Item No 16 - Analytical Results Morehead Commons No 1 Incide-OCR

Pc/vt
Case NarrativePRISM
LA8ORATORIES.INO
Date 05/22/07 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COC Group No 30507486
Contact Chris Ward Collection Dates 05/15/07
Address Box 7030 Lab Submittal Dates 05115107
Chadotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report
and Quality
Control Data totaling 14 pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are included in the sample comments section of the laboratoty report lbr each sample
affected
mi Volatile Analysis
Analysis NoteforQ23842 MS PCB1260 Recovery outside of the control limits
Analysis NoteforQ23642 MSD PCB-1260 Recovery outside of the control limits
Volatile Analysis
No Anomalies Reported
Metals Analysis
Analysis Note for Q23595 Method Blank Chromium MB is greater than 1/2 of the reporting limit but the sample is 20X the MB
Analysis Note for Q23595 MS Lead MS recovery outside of the control limits Poskilgestion spike recovery 109%is within the
acceptance limits 75-125%
Analysis Note for 023595 MSD Lead RPD value outside the control limits
Wet Lab and Micro Analysis
NIA
Please call if you have any questions relating to this analytical report
Date Reviewed by Paula Gilleland Project Manager
Signature AJA LAO Signature
Review Date 05/22107 Approval Date
Data Qualifiers Key Reference
Compound also detected in the method blank
th Result outside of the OC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect is present
Angela OvercashcaL.CMLd OVJA4
05/22/07
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories Inc The results in this
report relate only to the samples submitted for analysis
449 Spdngbrook Road P.O Box 240543 Charlotte NC 28224-0403
Phone [phone] Toll Free 800/529-6364 Fax [phone]
NC Certi11caon No 402 Laboratory ReportScCertificationNo99012
NC Drinking Water Ceil No 37735
Project ID Morehead Commons No Client Sample ID PS-I
Prism Sample ID 181686
Sample Matrix Soil COC Group G0507466
Time Collected 05/15/07 1520
Time Submitted 05/15/07 1625
Percent Solids Determination
Percent Solids
44-DDD
44-DDE
44-DDT
44-Methoxychlor
a-BHC
a-Chlordane
Aldrii
b-BhC
Chiordane
d-BHC
Dieldrin
Endosulfan
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin ftJdehyde
Endrin Ketone
g-BHC
g-Chlordarie
Heptachior
Heptachior Epoxide
Toxaphene
BRL pg/kg 2.5 0.75
SRI pg/kg 2.5 0.52
BRL pg/kg 2.5 0.86
BRL pg/kg 4.9 17
BRL pg/kg 2.5 0.22
BRL pg/kg 2.5 043
BRL pg/kg 2.5 0.49
BRL pg/kg 2.5 0.62
BRL pg/kg 61 14
BRL pg/kg 2.5 0.35
BRI pg/kg 1.2 0.51
BRL pg/kg 2.5 0.44
BRL pg/kg 2.5 0.55
SRI pg/kg 2.5 0.64
BRL pg/kg 2.5 074
BRL pg/kg 2.5 0.69
BRL pg/kg 2.5 0.49
BRL pg/kg 2.5 0.29
BRL pg/kg 2.5 0.40
BRL pg/kg 2.5 0.58
BRL pg/kg 2.5 0.45
BRL pg/kg 61 14
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Chailotte NC 28241
05/22/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
81.4
Organochiorine Pesticides by Gas Chromatography
SM2540 05/17/07 1400 brown
8081A 052007 954 jvogel Q23643
8081A 05/20/07 954 jvogel 023643
8081A 05120/07 954 jvogel 023643
8081A 05/20/07 954 ivogel 023643
8081A 05/20/07 954 jvogel 023643
BOB1A 05/20/07 954 Jvogel Q23643
6081A 0512007 954 jvogel 023643
8081A 05/20/07 954 1voge 023643
