6004_DukeMcGuireLF2_Dec2015_2ndSemiAnnual_DIN26346_20160226

McGuire Nuclear Station - Landfill #2
(Synthetically Lined) Permit No. 6004
Semiannual Groundwater
Monitoring Report
December 2015 Sampling Event

February 26, 2016

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004 December 2015 Sampling Event
CONTENTS

ii

Contents
Page
Report Verification i
Contents ii
Section 1 - Background 1
Section 2 - Methods 3
2.1 Sampling and Analysis Methods 3
2.2 Statement of Work 3
Section 3 - Results 5
3.1 Site Groundwater Flow 5
3.2 Analytical Results 5

FIGURES
1. Site Location Map
2. Sample Locations
3. Generalized Groundwater Surface Contours
TABLES
1. Well Construction Information
2. Groundwater Flow Velocities
3. Field Data Parameters
4. Groundwater Field and Analytical Results
5. Field and Analytical Results that Equal or Exceed 15A NCAC 2L Groundwater Quality
Standards
6. Surface Water Field and Analytical Results
7. Field and Analytical Results that Equal or Exceed 15A NCAC 2B Surface Water Quality
Standards
8. Leachate Sample Field and Analytical Results
9. Radiological Analytical Results
APPENDICES
A. Field Sampling Forms
B. Laboratory Report and Chain-of-Custody Forms

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004 December 2015 Sampling Event
SECTION 1 - BACKGROUND

1

Section 1 - Background
The McGuire Nuclear Station Landfill #2 (Synthetically Lined)1 is located at the Duke Energy
Carolinas, LLC (Duke Energy) McGuire Nuclear Station in Mecklenburg County, North Carolina.
The landfill is permitted to accept waste specified by the Permit to Operate. The landfill was
constructed with a high-density polyethylene (HDPE) synthetic liner and leachate collection and
removal system. Leachate and contact stormwater are collected in a lined leachate collection
basin and pumped to the McGuire Nuclear Station wastewater treatment system. The landfill is
permitted under the North Carolina Department of Environmental Quality (NCDEQ) Solid Waste
Permit No. 6004.
The landfill and nearby area are depicted on Figures 1 and 2. The landfill is located south of
North Carolina Highway 73, north of Cashion Road, and to the west of Linderman Road.
Cashion Road runs along a surface water divide, with surface flow draining to the northwest and
to the southeast. A surface water drainage feature is located to the northeast of the landfill. This
feature drains to the northwest to a perennial unnamed stream. Surface water sample location
SW-1 is located in this unnamed stream (north of the landfill) and is upstream from the
confluence with the surface water drainage feature. Surface water sample location SW-2 is also
located in this unnamed stream, downstream from SW-1 and west of the landfill. The unnamed
stream drains to the west to the Catawba River. A second surface water drainage feature is
located to the southwest of the landfill, draining to the northwest into the unnamed stream.
As described in the Sampling and Analysis Plan2 (SAP), the monitoring system at the landfill
consists of the following:
Monitoring Wells: MW-5 MW-5A
MW-6 MW-6A
MW-7 MW-7A
MW-8 MW-8A
MW-9 MW-9A
MW-10A

Surface Water Sample Locations SW-1 SW-2

Leachate Sample Locations: Leachate
Pond

1 In response to the North Carolina Division of Public Health, Radiation Protection Section, November 17,
2006 letter to Duke Energy, LLC, Duke Energy offered to indicate the McGuire Nuclear Station Landfill #2
as “(Synthetically Lined)” in reports.
2 Groundwater Monitoring Program Sampling and Analysis Plan, McGuire Nuclear Station, Landfill #2
(Synthetically Lined), Permit No. 6004-INDUS, March 28, 2014.
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004 December 2015 Sampling Event
SECTION 1 - BACKGROUND

2

The leachate sample is collected from the outfall of the leachate pipe which conveys leachate
from the landfill to the leachate collection basin. The locations of the monitoring wells, the
surface water sample locations, and the leachate collection basin are shown on Figure 2.
With the exception of well MW-10A, the wells are installed as well pairs with one shallow well
and one deeper well adjacent to one another. The well with the “A” designation is the deeper
well in each well pair. Well pair MW-9 and MW-9A are installed adjacent to and downgradient
from the leachate collection basin. The remaining wells are installed adjacent to the landfill.
Well construction information is provided in Table 1.
According to the SAP, monitoring wells MW-5 and MW-5A are the upgradient wells and are
considered the background wells for the site. Surface water sample location SW-1 is considered
the upgradient or background surface water sample location.
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004 December 2015 Sampling Event
SECTION 2 - METHODS

3

Section 2 - Methods
2.1 Sampling and Analysis Methods
Sample collection and documentation of sampling activities was performed by Duke Energy
personnel (Duke Energy Carolinas Field Certification #5193) in accordance with the North
Carolina Solid Waste Management Guidelines. Copies of the field sampling forms are included
in Appendix A. The parameters and constituents sampled were selected by Duke Energy and
the NCDEQ Division of Solid Waste. Alkalinity, chloride, sulfate, and metals were analyzed by
the Duke Energy Analytical Laboratory (North Carolina Laboratory Certification #248). Volatile
organic compounds (VOCs) and total petroleum hydrocarbons (TPHs) were analyzed by
TestAmerica Laboratories, Inc. (North Carolina Laboratory Certification #358). The laboratory
reports and chain-of-custody forms are included in Appendix B.
The groundwater, surface water, and leachate samples were analyzed for the following
constituents:
• Barium, chromium, and silver using Environmental Protection Agency (EPA) Method
200.7
• Arsenic, cadmium, lead, and selenium using EPA Method 200.8
• Mercury using EPA Method 245.1
• Chloride and sulfate using EPA Method 300.0
• VOCs using Solid Waste (SW)846 Method 8260B
• TPHs diesel range organics (DRO) using SW846 Method 8015C Modified
In addition, the following analyses were performed in accordance with the requirements of the
Radioactive Materials License No. 060-0379-7 issued by the North Carolina Department of
Health and Human Services Radiation Protection Section:
• Gross alpha radioactivity using EPA Method 900
• Gross beta radioactivity using EPA Method 900
• Tritium using EPA Method 906.0 Modified
• Gamma radioactivity for select isotopes
2.2 Statement of Work
HDR completed the following tasks:
• Received field sampling information provided by Duke Energy (performed by Duke
Energy personnel) for monitoring wells MW-5A, MW-6, MW-6A, MW-7A, MW-8, MW-8A,
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004 December 2015 Sampling Event
SECTION 2 - METHODS

4

MW-9, MW-9A, and MW-10A. Water level readings were obtained in MW-5 and MW-7;
however, samples were not collected due to insufficient water volume in these wells.
Data were also received for surface water sample locations SW-1 and SW-2 as well as
for the leachate pond sample. The samples were collected on December 7, 2015, and
HDR received the data on December 29, 2015.
• Reviewed the laboratory analytical results for the samples noted above. The Electronic
Data Deliverable (EDD), provided by Duke Energy, was adapted to conform to the
format requirements of the NCDEQ EDD template. HDR added an italicized J data
qualifier (J’) to indicate a concentration that equals or is greater than the laboratory’s
method reporting limit (MRL), but less than the Solid Waste Section Limit3 (SWSL), and
retained the laboratory-supplied qualifier J to indicate values that equal or are greater
than the laboratory’s method detection limit (MDL) but are less than the MRL. A copy of
the original EDD is retained in HDR’s files.
• Developed a generalized groundwater surface contour map using map data and
groundwater elevation data supplied by Duke Energy.
• Prepared and submitted this Semiannual Groundwater Monitoring Report to Duke
Energy.
3 The Solid Waste Section Limit (SWSL) is defined by NCDEQ as the lowest amount of analyte in a
sample that can be quantitatively determined with suitable precision and accuracy. The SWSL is the
concentration below which reported results must be qualified as estimated. NCDEQ Division of Waste
Management Memorandum dated February 23, 2007.
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004 December 2015 Sampling Event
SECTION 3 - RESULTS

5

Section 3 - Results
3.1 Site Groundwater Flow
Generalized groundwater surface contours and groundwater flow direction arrows for the site
are shown on Figure 3. These contours were developed using groundwater elevations
measured at the shallow wells on the date of sampling. Calculated groundwater flow velocities
are presented in Table 2.
Groundwater flow in the area of the landfill is generally from the southeast end of the landfill
toward the northwest and the unnamed stream described in Section 1. Groundwater flow on the
east side of the landfill is towards the northeast toward wells MW-6, MW-6A, MW-10A, and the
surface water drainage feature located northeast of the wells.
3.2 Analytical Results
The measured field data parameters are presented in Table 3.
The groundwater sampling field and analytical results are summarized in Table 4. The analysis
results for the constituents are compared to the groundwater standards found in Title 15A
NCAC 02L .0202 (g) (2L Standards). Concentrations that attain or exceed the 2L Standards are
noted on Table 4 by bold font. A summary of the analytical results that attain or exceed the 2L
Standards and a preliminary analysis of the cause and significance of the exceedances are
presented in Table 5.
Surface water sample locations SW-1 and SW-2 are located on an unnamed stream. The
unnamed stream is a tributary of the Catawba River, which is classified by the NCDEQ Division
of Water Quality as Class WS-IV surface water at the confluence with the unnamed stream. As
a result, the field and analytical results from these locations are compared to Title 15A, NCAC,
Subchapter 2B Standards (2B Standards) for Class WS-IV water. The field and analytical
results of surface water sampling are summarized in Table 6. Concentrations that attain or
exceed the 2B Standards are noted on Table 6 by bold font. A summary of the analytical results
that attain or exceed the 2B Standards and a preliminary analysis of the cause and significance
of the exceedances are presented in Table 7.
The MDL was greater than the respective 2L Standard for the following constituents:
• 1,2,3-Trichloropropane
• 1,2-Dibromo-3-chloropropane (DBCP)
• 1,2-Dibromoethane (EDB)
• Vinyl chloride
The MDL was greater than the respective 2B Standard for the following constituents:
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station - Landfill #2 (Synthetically Lined) Permit No. 6004 December 2015 Sampling Event
SECTION 3 - RESULTS

6

• Silver
The MDLs for the listed constituents were all below their corresponding SWSLs as required by
the February 23, 2007, NCDEQ memo. With the exception of the silver concentration reported
at surface water sample location SW-2, these constituents were not detected above the MDL in
the analyzed samples and are not considered to exceed their respective 2L or 2B Standards.
The field and analytical results for leachate sampling are summarized in Table 8.
Concentrations with values that equal to or greater than the SWSLs are noted in Tables 6 and 8
by gray-shaded cells.
Selected samples were diluted as is normal laboratory practice to bring samples within the
calibrated range of the analysis. Specifics regarding the samples that were diluted, including the
dilution amount, are reported in the EDD.
The results of the radiological analyses are presented in Table 9. A copy of this report has been
submitted to the North Carolina Department of Health and Human Services Radiation Protection
Section for reference. HDR did not evaluate this data.

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W
-
5
A
,

r
e
s
p
e
c
t
i
v
e
l
y
.

10
.

I
n
f
o
r
m
a
t
i
o
n

p
r
o
v
i
d
e
d

b
y

D
u
k
e

E
n
e
r
g
y

o
n

D
e
c
e
m
b
e
r

2
9
,

2
0
1
5
We
l
l

I
D
We
l
l

In
s
t
a
l
l
a
t
i
o
n

Da
t
e
Co
o
r
d
i
n
a
t
e
s
TO
C

Ele
v
a
t
i
o
n

(
f
t
.
)
Gr
o
u
n
d

S
u
r
f
a
c
e

Ele
v
a
t
i
o
n
(f
t
.
)
Sc
r
e
e
n
e
d

I
n
t
e
r
v
a
l

be
l
o
w

T
O
C
(f
t
.
)
Geology of Screened IntervalWell Diameter (in.)Casing Type
We
l
l

S
t
i
c
k
-
u
p

He
i
g
h
t

A
b
o
v
e

Gr
o
u
n
d

S
u
r
f
a
c
e

(f
t
.
)
Gr
o
u
n
d
w
a
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e
r

Ele
v
a
t
i
o
n
(ft
.
)
De
p
t
h

t
o

W
a
t
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r

be
l
o
w

T
O
C
(ft
.
)
To
t
a
l

W
e
l
l

De
p
t
h

b
e
l
o
w

TO
C
(f
t
.
)
De
p
t
h

t
o

T
o
p

o
f

Sc
r
e
e
n

f
r
o
m

T
O
C
(f
t
.
)
Page  1  of  1
Ta
b
l
e

2
–
G
r
o
u
n
d
w
a
t
e
r

F
l
o
w

V
e
l
o
c
i
t
i
e
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
2

(
S
y
n
t
h
e
t
i
c
a
l
l
y

L
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
We
l
l

I
D
Up
g
r
a
d
i
e
n
t

Gr
o
u
n
d
w
a
t
e
r

Co
n
t
o
u
r

El
e
v
a
t
i
o
n
(f
t
)
D
o
w
n
g
r
a
d
i
e
n
t

Gr
o
u
n
d
w
a
t
e
r

Co
n
t
o
u
r

El
e
v
a
t
i
o
n
(f
t
)
Li
n
e
a
r

Di
s
t
a
n
c
e

Be
t
w
e
e
n

Co
n
t
o
u
r
s

th
r
o
u
g
h

W
e
l
l
(f
t
)
Hy
d
r
a
u
l
i
c

Gr
a
d
i
e
n
t

(f
t
/
f
t
)
Hy
d
r
a
u
l
i
c

Co
n
d
u
c
t
i
v
i
t
y

(f
t
/
d
a
y
)
Ef
f
e
c
t
i
v
e

Po
r
o
s
i
t
y

(%
/
1
0
0
)
Groundwater Velocity (ft/day)
MW
-
5

7
0
5

7
0
4

8
1

0
.
0
1
3

0
.
4
1
1

0
.
2
5
9

0
.
0
2
1
MW
-
6
A

6
9
9

6
9
8

4
4

0
.
0
2
3

0
.
4
1
1

0
.
2
5
9

0
.
0
3
6
MW
-
7

6
9
1

6
9
0

4
7

0
.
0
2
1

0
.
4
1
1

0
.
2
5
9

0
.
0
3
4
MW
-
8

6
9
6

6
9
5

4
9

0
.
0
2
0

0
.
4
1
1

0
.
2
5
9

0
.
0
3
2
MW
-
9

6
8
6

6
8
5

6
2

0
.
0
1
6

0
.
4
1
1

0
.
2
5
9

0
.
0
2
5
MW
-
1
0
A

7
0
3

7
0
2

1
7
1

0
.
0
0
6

0
.
4
1
1

0
.
2
5
9

0
.
0
0
9
No
t
e
s
:
1
.

L
i
n
e
a
r

d
i
s
t
a
n
c
e

m
e
a
s
u
r
e
d

t
h
r
o
u
g
h

m
o
n
i
t
o
r
i
n
g

w
e
l
l
s

i
s

a
p
p
r
o
x
i
m
a
t
e
l
y

p
e
r
p
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n
d
i
c
u
l
a
r

t
o

g
r
o
u
n
d
w
a
t
e
r

c
o
n
t
o
u
r
s
.
2
.

A
t

m
o
n
i
t
o
r
i
n
g

w
e
l
l

l
o
c
a
t
i
o
n
s

w
h
e
r
e

d
o
w
n
g
r
a
d
i
e
n
t

c
o
n
t
o
u
r
s

a
r
e

n
o
t

p
r
e
s
e
n
t
,

t
h
e

g
r
o
u
n
d
w
a
t
e
r

e
l
e
v
a
t
i
o
n

a
t

t
h
e

m
o
n
i
t
o
r
i
n
g

w
e
l
l

i
s

u
s
e
d

a
s

t
h
e

d
o
w
n
g
r
a
d
i
e
n
t

g
r
o
u
n
d
w
a
t
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r

e
l
e
v
a
t
i
o
n
.
3
.

A
t

m
o
n
i
t
o
r
i
n
g

w
e
l
l

l
o
c
a
t
i
o
n
s

w
h
e
r
e

u
p
g
r
a
d
i
e
n
t

c
o
n
t
o
u
r
s

a
r
e

n
o
t

p
r
e
s
e
n
t
,

t
h
e

g
r
o
u
n
d
w
a
t
e
r

e
l
e
v
a
t
i
o
n

a
t

t
h
e

m
o
n
i
t
o
r
i
n
g

w
e
l
l

i
s

u
s
e
d

a
s

t
h
e

u
p
g
r
a
d
i
e
n
t

g
r
o
u
n
d
w
a
t
e
r

e
l
e
v
a
t
i
o
n
.
4
.

M
o
n
i
t
o
r
i
n
g

w
e
l
l
s

a
r
e

n
o
t

l
i
s
t
e
d

w
h
e
r
e

i
n
s
u
f
f
i
c
i
e
n
t

i
n
f
o
r
m
a
t
i
o
n

i
s

a
v
a
i
l
a
b
l
e

t
o

c
a
l
c
u
l
a
t
e

v
e
l
o
c
i
t
y
.
5
.

H
y
d
r
a
u
l
i
c

g
r
a
d
i
e
n
t
s

a
n
d

g
r
o
u
n
d
w
a
t
e
r

v
e
l
o
c
i
t
i
e
s

a
r
e

a
p
p
r
o
x
i
m
a
t
e
.
6
.

H
y
d
r
a
u
l
i
c

c
o
n
d
u
c
t
i
v
i
t
y

p
r
e
s
e
n
t
e
d

f
o
r

t
h
e

a
l
l
u
v
i
u
m
/
s
o
i
l
/
s
a
p
r
o
l
i
t
e

h
y
d
r
o
s
t
r
a
t
i
g
r
a
p
h
i
c

l
a
y
e
r

i
s

t
h
e

g
e
o
m
e
t
r
i
c

m
e
a
n

o
f

t
h
e

c
o
n
d
u
c
t
i
v
i
t
y

d
a
t
a

i
n

t
h
e

H
D
R

C
o
n
d
u
c
t
i
v
i
t
y

D
a
t
a
b
a
s
e

(
u
n
p
u
b
l
i
s
h
e
d

d
a
t
a

f
r
o
m

P
i
e
d
m
o
n
t

C
a
r
o
l
i
n
a

s
i
t
e
s

w
i
t
h

f
o
l
i
a
t
e
d
/
l
a
y
e
r
e
d

b
e
d
r
o
c
k
)
.
7
.

