Heatcraft GW Monitoring Report - Sept 2015

Hazardous Waste Section
File Room Document Transmittal Sheet

Name: Mary Siedlecki
EPA ID Number: NCD057451270
Facility Name: Former Heatcraft/Daikin Applied Americas
Document Group: Groundwater
Document Type: Groundwater Monitoring Report
Description: March 2015 Semi-Annual Groundwater Monitoring Report
Date of Document: 04/01/2015
Author(s) of Doc: Corr Environmental Resources

____________________________________________________________________________
File Room Use Only
Date Received
Date Scanned Scanner’s Initials:

Report Number:31500424
Client Project:HeatCraft
Laboratory Report of Analysis
Ray Roblin
CORR ENVIRONMENTAL
4609 Candlestick Drive
Garland, TX 75043
Dear Ray Roblin,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be
retained in our files for a period of five years in the event they are required for future reference. All results are
intended to be used in their entirety and SGS is not responsible for use of less than the complete report. Any
samples submitted to our laboratory will be retained for a maximum of thirty (30) days from the date of this report
unless other arrangements are requested.
If there are any questions about the report or services performed during this project, please call Amy J. Boehm at
[phone]. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America Inc.
__________________________________________________________________
Amy J. Boehm Date
Project Manager
[e-mail]
To:
Print Date: 03/24/2015 N.C. Certification # 481
This document is issued by the Company under its General Conditions of Service accessible at http://www.sgs.com/en/Terms-and-Conditions.htm. Attention is drawn
to the limitation of liability, indemnification and jurisdiction issues defined therein.
Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of
Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their
rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful
and offenders may be prosecuted to the fullest extent of the law.
WO# 31500424 Page 1 of 102
Laboratory Qualifiers
Report Definitions
DL Method, Instrument, or Estimated Detection Limit per Analytical Method
CL Control Limits for the recovery result of a parameter
LOQ Reporting Limit
DF Dilution Factor
RPD Relative Percent Difference
LCS(D) Laboratory Control Spike (Duplicate)
MS(D) Matrix Spike (Duplicate)
MB Method Blank
Qualifier Definitions
* Recovery or RPD outside of control limits
B Analyte was detected in the Lab Method Blank at a level above the LOQ
U Undetected (Reported as ND or < DL)
J Estimated Concentration.
E Amount detected is greater than the Upper Calibration Limit
TIC Tentatively Identified Compound
ND Not Detected
P RPD > 40% between results of dual columns
D Spike or surrogate was diluted out in order to achieve a parameter result within instrument calibration
range
Samples requiring manual integrations for various congeners and/or standards are marked and dated by the analyst. A
code definition is provided below:
M1 Mis-identified peak
M2 Software did not integrate peak
M3 Incorrect baseline construction (i.e. not all of peak included; two peaks integrated as one)
M4 Pattern integration required (i.e. DRO, GRO, PCB, Toxaphene and Technical Chlordane)
M5 Other - Explained in case narrative
Note Results pages that include a value for "Solids (%)" have been adjusted for moisture content.
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 2 of 102
Sample Summary
Client Sample ID Lab Sample ID Collected Received Matrix
CAM-1R 31500424001 03/09/2015 09:25 03/10/2015 15:50 Water
OSW-6C 31500424002 03/09/2015 10:20 03/10/2015 15:50 Water
OSW-6B 31500424003 03/09/2015 10:45 03/10/2015 15:50 Water
OSW-6A 31500424004 03/09/2015 11:05 03/10/2015 15:50 Water
OSW-5C 31500424005 03/09/2015 11:30 03/10/2015 15:50 Water
OSW-5B 31500424006 03/09/2015 12:00 03/10/2015 15:50 Water
OSW-5A 31500424007 03/09/2015 12:20 03/10/2015 15:50 Water
OSW-1 31500424008 03/09/2015 15:30 03/10/2015 15:50 Water
FNW-3A 31500424009 03/09/2015 15:50 03/10/2015 15:50 Water
FNW-4A 31500424010 03/09/2015 16:10 03/10/2015 15:50 Water
OSW-8C 31500424011 03/10/2015 13:50 03/10/2015 15:50 Water
OSW-8B 31500424012 03/10/2015 14:10 03/10/2015 15:50 Water
OSW-4 31500424013 03/10/2015 14:40 03/10/2015 15:50 Water
OSW-2 31500424014 03/10/2015 15:00 03/10/2015 15:50 Water
FW-1C 31500424015 03/10/2015 15:20 03/10/2015 15:50 Water
FWD-1C 31500424016 03/10/2015 15:25 03/10/2015 15:50 Water
Trip Blank 31500424017 03/10/2015 15:50 Water
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 3 of 102
Case Narrative
The nitrate analysis for sample OSW-5C was run 10 minutes outside the 48-hour hold time.
The nitrate analysis for sample OSW-6C was run 1 hour 34 minutes outside the 48-hour hold time.
FNW-4A
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
LCS for HBN 69651 [VXX/5590]
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
LCSD for HBN 69651 [VXX/5590]
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
MB for HBN 69651 [VXX/5590]
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
OSW-2
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 4 of 102
Detectable Results Summary
Client Sample ID: CAM-1R
Lab Sample ID: 31500424001-A UnitsParameterResult
cis-1,2-Dichloroethene ug/LSW-846 8260B 30.8
Client Sample ID: OSW-6C
Lab Sample ID: 31500424002-D UnitsParameterResult
Sulfate mg/LEPA 300.0 4.44
1,1-Dichloroethane ug/LSW-846 8260B 31.8
1,1-Dichloroethene ug/L28.9
Trichloroethene ug/L2.60
Vinyl chloride ug/L37.2
cis-1,2-Dichloroethene ug/L1100
trans-1,2-Dichloroethene ug/L14.1
Client Sample ID: OSW-6B
Lab Sample ID: 31500424003-B UnitsParameterResult
1,1-Dichloroethane ug/LSW-846 8260B 1.34
1,1-Dichloroethene ug/L1.26
Vinyl chloride ug/L1.42
cis-1,2-Dichloroethene ug/L52.6
Client Sample ID: OSW-5C
Lab Sample ID: 31500424005-F UnitsParameterResult
Sulfate mg/LEPA 300.0 35.1
1,1-Dichloroethane ug/LSW-846 8260B 135
1,1-Dichloroethene ug/L71.8
Vinyl chloride ug/L1870
cis-1,2-Dichloroethene ug/L2190
trans-1,2-Dichloroethene ug/L6.48
1,4 Dioxane ug/LSW-846 8270D 80.4
Client Sample ID: OSW-5B
Lab Sample ID: 31500424006-A UnitsParameterResult
1,1,1-Trichloroethane ug/LSW-846 8260B 5.37
1,1-Dichloroethane ug/L33.1
1,1-Dichloroethene ug/L49.6
Trichloroethene ug/L4.77
Vinyl chloride ug/L58.0
cis-1,2-Dichloroethene ug/L388
trans-1,2-Dichloroethene ug/L2.22
Client Sample ID: OSW-5A
Lab Sample ID: 31500424007-A UnitsParameterResult
1,1,1-Trichloroethane ug/LSW-846 8260B 6.67
1,1-Dichloroethane ug/L32.8
1,1-Dichloroethene ug/L51.0
Trichloroethene ug/L1.99
Vinyl chloride ug/L68.8
cis-1,2-Dichloroethene ug/L378
trans-1,2-Dichloroethene ug/L2.24
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 5 of 102
Detectable Results Summary
Client Sample ID: OSW-1
Lab Sample ID: 31500424008-D UnitsParameterResult
Sulfate mg/LEPA 300.0 44.2
1,1-Dichloroethane ug/LSW-846 8260B 172
1,1-Dichloroethene ug/L94.3
Trichloroethene ug/L10.8
Vinyl chloride ug/L2240
cis-1,2-Dichloroethene ug/L2250
trans-1,2-Dichloroethene ug/L8.82
Client Sample ID: FNW-3A
Lab Sample ID: 31500424009-D UnitsParameterResult
Sulfate mg/LEPA 300.0 82.3
1,1,1-Trichloroethane ug/LSW-846 8260B 764
1,1-Dichloroethane ug/L592
1,1-Dichloroethene ug/L1470
Trichloroethene ug/L1470
Vinyl chloride ug/L1140
cis-1,2-Dichloroethene ug/L10300
trans-1,2-Dichloroethene ug/L88.1
Client Sample ID: FNW-4A
Lab Sample ID: 31500424010-F UnitsParameterResult
Sulfate mg/LEPA 300.0 5.37
1,1,1-Trichloroethane ug/LSW-846 8260B 38.0
1,1-Dichloroethane ug/L126
1,1-Dichloroethene ug/L140
Trichloroethene ug/L936
Vinyl chloride ug/L4.59
cis-1,2-Dichloroethene ug/L282
1,4 Dioxane ug/LSW-846 8270D 2.37
Client Sample ID: OSW-4
Lab Sample ID: 31500424013-F UnitsParameterResult
Sulfate mg/LEPA 300.0 17.3
1,1-Dichloroethane ug/LSW-846 8260B 28.1
1,1-Dichloroethene ug/L39.5
Vinyl chloride ug/L10.3
cis-1,2-Dichloroethene ug/L505
1,4 Dioxane ug/LSW-846 8270D 39.0
Client Sample ID: OSW-2
Lab Sample ID: 31500424014-F UnitsParameterResult
Sulfate mg/LEPA 300.0 8.80
1,1-Dichloroethane ug/LSW-846 8260B 69.6
1,1-Dichloroethene ug/L69.5
Chloroethane ug/L1.24
Vinyl chloride ug/L116
cis-1,2-Dichloroethene ug/L1080
trans-1,2-Dichloroethene ug/L4.45
1,4 Dioxane ug/LSW-846 8270D 73.4
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 6 of 102
Detectable Results Summary
Client Sample ID: FW-1C
Lab Sample ID: 31500424015-F UnitsParameterResult
Sulfate mg/LEPA 300.0 14.2
1,1-Dichloroethane ug/LSW-846 8260B 47.1
1,1-Dichloroethene ug/L24.4
Vinyl chloride ug/L82.0
cis-1,2-Dichloroethene ug/L747
trans-1,2-Dichloroethene ug/L3.44
1,4 Dioxane ug/LSW-846 8270D 80.6
Client Sample ID: FWD-1C
Lab Sample ID: 31500424016-A UnitsParameterResult
1,1-Dichloroethane ug/LSW-846 8260B 45.6
1,1-Dichloroethene ug/L23.5
Vinyl chloride ug/L73.2
cis-1,2-Dichloroethene ug/L667
trans-1,2-Dichloroethene ug/L3.45
Client Sample ID: Trip Blank
Lab Sample ID: 31500424017-A UnitsParameterResult
Toluene ug/LSW-846 8260B 1.13
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 7 of 102
Client Sample ID: CAM-1R
Client Project ID: HeatCraft
Lab Sample ID: 31500424001-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 09:25
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CAM-1R
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 17:05
1,1,1-Trichloroethane ND ug/L 11.00 03/12/2015 17:05
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 17:05
1,1,2-Trichloroethane ND ug/L 11.00 03/12/2015 17:05
1,1-Dichloroethane ND ug/L 11.00 03/12/2015 17:05
1,1-Dichloroethene ND ug/L 11.00 03/12/2015 17:05
1,1-Dichloropropene ND ug/L 11.00 03/12/2015 17:05
1,2,3-Trichlorobenzene ND ug/L 11.00 03/12/2015 17:05
1,2,3-Trichloropropane ND ug/L 11.00 03/12/2015 17:05
1,2,4-Trichlorobenzene ND ug/L 11.00 03/12/2015 17:05
1,2,4-Trimethylbenzene ND ug/L 11.00 03/12/2015 17:05
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/12/2015 17:05
1,2-Dibromoethane ND ug/L 11.00 03/12/2015 17:05
1,2-Dichlorobenzene ND ug/L 11.00 03/12/2015 17:05
1,2-Dichloroethane ND ug/L 11.00 03/12/2015 17:05
1,2-Dichloropropane ND ug/L 11.00 03/12/2015 17:05
1,3,5-Trimethylbenzene ND ug/L 11.00 03/12/2015 17:05
1,3-Dichlorobenzene ND ug/L 11.00 03/12/2015 17:05
1,3-Dichloropropane ND ug/L 11.00 03/12/2015 17:05
1,4-Dichlorobenzene ND ug/L 11.00 03/12/2015 17:05
2,2-Dichloropropane ND ug/L 11.00 03/12/2015 17:05
2-Butanone ND ug/L 125.0 03/12/2015 17:05
2-Chlorotoluene ND ug/L 11.00 03/12/2015 17:05
2-Hexanone ND ug/L 15.00 03/12/2015 17:05
4-Chlorotoluene ND ug/L 11.00 03/12/2015 17:05
4-Isopropyltoluene ND ug/L 11.00 03/12/2015 17:05
4-Methyl-2-pentanone ND ug/L 15.00 03/12/2015 17:05
Acetone ND ug/L 125.0 03/12/2015 17:05
Benzene ND ug/L 11.00 03/12/2015 17:05
Bromobenzene ND ug/L 11.00 03/12/2015 17:05
Bromochloromethane ND ug/L 11.00 03/12/2015 17:05
Bromodichloromethane ND ug/L 11.00 03/12/2015 17:05
Bromoform ND ug/L 11.00 03/12/2015 17:05
Bromomethane ND ug/L 11.00 03/12/2015 17:05
n-Butylbenzene ND ug/L 11.00 03/12/2015 17:05
Carbon disulfide ND ug/L 11.00 03/12/2015 17:05
Carbon tetrachloride ND ug/L 11.00 03/12/2015 17:05
Chlorobenzene ND ug/L 11.00 03/12/2015 17:05
Chloroethane ND ug/L 11.00 03/12/2015 17:05
Chloroform ND ug/L 11.00 03/12/2015 17:05
Chloromethane ND ug/L 11.00 03/12/2015 17:05
Dibromochloromethane ND ug/L 11.00 03/12/2015 17:05
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 8 of 102
Client Sample ID: CAM-1R
Client Project ID: HeatCraft
Lab Sample ID: 31500424001-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 09:25
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CAM-1R
Date Analyzed
Dibromomethane ND ug/L 11.00 03/12/2015 17:05
Dichlorodifluoromethane ND ug/L 15.00 03/12/2015 17:05
cis-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 17:05
trans-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 17:05
Diisopropyl Ether ND ug/L 11.00 03/12/2015 17:05
Ethyl Benzene ND ug/L 11.00 03/12/2015 17:05
Hexachlorobutadiene ND ug/L 11.00 03/12/2015 17:05
Isopropylbenzene (Cumene) ND ug/L 11.00 03/12/2015 17:05
Methyl iodide ND ug/L 11.00 03/12/2015 17:05
Methylene chloride ND ug/L 15.00 03/12/2015 17:05
Naphthalene ND ug/L 11.00 03/12/2015 17:05
Styrene ND ug/L 11.00 03/12/2015 17:05
Tetrachloroethene ND ug/L 11.00 03/12/2015 17:05
Toluene ND ug/L 11.00 03/12/2015 17:05
Trichloroethene ND ug/L 11.00 03/12/2015 17:05
Trichlorofluoromethane ND ug/L 11.00 03/12/2015 17:05
Vinyl chloride ND ug/L 11.00 03/12/2015 17:05
Xylene (total)ND ug/L 12.00 03/12/2015 17:05
cis-1,2-Dichloroethene 30.8 ug/L 11.00 03/12/2015 17:05
m,p-Xylene ND ug/L 12.00 03/12/2015 17:05
n-Propylbenzene ND ug/L 11.00 03/12/2015 17:05
o-Xylene ND ug/L 11.00 03/12/2015 17:05
sec-Butylbenzene ND ug/L 11.00 03/12/2015 17:05
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/12/2015 17:05
tert-Butylbenzene ND ug/L 11.00 03/12/2015 17:05
trans-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 17:05
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/12/2015 17:05
Surrogates
1,2-Dichloroethane-d4 102 % 164.0-140 03/12/2015 17:05
4-Bromofluorobenzene 96.0 % 185.0-115 03/12/2015 17:05
Toluene d8 95.0 % 182.0-117 03/12/2015 17:05
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/12/2015 16:18
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 9 of 102
Client Sample ID: CAM-1R
Client Project ID: HeatCraft
Lab Sample ID: 31500424001-D
Lab Project ID: 31500424
Collection Date: 03/09/2015 09:25
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of CAM-1R
Date Analyzed
1,4 Dioxane ND ug/L 12.24 03/17/2015 12:01
Surrogates
Nitrobenzene-d5 62.3 % 150.0-150 03/17/2015 12:01