8081A 05/20/07 954 jvogel 023643
8081A 05/20/07 954 Ivogel Q23643
8081A 05/20/07 954 jvogel Q23643
8081A 05/20/07 954 jvogel 023643
8081A 05/20/07 954 jvogei 023643
8081A 05/20/07 954 jvogel 023643
8081A 05/20/07 954 jvogel 023643
8081A 05/20/07 954 jvogel 023643
8081A 0520/07 954 jvo9eI 023643
8081A 05/20/07 954 jvog 023643
BOBIA 05120/07 954 Ivogel 023643
8081A 05/20/07 954 jvogel 023643
8081 05/20/07 954 ivogel 023643
8081A 05/20/07 954 jvogel 023643
Page of
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Spring brook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 282411
Laboratory Report
05/22/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
PS-I
181686
G0507466
05/15107 1520
05/15107 1625
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DatefTime ID
29.98 10 niL 35506 05/19/07 900 dpope P18411
0.061
0.12
0061
0.061
0.061
0.061
0.061
0.011
0.050
0.020
0021
00085
0.021
0.016
Sample Preparation
yghlorinated Biphenyls PCBs by GC-ECD
PCB-1 016
BRL
PCB-1221 BRL
PCB-1232 BRL
PCB-1242 BRL
PCB.1248 BRL
PCB-1254 BRL
PCB-1260 BRL
Sample Prepaiflon
Volatile Organic Compounds by GC/MS
111 2-Tetrachloroethane BRL
11 1-Trichloroethane BRL
122-Tetrachloroethane BRL
11 .2-Trichloroethane BRL
1-Dichloroethane BRL
l-Dichloroethene BRL
11 -Dichloropropene BRL
23-Trichlorobenzene BRL
Surrogate Recovery Control Limits
Tetrachloro-rn-xylene TCMX 46 40-162
Decachlorobiphenyl DCB 139 26-204
8052 05120107 954 jvogel 023642
8082 05/20/07 954 jvogel 023642
8082 05/20/07 954 jvogel 023642
8082 05/20/07 954 jvogeL 023642
8082 05/20/07 954 jvogeL Q23642
8082 05/20/07 954 jvogel 023642
8082 05/20/07 954 jvogel 023642
10 rnL 35506 05/19/07 900 dpope P18410
Surrogate Recovery Control Limits
Tetrachloro-m-xylene TCMX 79 36 182
Decachlorobiphenyl DCB 119 34-182
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
29.98
5.2 0.51
5.2 0.29
5.2 0.53
52 0.32
5.2 0.37
5.2 0.39
5.2 0.45
10 0.57
826DB
826DB
826DB
826DB
82606
826DB
826DB
826DB
05/17/07 816
05/17/07 816
05/17/07 816
05/17/07 816
05/17/07 816
05/17/07 816
05/17/07 816
05/17/07 816
erussell
erussell
erussell
erussell
emssefl
erusseli
erusseil
erussell
023573
023573
023573
023573
023573
023573
023573
023573
Page of
NC Certification No 402 Laboratory ReportScCertificationNo99012
NC Drinking Water Cart No 37735
Project ID Morehead Commons No Client Sample ID PS-I
Prism Sample ID 181686
Sample Matrix Soil COC Group G0507466
Time Collected 05115/07 1520
Time Submitted 05/15107 1625
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories
inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
S.rki AnaIyda Eiytr
ESP Associates PA
Attri Chris Ward
Box 7030
Charlotte NC 28241
05/22/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
12a-Tdchforopropane BRL pg/kg 52 0.45 826GB 05/17/07 816 enissell 023573
12.4-Trichiorobenzene BRL pg/kg 10 0.49 826DB 05/17/07 816 enissell 023573
124-Trimethylbenzene 34 pg/kg 10 039 8260B 05/17/07 816 erussell 023573
t2-Dibromo-3-chloroPrOPafle BRL pg/kg 10 0.97 826DB 05/17/07 616 ewssefl Q23573
12-Dibromoethane EDB ERL pg/kg 5.2 0.093 826DB 05/17/07 816 erusseU 023573
I2-Dichlorobenzene BRL pg/kg 10 0.28 8260B 05/17/07 816 erusseli 023573
2-Dlchloroethane BRL pg/kg 5.2 0.52
