Paziuk GW Monitoring Report - Feb 2013

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February 18, 2013
NC Department of Environment and Natural Resources
Division of Waste Management
Inactive Hazardous Sites Branch
Attn.: Sue Robbins
127 Cardinal Drive Extension
Wilmington, North Carolina 28405
Environmental~
Geothermal & Well Drilling
f 1 Re.: Bradford Pools and Spas (Formerly Paziuk Warehouse) I J 71 0 Sunnydale Drive
Wilmington, North Carolina
f 1 Groundwater Incident No. 87038
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Dear Ms. Robbins,
The following information is provided for review:
Table 1
Table 2
Figure 1
Figure 2
Figure 3
Figure 4
Figure 5
Figure 6
Figure 7
Figure 8
Groundwater Table Elevations Summary
Historical Groundwater Sample Results Summary
Site Vicinity Map
Site Map With Monitoring And Abandoned Water Supply Well Locations
Groundwater Contours For Aquifer Zone #2 As Of 12/18/13
Cis-1,2-Dichloroethene Concentrations In Aquifer Zone #2 As Of 12/18/12
Trichloroethene Concentrations In Aquifer Zone #2 As Of 12/18/12
Tetrachloroethene Concentrations In Aquifer Zone #2 As Of 12/18/12
Vinyl Chloride Concentrations In Aquifer Zone #2 As Of 12/18/12
Proposed Monitoring Well and Air/ Soil Gas Sampling Locations
Appendix A Laboratory Results With Chain of Custody Records
Groundwater Sampling Activities
Figure 1 is a Site Vicinity Map showing the project location. The investigation included
limited groundwater sampling activities as recommended by S&ME in their Groundwater
Assessment Report dated May 11,2012. Monitoring wells (AMW-4D, AMW-6D,AMW-7D,
AMW-8D, AMW-9D, and AMW-13D) were gauged for water elevation, purged, and a
groundwater sample collected from each well and submitted for laboratory analysis per
Applied Resource Management, PC
P. 0. Box 882, 2!57 Transfer Station Road, Hampstead, NC 28443 910.270.2919 Fax [phone]
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February 18, 2013
EPA Methods 8260B and 82700. Well locations are depicted on Figure 2. Purge water
was contained in 55 gallon drums and stored on-site for future disposal. Water level
depths for Aquifer Zone #2 were found to range from 7.01 to 12.28 feet deep. A
Groundwater Table Elevation Summary is provided in Table 1. After the initial round of
sampling, it was found that the monitoring well tags in AMW-8S and AMW-80 had been
switched. As such, AMW-8S was sampled during the 12/18/12 event. After the switch was
discovered, we remobilized, gauged, purged, and sampled AMW-80 on 1/23/13. Based
on the calculated elevations, groundwater flow direction for Aquifer Zone#2 is to the south
and southwest, consistent with historical flow patterns. Groundwater Contours For Aquifer
Zone #2 As Of 12/18/12 are depicted on Figure 3.
Groundwater Sampling Results
Based on laboratory results, AMW-60 was found to be compliant for all compounds tested.
This well has remained compliant for three consecutive events. The other five monitoring
wells tested (AMW-40, AMW-70, AMW-80, AMW-90, and AMW-130) were found to
contain non-compliant compounds as compared to the NCAC T:15A 02L Groundwater
Quality Standards. Monitoring wells AMW-40, AMW-70, and AMW-80 revealed several
decreases in contaminant concentrations with the exception of cis-1 ,2-0ichloroethene
which increased at all three locations. AMW-40 increased from 2, 790 to 5,080 ppb, AMW-
70 increased from 994 to 4,250 ppb, and AMW-80 increased from 831 to 1,090 ppb.
AMW-90 revealed relatively no significant changes; however, vinyl chloride concentrations
continue to trend downward. AMW-130 revealed a significant increase in vinyl chloride
from below quantitation limits to 2,810 ppb. Also, significant decreases were found for
trichloroethene and cis 1 ,2-0ichloroethene concentrations with trichloroethene decreasing
from 134,000 ppb to a compliant 2.16 ppb estimated, and cis 1 ,2-0ichloroethene
decreasing from 71,400 ppb to 7,230 ppb. A Historical Groundwater Sample Results
Summary is provided in Table 2. Contaminant concentration maps were prepared for the
non-compliant monitoring wells within Aquifer Zone #2 and are depict on Figures 4 through
7. As shown on Figures 4 and 7, the cis-1 ,2-0ichloroethene and vinyl chloride plumes
remain undelineated to the south-southeast. Also, an encroaching plume from an off-site
source is present to the east. The trichloroethene and tetrachloroethene plumes shown
on Figures 5 and 6 are believed to be delineated within the property limits; however, this
sampling event did not collect enough downgradient data for confirmation. It should be
noted that the Roadway Express property to the immediate west was recently aquired by
Seven Ten, L.L.C.
Conclusions and Recommendations
Groundwater sampling activities were recently conducted at the site by ARM. Monitoring
wells (AMW-40, AMW-60, AMW-70, AMW-80, AMW-90, and AMW-130) were sampled
as recommended by S&ME in their Groundwater Assessment Report dated May 11, 2012.
Based on laboratory results, AMW -60 was found to be compliant for all compounds tested.
2
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February 18, 2013
The other five monitoring wells tested (AMW-40, AMW-70, AMW-80, AMW-90, and
AMW-130) were found to contain non-compliant compounds as compared to the NCAC
T:15A 02L Groundwater Quality Standards. The groundwater contaminant plumes at the
site are essentially delineated with the exception of the south -southwest portion of the
site. The following recommendations are made:
1.
2.
3.
Construct one Type I well adjacent to the former Roadway Express southeastern
property line in an attempt to delineate the groundwater plumes to the south-
southwest. The well should be constructed in the far south-southeastern portion
of the property. Also, the well should be installed on the top of the confining clay
unit which has been present between approximately 34 and 4 7 feet below ground
surface. The proposed well location is depicted on Figure 8.
Collect groundwater samples from the newly proposed well and AMW-120.
Analyze the samples per EPA Methods 82608 and 82700.
Conduct vapor intrusion monitoring to test the indoor air quality and soil gas
concentrations beneath the building's slab structure. One air sample should be
collected from inside the building structure and analyzed per EPA Method TO 15.
Also, two soil gas samples should be collected from beneath the building's slab in
areas where the highest contaminant concentrations are likely to exist. See Figure
8 for proposed air/soil gas sample locations.
r • If you have any questions or require additional information, please do not hesitate to call.
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Sincerely, ~-
' &z.A/( Josep~un~~h
l ' Project Manager/ Environmental Geologist
encs.
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cc: Mr. Mark Miller, Bradford Pools and Spas, w/encs.
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WELL I.D.
MW-1*
MW-2*
MW-3*
AMW-1*
AMW-2*
AMW-3*
TABLE 1 (page 1 of 4)
GROUNDWATER TABLE ELEVATIONS SUMMARY
BRADFORD POOLS AND SPAS
SUNNYVALE DRIVE
WILMINGTON, NORTH CAROLINA
DATE TOP OF DEPTH
GAUGED CASING ELEVATION TO WATER
(Feet) (Feet)
12/18/03 99.89 0.65
3/9/04 99.89 1.17
11/30/04 99.89 1.32
07/05/07 99.89 2.92
12/18/03 99.81 0.64
3/9/04 99.81 1.15
11/30/04 99.81 1.32
07/05/07 99.81 2.85
12/18/03 99.64 1.81
3/9/04 99.64 2.11
11/30/04 99.64 2.02
07/05/07 99.64 3.00
12/18/03 99.91 0.84
3/9/04 99.91 1.25
11/30/04 99.91 Inaccessible
07/05/07 99.91 2.97
12/18/03 100.00 0.03
3/9/04 100.00 0.52
11/30/04 100.00 0.69
07/05/07 100.00 2.80
12/18/03 100.84 1.14
3/9/04 100.84 1.58
11/30/04 100.84 1.68
07/05/07 100.84 2.85
WATER TABLE
ELEVATION
(Feet)
99.24
98.72
97.99
96.97
99.17
98.66
98.49
96.96
97.83
97.53
97.62
96.64
99.07
98.66
-
96.94
99.97
99.48
99.31
97.20
99.70
99.26
99.16
**97.99
TABLE 1 (page 2 of 4)
GROUNDWATER TABLE ELEVATIONS SUMMARY
BRADFORD POOLS AND SPAS
SUNNYVALE DRIVE
WILMINGTON, NORTH CAROLINA
WELL I.D. DATE TOP OF CASING DEPTH TO WATER TABLE
GAUGED ELEVATION WATER ELEVATION
(FEET) (FEET) (FEET)
AMW-4* 12/18/03 98.45 1.60 96.85
3/9/04 98.45 1.81 96.64
11/30/04 98.45 1.90 96.55
07105107 98.45 2.65 95.80
AMW-4D 3/9/04 98.35 15.20 83.15
11/30/04 98.35 14.92 83.43
07/05/07 98.35 18.39 79.96
12/18/12 98.35 12.28 86.07
AMW-5* 12/18/03 97.66 3.00 94.66
3/9/04 97.66 3.23 94.43
11/30/04 97.66 3.47 94.19
07/05/07 97.66 4.33 93.33
AMW-6D 3/9/04 104.05 11.73 92.32
11/30/04 104.05 11.81 92.24
07/05/07 104.05 14.43 89.62
12/18/12 104.05 11.78 92.27
AMW-7D 3/9/04 98.38 14.72 83.66
11/30/04 98.38 14.46 83.92
07/05/07 98.38 17.90 80.48
12/18/12 98.38 12.01 86.37
AMW-SS 3/9/04 98.46 4.36 94.10
11/30/04 98.46 3.90 94.56
07105107 98.46 5.35 93.11
12/18/12 98.46 4.14 94.32
AMW-SD 3/9/04 98.61 14.85 83.76
11/30/04 98.61 14.25 84.36
07/05/07 98.61 17.78 80.83
1/23/13 98.61 11.70 86.91
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WELL I.D.
AMW-9S*
AMW-9D
AMW-108*
AMW-10D*
AMW-118*
AMW-11D*
AMW-128*
AMW-12D*
AMW-13D
AMW-148*
TABLE 1 (page 3 of 4)
GROUNDWATER TABLE ELEVATIONS SUMMARY
BRADFORD POOLS AND SPAS
SUNNYVALE DRIVE
WILMINGTON, NORTH CAROLINA
DATE TOP OF CASING DEPTH TO
GAUGED ELEVATION WATER
(FEET) (FEET)
3/9/04 92.97 2.61
11/30/04 92.97 2.98
07/05/07 92.97 4.08
3/9/04 93.06 7.90
11/30/04 93.06 7.84
07/05/07 93.06 10.72
12/18/12 93.06 7.01
11/30/04 99.76 5.55
07/05/07 99.76 6.40
11/30/04 99.88 13.90
07/05/07 99.88 17.15
11/30/04 102.66 4.74
07/05/07 102.66 5.64
11/30/04 102.84 13.88
07/05/07 102.84 16.10
11/30/04 97.64 2.25
07/05/07 97.64 3.26
11/30/04 97.50 17.96
07/05/07 97.50 21.11
11/30/04 91.88 7.38
07/05/07 91.88 10.35
12/18/12 91.88 6.65
11/30/04 97.50 4.60
07/05/07 97.50 7.01
WATER TABLE
ELEVATION
(FEET)
90.36
89.99
88.89
85.16
85.22
82.34
86.05
94.21
93.36
85.98
82.73
97.92
97.02
88.96
86.74
95.39
94.38
79.54
76.39
84.50
81.53
85.23
92.90
90.49
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TABLE 1 (page 4 of 4)
GROUNDWATER TABLE ELEVATIONS SUMMARY
BRADFORD POOLS AND SPAS
SUNNYVALE DRIVE
WILMINGTON, NORTH CAROLINA
WELL I.D. DATE TOP OF CASING DEPTH TO WATER TABLE
GAUGED ELEVATION WATER ELEVATION
(FEET) (FEET) (FEET)
AMW-14D* 11/30/04 97.53 10.70 86.83
07/05/07 97.53 13.53 84.00
T-1* 3/9/04 98.48 14.79 83.69
11/30/04 98.48 14.31 84.17
07/05/07 98.48 17.06 81.42
T-2* 11/30/04 99.23 16.18 83.05
07/05/07 Destroyed Destroyed Destroyed
*=Not sampled during the 12/18/12 event.
It should be noted that AMW-88 was sampled during this event due to an accidental error in well
tag placement.
AMW-80 was measured and sampled on 1/23/13.
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TABLE 2
1 of4
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
FORMER PAZIUK WAREHOUSE
SUNNYVALE DRIVE
WILMINGTON, NORTH CAROLINA
ANALYTE NCAC 02L MW-1* MW-2* MW-3* AMW-1*
STANDARD
DATE SAMPLED 12/18/03 5/4/05 7/05/07 12/18/03 5/4/05 7/05/07 12/18/03 5/4/05 7/05/07 12/18/03 5/4/05
EPA METHOD 6210D (Concentrations in ppb)
CHLORODIBROMOMETHANE 0.41 BDL BQL BQL BDL BQL BQL BDL BQL BQL BQL BQL
TOLUENE 600 BDL BQL BQL 6.7 BQL BQL BDL BQL BQL BQL BQL
XYLENES 500 BDL BQL BQL 8.0 BQL BQL BDL BQL BQL BQL BQL
ETHYLBENZENE 600 BDL BQL BQL 1.8 BQL BQL BDL BQL BQL BQL BQL
4-ISOPROPYL TOLUENE NE BDL BQL BQL BDL BQL BQL BDL BQL BQL BQL BQL
NAPHTHALENE 6 BDL BQL BQL BDL BQL BQL BDL BQL BQL BQL BQL
n-PROPYLBENZENE 70 BDL BQL BQL BDL BQL BQL BDL BQL BQL BQL BQL
TETRACHLOROETHENE 0.7 !\(Ao . 0.56 ,.,;,·.~.~:4··~·~· :265:o·'> ,'1.78;1•·• ·•·· 608 ,, :·;·~·r'···· : BQL BQL ., .}i4~9-~:.·.!, BQL \>~ (~:,. . . ,.·:--\·'····;
1 ,4-DICHLOROBENZENE 6 BDL BQL BQL 2.3 BQL BQL BDL BQL BQL BQL BQL
n-BUTYLBENZENE 70 BDL BQL BQL BDL BQL BQL BDL BQL BQL BQL BQL
SEC-BUTYLBENZENE 70 BDL BQL BQL 2.4 BQL BQL BDL BQL BQL BQL BQL
1 ,2,4-TRIMETHYLBENZENE 400 BDL BQL BQL 2.2 BQL BQL BDL BQL BQL BQL BQL
ISOPROPYL BENZENE 70 BDL BQL BQL 1.4 BQL BQL BDL BQL BQL BQL BQL
ACETONE 6,000 BDL BQL BQL BDL BQL BQL BDL BQL 196 BDL BQL
TRANS-1 ,2-DICHLOROETHENE 70 BDL BQL 9.28 11.8 BQL BQL 21.1 BQL BQL '·\ .. #;Mg.o.o··· ..... BQL
1, 1-DICHLOROETHENE 7 BDL BQL BQL 1)<:'., 19A · .< BQL BQL 3.1 BQL BQL BQL BQL
1,1-DICHLOROETHANE 6 BDL BQL BQL 2.5 BQL BQL 10.7 BQL BQL BQL BQL
CHLOROETHANE 3,000 BDL BQL BQL BDL BQL BQL 7.7 BQL BQL BQL BQL
VINYL CHLORIDE 0.03 BDL BQL BQL ·:~ .. ~~QA> .\ 403· ·.·~ ' . ' ~, ~, 1 •. 1?9·. ' 10$~@··· ..•• <3~3.0,: , I ))J~Jr·: ;,;. y§,3oo· •. ?·)'' •...• 60QJ.i ' :
CARBON DISULFIDE 700 BDL BQL BQL BDL BQL BQL BDL BQL BQL BQL BQL
BROMODICHLOROMETHANE 0.6 BDL BQL BQL BDL BQL BQL BDL BQL BQL BQL BQL
,·.',, TRICHLOROETHENE 3 1.9 1.49 ··<~~3.J' > :4PM ···: . 0:16.7;, • '· 318 • '!>·~· /. BQL BQL '• ?9Mo.6••·. 5,280.0
CHLOROFORM 70 BDL BQL BQL
CIS-1 ,2-DICHLOROETHENE 70 1.6 1.69 '' ~2.(?;.
1 ,2-DICHLOROBENZENE 20 BDL BQL
ALL OTHER COMPOUNDS Varies BDL BQL
ALL COMPOUNDS Varies NA NA
Shaded areas represent concentrations exceedmg the NC Groundwater Standards.
BQL = Below Quantitation Limits
BDL = Below Detection Limits
ppb = parts per billion
NE = not established
• =Not sampled during this event 12/18/12
Newly amended 2L groundwater standards applied to most recent event only.
NA = Not Analyzed
BQL
BQL
NA
BDL
· .. ··: ..•. 3.13,5,0' '
3.2
BDL'
NA
BQL BQL BDL BQL BQL BQL BQL
.2.22', '},!)~0 ,' ''' ', ...... .•.. 2,525:0 ' '·,.·· 2,§?0,0 < i ·,· •)6$<h·, 6?,5Qp:o 27;300.Q
5.60 BQL BDL BQL BQL BQL BQL
BQL BQL BDL BQL BQL BQL BQL
EPA METHOD 8270D (Concentrations in ppb)
NA NA NA NA NA NA NA
AMW-2* AMW-3*
7/05/07 12/18/03 5/4/0,5 7/05/07 12/18/03 5/4/05 7/05/07
BQL BDL BQL BQL ,. ' ..... ·~A/<: BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQii. BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL 0.78 BQL BDL BQL BQL
BQL BDL 0.51 BQL BDL BQL BQL
BQL BDL 0.51 BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL 0.60 BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL 8.29 BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
.. , ·• 9,~o<.•··· BDL BQL. BQL ' .. ;12A .. :· .. .··•···•··· .. 51,f
; ...•• '.{149)'
BQL 8.5 BQl BQL BDL BQL BQL
BQL BDL BQL. BQL
·····'
~·.s. BQL BQL
< .. ~.asp.:· BDL BQL BQL 1.9 BQL BQL
BQL BDL BQL BQL 1.: 2.5 BQL BQL
.•. ' 34,500 .· ..•• BDL BQL BQL 24.1 ·;·.·· >' J 7,6.0 .);450.;•
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
NA NA NA NA NA NA NA
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ANALYTE NCAC 02L AMW-4*
STANDARD
DATE SAMPLED 12/18/03 5/4/05 7/05/07 3/8/04
CHLORODIBROMOM ETHANE 0.41 BDL BQL BQL BDL
TOLUENE 600 BDL BQL BQL BDL
XYLENES 500 BDL BQL BQL BDL
ETHYLBENZENE 600 BDL BQL BQL BDL
4-ISOPROPYL TOLUENE NE BDL BQL BQL BDL
NAPHTHALENE 6 BDL BQL BQL BDL
n-PROPYLBENZENE 70 BDL BQL BQL BDL
TETRACHLOROETHENE 0.7 245.0 BQL BQL -7.8 ..
1 ,4-DICHLOROBENZENE 6 BDL BQL BQL BDL
SEC-BUTYLBENZENE 70 BDL BQL BQL BDL
1 ,2,4· TRIMETHYLBENZENE 400 BDL BQL BQL BDL
1 ,3,5· TRIM ETHYLBENZENE 400 BDL BQL BQL 2.1
ISOPROPYL BENZENE 70 BDL BQL BQL BDL
ACETONE 6,000 BDL 5.92 8.86 BDL
TRANS-1 ,2-DICHLOROETHENE 70 BDL 0.60 BQL 10.0
1,1-DICHLOROETHENE 7 BDL BQL BQL BDL
1,1-DICHLOROETHANE 6 BDL BQL BQL 1.1
CHLOROETHANE 3,000 BDL BQL BQL BDL
VINYL CHLORIDE 0.03 BDL BQL 1.89' ... 90.0
CARBON DISULFIDE 700 BDL BQL BQL BDL
BROMODICHLOROMETHANE 0.6 BDL BQL BQL BDL
TRICHLOROETHENE 3 .•. 4.3;. 2.42 BQL ·.··. 15,2
CHLOROFORM 70 BDL BQL BQL BDL
CIS-1 ,2-DICHLOROETHENE 70 11.1 29.8 30.3 260.0
1 ,2-DICHLOROBENZENE 20 BDL BQL BQL BDL
ALL OTHER COMPOUNDS Varies BQL BQL BQL BQL
Bis(2-Ethylhexyl)phthalate 3 NA NA NA NA
ALL OTHER COMPOUNDS Varies NA NA NA NA
Shaded areas represent concentrations exceeding the NC Groundwater Standards.
BDL = Below Detection Limits
BQL= Below Quantitation Limits
ppb = parts per billion
NE = Not Established
*=Not sampled during this event 12/18/12
** = AMW-8S sampled instead of AMW-80 due to switched well tags.
Newly amended 2L groundwater standards applied to most recent event only.
