HomeMy WebLinkAboutItem No 24 - Initial Abatement Action Report Incident 9567 M-OCRepar
ESP Associates P.A
Dear Mr Schiff
On behalf of the property owner Beazer Homes ESP Associates P.A is pleased to provide the
attached Initial Abatement Action Report for the closure of the subject propertys petroleum
release ESP respectively requests classification of the release as Low Risk and issuance of no
further action notice pending completion of Notice of Residual Petroleum
and recordation of
deed restriction on groundwater usage
Thank you for your attention in this matter If you should have any questions please do not
hesitate to contact me at 803 835-0915
Sincerely
cc Jade Eastridge Beazer Homes
P.O Box 7030 Charlotte NC 28241
L800.960.7317 NC 7045834949 fax 704.583.4950 SC 803.8022440 fax 803.802.2513
www.espassociates.com
July 27 2007
NCDENR
UST Section
Mooresville Regional Office
919 North Main Street
Mooresville North Carolina 28115
Attention Mr Allen Schiff
Reference INITIAL ABATEMENT ACTION REPORT
Morehead Common Site Area No
1000 South Clarkson Street
Charlotte Mecklenburg County North Carolina
UST Incident No 9567
ESP Project No E6-UD42.601
ESP Associates P.A
Christopher Ward
Environmental Sez
NC License No
Initial Abatement Action Report
SITE iNFORMATION
Site Identification
El Date of Report July 27 2007
El Facility ID 0-0 14432
El UST Incident Number 9567
El Site Name Morehead Common Site Area No
El Site Street Address 1000 South Clarkson Street
El City/County/Zip Code Charlotte Mecklenburg County 28278
El Description of Geographical Data Point Approximate center of UST
El Location Method Mecklenburg County
Polaris GIS Map
El Latitude 5.2266
El Longitude -80.8589
Information about Contacts Associated with the Leaking UST System
El UST Owner Beazer Homes
1300 Blvd Suite Charlotte NC 28203-4265
704.370.7200
El UST Operator N/A
El Property Owner Same as above
El Property Occupant Same as above
El Consultant/Contractor ESP Associates P.A Chris Ward PG
P0 Box 7030 Charlotte NC 28241
803.835.0915
El Analytical Laboratory Prism Laboratories Inc
P0 Box 240543 Charlotte NC 28224-0403
704.529.6364
NC Certification No 402
Information about Release
El Date Discovered September 1992
El Estimated Quantity of Release Unknown
El Cause of Release Unknown
El Source of Release Diesel Fuel USTs
El Size and contents of UST
System from which release occurred Five USTs ranging from 1000 to 6000 gallons
in size
Certification
Iris Ward Professional Geologist for ESP Associates P.A do certify that the
rrnation contained in this report is correct and accurate to the best of my knowledge
Associates P.A is licensed to practice both geology and engineering in North Carolina
Associates certification numbers are Geology C-347 and Engineering C-0587
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 27 2007
INTRODUCTION
The subject site has an address of 1000 South Clarkson Street Tax Parcel No 07325207 in
Charlotte Mecklenburg County North Carolina see Figure Topographic Site Location Map
The area of the subject petroleum release associated with five former diesel underground storage
tanks USTs abandoned in 1992 has been designated by ESP as Area No of the Morehead
Common site The subject release site UST Incident No 9567 is the location of former Duke
Energy-Worth Keeter facility
SITE HISTORY AND CHARACTERIZATION
On May 29 2007 ESP responded on behalf of Beazer Homes to an encounter with apparent
impacted soil during trackhoe excavation associated with planned mass grading operations
at
the subject site Upon arriving at the site ESP observed soils with an apparent petroleum
odor
located on the west side of South Clarkson Street approximately 500 feet south of its intersection
with West Morehead Street see Figure As required ESP emailed notification of the release
discovery to Mr Steve Bograd of the Mooresville Regional Office of NCDENR on May 30
2007
Following NCDENR notification ESP reviewed available files at the NCDENR Mooresville
Regional Office and determined that impacted soils encountered on May 29 2007 were
associated with open UST Incident No 9567 Phase Limited Site Assessment LSA
performed by MACTEC documented soil impact and revealed that groundwater in one of the
three Phase LSA monitor wells had been impacted slightly above NC 2L Standards for
MADEP EPH Aliphatics C9-C22 0.340 mg/L
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 27 2007
Release Location
The subject site is located within an urban area of Charlotte which historically included
warehouse and commercial structures Site structures
associated with the former Duke Energy-
Worth Keeter Inc facility were recently demolished and the site mass graded as part of re
development as mixed-use development see Figures and
Based on our review of the Geologic Map of North Carolina 1985 the subject site is located
within the Charlotte Belt locally comprised of intrusive metamorphosed granitic rocks locally
pinkish gray massive to weakly foliated and containing hornblende Soils encountered in this
area are the residual product of chemical weathering of rock presently underlying
the site Soil
weathering is more advanced near the surface grading with depth to less weathered rock and
finally bedrock
UST Information
As reported by others total of five diesel USTs were excavated and removed from the subject
release area in 1992 These USTs included the following
PreviousTankInstallationRemovalSizeTankLastTankTankNoDate Date Gallons Dimensions Contents Contents
Unknown 9-15-92 6000 Unknown Diesel Unknown
Unknown 9-15-92 3000 Unknown Diesel Unknown
Unknown 9-15-92 2000 Unknown Diesel Unknown
Unknown 9-15-92 1000 Unknown Diesel Unknown
Unknown 9-15-92 6000 Unknown Diesel Unknown
Locations of the above USTs are depicted on Figure
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 27 2007
Previous Reporting
Atlantic Environmental Services submitted UST Closure Report dated October 30 1992
following closure of the subject sites USTs Report of Phase ILimited Site Assessment dated
April 15 2005 was submitted by MACTEC to NCDENR for the subject release Notice of
Residual Petroleum NORP was submitted by MACTEC to NCDENR on April 11 2007
NCDENR file notes indicate that the NORP has not been approved due to insufficient data ESP
emailed 24-Hour release notification to the Mooresville Regional Office of NCDENR on May
30 2007 see Appendix
MACTEC Phase LSA Groundwater Assessment
Details of an LSA groundwater assessment are provided in MACTECs Report of Phase
Limited Site Assessment dated April 15 2005 Three monitor wells designated 9567-1 9567-2
and 9567-3 were completed at the site on March 21 2005 see Figure The monitor wells
were installed to depth of 12 to 14.5 feet BLS while groundwater was gauged to be at depths of
10.35 to 12.54 feet below the wells top of casing which was approximately feet above land
surface
Groundwater samples collected from the three monitor wells by MACTEC on March 23 2005
were analyzed for volatile and semi-volatile organic compounds VOCs and SVOCs by EPA
Methods 602 and 625 and for MADEP VPH and EPH Results of the laboratory analyses
revealed that all constituents were below NC2L Standards with the exception of MADEP
aromatics C9-C22 in monitor well 9567-3 which was detected at concentration of 0.340 mgIL
which is slightly above its NC2L Standard of 0.210 mgIL Results of the laboratory analyses are
summarized on Table B-2
Monitor well 9567-3 was completed within the former UST pit for Tank Nos and see
Figure All three LSA monitor wells have since been abandoned by others
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 27 2007
INITIAL ABATEMENT ACTIVITIES
Waste Characterization Sampling
On May 29 2007 ESP collected waste characterization soil sample SP-3 from the area of
impacted soils at depth of approximately feet below land surface BLS using trackhoe
representative portion of the soil sample was screened in the field with an organic vapor analyzer
OVA and recorded reading of 42 ppm Soil sample SP-3 was submitted to Prism
Laboratories of Charlotte North Carolina for analysis of total petroleum hydrocarbons TPH for
diesel range organics DRO and gasoline range organics GRO oil grease OG by EPA
Method 9071A volatile organic compounds VOCs by EPA Method 8260B pesticides by EPA
Method 8081A PCBs by EPA Method 8082 and for total lead and chromium by EPA Method
60 lOB Waste characterization soil sample SP-3 was collected and analyzed to confirm that
release had occurred and to characterize contaminant types and concentrations for subsequent
off-site permitted disposal/treatment
As revealed by the laboratory analysis of SP-3 TPI-I-DRO was reported at concentration of 140
mg/Kg TPH-GRO at 23 mg/Kg OG at 270 mg/Kg while several VOCs were reported above
reporting limits Results for pesticides and PCBs were all below reporting limits BRLs while
total chromium and lead were both reported to be below soil-to-groundwater MSCCs See
Figure for soil sample location map Results of the waste characterization analyses are
summarized on Table B-i while the laboratory data report is included as Appendix
Contaminated Soil Excavation and Stockpile Sampling
On June 11 and 12 2007
ESP documented the excavation of 972.27 tons of impacted soil from
Area No by the sites grading contractor Gelder Thompson of Midland North Carolina The
excavation was advanced based on OVA readings and evidence of visible staining The resulting
excavation measured approximately 20 ft 47 ft 10 ft deep see Figure Previously
abandoned MACTEC monitor wells 9567-1 and 9567-3 associated with their April 15 2005
Phase LSA were uncovered during excavation of impacted soils Encountered soils generally
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 27 2007
consisted of reddish-brown clayey silt and silty sand Neither groundwater bedrock nor free
product was encountered within the tank pit See site photographs in Appendix
On June 11 and 12 2007
the 972.27 tons of excavated soil was transported by Gelder Thompson
to the CMS Landfill in Concord North Carolina for permitted disposal see non-hazardous waste
manifest in Appendix
Post-Excavation Confirmatory Sampling
On June 13 2007 following completion of the above excavation activities confirmatory soil
samples were collected at depth of feet BLS from each of the excavations four sides WS-1
through WS-4 while one sample was collected at depths of 10 feet BLS from the base of the
excavation B-i The sidewall samples were collected at the foot depth due to the occurrence
of elevated OVA readings at that depth The five soil samples were hand delivered on ice to
Prism Laboratories to be analyzed for NCDENR risk-based parameters which include VOCs
and SVOCs by EPA Methods 8260B and 8270C and for VPH/EPH by the MADEP method
Sample locations and excavation dimensions are depicted on Figure Soil Sample Location
Map Sampling was performed in general accordance with ESPs SOP see Appendix
Results of the laboratory analysis
of confirmatory samples WS-1 through WS-4 and B-i revealed
that all analyzed constituents were either BRL or below the lowest of the soil-to-groundwater or
residential MSCC with the exception of the SVOC benzoaanthracene 0.48 mg/Kg which was
reported to be above its soil-to-groundwater MSCC 0.34 mg/Kg but below the residential
MSCC 0.88 mg/Kg Laboratory analytical results for the confirmatory soil samples are
summarized on Table B-i The Prism laboratory data report is included as Appendix
RECEPTOR SURVEY
On July 20 2007
Mr Eddie Rogers of ESP performed receptor survey to document the
presence or absence of active and/or inactive water supply wells within 1500-foot radius of the
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 27 2007
subject UST release see Figure Receptor Survey
Map The receptor survey
included
interviews with available site occupants and visual observations for water supply wells and/or
municipal water meters All properties within 500 feet of the site were visited to determine well
status The area within 1000 feet of the subject release consists of commercial and industrial
development with numerous vacant structures No active or inactive water supply wells were
identified within 1000-foot radius of the subject release Municipal water and sewer have
historically been available within the area of the site Additionally no surface water bodies were
identified within 500 feet of the release see Figure
CONCLUSIONS AND RECOMMENDATIONS
The following conclusions have been formulated based on our completion of field activities
including abatement activities receptor survey and our review of laboratory data from the
analysis of collected soil samples
rJ The subject site the location of former Duke Energy-Worth Keeter facility has an
address of 1000 South Clarkson Street in Charlotte North Carolina and is identified as
UST Incident No 9567
On May 29 2007 ESP responded on behalf of Beazer Homes to an encounter with
apparent impacted soil during trackhoe excavation associated with planned mass
grading operations
at the subject site
2005 Phase LSA performed in the release area by MACTEC documented soil impact
and revealed that groundwater in one of the three Phase LSA monitor wells had been
impacted slightly above NC 2L Standards for MADEP EPH Aliphatics C9-C22
Analysis of SP-3 collected on May 29 2007 revealed that TPH-DRO was at
concentration of 140 mg/Kg TPH-GRO at 23 mg/Kg OG at 270 mg/Kg while several
VOCs were reported above reporting limits Results for pesticides and PCBs were all
BRLs while total chromium and lead were both reported to be below soil-to-groundwater
MSCCs
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 27 2007
On June 11 and 12 2007
ESP documented the excavation of 972.27 tons of impacted
soil from Area No by the sites grading contractor Geider Thompson The excavation
was advanced based on OVA readings and evidence of visible staining The resulting
excavation measured approximately 20 ft 47 ft 10 ft deep
On June 11 and 12 2007
the 972.27 tons of excavated soil was transported by Gelder
Thompson to the CMS Landfill in Concord North Carolina for permitted disposal
Results of the laboratory analysis of confirmatory samples WS-through WS-4 and B-i
revealed that all analyzed constituents were either BRL or below the lowest of the soil-to-
groundwater or residential MSCC with the exception of the SVOC benzoaanthracene
0.48 mg/Kg which was reported to be above its soil-to-groundwater MSCC 0.34
mg/Kg but below the residential MSCC 0.88 mg/Kg
Municipal water and sewer are available in the area of the release
No water supply wells were identified within 1000 feet of the release and
No surface water bodies were identified within 500 feet of the subject release
Based on the documented presence of one confirmatory soil sample with an analyzed risk-based
parameter above its North Carolina soil-to-groundwater but below its residential MSCCs the
detection of C9-C 18 Aliphatics above the NC2L Standard the absence of water supply wells
within 1000 feet of the release and the absence of surface water feature within 500 feet of the
release ESP recommends that NORP restricting groundwater usage be completed and
following recordation of deed restriction no further action notice be issued for the subject
release
Attachments
Table B-i Summary of Soil Sampling Results
Table B-2 Summary of Groundwater Sampling Results
Figure Topographic Site Location Map
Figure 2005 Aerial Photograph
Figure Former UST Location Map
Figure Soil Sample Location Map
Figure Receptor Survey Map
Appendix 24-Hour Release Notification Email
Appendix Manifests
Appendix Site Photographs
Appendix ESPs SOP
Appendix Prism Laboratory Data Reports
ATTACHMENTS
TABLES
GroundwaterNLSCC nib/kg
Residential MSCC mg/k
Industrial/Comniercial MSCC mfg
0.0005 Analyte less than the noted report limit
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
Date 7/10/07 Incident No 9567
5/29/07
Table
Date 7/10/07 Incident No 9567
SP-3 5/29/07 Waste Initial
ID Abatement
0.0005 Analyte less than the noted report limit
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
Summary of Soil Sampling Results
Morehead Common Area No Charlotte North
6010B 6010B
Carolina
8260B 8260B 8260B 8260B 8260B 8260B
j--C
-0
c3
...
ti
..
E-o E-o
26
8260B
35 0.0053 0.024 0.029 0.0053 0.0053 0.0053 0.0053
B-i 6/13/07 Pit Floor
WS-l 6/13/07 North Pit
Wall
Initial
Abatement NA NA 0.0049 0.0049 0.0049 0.0049 0.0049 0.0049 0.0049
WS-2 6/13/07 West Pit
Wall
Initial
Abatement NA NA 0.0040 0.0040 0.0040 0.0040 0.0040 0.0040 0.0040
WS-3 6/13/07 South Pit
Wall
Initial
Abatement NA NA 0.0049 0.0049 0.0049 0.0049 0.0049 0.0049 0.0049
WS-4 6/13/07 East Pit
Wall
Initial
Abatement NA NA 0.0055 0.0055 0.12 0.0055 0.0055 0.0055 0.0055
Initial
Abatement NA 0.0047 0.0047 0.048 0.0047 0.0047 0.0047 0.0047
1226 400
27 270 1.7 0.58 2.8 3.3 4.3 7.5 7.3
47 400 626 313 1564 626 626 782 782
16350 8176 40880 16350 16350 20440 20440
Table Summary of Soil Sampling Results
Date 7/10/07 Incident No 9567 Morehead Common Area No Charlotte North Carolina
tiua1ticat Method
titaminIŁtt oo cern-
Sample hate ouce ljIncident
ID CollctedU Ii asriQIrnI
SP-3 5/29/07 Waste Initial
ID Abatement
8260B 8260B 8260B 8081A 8082 8270C 8270C 8270C 8270C
8270C
ut
0.0053 0.0053 0.0053 BRL BRL NA NA NA NA NA
WS-1 6/13/07 North Pit
Wall
Initial
Abatement 0.0049 0.0049 0.0049 NA NA 0.36 0.36 0.36 0.36 0.36
WS-2 6/13/07 West Pit
Wall
Initial
Abatement 0.0040 0.0040 0.0040 NA NA 0.38 0.38 0.38 0.38 0.38
WS-3 6/13/07 South Pit
Wall
Initial
Abatement 0.0049 0.0049 0.0049 NA NA 0.45 0.80 0.41 0.55 0.48
WS-4 6/13/07 East Pit
Wall
Initial
Abatement 0.0055 0.0055 0.0055 NA NA 0.39 0.39 0.39 0.39 0.39
0.0047 0.0047 0.0047 NA NA 0.41 0.41 0.41 0.41 0.41B-i 6/13/07 Pit Floor 10 Imtial
Abatement
Soil to Ground ate SCC
Reside tial MSCC mg/kg
Industrial/Co er a1 CC g/kg
0.0005 Analyte less than the noted report limit
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
7.3 4.6 ----38 280 60 290 0.34
3129 3200 1560
----88 620 469 469 0.88
81760 82000 40000
----780 16400 12264 12264
Summary of Groundwater Sampling Results
Morehead Common Area No Charlotte North Carolina
602 602 602 602 602 625
200 55 1000 530 21 420
5000 200000 84500 257500 87500 15500
Table B-2
Date 7/23/07 Incident No 9567
1ii 1d
9567-1 3/23/05 9567-1 LSA 1.0
MADEP
VPH
MADEP
EPH
MADEP
EPH
MADEP
EPH
00-i r1c1c 00ca
1.0
9567-2 3/23/05 Fuel
Island 9567-2 LSA 1.0 1.0 1.0 1.0 10 5.0 100 170 640 140
1.0 1.0 1.0 5.0 100 100 170 100
1.09567-3 3/23/05 AB 9567-3 LSA 1.0
__________________2L Standard ug/L
2B Standard or EP
ati6l1Tteria ugIL
0.0005 Analyte less than the noted report limit
Results reported in micrograms per liter ugIL
Results reported in mg/kg
GCL gross contaminant level
1.0 1.0 5.0 100 340 170 170
210 4200 42000
Above groundwater samples were collected by MACTEC as reported in their April 15 2005 Report of Phase LSA
FIGURES
FiGURE
TOPOGRAPHIC 7E LOCA liON MAPUSGS CHARLOTTE EAST QUADRANGLE
MOREHEAD COMMON SiTEcHARLOTTENORThCAROliNA
FiGURE
2005 AERIAL PHOTOGRAPH
MOREHEAD COMMON ShE
CHARLOTTEI NORTH CAROLINA
0ECTNO SHEET TITLE FiGURECALfNTSFORMER UST LOGA 77CH MAP ESI PA
AlE 7/24/07 AREA 1Y
RAbWs BY PROJECT knIh
CHECKED BY MOREHEAD COMMON SiTE
CHARLOTTE NORTH CAROLINA
CDE
TANKS
LEGEND
ABANDONED MACTEC LSA MOM TOR WELL LOCA 770N
JUNE 2007 EXCA VA 710N DEPTH OF 10 FEET
FORMER LOCA 770N OF DIESEL USTs REMOVED IN 1992
20
LEGEND
1JCONF1RMA TORY SOIL SAMPLE LOCA 710N
EXCA VA 770N DEPTh OF 10 FEET
ABANDONED MACTEC LSA MONITOR I4fLL LOCA T1ON
ws-1
WS-2
20
APPROXIMA IE SCALEINFEET
MOREHEAD COMMCW 7E
cHARLOTTE NORTh CAROLINA
APPENDIX
24-HOUR RELEASE NOTIFICATION EMAIL
Page of3
Chris Ward _________________ ____
____
From Chris Ward
Sent Wednesday May 30 2007 144 PM
To Steve.Bograd@ncmail.net
Cc Jade Eastridge jeastrid@beazer.com kholdenr@beazer.com
Subject RE 24-Hour Notification Incidents No and
Attachments Incidents Nos and 3.pdf
Please see attachment that was left off the original email
From Chris Ward
Sent Wednesday May 30 2007 140 PM
To Steve.Bograd@ncmail.net
Cc Jade Eastridge jeastrid@beazer.com kholdenr@beazer.com
Subject 24-Hour Notification Incidents No and
Steve
On behalf of Beazer Homes am herein providing 24-Hour Notification of the discovery of
environmentally-impacted soils at two separate locations Incidents Nos and on Beazer
Homes Morehead Commons residential development currently being graded The Morehead
Commons property is located on the south side of West Morehead Street at its intersection
with South Clarkson Street in Charlotte Mecklenburg County
North Carolina
Incident No
On May 17 2007 during site grading operations
concrete vault-like structure was
encountered on the east side of Post Street Tax Parcel No 07325213 approximately 450 feet
south of its intersection with South Clarkson Street See attached 2005 Site Map On May 17
2007 Mr Chris Ward of ESP observed soils that exhibited some black staining however field
screening with an OVA did not reveal elevated readings In an attempt to confirm the absence
or presence of potential contaminants on May 17 ESP collected waste characterization soil
sample SP-1 of visibly stained soils from depth of approximately feet The soil sample was
analyzed for volatile organic compounds VOCs by EPA Method 8260B pesticides by EPA
Method 8081 polychlorinated biphenyls
PCBs by EPA Method 8082 oil and grease OG by
EPA Method 9071 for total petroleum hydrocarbons
TPH by EPA Methods 3550 and 5030
and for total lead and chromium by EPA Method 3051 Preliminary results of the analysis
attached revealed elevated levels of OG 3100 mg/kg TPH-DRO 420 mg/kg and PCB
1260 5.1 mg/kg The parcel was occupied by
Air Reduction Sales Company and Ohio Chemicals
Surgical Equipment from 1933 to between 1956 and 1965 before the property occupant was
listed as no listing
Incident No
On May 29 2007 during site grading operations visibly stained soils with an obvious petroleum
Page of
odor were encountered on the west side of South Clarkson Street approximately 450 feet
south of its intersection with West Morehead Street on Tax Parcel No 07325207 see
attached 2005 Site Map The vicinity of the impacted soils was once occupied by vehicular
service facility with closed USTs Incidents Nos 18101 and 9567 buke Energy-Worth Keeter
before being demolished On May 29 2007 Mr Chris Ward of ESP observed the
environmentally-impacted soils and directed the collection waste characterization soil sample
SP-3 of visibly impacted soils from depth of approximately feet The soil sample was
submitted to Prism Laboratories
to be analyzed for VOCs by EPA Method 8260B pesticides by
EPA Method 8081
PCBs by EPA Method 8082 OG by EPA Method 9071
for TPH by EPA
Methods 3550 and 5030 and for total lead and chromium by EPA Method 3051
Incident No
Please note that 24-Hour Notification for previously identified area of petroleum-impacted
soils was emailed to your attention on May 16 2007 and is referred as Incident No see
attached Site Map Results of the waste characterization analysis of the soil sample collected
from this area and designated PS-i revealed elevated concentrations of number of VOCs OG
10000 mg/kg
TPH-bRO 3600 mg/kg
and TPH-GRO 33 mg/kg
See attached Prism
laboratory report Starting today Incident No is being excavated with impacted soils
stockpiled on site for subsequent off-site disposal
Following receipt of the laboratory results for the waste characterization samples and landfill
disposal authorization ESP will direct the excavation of impacted soils from Incidents Nos
and and their subsequent off-site permitted disposal Confirmatory
soil samples will then be
collected from the walls and base of the excavation at Incidents Nos and Assuming
acceptable results initial abatement action reports will then be prepared for submittal to
NCbENR for each incident
The Responsible Party for the property is
Beazer Homes
1300 South Boulevard
Suite
Charlotte North Carolina 28203-4265
Mr Jade Eastridge
704.370.7200
Please call with any questions
Thanks
Chris Ward PG
Page3of3
Environmental Services Manager
ESP Associates
803.835.0915 direct office
803.802.2515 fax
704 506 7618 mobile
APPENDIX
MANIFESTS
Aw WASTEINDU5.TRIES INC
N.c.NHAzARDous Generators US EPA ID No Mani PageWASTEMANIFESTDocumentNoof 278
Generators Name and Mailing Address Truck No
NC 2iiJGeneratorsPhons
Transporter Company Name US EPA ID Number TransporteisIhe11
7.Trthisporter Company Name US EPA ID Number Transporters Phone
Facility Name and Site Address...10 us EPA ID Number Facilitys Phone
CMS Landfill 704 782 20045Q5.preheadRdConcordNC28027
ii.Waste Shipping Name and Description 12 Containers 13 14
Total Unit
No Type Quantity Wt/Vol
Pt$L It
I_________________________
15 Special Handling Instructions and Additional Information
16..GENERATORS CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of 1-tazardois Waste
PrWtted/Tipad Name Signature..t ..Month Dat Year
It -i
Printed Typed Name Signature Month Day Year
18 Transporter Acknowledgement of Receipt of Materials
Printed/Typed Name Signature Month Day Year
19 Discrepancy Indication Space......___
Facility Owner or Operator Cerification of receipt of waste materials covered by this manifest except as noted in item 19
LadfilI..____
Month Day YearSignature.i
AWl Form 121
Please print or type
for Use.oæ.elite 12 pitch typewriter q7
Additional Descriptions for Materials Listed Above Handling Codes for Wastes Listed Above
Transpprter Acknowledgement of Receiptof Materials /i
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TISIDIF/COPY
ALL WASTE
rint or
17
1degned forüseon elite 12 pitch pewrerJ
WASTE MANIFES
.Get0r Name end Maii
GenetatOrS Phone ____________________________________________
TrnsQr Company Name ick ftçt US EPA
ID Number
TranpOrter Company Name US EPA ID Number
9.Designated Fac
CMS Landfill
5105 Morehe
Concord NC
il.Waste Shippin
-R
Additio
15 Sneniel
19 Discrepancy Indication Space
20 Facility Owner or Operator Cerification of receipt of waste materials covered by this manifest except
as noted in item 19
CMS Landfill
Printed IType Name Signature 07
Veer
AWIFOrm121
TISIDIFI COPY
Manifest
Document No
ALLD WASTETPIESiJC
-yr
Uenerators US.EPAID No Manifest
Document No Page
of
Truck No
1.27834
US EPA ID Number Transporter
US EPA ID Number Transporters Phone
10 USEPA ID Number Facilitys Phone
704 7822004
12 Containers 13 14
Total UnitNoTypeQuantityWtfVol
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dI1PSe on elite 12 pitch typewriterNON-HAZARDOUSWASTEMANIFEST
Geneitors--FJame and Mailing Address
Generators Phone
Transporter Company Name
Transporter Company Name
Designated Facility Name and Site Address
CMS Landfill
51.05 Morehead Rd
Concbrd NC 28027
11 Waste Shipping Name and Description
-A
Additional Descriptions for Materials Listed Above
15 Special Handling Instructions and Additional Information
Handling Codes for Wastes Listed Above
16 GENERATORS CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
Printed /Typd Name Signature Month Da.V Yearth-/1
17 Transporter Acknowledgement of Rectof Materials
Printed /Typed Name Signature Month Day Year
\%..
