:130.26
Tetrachloroethene ug/L ND 1.0 12/01/15 03:130.46
Toluene ug/L ND 1.0 12/01/15 03:130.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/01/15 03:130.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616469
Associated Lab Samples:92277674001, 92277674002, 92277674003, 92277674004, 92277674005, 92277674006, 92277674007,
92277674008
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 12/01/15 03:130.26
trans-1,4-Dichloro-2-butene ug/L ND 100 12/01/15 03:131.0
Trichloroethene ug/L ND 1.0 12/01/15 03:130.47
Trichlorofluoromethane ug/L ND 1.0 12/01/15 03:130.20
Vinyl acetate ug/L ND 50.0 12/01/15 03:130.35
Vinyl chloride ug/L ND 1.0 12/01/15 03:130.62
Xylene (Total)ug/L ND 5.0 12/01/15 03:130.66
1,2-Dichloroethane-d4 (S)%97 70-130 12/01/15 03:13
4-Bromofluorobenzene (S)%103 70-130 12/01/15 03:13
Toluene-d8 (S)%100 70-130 12/01/15 03:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616470LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.050 88 80-125
1,1,1-Trichloroethane ug/L 47.550 95 71-129
1,1,2,2-Tetrachloroethane ug/L 41.950 84 79-124
1,1,2-Trichloroethane ug/L 46.050 92 85-125
1,1-Dichloroethane ug/L 49.050 98 73-126
1,1-Dichloroethene ug/L 51.650 103 66-135
1,2,3-Trichloropropane ug/L 44.150 88 75-130
1,2-Dibromo-3-chloropropane ug/L 39.550 79 71-133
1,2-Dibromoethane (EDB)ug/L 45.150 90 83-124
1,2-Dichlorobenzene ug/L 47.050 94 80-133
1,2-Dichloroethane ug/L 45.650 91 67-128
1,2-Dichloropropane ug/L 46.150 92 75-132
1,4-Dichlorobenzene ug/L 46.950 94 78-130
2-Butanone (MEK)ug/L 95.3J100 95 61-144
2-Hexanone ug/L 82.2100 82 68-143
4-Methyl-2-pentanone (MIBK)ug/L 93.9J100 94 72-135
Acetone ug/L 92.9J100 93 48-146
Acrylonitrile ug/L 239250 95 40-160
Benzene ug/L 48.850 98 80-125
Bromochloromethane ug/L 52.650 105 71-125
Bromodichloromethane ug/L 44.750 89 78-124
Bromoform ug/L 39.350 79 71-128
Bromomethane ug/L 46.150 92 40-160
Carbon disulfide ug/L 48.4J50 97 50-160
Carbon tetrachloride ug/L 48.750 97 69-131
Chlorobenzene ug/L 43.850 88 81-122
Chloroethane ug/L 50.250 100 39-148
Chloroform ug/L 49.050 98 73-127
Chloromethane ug/L 47.850 96 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 26 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616470LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 50.950 102 74-124
cis-1,3-Dichloropropene ug/L 44.550 89 72-132
Dibromochloromethane ug/L 41.450 83 78-125
Dibromomethane ug/L 50.250 100 82-120
Ethylbenzene ug/L 44.550 89 79-121
Iodomethane ug/L 94.2100 94 39-154
Methylene Chloride ug/L 51.050 102 64-133
Styrene ug/L 45.950 92 84-126
Tetrachloroethene ug/L 46.350 93 78-122
Toluene ug/L 47.450 95 80-121
trans-1,2-Dichloroethene ug/L 50.850 102 71-127
trans-1,3-Dichloropropene ug/L 44.650 89 69-141
trans-1,4-Dichloro-2-butene ug/L 34.0J50 68 40-160
Trichloroethene ug/L 46.550 93 78-122
Trichlorofluoromethane ug/L 54.150 108 53-137
Vinyl acetate ug/L 95.3100 95 40-160
Vinyl chloride ug/L 55.550 111 58-137
Xylene (Total)ug/L 132150 88 81-126
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1616471MATRIX SPIKE SAMPLE:
MSSpike
Result
92277673001
1,1,1,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,1-Trichloroethane ug/L 22.120 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.520 92 70-130ND
1,1,2-Trichloroethane ug/L 21.020 105 70-130ND
1,1-Dichloroethane ug/L 22.620 113 70-130ND
1,1-Dichloroethene ug/L 24.720 123 70-166ND
1,2,3-Trichloropropane ug/L 19.220 96 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.820 84 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.820 104 70-130ND
1,2-Dichlorobenzene ug/L 21.120 105 70-130ND
1,2-Dichloroethane ug/L 20.620 103 70-130ND
1,2-Dichloropropane ug/L 20.920 105 70-130ND
1,4-Dichlorobenzene ug/L 20.820 103 70-130ND
2-Butanone (MEK)ug/L 41.8J40 105 70-130ND
2-Hexanone ug/L 36.1J40 90 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 41.1J40 103 70-130ND
Acetone ug/L 44.0J40 104 70-130ND
Acrylonitrile ug/L 106J100 106 70-130ND
Benzene ug/L 23.220 114 70-1480.35J
Bromochloromethane ug/L 25.020 125 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
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[phone]
Page 27 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1616471MATRIX SPIKE SAMPLE:
MSSpike
Result
92277673001
Bromodichloromethane ug/L 19.220 96 70-130ND
Bromoform ug/L 16.520 83 70-130ND
Bromomethane ug/L 21.920 109 70-130ND
Carbon disulfide ug/L 22.6J20 113 70-130ND
Carbon tetrachloride ug/L 22.720 114 70-130ND
Chlorobenzene ug/L 20.920 104 70-146ND
Chloroethane ug/L 23.820 119 70-130ND
Chloroform ug/L 22.920 114 70-130ND
Chloromethane ug/L 23.520 117 70-130ND
cis-1,2-Dichloroethene ug/L 24.120 120 70-130ND
cis-1,3-Dichloropropene ug/L 19.620 98 70-130ND
Dibromochloromethane ug/L 18.620 93 70-130ND
Dibromomethane ug/L 22.720 113 70-130ND
Ethylbenzene ug/L 20.520 102 70-130ND
Iodomethane ug/L 37.440 93 70-130ND
Methylene Chloride ug/L 23.620 118 70-130ND
Styrene ug/L 20.220 101 70-130ND
Tetrachloroethene ug/L 21.620 108 70-130ND
Toluene ug/L 21.620 108 70-155ND
trans-1,2-Dichloroethene ug/L 24.220 121 70-130ND
trans-1,3-Dichloropropene ug/L 19.520 97 70-130ND
trans-1,4-Dichloro-2-butene ug/L 13.0J M1206570-130ND
Trichloroethene ug/L 20.720 104 69-151ND
Trichlorofluoromethane ug/L 25.720 129 70-130ND
Vinyl acetate ug/L 35.1J40 88 70-130ND
Vinyl chloride ug/L 27.3 M12013770-130ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277673002
1616472SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.94J 300.85J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L 0.47J 300.47J