TABLE 2 (Continued)
2of4
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
FORMER PAZIUK WAREHOUSE
SUNNYVALE DRIVE
WILMINGTON, NORTH CAROLINA
AMW-4D AMW-5* AMW-6D AMW-7D AMW-8S**
5/4/05 7/05/07 12/18/12 12/18/03 5/4/05 7/05/07 3/8-9/04 5/4/05 7/05/07 12/18/12 3/8-9/04 5/4/05 7/05/07 12/18/12 3/8-9/04 5/4/05 7/05/07 12/18/12
EPA METHOD 6210D and 82608 (Concentrations in ppb)
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND 3.0 BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL 0.54 BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL 336 j~'52J.··. ... -.1x.· BQL BQL BDL BQL BQL ND 4.5: ,83.?£ I• \,50~ i 360 BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL NO BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL 0.660 ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL 7.04 BQL 2,430.0 7.67 BQL ND 48.6 BQL BQL ND 126.0 BQL BQL ND
BQL BQL 64.2 BDL BQL BQL BDL BQL BQL ND ··'101.0' 20.0 BQL 56.4 BDL BQL 0.770 ND
BQL BQL 9.28 BDL BQL BQL BDL BQL BQL ND 7.6 BQL BQL : 18,1 . BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND 16.0 BQL BQL 3.44J BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL 226. 151 BDL BQL BQL BDL BQL BQL ND 164.0 BQL j .. ·.··58.4 · .. ·. 42.7 BDL BQL 1.31 ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
284.0. 2,890 ·' 49.3 ·.· 1.5 BQL BQL BDL BQL BQL ND 79.0. . 319.0 1,390' 1,220' BDL BQL 1.67 ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
'958.0 2,790 5,080 2.2 BQL 0.550 1.5 BQL BQL ND 4,950.0 872.0_. ,994 4,250 2.2 BQL 36.4 1.85
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
BQL BQL ND BDL BQL BQL BDL BQL BQL ND BDL BQL BQL ND BDL BQL BQL ND
EPA METHOD 8270D (Concentrations in ppb)
NA NA 6.44' NA NA NA NA NA NA ND NA NA NA 36~3 NA NA NA ND
NA NA ND NA NA NA NA NA NA ND NA NA NA ND NA NA NA ND
~~
')
'~
J
)
TABLE 2 (Continued)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
3 of4
FORMER PAZIUK WAREHOUSE
SUNNYVALE DRIVE
WILMINGTON, NORTH CAROLINA
ANALYTE NCAC 02L AMW-8D AMW-9S* AMW-9D AMW-10S*
STANDARD
DATE SAMPLED 3/8-9/04 5/4/05 7/05/07 1/23/13 3/8-9/04 5/4/05 7/05/07 3/8-9/04 5/4/05 7/05/07 12/18/12 11/30/04 5/4/05
EPA METHOD 6210D and 82608 (Concentrations in ppb)
CHLORODIBROMOMETHANE 0.41 BDL BQL BQL NA BDL BQL BQL BDL BQL BQL ND BDL BQL
TOLUENE 600 BDL BQL BQL <1.6 BDL BQL BQL 2.2 BQL BQL ND BDL BQL
XYLENES 500 BDL BQL BQL <3.1 BDL BQL BQL 3.5 BQL BQL 1.12J BDL BQL
ETHYLBENZENE 600 BDL BQL BQL <1.6 BDL BQL BQL BDL BQL BQL 1.57 BDL BQL
4-ISOPROPYL TOLUENE NE BDL BQL BQL NA BDL BQL BQL BDL BQL BQL 0.240J BDL BQL
NAPHTHALENE 6 BDL BQL BQL <2.0 BDL BQL BQL BDL BQL BQL 3.41 BDL BQL
n-PROPYLBENZENE 70 BDL BQL BQL <1.5 BDL BQL BQL BDL BQL BQL 1.05 BDL BQL
TETRACHLOROETHENE 0.7 BDL BQL BQL <1.8 BDL BQL BQL BDL BQL BQL ND i 360.0 . ~~ BQL
1 ,4-DICHLOROBENZENE 6 BDL BQL BQL <1.5 BDL BQL BQL BDL BQL BQL ND BDL BQL
SEC-BUTYLBENZENE 70 BDL BQL BQL <1.7 BDL BQL BQL BDL BQL BQL 0.700J BDL BQL
1,2,4-TRIMETHYLBENZENE 400 BDL BQL BQL <1.5 BDL BQL BQL BDL BQL BQL 7.70 BDL BQL
1,3,5-TRIM ETHYLBENZENE 400 BDL BQL BQL <1.3 BDL BQL BQL BDL BQL BQL 3.31 BDL BQL
ISOPROPYLBENZENE 70 BDL BQL BQL <1.6 BDL BQL BQL BDL BQL 1.39 2.12 BDL BQL
ACETONE 6,000 48.7 BQL BQL <10.0 BDL 6.28 6.12 4,515,0 ~ 137.0 14.1 ND BDL BQL
TRANS-1,2-DICHLOROETHENE 70 BDL BQL BQL 26.6 BDL BQL BQL 3.6 BQL BQL ND ·'160.0 27.6
1,1-DICHLOROETHENE 7 BDL BQL BQL 2.9J BDL BQL BQL BDL BQL BQL ND 15.8 BQL
1,1-DICHLOROETHANE 6 BDL BQL BQL 5.1 BDL BQL BQL BDL BQL BQL ND 4.2 BQL
CHLOROETHANE 3,000 BDL BQL BQL <1.6 BDL BQL BQL BDL BQL BQL ND BDL BQL
VINYL CHLORIDE 0.03 BDL BQL 34.0 12.6 BDL BQL BQL 16.9 4.88 2.23 2.15 155.0 20.4
CARBON DISULFIDE 700 BDL BQL BQL NA BDL BQL BQL BDL BQL BQL ND BDL BQL
BROMODICHLOROMETHANE 0.6 BDL BQL BQL <1.7 BDL BQL BQL ~·.• 1A .. BQL BQL ND BDL BQL
TRICHLOROETHENE 3 1M .. ~ 8.04 41;2 29.2 BDL BQL BQL 2.2 BQL BQL ND 1,240.0 553.0<
CHLOROFORM 70 BDL BQL BQL <1.9 BDL BQL BQL 9.2 BQL BQL ND BDL BQL
1,2-DICHLOROETHENE 70 BDL BQL BQL ~ 1,120 BDL BQL BQL BDL BQL BQL ND BDL BQL
CIS-1,2-DICHLOROETHENE 70 16.5 48.6 1····.·831 1,090 1.5 BQL BQL 112.5 ·~ 52.3 4.85 1.23 2,170.0 ·~·· 880.0
1,2-DICHLOROBENZENE 20 BDL BQL BQL <1.5 BDL BQL BQL BDL BQL BQL ND BDL BQL
tert-BUTYLBENZENE 70 BDL BQL BQL <1.6 BDL BQL BQL BDL BQL BQL ND BDL BQL
ALL OTHER COMPOUNDS Varies BDL BQL BQL <Varies BDL BQL BQL BDL BQL BQL ND BDL BQL
EPA METHOD 8270D (Concentrations in ppb)
Bis(2-Ethylhexyl)phthalate 3 NA NA NA <0.79 NA NA NA NA NA NA 4.67J NA NA
NAPHTHALENE 6 NA NA NA <0.34 NA NA NA NA NA NA 2.41J NA NA
ALL OTHER COMPOUNDS Varies NA NA NA <Varies NA NA NA NA NA NA ND NA NA
Shaded areas represent concentrations exceedmg the NC Groundwater Standards. BDL =Below Detectton Ltmtts BQL =Below Quantttatton Ltmtts
ppb = parts per billion NE = Not Established NA = Not Analyzed
*=Not sampled during this event 12/18/12
Newly amended 2L groundwater standards applied to most recent event only.
AMW-10D* AMW-115*
7/05/07 11/30/04 5/4/05 7/05/07 11/30/04 5/4/05 7/05/07
BQL 20.3~ BQL BQL BDL BQL BQL
BQL 2.3 BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL 13.8 ~~.~.·.
~ ·. . BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL 43.4 14.0 BDL 8.74 BQL
51.0 3.2 BQL BQL BDL BQL BQL
BQL BDL BQL 2.68 BDL BQL BQL
BQL BDL 4.26 BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
113 2.2 . 3.74 ~~·~. BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL 20.2. J BQL BQL BDL BQL BQL
639 ···~4,0 .~. ' BQL BQL BDL BQL BQL
BQL 19.8 ··. BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
. 2,290 ·~~ 107.0. BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
BQL BDL BQL BQL BDL BQL BQL
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
NA NA NA NA NA NA NA
n
J
TABLE 2 {Continued)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
4of4
I
FORMER PAZIUK WAREHOUSE
SUNNYVALE DRIVE
[
1 WILMINGTON, NORTH CAROLINA
,{ ANALYTE NCAC 02L AMW-11D* AMW-12S* AMW-12D* AMW-13D AMW-14S* AMW-14D* T-1* T-2*
STANDARD
I DATE SAMPLED 11/30/04 5/4/05 7/05/07 11/30/04 5/4/05 7/05/07 11/30/04 5/4/05 7/05/07 11/30/04 5/4/05 7/05/07 12/18/12 11/30/04 5/4/05 7/05/07 11/30/04 5/4/05 7/05/07 3/8·9/04 5/4/05 7/05/07 11/30/04 5/4/05 7/05/07
It CHLORODIBROMOM ETHANE
EPA METHOD 6210D (Concentrations in ppb)
0.41 BDL BQL BQL BDL BQL BQL '11,8" BQL BQL BDL BQL BQL NO BDL BQL BQL BDL BQL BQL .·.· 2.5 BQL BQL .·'3_.0'/ BQL D
r
' jTOLUENE 600 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL 0.80 BQL BDL BQL BQL 1.2 BQL BQL BDL BQL D
·I I[XYLENES 500 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL BQL BDL BQL BQL 3.1 BQL BQL BDL BQL D
JliETHYLBENZENE 600 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL BQL BDL BQL BQL 1.1 BQL BQL BDL BQL D
:4-ISOPROPYL TOLUENE NE BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL 0.85 0.960 BDL BQL BQL BDL BQL BQL BDL BQL D I
1rNAPHTHALENE 6 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL D
~n-PROPYLBENZENE 70 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL D
)TETRACHLOROETHENE 0.7 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL i(J.850. BDL BQL BQL jc.J7 ·.··.··.· J4 .. 8~ _:14:3, BDL BQL D
lt~,4-DICHLOROBENZENE 6 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL 18.8 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL D
,SEC-BUTYLBENZENE 70 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO 1.5 0.84 1.03 BDL BQL BQL BDL BQL BQL BDL BQL D
~~~ ,2,4· TRIMETHYLBENZENE 400 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO 2.1 2.02 5.49 BDL BQL BQL 2.0 BQL BQL BDL BQL D
11,1 ,3,5-TRIMETHYLBENZENE 400 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL 1.61 BDL BQL BQL 1.5 BQL BQL BDL BQL D
ISOPROPYLBENZENE 70 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL 0.69 BQL BDL BQL BQL BDL BQL BQL BDL BQL D
,,ACETONE . 6,000 BDL BQL BQL BDL BQL BQL BDL 113.0 BQL BDL BQL BQL NO BDL 35.4 BQL BDL 27.0 BQL BDL BQL BQL BDL BQL D
111TRANS-1 ,2-DICHLOROETHENE 70 BDL BQL BQL BDL BQL BQL BDL 0.77 BQL 3.3 0.77 BQL 29.1 BDL BQL BQL BDL BQL BQL 13.5 BQL 4.32 BDL BQL D
1, 1-DICHLOROETHENE 7 BDL BQL BQL BDL BQL BQL BDL BQL BQL 1.3 BQL BQL __ .19:1 .. BDL BQL BQL BDL BQL 0.750 1.6 BQL BQL BDL BQL D
1(1, 1-DICHLOROETHANE 6 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL BQL 2.1 0.77 BQL 1.9 BQL . BQL BDL BQL D
'cHLOROETHANE 3,000 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL D
11·VINYL CHLORIDE 0.03 BDL BQL BQL BDL BQL BQL BDL BQL . 40.2 · ... · 2.8 BQL BQL 1 .2,810 .· BDL BQL 0.650 BDL BQL BQL . 51.0 BQL BQL BDL BQL D
ltcARBON DISULFIDE 700 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL BQL 3.4 BQL BQL BDL BQL BQL BDL BQL D
BROMODICHLOROMETHANE 0.6 BDL BQL BQL BDL BQL BQL ··1Q.3 BQL BQL BDL BQL BQL NO BDL BQL BQL BDL BQL BQL · .. · 2.6·.·.· .• ·. BQL BQL 1.7 . BQL D
rTRICHLOROETHENE 3 BDL BQL BQL BDL BQL BQL BDL 0.89 BQL 109500 131,000 134,000 2.16J BDL BQL BQL BDL BQL BQL .. 60.9, .. ·.•·.57,7, BDL BQL D 93.0 ..
II~HLOROBENZENE 50 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL 2.56 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL D
CHLOROFORM 70 BDL BQL BQL BDL BQL BQL · .. ; .10.3 ,·· ·0.99, BQL BDL BQL BQL NO BDL BQL BQL BDL BQL BQL '. ~.8 BQL BQL 24.6 '.· ·;:'3.86 . D
lfciS-1 ,2-DICHLOROETHENE 70 BDL BQL BQL BDL BQL BQL BDL 32.7 ·• 136> 28,000.0 _51,600 '71,400 7,230 ' 2.0 0.61 0.780 7.2 3.38 1.98 1}9.0 82.4 ,; 9~.4 21.1 4.29 D
'1 ,2-DICHLOROBENZENE 20 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL D
f
11.tert-BUTYLBENZENE 70 BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL 0.510 BDL BQL BQL BDL BQL BQL BDL BQL D
li_ALL OTHER COMPOUNDS Varies BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL BQL NO BDL BQL BQL BDL BQL BQL BDL BQL BQL BDL BQL D
EPA METHOD 8270D (Concentrations in ppb)
J 1 4 llmcHLOROB~NZENE 6 NA NA NA NA NA NA NA NA NA NA NA NA 20.1 NA NA NA NA NA NA NA NA NA NA NA NA
PHENANTHRENE 200 NA NA NA NA NA NA NA NA NA NA NA NA 3.36J NA NA NA NA NA NA NA NA NA NA NA NA
u'ALL OTHER COMPOUNDS Varies NA NA NA NA NA NA NA NA NA NA NA NA NO NA NA NA NA NA NA NA NA NA NA NA NA
Shaded areas represent concentrations exceedmg the NC Groundwater Standards.
f JL = Below Detection Limits BQL = Below Quantitation Limits l >b = parts per billion NE = Not Established
u' = Destroyed * = Not sampled during this event 12/18/12
Newly amended 2L groundwater standards applied to most recent event only. l 'A = Not Analyzed
l '
1
f
FIGURES
l
r
Adapted from USGS Topographic
"Wilmington, N.C.," 1970, Photorevised 1979
Contour Interval = 5 Feet
plied Resource Management PC
P.O. Box 882. Hampstead, NC 28443
9 10) 270-2919 FAX [phone]
TITLE:
JOB:
I o7o98
I
SITE VICINITY MAP
SCALE:
1"=2,000'
DATE:
2/ll /08
DRAWN BY:
KLC
N
~
FIGURE:
l
i'r i j
17
( -,
I
l .
I
AMN-1 1D~ AMW-1 1S
~~~op? ~
lEGEND * Abandoned Water Supply Well
EEl Type I Monrrorlng Well
~ Type II Monitoring Well
@ Type Ill Monitoring Well
A;-2 I.--_,,, ~
MW-1
Warehouse
Former lnclnerat~j
Area
1 L....,_----L_---1
DID
-! : : ai
!
,bAMN-1
: I a ,. f:§
!1 •• !.'-?
I'> j
IM#-3
~T-1LU
@ Dtum St~ I EB@
Area !AMW-7D
!
AMW-1 4S6@AMN-1 4D
@
Yelton Trucking
1 Office
Loading Area
• • • • • •
1--Cafeteria ~-1 os
a'-0 A~-1DD ~] • • AMW-5~
8i~
I I ---; <;
Maintenance Shop I
1
Gate
AMW-~D 1_2 t AMW-4~~ @ l ){ )( )( )( )( )( )( )( )( )( )( )( )( '¥'( )( )( )( )( )( )( )( )( )( )( )( )( )( )( AMW-BS ~EJ:) AMN-BD j ence
:
I I
Ditch
APPROXIMATE LOCATION OF Well #2
ABANDONED WATER SUPPLY WELL*
'Roadway
: Express
AMW-12S~@)AMW-12D
·Fence
AMW-9S
~
AMW-9DEJ:)
LIJ ~MW-130 > EEl, C2:: ~'/ 0
LIJ
® ~ Land
z z ::> (f)
Title: Figure:
Site Map With Monitoring
And Abandoned
Water Supply Well Locations 2
Job:
0341
Drawn By:
JLZ
Scale:
1"=60'
Date:
2/13/08
pplied Resource Management PC
0. BoxBB2, [phone]
ampstead, NC 28443 FAX [phone]
r~
i J
fl
' ' L __ J
r -
i I J
' '
!
' c '
l >
r c "
AMW-60
(92.27) $ .,. D
,...,...,...::(bandoned USTs 7mp 10z.~ers
tqz.OO),... ---:* ,.., '\..
~**''*"'******li*l'*''**'*,.~,.~~1i""TTn AST~ ........
,... ........ :;lo-well #1 AMW-3 ~ ~;
~9,.ofYr' •n .I
AMW-1 4$~ AM-11-140
@ (NM)
,------, ~--'Yelton Trucking I ~ Office
MW-1 ~ .;.; ~· AMW-2 ,r---,r ~ M-11-2 t .;/
!1111-....
---.. : /1 tqo.OO) -· -, loading Area .j
0 0 0
" .,..;-:,'/
0
IJt'l<'*;****J''**~~'*'~·Fiteen>tclte**~~f*i~
! __ r;;_.,... I
~~~op7 /
LEGEND
Ell Type I Monrroring Well
~ Type II Monitoring Well
~ Type 111 Monitoring Well
@ PowerPole
~ Fire Hydrant
OlD Drain
@ Sanrrary Sewer Manhole * Abandoned Water Supply Well
(89.00) Potentiometric Surface Elevation Measured In Feet
D Destroyed
(NM) Not Measured
(NI) Not Included
---+ Groundwater Flow Direction
Note:
1. Type II wells MW-1 through MW-3 previousty Installed
by Clark Environmental Services, RC.
2. Contour Interval ~ 1'
Warehouse _ • ----1 (89.00) --__ _,_____ ',~ i
! r--Cafeteria , ~ 1 I I It-~AMW-10S'"l / f
! AMW-1 ~ " AMW-100 r_j_ / I
lB · c• --/ .=:;: ............ I I JJ _________ _..--lo
1
ffices /
" ~l I UIII,...-r:_L._, ,_. · I
t81 .oo) _!Mw-3 ....... 1 --; ~ 11
Drum Storage ~~~~ L.l..,r'-..._. U. MaintenanceS lOP I / Area ~ • •• ~ '-~ · /
@ AMW-70 EE@ T-1 '-, i //
~ ' / I ,...., .,.;
' ...... ...._....., Gate ,_,.,.,.
AMW-4D T-2 .1 __ _. AMW"8D
AMW $1 (86.07) @(D) . * (NI)
-4 ; >E)< l< )C )E ;c 3< :c '' 3< lC )C ;c '~'< :c ;c l< l< 3c )( H lc )C l< ;c ;c lC lC A'"" as ~$ I ~--
j
f !
Ditch
Approximate location
Of Inactive Water Supply Well #2
* CRoadway·
~ Express
3. Groundwater Aquifer Wells Not Included In Groundwater Table Aquifer Contours
4. AMW-8 measured and sampled on 1/23/13 .. Not included in contour calculations
due to differing date.
AMW-120
AMW-12S ~@) INM)
AMW-9S jMW-1SD ~I ;85.231 ~
AMW-9Dtfy $, B
186.051 I
I I I @
I
I •
Title:
~elope7
Land/
Figure:
Groundwater Contours
For Aquifer Zone #2
As Of 12/18/13 3
Job:
07098
Drawn By: Scale:
JLZ/JAK 1 "=60'
Date:
1/25/13
pplied Resource Management PC
O.Box882, [phone]
Hampstead, NC 28443 FAX [phone]
.
[]
n
' I ' ~
ll
I l J
ll
' ' l 0
r '
I
I '
I ,
r ,
i
l '
I
I -
I I ,
I
l '
i '
AMW-110 ~AMW-11S
(NS)
~~~op~ /
LEGEND
ffi Type I Monitoring Well
~ Type II Monitoring Well
~ Type Ill Monitoring Well
@ PowerPole
<e> Fire Hydrant
DD! Drain
@ Sanitary Sewer Manhole * Abandoned Water Supply Well
(70) cis-1 ,2-Dichloroethene Concentration In parts per billion
(D) Destroyed
Note:
1. Type II wells MW-1 through MW-3 previous~ installed
by Clark Environmental Services, RC.
AMW-60 E!)
(NO)
Abandoned USTs D 7mp T~ra..,ilers
----.~
:t*****~**''*''*'~HH<HH<c**c**H-,--,-i--,-, AST~
Well#l AMW-3 ~
I
I
AMW-2
~
Warehouse
:
I aj a • • •
i I
hAMW-1
'i :Ji-..-a-a --a-..
<f/!'1 -s;
.___~""--""~--~ II
C/Jf --- -~--.
/
/
~.;.-~ : ........ -
_,; !MW-3 ......_.
DID
-~D~_sto .. ra~e_--_.IJ~( , LU. · '·Area·_,. • - -...;..,;.
/
-__ a _____ -·,. i ~T-1 .
if' IAMW-?o-· -
•
I -/ i r4.25o) / _ ...:..s V '-Gate
15 080)ffi i 0 lfl. T-2 lMW-40 -o.g , t
\ ' ~~ ' ~(D) /--'-'---,T--t_ M .W-4 /X)( )( J( )(!)( )( )( )( )( K )( )( JU( )( )( ){ JE )( JE J( ~( J( J( J( )( J( -~ 1 \ Fence
\
\ ,_
\ 'i \
\\ ':1' J· \ _, -,, --~
: -...
? ? ? •
rrc
Well#2
* Roadway
Express
AMW-14S~ AMW-140
@ (NS)
Yelton Trucking
Otfice
Loading Area
•
AMW-6~
.....
<J>' '
' \
AMW-8S ~E!) \
AMW-80\
' (1.090)
? •
•70
' \
2. Type Ill well T-1 was not used tor contouring contaminant concentrations.
3, Contour Interval ~ 2,000 ppb
4. AMW-8D sampled on 1/23/13 AMW-12S
~~AMW-120 ~ (NS)
\
\
? •
? •
~elope7
Land/
Title: Figure:
cis-1 ,2-Dichloroethene
Concentrations In Aquifer 4
Zone #2 As Of 12/18/12
Job:
07098
Drawn By: Scale:
JLZ/JAK 1"=60'
Date:
2/7/13
pplied Resource Management PC
0, Box 882, (910[270-2919
Hampstead, NC 28443 FAX [phone]
I I
I
AMW-ll O E!)~ AMW-11 S [NS)
~~~op7 ~
LEGEND
E£) Type I Monitoring Well
~ Type II Monitoring Well
~ Type Ill Monitoring Well
@ PowerPole
~ Fire Hydrant
UID Drain
@ Sanitary Sewer Manhole * Abandoned Water Supply Well
(3) Trlchloroethene Concentranon in parts per billion
(D) Destroyed
Note:
1. Type II wells MW-1 through MW-3 previous¥ installed
by Clark Environmental Services, P.C.
Former
Incinerator
Area
/
I
I.
I
\.
\
•
? •
AMW-60 E!)
[NO)
AMW-2
~
Warehouse
2. Type Ill well T-1 was not used for contouring contaminant concentrations.
3. Contour Interval ~ 500 ppb
4. AMW-8D sampled on 1/23/13
DITch
AMW-14S ~E!) AMW-140
@ [NS)
Yelton Trucking
Office
Loading Area
AMW-5~
----AMW-100
[NS)
H l! J( )( lHHHt JOE: ? •
Well#2
*
.... ....
Roadway
Express
AMW-12D
[NS)
AMW-12S ~E!)
AMW-8S ~EEl AMW-80
[29.2 I
' '
ence
\
? •
AMW-9S ~MW-13D blJ
~X [2.16J) >
AMW-9D E!) X E!) 6':
[ND) ~ . 0
uu ---' ~ z z ::> en
~elope?
Land/
Title: Trichloroethene
Concentrations In Aquifer
Zone #2
Figure:
5
Job:
07098
As Of 12/18!12
Drawn By: Scale:
JLZ 1 "=60'
Date:
2/7!13
pplied Resource Management PC
0. Box 882, [910) 270-2919
Hampstead, NC 28443 FAX [phone]
J
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1
AMW-6D$
(ND) Abandon~~D 7S::
:t*************************~r-r..-.,.-...--. AST~
Well#1 AMW-3 ~
AMW-14S ~ AMW-14D
@ (N5)
Yelton Trucking
AMW-11D ~AMW-115 (N5)
~~~07 /
LEGEND
EB Type I Monitoring Well
~ Type II Monitoring Well
~ Type Ill Monitoring Well
@ PowerPole
~ Fire Hydrant
DID Drain
@ Sanitary Sewer Manhole * Abandoned Water Supply Well
(0. 7) Tetrachloroethene Concentration in parts per billion
(D) Destroyed
Note:
1. Type II wells MW-1 through MW-3 previously Installed
by Clark Environmental Services, P.C.
2. Type Ill well T-1 was not used for contouring contaminant concentration.
3. Contour Interval = 1 00 ppb
4. AMW-BD sampled on 1/23/13
AMW-2
·~
Warehouse
I
? •
..
Ditch
II
"
' \
Well#2
*
..
a
"
a
"
AMW-lOD
(N5)
CRoadway
:: Express
"
Office
Loading Area
AMW-85 ~$ AMW-8D
(<1.8)
AMW-12D
AMW-125 ~@ (N5)
AMW-95
~
AMW-9D$
(ND)
AMW-13D
(ND) ~
$ (:!:::
0
Ll.l __J ~ z z :::> C/)
~elope?
Land/
Title: Tetrachloroethene
Concentrations In
Aquifer Zone #2
As Of 12!18/l 2
Figure:
6
Job:
07098
Drawn By:
JLZ
Scale:
111=601
Date:
2/7/13
pplied Resource Management PC
0. Box 882, [phone]
Hampstead, NC 28443 FAX [phone]
n ; J
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AMW-60 $
(NO)
A--2
~
A-·14S~ A-·140
@ (NS)
Yelton Trucking
Office
Loading Area ??? '!J
/ 1
IR**********"*'"*'"*'"*'"*'"*''*'~&c ence f3 o-[1
A--l1D ~A-·11S (NS) ,
~~~op7 /
LEGEND
ffi Type I Monitoring Well
~ Type II Monitoring Well
~ Type Ill Monitoring Well
© PowerPole
~ Fire Hydrant
ll!ll Drain
@ Sanitary Sewer Manhole * Abandoned Water Supply Well
(0.03) Vinyl Chlonde Concentration in parts per billion
(D) Destroyed
Note:
1, Type II wells MW-1 through MW-3 previous~ installed
by Clark Environmental Services, RC.
0 Warehouse
:
1b AMW-1
l a a
m I :Sf:-.... -
li ml "'' ~~ i : MW-3
DID
DrumS!oroge I.L-1 LU
@ ~ .... ~~-1 ..... -
'/ iAM\\1.70
0 0
0 0
.... -.........
......