E
f
f
e
c
t
i
v
e

p
o
r
o
s
i
t
y

p
r
e
s
e
n
t
e
d

f
o
r

t
h
e

a
l
l
u
v
i
u
m
/
s
o
i
l
/
s
a
p
r
o
l
i
t
e

h
y
d
r
o
s
t
r
a
t
i
g
r
a
p
h
i
c

l
a
y
e
r

i
s

t
h
e

m
e
a
n

v
a
l
u
e

e
s
t
i
m
a
t
e
d

f
r
o
m

g
r
a
i
n

s
i
z
e

d
a
t
a

u
s
i
n
g

F
e
t
t
e
r
/
B
e
a
r

D
i
a
g
r
a
m
s
.

8
.

T
h
e

h
y
d
r
o
s
t
r
a
t
i
g
r
a
p
h
i
c

l
a
y
e
r

i
n
f
o
r
m
a
t
i
o
n

i
s

n
o
t

a
v
a
i
l
a
b
l
e

f
o
r

m
o
n
i
t
o
r
i
n
g

M
W
-
5
.

T
h
i
s

w
e
l
l

i
s

a
s
s
u
m
e
d

t
o

b
e

s
c
r
e
e
n
e
d

i
n

t
h
e

a
l
l
u
v
i
u
m
/
s
o
i
l
/
s
a
p
r
o
l
i
t
e

l
a
y
e
r
.
9
.

H
y
d
r
a
u
l
i
c

g
r
a
d
i
e
n
t
s

a
n
d

g
r
o
u
n
d
w
a
t
e
r

v
e
l
o
c
i
t
i
e
s

b
a
s
e
d

o
n

g
r
o
u
n
d
w
a
t
e
r

d
e
p
t
h
s

m
e
a
s
u
r
e
d

o
n

D
e
c
e
m
b
e
r

7
,

2
0
1
5
.
Page 1 of 1
Ta
b
l
e

3
–
F
i
e
l
d

D
a
t
a

P
a
r
a
m
e
t
e
r
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
2

(
S
y
n
t
h
e
t
i
c
a
l
l
y

L
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
12
/
7
/
2
0
1
5
MW
-
5
63
.
9
0

6
3
.
2
6

7
0
5
.
0
5

N
S
NS

N
S

N
S

0
.
1
0

N
S

N
S

N
S
NS
NS

N
S
NS

N
S
12
/
7
/
2
0
1
5
MW
-
5
A

9
6
.
0
0

6
5
.
2
8

7
0
3
.
1
4

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

5
.
0
1

1
5
.
2
5

N
O

1
6
.
2
4
56
6.4

1
.
2
390

7
.
6
6
12
/
7
/
2
0
1
5
MW
-
6
37
.
2
0

3
1
.
6
5

6
9
6
.
8
0

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

0
.
9
1

5
.
0
0

N
O

1
5
.
3
2
13
7
6.1

3
.
9
401

6
.
3
1
12
/
7
/
2
0
1
5
MW
-
6
A

4
7
.
9
0

3
0
.
8
4

6
9
8
.
1
4

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

2
.
7
8

9
.
0
0

N
O

1
5
.
5
8
63
5.6

1
.
1
427

7
.
9
0
12
/
7
/
2
0
1
5
MW
-
7
37
.
3
0

3
5
.
9
5

6
8
9
.
9
1

N
S
NS

N
S

N
S

0
.
2
2

N
S

N
S

N
S
NS
NS

N
S
NS

N
S
12
/
7
/
2
0
1
5
MW
-
7
A

5
9
.
4
0

3
4
.
4
0

6
9
0
.
2
6

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

4
.
0
8

1
2
.
7
5

N
O

1
6
.
2
6
12
0
6.5

2
.
2
369

6
.
7
3
12
/
7
/
2
0
1
5
MW
-
8
71
.
5
0

6
4
.
4
3

6
9
5
.
1
7

N
o
r
m
a
l

N
o
n
e

E
O
P

N
/
A

1
.
1
5

0
.
5
4

N
/
A

1
4
.
8
2
14
6
6.5

5
.
7
380

7
.
5
4
12
/
7
/
2
0
1
5
MW
-
8
A

8
4
.
4
0

6
4
.
5
2

6
9
5
.
1
6

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

3
.
2
4

1
0
.
5
0

N
O

1
5
.
8
4
10
3
6.7

2
.
5
378

7
.
5
8
12
/
7
/
2
0
1
5
MW
-
9
30
.
8
0

2
6
.
5
6

6
8
5
.
3
1

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

0
.
6
9

3
.
0
0

N
O

1
7
.
6
7
10
5
5.9

1
.
9
389

5
.
8
4
12
/
7
/
2
0
1
5
MW
-
9
A

4
7
.
8
0

2
7
.
0
4

6
8
5
.
0
9

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

3
.
3
9

1
0
.
5
0

N
O

1
7
.
2
7
11
6
6.3

1
.
8
370

3
.
7
2
12
/
7
/
2
0
1
5
MW
-
1
0
A

5
9
.
2
3

5
3
.
3
1

7
0
2
.
4
7

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A

0
.
9
7

1
.
0
0

Y
E
S

1
4
.
5
5
38
5.9

1
7
.
5

3
9
3

7
.
0
6
12
/
7
/
2
0
1
5
SW
-
1
N/A

N
/
A

N
/
A

N
o
r
m
a
l

N
o
n
e

N
/
A

N
/
A

N
/
A

N
/
A

N
/
A

1
1
.
2
0
91
6.5

1
4
.
2

2
3
6

8
.
5
1
12
/
7
/
2
0
1
5
SW
-
2
N/A

N
/
A

N
/
A

N
o
r
m
a
l

N
o
n
e

N
/
A

N
/
A

N
/
A

N
/
A

N
/
A

1
1
.
2
9
10
0
7.1

1
0
.
3

2
3
1

1
0
.
4
6
12
/
7
/
2
0
1
5

L
E
A
C
H
A
T
E

P
O
N
D

N
/
A

N
/
A

N
/
A

N
o
r
m
a
l

N
o
n
e

N
/
A

N
/
A

N
/
A

N
/
A

N
/
A

1
8
.
4
7
81
6
7.0

4
.
8
202

3
.
9
6
No
t
e
s
:

1
.

P
u
r
g
e

M
e
t
h
o
d
s
;

L
F
=
L
o
w

F
l
o
w
,

C
P
=
C
o
n
v
e
n
t
i
o
n
a
l

P
u
r
g
e

(
3
-
5

w
e
l
l

v
o
l
u
m
e
s
)
,

N
P
=
N
o

P
u
r
g
e

(
H
y
d
r
a
S
l
e
e
v
e
)
,

E
O
P
=
E
q
u
i
p
m
e
n
t

O
n
l
y

P
u
r
g
e
.

P
u
m
p

r
a
t
e

a
p
p
l
i
c
a
b
l
e

t
o

L
F

p
u
r
g
i
n
g

o
n
l
y
.

2
.

F
i
e
l
d

s
a
m
p
l
i
n
g

p
e
r
f
o
r
m
e
d

b
y

D
u
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C

p
e
r
s
o
n
n
e
l
.

3
.

E
V
A
C

i
n
d
i
c
a
t
e
s

w
h
e
t
h
e
r

t
h
e

w
a
t
e
r

l
e
v
e
l

i
n

t
h
e

w
e
l
l

w
a
s

d
r
a
w
n

d
o
w
n

t
o

t
h
e

l
e
v
e
l

o
f

t
h
e

p
u
m
p

d
u
r
i
n
g

p
u
r
g
i
n
g
.

4
.

N
S

i
n
d
i
c
a
t
e
s

n
o

s
a
m
p
l
e

w
a
s

c
o
l
l
e
c
t
e
d
.

T
h
e
r
e

w
a
s

i
n
s
u
f
f
i
c
i
e
n
t

w
a
t
e
r

i
n

M
W
-
5

a
n
d

M
W
-
7

t
o

c
o
l
l
e
c
t

a

g
r
o
u
n
d
w
a
t
e
r

s
a
m
p
l
e
.

5
.

µ
Լ /c
m

i
n
d
i
c
a
t
e
s

m
i
c
r
o
m
h
o
s

p
e
r

c
e
n
t
i
m
e
t
e
r
.

6
.

S
U

i
n
d
i
c
a
t
e
s

S
t
a
n
d
a
r
d

U
n
i
t
s
.

7
.

N
T
U

i
n
d
i
c
a
t
e
s

N
e
p
h
e
l
o
m
e
t
r
i
c

T
u
r
b
i
d
i
t
y

U
n
i
t
s
.

8
.

m
V
-
N
H
E

i
n
d
i
c
a
t
e
s

m
i
l
l
i
v
o
l
t
s
-
N
o
r
m
a
l

H
y
d
r
o
g
e
n

E
l
e
c
t
r
o
d
e
.

9
.

m
L
/
m
i
n

i
n
d
i
c
a
t
e
s

m
i
l
l
i
l
i
t
e
r
s

p
e
r

m
i
n
u
t
e
.
10
.

m
g
/
L

i
n
d
i
c
a
t
e
s

m
i
l
l
i
g
r
a
m
s

p
e
r

l
i
t
e
r
.
11
.

N
/
A

i
n
d
i
c
a
t
e
s

n
o
t

a
p
p
l
i
c
a
b
l
e
.
12
.

M
W
-
5

a
n
d

M
W
-
7

w
e
r
e

n
o
t

s
a
m
p
l
e
d

a
s

t
h
e
r
e

w
a
s

i
n
s
u
f
f
i
c
i
e
n
t

w
a
t
e
r

v
o
l
u
m
e

i
n

w
e
l
l
s

a
t

t
i
m
e

o
f

s
a
m
p
l
i
n
g

e
v
e
n
t
.
12
.

I
n
f
o
r
m
a
t
i
o
n

p
r
o
v
i
d
e
d

b
y

D
u
k
e

E
n
e
r
g
y

o
n

D
e
c
e
m
b
e
r

2
9
,

2
0
1
5
.
DA
T
E

S
A
M
P
L
E

I
D
WE
L
L
DE
P
T
H
(f
e
e
t
)
DE
P
T
H

T
O
WA
T
E
R
(f
e
e
t
)
WA
T
E
R
EL
E
V
.
(f
e
e
t
)

A
P
P
E
A
R
A
N
C
E
DO (mg/L)
OD
O
R
PU
R
G
E
ME
T
H
O
D

PU
M
P

RA
T
E
(m
L
/
m
i
n
)
WE
L
L
VO
L
U
M
E
(g
a
l
)
EV
A
C
VO
L
U
M
E
(g
a
l
)
EV
A
C
(y
e
s
/
n
o
)
TE
M
P
(d
e
g

C
)
SP
E
C
I
F
I
C
CO
N
D
U
C
T
A
N
C
E
(µ
Լ /c
m
)
pH
(S
U
)
TURBIDITY (NTU)ORP (mV-NHE)Page 1 of 1
Ta
b
l
e

4
–
G
r
o
u
n
d
w
a
t
e
r

F
i
e
l
d

a
n
d

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
2

(
S
y
n
t
h
e
t
i
c
a
l
l
y

L
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
Fi
e
l
d

p
H
32
0

S
U

5
1
9
3
-

N
E

6
.
5
-
8
.
5

6
.
5
-
8
.
5
*
Sp
e
c
i
f
i
c

C
o
n
d
u
c
t
a
n
c
e

3
2
3

µ
Լ /c
m

5
1
9
3
-NE

N
E

N
E
Te
m
p
e
r
a
t
u
r
e

3
2
5

°
C

5
1
9
3
-NE

N
E

N
E
To
p

C
a
s
i
n
g

3
2
8

f
e
e
t

-
-NE

N
E

N
E
De
p
t
h

t
o

W
a
t
e
r

3
1
8

f
e
e
t

-
-NE

N
E

N
E
Wa
t
e
r

E
l
e
v
a
t
i
o
n

4
2
7

f
e
e
t

-
-NE

N
E

N
E
We
l
l

D
e
p
t
h

4
1
1

f
e
e
t

-
-NE

N
E

N
E
Ar
s
e
n
i
c

1
4

µ
g
/
L

2
4
8

0
.
5
4
3

J

0
.
1
3
5

J

0
.
0
7
8

U

0
.
2
3

J

0
.
0
7
8

1
0

1
0

1
0
Ba
r
i
u
m

1
5

µ
g
/
L

2
4
8

2
4
.
6
J'
47
.
9
J'
53
.
7
J'
4.
7
9

J

0
.
1

1
0
0

7
0
0

2
,
0
0
0
Ca
d
m
i
u
m

3
4

µ
g
/
L

2
4
8

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

U

0
.
1
0
1

1

2

5
Ch
l
o
r
i
d
e

4
5
5

µ
g
/
L

2
4
8

1
,
2
5
0

1
1
,
2
0
0

5
,
5
7
0

1
,
2
8
0

2
2

N
E

2
5
0
,
0
0
0

2
5
0
,
0
0
0
*
Ch
r
o
m
i
u
m

5
1

µ
g
/
L

2
4
8

0
.
5

U

1
.
4
9

J

0
.
5

U

0
.
5

U

0
.
5

1
0

1
0

1
0
0
Le
a
d

1
3
1

µ
g
/
L

2
4
8

0
.
0
6
5

U

0
.
0
6
5

U

0
.
0
6
5

U

0
.
0
6
5

U

0
.
0
6
5

1
0

1
5

1
5
Me
r
c
u
r
y

1
3
2

µ
g
/
L

2
4
8

0
.
0
0
6

U

0
.
0
0
6

U

0
.
0
0
6

U

0
.
0
0
6

U

0
.
0
0
6

0
.
2

1

2
Se
l
e
n
i
u
m

1
8
3

µ
g
/
L

2
4
8

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

U

0
.
0
9
2

1
0

2
0

5
0
Si
l
v
e
r

1
8
4

µ
g
/
L

2
4
8

0
.
7

U

0
.
7

U

0
.
7

U

0
.
7

U

0
.
7

1
0

2
0

1
0
0
*
Su
l
f
a
t
e

3
1
5

µ
g
/
L

2
4
8

2
,
6
7
0
J'
33
9
J'
46

J

3
0
3
J'
18

2
5
0
,
0
0
0

2
5
0
,
0
0
0

2
5
0
,
0
0
0
*
TP
H

D
R
O

N
E

m
g
/
L

3
5
8

5
0
.
6
J
77
.
9
J
56
.
7
J
60
.
3
J
50

N
E
NE NE
EP
A

8
2
6
0
B

(
V
O
C
s
)
No
t
e
s
:
1
.

C
o
n
c
e
n
t
r
a
t
i
o
n
s

p
r
e
s
e
n
t
e
d

i
n

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r

(
µ
g
/
L
)

a
n
d

m
i
l
l
i
g
r
a
m
s

p
e
r

l
i
t
e
r

(
m
g
/
L
)
.
2
.

S
W
S

I
D

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

I
d
e
n
t
i
f
i
c
a
t
i
o
n

N
u
m
b
e
r
.
3
.

M
D
L

i
s

t
h
e

l
a
b
o
r
a
t
o
r
y

m
e
t
h
o
d

d
e
t
e
c
t
i
o
n

l
i
m
i
t
.

T
h
e

M
D
L

v
a
l
u
e
s

p
r
e
s
e
n
t
e
d

a
r
e

f
o
r

s
a
m
p
l
e
s

n
o
t

d
i
l
u
t
e
d

b
y

t
h
e

l
a
b
o
r
a
t
o
r
y

d
u
r
i
n
g

a
n
a
l
y
s
i
s
.

4
.

S
W
S
L

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

L
i
m
i
t
.

N
C
D
E
Q

d
e
f
i
n
e
s

t
h
e

S
W
S
L

a
s

t
h
e

l
o
w
e
s
t

a
m
o
u
n
t

o
f

a
n
a
l
y
t
e

i
n

a

s
a
m
p
l
e

t
h
a
t

c
a
n

b
e

q
u
a
n
t
i
t
a
t
i
v
e
l
y

d
e
t
e
r
m
i
n
e
d

w
i
t
h

s
u
i
t
a
b
l
e

p
r
e
c
i
s
i
o
n

a
n
d

a
c
c
u
r
a
c
y
.

5
.

1
5
A

N
C
A
C

2
L

S
t
a
n
d
a
r
d

r
e
f
e
r
s

t
o

C
l
a
s
s

G
A

S
t
a
n
d
a
r
d
s

a
s

f
o
u
n
d

i
n

1
5
A

N
C
A
C

0
2
L

.
0
2
0
2

G
r
o
u
n
d
w
a
t
e
r

Q
u
a
l
i
t
y

S
t
a
n
d
a
r
d
s
,

l
a
s
t

a
m
e
n
d
e
d

o
n

A
p
r
i
l

1
,

2
0
1
3
.

6
.

M
C
L

i
s

t
h
e

F
e
d
e
r
a
l

M
a
x
i
m
u
m

C
o
n
t
a
m
i
n
a
n
t

L
e
v
e
l

a
s

f
o
u
n
d

i
n

4
0

C
F
R
,

S
u
b
p
a
r
t

G
,

§
1
4
1
.
6
2
.
7
.