1,2-Dichloropropane ug/L 1.9 7 302.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
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Huntersville, NC 28078
[phone]
Page 28 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277673002
1616472SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L 4.4 5 304.6
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.88J 300.88J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 1.3J 7 301.3J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 2.6J 5 302.5J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%99 297
4-Bromofluorobenzene (S)%105 0104
Toluene-d8 (S)%99 198
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
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[phone]
Page 29 of 33
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:41 PM
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[phone]
Page 30 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92277674
SURRY MSWLF SWs
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92277674001 MPRP/20147 ICP/18175SW-1 EPA 3010 EPA 6010
92277674002 MPRP/20147 ICP/18175SW-2 EPA 3010 EPA 6010
92277674003 MPRP/20147 ICP/18175SW-3 EPA 3010 EPA 6010
92277674004 MPRP/20147 ICP/18175SW-4 EPA 3010 EPA 6010
92277674005 MPRP/20148 ICP/18176SWN-1 EPA 3010 EPA 6010
92277674006 MPRP/20148 ICP/18176SWN-2 EPA 3010 EPA 6010
92277674007 MPRP/20148 ICP/18176SW-A EPA 3010 EPA 6010
92277674008 MPRP/20148 ICP/18176SW-B EPA 3010 EPA 6010
92277674001 MSV/34482SW-1 EPA 8260
92277674002 MSV/34482SW-2 EPA 8260
92277674003 MSV/34482SW-3 EPA 8260
92277674004 MSV/34482SW-4 EPA 8260
92277674005 MSV/34482SWN-1 EPA 8260
92277674006 MSV/34482SWN-2 EPA 8260
92277674007 MSV/34482SW-A EPA 8260
92277674008 MSV/34482SW-B EPA 8260
REPORT OF LABORATORY ANALYSIS
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Page 31 of 33
Page 32 of 33
Page 33 of 33
#=CL#
December 03, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92277681
92277681
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Surry Closed-Mt.Airy (Bromide)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on November 25, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 12
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92277681
Surry Closed-Mt.Airy (Bromide)
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174Alabama Certification #: 41320
Connecticut Certification #: PH-0216Delaware Certification: FL NELAC ReciprocityFlorida Certification #: E83079
Georgia Certification #: 955Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC ReciprocityIllinois Certification #: 200068Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC ReciprocityLouisiana Environmental Certificate #: 05007Maryland Certification: #346
Michigan Certification #: 9911Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958New York Certification #: 11608North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710North Dakota Certification #: R-216
Oklahoma Certification #: D9947Pennsylvania Certification #: 68-00547Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001Tennessee Certification #: TN02974
Texas Certification: FL NELAC ReciprocityUS Virgin Islands Certification: FL NELAC ReciprocityVirginia Environmental Certification #: 460165
West Virginia Certification #: 9962CWisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 2 of 12
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92277681
Surry Closed-Mt.Airy (Bromide)
Lab ID Sample ID Matrix Date Collected Date Received
92277681001 MW-1 Water 11/22/15 15:10 11/25/15 14:00
92277681002 MW-13 Water 11/22/15 11:15 11/25/15 14:00
92277681003 MW-16 Water 11/22/15 15:50 11/25/15 14:00
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 3 of 12
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92277681
Surry Closed-Mt.Airy (Bromide)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92277681001 MW-1 EPA 300.0 1 PASI-OKEK
92277681002 MW-13 EPA 300.0 1 PASI-OKEK
92277681003 MW-16 EPA 300.0 1 PASI-OKEK
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 4 of 12
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277681
Surry Closed-Mt.Airy (Bromide)
Sample:MW-1 Lab ID:92277681001 Collected:11/22/15 15:10 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Bromide ND mg/L 12/02/15 21:12 24959-67-90.10 0.069 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/03/2015 06:08 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 5 of 12
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277681
Surry Closed-Mt.Airy (Bromide)
Sample:MW-13 Lab ID:92277681002 Collected:11/22/15 11:15 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Bromide 0.25 mg/L 12/02/15 21:34 24959-67-90.10 0.069 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/03/2015 06:08 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 6 of 12
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277681
Surry Closed-Mt.Airy (Bromide)
Sample:MW-16 Lab ID:92277681003 Collected:11/22/15 15:50 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Bromide 0.22 mg/L 12/02/15 21:56 24959-67-90.10 0.069 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2015 06:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 12
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277681
Surry Closed-Mt.Airy (Bromide)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/52645
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92277681001, 92277681002, 92277681003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1407723