18 Transporter Acknowledgement of Receipt of Materials
Printed-/-Tiied Name
19 Discrepancy Indication Space
20 Facility Owner or Operator Cerification of receipt of waste materials covered by this manifest except as noted in item 19
CMS Landfill .-
Printed Type Name _7 signature Month Day Year4Jz2//
17
TISID/FI COPY
AWIForm
ALLD WASTE
please print or type
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16 GENERATORS CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
Printed Tped Name -z Si naturŁ
Month bay Year
17 Transporter Acknowledgement of Receipt of Materials
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19 Discrepancy Indication Space
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17 Transporter Acknowledgement of Receipt of Materials
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18 Transporter Acknowledgement of Receipt of Materials
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5105 MOrehead Rd
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11 Waste Shipping Name and Description
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16 GENERATOR CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
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17 Transporter Acknowledgement of Receipt of Materials
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16 GENERATOR CERTIFICATION certify the materials described above on
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Printed Typed Name SgntUe
Month Day Year
17 Transporter cknoWledgement of Receipt of Materials
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17 Transporter Acknowledgement of Receipt of Materials
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16 GENERATOR CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
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19 Discrepancy Indication Space
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5105 Mdrehead Rd
Concord NC 28027
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16 GENERATOR CERTIFICATION certify the materials described above on this manifest are not sublect to federal regulations for rpporting proper disposal of Hazardous Waste
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17 Transporter Acknowledgement 01 Receipt of Materials
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18 Transporter Acknowledgement of Receipt of Materials
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Concord NC 28027
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15 Specil I4andling Instructions and Additional Information
16 GENERATORS CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Haardous Waste
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17 Transporter Acknowledgement of Receipt of Materials
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ConOord NC 28027
11 Waste Shipping Name and Description 12 Containers 13 14
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Mditiônal Decriptions for Materials Listed Above Handlirig Codes for Wastes Listed Above
15 Special Handling Instructions and Additional Information
16 GENERATOR CERTIFICATION certify the materials described above on this manifest are not subect to federal regulations for reporting proper disposal of Hazardous Waste
Printed /Tped Name jgnature Month Day VearA4
17.TranspOrter AcknoIŁdgerneOiof Receipt of Materials
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5105 Morehôacl Rd...Cohcórd NC 28027
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16 GENERATOR CERTIFICATION certify the matenals descnbed above on this manifest are not sublect to federal regulations for reporting proper disposal of Hazardous Waste.Printed./TName .rJ iaturP Month Day Year
17 Transporter Acknowledgement of Receipt of Materials
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18 Transpotter Acknowledgement of Receipt of Materials
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16 GENERATOR CERTIFICATION certuty the materials escrubed above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous WastePrintedTypedName
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17 Transporter Acknowledgement of Receipt of Materials
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18 Transporter Acknowledgement of Recetpf of Materials
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19 Discrepancy Indication Space
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11.Waste Shipping Name and Description 12 Containers 13 14
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16 GENERATOR CERTIFICATION certify the materials described above on this manifest are not sublect to federal regulations for reporting proper disposal of Hazardous Waste
Printed/Typed Name
.JSi9natu 7.7 i.Mocth DaY Year/1 /t4
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19 Discrepancy Indication Space .-
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5105 Morehead Rd
Codcord NC 28027
11 Waste Shipping Name and Description 12 Cpntainers 13 14
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Concord NC 28027 ..
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16 GENERATORS CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
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15 Special Handling Instructions and Additional Information
6.GENERATORS CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
Pnnted Typed Name Signatur Month
17 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name
18 Transporter Acknowledgement of Receipt of Materials
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19 Discrepancy Indication Space
20 Facility Owner or Operator Cerification of receipt of waste materials covered by this manifest except as noted in item 19
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Printed Type Name Signatur d7
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CMS Landfill 704 782-2004
5105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Description 12 Containers 13 14
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Printed /Typed Name Month Day Year
17 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name Sl9nature/Monih Day Year
18 Transporter Acknowledgement of Receipt of Materials
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Concord NC 28027
11 Waste Shipping Name and Description
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15 SpeciaL Handling Instructions and Additional Information
16 GENERATORS CERTlFICATION certify the materials described above on this manifest are not subiect to federal regulations for reporting proper disposal of Hazardous Waste
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Concord NC 28027
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15 Special Handling Instructions and Additional Information
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nature7 Month Day year
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ALLE WASTEINDUSTRIESINC //f/jNON-HAZARDOUS 1.GeneratorsUS EPAlD No.Manifest.2PagŁWASTEMANIFESTDocumentNoof 127816
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11 Waste Shipping Name and Description 12 Containers 13 14
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16 GENERATOR CERTIFICATION certify the materials described above on this manifest are not sublect to federal regulations
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16 GENERATOR CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
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11 Waste Shipping Name nd Description
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15 Special Handling Instructions and Additional Information
16 GENERATOR CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
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Concord NC 28027
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Concord NC 28027
11 Waste Shipping Name and Description
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704 782-2004
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16 GENERATORS CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
Printed Typed Name
Day
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T/SIDIF/.CQpY
APPENDIX
SITE PHOTOGRAPHS
APPENDIX
ESPS SOP
STANbARb OPERATING PROCEbURE
SOP-6
SOIL SAMPLE COLLECTION
ESP Associates P.A Revision bate 3/7/06
This standard operating procedure SOP covers the collection of soil sample for
laboratory analysis
Follow these steps when collecting the soil sample unless
otherwise instructed by the project manager
Gather needed field supplies noted below
Confirm lab cooler contains needed sample containers fill cooler with
ice
Upon arriving at site check in with the property owner or company
representative
becontaminate the stainless steel hand auger before and between sample
collection by washing with Alconox soap and scrub brush rinsing with
distilled water and spraying with Isopropyl alcohol Wrap clean sampler
in aluminum foil
Wear disposal latex or nitrile gloves and change into new pair between
samples
buring advancement of the hand auger collect soil samples at regular
intervals for describing lithology Note lithology and other
characteristics of soils in field book relative to depth
If appropriate place representative portion of soil sample into
resealable plastic bag label with boring number and depth interval and
allow to equilibrate Screen soil in bag for volatile organics using
an OVA
or Hnu Enter results into field book
Advance hand auger boring to previously specified sampling depth
Collect soil sample from this depth and place in laboratory provided
containers Label containers with boring number and sample depth using
the following sampling scheme i.e B-i ft B-i 10 ft B-2 ft etc
Denote boring location in field book relevant to pertinent site features
10 Following collection of the soil samples abandon all boreholes feet or
greater in depth with cement grout
11 Complete and sign the labs chain-of-custody
12 Keep the sample cooler in secure location until delivered under normal
chain-of-custody procedures to laboratory
SOP-6 Soil Sample Collection levision bate 3/7/06
ESP Associates Page of
SUPPLIES
SOP-6
Stainless steel hand auger with needed extensions or sampling
spoon
OVA or Hnu
Measuring tape
Plastic zip-lock bags
Isopropyl alcohol
bistilled water
5-gallon wash bucket scrub brush and Alconox soap
Cement with wheel barrow for mixing
Cooler with sample containers and chain-of-custody
Ice
Permanent marker
bisposable gloves
Knife
Field book
Site plan with site specific sampling instructions
Camera
APPENDIX
PRISM LABORATORY DATA REPORTS
PRISM
LABORATORIESINC
Date 06/25/07
Company ESP Associates PA
Contact Chris Ward
Address Box 7030
Charlotte NC 28241
Client Project ID
Prism COC Group No
Collection Dates
Lab Submittal Dates
Case Narrative
Morehead Commons No
G0607392
06113/07
06/13107
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report
and Quality
Control Data totaling 44 pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are induded in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
No Anomalies Reported
Metals Analysis
N/A
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by Paula Gilleland Project Manager
Signature ....A ii2t k_Signature
Review Date 06/25/07
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect Is present
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories Inc The results in this
report relate only to the samples submitted for analysis
449 Sptingbrook Road P.O Box 240543 Charlotte NC 2B224-0403
Phone 704/529 6364 ToIl Free 800/529.6364 Fax 704/525-0409
Approval Date 06/25/07
Percent Solids Determination
Percent Solids
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Sample Weight Determination
Weight BisulIate
Weight Bisulfate
Weight Methanol
StvkeAnycI EnvIrannrn
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/25/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-1
l84315
G0607392
06/13/07 1330
06/13/07 1545
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
90.5 SM2540 06118/07 1700 brown
brown
brown
brown
6.19 5035 06/18/07 000
5.65 5035 06/18/07 000
7.05 5035 06/18/07 000
Volatile Organic Compounds by GC/MS
11 1-Trichloroethane BRL mg/kg 0.0049 0.00027 8260B 06/15/07 1728 enissI Q24312
1.1 .22-Tetrachloroethane BRL mg/kg 0.0049 0.0005 8260B 06/15/07 1728 erussell 024312
112-Trichloroethane BRL mg/kg 0.0049 0.0003 8260B 06/15/07 1728 erusset 024312
tI-Dichioroethane BRL mg/kg 0.0049 0.00035 8260B 06/15/07 1728 erussell 024312
11-Dichloroethene BRL mg/kg 0.0049 0.00037 82608 06/15/07 1728 erussell 024312
11-Dichloropropene BRL mg/kg 0.0049 0.00043 82608 06/15/07 1728 erussell 024312
123-Trichlorobenzene BRL mg/kg 0.0049 0.00054 8260B 06/15/07 1728 erusset 024312
23-Tichloropropane BRL mg/kg 0.0049 0.00043 8260B 06/15/07 1728 erussell 024312
12.4-Trichlorobenzene BRL mg/kg 0.0049 0.00047 8260B 06/15/07 1728 erussell Q24312
24-Trimethylbenzene BRL mg/kg 0.0049 0.00037 82608 06/15/07 1728 erussell 024312
.2-Dibromoethane EDB BRL mg/kg 0.0049 0.000088 8260B 06/15/07 1728 erusset 024312
2-Dichlorobenzene BRL mg/kg 0.0049 0.00026 8260B 06/15/07 1728 erussell 024312
2-Dichloroethana BRL mg/kg 0.0049 0.00049 8260B 06/15/07 1728 erussell 024312
2-Dichloropropane BRL mg/kg 0.0049 0.00036 8260B 06/15/07 1728 erussell 024312
35-Trimethylbenzerie BRL mg/kg 0.0049 0.00041 8260B 06/15/07 1728 erussefl 024312
13-Dichlorobenzene BRL mg/kg 0.0049 0.00042 8260B 06/15107 1728 erussell 024312
13-Dichloropropane BRL mg/kg 0.0049 0.00033 82608 06/15/07 1728 erussell 024312
4-Dichlorobenzene BRL mg/kg 0.0049 0.00038 8260B 06/15107 1728 erussefl 024312
22-Dichloropropane BRL mg/kg 0.0049 0.00024 8260B 06115/07 1728 erussell 024312
2-Chiorotoluene BRL mg/kg 0.0049 0.00036 8260B 06/15/07 1728 enissell 024312
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/525364 Toll Free Number 1-800529-664 Fax 7041525-0409 Pagelof3s
F..5ervce AI.......nvIonmna SOIutIor%s
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix SOil COC Group
Time Collected
Time Submitted
WS-1
184315
G0607392
06/13/07 1330
06/13/07 1545
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 7041525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
2-Hexanone BRL mg/kg 0.049 0.00051 8260B 06/15/07 1728 erusseR Q24312
4-Chlorotoluene BRL mg/kg 0.0049 0.00025 826GB 06115/07 1728 erussell 024312
.-4-Methyl-2-pentanone MISK BRL mg/kg 0.049 0.00049 826GB 06/15/07 1728 erussell 024312
Acetone BRL mg/kg 0.049 0.0019 8260B 06/15/07 1728 erussefl Q24312
Benzene BRL mg/kg 0.0029 0.00039 8260B 06/15/07 1728 mussell 024312
Bromobenzene BRL mg/kg 0.0049 0.00034 826GB 06/15/07 1728 erusseil 024312
Bromochioromethane BRL mg/kg 0.0049 0.00029 826GB 06/15/07 1728 erussell 024312
Bromodichioromethane BRL mg/kg 0.0049 0.00043 826GB 06I15/07 1728 erussell 024312
Bromoforrn BRL mg/kg 0.0049 0.00036 826GB 06/15/07 1728 erussell 024312
Bromomethane BRL mg/kg 0.0098 0.00057 826GB 06/15/07 1728 erussell Q2431
Carbon tetrachloride BRL mg/kg 0.0049 0.00028 826GB 06/15/07 1728 erussell 024312
Chloroberizene BRL mg/kg 0.0049 0.00037 826GB 06/15/07 1728 erussell 024312
Chiorodlbromomethane BRL mg/kg 0.0049 0.00033 826GB 06/15/07 1728 erussell 024312
Chioroethane BRL mgfkg 0.0098 0.0004 8260B 06/15/07 1728 erussell 024312
Chloroform BRL mg/kg 0.0049 0.00036 626GB 06/15/07 1728 erussell 024312
Chloromethane BRL mg/kg 0.0049 0.00034 826GB 06/15/07 1728 erussell 024312
cis-12-Dichloroethene BRL mg/kg 0.0049 0.00022 826GB 06/15/07 1728 ewesell 024312
cis-13-Dichloropropene BRL mg/kg 0.0049 0.00031 82608 06/15/07 1728 erusseli 024312
Dichlorodifluoromethane BRL mg/kg 0.0049 0.0011 826GB 06/15/07 1728 erussell 024312
Ethylbenzene BRL mg/kg 0.0049 0.00034 826DB 06/15/07 1728 erussell Q24312
Isopropyl ether IPE BRL mg/kg 00049 0.00017 8260B 06/15/07 1728 erussell 024312
lsopropylbenzene BRL mg/kg 0.0049 0.00039 826GB 06/15/07 1728 enissell 024312
mp-Xylenes BRL mg/kg 0.0098 0.00068 826GB 06115/07 1728 enissell 024312
Methyl ethyl ketone MEK BRL mg/kg 0.098 0.0014 826GB 06/15/07 1728 erussell Q24312
Methyl t-butyl ether MTBE BRL mg/kg 0.0098 0.00028 826GB 06/15/07 1728 erussell 024312
Methylene chloride BRL mg/kg 0.0049 0.0004 826GB 06/15/07 1728 erussell 024312
n-Butylbenzene BRL mg/kg 0.0049 0.00039 8260B 06/15/07 1728 erussell 024312
Page of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06125107
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-1
184315
G0607392
06/13/07 1330
06113/07 1545
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
0.0049 0.00029 826DB 06/15/07 1728 erussell 024312
0.0098 0.00057 8260B 06/15107 1726 erussell 024312
0.0049 0.00029 8260B 06/15/07 1728 erussell 024312
0.0049 0.0004 826DB 06/15/07 1728 erussell 024312
0.0049 0.00032 826DB 06/15/07 1728 ewesell 024312
0.0049 0.00049 826DB 06/15/07 1728 erussell Q24312
0.0049 0.0003 826DB 06/15/07 1728 erussell Q24312
0.0049 0.00084 826DB 06/15/07 1728 enissell 024312
0.0049 0.00033 826DB 06/15/07 1728 erussell 024312
0.0049 0.00037 8260B 06/15/07 1728 erussell 024312
0.0049 0.00034 826DB 06/15/07 1728 enissell 024312
0.0049 0.00029 8260B 06/15/07 1728 erussell 024312
0.0049 0.0004 826DB 06/15/07 1728 erussell 024312
0.024 0.0018 826DB 06/15/07 1728 erussell 024312
0.0049 000063 82609 06/15/07 1728 ensseiI 024312
n-Propylbenzene BRL
Naphthalene BRL
o-Xylene BRL
p-lsopropyltoluene BRL
sec-Butylbenzene BRL
Styrene BRL
tert-Butylbenzene BRL
Tetrachloroethene BRL
Toluene BRL
trans-I 2-Dichloroethene BRL
trans-I 3-Dichloropropene BRL
Trlchloroethene BRL
Trichlorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Compounds by CC/MS
24-Trichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
2.45-Trichiorophenol BRL