826GB 05/17/07 816 erusseU 023573
12-Dichloropropane BRL pg/kg 52 0.38 8260B 05/17/07 816 enissell Q23573
135-Trimothylbenzene II pg/kg 10 0.43 8260B 05/17/07 816 erusset Q23573
.3-Dichlorobenzene BRL pg/kg 10 0.44 826GB 05/17/07 816 enissell 023573
3-Iichloropropane BRL pg/kg 5.2 0.35
8260B 05/17/07 816 erusseil Q23573
1.4-Dichlorobenzene BRL pg/kg 10 0.40 826GB 05/17/07 816 erussell 023573
22-Dithloropropane BRL pg/kg 5.2 0.26
8260B 05/17/07 816 erussell 023573
2-Chioroethyl vinyl ether BRL pg/kg 10 0.38 826GB 05/17/07 818 enissell 023573
2-Chiorotoluene BRL pg/kg 10 0.38 826GB 05/17/07 816 erussell 023573
2-Hexanone SRI pg/kg 52 054 826GB 05/17/07 816 erussell Q23573
4-Chlorotoluene BRL pg/kg 10 0.27 826GB 05/17/07 816 erussell 023573
4-Methyl-2-pentanone MIBK BRL pg/kg 10 0.52 826GB 05/17/07 816 enJssell 023573
Acetone BRL pg/kg 21 2.0 826GB 05/17/07 816 erussell 023573
Bensene BRL pg/kg 3.1 0.41 826GB 05/17/07 816 erusseli 023573
Brornobenzene BRL pg/kg 5.2 0.36
826DB 05/17/07 818 erussell 023573
Brornocliloromethane BRI pg/kg 5.2 0.31 8260B 05/17/07 816 erusseU 023573
Brornodichloromethane BRL pg/kg 5.2 0.45
82608 05/17/07 816 erussell 023573
Brornofomi BRL pg/kg 5.2 0.38 826DB 05/17/07 816 enissell 023573
Brornomethane BRL pg/kg 10 0.60 826GB 05/17/07 818 erussell 023573
Carbon disulfide BRI pg/kg 10 0.33 826GB 05/17/07 816 erussell 023573
Carbon tetrachioride BRL pg/kg 5.2 0.30 82603 05/17/07 816 erussell 023573
Page of
R-.reAml..JcI .ion Soijons
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
This report should not
be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No.37735
Laboratory Report
05/22/07
Project ID Morehead Commons No Client Sample ID PS-I
Prism Sample ID 181686
Sample Matrix Soil COG Group G0507466
Time Collected 05115107 1520
Time Submitted 05/1 5/07 1625
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Chlorobenzene BRL pg/kg 5.2 0.39
826DB 05117/07 816 erussell 023573
Chlorodibromometharre BRL pg/kg 5.2 0.35
826DB 05/17/07 816 erussell 023573
Chioroethane BRL pg/kg 10 0.42 82603 05/17/07 816 erussell Q23573
Chloroform BRL pg/kg 5.2 0.38
826DB 05/17/07 816 erussell 023573
Chioromethane BRL pg/kg 10 0.36 8260B 05/17/07 816 erussell 023573
cis-12-Dichloroethene BRL pg/kg 5.2 0.23
8260B 05/17107 816 erussell 023573
cis13-Dichloropropene BRL pg/kg 5.2 0.33
82603 05/17/07 816 erussell 023573
Dibromomethane BRL pg/kg 5.2 0.38
82603 0517/07
816 erussell 023573
Dichlorodifluoromethane BRL pg/kg 10 1.2 82603 05/17/07 816 erusselt 0.23573
Ethylbenzene 3.8 pg/kg 5.2 0.36 82603 05/17/07 816 erussell Q23573
Hexachiorobutadiene BRL pg/kg 15 0.64 826DB 05/17/07 816 erussell 023573
lsopropyl etherIPE BRL pg/kg 5.2 0.18
826DB 05117/07 816 erussetl 023573
lsopropylbenzene BRL pg/kg 10 0.41 826DB 05/17/07 816 erussell 023573
mp..Xylenes 8.6 pg/kg 10 0.72 82603 05/17/07 816 erussell 023573
Methyl ethyl ketone MEK BRL pg/kg 21 1.4 82603 05117/07 816 erussell 023573
Methyl t-butyl ether PVITBE BRL pg/kg 5.2 0.30
826DB 05/17/07 816 erussell 023573
Methylene chloride BRL pg/kg 10 0.42 826DB 05/17/07 816 erussoll 023573
n-Butylbenzene 13 pg/kg 15 0.41 826DB 05/17/07 816 erussell 023573
n-Propylbenzene 6.7 pg/kg 10 0.31 826DB 0517/07 816 erussell 023573