Associated Lab Samples:
Matrix:Water
AnalyzedMDL
Bromide mg/L ND 0.10 12/02/15 20:280.069
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1407724LABORATORY CONTROL SAMPLE:
LCSSpike
Bromide mg/L 1010 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1407727MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35218806001
1407728
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromide mg/L 10 95 90-11094 0 20100.19 9.6 9.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/03/2015 06:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 12
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92277681
Surry Closed-Mt.Airy (Bromide)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - Ormond BeachPASI-O
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/03/2015 06:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 12
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92277681
Surry Closed-Mt.Airy (Bromide)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92277681001 WETA/52645MW-1 EPA 300.0
92277681002 WETA/52645MW-13 EPA 300.0
92277681003 WETA/52645MW-16 EPA 300.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/03/2015 06:08 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 12
Page 11 of 12
Page 12 of 12
#=CL#
December 08, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92277672
92277672
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY BLANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on November 25, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92277672
SURRY BLANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Huntersville, NC 28078
[phone]
Page 2 of 24
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92277672
SURRY BLANKS
Lab ID Sample ID Matrix Date Collected Date Received
92277672001 EB Water 11/24/15 14:00 11/25/15 14:00
92277672002 FB Water 11/24/15 14:15 11/25/15 14:00
92277672003 TB Water 11/24/15 00:00 11/25/15 14:00
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 3 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92277672
SURRY BLANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92277672001 EB EPA 6010 16 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 67 PASI-CNB
92277672002 FB EPA 6010 16 PASI-ACDF
EPA 7470 1 PASI-ASH1
EPA 8260 67 PASI-CNB
92277672003 TB EPA 8260 67 PASI-CNB
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 4 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277672
SURRY BLANKS
Sample:EB Lab ID:92277672001 Collected:11/24/15 14:00 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 02:47 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 02:47 7440-38-212/01/15 19:0010.0 2.5 1
Barium ND ug/L 12/05/15 02:47 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 02:47 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 02:47 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 02:47 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 02:47 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 02:47 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 02:47 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 02:47 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 02:47 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 02:47 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/05/15 02:47 7440-28-012/01/15 19:005.5 5.0 1
Tin ND ug/L 12/05/15 02:47 7440-31-512/01/15 19:001002.5 1
Vanadium ND ug/L 12/05/15 02:47 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 02:47 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/07/15 15:46 7439-97-612/04/15 16:300.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 07:13 67-64-110010.0 1
Acetonitrile ND ug/L 12/01/15 07:13 75-05-855.0 2.2 1
Acrolein ND ug/L 12/01/15 07:13 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 12/01/15 07:13 107-13-12001.9 1
Allyl chloride ND ug/L 12/01/15 07:13 107-05-110.0 1.5 1
Benzene ND ug/L 12/01/15 07:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 07:13 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 07:13 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 07:13 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 07:13 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 07:13 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 07:13 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 07:13 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 07:13 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 07:13 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 07:13 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 07:13 74-87-31.0 0.11 1
Chloroprene ND ug/L 12/01/15 07:13 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 07:13 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 07:13 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 07:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 07:13 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 07:13 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 12/01/15 07:13 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 12/01/15 07:13 106-46-71.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277672
SURRY BLANKS