246-Trithlorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Bromofluorobenzene 100 77-128
Dibromofluoromethane 106 67 143
Toluene-d8 98 81 128
0.36
0.36
0.36
0.36
0.36
0.36
0.036
0.027
DM26
0.033
0.037
0.035
82700
82700
827CC
8270C
8270C
82700
06/18/07 1309 kcarnplgotlo
06/18/07 1309 kcampigOttO
06/18/07 1309 kcampigotlo
06/18/07 1309 kcampigotto
06/18/07 1309 kcampigotto
06/18/07 1309 kcampigotto
024348
024348
024348
024348
024348
024348
This report shoud not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-6364 Toll Free Number 1-800/529-6364 Fax 7041525-0409 Page of 35
ESP Associates PA
Attn Chris Ward
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Parameter
24-IDichlorophenol
24-Dimethyiphenol
24-Dinitrophenol
24-Dinitrotoluene
26-Dinitrotoluene
2-Chloronaphthalene
2-Chiorophenol
2-Methylnaphthalene
2-Methyiphenol
2-Nitropherol
34MethylphenoI
33-Dichloroberizidine
46-Dinitro-2-methylphenol
4-Bromophenyiphenylether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyiphenylettier
4-Nitrophenol
Acenaphthene
Acenaphthylene
Arithracene
Azobenzene
Benzoeanthracerie
Benzoapyrene
Benzobfluoranthene
Benzog.hiperylene
Benzokfiuoranthene
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kvarnpigotto Q24348
06118/07 1309 kcampigotto 024348
06/18/07 1309 kcampigotto 024348
06116/07 1309 kcampgotto 024348
06/18/07 1309 kcampigotto Q24348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcanpigotto 024348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcampigolto 024348
06/18/07 1309 kcampiotto 024348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 koampigotto 024348
06/18/07 1309 koampigotto Q2434a
06/18/07 1309 kcampigotto Q24348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcampigotto 024348
06/18/07 1309 kcampigotto 024348
8270C 06/18/07 1309 kcampigotto 024346
8270C 06118/07 1309 kcampigotto Q24348
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 184315
Sample Matrix Soil COG Group G0607392
Time Collected 06/13/07 1330
Time Submitted 06/13/07 1545
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
BRL mg/kg 0.36 0.031 827CC
BRL mg/kg 0.36 0.035 827CC
BRL mg/kg 1.8 0.041 827CC
BRL mg/kg 0.36 0.021 827CC
BRL mg/kg 0.36 0.039 827CC
BRL mg/kg 036 0.038 8270C
BRL mg/kg 0.36 0.029 827CC
BRL mg/kg 0.36 0.029 827CC
BRL mg/kg 0.36 0.034 8270C
BRL mg/kg 0.36 0.044 827CC
BRL mg/kg 0.36 0.037 8270C
BRL mg/kg 0.73 0.023 8270C
BRL mg/kg 1.8 0.022 827CC
BRI mg/kg 0.36 0.035 827CC
BRL mg/kg 0.73 0.027 827CC
BRL mg/kg 0.36 0.047 827CC
BRL mg/kg 0.36 0.023 627CC
BRL mg/kg 1.8 0.024 82700
BRL mg/kg 0.36 0.036 82700
BRL mg/kg 0.38 0.036 8270C
BRL mg/kg 0.36 0.028 82700
BRL mg/kg 18 0.034 82700
BRL mg/kg 0.36 0.051 8270C
BRL mg/kg 0.36 0.042 827CC
BRL mg/kg 0.36 0.016 8270C
BRL mg/kg 0.36 0.017
BRL mg/kg 0.36 0.030
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1400/529-6364 Fax 704/525-0409 Page of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
FuU $BrYlcs Aualytkul vtrnmntat S01ut011
ESP Associates PA Project ID
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/25/07
Morehead Commons No GIiet Sample ID WS-1
Prism Sample ID 184315
COG Group 00607392
Time Collected 06/13/07 1330
Time Submitted 06/13/07 1545
This report should not be reproduced except in its entirety without the written consent of Piisrn Laboratories Inc
449 Spring brook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
Sample Matrix Soil
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
1.8 0.15BenzoicacidBRLmg/kg 827CC 06/18/07 1309 kcampigotto 024348
Benzyl alcohol BRL mg/kg 0.73 0.038 827CC 06/18/07 1309 kampigotto Q24348
Bis2-chloroethoxymethane BRL mg/kg 0.36 0.042 827CC 06/18/07 1309 kcampigotto 024348
Bis2-chloroethylether BRL mg/kg 0.36 0.040 8270C 06/18/07 1309 kcampigotto 024348
Bis2-chloroisopropylether BRL mg/kg 0.36 0.031 8270C 06/18/07 1309 kcampigotto 024348
Bis2-ethylhexylphthalate BRL mg/kg 0.36 0.018 8270C 06/18/07 1309 koampigotto 024343
Butylbenzylphthalate BRL mg/kg 0.36 0.022 827CC 06/18/07 1309 kcampigotto 024348
Chrysene BRL mg/kg 0.36 0.061 827CC 06/18/07 1309 kcampigotto 024348
Di-n-butylphthalate BRL mg/kg 0.36 0.017 827CC 08/18/07 1309 kcampigotto 024348
Di-n-octylphthalate BRL mg/kg 0.36 0.027 827CC 06/18/07 1309 kcampigotto 024348
Dibenzoahanthracene BRL mg/kg 0.36 0.037 827CC 06118/07 1309 kcampigotto 024348
Dibenzofuran BRL mg/kg 0.36 0.031 3270C 06/18/07 1309 kcampigotto 024348
Diethylphthalate BRL mg/kg 0.36 0.022 827CC 06/18/07 1309 kcampigolto 024348
Dimethylphthalate BRL mg/kg 0.36 0.025 827CC 06/18/07 1309 kcampigotto 024348
Fluorantherie BRL mg/kg 0.36 0.025 827CC 06118/07 1309 kcampigotto 024348
Fluorene BRL mg/kg 0.36 0.022 827CC 06/18/07 1309 kcampi9otto Q24348
Hexachlorobenzene BRL mg/kg 0.36 0.019 827CC 06/18/07 1309 kcampigotto 024348
Hexachiorobutadiene BRL mg/kg 0.36 0.035 827CC 06/18/07 1309 kcampigofto 024348
Hexachlorocyclopentadiene BRL mg/kg 0.36 0.039 827CC 06/18/07 1309 kcampigotto 024348
Hexachioroethane BRL mg/kg 0.36 0.037 827CC 06/18/07 1309 kcampigotto 024348
Indeno123-cdpyrene BRL mg/kg 0.36 0.037 827CC 06/18/07 1309 kcampigotto 024343
Isophororie BRL mg/kg 0.38 0.033 827CC 06/18/07 1309 kcampigotto Q24343
N-Nitrosodi-n-propylamine BRL mg/kg 0.36 0.041 827CC 06/18/07 1309 keampigotto 024348
N-Nitrosodiphenylamine BRL mg/kg 0.36 0.019 827CC 06/18/07 1309 kcampigotto 024343
Naphthalene BRL mg/kg 0.36 0.040 827CC 06/18/07 1309 kcampigotto 024348
Nitrobenzene BRL mg/kg 0.36 0.035 827CC 06/18/07 1309 kcampigotto 024348
Pentachlorophenol BRL mg/kg 1.8 0.031 8270C 06/18/07 1309 kcamplgotto 024348
Page of 35
ESP Associates PA
Attri Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
WS-1
184315
00607392
06/1 3/07 1330
06/13/07 1545
Extractable Petroleum Hydrocarbons by GC-FID
Cl 1-C22 Aromatics BRL mg/kg
C19-C36Aliphatics BRL mg/kg
C9.C18 Aliphatics BRL mg/kg
analysis Note for CllC22 Aromatics
Sample Preparation
MDL
erylce Arcelydcel Enonrrcenel
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report
Limit
Phenanthrene BRL mg/kg 0.36 0.018
Phenol BRL mg/kg 0.36 0.040
Pyrene BRL mg/kg 0.36 0.025
Method
Sample Preparation
Dilution
Factor
Analyst
8270C
8270C
8270C
Analysis
Date/Time
06/18/07 1309 kc.ampigotto
06118/07 1309 keampigotto
06/18/07 1309 koampigotto
Batch
ID
024348
Q24348
Q24348
29.98 mL 355DB 06115/07 900 dpope P1 8642
Surrogate Recovery Control Limits
Nitrobenzene-d5 88 14-103
Phenol-d5 85 13-95
Terphenyl-d14 101 41 136
246-Tribromophenol 113 25-123
2-Fluorobiphenyl 91 21 108
2-Fluorophenol 89 14 89
MADEP EPH
MADEP EPH
MADEP EPH
11 5.7
11 1.6
11 3.4
Adjusted value
1O.5g 2mL
06/20/07
06/2007
06/20/07
2228 grappaccioli
2228 grappaccioli
2228 grappaccioli
024425
024425
024425
P1 8669EPH06/19/07 1000 jvogel
Surrogate Recovery Control Limits
1-Chloro-octadecane 104 40-140
2-Bromonaphthalene 110 40-140
2-Fluoroblphenyl 117 40-140
o-Terpheriyl 101 40-140
Volatile Petroleum Hydrocarbons by GC-PIDIFID
CS-Ca Aliphatics BRL
C9-Cl0Aromatics BRL
C9-C12 Aliphatics BRL
mg/kg
mg/kg
mglkg
5.5 1.1
5.5 0.033
5.5 1.7
MADEPVPH
MADEPVPI-1
MADEPVPH
06/21/07 032 hwagner
06/2107 032 hwagner
06/21/07 032 hwagner
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
Q24410
Q2441
024410
Page of 35
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 124 70-130
25-Dibromotoluene-PID 101 70-130
Sample Weight Determination
Weight 14.85 MADEP VPH 06/18/07 000 thrown
Weight 16.34 MADEP VPH 06/18/07 000 thrown
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Sevk AiatJI Environmnta Soh5on
Laboratory Report
06 /25107
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-1
Attn Chris Ward Prism Sample ID 184315
Box 7030 Sample Matrix Soil COC Group G0607392
Charlotte NC 28241 Time Collected 06/13/07 1330
Time Submitted 06/13/07 1545
Angela Overcash V.P Laboratory Services
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of 35
Percent Solids Determination
Percent Solids
NC CertificaUon No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06 /25107
WS-2
184316
G0607392
06/13/07
06113107
1345
1545
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
86.8 SM2540 06/18/07 1700 lbrown
5.12
7.16
5.23
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Volatile Organic Compounds by GC/MS
11 -Trichloroethane
11 22-Tetrachloroethane
11 2-Trichloroethane
1-Dichloroethane
1-Dichioroethene
11 -Dichloropropene
23-Trichlorobenzene
23-Trichloropropane
.24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichlorobenzene
22-Dichioropropane
2-Chlorotoluene
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
mg/kg 0.0040
5035
5035
5035
8260B
8260B
82608
82608
8260B
8260B
8260B
8260B
8260B
8260B
8260B
82608
8260B
8260B
8260B
8260B
82608
8260B
8260B
8260B
06/18/07 000
06/18/07 000
06/18/07 000
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15/07 1811
06/15107 1811
06/15/07 1811
06/15/07 1811
06115/07 1811
06/15/07 1811
0.00023
0.00041
0.00025
0.00029
0.00031
0.00035
000044
0.00035
0.00039
0.00031
0.000072
0.00022
0.0004
0.0003
0.00034
0.00035
0.00027
0.00031
0.0002
0.0003
Ibrown
Ibrown
Ibrown
ensselI
enssel
erussefl
en.jssell
enissell
erussell
enissefl
erussell
erusselJ
erussell
erussel
erusse
enjssefl
ewssefl
erussell
erussell
erussell
erussoll
erussel
erussell
024312
024312
024312
024312
024312
024312
024312
024312
024312
Q2431
024312
024312
024312
024312
024312
024312
024312
Q24312
024312
024312
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax 7041525-0409 Page 8of35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-8364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/25/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COO Group
Time Collected
Time Submitted
WS-2
184316
G0607392
06/13/07 1345
06/13/07 1545
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0040 0.00042 8260B 06/15/07 1811 erussell 024312
4-Chlorotoluene BRL mg/kg 0.0040 0.00021 826DB 06/15/07 1811 erussell 024312
4-Methyl-2-pentanone MIBK BRL mg/kg 0.040 0.0004 826DB 06/15/07 1811 erussell 024312
Acetone BRL mg/kg 0.040 0.0016 826DB 06/15/07 1811 erussell 024312
Benzene BRL mg/kg 0.0024 0.00032 8260B 06115/07 1811 erussell 024312
Bromobenzene BRL mg/kg 0.0040 0.00028 826DB 06/15/07 1811 erussetl Q24312
Bromochloromethane BRL mg/kg 0.0040 0.00024 826DB 06/15/07 181 erussell 024312
Bromodichioromethane BRL mg/kg 0.0040 0.00035 8260B 06/15/07 1811 erussell 024312
Bromofomi BRL mg/kg 0.0040 0.0003 826DB 06/15/07 1811 erussell 024312
Bromomethane BRL mg/kg 0.0080 0.00047 826DB 06/15/07 1811 erussell 024312
Carbon tetrachloride BRL mg/kg 0.0040 0.00023 8260B 06/15/07 1811 erussefl 024312
Chlorobenzene BRL mg/kg 0.0040 0.00031 826DB 08/15/07 1811 erussell Q24312
Chiorodibromomethane BRL mg/kg 0.0040 0.00027 826DB 06/15/07 1811 erussell Q2431
Chioroethane BRL mg/kg 0.0080 0.00033 82608 06/15/07 1811 erussell Q24312
Chloroform BRL mg/kg 0.0040 0.0003 826DB 06/15/07 1811 erussell Q24312
Chioromethane BRL mg/kg 0.0040 0.00028 82609 06/15/07 1811 erussell 024312
dc-i 2-Dichloroetherie BRL mg/kg 0.0040 0.00018 8260B 06/15/07 1811 erussell Q24312
cis-1 3-Dichloropropene BRL mg/kg 0.0040 0.00026 826DB 06/15/07 1811 erussell Q24312
Dichlorodifluorametharre BRL mg/kg 0.0040 0.0009 82608 06/15/07 1811 erussell Q24312
Ethylbenzene BRL mg/kg 0.0040 0.00028 82609 06/15/07 1811 erussell Q24312
Isopropyl ether IPE BRL mg/kg 0.0040 0.00014 826DB 06/15107 1811 erussell Q24312
lsopropylbenzene BRL mg/kg 0.0040 0.00032 826DB 08/15/07 1811 erussel Q24312
mp-Xylenes BRL mg/kg 0.0080 0.00056 826DB 06/15/07 1811 erussell Q24312
Methyl ethyl ketone MEK BRL mg/kg 0.080 0.0011 826DB 06/15/07 1811 erussell 024312
Methyl t-butyl ether MIBE BRL mg/kg 0.0080 0.00023 8260B 06/15/07 1811 erussell 024312
Methylerre chloride BRL mg/kg 00040 0.00033 826DB 06/15/07 1811 erussell 024312
n-Butylbenzene BRL mg/kg 0.0040 0.00032 826DB 06116/07 1811 erussell 024312
Page of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/25/07
WS-2
184316
G0607392
06/13/07 1345
06/13/07 1545
Semi-volatile Organic Compounds by GCMS
124-Trichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzeno BRL
4-Dichlorobenzene BRL
245-Trichiorophenol BRL
246-Trichiorophenol BRL
Furl Sric AnIytfcaI Envroimental SoI
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Date/Time lID
n-Propylbenzene
Naphthalene
o-Xylene
p-lsopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachioroethene
Toluene
trans-i 2-Dichloroethene
trans-i3-Dichoropropene
Trichioroethene
Trichiorofluoromethane
Vinyl acetate
Vinyl chloride
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Limit Factor
0.0040 0.00024
826GB 06/15/07 1811 erussell 024312
0.0080 0.00047 826GB 06/15/07 1811 erussell 024312
0.0040 0.00024 826GB 06/15107 1811 ecussell 024312
0.0040 0.00033 826GB 06115107 1811 erussell 024312
0.0040 0.00027 826GB 06/15107 1811 erusseli 024312
0.0040 0.0004 826GB 06/15/07 1811 erussell 024312
0.0040 000025 826GB 06115/07 1811 erussell 024312
0.0040 0.00069 626GB 06115107 1811 erussell 024312
0.0040 0.00027 626GB 06/15/07 1811 erussell Q24312
0.0040 0.00031 82606 06/15/07 1811 erussell 024312
0.0040 0.00028 626GB 06/15/07 1811 erussell 024312
0.0040 0.00024 826GB 06/15/07 1811 erusseI Q24312
0.0040 0.00033 8260B 06/15/07 1811 erussell 024312
0.020 0.0015 8260B 06/15107 1811 erussell 024312
0.0040 0.00051 8260B 06/15/07 1811 erussefl Q24312
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Bromofluorobenzene 115 77-128
Dibromofluoromethane 104 67-143
Toluene-d8 98 81 128
0.38
0.38
0.38
0.38
0.38
0.38
0038
0.028
0.028
0.034
0.039
0.037
82700
82700
8270C
8270C
8270C
8270C
06/18/07 1628 kcampFgotto
06/18/07 1628 kcampigotto
06/18/07 1628 kcampigotto
06/18/07 1628 kcampigotto
08/18/07 1628 kcampigotto
06/18/07 1628 keampigotto
024348
024348
024348
024348
024348
024348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 10 of 35
ESP Associates PA
Attn Chris Ward
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24-Dichlorophenol
24-Dimethylphenol
24-Dinitrophenol
24-Dinitrotoluene
26-Dinitrotoluerie
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthaiene
2-Methyiphenol
2-Nitrophenol
34-Methylphenol
33-Dichlorobenzidine
46-Dinitro-2-methylphenol
4-Bromophenylphenylether
4-Chloro-3-methylphenol
4-Chloroanilirie
4-Chlorophenylphenyether
4-Nitrophenol
Aceriaphthene
Acenaphthylene
Anthracene
Pzobenzene
Benzoaanthracerie
Benzoapyrene
Benzobfluoranthene
Benzoghiperylene
Benzokftuoranthene
Result Units Report MDL Dilution Method
Limit Factor
BRL mg/kg 0.38 0.032
BRL mg/kg 0.38 0.037
BRL mg/kg 1.9 0.043
BRL mg/kg 0.38 0.022
BRL mg/kg 0.38 0.040
BRL mg/kg 0.38 0.039
BRL mg/kg 0.38 0.030
BRL mg/kg 0.38 0.030
BRL mg/kg 0.38 0.036
BRL mg/kg 0.38 0.046
BRL mg/kg 0.38 0.039
BRL mg/kg 0.76 0.024
BRL mg/kg 1.9 0.023
BRL mg/kg 0.38 0.036
BRL mg/kg 0.76 0.028
BRL mg/kg 0.38 0.049
BRL mg/kg 038 0.024
BRL mg/kg 1.9 0.025
BRL mg/kg 0.38 0.037
BRL mg/kg 0.38 0.038
BRL mg/kg 0.38 0.029
BRL mg/kg 1.9 0.035
BRL mg/kg 0.38 0.053
BRL mg/kg 0.38 0.044
BRL mg/kg 0.38 0.017
BRL mg/kg 0.38 0.018
BRL mg/kg 0.38 0.031
Analysis Analyst
Batch
Date/Time ID
06/18/07 1628 kcampigotto 024348
06/18/07 1628 kcampigOtto Q24348
06/18/07 1628 kcampigotto Q24348
06/18/07 1628 kcarnplgotto Q24348
06/18/07 1628 kcampigotto 024348
06/18/07 1628 kampigotto 024348
06/18/07 1628 kcampigotto 024348
06/18/07 1628 kcampigotto Q24348
06/18/07 1628 kcampigotto 024348
06/18/07 1628 kcampigotlo Q24348
06/18/07 1628 kcampigotto 024348
06/18/07 1628 kcampigotto 024348
06/18/07 1628 kcarnpigotto 024348
06/18/07 1628 kcampigotto 024348
06118/07 1628 kcampigotto 024348
06/18/07 1628 kearnpigotto 024348
06/18/07 1628 kcampigotto Q24348
06/18/07 1628 kcamplgotto Q24348
06/18/07 1628 kcampigotto 024348
06118/07 1628 kcampigotto 024348
06/18/07 1628 kcampigotto 024348
06/18/07 1628 kcampigotto 024348
06/18/07 1628 kcampigotto 024348
06/18107 1628 kcampigotto 024346
06/18107 1628 kcampigotto 024348
06/18/07 1628 kcampigotto 024348
06/18/07 1628 kcarnpigotto 024348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springb rook Road P.O Box 240543 Charlotte NC 28224.0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
FIII SeMca Analytical EnvlnnnnlaISoIaUnna
NC Certification No 402
SC Certification No.99012
NC Drinking Water Cart No 37735
Laboratory Report
08/25/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 184316
Sample Matrix Soil COC Group G0607392
Time Collected 06/13/07 1345
Time Submitted 06/13/07 1545
Parameter
827CC
827CC
827CC
6270C
827CC
827CC
827CC
8270C
827CC
8270C
8270C
827CC
6270C
827CC
827CC
8270C
827CC
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
Page 11 of35
IuII 2ervkeAiialyUcal Ennmnti $olutkus
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter
Benzoic acid
Benzyl alcohol
Bis2-chloroethoxymethane
Bis2-chloroethylether
Bis2.chloroisopropylether
Bis2-ethylhexylphthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenoahanthracene
Diberizoftiran
Diethylphthalate
Dimethylphthatate
Fluoranthene
Fluorene
l-lexachlorobenzene
Hexachiorobutadiene
Hexachiorocyclopentadiene
Hexachioroethane
lndeno1 23-cdpyrene
Isophorone
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachiorophenol
This report should not be reproduced except in its entirety without the written consent of Piism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-6364 Toil Free Number 1-800/529-6364 Fax 704/525-0409
NC Certification No 402
SC Certification No 90012
NC Drinking Water Cert No 37735
Laboratory Report
06125107
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 184316
Sample Matrix Soil coc Group G0607392
Time Collected 06113/07 1345
Time Submitted 06/13/07 1545
Result Units Report MDL Dilution Method
Limit Factor
Analysis Analyst
Batch
Date/Time ID
BRL mg/kg 1.9 0.16 8270C 06/18107 1625 kcampigotto 024348