0
0 -
0
A--100
(NSf
. / ! (42,7)
t' l~if$7•"oo.· @f~ .. ·.·_ .. ·· ·_.· __ ·.· 6'o ....... _.· ...• · ...•. ·Gi"
L--=-"~-~-4 ! lOI H H ~~I JOI Jl Jl Jl J0~~~/,~1 ll Jl ll ll H Jl~ )~Jill~
\. \ 'i ·. . ' \ \ i'-' \
\
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~.-I
.... I
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Ditch
Well#2 * r--'-----,
Roadway
Express
0
0 ·O.y
A-·8S ~$
A--8D
(12,6)
? •
2. Type Ill well T· 1 was not used tor contouring contaminant concentrations.
3, Contour Interval ~ 50 ppb
Contour Interval between AMW-9D and AMW-1 3D ~ 1,000
4. AMW-8D sampled on 1/23/1 3
A-·12S
~~A-·120 W (NS)
'
AMW-5~
' ·' ' \
\
? •
'tv' o· J
I I, ..
A-·95 ~' I ~ ~~-130
AMW-90 F' I $. ' • (2,810[ (2,15) .• :
t ®!
\ s\ i
~elope7
Land/
·w
-'
\\ J \ ·.~ \f;
Title:
\ .•? y·
?
Figure:
Vinyl Chloride
Concentrations In Aquifer
Zone #2 As Of 12!18/12 7
Job:
07098
Drawn By: Scale:
JLZ/JAK 1 "=60'
Date:
2/7!13
pplied Resource Management PC
O.Box882, [phone]
ampstead, NC 28443 FAX [phone]
fl
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AMW-llD ~AMW-11S
~~~op~ ~
AMW-60 $
Abandoned USTs D 7mp T~ra .. ilers ---..~~
~'***********"'***'tl~ ~ AST~
Well#l AMW-3 ~
AMW-2
~
Warehouse
/
/
DID
/
I
DrumStorage i~
Area-_,. iEEl(~)T-1
MW-2 ~
1!111 I
0 0
-....
0 0 0
--0 --0
Estimated Extent Of l lAMW-7D I . -
: CGOte Groundwater Contamination~ _
1 AMW-40$1.--···-········ @:~----·-·--··· __ •. _. __ <._ •. · / .••.. _ •...••. -.···---··-;
LEGEND
EEl Type I Monitoring Well
~ Type II Mon~orlng Well
~ Type Ill Monitoring Well
@ PowerPole
~ Fire Hydrant
Uin Drain
@ Sanitary Sewer Manhole * Abandoned Water Supply Well
Q Proposed Air/ Soli Gas Sample Locations
@ Proposed Type Ill Well Location
(D) Destroyed
Note:
1, Type II wells MW-1 through MW-3 prevlousf{ installed
by Clark Environmental Services, P.C
L_-'---'-'--'---'-AMW-4 I)(}()(_)()()( ){_)()( )( _J( )( H )~~ribk( )( K )( )( )( )( )_~ lJ )( )( )( H l ' -- - - ' ' .
:
I \
\ i ' Ditch
? •
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Well#2 ~---~
* Roadway
Express
AMW-14S~ AMW-140
@
Yelton Trucking
0
Office
Loading Area
AMW-6~
'
ence
' ' '
I
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AMW-9S~i
AMW-9D $ $,
I
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0::: 0
w --' ' ' ,:{
~elope?
Land/
AMW-SS ~$ '
\ ' ·~ ,~ 5
AMW,SD '
? •
Proposed Type Ill
Well Location ~
@
: (/')
\!
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Title: Figure:
Proposed Monitoring Well 8 and Air/Soil Gas
Sampling Locations
Job:
07098
Drawn By: Scale:
JLZ/JAK l "=601
Date:
2/7/13
AMW-12S pplied Resource Management PC
O.Box8B2. [phone] ~@ AMW-120 ampstead, NC 28443 FAX [phone]
: r l
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APPENDIX A
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Laboratory Report of Analysis
To: Joe Zuncich
APPLIED RESOURCE MANAGEMENT
P.O. Box 882
Hampstead, NC 28443
Report Number: 31204038
Client Project: Former Pazivk Warehouse
Dear Joe Zuncich,
Enclosed are the results of the analytical services performed under the referenced project for the received samples
and associated QC as applicable. The samples are certified to meet the requirements of the National Environmental
Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be retained in our files
for a period of five years in the event they are required for future reference. All results are intended to be used in their
entirety and SGS is not responsible for use of less than the complete report. Any samples submitted to our
laboratory will be retained for a maximum of thirty (30) days from the date of this report unless other arrangements
are requested.
If there are any questions about the report or services performed during this project, please call Michael D. Page at
[phone]. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you again
on any additional analytical needs.
Sincerely,
SGS North America Inc.
Michael D. Page
Project Manager
[e-mail]
Print Date. 0110312013
Digitally signed by: Michael Page
Date: 2013.01.03 12:13:43 -05'00'
Date
ANAlYTICAl PERSPECTIVES IS NOW PART OF SGS, THE WORUl'S lEADING INSPECTION,
l_ VERIFICATION, TESTING AND CERTIFICATION COMPANY.
SGS .A 1131)·1•::01 Pc:rspe ~~·,·es 55{!{1 Busintss Or. US l'M05 · Wilmin{)10n. NC t 1 I 910 JSO 1901 f t 1 910 350 1557 www S{J$ o;;n
Page 1 of34
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.(~------~-------------------------------L_a_b_o_rn_t_o_~ __ Q_u_a_lif-ie_r_s __________ ~--------------~~----~--J]
Report Definitions
DL
CL
LOQ
Method, Instrument, or Estimated Detection Limit per Analytical Method
Control Limits for the recovery result of a parameter
Reporting Limit
DF Dilution Factor
RPD
LCS(D)
MS(D)
MB
Relative Percent Difference
Laboratory Control Spike (Duplicate)
Matrix Spike (Duplicate)
Method Blank
Qualifier Definitions
B
u
v
A
J
0
E
s
Q
Recovery or RPD outside of control limits
Analyte was detected in the Lab Method Blank at a level above the LOQ
Undetected (Reported as ND or < DL)
Recovery is below quality control limit. The data has be.en validated based on a favorable signal-to-noise
and detection limit
Amount detected is less than the Lower Method Calibration Limit
Estimated Concentration.
The recovery of this analyte in the OPR is above the Method QC Limits and the reported concentration in
ihe sample may be biased high
Amount detected is greater than the Upper Calibration Limit
The amount of analyte present has saturated the detector. This situation results in an
underestimation of the affected analyte(s)
Indicates the presence of a quantitative interference. This situation may result in an
underestimation of the affected analyte(s)
Indicates the presence of a qualitative interference that could cause a false positive or an
overestimation of the affected analyte(s)
DPE Indicates the presence of a peak in the polychlorinated diphenylether channel that could
cause a false positive or an overestimation of the affected analyte(s)
TIC Tentatively Identified Compound
EMPC Estimated Maximum possible Concentration due to ion ratio failure
ND Not Detected
K Result is estimated due to ion ratio failure in High Resolution PCB Analysis
P RPD > 40% between results of dual columns
D Spike or surrogate was diluted out in order to achieve a parameter result within instrument calibration
range
Samples requiring manual integrations for various congeners and/or standards are marked and dated by the analyst. A
code definition is provided below:
M1 Mis-identified peak
Note Results pages that include a value for "Solids(%)" have been adjusted for moisture content.
F'rint Date· o·tf03i20'1.3
Page 2 of34
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Client Sample 10
AMW-40
AMW-60
AMW-70
AMW-80
AMW-90
AMW-130
Trip Blank (not on COC)
Print Date· 0110312013
Sample Summary )
Lab Sample 10 Collected Received Matrix
31204038001 12/18/2012 12:32 12/19/2012 09:10 Water
31204038002 12/18/2012 14:02 12/19/2012 09:10 Water
31204038003 12/18/2012 11:40 12/19/2012 09:10 Water
31204038004 12118/2012 1o:5o 12/19/2012 09:10 Water
31204038005 12/18/2012 15:25 12/19/2012 09:10 Water
31204038006 12/18/2012 16:32 12/19/2012 09:10 Water
31204038007 12/18/2012 00:00 12/19/2012 09:10 Water
!~.C Certification# 481
SGS An;tlyi''"l Persp0:\i\'('S SSOO Business Or. US :l'Ml)5 · Wilminglon, ~lC t i1910 35(! 1903 f [phone] www.sgs con\
Page 3 of34
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Resuits of AMW-40
Client Sample ID: AMW-40
Client Project lb: Former Paziv~ Warehouse
Lab Sample ID: 31204038001-B
Lab Project ID: 31204038
.Results by SW-846 82608 .... , ~:···-· ,y... . . · .•.. ,. __
Parameter
1,1, 1 ,2-Tetrachloroethane
1,1, 1-Trichloroethane
1,1 ,2,2-Tetrachloroethane
1,1 ,2-Trichloroethane
1, 1-Dichloroethane
1 , 1-Dichloroethene
1, 1-Dichloropropene
1 ,2,3-Trichlorobenzene
1 ,2,3-Trichloropropane
1 ,2,4-Trichlorobenzene
1 ,2,4-Trimethylbenzene
1 ,2-Dibromo-3-chloropropane
1 ,2-Dibromoethane
1 ,2-Dichlorcibenzene
1 ,2-Dichloroethane
1 ,2-Dichloropropane
1 ,3,5-Trimethylbenzene
1 ,3-Dichlorobenzene
1 ,3-Dichloropropane
1 A-Dichlorobenzene
2,2-Dichloropropane
2-Butanone
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-lsopropyltoluene
4-Methyl-2-pentanone
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
hint Date· 01!03/201.3
Result
ND
ND
ND
ND
ND
9.28
ND
ND
ND
ND
ND
NO
NO
ND
ND
ND
ND
ND
ND
ND
NO
NO
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
NO
NO
NO
ND
ND
ND
ND
ND
ND
ND
ND
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
DL
2.84
1.64
2.31
2.36
1.72
2.30
1.62
2.86
3.37
1.62
2.45
15.0
2.75
2.38
2.37
1.29
2.20
2.59
2.56
3.70
1.91
12.2
2.39
9.92
3.37
1.62
10.2
11.3
1.25
2.34
1.75
2.91
3.97
1.34
1.46
0.872
2.16
2.15
1.72
1.47
1.06
3.06
3.09
Collection Date: 12/18/2012 12:32
Received Date: 12/19/2012 09:10
Matrix: Water
LOQ/CL
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
40.0
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
200
8.00
40.0
8.00
8.00
40.0
200
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugtL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DF
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
Date Analyzed
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
12/21/2012 19:44
N.C Certification II. 461
SGS .c\r1J!yt·:&l Pc·tspe~(,ves I SSOO Businm Dr. US· tl1t'Hli5 · 'Will'llifl\)10I\ t•JC t J.l 91035(] 1903 f t 1 910 3501557 www.Sl)HOffl
M'.!Hibf'.-uf the &GS Group-ISGSS~\1
Page 4 of34
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;Results of AMW-40 . '· ~ -.., '-:~
Client Sample ID: AMW-40
Client Project I D: Form.er Pazivk Warehouse
Lab Sample ID: 312040313001"8
Lab Project ID: 31204038
c•'~'C• •-• • '" • • ·•-• '"
;Results by SW-846 82608 .. ··--:-;~ ..... ' . :·.~---,· ... -,-.. . .
Parameter Result
Dichlorodifluoromethane ND
cis~ 1 ,3-Dichloropropene ND
trans-1 ,3-Dichloropropene ND
Diisopropyl Ether ND
Ethyl Benzene ND
Hexachlorobutadiene ND
lsopropylbenzene (Cumene) ND
Methyl iodide ND
Methylene chloride ND
Naphthalene ND
Styrene ND
Tetrachloroethane 3.52
Toluene ND
Trichloroethane 49.3
Trichlorofluoromethane ND
Vinyl chloride 151
Xylene (total) ND
cis-1 ,2-Dichloroethene 5080
m,p-Xylene ND
n-Propylbenzene ND
o-Xylene ND
sec-Butylbenzene ND
tert-Butyl methyl ether (MTBE) NO
iert-Butylbenzene ND
trans-1 ,2-Dichloroethene 64.2
trans-1 ,4-Dichloro-2-butene ND
Surrogates
1 ,2-Dichloroethane~d4 105
4-Bromofluorobenzene 98.0
Toluene dB 102
Print Date: 01!0312013
Collection Date: 12/18/2012 12:32
RE)c;eived Date: 12/19/2012 09:10
Matrix: Water
"{
Qual DL LOQ/CL Units DF Date Analyzed
u 1.28 40.0 ug/L 8 12/21/2012 19:44
u 2.15 8.00 ug/L 8 12/21/2012 19:44
u 2.10 8.00 ug/L 8 12/21/2012 19:44
u 1.67 8.00 ug/L 8 12/21/2012 19:44
u 2.01 8.00 ug/L 8 12/21/2012 19:44
u 2.19 8.00 ug/L 8 12/21/2012 19:44
u 2.29 8.00 ug/L 8 12/21/2012 19:44
u 1.18 8.00 ug/L 8 12/21/2012 19:44
u 1.29 40.0 lig/L 8 12/21/2012 19:44
u 1.74 8.00 ug/L 8 12/21/2012 19:44
u 1.79 8.00 ug/L 8 12/21/2012 19:44
J 2.11 8.00 ug/L 8 12/21/2012 19:44
u 1.56 8.00 ug/L 8 12/21/2012 19:44
1.82 8.00 ug/L 8 12/21/2012 19:44
u 1.11 8.00 ug/L 8 12/21/2012 19:44
1.51 8.00 ug/L 8 12/21/2012 19:44
u 2.38 16.0 ug/L 8 12/21/2012 19:44
120 400 ug/L 400 12/20/2012 19:25
u 2.24 16.0 ug/L 8 12/21/2012 19:44
u 2.38 8.00 ug/L 8 12/21/2012 19:44
u 2:38 8.00 ug/L 8 12/21/2012 19:44
u 1.93 8.00 ug/L 8 12/21/2012 19:44
u 1.60 8.00 ug/L 8 12/21/2012 19:44
u 2.34 8.00 ug/L 8 12/21/2012 19:44
1.70 8.00 ug/L 8 12/21/2012 19:44
u 18.9 40.0 ug/L 8 12/21/2012 19:44
64.0-140 % 8 12/21/2012 19:44
85.0-115 % 8 12/21/2012 19:44
82.0-117 % 8 12/21/2012 19:44
N.C. Certification# 481
Page 5 of34
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1 Results of AMW-40
Client Sample ID: AMW-40
Client Project I D: Forme.r Pazivk Warehouse
Lab Sample ID: 31204038001"8
Lab Project ID: 31204038
:Results by SW-846 82608
Parameter
f l Batch Information
r ,
l
Analytical Balch: VMS2790
Analytical Method: SW-846 82608
Instrument: MSD8
Analyst BWS
Analytical Balch: VMS2793
Analytical Method: SW-846 82608
Instrument MSDS
Analyst BWS
Print Date· 01i03i201.3
Collection Date: 12/18/2012 12:32
Received Date: 12/19/2012 09:10
Matrix: Water
DF
Prep Balch: VXX4452
Prep Method: SW-846 50308
Prep Date/Time: 12/20/2012 08:25
Prep Initial Wt.NoL: 40 mL
Prep Extract Vol: 40 mL
Prep Batch: VXX4458
Prep Method: SW-846 50308
Prep Date/Time: 12/21/2012 08:34
Prep Initial Wt.Nol.: 40 mL
Prep Extract Vol: 40 mL
Date Analyzed
N.C Celtifiealion i/481
SGS .~naly1•·:GI PerspNi<\'es SSOO Business Dr. US· 1'1}405 · Wiln1irlgton, NC t [phone] f t 1 910 350 1551 www.sgs (;!)m
Page 6 of34
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!1 ;Results of AMW-40
{.(;:.· . . . . ; ··: : ,~~. ~' ·::,-·
Client Sample ID: AMW-40 Collection Date: 12/18/2012 12:32
n Client Project lb: FormerPazivk Warehouse Received Date: 12/19/2012 09:10
Lab Sample ID: 31204038001-D Matrix: Water
Lab ProjectiD: 31204038
[] :R~~u,lt$,~¥ ~lJ\1·846 _8770[:)c ..
Parameter Result Qual DL LOQ/CL Units OF Date Analyzed
[j 1 ,2,4-Trichlorobenzene Nb u 1:73 4.99 ug/L 12/20/2012 20:34
1 ,2-Dichlorobenzene NO u 1.71 4.99 ug/L 12/20/2012 20:34
1 ,3"Dichlorobenzene ND u 1.65 4.99 ug/L 12/20/2012 20:34
1 A-Dichlorobenzene NO u 1.63 4:99 ug/L 12/20/2012 20:34
t ~ 2,4-Dinitrotoluene ND u 1.84 4.99 ug/L 12/20/2012 20:34
2,6-Dinitrotoluene NO u 1.88 4.99 ug/L 12/20/2012 20:34
2cChlbrbnaphthalene NO u 2.00 4;99 ug/L 12/20/2012 20:34
2-Methylnaphthalene NO u 1.94 4:99 ug/L 12/20/2012 20:34 I ~ 2-Nitroaniline ND u 1.69 4.99 ug/L 12/20/2012 20:34
3,3'-Dichlorobenzidine ND u 1.75 9.98 ug/L .12/20/2012 20:34
3-Nitroaniline NO u 1.65 25.0 ug/L 12/20/2012 20:34
[: 4-Chloroaniline NO u 1.88 25.0 ug/L 12/20/2012 20:34
4-Chlorophenyl phenyl ether NO u 2:46 4.99 ug/L 12/20/2012 20:34
Acenaphthene ND u 2.06 4.99 ug/L 12/20/2012 20:34
Acenaphthylene ND u 2.00 4.99 ug/L 1212012012 2o:34
[ ~ Anthracene NO u 1.93 4;99 ug/L 12/20/2012 20:34
Benzo(a)anthracene NO u 1.96 4.99 ug/L 12/20/2012 20:34
Benzo(a)pyrene NO u 1.86 4.99 ug/L 12/20/2012 20:34
[: Benzo(b )fluoranthene ND u 1.96 4c99 ug/L 12/20/2012 20:34
Benzo(g,h,i)perylene ND u 2.15 4:99 ug/L 12/20/2012 20:34
Benzo(k)fluoranthene NO u 2.31 4.99 ug/L 1.2/20/2012 20:34
Bis(2-Chloroethoxy)methane NO u 2.12 4.99 ug/L 12/20/2012 20:34 r: Bis(2-Chloroethyl)ether NO u 2.21 4.99 ug/L 12/20/2012 20:34
Bis(2-Chloroisopropyl)ether NO u 2.04 4.99 ug/L 12/20/2012 20:34
Bis(2-Ethylhexyl)phthalate 6.44 1.95 4.99 ug/L 12/20/2012 20:34
4-Bromophenyl phenyl ether NO u 2.04 4.99 ug/L 12/20/2012 20:34 L Butyl benzyl phthalate NO u 1.89 4.99 ug/L 12/20/2012 20:34
Chrysene NO u 2.20 4.99 ug/L 12/20/2012 20:34
Di-n-butyl phthalate NO u 1.91 4.99 ug/L 12/20/2012 20:34
r . Di-n-octyl phthalate NO u 1.46 4.99 ug/L 12/20/2012 20:34
l ~ Dibenz{a,h)anthracene ND u 2.02 4.99 ug/L 12/20/2012 20:34
Dibenzofuran NO u 2.22 4.99 ug/L 12/20/2012 20:34
Diethyl phthalate NO u 2.10 4.99 ug/L 12/20/2012 20:34
L Dimethyl phthalate NO u 2.14 4.99 ug/L 12/20/2012 20:34
Diphenylamine NO u 2.02 4.99 ug/L 12/20/2012 20:34
Fluoranthene NO u 2.02 4.99 ug/L 12/20/2012 20:34
L Fluorene NO u 2.44 4.99 ug/L 12/20/2012 20:34
Hexachlorobenzene NO u 1.93 4.99 ug/L 12/20/2012 20:34
Hexachlorobutadiene NO u 1.52 4.99 ug/L 12/20/2012 20:34
Hexachlorocyclopentadiene NO u 0.786 9.98 ug/L 12/20/2012 20:34
L Hexachloroethane NO u 1.40 4.99 ug/L 12/20/2012 20:34
lndeno(1 ,2,3-cd)pyrene ND u 2.02 4.99 ug/L 12/20/2012 20:34
lsophorone ND u 2.09 4.99 ug/L 12/20/2012 20:34
Print Dale: 01'03!2013 N.C Certification# 481
SGS Anol)·t>.::~l Perspeni·,.es 55\10 Businm Dr US · t'BII05 · \<1/ilnlirJgtM, tJC tl191035\l1903 It 1 910 351) 1557 www.sgs co·m
I M•lm~or t<f the SG> Grou.,{SGS S•\1 L ,
Page 7 of34
n
n
n
fl I I
l J
f '
l
!Results of AMW-40
Client Sample ID: AMW-40
Client Project Jb: Former Pazivk Warehouse
Lab Sample ID: 31204038001-D
Lab ProjectiD: 31204038
;Results by SW-846 82700
'·•c;;.,<".>'." • "00
Parameter Result
Naphthalene ND
4-Nitroaniline ND
Nitrobenzene ND
Phenanthrene ND
Pyrene ND
n-Nitrosodi-n-propylamine ND
Surrogates
2,4,6-Tribromophenol 91.0
2-Fiuorobiphenyl 84.0
2-Fiuorophenol 80.0
Nitrobenzene-d5 81.0
Phenol-d6 87.0
Terphenyl-d14 82.0
Batch Information
Analytical Batch: XMS1777
Analytical Method: SW-846 82700
Instrument: MSDS
Analyst cr.~P
Print Date: 01;1)312013
Qual DL
u 1:94
u 1.68
u 2.19
u 1.99
u 2.01
u 2.23
Collection Date: 12/18/2012 12:32
Rec;eivedDate: 12/19/2012 09:10
Matrix: ·Water
LOQ/CL Units DF
4.99 ug/L
25.0 ug/L
4.99 ug/L
4.99 ug/L
4.99 ug/L
4.99 ug/L
29.3-152 %
50.0-107 %
33.1-1.18 %
46.0-118 %
49.0~120 %
22.1-142 %
Prep Batch: XXX3426
Prep Method: SW-846 3520C
Prep Date/Time: 12119/2012 14:49
Prep li1itial VVt.Nol.: 1002 mL
Prep Extract Vol: 5 mL
Date Analyzed
12/20/2012 20:34
12/20/2012 20:34
12/20/2012 20:34
12/20/2012 20:34
12/20/2012 20:34
12/20/2012 20:34
12/20/2012 20:34
12/20/2012 20:34
12/20/2012 20:34
12/20/2012 20:34
12/20/2012 20:34
12/20/2012 20:34
N.C. Certification it 481
SGS 1\ nal)·tc.;;;! Perspenives 5500 Businuss Dr. US· 284115 · Wilmim~ton, NC t d 910 35() 190~ f + 1 910 350 15S7 wVNI.SQS com
Page 8 of 34
n
n
"'ll\.l.'VT1<;'M f'FR1>1'11XmVJ;"
n Results of AMW-60
Client Sample ID: AMW-60 Collection Date: 12/18/2012 14:02
n Client Project lb: FormerPazivk Warehouse Received Date: 12/19/2012 09:10
Lab Sample ID: 31204038()o2~A Matrix: Water
Lab Project ID: 31204038
lJ 'Results by SW-846 82608
~ .. ; --, '':·-: , ..... '. ,.