Sample:EB Lab ID:92277672001 Collected:11/24/15 14:00 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 07:13 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 12/01/15 07:13 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 12/01/15 07:13 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 07:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 07:13 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 07:13 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 07:13 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 07:13 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 12/01/15 07:13 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 12/01/15 07:13 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 12/01/15 07:13 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 07:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 07:13 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 12/01/15 07:13 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 12/01/15 07:13 97-63-2 L210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 12/01/15 07:13 87-68-310.0 0.71 1
2-Hexanone ND ug/L 12/01/15 07:13 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 07:13 74-88-410.0 0.32 1
Isobutanol ND ug/L 12/01/15 07:13 78-83-110035.0 1
Methacrylonitrile ND ug/L 12/01/15 07:13 126-98-71000.93 1
Methylene Chloride 1.1 ug/L 12/01/15 07:13 75-09-2 C91.0 0.97 1
Methyl methacrylate ND ug/L 12/01/15 07:13 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 07:13 108-10-11000.33 1
Naphthalene ND ug/L 12/01/15 07:13 91-20-310.0 0.24 1
Propionitrile ND ug/L 12/01/15 07:13 107-12-01503.6 1
Styrene ND ug/L 12/01/15 07:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 07:13 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 07:13 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 07:13 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 07:13 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 12/01/15 07:13 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 12/01/15 07:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 07:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 07:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 07:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 07:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 07:13 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 07:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 07:13 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %12/01/15 07:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %12/01/15 07:13 17060-07-070-130 1
Toluene-d8 (S)101 %12/01/15 07:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277672
SURRY BLANKS
Sample:FB Lab ID:92277672002 Collected:11/24/15 14:15 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 12/05/15 02:54 7440-36-012/01/15 19:006.0 3.8 1
Arsenic ND ug/L 12/05/15 02:54 7440-38-212/01/15 19:0010.0 2.5 1
Barium ND ug/L 12/05/15 02:54 7440-39-312/01/15 19:001002.5 1
Beryllium ND ug/L 12/05/15 02:54 7440-41-712/01/15 19:001.0 0.50 1
Cadmium ND ug/L 12/05/15 02:54 7440-43-912/01/15 19:001.0 0.50 1
Chromium ND ug/L 12/05/15 02:54 7440-47-312/01/15 19:0010.0 2.5 1
Cobalt ND ug/L 12/05/15 02:54 7440-48-412/01/15 19:0010.0 2.5 1
Copper ND ug/L 12/05/15 02:54 7440-50-812/01/15 19:0010.0 2.5 1
Lead ND ug/L 12/05/15 02:54 7439-92-112/01/15 19:0010.0 2.5 1
Nickel ND ug/L 12/05/15 02:54 7440-02-012/01/15 19:0050.0 2.5 1
Selenium ND ug/L 12/05/15 02:54 7782-49-212/01/15 19:0010.0 5.0 1
Silver ND ug/L 12/05/15 02:54 7440-22-412/01/15 19:0010.0 2.5 1
Thallium ND ug/L 12/07/15 18:09 7440-28-012/01/15 19:005.5 5.0 1
Tin ND ug/L 12/05/15 02:54 7440-31-512/01/15 19:001002.5 1
Vanadium ND ug/L 12/05/15 02:54 7440-62-212/01/15 19:0025.0 2.5 1
Zinc ND ug/L 12/05/15 02:54 7440-66-612/01/15 19:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 12/07/15 15:48 7439-97-612/04/15 16:300.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 07:30 67-64-110010.0 1
Acetonitrile ND ug/L 12/01/15 07:30 75-05-855.0 2.2 1
Acrolein ND ug/L 12/01/15 07:30 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 12/01/15 07:30 107-13-12001.9 1
Allyl chloride ND ug/L 12/01/15 07:30 107-05-110.0 1.5 1
Benzene ND ug/L 12/01/15 07:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 07:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 07:30 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 07:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 07:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 07:30 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 07:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 07:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 07:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 07:30 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 07:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 07:30 74-87-31.0 0.11 1
Chloroprene ND ug/L 12/01/15 07:30 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 07:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 07:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 07:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 07:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 07:30 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 12/01/15 07:30 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 12/01/15 07:30 106-46-71.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277672
SURRY BLANKS