Naphthalene 15 pg/kg 5.2 0.60
8260B 0517/07 816 erussell 023573
o-Xylene 7.9 pg/kg 5.2 0.31 826DB 05/17/07 816 erussell 023573
p-lsopropyltoluene BRL pg/kg 15 0.42 826DB 05/17/07 816 erusseIl 023573
sec-Butylbenzene 25 pg/kg 15 0.34 82603 05/17/07 816 enJssell 023573
Styrene BRL pg/kg 5.2 0.52
826DB 05/17/07 816 erussell 023573
tert-Butylbenzene BRL pg/kg 21 0.32 8260B 05/17/07 816 erusseil 023573
Tetrachioroethene BRL pg/kg 10 0.89 82603 05/17/07 816 erussell 023573
Toluene 2.2J pg/kg 5.2 0.35
8260B 05/17/07 816 erussell 023573
Page of
NCC6TUfiCatIOn No.402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 05122/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID PS-I
Attn Chris Ward Prism Sample ID 181686
Box 7030 Sample Matrix Soil COC Group G0507466
Chariotte NC 28241 Time Collected 05/15/07 1520
Time Submitted 05/15/07 1625
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
trans.12-Dichloroethene BRL pg/kg 5.2 0.39
826DB 05/17107 816 erussell 023573
trans.13-Dichloropropene BRL pg/kg 5.2 0.36 826DB 05/17/07 816 enissell 023573
Trichloroethene BRL pg/kg 5.2 0.31
82603 05/17/07 816 erussefi 023573
Trichiorofluoromethane BRL pg/kg 5.2 0.42
826DB 05/17/07 816 erussell 023573
Vinyl chloride BRI pg/kg 10 0.66 826DB 05/17/07 816 erussell 023573
One surrogate recovery
was outside of the control limits Matrix interference
is suspected
Surrogate Recovery Control Limits
Toluene-d8 86 81 128
Dibromofluoronielhane 98 67-143
Bromofiuorobenzene 205 77-128
Samoe Weight Determination
Weight Bisulfate 5.96 5035 05/18/07 000 lbmwn
WeightBisulfate2 5.81 5035 05/18/07 000 lbrcwn
Weight Methanol 5.73 5035 05/18/07 000 Ibrown
Oil and Grease by Soxhiet Extraction
Oil and Grease 10000 mg/kg 43 33 9071A 05/18/07 700 smanvanh Q23622
Diesel Range Organics DRO by GC-FID
Diesel Range Organics DRO 3600 mg/kg 170 22 20 801 5B 05/18/07 1334 Ivogel 023604
Sample Preparation 25.2 mL 3545 05/17/07 1300 onder P18397
Surrogate Recovery Control Limits
o-Terphenyl DO 49-124
Sample Weight Determination
Weight 5.86 GRO 05/18/07 000 brown
Weight 5.94 GRO 05/18/07 000 Jbrown
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Spring brook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
ESF Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No CJient Sample ID
Prism Sample ID
Sample Matrix Soil COO Group
Time Collected
Time Submitted
PS-I
181686
G0507466
05/15/07 1520
05/15/07 1625
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Gasoline Range Organics IGRO by GC-FID
Gasoline Range Organics GRO 33 mg/kg 6.1 0.64 50 8015B 05/17/07 1423 hwagner 023598
Surrogate Recovery Control Limits
aaa-TFT 100 55-129
by ICR
Chromium 22 mg/kg 0.62 0.037 BOlOB 05/17107 2237 mcampbell 023595
Lead 28 mg/kg 0.62 0.052 601DB 05/17/07 2237 mcampbeil Q23595
Sample Preparation 1.97 50 mL 305GB 05/17/07 710 Jhoppei P18387
Sample Comments
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
WEL4C certification except for those instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the wiitten consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
FuiI So .AmayI E1ronmw
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
05/22/07
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
111 2-Tetmchloroethane