*

C
o
n
c
e
n
t
r
a
t
i
o
n

l
i
s
t
e
d

i
s

a

s
e
c
o
n
d
a
r
y

m
a
x
i
m
u
m

c
o
n
t
a
m
i
n
a
n
t

l
e
v
e
l

(
S
M
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5
Page 1 of 1
Ta
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Leachate PondSW-1 Page 1 of 1

A
Appendix A
Field Sampling Forms

ANALYZER SERIAL #:
WEATHER CONDITIONS:
DATE:TIME:DATE:TIME:
Calibation Instrument Standard Instrument Standard
Standard Value Value Value Value
SS 0.0 ▬/▬►0.0 0.0 ▬/▬►0.0
SS 227.2 ▬▬►227 227.1 ▬/▬►227
SS 74.7 ▬/▬►75 74.8 ▬/▬►75
SS ▬/▬►▬/▬►
B (7.00)7.03 ▬▬►7.02 7.08 ▬/▬►7.02
B (4.00)3.94 ▬▬►4.00 4.13 ▬/▬►4.00
B (10.00)9.91 ▬/▬►10.06 10.07 ▬/▬►10.06
19.93 19.70
pH Check B (7.00)▬▬►
Time:
SS (7.00)290 ▬▬►295 288 ▬/▬►296
SS (4.00)N/A ▬/▬►470 N/A ▬/▬►470
19.99 19.70
W 8.90 8.80
W 8.90 8.90
AW 8.79 ▬▬►8.90 9.00 ▬/▬►8.85
SS 53.8 ▬/▬►54.3 54.4 ▬/▬►54.3
NIST N/A ▬/▬►N/A N/A ▬/▬►N/A
KEY:
NOTES:
SS = Standard solution AW = Average Winkler ▬/▬►= Not Adjusted To
(mmHg)
B = Buffer W = Winkler ▬▬► = Adjusted To N/A = Not Applicable
Replaced DO electrolyte See Notes
Field Barometric Pressure
Beginning BP 748.3 (mmHg)Ending BP 745.2
Tested - OK See Notes Tested - OK See Notes
Dissolved Oxygen Subsystem
Replaced Teflon Membrane Cleaned Electrode
Tested - OK See Notes
Oxidation Reduction Subsystem Temperature Subsystem
Cleaned Electrode Cleaned Electrode
Tested - OK Replaced ref Electrode KCL
See Notes Replaced Ref. Electrode Tip
INSTRUMENT MAINTENANCE DATE / TIME
Conductance Subsystem pH Subsystem
Cleaned Electrodes Cleaned Electrodes
Temp Cert Device #
TEMP
(deg C)Adjustment Not Available Adjustment Not Available
ORP Temp.ORP Temp.
Calibration Pass
TURB
(ntu)Calibration Accepted Calibration Accepted
DO
(mg/L)Calibration Accepted
Buffer Temp.
Calibration Accepted Calibration Pass
pH
(units)
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Buffer Temp.Buffer Temp.
Parameter Calibration Results Calibration Results
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
CHECK (uS/cm)
SPEC. COND.
(uS/cm)
Instrument Zeroed Zero Pass
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Calibration Date / Time 7-Dec-15 5:45 8-Dec-15 5:20
CALIBRATION BP (mmHg)748.3 CALIBRATION BP (mmHg)745.2
COLLECTORS:LDC, PSP SURFACE UNIT SERIAL #:3858
ANALYZER MODEL#:MS5 66121
PROCEDURE #:HYDROLAB 3210.5 VALIDATED BY:
FIELD SAMPLING CALIBRATION FORM
STUDY:McGUIRE NUCLEAR STATION - LANDFILL 2 GROUNDWATER MONITORING
DATE (s):December 7, 2015 SURFACE UNIT READER:LDC
OTHER EQUIPMENT:TURBIDIMETER NO.2 - 3260-GW Clear, calm, 35 to 55 deg F
ANALYZER SERIAL #:
WEATHER CONDITIONS:
DATE:TIME:DATE:TIME:
Calibation Instrument Standard Instrument Standard
Standard Value Value Value Value
SS 0.0 ▬/▬►0.0 0.0 ▬/▬►0.0
SS 225.5 ▬▬►227 226.3 ▬/▬►227
SS 73.4 ▬/▬►75 72.6 ▬/▬►75
SS ▬/▬►▬/▬►
B (7.00)6.82 ▬▬►7.02 7.04 ▬/▬►7.02
B (4.00)3.98 ▬▬►4.00 4.02 ▬/▬►4.00
B (10.00)10.13 ▬/▬►10.06 10.18 ▬/▬►10.06
19.95 19.70
pH Check B (7.00)▬▬►
Time:
SS (7.00)301 ▬▬►295 289 ▬/▬►296
SS (4.00)N/A ▬/▬►470 N/A ▬/▬►471
20.03 19.67
W 8.90 8.80
W 8.90 8.90
AW 8.89 ▬▬►8.90 8.89 ▬/▬►8.85
SS 54.8 ▬/▬►54.1 54.4 ▬/▬►54.1
NIST N/A ▬/▬►N/A N/A ▬/▬►N/A
KEY:
NOTES:
SS = Standard solution AW = Average Winkler ▬/▬►= Not Adjusted To
(mmHg)
B = Buffer W = Winkler ▬▬► = Adjusted To N/A = Not Applicable
Replaced DO electrolyte See Notes
Field Barometric Pressure
Beginning BP 748.3 (mmHg)Ending BP 745.2
Tested - OK See Notes Tested - OK See Notes
Dissolved Oxygen Subsystem
Replaced Teflon Membrane Cleaned Electrode
Tested - OK See Notes
Oxidation Reduction Subsystem Temperature Subsystem
Cleaned Electrode Cleaned Electrode
Tested - OK Replaced ref Electrode KCL
See Notes Replaced Ref. Electrode Tip
INSTRUMENT MAINTENANCE DATE / TIME
Conductance Subsystem pH Subsystem
Cleaned Electrodes Cleaned Electrodes
Temp Cert Device #
TEMP
(deg C)Adjustment Not Available Adjustment Not Available
ORP Temp.ORP Temp.
Calibration Pass
TURB
(ntu)Calibration Accepted Calibration Accepted
DO
(mg/L)Calibration Accepted
Buffer Temp.
Calibration Accepted Calibration Pass
pH
(units)
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Buffer Temp.Buffer Temp.
Parameter Calibration Results Calibration Results
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
CHECK (uS/cm)
SPEC. COND.
(uS/cm)
Instrument Zeroed Zero Pass
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Calibration Date / Time 7-Dec-15 5:35 8-Dec-15 5:10
CALIBRATION BP (mmHg)748.3 CALIBRATION BP (mmHg)745.2
COLLECTORS:LDC, PSP SURFACE UNIT SERIAL #:S05042
ANALYZER MODEL#:MS5 66120
PROCEDURE #:HYDROLAB 3210.5 VALIDATED BY:
FIELD SAMPLING CALIBRATION FORM
STUDY:McGUIRE NUCLEAR STATION - LANDFILL 2 GROUNDWATER MONITORING
DATE (s):December 7, 2015 SURFACE UNIT READER:PSP
OTHER EQUIPMENT:TURBIDIMETER NO.1 - 3260-GW Clear, calm, 35 to 55 deg F
49.90 63.90
38 (psi)10 (sec)(sec)
(gal)
0.10 (gal)
@
QC By:
NO SAMPLE, Insufficient Volume to sample
DATE TIME
DISSOLVED
OXYGEN
12/7/2015
Sample preservation verified to pH
(units)
ORP
(ft)(YES/NO)
VOLUME EVACUATION COND.
PURGE METHOD
Conventional
DISCHARGERECHARGEPRESSURE 5
PUMP CONTROLLER SETTINGS
0.1631CONVERSION FACTOR
Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
0.10WELL VOLUME
(gal)
FIELD CREW LDC, PSP
MONITORING WELL INFORMATION
2
N/A
PROCEDURE NO 3175.2DUKE ENERGY
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING
SAMPLING DATE(s)7-Dec-2015
63.58
62.90PUMP INTAKE DEPTH (ft TOC)63.90
TOC ELEV (ft msl)
GS ELEV (ft msl)
768.31
766.42
WELL/LOCATION NAME MW-5
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27
WELL DEPTH (ft TOC)
WELL DIAMETER (in)MIDDLE OF WETTED SCREEN (ft toc)
WELL VOL
SCREEN INTERVAL (ft TOC)TO
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)63.26 WATER COLUMN (ft)0.64
EQUIPMENT INFORMATION
LEVEL METER SERIAL#26056 SAMPLING EQUIPMENT
TUBING DIAMETER (in)1/2 OD
QED T1200
PURGE COMPLETE TEMP SPECIFIC pH TURBIDITY
WATER ELEVATION (ft msl)705.05
APPEARANCE
DETECTED ODOR None
WATER LEVEL
AFTER PURGE *(recalculates on
current water
level)(deg C)(umho/cm)(SU)(NTU)(mV-NHE)(mg/L)
N/A N/A
CHLORINE (mg/l)SAMPLE COLLECTED BY
N/A
TOTAL PURGE
VOLUME
0.00
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
WELL CASING
WELL CONDITION
PROTECTIVE CASING
WELL PAD
WELL TAG
Good Condition
Good Condition
Good Condition
SAMPLING NOTES
ADDITIONAL WELL CONDITION NOTES
Good Tag
82.00 96.00
50 (psi)10 (sec)(sec)
(gal)
5.01 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
15.25 PSP 12/7/2015 1035 0
5.00 NO 16.24 56 6.40 1.2 390 7.66
5.00 NO 16.35 56 6.39 1.0 389 7.63
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
5.25 NO 16.33 54 6.35 1.5 385
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
7.58
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)65.28 WATER COLUMN (ft)30.72 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)703.14 WELL VOLUME 5.01
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26056 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)768.42 MIDDLE OF WETTED SCREEN (ft toc)89.00
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)96.00 GS ELEV (ft msl)766.45 PUMP INTAKE DEPTH (ft TOC)95.00
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME MW-5A
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
23.20 37.20
20 (psi)10 (sec)(sec)
(gal)
0.91 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME MW-6
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)728.45 MIDDLE OF WETTED SCREEN (ft toc)34.43
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)37.20 GS ELEV (ft msl)726.79 PUMP INTAKE DEPTH (ft TOC)36.20
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26056 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)31.65 WATER COLUMN (ft)5.55 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)696.80 WELL VOLUME 0.91
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
1.00 NO 15.35 119 5.86 1.5 402
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
6.76
1.00 NO 15.34 132 6.03 2.2 396 6.42
1.00 NO 15.16 124 5.94 1.4 399 6.52
1.00 NO 15.32 137 6.08 3.9 401 6.31
1.00 NO 15.24 132 6.06 3.3 400 6.44
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
5.00 PSP 12/7/2015 0820 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
33.90 47.90
25 (psi)13 (sec)(sec)
(gal)
2.78 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME MW-6A
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)728.98 MIDDLE OF WETTED SCREEN (ft toc)40.90
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)47.90 GS ELEV (ft msl)727.54 PUMP INTAKE DEPTH (ft TOC)46.90
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 7
26056 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)30.84 WATER COLUMN (ft)17.06 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)698.14 WELL VOLUME 2.78
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
3.00 NO 15.55 61 5.44 2.5 425
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
8.20
3.00 NO 15.58 63 5.57 1.1 427 7.90
3.00 NO 15.74 62 5.55 1.5 426 8.06
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
9.00 PSP 12/7/2015 0830 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
23.30 37.30
(psi)(sec)(sec)
(gal)
0.22 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME MW-7
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)725.86 MIDDLE OF WETTED SCREEN (ft toc)36.63
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)37.30 GS ELEV (ft msl)723.72 PUMP INTAKE DEPTH (ft TOC)36.30
No sample - Insufficient volume to pump PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE
23585 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)35.95 WATER COLUMN (ft)1.35 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)689.91 WELL VOLUME 0.22
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
N/A
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
N/A
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
0.00 12/7/2015 N/A
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
No sample - Insufficient volume to pump.
45.40 59.40
30 (psi)10 (sec)(sec)
(gal)
4.08 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME MW-7A
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)724.66 MIDDLE OF WETTED SCREEN (ft toc)52.40
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)59.40 GS ELEV (ft msl)722.74 PUMP INTAKE DEPTH (ft TOC)58.40
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)34.40 WATER COLUMN (ft)25.00 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)690.26 WELL VOLUME 4.08
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
4.25 NO 16.19 115 6.57 3.9 374
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
6.78
4.25 NO 16.26 120 6.46 2.2 369 6.73
4.25 NO 16.24 118 6.55 3.5 375 6.76
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
12.75 LDC 12/7/2015 1005 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
57.50 71.50
35 (psi)10 (sec)(sec)
(gal)
1531 (ml)
495 (ml)
2026 (ml)=0.54 (gal)@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR EQUIPMENT PURGE ONLY SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME MW-8
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)759.60 MIDDLE OF WETTED SCREEN (ft toc)67.97
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)71.50 GS ELEV (ft msl)757.30 PUMP INTAKE DEPTH (ft TOC)70.50
See note below PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Equip. Only Purge
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)64.43 WATER COLUMN (ft)7.07 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)695.17 WELL VOLUME 1.15
INITIAL FLOW FINAL TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
(ft)(ml/min)(ft)(deg C)(umho/cm)(SU)(NTU)(mV-NHE)(mg/L)
WATER LEVEL RATE WATER LEVEL COND.OXYGEN
5.7 380 7.54 N/A
Tubing Volume Removed 1.0 gal.EQUIPMENT PURGE ONLY SAMPLE CHLORINE
(mg/l)Pump (Bladder) Volume
64.43 N/A Below pump 14.82 146 6.48
0
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
SAMPLE COLLECTED BY DATE TIME
Total Purge Volume LDC 12/7/2015 0745
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
Slow recharge well - Account for tubing and bladder volume - record field measurements and begin sampling.
70.40 84.40
45 (psi)10 (sec)(sec)
(gal)
3.24 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME MW-8A
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)759.68 MIDDLE OF WETTED SCREEN (ft toc)77.40
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)84.40 GS ELEV (ft msl)757.61 PUMP INTAKE DEPTH (ft TOC)83.40
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)64.52 WATER COLUMN (ft)19.88 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)695.16 WELL VOLUME 3.24
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
3.50 NO 15.73 102 6.68 2.7 369
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
7.64
3.50 NO 15.84 103 6.69 2.5 378 7.58
3.50 NO 15.75 103 6.67 2.5 371 7.59
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
10.50 LDC 12/7/2015 0845 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
QC for DRO collected
16.80 30.80
15 (psi)11 (sec)(sec)
(gal)
0.69 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME MW-9
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)711.87 MIDDLE OF WETTED SCREEN (ft toc)28.68
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)30.80 GS ELEV (ft msl)710.27 PUMP INTAKE DEPTH (ft TOC)29.80
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 4
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)26.56 WATER COLUMN (ft)4.24 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)685.31 WELL VOLUME 0.69
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
0.75 NO 17.59 92 5.85 2.7 397
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
5.37
0.75 NO 17.66 102 5.89 1.8 394 5.79
0.75 NO 17.63 100 5.77 2.0 390 5.42
0.75 NO 17.67 105 5.91 1.9 389 5.84
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
3.00 LDC 12/7/2015 1130 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
33.80 47.80
25 (psi)10 (sec)(sec)
(gal)
3.39 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME MW-9A
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)712.13 MIDDLE OF WETTED SCREEN (ft toc)40.80
SCREEN LENGTH (ft)14.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)47.80 GS ELEV (ft msl)710.30 PUMP INTAKE DEPTH (ft TOC)46.80
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26054 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)27.04 WATER COLUMN (ft)20.76 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)685.09 WELL VOLUME 3.39
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
3.50 NO 17.27 119 6.15 1.7 383
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
3.36
3.50 NO 17.27 116 6.33 1.8 370 3.72
3.50 NO 17.31 117 6.31 1.6 372 3.63
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
10.50 LDC 12/7/2015 1120 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
44.23 59.23
30 (psi)10 (sec)(sec)
(gal)
0.97 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME MW-10A
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)755.78 MIDDLE OF WETTED SCREEN (ft toc)56.27
SCREEN LENGTH (ft)15.00 ELEV REF NGVD 27 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)59.23 GS ELEV (ft msl)753.87 PUMP INTAKE DEPTH (ft TOC)58.23
Well Evacuated @ 0925 On 12/7/15 PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26056 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)53.31 WATER COLUMN (ft)5.92 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)702.47 WELL VOLUME 0.97
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
1.00 BELOW PUMP YES 14.55 38 5.87 17.5 393
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
7.06 N/A
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
1.00 PSP 12/7/2015 1205 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
Water level at 1200 hrs was 53.27 feet = 0.97 gallons, full recovery.
0.00 0.00
N/A (psi)N/A (sec)(sec)
(gal)
(ft)=(in)@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR NO PURGE SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME SW-1
MONITORING WELL INFORMATION
WELL DIAMETER (in)TOC ELEV (ft msl)N/A MIDDLE OF WETTED SCREEN (ft toc)
SCREEN LENGTH (ft)ELEV REF SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)GS ELEV (ft msl)PUMP INTAKE DEPTH (ft TOC)N/A
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE N/A
N/A SAMPLING EQUIPMENT PERISTALTIC PUMP PURGE METHOD
TUBING DIAMETER (in)3/8 OD No Purge
DETECTED ODOR None CONVERSION FACTOR
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)N/A WATER COLUMN (ft)Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)WELL VOLUME
TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
TIME
PSP 12/7/2015
LENGTH DEPTH (top)DEPLOYED COND.OXYGEN
(inches)(ft TOC)(deg C)(umho/cm)(SU)
HYDRASLEEVE DEPLOYED DATE
(NTU)(mV-NHE)(mg/L)
N/A N/A N/A 11.20 91 6.52 14.2
1130
236 8.51
0
N/A
Deployed Water Column In Screen
Above Top Of Hydrasleeve
NO PURGE SAMPLE CHLORINE
(mg/l)Top Weight SAMPLE COLLECTED BY DATE
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING
WELL PAD
WELL CASING
WELL TAG
SAMPLING NOTES
0.00 0.00
N/A (psi)N/A (sec)(sec)
(gal)
(ft)=(in)@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR NO PURGE SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME SW-2
MONITORING WELL INFORMATION
WELL DIAMETER (in)TOC ELEV (ft msl)N/A MIDDLE OF WETTED SCREEN (ft toc)
SCREEN LENGTH (ft)ELEV REF SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)GS ELEV (ft msl)PUMP INTAKE DEPTH (ft TOC)N/A
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE N/A
N/A SAMPLING EQUIPMENT PERISTALTIC PUMP PURGE METHOD
TUBING DIAMETER (in)3/8 OD No Purge
DETECTED ODOR None CONVERSION FACTOR
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)N/A WATER COLUMN (ft)Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)WELL VOLUME
TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
TIME
LDC 12/7/2015
LENGTH DEPTH (top)DEPLOYED COND.OXYGEN
(inches)(ft TOC)(deg C)(umho/cm)(SU)
HYDRASLEEVE DEPLOYED DATE
(NTU)(mV-NHE)(mg/L)
N/A N/A N/A 11.29 100 7.07 10.3
1245
231 10.46
0
N/A
Deployed Water Column In Screen
Above Top Of Hydrasleeve
NO PURGE SAMPLE CHLORINE
(mg/l)Top Weight SAMPLE COLLECTED BY DATE
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING
WELL PAD
WELL CASING
WELL TAG
SAMPLING NOTES
0.00 0.00
N/A (psi)N/A (sec)(sec)
(gal)
(ft)=(in)@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR NO PURGE SAMPLING
PROJECT NAME LANDFILL 2 GROUNDWATER MONITORING FIELD CREW LDC, PSP
SAMPLING DATE(s)7-Dec-2015 WELL/LOCATION NAME LEACHATE POND
MONITORING WELL INFORMATION
WELL DIAMETER (in)TOC ELEV (ft msl)N/A MIDDLE OF WETTED SCREEN (ft toc)
TUBING DIAMETER (in)No Purge
PURGE METHOD
SCREEN LENGTH (ft)ELEV REF SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)GS ELEV (ft msl)PUMP INTAKE DEPTH (ft TOC)N/A
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE N/A
N/A SAMPLING EQUIPMENT GRAB
DETECTED ODOR None CONVERSION FACTOR
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)N/A WATER COLUMN (ft)Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)WELL VOLUME
TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
TIME
LDC 12/7/2015
LENGTH DEPTH (top)DEPLOYED COND.OXYGEN
(inches)(ft TOC)(deg C)(umho/cm)(SU)
HYDRASLEEVE DEPLOYED DATE
(NTU)(mV-NHE)(mg/L)
N/A N/A N/A 18.47 816 7.02 4.8
1215
202 3.96
0
N/A
Deployed Water Column In Screen
Above Top Of Hydrasleeve
NO PURGE SAMPLE CHLORINE
(mg/l)Top Weight SAMPLE COLLECTED BY DATE
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING
WELL PAD
WELL CASING
WELL TAG
SAMPLING NOTES
Pipe discharge flow rate =2.8 gal/min.
PERMIT #
MW-5 MW-5A MW-6 MW-6A MW-7 MW-7A MW-8 MW-8A MW-9 MW-9A MW-10A SW-1 SW-2
YES YES YES YES YES YES YES YES YES YES YES YES YES
YES YES YES YES YES YES YES YES YES YES YES YES YES
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
YES YES YES YES YES YES YES YES YES YES YES N/A N/A
Lacks required information - Total well depth
Lacks required information - Depth to screen
Lacks required information - Non potable tag
NOTE:
Lacks required information - Completion date
FLUSH MOUNT WELLS
Vault in good condition
Water inside vault
Vault bolt holes broken or stripped
Bolts stripped
Vault lid cracked or broken
WELL ID TAGS
Well tag in good condition
Well tag missing
Well tag damaged / illegible
Lacks required information - Driller Reg #
Replaced damaged well cap
Fire ants around concrete pad
WELL PROTECTIVE CASINGS
Casing in good condition
Damaged casing / still functional
Damaged casing / repair required
Broken hinge on protective lid
Wasp nest inside protective casing
Ants inside protective casing
WELL CAPS
Well cap in good conditon
Damaged / needs replacement
Undermined / washing out
Lock in good condition
Lock rusted, difficult to open / needs replacing
Replaced damaged lock
WELL CASINGS
Casing in good condition
Damaged casing / still functional
Damaged casing / repair required
CONCRETE PADS
Pad in good condition
Minor cracks
Major cracks / broken / repair required
WELL LOCK CONDITION
PAGE 1 OF 1
ACCESS TO WELLS
Access cleared into well
Access cleared around well
Tall grass or weeds - needs mowing
Road washing out / muddy / needs grading
Fallen tree blocking access
WELL SECURITY
Well found locked
Well found unlocked
SITE CONTACT John Williamson, Bill Spencer FIELD CREW LDC, PSP
WEATHER Clear, calm, 35 to 55 deg F
NORTH CAROLINA GROUNDWATER SAMPLING SITE CHECKLIST
LOCATION / SITE McGUIRE NUCLEAR STATION - LANDFILL #2 GROUNDWATER MONITORING 60-04 SAMPLE DATE December 7, 2015
WELL DEPTH TO WATER Purge AVG *WELL EVAC SPECIFIC
WELL DEPTH WATER ELEV.Method PMP RATE VOL VOL EVAC TEMP CONDUCTANCE pH TURBIDITY ORP DO
DATE NO.(feet-toc)(feet-toc)(feet)APPEARANCE ODOR (ml/min)(gal)(gal)(yes/no)(deg C)(umho/cm)(units)(NTU)(mV-NHE)(mg/l)
12/7/2015 MW-5 63.90 63.26 705.05 NS NS NS NS 0.10 NS NS NS NS NS NS NS NS
12/7/2015 MW-5A 96.00 65.28 703.14 Normal None C N/A 5.01 15.25 NO 16.24 56 6.4 1.2 390 7.66
12/7/2015 MW-6 37.20 31.65 696.80 Normal None C N/A 0.91 5.00 NO 15.32 137 6.1 3.9 401 6.31
12/7/2015 MW-6A 47.90 30.84 698.14 Normal None C N/A 2.78 9.00 NO 15.58 63 5.6 1.1 427 7.90
12/7/2015 MW-7 37.30 35.95 689.91 NS NS NS NS 0.22 NS NS NS NS NS NS NS NS
12/7/2015 MW-7A 59.40 34.40 690.26 Normal None C N/A 4.08 12.75 NO 16.26 120 6.5 2.2 369 6.73
12/7/2015 MW-8 71.50 64.43 695.17 Normal None EOP N/A 1.15 0.54 N/A 14.82 146 6.5 5.7 N/A N/A
12/7/2015 MW-8A 84.40 64.52 695.16 Normal None C N/A 3.24 10.50 NO 15.84 103 6.7 2.5 378 7.58
12/7/2015 MW-9 30.80 26.56 685.31 Normal None C N/A 0.69 3.00 NO 17.67 105 5.9 1.9 389 5.84
12/7/2015 MW-9A 47.80 27.04 685.09 Normal None C N/A 3.39 10.50 NO 17.27 116 6.3 1.8 370 3.72
12/7/2015 MW-10A 59.23 53.31 702.47 Normal None C N/A 0.97 1.00 YES 14.55 38 5.9 17.5 393 7.06
12/7/2015 SW-1 N/A N/A N/A Normal None NP N/A N/A N/A N/A 11.20 91 6.5 14.2 236 8.51
12/7/2015 SW-2 N/A N/A N/A Normal None NP N/A N/A N/A N/A 11.29 100 7.1 10.3 231 10.46
12/7/2015 LEACHATE POND N/A N/A N/A Normal None NP N/A N/A N/A N/A 18.47 816 7.0 4.8 202 3.96
Purge Methods
LF = Low Flow
LF(M) = Low Flow (Mod.)
C = Connventional
NP = No Purge
EOP = Equip. Only Purge
LO = Level Only
NS = Not Sampled / Insufficient Volume
* = Applicable to LF & LF(M) Purging Only
McGUIRE NUCLEAR STATION
LANDFILL 2 GROUNDWATER MONITORING
GROUNDWATER MONITORING FIELD DATA
PERMIT #60-04