BRL mg/kg 0.76 0.040 8270C 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.044 8270C 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.041 8270C 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.033 8270C 06/18/07 1628 kcamplgotto 024348
BRL mg/kg 0.38 0.019 527CC 06/18/07 1628 kcampigotto Q24348
BRL mg/kg 0.38 0.023 827CC 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.063 827CC 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.017 827CC 06118/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.028 8270C 06/18/07 1628 kcamplgotto 024348
BRL mg/kg 0.38 0.038 8270C 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.033 827CC 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.023 827CC 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.026 8270C 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.026 827CC 06/1 8/07 1628 kcarnpigotto 024348
BRL mg/kg 0.38 0.023 8270C 06/18/07 1625 kcampigotto 024348
BRL mg/kg 0.38 0.020 8270C 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.037 827CC 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.040 8270C 06/18/Cl 1628 kcamplgotto 024348
BRL mg/kg 0.38 0.039 8270C 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.030 8270C 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.034 827CC 06118/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.043 827CC 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.019 827CC 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.042 827CC 06/18/07 1628 kcampigotto 024348
BRL mg/kg 0.38 0.037 8270C 06/18/07 1628 kcampigotto 024348
BRL mg/kg 1.9 0.032 821CC 06/18/07 1628 kcampigotto 024348
Page 12 of35
ESP Associates PA
Attn Chris Ward
Box 7030
CharIotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
184316
G0607392
06113107
06/13/07
Sample Preparation 29.91 mL 3550B 06/15/07 900 dpope P18642
Extractable Petroleum Hydrocarbons by GC-FID
Cl 1-C22 Aromatics BRL mg/kg
C19-C36Allphatics BRL mg/kg
C9-C18 Aliphatics BRL mg/kg
Analysis Note for Cll-C22 Aromatics
Sample Preparation
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Parameter Result Units
1345
1545
MDL
Phenanthrene BRL mg/kg
Phenol BRL mg/kg
Pyrene BRL mg/kg
MethodReport
Limit
0.38
0.38
0.38
Dilution
Factor
Analyst
0.019
0.042
0.026
8270C
8270C
8270C
Analysis
Date/Time
06/18107 1628 kcampigotto
06/18/07 1628 koampigotto
06/18/07 1628 kcampigottO
Batch
ID
024345
024348
024348
Surrogate Recovery Control Limits
246-Tribromophenol 109 25-123
2-Fluorobiphenyl 92 21 108
2-Fluorophenol 82 14-89
Nitrobenzene-d5 84 14-103
Phenol-d5 76 13-95
Terphenyl-d14 106 41 136
11 6.1 MADEP EPH
06/21/07 012 grappacclot Q24425
11 1.7 MADEP EPH 06121/07 012 grappaccioli 024425
11 3.6 MADEP EPH 06/21/07 012 grappaccioli 024425
Adjusted value
10.16 mL EPH 06/19/07 1000 ivogel P18669
Surrogate Recovery Control Limits
1-Chloro-octadecane 117 40-140
2-Bromonaphthalene 107 40-140
2-Fluorobiphenyl 110 40-140
o-Terphenyl 98 40-140
Volatile Petroleum Hydrocarbons by GC-PID/FID
C5-C8Aliphatics BRL mg/kg 5.8 1.1 MADEPVPH 06121107 114 hwagner 024410
C9-Cl0Aromatics BRL mg/kg 5.8 0.035 MADEPVPH 06/21/07 114 hwagner 024410
C9-C12 AliphaUcs BRL mg/kg 5.8 1.8 MADEP VPH 06/2107 114 hwagner 024410
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 13 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Analysis Note for C5C8 Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
One surrogate recovery
was outside the control limits No target compounds were detected inthissampleNofurtheractionwastaken
Sample Weight Determination
Weight
Weight
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Umit and the MDL
The results in this reportrelate only to the samples submitted for analysis and meet state certification requirements other thanNELAcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
06/25/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 184316
Sample Matrix Soil coc Group G0607392
Time Collected 06/13107 1345
Time Submitted 06/13/07 1545
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 133 70-130
25-Dibromotoluene-PID 104 70-130
12.07
12.08
MADEP VPR 06/18/07 000 brown
MADEP VPH 06/18/07 000 brown
Angela Overcash V.P Laboratory Services
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409 Page 14 of 35
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
WS-3
184317
G0607392
06/13/07 1400
06113107 1545
Percent Solids Determination
Percent Solids
SamIe Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
Full Srjicu Analytiual Enukonmuriel Salutlonu
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
88.5 SM2540 06/18107 1700 brown
5.90
5.79
5.46
BRL
BRI
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Volatile Organic Comoounds by GCIMS
11-Trichloroethane
11 22-Tetrachloroethane
112-Trichloroethane
1-Dichloroethane
1-Dichloroethene
.1-Dichioropropene
23-Trichlorobenzene
23-Trichloropropane
.24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichioroethane
2-Dichioropropane
36-Trimethylbenzerie
3-Dichlorobenzene
3-Dichioropropare
4-Dichlorobenzene
22-Dicliloropropane
2-Chiorotoiuene
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg O.004
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
mg/kg 0.0049
5035
5035
5035
82608
826DB
82608
8260B
8260B
8260B
826DB
826DB
82606
6260B
826DB
82806
8260B
826DB
82608
626DB
8260B
82608
826DB
82608
06/18/07
06/18/07
06/18/07
06/1 8/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
05/18/07
06/18/07
000
000
000
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
1235
0.00027
0.0005
0.0003
0.00035
0.00037
0.00043
0.00054
0.00043
0.00047
0.00037
0.000088
0.00026
0.00049
0.00036
0.00041
0.00042
0.00033
0.00038
0.00024
0.00036
Ibrown
brown
brown
ewsseli
erussell
erusseil
erusseU
erusseif
erussell
erusseli
erusseli
erussell
ensseii
erusseil
erusseii
erussell
erusseli
erussef
erussef
ewssell
erusseil
erussell
erussell
024312
Q24312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
Q24312
024312
024312
024312
024312
Q24312
024312
Q24312
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Spring brook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax 7041525-0409 Page 15 of35
Project ID Morehead Commons
No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
lime Submitted
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprinybrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert Mo 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/25/0
WS-3
184317
G0607392
06/13/07
06/13/07
Parameter Result Units Report MDL Dilution Method
1400
1545
Analyst Batch
ID
Analysis
Limit Factor Date/Time
2-Hexanone BRI mg/kg 0.049 0.00051 826DB 05/18/07 1235 erussell 024312
4-Chiorotoluene BRL mg/kg 0.0049 0.00025 82609 06/18/07 1235 erusset Q24312
4-Methyl-2-pentanone MIBK BRL mg/kg 0.049 0.00049 826DB 06/18/07 1235 erussell 024312
Acetone BRL mg/kg 0.049 0.0019 826DB 06/18/07 1235 erussell 024312
Benzene BRL mg/kg 0.0029 0.00039 82608 06/18/07 1235 erussell 024312
Bromobenzene BRL mg/kg 0.0049 0.00034 826DB 06/18/07 1235 erussell 024312
Bromochloromethane BRL mg/kg 0.0049 0.00029 8260B 06/18/07 1235 erusselt 024312
Bromodichloromethane BRL mg/kg 0.0049 0.00043 526DB 06/18/07 1235 etussell 024312
Bromoform BRL mg/kg 0.0049 0.00036 826DB 05/18/07 1235 etussell 024312
Bromomethane BRL mg/kg 0.0098 0.00057 826DB 06/18/07 1235 ensselI 024312
Carbon tetrachioride BRL mg/kg 0.0049 0.00028 826DB 06/18/07 1235 etussell 024312
Chlorobenzene BRL mg/kg 0.0049 0.00037 826DB 06/18/07 1235 erusseli 024312
Chiorodibromomethane BRL mg/kg 0.0049 000033 8260B 06/18/07 1235 erussell 024312
Chioroethane BRL mg/kg 0.0098 0.0004 8260B 06/18/07 1235 erussell 024312
Chloroform BRL mg/kg 0.0049 0.00036 8260B 06/18/07 1235 erussell 024312
Chioromethane BRL mg/kg 0.0049 0.00034 826DB 06/18/07 1235 ensseIl 024312
cis-12-Dichloroethene BRL mg/kg 0.0049 0.00021 826DB 06/18/07 1235 ejussell 024312
cis-13-Dichloropropene BRL mg/kg 0.0049 0.00031 8260B 06/18/07 1235 erussetl 024312
Dchlorodifluoromethane BRL mg/kg 0.0049 0.0011 826DB 06/18/07 1235 erussell 024312
Ethylbenzene BRL mg/kg 0.0049 0.00034 826DB 06/18/07 1235 eiJssetl Q24312
Isopropyl etherIPE BRL mg/kg 0.0049 0.00017 8260B 06/18/07 1235 erussell 024312
Isopropylbenzene BRL mg/kg 0.0049 0.00039 826DB 06/18/07 1235 enissell 024312
mp-Xylenes BRL mg/kg 0.0098 0.00068 826DB 06/18/07 1235 erussell 024312
Methyl ethyl ketone MEK BRL mg/kg 0.098 0.00 14 8260B 06/15/07 1235 erussell 024312
Methyl t-butyl ether MTBE BRL mg/kg 0.0098 0.00028 82608 06/18/07 1235 erussell 024312
Methylene chloride BRL mg/kg 0.0049 0.0004 8260B 06/16/07 1235 erusseH 024312
n-Butylbenzene BRL mg/kg 0.0049 0.00039 826DB 06/18/07 1235 erussel 024312
Page 16 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-3
Attn Chris Ward Prism Sample ID 184317
Box 7030 Sample Matrix Soil COC Group G0607392
Charlotte NC 28241 Time Collected 06/13/07 1400
Time Submitted 06/13/07 1545
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
n-Propylbenzene BRL mg/kg 0.0049 0.00029 82608 06/18/07 1235 erus5eII 024312
Naphthalene BRL mg/kg 0.0098 0.00057 82608 06118/07 1235 eruseII 024312
o-Xylene BRL mg/kg 0.0049 0.00029 8260B 06/18/07 1235 erussell 024312
p-Isopropyltoluene BRL mg/kg 0.0049 0.0004 8260B 06/18/07 1235 erussell 024312
sec-Butylbenzene BRL mg/kg 0.0049 0.00032 82608 06/18/07 1235 enissell 024312
Styrene BRL mg/kg 0.0049 0.00049 8260B 06/18/07 1235 erussell Q24312
tert-Butylbenzene BRL mg/kg 0.0049 0.0003 8260B 06/18/07 1235 erussell 024312
Tetrachloroethene BRL mg/kg 0.0049 0.00084 82608 06/18/07 1235 ensselI 024312
Toluene BRL mg/kg 0.0049 0.00033 82606 06/18107 1235 erussell 024312
trans-12-Dichloroethene BRL mg/kg 0.0049 0.00037 82606 06/18107 1235 erussell 024312
trans-13-Dichloropropene BRL mg/kg 0.0049 0.00034 82608 06/18/07 1235 erussell 024312
Trichioroethene BRL mg/kg 0.0049 0.00029 8260B 06/18/07 1235 erusseli 024312
Trichlorofluoromethane BRL mg/kg 0.0049 0.0004 8260B 06/18/07 1235 erussell Q24312
Vinyl acetate BRL mg/kg 0.024 0.0018 82608 06/18/07 1235 erussell Q24312
Vinyl chloride BRL mg/kg 0.0049 0.00062 8260B 06/18/07 1235 erussell 024312
Surrogate Recovery Control Limits
Brornofluorobenzene 104 77-128
Dibromofluoromethane 101 67 143
Toluene-d8 97 81 128
Semi-volatile Organic Compounds by GC/MS
124-Trichlorobenzene BRL mg/kg 0.37 0.037 8270C 06/19/07 1044 kcampigotto Q24348
12-Dichlorobenzene BRL mg/kg 0.37 0.028 8270C 06/19/07 1044 kcampigotto 024348
13-Dichlorobenzene BRL mglkg 0.37 0.027 8270C 06/19/07 1044 kcampigotto 024348
14-Dichlorobenzene BRL mg/kg 0.37 0.034 8270C 06/19/07 1044 kcarnpigotto 024345
245-Trichlorophenol BRL mg/kg 0.37 0.038 8270C 06/19/07 1044 kcampigotto 024348
246-Trichlorophenol BRL mg/kg 0.37 0.036 8270C 06/19/07 1044 kcampigotto 024348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 17 of 35
NC Certification Nc 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Spring brook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-8364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
FIJ Srk AnalyaI EnviromenIai Sht1a
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/25/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-3
184317
G0607392
06/1307 1400
06/13/07 1545
Parameter Result Units Report MDL Dilution Method Analyst Batch
Limit Factor ID
Analysis
DateiTime
24-Dichlorophenol BRL mg/kg 0.37 0.031 8270C 06/19/07 1044 kCampigotlo 024348
24-Dimethylphenol BRL mg/kg 0.37 0.036 8270C 06/19/07 1044 kcampigotto 024348
24-Dinitrophenol BRL mg/kg 1.9 0.042 8270C 06/19/07 1044 kcampigotto 024348
24-Dinitrotoluene BRL mg/kg 0.37 0.021 827CC 06/19/07 1044 kcampigotto 024348
26-Dinitrotoluene BRL mg/kg 0.37 0.040 827CC 06/19/07 1044 kcampigotto 024348
2-Chloronaphthalene BRL mg/kg 0.37 0.039 827CC 06/19/07 1044 kcampigotto 024345
2-Chorophenol BRI mg/kg 0.37 0.029 5270C 06/19/07 1044 kcanipigot 024348
2-Methylnaphthalene BRL mg/kg 0.37 0.030 827CC 06/19/07 1044 kcsmpigotto 024348
2-Methylphenol BRL mg/kg 0.37 0.035 82700 0619/07 1044 kcampigotto 024348
2-Nitrophenol BRL mg/kg 0.37 0.045 8270C 0619/07 1044 kcampigotto 024348
34-Methylphenol BRL mg/kg 0.37 0.038 8270C 06/19/07 1044 kcampigotto 024348
33-Dichlorobenzldine BL mg/kg 0.75 0.023 827CC 06/19/07 1044 kcampigotto 024348
46-Dinitro-2-methylphenol BRL mg/kg 1.9 0.023 82700 06/19/07 1044 kcampigotto 024348
4-Bromophenylphenylether BRL mg/kg 0.37 0.036 8270C 06/19/07 1044 kcampigotto 024345
4-Chloro-3-rnethylphenol BRL mg/kg 0.75 0.027 827CC 06/19/07 1044 kcampigotto 024348
4-Chloroaniline BRL mg/kg 0.37 0.048 8270C 06/19/07 1044 kcampgotto 024348
4-Chlorophenylpheriylether BRL mg/kg 0.37 0.023 8270C 06/19/07 1044 kcanipigotto Q24348
4-Nitrophenol BRL mg/kg 1.9 0.025 8270C 06119/07 1044 kcampigotto 024348
Acenaphthene BRL mg/kg 0.37 0.037 8270C 06119/07 1044 koampigotto 024348
Acenaphthylene BRL mg/kg 0.37 0.037 827CC 06/19/07 1044 kcampigc4to 024348
Anthracene 0.097J mg/kg 0.37 0.028 827CC 06/19/07 1044 kcampgoUo 024348
Azobenzene BRL mg/kg 1.9 0.035 82700 06/19/07 1044 kcampigotto 024348
Benzoaanthracene 0.48 mg/kg 0.37 0.052 8270C 06119/07 1044 kcanipigotto 024348
Benzoapyrene 0.30 mg/kg 0.37 0.043 8270C 06/19/07 1044 kcampigotto Q24348
Benzobfluoranthene 0.37 mg/kg 0.31 0.017 82700 06/19/07 1044 kcampigotto Q24348
Benzoghiperylerie BRL mg/kg 0.37 0.018 827CC 06119/07 1044 kcampigotlo 024348
Benzokfluoranthene 0.26 mg/kg 0.37 0.030 827CC 06/19/07 1044 kcanipigotlo 024348
Page 18 of 35
Service Aibcal ImhtaI .soIttioji
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-3
184317
G0607392
06/13/07 1400
06/13/07 1545
Benzoic acid
Benzyl alcohol
Bis2-chlorcethoxymethane
Bis2-chloroethylether
Bis2-chloroisopropylether
Bis2-ethylhexylphthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Dln-octyIphthaIate
Dibenzoahanthracerie
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthens
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
1-lexachiorocyclopentadiene
Hexachioroethane
lndeno1 23-cdpyrene
leophorone
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
This report should not be reproduced except in its entirely without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Parameter Result Units Report MDL Dilution Method
Limit Factor
AnalystAnalysis Batch
Date/Time ID
BRL mg/kg 1.9 0.16 8270C 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.75 0.039 827CC 06/19/07 1044 kcampigotto 024348
ERL mg/kg 0.37 0.043 527CC 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.041 8270C 06/19/07 1044 kc2nlplgotto 024348
BRL mg/kg 0.37 0.032 8270C 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.018 8270C 06/19/07 1044 keampigotto Q24348
BRL mg/kg 0.37 0.023 827CC 06/19/07 1044 kcampigotto 024348
0.45 mg/kg 0.37 0.062 8270C 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.017 8270C 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.028 8270C 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.038 827CC 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.032 827CC 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.023 827CC 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.026 827CC 06/19/07 1044 kcanipigotto 024348
0.80 mg/kg 0.37 0.026 827CC 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.022 827CC 06/19/07 1044 kcampigotto 024348
RRL mg/kg 0.37 0.019 827CC 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.036 8270C 06/19/07 1044 keampigotto 024348
BRL mg/kg 0.37 0.040 827CC 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.038 827CC 06/19/07 1044 kcampigotto 0.24348
0.24 mg/kg 0.37 0.038 827CC 06/19/07 1044 kcarnpigotto 024348
BRL mg/kg 0.37 0.033 827CC 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.042 8270C 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.019 827CC 06/19/07 1044 kcampigotlo Q24348
BRL mg/kg 0.37 0.041 827CC 06/19/07 1044 kcampigotto 024348
BRL mg/kg 0.37 0.036 827CC 06/19/07 1044 kcampigotto 024348
ERL mg/kg 1.9 0.031 827CC 06/19/07 1044 keampigotto 024348
Page 19 p135
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Sample Preparation 29.88 rnL 3550B 06/15107 900 dpope P18642
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/25/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
WS-3
184317
00607392
06/1 3/07 1400
06/13/07 1545
Parameter Result Units Analyst Batch
ID
MDL
Phenanthrene 0.41 mg/kg
Phenol BRL mg/kg
Pyrene 0.55 mg/kg
MethodReport
Limit
0.37
0.37
0.37
Dilution
Factor
0.018
0.041
0.026
Analysis
Date/Time
06/19/07 1044
06/19/07 1044
06/19/07 1044
8270C
8270C
8270C
kcampigotto
kcampigotto
kcarnpigotto
Q24348
024346
024348
Surrogate Recovery Control Limits
246-Trlbromophenol 120 25-123
2-Fluorobiphenyl 97 21 108
2-Fluorophenol 87 14-89
Nitrobenzene-dS 96 14-103
Phenol-d5 85 13 95
Terphenyl-d14 105 41 136
Extractable Petroleum Hydrocarbons by GC-FID
C11-C22Aromatics BRL mglkg 11 6.1
C19-C36 Aliphatics BRL mg/kg 11 1.7
C9-Cl8Aliphatics 21 mg/kg 11 3.6
Analysis Note for Cll-C22 Aromatics Adjusted value
Sample Preparation 10.08 mL EPH 06/19/07 1000 jvogel
MADEP EPH 06/21/07 156 grappaccioii 024425
MADEP EPH 06/21/07 156 grappaccioli 024425
MADEP EPH 06/21/07 156 grappacdoli 024425
P18669
Surrogate Recovery Control Limits
1-Chloro-octadecane 108 40-140
2-Bromonaphthalene 102 40-140
2-Fluorobiphenyl 101 40 140
o-Terphenyl 99 40-140
Volatile Petroleum Hydrocarbons by GC-PIDIFID
C5-C8Aliphatics BRL mg/kg 5.6 1.1 MADEPVPH 06/21/07 156 hwagner 024410
C9-Cl0Aromatics BRL mg/kg 5.6 0.034 MADEPVPI-06/21/07 156 hwagner 024410
C9C12AJiphatics BRL mg/kg 5.6-1.7 MADEPVPH 06/21/07 156 hwagner 024410
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springb rook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 20 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-3
184317
G0607392
06113107 1400