1lj-Trichloroethane
11 22-Tetrachloroethane
12-Trichloroethane
1-Dichloroelhane
.1-Dichloroethene
1-Dichloropropene
23-Trichlorobenzene
.23-Trichloropropane
24-Trlchlorobenzene
24-Trimethylbenzene
.2-Dibromo-3-chbropropane
2-Dibromoethane EDB
12-Dichlorobenzene
12-Dichioroethane
12-Dichioropropane
.3 5-Trim ethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichlorobenzene
22-Dichioropropane
2-Chioroethyl vinyl ether
2-Chiorotoluene
2-H exanone
4-Chiorotoluene
4-Methyl-2-pentanone MIBK
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromornethane
Carbon disulfide
NC CertifIcation No.402
SC Certification No 99012
NC Drinking Water Cert No 37735
ND 2.5
ND 10
ND Z5
ND 10
ND 10
ND 50 25
ND 10
ND 10
ND 20 10
ND 1.5
ND 25
ND 2.5
ND 2.5
ND 2.5
pgikg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
023573
023573
023573
023573
023573
023573
023573
Q23573
023573
023573
023573
023573
023573
023573
023573
023573
023573
023573
023573
023573
023573
023573
023573
023573
023573
023573
023573
Q23573
023573
023573
023573
023573
023573
023573
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Level II QC Report
5122107
Project 10 Morehead Commons COC Group Number G0507466
Date/Time Submitted 5115/07 1625
Volatile Organic -----k.IIffijuIuIpuuIIuaLy hint flit
Method Blank ac Batth
Result RL Conl1o Unit linUs
It
ND 2.5 pg/kg
ND 2.5 pg/kg
ND 2.5 pg/kg
ND 2.5 pg/kg
ND 2.5 pg/kg
ND 2.5 pg/kg
ND 2.5 pg/kg
ND 10 pg/kg
ND 2.5 pg/kg
ND 10 pg/kg
ND 10 pg/kg
ND 2.5 pg/kg
ND 2.5 pg/kg
ND 10 pg/kg
MD 2.5 pg/kg
ND 2.5 pg/kg
ND 10 pg/kg
ND IC pg/kg
ND 10 pg/kg
MD 10 pg/kg
Page of
Cathon tetrachloride
Chlorobenzene
Chiorodibromomethane
Chioroethane
Chloroform
Chioromethane
cis-1 2-Dlchloroethene
cis-1 3-Dichloropropene
Dibromomethane
Dichiorodifluoromethane
Ethytbenzene
Hexachiorobutadiene
Isopropyl ether IPE
lsopropylbenzene
mp-Xylenes
Methyl ethyl ketone MEK
Methyl t-butyl ether MTBE
Methylene chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p.4sopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachioroethene
Toluene
trans-i 2-Dlchloroethene
trans-I 3-Dichloropropene
Trichioroethene
Trichlorofluoromethane
Vinyl chloride
Laboratory Control Sample
1-Dlthloroethene
NCCertificalion No 402 Level II QC ReportSCCertificationNo99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons COC Group Number 60507466
Date/Time Submitted 5/15/07 1625
ESP Associates PA
Attn Chris Ward
Box7030
Ghadotte NC 28241
Method Blank
5/22/07
Result RI Contiol IJmlt Unls
00 Batch
ID
ND 2.5 pg/kg Q23573
ND 2.5 pg/kg 023573
ND 2.5 pg/kg 023573
ND 10 pg/kg 023573
ND 2.5 pg/kg 023573
ND 10 pg/kg 023573
ND 2.5 pg/kg 023573
ND 2.5 pg/kg 023573
ND 2.5 pg/kg 023573
ND 10 pg/kg 023573
ND 2.5 pg/kg 023573
ND 15 7.5 pg/kg Q23573
ND 2.5 pg/kg 023573
ND 10 pg/kg 023573
ND 10 pg/kg 023573
ND 20 10 pg/kg 023573
ND 2.5 pg/kg 023573
ND 10 pg/kg 023573
ND 15 7.5 pg/kg 023573
ND 10 pg/kg 023573
ND 2.5 p91kg 023573
ND 2.5 pg/kg 023573
ND 15 7.5 pg/kg 023573
ND 15 75 pg/kg 023573
ND 2.5 pg/kg Q23573
ND 20 10 pg/kg 023573
ND 10 pg/kg 023573
ND 2.5 pg/kg 023573
ND 2.5 pg/kg 023573
ND 2.5 pg/kg 023573
ND 2.5 pg/kg 023573
ND 2.5 pg/kg 023573
ND 10 pg/kg 023573
Recovery Reco
Ranges QC Batch
Result SpIke Amount Unils ID