Batch Information
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Prep Initial Wt./Vol.: 891 mL
Prep Extract Vol: 1 mL
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 10 of 102
Client Sample ID: OSW-6C
Client Project ID: HeatCraft
Lab Sample ID: 31500424002-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 10:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-6C
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 22.00 03/13/2015 16:51
1,1,1-Trichloroethane ND ug/L 22.00 03/13/2015 16:51
1,1,2,2-Tetrachloroethane ND ug/L 22.00 03/13/2015 16:51
1,1,2-Trichloroethane ND ug/L 22.00 03/13/2015 16:51
1,1-Dichloroethane 31.8 ug/L 22.00 03/13/2015 16:51
1,1-Dichloroethene 28.9 ug/L 22.00 03/13/2015 16:51
1,1-Dichloropropene ND ug/L 22.00 03/13/2015 16:51
1,2,3-Trichlorobenzene ND ug/L 22.00 03/13/2015 16:51
1,2,3-Trichloropropane ND ug/L 22.00 03/13/2015 16:51
1,2,4-Trichlorobenzene ND ug/L 22.00 03/13/2015 16:51
1,2,4-Trimethylbenzene ND ug/L 22.00 03/13/2015 16:51
1,2-Dibromo-3-chloropropane ND ug/L 210.0 03/13/2015 16:51
1,2-Dibromoethane ND ug/L 22.00 03/13/2015 16:51
1,2-Dichlorobenzene ND ug/L 22.00 03/13/2015 16:51
1,2-Dichloroethane ND ug/L 22.00 03/13/2015 16:51
1,2-Dichloropropane ND ug/L 22.00 03/13/2015 16:51
1,3,5-Trimethylbenzene ND ug/L 22.00 03/13/2015 16:51
1,3-Dichlorobenzene ND ug/L 22.00 03/13/2015 16:51
1,3-Dichloropropane ND ug/L 22.00 03/13/2015 16:51
1,4-Dichlorobenzene ND ug/L 22.00 03/13/2015 16:51
2,2-Dichloropropane ND ug/L 22.00 03/13/2015 16:51
2-Butanone ND ug/L 250.0 03/13/2015 16:51
2-Chlorotoluene ND ug/L 22.00 03/13/2015 16:51
2-Hexanone ND ug/L 210.0 03/13/2015 16:51
4-Chlorotoluene ND ug/L 22.00 03/13/2015 16:51
4-Isopropyltoluene ND ug/L 22.00 03/13/2015 16:51
4-Methyl-2-pentanone ND ug/L 210.0 03/13/2015 16:51
Acetone ND ug/L 250.0 03/13/2015 16:51
Benzene ND ug/L 22.00 03/13/2015 16:51
Bromobenzene ND ug/L 22.00 03/13/2015 16:51
Bromochloromethane ND ug/L 22.00 03/13/2015 16:51
Bromodichloromethane ND ug/L 22.00 03/13/2015 16:51
Bromoform ND ug/L 22.00 03/13/2015 16:51
Bromomethane ND ug/L 22.00 03/13/2015 16:51
n-Butylbenzene ND ug/L 22.00 03/13/2015 16:51
Carbon disulfide ND ug/L 22.00 03/13/2015 16:51
Carbon tetrachloride ND ug/L 22.00 03/13/2015 16:51
Chlorobenzene ND ug/L 22.00 03/13/2015 16:51
Chloroethane ND ug/L 22.00 03/13/2015 16:51
Chloroform ND ug/L 22.00 03/13/2015 16:51
Chloromethane ND ug/L 22.00 03/13/2015 16:51
Dibromochloromethane ND ug/L 22.00 03/13/2015 16:51
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 11 of 102
Client Sample ID: OSW-6C
Client Project ID: HeatCraft
Lab Sample ID: 31500424002-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 10:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-6C
Date Analyzed
Dibromomethane ND ug/L 22.00 03/13/2015 16:51
Dichlorodifluoromethane ND ug/L 210.0 03/13/2015 16:51
cis-1,3-Dichloropropene ND ug/L 22.00 03/13/2015 16:51
trans-1,3-Dichloropropene ND ug/L 22.00 03/13/2015 16:51
Diisopropyl Ether ND ug/L 22.00 03/13/2015 16:51
Ethyl Benzene ND ug/L 22.00 03/13/2015 16:51
Hexachlorobutadiene ND ug/L 22.00 03/13/2015 16:51
Isopropylbenzene (Cumene) ND ug/L 22.00 03/13/2015 16:51
Methyl iodide ND ug/L 22.00 03/13/2015 16:51
Methylene chloride ND ug/L 210.0 03/13/2015 16:51
Naphthalene ND ug/L 22.00 03/13/2015 16:51
Styrene ND ug/L 22.00 03/13/2015 16:51
Tetrachloroethene ND ug/L 22.00 03/13/2015 16:51
Toluene ND ug/L 22.00 03/13/2015 16:51
Trichloroethene 2.60 ug/L 22.00 03/13/2015 16:51
Trichlorofluoromethane ND ug/L 22.00 03/13/2015 16:51
Vinyl chloride 37.2 ug/L 22.00 03/13/2015 16:51
Xylene (total)ND ug/L 24.00 03/13/2015 16:51
cis-1,2-Dichloroethene 1100 ug/L 100100 03/12/2015 23:17
m,p-Xylene ND ug/L 24.00 03/13/2015 16:51
n-Propylbenzene ND ug/L 22.00 03/13/2015 16:51
o-Xylene ND ug/L 22.00 03/13/2015 16:51
sec-Butylbenzene ND ug/L 22.00 03/13/2015 16:51
tert-Butyl methyl ether (MTBE) ND ug/L 22.00 03/13/2015 16:51
tert-Butylbenzene ND ug/L 22.00 03/13/2015 16:51
trans-1,2-Dichloroethene 14.1 ug/L 22.00 03/13/2015 16:51
trans-1,4-Dichloro-2-butene ND ug/L 210.0 03/13/2015 16:51
Surrogates
1,2-Dichloroethane-d4 102 % 264.0-140 03/13/2015 16:51
4-Bromofluorobenzene 95.0 % 285.0-115 03/13/2015 16:51
Toluene d8 89.0 % 282.0-117 03/13/2015 16:51
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 12 of 102
Client Sample ID: OSW-6C
Client Project ID: HeatCraft
Lab Sample ID: 31500424002-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 10:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-6C
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 13 of 102
Client Sample ID: OSW-6C
Client Project ID: HeatCraft
Lab Sample ID: 31500424002-D
Lab Project ID: 31500424
Collection Date: 03/09/2015 10:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by EPA 300.0
Results of OSW-6C
Date Analyzed
Sulfate 4.44 mg/L 11.00 03/11/2015 11:54
Nitrate as N ND mg/L 10.300 03/11/2015 11:54
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 11:54
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 14 of 102
Client Sample ID: OSW-6B
Client Project ID: HeatCraft
Lab Sample ID: 31500424003-B
Lab Project ID: 31500424
Collection Date: 03/09/2015 10:45
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-6B
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 11:02
1,1,1-Trichloroethane ND ug/L 11.00 03/13/2015 11:02
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 11:02
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 11:02
1,1-Dichloroethane 1.34 ug/L 11.00 03/13/2015 11:02
1,1-Dichloroethene 1.26 ug/L 11.00 03/13/2015 11:02
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 11:02
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 11:02
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 11:02
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 11:02
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 11:02
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 11:02
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 11:02
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 11:02
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 11:02
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 11:02
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 11:02
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 11:02
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 11:02
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 11:02
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 11:02
2-Butanone ND ug/L 125.0 03/13/2015 11:02
2-Chlorotoluene ND ug/L 11.00 03/13/2015 11:02
2-Hexanone ND ug/L 15.00 03/13/2015 11:02
4-Chlorotoluene ND ug/L 11.00 03/13/2015 11:02
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 11:02
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 11:02
Acetone ND ug/L 125.0 03/13/2015 11:02
Benzene ND ug/L 11.00 03/13/2015 11:02
Bromobenzene ND ug/L 11.00 03/13/2015 11:02
Bromochloromethane ND ug/L 11.00 03/13/2015 11:02
Bromodichloromethane ND ug/L 11.00 03/13/2015 11:02
Bromoform ND ug/L 11.00 03/13/2015 11:02
Bromomethane ND ug/L 11.00 03/13/2015 11:02
n-Butylbenzene ND ug/L 11.00 03/13/2015 11:02
Carbon disulfide ND ug/L 11.00 03/13/2015 11:02
Carbon tetrachloride ND ug/L 11.00 03/13/2015 11:02
Chlorobenzene ND ug/L 11.00 03/13/2015 11:02
Chloroethane ND ug/L 11.00 03/13/2015 11:02
Chloroform ND ug/L 11.00 03/13/2015 11:02
Chloromethane ND ug/L 11.00 03/13/2015 11:02
Dibromochloromethane ND ug/L 11.00 03/13/2015 11:02
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 15 of 102
Client Sample ID: OSW-6B
Client Project ID: HeatCraft
Lab Sample ID: 31500424003-B
Lab Project ID: 31500424
Collection Date: 03/09/2015 10:45
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-6B
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 11:02
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 11:02
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 11:02
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 11:02
Diisopropyl Ether ND ug/L 11.00 03/13/2015 11:02
Ethyl Benzene ND ug/L 11.00 03/13/2015 11:02
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 11:02
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 11:02
Methyl iodide ND ug/L 11.00 03/13/2015 11:02
Methylene chloride ND ug/L 15.00 03/13/2015 11:02
Naphthalene ND ug/L 11.00 03/13/2015 11:02
Styrene ND ug/L 11.00 03/13/2015 11:02
Tetrachloroethene ND ug/L 11.00 03/13/2015 11:02
Toluene ND ug/L 11.00 03/13/2015 11:02
Trichloroethene ND ug/L 11.00 03/13/2015 11:02
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 11:02
Vinyl chloride 1.42 ug/L 11.00 03/13/2015 11:02
Xylene (total)ND ug/L 12.00 03/13/2015 11:02
cis-1,2-Dichloroethene 52.6 ug/L 11.00 03/13/2015 11:02
m,p-Xylene ND ug/L 12.00 03/13/2015 11:02
n-Propylbenzene ND ug/L 11.00 03/13/2015 11:02
o-Xylene ND ug/L 11.00 03/13/2015 11:02
sec-Butylbenzene ND ug/L 11.00 03/13/2015 11:02
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 11:02
tert-Butylbenzene ND ug/L 11.00 03/13/2015 11:02
trans-1,2-Dichloroethene ND ug/L 11.00 03/13/2015 11:02
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 11:02
Surrogates
1,2-Dichloroethane-d4 101 % 164.0-140 03/13/2015 11:02
4-Bromofluorobenzene 95.0 % 185.0-115 03/13/2015 11:02
Toluene d8 92.0 % 182.0-117 03/13/2015 11:02
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 16 of 102
Client Sample ID: OSW-6A
Client Project ID: HeatCraft
Lab Sample ID: 31500424004-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 11:05
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-6A
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 17:30
1,1,1-Trichloroethane ND ug/L 11.00 03/12/2015 17:30
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 17:30
1,1,2-Trichloroethane ND ug/L 11.00 03/12/2015 17:30
1,1-Dichloroethane ND ug/L 11.00 03/12/2015 17:30
1,1-Dichloroethene ND ug/L 11.00 03/12/2015 17:30
1,1-Dichloropropene ND ug/L 11.00 03/12/2015 17:30
1,2,3-Trichlorobenzene ND ug/L 11.00 03/12/2015 17:30
1,2,3-Trichloropropane ND ug/L 11.00 03/12/2015 17:30
1,2,4-Trichlorobenzene ND ug/L 11.00 03/12/2015 17:30
1,2,4-Trimethylbenzene ND ug/L 11.00 03/12/2015 17:30
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/12/2015 17:30
1,2-Dibromoethane ND ug/L 11.00 03/12/2015 17:30
1,2-Dichlorobenzene ND ug/L 11.00 03/12/2015 17:30
1,2-Dichloroethane ND ug/L 11.00 03/12/2015 17:30
1,2-Dichloropropane ND ug/L 11.00 03/12/2015 17:30
1,3,5-Trimethylbenzene ND ug/L 11.00 03/12/2015 17:30
1,3-Dichlorobenzene ND ug/L 11.00 03/12/2015 17:30
1,3-Dichloropropane ND ug/L 11.00 03/12/2015 17:30
1,4-Dichlorobenzene ND ug/L 11.00 03/12/2015 17:30
2,2-Dichloropropane ND ug/L 11.00 03/12/2015 17:30
2-Butanone ND ug/L 125.0 03/12/2015 17:30
2-Chlorotoluene ND ug/L 11.00 03/12/2015 17:30
2-Hexanone ND ug/L 15.00 03/12/2015 17:30
4-Chlorotoluene ND ug/L 11.00 03/12/2015 17:30
4-Isopropyltoluene ND ug/L 11.00 03/12/2015 17:30
4-Methyl-2-pentanone ND ug/L 15.00 03/12/2015 17:30
Acetone ND ug/L 125.0 03/12/2015 17:30
Benzene ND ug/L 11.00 03/12/2015 17:30
Bromobenzene ND ug/L 11.00 03/12/2015 17:30
Bromochloromethane ND ug/L 11.00 03/12/2015 17:30
Bromodichloromethane ND ug/L 11.00 03/12/2015 17:30
Bromoform ND ug/L 11.00 03/12/2015 17:30
Bromomethane ND ug/L 11.00 03/12/2015 17:30
n-Butylbenzene ND ug/L 11.00 03/12/2015 17:30
Carbon disulfide ND ug/L 11.00 03/12/2015 17:30
Carbon tetrachloride ND ug/L 11.00 03/12/2015 17:30
Chlorobenzene ND ug/L 11.00 03/12/2015 17:30
Chloroethane ND ug/L 11.00 03/12/2015 17:30
Chloroform ND ug/L 11.00 03/12/2015 17:30
Chloromethane ND ug/L 11.00 03/12/2015 17:30
Dibromochloromethane ND ug/L 11.00 03/12/2015 17:30
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 17 of 102
Client Sample ID: OSW-6A
Client Project ID: HeatCraft
Lab Sample ID: 31500424004-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 11:05
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-6A
Date Analyzed
Dibromomethane ND ug/L 11.00 03/12/2015 17:30
Dichlorodifluoromethane ND ug/L 15.00 03/12/2015 17:30
cis-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 17:30
trans-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 17:30
Diisopropyl Ether ND ug/L 11.00 03/12/2015 17:30
Ethyl Benzene ND ug/L 11.00 03/12/2015 17:30
Hexachlorobutadiene ND ug/L 11.00 03/12/2015 17:30
Isopropylbenzene (Cumene) ND ug/L 11.00 03/12/2015 17:30
Methyl iodide ND ug/L 11.00 03/12/2015 17:30
Methylene chloride ND ug/L 15.00 03/12/2015 17:30
Naphthalene ND ug/L 11.00 03/12/2015 17:30
Styrene ND ug/L 11.00 03/12/2015 17:30
Tetrachloroethene ND ug/L 11.00 03/12/2015 17:30
Toluene ND ug/L 11.00 03/12/2015 17:30
Trichloroethene ND ug/L 11.00 03/12/2015 17:30
Trichlorofluoromethane ND ug/L 11.00 03/12/2015 17:30
Vinyl chloride ND ug/L 11.00 03/12/2015 17:30
Xylene (total)ND ug/L 12.00 03/12/2015 17:30
cis-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 17:30
m,p-Xylene ND ug/L 12.00 03/12/2015 17:30
n-Propylbenzene ND ug/L 11.00 03/12/2015 17:30
o-Xylene ND ug/L 11.00 03/12/2015 17:30
sec-Butylbenzene ND ug/L 11.00 03/12/2015 17:30
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/12/2015 17:30
tert-Butylbenzene ND ug/L 11.00 03/12/2015 17:30
trans-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 17:30
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/12/2015 17:30
Surrogates
1,2-Dichloroethane-d4 102 % 164.0-140 03/12/2015 17:30
4-Bromofluorobenzene 96.0 % 185.0-115 03/12/2015 17:30
Toluene d8 95.0 % 182.0-117 03/12/2015 17:30
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/12/2015 16:18
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 18 of 102