06113107 1545
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Dateflime ID
Pnalysis Nate for C5-C8 Aliphatics Adjusted value
na1ysia Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 122 70-130
25-Dibromotoluene-PID 100 70-130
Sample Weight Determination
Weight 12.53 MADEP VPH 06/15107 000 Ibrown
Weight 16.01 MADEP VPH 06/18107 000 brown
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments
All results are reported on dr/-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprinybrook Road P.O Box 240543 Charlotte NC 28224-0543
-__
FL dcal Envlronmeiflal StuUons
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax704/525-0409 Page 21 of 35
Percent Solids Determination
Percent Solids
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
ESP Associates PA
Attn Chris Ward
P.O ox 7030
Charlotte NC 28241
Laboratory Report
06/25/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
WS-4
184318
G0607392
06/13107 1415
06/13/07 1545
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
84.6 SM2540 06/18/07 1700 brown
06/18/07 000
06/18/07 000
06/18/07 000
brown
Ibrown
brown
06/18/07 1319 erussell
06/18/07 1319 eiissell
06/18/07 1319 erussell
06/18/07 1319 erussell
06/18/07 1319 ejusselI
5.35
5.33
4.87
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Volatile Organic Compounds by GCIMS
11 1-Tiichtoroethane
11 22-Tetrachloroethane
11 2-Trichloroethane
1-Dichloroethane
1-Dichloroethene
.1-Dichioropropene
23-Trichlorobenzene
.23-Trichioropropane
24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichorobenzene
22-Dichloropropane
2-Chiorotoluene
5035
5035
5035
8260B
826GB
826GB
826GB
826GB
826GB
826GB
826DB
826DB
826GB
826DB
826GB
826DB
826GB
826DB
826GB
826DB
826DB
826DB
8260B
0.0055 0.00031
0.0055 0.00057
0.0055 0.00034
0.0055 0.0004
0.0055 0.00042
0.0055 0.00G49
0.0055 0.00061
0.0055 0.00049
00055 0.00053
0.0055 0.00042
0.0055 0.0001
0.0055 0.0003
0.0055 0.00055
0.0055 0.00041
0.0055 0.00047
0.0055 0.00048
0.0055 0.00038
0.0055 0.00043
0.0055 0.00028
0.0055 0.00041
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
06/I 8/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/18/07
06/1 8/07
06/18/07
06/1 8/07
06/18/07
1319 erusseU
1319 erussefl
1319 erussell
1319 eiussell
1319 erusselt
1319 enissell
1319 erussell
1319 erusseU
1319 erussell
1319 erussell
1319 erussell
1319 erussel
1319 erusseil
1319 ewssefl
1319 erussellBRLmg/kg
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800529-6364 Fax 7041525-0409 Page 22 of 35
Pull SerykeAiialytlcal
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
WS-4
184318
G0607392
06/13/07 1415
06/13/07 1545
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Spring brook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7O4I529-634 Toll Free Number 1-8001529-6364 Fax 704/525-0409
NC Certification No 402
SC Certification No ggoi
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Parameter Result Units Report MDL Dilution Method
Limit
Analyst Batch
ID
Analysis
Factor Date/Time
2-Hexanone BRL mg/kg 0.055 0.00058 82608 06/18/07 1319 erussell 024312
4-Chiorotoluene BRL mg/kg 0.0055 0.00029 826GB 06/18/07 1319 erussell 024312
4-Methyl-2-pentanone MIBK BRL mg/kg 0.055 0.00055 826GB 06/18/07 1319 erussell 024312
Acetone 0.12 mg/kg 0.055 0.0022 8260B 06/18/07 1319 eiussell 024312
Benzene BRL mg/kg 0.0033 0.00044 82603 06/18/07 1319 erussell Q2431
Bromobenzene BRL mg/kg 0.0055 0.00039
826GB 06/16/07 1319 erusselL 024312
Bromochioromethane BRL mg/kg 0.0055 0.00033 826GB 06/18/07 1319 erussefl 024312
Bromodichioromethane BRL mg/kg 0.0055 0.00049
8260 06/18/07 1319 erussell 024312
Bromoform BRL mg/kg 0.0055 0.00041 826GB 06/18/07 1319 erussell Q24312
Bromomethano BRL mg/kg 0.011 0.00064 8260B 06I18/07 1319 enissell 024312
Carbon tetracliloride BRI mg/kg 0.0055 0.00032
82608 06/1 8/07 1319 erussell 024312
Chlorobenzene BRL mg/kg 0.0055 0.00042 8260B 06/18/07 1319 erussell Q24312
Chiorodibromomethane BRL mg/kg 0.0055 0.00038 8260B 06/18/07 1319 enissell 024312
Chioroethane BRL mg/kg 0Oil 0.00045 8260B 06/18/07 1319 enissell 024312
Chloroform BRL mg/kg 0.0055 0.00041 826GB 06/18/07 1319 erussell 024312
Chiorornethane BRL mg/kg 0.0055 0.00039
826GB 06/18/07 1319 erussell 024312
cis-12-Dichloroethene BRL mg/kg 0.0055 0.00024 82608 06/18/07 1319 erussell 024312
cis-13-Dlchloropropene BRL mg/kg 0.0055 0.00035 82608 06118/07 1319 erussell 024312
Dichiorodifluoromethane BRL mg/kg 0.0055 0.0012 826GB 06/18/07 1319 erussell 024312
Ethylbenzene BRL mg/kg 0.0055 000039 826GB 06/18/07 1319 erussell 024312
Isopropyl ether IPE BRL mg/kg 0.0055 000019 826GB 06/18/07 1319 erussell 024312
lsopropylbenzene BRL mg/kg 0.0055 0.00044 8260B 06/18/07 1319 erussell 024312
mp-Xylenes BRL mg/kg 0.011 0.00078 826GB 06/18/07 1319 erussell 024312
Methyl ethyl ketone MEK BRL mg/kg 0.11 0.0016 82608 06/18/07 1319 erussell 024312
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00032 626GB 06/18/07 1319 erussell Q24312
Methylene chloride BRL mg/kg 0.0055 0.00045 826DB 06/18/07 1319 ewsasll 024312
n-Butylbenzene BRL mg/kg 0.0055 0.00044 826DB 06/18/07 1319 erussell 024312
Page 23 of 35
This report should not be reproduced except in its entrety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte1 NC 28224-0543
Phone 7041529-6364 Toll Free Number 1-8001529-6364 Fax 70415250409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
05/25/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil CbC Group
Time Collected
Time Submitted
WS-4
184318
G0607392
06/13/07 1415
06/13/07 1545
Parameter Result Units Report MDL Dilution Method
Limit
AnalystAnalysis Batch
Factor Dateffime ID
8260B 06/18/07 1319 snissell Q24312
826DB 06/18/07 1319 erussell 024312
826DB 06/18/07 1319 enissell 024312
8260B 06/18/07 1319 erussell Q24312
826DB 06/18/07 1319 erussell 024312
826DB 06/18/07 1319 erussell 024312
826DB 06/18/07 1319 erussell 024312
8260B 06/18/07 1319 erussel 024312
826DB 06/18/07 1319 erussell 024312
8260B 06/18/07 1319 erussel 024312
8260B 06/18/07 1319 erussell 024312
8260B 06/18/07 1319 erussell Q24312
826DB 06/18/07 1319 erusseI 024312
8260B 06/18/07 1319 erussell 024312
82609 06/18/07 1319 erussell Q24312
n-Propylbenzene BRL
Naphthalene BRL
o-Xylene BRL
p-lsopropyltoluene BRL
sec-Butylbenzene BRI
Styrene BRL
tert-Butylbenzene BRL
Tetrachioroethene BRL
Toluerie BRL
trans-I 2-Dichloroethene BRL
trans-I 3-Dichloropropene BRL
Trichloroethene BRL
Trichiorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Compounds by GC1MS
24-Tiichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
245-Trichiorophenol BRL
246-Trichiorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.0055
0.011
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.028
0.0055
0.39
0.39
0.39
0.39
0.39
0.39
0.00033
0.00064
0.00033
0.00045
0.00037
0.00055
0.00034
0.00095
0.00038
0.00042
0.00039
0.00033
0.00045
0.0020
0.00071
0.039
0.029
0.028
0.035
0.040
0.038
Surrogate Recovery Control Limits
Bromofluorobenzene 88 77 128
Dibromofluoromethane 92 67 143
Toluene-d8 102 81-128
827CC
8270C
827CC
8270C
827CC
8270C
06/18/07 1718 kcamplgotto
06/18/07 1718 kcampigotto
06/18/07 1718 kcampigotto
06/18/07 1718 kcampigotto
06/I 8/07 1718 kcampigotto
06/18/07 1718 kcamprgotto
024348
024348
024348
024348
024348
024348
Page 24 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter
24-Dichiorophenol
24-Dimethyiphenol
24-Dinitrophenol
24-Dinitrotoluene
26-Dinitrotoluerie
2-Chomnaphthalene
2-Chiorophenol
2-Methylnaphthalene
2-Methyiphenol
2-Nitrophenol
34-Methylphenol
33-Dichlorobenzidine
46-Dinitro-2-methylphenol
4-Bromophenylphenylether
4-Chloro-3-methylphenol
4-Chioroaniline
4-Chlorophenylphenylether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzoaanthracene
Benzoapyrene
Benzobuluoranthene
Benzoghiperylene
Benzokfluoranthene
Laboratory Report
06/25/07
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 184318
Sample Matrix Soil COG Group G0607392
Time Collected 06/13/07 1415
Time Submitted 06/1 3/07 1545
06118107 1718 kcampigotto 024348
06/18/07 1715 kcampigotto 024348
06/18/07 1718 kcampigOtto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampgotto 024348
06/18107 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06118/07 1718 kcempigotto 024348
06/18/07 1718 kcampigotto Q24348
06/18/07 1718 kcamplgotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 koampigotto 024348
06/18107 1718 kcampigotto 024348
06118107 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18107 1718 koampigotto 024348
06/18/07 1718 koampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcamplgotto 024348
06/18/07 1718 koampigotto 024348
06/18/07 1718 koampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 koampigotto 024348
06/18/07 1718 kcampigotto 024348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
Full Srvlc AnaIytfc Ewiroimuilal L...llonu
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRL mg/kg 0.39 0.033 82706
BRL mg/kg 0.39 0.038 82706
BRL mg/kg 2.0 0.044 82706
BRL mg/kg 0.39 0.022 82706
BRL mg/kg 0.39 0.042 8270C
BRL mg/kg 0.39 0.040 8270C
BRL mg/kg 0.39 0.031 82706
ERL mg/kg 0.39 0.031 82706
BRL mg/kg 0.39 0.037 82706
BRL mg/kg 0.39 0.047 8270C
BRL mg/kg 0.39 0.040 82706
BRL mg/kg 0.79 0.025 82706
BRL mg/kg 2.0 0.024 8270C
BRL mg/kg 0.39 0.037 82706
BRI mg/kg 0.79 0.029 82706
BRL mg/kg 0.39 0.050 82706
BRL mg/kg 0.39 0.024 8270C
BRL mg/kg 2.0 0.026 8270C
BRL mg/kg 0.39 0039 8270C
BRL mg/kg 0.39 0.039 8270C
BRL mg/kg 0.39 0.030 82706
BRL mg/kg 2.0 0.036 8270C
BRL mg/kg 0.39 0.055 82706
BRL mg/kg 0.39 0.045 8270C
BRL mg/kg 0.39 0.018 8270C
BRL mg/kg 0.39 0.019 82706
BRL mg/kg 0.39 0.032 82700
Page 25 of 35
Laboratory Report
0612 5107
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 184318
Sample Matrix Soil COC Group G0607392
Time Collected 06/1 3/07 1415
Time Submitted 06/13/07 1545
Parameter
Benzoic acid
Benzyl alcohol
Bis2-chloroethoxyrnethane
Bis2-chloroethylether
Bis2-chloroisopropylether
Bis2-ethylhexylphthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenzoahanthracerie
Dlbenzofurari
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachiorobutadiene
Hexachiorocyclopentadiene
Hexachloroethane
lndeno1 .23-cd pyrene
Isophorone
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Peiitachlorophenol
mg/kg 2.0 0.17
mg/kg 0.79 0.041
mg/kg 0.39 0.045
mg/kg 0.39 0.043
mg/kg 0.39 0.034
mg/kg 0.39 0.019
mg/kg 0.39 0.024
mg/kg 0.39 0.065
mg/kg 039 0.018
mg/kg 0.39 0.029
mg/kg 0.39 0.039
mg/kg 0.39 0.034
mg/kg 0.39 0.024
mg/kg 0.39 0.027
mg/kg 0.39 0.027
mg/kg 0.39 0.023
mg/kg 0.39 0.020
mg/kg 0.39 0.038
mg/kg 0.39 0.042
mg/kg 0.39 0.040
mg/kg 0.39 0.040
mg/kg 0.39 0.035
mg/kg 0.39 0.045
mg/kg 0.39 0.020
mg/kg 0.39 0.043
mg/kg 0.39 0.038
mg/kg 2.0 0.033
Method Analysis Analyst Batch
Date/Time ID
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06118/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto Q24348
06/18/07 1718 kcampigotto Q24348
06/18/07 1718 kcampigotto 024348
06/18107 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigofto Q24348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06118/07 1718 kcampigotto Q24348
06/18/07 1718 kcampigotto Q24348
06/18/07 1718 koampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 koampigotto 024348
06/18/07 1718 kcampigotto 024348
06/18/07 1718 kcampigotto 024346
06/18/07 1718 kcampigotto 024348
This report should not be reproduced except In its entirety without the written consent of Piism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
Sric Ana4icl Envlronmm._..-_._._ns
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Result Units Report MDL Dilution
Limit Factor
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
827CC
82700
827CC
82700
82700
8270C
827CC
8270C
827CC
827CC
827CC
827CC
8270C
827CC
827CC
827CC
827CC
827CC
827CC
8270C
8270C
827CC
82700
8270C
827CC
827CC
827CC
Page 26 of 35
PuB SeMu AiiI
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Prolect ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
WS-4
184318
G0607392
06/13107 1415
06113107 1545
Parameter
Phenanthrene
Phenol
Pyrene
Report
Limit
0.39
0.39
0.39
Analysis
Date/Time
06/18/07 1718 kcampigotto
06/18/07 1718 kcampigotto
06/18/07 1718 kcampigotto
Q24348
Q24348
Q24348
Extractable Petroleum Hydrocarbons by GC-FID
Cl 1-C22 Aromatics BRL mg/kg
C19-C36Aliphatics BRL mg/kg
C9-C18 Aliphatics BRL mg/kg
Analysis Note for Cl1-C22 Aromatics
Sample Preparation
Volatile Petroleum Hydrocarbons by GC-PID/FID
C5-C8 AliphaUcs BRL
C9-C10 Aromatics BRL
C9-C12 Aliphatics BRL
Laboratory Report
06/25/07
Result Units MDL Method
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
Sample Preparation
Dilution
Factor
0.019
0.043
0.027
Analyst Batch
ID
8270C
827CC
827CC
29.78 mL 35508 06/15/07 900 dpope P18642
Surrogate Recovery Control Limits
246-Tribromophenol 104 25 123
2-Fluorobiphenyl 82 21 108
2-Fluorophenol 72 14-89
Nitrobenzene-d5 75 14-103
Phenol-d5 71 13-95
Terphenyl-d14 115 41-136
11 6.1 MADEP EPH
06/21/07 340 grappaccioli Q24425
11 1.7 MADEP EPH 06/21/07 340 grappaccioti Q4425
11 3.6 MADEP EPH 06/21/07 340 grappaccioli Q24425
Adjusted value
10.52 mL EPH 06/19/07 1000 jvoget P18669
Surrogate Recovery Control Limits
1-Chloro-octadecane 89 40 140
2-Brornonaphthalene 101 40-140
2-Fluorobiphenyl 100 40-140
o-Terpheriyl 83 40-140
mg/kg 5.9 1.1 MADEPVPH 06/21/07 237 hwagner 024410
mg/kg 5.9 0.035 MADEP VPH 06/21/07 237 hwagner Q24410
mg/kg 5.9 1.8 MADEP VPH 06/21/07 237 hwagner Q24410
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 ToIl Free Number 1-800/529-6364 Fax 7041525-0409 Page 27 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Analysis Note for C5-C8 Aliphatics Adjustedvalue
Analysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluerie-PID 83 70 130
25-Dibromotoluene-FID 116 70 130
Sam1e Weight Determination
Weight 12.71 MADEP VPH 06/18/07 000 brown
Weight 13.01 MADEP VPH 06/18/07 000 Ibrown
Sample Comments
BRL Below Reporting Umit
J-Estimated value
between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated
in the case narrative and/or test comments
All results are reported on dry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Ffl e.icMytical Envronmta
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 184318
Sample Matrix Soil COC Group G0607392
Time Collected 06/13/07
Time Submitted 06/13107
1415
1545
Angela ID Overcash V.P Laboratory Services
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax 704525.0409 Page 28 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
EnvTmnISeFiHJons
ESP Associates PA Project ID
Attn Chris Ward
Box 7030
Charlotte NC 28241
Morehead Commons No Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
B-I
184319
G0607392
06/13107 1430
06/13/07 1545
Percent Solids
Determination
Percent Solids
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
1-Dichloroethane
1DichIoroethene
1-Dichloropropene
23-Trichiorobenzene
23-Trichloropropane
24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropana
4-Dlchlorobenzene
22-Dichloropropane
2-Chiorotoluene
Laboratory Report
06/25/07
Sample Matrix Soil
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
SM2540 06118/07 1700 brown
Volatile Organic Compounds by GC/MS
11 1-Trichloroethane
11 22-Tetrachloroethane
11 2-Trichloroethane
80.0
5.31
6.62
6.15
BRL mg/kg 0.0047 0.00026
BRL mg/kg 0.0047 0.00048
BRL mg/kg 0.0047 0.00029
BRL mg/kg 0.0047 0.00034
BRL mg/kg 0.0047 0.00036
BRL mg/kg 0.0047 0.00042
BRL mg/kg 0.0047 0.00052
BRL mg/kg 0.0047 0.00042
BRL mg/kg 0.0047 0.00045
BRL mg/kg 0.0047 0.00036
BRL mg/kg 0.0047 0.000085
BRL mg/kg 0.0047 0.00025
BRL mg/kg 0.0047 0.00047
BRL mg/kg 0.0047 0.00035
BRL mg/kg 0.0047 0.0004
BRL mg/kg 0.0047 0.0004
BRL mg/kg 0.0047 0.00032
BRL mg/kg 0.0047 0.00037
BRL mg/kg 0.0047 0.00024
BRL mg/kg 0.0047 0.00035
5035
5035
5035
826DB
826DB
826GB
82603
82603
82608
826DB
826DB
8260B
826DB
826GB
826DB
826DB
826GB
826DB
826DB
82608
826GB
826DB
826GB
06/18/07 000
06/18/07 000
06/18107 000
06/19/07 1631
06/19/07 1631
06/19/07 1631
06/19/07 1631
06/19/07 1631
06/19/07 1631
06/19/07 1631
06/19/07 1631
08/19/07 1631
06/19/07 1631
06/19/07 1631
06/19/07 1631
06/19107 1631
06/19/07 1631
06/19/07 1631
06/19107 1631
06/19/07 1631
06/19/07 1631
06/19/07 1631
Ibrown
Ibrown
brown
en2sselI
enissell
ejussell
erussell
enissell
erussell
erussell
erussell
erussell
erussell
erussell
erusselt
erusselt
erussell
erussell
enissell
erussell
erussefl
erussell
Q24312
Q24312
024312
Q24312
024312
024312
024312
Q24312
024312
024312
024312
024312
024312
Q24312
024312
024312
024312
024312
024312
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/526-0409
06/19/07 1631 erussell 024312
Page 29 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-8O0l5296364 Fax 704/525-0409
Laboratory Report
06/25/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID 8-1
Attn Chris Ward Prism Sample ID 184319
Box 7030 Sample Matrix Soil COC Group G0607392
Charlotte NC 28241 Time Collected 06/13/07 1430
Time Submitted 06/13/07 1545
Parameter Resutt Units Report MDL Dilution Method
Factor
AnalystAnalysis Batch
Limit Date/Time ID
2-Hexanone BRL mg/kg 0.047 0.00049
82608 06/19/07 1631 erussell Q24312
4-Chiorotoluene BRL mg/kg 0.0047 0.00025 8260B 06/19/07 1631 erussell 024312
4-Methyl-2-pentancne MIBK BRL mg/kg 0.047 0.00047 8260B 06/19/07 1631 erussell 024312
Acetone 0.048 mg/kg 0.047 0.0019
82608 06/19/07 1631 ewssell 024312
Benzene BRL mg/kg 0.0028 0.00038 82608 06/19/07 1631 erussell 024312
Bromobenzene BRL mg/kg 0.0047 0.00033 826GB 06/19/07 1631 erussell 024312
Bromochioromethane BRL mg/kg 0.0047 0.00028 826GB 06/19/07 1631 eiussell 024312
Broniodichloromethane BRL mg/kg 0.0047 0.00042 826GB 06/19/07 1631 eiussell 024312
Bromoform BRL mg/kg 0.0047 0.00035 826GB 06/19/07 1631 erussefl Q24312