43.74 50 pg/kg 87 57-122 023573
This report should not be reproduced except in its entirety without the wntten consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page of
ESP Associates PA
Attn Chris Ward
Box7030
Chadotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
75-125 0-20 023595
75-125 33 0-20 023595
This report should not be reproduced except in its enUrety without the wtitten consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-600/529-6364 Fax [phone]
Level II QC Report
5/22/07
Project ID Morehead Commons COG Group Number G0507466
Date/Time Submitted 5/15/07 1625
LaboratOly Control Sample Recovery QC Batch
Result Spike Amount Units rn--
Benzene 46.51 50 pgIkg 93 62-119 Q23573
Chlorobenzene 46.49 50 pg/kg 93 61-124 023573
Toluene 46.08 50 p91kg 92 57-122 023573
Trichlomethene 46.14 50 pg/kg 92 59-129 023573
Matrix Spike Recovery cc Batch
sample io Result Spike Amount Units ID
.-..-..-
161577 lj-Dichloroethene 28.98 50 pg/kg 58 44-140 023573
Benzene 34.44 50 pg/kg 69 46-136 023573
Chorobenzene 35.36 50 pg/kg 71 47-135 023573
Toluene 34.06 50 pg/kg 68 47-136 023573
Trichloroethene 35.7 50 pg/kg 71 45-141 0.23573
Matrix Spike Duplicate Recavely Recovery RPI Qc Batch
Sample Result Spike
Amount Units ID
181577 11-Dichloroethene 29.52 50 pg/kg 59 44.140 0-23 023573
Berizene 34.31 pg/kg 69 46-135 0-22 Q23573
Chlorobenzene 35.64 50 pg/kg 71 47-1 35 0-22 023573
Toluene 33.9 50 pg/kg 68 47-136
0-22 023573
Trichloroethene 36.41 50 pg/kg 73 4.5-141 0-23 023573
Metals by ICP method 601DB
Method Blank OC Batch
Result RL Control Umlt ID
Chromium 0.2011 0.25 0.125 mg/kg 023595
Lead 0.0466 0.25 0.125 mg/kg 023595
Laboratory Control Sample Recovery
Result Spike Amount Units
Ranges
Chromium 24.2754 25 mg/kg 97 80-120 023595
Lead 23.71 25 mg/kg 95 80-120 023595
Matrix Spike Recovery Recovery cc saicir
Sample Resull Spike Amount Units ID
181686 Chromium
40.9681 24.752 mg/kg 92 75-125 023595
Lead 59.3997 24152 mg/kg 149 75-1 25 023595
MatrixSpiko Duplicate Recovery OCRatch
sample it Result SPIke Amount Units to
181686 Chromium
Lead
37.4234 25.380
42.4519 25.380
mg/kg
mg/kg
76
79
Page of
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
CC Batch
ID
023622
QC Balth
ID
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water CerL No 37135
Level II QC Report
5/22/07
Project ID Morehead Commons COC Group Number G0507466
Date/Time Submitted 5/15107 1625
Gasoline Range Organics GRO by GC-FID method 80158
Method Blank ac Batch
Result RI Control limit Units
Gasoline Range Organics GRO ND 2.5 mg/kg 023598
Laboratory Control Sample Recovery QC eulcRangesResultSpikeAmountUnitsID
Gasoline Range Organlcs GRO 51.1 50 mg/kg 102 67-116 023598
Matrix Spike ROcOY Ranges CC Batch
Sample ID Result Spike
Amount Units it ID
181686 Gasoline Range Organics CR0 66 50 mg/kg 79
57-113 023598
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range
Sample 1k
Result Spike Amount Units
181686 Gasoline Range Organics GRO 68.1 50 mg/kg 83 57-113 -23 023598
Diesel Ranqo Orcianics DRO by GC-FID method 8015B
Method Blank
Renult RI Control limit Units ID
Diesel Range Organlcs DRO ND 3.5 mg/kg 023604
Laboratory Control Sample Recovery Recovery
Ranges cia Batch
IDResultSpikeAmountUnits