B
Appendix B
Laboratory Report and
Chain-of-Custody Forms

13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J15120015
Project Name:MCGUIRE - GW LF2
Lab Contact:Peggy Kendall
Date:12/28/2015
Customer Address:13225 Hagers Ferry Rd
Customer Name(s):TIM HUNSUCKER, CHUCK CAMPBELL
Mail Code: MG01CH
Huntersville, NC 28078-8985
Phone:
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Peggy Kendall) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Peggy Kendall
Page 1 of 78
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2015037421 MCGUIRE 07-Dec-15 6:15 AM PSP TRIP BLANK
2015037423 MCGUIRE 07-Dec-15 10:35 AM PSP MW-5A
2015037424 MCGUIRE 07-Dec-15 8:20 AM PSP MW-6
2015037425 MCGUIRE 07-Dec-15 8:30 AM PSP MW-6A
2015037427 MCGUIRE 07-Dec-15 10:05 AM LDC MW-7A
2015037428 MCGUIRE 07-Dec-15 7:45 AM LDC MW-8
2015037429 MCGUIRE 07-Dec-15 8:45 AM LDC MW-8A
2015037430 MCGUIRE 07-Dec-15 11:30 AM LDC MW-9
2015037431 MCGUIRE 07-Dec-15 11:20 AM LDC MW-9A
2015037432 MCGUIRE 07-Dec-15 12:05 PM PSP MW-10A
2015037433 MCGUIRE 07-Dec-15 11:30 AM PSP SW-1
2015037434 MCGUIRE 07-Dec-15 12:45 PM LDC SW-2
2015037435 MCGUIRE 07-Dec-15 12:15 PM LDC LEACHATE POND
2015037436 MCGUIRE 07-Dec-15 8:45 AM LDC QC - WELL # MW-8A
2015037437 MCGUIRE 07-Dec-15 12:55 PM PSP FIELD BLANK
15 Total Samples
Page 2 of 78
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:12/28/2015
Electronic Data Deliverable (EDD) Sent Separatel
Page 3 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037421
Collection Date:07-Dec-15 6:15 AM
Site:TRIP BLANK
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 4 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037423
Collection Date:07-Dec-15 10:35 AM
Site:MW-5A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)21 mg/L
(CaCO3)
SM 2320B4d 12/08/2015 18:02 GHUTCHI51
INORGANIC IONS BY IC
Chloride 1.2 mg/L EPA 300.0 12/10/2015 14:11 BGN90340.1 1
Sulfate 2.7 mg/L EPA 300.0 12/10/2015 14:11 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 11:35 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.025 mg/L EPA 200.7 12/14/2015 11:05 FCJORDA0.005 1
Calcium (Ca)3.00 mg/L EPA 200.7 12/14/2015 11:05 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 11:05 FCJORDA0.005 1
Magnesium (Mg)1.51 mg/L EPA 200.7 12/14/2015 11:05 FCJORDA0.005 1
Potassium (K)0.975 mg/L EPA 200.7 12/14/2015 11:05 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 11:05 FCJORDA0.005 1
Sodium (Na)6.10 mg/L EPA 200.7 12/14/2015 11:05 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 09:14 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 09:14 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 09:14 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 09:14 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 5 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037424
Collection Date:07-Dec-15 8:20 AM
Site:MW-6
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)46 mg/L
(CaCO3)
SM 2320B4d 12/08/2015 18:02 GHUTCHI51
INORGANIC IONS BY IC
Chloride 11 mg/L EPA 300.0 12/10/2015 17:00 BGN90340.2 2
Sulfate 0.34 mg/L EPA 300.0 12/10/2015 17:00 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 11:37 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.048 mg/L EPA 200.7 12/14/2015 11:17 FCJORDA0.005 1
Calcium (Ca)14.1 mg/L EPA 200.7 12/14/2015 11:17 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 11:17 FCJORDA0.005 1
Magnesium (Mg)5.14 mg/L EPA 200.7 12/14/2015 11:17 FCJORDA0.005 1
Potassium (K)0.743 mg/L EPA 200.7 12/14/2015 11:17 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 11:17 FCJORDA0.005 1
Sodium (Na)5.25 mg/L EPA 200.7 12/14/2015 11:17 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 06:04 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 06:04 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 06:04 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 06:04 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 6 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037425
Collection Date:07-Dec-15 8:30 AM
Site:MW-6A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)12 mg/L
(CaCO3)
SM 2320B4d 12/08/2015 18:02 GHUTCHI51
INORGANIC IONS BY IC
Chloride 5.6 mg/L EPA 300.0 12/10/2015 15:19 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 300.0 12/10/2015 15:19 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 11:39 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.054 mg/L EPA 200.7 12/14/2015 11:21 FCJORDA0.005 1
Calcium (Ca)5.02 mg/L EPA 200.7 12/14/2015 11:21 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 11:21 FCJORDA0.005 1
Magnesium (Mg)1.65 mg/L EPA 200.7 12/14/2015 11:21 FCJORDA0.005 1
Potassium (K)0.249 mg/L EPA 200.7 12/14/2015 11:21 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 11:21 FCJORDA0.005 1
Sodium (Na)3.63 mg/L EPA 200.7 12/14/2015 11:21 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 06:32 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 06:32 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 06:32 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 06:32 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 7 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037427
Collection Date:07-Dec-15 10:05 AM
Site:MW-7A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)60 mg/L
(CaCO3)
SM2320B 12/08/2015 16:59 GHUTCHI201
INORGANIC IONS BY IC
Chloride 1.3 mg/L EPA 300.0 12/10/2015 15:35 BGN90340.1 1
Sulfate 0.30 mg/L EPA 300.0 12/10/2015 15:35 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 11:42 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)< 0.005 mg/L EPA 200.7 12/14/2015 11:25 FCJORDA0.005 1
Calcium (Ca)15.0 mg/L EPA 200.7 12/14/2015 11:25 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 11:25 FCJORDA0.005 1
Magnesium (Mg)3.61 mg/L EPA 200.7 12/14/2015 11:25 FCJORDA0.005 1
Potassium (K)0.469 mg/L EPA 200.7 12/14/2015 11:25 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 11:25 FCJORDA0.005 1
Sodium (Na)4.11 mg/L EPA 200.7 12/14/2015 11:25 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 06:39 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 06:39 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 06:39 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 06:39 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 8 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037428
Collection Date:07-Dec-15 7:45 AM
Site:MW-8
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)69 mg/L
(CaCO3)
SM2320B 12/08/2015 16:59 GHUTCHI201
INORGANIC IONS BY IC
Chloride 1.5 mg/L EPA 300.0 12/10/2015 15:52 BGN90340.1 1
Sulfate 0.64 mg/L EPA 300.0 12/10/2015 15:52 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 11:44 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.020 mg/L EPA 200.7 12/14/2015 11:29 FCJORDA0.005 1
Calcium (Ca)16.9 mg/L EPA 200.7 12/14/2015 11:29 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 11:29 FCJORDA0.005 1
Magnesium (Mg)3.55 mg/L EPA 200.7 12/14/2015 11:29 FCJORDA0.005 1
Potassium (K)1.02 mg/L EPA 200.7 12/14/2015 11:29 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 11:29 FCJORDA0.005 1
Sodium (Na)6.70 mg/L EPA 200.7 12/14/2015 11:29 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 06:46 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 06:46 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 06:46 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 06:46 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 9 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037429
Collection Date:07-Dec-15 8:45 AM
Site:MW-8A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)44 mg/L
(CaCO3)
SM 2320B4d 12/08/2015 18:02 GHUTCHI51
INORGANIC IONS BY IC
Chloride 2.1 mg/L EPA 300.0 12/10/2015 16:09 BGN90340.1 1
Sulfate 1.2 mg/L EPA 300.0 12/10/2015 16:09 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 11:47 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.028 mg/L EPA 200.7 12/14/2015 11:32 FCJORDA0.005 1
Calcium (Ca)10.5 mg/L EPA 200.7 12/14/2015 11:32 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 11:32 FCJORDA0.005 1
Magnesium (Mg)3.38 mg/L EPA 200.7 12/14/2015 11:32 FCJORDA0.005 1
Potassium (K)1.20 mg/L EPA 200.7 12/14/2015 11:32 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 11:32 FCJORDA0.005 1
Sodium (Na)4.69 mg/L EPA 200.7 12/14/2015 11:32 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 06:53 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 06:53 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 06:53 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 06:53 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 10 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037430
Collection Date:07-Dec-15 11:30 AM
Site:MW-9
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)45 mg/L
(CaCO3)
SM 2320B4d 12/08/2015 18:02 GHUTCHI51
INORGANIC IONS BY IC
Chloride 1.9 mg/L EPA 300.0 12/10/2015 16:26 BGN90340.1 1
Sulfate 0.12 mg/L EPA 300.0 12/10/2015 16:26 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 11:49 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.024 mg/L EPA 200.7 12/14/2015 11:36 FCJORDA0.005 1
Calcium (Ca)10.5 mg/L EPA 200.7 12/14/2015 11:36 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 11:36 FCJORDA0.005 1
Magnesium (Mg)4.78 mg/L EPA 200.7 12/14/2015 11:36 FCJORDA0.005 1
Potassium (K)0.405 mg/L EPA 200.7 12/14/2015 11:36 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 11:36 FCJORDA0.005 1
Sodium (Na)3.56 mg/L EPA 200.7 12/14/2015 11:36 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 07:21 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 07:21 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 07:21 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 07:21 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 11 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037431
Collection Date:07-Dec-15 11:20 AM
Site:MW-9A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)44 mg/L
(CaCO3)
SM 2320B4d 12/08/2015 18:02 GHUTCHI51
INORGANIC IONS BY IC
Chloride 1.7 mg/L EPA 300.0 12/10/2015 16:43 BGN90340.1 1
Sulfate 0.19 mg/L EPA 300.0 12/10/2015 16:43 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 11:56 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.011 mg/L EPA 200.7 12/14/2015 11:40 FCJORDA0.005 1
Calcium (Ca)11.1 mg/L EPA 200.7 12/14/2015 11:40 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 11:40 FCJORDA0.005 1
Magnesium (Mg)4.91 mg/L EPA 200.7 12/14/2015 11:40 FCJORDA0.005 1
Potassium (K)0.509 mg/L EPA 200.7 12/14/2015 11:40 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 11:40 FCJORDA0.005 1
Sodium (Na)5.15 mg/L EPA 200.7 12/14/2015 11:40 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 07:28 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 07:28 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 07:28 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 07:28 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 12 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037432
Collection Date:07-Dec-15 12:05 PM
Site:MW-10A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)5.8 mg/L
(CaCO3)
SM 2320B4d 12/08/2015 18:02 GHUTCHI51
INORGANIC IONS BY IC
Chloride 1.3 mg/L EPA 300.0 12/10/2015 18:08 BGN90340.1 1
Sulfate 0.51 mg/L EPA 300.0 12/10/2015 18:08 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 12:03 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.021 mg/L EPA 200.7 12/14/2015 11:44 FCJORDA0.005 1
Calcium (Ca)1.63 mg/L EPA 200.7 12/14/2015 11:44 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 11:44 FCJORDA0.005 1
Magnesium (Mg)1.26 mg/L EPA 200.7 12/14/2015 11:44 FCJORDA0.005 1
Potassium (K)0.993 mg/L EPA 200.7 12/14/2015 11:44 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 11:44 FCJORDA0.005 1
Sodium (Na)1.76 mg/L EPA 200.7 12/14/2015 11:44 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 07:35 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 07:35 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 07:35 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 07:35 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 13 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037433
Collection Date:07-Dec-15 11:30 AM
Site:SW-1
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)38 mg/L
(CaCO3)
SM2320B 12/08/2015 16:59 GHUTCHI201
INORGANIC IONS BY IC
Chloride 2.4 mg/L EPA 300.0 12/10/2015 18:58 BGN90340.1 1
Sulfate 3.3 mg/L EPA 300.0 12/10/2015 18:58 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 12:05 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.033 mg/L EPA 200.7 12/14/2015 11:48 FCJORDA0.005 1
Calcium (Ca)7.54 mg/L EPA 200.7 12/14/2015 11:48 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 11:48 FCJORDA0.005 1
Magnesium (Mg)3.19 mg/L EPA 200.7 12/14/2015 11:48 FCJORDA0.005 1
Potassium (K)1.08 mg/L EPA 200.7 12/14/2015 11:48 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 11:48 FCJORDA0.005 1
Sodium (Na)4.76 mg/L EPA 200.7 12/14/2015 11:48 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 07:42 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 07:42 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 07:42 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 07:42 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 14 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037434
Collection Date:07-Dec-15 12:45 PM
Site:SW-2
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)44 mg/L
(CaCO3)
SM2320B 12/08/2015 16:59 GHUTCHI201
INORGANIC IONS BY IC
Chloride 2.4 mg/L EPA 300.0 12/10/2015 19:15 BGN90340.1 1
Sulfate 3.9 mg/L EPA 300.0 12/10/2015 19:15 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 12:08 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.026 mg/L EPA 200.7 12/14/2015 12:00 FCJORDA0.005 1
Calcium (Ca)9.37 mg/L EPA 200.7 12/14/2015 12:00 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 12:00 FCJORDA0.005 1
Magnesium (Mg)3.75 mg/L EPA 200.7 12/14/2015 12:00 FCJORDA0.005 1
Potassium (K)1.13 mg/L EPA 200.7 12/14/2015 12:00 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 12:00 FCJORDA0.005 1
Sodium (Na)5.04 mg/L EPA 200.7 12/14/2015 12:00 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 07:49 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 07:49 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 07:49 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 07:49 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 15 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037435
Collection Date:07-Dec-15 12:15 PM
Site:LEACHATE POND
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)300 mg/L
(CaCO3)
SM2320B 12/08/2015 16:59 GHUTCHI201
INORGANIC IONS BY IC
Chloride 14 mg/L EPA 300.0 12/14/2015 10:42 BGN9034110
Sulfate 120 mg/L EPA 300.0 12/14/2015 10:42 BGN9034220
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 12:10 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.087 mg/L EPA 200.7 12/14/2015 12:25 FCJORDA0.005 1
Calcium (Ca)101 mg/L EPA 200.7 12/14/2015 12:25 FCJORDA0.1 10
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 12:25 FCJORDA0.005 1
Magnesium (Mg)15.6 mg/L EPA 200.7 12/14/2015 12:25 FCJORDA0.005 1
Potassium (K)11.8 mg/L EPA 200.7 12/14/2015 12:25 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 12:25 FCJORDA0.005 1
Sodium (Na)34.3 mg/L EPA 200.7 12/14/2015 12:25 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)1.69 ug/L EPA 200.8 12/15/2015 07:56 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 07:56 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 07:56 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 07:56 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 16 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037436
Collection Date:07-Dec-15 8:45 AM
Site:QC - WELL # MW-8A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 17 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
2015037437
Collection Date:07-Dec-15 12:55 PM
Site:FIELD BLANK
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)< 5 mg/L
(CaCO3)
SM 2320B4d 12/08/2015 18:02 GHUTCHI51
INORGANIC IONS BY IC
Chloride < 0.1 mg/L EPA 300.0 12/10/2015 13:54 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 300.0 12/10/2015 13:54 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 12/22/2015 12:12 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)< 0.005 mg/L EPA 200.7 12/14/2015 12:07 FCJORDA0.005 1
Calcium (Ca)< 0.01 mg/L EPA 200.7 12/14/2015 12:07 FCJORDA0.01 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 12:07 FCJORDA0.005 1
Magnesium (Mg)< 0.005 mg/L EPA 200.7 12/14/2015 12:07 FCJORDA0.005 1
Potassium (K)< 0.1 mg/L EPA 200.7 12/14/2015 12:07 FCJORDA0.1 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 12:07 FCJORDA0.005 1
Sodium (Na)< 0.05 mg/L EPA 200.7 12/14/2015 12:07 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 08:03 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 08:03 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 08:03 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 12/15/2015 08:03 MHALL311
TOTAL PETROLEUM HYDROCARBONS - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 18 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
Q15120212 ALK_FIX4.5 ALKALINITY (FIXED END POINT 4.5)
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Duplicate # 1
RPD
Parent Sample: J15120015 -- 2015037427
Alkalinity (mg/L CaCO3)0.276mg/L
(CaCO3)
-159.7
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Alkalinity (mg/L CaCO3)81.6 101mg/L
(CaCO3)
-12080182.8
Page 19 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
Q15120213 ALK_LL_Fix LOW LEVEL ALKALINITY (FIXED END POINT)
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Duplicate # 1
RPD
Parent Sample: J15120015 -- 2015037423
Alkalinity (mg/L CaCO3)0.932mg/L
(CaCO3)
-120.7
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Alkalinity (mg/L CaCO3)8.16 85.6mg/L
(CaCO3)
-1208016.98
Page 20 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
Q15120260 Dionex INORGANIC IONS BY IC
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Chloride 0.0265 mg/L -10.0265 0.1 < 1/2 RDL
Sulfate 0.002 mg/L -10.002 0.1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
IS # 1
% Recovery LCL UCLSpike
Chloride 6.34 5 103mg/L -1208016.34
Sulfate 7.8 5 105mg/L -1208017.8
Final QualifierDilMeasuredUnits:Parameter
ISD # 1
RPD% Recovery LCL UCLSpike
Chloride 6.53 5 107 3.56mg/L -1208016.53
Sulfate 7.83 5 105 0.433mg/L -1208017.83
Final QualifierDilMeasuredUnits:Parameter
IS # 2
% Recovery LCL UCLSpike
Chloride 6.47 5 105mg/L -1208016.47
Sulfate 5.74 5 105mg/L -1208015.74
Final QualifierDilMeasuredUnits:Parameter
ISD # 2
RPD% Recovery LCL UCLSpike
Chloride 6.45 5 104 0.358mg/L -1208016.45
Sulfate 5.75 5 105 0.152mg/L -1208015.75
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Chloride 5.05 5 101mg/L -1208015.05
Sulfate 5.09 5 102mg/L -1208015.09
Page 21 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
Q15120457 HG 245.1 MERCURY (COLD VAPOR) IN WATER
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Mercury (Hg) -0.008 ug/L -1-0.008 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
Blank # 2
RDL Relative Concentration
Mercury (Hg) -0.004 ug/L -1-0.004 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Mercury (Hg) 2.11 2 105ug/L -1158512.11
Final QualifierDilMeasuredUnits:Parameter
LCS # 2
% Recovery LCL UCLSpike
Mercury (Hg) 2.08 2 104ug/L -1158512.08
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J15110243 -- 2015036235
Mercury (Hg) 0.97 100 98.4ug/L -1307010097
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J15110243 -- 2015036235
Mercury (Hg) 0.979 100 99.4 0.961ug/L -1307010097.9
Final QualifierDilMeasuredUnits:Parameter
MS # 2
% Recovery LCL UCLSpike
Parent Sample: J15120015 -- 2015037431
Mercury (Hg) 0.967 1 96.9ug/L -1307010.967
Final QualifierDilMeasuredUnits:Parameter
MSD # 2
RPD% Recovery LCL UCLSpike
Parent Sample: J15120015 -- 2015037431