Bromomethane BRL mg/kg 0.0094 0.00055 8260B 06/19/07 1631 erussell 024312
Carbon tetrachioride BRL mg/kg 0.0047 0.00027 826GB 06/19/07 1631 erussell 024312
Chlorobenzene BRL mg/kg 0.0047 0.00036 8260B 06/19/07 1631 en.issel 024312
Chiorodibromomethane BRL mg/kg 0.0047 0.00032 826GB 06/19/07 1631 erussell 024312
Chloroethane BRL mg/kg 0.0094 0.00039 82608 06/19/07 1631 erussell 024312
Chloroform BRL mg/kg 0.0047 0.00035 826GB 06/19/07 1631 erussell 024312
Chioromethane BRL mg/kg 0.0047 0.00033 826GB 06/19/07 1631 erussell 024312
cis-1 2-Dichloroethene BRL mg/kg 0.0047 0.00021
826GB 06/19/07 1631 erussell 024312
cis-13-Dichloropropene BRL mg/kg 0.0047 0.0003 826GB 06/19/07 1631 erussel 024312
Dichlorodifluoromethane BRL mg/kg 0.0047 0.0011 826GB 06/19/07 1631 erussell 024312
Ethylbenzene BRL mg/kg 0.0047 0.00033 82608 06/19/07 1631 erussell 024312
Isopropyl ether IPE BRL mg/kg 0.0047 0.00016 826GB 06/19/07 1631 erussell 024312
Isopropylbenzene BRL mg/kg 0.0047 0.00038 82608 06/19/07 1631 erussell 024312
mp-Xylenes BRL mg/kg 0.0094 0.00066 826GB 06/19/07 1631 erussell 024312
Methyl ethyl ketone MEK BRL mg/kg 0.094 0.0013 826GB 06/19/07 1631 erussell 024312
Methyl t-butyl ether MTBE BRL mg/kg 0.0094 0.00027 826GB 06/19/07 1631 erussell 024312
Methytene chloride BRL mg/kg 0.0047 0.00039 826GB 06/19/07 1631 erussell 024312
n-Butylbenzene BRL mg/kg 0.0047 000038 826GB 06/19/07 1631 eussell 024312
Page 30 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
B-I
184319
G0607392
06/13/07 1430
06/13/07 1545
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
0.0047 0.00028 826DB 06/19/07 1631 eniseIl 024312
0.0094 0.00055
826DB 06/19/07 1631 erussell 024312
0.0047 0.00028 82606 06/19/07 1631 erussell 024312
0.0047 0.00039 826DB 06/19/07 1631 enissefl 024312
0.0047 0.00031
826DB 06/19/07 1631 erussell Q2431
0.0047 0.00047 826DB 06/19/07 1631 erussell Q24312
0.0047 0.00029 826DB 06/19/07 1631 erussefl Q24312
0.0047 0.00081 826DB 06/19/07 1631 enissell 024312
0.0047 0.00032 82606 06/19/07 1631 wsse11 024312
0.0047 0.00036 82606 06/19/07 1631 erussel 024312
0.0047 0.00033 826DB 06/19107 1631 erussell 024312
0.0047 0.00028 826DB 06/19/07 1631 erussell 024312
0.0047 0.00039 826DB 06/19/07 1631 erussell 024312
0.024 0.0017 826DB 06/19/07 1631 erussell Q24312
0.0047 0.0006 826DB 06/19/07 1631 en.rsseU Q24312
n-Propylbenzene BRL
Naphthalene BRL
o-Xylene BRL
p-lsopropyltoluene BRL
sec-Butylbenzens BRI
Styrene BRL
tert-Butylbenzene BRL
Tetrachloroethene BRL
Toluene BRL
trans-i 2-Dichloroethene BRL
trans-i 3-Dichloropropene BRI
Trichloroethene BRL
Trichiorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRI
Semi-volatile Organic Compounds by GC/MS
24-Trichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
245-Trichlorophenol BRL
246-Trichlorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Dibromofluoromethane 95 67 143
Bromolluoroberizerie 79 77 128
Toluene-d8 97 81-128
0.41
0.41
0.41
0.41
0.41
0.41
0.041
0.030
0.030
0.037
0.042
0.039
8270C
827DC
8270C
8270C
8270C
627DC
06/18/07 1807
06/18/07 1807
06/18/07 1807
06/18/07 1807
06/18/07 1807
06/18/07 1807
kcampigotto
kcampigotto
kcampigotto
kcampigouo
kcampigotto
kcamplgotto
024348
Q24348
024348
Q24348
024348
024348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories lnc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 31 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project lD Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
B-i
184319
00607392
08/13/07 1430
06/1 3/07 1545
24-Dichlorophenol
24-Dimethyiphenol
24-Dirritropherrol
24-Dinitrotoluene
26-Dirritrotoluene
2-Choronaphthalerre
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
34-Methylphenol
33-Dichlorobenzidine
46-Dinitro-2-methylphenol
4-Bromophenyiphenylether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenylphenylether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Arrthracene
4zobenzene
Benzoaanthracene
Benzoapyrene
Benzobfluoranthene
Benzoghiperylene
Benzokfluomntherre
AnalystAnalysis
Date/Time
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06118107 1807 kcampigotto
06118/07 1807 kcamptgotto
06118/07 1807 kcampigotto
06/18/07 1807 keampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcamplgotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
0618/07 1807 kcampigotto
06/18/07 1807 koampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcampigotto
06/18/07 1807 kcarnpigotto
024348
024348
024348
024348
Q24348
Q24348
024348
024348
024348
024348
024348
Q24348
024348
024348
024348
024348
024348
024348
024348
.024348
024348
024348
024348
024348
024348
024348
024348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 7D4/525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Parameter Result Units Report MDL Dilution Method
Limit Factor
Batch
ID
BRL mg/kg 0.41 0.034 827CC
BRL mg/kg 0.41 0.039 827CC
BRL mg/kg 2.0 0.046 82700
BRL mg/kg 0.41 0.023 82700
BRL mg/kg 0.41 0.043 82700
BRL mg/kg 0.41 0.042 82700
BRL mg/kg 0.41 0.032 82700
BRL mg/kg 0.41 0.033 82700
BRL mg/kg 0.41 0.038 8270C
BRL mg/kg 0.41 0.049 827CC
BRL mg/kg 0.41 0.042 827CC
BRL mg/kg 0.82 0.026 82700
BRL mg/kg 2.0 0.025 82700
BRL mg/kg 0.41 0.039 82700
BRL mg/kg 0.82 0.030 82700
BRL mg/kg 0.41 0.052 827CC
BRL mg/kg 0.41 0.025 82700
BRL mg/kg 2.0 0.027 827oC
BRL mg/kg 0.41 0.040 82700
BRL mg/kg 0.41 0.041 8270C
BRL mg/kg 0.41 0.031 82700
BRL mg/kg 2.0 0.038 82700
BRL mg/kg 0.41 0.057 82700
BRL mg/kg 0.41 0.047 8270C
BRL mg/kg 0.41 0.018 827CC
BRL mg/kg 0.41 0.019 8270C
BRL mg/kg 0.41 0.033 82700
Page 32 of 35
Laboratory Report
06125/07
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID 184319
Sample Matrix Soil COC Group G0607392
Time Collected 06/13/07 1430
Time Submitted 06/13/07 1545
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Eu Service MalyScul EnvIronmcrfl ........ionu
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method
Limit Factor
_______________
Analyst Batch
ID
Analysis
Date/Time
Benzoic acid BRL mg/kg 2.0 0.17 8270C 06118/07 1807 kcampigotto 024348
Benzyl alcohol BRL mg/kg 0.82 0.043 8270C 06/18/07 1507 kcampigotto 024348
Bis2-chloroethoxymethane BRL mg/kg 0.41 0.047 8270C 06/18/07 1807 kcampigotto 024348
Bis2-chloroethylether BRL mg/kg 0.41 0.044 8270C 06/18/07 1807 kcampigotto Q24348
Bis2-chloroisopropylether BRL mg/kg 0.41 0.035 8270C 06/18/07 1807 kcampigotto 024348
Bis2-ethylhexylphthalate BRL mg/kg 0.41 0.020 8270C 06/18/07 1807 kcampigotto 024348
Butylbenzylphthalate BRL mg/kg 0.41 0.025 8270C 06/18/07 1807 kcampigotto 024348
Chrysene BRL mg/kg 0.41 0.068 8270C 06/18/07 1807 kcampigotto 024348
Di-n-butylphthalate BRL mg/kg 0.41 0.019 8270C 06/18/07 1807 kcampigotto 024348
Di-n-octylphthalate BRL mg/kg 0.41 0.030 8270C 06/18/07 1807 kcampigotto 024348
Dibenzoahanthracene BRL mg/kg 0.41 0.041 8270C 06/18/07 1807 kcampigotto 024348
Dibenzofuran BRL mg/kg 0.41 0.035 8270C 06/18/07 1807 keampigotto 024348
Diethylphthalate BRL mg/kg 0.41 0.025 8270C 06/18/07 1807 kcampigotto 024348
Dimethylphthalate BRL mg/kg 0.41 0.028 8270C 06/18/07 1807 kcampigotto Q24348
Fluoranthene BRL mg/kg 0.41 0.028 8270C 06/18/07 1807 kcampigotto 024348
Fluorene BRL mg/kg 0.41 0.024 8270C 06/18/07 1807 kcampigotto 024348
Hexachlorobenzene BRL mg/kg 0.41 0.021 8270C 06/18/07 1807 kcampigotto 024345
Hexathlorobutadiene BRL mg/kg 0.41 0.040 8270C 06/18/07 1807 kcampigotto 024348
Hexachiorocyclopentadierie BRL mg/kg 0.41 0.043 8270C 06/18/07 1807 kcampigetto Q24348
Hexachloroethane BRL mg/kg 0.41 0.042 8270C 06/18/07 1807 kcampigotto 024348
lndeno1 23-cdpyrene BRL mg/kg 0.41 0.042 8270C 06/18/07 1807 kcampigotto 024348
Isophorone BRL mg/kg 0.41 0.037 8270C 06/18/07 1807 kcarnpigotto 024348
N-Nitrosodi-n-propylamine BRL mglkg 0.41 0.046 8270C 06/18/07 1807 kcampigotto Q24348
N-Nitrosodiphenylamine BRL mg/kg 0.41 0.021 8270C 06/18/07 1807 kcampigotto 024348
Naphthalene BRL mg/kg 0.41 0.045 8270C 06/18/07 1807 kcampigofto 024348
Nitrobenene BRL mg/kg 0.41 0.040 8270C 06/18/07 1807 kcampigotto 024348
Perttachlorophenol BRL mg/kg 2.0 0.034 8270C 06/18/07 1807 kcampigotto Q24348
Page 33 of 35
lceAnCytfcotEwironsontol Solutions
ESP Associates PA
Attn Chris
Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
B-I
184319
G0607392
06/13107 1430
06/I 3/07 1545
Sample Preparation 30.25 mL 35508 06/15107 900 dpope P18642
Extractable Petroleum Hydrocarbons by GC-FID
ClI-C22 Aromatics 6.8 mg/kg
Cl 9-C36 Aliphatics BRL mg/kg
C9-C18 Aliphatics 36 mg/kg
Analysis Note for C1l-C22 Aromatics
Sample Preparation
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/25/07
Parameter Result Units Analyst Batch
ID
MDL
Phenanthrene BRL mg/kg
Phenol BRL mg/kg
Pyrene BRL mg/kg
MethodReport
Limit
0.41
0.41
0.41
Dilution
Factor
0.020
0.045
0.028
8270C
8270C
827CC
Analysis
Date/Time
06/18/07 1807
06/18/07 1807
06/18/07 1807
koampigotto
kcamplgotto
kcampigotto
024348
Q24348
Q24348
Surrogate Recovery Control Limits
Terphenyl-d14 98 41 136
Phenol-d5 77 13-95
2-Fluorobiphenyl 85 21 108
Nitrobenzene-d5 79 14-103
246-Tribromophenol 99 25-123
2-Fluorophenol 73 14 89
12 6.5 MADEP EPH 06/21/07 524 grappaccioli 024425
12 1.8 MADEP EPH
06/21/07 524 grappaccioli 024425
12 3.9 MADEP EPH 06/21/07 524 grappacciofl 024425
Adjusted value
10.35 mL EPH 06/19/07 1000 jvogel P18669
Surrogate Recovery Control Limits
2-Fluorobiphenyl 86 40-140
2-Bromonaphthalene 90 40-140
o-Terphenyl 78 40-140
1-Chloro-octadecane 90 40 140
Volatile Petroleum Hydrocarbons by GC-PIDIFIO
C5-C8AIiphatics BRL mg/kg 6.3 1.2 MADEP VPH 06/21/07 319 hwagner 024410
C9-C10 Aromatics BRL mg/kg 6.3 0.037 MADEP VPH 06/21/07 319 hwagner 024410
C9-C12 Aliphatics BRL mg/kg 6.3 1.9 MADEP VPH 06/21/07 319 hwagner Q24410
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 70415296364 Toll Free Number 1-8001529-6364 Fax 7041525.0409 Page 34 of 35
fl NO.12 Laboratory Report
NC Drinking Water Cert No 37735 06/25/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID B-I
Attn Chris Ward Prism Sample ID 184319
Box 7030 Sample Matrix Soil coc Group 00607392
Charlotte NC 28241 Time Collected 06/13/07 1430
Time Submitted 06/I 3/07 1545
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
na1ysis Note for C5-C8 Aliphatics Adjusted value
ria1ysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 117 70-130
25-Dibromotoluene-PID 115 70 130
Sample Weight Determination
Weight 17.01 MADEP VPH 06/18/07 000 Ibrown
Weight 12.45 MADEP VPH 06/18/07 000 Ibrown
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated
in the case narrative and/or test comments
All results are reported on thy-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409 Page 35 of 35
ESP Associates PA
Attn Chils Ward
P.O Box 7030
Charlotte NC 28241
11-Trichloroethane
122-Tetrachloroethane
12-Trichloroethane
1-Dichloroethane
l-Dtchloroethene
1.1-Dichioropropene
23-Trichorobenzene
123-Trichioropropane
24-.Trichtorobenzene
24-Trimethylbenzene
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichloroetharie
2-Dichloropropane
135-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
14-Dichlorobenzene
22-Dichioropropane
2-Chiorotoluene
2-Hexanone
4-Chiorotoluene
4-Meth4-2-pentanone MIBK
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichioromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chorobenzene
Chlorodibromomethane
Chioroethane
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.05 0.025
ND 0.005 0.0025
ND 0.05 0.025
ND 0.05 0.025
ND 0.003 0.0015
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.01 0.005
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.01 0.005
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
024312
Q24312
024312
024312
024312
024312
024312
Q2431
Q24312
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-5364 Toll Free Number 1-8001529-6364 Fax 704/525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6/25/07
Project ID Morehead Commons No COG Group Number G0607392
Date/Time Submitted
6/13/07 1545
Volatile 1.......I..I OflDJIL4dIuII..UJIIFJUUIIUD UT IIIuIUU .UULJ
Method Blank QC Batch
Result RL Conimi Urrut Units ID
Page 018
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6125/07
Method Blank QC Batch
Result RI Contm limit Units ID
Chloroform ND 0.005 0.0025 mg/kg Q24312
Chloromethane ND 0.005 0.0025 mg/kg Q24312
cis-12-Dichloroethene ND 0.005 0.0025 mg/kg 024312
cis-13-Dichloropropene ND 0.005 0.0025 mg/kg 024312
Dichiorodifluoromethane ND 0.005 0.0025 mg/kg 024312
Ethylbenzene ND 0.005 0.0025 mg/kg 024312
Isopropyl ether IPE ND 0.005 0.0025 mg/kg 024312
lsopropylbenzene ND 0.005 0.0025 mg/kg 024312
mp-Xylenes ND 0.01 0.005 mg/kg Q24312
Methylethyl ketoneMEK ND 0.1 0.05 mg/kg Q24312
Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg 024312
Methylene chloride ND 0.005 0.0025 mg/kg 024312
n-Butylbenzene ND 0.005 0.0025 mg/kg 024312
n-Propylbenzene ND 0.005 0.0025 mg/kg 024312
Naphthalene ND 0.01 0.005 mg/kg 024312
o-Xylene Nt 0.005 0.0025 mg/kg 024312
p-lsopropyltoluene ND 0.005 0.0025 mg/kg 024312
sec-Butylbenzene ND 0.005 0.0025 mg/kg 024312
Styrene ND 0.005 0.0025 mg/kg 024312
tert-Butylbenzene ND 0.005 0.0025 mg/kg Q24312
Tetrachkroethene ND 0.005 0.0025 mg/kg 024312
Toluene ND 0.005 0.0025 mg/kg Q24312
trans-12-Dichloroethene ND 0.005 0.0025 mg/kg 024312
trans-I 3-Dichloroproperie ND 0.005 0.0025 mg/kg 024312
Trichioroethene ND 0.005 0.0025 mg/kg 024312
Trichiorofluoromethano ND 0.005 0.0025 mg/kg 024312
Vinyl acetate ND 0.025 0.0125 mg/kg 024312
Vinyl chloride ND 0.005 0.0025 mg/kg 024312
tw control sample RecoveY QCBSCh
Result Spike Amount Units ID
11-Dichloroethene 0.03403 0.05 mg/kg 68 51-122 024312
Benzene 0.03684 0.05 mg/kg 74 62-119 024312
Chlorobenzene 0.04043 0.05 mg/kg 81 61-124 024312
Toluerte 0.03928 0.05 mg/kg 79 57-122 024312
Trichloroethene 0.04412 0.05 mg/kg 88 59-129 024312
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-6364 Toll Free Number 1-800/529-6364 Fax 7041525-0409
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No COC Group Number G0607392
Date/Time Submitted
6/13/07 1545
Page of
NC Certification No 402
SC Certification No.99012
NC Drinking Water Cart No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
448 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-8364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
Full ceAnlytlcaJ Enulmumontal Sotutienu
ESP Associates PA
Attn Chils Ward
Box 7030
Charlotte NC 28241
Level II QC Report
6/25/07
Project ID Morehead Commons No COC Group Nurnber G0607392
Date/Time Submitted
6/13/07 1545
Matrix Spike Recovery Recovery OC BatthRanges
Sample ID Result SpikeAmount Units 0k ID
184326 11-Dichloroethene 0.03513 0.05 mg/kg 70 44-140 024312
Benzene 0.03664 0.05 mg/kg 73 46-136 024312
Chlorobenzene 0.03947 0.05 mg/kg 79 47-135 024312
Toluene 0.03821 0.05 mg/kg 76 47-136 024312
Trichloroethene 0.04101 0.05 mg/kg 82 45-141 024312
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD pange QC BStth
Sample ID Result Spike Amount Units ID
184326 11-Dichloroethene 0.03565 0.05 mg/kg 71 44-140 -23 024312
Benzene 0.03548 0.05 mg/kg 71 46-136
0-22 024312
Chlorobenzene 0.04002 0.05 mg/kg 80 47-135 0-22 024312
Toluene 0.03763 0.05 mg/kg 75 47-136 0-22 024312
Trichloroethene 0.0411 0.05 mg/kg 82 45-141 0-23 024312
Page of
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241II tGCIMS method 8270C
Method Blank CC Batch
Result RL Control Umit Units ID
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte1 NC 28224.0543
Phone 7041529-6364 Toll Free Number 1-8001529-6364 Fax 7041525-0409
1...eAuly5cal Envlmnmental Shjtlona
NC Certification No 402
SC CertIfication No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6/25/07
Project ID Morehead Commons No coc Group Number G0607392
Date/Time Submitted
6/13107 1545
24Trichlorobenzene ND 0.33 0.165 mg/kg 024348
12-Dichlorobenzerte ND 0.33 0.165 mg/kg 024348
13-Dichlorobenzene ND 0.33 0.165 mg/kg Q24348
14-Dichlorobenzene ND 0.33 0.165 mg/kg 024348
245-Trichiorophenol ND 0.33 0.165 mg/kg 024348
246-Trithiorophenol ND 0.33 0.165 mg/kg 024348
2.4-Dichiorophenol ND 0.33 0.165 mg/kg Q24348
2.4-Dimethyiphenol ND 0.33 0.165 mg/kg 024348
24-Dinilmphenol ND 1.65 0.825 mg/kg 024348
24-Dinitrotoluene ND 0.33 0.165 mg/kg 024348
26-Dinitrotoluene ND 0.33 0.165 mg/kg 024348
2-Chloronaphthalene ND 0.33 0.165 mg/kg 024348
2-Chlorophenol ND 0.33 0.165 mg/kg Q24348
2-Methylnaphthalene ND 0.33 0.165 mg/kg 024348
2-Methylphenol ND 0.33 0.165 mg/kg 024348
2-Nitrophenol ND 0.33 0.165 mg/kg 024348
34-Melhylphenol ND 0.33 0.165 mg/kg 024348
33-Dichlorobenzidine ND 0.66 0.33 mg/kg 024348
46-Dinitro-2-methyiphenol ND 1.65 0.825 mg/kg 024348
4-8romophenylphenylether ND 0.33 0.165 mg/kg 024348
4-Chloro-3-methylpheno ND 0.66 0.33 mg/kg 024348
4-Chioroaniline ND 0.33 0.165 mg/kg 024348
4-Chiorophenyiphenylether ND 0.33 0.165 mg/kg 024348
4-Nitrophenol ND 1.65 0.825 mg/kg 024348
Acerraphthene ND 0.33 0.165 mg/kg Q24348
Acenaphthylene ND 0.33 0.165 mg/kg 024348
Anthracene ND 0.33 0.165 mg/kg 024348
Azobenzene ND 1.65 0.825 mg/kg 024348
Benzoaanthracene ND 0.33 0.165 mg/kg 024348
Benzoapyrene ND 0.33 0.165 mg/kg 024348
Benzobfluoranthene ND 0.33 0.165 mg/kg 024348
BenzoghJperylene ND 0.33 0.165 mg/kg 024348
8enzokfluoranthene ND 0.33 0.165 mg/kg 024348
BenoicacjcJ ND 1.65 0.825 mg/kg 024348
Page of
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Assodates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Level II QC Report
6/25/07
Project ID Marehead Commons No coc Group Number G0607392
Date/Time Submitted 6/13/07 1545
ftllethod Blank
Result RL Control Umit Units II
Benzyl alcohol ND 0.66 0.33 mg/kg 024348
Bis2-chloroethoxymethane NI 0.33 0.165 mg/kg 024348
Bis2.-chloroethylether ND 0.33 0.165 mg/kg 024348
Bis2-chIoroisopipyIether ND 0.33 0.165 mg/kg Q24348