Diesel Range Organics DRO 69.5 80 mg/kg 87 55-109 023604
Matrix Spike Recovery Recovery
Ranges 00 Batch
sample io Result Spike Amount Units ID
181378 DIesel Range Organics DRO 72.4 80 mg/kg 85 50-117 023604
Matrix Spike Duplicate Feco Recovery RPD
Ranges RPD Ra CC Batch
Sample ID Result Spike Amount Units it ID
181 378 Diesel Range Organics DRO 66.2 80 mg/kg 77 50-117 0-24 023604
Oil and Grease by Soxhiet Extraction method 91171A
Method Blank
Result RI Control Umrl UnIts
ND 35 17.5 mg/kgOilandGrease
Laboratory Control Sample
Oil and Grease
Result Spike Amount
5410 5355
Units
mg/kg
Recovery Recovery
Ranges
101 80-120 023622
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Chailotte1 NC 28241
182049 PCB-1016
P09-1260
0.278 0.333
0.333
mg/kg 83 14-192
mg/kg -1384 10-192
0-40 023642
0-40 023642
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
5/22/07
Project ID Morehead Commons COO Group Number G0507466
Date/Time Submitted 5/15/07 1625
1DfD h.frpri 8082rtPIYtJIIUI 1IIC1flU IlI34 Ic.IyIa It .LJaI sae..
Method Blank
Result RL Conlml Uroft ljnfts ID
PCB-1 016
ND 0.05 0.025 mg/kg 023642
PCB-1 221 ND 0.1 0.05 mg/kg 023642
PCB-1232 ND 0.05 0025 mg/kg 023642
PCB-1242 ND 0.05 0.025 mg/kg 023642
PCB-1248 ND 0.05 0.025 mg/kg 023642
PCB-1254 ND 0.05 0.025 mg/kg 023642
PCB-1260 ND 0.05 0.025 mg/kg 023642
Laboratory Control SampiB ReCOv Recovery Batch
Result Spiko Amount Units ID
PCB-1016 0.288 0.333 mg/kg 86 64-1 51 023642
P09-I 260 0.292 0.333 mg/kg 88 45466
023642
Matrix Spike Recovery
Ru
sample Il Rasult Spike Amount Units It
182049 PCB-1016
0.288 0.333 mg/kg 86 14-192 023642
PCB-1260 0.333 mg/kg -1384
10-192 023642
Matrix Spike Duplicate Recovery Recovery RPD ac
Sample Result Spike Amount Units ID
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
181686 44-DDT
AIdrin
Dleldrin
33
33
33
pg/kg
pg/kg
pg/kg
56-163
57-137
60-141
Q23643
Q23643
023643
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] ToIl Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
5/22/07
Project ID Morehead Commons COC Group Number 00507466
DateTIme Submitted 5/15/07 1625
by Gas L..._..I....1 0fl044.....fl.._LatH UIIIOItflhI aW1IV IhIULIItJtI tJyU 11
Method Blank Batch
Result RL Control LImit UnIts
44-DDD ND pg/kg 023643
44-DDE NO pg/kg Q23643
44-DDT ND pg/kg Q23643
44-Methoxychlor ND pg/kg 023643
a-BUC ND pg/kg Q23643
a-Chlordane ND pg/kg 023643
Aidrin ND ug/ky 023643
b-BIIC ND pg/kg 023543
Chiordane ND 50 25 pg/kg 023643
d..BHC ND pg/kg Q23643
Dielddn ND 0.5 pg/kg 023643
Endosulfan ND pg/kg 023643
Endosulfan II ND pg/kg 023643
Endosulfan Sulfate ND pg/kg 023643
Endrin ND pg/kg 023643
Endrin Aidehyde ND Ps/kY 023643
Endrin Ketone ND pg/kg 023643
g-BHC ND pg/kg 023643
g-Chlotane ND pg/kg 023643
Heptachior ND pg/kg 023643
Hepthchlor Epoxido ND pg/kg 023643
Toxaphene ND 50 25 pg/kg 023643
Laboratory Control Sample Recovery Recovety OC Batch
Result SpiKe Amount UnIts lID
44-DDT 36.03 33 pg/kg 115 75-141 023643
Aidrin 3493 33 pg/kg 106 66-132 023643
Dieldrin 35.14 33 pg/kg 106 72-136 023643
Endrin 35.04 33 pg/kg 106 74-147 023643
Heptachlor 31.28 33 pg/kg 95 72-134 023643
Matrix Spike Resovy Recovery
Sample lID Result SpiRo Amount Units ID
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