Client Sample ID: OSW-5C
Client Project ID: HeatCraft
Lab Sample ID: 31500424005-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 11:30
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-5C
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 44.00 03/13/2015 17:16
1,1,1-Trichloroethane ND ug/L 44.00 03/13/2015 17:16
1,1,2,2-Tetrachloroethane ND ug/L 44.00 03/13/2015 17:16
1,1,2-Trichloroethane ND ug/L 44.00 03/13/2015 17:16
1,1-Dichloroethane 135 ug/L 44.00 03/13/2015 17:16
1,1-Dichloroethene 71.8 ug/L 44.00 03/13/2015 17:16
1,1-Dichloropropene ND ug/L 44.00 03/13/2015 17:16
1,2,3-Trichlorobenzene ND ug/L 44.00 03/13/2015 17:16
1,2,3-Trichloropropane ND ug/L 44.00 03/13/2015 17:16
1,2,4-Trichlorobenzene ND ug/L 44.00 03/13/2015 17:16
1,2,4-Trimethylbenzene ND ug/L 44.00 03/13/2015 17:16
1,2-Dibromo-3-chloropropane ND ug/L 420.0 03/13/2015 17:16
1,2-Dibromoethane ND ug/L 44.00 03/13/2015 17:16
1,2-Dichlorobenzene ND ug/L 44.00 03/13/2015 17:16
1,2-Dichloroethane ND ug/L 44.00 03/13/2015 17:16
1,2-Dichloropropane ND ug/L 44.00 03/13/2015 17:16
1,3,5-Trimethylbenzene ND ug/L 44.00 03/13/2015 17:16
1,3-Dichlorobenzene ND ug/L 44.00 03/13/2015 17:16
1,3-Dichloropropane ND ug/L 44.00 03/13/2015 17:16
1,4-Dichlorobenzene ND ug/L 44.00 03/13/2015 17:16
2,2-Dichloropropane ND ug/L 44.00 03/13/2015 17:16
2-Butanone ND ug/L 4100 03/13/2015 17:16
2-Chlorotoluene ND ug/L 44.00 03/13/2015 17:16
2-Hexanone ND ug/L 420.0 03/13/2015 17:16
4-Chlorotoluene ND ug/L 44.00 03/13/2015 17:16
4-Isopropyltoluene ND ug/L 44.00 03/13/2015 17:16
4-Methyl-2-pentanone ND ug/L 420.0 03/13/2015 17:16
Acetone ND ug/L 4100 03/13/2015 17:16
Benzene ND ug/L 44.00 03/13/2015 17:16
Bromobenzene ND ug/L 44.00 03/13/2015 17:16
Bromochloromethane ND ug/L 44.00 03/13/2015 17:16
Bromodichloromethane ND ug/L 44.00 03/13/2015 17:16
Bromoform ND ug/L 44.00 03/13/2015 17:16
Bromomethane ND ug/L 44.00 03/13/2015 17:16
n-Butylbenzene ND ug/L 44.00 03/13/2015 17:16
Carbon disulfide ND ug/L 44.00 03/13/2015 17:16
Carbon tetrachloride ND ug/L 44.00 03/13/2015 17:16
Chlorobenzene ND ug/L 44.00 03/13/2015 17:16
Chloroethane ND ug/L 44.00 03/13/2015 17:16
Chloroform ND ug/L 44.00 03/13/2015 17:16
Chloromethane ND ug/L 44.00 03/13/2015 17:16
Dibromochloromethane ND ug/L 44.00 03/13/2015 17:16
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 19 of 102
Client Sample ID: OSW-5C
Client Project ID: HeatCraft
Lab Sample ID: 31500424005-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 11:30
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-5C
Date Analyzed
Dibromomethane ND ug/L 44.00 03/13/2015 17:16
Dichlorodifluoromethane ND ug/L 420.0 03/13/2015 17:16
cis-1,3-Dichloropropene ND ug/L 44.00 03/13/2015 17:16
trans-1,3-Dichloropropene ND ug/L 44.00 03/13/2015 17:16
Diisopropyl Ether ND ug/L 44.00 03/13/2015 17:16
Ethyl Benzene ND ug/L 44.00 03/13/2015 17:16
Hexachlorobutadiene ND ug/L 44.00 03/13/2015 17:16
Isopropylbenzene (Cumene) ND ug/L 44.00 03/13/2015 17:16
Methyl iodide ND ug/L 44.00 03/13/2015 17:16
Methylene chloride ND ug/L 420.0 03/13/2015 17:16
Naphthalene ND ug/L 44.00 03/13/2015 17:16
Styrene ND ug/L 44.00 03/13/2015 17:16
Tetrachloroethene ND ug/L 44.00 03/13/2015 17:16
Toluene ND ug/L 44.00 03/13/2015 17:16
Trichloroethene ND ug/L 44.00 03/13/2015 17:16
Trichlorofluoromethane ND ug/L 44.00 03/13/2015 17:16
Vinyl chloride 1870 ug/L 200200 03/13/2015 0:06
Xylene (total)ND ug/L 48.00 03/13/2015 17:16
cis-1,2-Dichloroethene 2190 ug/L 200200 03/13/2015 0:06
m,p-Xylene ND ug/L 48.00 03/13/2015 17:16
n-Propylbenzene ND ug/L 44.00 03/13/2015 17:16
o-Xylene ND ug/L 44.00 03/13/2015 17:16
sec-Butylbenzene ND ug/L 44.00 03/13/2015 17:16
tert-Butyl methyl ether (MTBE) ND ug/L 44.00 03/13/2015 17:16
tert-Butylbenzene ND ug/L 44.00 03/13/2015 17:16
trans-1,2-Dichloroethene 6.48 ug/L 44.00 03/13/2015 17:16
trans-1,4-Dichloro-2-butene ND ug/L 420.0 03/13/2015 17:16
Surrogates
1,2-Dichloroethane-d4 104 % 464.0-140 03/13/2015 17:16
4-Bromofluorobenzene 96.0 % 485.0-115 03/13/2015 17:16
Toluene d8 89.0 % 482.0-117 03/13/2015 17:16
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 20 of 102
Client Sample ID: OSW-5C
Client Project ID: HeatCraft
Lab Sample ID: 31500424005-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 11:30
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-5C
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 21 of 102
Client Sample ID: OSW-5C
Client Project ID: HeatCraft
Lab Sample ID: 31500424005-D
Lab Project ID: 31500424
Collection Date: 03/09/2015 11:30
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of OSW-5C
Date Analyzed
1,4 Dioxane 80.4 ug/L 511.2 03/17/2015 16:37
Surrogates
Nitrobenzene-d5 78.0 % 550.0-150 03/17/2015 16:37
Batch Information
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Prep Initial Wt./Vol.: 891 mL
Prep Extract Vol: 1 mL
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 22 of 102
Client Sample ID: OSW-5C
Client Project ID: HeatCraft
Lab Sample ID: 31500424005-F
Lab Project ID: 31500424
Collection Date: 03/09/2015 11:30
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by EPA 300.0
Results of OSW-5C
Date Analyzed
Sulfate 35.1 mg/L 11.00 03/11/2015 11:40
Nitrate as N ND mg/L 10.300 03/11/2015 11:40
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 11:40
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 23 of 102
Client Sample ID: OSW-5B
Client Project ID: HeatCraft
Lab Sample ID: 31500424006-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 12:00
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-5B
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 15:36
1,1,1-Trichloroethane 5.37 ug/L 11.00 03/13/2015 15:36
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 15:36
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 15:36
1,1-Dichloroethane 33.1 ug/L 11.00 03/13/2015 15:36
1,1-Dichloroethene 49.6 ug/L 11.00 03/13/2015 15:36
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 15:36
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 15:36
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 15:36
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 15:36
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 15:36
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 15:36
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 15:36
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 15:36
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 15:36
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 15:36
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 15:36
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 15:36
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 15:36
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 15:36
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 15:36
2-Butanone ND ug/L 125.0 03/13/2015 15:36
2-Chlorotoluene ND ug/L 11.00 03/13/2015 15:36
2-Hexanone ND ug/L 15.00 03/13/2015 15:36
4-Chlorotoluene ND ug/L 11.00 03/13/2015 15:36
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 15:36
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 15:36
Acetone ND ug/L 125.0 03/13/2015 15:36
Benzene ND ug/L 11.00 03/13/2015 15:36
Bromobenzene ND ug/L 11.00 03/13/2015 15:36
Bromochloromethane ND ug/L 11.00 03/13/2015 15:36
Bromodichloromethane ND ug/L 11.00 03/13/2015 15:36
Bromoform ND ug/L 11.00 03/13/2015 15:36
Bromomethane ND ug/L 11.00 03/13/2015 15:36
n-Butylbenzene ND ug/L 11.00 03/13/2015 15:36
Carbon disulfide ND ug/L 11.00 03/13/2015 15:36
Carbon tetrachloride ND ug/L 11.00 03/13/2015 15:36
Chlorobenzene ND ug/L 11.00 03/13/2015 15:36
Chloroethane ND ug/L 11.00 03/13/2015 15:36
Chloroform ND ug/L 11.00 03/13/2015 15:36
Chloromethane ND ug/L 11.00 03/13/2015 15:36
Dibromochloromethane ND ug/L 11.00 03/13/2015 15:36
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 24 of 102
Client Sample ID: OSW-5B
Client Project ID: HeatCraft
Lab Sample ID: 31500424006-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 12:00
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-5B
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 15:36
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 15:36
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 15:36
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 15:36
Diisopropyl Ether ND ug/L 11.00 03/13/2015 15:36
Ethyl Benzene ND ug/L 11.00 03/13/2015 15:36
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 15:36
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 15:36
Methyl iodide ND ug/L 11.00 03/13/2015 15:36
Methylene chloride ND ug/L 15.00 03/13/2015 15:36
Naphthalene ND ug/L 11.00 03/13/2015 15:36
Styrene ND ug/L 11.00 03/13/2015 15:36
Tetrachloroethene ND ug/L 11.00 03/13/2015 15:36
Toluene ND ug/L 11.00 03/13/2015 15:36
Trichloroethene 4.77 ug/L 11.00 03/13/2015 15:36
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 15:36
Vinyl chloride 58.0 ug/L 2020.0 03/12/2015 20:48
Xylene (total)ND ug/L 12.00 03/13/2015 15:36
cis-1,2-Dichloroethene 388 ug/L 2020.0 03/12/2015 20:48
m,p-Xylene ND ug/L 12.00 03/13/2015 15:36
n-Propylbenzene ND ug/L 11.00 03/13/2015 15:36
o-Xylene ND ug/L 11.00 03/13/2015 15:36
sec-Butylbenzene ND ug/L 11.00 03/13/2015 15:36
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 15:36
tert-Butylbenzene ND ug/L 11.00 03/13/2015 15:36
trans-1,2-Dichloroethene 2.22 ug/L 11.00 03/13/2015 15:36
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 15:36
Surrogates
1,2-Dichloroethane-d4 104 % 164.0-140 03/13/2015 15:36
4-Bromofluorobenzene 95.0 % 185.0-115 03/13/2015 15:36
Toluene d8 90.0 % 182.0-117 03/13/2015 15:36
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 25 of 102
Client Sample ID: OSW-5B
Client Project ID: HeatCraft
Lab Sample ID: 31500424006-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 12:00
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-5B
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 26 of 102
Client Sample ID: OSW-5A
Client Project ID: HeatCraft
Lab Sample ID: 31500424007-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 12:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-5A
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 16:01
1,1,1-Trichloroethane 6.67 ug/L 11.00 03/13/2015 16:01
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 16:01
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 16:01
1,1-Dichloroethane 32.8 ug/L 11.00 03/13/2015 16:01
1,1-Dichloroethene 51.0 ug/L 11.00 03/13/2015 16:01
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 16:01
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 16:01
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 16:01
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 16:01
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 16:01
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 16:01
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 16:01
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 16:01
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 16:01
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 16:01
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 16:01
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 16:01
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 16:01
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 16:01
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 16:01
2-Butanone ND ug/L 125.0 03/13/2015 16:01
2-Chlorotoluene ND ug/L 11.00 03/13/2015 16:01
2-Hexanone ND ug/L 15.00 03/13/2015 16:01
4-Chlorotoluene ND ug/L 11.00 03/13/2015 16:01
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 16:01
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 16:01
Acetone ND ug/L 125.0 03/13/2015 16:01
Benzene ND ug/L 11.00 03/13/2015 16:01
Bromobenzene ND ug/L 11.00 03/13/2015 16:01
Bromochloromethane ND ug/L 11.00 03/13/2015 16:01
Bromodichloromethane ND ug/L 11.00 03/13/2015 16:01
Bromoform ND ug/L 11.00 03/13/2015 16:01
Bromomethane ND ug/L 11.00 03/13/2015 16:01
n-Butylbenzene ND ug/L 11.00 03/13/2015 16:01
Carbon disulfide ND ug/L 11.00 03/13/2015 16:01
Carbon tetrachloride ND ug/L 11.00 03/13/2015 16:01
Chlorobenzene ND ug/L 11.00 03/13/2015 16:01
Chloroethane ND ug/L 11.00 03/13/2015 16:01
Chloroform ND ug/L 11.00 03/13/2015 16:01
Chloromethane ND ug/L 11.00 03/13/2015 16:01
Dibromochloromethane ND ug/L 11.00 03/13/2015 16:01
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 27 of 102
Client Sample ID: OSW-5A
Client Project ID: HeatCraft
Lab Sample ID: 31500424007-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 12:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-5A
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 16:01
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 16:01
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 16:01
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 16:01
Diisopropyl Ether ND ug/L 11.00 03/13/2015 16:01
Ethyl Benzene ND ug/L 11.00 03/13/2015 16:01
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 16:01
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 16:01
Methyl iodide ND ug/L 11.00 03/13/2015 16:01
Methylene chloride ND ug/L 15.00 03/13/2015 16:01
Naphthalene ND ug/L 11.00 03/13/2015 16:01
Styrene ND ug/L 11.00 03/13/2015 16:01
Tetrachloroethene ND ug/L 11.00 03/13/2015 16:01
Toluene ND ug/L 11.00 03/13/2015 16:01
Trichloroethene 1.99 ug/L 11.00 03/13/2015 16:01
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 16:01
Vinyl chloride 68.8 ug/L 11.00 03/13/2015 16:01
Xylene (total)ND ug/L 12.00 03/13/2015 16:01
cis-1,2-Dichloroethene 378 ug/L 2020.0 03/12/2015 21:13