Parameter Result Qual DL LOQ/CL Units OF Date Analyzed
r J
1,1, 1 ,2-Tetrachloroethane NO u 0.355 1.00 ug/L 12/21/2012 16:52
1,1, 1-Trichloroethane NO u 0.205 1.00 ug/L 12/21/2012 16:52
1,1 ,2,2-Tetrachloroethane NO u 0.289 1:00 ug/L 12/21/2012 16:52
1,1 ,2-Trichloroethane NO u 0.295 1.00 ug/L 12/21/2012 16:52
r] 1, 1-Dichloroethane NO u 0.215 1.00 ug/L 12/21i2012 16:52
1, 1-Dichloroethene ND u 0.288 1.00 ug/L 12/21/2012 16:52
1 , 1 ~Dichloropropene NO u 0.203 1.00 ug/L 12/21/2012 16:52
1 ,2,3-Trichlorobenzene NO u 0.358 1.00 ug/L 12/21/2012 16:52 l ~ 1 ,2,3-Trichloropropane ND u 0,421 1.00 ug/L 12/21/2012 16:52
1 ,2,4-Trichlorobenzene NO u 0.202 1.00 ug/L 12/21/2012 16:52
1 ,2,4cTrimethylbenzene NO u 0.306 1.00 ug/L 12/21/2012 16:52
l : 1 ,2-Dibromo-3-chloropropane NO u 1.88 5.00 ug/L 12/21/2012 16:52
1 ,2-Dibromoethane NO u 0.344 1.00 ug/L 12/21/2012 16:52
1 ,2-Dichlorobenzene ND u 0.298 1.00 ug/L 12/21/2012 16:52
1 ,2-Dichloroethane NO u 0.296 1.00 ug/L 12/21/2012 16:52 l: 1 ,2-Dichloropropane NO u 0.161 1.00 ug/L 12/21/2012 16:52
1 ,3,5-Trimethylbenzene NO u 0.275 1.00 ug/L 12/21/2012 16:52
1 ,3-Dichlorobenzene NO u 0.324 1.00 ug/L 12/21/2012 16:52
l: 1 ,3-Dichloropropane NO u 0.320 1.00 ug/L 12/21/2012 16:52
1 A-Dichlorobenzene ND u 0.463 1.00 ug/L 12/21/2012 16:52
2,2-Dichloropropane NO u 0.239 1.00 ug/L 12/21/2012 16:52
2-Butanone NO u 1.53 25.0 ug/L 12/21/2012 16:52
[' 2-Chlorotoluene NO u 0.299 1.00 ug/L 12/21/2012 16:52
l ' 2"Hexanone NO u 1.24 5.00 ug/L 12/21/2012 16:52
4-Chlorotoluene NO u 0.421 1.00 ug/L 12/21/2012 16:52
4-lsopropyltoluene .NO u 0.203 1.00 ug/L 12/21/2012 16:52
r . 4"Methyl-2-pentanone NO u 1.28 5.00 ug/L 12/21/2012 16:52
( ~ Acetone NO u 1.41 25.0 ug/L 12/21/2012 16:52
Benzene NO u 0.156 1.00 ug/L 12/21/2012 16:52
I: Bromo benzene NO u 0.293 1.00 ug/L 12/21/2012 16:52
Bromochloromethane NO u 0.219 1.00 ug/L 12/21/2012 16:52
Bromodichloromethane NO u 0.364 1.00 ug/L 12/21/2012 16:52
Bromoform NO u 0.496 1.00 ug/L 12/21/2012 16:52
Bromomethane NO u 0.168 1.00 ug/L 12/21/2012 16:52
n-Butylbenzene NO u 0.183 1.00 ug/L 12/21/2012 16:52
Carbon disulfide NO u 0.109 1.00 ug/L 12/21/2012 16:52
l: Carbon tetrachloride NO u 0.270 1.00 ug/L 12/21/2012 16:52
Chlorobenzene NO u 0.269 1.00 ug/L 12/21/2012 16:52
Chloroethane NO u 0.215 1.00 ug/L 12/21/2012 16:52
Chloroform NO u 0.184 1.00 ug/L 12/21/2012 16:52
r . Chloromethane NO u 0.132 1.00 ug/L 12/21/2012 16:52
l j Oibromochloromethane NO u 0.383 1.00 ug/L 12/21/2012 16:52
Oibromomethane NO u 0.386 1.00 ug/L 12/21/2012 16:52
l ~ f0rinl Date· 0110312013 N.C Certification if 4S·J
SGS .~ •.wly1'(:31 Per spcn•ves SS'I}!l Business Dr. US · tJ141J5 · Wilmitlgton. t4C til 1110:)50 1903 h19103501557 www.sr.;s cr:rm
l : ~.1,.!m~~; uf thL• S<.!S G1oup ISG S St\1
Page 9 of 34
n
n
n Results of AMW-6D
~--: ' : ' c' '
Client Sample H):. AMW-6D Collection Date: 12/18/2012 14:02
Client ProjectiD: Former Pazivk Warehouse Received Date: 12/19/2012 09:10
Lab Sample ID: 31204038002-A Matrix: Water
Lab Project ID: 31204038
~-c .. ' ' -. ··~·---· " ....
· :Results by SW-846 82608
•. r _, • •• • r,· •·~ • []
Parameter Result Qual DL LOQ/CL Units DF Date Anal~zed
Dichlorodifluoromethane ND u 0.160 5.00 ug/L 12/21/2012 16:52
cis~1 ,3-Dichloropropene ND u 0.269 1.00 ug/L 12/21/2012 16:52
trans-1 ,3-Dichloropropene ND u 0.262 1.00 ug/L 12/21/2012 16:52 tJ
Diisopropyl Ether ND u 0.209 1.00 ug/L 12/21/2012 16:52
Ethyl Benzene ND u 0.251 1.00 ug/L 12/21/2012 16:52
Hexachlorobutadiene ND u 0.274 1.00 ug/L 12/21/2012 16:52
lsopropylbenzene (Cumene) ND u 0.286 1.00 ug/L 12/21/2012 16:52
Methyl iodide ND u 0.148 1.00 ug/L 12/21/2012 16:52
Methylene chloride ND u 0.161 5.00 ug/L 12/21/2012 16:52
Naphthalene ND u 0.217 1.00 ug/L 12/21/2012 16:52
Styrene ND u 0.224 1.00 ug/L 12/21/2012. 16:52
Tetrachloroethene ND u 0.264 1.00 ug/L 12/21/2012 16:52
Toluene ND u 0.195 1.00 ug/L 12/21/2012 16:52
Trichloroethene ND u 0.227 1.00 ug/L 12/21/2012 16:52
Trichlorofluoromethane ND u 0.139 1.00 ug/L 12/21/2012 16:52
Vinyl chloride ND u 0.189 1.00 ug/L 12/21/2012 16:52
Xylene (total) ND u 0.298 2.00 ug/L 12/21/2012 16:52 [:
cis-1 ,2-Dichloroethene ND u 0.299 1.00 ug/L 12/21/2012 16:52
m,p-Xylene ND u 0.280 2.00 ug/L 12/21/2012 16:52
n-Propylbenzene ND u 0.297 1.00 ug/L 12/21/2012 16:52
a-Xylene ND u 0 .. 298 1.00 ug/L 12/21/2012 16:52
sec-Butylbenzene ND u 0.241 1.00 ug/L 12/21/2012 16:52
tert-Butyl methyl ether (MTBE) ND u 0.200 1.00 ug/L 12/21/2012 16:52
tert~Butylbenzene ND u 0.293 1.00 ug/L 12/21/2012 16:52
trans-1 ,2-Dichloroethene ND u 0.213 1.00 ug/L 12/21/2012 16:52
trans-1 ,4-Dichloro-2-butene ND u 2.36 5.00 ug/L 12/21/2012 16:52
Surrogates
1 ,2-Dichloroethane-d4 108 64.0-140 % 12/21/2012 16:52
4-Bromofluorobenzene 103 85.0-115 % 12/21/2012 16:52
Toluene dB 107 82.0-117 % 12/21/2012 16:52
Batch Information
Analytical Batch: VMS2793 Prep Batch: VXX4458
Analytical Method: SW-84G 32608 Prep Method: SW-846 50308
Instrument: fl!iSDS Prep Date/Time: 1212112012 08:34
Analyst: BWS Prep Initial Wt.Nol.: 40 mL
Prep Extract Vol: 40 mL
Print Date: 0110312013 N.C. Certification t/. 481
Page 10 of 34
rl
n
A>tM.l"flA"l. f'TAA-"fiCJtVF)i
[] . Results of AMW-60
L.-";·: .• ,,
Client Sample ID: AMW-60 Collection Date: 12/18/2012 14:02
r-l
Client Project ID: Former Pazivk Warehouse Received Date: 12/19/2012 09:10
Lab Sample ID: 31204038002-D Matrix: Water
Lab Project ID; 31204038
ll ~. " "" .. ~ " ... ,_
(Results bySW-846 8~700 :.~ ( )
Parameter Result Qual DL LOQ/CL Units OF Date Anal~zed
[ i 1 ,2,4-Trichlorobenzene NO u 1.74 5.04 ug/L 12120/2012 20:58
1 ,2-Dichlorobenzene NO u 1.72 5.04 ug/L 12/20/2012 20:58
_! 1 ,3-Dichlorobenzene NO u 1.66 5.04 ug/L 12/20/2012 20:58
1 ,4-Dichlorobenzene NO u 1.64 5.04 ug/L 12/20/2012 20:58
r j 2,4-Dinitrotoluene ND u 1.85 5.04 ug/L 12/20/2012 20:58
2,6-Dinitrotoluene NO u 1.90 5.04 ug/L 12/20/2012 20:58
2-Chloronaphthalene NO u 2.02 5.04 ug/L 12/20/2012 20:58
2-Methylnaphthalene NO u 1.96 5.04 ug/L 12/20/2012 20:58
[ ~ 2-Nitroaniline NO u 1.70 5.04 ug/L 12/20/2012 20:58
3,3'-Dichlorobenzidine NO u 1.76 10.1 ug/L 12/20/2012 20:58
3-Nitroaniline NO u 1.66 25.2 ug/L 12/20/2012 20:58
l ~ 4~Chloroaniline NO u 1.90 25.2 ug/L 12/20/2012 20:58
4-Chlorophenyl phenyl ether NO u 2.48 5.04 ug/L 12/20/2012 20:58
Acenaphthene NO u 2.08 5.04 ug/L 12/20/2012 20:58
Acenaphthylene NO u 2.02 5.04 ug/L 12/20/2012 20:58
l -~ Anthracene NO u 1.95 5.04 ug/L 12/20/2012 20:58
Benzo(a)anthracene NO u 1.98 5.04 ug/L 12/20/2012 20:58
Benzo(a)pyrene NO u 1.88 5.04 ug/L 12/20/2012 20:58
[ ~ Benzo(b)fluoranthene NO u 1.98 5,04 ug/L 12/20/2012 20:58
Benzo(g,h,i)perylene NO u 2.17 5.04 ug/L 12/20/2012 20:58
Benzo(k)fluoranthene ND u 2,33 5.04 ug/L 12/20/2012 20:58
Bis(2-Chloroethoxy)methane ND u 2.14 5.04 ug/L 12/20/2012 20:58
[ : Bis(2-Chloroethyl)ether ND u 2.23 5.04 ug/L 12/20/2012 20:58
Bis(2-Chloroisopropyl)ether ND u 2.06 5.04 ug/L 12/20/2012 20:58
Bis(2-Ethylhexyl)phthalate ND u 1.97 5.04 ug/L 12/20/2012 20:58
4-Bromophenyl phenyl ether ND u 2.06 5.04 ug/L 12/20/2012 20:58
Butyl benzyl phthalate NO u 1.91 5.04 ug/L 12/20/2012 20:58
Chrysene NO u 2.22 5.04 ug/L 12/20/2012 20:58
Di-n-butyl phthalate ND u 1.93 5.04 ug/L 12/20/2012 20:58
Di-n-cetyl phthalate NO u 1.47 5.04 ug/L 12/20/2012 20:58
Dibenz(a,h)anthracene ND u 2.04 5.04 ug/L 12/20/2012 20:58
Dibenzofuran ND u 2.24 5.04 ug/L 12/20/2012 20:58
Diethyl phthalate ND u 2.12 5.04 ug/L 12/20/2012 20:58
l ' Dimethyl phthalate ND u 2.16 5.04 ug/L 12/20/2012 20:58
Diphenylamine ND u 2.04 5.04 ug/L 12/20/2012 20:58
Fluoranthene ND u 2.04 5.04 ug/L 12/20/2012 20:58
L Fluorene ND u 2.46 5.04 ug/L 12/20/2012 20:58
Hexachlorobenzene NO u 1.95 5.04 ug/L 12/20/2012 20:58
Hexachlorobutadiene NO u 1.53 5.04 ug/L 12/20/2012 20:58
Hexachlorocyclopentadiene ND u 0.794 10.1 ug/L 12/20/2012 20:58
ll Hexachloroethane ND u 1.41 5.04 ug/L 12/20/2012 20:58
lndeno(1 ,2,3-cd)pyrene ND u 2.04 5.04 ug/L 12/20/2012 20:58
lsophorone ND u 2.11 5.04 ug/L 12/20/2012 20:58
I
Print Date· 01/03!2013 N.C. Certification# {~81
. )
SGS .4nol)'1•·::c·l Pcrspcc;,·,·cs 5SOO t31Jsine~s Dr US · !ll405 · Wilmingion, I>JC t d 91035() 1903 If 1 910 350 t557 WWW.S<JS.>CO'm
I
l ' MI!Hiber uf tl-te SG-s Grt~JJP fSfiS S1\l
Page 11 of 34
[l
n
[l
fl l J
r J
f I
L J
f l,
.Results of AMW-60
Client Sample ID: AMW-60
Cl_ient Project ID: Former Pazivk Warehouse
Lab Sample ID: 31204038002-D
Lab Project ID: 31204038
Results by SW-846 82700
. ''?··,:·.·: -.. ~ < •• ' .1--
Parameter
Naphthalene
4-Nitroaniline
Nitrobenzene
Phenanthrene
Pyrene
n-Nitrosodi-n-propylamine
-Surrogates
2,4,6-Tribromophenol
2-Fiuorobiphenyl
2~Fiuorophenol
Nitrobenzene-d5
Phenol-d6
Terphenyl-d14
'Batch Information
Result
NO
NO
NO
NO
NO
NO
95.0
88.0
89.0
88.0
94.0
90.0
Analytical Batch: XMS1777
Analytical Method: SW-846 82700
Instrument: MSD6
Analyst: CMP
Print Date: 0110312013
Qual
u
u
u
u
u
u
DL
1.96
1.69
2.21
2.01
2.03
2.25
Collection Date: 12/18/2012 14:02
Received Date: 12/19/2012 09:10
Matrix: Water
LOQ/CL Units OF
5.04 ug/L 1
25.2 ug/L
5.04 ug/L
5.04 ug/L
5.04 ug/L
5.04 ug/L
29.3-152 %
50.0-107 %
33.1-118 %
46.0-118 %
49.0-120 %
22.1-142 %
Prep Batch: XXX3426
Prep Method: SW-846 3520C
Prep Date/Time: 121'19/2012 14:49
Prep Initial Wt.NoL: 992 mL
Prep Extract Vol: 5 mL
Date Analyzed
12/20/2012 20:58
12/20/2012 20:58
12/20/2012 20:58
12/20/2012 20:58
12/20/2012 20:58
12/20/2012 20:58
12/20/2012 20:58
12/20/2012 20:58
12/20/2012 20:58
12/20/2012 20:58
12/20/2012 20:58
12/20/2012 20:58
N C Certification II-481
SGS t.n.)lyi•:c•l PerspNtl\'(S 5WO Business Or. us-:1:34!)5. Wilmington. f~C ( tl 911)35(! 190:! r t 1 910 351) 1557 WWW.S{ISCOrn
Page 12 of 34
n
n
n
fj
ll ! ! -'
l-' '
' i
t :
! L ,
i A>!Ab'O>CAJ. r'VW'F.cmrn
' -., ... . ..
;Results of AMW-70 ~ ;F:,;.;;;_:;-.-:~. _,~ ~ '·-.,~--:-:-,;-.. ··· ··;__;·;::'
Client Sample ID: AMW-70
Client Project ID: Former Pazivk Warehouse
Lab Sample ID: 3120403800:3-8
Lab Project ID: 31204038
:R~;~~i~ -by 5iN-~846-s2sos
'·· ··. ·<:·:,,~ ~::::-'.;--:·,::··· ·.
Parameter
1,1, 1 ,2-Tetrachloroethane
1,1, 1-Trichloroethane
1,1 ,2,2-Tetrachloroethane
1,1 ,2-Trichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
1, 1-Dichloropropene
1 ,2,3-Trichlorobenzene
1 ,2,3-Trichloropropane
1 ,2,4-Trichlorobenzene
1 ,2,4-Trimethylbenzene
1 ,2-Dibromo-3-chloropropane
1 ,2-Dibromoethane
1 ,2-Dichlorobenzene
1 ,2-Dichloroethane
1 ,2-Dichloropropane
1 ,3,5-Trimethylbenzene
1 ,3-Dichlorobentene
1 ,3-Dichloropropane
1 A-Dichlorobenzene
2,2-Dichloropropane
2-Butanone
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-lsopropyltoluene
4-Methyl-2-pentanone
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
Print Date: 01/03/2013
Result
No
NO
NO
NO
3.44
18;1
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
Qual
u
u
u
u
J
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
DL
1.42
0.820
1.16
1.18
0.860
1.15
0.812
1.43
1.68
0.808
1.22
7.52
1.38
1.19
1.18
0.644
1.10
1.30
1.28
1.85
0.956
6.12
1.20
4.96
1.68
0.812
5.12
5.64
0.624
1.17
0.876
1.46
1.98
0.672
0.732
0.436
1.08
1.08
0.860
0.736
0.528
1.53
1.54
Collection Date: 12/18/2012 11 :40
Rec:eived Date: 12/19/2012 09:10
Matrix:· Water
LOQ/CL
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
20.0
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
100
4.00
20.0
4.00
4.00
20.0
100
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
OF
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
Date Analyzed
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/2412012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
N.C Cer\il'icaiioll # 481
SGS ;. n;Jiy1i; Bl Perspct~•Yes SSGO Business Dr. US · £ll•1j)5 ·Wilmington, NC t 11 910 350 19tH f t 1 910 3501557 www.Si)s tom
Page 13 of 34
fl
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;Results of AMW-70
• ~.:~·:·.~ ~;-.~~·"-?,:,·:~'.:I·'.:-~:~'-. -':~--:,:;::t;>.-£ · ·-·,·::'
Client Sample ID: AMW-70
Client Project 10: Form~r Pazivk Warehouse
Lab Sample ID: 31204038003~8
Lab Project !D: 31204038
Parameter Result
Dichlorodifluoromethane NO
cis~ 1 ,3-Dichloropropene NO
trans-1 ,3-Dichloropropene NO
Diisopropyl Ether NO
Ethyl Benzene NO
Hexachlorcibutadiene NO
lsopropylbenzene (Cumene) NO
Methyl iodide NO
Methylene chloride NO
Naphthalene NO
Styrene NO
Tetrachloroethene 360
Toluene NO
Trichloroethene 1220
Trichlorofluoromethane NO
Vinyl chloride 42.7
Xylene (total) NO
cis-1 ,2-Dichloroethene 4250
m,p-Xylene NO
n-Propylbenzene NO
a-Xylene NO
sec-Butyl benzene NO
tert-Butyl methyl ether (MTBE) NO
tert-Butylbenzene NO
trans-1 ,2-Dichloroethene 56.4
trans-1 ,4-Dichloro-2-butene NO
Surrogates
1 ,2-Dichloroethane-d4 104
4-Bromofluorobenzene 95.0
Toluene d8 99.0
Print Date: O·!i0312013
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
--,
:~.------------..,...---------------"""
DL
0.640
1.08
1.05
0.836
1.00
1.10
1.14
0.592
0.644
0.868
0.896
52.8
0.780
45.4
0.556
0.756
1.19
59.8
. 1.12
1.19
1.19
0.964
0.800
1.17
0.852
9.44
Collection Date: 12/18/2012 11 :40
Received Date: 12/19/2012 09:10
-Matrix: • Water
LOQ/CL Units OF
20.0 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
20.0 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
200 ug/L 200
4.00 ug/L 4
200 ug/L 200
4.00 ug/L 4
4.00 ug/L 4
8.00 ug/L 4
200 ug/L 200
8.00 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
4.00 ug/L 4
20.0 ug/L 4
64.0-140 % 4
85.0-115 % 4
82.0-117 % 4
Date Anal~zed
12/24/2012 18:56
12/24/2012 .18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/21/2012 18:55
12/24/2012 18:56
12/21/2012 18:55
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/21/2012 18:55
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
12/24/2012 18:56
N.C. Certification# 481
SGS Anol·f1•·~31 rerspect•ves SSt}OBDsinn:ss Dr. US 28405 ·Wilmington, NC t l1 !l10J5-0 1903 f + 1 911) 350 1557 www.sr;scom
Mom!><! uflh• SGS Gruup ISG-S St\1
Page 14 of 34
n
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lj
[ ~
;Results of AMW-70
. . ':_: :~-~.'·"' ':"; .. ~;:! ~.'. -' . -· ~ :'.:~·; :-:_· ;:--;': ." "' .' ;.~:·' ;:,'·'·;. ·:j -~ ~;. ........ ,.; ·::_:.:') .; <;·',',:.' • ' • • -.
Client Sample ID: AMW-70
Client Project Jb: Former Pazivk Warehouse
Lab Sample ID: 31204038003-B
Lab ProjectiD: 31204038
rResults by SW-84Gs26o8'
'• ·~' ',}' : '. :,"."• • .. ·. ··, :.' ._.,..,_.: ",~_,._ :·: ::.· · ... ·. -. -..
Parameter
'Batch Information
Analytical Batch: VMS2793
Analytical Method: SW-846 82608
Instrument: MSD8
Analyst: BWS
Analytical Batch: VMS2794
Analytical Method: SW-846 82608
lnstrume1it: MSD8
Analyst: BWS
Print Date· 01!03i20B
Collection Date: 12/18/2012 11:40
Received Date: 12/19/2012 09:10
Matrix: Water
Prep Batch: VXX4458
Prep Method: SW-846 50308
Prep Date/Time: 12/21/2012 08:34
Prep Initial WUVol.: 40 mL
Prep Extract Vol: 40 mL
Prep Batch: VXX4463
Prep Method: SW-846 50308
Prep Date/Time: 12/24/2012 11:58
Prep Initial Wt.Nol.: 40 ml
Prep Extract Vol: 40 ml
Date Analyzed
N.C Certification# 481
SGS A nolyl:~ 31 Perspectives S':iOtlBusinccss Or. US· M4Q!) · Wiimin910n, tJC t 11 910J5{J 19tH f tl 910 350 1557 www.~s cr:rrn
Page 15 of 34
ll
I i l J
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!Result~ ~fAMw-7o
I. y~, ·'" ''"" i'"·~·''" ....
Client Sample ID: AMW-70
Client Project I b: Former Pazivk Warehouse
Lab Sample ID: 31204038003-D
Lab Project ID: 31204038
.. -,.-,·-···~--... , , .. ~~----
:Results by SW-846 82700 .. _, .. ·.· .• _., .. -.~---·:.:· ._: ;>:' ·::: :· {-. ~-. :::;; :· ; ·" :; . ,. ~--·}· \'' .::.~:-··' • ,. ' ··' ~
Parameter
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Methylnaphthalene
2-Nitroaniline
3,3'-Dichlorobenzidine
3-Nitroaniline
4-Chloroaniline
4-Chlorophenyl phenyl ether
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Bis(2-Chloroethoxy)methane
Bis(2-Chloroethyl)ether
Bis(2-Chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Chrysene
Di-n-butyl phthalate
Di-n-octyl phthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
Diphenylamine
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1 ,2,3-cd)pyrene
lsophorone
Print Date: 01/0312013
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
36.3
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
DL
1.77
1.75
1.69
1.67
1.88
1.92
2.05
1.99
1.73
1.79
1.69
1.92
2.52
2.11
2.05
1.98
2.0.1
1.90
2.01
2.20
2.36
2.17
2.26
2.09
2.00
2.09
1.93
2.25
1.95
1.49
2.07
2.27
2.15
2.19
2.07
2.07
2.50
1.98
1.56
0.807
1.43
2.07
2.14
Collection Date: 12/18/2012 11:40
R.eceived Date: 12/19/2012 09:10
Matrix: • Water
LOQ/CL Units DF
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
10.2 ug/L
25.6 ug/L
25.6 ug/L
5.12 ug/L
5.12 ug/L
5;12 ug/L
5:12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
10.2 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
Date Anal~zed
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 .19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/20.13 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013'19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
N.C Certification# 48i
SGS Analyl•.:-61 Perspec-1ives SSOO flusin~:ss Or. US· £W!l}5 · Wilmiogloo, NC t +1 91035{! 1903 f tl 910 3501557 www.S{lHI)fO
Page 16 of 34
[1
n
n
n
fj
!R~sults of AMW-70
"'i~~:-, ,;C-~ ·)-,<"~)(:?:-·-,,· .:-:-:y, '' ·
Client Sample 10: AMW-70
Cl.ient Project 10: Former Pazivk Warehouse
Lab Sample 10: 31204038003"0
Lab Project ID: 31204038
, Results by SW-846 82700
t·:~.r· ·: ;;-c:.--·F·,;_,;·.· :,~ ";• .