Mercury (Hg) 0.98 1 98.2 1.33ug/L -1307010.98
Page 22 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
Q15120219 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Barium (Ba) -0.000085 mg/L -1-0.000085 0.005 < 1/2 RDL
Calcium (Ca) 0.000776 mg/L -10.000776 0.01 < 1/2 RDL
Chromium (Cr) -0.000736 mg/L -1-0.000736 0.005 < 1/2 RDL
Magnesium (Mg) 0.000264 mg/L -10.000264 0.005 < 1/2 RDL
Potassium (K) -0.0996 mg/L -1-0.0996 0.1 < 1/2 RDL
Silver (Ag) 0.000206 mg/L -10.000206 0.005 < 1/2 RDL
Sodium (Na) -0.00427 mg/L -1-0.00427 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Barium (Ba) 5.24 5 105mg/L -1208015.24
Calcium (Ca) 4.78 5 95.6mg/L -1208014.78
Chromium (Cr) 4.97 5 99.4mg/L -1208014.97
Magnesium (Mg) 5.06 5 101mg/L -1208015.06
Potassium (K) 5.14 5 103mg/L -1208015.14
Silver (Ag) 0.512 0.5 102mg/L -1208010.512
Sodium (Na) 5.16 5 103mg/L -1208015.16
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J15120015 -- 2015037423
Barium (Ba) 5.26 5 105mg/L -1257515.26
Calcium (Ca) 7.98 5 99.5mg/L -1257517.98
Chromium (Cr) 4.96 5 99.2mg/L -1257514.96
Magnesium (Mg) 6.6 5 102mg/L -1257516.6
Potassium (K) 6.06 5 102mg/L -1257516.06
Silver (Ag) 0.505 0.5 101mg/L -1257510.505
Sodium (Na) 10.9 5 95.9mg/L -12575110.9
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J15120015 -- 2015037423
Barium (Ba) 5.28 5 105 0.42mg/L -1257515.28
Calcium (Ca) 8 5 100 0.441mg/L -1257518
Chromium (Cr) 4.99 5 99.8 0.563mg/L -1257514.99
Magnesium (Mg) 6.63 5 102 0.47mg/L -1257516.63
Potassium (K) 6.11 5 103 0.998mg/L -1257516.11
Silver (Ag) 0.508 0.5 102 0.629mg/L -1257510.508
Sodium (Na) 10.9 5 96.7 0.893mg/L -12575110.9
Page 23 of 78
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120015
Q15120221 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Arsenic (As) 0.0727 ug/L -10.0727 1 < 1/2 RDL
Cadmium (Cd) 0.0037 ug/L -10.0037 1 < 1/2 RDL
Lead (Pb) -0.0093 ug/L -1-0.0093 1 < 1/2 RDL
Selenium (Se) 0.0156 ug/L -10.0156 1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Arsenic (As) 50.9 50 102ug/L -12080150.9
Cadmium (Cd) 50.5 50 101ug/L -12080150.5
Lead (Pb) 51.5 50 103ug/L -12080151.5
Selenium (Se) 50.1 50 100ug/L -12080150.1
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J15120015 -- 2015037424
Arsenic (As) 49.9 50 99.5ug/L -12080149.9
Cadmium (Cd) 49.8 50 99.7ug/L -12080149.8
Lead (Pb) 50 50 100ug/L -12080150
Selenium (Se) 48.5 50 97ug/L -12080148.5
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J15120015 -- 2015037424
Arsenic (As) 49.8 50 99.4 0.101ug/L -12080149.8
Cadmium (Cd) 50.2 50 100 0.64ug/L -12080150.2
Lead (Pb) 50.2 50 100 0.36ug/L -12080150.2
Selenium (Se) 48.7 50 97.4 0.35ug/L -12080148.7
Page 24 of 78
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-93697-1
Client Project/Site: MNS Landfill #2 J15120015
For:
Duke Energy Corporation
13339 Hagers Ferry Road
Huntersville, North Carolina 28078
Attn: Lab Customer
Authorized for release by:
12/22/2015 11:36:08 AM
Shali Brown, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Page 25 of 78
Table of Contents
Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
TestAmerica Job ID: 490-93697-1
Page 2 of 53 TestAmerica Nashville12/22/2015
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .48
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53
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Sample Summary
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-93697-1 TRIP BLANK Water 12/07/15 06:15 12/09/15 10:10
490-93697-2 MW-5A Water 12/07/15 10:35 12/09/15 10:10
490-93697-3 MW-6 Water 12/07/15 08:20 12/09/15 10:10
490-93697-4 MW-6A Water 12/07/15 08:30 12/09/15 10:10
490-93697-5 MW-7A Water 12/07/15 10:05 12/09/15 10:10
490-93697-6 MW-8 Water 12/07/15 07:45 12/09/15 10:10
490-93697-7 MW-8A Water 12/07/15 08:45 12/09/15 10:10
490-93697-8 MW-9 Water 12/07/15 11:30 12/09/15 10:10
490-93697-9 MW-9A Water 12/07/15 11:20 12/09/15 10:10
490-93697-10 MW-10A Water 12/07/15 12:05 12/09/15 10:10
490-93697-11 SW-1 Water 12/07/15 11:30 12/09/15 10:10
490-93697-12 SW-2 Water 12/07/15 12:45 12/09/15 10:10
490-93697-13 LEACHATE POND Water 12/07/15 12:15 12/09/15 10:10
490-93697-14 FIELD BLANK Water 12/07/15 12:55 12/09/15 10:10
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Case Narrative
Client: Duke Energy Corporation TestAmerica Job ID: 490-93697-1
Project/Site: MNS Landfill #2 J15120015
Job ID: 490-93697-1
Laboratory: TestAmerica Nashville
Narrative
CASE NARRATIVE
Client: Duke Energy Corporation
Project: MNS Landfill #2 J15120015
Report Number: 490-93697-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
TestAmerica Nashville attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses
performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the
application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data
have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions
to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written
approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
All solid sample results are reported on an "as received" basis unless otherwise indicated by the presence of a % solids value in the
method header.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT
The samples were received on 12/9/2015 10:10 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 3 coolers at receipt time were 1.3º C, 1.8º C and 2.0º C.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples TRIP BLANK (490-93697-1), MW-5A (490-93697-2), MW-6 (490-93697-3), MW-6A (490-93697-4), MW-7A (490-93697-5), MW-8
(490-93697-6), MW-8A (490-93697-7), MW-9 (490-93697-8), MW-9A (490-93697-9), MW-10A (490-93697-10), SW-1 (490-93697-11), SW-2
(490-93697-12), LEACHATE POND (490-93697-13) and FIELD BLANK (490-93697-14) were analyzed for volatile organic compounds
(GC-MS) in accordance with EPA SW-846 Method 8260B. The samples were analyzed on 12/13/2015.
Carbon disulfide was detected in method blank MB 490-306017/7 at a level that was above the method detection limit but below the
reporting limit. The value should be considered an estimate, and has been flagged. If the associated sample reported a result above the
MDL and/or RL, the result has been flagged. Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
DIESEL RANGE ORGANICS (DRO)
Samples MW-5A (490-93697-2), MW-6 (490-93697-3), MW-6A (490-93697-4), MW-7A (490-93697-5), MW-8 (490-93697-6), MW-8A
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Case Narrative
Client: Duke Energy Corporation TestAmerica Job ID: 490-93697-1
Project/Site: MNS Landfill #2 J15120015
Job ID: 490-93697-1 (Continued)
Laboratory: TestAmerica Nashville (Continued)
(490-93697-7), MW-9 (490-93697-8), MW-9A (490-93697-9), MW-10A (490-93697-10), SW-1 (490-93697-11), SW-2 (490-93697-12),
LEACHATE POND (490-93697-13) and FIELD BLANK (490-93697-14) were analyzed for diesel range organics (DRO) in accordance with
EPA SW-846 Method 8015C - DRO. The samples were prepared on 12/14/2015 and analyzed on 12/15/2015 and 12/16/2015.
Surrogates are added during the extraction process prior to dilution. When the sample dilution is 5X or greater, surrogate recoveries are
diluted out and no corrective action is required.
o-Terphenyl (Surr) failed the surrogate recovery criteria high for MW-10A (490-93697-10). o-Terphenyl (Surr) failed the surrogate recovery
criteria high for SW-1 (490-93697-11). There was insufficient sample to perform a re-extraction; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC Semi VOA
Qualifier Description
X Surrogate is outside control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-1Client Sample ID: TRIP BLANK
Matrix: WaterDate Collected: 12/07/15 06:15
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 15:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 15:31 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 15:31 1BenzeneND
1.00 0.150 ug/L 12/13/15 15:31 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 15:31 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 15:31 1BromoformND
1.00 0.350 ug/L 12/13/15 15:31 1BromomethaneND
50.0 2.64 ug/L 12/13/15 15:31 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 15:31 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 15:31 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 15:31 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 15:31 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 15:31 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 15:31 1ChloroformND
1.00 0.360 ug/L 12/13/15 15:31 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 15:31 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 15:31 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 15:31 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 15:31 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 15:31 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 15:31 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 15:31 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 15:31 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 15:31 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 15:31 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 15:31 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 15:31 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 15:31 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 15:31 1IodomethaneND
1.00 1.00 ug/L 12/13/15 15:31 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 15:31 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 15:31 1StyreneND
1.00 0.150 ug/L 12/13/15 15:31 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 15:31 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 15:31 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 15:31 1TolueneND
5.00 0.460 ug/L 12/13/15 15:31 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 15:31 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 15:31 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 15:31 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 15:31 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 15:31 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 15:31 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 15:31 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 15:31 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 15:31 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 15:31 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-1Client Sample ID: TRIP BLANK
Matrix: WaterDate Collected: 12/07/15 06:15
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)80 70-130 12/13/15 15:31 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)114 12/13/15 15:31 170-130
1,2-Dichloroethane-d4 (Surr)101 12/13/15 15:31 170-130
Toluene-d8 (Surr)91 12/13/15 15:31 170-130
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-2Client Sample ID: MW-5A
Matrix: WaterDate Collected: 12/07/15 10:35
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 17:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 17:50 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 17:50 1BenzeneND
1.00 0.150 ug/L 12/13/15 17:50 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 17:50 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 17:50 1BromoformND
1.00 0.350 ug/L 12/13/15 17:50 1BromomethaneND
50.0 2.64 ug/L 12/13/15 17:50 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 17:50 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 17:50 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 17:50 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 17:50 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 17:50 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 17:50 1ChloroformND
1.00 0.360 ug/L 12/13/15 17:50 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 17:50 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 17:50 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 17:50 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 17:50 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 17:50 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 17:50 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 17:50 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 17:50 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 17:50 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 17:50 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 17:50 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 17:50 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 17:50 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 17:50 1IodomethaneND
1.00 1.00 ug/L 12/13/15 17:50 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 17:50 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 17:50 1StyreneND
1.00 0.150 ug/L 12/13/15 17:50 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 17:50 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 17:50 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 17:50 1TolueneND
5.00 0.460 ug/L 12/13/15 17:50 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 17:50 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 17:50 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 17:50 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 17:50 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 17:50 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 17:50 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 17:50 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 17:50 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 17:50 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 17:50 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-2Client Sample ID: MW-5A
Matrix: WaterDate Collected: 12/07/15 10:35
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)86 70-130 12/13/15 17:50 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)118 12/13/15 17:50 170-130
1,2-Dichloroethane-d4 (Surr)102 12/13/15 17:50 170-130
Toluene-d8 (Surr)89 12/13/15 17:50 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 50.6 J 99.0 49.5 ug/L 12/14/15 11:08 12/15/15 22:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)69 50-150 12/14/15 11:08 12/15/15 22:03 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-3Client Sample ID: MW-6
Matrix: WaterDate Collected: 12/07/15 08:20
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 18:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 18:18 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 18:18 1BenzeneND
1.00 0.150 ug/L 12/13/15 18:18 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 18:18 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 18:18 1BromoformND
1.00 0.350 ug/L 12/13/15 18:18 1BromomethaneND
50.0 2.64 ug/L 12/13/15 18:18 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 18:18 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 18:18 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 18:18 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 18:18 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 18:18 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 18:18 1ChloroformND
1.00 0.360 ug/L 12/13/15 18:18 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 18:18 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 18:18 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 18:18 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 18:18 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 18:18 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 18:18 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 18:18 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 18:18 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 18:18 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 18:18 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 18:18 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 18:18 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 18:18 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 18:18 1IodomethaneND
1.00 1.00 ug/L 12/13/15 18:18 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 18:18 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 18:18 1StyreneND
1.00 0.150 ug/L 12/13/15 18:18 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 18:18 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 18:18 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 18:18 1TolueneND
5.00 0.460 ug/L 12/13/15 18:18 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 18:18 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 18:18 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 18:18 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 18:18 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 18:18 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 18:18 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 18:18 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 18:18 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 18:18 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 18:18 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-3Client Sample ID: MW-6
Matrix: WaterDate Collected: 12/07/15 08:20
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)85 70-130 12/13/15 18:18 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)116 12/13/15 18:18 170-130
1,2-Dichloroethane-d4 (Surr)101 12/13/15 18:18 170-130
Toluene-d8 (Surr)87 12/13/15 18:18 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 77.9 J 99.0 49.5 ug/L 12/14/15 11:08 12/15/15 22:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)80 50-150 12/14/15 11:08 12/15/15 22:18 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-4Client Sample ID: MW-6A
Matrix: WaterDate Collected: 12/07/15 08:30
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 18:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 18:46 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 18:46 1BenzeneND
1.00 0.150 ug/L 12/13/15 18:46 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 18:46 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 18:46 1BromoformND
1.00 0.350 ug/L 12/13/15 18:46 1BromomethaneND
50.0 2.64 ug/L 12/13/15 18:46 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 18:46 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 18:46 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 18:46 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 18:46 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 18:46 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 18:46 1ChloroformND
1.00 0.360 ug/L 12/13/15 18:46 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 18:46 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 18:46 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 18:46 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 18:46 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 18:46 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 18:46 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 18:46 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 18:46 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 18:46 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 18:46 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 18:46 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 18:46 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 18:46 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 18:46 1IodomethaneND
1.00 1.00 ug/L 12/13/15 18:46 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 18:46 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 18:46 1StyreneND
1.00 0.150 ug/L 12/13/15 18:46 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 18:46 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 18:46 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 18:46 1TolueneND