Sample:FB Lab ID:92277672002 Collected:11/24/15 14:15 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 07:30 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 12/01/15 07:30 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 12/01/15 07:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 07:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 07:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 07:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 07:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 07:30 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 12/01/15 07:30 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 12/01/15 07:30 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 12/01/15 07:30 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 07:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 07:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 12/01/15 07:30 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 12/01/15 07:30 97-63-2 L210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 12/01/15 07:30 87-68-310.0 0.71 1
2-Hexanone ND ug/L 12/01/15 07:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 07:30 74-88-410.0 0.32 1
Isobutanol ND ug/L 12/01/15 07:30 78-83-110035.0 1
Methacrylonitrile ND ug/L 12/01/15 07:30 126-98-71000.93 1
Methylene Chloride 0.99J ug/L 12/01/15 07:30 75-09-2 C91.0 0.97 1
Methyl methacrylate ND ug/L 12/01/15 07:30 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 07:30 108-10-11000.33 1
Naphthalene ND ug/L 12/01/15 07:30 91-20-310.0 0.24 1
Propionitrile ND ug/L 12/01/15 07:30 107-12-01503.6 1
Styrene ND ug/L 12/01/15 07:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 07:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 07:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 07:30 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 07:30 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 12/01/15 07:30 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 12/01/15 07:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 07:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 07:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 07:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 07:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 07:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 07:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 07:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %12/01/15 07:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/01/15 07:30 17060-07-070-130 1
Toluene-d8 (S)101 %12/01/15 07:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277672
SURRY BLANKS
Sample:TB Lab ID:92277672003 Collected:11/24/15 00:00 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/01/15 07:47 67-64-110010.0 1
Acetonitrile ND ug/L 12/01/15 07:47 75-05-855.0 2.2 1
Acrolein ND ug/L 12/01/15 07:47 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 12/01/15 07:47 107-13-12001.9 1
Allyl chloride ND ug/L 12/01/15 07:47 107-05-110.0 1.5 1
Benzene ND ug/L 12/01/15 07:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/01/15 07:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/01/15 07:47 75-27-41.0 0.18 1
Bromoform ND ug/L 12/01/15 07:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/01/15 07:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/01/15 07:47 78-93-31000.96 1
Carbon disulfide ND ug/L 12/01/15 07:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/01/15 07:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/01/15 07:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/01/15 07:47 75-00-310.0 0.54 1
Chloroform ND ug/L 12/01/15 07:47 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/01/15 07:47 74-87-31.0 0.11 1
Chloroprene ND ug/L 12/01/15 07:47 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 12/01/15 07:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/01/15 07:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/01/15 07:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/01/15 07:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/01/15 07:47 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 12/01/15 07:47 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 12/01/15 07:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/01/15 07:47 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 12/01/15 07:47 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 12/01/15 07:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/01/15 07:47 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/01/15 07:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/01/15 07:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/01/15 07:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/01/15 07:47 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 12/01/15 07:47 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 12/01/15 07:47 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 12/01/15 07:47 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 12/01/15 07:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/01/15 07:47 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 12/01/15 07:47 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 12/01/15 07:47 97-63-2 L210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 12/01/15 07:47 87-68-310.0 0.71 1
2-Hexanone ND ug/L 12/01/15 07:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/01/15 07:47 74-88-410.0 0.32 1
Isobutanol ND ug/L 12/01/15 07:47 78-83-110035.0 1
Methacrylonitrile ND ug/L 12/01/15 07:47 126-98-71000.93 1
Methylene Chloride ND ug/L 12/01/15 07:47 75-09-2 C91.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277672
SURRY BLANKS
Sample:TB Lab ID:92277672003 Collected:11/24/15 00:00 Received:11/25/15 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 12/01/15 07:47 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/01/15 07:47 108-10-11000.33 1