Parameter Result
Naphthalene ND
4-Nitroaniline ND
Nitrobenzene ND
Phenanthrene ND
Pyrene ND
n-Nitrosodi-n-propylamine ND
Surrogates
2,4,6-Tribromophenol 120
2-Fiuorobiphenyl 95.0
2-Fiuorophenol 78.0
Nitrobenzene-d5 90.0
Phenol-dB 96.0
Terphenyl-d 14 97.0
Analytical Batch: XMS1781
Analytical Method: SW-846 82700
Instrument: IVISD6
Analyst CMP
Print Date: 0"!/031201.3
;.~
Qual DL
u 1.99
u 1.72
u 2.24
u 2.04
u 2.06
u 2.28
Collection Date: 12/18/2012 11 :40
Received Date: 12/19/20.12 09:10
Matrix: Water
LOQ/CL Units DF
5.12 ug/L
25.6 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
5.12 ug/L
29.3-152 %
50.0-107 %
33.1-118 %
46.0-118 %
49.0-120 %
22.1-142 %
Prep Batch: XXX3426
Prep Method: SW-846 3520C
Prep Date/Time: 12/19/2012 14:49
Prep Initial WtNoL: 977 mL
Prep Extract Vol: 5 mL
Date Analyzed
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
01/2/2013 19:58
N.C. Ceriific<Jtion 11481
SGS 1\nalytr::;;l Perspec<•YC' SSQO Su~inm Or. US· 2"l}ll1!5 ·Wilmington, t4C t [phone] f tl 910 350 155? www.s-i)s.com
Page 17 of 34
ll l J
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f '
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ANII.Il"'m~~ "-t"Y<JVP
':;:~:::;~;;~~,, ,,, " • AM~: Collection Date: 12/18/2012 10:50
Client Project ID:~Warehouse Received Date: 12/19/2012 09:10
Lab Sample ID: 31204038004-A Matrix: Water
Lab Project ID: 31204038
••·v~···•-"""""""" -•
Parameter Result Qual DL LOQ/CL Units DF Date Anal~zed
1,1, 1 ,2-Tetrachloroethane ND u 0.355 1.00 ug/L 12/21/2012 17:17
1,1, 1-Trichloroethane ND u 0.205 1.00 ug/L 12/21/2012 17:17
1,1 ,2,2-Tetrachloroethane ND u 0.289 1.00 ug/L 12/21/2012 17:17
1,1 ,2-Trichloroethane ND u 0.295 1.00 ug/L 12/21/2012 17:17
1 , 1-Dichloroethane ND u 0.215 1.00 ug/L 12/21/2012 17:17
1 , 1-Dichloroethene ND u 0.288 1.00 ug/L 12/21/2012 17:17
1 , 1-Dichloropropene ND u 0.203 1.00 ug/L 12/21/2012 17:17
1 ,2,3-Trichlorobenzene ND u 0.358 1.00 ug/L 12/21/2012 17:17
1 ,2,3-Trichloropropane ND u 0.421 1.00 ug/L 12/21/2012 17:17
1 ,2,4-Trichlorobenzene ND u 0.202 1.00 ug/L 12/21/2012 17:17
1 ,2,4-Trimethylbenzene ND u 0.306 1.00 ug/L 12/21/2012 17:17
1 ,2-Dibromo-3-chloropropane ND u 1.88 5.00 ug/L 12/21/2012 17:17
1 ,2-Dibromoethane ND u 0.344 1.00 ug/L 12/21/20.12 17:17
1 ,2-Dichlorobenzene ND u 0.298 1.00 ug/L 12/21/2012 17:17
1 ,2-Dichloroethane ND u 0.296 1.00 ug/L 12/21/2012 17:17
1 ,2-Dichloropropane ND u 0.161 1.00 ug/L 12/21/2012 17:17
1 ,3,5-Trimethylbenzene ND u 0.275 1.00 ug/L 12/21/2012 17:17
1 ,3-Dichlorobenzene ND u 0.324 1.00 ug/L 12/21/2012 17:17
1 ,3-Dichloropropane ND u 0.320 1.00 ug/L 12/21/2012 17:17
1 A-Dichlorobenzene ND u 0.463 1.00 ug/L 12/21/2012 17:17
2,2-Dichloropropane ND u 0.239 1.00 ug/L 12/21/2012 17:17
2-Butanone ND u 1.53 25.0 ug/L 12/21/2012 17:17
2-Chlorotoluetie ND u 0.299 1.00 ug/L 12/21/2012 17:17
2-Hexanone ND u 1.24 5.00 ug/L 12/21/2012 17:17
4-Chlorotoluene ND u 0.421 1.00 ug/L 12/21/2012 17:17
4-lsopropyltoluene ND u 0.203 1.00 ug/L 12/21/2012 17:17
4-Methyl-2cpentanone ND u 1.28 5.00 ug/L 12/21/2012 17:17
Acetone ND u 1.41 25.0 ug/L 12/21/2012 17:17
Benzene ND u 0.156 1.00 ug/L 12/21/2012 17:17
Bromobenzene ND u 0.293 1.00 ug/L 12/21/2012 17:17
Bromochloromethane ND u 0.219 1.00 ug/L 12/21/2012 17:17
Bromodichloromethane ND u 0.364 1.00 ug/L 12/21/2012 17:17
Bromoform ND u 0.496 1.00 ug/L 12/21/2012 17:17
Bromomethane ND u 0.168 1.00 ug/L 12/21/2012 17:17
n-Butylbenzene ND u 0.183 1.00 ug/L 12/21/2012 17:17
Carbon disulfide ND u 0.109 1.00 ug/L 12/21/2012 17:17
Carbon tetrachloride ND u 0.270 1.00 ug/L 12/21/2012 17:17
Chlorobenzene ND u 0.269 1.00 ug/L 12/21/2012 17:17
Chloroethane ND u 0.215 1.00 ug/L 12/21/2012 17:17
Chloroform ND u 0.184 1.00 ug/L 12/21/2012 17:17
Chloromethane NO u 0.132 1.00 ug/L 12/21/2012 17:17
Dibromochloromethane NO u 0.383 1.00 ug/L 12/21/2012 17:17
Dibromomethane NO u 0.386 1.00 ug/L 12/21/2012 17:17
Prin! Dale: 011031201.3 N.C Certification iJ. 481
SGS Aoalylr(ol PerspNti\'CS 'SSOOilusiocss Dr. LIS· t'M05 ·Wilmington, NC t 1·1 910350 i903 f + 1910 350 1557 www.fi'JS ~crm
Page 18 of 34
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)R~sults of AMW-Illd' f . l'"""==',....::;-~~:H?-----------~------""" '~li~~;~~~p·l~· I~; ~)1;1\:.{'t:J :· ·~'?
Client Project ID: Former Pazivk Warehouse
Lab Sample ID: 31204038004-A
Lab Project ID: 31204038
Parameter
Dichlorodifluoromethane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Diisopropyl Ether
Ethyl Benzene
Hexachlorobutadiene
lsopropylbenzene (Cumene)
Methyl iodide
Methylene chloride
Naphthalene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylene (total)
cis-1 ,2-Dichlciroethene
m,p7Xylene
n-Propylbenzene
a-Xylene
sec-Butylbenzehe
tert-Butyl methyl ether (MTBE)
tert-Butylbenzene
trans-1 ,2-Dichloroethene
trans-1 ,4-Dichloro-2-butene
Surrogates
1 ,2-Dichloroethane-d4
4-Bromofluorobenzene
Toluene d8
'Batch Information
Analytical Batch: VMS2793
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.85
ND
ND
ND
ND
ND
ND
ND
ND
102
97.0
104
Analytical Method: SW-846 82608
Instrument: MSDS
Analyst: BWS
Print Date: 0110312013
Qual DL
u 0.160
u 0.269
u 0.262
u 0.209
u 0.251
u 0.274
u 0.286
u 0.148
u 0.161
u 0.217
u 0.224
u 0.264
u 0.195
u 0.227
u 0.139
u 0.189
u 0:298
0.299
u 0.280
u 0.297
u 0.298
u 0.241
u 0.200
u 0.293
u 0.213
u 2.36
Collection Date: 12/18/2012 10:50
Received Date: 12/19/2012 09:10
Matrix: ··Water
LOQ/CL Units DF
5.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
5.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
2.00 ug/L
1.00 ug/L
2.00 ug/L
1;00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
5.00 ug/L
64.0-140 %
85.0-115 %
82.0-117 %
Prep Batch: VXX4458
Prep Method: SW-846 50308
Prep Date/Time: 1212112012 08:34
Prep Initial Wt.Nol.: 40 ml
Prep Extract Vol: 40 mL
Date Analyzed
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
12/21/2012 17:17
i'l.C Certii'ication # 481
SGS i'•O;Jiy1··:31 Perspc~'"·cs SSOO Business Dr. US· ;?.1}4()5 ·Wilmington. NC l +1 910:15{1 1903 f t 1 910 350 1557 www.Sf,Js~om
Page 19 of 34
[J
rl
l J
ll I ,
l J
r l
I
l '
r ,
I
' l '
r l
r,
l
r
l '
l.
'~;!§~~~:~·f&~'M«tJ·:is
Client Project ID: Former Pazivk Warehouse
lab Sample ID:. 31204038004-D
Lab Project ID: 3.1204038
Parameter
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4~Dichlorobenzene
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2~Ciiloronaphthalene
2-Methylnaphthalene
2-Nitroaniline
3,3'-Dichlorobenzidine
3-Nitroaniline
4-Chloroaniline
4-Chlorophehyl phenyl ether
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Bis(2-Chloroeihoxy)methane
Bis(2-Chloroethyl)ether
Bis(2-Chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Chrysene
Di-n-butyl phthalate
Di-n-octyl phthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
Diphenylamine
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1 ,2,3-cd)pyrene
lsophorone
Print Date: 01l03120'13
Result
NO
NO
NO
NO
NO
ND
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
ND
NO
NO
NO
NO
ND
NO
ND
ND
ND
ND
NO
ND
NO
ND
NO
ND
ND
NO
NO
ND
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
DL
1.76
1.74
1.68
1.66
1.87
1.91
2.03
1.97
1.72
1.78
1.68
1.91
2.50
2.10
2.03
1.96
1.99
1.89
1.99
2.19
2.35
2.16
2.25
2.08
1.98
2.08
1.92
2.24
1.94
1.49
2.05
2.26
2.14
2.18
2.05
2.05
2.48
1.96
1.55
0.802
1.42
2.05
2.13
Collection Date: 12/18/2012 10:50
Received Date: 12/19/2012 09:10 . . . .
Matrix: Water
LOQ/CL
5.09
5.09
5.09
5.09.
5.09
5.09
5.09
5.09
5.09
10.2
25.4
25.4
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
5.09
10.2
5.09
5.09
5.09
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Date Analyzed
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21 :24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21 :24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21 :24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21 :24
12/20/2012 21 :24
12/20/2012 21 :24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21 :24
12/20/2012 21 :24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21 :24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
N.C. c~:rtificcttion # 481
SGS AnalyK31 PerspN\ivcs SSW 6l•SiM~S Or. US· lMiJ5 ·Wilmington. NC t t1 910J50 1903 f tl 910 350 1557 IWiw.~swm
Page 20 of 34
n
n
r1 ... l j
rJ
lJ
[ ]
[:
r I l)
r •
l )
~\11· ;Res~lts~f AMw-~7 ······ ·· · ·· · ··· ';j'~~"""""'-4------------------~------
·~;i;~t~;~;~·~·;~"~ '~:2fJs='
Client Project ID: Former Pazivk Warehouse
Lab Sample ID: 31204038004-D
Lab Project ID: 31204038
;;-··--
;Results by SW-846 82700
<,., •• <, ~.;,~;::-:·.;,·. ;·:;-~::. ·-·\·/';~'.;·.· ·:-:<' .• ,;::<·.
Parameter Result
Naphthalene ND
4-Nitroaniline NO
Nitrobenzene NO
Phenanthrene ND
Pyrene NO
n-Nitrosodi-n-propylamine ND
2,4,6-Tribromophenol 96.0
2-Fiuorobiphenyl 95.0
2-Fiuorophenol 88.0
Nitrobeilzene-d5 89.0
Phenol-d6 92.0
Terphenyl-d14 62.0
Analytical Batch: XMS1777
Analytical Method: SW-846 82700
Instrument: MSD6
Analyst: CMP
Print Date: 01103;2013
DL
1.97
u 1.71
u 2.23
u 2.02
u 2.04
u 2.27
Collection Date: 12/18/2012 10:50
Received Date: 12/19/2012 09:10
Matrix: .Water
Units DF
5.09 ug/L
25.4 ug/L
5.09 ug/L
5.09 ug/L
5.09 ug/L
5.09 ug/L
29.3-152 %
50.0-107 %
33.1-118 %
46.0-118 %
49.0-120 %
22.1-142 %
Prep Bati::h: XXX3426
Prep Method: SW-846 3520C
Prep Date/Time: 12119/2012 14:49
Prep Initial Wt./Vol.: 983 mL
Prep Extract Vol: 5 mL
Date Anal~zed
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
12/20/2012 21:24
N.C. Ce1tification # ·181
SGS ,';nJI\'1'cal Perspcct,\·cs SS(}llSusinoss Dr. US· ii.B405 · Wilmillgton, NC t+1910.3SQ1903 f ~1910 3501557 www.sgscowt
Page 21 of 34
n
n !\.WJ.nt(W. ~!Wffil£--
n fResJit~ of AMW-90
···::~:;;.)-7;\:~·.:.,-;.-\~':';t'-.1'':·:. :'·: -. .-. ·.··--'~:· .. :_:; ::
( ) Client Sample ID: AMW-90 Collection Date: 12/18/2012 15:25
[]
Client Project ID: Former Pazivk Warehouse Received Date: 12/19/2012 09:10
Lab Sample ID: 31204038005-A Matrix: • Water
Lab Project ID: 31204038
lJ
f"""'""r• • .... , ... ,. __ . ____ ,_.,.,. ___ ,. . .. -----... ·--~-"
)Results by SW-846 82608
-~i>Y~:-;c•·-,:~-:-;.•-::::;.:.;· /: ·.·.·.: :-;. ~~:·::-.--~:--;~ ·.;::,-.,-:-
Parameter Result Qual DL LOQ/CL Units DF Date Analyzed
1,1, 1 ,2-Tetrachloroethane ND u 0.355 1.00 ug/L 12/21/2012 17:42
l J
1,1, 1-Trichloroethane ND u 0.205 1.00 ug/L 12/21/2012 17:42
1,1 ,2,2~ Tetrachloroethane ND u 0.289 1.00 ug/L 12/21/2012 17:42
1,1 ,2-Trichloroethane ND u 0.295 1.00 ug/L 12/21/2012 17:42
f J
1 , 1-Dichloroethane ND u 0.215 1.00 ug/L 12/21/2012 17:42
1, 1-Dichloroethene ND u 0.288 1.00 ug/L 12/21/2012 17:42
1, 1-Dichloropropene ND u 0.203 1.00 ug/L 12/21/2012 17:42
1 ,2,3-Trichlorobenzene ND u 0.358 1.00 ug/L 12/21/2012 17:42
l~ 1 ,2,3-Trichloropropane ND u 0.421 1.00 ug/L 12/21/2012 17:42
1 ,2,4-Trichlorobenzene ND u 0.202 1.00 ug/L 12/21/2012 17:42
1 ,2,4-Trimethylbenzene 7.70 0.306 1.00 ug/L 12/21/2012 17:42
r ~ 1 ,2-Dibromo-3-chloropropane ND u 1.88 5.00 ug/L 12/21/2012 17:42
1 ,2-Dibromoethane ND u 0.344 1.00 ug/L 12/21/2012 17:42
1 ,2-Dichlorobenzene ND u 0.298 1.00 ug/L 12/21/2012 17:42
1 ,2-Dichloroettiane ND u 0.296 1.00 ug/L 12/21/2012 17:42
l' 1 ,2-Dichloropropane ND u 0.161 1.00 ug/L 12/21/2012 17:42
1 ,3,5-Trimethylbenzene 3.31 0.275 1.00 ug/L 12/21/2012 17:42
1 ,3-Dichlorobenzene ND u 0.324 1.00 ug/L 12i21/2012 17:42
1 ,3-Dichloropropane ND u 0.320 1.00 ug/L 12/21i2012 17:42
[ 1 1 ,4-Dichiorobenzene ND u 0.463 1.00 ug/L 12/21/2012 17:42
2,2-Dichloropropane ND u 0.239 1.00 ug/L 12/21/2012 17:42
2-Butanone ND u 1.5.3 25.0 ug/L 12/21/2012 17:42
[ 1
2-Chlorotoluene ND u 0.299 1.00 ug/L 12/21/2012 17:42
2-Hexanone ND u 1.24 5.00 ug/L 12/21/2012 17:42
4-Chlorotoluene ND u 0.421 1.00 ug/L 12/21/2012 17:42
4-lsopropyltoluene 0.240 J 0.203 1.00 ug/L 12/21/2012 17:42
4-Methyl-2-pentanone ND u 1.28 5.00 ug/L 12/21/2012 17:42
Acetone ND u 1.41 25.0 ug/L 12/21/2012 17:42
Benzene ND u 0.156 1.00 ug/L 12/21/2012 17:42
Bromobenzene ND u 0.293 1.00 ug/L 12/21/2012 17:42
Bromochloromethane ND u 0.219 1.00 ug/L 12/21/2012 17:42
Bromodichloromethane ND u 0.364 1.00 ug/L 12/21/2012 17:42
Bromoform ND u 0.496 1.00 ug/L 12/21/2012 17:42
r Bromomethane ND u 0.168 1.00 ug/L 12/21/2012 17:42
l j
n-Butylbenzene ND u 0.183 1.00 ug/L 12/21/2012 17:42
Carbon disulfide ND u 0.109 1.00 ug/L 12/21/2012 17:42
Carbon tetrachloride ND u 0.270 1.00 ug/L 12/21/2012 17:42
l : Chlorobenzene ND u 0.269 1.00 ug/L 12/21/2012 17:42
Chloroethane ND u 0.215 1.00 ug/L 12/21/2012 17:42
Chloroform ND u 0.184 1.00 ug/L 12/21/2012 17:42 l ' Chloromethane ND u 0.132 1.00 ug/L 12/21/2012 17:42
Dibromochloromethane ND u 0.383 1.00 ug/L 12/21/2012 17:42
Dibromomethane ND u 0.386 1.00 ug/L 12/21/2012 17:42
l ~ Print Date: 0110ai2013 N.C. Ce:tification # 481
SGS An;;ly1<C:31 Perspew•cs SSOO :f31Jsin~ss Or. US · :tJMtl5 · Wilmington. NC ( !1911}35(!1903 I+ 1 910 350 1557 www.sgscarn
l J
M<mb<t uf to• SGS Gro1w fSliS SJ\1
Page 22 of34
I I : I l j
r l
l J
ll : I l )
r 1
i ' )
r ,
! '
i j
L /
'Results of AMW-90
Client Sample 10: AMW-90
Client Project 10: Former Pazivk Warehouse
Lab S~mple ID: 3120403800o~A
Lab Project ID: 31204038
Parameter
Dichlorodifluoromethane
cis-1 ,3-Dichloropropene
trans-1 ,3"Dichloropropene
Diisopropyl Ether
Ethyl Benzene
Hexachlorobutadiene
lsopropylbenzene (Cumene)
Methyl iodide
Methylene chloride
Naphthalene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylene (total)
cis-1 ,2-Dichloroethene
m,p-Xylene
n-Propylbenzene
o-Xylehe
sec-Butylbenzene
tert-Butyl methyl ether (MTBE)
tert-Butylbenzene
trans-1 ,2-Dichloroethene
trans-1 ,4-Dichloro-2-butene
Surrogates
1 ,2-Dichloroethane-d4
4-Bromofluorobenzene
Toluene d8
:Batch Information
(:,··.· ···: .. ··:-~·, .....
Result
NO
NO
NO
NO
1.57
NO
2.12
NO
NO
3.41
NO
NO
NO
NO
NO
2.15
1.12
1.23
0.840
1.05
NO
0.700
NO
NO
NO
NO
106
97.0
106
Analytical Batch: VMS2793
Analytical Method: SW-846 82608
Instrument: MSDS
Analyst: BWS
Print Date: 01/03.'201'3
Qual
u
u
DL
0.160
0.269
u 0.262
u 0.209
u
0.251
0.274
0.286
u 0.148
u 0.161
0.217
u 0.224
u 0.264
u 0.195
u 0.227
u 0.139
0.189
J 0.298
0.299
J 0.280
0.297
u 0.298
J 0.241
u 0.200
u 0.293
u 0.213
u 2.36
Collection Date: 12/18/2012 15:25
Received Date: 12/19/2012 09:10
Matrix: . Water
LOQ/CL Units OF
5.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
5.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
2.00 ug/L
1.00 ug/L
2.00 ugtL
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
5.00 ug/L
64.0-140 %
85.0-115 %
82.0-117 %
Prep Batch: VXX4458
Prep Method: SW-846 50308
Prep Dale/Time: 12/21/2012 08:34
Prep Initial Wt.Nol.: 4·0 ml
Prep Extract Vol: 4.0 mL
Date Analyzed
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/2012 17:42
12/21/201~ 17:42
12/21/2012 17:42
N.C Ceriification # 481
SGS ,\oal)'\;c;;l Perspwi\'es SSOO ilusiness Or. US· :nNil5 · Wilmillgton. NC t * 1 911)35\l 1903 f 11 910 350 1557 www.sgscam
Page 23 of34
(
n
n
ll l J
t ~
I
(_'
f
('
:Results of AMW-90
Client Sample ID: AMW-90
Client Project ID: ForiJler Pazivk Warehouse
Lab Sample ID: 31204038005-b
Lab Project ID: 31204038
(Results by sw.846.827oo. ·
! .. ,:~:-; ;-;',-:' ).;:<·,;·:;>:.·:;:':-:·:·\'0•;: .;;, :C •_::(.,;;~:' .'_:'oj.;::.:<'";~ -:;;···:-( :
Parameter Result
1 ,2,4-Trichlorobenzene NO
1 ,2-Dichlorobenzene ND
1 ,3-Dichlorobenzene ND
1 A-Dichlorobenzene ND
2,4-Dinitrotoluene ND
2,6-Dinitrotoluene ND
2-Chloronaphthalene ND
2-Methylnaphthalene ND
2-Nitroaniline ND
3,3'-Dichlorobenzidirie ND
3-Nitroaniline ND
4-Chloroaniline ND
4-Chlorophenyl phenyl ether ND
Acenaphthene ND
Acenaphthylene ND
Anthracene ND
Benzo(a)anthracene ND
Benzo(a)pyrene ND
Benzo(b)fluoranthene NO
Berizo(g,h,i)perylene ND
BeriZo(k)fluoranthene ND
Bis(2-Chloroethoxy)methane ND
Bis(2-Chloroethyl)ether ND
Bis(2-Chloroisopropyl)ether ND
Bis(2-Ethylhexyl)phthalate 4.67
4-Bromophenyl phenyl ether ND
Butyl benzyl phthalate ND
Chrysene ND
Di-n-butyl phthalate ND
Di-n-octyl phthalate ND
Dibenz(a,h)anthracene ND
Dibenzofuran ND
Diethyl phthalate ND
Dimethyl phthalate ND
Diphenylamine ND
Fluoranthene ND
Fluorene ND
Hexachlorobenzene ND
Hexachlorobutadiene ND
Hexachlorocyclopentadiene ND
Hexachloroethane ND
lndeno(1 ,2,3-cd)pyrene ND
lsophorone ND
Print Dale: 0'110312013
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
J
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
DL
1.74
1.72
1.66
1.64
1.85
1.89
2.01
1.95
1:70
1.76
1.66
1.89
2.47
2.07
2.01
1.94
1.97
1.87
1.97
2.16
2.32
2.13
2.22
2.05
1.96
2.05
1.90
2.21
1.92
1.47
2.03
2.23
2.11
2.15
2.03
2.03
2.45
1.94
1.53
0.792
1.41
2.03
2.10
Collection Date: 12/18/2012 15:25
Received Date: 12/19/2012 09:10
Matrix: . Water
LOQ/CL
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
10.1
25.1
25.1
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
5.03
10.1
5.03
5.03
5.03
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugtL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DF
1
Date Analyzed
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/2Q/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
N.C. Ce11ificalion # 481
SGS Anol)'1ical Perspenives SSOO 8usinoss Or. US· ZJ14(J5 · Wilf1liilgton, NC l 11 91035<11903 It 1 910 350 1557 www.s>gs ~om
Page 24 of 34
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Client Sample ID: AMW-90
Client Project ID: Former Pazivk Warehouse
Lab Sample ID: 31204038005~D
Lab Project ID: 31204038
Parameter
Naphthalene
4-Nitroaniline
Nitrobenzene
Phenanthrene
Pyrene
n-Nitrosodi-n-propylamine
Surrogates
2,4,6-Tribromophenol
2-Fiuorobiphenyl
2-Fiuorophenol
Nitrobenzene-d5
Phenol-d6
Terphenyl-d14
,Batch Information
Result
2,41
ND
NO
ND
NO
NO
104
90.0
91.0
88.0
93.0
82.0
Analytical Batch: XMS1777
Analytical Method: SW-846 8270D
Instrument: MSDG
Analyst: CMP
Qual
J
u
u
u
u
u
DL
1.95
1.69
2.20
2.00
2.02
2.24
Collection Date: 12/18/2012 15:25
Received Date: 12/19/2012 09:10
Matrix: Water
LOQ/CL Units OF
5.03 ug/L 1
25.1 ug/L
5,03 ug/L
5:03 ug/L
5.03 ug/L
5.03 ug/L
29.3-152 %
50.0-107 %
33.1-118 %
46.0~118 %
49.0-120 %
22.1-142 %
Prep Batch: XXX3426
Prep Method: SW-846 3520C
Prep Date/Time: 12/19/2012 14:49
Prep Initial Wt./Vol.: 995 mL
Prep Extract Vol: 5 mL
Date Analyzed
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
12/20/2012 21:47
N.C Certification# 48i
SGS AnJiylrr.al Perspectives SSilllBu~<infrSS Dr. LIS ·lMt:!!> · Wilmillgion, NC l tl 910Jrl{! 1903 f f 1 910 350 1557 IWIW.SfJS com
Page 25 of 34
[]
[j
!Results of AMW-130
Client Sample ID: AMW-130
Client Project ID: Former Pazivk Warehouse
Lab Sample ID: 31204038006-B
Lab Pmject ID: 31204038
;R.esults by sw~84s 826or3
• ',...;"':.'1:<';.-;':c: ~~-~· .-;_'.$ \;'-:-" <· • ·'\\''
Parameter
1,1, 1 ,2-Tetrachloroethane
1,1, 1-Trichloroethane
1,1 ,2,2-Tetrachloroethane
1,1 ,2-Trichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
1, 1-Dichloropropene
1 ,2,3-Trichlorobenzene
1 ,2,3-Trichloropropane
1 ,2,4-Trichlorobenzene
1 ,2,4-Trimethylbenzene
1 .2~Dibromo-3-chloropropane
1 ,2~Dibromoethane
1 ,2-Dichlorobenzene
1 ,2-Dichloroethahe
1 ,2-Dichloropropane
1 ,3,5-Trimethylbenzene
1 ,3-Dichlorobenzene
1 ,3-Dichloropropane
1 A-Dichlorobenzene
2,2"Dichloropropane
2-Butanone
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-lsopropyltoluene
4-Methyl-2-pentanone
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
Print Date: 01!0:312013
Result
ND
ND
ND
ND
ND
19.4
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
18.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
2.56
ND
ND
ND
ND
ND
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
J
u
u
u
u
u
DL
2.84
1.64
2.31
2.36
1.72
2.30
1.62
2.86
3.37
1.62
2.45
15.0
2.75
2.38
2.37
1.29
2.20
2.59
2.56
3.70
1.91
12.2
2;39
9.92
3.37
1.62
10.2
11.3
1.25
2.34
1.75
2.91
3.97
1.34
1.46
0.872
2.16
2.15
1.72
1.47
1.06
3.06
3.09
Collection Date: 12/18/2012 16:32
Received Date: 12/19/2012 09:10
Matrix: Water
LOQ/CL
8.00
8.00
8.00
8,oo
8.00
8.00
8.00
s:oo
8.00
8.00
8.00
40.0
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8:00
200
8.00
40.0
8.00
8.00
40.0
200
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DF
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
Date Analyzed
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
1.2/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
12/24/2012 19:45
N.C. Certification# 481
SGS i<n'i1)·1r:oll'c·rspectives ~.AJij) lBL'SiMS$ Or. US ·lfi4ll5 ·Wilmington. NC t i19103SO 1903 f + 1 911) 350 1557 wW\•;.sgstom
Page 26 of34
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il i .