m,p-Xylene ND ug/L 12.00 03/13/2015 16:01
n-Propylbenzene ND ug/L 11.00 03/13/2015 16:01
o-Xylene ND ug/L 11.00 03/13/2015 16:01
sec-Butylbenzene ND ug/L 11.00 03/13/2015 16:01
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 16:01
tert-Butylbenzene ND ug/L 11.00 03/13/2015 16:01
trans-1,2-Dichloroethene 2.24 ug/L 11.00 03/13/2015 16:01
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 16:01
Surrogates
1,2-Dichloroethane-d4 104 % 164.0-140 03/13/2015 16:01
4-Bromofluorobenzene 95.0 % 185.0-115 03/13/2015 16:01
Toluene d8 90.0 % 182.0-117 03/13/2015 16:01
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 28 of 102
Client Sample ID: OSW-5A
Client Project ID: HeatCraft
Lab Sample ID: 31500424007-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 12:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-5A
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 29 of 102
Client Sample ID: OSW-1
Client Project ID: HeatCraft
Lab Sample ID: 31500424008-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 15:30
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-1
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 22.00 03/13/2015 18:30
1,1,1-Trichloroethane ND ug/L 22.00 03/13/2015 18:30
1,1,2,2-Tetrachloroethane ND ug/L 22.00 03/13/2015 18:30
1,1,2-Trichloroethane ND ug/L 22.00 03/13/2015 18:30
1,1-Dichloroethane 172 ug/L 100100 03/12/2015 23:41
1,1-Dichloroethene 94.3 ug/L 22.00 03/13/2015 18:30
1,1-Dichloropropene ND ug/L 22.00 03/13/2015 18:30
1,2,3-Trichlorobenzene ND ug/L 22.00 03/13/2015 18:30
1,2,3-Trichloropropane ND ug/L 22.00 03/13/2015 18:30
1,2,4-Trichlorobenzene ND ug/L 22.00 03/13/2015 18:30
1,2,4-Trimethylbenzene ND ug/L 22.00 03/13/2015 18:30
1,2-Dibromo-3-chloropropane ND ug/L 210.0 03/13/2015 18:30
1,2-Dibromoethane ND ug/L 22.00 03/13/2015 18:30
1,2-Dichlorobenzene ND ug/L 22.00 03/13/2015 18:30
1,2-Dichloroethane ND ug/L 22.00 03/13/2015 18:30
1,2-Dichloropropane ND ug/L 22.00 03/13/2015 18:30
1,3,5-Trimethylbenzene ND ug/L 22.00 03/13/2015 18:30
1,3-Dichlorobenzene ND ug/L 22.00 03/13/2015 18:30
1,3-Dichloropropane ND ug/L 22.00 03/13/2015 18:30
1,4-Dichlorobenzene ND ug/L 22.00 03/13/2015 18:30
2,2-Dichloropropane ND ug/L 22.00 03/13/2015 18:30
2-Butanone ND ug/L 250.0 03/13/2015 18:30
2-Chlorotoluene ND ug/L 22.00 03/13/2015 18:30
2-Hexanone ND ug/L 210.0 03/13/2015 18:30
4-Chlorotoluene ND ug/L 22.00 03/13/2015 18:30
4-Isopropyltoluene ND ug/L 22.00 03/13/2015 18:30
4-Methyl-2-pentanone ND ug/L 210.0 03/13/2015 18:30
Acetone ND ug/L 250.0 03/13/2015 18:30
Benzene ND ug/L 22.00 03/13/2015 18:30
Bromobenzene ND ug/L 22.00 03/13/2015 18:30
Bromochloromethane ND ug/L 22.00 03/13/2015 18:30
Bromodichloromethane ND ug/L 22.00 03/13/2015 18:30
Bromoform ND ug/L 22.00 03/13/2015 18:30
Bromomethane ND ug/L 22.00 03/13/2015 18:30
n-Butylbenzene ND ug/L 22.00 03/13/2015 18:30
Carbon disulfide ND ug/L 22.00 03/13/2015 18:30
Carbon tetrachloride ND ug/L 22.00 03/13/2015 18:30
Chlorobenzene ND ug/L 22.00 03/13/2015 18:30
Chloroethane ND ug/L 22.00 03/13/2015 18:30
Chloroform ND ug/L 22.00 03/13/2015 18:30
Chloromethane ND ug/L 22.00 03/13/2015 18:30
Dibromochloromethane ND ug/L 22.00 03/13/2015 18:30
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 30 of 102
Client Sample ID: OSW-1
Client Project ID: HeatCraft
Lab Sample ID: 31500424008-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 15:30
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-1
Date Analyzed
Dibromomethane ND ug/L 22.00 03/13/2015 18:30
Dichlorodifluoromethane ND ug/L 210.0 03/13/2015 18:30
cis-1,3-Dichloropropene ND ug/L 22.00 03/13/2015 18:30
trans-1,3-Dichloropropene ND ug/L 22.00 03/13/2015 18:30
Diisopropyl Ether ND ug/L 22.00 03/13/2015 18:30
Ethyl Benzene ND ug/L 22.00 03/13/2015 18:30
Hexachlorobutadiene ND ug/L 22.00 03/13/2015 18:30
Isopropylbenzene (Cumene) ND ug/L 22.00 03/13/2015 18:30
Methyl iodide ND ug/L 22.00 03/13/2015 18:30
Methylene chloride ND ug/L 210.0 03/13/2015 18:30
Naphthalene ND ug/L 22.00 03/13/2015 18:30
Styrene ND ug/L 22.00 03/13/2015 18:30
Tetrachloroethene ND ug/L 22.00 03/13/2015 18:30
Toluene ND ug/L 22.00 03/13/2015 18:30
Trichloroethene 10.8 ug/L 22.00 03/13/2015 18:30
Trichlorofluoromethane ND ug/L 22.00 03/13/2015 18:30
Vinyl chloride 2240 ug/L 100100 03/12/2015 23:41
Xylene (total)ND ug/L 24.00 03/13/2015 18:30
cis-1,2-Dichloroethene 2250 ug/L 100100 03/12/2015 23:41
m,p-Xylene ND ug/L 24.00 03/13/2015 18:30
n-Propylbenzene ND ug/L 22.00 03/13/2015 18:30
o-Xylene ND ug/L 22.00 03/13/2015 18:30
sec-Butylbenzene ND ug/L 22.00 03/13/2015 18:30
tert-Butyl methyl ether (MTBE) ND ug/L 22.00 03/13/2015 18:30
tert-Butylbenzene ND ug/L 22.00 03/13/2015 18:30
trans-1,2-Dichloroethene 8.82 ug/L 22.00 03/13/2015 18:30
trans-1,4-Dichloro-2-butene ND ug/L 210.0 03/13/2015 18:30
Surrogates
1,2-Dichloroethane-d4 103 % 264.0-140 03/13/2015 18:30
4-Bromofluorobenzene 97.0 % 285.0-115 03/13/2015 18:30
Toluene d8 88.0 % 282.0-117 03/13/2015 18:30
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 31 of 102
Client Sample ID: OSW-1
Client Project ID: HeatCraft
Lab Sample ID: 31500424008-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 15:30
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-1
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 32 of 102
Client Sample ID: OSW-1
Client Project ID: HeatCraft
Lab Sample ID: 31500424008-D
Lab Project ID: 31500424
Collection Date: 03/09/2015 15:30
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by EPA 300.0
Results of OSW-1
Date Analyzed
Sulfate 44.2 mg/L 11.00 03/11/2015 12:50
Nitrate as N ND mg/L 10.300 03/11/2015 12:50
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 12:50
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 33 of 102
Client Sample ID: FNW-3A
Client Project ID: HeatCraft
Lab Sample ID: 31500424009-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 15:50
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FNW-3A
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 88.00 03/13/2015 18:55
1,1,1-Trichloroethane 764 ug/L 200200 03/13/2015 0:31
1,1,2,2-Tetrachloroethane ND ug/L 88.00 03/13/2015 18:55
1,1,2-Trichloroethane ND ug/L 88.00 03/13/2015 18:55
1,1-Dichloroethane 592 ug/L 200200 03/13/2015 0:31
1,1-Dichloroethene 1470 ug/L 200200 03/13/2015 0:31
1,1-Dichloropropene ND ug/L 88.00 03/13/2015 18:55
1,2,3-Trichlorobenzene ND ug/L 88.00 03/13/2015 18:55
1,2,3-Trichloropropane ND ug/L 88.00 03/13/2015 18:55
1,2,4-Trichlorobenzene ND ug/L 88.00 03/13/2015 18:55
1,2,4-Trimethylbenzene ND ug/L 88.00 03/13/2015 18:55
1,2-Dibromo-3-chloropropane ND ug/L 840.0 03/13/2015 18:55
1,2-Dibromoethane ND ug/L 88.00 03/13/2015 18:55
1,2-Dichlorobenzene ND ug/L 88.00 03/13/2015 18:55
1,2-Dichloroethane ND ug/L 88.00 03/13/2015 18:55
1,2-Dichloropropane ND ug/L 88.00 03/13/2015 18:55
1,3,5-Trimethylbenzene ND ug/L 88.00 03/13/2015 18:55
1,3-Dichlorobenzene ND ug/L 88.00 03/13/2015 18:55
1,3-Dichloropropane ND ug/L 88.00 03/13/2015 18:55
1,4-Dichlorobenzene ND ug/L 88.00 03/13/2015 18:55
2,2-Dichloropropane ND ug/L 88.00 03/13/2015 18:55
2-Butanone ND ug/L 8200 03/13/2015 18:55
2-Chlorotoluene ND ug/L 88.00 03/13/2015 18:55
2-Hexanone ND ug/L 840.0 03/13/2015 18:55
4-Chlorotoluene ND ug/L 88.00 03/13/2015 18:55
4-Isopropyltoluene ND ug/L 88.00 03/13/2015 18:55
4-Methyl-2-pentanone ND ug/L 840.0 03/13/2015 18:55
Acetone ND ug/L 8200 03/13/2015 18:55
Benzene ND ug/L 88.00 03/13/2015 18:55
Bromobenzene ND ug/L 88.00 03/13/2015 18:55
Bromochloromethane ND ug/L 88.00 03/13/2015 18:55
Bromodichloromethane ND ug/L 88.00 03/13/2015 18:55
Bromoform ND ug/L 88.00 03/13/2015 18:55
Bromomethane ND ug/L 88.00 03/13/2015 18:55
n-Butylbenzene ND ug/L 88.00 03/13/2015 18:55
Carbon disulfide ND ug/L 88.00 03/13/2015 18:55
Carbon tetrachloride ND ug/L 88.00 03/13/2015 18:55
Chlorobenzene ND ug/L 88.00 03/13/2015 18:55
Chloroethane ND ug/L 88.00 03/13/2015 18:55
Chloroform ND ug/L 88.00 03/13/2015 18:55
Chloromethane ND ug/L 88.00 03/13/2015 18:55
Dibromochloromethane ND ug/L 88.00 03/13/2015 18:55
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 34 of 102
Client Sample ID: FNW-3A
Client Project ID: HeatCraft
Lab Sample ID: 31500424009-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 15:50
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FNW-3A
Date Analyzed
Dibromomethane ND ug/L 88.00 03/13/2015 18:55
Dichlorodifluoromethane ND ug/L 840.0 03/13/2015 18:55
cis-1,3-Dichloropropene ND ug/L 88.00 03/13/2015 18:55
trans-1,3-Dichloropropene ND ug/L 88.00 03/13/2015 18:55
Diisopropyl Ether ND ug/L 88.00 03/13/2015 18:55
Ethyl Benzene ND ug/L 88.00 03/13/2015 18:55
Hexachlorobutadiene ND ug/L 88.00 03/13/2015 18:55
Isopropylbenzene (Cumene) ND ug/L 88.00 03/13/2015 18:55
Methyl iodide ND ug/L 88.00 03/13/2015 18:55
Methylene chloride ND ug/L 840.0 03/13/2015 18:55
Naphthalene ND ug/L 88.00 03/13/2015 18:55
Styrene ND ug/L 88.00 03/13/2015 18:55
Tetrachloroethene ND ug/L 88.00 03/13/2015 18:55
Toluene ND ug/L 88.00 03/13/2015 18:55
Trichloroethene 1470 ug/L 200200 03/13/2015 0:31
Trichlorofluoromethane ND ug/L 88.00 03/13/2015 18:55
Vinyl chloride 1140 ug/L 200200 03/13/2015 0:31
Xylene (total)ND ug/L 816.0 03/13/2015 18:55
cis-1,2-Dichloroethene 10300 ug/L 200200 03/13/2015 0:31
m,p-Xylene ND ug/L 816.0 03/13/2015 18:55
n-Propylbenzene ND ug/L 88.00 03/13/2015 18:55
o-Xylene ND ug/L 88.00 03/13/2015 18:55
sec-Butylbenzene ND ug/L 88.00 03/13/2015 18:55
tert-Butyl methyl ether (MTBE) ND ug/L 88.00 03/13/2015 18:55
tert-Butylbenzene ND ug/L 88.00 03/13/2015 18:55
trans-1,2-Dichloroethene 88.1 ug/L 88.00 03/13/2015 18:55
trans-1,4-Dichloro-2-butene ND ug/L 840.0 03/13/2015 18:55
Surrogates
1,2-Dichloroethane-d4 103 % 864.0-140 03/13/2015 18:55
4-Bromofluorobenzene 95.0 % 885.0-115 03/13/2015 18:55
Toluene d8 89.0 % 882.0-117 03/13/2015 18:55
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 35 of 102
Client Sample ID: FNW-3A
Client Project ID: HeatCraft
Lab Sample ID: 31500424009-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 15:50
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FNW-3A
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 36 of 102
Client Sample ID: FNW-3A
Client Project ID: HeatCraft
Lab Sample ID: 31500424009-D
Lab Project ID: 31500424
Collection Date: 03/09/2015 15:50
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by EPA 300.0
Results of FNW-3A
Date Analyzed
Sulfate 82.3 mg/L 1010.0 03/13/2015 16:11
Nitrate as N ND mg/L 10.300 03/11/2015 13:04
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 13:04
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Prep Batch: INO3710
Prep Method: EPA 300.0
Prep Date/Time: 03/13/2015 16:11
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3710
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 37 of 102
Client Sample ID: FNW-4A
Client Project ID: HeatCraft
Lab Sample ID: 31500424010-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 16:10
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FNW-4A
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/17/2015 17:58
1,1,1-Trichloroethane 38.0 ug/L 2020.0 03/12/2015 21:38
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/17/2015 17:58
1,1,2-Trichloroethane ND ug/L 11.00 03/17/2015 17:58
1,1-Dichloroethane 126 ug/L 2020.0 03/12/2015 21:38
1,1-Dichloroethene 140 ug/L 2020.0 03/12/2015 21:38
1,1-Dichloropropene ND ug/L 11.00 03/17/2015 17:58
1,2,3-Trichlorobenzene ND ug/L 11.00 03/17/2015 17:58
1,2,3-Trichloropropane ND ug/L 11.00 03/17/2015 17:58
1,2,4-Trichlorobenzene ND ug/L 11.00 03/17/2015 17:58
1,2,4-Trimethylbenzene ND ug/L 11.00 03/17/2015 17:58
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/17/2015 17:58
1,2-Dibromoethane ND ug/L 11.00 03/17/2015 17:58
1,2-Dichlorobenzene ND ug/L 11.00 03/17/2015 17:58
1,2-Dichloroethane ND ug/L 11.00 03/17/2015 17:58
1,2-Dichloropropane ND ug/L 11.00 03/17/2015 17:58
1,3,5-Trimethylbenzene ND ug/L 11.00 03/17/2015 17:58
1,3-Dichlorobenzene ND ug/L 11.00 03/17/2015 17:58
1,3-Dichloropropane ND ug/L 11.00 03/17/2015 17:58
1,4-Dichlorobenzene ND ug/L 11.00 03/17/2015 17:58
2,2-Dichloropropane ND ug/L 11.00 03/17/2015 17:58
2-Butanone ND ug/L 125.0 03/17/2015 17:58
2-Chlorotoluene ND ug/L 11.00 03/17/2015 17:58
2-Hexanone ND ug/L 15.00 03/17/2015 17:58
4-Chlorotoluene ND ug/L 11.00 03/17/2015 17:58
4-Isopropyltoluene ND ug/L 11.00 03/17/2015 17:58
4-Methyl-2-pentanone ND ug/L 15.00 03/17/2015 17:58
Acetone ND ug/L 125.0 03/17/2015 17:58
Benzene ND ug/L 11.00 03/17/2015 17:58
Bromobenzene ND ug/L 11.00 03/17/2015 17:58
Bromochloromethane ND ug/L 11.00 03/17/2015 17:58
Bromodichloromethane ND ug/L 11.00 03/17/2015 17:58
Bromoform ND ug/L 11.00 03/17/2015 17:58
Bromomethane ND ug/L 11.00 03/17/2015 17:58
n-Butylbenzene ND ug/L 11.00 03/17/2015 17:58
Carbon disulfide ND ug/L 11.00 03/17/2015 17:58
Carbon tetrachloride ND ug/L 11.00 03/17/2015 17:58
Chlorobenzene ND ug/L 11.00 03/17/2015 17:58
Chloroethane ND ug/L 11.00 03/17/2015 17:58
Chloroform ND ug/L 11.00 03/17/2015 17:58
Chloromethane ND ug/L 11.00 03/17/2015 17:58
Dibromochloromethane ND ug/L 11.00 03/17/2015 17:58
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 38 of 102
Client Sample ID: FNW-4A
Client Project ID: HeatCraft
Lab Sample ID: 31500424010-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 16:10
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FNW-4A
Date Analyzed
Dibromomethane ND ug/L 11.00 03/17/2015 17:58
Dichlorodifluoromethane ND ug/L 15.00 03/17/2015 17:58
cis-1,3-Dichloropropene ND ug/L 11.00 03/17/2015 17:58
trans-1,3-Dichloropropene ND ug/L 11.00 03/17/2015 17:58