5/22/07
Project 1D Morehead Commons CCC Group Number G0507466
Date/Time Submitted 5/15/07 1625
Matrix Spike Recovery
Ranges QC Balth
Sample it Result Spike Mourtt units ID
181686 Endrlni 33 pg/kg 65-164 Q23643
Heptachior 33 pg/kg 63-142 023643
Matrix Spike Duplicate Recovery Recovery RPI
Ranges RPD pg QC Bstd
SampleID flessit SpikeAmount IJft ID
181686 44-DDT 33 pglkg 56-163 0-38 023643
Aidrin 33 pg/kg 57-1 37 -29 023643
Dicidrin 33 60-141 -30 Q23643
Endrin 33 pg/kg 65-1 64 0-21 023643
Heptachior 33 pg/kg 63-1 42 -27 023643
4-See Case Narrative
Page of
449 Sp1ngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Fax
Client Company Name
Report To/Contact Name
Reporting Address
Phone51 Fax Yes No
Email Yes No Email Address_____________________
EDD Type PDF_Ex9el ...Other_________________
Site Location Name ViOVi.4ci DIfl1O7
Site Location Physical Address JbkLJk
CHAIN OF CUSTODY RECORD
PAGE ..L OFL_QUOTE TO EP4SUR PROPER BILUNG
Project Name iV
Short Hold Analysis Yes No UST Project Yes
pIease ATTACH any project specific reporting QC LEVEL 111111
provisions and/9.QCpequirements
Invoice To Si
Address
Purchase Order No./BiIIing Reference _________________________
Requested DUE Date Day 02 Days Days
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Samples received after 1500 will be processed next business day
Turnaround time Is based on busIness days excluding weekends and holidays
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Samplers Sampled By
Print Name /4-e /C4 Affiliation
Upon relinquishing Is In of odour authorization for Prism to proceed with the analyses as requested above Any changes
must be
submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been Initialized
RelInquIshed By SIgnature RecelvCd By Signature Date
Ftoflnqulshed By
Method at Shlpme NOt AMPLE OOLE
5AI5LES ARE NOT ACC
Fed Ex UPS__-land-delivered PrIsm
ED
Field
ULD BE TAPED SHIJI ODY sE4LS FOR TRANSPORtATION
TO THE LABORATORY
VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY
SoMca Other__________________________________________________________________
IifôCOOroup
st7O
NPDES liST tROUNDWATER DRINKING WATER SOLID WASTE FlORA CERCLA LANDFILL OTHER
UNC USCI UNC USC USC 1JNC USC IJNC USC ONC USC UNC USC UNC USC ONC
USC
0____i0.__I _____0___.0____________________CONTAINER TYPE CODES Amber Clear Glass Plastic IL Teflon-Lined Cap VOA Voiatile Organics Analysis Zero Head Space
Site Departure Time
Field Tech Fee
Mileage
PRISM
LAaORATOalEa INC
FutI SerVice Analytical Environmental Solutions
CL Ahivd
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LAB USE ONLY__
Samples INTACT upon amval
eeivd9WETlQETemp ..._
PROPER PRESERVATIVES indicated
.edelVŁd.WlTHiN HOLDING.TIMES
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VOLATlLES.reod W/OUT HEADSPACE
PAbPERCONTAINERS.USed Tiiiiii
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE_FL ____
SQ...._OThER _____N/A _____
Water Chlorinated YES NO
Sample Iced Upon Collection YES.j NO_________
SAMPLE DESCRIPTION COLLECTED
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COLLECTED
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SAMPLE CONTAINER \UANALYSES UESTED
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