' i c j Client Sample 10: AMW-130 Collection Date: 12/18/2012 16:32
fl Client Project ID: Former Pazivk Warehouse Received Date: 12/19/2012 09:10
i Lab Sarnple ID: 31204038006-B Matrix: Water
I Lab Project 10: 31204038 •, )
r '
Parameter Result Qual DL LOQ/CL Units DF Date Analyzed
Dichlorodifluoromethane NO u 1.28 40.0 ug/L 8 12/24/2012 19:45 \' cis-1 ,3-Dichloropropene NO u 2.15 8.00 ug/L 8 12/24/2012 19:45 I
trans-1 ,3-Dichloropropene NO u 2.10 8.00 ug/L 8 12/24/2012 19:45
Diisopropyl Ether NO u 1.67 8.00 ug/L 8 12/24/2012 19:45
r , Ethyl Benzene NO u 2.01 8.00 ug/L 8 12/24/2012 19:45
! Hexachlorobutadiene NO u 2.19 8.00 ug/L 8 12/24/2012 19:45 I l lsopropylbenzene (Cumene) NO u 2.29 8.00 ug/L 8 12/24/2012 19:45
Methyl iodide NO u 1.18 8.00 ug/L 8 12/24/2012 19:45 r. Methylene chloride NO u 1.29 40.0 ug/L 8 12/24/2012 19:45 I
Naphthalene NO u 1.74 8.00 ug/L 8 12/24/2012 19:45
Styrene NO u 1.79 8.00 ug/L 8 . 12/24/2012 19:45
Tetrachloroethene NO u 2.11 8.00 ug/L 8 12/24/2012 19:45
Toluene NO u 1.56 8.00 ug/L 8 12/24/2012 19:45
Trichloroethene 2.16 J 1.82 8.00 ug/L 8 12/24/2012 19:45
Trichlorofluoromethane NO u 1.11 8.00 ug/L 8 12/24/2012 19:45
Vinyl chloride 2810 75.6 400 ug/L 400 12/21/2012 19:20
Xylene (total) NO u 2.38 16.0 ug/L 8 12/24/2012 19:45
cis-1 ,2-Dichloroethene 7230 120 400 ug/L 400 12/21/2012 19:20
m,p-Xylene NO u 2.24 16.0 ug/L 8 12/24/2012 19:45
n-Propylbenzene NO u 2.38 8.00 ug/L 8 12/24/2012 19:45
a-Xylene NO u 2.38 8.00 ug/L 8 12/24/2012 19:45
sec-Butylbenzerie NO u 1.93 8.00 ug/L 8 12/24/2012 19:45
tert-Butyl methyl ether (MTBE) NO u 1.60 8.00 ug/L 8 12/24/2012 19:45
tert-Butylbenzene NO u 2.34 8.00 ug/L 8 12/24/2012 19:45
trans-1 ,2-Dichloroethene 29.1 1.70 8.00 ug/L 8 12/24/2012 19:45
trans-1 ,4-Dichloro-2-butene NO u 18.9 40.0 ug/L 8 12/24/2012 19:45
Surrogates
1 ,2-Dichloroethane-d4 107 64.0-140 % 8 12/24/2012 19:45
4-Bromofluorobenzene 96.0 85.0-115 % 8 12/24/2012 19:45
Toluene dB 106 82.0-117 % 8 12/24/2012 19:45
Print Date: 01/0312013 N.C. Certification# 481
SGS Analy1,:31 PerspNtil'es SSOO lll<sinfr's& Or. US, l./341)5 ·Wilmington. NC t 11 910.JS(! 1903 f + 1 910 3501557 www.sgswm
Momber uf tic• $liS Group !SuS Sl\1
Page 27 of34
n
n
[]
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:Results of AMW-130
Client Sample ID: AMW-130
Client Project ID: Former Pazivk Warehouse
Lab. Sample ID: 31204038006-B
Lab Project ID: 31204038
;-R·~~~~t~ ·t;;·sw~s4s '826o·8··
1'.;:,;":~·:·_,,>; {i;.::~,''i-.S:'"' , ''.:.•;:'-':.\' ·.·'.~ ~_::\·;': <·':'·: .·.;·:.-• ··<~ : >.;
Parameter Result
Analytical Balch: VMS2793
Analytical Method: SW-846 82608
Instrument: MSD8
Analyst: BWS
Analytical Batch: VMS2794
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Dat<?.: 0110312013
Collection Date.: 12/18/2012 16:32
Received Date: 12/19/2012 09:10
Matrix:. Water
Prep Batch: VXX4458
Prep Method: SW-846 5030B
Prep Date/Time: 12/21/2012 08:34
Prep Initial Wt.Nol.: 40 mL
Prep Extract Vol: 40 mL
Prep Batch: VXX4463
Prep Method: SW-846 50308
Prep Date/Time: 12/24/2012 11:58
Prep Initial Wt.Nol.: 40 mL
Prep Extract Vol: 40 mL
Date Analyzed
N.C. Certification f!. 481
SGS i'<na!y1ic:sl Pcrspl'nives SSOO 6wsirmss Dr. US· 1:8405 · Wilmillgton, NC t 11 910 JSQ 1903 f + 1 910 350 1557 www.sgs com
Mom&er ullh• Wl1 Group !SUS St\1
Page 28 of34
l
Client Sample ID: AMW-130 Collection Date: 12/18/2012 16:32
fl Client ProjectJD: Former Pazivk Warehouse Received Date: 12/19/2012 09:10
. Lab Sample ID: 31204038006-D Matrix: Water .,
~ ) Lab Project ID: 31204038
f l
',: .. ,_-~.v:....;"-"-'''
:Results by SW-846 82700 '· '". ,_ , ......... ,_ .-_, ...... , ..... " ;·~:·."-'-':.;:;·.·.·' ; ....
Parameter Result Qual DL LOQ/CL Units bF Date Anal~zed
1 ,2,4-Trichlorobenzene ND u 1.73 5.01 ug/L 1 12/20/2012 22:12 I , 1 ,2-Dichlorobenzene ND u 1.71 5.01 ug/L 12/20/2012 22:12
1 ,3-Dichlorobenzene ND u 1.65 5.01 ug/L 12/20/2012 22:12
1 A-Dichlorobenzene 20.1 1.63 5.01 ug/L 12/20/2012 22:12
2,4-Dinitrotoluene ND u 1.84 5.01 ug/L 12/20/20.12 22:12
2,6-Dinitrotoluene ND u 1.88 5.01 ug/L 12/20/2012 22:12
2-Chloronaphthalene ND u 2.00 5.01 ug/L 12/20/2012 22:12
2-Methylnaphthalene ND u 1.94 5.01 ug/L 12/20/2012 22:12
2-Nitroaniline ND u 1.69 5.01 ug/L 12/20/2012 22:12
3,3'-Dichlorobenzidine ND u 1.75 10.0 ug/L 12/20/2012 22:12
3-Nitroaniline ND u 1.65 25.1 ug/L 12/20/2012 22:12
4-Chloroaniline ND u 1.88 25.1 ug/L 12/20/2012 22:12
4-Chlorophenyl phenyl ether ND u 2.46 5.01 ug/L 12/20/2012 22:12
Acenaphthene ND u 2.06 5.01 ug/L 12/20/2012 22:12
Acenaphthylene ND u 2.00 5.01 ug/L 12/20/2012 22:12
Anthracene ND u 1.93 5.01 ug/L 12/20/2012 22:12
Benzo(a)anthracene ND u 1.96 5.01 ug/L 12/20/2012 22:12
Benzo(a)pyrene ND u 1.86 5.01 ug/L 12/20/2012 22:12
Benzo(b)fluoranthene ND u 1.96 5.01 ug/L 12/20/2012 22:12
Benzo(g,h,i)perylene ND u 2.15 5.01 ug/L 12/20/2012 22:12
Benzo(k)fluoranthene ND u 2.31 5.01 ug/L 12/20/2012 22:12
Bis(2-Chloroethoxy)methane ND u 2.12 5.01 ug/L 12/20/2012 22:12
Bis(2-Chloroethyl)ether ND u 2.21 5.01 ug/L 12/20/2012 22:12
Bis(2-Chloroisopropyl)ether ND u 2.04 5.01 ug/L 12/20/2012 22:12
Bis(2-Ethylhexyl)phthalate ND u 1.95 5.01 ug/L 12/20/2012 22:12
4-Bromophenyl phenyl ether ND u 2.04 5.01 ug/L 12/20/2012 22:12
Butyl benzyl phthalate ND u 1.89 5.01 ug/L 12/20/2012 22:12
Chrysene ND u 2.20 5.01 ug/L 12/20/2012 22:12
Di-n-butyl phthalate ND u 1.91 5.01 ug/L 12/20/2012 22:12
Di-n-octyl phthalate ND u 1.46 5.01 ug/L 12/20/2012 22:12
Dibenz(a,h)anthracene ND u 2.02 5.01 ug/L 12/20/2012 22:12
Dibenzofuran ND u 2.22 5.01 ug/L 12/20/2012 22:12
Diethyl phthalate ND u 2.10 5.01 ug/L 12/20/2012 22:12
Dimethyl phthalate ND u 2.14 5.01 ug/L 12/20/2012 22:12
Diphenylamine ND u 2.02 5.01 ug/L 12/20/2012 22:12
Fluoranthene ND u 2.02 5.01 ug/L 12/20/2012 22:12
Fluorene ND u 2.44 5.01 ug/L 12/20/2012 22:12
Hexachlorobenzene ND u 1.93 5.01 ug/L 12/20/2012 22:12
Hexachlorobutadiene ND u 1.52 5.01 ug/L 12/20/2012 22:12
Hexachlorocyclopentadiene ND u 0.790 10.0 ug/L 12/20/2012 22:12
Hexachloroethane ND u 1.40 5.01 ug/L 12/20/2012 22:12
lndeno(1 ,2,3-cd)pyrene ND u 2.02 5.01 ug/L 12/20/2012 22:12
lsophorone ND u 2.09 5.01 ug/L 12/20/2012 22:12
Print Date: o·1f0312()1.3 N.C Certification# 481
SGS AnJI)'ti::ai Perspcnives '5st'lll 'Business Or. US · tli:405 · Wilmingion, NC lt1910150 1903 f [phone] www.Si)Ht)m
M•mb.r uf 1h• WS G1 oup (S!;S Sl\1
Page 29 of 34
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' JResults of AMW-130
Client Sample ID:. AMW-130
Client Project I D: Forme.r Pazivk Warehouse
Lab Sample ID: 31204038006-D
Lab Pr'ciject ID: 31204038
Parameter Result
Naphthalene NO
4-Nitroaniline NO
Nitrobenzene NO
Phenanthrene 3.36
Pyrene NO
n-Nitrosodi-n-propylamine NO
Surrogates
2,4,6-Tribromophenol 103
2-Fiuorobiphenyl 89.0
2-Fiuorophenol 87.0
Nitrobenzene-d5 88.0
Phenol-d6 91.0
Terphenyl-d14 77.0
-;Batch Information
Analytical Batch: XMS1777
Analytical Method: SW-846 8270D
Instrument: MSDG
Analyst: CMP
Print Date: 0·1t0312013
Qual OL
u 1.94
u 1.68
u 2.19
J 1.99
u 2.01
u 2,23
Collection Date: 12/18/2012 16:32
Received Date: 12/19/2012 09:10
Matrix: Water
LOQ/CL Units OF
5.01 ug/L
25.1 ug/L
5.01 ug/L
5.01 ug/L
5.01 ug/L
5.01 ug/L
29.3-152 %
50.0-107 %
33.1-118 %
46.0-118 %
49.0-120 %
22.1-142 %
Prep Batch: XXX3426
Prep Method: SW-846 3520C
Prep Date/Time: 12/19/2012 14:49
Prep Initial Wt.Nol.: 998 mL
Prep Extract Vol: 5 mL
Date Analyzed
12/20/2012 22:12
12/20/2012 22:12
12/20/2012 22:12
12/20/2012 22:12
12/20/2012 22:12
12/20/2012 22:12
12/20/2012 22:12
12/20/2012 22:12
12/20/2012 22:12
12/20/2012 22:12
12/20/2012 22:12
12/20/2012 22:12
N.C. Certiflc.~,tion # 481
SGS ;\naly1i:;;l Perspc-cl•vcs SSOOIB~JSin~ss Dr. US· :?.64ti5 · Wilntiflgion, NC t 1i 91035111903 f + 1 910 3501557 www.sgstam
Page 30 of 34
lJ
ll
l J I'.IWYm>A.tP~"'~
ll ;Results of Trip Blank (not on CCC) I . ··~:..,,-.:;..;·:; ·. __ , j ::·~,y· l J Client Sample ID: Trip Blank (not on CCC) Collection Date: .12/18/2012 00:00
Client Project ID: Former Pazivk Warehouse Received Date: 12/19/2012 09:10 r: Lab Sample ID: 31204038007-A Matrix: Water I ' l j Lab Project ID: 31204038
.. ---~ ····--' ., __ .-·-· r ,
-·.·-.. -~.
i 0 Parameter Result Qual DL LOQ/CL Units DF Date Analyzed
1,1, 1 ,2-Tetrachloroethane ND u 0.355 1.00 ug/L 12/21/2012 12:22 I l 1,1, 1-Trichloroethane ND u 0.205 1.00 ug/L 12/21/2012 12:22
1,1 ,2,2-Tetrachloroethane ND u 0.289 1.00 ug/L 12/21/2012 12:22
1,1 ,2-Trichloroethane ND u 0.295 1,00 ug/L 12/21/2012 12:22
1, 1-Dichloroethane ND u 0.215 1.00 ug/L 12/21/2012 12:22 r 1 , 1-Dichloroethene ND u 0.288 1.00 ug/L 12/21/2012 12:22 I l 0 1, 1-Dichloropropene ND u 0.203 1.00 ug/L 1 12/21/2012 12:22
1 ,2,3-Trichlorobenzene ND u 0.358 1;00 ug/L 12/21/2012 12:22
1 ,2,3-Trichloropropane ND u 0.421 1.00 ug/L 12/21/2012 12:22
1 ,2,4-Trichlorobenzene ND u 0.202 1.00 ug/L 12/21/2012 12:22
l ' 1 ,2,4-Trimethylbenzene ND u 0.306 1.00 ug/L 12/21/2012 12:22
1 ,2-Dibromo-3-chloropropane ND u 1.88 5.00 ug/L 12/21/2012 12:22
1 ,2-Dibromoethane ND u 0.344 1.00 ug/L 12/21/2012 12:22
1 ,2-Dichlorobenzene ND u 0.298 1.00 ug/L 12/21/2012 12:22
1 ,2-Dichloroethane ND u 0.296 1.00 ug/L 12/21/2012 12:22
1 ,2-Dichloropropane ND u 0.161 1.00 ug/L 12/21/2012 12:22
1 ,3,5-Trimethylbenzene ND u 0.275 1.00 ug/L 12/21/2012 12:22
1 ,3-Dichlorobenzene ND u 0.324 1.00 ug/L 12/21/2012 12:22
1 ,3-Dichloropropane ND u 0.320 1.00 ug/L 12/21/2012 12:22
1 A-Dichlorobenzene ND u 0.463 1.00 ug/L 12/21/2012 12:22
2,2-Dichloropropane ND u 0.239 1.00 ug/L 12/21/2012 12:22
2-Butanone ND u 1.53 25.0 ug/L 12/21/2012 12:22
2-Chlorotoluene ND u 0.299 1.00 ug/L 12/21/2012 12:22
2-Hexanone ND u 1.24 5.00 ug/L 12/21/2012 12:22
4-Chlorotoluene ND u 0.421 1.00 ug/L 12/21/2012 12:22
4-lsopropyltoluene ND u 0.203 1.00 ug/L 12/21/2012 12:22
4-Methyl-2-pentanone ND u 1.28 5.00 ug/L 12/21/2012 12:22
Acetone ND u 1.41 25.0 ug/L 12/21/2012 12:22
Benzene ND u 0.156 1.00 ug/L 12/21/2012 12:22
Bromobenzene ND u 0.293 1.00 ug/L 12/21/2012 12:22
Bromochloromethane ND u 0.219 1.00 ug/L 12/21/2012 12:22
Bromodichloromethane ND u 0.364 1.00 ug/L 12/21/2012 12:22
Bromoform ND u 0.496 1.00 ug/L 12/21/2012 12:22
Bromomethane ND u 0.168 1.00 ug/L 12/21/2012 12:22
n-Butylbenzene ND u 0.183 1.00 ug/L 12/21/2012 12:22
Carbon disulfide ND u 0.109 1.00 ug/L 12/21/2012 12:22
Carbon tetrachloride ND u 0.270 1.00 ug/L 12/21/2012 12:22
Chlorobenzene ND u 0.269 1.00 ug/L 12/21/2012 12:22
Chloroethane ND u 0.215 1.00 ug/L 12/21/2012 12:22
Chloroform ND u 0.184 1.00 ug/L 12/21/2012 12:22
Chloromethane ND u 0.132 1.00 ug/L 12/21/2012 12:22
Dibromochloromethane ND u 0.383 1.00 ug/L 12/21/2012 12:22
Dibromomethane ND u 0.386 1.00 ug/L 12/21/2012 12:22
Print Date· 01/031201.'3 N.C. Celiification # 4·81
SGS ;\nalyi:c31 Pe•spc:·hes ~!{} :Businll'SS Or. US M4ii5 Wilmi~gton, NC t1t 9Hil501S03 ft·l910350 1557 l'rt•w.sgs (:On~
M•mb01 oflh• SGS Gwup ISllSSO,I
Page 31 of 34
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Client Sample ID:• Trip Blank (not on COC)
Client Project ID: Former Pazivk Warehouse
Lab Sample ID: 31204038007-A
LabProject ID: 31204038
!~····~. . .. --. -~-' ..
; Results by SW-846 82608
···;.:-:,:;;:;·:\:·;-... ',";•;.,.,.
Parameter Result
Dichlorodifluoromethane ND
cis-1 ,3-Dichloropropene ND
trans-1 ,3-Dichloropropene ND
Diisopropyl Ether ND
Ethyl Benzene ND
Hexachlorobutadiene ND
lsopropylbenzene (Cumene) ND
Methyl iodide ND
Methylene chloride ND
Naphthalene ND
Styrene ND
Tetrachloroethene ND
Toluene ND
Trichloroethene ND
Trichlorofluoromethane ND
Vinyl chloride ND
Xylene (total) ND
cis-1 ,2-Dichloroethene ND
m,p-Xylene ND
n-Propylbenzene ND
a-Xylene ND
sec-Butylbenzene ND
tert-Butyl methyl ether (MTBE) ND
tert-Butylbenzene ND
trans-1 ,2-Dichloroethene ND
trans-1 ,4-Dichloro-2-butene ND
Surrogates
1 ,2-Dichloroethane-d4 99.0
4-Bromofluorobenzene 91.0
Toluene d8 99.0
1Batch Information
Analytical Batch: VMS2793
Anal}1tical Method: SW-84.6 8260B
Instrument: MSD8
Analyst BWS
Print Datror 01103!2013
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
DL
0.160
0.269
0.262
0.209
0.251
0.274
0.286
0.148
0.161
0.217
0.224
0.264
0.195
0.227
0.139
0.189
0.298
0.299
0.280
0.297
0.298
0.241
0.200
0.293
0.213
2.36
Collection Date: 12/18/2012 00:00
Received Date: 12/19/2012 09:10
Matrix: Water
LOQ/CL Units DF
5.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
5.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
2.00 ug/L
1.00 ug/L
2.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
1.00 ug/L
5.00 ug/L
64.0-140 %
85.0-115 %
82.0-117 %
Prep Batch: VXX4458
Prep Method: SW-846 50308
Prep Date/Time: 12/2112012 08:34
Prep Initial Wt.No!.: 40 ml
Prep Extract Vol: 40 mL
Page 32 of34
Date Analyzed
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/2112012 12:22
12/21/2012 12:22
12/21/2012 12:22
12/21/2012 12:22
N.C Certificc,fion if. 481
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SGS North America Inc.
Sample Receipt Checklist (SRC)
Client: ARM
1. X Shipped
-Hand Delivered
2. ~ COC Present on Receipt
NoCOC
Additional Transmittal Forms
3. Custody Tape on Container
X No Custody Tape
4. X Samples Intact
=Samples Broken I Leaking
Work Order No.:
Notes:
31204038 --------
5. X Chilled on Receipt Actual Temp.(s) in oc: ..;;2~.9;....0 _____________ _
-Ambient on Receipt
-Walk-in on Ice; Coming down to temp.