Diisopropyl Ether ND ug/L 11.00 03/17/2015 17:58
Ethyl Benzene ND ug/L 11.00 03/17/2015 17:58
Hexachlorobutadiene ND ug/L 11.00 03/17/2015 17:58
Isopropylbenzene (Cumene) ND ug/L 11.00 03/17/2015 17:58
Methyl iodide ND ug/L 11.00 03/17/2015 17:58
Methylene chloride ND ug/L 15.00 03/17/2015 17:58
Naphthalene ND ug/L 11.00 03/17/2015 17:58
Styrene ND ug/L 11.00 03/17/2015 17:58
Tetrachloroethene ND ug/L 11.00 03/17/2015 17:58
Toluene ND ug/L 11.00 03/17/2015 17:58
Trichloroethene 936 ug/L 2020.0 03/12/2015 21:38
Trichlorofluoromethane ND ug/L 11.00 03/17/2015 17:58
Vinyl chloride 4.59 ug/L 11.00 03/17/2015 17:58
Xylene (total)ND ug/L 12.00 03/17/2015 17:58
cis-1,2-Dichloroethene 282 ug/L 2020.0 03/12/2015 21:38
m,p-Xylene ND ug/L 12.00 03/17/2015 17:58
n-Propylbenzene ND ug/L 11.00 03/17/2015 17:58
o-Xylene ND ug/L 11.00 03/17/2015 17:58
sec-Butylbenzene ND ug/L 11.00 03/17/2015 17:58
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/17/2015 17:58
tert-Butylbenzene ND ug/L 11.00 03/17/2015 17:58
trans-1,2-Dichloroethene ND ug/L 11.00 03/17/2015 17:58
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/17/2015 17:58
Surrogates
1,2-Dichloroethane-d4 103 % 164.0-140 03/17/2015 17:58
4-Bromofluorobenzene 96.0 % 185.0-115 03/17/2015 17:58
Toluene d8 94.0 % 182.0-117 03/17/2015 17:58
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 39 of 102
Client Sample ID: FNW-4A
Client Project ID: HeatCraft
Lab Sample ID: 31500424010-A
Lab Project ID: 31500424
Collection Date: 03/09/2015 16:10
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FNW-4A
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5590
Prep Method: SW-846 5030B
Prep Date/Time: 03/17/2015 13:37
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3554
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 40 of 102
Client Sample ID: FNW-4A
Client Project ID: HeatCraft
Lab Sample ID: 31500424010-D
Lab Project ID: 31500424
Collection Date: 03/09/2015 16:10
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of FNW-4A
Date Analyzed
1,4 Dioxane 2.37 ug/L 12.11 03/17/2015 13:30
Surrogates
Nitrobenzene-d5 75.0 % 150.0-150 03/17/2015 13:30
Batch Information
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Prep Initial Wt./Vol.: 949 mL
Prep Extract Vol: 1 mL
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 41 of 102
Client Sample ID: FNW-4A
Client Project ID: HeatCraft
Lab Sample ID: 31500424010-F
Lab Project ID: 31500424
Collection Date: 03/09/2015 16:10
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by EPA 300.0
Results of FNW-4A
Date Analyzed
Sulfate 5.37 mg/L 11.00 03/11/2015 13:18
Nitrate as N ND mg/L 10.300 03/11/2015 13:18
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 13:18
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 42 of 102
Client Sample ID: OSW-8C
Client Project ID: HeatCraft
Lab Sample ID: 31500424011-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 13:50
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-8C
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 17:55
1,1,1-Trichloroethane ND ug/L 11.00 03/12/2015 17:55
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 17:55
1,1,2-Trichloroethane ND ug/L 11.00 03/12/2015 17:55
1,1-Dichloroethane ND ug/L 11.00 03/12/2015 17:55
1,1-Dichloroethene ND ug/L 11.00 03/12/2015 17:55
1,1-Dichloropropene ND ug/L 11.00 03/12/2015 17:55
1,2,3-Trichlorobenzene ND ug/L 11.00 03/12/2015 17:55
1,2,3-Trichloropropane ND ug/L 11.00 03/12/2015 17:55
1,2,4-Trichlorobenzene ND ug/L 11.00 03/12/2015 17:55
1,2,4-Trimethylbenzene ND ug/L 11.00 03/12/2015 17:55
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/12/2015 17:55
1,2-Dibromoethane ND ug/L 11.00 03/12/2015 17:55
1,2-Dichlorobenzene ND ug/L 11.00 03/12/2015 17:55
1,2-Dichloroethane ND ug/L 11.00 03/12/2015 17:55
1,2-Dichloropropane ND ug/L 11.00 03/12/2015 17:55
1,3,5-Trimethylbenzene ND ug/L 11.00 03/12/2015 17:55
1,3-Dichlorobenzene ND ug/L 11.00 03/12/2015 17:55
1,3-Dichloropropane ND ug/L 11.00 03/12/2015 17:55
1,4-Dichlorobenzene ND ug/L 11.00 03/12/2015 17:55
2,2-Dichloropropane ND ug/L 11.00 03/12/2015 17:55
2-Butanone ND ug/L 125.0 03/12/2015 17:55
2-Chlorotoluene ND ug/L 11.00 03/12/2015 17:55
2-Hexanone ND ug/L 15.00 03/12/2015 17:55
4-Chlorotoluene ND ug/L 11.00 03/12/2015 17:55
4-Isopropyltoluene ND ug/L 11.00 03/12/2015 17:55
4-Methyl-2-pentanone ND ug/L 15.00 03/12/2015 17:55
Acetone ND ug/L 125.0 03/12/2015 17:55
Benzene ND ug/L 11.00 03/12/2015 17:55
Bromobenzene ND ug/L 11.00 03/12/2015 17:55
Bromochloromethane ND ug/L 11.00 03/12/2015 17:55
Bromodichloromethane ND ug/L 11.00 03/12/2015 17:55
Bromoform ND ug/L 11.00 03/12/2015 17:55
Bromomethane ND ug/L 11.00 03/12/2015 17:55
n-Butylbenzene ND ug/L 11.00 03/12/2015 17:55
Carbon disulfide ND ug/L 11.00 03/12/2015 17:55
Carbon tetrachloride ND ug/L 11.00 03/12/2015 17:55
Chlorobenzene ND ug/L 11.00 03/12/2015 17:55
Chloroethane ND ug/L 11.00 03/12/2015 17:55
Chloroform ND ug/L 11.00 03/12/2015 17:55
Chloromethane ND ug/L 11.00 03/12/2015 17:55
Dibromochloromethane ND ug/L 11.00 03/12/2015 17:55
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 43 of 102
Client Sample ID: OSW-8C
Client Project ID: HeatCraft
Lab Sample ID: 31500424011-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 13:50
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-8C
Date Analyzed
Dibromomethane ND ug/L 11.00 03/12/2015 17:55
Dichlorodifluoromethane ND ug/L 15.00 03/12/2015 17:55
cis-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 17:55
trans-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 17:55
Diisopropyl Ether ND ug/L 11.00 03/12/2015 17:55
Ethyl Benzene ND ug/L 11.00 03/12/2015 17:55
Hexachlorobutadiene ND ug/L 11.00 03/12/2015 17:55
Isopropylbenzene (Cumene) ND ug/L 11.00 03/12/2015 17:55
Methyl iodide ND ug/L 11.00 03/12/2015 17:55
Methylene chloride ND ug/L 15.00 03/12/2015 17:55
Naphthalene ND ug/L 11.00 03/12/2015 17:55
Styrene ND ug/L 11.00 03/12/2015 17:55
Tetrachloroethene ND ug/L 11.00 03/12/2015 17:55
Toluene ND ug/L 11.00 03/12/2015 17:55
Trichloroethene ND ug/L 11.00 03/12/2015 17:55
Trichlorofluoromethane ND ug/L 11.00 03/12/2015 17:55
Vinyl chloride ND ug/L 11.00 03/12/2015 17:55
Xylene (total)ND ug/L 12.00 03/12/2015 17:55
cis-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 17:55
m,p-Xylene ND ug/L 12.00 03/12/2015 17:55
n-Propylbenzene ND ug/L 11.00 03/12/2015 17:55
o-Xylene ND ug/L 11.00 03/12/2015 17:55
sec-Butylbenzene ND ug/L 11.00 03/12/2015 17:55
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/12/2015 17:55
tert-Butylbenzene ND ug/L 11.00 03/12/2015 17:55
trans-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 17:55
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/12/2015 17:55
Surrogates
1,2-Dichloroethane-d4 102 % 164.0-140 03/12/2015 17:55
4-Bromofluorobenzene 96.0 % 185.0-115 03/12/2015 17:55
Toluene d8 94.0 % 182.0-117 03/12/2015 17:55
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/12/2015 16:18
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 44 of 102
Client Sample ID: OSW-8B
Client Project ID: HeatCraft
Lab Sample ID: 31500424012-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 14:10
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-8B
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 18:20
1,1,1-Trichloroethane ND ug/L 11.00 03/12/2015 18:20
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 18:20
1,1,2-Trichloroethane ND ug/L 11.00 03/12/2015 18:20
1,1-Dichloroethane ND ug/L 11.00 03/12/2015 18:20
1,1-Dichloroethene ND ug/L 11.00 03/12/2015 18:20
1,1-Dichloropropene ND ug/L 11.00 03/12/2015 18:20
1,2,3-Trichlorobenzene ND ug/L 11.00 03/12/2015 18:20
1,2,3-Trichloropropane ND ug/L 11.00 03/12/2015 18:20
1,2,4-Trichlorobenzene ND ug/L 11.00 03/12/2015 18:20
1,2,4-Trimethylbenzene ND ug/L 11.00 03/12/2015 18:20
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/12/2015 18:20
1,2-Dibromoethane ND ug/L 11.00 03/12/2015 18:20
1,2-Dichlorobenzene ND ug/L 11.00 03/12/2015 18:20
1,2-Dichloroethane ND ug/L 11.00 03/12/2015 18:20
1,2-Dichloropropane ND ug/L 11.00 03/12/2015 18:20
1,3,5-Trimethylbenzene ND ug/L 11.00 03/12/2015 18:20
1,3-Dichlorobenzene ND ug/L 11.00 03/12/2015 18:20
1,3-Dichloropropane ND ug/L 11.00 03/12/2015 18:20
1,4-Dichlorobenzene ND ug/L 11.00 03/12/2015 18:20
2,2-Dichloropropane ND ug/L 11.00 03/12/2015 18:20
2-Butanone ND ug/L 125.0 03/12/2015 18:20
2-Chlorotoluene ND ug/L 11.00 03/12/2015 18:20
2-Hexanone ND ug/L 15.00 03/12/2015 18:20
4-Chlorotoluene ND ug/L 11.00 03/12/2015 18:20
4-Isopropyltoluene ND ug/L 11.00 03/12/2015 18:20
4-Methyl-2-pentanone ND ug/L 15.00 03/12/2015 18:20
Acetone ND ug/L 125.0 03/12/2015 18:20
Benzene ND ug/L 11.00 03/12/2015 18:20
Bromobenzene ND ug/L 11.00 03/12/2015 18:20
Bromochloromethane ND ug/L 11.00 03/12/2015 18:20
Bromodichloromethane ND ug/L 11.00 03/12/2015 18:20
Bromoform ND ug/L 11.00 03/12/2015 18:20
Bromomethane ND ug/L 11.00 03/12/2015 18:20
n-Butylbenzene ND ug/L 11.00 03/12/2015 18:20
Carbon disulfide ND ug/L 11.00 03/12/2015 18:20
Carbon tetrachloride ND ug/L 11.00 03/12/2015 18:20
Chlorobenzene ND ug/L 11.00 03/12/2015 18:20
Chloroethane ND ug/L 11.00 03/12/2015 18:20
Chloroform ND ug/L 11.00 03/12/2015 18:20
Chloromethane ND ug/L 11.00 03/12/2015 18:20
Dibromochloromethane ND ug/L 11.00 03/12/2015 18:20
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 45 of 102
Client Sample ID: OSW-8B
Client Project ID: HeatCraft
Lab Sample ID: 31500424012-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 14:10
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-8B
Date Analyzed
Dibromomethane ND ug/L 11.00 03/12/2015 18:20
Dichlorodifluoromethane ND ug/L 15.00 03/12/2015 18:20
cis-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 18:20
trans-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 18:20
Diisopropyl Ether ND ug/L 11.00 03/12/2015 18:20
Ethyl Benzene ND ug/L 11.00 03/12/2015 18:20
Hexachlorobutadiene ND ug/L 11.00 03/12/2015 18:20
Isopropylbenzene (Cumene) ND ug/L 11.00 03/12/2015 18:20
Methyl iodide ND ug/L 11.00 03/12/2015 18:20
Methylene chloride ND ug/L 15.00 03/12/2015 18:20
Naphthalene ND ug/L 11.00 03/12/2015 18:20
Styrene ND ug/L 11.00 03/12/2015 18:20
Tetrachloroethene ND ug/L 11.00 03/12/2015 18:20
Toluene ND ug/L 11.00 03/12/2015 18:20
Trichloroethene ND ug/L 11.00 03/12/2015 18:20
Trichlorofluoromethane ND ug/L 11.00 03/12/2015 18:20
Vinyl chloride ND ug/L 11.00 03/12/2015 18:20
Xylene (total)ND ug/L 12.00 03/12/2015 18:20
cis-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 18:20
m,p-Xylene ND ug/L 12.00 03/12/2015 18:20
n-Propylbenzene ND ug/L 11.00 03/12/2015 18:20
o-Xylene ND ug/L 11.00 03/12/2015 18:20
sec-Butylbenzene ND ug/L 11.00 03/12/2015 18:20
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/12/2015 18:20
tert-Butylbenzene ND ug/L 11.00 03/12/2015 18:20
trans-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 18:20
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/12/2015 18:20
Surrogates
1,2-Dichloroethane-d4 102 % 164.0-140 03/12/2015 18:20
4-Bromofluorobenzene 98.0 % 185.0-115 03/12/2015 18:20
Toluene d8 94.0 % 182.0-117 03/12/2015 18:20
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/12/2015 16:18
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 46 of 102
Client Sample ID: OSW-4
Client Project ID: HeatCraft
Lab Sample ID: 31500424013-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 14:40
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-4
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 16:26
1,1,1-Trichloroethane ND ug/L 11.00 03/13/2015 16:26
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 16:26
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 16:26
1,1-Dichloroethane 28.1 ug/L 11.00 03/13/2015 16:26
1,1-Dichloroethene 39.5 ug/L 11.00 03/13/2015 16:26
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 16:26
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 16:26
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 16:26
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 16:26
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 16:26
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 16:26
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 16:26
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 16:26
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 16:26
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 16:26
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 16:26
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 16:26
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 16:26
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 16:26
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 16:26
2-Butanone ND ug/L 125.0 03/13/2015 16:26
2-Chlorotoluene ND ug/L 11.00 03/13/2015 16:26
2-Hexanone ND ug/L 15.00 03/13/2015 16:26
4-Chlorotoluene ND ug/L 11.00 03/13/2015 16:26
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 16:26
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 16:26
Acetone ND ug/L 125.0 03/13/2015 16:26
Benzene ND ug/L 11.00 03/13/2015 16:26
Bromobenzene ND ug/L 11.00 03/13/2015 16:26
Bromochloromethane ND ug/L 11.00 03/13/2015 16:26
Bromodichloromethane ND ug/L 11.00 03/13/2015 16:26
Bromoform ND ug/L 11.00 03/13/2015 16:26
Bromomethane ND ug/L 11.00 03/13/2015 16:26
n-Butylbenzene ND ug/L 11.00 03/13/2015 16:26
Carbon disulfide ND ug/L 11.00 03/13/2015 16:26
Carbon tetrachloride ND ug/L 11.00 03/13/2015 16:26
Chlorobenzene ND ug/L 11.00 03/13/2015 16:26
Chloroethane ND ug/L 11.00 03/13/2015 16:26