5.00 0.460 ug/L 12/13/15 18:46 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 18:46 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 18:46 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 18:46 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 18:46 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 18:46 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 18:46 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 18:46 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 18:46 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 18:46 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 18:46 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-4Client Sample ID: MW-6A
Matrix: WaterDate Collected: 12/07/15 08:30
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)87 70-130 12/13/15 18:46 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)115 12/13/15 18:46 170-130
1,2-Dichloroethane-d4 (Surr)101 12/13/15 18:46 170-130
Toluene-d8 (Surr)88 12/13/15 18:46 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 56.7 J 99.0 49.5 ug/L 12/14/15 11:08 12/15/15 22:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)82 50-150 12/14/15 11:08 12/15/15 22:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-5Client Sample ID: MW-7A
Matrix: WaterDate Collected: 12/07/15 10:05
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 19:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 19:13 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 19:13 1BenzeneND
1.00 0.150 ug/L 12/13/15 19:13 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 19:13 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 19:13 1BromoformND
1.00 0.350 ug/L 12/13/15 19:13 1BromomethaneND
50.0 2.64 ug/L 12/13/15 19:13 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 19:13 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 19:13 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 19:13 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 19:13 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 19:13 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 19:13 1ChloroformND
1.00 0.360 ug/L 12/13/15 19:13 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 19:13 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 19:13 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 19:13 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 19:13 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 19:13 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 19:13 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 19:13 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 19:13 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 19:13 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 19:13 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 19:13 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 19:13 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 19:13 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 19:13 1IodomethaneND
1.00 1.00 ug/L 12/13/15 19:13 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 19:13 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 19:13 1StyreneND
1.00 0.150 ug/L 12/13/15 19:13 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 19:13 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 19:13 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 19:13 1TolueneND
5.00 0.460 ug/L 12/13/15 19:13 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 19:13 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 19:13 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 19:13 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 19:13 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 19:13 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 19:13 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 19:13 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 19:13 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 19:13 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 19:13 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-5Client Sample ID: MW-7A
Matrix: WaterDate Collected: 12/07/15 10:05
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)75 70-130 12/13/15 19:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)116 12/13/15 19:13 170-130
1,2-Dichloroethane-d4 (Surr)100 12/13/15 19:13 170-130
Toluene-d8 (Surr)90 12/13/15 19:13 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 60.3 J 99.0 49.5 ug/L 12/14/15 11:08 12/15/15 22:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)79 50-150 12/14/15 11:08 12/15/15 22:49 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-6Client Sample ID: MW-8
Matrix: WaterDate Collected: 12/07/15 07:45
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 19:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 19:41 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 19:41 1BenzeneND
1.00 0.150 ug/L 12/13/15 19:41 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 19:41 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 19:41 1BromoformND
1.00 0.350 ug/L 12/13/15 19:41 1BromomethaneND
50.0 2.64 ug/L 12/13/15 19:41 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 19:41 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 19:41 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 19:41 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 19:41 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 19:41 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 19:41 1ChloroformND
1.00 0.360 ug/L 12/13/15 19:41 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 19:41 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 19:41 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 19:41 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 19:41 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 19:41 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 19:41 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 19:41 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 19:41 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 19:41 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 19:41 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 19:41 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 19:41 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 19:41 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 19:41 1IodomethaneND
1.00 1.00 ug/L 12/13/15 19:41 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 19:41 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 19:41 1StyreneND
1.00 0.150 ug/L 12/13/15 19:41 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 19:41 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 19:41 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 19:41 1TolueneND
5.00 0.460 ug/L 12/13/15 19:41 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 19:41 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 19:41 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 19:41 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 19:41 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 19:41 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 19:41 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 19:41 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 19:41 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 19:41 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 19:41 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-6Client Sample ID: MW-8
Matrix: WaterDate Collected: 12/07/15 07:45
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)86 70-130 12/13/15 19:41 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)116 12/13/15 19:41 170-130
1,2-Dichloroethane-d4 (Surr)100 12/13/15 19:41 170-130
Toluene-d8 (Surr)88 12/13/15 19:41 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 135 99.0 49.5 ug/L 12/14/15 11:08 12/15/15 23:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)123 50-150 12/14/15 11:08 12/15/15 23:04 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-7Client Sample ID: MW-8A
Matrix: WaterDate Collected: 12/07/15 08:45
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 20:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 20:09 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 20:09 1BenzeneND
1.00 0.150 ug/L 12/13/15 20:09 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 20:09 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 20:09 1BromoformND
1.00 0.350 ug/L 12/13/15 20:09 1BromomethaneND
50.0 2.64 ug/L 12/13/15 20:09 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 20:09 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 20:09 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 20:09 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 20:09 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 20:09 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 20:09 1ChloroformND
1.00 0.360 ug/L 12/13/15 20:09 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 20:09 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 20:09 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 20:09 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 20:09 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 20:09 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 20:09 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 20:09 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 20:09 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 20:09 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 20:09 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 20:09 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 20:09 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 20:09 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 20:09 1IodomethaneND
1.00 1.00 ug/L 12/13/15 20:09 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 20:09 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 20:09 1StyreneND
1.00 0.150 ug/L 12/13/15 20:09 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 20:09 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 20:09 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 20:09 1TolueneND
5.00 0.460 ug/L 12/13/15 20:09 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 20:09 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 20:09 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 20:09 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 20:09 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 20:09 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 20:09 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 20:09 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 20:09 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 20:09 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 20:09 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-7Client Sample ID: MW-8A
Matrix: WaterDate Collected: 12/07/15 08:45
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)83 70-130 12/13/15 20:09 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)114 12/13/15 20:09 170-130
1,2-Dichloroethane-d4 (Surr)99 12/13/15 20:09 170-130
Toluene-d8 (Surr)89 12/13/15 20:09 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 63.1 J 100 50.0 ug/L 12/14/15 11:08 12/15/15 23:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)92 50-150 12/14/15 11:08 12/15/15 23:19 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-8Client Sample ID: MW-9
Matrix: WaterDate Collected: 12/07/15 11:30
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 20:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 20:37 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 20:37 1BenzeneND
1.00 0.150 ug/L 12/13/15 20:37 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 20:37 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 20:37 1BromoformND
1.00 0.350 ug/L 12/13/15 20:37 1BromomethaneND
50.0 2.64 ug/L 12/13/15 20:37 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 20:37 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 20:37 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 20:37 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 20:37 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 20:37 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 20:37 1ChloroformND
1.00 0.360 ug/L 12/13/15 20:37 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 20:37 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 20:37 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 20:37 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 20:37 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 20:37 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 20:37 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 20:37 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 20:37 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 20:37 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 20:37 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 20:37 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 20:37 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 20:37 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 20:37 1IodomethaneND
1.00 1.00 ug/L 12/13/15 20:37 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 20:37 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 20:37 1StyreneND
1.00 0.150 ug/L 12/13/15 20:37 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 20:37 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 20:37 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 20:37 1TolueneND
5.00 0.460 ug/L 12/13/15 20:37 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 20:37 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 20:37 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 20:37 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 20:37 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 20:37 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 20:37 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 20:37 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 20:37 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 20:37 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 20:37 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-8Client Sample ID: MW-9
Matrix: WaterDate Collected: 12/07/15 11:30
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)88 70-130 12/13/15 20:37 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)114 12/13/15 20:37 170-130
1,2-Dichloroethane-d4 (Surr)100 12/13/15 20:37 170-130
Toluene-d8 (Surr)89 12/13/15 20:37 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 108 99.0 49.5 ug/L 12/14/15 11:08 12/16/15 00:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)94 50-150 12/14/15 11:08 12/16/15 00:05 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-9Client Sample ID: MW-9A
Matrix: WaterDate Collected: 12/07/15 11:20
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 21:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 21:05 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 21:05 1BenzeneND
1.00 0.150 ug/L 12/13/15 21:05 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 21:05 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 21:05 1BromoformND
1.00 0.350 ug/L 12/13/15 21:05 1BromomethaneND
50.0 2.64 ug/L 12/13/15 21:05 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 21:05 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 21:05 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 21:05 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 21:05 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 21:05 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 21:05 1ChloroformND
1.00 0.360 ug/L 12/13/15 21:05 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 21:05 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 21:05 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 21:05 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 21:05 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 21:05 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 21:05 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 21:05 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 21:05 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 21:05 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 21:05 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 21:05 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 21:05 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 21:05 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 21:05 1IodomethaneND
1.00 1.00 ug/L 12/13/15 21:05 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 21:05 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 21:05 1StyreneND
1.00 0.150 ug/L 12/13/15 21:05 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 21:05 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 21:05 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 21:05 1TolueneND
5.00 0.460 ug/L 12/13/15 21:05 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 21:05 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 21:05 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 21:05 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 21:05 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 21:05 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 21:05 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 21:05 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 21:05 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 21:05 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 21:05 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-9Client Sample ID: MW-9A
Matrix: WaterDate Collected: 12/07/15 11:20
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)87 70-130 12/13/15 21:05 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)116 12/13/15 21:05 170-130
1,2-Dichloroethane-d4 (Surr)98 12/13/15 21:05 170-130
Toluene-d8 (Surr)86 12/13/15 21:05 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 59.0 J 100 50.0 ug/L 12/14/15 11:08 12/16/15 00:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)80 50-150 12/14/15 11:08 12/16/15 00:20 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-10Client Sample ID: MW-10A
Matrix: WaterDate Collected: 12/07/15 12:05
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 21:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 21:33 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 21:33 1BenzeneND
1.00 0.150 ug/L 12/13/15 21:33 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 21:33 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 21:33 1BromoformND
1.00 0.350 ug/L 12/13/15 21:33 1BromomethaneND
50.0 2.64 ug/L 12/13/15 21:33 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 21:33 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 21:33 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 21:33 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 21:33 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 21:33 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 21:33 1ChloroformND
1.00 0.360 ug/L 12/13/15 21:33 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 21:33 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 21:33 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 21:33 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 21:33 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 21:33 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 21:33 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 21:33 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 21:33 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 21:33 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 21:33 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 21:33 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 21:33 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 21:33 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 21:33 1IodomethaneND