Naphthalene ND ug/L 12/01/15 07:47 91-20-310.0 0.24 1
Propionitrile ND ug/L 12/01/15 07:47 107-12-01503.6 1
Styrene ND ug/L 12/01/15 07:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/01/15 07:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/01/15 07:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/01/15 07:47 127-18-41.0 0.46 1
Toluene ND ug/L 12/01/15 07:47 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 12/01/15 07:47 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 12/01/15 07:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/01/15 07:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/01/15 07:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/01/15 07:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/01/15 07:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/01/15 07:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/01/15 07:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/01/15 07:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %12/01/15 07:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/01/15 07:47 17060-07-070-130 1
Toluene-d8 (S)99 %12/01/15 07:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
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Page 10 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277672
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/8724
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92277672001, 92277672002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1619751
Associated Lab Samples:92277672001, 92277672002
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 12/07/15 15:060.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1619752LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1619753MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277476002
1619754
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M12.5 76 75-12573 4 252.5<0.20 1.9 1.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
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Huntersville, NC 28078
[phone]
Page 11 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277672
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20147
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92277672001, 92277672002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617580
Associated Lab Samples:92277672001, 92277672002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/05/15 01:553.8
Arsenic ug/L ND 10.0 12/05/15 01:552.5
Barium ug/L ND 100 12/05/15 01:552.5
Beryllium ug/L ND 1.0 12/05/15 01:550.50
Cadmium ug/L ND 1.0 12/05/15 01:550.50
Chromium ug/L ND 10.0 12/05/15 01:552.5
Cobalt ug/L ND 10.0 12/05/15 01:552.5
Copper ug/L ND 10.0 12/05/15 01:552.5
Lead ug/L ND 10.0 12/05/15 01:552.5
Nickel ug/L ND 50.0 12/05/15 01:552.5
Selenium ug/L ND 10.0 12/05/15 01:555.0
Silver ug/L ND 10.0 12/05/15 01:552.5
Thallium ug/L ND 5.5 12/05/15 01:555.0
Tin ug/L ND 100 12/05/15 01:552.5
Vanadium ug/L ND 25.0 12/05/15 01:552.5
Zinc ug/L ND 10.0 12/05/15 01:555.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617581LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 454500 91 80-120
Arsenic ug/L 430500 86 80-120
Barium ug/L 502500 100 80-120
Beryllium ug/L 513500 103 80-120
Cadmium ug/L 466500 93 80-120
Chromium ug/L 494500 99 80-120
Cobalt ug/L 454500 91 80-120
Copper ug/L 479500 96 80-120
Lead ug/L 452500 90 80-120
Nickel ug/L 469500 94 80-120
Selenium ug/L 437500 87 80-120
Silver ug/L 236250 95 80-120
Thallium ug/L 454500 91 80-120
Tin ug/L 462500 92 80-120
Vanadium ug/L 476500 95 80-120
Zinc ug/L 444500 89 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277672
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1617582MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277330004
1617583
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 87 75-12583 5 25500ND437417
Arsenic ug/L 500 83 75-12579 6 25500ND418395
Barium ug/L 500 97 75-12591 6 2550019.2 503 476
Beryllium ug/L 500 99 75-12594 6 25500ND497468
Cadmium ug/L 500 90 75-12585 5 25500ND448426
Chromium ug/L 500 95 75-12590 6 25500ND475449
Cobalt ug/L 500 87 75-12583 5 25500ND436416
Copper ug/L 500 94 75-12588 6 25500ND468441
Lead ug/L 500 86 75-12582 5 25500ND433411
Nickel ug/L 500 90 75-12585 5 25500ND449427
Selenium ug/L 500 84 75-12580 4 25500ND418401
Silver ug/L 250 91 75-12586 5 25250ND228216
Thallium ug/L 500 87 75-12584 3 255005.2J 438 424
Tin ug/L 500 89 75-12585 5 25500ND445425
Vanadium ug/L 500 92 75-12587 5 25500ND460436
Zinc ug/L 500 85 75-12581 5 255007.9J 432 411
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277672
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34482
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92277672001, 92277672002, 92277672003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616469
Associated Lab Samples:92277672001, 92277672002, 92277672003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/01/15 03:130.33
1,1,1-Trichloroethane ug/L ND 1.0 12/01/15 03:130.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/01/15 03:130.40
1,1,2-Trichloroethane ug/L ND 1.0 12/01/15 03:130.29
1,1-Dichloroethane ug/L ND 5.0 12/01/15 03:130.32
1,1-Dichloroethene ug/L ND 5.0 12/01/15 03:130.56
1,1-Dichloropropene ug/L ND 5.0 12/01/15 03:130.49
1,2,3-Trichloropropane ug/L ND 1.0 12/01/15 03:130.41