Chloroform ND ug/L 11.00 03/13/2015 16:26
Chloromethane ND ug/L 11.00 03/13/2015 16:26
Dibromochloromethane ND ug/L 11.00 03/13/2015 16:26
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 47 of 102
Client Sample ID: OSW-4
Client Project ID: HeatCraft
Lab Sample ID: 31500424013-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 14:40
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-4
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 16:26
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 16:26
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 16:26
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 16:26
Diisopropyl Ether ND ug/L 11.00 03/13/2015 16:26
Ethyl Benzene ND ug/L 11.00 03/13/2015 16:26
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 16:26
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 16:26
Methyl iodide ND ug/L 11.00 03/13/2015 16:26
Methylene chloride ND ug/L 15.00 03/13/2015 16:26
Naphthalene ND ug/L 11.00 03/13/2015 16:26
Styrene ND ug/L 11.00 03/13/2015 16:26
Tetrachloroethene ND ug/L 11.00 03/13/2015 16:26
Toluene ND ug/L 11.00 03/13/2015 16:26
Trichloroethene ND ug/L 11.00 03/13/2015 16:26
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 16:26
Vinyl chloride 10.3 ug/L 11.00 03/13/2015 16:26
Xylene (total)ND ug/L 12.00 03/13/2015 16:26
cis-1,2-Dichloroethene 505 ug/L 1010.0 03/12/2015 19:59
m,p-Xylene ND ug/L 12.00 03/13/2015 16:26
n-Propylbenzene ND ug/L 11.00 03/13/2015 16:26
o-Xylene ND ug/L 11.00 03/13/2015 16:26
sec-Butylbenzene ND ug/L 11.00 03/13/2015 16:26
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 16:26
tert-Butylbenzene ND ug/L 11.00 03/13/2015 16:26
trans-1,2-Dichloroethene ND ug/L 11.00 03/13/2015 16:26
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 16:26
Surrogates
1,2-Dichloroethane-d4 103 % 164.0-140 03/13/2015 16:26
4-Bromofluorobenzene 97.0 % 185.0-115 03/13/2015 16:26
Toluene d8 89.0 % 182.0-117 03/13/2015 16:26
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 48 of 102
Client Sample ID: OSW-4
Client Project ID: HeatCraft
Lab Sample ID: 31500424013-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 14:40
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-4
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 49 of 102
Client Sample ID: OSW-4
Client Project ID: HeatCraft
Lab Sample ID: 31500424013-D
Lab Project ID: 31500424
Collection Date: 03/10/2015 14:40
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of OSW-4
Date Analyzed
1,4 Dioxane 39.0 ug/L 24.30 03/17/2015 17:20
Surrogates
Nitrobenzene-d5 57.4 % 250.0-150 03/17/2015 17:20
Batch Information
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Prep Initial Wt./Vol.: 930 mL
Prep Extract Vol: 1 mL
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 50 of 102
Client Sample ID: OSW-4
Client Project ID: HeatCraft
Lab Sample ID: 31500424013-F
Lab Project ID: 31500424
Collection Date: 03/10/2015 14:40
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by EPA 300.0
Results of OSW-4
Date Analyzed
Sulfate 17.3 mg/L 11.00 03/11/2015 12:08
Nitrate as N ND mg/L 10.300 03/11/2015 12:08
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 12:08
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 51 of 102
Client Sample ID: OSW-2
Client Project ID: HeatCraft
Lab Sample ID: 31500424014-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:00
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-2
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/17/2015 21:18
1,1,1-Trichloroethane ND ug/L 11.00 03/17/2015 21:18
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/17/2015 21:18
1,1,2-Trichloroethane ND ug/L 11.00 03/17/2015 21:18
1,1-Dichloroethane 69.6 ug/L 11.00 03/17/2015 21:18
1,1-Dichloroethene 69.5 ug/L 5050.0 03/12/2015 22:52
1,1-Dichloropropene ND ug/L 11.00 03/17/2015 21:18
1,2,3-Trichlorobenzene ND ug/L 11.00 03/17/2015 21:18
1,2,3-Trichloropropane ND ug/L 11.00 03/17/2015 21:18
1,2,4-Trichlorobenzene ND ug/L 11.00 03/17/2015 21:18
1,2,4-Trimethylbenzene ND ug/L 11.00 03/17/2015 21:18
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/17/2015 21:18
1,2-Dibromoethane ND ug/L 11.00 03/17/2015 21:18
1,2-Dichlorobenzene ND ug/L 11.00 03/17/2015 21:18
1,2-Dichloroethane ND ug/L 11.00 03/17/2015 21:18
1,2-Dichloropropane ND ug/L 11.00 03/17/2015 21:18
1,3,5-Trimethylbenzene ND ug/L 11.00 03/17/2015 21:18
1,3-Dichlorobenzene ND ug/L 11.00 03/17/2015 21:18
1,3-Dichloropropane ND ug/L 11.00 03/17/2015 21:18
1,4-Dichlorobenzene ND ug/L 11.00 03/17/2015 21:18
2,2-Dichloropropane ND ug/L 11.00 03/17/2015 21:18
2-Butanone ND ug/L 125.0 03/17/2015 21:18
2-Chlorotoluene ND ug/L 11.00 03/17/2015 21:18
2-Hexanone ND ug/L 15.00 03/17/2015 21:18
4-Chlorotoluene ND ug/L 11.00 03/17/2015 21:18
4-Isopropyltoluene ND ug/L 11.00 03/17/2015 21:18
4-Methyl-2-pentanone ND ug/L 15.00 03/17/2015 21:18
Acetone ND ug/L 125.0 03/17/2015 21:18
Benzene ND ug/L 11.00 03/17/2015 21:18
Bromobenzene ND ug/L 11.00 03/17/2015 21:18
Bromochloromethane ND ug/L 11.00 03/17/2015 21:18
Bromodichloromethane ND ug/L 11.00 03/17/2015 21:18
Bromoform ND ug/L 11.00 03/17/2015 21:18
Bromomethane ND ug/L 11.00 03/17/2015 21:18
n-Butylbenzene ND ug/L 11.00 03/17/2015 21:18
Carbon disulfide ND ug/L 11.00 03/17/2015 21:18
Carbon tetrachloride ND ug/L 11.00 03/17/2015 21:18
Chlorobenzene ND ug/L 11.00 03/17/2015 21:18
Chloroethane 1.24 ug/L 11.00 03/17/2015 21:18
Chloroform ND ug/L 11.00 03/17/2015 21:18
Chloromethane ND ug/L 11.00 03/17/2015 21:18
Dibromochloromethane ND ug/L 11.00 03/17/2015 21:18
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 52 of 102
Client Sample ID: OSW-2
Client Project ID: HeatCraft
Lab Sample ID: 31500424014-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:00
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-2
Date Analyzed
Dibromomethane ND ug/L 11.00 03/17/2015 21:18
Dichlorodifluoromethane ND ug/L 15.00 03/17/2015 21:18
cis-1,3-Dichloropropene ND ug/L 11.00 03/17/2015 21:18
trans-1,3-Dichloropropene ND ug/L 11.00 03/17/2015 21:18
Diisopropyl Ether ND ug/L 11.00 03/17/2015 21:18
Ethyl Benzene ND ug/L 11.00 03/17/2015 21:18
Hexachlorobutadiene ND ug/L 11.00 03/17/2015 21:18
Isopropylbenzene (Cumene) ND ug/L 11.00 03/17/2015 21:18
Methyl iodide ND ug/L 11.00 03/17/2015 21:18
Methylene chloride ND ug/L 15.00 03/17/2015 21:18
Naphthalene ND ug/L 11.00 03/17/2015 21:18
Styrene ND ug/L 11.00 03/17/2015 21:18
Tetrachloroethene ND ug/L 11.00 03/17/2015 21:18
Toluene ND ug/L 11.00 03/17/2015 21:18
Trichloroethene ND ug/L 11.00 03/17/2015 21:18
Trichlorofluoromethane ND ug/L 11.00 03/17/2015 21:18
Vinyl chloride 116 ug/L 5050.0 03/12/2015 22:52
Xylene (total)ND ug/L 12.00 03/17/2015 21:18
cis-1,2-Dichloroethene 1080 ug/L 5050.0 03/12/2015 22:52
m,p-Xylene ND ug/L 12.00 03/17/2015 21:18
n-Propylbenzene ND ug/L 11.00 03/17/2015 21:18
o-Xylene ND ug/L 11.00 03/17/2015 21:18
sec-Butylbenzene ND ug/L 11.00 03/17/2015 21:18
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/17/2015 21:18
tert-Butylbenzene ND ug/L 11.00 03/17/2015 21:18
trans-1,2-Dichloroethene 4.45 ug/L 11.00 03/17/2015 21:18
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/17/2015 21:18
Surrogates
1,2-Dichloroethane-d4 105 % 164.0-140 03/17/2015 21:18
4-Bromofluorobenzene 97.0 % 185.0-115 03/17/2015 21:18
Toluene d8 90.0 % 182.0-117 03/17/2015 21:18
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 53 of 102
Client Sample ID: OSW-2
Client Project ID: HeatCraft
Lab Sample ID: 31500424014-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:00
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-2
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5590
Prep Method: SW-846 5030B
Prep Date/Time: 03/17/2015 13:37
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3554
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 54 of 102
Client Sample ID: OSW-2
Client Project ID: HeatCraft
Lab Sample ID: 31500424014-D
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:00
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of OSW-2
Date Analyzed
1,4 Dioxane 73.4 ug/L 510.7 03/17/2015 17:42
Surrogates
Nitrobenzene-d5 74.5 % 550.0-150 03/17/2015 17:42
Batch Information
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Prep Initial Wt./Vol.: 932 mL
Prep Extract Vol: 1 mL
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 55 of 102
Client Sample ID: OSW-2
Client Project ID: HeatCraft
Lab Sample ID: 31500424014-F
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:00
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by EPA 300.0
Results of OSW-2
Date Analyzed
Sulfate 8.80 mg/L 11.00 03/11/2015 12:22
Nitrate as N ND mg/L 10.300 03/11/2015 12:22
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 12:22
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 56 of 102
Client Sample ID: FW-1C
Client Project ID: HeatCraft
Lab Sample ID: 31500424015-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FW-1C
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 17:40
1,1,1-Trichloroethane ND ug/L 11.00 03/13/2015 17:40
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 17:40
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 17:40
1,1-Dichloroethane 47.1 ug/L 11.00 03/13/2015 17:40
1,1-Dichloroethene 24.4 ug/L 11.00 03/13/2015 17:40
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 17:40
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 17:40
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 17:40
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 17:40
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 17:40
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 17:40
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 17:40
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 17:40
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 17:40
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 17:40
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 17:40
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 17:40
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 17:40
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 17:40
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 17:40
2-Butanone ND ug/L 125.0 03/13/2015 17:40
2-Chlorotoluene ND ug/L 11.00 03/13/2015 17:40
2-Hexanone ND ug/L 15.00 03/13/2015 17:40
4-Chlorotoluene ND ug/L 11.00 03/13/2015 17:40
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 17:40
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 17:40
Acetone ND ug/L 125.0 03/13/2015 17:40
Benzene ND ug/L 11.00 03/13/2015 17:40
Bromobenzene ND ug/L 11.00 03/13/2015 17:40
Bromochloromethane ND ug/L 11.00 03/13/2015 17:40
Bromodichloromethane ND ug/L 11.00 03/13/2015 17:40
Bromoform ND ug/L 11.00 03/13/2015 17:40
Bromomethane ND ug/L 11.00 03/13/2015 17:40
n-Butylbenzene ND ug/L 11.00 03/13/2015 17:40
Carbon disulfide ND ug/L 11.00 03/13/2015 17:40
Carbon tetrachloride ND ug/L 11.00 03/13/2015 17:40
Chlorobenzene ND ug/L 11.00 03/13/2015 17:40
Chloroethane ND ug/L 11.00 03/13/2015 17:40
Chloroform ND ug/L 11.00 03/13/2015 17:40
Chloromethane ND ug/L 11.00 03/13/2015 17:40
Dibromochloromethane ND ug/L 11.00 03/13/2015 17:40
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 57 of 102
Client Sample ID: FW-1C
Client Project ID: HeatCraft
Lab Sample ID: 31500424015-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FW-1C
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 17:40
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 17:40
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 17:40
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 17:40
Diisopropyl Ether ND ug/L 11.00 03/13/2015 17:40
Ethyl Benzene ND ug/L 11.00 03/13/2015 17:40
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 17:40
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 17:40
Methyl iodide ND ug/L 11.00 03/13/2015 17:40
Methylene chloride ND ug/L 15.00 03/13/2015 17:40
Naphthalene ND ug/L 11.00 03/13/2015 17:40
Styrene ND ug/L 11.00 03/13/2015 17:40
Tetrachloroethene ND ug/L 11.00 03/13/2015 17:40
Toluene ND ug/L 11.00 03/13/2015 17:40
Trichloroethene ND ug/L 11.00 03/13/2015 17:40
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 17:40
Vinyl chloride 82.0 ug/L 4040.0 03/12/2015 22:02
Xylene (total)ND ug/L 12.00 03/13/2015 17:40
cis-1,2-Dichloroethene 747 ug/L 4040.0 03/12/2015 22:02
m,p-Xylene ND ug/L 12.00 03/13/2015 17:40
n-Propylbenzene ND ug/L 11.00 03/13/2015 17:40
o-Xylene ND ug/L 11.00 03/13/2015 17:40
sec-Butylbenzene ND ug/L 11.00 03/13/2015 17:40
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 17:40
tert-Butylbenzene ND ug/L 11.00 03/13/2015 17:40
trans-1,2-Dichloroethene 3.44 ug/L 11.00 03/13/2015 17:40
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 17:40
Surrogates
1,2-Dichloroethane-d4 104 % 164.0-140 03/13/2015 17:40
4-Bromofluorobenzene 96.0 % 185.0-115 03/13/2015 17:40
Toluene d8 89.0 % 182.0-117 03/13/2015 17:40
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 58 of 102
Client Sample ID: FW-1C
Client Project ID: HeatCraft
Lab Sample ID: 31500424015-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FW-1C
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 59 of 102
Client Sample ID: FW-1C
Client Project ID: HeatCraft
Lab Sample ID: 31500424015-D
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of FW-1C
Date Analyzed
1,4 Dioxane 80.6 ug/L 510.5 03/17/2015 18:04
Surrogates
Nitrobenzene-d5 81.0 % 550.0-150 03/17/2015 18:04
Batch Information
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Prep Initial Wt./Vol.: 949 mL
Prep Extract Vol: 1 mL
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 60 of 102