=Received Outside of Temperature Specifications
6. X Sufficient Sample Submitted
=Insufficient Sample Submitted
7. Chlorine absent
HN03 < 2
HCL <2
Additional Preservatives verified (see notes)
8. X Received Within Holding Time
-Not Received Within Holding Time
9. X No Discrepancies Noted
-Discrepancies Noted
NCDENR notified of Discrepancies*
10. X No Heads pace present in VOC vials
-Headspace present in VOC vials >6mm
Comments: ----------------------------------------------
Inspected and Logged in by:-=B;;..,A;.:,.H;...._,..,....,..,..,...,..,__,."":""""':-
Date: Wed-12/19/12 00:00
*NCDENR must be notified when collection, holding time or preservation requirements are not met. Ml_11.6
Page 34 of 34
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. www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
February 07, 2013
Karen Corbett
ARM's Waterworks
P.O. Box 1277
Hampstead, NC 28143
RE: Project: Former Pzaiuk Warehouse 07098
Pace Project No.: 92145859
Dear Karen Corbett:
Enclosed are the analytical results for sample{s) received by the laboratory on January 24, 2013.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely, tr'--' ~~.u(._y
Jon D Bradley for
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc: James Cornette, ARM'S Waterworks
Joe Zunich, ARM'S Waterworks
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Page 1 of 19
Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Project: Former Pzaiuk Warehouse 07098
Pace Project No.: 92145859
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19
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Pace Analytical SeN Ices, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical SeNices, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical SeiVices, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Former Pzaiuk Warehouse 07098
Pace Project No.: 92145859
Sample: AMW-80
Parameters
8270 MSSV Semivolatile Organic
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrena
1 ,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fiuorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fiuorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV
Acetone
Benzene
Bromo benzene
Bromo chloromethane
Bromodichloromethane
Bromoform
Bromo methane
2-Butanone (MEK)
tert-Butyl Alcohol
n-Butylbenzene
sec-Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Date: 02/07/2013 12:11 PM
LabiD: 92145859001 Collected: 01/23/1313:22 Received: 01/24/1310:10 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No.
Analytical Method: EPA 8270 Preparation Method: EPA 3510
<0.32 ug/L
<0.28 ug/L
<1.6 ug/L
<2.0 ug/L
<0.34 ug/L
<2.0 ug/L
<2.0 ug/L
<2.1 ug/L
<1.1 ug/L
<0.91 ug/L
<4.1 ug/L
<0.91 ug/L
<0.99 ug/L
<1.0 ug/L
<4.6 ug/L
<0.22 ug/L
<1.9 ug/L
<0.19 ug/L
<0.98 ug/L
<0.92 ug/L
<1.3 ug/L
49%
54%
57%
20%
28%
58%
Analytical Method: EPA 8260
<10.0 ug/L
<1.7 ug/L
<1.5 ug/L
<2.2 ug/L
<1.7 ug/L
<1.5 ug/L
<2.5 ug/L
<4.9 ug/L
<57.7 ug/L
<1.9 ug/L
<1.7 ug/L
<1.6 ug/L
<1.9 ug/L
<1.7 ug/L
<1.6 ug/L
<1.9 ug/L
<1.5 ug/L
10.0
10.0
10.0
10.0
10.0
50.0
50.0
20.0
10.0
10.0
50.0
10.0
10.0
10.0
25.0
10.0
10.0
10.0
10.0
10.0
10.0
21-110
27-110
31-107
10-110
12-110
27-110
25.0
5.0
5.0
5.0
5.0
5.0
10.0
10.0
100
5.0
5.0
5.0
5.0
5.0
10.0
5.0
5.0
01/30/13 07:50 02/04/1315:32 90-12-0
01/30/13 07:50 02/04/1315:32 91-57-6
01/30/13 07:50 02/04/1315:32 95-48-7
01/30/13 07:50 02/04/13 15:32
01/30/13 07:50 02/04/1315:32 91-20-3
01/30/13 07:50 02/04/1315:32 88-74-4
01/30/13 07:50 02/04/13 15:32 99-09-2
01/30/13 07:50 02/04/13 15:32 100-01-6
01/30/13 07:50 02/04/13 15:32 98-95-3
01/30/13 07:50 02/04/1315:32 88-75-5
01/30/13 07:50 02/04/1315:32 100-02-7
01/30/13 07:50 02/04/1315:32 62-75-9
01/30/13 07:50 02/04/13 15:32 621-64-7
01/30/13 07:50 02/04/13 15:32 86-30-6
01/30/13 07:50 02/04/13 15:32 87-86-5
01/30/13 07:50 02/04/13 15:32 85-01-8
01/30/13 07:50 02/04/13 15:32 108-95-2
01/30/13 07:50 02/04/13 15:32 129-00-0
01/30/13 07:50 02/04/13 15:32 120-82-1
01/30/13 07:50 02/04/13 15:32 95-95-4
01/30/13 07:50 02/04/13 15:32 88-06-2
01/30/13 07:50 02/04/13 15:32 4165-60-0
01/30/13 07:50 02/04/13 15:32 321-60-8
01/30/13 07:50 02/04/13 15:32 1718-51-0
01/30/13 07:50 02/04/13 15:32 13127-88-3
01/30/13 07:50 02/04/1315:32 367-12-4
01/30/13 07:50 02/04/13 15:32 118-79-6
02/05/13 16:51 67-64-1
02/05/13 16:51 71-43-2
02/05/13 16:51 108-86-1
02/05/13 16:51 74-97-5
02/05/1316:51 75-27-4
02/05/1316:51 75-25-2
02/05/1316:51 74-83-9
02/05/13 16:51 78-93-3
02/05/13 16:51 75-65-0
02/05/13 16:51 104-51-8
02/05/1316:51 135-98-8
02/05/1316:51 98-06-6
02/05/13 16:51 56-23-5
02/05/13 16:51 108-90-7
02/05/13 16:51 75-00-3
02/05/13 16:51 67-66-3
02/05/13 16:51 74-87-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Qual
Page 5 of 19
n/2 l J ®
ace Analytical [-J / www.pacelabs.com
ll
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Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Former Pzaiuk Warehouse 07098
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Pace Project No.: 92145859
Sample: AMW-80
Parameters
8270 MSSV Semivolatile Organic
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i}perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl} ether
bis(2-Chloroisopropyl} ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h}anthracene
Dibenzofuran
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2, 6-D initroto I uene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1 ,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno( 1 ,2,3-cd)pyrene
lsophorone
Date: 02/07/2013 12:11 PM
LabiD: 92145859001 Collected: 01/23/13 13:22 Received: 01/24/13 10:10 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No.
Analytical Method: EPA 8270 Preparation Method: EPA 3510
<0.25 ug/L
<0.21 ug/L
<2.0 ug/L
<0.14 ug/L
<0.33 ug/L
<0.30 ug/L
<0.28 ug/L
<0.38 ug/L
<0.43 ug/L
<11.5 ug/L
<2.4 ug/L
<0.82 ug/L
<0.79 ug/L
<3.7 ug/L
<2.8 ug/L
<0.92 ug/L
<1.0 ug/L
<0.95 ug/L
<0.98 ug/L
<1.3 ug/L
<0.87 ug/L
<0.21 ug/L
<0.55 ug/L
<0.89 ug/L
<0.88 ug/L
<0.81 ug/L
<0.95 ug/L
<2.1 ug/L
<1.7 ug/L
<0.58 ug/L
<1.2 ug/L
<0.76 ug/L
<0.75 ug/L
<2.6 ug/L
<9.0 ug/L
<0.90 ug/L
<0.98 ug/L
<0.66 ug/L
<0.79 ug/L
<0.21 ug/L
<0.21 ug/L
<0.94 ug/L
<0.72 ug/L
<0.88 ug/L
<1.1 ug/L
<0.29 ug/L
<0.89 ug/L
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
50.0
20.0
10.0
10.0
20.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
20.0
50.0
10.0
10.0
10.0
6.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
01/30/13 07:50 02/04/13 15:32 83-32-9
01/30/13 07:50 02/04/13 15:32 208-96-8
01/30/13 07:50 02/04/13 15:32 62-53-3
01/30/13 07:50 02/04/1315:32 120-12-7
01/30/13 07:50 02/04/13 15:32 56-55-3
01/30/13 07:50 02/04/13 15:32 50-32-8
01/30/13 07:50 02/04/13 15:32 205-99-2
01/30/13 07:50 02/04/13 15:32 191-24-2
01/30/13 07:50 02/04/13 15:32 207-08-9
01/30/13 07:50 02/04/13 15:32 65-85-0
01/30/13 07:50 02/04/13 15:32 100-51-6
01/30/13 07:50 02/04/13 15:32 101-55-3
01/30/13 07:50 02/04/13 15:32 85-68-7
01/30/13 07:50 02/04/13 15:32 59-50-7
01/30/13 07:50 02/04/1315:32 106-47-8
01/30/13 07:50 02/04/1315:32 111-91-1
01/30/13 07:50 02/04/1315:32 111-44-4
01/30/13 07:50 02/04/1315:32 108-60-1
01/30/13 07:50 02/04/1315:32 91-58-7
01/30/13 07:5(} 02/04/13 15:32 95-57-8
01/30/13 07:50 02/04/13 15:32 7005-72-3
01/30/13 07:50 02/04/13 15:32 218-01-9
01/30/13 07:50 02/04/1315:32 53-70-3
01/30/13 07:50 02/04/1315:32 132-64-9
01/30/13 07:50 02/04/1315:32 95-50-1
01/30/13 07:50 02/04/1315:32 541-73-1
01/30/13 07:50 02/04/13 15:32 106-46-7
01/30/13 07:50 02/04/13 15:32 91-94-1
01/30/13 07:50 02/04/13 15:32 120-83-2
01/30/13 07:50 02/04/13 15:32 84-66-2
01/30/13 07:50 02/04/13 15:32 105-67-9
01/30/13 07:50 02/04/1315:32 131-11-3
01/30/13 07:50 02/04/13 15:32 84-74-2
01/30/13 07:50 02/04/13 15:32 534-52-1
01/30/13 07:50 02/04/13 15:32 51-28-5
01/30/13 07:50 02/04/1315:32 121-14-2
01/30/13 07:50 02/04/13 15:32 606-20-2
01/30/13 07:50 02/04/13 15:32 117-84-0
01/30/13 07:50 02/04/13 15:32 117-81-7
01/30/13 07:50 02/04/1315:32 206-44-0
01/30/13 07:50 02/04/1315:32 86-73-7
01/30/13 07:50 02/04/13 15:32 87-68-3
01/30/13 07:50 02/04/13 15:32 118-74-1
01/30/13 07:50 02/04/13 15:32 77-47-4
01/30/13 07:50 02/04/13 15:32 67-72-1
01/30/13 07:50 02/04/13 15:32 193-39-5
01/30/13 07:50 02/04/13 15:32 78-59-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Qual
Page 4 of 19
[l ~ ®
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Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Former Pzaiuk Warehouse 07098
r 1
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Pace Project No.: 92145859
Sample: AMW-80
Parameters
8260 MSV
2-Chlorotoluene
4-Chlorotoluene
1 ,2-Dibromo-3-chloropropane
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1 ,3-Dichlorobenzene
.1 A-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1,2-Dichloroethene (Total)
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1 ,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichloropropene
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Diisopropyl ether
Ethyl benzene
Hexachloro-1 ,3-butadiene
2-Hexanone
lsopropylbenzene (Cumene)
p-lsopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tart-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1, 1 ,2-Tetrachloroethane
1 , 1 ,2 ,2-Tetrachloroethane
Tetrachloroethane
Toluene
1 ,2,3-Trichlorobenzene
1 ,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethane
Trichlorofluoromethane
1 ,2,3-Trichloropropane
1 ,2,4-Trimethylbenzene
1 ,3,5-Trimethylbenzene
Date: 02/07/2013 12:11 PM
Lab ID: 92145859001 Collected: 01/23/13 13:22 Received: 01/24/13 10:10 Matrix: Water
Results Units
Analytical Method: EPA 8260
<1.5 ug/L
<1.6 ug/L
<1.7 ug/L
<1.8 ug/L
<1.7 ug/L
<2.0 ug/L
<1.5 ug/L
<1.5 ug/L
<1.5 ug/L
<1.6 ug/L
5.1 ug/L
<1.8 ug/L
1120 ug/L
2.9J ug/L
1090 ug/L
26.6 ug/L
<1.7 ug/L
<1.7 ug/L
<1.6 ug/L
<1.7 ug/L
<1.6 ug/L
<1.6 ug/L
<1.7 ug/L
<1.6 ug/L
<1.8 ug/L
<3.8 ug/L
<1.6 ug/L
<1.6 ug/L
<1.9 ug/L
<3.6 ug/L
<1.7 ug/L
<2.0 ug/L
<1.5 ug/L
<1.6 ug/L
<1.7 ug/L
<1.5 ug/L
<1.8 ug/L
<1.6 ug/L
<2.0 ug/L
<1.7 ug/L
<1.9 ug/L
<1.7 ug/L
29.2 ug/L
<1.7 ug/L
<1.5 ug/L
<1.5 ug/L
<1.3 ug/L
POL DF Prepared
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100 20
5.0 1
100 20
5.0 1
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed CAS No.
02/05/13 16:51 95-49-8
02/05/13 16:51 106-43-4
02/05/13 16:51 96-12-8
02/05/13 16:51 124-48-1
02/05/1316:51 106-93-4
02/05/13 16:51 74-95-3
02/05/13 16:51 95-50-1
02/05/13 16:51 541-73-1
02/05/13 16:51 106-46-7
02/05/13 16:51 75-71-8
02/05/13 16:51 75-34-3
02/05/13 16:51 107-06-2
02/06/13 15:26 540-59-0
02/05/13 16:51 75-35-4
02/06/13 15:26 156-59-2
02/05/1316:51 156-60-5
02/05/13 16:51 78-87-5
02/05/1316:51 142-28-9
02/05/13 16:51 594-20-7
02/05/13 16:51 563-58-6
02/05/13 16:51 10061-01-5
02/05/13 16:51 10061-02-6
02/05/13 16:51 108-20-3
02/05/13 16:51 100-41-4
02/05/13 16:51 87-68-3
02/05/13 16:51 591-78-6
02/05/13 16:51 98-82-8
02/05/13 16:51 99-87-6
02/05/13 16:51 75-09-2
02/05/13 16:51 108-10-1
02/05/13 16:51 1634-04-4
02/05/13 16:51 91-20-3
02/05/13 16:51 103-65-1
02/05/13 16:51 100-42-5
02/05/13 16:51 630-20-6
02/05/13 16:51 79-34-5
02/05/13 16:51 127-18-4
02/05/13 16:51 108-88-3
02/05/13 16:51 87-61-6
02/05/13 16:51 120-82-1
02/05/13 16:51 71-55-6
02/05/13 16:51 79-00-5
02/05/13 16:51 79-01-6
02/05/13 16:51 75-69-4
02/05/13 16:51 96-18-4
02/05/13 16:51 95-63-6
02/05/13 16:51 108-67-8
Qual
Page 6 of 19
Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
(336}623-8921
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828}254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 }875-9092
Project: Former Pzaiuk Warehouse 07098
r-l Pace Project No.: 92145859
( j Sample: AMW-80
r I
f '
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i I I )
r ,
Parameters
8260 MSV
Vinyl acetate
Vinyl chloride
m&p-Xylene
a-Xylene
Surrogates
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1 ,2-Dichloroethane-d4 (S)
Toluene-dB (S)
Date: 02/07/2013 12:11 PM
Lab ID: 92145859001 Collected: 01/23/1313:22 Received: 01/24/13 10:10 Matrix: Water
Results Units PQL DF Prepared
Analytical Method: EPA 8260
<2.3 ug/L 10.0
12.6 ug/L 5.0
<3.1 ug/L 10.0
<1.6 ug/L 5.0
89% 70-130
102 % 70-130
107 % 70-130
98% 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed CAS No.
02/05/13 16:51 108-05-4
02/05/13 16:51 75-01-4
02/05/13 16:51 179601-23-1
02/05/13 16:51 95-47-6
02/05/13 16:51 460-00-4
02/05/13 16:51 1868-53-7
02/05/13 16:51 17060-07-0
02/05/1316:51 2037-26-5
Qual
Page 7 of 19
f l !
l ~
r 1 I L
r 1
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r.
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Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
{336)623-8921
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
{828)254-7176
QUALITY CONTROL DATA
Project: Former Pzaiuk Warehouse 07098
Pace Project No.: 92145859
QC Batch: MSV/21901 Analysis Method: EPA8260
QC Batch Method: EPA8260 Analysis Description: 8260 MSV
Associated Lab Samples: 92145859001
METHOD BLANK: 916394 Matrix: Water
Associated Lab Samples: 92145859001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1, 1 ,2-Tetrachloroethane ug/L <1.7 5.0 02/05/13 15:56
1,1, 1-Trichloroethane ug/L <1.9 5.0 02/05/13 15:56
1,1 ,2,2-Tetrachloroethane ug/L <1.5 5.0 02/05/13 15:56
1,1 ,2-Trichloroethane ug/L <1.7 5.0 02/05/13 15:56
1 , 1-Dichloroethane ug/L <1.8 5.0 02/05/13 15:56
1, 1-Dichloroethene ug/L <1.9 5.0 02/05/13 15:56
1, 1-Dichloropropene ug/L <1.7 5.0 02/05/13 15:56
1 ,2 ,3-Trichlorobenzene ug/L <2.0 5.0 02/05/13 15:56
1 ,2,3-Trichloropropane ug/L <1.5 5.0 02/05/13 15:56
1 ,2,4-Trichlorobenzene ug/L <1.7 5.0 02/05/13 15:56
1 ,2,4-Trimethylbenzene ug/L <1.5 5.0 02/05/13 15:56
1 ,2-Dibromo-3-chloropropane ug/L <1.7 5.0 02/05/13 15:56
1 ,2-Dibromoethane (EDB) ug/L <1.7 5.0 02/05/13 15:56
1 ,2-Dichlorobenzene ug/L <1.5 5.0 02/05/13 15:56
1 ,2-Dichloroethane ug/L <1.8 5.0 02/05/13 15:56
1 ,2-Dichloroethene (Total) ug/L <4.4 5.0 02/05/13 15:56
1 ,2-Dichloropropane ug/L <1.7 5.0 02/05/13 15:56
1 ,3,5-Trimethylbenzene ug/L <1.3 5.0 02/05/13 15:56
1 ,3-Dichlorobenzene ug/L <1.5 5.0 02/05/13 15:56
1 ,3-Dichloropropane ug/L <1.7 5.0 02/05/13 15:56
1 A-Dichlorobenzene ug/L <1.5 5.0 02/05/13 15:56
2,2-Dichloropropane ug/L <1.6 5.0 02/05/13 15:56
2-Butanone (MEK) ug/L <4.9 10.0 02/05/13 15:56
2-Chlorotoluene ug/L <1.5 5.0 02/05/13 15:56
2-Hexanone ug/L <3.8 10.0 02/05/13 15:56
4-Chlorotoluene ug/L <1.6 5.0 02/05/13 15:56
4-Methyl-2-pentanone (MIBK) ug/L <3.6 10.0 02/05/13 15:56
Acetone ug/L <10.0 25.0 02/05/13 15:56
Benzene ug/L <1.7 5.0 02/05/13 15:56
Bromobenzene ug/L <1.5 5.0 02/05/13 15:56
Bromochloromethane ug/L <2.2 5.0 02/05/13 15:56
Bromodichloromethane ug/L <1.7 5.0 02/05/13 15:56
Bromoform ug/L <1.5 5.0 02/05/13 15:56
Bromo methane ug/L <2.5 10.0 02/05/13 15:56
Carbon tetrachloride ug/L <1.9 5.0 02/05/13 15:56
Chlorobenzene ug/L <1.7 5.0 02/05/13 15:56
Chloroethane ug/L <1.6 10.0 02/05/13 15:56
Chloroform ug/L <1.9 5.0 02/05/13 15:56
Chloromethane ug/L <1.5 5.0 02/05/13 15:56
cis-1 ,2-Dichloroethene ug/L <1.8 5.0 02/05/13 15:56
cis-1 ,3-Dichloropropene ug/L <1.6 5.0 02/05/13 15:56
Dibromochloromethane ug/L <1.8 5.0 02/05/13 15:56
Dibromomethane ug/L <2.0 5.0 02/05/13 15:56
Date: 02/07/2013 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
{704)875-9092
Page 8 of 19
r l
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Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Former Pzaiuk Warehouse 07098
Pace Project No.: 92145859
METHOD BLANK: 916394 Matrix: Water
Associated Lab Samples: 92145859001
Blank Reporting
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units Result Limit Analyzed Qualifiers
Dichlorodifluoromethane ug/L <1.6 5.0 02/05/13 15:56
Diisopropyl ether ug/L <1.7 5.0 02/05/13 15:56
Ethyl benzene ug/L <1.6 5.0 02/05/13 15:56
Hexachloro-1,3-butadiene ug/L 2.1J 5.0 02/05/13 15:56
lsopropylbenzene (Cumene) ug/L <1.6 5.0 02/05/13 15:56
m&p-Xylene ug/L <3.1 10.0 02/05/13 15:56
Methyl-tert-butyl ether ug/L <1.7 5.0 02/05/13 15:56
Methylene Chloride ug/L <1.9 5.0 02/05/13 15:56
n-Butylbenzene ug/L <1.9 5.0 02/05/13 15:56
n-Propylbenzene ug/L <1.5 5.0 02/05/13 15:56
Naphthalene ug/L <2.0 5.0 02/05/13 15:56
o-Xylene ug/L <1.6 5.0 02/05/13 15:56
p-lsopropyltoluene ug/L <1.6 5.0 02/05/13 15:56
sec-Butyl benzene ug/L <1.7 5.0 02/05/13 15:56
Styrene ug/L <1.6 5.0 02/05/13 15:56
tert-Butyl Alcohol ug/L <57.7 100 02/05/13 15:56
tert-Butylbenzene ug/L <1.6 5.0 02/05/13 15:56
Tetrachloroethane ug/L <1.8 5.0 02/05/13 15:56
Toluene ug/L <1.6 5.0 02/05/13 15:56
trans-1,2-Dichloroethene ug/L <1.8 5.0 02/05/13 15:56
trans-1,3-Dichloropropene ug/L <1.6 5.0 02/05/13 15:56
Trichloroethane ug/L <1.8 5.0 02/05/13 15:56
Trichlorofluoromethane ug/L <1.7 10.0 02/05/13 15:56
Vinyl acetate ug/L <2.3 10.0 02/05/13 15:56
Vinyl chloride ug/L <1.5 5.0 02/05/13 15:56
1 ,2-Dichloroethane-d4 (S) % 104 70-130 02/05/13 15:56
4-Bromofluorobenzene (S) % 89 70-130 02/05/13 15:56
Dibromofluoromethane (S) % 100 70-130 02/05/13 15:56
Toluene-dB (S) % 101 70-130 02/05/13 15:56
LABORATORY CONTROL SAMPLE: 916395
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
1,1,1 ,2-Tetrachloroethane ug/L 50 46.4 93 70-130
1,1,1-Trichloroethane ug/L 50 50.8 102 70-137
1,1 ,2,2-Tetrachloroethane ug/L 50 54.1 108 70-130
1, 1,2-Trichloroethane ug/L 50 52.9 106 70-130
1, 1-Dichloroethane ug/L 50 54.6 109 70-137
1, 1-Dichloroethene ug/L 50 55.9 112 70-138
1, 1-Dichloropropene ug/L 50 53.5 107 70-130
1 ,2,3-Trichlorobenzene ug/L 50 48.2 96 70-143
1 ,2,3-Trichloropropane ug/L 50 51.5 103 70-130
1 ,2,4-Trichlorobenzene ug/L 50 48.8 98 70-138
1 ,2,4-Trimethylbenzene ug/L 50 48.4 97 70-130
1 ,2-Dibromo-3-chloropropane ug/L 50 44.3 89 68-134
Date: 02/07/2013 12:11 PM REPORT OF LABORATORY ANALYSIS Page 9 of 19
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Se!Vices, Inc ..