1,2,4-Trichlorobenzene ug/L ND 10.0 12/01/15 03:130.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/01/15 03:132.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/01/15 03:130.27
1,2-Dichlorobenzene ug/L ND 5.0 12/01/15 03:130.30
1,2-Dichloroethane ug/L ND 1.0 12/01/15 03:130.24
1,2-Dichloropropane ug/L ND 1.0 12/01/15 03:130.27
1,3-Dichlorobenzene ug/L ND 5.0 12/01/15 03:130.24
1,3-Dichloropropane ug/L ND 1.0 12/01/15 03:130.28
1,4-Dichlorobenzene ug/L ND 1.0 12/01/15 03:130.33
2,2-Dichloropropane ug/L ND 15.0 12/01/15 03:130.13
2-Butanone (MEK)ug/L ND 100 12/01/15 03:130.96
2-Hexanone ug/L ND 50.0 12/01/15 03:130.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/01/15 03:130.33
Acetone ug/L ND 100 12/01/15 03:1310.0
Acetonitrile ug/L ND 55.0 12/01/15 03:132.2
Acrolein ug/L ND 53.0 12/01/15 03:131.6
Acrylonitrile ug/L ND 200 12/01/15 03:131.9
Allyl chloride ug/L ND 10.0 12/01/15 03:131.5
Benzene ug/L ND 1.0 12/01/15 03:130.25
Bromochloromethane ug/L ND 3.0 12/01/15 03:130.17
Bromodichloromethane ug/L ND 1.0 12/01/15 03:130.18
Bromoform ug/L ND 3.0 12/01/15 03:130.26
Bromomethane ug/L ND 10.0 12/01/15 03:130.29
Carbon disulfide ug/L ND 100 12/01/15 03:131.2
Carbon tetrachloride ug/L ND 1.0 12/01/15 03:130.25
Chlorobenzene ug/L ND 3.0 12/01/15 03:130.23
Chloroethane ug/L ND 10.0 12/01/15 03:130.54
Chloroform ug/L ND 5.0 12/01/15 03:130.14
Chloromethane ug/L ND 1.0 12/01/15 03:130.11
Chloroprene ug/L ND 20.0 12/01/15 03:130.27
cis-1,2-Dichloroethene ug/L ND 5.0 12/01/15 03:130.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/01/15 03:130.13
Dibromochloromethane ug/L ND 3.0 12/01/15 03:130.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277672
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616469
Associated Lab Samples:92277672001, 92277672002, 92277672003
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 12/01/15 03:130.21
Dichlorodifluoromethane ug/L ND 5.0 12/01/15 03:130.21
Ethyl methacrylate ug/L ND 10.0 12/01/15 03:130.20
Ethylbenzene ug/L ND 1.0 12/01/15 03:130.30
Hexachloro-1,3-butadiene ug/L ND 10.0 12/01/15 03:130.71
Iodomethane ug/L ND 10.0 12/01/15 03:130.32
Isobutanol ug/L ND 100 12/01/15 03:1335.0
Methacrylonitrile ug/L ND 100 12/01/15 03:130.93
Methyl methacrylate ug/L ND 30.0 12/01/15 03:132.0
Methylene Chloride ug/L ND 1.0 12/01/15 03:130.97
Naphthalene ug/L ND 10.0 12/01/15 03:130.24
Propionitrile ug/L ND 150 12/01/15 03:133.6
Styrene ug/L ND 1.0 12/01/15 03:130.26
Tetrachloroethene ug/L ND 1.0 12/01/15 03:130.46
Toluene ug/L ND 1.0 12/01/15 03:130.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/01/15 03:130.49
trans-1,3-Dichloropropene ug/L ND 1.0 12/01/15 03:130.26
trans-1,4-Dichloro-2-butene ug/L ND 100 12/01/15 03:131.0
Trichloroethene ug/L ND 1.0 12/01/15 03:130.47
Trichlorofluoromethane ug/L ND 1.0 12/01/15 03:130.20
Vinyl acetate ug/L ND 50.0 12/01/15 03:130.35
Vinyl chloride ug/L ND 1.0 12/01/15 03:130.62
Xylene (Total)ug/L ND 5.0 12/01/15 03:130.66
1,2-Dichloroethane-d4 (S)%97 70-130 12/01/15 03:13
4-Bromofluorobenzene (S)%103 70-130 12/01/15 03:13
Toluene-d8 (S)%100 70-130 12/01/15 03:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616470LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.050 88 80-125
1,1,1-Trichloroethane ug/L 47.550 95 71-129
1,1,2,2-Tetrachloroethane ug/L 41.950 84 79-124
1,1,2-Trichloroethane ug/L 46.050 92 85-125
1,1-Dichloroethane ug/L 49.050 98 73-126
1,1-Dichloroethene ug/L 51.650 103 66-135
1,1-Dichloropropene ug/L 51.750 103 74-135
1,2,3-Trichloropropane ug/L 44.150 88 75-130
1,2,4-Trichlorobenzene ug/L 43.250 86 75-134
1,2-Dibromo-3-chloropropane ug/L 39.550 79 71-133
1,2-Dibromoethane (EDB)ug/L 45.150 90 83-124
1,2-Dichlorobenzene ug/L 47.050 94 80-133
1,2-Dichloroethane ug/L 45.650 91 67-128
1,2-Dichloropropane ug/L 46.150 92 75-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277672
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616470LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 47.750 95 77-130
1,3-Dichloropropane ug/L 43.250 86 76-131
1,4-Dichlorobenzene ug/L 46.950 94 78-130
2,2-Dichloropropane ug/L 42.750 85 40-160
2-Butanone (MEK)ug/L 95.3J100 95 61-144
2-Hexanone ug/L 82.2100 82 68-143
4-Methyl-2-pentanone (MIBK)ug/L 93.9J100 94 72-135
Acetone ug/L 92.9J100 93 48-146
Acetonitrile ug/L 443500 89 62-150
Acrolein ug/L 251250 101 24-160
Acrylonitrile ug/L 239250 95 40-160
Allyl chloride ug/L 43.850 88 66-137
Benzene ug/L 48.850 98 80-125
Bromochloromethane ug/L 52.650 105 71-125
Bromodichloromethane ug/L 44.750 89 78-124
Bromoform ug/L 39.350 79 71-128
Bromomethane ug/L 46.150 92 40-160
Carbon disulfide ug/L 48.4J50 97 50-160
Carbon tetrachloride ug/L 48.750 97 69-131
Chlorobenzene ug/L 43.850 88 81-122
Chloroethane ug/L 50.250 100 39-148
Chloroform ug/L 49.050 98 73-127
Chloromethane ug/L 47.850 96 44-146
Chloroprene ug/L 53.150 106 75-145
cis-1,2-Dichloroethene ug/L 50.950 102 74-124
cis-1,3-Dichloropropene ug/L 44.550 89 72-132
Dibromochloromethane ug/L 41.450 83 78-125
Dibromomethane ug/L 50.250 100 82-120
Dichlorodifluoromethane ug/L 59.950 120 34-157
Ethyl methacrylate ug/L 40.7 L0508182-121
Ethylbenzene ug/L 44.550 89 79-121
Hexachloro-1,3-butadiene ug/L 39.350 79 72-131
Iodomethane ug/L 94.2100 94 39-154
Isobutanol ug/L 8111000 81 34-160
Methacrylonitrile ug/L 481500 96 74-134
Methyl methacrylate ug/L 42.550 85 84-124
Methylene Chloride ug/L 51.050 102 64-133
Naphthalene ug/L 43.150 86 73-133
Propionitrile ug/L 450500 90 73-140
Styrene ug/L 45.950 92 84-126
Tetrachloroethene ug/L 46.350 93 78-122