Client Sample ID: FW-1C
Client Project ID: HeatCraft
Lab Sample ID: 31500424015-F
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:20
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by EPA 300.0
Results of FW-1C
Date Analyzed
Sulfate 14.2 mg/L 11.00 03/11/2015 12:36
Nitrate as N ND mg/L 10.300 03/11/2015 12:36
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 12:36
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 61 of 102
Client Sample ID: FWD-1C
Client Project ID: HeatCraft
Lab Sample ID: 31500424016-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:25
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FWD-1C
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 18:05
1,1,1-Trichloroethane ND ug/L 11.00 03/13/2015 18:05
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 18:05
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 18:05
1,1-Dichloroethane 45.6 ug/L 11.00 03/13/2015 18:05
1,1-Dichloroethene 23.5 ug/L 11.00 03/13/2015 18:05
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 18:05
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 18:05
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 18:05
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 18:05
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 18:05
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 18:05
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 18:05
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 18:05
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 18:05
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 18:05
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 18:05
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 18:05
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 18:05
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 18:05
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 18:05
2-Butanone ND ug/L 125.0 03/13/2015 18:05
2-Chlorotoluene ND ug/L 11.00 03/13/2015 18:05
2-Hexanone ND ug/L 15.00 03/13/2015 18:05
4-Chlorotoluene ND ug/L 11.00 03/13/2015 18:05
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 18:05
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 18:05
Acetone ND ug/L 125.0 03/13/2015 18:05
Benzene ND ug/L 11.00 03/13/2015 18:05
Bromobenzene ND ug/L 11.00 03/13/2015 18:05
Bromochloromethane ND ug/L 11.00 03/13/2015 18:05
Bromodichloromethane ND ug/L 11.00 03/13/2015 18:05
Bromoform ND ug/L 11.00 03/13/2015 18:05
Bromomethane ND ug/L 11.00 03/13/2015 18:05
n-Butylbenzene ND ug/L 11.00 03/13/2015 18:05
Carbon disulfide ND ug/L 11.00 03/13/2015 18:05
Carbon tetrachloride ND ug/L 11.00 03/13/2015 18:05
Chlorobenzene ND ug/L 11.00 03/13/2015 18:05
Chloroethane ND ug/L 11.00 03/13/2015 18:05
Chloroform ND ug/L 11.00 03/13/2015 18:05
Chloromethane ND ug/L 11.00 03/13/2015 18:05
Dibromochloromethane ND ug/L 11.00 03/13/2015 18:05
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 62 of 102
Client Sample ID: FWD-1C
Client Project ID: HeatCraft
Lab Sample ID: 31500424016-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:25
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FWD-1C
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 18:05
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 18:05
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 18:05
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 18:05
Diisopropyl Ether ND ug/L 11.00 03/13/2015 18:05
Ethyl Benzene ND ug/L 11.00 03/13/2015 18:05
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 18:05
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 18:05
Methyl iodide ND ug/L 11.00 03/13/2015 18:05
Methylene chloride ND ug/L 15.00 03/13/2015 18:05
Naphthalene ND ug/L 11.00 03/13/2015 18:05
Styrene ND ug/L 11.00 03/13/2015 18:05
Tetrachloroethene ND ug/L 11.00 03/13/2015 18:05
Toluene ND ug/L 11.00 03/13/2015 18:05
Trichloroethene ND ug/L 11.00 03/13/2015 18:05
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 18:05
Vinyl chloride 73.2 ug/L 4040.0 03/12/2015 22:27
Xylene (total)ND ug/L 12.00 03/13/2015 18:05
cis-1,2-Dichloroethene 667 ug/L 4040.0 03/12/2015 22:27
m,p-Xylene ND ug/L 12.00 03/13/2015 18:05
n-Propylbenzene ND ug/L 11.00 03/13/2015 18:05
o-Xylene ND ug/L 11.00 03/13/2015 18:05
sec-Butylbenzene ND ug/L 11.00 03/13/2015 18:05
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 18:05
tert-Butylbenzene ND ug/L 11.00 03/13/2015 18:05
trans-1,2-Dichloroethene 3.45 ug/L 11.00 03/13/2015 18:05
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 18:05
Surrogates
1,2-Dichloroethane-d4 103 % 164.0-140 03/13/2015 18:05
4-Bromofluorobenzene 95.0 % 185.0-115 03/13/2015 18:05
Toluene d8 89.0 % 182.0-117 03/13/2015 18:05
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 63 of 102
Client Sample ID: FWD-1C
Client Project ID: HeatCraft
Lab Sample ID: 31500424016-A
Lab Project ID: 31500424
Collection Date: 03/10/2015 15:25
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of FWD-1C
Date Analyzed
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 64 of 102
Client Sample ID: Trip Blank
Client Project ID: HeatCraft
Lab Sample ID: 31500424017-A
Lab Project ID: 31500424
Collection Date:
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of Trip Blank
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 16:40
1,1,1-Trichloroethane ND ug/L 11.00 03/12/2015 16:40
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 16:40
1,1,2-Trichloroethane ND ug/L 11.00 03/12/2015 16:40
1,1-Dichloroethane ND ug/L 11.00 03/12/2015 16:40
1,1-Dichloroethene ND ug/L 11.00 03/12/2015 16:40
1,1-Dichloropropene ND ug/L 11.00 03/12/2015 16:40
1,2,3-Trichlorobenzene ND ug/L 11.00 03/12/2015 16:40
1,2,3-Trichloropropane ND ug/L 11.00 03/12/2015 16:40
1,2,4-Trichlorobenzene ND ug/L 11.00 03/12/2015 16:40
1,2,4-Trimethylbenzene ND ug/L 11.00 03/12/2015 16:40
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/12/2015 16:40
1,2-Dibromoethane ND ug/L 11.00 03/12/2015 16:40
1,2-Dichlorobenzene ND ug/L 11.00 03/12/2015 16:40
1,2-Dichloroethane ND ug/L 11.00 03/12/2015 16:40
1,2-Dichloropropane ND ug/L 11.00 03/12/2015 16:40
1,3,5-Trimethylbenzene ND ug/L 11.00 03/12/2015 16:40
1,3-Dichlorobenzene ND ug/L 11.00 03/12/2015 16:40
1,3-Dichloropropane ND ug/L 11.00 03/12/2015 16:40
1,4-Dichlorobenzene ND ug/L 11.00 03/12/2015 16:40
2,2-Dichloropropane ND ug/L 11.00 03/12/2015 16:40
2-Butanone ND ug/L 125.0 03/12/2015 16:40
2-Chlorotoluene ND ug/L 11.00 03/12/2015 16:40
2-Hexanone ND ug/L 15.00 03/12/2015 16:40
4-Chlorotoluene ND ug/L 11.00 03/12/2015 16:40
4-Isopropyltoluene ND ug/L 11.00 03/12/2015 16:40
4-Methyl-2-pentanone ND ug/L 15.00 03/12/2015 16:40
Acetone ND ug/L 125.0 03/12/2015 16:40
Benzene ND ug/L 11.00 03/12/2015 16:40
Bromobenzene ND ug/L 11.00 03/12/2015 16:40
Bromochloromethane ND ug/L 11.00 03/12/2015 16:40
Bromodichloromethane ND ug/L 11.00 03/12/2015 16:40
Bromoform ND ug/L 11.00 03/12/2015 16:40
Bromomethane ND ug/L 11.00 03/12/2015 16:40
n-Butylbenzene ND ug/L 11.00 03/12/2015 16:40
Carbon disulfide ND ug/L 11.00 03/12/2015 16:40
Carbon tetrachloride ND ug/L 11.00 03/12/2015 16:40
Chlorobenzene ND ug/L 11.00 03/12/2015 16:40
Chloroethane ND ug/L 11.00 03/12/2015 16:40
Chloroform ND ug/L 11.00 03/12/2015 16:40
Chloromethane ND ug/L 11.00 03/12/2015 16:40
Dibromochloromethane ND ug/L 11.00 03/12/2015 16:40
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 65 of 102
Client Sample ID: Trip Blank
Client Project ID: HeatCraft
Lab Sample ID: 31500424017-A
Lab Project ID: 31500424
Collection Date:
Received Date: 03/10/2015 15:50
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of Trip Blank
Date Analyzed
Dibromomethane ND ug/L 11.00 03/12/2015 16:40
Dichlorodifluoromethane ND ug/L 15.00 03/12/2015 16:40
cis-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 16:40
trans-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 16:40
Diisopropyl Ether ND ug/L 11.00 03/12/2015 16:40
Ethyl Benzene ND ug/L 11.00 03/12/2015 16:40
Hexachlorobutadiene ND ug/L 11.00 03/12/2015 16:40
Isopropylbenzene (Cumene) ND ug/L 11.00 03/12/2015 16:40
Methyl iodide ND ug/L 11.00 03/12/2015 16:40
Methylene chloride ND ug/L 15.00 03/12/2015 16:40
Naphthalene ND ug/L 11.00 03/12/2015 16:40
Styrene ND ug/L 11.00 03/12/2015 16:40
Tetrachloroethene ND ug/L 11.00 03/12/2015 16:40
Toluene 1.13 ug/L 11.00 03/12/2015 16:40
Trichloroethene ND ug/L 11.00 03/12/2015 16:40
Trichlorofluoromethane ND ug/L 11.00 03/12/2015 16:40
Vinyl chloride ND ug/L 11.00 03/12/2015 16:40
Xylene (total)ND ug/L 12.00 03/12/2015 16:40
cis-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 16:40
m,p-Xylene ND ug/L 12.00 03/12/2015 16:40
n-Propylbenzene ND ug/L 11.00 03/12/2015 16:40
o-Xylene ND ug/L 11.00 03/12/2015 16:40
sec-Butylbenzene ND ug/L 11.00 03/12/2015 16:40
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/12/2015 16:40
tert-Butylbenzene ND ug/L 11.00 03/12/2015 16:40
trans-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 16:40
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/12/2015 16:40
Surrogates
1,2-Dichloroethane-d4 102 % 164.0-140 03/12/2015 16:40
4-Bromofluorobenzene 96.0 % 185.0-115 03/12/2015 16:40
Toluene d8 95.0 % 182.0-117 03/12/2015 16:40
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/12/2015 16:18
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 66 of 102
Batch Summary
SW-846 8260B SW-846 5030BAnalytical Method:Prep Method:
VXX5581
03/12/2015 07:56
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
LCS for HBN 69384 [VXX/5581]03/12/2015 15:00 MSD8 BWS161921VMS3548
LCSD for HBN 69384 [VXX/5581]03/12/2015 15:25 MSD8 BWS161922VMS3548
MB for HBN 69384 [VXX/5581]03/12/2015 16:15 MSD8 BWS161923VMS3548
Trip Blank 03/12/2015 16:40 MSD8 BWS31500424017VMS3548
CAM-1R 03/12/2015 17:05 MSD8 BWS31500424001VMS3548
OSW-6A 03/12/2015 17:30 MSD8 BWS31500424004VMS3548
OSW-8C 03/12/2015 17:55 MSD8 BWS31500424011VMS3548
OSW-8B 03/12/2015 18:20 MSD8 BWS31500424012VMS3548
OSW-4 03/12/2015 19:59 MSD8 BWS31500424013VMS3548
OSW-5B 03/12/2015 20:48 MSD8 BWS31500424006VMS3548
OSW-5A 03/12/2015 21:13 MSD8 BWS31500424007VMS3548
FNW-4A 03/12/2015 21:38 MSD8 BWS31500424010VMS3548
FW-1C 03/12/2015 22:02 MSD8 BWS31500424015VMS3548
FWD-1C 03/12/2015 22:27 MSD8 BWS31500424016VMS3548
OSW-2 03/12/2015 22:52 MSD8 BWS31500424014VMS3548
OSW-6C 03/12/2015 23:17 MSD8 BWS31500424002VMS3548
OSW-1 03/12/2015 23:41 MSD8 BWS31500424008VMS3548
OSW-5C 03/13/2015 00:06 MSD8 BWS31500424005VMS3548
FNW-3A 03/13/2015 00:31 MSD8 BWS31500424009VMS3548
FNW-3A(161786MS)03/13/2015 00:56 MSD8 BWS162355VMS3548
FNW-3A(161786MSD)03/13/2015 01:21 MSD8 BWS162356VMS3548
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 67 of 102
Blank ID: MB for HBN 69384 [VXX/5581]
Blank Lab ID: 161923
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500424001, 31500424002, 31500424004, 31500424005, 31500424006, 31500424007, 31500424008, 31500424009, 31500424010,
31500424011, 31500424012, 31500424013, 31500424014, 31500424015, 31500424016, 31500424017
Dichlorodifluoromethane ND 5.00 ug/L 1
Chloromethane ND 1.00 ug/L 1
Vinyl chloride ND 1.00 ug/L 1
Bromomethane ND 1.00 ug/L 1
Chloroethane ND 1.00 ug/L 1
Trichlorofluoromethane ND 1.00 ug/L 1
1,1-Dichloroethene ND 1.00 ug/L 1
Acetone ND 25.0 ug/L 1
Methylene chloride ND 5.00 ug/L 1
trans-1,2-Dichloroethene ND 1.00 ug/L 1
tert-Butyl methyl ether (MTBE) ND 1.00 ug/L 1
1,1-Dichloroethane ND 1.00 ug/L 1
Diisopropyl Ether ND 1.00 ug/L 1
2,2-Dichloropropane ND 1.00 ug/L 1
cis-1,2-Dichloroethene ND 1.00 ug/L 1
2-Butanone ND 25.0 ug/L 1
Bromochloromethane ND 1.00 ug/L 1
Chloroform ND 1.00 ug/L 1
1,1,1-Trichloroethane ND 1.00 ug/L 1
Carbon tetrachloride ND 1.00 ug/L 1
1,1-Dichloropropene ND 1.00 ug/L 1
Benzene ND 1.00 ug/L 1
1,2-Dichloroethane ND 1.00 ug/L 1
Trichloroethene ND 1.00 ug/L 1
1,2-Dichloropropane ND 1.00 ug/L 1
Dibromomethane ND 1.00 ug/L 1
Bromodichloromethane ND 1.00 ug/L 1
cis-1,3-Dichloropropene ND 1.00 ug/L 1
4-Methyl-2-pentanone ND 5.00 ug/L 1
Toluene ND 1.00 ug/L 1
Methyl iodide ND 1.00 ug/L 1
trans-1,3-Dichloropropene ND 1.00 ug/L 1
Carbon disulfide ND 1.00 ug/L 1
1,1,2-Trichloroethane ND 1.00 ug/L 1
Tetrachloroethene ND 1.00 ug/L 1
1,3-Dichloropropane ND 1.00 ug/L 1
2-Hexanone ND 5.00 ug/L 1
Dibromochloromethane ND 1.00 ug/L 1
1,2-Dibromoethane ND 1.00 ug/L 1
Chlorobenzene ND 1.00 ug/L 1
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 1
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 68 of 102
Blank ID: MB for HBN 69384 [VXX/5581]
Blank Lab ID: 161923
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500424001, 31500424002, 31500424004, 31500424005, 31500424006, 31500424007, 31500424008, 31500424009, 31500424010,
31500424011, 31500424012, 31500424013, 31500424014, 31500424015, 31500424016, 31500424017
Bromoform ND 1.00 ug/L 1
Bromobenzene ND 1.00 ug/L 1
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 1
1,2,3-Trichloropropane ND 1.00 ug/L 1
Ethyl Benzene ND 1.00 ug/L 1
m,p-Xylene ND 2.00 ug/L 1
Styrene ND 1.00 ug/L 1
o-Xylene ND 1.00 ug/L 1
Xylene (total)ND 2.00 ug/L 1
Isopropylbenzene (Cumene) ND 1.00 ug/L 1
n-Propylbenzene ND 1.00 ug/L 1
2-Chlorotoluene ND 1.00 ug/L 1
4-Chlorotoluene ND 1.00 ug/L 1
1,3,5-Trimethylbenzene ND 1.00 ug/L 1
tert-Butylbenzene ND 1.00 ug/L 1
1,2,4-Trimethylbenzene ND 1.00 ug/L 1
sec-Butylbenzene ND 1.00 ug/L 1
1,3-Dichlorobenzene ND 1.00 ug/L 1
4-Isopropyltoluene ND 1.00 ug/L 1
1,4-Dichlorobenzene ND 1.00 ug/L 1
1,2-Dichlorobenzene ND 1.00 ug/L 1
n-Butylbenzene ND 1.00 ug/L 1
1,2-Dibromo-3-chloropropane ND 5.00 ug/L 1
1,2,4-Trichlorobenzene ND 1.00 ug/L 1
Hexachlorobutadiene ND 1.00 ug/L 1