r1(2 l J ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
ll -ace~~21!f.!! 205 East Meadow Road -Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
I i I [phone] [phone] [phone]
l )
[ J
QUALITY CONTROL DATA
Project: Former Pzaiuk Warehouse 07098
ll Pace Project No.: 92145859
l j LABORATORY CONTROL SAMPLE: 916395
Spike LCS LCS %Rec
f l Parameter Units Cone. Result %Rec Limits Qualifiers
l 1 ,2-Dibromoethane (EDB) ug/L 50 52.4 105 70-130
1 ,2-Dichlorobenzene ug/L 50 49.1 98 70-130
1 ,2-Dichloroethane ug/L 50 53.8 108 70-133 r 1 1 ,2-Dichloroethene (Total) ug/L 100 109 109 70-130
1 ,2-Dichloropropane ug/L 50 54.5 109 70-130
1 ,3,5-Trimethylbenzene ug/L 50 49.4 99 70-130
1 ,3-Dichlorobenzene ug/L 50 49.8 100 70-130
1 ,3-Dichloropropane ug/L 50 53.4 107 70-130
1 ,4-Dichlorobenzene ug/L 50 50.2 100 70-130
2,2-Dichloropropane ug/L 50 50.0 100 61-142
2-Butanone (MEK) ug/L 100 134 134 63-150
2-Chlorotoluene ug/L 50 50.0 100 70-130
2-Hexanone ug/L 100 123 123 70-137
4-Chlorotoluene ug/L 50 51.1 102 70-130
4-Methyl-2-pentanone (MIBK) ug/L 100 126 126 70-134
Acetone ug/L 100 124 124 68-160
Benzene ug/L 50 54.6 109 70-130
Bromobenzene ug/L 50 49.5 99 70-130
Bromochloromethane ug/L 50 51.3 103 70-135
Bromodichloromethane ug/L 50 48.3 97 70-130
Bromoform ug/L 50 41.9 84 70-130
Bromomethane ug/L 50 50.7 101 63-130
Carbon tetrachloride ug/L 50 45.7 91 70-146
Chlorobenzene ug/L 50 51.3 103 70-130
Chloroethane ug/L 50 51.0 102 60-151
Chloroform ug/L 50 52.6 105 70-130
Chloromethane ug/L 50 55.1 110 65-133
cis-1 ,2-Dichloroethene ug/L 50 54.1 108 70-134
cis-1 ,3-Dichloropropene ug/L 50 52.0 104 70-130
Dibromochloromethane ug/L 50 45.6 91 70-130
Dibromomethane ug/L 50 50.2 100 70-130
Dichlorodifluoromethane ug/L 50 40.2 80 66-130
Diisopropyl ether ug/L 50 59.1 118 70-133
Ethyl benzene ug/L 50 51.1 102 70-130
Hexachloro-1 ,3-butadiene ug/L 50 48.4 97 58-151
lsopropylbenzene (Cumene) ug/L 50 48.9 98 70-130
m&p-Xylene ug/L 100 104 104 70-130
Methyl-tert-butyl ether ug/L 50 48.6 97 70-136
Methylene Chloride ug/L 50 71.8 144 70-130 LO
n-Butylbenzene ug/L 50 50.2 100 70-130
n-Propylbenzene ug/L 50 51.6 103 70-130
Naphthalene ug/L 50 47.5 95 70-139
a-Xylene ug/L 50 49.2 98 70-130
p-Jsopropyltoluene ug/L 50 50.3 101 70-130
sec-Butyl benzene ug/L 50 53.0 106 70-130
Styrene ug/L 50 51.3 103 70-130
tert-Butyl Alcohol ug/L 500 426 85 69-151
tert-Butylbenzene ug/L 50 50.4 101 70-130
Date: 02/07/2013 12:11 PM REPORT OF LABORATORY ANALYSIS Page 10 of 19
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
ll
' I I ,
l J
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Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
{336)623-8921
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
{828)254-7176
QUALITY CONTROL DATA
Project: Former Pzaiuk Warehouse 07098
Pace Project No.: 92145859
LABORATORY CONTROL SAMPLE: 916395
Parameter Units
Tetrachloroethane ug/L
Toluene ug/L
trans-1 ,2-Dichloroethene ug/L
trans-1 ,3-Dichloropropene ug/L
Trichloroethane ug/L
Trichlorofluoromethane ug/L
Vinyl acetate ug/L
Vinyl chloride ug/L
1 ,2-Dichloroethane-d4 (S) %
4-Bromofluorobenzene (S) %
Dibromofluoromethane (S) %
Toluene-dB (S) %
Date: 02/07/2013 12:11 PM
Spike LCS LCS
Cone. Result %Rec
50 49.6 99
50 51.7 103
50 54.4 109
50 50.6 101
50 50.3 101
50 48.0 96
100 141 141
50 52.2 104
103
99
102
100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
%Rec
Limits
70-130
70-130
70-130
70-130
70-130
70-130
67-148
67-133
70-130
70-130
70-130
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
{704)875-9092
Qualifiers
Page 11 of 19
[];&A I. J' Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
[l ace !2.~!!!!f.!m 205 East Meadow Road -Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
l J I [phone] [phone] (704 )875-9092
[J QUALITY CONTROL DATA
Project: Former Pzaiuk Warehouse 07098
lJ
Pace Project No.: 92145859
QC Batch: OEXT/20564 Analysis Method: EPA8270
QC Batch Method: EPA3510 Analysis Description: 8270 Water MSSV
r l Associated Lab Samples: 92145859001
l j METHOD BLANK: 912945 Matrix: Water
Associated Lab Samples: 92145859001
r l Blank Reporting
l j
Parameter Units Result Limit Analyzed Qualifiers
1 ,2,4-Trichlorobenzene ug/L <0.98 10.0 02/04/13 15:00 r, 1 ,2-Dichlorobenzene ug/L <0.88 10.0 02/04/13 15:00
1 ,3-Dichlorobenzene ug/L <0.81 10.0 02/04/13 15:00 I J 1 A-Dichlorobenzene ug/L <0.95 10.0 02/04/13 15:00
1-Methylnaphthalene ug/L <0.32 10.0 02/04/13 15:00
r l
2,4,5-Trichlorophenol ug/L <0.92 10.0 02/04/13 15:00
2,4,6-Trichlorophenol ug/L <1.3 10.0 02/04/13 15:00 I 2,4-Dichlorophenol ug/L <1.7 10.0 02/04/13 15:00 L
2,4-Dimethylphenol ug/L <1.2 10.0 02/04/13 15:00
r , 2 ,4-Dinitrophenol ug/L <9.0 50.0 02/04/13 15:00
2,4-Dinitrotoluene ug/L <0.90 10.0 02/04/13 15:00
2 ,6-Dinitrotoluene ug/L <0.98 10.0 02/04/13 15:00
2-Chloronaphthalene ug/L <0.98 10.0 02/04/13 15:00
2-Chlorophenol ug/L <1.3 10.0 02/04/13 15:00
2-Methylnaphthalene ug/L <0.28 10.0 02/04/13 15:00
2-Methylphenol( a-Cresol) ug/L <1.6 10.0 02/04/13 15:00
2-Nitroaniline ug/L <2.0 50.0 02/04/13 15:00
2-Nitrophenol ug/L <0.91 10.0 02/04/13 15:00
3&4-Methylphenol(m&p Cresol) ug/L <2.0 10.0 02/04/13 15:00
3,3'-Dichlorobenzidine ug/L <2.1 20.0 02/04/13 15:00
3-Nitroaniline ug/L <2.0 50.0 02/04/13 15:00
4,6-Dinitro-2-methylphenol ug/L <2.6 20.0 02/04/13 15:00
4-Bromophenylphenyl ether ug/L <0.82 10.0 02/04/13 15:00
4-Chloro-3-methylphenol ug/L <3.7 20.0 02/04/13 15:00
4-Chloroaniline ug/L <2.8 20.0 02/04/13 15:00
4-Chlorophenylphenyl ether ug/L <0.87 10.0 02/04/13 15:00
4-Nitroaniline ug/L <2.1 20.0 02/04/13 15:00
4~Nitrophenol ug/L <4.1 50.0 02/04/13 15:00
Acenaphthene ug/L <0.25 10.0 02/04/13 15:00
Acenaphthylene ug/L <0.21 10.0 02/04/13 15:00
Aniline ug/L <2.0 10.0 02/04/13 15:00
Anthracene ug/L <0.14 10.0 02/04/13 15:00
Benzo(a)anthracene ug/L <0.33 10.0 02/04/13 15:00
Benzo( a )pyrene ug/L <0.30 10.0 02/04/13 15:00
Benzo(b )fluoranthene ug/L <0.28 10.0 02/04/13 15:00
Benzo(g,h,i)perylene ug/L <0.38 10.0 02/04/13 15:00
r
Benzo(k)fluoranthene ug/L <0.43 10.0 02/04/13 15:00
Benzoic Acid ug/L <11.5 50.0 02/04/13 15:00 l > Benzyl alcohol ug/L <2.4 20.0 02/04/13 15:00
bis(2-Chloroethoxy)methane ug/L <0.92 10.0 02/04/13 15:00
bis(2-Chloroethyl) ether ug/L <1.0 10.0 02/04/13 15:00
bis(2-Chloroisopropyl) ether ug/L <0.95 10.0 02/04/13 15:00
bis(2-Ethylhexyl)phthalate ug/L <0.79 6.0 02/04/13 15:00
Date: 02/07/2013 12:11 PM REPORT OF LABORATORY ANALYSIS Page 12 of 19
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
''(2 : I 1
j -ace Ana/ytica(
r l www.pacelabs.com
l. )
r ' . :
I I
Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
(336}623-8921
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828}254-7176
QUALITY CONTROL DATA
r. J Project: Former Pzaiuk Warehouse 07098
(I Pace Project No.: 92145859
METHOD BLANK: 912945 Matrix: Water
Associated Lab Samples: 92145859001
r 1 Blank Reporting
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 }875-9092
Parameter Units Result Limit Analyzed Qualifiers
l )
r '
I I
I )
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz( a, h )anthracene
Dibenzofuran
Diethylphthalate
Dimethyl phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fiuorobiphenyl (S)
2-Fiuorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
LABORATORY CONTROL SAMPLE:
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1 A-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
Date: 02/07/2013 12:11 PM
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
912946
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
<0.79 10.0 02/04/13 15:00
<0.21 10.0 02/04/13 15:00
<0.75 10.0 02/04/13 15:00
<0.66 10.0 02/04/13 15:00
<0.55 10.0 02/04/13 15:00
<0.89 10.0 02/04/13 15:00
<0.58 10.0 02/04/13 15:00
<0.76 10.0 02/04/13 15:00
<0.21 10.0 02/04/13 15:00
<0.21 10.0 02/04/13 15:00
<0.94 10.0 02/04/13 15:00
<0.72 10.0 02/04/13 15:00
<0.88 10.0 02/04/13 15:00
<1.1 10.0 02/04/13 15:00
<0.29 10.0 02/04/13 15:00
<0.89 10.0 02/04/13 15:00
<0.99 10.0 02/04/13 15:00
<0.91 10.0 02/04/13 15:00
<1.0 10.0 02/04/13 15:00
<0.34 10.0 02/04/13 15:00
<1.1 10.0 02/04/13 15:00
<4.6 25.0 02/04/13 15:00
<0.22 10.0 02/04/13 15:00
<1.9 10.0 02/04/13 15:00
<0.19 10.0 02/04/13 15:00
49 27-110 02/04/13 15:00
52 27-110 02/04/13 15:00
24 12-110 02/04/13 15:00
42 21-110 02/04/13 15:00
16 10-110 02/04/13 15:00
69 31-107 02/04/13 15:00
Spike LCS LCS %Rec
Cone. Result % Rec Limits Qualifiers
50 19.9 40 10-110
50 18.0 36 10-110
50 17.3 35 10-110
50 17.8 36 10-110
50 20.9 42 21-110
50 23.8 48 23-116
50 20.9 42 21-114
50 19.9 40 22-120
50 19.0 38 15-109
250 230 92 10-103
REPORT OF LABORATORY ANALYSIS Page 13 of 19
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
fl/2 Pace Analytical Services, Inc. Pace Analytical Services, Inc . Pace Analytical Services, Inc. • j ® ~l ace~~f!!!£~1 205 East Meadow Road -Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
l J I [phone] [phone] (704 )875-9092
\l QUALITY CONTROL DATA
( ) Project: Former Pzaiuk Warehouse 07098
Pace Project No.: 92145859 ~··
LABORATORY CONTROL SAMPLE: 912946 l )
Spike LCS LCS %Rec
Parameter Units Cone. I I
Result %Rec Limits Qualifiers
2,4-Dinitrotoluene ug/L 50 35.8 72 24-119
2 ,6-Dinitrotoluene ug/L 50 25.5 51 25-116
2-Chloronaphthalene ug/L 50 19.3 39 18-110
c 1 2-Chlorophenol ug/L 50 17.1 34 10-104
2-Methylnaphthalene ug/L 50 20.0 40 16-110
2-Methylphenol( a-Cresol) ug/L 50 15.5 31 13-110
2-Nitroaniline ug/L 100 51.2 51 20-117 r, 2-Nitrophenol ug/L 50 19.9 40 16-108
3&4-Methylphenol(m&p Cresol) ug/L 50 13.7 27 14-110
3,3'-Dichlorobenzidine ug/L 100 93.6 94 13-131
3-Nitroaniline ug/L 100 70.1 70 15-117 r , 4,6-Dinitro-2-methylphenol ug/L 100 99.6 100 13-119
4-Bromophenylphenyl ether ug/L 50 31.4 63 23-120
l ' 4-Chloro-3-methylphenol ug/L 100 41.0 41 21-119
4-Chloroaniline ug/L 100 39.1 39 10-122
4-Chlorophenylphenyl ether ug/L 50 28.1 56 22-112
4-Nitroaniline ug/L 100 99.1 99 14-118
4-Nitrophenol ug/L 250 109 44 10-110
Acenaphthene ug/L 50 22.5 45 20-105
Acenaphthylene ug/L 50 21.4 43 23-106
Aniline ug/L 50 15.2 30 10-110
Anthracene ug/L 50 37.8 76 25-120
Benzo( a )anthracene ug/L 50 45.3 91 21-128
Benzo( a )pyrene ug/L 50 48.1 96 25-116
Benzo(b )fluoranthene ug/L 50 46.2 92 23-117
Benzo(g,h,i)perylene ug/L 50 48.6 97 17-128
Benzo(k)fluoranthene ug/L 50 47.2 94 25-127
Benzoic Acid ug/L 250 26.8J 11 10-110
Benzyl alcohol ug/L 100 30.8 31 10-101
bis(2-Chloroethoxy)methane ug/L 50 18.5 37 19-107
bis(2-Chloroethyl) ether ug/L 50 18.6 37 10-108
bis(2-Chloroisopropyl) ether ug/L 50 14.4 29 10-108
bis(2-Ethylhexyl)phthalate ug/L 50 34.9 70 16-123
Butylbenzylphthalate ug/L 50 33.0 66 20-118
Chrysene ug/L 50 43.8 88 24-125
Di-n-butylphthalate ug/L 50 37.0 74 23-115
Di-n-octylphthalate ug/L 50 32.0 64 20-115
Dibenz(a,h)anthracene ug/L 50 48.5 97 18-131
Dibenzofuran ug/L 50 23.9 48 23-106
Diethylphthalate ug/L 50 34.2 68 24-115
Dimethylphthalate ug/L 50 28.4 57 22-113
Fluoranthene ug/L 50 49.5 99 24-125
Fluorene ug/L 50 28.2 56 24-114
Hexachloro-1 ,3-butadiene ug/L 50 19.3 39 10-110
Hexachlorobenzene ug/L 50 33.2 66 22-127
Hexachlorocyclopentadiene ug/L 50 23.9 48 10-110
Hexachloroethane ug/L 50 15.6 31 10-110
lndeno(1 ,2,3-cd)pyrene ug/L 50 48.2 96 18-130
Date: 02/07/2013 12:11 PM REPORT OF LABORATORY ANALYSIS Page 14 of 19
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
ll ( J
Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Former Pzaiuk Warehouse 07098
Pace Project No.: 92145859
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
' LABORATORY CONTROL SAMPLE: 912946 l J
( I
Parameter
lsophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fiuorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
Units
Spike
Cone.
50
50
50
50
50
50
100
50
50
50
LCS
Result
14.5
17.1
11.0
30.9
19.7
15.2
97.1
37.7
7.8J
44.4
LCS
%Rec
29
34
22
62
39
30
97
75
16
89
60
36
18
33
12
78
%Rec
Limits
23-114
21-114
10-110
24-123
14-110
16-106
10-123
25-119
10-110
22-127
27-110
27-110
12-110
21-110
10-110
31-107
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 912947 912948
Parameter
1 ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2 ,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol( a-Cresol)
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol{m&p
Cresol)
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenylphenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
Date: 02/07/2013 12:11 PM
MS MSD
92145859001 MS
Units Result
Spike
Cone.
Spike
Cone. Result
MSD
Result
MS
%Rec
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
<0.98
<0.88
<0.81
<0.95
<0.32
<0.92
<1.3
<1.7
<1.2
<9.0
<0.90
<0.98
<0.98
<1.3
<0.28
<1.6
<2.0
<0.91
<2.0
<2.1
<2.0
<2.6
<0.82
<3.7
<2.8
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
200
100
100
200
200
200
100
200
200
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
200
100
100
200
200
200
100
200
200
52.2
43.5
42.3
43.2
54.0
62.1
56.3
55.6
53.8
468
69.7
53.5
48.6
44.8
52.0
45.7
114
53.8
43.2
151
145
186
60.0
115
102
53.0
43.8
42.0
43.0
57.4
66.4
61.2
61.7
59.8
398
58.0
50.0
52.0
46.8
55.6
49.7
109
56.3
47.5
142
123
166
60.0
124
114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
52
43
42
43
54
62
56
56
54
94
70
53
49
45
52
46
57
54
43
75
72
93
60
58
51
MSD
%Rec
% Rec
Limits RPD
53 10-110 2
44 10-110
42 10-110
43 10-110 0
57 14-110 6
66 19-105 7
61 13-108 8
62 29-111 10
60 21-103 11
80 10-109 16
58 27-104 18
50 28-101 7
52 14-102 7
47 16-110 4
56 13-110 7
50 19-110 8
55 26-103 5
56 20-110 5
48 20-110 10
71 25-112 6
62 29-110 16
83 10-117 11
60 20-105 0
62 22-110 7
57 20-100 11
Qual
Page 15 of 19
I ~Analytical' ,r~fA ---Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Former Pzaiuk Warehouse 07098
Pace Project No.: 92145859
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 912947 912948
Parameter
4-Chlorophenylphenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethyl phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fiuorobiphenyl (S)
2-Fiuorophenol (S)
Nitrobenzene-d5 (S)
Date: 02/07/2013 12:11 PM
MS MSD
92145859001 MS
Units Result
Spike
Cone.
Spike
Cone. Result
MSD
Result
MS
% Rec
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
<0.87
<2.1
<4.1
<0.25
<0.21
<2.0
<0.14
<0.33
<0.30
<0.28
<0.38
<0.43
<11.5
<2.4
<0.92
<1.0
<0.95
<0.79
<0.79
<0.21
<0.75
<0.66
<0.55
<0.89
<0.58
<0.76
<0.21
<0.21
<0.94
<0.72
<0.88
<1.1
<0.29
<0.89
<0.99
<0.91
<1.0
<0.34
<1.1
<4.6
<0.22
<1.9
<0.19
100
200
500
100
100
100
100
100
100
100
100
100
500
200
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
200
100
100
100
100
200
500
100
100
100
100
100
100
100
100
100
500
200
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
200
100
100
100
63.1
198
337
54.6
52.6
27.5
67.1
84.1
87.4
86.0
87.2
84.3
154
95.0
48.7
45.8
35.3
82.5
63.1
82.1
67.3
61.6
87.0
55.7
67.9
58.3
89.8
61.6
52.3
60.3
65.9
39.4
86.7
40.2
45.9
36.9
56.2
51.2
38.4
181
67.2
30.4
82.3
62.9
153
228
56.8
55.1
31.3
60.4
79.5
82.3
80.9
81.4
80.7
181
101
51.0
47.2
36.4
83.2
61.2
77.5
60.5
58.1
81.3
56.4
57.6
53.2
77.3
58.8
53.0
60.9
69.1
39.0
81.0
42.9
48.9
34.7
55.1
52.7
39.3
156
59.9
29.6
80.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
63
99
67
55
53
27
67
84
87
86
87
84
31
48
49
46
35
82
63
82
67
62
87
56
68
58
90
62
52
60
66
39
87
40
46
37
56
51
38
91
67
30
82
55
43
29
41
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec MSD
%Rec Limits RPD Qual
63 19-102
76 29-110
46 10-110
57 17-100
55 21-100
31 10-110
60 24-109
80 22-117
82 23-104
81 23-103
81 18-111
81 22-113
36 10-110
50 19-101
51 22-110
47 16-110
36 14-110
83 23-102
61 25-110
77 23-115
61 26-110
58 22-110
81 21-112
56 19-102
58 29-110
53 27-110
77 23-112
59 22-104
53 10-110
61 21-116
69 10-110
39 10-110
81 20-113
43 50-150
49 21-105
35 10-110
55 23-107
53 10-110
39 20-110
78 10-118
60 24-106
30 12-110
80 24-114
52 27-110
46 27-110
27 12-110
41 21-110
0
25
38 R1
4
5
13
11
6
6
6
7
4
17
6
5
3
3
3
6
11
6
7
16
9
15
5
1
5
1
7
7 MO,M1
6
6
2
3
2
15
12
3
3
Page16of19
n
n
n
n
t:
L
Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
QUALIFIERS
Project: Former Pzaiuk Warehouse 07098
Pace Project No.: 92145859
DEFINITIONS
OF -Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO -Not Detected at or above adjusted reporting limit.
J -Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PRL-Pace Reporting Limit.
RL -Reporting Limit.
S -Surrogate
1 ,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D)-Laboratory Control Sample (Duplicate)
MS(D)-Matrix Spike (Duplicate)
DUP -Sample Duplicate
RPD -Relative Percent Difference
NC -Not Calculable.
SG -Silica Gel -Clean-Up
U -Indicates the compound was analyzed for, but not detected.
· N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services -Charlotte
ANALYTE QUALIFIERS
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
MO
M1
R1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
RPD value was outside control limits.
Date: 02/07/2013 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
(704 )875-9092
Page 18 of 19
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Client Name: Proje~t #-i,;,.~~~;..........:...-
Where Received: _-.q Huntersville ~~viile · 0 Eden · 0 Raleigh
. Courier (Circle): ~ UPS USPS Client Commercial Pace Other ·
c'ustody Seal on Cooler/~ ox Present: 0 yes. ~ Seals intact: D yes .~a-··.
·Packlng.Materlal; 0 Bub_bleWrap ~Bags 0 Non~ Other __ _
Clrcla Thermometer Used~ I~ Gun#~-~ Type of Ice: ~ Blue None ~son loa, ·cooling procee~ has b?gun
IR Gun Bac U • ~565~5 '
Temp·.Correctlon Fa~tor: Add I~. · , . c . ·. . /J ,4
corrected Caolitt Temp.:' _::I . 7 c · · Biological Tissue Is Frozen: ·Yes ·No NIA I.·. :Oat~ and.h'li,7'.J.!/~" . (J('f..)fjJ' · · . · . contents~ Temp should be above free1!lng to 6'C · . Comments: . //
Chain. of Custody Present: ~No ONIA 1.
,. ..
Chain of Custody_Fllled Out: ~No DNIA 2.
Chain of Custody. Relinquished: Jih'ii'SONo o~iA 3.
Sampler .Name & Signature on COC: ~No DNIA 4.
Samples Arrived within Hold i'ime: ~No CJNtA ~-
Short Hold Time Analy-sis (<72tir): ClYes ~N/A 6.
,_ Rt!sh Turn Around Time Requested: O.Yes ONo ~ J.
Sufficient Volunie: "~ONo ON/A 8. ..
correct ConMlners Used: MS[JND DNIA 9; . .
-Pace.Contaln·ers Used: ~No DN/A
Cor:Jialners ln~ot: ~No DNIA 10.
. Filtered volume received for Dissolved tests DYes CINo ~ TJ,
Sample Lab~ls match COC: . ~No ON/A 12.
·Includes date/tlme/ID/Analysls. Matrix: ILJY -·.
All containers needing preeervallon have bean checked. · ~ONo ON/A· rffM ~It containers needing preservation are found to be in ~D ON/A compliance with EP~ recomrpendatlon.
exception~ coliform, TOO, O&G, WJ.ORO (wal!lrl OYes~b '·
lnllfJt When comp!eted
SamJ>_Ies checked for dechlorination: LIVe& CINo ~ 14.
Headspace In VOA VIals ( >6mm): · ' QYes ~ON/A 15.
Trip Blank Present: DYes ONo r 16.
Trip Blank custody Seals Present DYes DNo WA
Pace Trip Blank Lot #(If purchased):
Client Notification/ Resolution: Field Data Required? Y I N
Person Contacted: _______ _..;,_ ____ Date/Time: ____ ....._ __
Comments/Resolution: __________ ___,... ______________________ _
' SCURF Review: SRF Review: Date: I-.\.IF-1-'-'+' ............
Note: When~ver there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent.to the North C
Certlfica!lon Offloe ( i.e out of hqid, Incorrect presmvatlve, out of temp, inoorrect containers)
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