1.00 1.00 ug/L 12/13/15 21:33 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 21:33 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 21:33 1StyreneND
1.00 0.150 ug/L 12/13/15 21:33 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 21:33 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 21:33 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 21:33 1TolueneND
5.00 0.460 ug/L 12/13/15 21:33 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 21:33 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 21:33 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 21:33 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 21:33 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 21:33 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 21:33 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 21:33 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 21:33 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 21:33 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 21:33 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-10Client Sample ID: MW-10A
Matrix: WaterDate Collected: 12/07/15 12:05
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)74 70-130 12/13/15 21:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)117 12/13/15 21:33 170-130
1,2-Dichloroethane-d4 (Surr)100 12/13/15 21:33 170-130
Toluene-d8 (Surr)87 12/13/15 21:33 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 206 104 52.1 ug/L 12/14/15 11:08 12/16/15 00:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)184 X 50-150 12/14/15 11:08 12/16/15 00:36 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-11Client Sample ID: SW-1
Matrix: WaterDate Collected: 12/07/15 11:30
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 22:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 22:01 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 22:01 1BenzeneND
1.00 0.150 ug/L 12/13/15 22:01 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 22:01 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 22:01 1BromoformND
1.00 0.350 ug/L 12/13/15 22:01 1BromomethaneND
50.0 2.64 ug/L 12/13/15 22:01 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 22:01 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 22:01 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 22:01 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 22:01 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 22:01 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 22:01 1ChloroformND
1.00 0.360 ug/L 12/13/15 22:01 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 22:01 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 22:01 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 22:01 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 22:01 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 22:01 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 22:01 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 22:01 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 22:01 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 22:01 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 22:01 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 22:01 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 22:01 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 22:01 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 22:01 1IodomethaneND
1.00 1.00 ug/L 12/13/15 22:01 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 22:01 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 22:01 1StyreneND
1.00 0.150 ug/L 12/13/15 22:01 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 22:01 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 22:01 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 22:01 1TolueneND
5.00 0.460 ug/L 12/13/15 22:01 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 22:01 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 22:01 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 22:01 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 22:01 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 22:01 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 22:01 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 22:01 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 22:01 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 22:01 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 22:01 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-11Client Sample ID: SW-1
Matrix: WaterDate Collected: 12/07/15 11:30
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)82 70-130 12/13/15 22:01 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)117 12/13/15 22:01 170-130
1,2-Dichloroethane-d4 (Surr)100 12/13/15 22:01 170-130
Toluene-d8 (Surr)88 12/13/15 22:01 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 265 99.0 49.5 ug/L 12/14/15 11:08 12/16/15 00:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)230 X 50-150 12/14/15 11:08 12/16/15 00:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-12Client Sample ID: SW-2
Matrix: WaterDate Collected: 12/07/15 12:45
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 22:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 22:29 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 22:29 1BenzeneND
1.00 0.150 ug/L 12/13/15 22:29 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 22:29 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 22:29 1BromoformND
1.00 0.350 ug/L 12/13/15 22:29 1BromomethaneND
50.0 2.64 ug/L 12/13/15 22:29 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 22:29 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 22:29 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 22:29 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 22:29 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 22:29 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 22:29 1ChloroformND
1.00 0.360 ug/L 12/13/15 22:29 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 22:29 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 22:29 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 22:29 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 22:29 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 22:29 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 22:29 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 22:29 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 22:29 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 22:29 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 22:29 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 22:29 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 22:29 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 22:29 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 22:29 1IodomethaneND
1.00 1.00 ug/L 12/13/15 22:29 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 22:29 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 22:29 1StyreneND
1.00 0.150 ug/L 12/13/15 22:29 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 22:29 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 22:29 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 22:29 1TolueneND
5.00 0.460 ug/L 12/13/15 22:29 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 22:29 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 22:29 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 22:29 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 22:29 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 22:29 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 22:29 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 22:29 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 22:29 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 22:29 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 22:29 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-12Client Sample ID: SW-2
Matrix: WaterDate Collected: 12/07/15 12:45
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)87 70-130 12/13/15 22:29 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)115 12/13/15 22:29 170-130
1,2-Dichloroethane-d4 (Surr)100 12/13/15 22:29 170-130
Toluene-d8 (Surr)91 12/13/15 22:29 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 114 99.0 49.5 ug/L 12/14/15 11:08 12/16/15 01:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)101 50-150 12/14/15 11:08 12/16/15 01:06 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-13Client Sample ID: LEACHATE POND
Matrix: WaterDate Collected: 12/07/15 12:15
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 9.42 J 25.0 2.66 ug/L 12/13/15 22:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 22:57 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 22:57 1BenzeneND
1.00 0.150 ug/L 12/13/15 22:57 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 22:57 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 22:57 1BromoformND
1.00 0.350 ug/L 12/13/15 22:57 1BromomethaneND
50.0 2.64 ug/L 12/13/15 22:57 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 22:57 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 22:57 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 22:57 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 22:57 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 22:57 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 22:57 1ChloroformND
1.00 0.360 ug/L 12/13/15 22:57 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 22:57 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 22:57 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 22:57 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 22:57 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 22:57 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 22:57 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 22:57 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 22:57 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 22:57 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 22:57 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 22:57 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 22:57 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 22:57 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 22:57 1IodomethaneND
1.00 1.00 ug/L 12/13/15 22:57 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 22:57 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 22:57 1StyreneND
1.00 0.150 ug/L 12/13/15 22:57 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 22:57 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 22:57 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 22:57 1Toluene30.9
5.00 0.460 ug/L 12/13/15 22:57 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 22:57 1trans-1,2-Dichloroethene 0.332 J
1.00 0.170 ug/L 12/13/15 22:57 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 22:57 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 22:57 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 22:57 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 22:57 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 22:57 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 22:57 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 22:57 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 22:57 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-13Client Sample ID: LEACHATE POND
Matrix: WaterDate Collected: 12/07/15 12:15
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)87 70-130 12/13/15 22:57 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)117 12/13/15 22:57 170-130
1,2-Dichloroethane-d4 (Surr)103 12/13/15 22:57 170-130
Toluene-d8 (Surr)89 12/13/15 22:57 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 871 99.0 49.5 ug/L 12/14/15 11:08 12/16/15 01:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)72 50-150 12/14/15 11:08 12/16/15 01:21 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-14Client Sample ID: FIELD BLANK
Matrix: WaterDate Collected: 12/07/15 12:55
Date Received: 12/09/15 10:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 15:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 12/13/15 15:59 1AcrylonitrileND
1.00 0.200 ug/L 12/13/15 15:59 1BenzeneND
1.00 0.150 ug/L 12/13/15 15:59 1BromochloromethaneND
1.00 0.170 ug/L 12/13/15 15:59 1BromodichloromethaneND
1.00 0.290 ug/L 12/13/15 15:59 1BromoformND
1.00 0.350 ug/L 12/13/15 15:59 1BromomethaneND
50.0 2.64 ug/L 12/13/15 15:59 12-Butanone (MEK)ND
1.00 0.220 ug/L 12/13/15 15:59 1Carbon disulfide ND
1.00 0.180 ug/L 12/13/15 15:59 1Carbon tetrachloride ND
1.00 0.180 ug/L 12/13/15 15:59 1ChlorobenzeneND
1.00 0.250 ug/L 12/13/15 15:59 1ChlorodibromomethaneND
1.00 0.360 ug/L 12/13/15 15:59 1ChloroethaneND
1.00 0.230 ug/L 12/13/15 15:59 1ChloroformND
1.00 0.360 ug/L 12/13/15 15:59 1ChloromethaneND
1.00 0.210 ug/L 12/13/15 15:59 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 15:59 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 12/13/15 15:59 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 12/13/15 15:59 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 12/13/15 15:59 1DibromomethaneND
1.00 0.190 ug/L 12/13/15 15:59 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 12/13/15 15:59 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 12/13/15 15:59 11,1-Dichloroethane ND
1.00 0.200 ug/L 12/13/15 15:59 11,2-Dichloroethane ND
1.00 0.250 ug/L 12/13/15 15:59 11,1-Dichloroethene ND
1.00 0.250 ug/L 12/13/15 15:59 11,2-Dichloropropane ND
1.00 0.190 ug/L 12/13/15 15:59 1EthylbenzeneND
10.0 1.28 ug/L 12/13/15 15:59 12-Hexanone ND
10.0 1.50 ug/L 12/13/15 15:59 1IodomethaneND
1.00 1.00 ug/L 12/13/15 15:59 1Methylene Chloride ND
10.0 0.810 ug/L 12/13/15 15:59 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 12/13/15 15:59 1StyreneND
1.00 0.150 ug/L 12/13/15 15:59 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 12/13/15 15:59 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 12/13/15 15:59 1TetrachloroetheneND
1.00 0.170 ug/L 12/13/15 15:59 1TolueneND
5.00 0.460 ug/L 12/13/15 15:59 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 12/13/15 15:59 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 12/13/15 15:59 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 12/13/15 15:59 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 12/13/15 15:59 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 12/13/15 15:59 1TrichloroetheneND
1.00 0.210 ug/L 12/13/15 15:59 1TrichlorofluoromethaneND
1.00 0.230 ug/L 12/13/15 15:59 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 12/13/15 15:59 1Vinyl acetate ND
1.00 0.180 ug/L 12/13/15 15:59 1Vinyl chloride ND
3.00 0.580 ug/L 12/13/15 15:59 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Lab Sample ID: 490-93697-14Client Sample ID: FIELD BLANK
Matrix: WaterDate Collected: 12/07/15 12:55
Date Received: 12/09/15 10:10
4-Bromofluorobenzene (Surr)84 70-130 12/13/15 15:59 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)113 12/13/15 15:59 170-130
1,2-Dichloroethane-d4 (Surr)102 12/13/15 15:59 170-130
Toluene-d8 (Surr)89 12/13/15 15:59 170-130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
C10-C28 ND 100 50.0 ug/L 12/14/15 11:08 12/16/15 01:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr)65 50-150 12/14/15 11:08 12/16/15 01:36 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
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QC Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-306017/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306017
RL MDL
Acetone ND 25.0 2.66 ug/L 12/13/15 14:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.50010.0 ug/L 12/13/15 14:35 1Acrylonitrile
ND 0.2001.00 ug/L 12/13/15 14:35 1Benzene
ND 0.1501.00 ug/L 12/13/15 14:35 1Bromochloromethane
ND 0.1701.00 ug/L 12/13/15 14:35 1Bromodichloromethane
ND 0.2901.00 ug/L 12/13/15 14:35 1Bromoform
ND 0.3501.00 ug/L 12/13/15 14:35 1Bromomethane
ND 2.6450.0 ug/L 12/13/15 14:35 12-Butanone (MEK)
0.2707 J 0.2201.00 ug/L 12/13/15 14:35 1Carbon disulfide
ND 0.1801.00 ug/L 12/13/15 14:35 1Carbon tetrachloride
ND 0.1801.00 ug/L 12/13/15 14:35 1Chlorobenzene
ND 0.2501.00 ug/L 12/13/15 14:35 1Chlorodibromomethane
ND 0.3601.00 ug/L 12/13/15 14:35 1Chloroethane
ND 0.2301.00 ug/L 12/13/15 14:35 1Chloroform
ND 0.3601.00 ug/L 12/13/15 14:35 1Chloromethane
ND 0.2101.00 ug/L 12/13/15 14:35 1cis-1,2-Dichloroethene
ND 0.1701.00 ug/L 12/13/15 14:35 1cis-1,3-Dichloropropene
ND 0.94010.0 ug/L 12/13/15 14:35 11,2-Dibromo-3-Chloropropane
ND 0.2101.00 ug/L 12/13/15 14:35 11,2-Dibromoethane (EDB)
ND 0.4501.00 ug/L 12/13/15 14:35 1Dibromomethane
ND 0.1901.00 ug/L 12/13/15 14:35 11,2-Dichlorobenzene
ND 0.1701.00 ug/L 12/13/15 14:35 11,4-Dichlorobenzene
ND 0.2401.00 ug/L 12/13/15 14:35 11,1-Dichloroethane
ND 0.2001.00 ug/L 12/13/15 14:35 11,2-Dichloroethane
ND 0.2501.00 ug/L 12/13/15 14:35 11,1-Dichloroethene
ND 0.2501.00 ug/L 12/13/15 14:35 11,2-Dichloropropane
ND 0.1901.00 ug/L 12/13/15 14:35 1Ethylbenzene
ND 1.2810.0 ug/L 12/13/15 14:35 12-Hexanone
ND 1.5010.0 ug/L 12/13/15 14:35 1Iodomethane
ND 1.001.00 ug/L 12/13/15 14:35 1Methylene Chloride
ND 0.81010.0 ug/L 12/13/15 14:35 14-Methyl-2-pentanone (MIBK)
ND 0.2801.00 ug/L 12/13/15 14:35 1Styrene
ND 0.1501.00 ug/L 12/13/15 14:35 11,1,1,2-Tetrachloroethane
ND 0.1901.00 ug/L 12/13/15 14:35 11,1,2,2-Tetrachloroethane
ND 0.1401.00 ug/L 12/13/15 14:35 1Tetrachloroethene
ND 0.1701.00 ug/L 12/13/15 14:35 1Toluene
ND 0.4605.00 ug/L 12/13/15 14:35 1trans-1,4-Dichloro-2-butene
ND 0.2301.00 ug/L 12/13/15 14:35 1trans-1,2-Dichloroethene
ND 0.1701.00 ug/L 12/13/15 14:35 1trans-1,3-Dichloropropene
ND 0.1901.00 ug/L 12/13/15 14:35 11,1,1-Trichloroethane
ND 0.1901.00 ug/L 12/13/15 14:35 11,1,2-Trichloroethane
ND 0.2001.00 ug/L 12/13/15 14:35 1Trichloroethene
ND 0.2101.00 ug/L 12/13/15 14:35 1Trichlorofluoromethane
ND 0.2301.00 ug/L 12/13/15 14:35 11,2,3-Trichloropropane
ND 1.7110.0 ug/L 12/13/15 14:35 1Vinyl acetate
ND 0.1801.00 ug/L 12/13/15 14:35 1Vinyl chloride
ND 0.5803.00 ug/L 12/13/15 14:35 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-306017/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306017
4-Bromofluorobenzene (Surr)86 70-130 12/13/15 14:35 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
112 12/13/15 14:35 1Dibromofluoromethane (Surr)70-130
98 12/13/15 14:35 11,2-Dichloroethane-d4 (Surr)70-130
89 12/13/15 14:35 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-306017/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306017
Acetone 250 237.6 ug/L 95 54-145
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 467.0 ug/L 93 61-140
Benzene 50.0 55.11 ug/L 110 80-121
Bromochloromethane 50.0 63.77 ug/L 128 78-129
Bromodichloromethane 50.0 52.35 ug/L 105 75-129
Bromoform 50.0 48.41 ug/L 97 46-145
Bromomethane 50.0 51.09 ug/L 102 41-150
2-Butanone (MEK)250 264.7 ug/L 106 62-133
Carbon disulfide 50.0 55.26 ug/L 111 77-126
Carbon tetrachloride 50.0 52.40 ug/L 105 64-147
Chlorobenzene 50.0 50.71 ug/L 101 80-120
Chlorodibromomethane 50.0 51.18 ug/L 102 69-133
Chloroethane 50.0 50.62 ug/L 101 72-120
Chloroform 50.0 59.15 ug/L 118 73-129
Chloromethane 50.0 56.73 ug/L 113 12-150
cis-1,2-Dichloroethene 50.0 59.74 ug/L 119 76-125
cis-1,3-Dichloropropene 50.0 54.20 ug/L 108 74-140
1,2-Dibromo-3-Chloropropane 50.0 41.60 ug/L 83 54-125
1,2-Dibromoethane (EDB)50.0 49.89 ug/L 100 80-129
Dibromomethane 50.0 50.78 ug/L 102 71-125
1,2-Dichlorobenzene 50.0 50.00 ug/L 100 80-121
1,4-Dichlorobenzene 50.0 49.40 ug/L 99 80-120
1,1-Dichloroethane 50.0 48.58 ug/L 97 78-125
1,2-Dichloroethane 50.0 47.19 ug/L 94 77-121
1,1-Dichloroethene 50.0 54.22 ug/L 108 79-124
1,2-Dichloropropane 50.0 56.04 ug/L 112 75-120
Ethylbenzene 50.0 51.10 ug/L 102 80-130
2-Hexanone 250 239.9 ug/L 96 60-142
Iodomethane 50.0 54.85 ug/L 110 40-150
Methylene Chloride 50.0 54.19 ug/L 108 79-123
4-Methyl-2-pentanone (MIBK)250 269.7 ug/L 108 60-137
Styrene 50.0 50.58 ug/L 101 80-127
1,1,1,2-Tetrachloroethane 50.0 50.91 ug/L 102 74-135