Bis2-ethylhexylphthalate ND 0.33 0.165 mg/kg 024348
Butylbenzylphthalate ND 0.33 0.165 mg/kg Q24348
Chrysene ND 0.33 0.165 mg/kg Q24348
Di-n-butylphthalate ND 0.33 0.165 mg/kg 024348
Di-n-octylphthalate ND 0.33 0.165 mg/kg 024348
Dibenzoahanthracene ND 0.33 0.165 mg/kg 024348
Dibenzofuran ND 0.33 0.165 mg/kg 024348
Diethylphthalate ND 0.33 0.165 mg/kg 024348
Dimethylphthalate ND 0.33 0.165 mg/kg 024348
Fluoranthene ND 0.33 0.165 mg/kg 024348
Fluorene ND 0.33 0.165 mg/kg 024348
Hexachlorobenzene ND 0.33 0.165 mg/kg 024348
Hexachlorobutadiene ND 0.33 0.165 mg/kg 024348
I-Iexachlorocyclopentadiene ND 0.33 0.165 mg/kg 024348
Hexachioroethane ND 0.33 0.165 mg/kg Q24348
Indeno123-cdpyrene ND 0.33 0.165 mg/kg 024348
Isophorone ND 0.33 0.165 mg/kg 024348
N-Nitrosodi-n-propylamine ND 0.33 0.165 mg/kg 024348
N-Nitrosodiphenylamine MD 0.33 0.165 mg/kg 024348
Naphthalene ND 0.33 0.165 mg/kg 024348
Nitrobenzene ND 0.33 0.165 mg/kg 024348
Pentachlorophenol ND 1.65 0.825 mg/kg 024348
Phenanthrene ND 0.33 0.165 mg/kg 024348
Phenol ND 0.33 0.165 mg/kg 024348
Pyrene ND 0.33 0.165 mg/kg Q24348
Laboratory Control Sample Recovey Recover QC SaIth
Result Spike Motint Units PU
124-Thchojtbenzene 1.39016 1.6620 mg/kg 84 39-98 Q24348
14-Dichlorobenzene 1.27185 1.6620 mg/kg 77 37-95 024348
24-Dinitrotoluene 1.72881 1.6620 mg/kg 104 56-128 024348
2-Chlorophenol 1.30242 1.6620 mg/kg 78 37-98 024348
4-Chloro-3-methylphenol 1.47391 1.6620 mg/kg 89 45-111 024348
This report should not be reproduced except In its entirety without the wiitten consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Chaulotte MC 282240543
Phone 704/529-6364 Toll Free Number 1-3001529-6364 Fax 704/525-0409 Page of
This report should not be reproduced except in its entirety without The written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800I529..6364 Fax 7041525-0409
Full SeniceAnaIytlal Environmental Sthfllon
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Project ID Morehead Commons No
Level II QC Report
6/25/07
COC Group Number 00607392
DatelTime Submitted 6113/07 1545
Laboratory Control Sample Recovery Recovery QC BaRanges
Result Spike
Amount Units
4-Nitrophenol 2.24094 1.6620 mg/kg 135 20-157 024348
Acenaphthene .521 43 1.6620 mg/kg 92 44-110 024348
N-Nitrosodi-n-propylarnine 1.32436 1.6620 mg/kg 80 38-101 024348
Pentachlorophenol 2.01495 1.6620 mg/kg 121 53-127
024348
Phenol 1.21801 1.6620 mg/kg 73 34-102 024348
Pyrene 1.51944 1.6620 mg/kg 91 54-131 024348
Matrix Spike Recovety Recovery QC BatchRanges
Sample ID Result Spike
Amount Units ID
184315 124-Trichtorobenzene 1.35823 1.6603 mg/kg 82 26-97 Q24348
14-Dichlorobenzene 127124 1.6603 mg/kg 77 23-92 024348
24-Dinitrotoluerie 1.85292 1.6603 mg/kg 112 45-127
024348
2-Chlorophenol 1.301 79 1.6603 mg/kg 78 25-94 024348
4-Chloro-3-methylphenol 1.64774 1.6603 mg/kg 99 31-113 Q24348
4-Nitrophenol 2.07835 1.6603 mg/kg 125 17-150 024348
Acenaphthene 158366 1.6603 mg/kg 95 36-107 024348
N-Nitrosodi-n-propylamino 1.50332 1.6603 mg/kg 91 22-1 05 024348
Pentathlonphenol 2.03353 1.6603 mg/kg 122 39-137 024348
Phenol 1.24302 1.6603 mg/kg 75 23-97 024348
Pyrene 1.77954 1.6603 mg/kg 107 45-133 Q24348
Matrix Spike Duplicate Reco Recovery RPD
Ranges RPD Range QC Batch
Sample Itk Result Spike Amesrit Units
184315 24-Tnchlorobenzene 1.26892 1.6603 mg/kg 76 26-97 -37 024348
14-Dichlorobenzene 119223 1.6603 mg/kg 72 23-92 0-36 024348
24-Dinitrotoluene 1.75298 1.6603 mg/kg 106 45-127 0-29 024348
2-Chiorophenol 1.20019 1.6603 mg/kg 72 25-94 0-37 024348
4-Chloro-3-methylphenol 1.49535 1.6603 mg/kg 90 31-113 10 0-32 024348
4-Nitrophenol 2.22045 1.6603 mg/kg 134 17-150 -32 Q24348
Acenaphthene 1.45252 1.6603 mg/kg 87 36-1 07 0-32 024348
N-Nitrosodi-n-propylamine 1.27954 1.6603 mg/kg 77 22-1 05 16 0-37 024348
Pentachlorophenol 1.97908 1.6603 mg/kg 119 39-137 0-27 024348
Phenol .202 19 1.6603 mg/kg 72 23-97 0-42 024348
Pyrene 1.57270 1.6603 mg/kg 95 45-133 12 0-27 024348
Page of
NC Certificaon No 402
Sc Certificalion No 99012
NC Drinking Water Cert No 37735
ESP Associates PA Project ID Morehead Commons No
Attn Chris Ward
Box 7030
Charlotte NC28241
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-6364 Toll Free Number 1-8001529-6364 Fax 7041525-0409
Full rvlceAmalyaI Ewlrenmenlal Solutions
Level II QC Report
6125/07
COG Group Number
Date/Time Submitted
by GC.PID/FID method
MAflP VPH
G0607392
6/13/07 1545
Method Blank QC Batch
Result RL Control Limit Units ID
C5-CBAliphatics ND 2.5 mg/kg 024410
C9-C10 Aromatics ND 2.5 mg/kg Q24410
C9-C12 Aliphatics ND 2.5 mg/kg 024410
Laboratory Control Sample Rver Recovery QCRanges
Result Spike Amount Units ID
C5-C8Aliphalics 16.564 15 mg/kg 110 70-130 024410
C9-Cl0Aromatics 5.780 mg/kg 116 70-130 024410
C9-Cl2Aliphatics 11.106 10 mg/kg 111 70-130 Q24410
Matrix Spike Recovery Recovery QC BatchRanges
Sample ID Result Spike
Amount Units 1k ID
183776 C5-CBAliphalics 16.758 15 mg/kg 112 70-130 024410
C9-C10 Arornatics 5.291 mg/kg 106 70-130 024410
C9-Cl2Aliphatics 11.837 10 mg/kg 118 70-130 024410
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RP1 Range QC Batch
sample 1D Result Spike Amount Units 1k ID
183776 C5-C8 Atiphatics 19.497 15 mg/kg 130 70-130 15 0-25 024410
C9-C10 Aromatics 5.249 mg/kg 105 70-1 30 -25 024410
C9-Cl2Aliphatics 12.558 10 mg/kg 126 70-130 0-25 024410
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charfotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Level II QC Report
6/25/07
COC Group Number G0607392
DatelTime Submitted
6113/07 1545
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 7041525-0449
__I
Furl .me ArityrIcal EnTtninoriI 5tutins
tFIfl EPH....flVUIUUWUUuI UT
Method Blank 00 Batch
Result RL Control Umit Units ID
Cl l-C22 Aromatics MD 10 mg/kg 024425
C19-C36AIiphaiics ND 10 mg/kg 024425
C9-C1 Aliphatics ND 10 mg/kg 024425
Laboratory Control Sample Recovery RecoverY QC Batch
Result Spike Amount Units
C11-C22Aromatics 152.84 170 mg/kg 90 40-140 024425
C19-C36Aliphatics 67.34 80 mg/kg 84 40-140 Q24425
C9-C18 Aliphatics 47.44 60 mg/kg 79 40-140 024425
Matrix Spike Recovery 00 Batch
Sample ID Result SpikeArnount Units ID
184329 Cl 1-C22 Arornatics 174.78 170 mg/kg 103 40-140 024425
C19-C36 Atiphatics 61.66 80 mg/kg 77 40-140 024425
C9-C18 Aliphatics 44.08 60 mg/kg 73 40-140 024425
Matrix Spike Duplicate Recovery Recovery RPD Range QC Batch
Sample ii Result Spike Amount Units 9u ID
184329 Cl 1-022 Arornatics 162.54 170 mg/kg 96 40-140 0-50 024425
C19-C36 Atiphatics 61.88 80 mg/kg 77 40-140 0-50 024425
C9-C18 Aliphatics 42.84 60 mg/kg 71 40-140
0-50 024425
-See Case Narrative
Page of
NPDES UJ GROUNDWATER
ONC USC NC.0SC ONC OSO________
Requested Due Date Day 02 Days 03 Days 4.Days
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Working Days 06-9 Days Standard 10 days us ust Be
Samples received after 15bO will be processed next business day
Turnaround time is based on business days excluding weekends and holidays
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CUent Company Name J/V cqi.i4
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CHAIN OF CUSTODY RECORD
PAGE _/_OF _.L QUO EN USE
ILLING
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please ATTACH arty project specific
reporting QC LEVEL 111111 IV
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invoice To Id ii
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TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC__USACE_FL____NC_IL
SC__OTHER ______N/A _____
Water Chlorinated YES_NO
Sample Iced Upon Collection YES _Z$lO
CLIENT
SAMPLE DESCRIPTION
Ui
W52
-4-I
DATE
COLLECTED
-/-C
TIME
COLLECTED
MILITARY
tW/i
/4oz/4j
MATRIX
SOILWATER OR
SAMPLE CONTAINER PRESERVA-
TIVES
tJ ftALY
ifLIL_
LJ_
SES UESTED PRISM
LAB
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.-c
3Lc
SEE BELOW NO SIZE
-______.r
Raiinqulsflecl by uignature
Saples Signature Sampled By Print Name Afffflaon 5P
Upon relinquishing this Chiof CustoSs your authorization forPrism to proceed with the analyses as requested above Any changes
must be
submitted in writIng to the Prism Project Manager There will be charges for any changes after analyses have been InitIalIzed
Miiihn/I1flflReceivedBySi9fltUtDate
Relinquish
Relinquish
Method
Fed Ex
ad By Sig
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nature
re/
SAM.kES ARE NO
1nd.deIivered
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TED SH UUSTODY SEALS FOR
TRANSPORTATION TO THE LABORATORY
lED AGAINST UNTIL RECEIVED AT THE LABORATORY
Other
Date
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COO roup No
Additional Comments
DRINKING WATER SOLiD WASTE RCRA CERCLA LANDFILL OTHER
Owe USC ONC USC ONC OSCI ONC USC UNC USC
UNC DSC_____________o10 ________ ____
SEE REVERSE FORTERMSCONDITIONS
ORIGINAL
Case Narrative
Piusivi
LA3ORATOlIES.INC
Date 06/05107 Client Project ID Morehead Commons No
Company ESP Associates PA Piism COC Group No 00507786
Contact Chris Ward Collection Dates 05/29/07
Address Box 7030 Lab Submittal Dates 05/29/07
Chariotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report
and Quality
Control Data totaling 14 pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Quality
control statements andlor sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
No Anomalies Reported
Metals Analysis
Analysis Note for Q23929 MS Chromium MS recovery outside of the control limits Post-digstion spike recovery 81%is within
the acceptance limits 75-125%
Analysis Note for Q23929 MS Lead MS recovery outside of the control limits Post-digstion spike recovery 81%is within the
acceptance limits 75-125%
Analysis Note for Q23929 MSD Lead Matrix interference is suspected
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by Paula Gilleland Project Manager AngelgD vercash
Signature a..uS .\h.kck Signature
Review Date 06/05/07 Approval Date 06/05107
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identilied but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect is present
Notes This report should not be reproduced except in its entirety without the wiittten consent of Prism Laboratories Inc The resuJts in this
report relate only to the samples submitted for analysis
449 SprtngbiDok Road P.0 Box 240543 Chajlotte NC 28224-0403
Phone 704/529.6364 Toll Free 800/529-6364 Fax 704/529-0409
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 06105107
Project ID Morehead Commons No Client Sample ID SP-3
Prism Sample ID 182794
Sample Matrix Soil COG Group G0507786
Time Collected 05/29/07 1430
Time Submitted 05/29/07 1520
Parameter Result Units Report MDL Dilution Method
Limit Factor
Analysis Analyst
Batch
Date/Time
Percent Solids DethrminHnn
Percent Solids 85.4 SM2540 05131107 1450 atliso
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road .-P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409
ESP Associates PA
Attn Chris Ward
0.Box 7030
Charlotte NC 28241
Orcianochiorine Pesticides by Gas Chromatography
44-DDD BRL pg/kg 2.3 0.71 8081A 06/05/07 759 ivogel 024026
44-DDE BRL pg/kg 2.3 0.50 8081A 06/05/07 759 Jvogel 024026
44-DDT BRL pg/kg 2.3 0.84 8081A 06/05/07 759 ivogel 024026
44-Methoxychlor BRL pg/kg 4.7 1.6 8081A 06/05/07 759 Ivogel 024026
a-BHC BRL pg/kg 2.3 0.21 8081A 06/05/07 759 Jvogel 024026
a-Chlordane BRL pg/kg 2.3 0.41 8081A 06/05107 759 Jvogel 024026
/Jdrin BRL pg/kg 2.3 0.47 8081A 06/05/07 759 jvogel 024026
b-BHC BRL pg/kg 2.3 0.59 8081A 06/05/07 759 jvogel 024026
Chiordane BRL pg/kg 59 13 8081A 06/05101 759 jvogel 024026
d-BFIC BRL pg/kg 2.3 0.33 8081A 06/05107 759 vogel 024026
Dieldrin BRL pg/kg 1.2 0.49 8081A 06/05/07 759 Jvogel 024026
Endosulfan BRL pg/kg 2.3 0.42 8081A 06/05/07 759 Jvogel 024026
Endosulfan II BRL pg/kg 2.3 0.53 8081A 06/05107 759 Jvogel 024026
Endosulfan Sulfate BRL pg/kg 2.3 0.61 8081A 06/05/07 759 .ivogel 024026
Endrin BRL pg/kg 2.3 0.70 8081A 06/05/07 759 Ivogel 024026
EndrinAldehyde BRL pg/kg 2.3 0.66 8081A 06/05/07 759 jvogel 024026
Endrin Ketone BRL pg/kg 2.3 0.46 8081A 06/05/07 759 jvogel 024026
g-Bl-IC BRL pg/kg 2.3 0.27 8081A 06/05/07 759 jvogel 024026
g-Chlordane BRL pg/kg 2.3 0.38 8081A 06/05/07 759 lvogel 024026
Heptachior BRL pg/kg 2.3 0.55 8081A 06/05/07 759 Jvogel 024025
Heptachior Epoxide BRL pg/kg 2.3 0.43 8081A 06105/07 759 jvogel 024026
Toxaphene BRL pg/kg 59 13 8081A 06/05/07 759 jvogel 024026
Page of
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Sample Preparation 30.02 10 mL 355GB 05/30/07 1100 Jvogel P18490
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-8001529.6364 Fax 704/525-0409
Laboratory Report
06/05/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID SP-3
Attn Chris Ward Prism Sample ID 182794
Box 7030 Sample Matrix Soil COG Group 00507786
Charlotte NC 28241 Time Collected 05/29/07 1430
Time Submitted 05129/07 1520
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
30.02 lOraL 3550B 05/30/07 1100 Jvogel P1 8489SamplePreparation
Polychlorinated Biphenyls PCBs by GC-ECD
PCB-1016 BRL
PCB-1221 BRL
PCB-1232 BRL
PCB-1242 BRL
PCB-1248 BRL
PCB-1254 BRL
PCB-1260 BRL
Surrogate Recovery Control Limits
Tetrachloro-m-xylene TCMX 90 40 162
Decachiorobiphenyl 0GB 114 26 204
0.059
0.12
0.059
0.059
0.059
0.059
0.059
0.011
0.047
0.019
0.020
0.0081
0.020
0.016
8082
8082
8082
8082
8082
8082
8082
06/05/07 759
06/0507 759
06/05/07 759
06/05/07 759
06/05/07 759
06l05/07 759
06/05/07 759
jvogel
jvogel
jvogel
jvogel
jvogel
jvogel
jvoge
024024
024024
024024
024024
024024
024024
Q24024
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
Surrogate Recovery Control Limits
Decachiorobiphenyl 0GB 115 34 182
Tetrachloro-m-xylene TCMX 91 36 182
Volatile Organic Compounds by GC/MS
111 2-Tetrachloroethane
11 1-Trichloroethane
11 22-Tetrachloroethane
11 2-Trichloroethane
11-Dichioroethane
1-Dichloroethene
1-Dichloropropene
23-Trichlorobenzene
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
5.3 0.52
5.3 0.30
5.3 0.54
5.3 0.33
5.3 0.38
5.3 0.40
5.3 0.47
11 0.58
8260B
8260B
826GB
82608
82603
8260B
82608
82608
05/31/07 029
05/31/07 029
05/31/07 029
05/31107 029
05/31/07 029
05/3 1/07 029
05/31/07 029
05/31/07 029
erussell
erussell
enissell
ezussell
erussell
erussell
erusset
erussell
Q23880
Q23880
023880
Q23880
023880
023880
023880
023880
Page of
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID SP3
Prism Sample ID 182794
Sample Matrix Soil COC Group G0507786
Time Collected 05/29/07 1430
Time Submitted 05/29/07 1520
Bromomethane
Carbon disulfide
Carbon tetrachioride
BRL pg/kg
BRL pg/kg
5.4 pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
2.2 pg/kg
BRL pg/kg
BRL pg/kg
BRI pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
29 pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
8RL pg/kg
BRL pg/kg
5.3 0.47
11 0.51
11 0.40
5.3 0.84
5.3 0.096
11 0.29
5.3 0.53
5.3 0.39
11 0.45
11 0.46
5.3 0.36
11 0.41
5.3 0.27
11 0.39
11 0.39
53 0.55
11 0.28
11 0.53
21 2.1
3.2 0.43
5.3 0.37
5.3 0.32
5.3 0.47
5.3 0.39
11 0.62
11 0.34
5.3 0.31
05/31/07 029 erus5eH
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 enissell
05/31/07 029 erusseH
05/31/07 029 erussell
05/31/07 029 erussell
05131/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussefl
05/31/07 029 erusseD
05/31/07 029 enissell
05/3107 029 erussell
05/31107 029 enissefl
05131/07 029 erusset
05/3107 029 erussell
05/31/07 029 erussefl
05/31/07 029 erusseU
826GB 05/31/07 029 erusset
826GB 05/31/07 029 erussell
Q23880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023680
023880
023880
023880
023880
023880
023880
023880
023880
Q23680
023880
023880
023880
023880
023880
023880
023880
This report should not be reproduced except in its entFrety without the written consent of Prism Laboratories Iris
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
06/05/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
23-Trichloropropane
24-Trichlorobenzene
24-Tiimethylbenzene
2-Dibronio-3-choropropane
2-Dibromoethane EDB
2Dichlorobenzene
2-Dichloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichlorobenzene
22-Dichioropropane
2-Chioroethyl vinyl ether
2-Chlorotoluene
2-Hexanone
4-Chiorotoluene
4-Methyl-2-pentanone MIBK
Acetone
Benzene
Bromobenzeæe
Bromochloromethane
Bromodichloromethane
Bromoform
826GB
8260B
826GB
826GB
826GB
826GB
826GB
8260B
82608
826GB
8260B
8260B
82608
826GB
826GB
826GB
826GB
82608
82608
82608
8260B
826GB
826GB
826GB
82608
Page of
NC Certification No 402
SC Certification No 99012 Laboratory Report
NC Drinking Water Cert No 37735
BRL
BRL
BRL
BRI
BRL
BRI
BRL
BRI
BRI
BRI
BRL
BRI
BRL
BRL
BRL
BRL
BRL
4.1
BRL
24
BRL
BRI
6.3J
BRL
BRL
BRL
BRL
Project ID Morehead Commons No Client Sample ID SP-3
Prism Sample ID 182794
Sample Matrix Soil COC Group 00507786
Time Collected 05129/07 1430
Time Submitted 05/29/07 1520
8260B
82608
8260B
826GB
826GB
8260B
8260B
8260B
8260B
8260B
8260B
82603
8260B
82608
8260B
8260B
82603
826GB
8260B
8260B
8260B
8260B
8260B
82608
8260B
8260B
82608
05/31/07 029 eru3sefl
05/31/07 029 erussell
05/31/07 029 eJussell
05/31/07 029 erussell
05/31/07 029 enissell
05131107 029 erussell
05/31/07 029 erussefl
05/31/07 029 erussl
05/31/07 029 erusset
05/31/07 029 erusset
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erusselt
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erusseil
05/31/07 029 enissell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussell
05/31/07 029 erussefl
05/31/07 029 erussell
05/31/07 029 enissell
05/31/07 029 erussell
05/31/07 029 erussefl
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
Q23880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023880
Q23880
023880
023880
023880
023880
023880
023880
023880
Q23680
023880
023860
023880
023880
023880
023680
023880
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
06/05/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Chlorobenzene
Clilorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1 2-Dichloroetherie
cis-1 3-Dichloropropene
Dibromomethane
Dichiorodifluoromethane
Ethylbenzene
Hexachiorobutadiene
lsopropyl ether IPE
lsopropylbenzene
m.p-Xylenes
Meth1 ethyl ketone MEK
Methyl t-butyl ether MTBE
Methylene chloride
n-Butylbenzene
n-Propylbenzene
Nlaphthalene
o-Xylene
p-lsopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachioroethene
Toluene
pg/kg 5.3 0.40
pg/kg 5.3 0.36
pg/kg 11 0.44
pg/kg 5.3 0.39
pg/kg 11 0.37
pg/kg 5.3 0.23
pg/kg 5.3 0.34
pg/kg 5.3 0.39
pg/kg 11 1.2
pg/kg 5.3 0.37
pg/kg 16 0.66
pg/kg 5.3 0.18
pg/kg 11 0.43
pg/kg 11 0.74
pg/kg 21 1.5
pg/kg 5.3 0.31
pg/kg 11 0.44
pg/kg 16 0.43
pg/kg 11 0.32
pg/kg 5.3 0.62
pg/kg 5.3 0.32
pg/kg 16 0.44
pg/kg 16 0.35
pg/kg 5.3 0.53
pg/kg 21 0.33
pg/kg 11 0.91
pg/kg 5.3 0.36
Page 4of6
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/05/07
SP-3
182794
G0507786
05/29/07 1430
05129/07 1520
5035
5035
5035
06101/07 000 Ibrown
06/01/07 000 Ibrown
06/01/07 000 Ibrown
Oil and Grease by Soxhiet Extraction
Od and Grease 270 mg/kg 41 32 9071A 06/04/07 700 smanivanh 024000
Sample Preparation
Sample Weight Determination
Weight
Weight
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409
FuISgvkeAtatytiaI Envhonment3t
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method
Limit Factor
Analyst Batch
ID
trans-I 2-Dichloroethene BRL pg/kg 5.3 0.40 8260B
trans-I 3-Dichloropropene BRL pg/kg 5.3 0.37 8260B
Trichloroethene BRL pg/kg 5.3 0.32 8260B
Trlchiorofluoromethane BRL pg/kg 5.3 0.44
626GB
Vinyl chloride BRL pg/kg 11 0.68 8260B
Analysis
Date/Time
05131/07 029
05131/07 029
05131/07 029
05/31/07 029
05/31/07 029
erussell
erusselt
erussell
erusseli
emssell
023880
023880
023880
023880
023880
Surrogate Recovery Control Limits
Bromofluorobenzene 105 77-128
Dibromofluoromethane 101 67-143
Toluene-d8 97 81 128
Sample Weight Determination
Weight Bisulfate 5.51
Weight Blsulfate 5.66
Weight Methanol 5.23
Diesel Range Organics 1DR0 by GC-FJD
Diesel Range Organics DRO 140 mg/kg 8.2 1.0 8015B 06/04107 1209 jvogel Q23955
25.04 mL 3545 05/31/07 1100 onder P18515
5.55
5.45
Surrogate Recovery Control Limits
o-Terphenyl 92 49 124
CR0 06/04/07 000 Ibrown
GRO 06/04/07 000 Ibrown
Page of
Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
SP-3
182794
G0507786
05129/07 1430
05/29/07 1520
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Dale/Time ID
Gasoline Range Orianics GRO by GC-FID
Gasoline Range Organics GRO 23 mg/kg 5-9 0.61 50 801 SB 05/31/07 416 hwagner 023897
Surrogate Recovery Control Limits
aaa-TFT 86 55-129
Metals by iCR
Chromium 26 mg/kg 0.58 0.035 60103 05/31/07 2257 mcampbell 023929
Lead 35 mg/kg 0.58 0.048 6010B 05/31/07 2257 mcampbell 023929
Sample Preparation 2.03 50 mL 3050B 05/31/07 750 jhoppel P18497
Sample Comments
BRL Be/ow Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances
indicated in the case narrative and/or test comments
All results are reported on dr/-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 23224-0543
ESP Associates PA
AUn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Sample Matrix Soil
Laboratory Report
06/05/07
Angela Overcash V.P Laboratory Services
Phone 7041529-6364 Toll Free Number 1-800/529-6364 Fax 7041525-0409 Page of
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
L.VQJaUI JIgIuI I.uulspuuIIu tJy
Method Blank OC Batch
Result RL Control Limit Units ID
11 I-Trichloroethane
11 22-Tetrachloroethane
11 2-Trichloroethane
1-Dichioroethane
1-Dichloroethene
1-Dichloropropene
23-Trichlorobenzene
23-Trichloropropane
24-Trichlorobenzene
124-Trimethylbenzene
2-Dibromoethane EDB
2-Dichlorobenzene
12-Dichioroethane
2-Dichloropropane
135-Trimethylbenzene
13-Dichlorobenzene
13-Dichioropropane
4-Dichlorobenzene
22-Dichioropropane
2-Chlorotoluene
2-Hexanone
4-Chiorotoluene
4-Methyl-2-pentanorie MIBK
Acetone
Benzene
Bromobenzene
Brornochlorometharte
Bromodichioromethane
Bromoform
Brornomethane
Carbon tetrachioride
Chlorobenzene
Chiorodibrornomethane
Chioroethane
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
MD 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.05 0.025
ND 0.005 0.0025
ND 0.05 0.025
ND 0.05 0.025
ND 0.003 0.0015
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.01 0.005
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.01 0.005
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Q23880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023880
Q23880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023880
023880
Q23880
023880
023880
023880
023880
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240643 Charlotte NC 28224-0543
Phone 704/529-5364 Toll Free Numbec 1-800/529.6364 Fax 7041525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6/5107
Project ID Morehead Commons No COC Group Number G0507786
Date/Time Submitted 5129/07 1520
Page of
NC Certificaflon No 402
SC Certification No 99012
NC Drinking Water CerL No 37735
Method Blank ac
Result RL Control limit Units ID
Chloroform ND 0.005 0.0025 mg/kg Q23880
Chloromethane ND 0.005 0.0025 mg/kg Q23880
cis-1 2-Dichloroetherie ND 0.005 0.0025 mg/kg 023880
cis-i3-Dichloropropene ND 0.005 0.0025 mg/kg 023880
Dichlorodifluoromethane ND 0.005 0.0025 mg/kg 023881
Ethylbenzene ND 0.005 0.0025 mg/kg 023880
Isopropyl ether IPE ND 0.005 0.0025 mg/kg 023880
lsopropylbenzene ND 0.005 0.0025 mg/kg 023880
mp-Xylenes ND 0.01 0.005 mg/kg 023880
Methyl ethyl ketone MEK ND 0.1 0.05 mg/kg 023880
Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg 023880
Methylene chloride ND 0.005 0.0025 mg/kg 023881
n-Butyibenzene ND 0.005 0.0025 mg/kg 023880
n-Propylbenzene ND 0.005 0.0025 mg/kg 023880
Naphthalene ND 0.01 0.005 mg/kg 023880
o-Xylene ND 0.005 0.0025 mg/kg 023880
p-lsopropyltoluene ND 0.005 0.0025 mg/kg 023880
sec-Butylbenzene NI 0.005 0.0025 mg/kg 023880
Styrene NI 0.005 0.0025 mg/kg 023880
Lert-Butylbenzene ND 0.005 0.0025 mg/kg 023880
Tetrathloroethene ND 0.005 0.0025 mg/kg 023880
Toluene NI 0.005 0.0025 mg/kg 023880
trans-i 2-Dichloroethene ND 0.005 0.0025 mg/kg 023860
trans-i 3-Dichloropropene ND 0.005 0.0025 mg/kg Q23880
Trichlorocihene ND 0.005 0.0025 mg/kg 023880
Trichiorofluoromethane ND 0.005 0.0025 mg/kg 023880
Vinyl acetate ND 0.025 0.01 25 mg/kg 023880
Vinyl chloride Nt 0.005 0.0025 mg/kg 023880
Laboratory Control Sample Recovery
Result Spike
Amount Units ID
11-Dichloroethene 0.05073 0.05 mg/kg 101
57-122 023880
Benzene 0.04917 0.05 mg/kg 98 62-119 023880
Chlorobenzerie 0.04957 0.05 mg/kg 99 61-124 023880
Toluene 0.04974 0.05 mg/kg 99 57-1 22 023880
Trichloroethene 0.05313 0.05 mg/kg 106 59-129 Q23880
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Level 11 QC Report
615/07
Project ID Moreheaci Commons No COC Group Number 00507786
Date/Time Submitted 5129107 1520
Page of
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
182585 Gasoline Range Organics GR 46.6 50 mg/kg 93 57-113 10 0-23 023897
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Spnngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-6364 Toll Free Number 1-8001529-6364 Fax 7041525-0409
ESP Associates PA
Atm Chris Ward
Box 7030
Charlotte NC 28241
Level II QC Report
6/5/07
Project ID Morehead Commons No COC Group Number G0507786
Date/Time Submitted
5129/07 1520
Matrix Spike Recovery Recovery cCRangesResultSpikeAmountUnitsSampleID
182653 11-Dichloroethene 0.04636 0.05 mg/kg 93 44-140 023880
Benzene 0.0468 0.05 mg/kg 94 46-1 36 023880
Chlorobenzene 0.04473 0.05 mg/kg 89 47-1 35 023880
Toluene 0.04502 0.05 mg/kg 90 47-1 36 Q23880
Trichioroethene 0.04446 0.05 mg/kg 89 45-141 023880
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range
Sample ID Resuft Spike Amount Units
182653 11-Dichloroethene 0.04718 0.05 mg/kg 94 44-140 0-23 Q23880
Benzene 0.04679 0.05 mg/kg 94 46-136 0-22 023880
Chlorobenzene 0.04475 0.05 mg/kg 90 47-1 35 -22 023880
Toluene 0.04557 0.05 mg/kg 91 47-136 0-22 023880
Trichloroethene 0.04564 0.05 mg/kg 91 45-1 41 0-23 023880
Gasoline Range Organics GRO by GC-FID method 8015B
Method Blank QC Batch
Result RL Control Limit Units ID
Gasoline Range Organics GR ND 2.5 mg/kg Q23897
Laboratory Control Sample Recovery Ranges cc Batch
IDResultSpikeAmountlinus
Gasoline Range OrganicsGR
47.35 50 mg/kg 95 67-116 023897
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample 10 Result Spike Amount Units II
182585 Gasoline Range Organics GR 51.45 50 mg/kg 103 57-113 023897
Matrix Spike Duplicate Recovery Recoverr RPD
0tchRangesRPDRange
Sample ID Result Spike Amount UnitS
Page of
ESP Associates PA
Attn Chris
Ward
Box 7030
Charlotte NC 28241
MtaIs 1w ICP BOIOB
182472 DIesel Range Organics DRO 92.8 80 mg/kg 82 50-117 22 0-24 023966
This report should not be reproduced except in its entirety without the written consent of Prism Laborotories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-6364 Toll Free Number 1-8001529-6364 Fax 7041525-0409
Pu.ie AnalytimIS Envirenmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level 11 QC Report
615107
Project ID Morehead Commons No COC Group Number G0507786
DatelTime Submitted 5/29/07 1520
Method Blank ctc Batch
Result RL Control Limit Units ID
Chromium 0.0273 0.25 0.125 mg/kg 023929
Lead -0.0246 0.25
0.125 mg/kg 023929
Laboratory Control Sample Recovery Recovery QC BelchRanges
Result Spike Amount Units 10
Chromium 23.8683 25 mg/kg 95 9-12O
023929
Lead 23.5127 25 mg/kg 94 80-120 023929
Matrix Spike Recovery Recovery
Ranges
Sample ID Result Spike
Amount Units ID
182794 Chromium
561913 24.630 mg/kg 138 75-125 Q23929
Lead 28.7777 24.630 mg/kg -5 75-125 Q23929
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range OC Batch
Sample ID Result Spike Amount Units ID
182794 Chromium 47.9427 24.875 mg/kg 103 75-125 16 0-20 Q23929
Lead 27.7151 24.875 mg/kg -10 75-125 -20 023929
Diesel Range Organics IDRO by OC-FID method 801 SB
Method Blank QCBatth
Result RL Control Umit Units ID
Diesel Range Organics DRO ND 3.5 mg/kg Q23966
Laboratory Control Sample Recovery Recovery DC Batch
Result Spike Amount Units
Ranges
Diesel Range Organics DRO 58.6 80 mg/kg 73 55-109 023966
Matrix Spike Recovery
Ranges DC Batch
Sample ID Result Spike Amount Units 15 ID
182472 Diesel Range Organics DRO 74.5 80 mg/kg 59 50-117 023966
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPO Range DC Batch
Sample ID Result Spike Amount Units It
Page4of7
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should riot be repreduced except in its entirety without the written óonsent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte1 NC 28224-0543
Phone 7041529-6364 Toll Free Number 1.800/529-6364 Fax 704/525-0409
ESP Associates PA
Attn Chris
Ward
Box 7030
Charlotte NC 28241
Level II QC Report
6/5107
Project ID Morehead Commons No COC Group Number 00507786
Date/Time Submitted
5/29/07 1520
Oil ----mmthnd O71A-oeone IJv
Method Blank CC Batch
Result RI Control Limit Units ID
Oil and Grease ND 35 17.5 mg/kg 024000
Laboratory Control Sample Recovay Recovery oc BatchRangesIDResultSpikeAmountUnits
Oil and Grease 4933 4899 mg/kg 101 80-120
Q24000
Matrix Spike Recovery oceatch
Ranges
Sample lL Result Spike Amount Units ID
182049 Oil and Grease 27420 24295 mg/kg 100 80-120 024000
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range QC BatCh
ItSampleIDResult Spike Amount Units
182049 Oil and Grease 30660 24653 mg/kg 112 80-120 11 0-20 Q24000
Polychiorinated Blohenvis PCBs by GC-ECD method 8082
Method Blank CC Batch
Result RL Control Limit Units
PCB-1016 ND 0.05 0.025 mg/kg 024024
PCB-1221 ND 0.1 0.05 mg/kg 024024
PCB-1232 ND 0.05 0.025 mg/kg 024024
PCB-1 242 ND 0.05 0.025 mg/kg Q24024
PCB-1248 ND 0.05 0.025 mg/kg 024024
PCB-1254 ND 0.05 0.025 mg/kg 024024
PCB-l 260 ND 0.05 0.025 mg/kg 024024
Laboratory Control Sample Recovery Recovery
Ranges IDResultSpikeAmountUnitS70
PCB-1016 0.351 0.333 mg/kg 105 61-151
024024
PCB-1 260 0.365 0.333 mg/kg 110 45-166 Q24024
Matrix Spike Recovery Recovery
Ranges CC B3tCh
Sample ID Result Spike Amount Units II
182794 PCB-1016 0.330 0.333 mg/kg 99 14-192 024024
PCB-1260 0.416 0.333 mg/kg 125 10-192 024024
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPI Range QC Batch
Sample ID Result Spike Amount Units ID
182794 PCB-1016 0.347 0.333 mg/kg 104 14-192 0-40 024024
PCB-1 260 0.361 0.333 mg/kg 108 10-1 92 14 0-40 024024
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Level II QC Report
6/5/07
COC Group Number G0507786
Date/Time Submitted
5129107 1520
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Spnngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-6354 Toll Free Number 1-8001529-6364 Fax 7041525-0409
by Gas nighnd RC1A.11 304 Id.IIIdIflUI
Method Blank 00 Batch
Result RL ContrOl Umit Units ID
44-DDD ND pg/kg 024026
44-DDE ND pg/kg 024026
44-DDT ND pg/kg 024026
44-Methoxychlor ND ijglkg 024026
a-BHC ND pg/kg 024026
a-Chlordane ND pg/kg 024026
Atdiin ND pg/kg 024026
b-BHC ND pg/kg 024026
Chiordane ND 50 25 pg/kg 024026
d-BHC ND pg/kg 024026
Dieldrin NI 0.5 pg/kg 024026
Endosulfan ND pg/kg 024026
Endosulfan II ND pg/kg 024026
Endosulfan Sulfate ND pg/kg 024026
Endrin ND pg/kg 024026
Endrin Aldehyde ND pg/kg 024026
Endrin Ketone ND pg/kg 024026
g-BHC ND pg/kg 024026
g-Chtordane ND pg/kg 024026
Heptachiom NI pg/kg Q24026
1-leptachlor Epoxide ND pg/kg 024026
Toxaphene ND 50 25 pg/kg 024026
Laboratory Control Sample Recovery Recovery
RangesResultSpikeAmountUnits
44-DDT 36.117 33 pg/kg i09 75-141 024026
Aldrin 39.657 33 pg/kg 120 66-132 024026
Dieldrin 37.597 33 pg/kg 114 72-1 36 024026
Endrin 37.507 33 pg/kg 114 74-147 024026
Heptachlor 38.32 33 pg/kg 116 72-134 024026
Matrix Spike Recovery Recovery OCBatchRanges
Sample Result SpikeAmount Units
182794 44-DDT 32.1 33 pg/kg 97 56-1 63 024026
AIdrin 34.3 33 pg/kg 104 57-137 024026
Dieldiin 33.9 33 pg/Kg 103 60-141 024026
Page of
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
.See Case Narrative
This report should not be reproduced except in its entirety without The written consent of Prism Laboratories Inc
449 Sprirtgbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toil Free Number 1.8001529-6364 Fax 7041525-0409
Full Survicu Anulytlcl Eiwlronmuril1r
NC Certification No.402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6/5/07
Project ID Morehead Commons No COC Group Number G0507786
Dateilime Submitted 5129/07 1520
Matrix Spike Recovery Recovery QODatciRanges
Sample ID Result Spike Amount Units ID
182794 Endrin 31.8 33 pg/kg 96 65-164 024025
Heptachlor 33.5 33 pglkg 102 63-142
024026
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range OC Batch
sample ID Result Spike Amount Units 16 ID
182794 44-DDT 29.3 33 pg/kg 89 56-1 63 0-38 024026
Aldrin 35.3 33 pg/kg 107 57-1 37 0-29 024026
Dieldrin 32.9 33 pg/kg 100 60-1 41 -30 024026
Endrin 30.5 33 pglkg 92 65-164 -21 024026
Heptachlor 35.9 33 pg/kg 109 63-1 42 0-27 024026
Page of
Full Service AnelyUcal Envinnmentai Solutions
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Fax 704/525-
Client Company Name .fr4a.hS
Report To/Contact Name
Reporting Address .-c__
CHAIN OF CUSTODY RECORD
QUOT If TO NSURE
BILUNG.PAGE..LOF_L
Project Name
Short Hold Analysis Yes No LIST Project Yes No
please ATTACH any project specific reporting
QO LEVEL 111111 IV
provisions and/or Q9_RquiempInvoiceTo
Address 54f _.i
Purchase Order Nc./Billing Reference AI1fZ
Requested Due Date Day
02 Days ays 04 Days 05 Days
Working Days 5-9 Days Standard 10 days Rush Work Must Be
Pra Approved
Samples received after 1500 witi be processed
next business day
Turnaround time is based on
business days excluding weekends and holidays
SEE REVERSE FOR TRMS CONDTIONS REGARDING
SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIENT _________________
Phone Fax Yes No
Email Yes No Email Address
EDD Type PDF__Exce
Site Location Name
Site Location Physical Address
TO BE
FILLED IN BY CLIENTISAMPLING PERSONNEL
Certilicatidn NELAC__USACE_FL
SC__OTHER _____N/A _____
Water Chlorinated YES NO
Sarrle Iced Upon Collection YES NO _________
CLIENT
SAMPLE DESCRIPTION
TIME
DATE COLLECTED
COLLECTED MILITARY
c-2O7J
MATRIX
SOIL
SLUDGE
côiJ
SAMPLE CONTAINER
PRESERVA-
TIVES
ANAL tid\
çy REMARKS PSBM
ID NO
---SEE BELOWvr NO SIZE
Neil Isnmcy iignaiure
Samplers Signature Sampled By Print Name Affiliation
Upon relinquishing this am of Custody is your authorization for Prism to proceed with the analyses as requested above Any changes
must be
submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been initializedinntr Date Miiia/HoUrSi-lecebveu
inqijiehed By Signature Received By Signature
Relinquished By Signature Roe ye For Prism Laboratories By
titod of Shipment NO ALL SAMP OOLERSSFIOULD BE
TAPED SHU NI uSTODY SEALS FOR
TRANSPORTATION TO TIlE LABORATORY
StPLES ARE NOT ACCEPTED AND VERIFIED AGAINST NTIL RECEIVED AT THE LABORATORY
Fed Ex UPS lf Hand-delivered Prism FIeld Service Other
Dat1/00 roup No
Additional Comments
NPDES LIST GROUNDWATER DRlNKlNi WATER SOLID WASTE RCRA CERCLA
LANDFILL OTHER
ONC USC EJNC USC INC USC JNC USC UNC OSC
UNO USC
UNC USC UNC USC UNC
USC___D_______0 ______
_____________
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SEEREVERSEFORTERMSCONDITIONS
ORIGINAL
Corporate Office
Mailing
P0 Box 7030
Charlotte North Carolina 28241
Physical
3475 Lakemont
Boulevard
Fort Mill SC 29708
803.802.2440
Raleigh
14001 Weston Parkway
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Caty North Carolina 27513
919.678.1070
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2120-B Capital Drive
Wilmington North Carolina 28405
910.313.6648
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4601 Corporate Drive NW
Suite 165
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704.793.9855
800.960.7317
www.espassociales.com
ESP Associates P.A