Toluene ug/L 47.450 95 80-121
trans-1,2-Dichloroethene ug/L 50.850 102 71-127
trans-1,3-Dichloropropene ug/L 44.650 89 69-141
trans-1,4-Dichloro-2-butene ug/L 34.0J50 68 40-160
Trichloroethene ug/L 46.550 93 78-122
Trichlorofluoromethane ug/L 54.150 108 53-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
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[phone]
Page 16 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277672
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616470LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 95.3100 95 40-160
Vinyl chloride ug/L 55.550 111 58-137
Xylene (Total)ug/L 132150 88 81-126
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1616471MATRIX SPIKE SAMPLE:
MSSpike
Result
92277673001
1,1,1,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,1-Trichloroethane ug/L 22.120 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.520 92 70-130ND
1,1,2-Trichloroethane ug/L 21.020 105 70-130ND
1,1-Dichloroethane ug/L 22.620 113 70-130ND
1,1-Dichloroethene ug/L 24.720 123 70-166ND
1,1-Dichloropropene ug/L 24.420 122 70-130ND
1,2,3-Trichloropropane ug/L 19.220 96 70-130ND
1,2,4-Trichlorobenzene ug/L 18.220 91 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.820 84 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.820 104 70-130ND
1,2-Dichlorobenzene ug/L 21.120 105 70-130ND
1,2-Dichloroethane ug/L 20.620 103 70-130ND
1,2-Dichloropropane ug/L 20.920 105 70-130ND
1,3-Dichlorobenzene ug/L 21.520 107 70-130ND
1,3-Dichloropropane ug/L 19.620 98 70-130ND
1,4-Dichlorobenzene ug/L 20.820 103 70-130ND
2,2-Dichloropropane ug/L 18.320 92 70-130ND
2-Butanone (MEK)ug/L 41.8J40 105 70-130ND
2-Hexanone ug/L 36.1J40 90 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 41.1J40 103 70-130ND
Acetone ug/L 44.0J40 104 70-130ND
Acetonitrile ug/L 188200 94 70-130ND
Acrolein ug/L 102100 102 70-130ND
Acrylonitrile ug/L 106J100 106 70-130ND
Allyl chloride ug/L 20.520 102 70-130ND
Benzene ug/L 23.220 114 70-1480.35J
Bromochloromethane ug/L 25.020 125 70-130ND
Bromodichloromethane ug/L 19.220 96 70-130ND
Bromoform ug/L 16.520 83 70-130ND
Bromomethane ug/L 21.920 109 70-130ND
Carbon disulfide ug/L 22.6J20 113 70-130ND
Carbon tetrachloride ug/L 22.720 114 70-130ND
Chlorobenzene ug/L 20.920 104 70-146ND
Chloroethane ug/L 23.820 119 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277672
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1616471MATRIX SPIKE SAMPLE:
MSSpike
Result
92277673001
Chloroform ug/L 22.920 114 70-130ND
Chloromethane ug/L 23.520 117 70-130ND
Chloroprene ug/L 24.720 123 70-130ND
cis-1,2-Dichloroethene ug/L 24.120 120 70-130ND
cis-1,3-Dichloropropene ug/L 19.620 98 70-130ND
Dibromochloromethane ug/L 18.620 93 70-130ND
Dibromomethane ug/L 22.720 113 70-130ND
Dichlorodifluoromethane ug/L 29.8 M12014970-130ND
Ethyl methacrylate ug/L 18.320 91 70-130ND
Ethylbenzene ug/L 20.520 102 70-130ND
Hexachloro-1,3-butadiene ug/L 16.320 82 70-130ND
Iodomethane ug/L 37.440 93 70-130ND
Isobutanol ug/L 309400 77 70-130ND
Methacrylonitrile ug/L 216200 108 70-130ND
Methyl methacrylate ug/L 18.3J20 91 70-130ND
Methylene Chloride ug/L 23.620 118 70-130ND
Naphthalene ug/L 17.320 86 70-130ND
Propionitrile ug/L 192200 96 70-130ND
Styrene ug/L 20.220 101 70-130ND
Tetrachloroethene ug/L 21.620 108 70-130ND
Toluene ug/L 21.620 108 70-155ND
trans-1,2-Dichloroethene ug/L 24.220 121 70-130ND
trans-1,3-Dichloropropene ug/L 19.520 97 70-130ND
trans-1,4-Dichloro-2-butene ug/L 13.0J M1206570-130ND
Trichloroethene ug/L 20.720 104 69-151ND
Trichlorofluoromethane ug/L 25.720 129 70-130ND
Vinyl acetate ug/L 35.1J40 88 70-130ND
Vinyl chloride ug/L 27.3 M12013770-130ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277673002
1616472SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.94J 300.85J
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277672
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277673002
1616472SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L 0.47J 300.47J
1,2-Dichloropropane ug/L 1.9 7 302.0
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 4.4 5 304.6
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L 0.88J 300.88J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 1.3J 7 301.3J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 2.6J 5 302.5J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L 0.38J 300.50J
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277672
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277673002
1616472SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%99 297
4-Bromofluorobenzene (S)%105 0104
Toluene-d8 (S)%99 198
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 24
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92277672
SURRY BLANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associatedsamples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 24
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92277672
SURRY BLANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92277672001 MPRP/20147 ICP/18175EBEPA 3010 EPA 6010
92277672002 MPRP/20147 ICP/18175FBEPA 3010 EPA 6010
92277672001 MERP/8724 MERC/8382EBEPA 7470 EPA 7470
92277672002 MERP/8724 MERC/8382FBEPA 7470 EPA 7470
92277672001 MSV/34482EBEPA 8260
92277672002 MSV/34482FBEPA 8260
92277672003 MSV/34482TBEPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/08/2015 09:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 24
Page 23 of 24
Page 24 of 24
Appendix B
Field Sampling Parameter Data Sheet(s)