1,1,2,2-Tetrachloroethane 50.0 46.99 ug/L 94 69-131
Tetrachloroethene 50.0 48.39 ug/L 97 80-126
Toluene 50.0 50.41 ug/L 101 80-126
trans-1,4-Dichloro-2-butene 50.0 43.81 ug/L 88 41-147
trans-1,2-Dichloroethene 50.0 51.04 ug/L 102 79-126
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QC Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-306017/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306017
trans-1,3-Dichloropropene 50.0 52.55 ug/L 105 63-134
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 50.56 ug/L 101 78-135
1,1,2-Trichloroethane 50.0 50.23 ug/L 100 80-124
Trichloroethene 50.0 53.57 ug/L 107 80-123
Trichlorofluoromethane 50.0 49.10 ug/L 98 65-124
1,2,3-Trichloropropane 50.0 46.37 ug/L 93 70-131
Vinyl acetate 100 93.36 ug/L 93 54-139
Vinyl chloride 50.0 54.50 ug/L 109 68-120
Xylenes, Total 100 102.9 ug/L 103 80-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
88
LCS LCS
Qualifier Limits%Recovery
97Dibromofluoromethane (Surr)70 -130
871,2-Dichloroethane-d4 (Surr)70 -130
93Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-93783-B-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306017
Acetone ND 250 229.5 ug/L 92 45-141
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile ND 500 437.2 ug/L 87 50-148
Benzene ND 50.0 49.00 ug/L 98 75-133
Bromochloromethane ND 50.0 58.49 ug/L 117 67-139
Bromodichloromethane ND 50.0 51.88 ug/L 104 70-140
Bromoform ND 50.0 49.19 ug/L 98 42-147
Bromomethane ND 50.0 39.92 ug/L 80 16-163
2-Butanone (MEK)ND 250 252.6 ug/L 101 50-138
Carbon disulfide ND 50.0 35.06 ug/L 70 48-152
Carbon tetrachloride ND 50.0 49.84 ug/L 100 62-164
Chlorobenzene ND 50.0 50.08 ug/L 100 80-129
Chlorodibromomethane ND 50.0 52.32 ug/L 105 66-140
Chloroethane ND 50.0 43.53 ug/L 87 58-137
Chloroform ND 50.0 59.54 ug/L 119 66-138
Chloromethane ND 50.0 46.00 ug/L 92 10-169
cis-1,2-Dichloroethene ND 50.0 52.94 ug/L 106 68-138
cis-1,3-Dichloropropene ND 50.0 44.98 ug/L 90 71-141
1,2-Dibromo-3-Chloropropane ND 50.0 40.87 ug/L 82 52-126
1,2-Dibromoethane (EDB)ND 50.0 46.25 ug/L 92 75-137
Dibromomethane ND 50.0 46.34 ug/L 93 58-140
1,2-Dichlorobenzene ND 50.0 49.75 ug/L 100 79-128
1,4-Dichlorobenzene ND 50.0 47.63 ug/L 95 78-126
1,1-Dichloroethane 0.718 J 50.0 46.49 ug/L 92 71-139
1,2-Dichloroethane ND 50.0 44.20 ug/L 88 64-136
1,1-Dichloroethene 25.7 50.0 69.29 ug/L 87 70-142
1,2-Dichloropropane ND 50.0 53.79 ug/L 108 67-131
Ethylbenzene ND 50.0 48.46 ug/L 97 79-139
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QC Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-93783-B-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306017
2-Hexanone ND 250 220.8 ug/L 88 50-150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Iodomethane ND 50.0 44.10 ug/L 88 34-191
Methylene Chloride ND 50.0 48.34 ug/L 97 64-139
4-Methyl-2-pentanone (MIBK)ND 250 253.9 ug/L 102 50-147
Styrene ND 50.0 49.27 ug/L 99 61-148
1,1,1,2-Tetrachloroethane ND 50.0 53.11 ug/L 106 73-141
1,1,2,2-Tetrachloroethane ND 50.0 48.35 ug/L 97 56-143
Tetrachloroethene 39.8 50.0 81.21 ug/L 83 72-145
Toluene ND 50.0 46.08 ug/L 92 75-136
trans-1,4-Dichloro-2-butene ND 50.0 33.23 ug/L 66 29-156
trans-1,2-Dichloroethene ND 50.0 40.35 ug/L 81 66-143
trans-1,3-Dichloropropene ND 50.0 45.73 ug/L 91 59-135
1,1,1-Trichloroethane 0.608 J 50.0 49.81 ug/L 98 76-149
1,1,2-Trichloroethane ND 50.0 51.07 ug/L 102 74-134
Trichloroethene 0.342 J 50.0 47.09 ug/L 93 73-144
Trichlorofluoromethane ND 50.0 46.21 ug/L 92 58-139
1,2,3-Trichloropropane ND 50.0 44.93 ug/L 90 53-144
Vinyl acetate ND 100 76.29 ug/L 76 37-154
Vinyl chloride ND 50.0 45.23 ug/L 90 56-129
Xylenes, Total ND 100 98.01 ug/L 98 74-141
4-Bromofluorobenzene (Surr)70 -130
Surrogate
86
MS MS
Qualifier Limits%Recovery
98Dibromofluoromethane (Surr)70 -130
841,2-Dichloroethane-d4 (Surr)70 -130
94Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-93783-C-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306017
Acetone ND 250 227.4 ug/L 91 45-141 1 21
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile ND 500 437.9 ug/L 88 50-148 0 18
Benzene ND 50.0 47.17 ug/L 94 75-133 4 17
Bromochloromethane ND 50.0 55.99 ug/L 112 67-139 4 17
Bromodichloromethane ND 50.0 49.42 ug/L 99 70-140 5 18
Bromoform ND 50.0 46.64 ug/L 93 42-147 5 16
Bromomethane ND 50.0 40.24 ug/L 80 16-163 1 50
2-Butanone (MEK)ND 250 250.9 ug/L 100 50-138 1 19
Carbon disulfide ND 50.0 34.10 ug/L 68 48-152 3 21
Carbon tetrachloride ND 50.0 47.69 ug/L 95 62-164 4 19
Chlorobenzene ND 50.0 47.58 ug/L 95 80-129 5 14
Chlorodibromomethane ND 50.0 49.69 ug/L 99 66-140 5 15
Chloroethane ND 50.0 42.64 ug/L 85 58-137 2 20
Chloroform ND 50.0 56.63 ug/L 113 66-138 5 18
Chloromethane ND 50.0 46.01 ug/L 92 10-169 0 31
cis-1,2-Dichloroethene ND 50.0 51.23 ug/L 102 68-138 3 17
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QC Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-93783-C-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306017
cis-1,3-Dichloropropene ND 50.0 43.56 ug/L 87 71-141 3 15
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2-Dibromo-3-Chloropropane ND 50.0 39.85 ug/L 80 52-126 3 24
1,2-Dibromoethane (EDB)ND 50.0 43.85 ug/L 88 75-137 5 15
Dibromomethane ND 50.0 44.48 ug/L 89 58-140 4 16
1,2-Dichlorobenzene ND 50.0 48.41 ug/L 97 79-128 3 15
1,4-Dichlorobenzene ND 50.0 46.56 ug/L 93 78-126 2 15
1,1-Dichloroethane 0.718 J 50.0 44.67 ug/L 88 71-139 4 17
1,2-Dichloroethane ND 50.0 42.35 ug/L 85 64-136 4 17
1,1-Dichloroethene 25.7 50.0 67.65 ug/L 84 70-142 2 17
1,2-Dichloropropane ND 50.0 52.00 ug/L 104 67-131 3 17
Ethylbenzene ND 50.0 46.28 ug/L 93 79-139 5 15
2-Hexanone ND 250 213.3 ug/L 85 50-150 3 15
Iodomethane ND 50.0 43.25 ug/L 86 34-191 2 23
Methylene Chloride ND 50.0 47.03 ug/L 94 64-139 3 17
4-Methyl-2-pentanone (MIBK)ND 250 243.1 ug/L 97 50-147 4 17
Styrene ND 50.0 47.45 ug/L 95 61-148 4 24
1,1,1,2-Tetrachloroethane ND 50.0 49.99 ug/L 100 73-141 6 16
1,1,2,2-Tetrachloroethane ND 50.0 46.40 ug/L 93 56-143 4 20
Tetrachloroethene 39.8 50.0 78.10 ug/L 77 72-145 4 16
Toluene ND 50.0 43.94 ug/L 88 75-136 5 15
trans-1,4-Dichloro-2-butene ND 50.0 33.79 ug/L 68 29-156 2 26
trans-1,2-Dichloroethene ND 50.0 40.13 ug/L 80 66-143 1 16
trans-1,3-Dichloropropene ND 50.0 43.81 ug/L 88 59-135 4 14
1,1,1-Trichloroethane 0.608 J 50.0 47.84 ug/L 94 76-149 4 17
1,1,2-Trichloroethane ND 50.0 48.46 ug/L 97 74-134 5 15
Trichloroethene 0.342 J 50.0 45.67 ug/L 91 73-144 3 17
Trichlorofluoromethane ND 50.0 44.61 ug/L 89 58-139 4 18
1,2,3-Trichloropropane ND 50.0 44.69 ug/L 89 53-144 1 19
Vinyl acetate ND 100 74.20 ug/L 74 37-154 3 21
Vinyl chloride ND 50.0 44.94 ug/L 90 56-129 1 17
Xylenes, Total ND 100 94.39 ug/L 94 74-141 4 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
86
MSD MSD
Qualifier Limits%Recovery
97Dibromofluoromethane (Surr)70 -130
851,2-Dichloroethane-d4 (Surr)70 -130
93Toluene-d8 (Surr)70 -130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
Client Sample ID: Method BlankLab Sample ID: MB 490-306146/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306597 Prep Batch: 306146
RL MDL
C10-C28 ND 100 50.0 ug/L 12/14/15 11:08 12/15/15 21:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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QC Sample Results
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
(Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-306146/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306597 Prep Batch: 306146
o-Terphenyl (Surr)67 50-150 12/15/15 21:32 1
MB MB
Surrogate
12/14/15 11:08
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-306146/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306597 Prep Batch: 306146
C10-C28 1000 580.5 ug/L 58 46-132
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl (Surr)50 -150
Surrogate
72
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: MW-8ALab Sample ID: 490-93697-7 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306597 Prep Batch: 306146
C10-C28 63.1 J 1000 627.1 ug/L 56 10-138
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
o-Terphenyl (Surr)50 -150
Surrogate
74
MS MS
Qualifier Limits%Recovery
Client Sample ID: MW-8ALab Sample ID: 490-93697-7 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 306597 Prep Batch: 306146
C10-C28 63.1 J 1000 699.0 ug/L 64 10-138 11 31
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
o-Terphenyl (Surr)50 -150
Surrogate
76
MSD MSD
Qualifier Limits%Recovery
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QC Association Summary
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
GC/MS VOA
Analysis Batch: 306017
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-93697-1 TRIP BLANK Total/NA
Water 8260B490-93697-2 MW-5A Total/NA
Water 8260B490-93697-3 MW-6 Total/NA
Water 8260B490-93697-4 MW-6A Total/NA
Water 8260B490-93697-5 MW-7A Total/NA
Water 8260B490-93697-6 MW-8 Total/NA
Water 8260B490-93697-7 MW-8A Total/NA
Water 8260B490-93697-8 MW-9 Total/NA
Water 8260B490-93697-9 MW-9A Total/NA
Water 8260B490-93697-10 MW-10A Total/NA
Water 8260B490-93697-11 SW-1 Total/NA
Water 8260B490-93697-12 SW-2 Total/NA
Water 8260B490-93697-13 LEACHATE POND Total/NA
Water 8260B490-93697-14 FIELD BLANK Total/NA
Water 8260B490-93783-B-2 MS Matrix Spike Total/NA
Water 8260B490-93783-C-2 MSD Matrix Spike Duplicate Total/NA
Water 8260BLCS 490-306017/4 Lab Control Sample Total/NA
Water 8260BMB 490-306017/7 Method Blank Total/NA
GC Semi VOA
Prep Batch: 306146
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C490-93697-2 MW-5A Total/NA
Water 3510C490-93697-3 MW-6 Total/NA
Water 3510C490-93697-4 MW-6A Total/NA
Water 3510C490-93697-5 MW-7A Total/NA
Water 3510C490-93697-6 MW-8 Total/NA
Water 3510C490-93697-7 MW-8A Total/NA
Water 3510C490-93697-7 MS MW-8A Total/NA
Water 3510C490-93697-7 MSD MW-8A Total/NA
Water 3510C490-93697-8 MW-9 Total/NA
Water 3510C490-93697-9 MW-9A Total/NA
Water 3510C490-93697-10 MW-10A Total/NA
Water 3510C490-93697-11 SW-1 Total/NA
Water 3510C490-93697-12 SW-2 Total/NA
Water 3510C490-93697-13 LEACHATE POND Total/NA
Water 3510C490-93697-14 FIELD BLANK Total/NA
Water 3510CLCS 490-306146/2-A Lab Control Sample Total/NA
Water 3510CMB 490-306146/1-A Method Blank Total/NA
Analysis Batch: 306597
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8015C 306146490-93697-2 MW-5A Total/NA
Water 8015C 306146490-93697-3 MW-6 Total/NA
Water 8015C 306146490-93697-4 MW-6A Total/NA
Water 8015C 306146490-93697-5 MW-7A Total/NA
Water 8015C 306146490-93697-6 MW-8 Total/NA
Water 8015C 306146490-93697-7 MW-8A Total/NA
Water 8015C 306146490-93697-7 MS MW-8A Total/NA
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QC Association Summary
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
GC Semi VOA (Continued)
Analysis Batch: 306597 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8015C 306146490-93697-7 MSD MW-8A Total/NA
Water 8015C 306146490-93697-8 MW-9 Total/NA
Water 8015C 306146490-93697-9 MW-9A Total/NA
Water 8015C 306146490-93697-10 MW-10A Total/NA
Water 8015C 306146490-93697-11 SW-1 Total/NA
Water 8015C 306146490-93697-12 SW-2 Total/NA
Water 8015C 306146490-93697-13 LEACHATE POND Total/NA
Water 8015C 306146490-93697-14 FIELD BLANK Total/NA
Water 8015C 306146LCS 490-306146/2-A Lab Control Sample Total/NA
Water 8015C 306146MB 490-306146/1-A Method Blank Total/NA
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Lab Chronicle
Client: Duke Energy Corporation TestAmerica Job ID: 490-93697-1
Project/Site: MNS Landfill #2 J15120015
Client Sample ID: TRIP BLANK Lab Sample ID: 490-93697-1
Matrix: WaterDate Collected: 12/07/15 06:15
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 15:31 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-5A Lab Sample ID: 490-93697-2
Matrix: WaterDate Collected: 12/07/15 10:35
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 17:50 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/15/15 22:03 TRF TAL NSHTotal/NA
Client Sample ID: MW-6 Lab Sample ID: 490-93697-3
Matrix: WaterDate Collected: 12/07/15 08:20
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 18:18 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/15/15 22:18 TRF TAL NSHTotal/NA
Client Sample ID: MW-6A Lab Sample ID: 490-93697-4
Matrix: WaterDate Collected: 12/07/15 08:30
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 18:46 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/15/15 22:33 TRF TAL NSHTotal/NA
Client Sample ID: MW-7A Lab Sample ID: 490-93697-5
Matrix: WaterDate Collected: 12/07/15 10:05
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 19:13 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/15/15 22:49 TRF TAL NSHTotal/NA
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Lab Chronicle
Client: Duke Energy Corporation TestAmerica Job ID: 490-93697-1
Project/Site: MNS Landfill #2 J15120015
Client Sample ID: MW-8 Lab Sample ID: 490-93697-6
Matrix: WaterDate Collected: 12/07/15 07:45
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 19:41 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/15/15 23:04 TRF TAL NSHTotal/NA
Client Sample ID: MW-8A Lab Sample ID: 490-93697-7
Matrix: WaterDate Collected: 12/07/15 08:45
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 20:09 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/15/15 23:19 TRF TAL NSHTotal/NA
Client Sample ID: MW-9 Lab Sample ID: 490-93697-8
Matrix: WaterDate Collected: 12/07/15 11:30
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 20:37 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/16/15 00:05 TRF TAL NSHTotal/NA
Client Sample ID: MW-9A Lab Sample ID: 490-93697-9
Matrix: WaterDate Collected: 12/07/15 11:20
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 21:05 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/16/15 00:20 TRF TAL NSHTotal/NA
Client Sample ID: MW-10A Lab Sample ID: 490-93697-10
Matrix: WaterDate Collected: 12/07/15 12:05
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 21:33 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/16/15 00:36 TRF TAL NSHTotal/NA
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Lab Chronicle
Client: Duke Energy Corporation TestAmerica Job ID: 490-93697-1
Project/Site: MNS Landfill #2 J15120015
Client Sample ID: SW-1 Lab Sample ID: 490-93697-11
Matrix: WaterDate Collected: 12/07/15 11:30
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 22:01 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/16/15 00:51 TRF TAL NSHTotal/NA
Client Sample ID: SW-2 Lab Sample ID: 490-93697-12
Matrix: WaterDate Collected: 12/07/15 12:45
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 22:29 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/16/15 01:06 TRF TAL NSHTotal/NA
Client Sample ID: LEACHATE POND Lab Sample ID: 490-93697-13
Matrix: WaterDate Collected: 12/07/15 12:15
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 22:57 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/16/15 01:21 TRF TAL NSHTotal/NA
Client Sample ID: FIELD BLANK Lab Sample ID: 490-93697-14
Matrix: WaterDate Collected: 12/07/15 12:55
Date Received: 12/09/15 10:10
Analysis 8260B 12/13/15 15:59 WC11 306017 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 306146 12/14/15 11:08 MRM TAL NSHTotal/NA
Analysis 8015C 1 306597 12/16/15 01:36 TRF TAL NSHTotal/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-93697-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #2 J15120015
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8468015CNonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Duke Energy Corporation TestAmerica Job ID: 490-93697-1
Project/Site: MNS Landfill #2 J15120015
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-15 *
TestAmerica Nashville
* Certification renewal pending - certification considered valid.
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Login Sample Receipt Checklist
Client: Duke Energy Corporation Job Number: 490-93697-1
Login Number: 93697
Question Answer Comment
Creator: McBride, Mike
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a
survey meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.2.0
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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Page 77 of 78
Page 78 of 78
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J15120016
Project Name:MCGUIRE -
Lab Contact:Peggy Kendall
Date:12/22/2015
Customer Address:13225 Hagers Ferry Rd
Customer Name(s):TIM HUNSUCKER, CHUCK CAMPBELL
Mail Code: MG01CH
Huntersville, NC 28078-8985
Phone:
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Peggy Kendall) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Peggy Kendall
Page 1 of 8
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2015037438 MCGUIRE 07-Dec-15 11:30 AM PSP SW-1
2015037439 MCGUIRE 07-Dec-15 1:00 PM LDC SW-2
2 Total Samples
Page 2 of 8
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:Peggy Kendall Date:12/22/2015
Electronic Data Deliverable (EDD) Sent Separatel
Page 3 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120016
2015037438
Collection Date:07-Dec-15 11:30 AM
Site:SW-1
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP
Barium (Ba)0.031 mg/L EPA 200.7 12/14/2015 12:48 FCJORDA0.005 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 12:48 FCJORDA0.005 1
Silver (Ag)< 0.005 mg/L EPA 200.7 12/14/2015 12:48 FCJORDA0.005 1
DISSOLVED METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 04:54 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 04:54 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 04:54 MHALL311
Page 4 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120016
2015037439
Collection Date:07-Dec-15 1:00 PM
Site:SW-2
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP
Barium (Ba)0.023 mg/L EPA 200.7 12/14/2015 13:00 FCJORDA0.005 1
Chromium (Cr)< 0.005 mg/L EPA 200.7 12/14/2015 13:00 FCJORDA0.005 1
Silver (Ag)0.013 mg/L EPA 200.7 12/14/2015 13:00 FCJORDA0.005 1
DISSOLVED METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 12/15/2015 05:15 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 12/15/2015 05:15 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 12/15/2015 05:15 MHALL311
Page 5 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120016
Q15120300 ICP Dissolved DISSOLVED METALS BY ICP
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Barium (Ba) 0.000052 mg/L -10.000052 0.005 < 1/2 RDL
Chromium (Cr) -0.000474 mg/L -1-0.000474 0.005 < 1/2 RDL
Silver (Ag) 0.000004 mg/L -10.000004 0.005 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Barium (Ba) 1 1 100mg/L -1158511
Chromium (Cr) 1.01 1 101mg/L -1158511.01
Silver (Ag) 0.884 1 88.4mg/L -1158510.884
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J15120016 -- 2015037438
Barium (Ba) 5.35 5 106mg/L -1307015.35
Chromium (Cr) 5.08 5 102mg/L -1307015.08
Silver (Ag) 0.474 0.5 94.8mg/L -1307010.474
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J15120016 -- 2015037438
Barium (Ba) 5.37 5 107 0.375mg/L -1307015.37
Chromium (Cr) 5.11 5 102 0.51mg/L -1307015.11
Silver (Ag) 0.471 0.5 94.2 0.55mg/L -1307010.471
Page 6 of 8
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15120016
Q15120313 IMS Dissolved DISSOLVED METALS BY ICP-MS
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Arsenic (As) 0.0101 ug/L -10.0101 1 < 1/2 RDL
Cadmium (Cd) 0.0073 ug/L -10.0073 1 < 1/2 RDL
Lead (Pb) -0.0124 ug/L -1-0.0124 1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Arsenic (As) 81 80 101ug/L -11585181
Cadmium (Cd) 7.96 8 99.4ug/L -1158517.96
Lead (Pb) 80.7 80 101ug/L -11585180.7
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J15120016 -- 2015037438
Arsenic (As) 51.5 50 103ug/L -13070151.5
Cadmium (Cd) 50.1 50 100ug/L -13070150.1
Lead (Pb) 50.7 50 101ug/L -13070150.7
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J15120016 -- 2015037438
Arsenic (As) 51 50 102 0.94ug/L -13070151
Cadmium (Cd) 49.7 50 99.3 0.743ug/L -13070149.7
Lead (Pb) 49.9 50 99.7 1.47ug/L -13070149.9
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