Naphthalene ND 1.00 ug/L 1
trans-1,4-Dichloro-2-butene ND 5.00 ug/L 1
1,2,3-Trichlorobenzene ND 1.00 ug/L 1
Surrogates
1,2-Dichloroethane-d4 102 64.0-140 %1
Toluene d8 96.0 82.0-117 %1
4-Bromofluorobenzene 95.0 85.0-115 %1
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 3/12/2015 7:56:33AM
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 69 of 102
Blank Spike ID: LCS for HBN 69384 [VXX/5581]
Blank Spike Lab ID: 161921
Date Analyzed: 03/12/2015 15:00
Spike Duplicate ID: LCSD for HBN 69384 [VXX/5581]
Spike Duplicate Lab ID: 161922
Date Analyzed: 03/12/2015 15:25
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500424001, 31500424002, 31500424004, 31500424005, 31500424006, 31500424007, 31500424008,
31500424009, 31500424010, 31500424011, 31500424012, 31500424013, 31500424014, 31500424015,
31500424016, 31500424017
QC for Samples:
Dichlorodifluoromethane 5.00 5.30 5.21065.00 5.03 101 33.0-170 30.00
Chloromethane 5.00 5.11 0.201025.00 5.10 102 57.0-132 30.00
Vinyl chloride 5.00 5.30 3.81065.00 5.10 102 59.0-138 30.00
Bromomethane 5.00 5.42 0.921085.00 5.47 109 51.0-134 30.00
Chloroethane 5.00 4.38 6.6885.00 4.68 94 64.0-145 30.00
Trichlorofluoromethane 5.00 5.36 1.11075.00 5.30 106 64.0-133 30.00
1,1-Dichloroethene 5.00 5.29 2.51065.00 5.16 103 71.0-128 30.00
Acetone 25.0 ND 0.527725.0 ND 77 52.0-140 30.00
Methylene chloride 5.00 5.32 2.71065.00 5.18 104 70.0-113 30.00
trans-1,2-Dichloroethene 5.00 5.47 2.61095.00 5.33 107 57.0-138 30.00
tert-Butyl methyl ether (MTBE)5.00 5.17 5.21035.00 4.91 98 47.0-142 30.00
1,1-Dichloroethane 5.00 5.23 1.91055.00 5.13 103 68.0-133 30.00
Diisopropyl Ether 5.00 5.04 3.01015.00 4.89 98 66.0-132 30.00
2,2-Dichloropropane 5.00 5.33 6.41075.00 5.00 100 74.0-125 30.00
cis-1,2-Dichloroethene 5.00 5.24 2.51055.00 5.11 102 73.0-128 30.00
2-Butanone 25.0 ND 4.19025.0 ND 86 58.0-134 30.00
Bromochloromethane 5.00 5.55 2.01115.00 5.44 109 73.0-128 30.00
Chloroform 5.00 5.25 1.71055.00 5.16 103 74.0-124 30.00
1,1,1-Trichloroethane 5.00 5.19 0.01045.00 5.19 104 76.0-119 30.00
Carbon tetrachloride 5.00 5.16 0.971035.00 5.11 102 75.0-120 30.00
1,1-Dichloropropene 5.00 5.05 2.01015.00 4.95 99 76.0-124 30.00
Benzene 5.00 5.14 0.191035.00 5.15 103 76.0-124 30.00
1,2-Dichloroethane 5.00 5.17 2.21035.00 5.06 101 76.0-119 30.00
Trichloroethene 5.00 4.61 8.5925.00 5.02 100 74.0-121 30.00
1,2-Dichloropropane 5.00 4.74 0.21955.00 4.73 95 74.0-124 30.00
Dibromomethane 5.00 5.22 3.31045.00 5.05 101 71.0-128 30.00
Bromodichloromethane 5.00 4.93 0.0995.00 4.93 99 72.0-120 30.00
cis-1,3-Dichloropropene 5.00 5.08 2.61025.00 4.95 99 73.0-122 30.00
4-Methyl-2-pentanone 25.0 23.6 6.69425.0 22.1 88 65.0-124 30.00
Toluene 5.00 5.05 1.21015.00 4.99 100 75.0-123 30.00
Methyl iodide 5.00 5.02 1.61005.00 4.94 99 55.0-123 30.00
trans-1,3-Dichloropropene 5.00 5.01 2.81005.00 4.87 97 70.0-125 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 70 of 102
Blank Spike ID: LCS for HBN 69384 [VXX/5581]
Blank Spike Lab ID: 161921
Date Analyzed: 03/12/2015 15:00
Spike Duplicate ID: LCSD for HBN 69384 [VXX/5581]
Spike Duplicate Lab ID: 161922
Date Analyzed: 03/12/2015 15:25
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500424001, 31500424002, 31500424004, 31500424005, 31500424006, 31500424007, 31500424008,
31500424009, 31500424010, 31500424011, 31500424012, 31500424013, 31500424014, 31500424015,
31500424016, 31500424017
QC for Samples:
Carbon disulfide 5.00 5.12 1.41025.00 5.05 101 65.0-132 30.00
1,1,2-Trichloroethane 5.00 5.10 2.01025.00 5.00 100 76.0-121 30.00
Tetrachloroethene 5.00 5.18 0.191045.00 5.17 103 59.0-112 30.00
1,3-Dichloropropane 5.00 5.03 7.41015.00 4.67 93 74.0-120 30.00
2-Hexanone 25.0 22.5 2.79025.0 21.9 88 56.0-133 30.00
Dibromochloromethane 5.00 4.91 2.9985.00 4.77 95 67.0-122 30.00
1,2-Dibromoethane 5.00 4.98 2.41005.00 4.86 97 74.0-119 30.00
Chlorobenzene 5.00 5.09 3.01025.00 4.94 99 74.0-120 30.00
1,1,1,2-Tetrachloroethane 5.00 4.89 2.5985.00 4.77 95 73.0-119 30.00
Bromoform 5.00 5.11 4.81025.00 4.87 97 62.0-127 30.00
Bromobenzene 5.00 5.28 3.31065.00 5.11 102 75.0-120 30.00
1,1,2,2-Tetrachloroethane 5.00 5.17 5.61035.00 4.89 98 68.0-129 30.00
1,2,3-Trichloropropane 5.00 5.28 6.01065.00 4.97 99 67.0-126 30.00
Ethyl Benzene 5.00 4.69 0.43945.00 4.67 93 76.0-123 30.00
m,p-Xylene 10.0 9.57 0.429610.0 9.61 96 76.0-124 30.00
Styrene 5.00 4.60 0.0925.00 4.60 92 76.0-121 30.00
o-Xylene 5.00 4.36 2.0875.00 4.45 89 75.0-124 30.00
Isopropylbenzene (Cumene)5.00 4.56 0.44915.00 4.58 92 77.0-120 30.00
n-Propylbenzene 5.00 4.75 0.0955.00 4.75 95 77.0-123 30.00
2-Chlorotoluene 5.00 4.90 0.61985.00 4.93 99 74.0-127 30.00
4-Chlorotoluene 5.00 5.06 0.201015.00 5.07 101 77.0-123 30.00
1,3,5-Trimethylbenzene 5.00 4.77 1.0955.00 4.82 96 76.0-122 30.00
tert-Butylbenzene 5.00 4.66 0.85935.00 4.70 94 67.0-122 30.00
1,2,4-Trimethylbenzene 5.00 4.81 0.42965.00 4.79 96 76.0-124 30.00
sec-Butylbenzene 5.00 4.81 0.83965.00 4.85 97 78.0-121 30.00
1,3-Dichlorobenzene 5.00 5.07 1.61015.00 5.15 103 75.0-120 30.00
4-Isopropyltoluene 5.00 4.70 0.85945.00 4.74 95 77.0-120 30.00
1,4-Dichlorobenzene 5.00 4.99 0.401005.00 4.97 99 70.0-125 30.00
1,2-Dichlorobenzene 5.00 5.05 1.81015.00 4.96 99 76.0-118 30.00
n-Butylbenzene 5.00 4.67 0.21935.00 4.66 93 78.0-118 30.00
1,2-Dibromo-3-chloropropane 30.0 27.9 6.79330.0 26.1 87 62.0-130 30.00
1,2,4-Trichlorobenzene 5.00 4.76 2.3955.00 4.65 93 72.0-119 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 71 of 102
Blank Spike ID: LCS for HBN 69384 [VXX/5581]
Blank Spike Lab ID: 161921
Date Analyzed: 03/12/2015 15:00
Spike Duplicate ID: LCSD for HBN 69384 [VXX/5581]
Spike Duplicate Lab ID: 161922
Date Analyzed: 03/12/2015 15:25
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500424001, 31500424002, 31500424004, 31500424005, 31500424006, 31500424007, 31500424008,
31500424009, 31500424010, 31500424011, 31500424012, 31500424013, 31500424014, 31500424015,
31500424016, 31500424017
QC for Samples:
Hexachlorobutadiene 5.00 5.19 7.01045.00 4.84 97 69.0-121 30.00
Naphthalene 5.00 4.47 4.8895.00 4.26 85 67.0-122 30.00
trans-1,4-Dichloro-2-butene 25.0 23.6 6.19425.0 22.2 89 61.0-132 30.00
1,2,3-Trichlorobenzene 5.00 4.96 3.3995.00 4.80 96 68.0-123 30.00
Surrogates
1,2-Dichloroethane-d4 104 99 64.0-140
Toluene d8 102 101 82.0-117
4-Bromofluorobenzene 103 102 85.0-115
Batch Information
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/12/2015 07:56
Spike Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Dupe Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 72 of 102
Original Sample ID: 31500424009 (FNW-3A)
MS Sample ID: 162355
MSD Sample ID: 162356
Analysis Date: 03/13/2015 00:31
Analysis Date: 03/13/2015 00:56
Analysis Date: 03/13/2015 01:21
Matrix: Water
Results by SW-846 8260B
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/L)Spike Duplicate (ug/L)
CL RPD CL
QC for Samples:31500424001, 31500424002, 31500424004, 31500424005, 31500424006, 31500424007, 31500424008,
31500424009, 31500424010, 31500424011, 31500424012, 31500424013, 31500424014, 31500424015,
31500424016, 31500424017
1,1,1-Trichloroethane 764 1000 1840 1000 1840 107 0.0107 30.0078.0-121
1,1-Dichloroethane 592 1000 1670 1000 1670 108 0.0107 30.0076.0-128
1,1-Dichloroethene 1470 1000 2520 1000 2580 111 2.4105 30.0064.0-130
Trichloroethene 1470 1000 2480 1000 2560 108 3.2101 30.0085.0-136
Vinyl chloride 1140 1000 2140 1000 2280 115 6.3100 30.0068.0-137
cis-1,2-Dichloroethene 10300 1000 11400 1000 12000 166 *5.1115 30.0073.0-134
Batch Information
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:23
MS Init Wt./Vol.: 40 mL Extract Vol.: 40 mL
MSD Init Wt./Vol.: 40 mL Extract Vol.: 40 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 73 of 102
Batch Summary
SW-846 8260B SW-846 5030BAnalytical Method:Prep Method:
VXX5587
03/13/2015 08:20
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
LCS for HBN 69413 [VXX/5587]03/13/2015 09:23 MSD8 BWS162068VMS3552
LCSD for HBN 69413 [VXX/5587]03/13/2015 09:48 MSD8 BWS162069VMS3552
MB for HBN 69413 [VXX/5587]03/13/2015 10:37 MSD8 BWS162070VMS3552
OSW-6B 03/13/2015 11:02 MSD8 BWS31500424003VMS3552
OSW-5B 03/13/2015 15:36 MSD8 BWS31500424006VMS3552
OSW-5A 03/13/2015 16:01 MSD8 BWS31500424007VMS3552
OSW-4 03/13/2015 16:26 MSD8 BWS31500424013VMS3552
OSW-6C 03/13/2015 16:51 MSD8 BWS31500424002VMS3552
OSW-5C 03/13/2015 17:16 MSD8 BWS31500424005VMS3552
FW-1C 03/13/2015 17:40 MSD8 BWS31500424015VMS3552
FWD-1C 03/13/2015 18:05 MSD8 BWS31500424016VMS3552
OSW-1 03/13/2015 18:30 MSD8 BWS31500424008VMS3552
FNW-3A 03/13/2015 18:55 MSD8 BWS31500424009VMS3552
RW-2(161981MS)03/13/2015 19:44 MSD8 BWS162388VMS3552
RW-2(161981MSD)03/13/2015 20:09 MSD8 BWS162389VMS3552
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 74 of 102
Blank ID: MB for HBN 69413 [VXX/5587]
Blank Lab ID: 162070
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500424002, 31500424003, 31500424005, 31500424006, 31500424007, 31500424008, 31500424009, 31500424013, 31500424015,
31500424016
Dichlorodifluoromethane ND 5.00 ug/L 1
Chloromethane ND 1.00 ug/L 1
Vinyl chloride ND 1.00 ug/L 1
Bromomethane ND 1.00 ug/L 1
Chloroethane ND 1.00 ug/L 1
Trichlorofluoromethane ND 1.00 ug/L 1
1,1-Dichloroethene ND 1.00 ug/L 1
Acetone ND 25.0 ug/L 1
Methylene chloride ND 5.00 ug/L 1
trans-1,2-Dichloroethene ND 1.00 ug/L 1
tert-Butyl methyl ether (MTBE) ND 1.00 ug/L 1
1,1-Dichloroethane ND 1.00 ug/L 1
Diisopropyl Ether ND 1.00 ug/L 1
2,2-Dichloropropane ND 1.00 ug/L 1
cis-1,2-Dichloroethene ND 1.00 ug/L 1
2-Butanone ND 25.0 ug/L 1
Bromochloromethane ND 1.00 ug/L 1
Chloroform ND 1.00 ug/L 1
1,1,1-Trichloroethane ND 1.00 ug/L 1
Carbon tetrachloride ND 1.00 ug/L 1
1,1-Dichloropropene ND 1.00 ug/L 1
Benzene ND 1.00 ug/L 1
1,2-Dichloroethane ND 1.00 ug/L 1
Trichloroethene ND 1.00 ug/L 1
1,2-Dichloropropane ND 1.00 ug/L 1
Dibromomethane ND 1.00 ug/L 1
Bromodichloromethane ND 1.00 ug/L 1
cis-1,3-Dichloropropene ND 1.00 ug/L 1
4-Methyl-2-pentanone ND 5.00 ug/L 1
Toluene ND 1.00 ug/L 1
Methyl iodide ND 1.00 ug/L 1
trans-1,3-Dichloropropene ND 1.00 ug/L 1
Carbon disulfide ND 1.00 ug/L 1
1,1,2-Trichloroethane ND 1.00 ug/L 1
Tetrachloroethene ND 1.00 ug/L 1
1,3-Dichloropropane ND 1.00 ug/L 1
2-Hexanone ND 5.00 ug/L 1
Dibromochloromethane ND 1.00 ug/L 1
1,2-Dibromoethane ND 1.00 ug/L 1
Chlorobenzene ND 1.00 ug/L 1
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 1
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 75 of 102
Blank ID: MB for HBN 69413 [VXX/5587]
Blank Lab ID: 162070
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500424002, 31500424003, 31500424005, 31500424006, 31500424007, 31500424008, 31500424009, 31500424013, 31500424015,
31500424016
Bromoform ND 1.00 ug/L 1
Bromobenzene ND 1.00 ug/L 1
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 1
1,2,3-Trichloropropane ND 1.00 ug/L 1
Ethyl Benzene ND 1.00 ug/L 1
m,p-Xylene ND 2.00 ug/L 1
Styrene ND 1.00 ug/L 1
o-Xylene ND 1.00 ug/L 1
Xylene (total)ND 2.00 ug/L 1
Isopropylbenzene (Cumene) ND 1.00 ug/L 1
n-Propylbenzene ND 1.00 ug/L 1
2-Chlorotoluene ND 1.00 ug/L 1
4-Chlorotoluene ND 1.00 ug/L 1
1,3,5-Trimethylbenzene ND 1.00 ug/L 1
tert-Butylbenzene ND 1.00 ug/L 1
1,2,4-Trimethylbenzene ND 1.00 ug/L 1
sec-Butylbenzene ND 1.00 ug/L 1
1,3-Dichlorobenzene ND 1.00 ug/L 1
4-Isopropyltoluene ND 1.00 ug/L 1
1,4-Dichlorobenzene ND 1.00 ug/L 1
1,2-Dichlorobenzene ND 1.00 ug/L 1
n-Butylbenzene ND 1.00 ug/L 1
1,2-Dibromo-3-chloropropane ND 5.00 ug/L 1
1,2,4-Trichlorobenzene ND 1.00 ug/L 1
Hexachlorobutadiene ND 1.00 ug/L 1
Naphthalene ND 1.00 ug/L 1
trans-1,4-Dichloro-2-butene ND 5.00 ug/L 1
1,2,3-Trichlorobenzene ND 1.00 ug/L 1
Surrogates
1,2-Dichloroethane-d4 102 64.0-140 %1
Toluene d8 93.0 82.0-117 %1
4-Bromofluorobenzene 96.0 85.0-115 %1
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 3/13/2015 8:20:39AM
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 76 of 102
Blank Spike ID: LCS for HBN 69413 [VXX/5587]
Blank Spike Lab ID: 162068
Date Analyzed: 03/13/2015 09:23
Spike Duplicate ID: LCSD for HBN 69413 [VXX/5587]
Spike Duplicate Lab ID: 162069
Date Analyzed: 03/13/2015 09:48
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500424002, 31500424003, 31500424005, 31500424006, 31500424007, 31500424008, 31500424009,
31500424013, 31500424015, 31500424016
QC for Samples:
Dichlorodifluoromethane 5.00 5.15 6.41035.00 ND 97 33.0-170 30.00
Chloromethane 5.00 5.09 4.41025.00 4.87 97 57.0-132 30.00
Vinyl chloride 5.00 5.16 4.61035.00 4.93 99 59.0-138 30.00
Bromomethane 5.00 4.77 2.3955.00 4.66 93 51.0-134 30.00
Chloroethane 5.00 5.04 3.51015.00 5.22 104 64.0-145 30.00
Trichlorofluoromethane 5.00 5.51 4.61105.00 5.26 105 64.0-133 30.00
1,1-Dichloroethene 5.00 5.16 0.971035.00 5.11 102 71.0-128 30.00
Acetone 25.0 ND 2.19525.0 ND 93 52.0-140 30.00
Methylene chloride 5.00 5.14 0.191035.00 5.13 103 70.0-113 30.00
trans-1,2-Dichloroethene 5.00 5.30 2.31065.00 5.18 104 57.0-138 30.00
tert-Butyl methyl ether (MTBE)5.00 4.62 2.2925.00 4.52 90 47.0-142 30.00
1,1-Dichloroethane 5.00 5.31 2.91065.00 5.16 103 68.0-133 30.00
Diisopropyl Ether 5.00 4.75 0.0955.00 4.75 95 66.0-132 30.00
2,2-Dichloropropane 5.00 5.57 0.721115.00 5.53 111 74.0-125 30.00
cis-1,2-Dichloroethene 5.00 5.00 0.401005.00 4.98 100 73.0-128 30.00
2-Butanone 25.0 ND 2.69325.0 ND 91 58.0-134 30.00
Bromochloromethane 5.00 5.11 1.61025.00 5.03 101 73.0-128 30.00
Chloroform 5.00 5.06 0.791015.00 5.02 100 74.0-124 30.00
1,1,1-Trichloroethane 5.00 5.17 1.21035.00 5.11 102 76.0-119 30.00
Carbon tetrachloride 5.00 5.18 0.961045.00 5.23 105 75.0-120 30.00
1,1-Dichloropropene 5.00 4.83 1.9975.00 4.74 95 76.0-124 30.00
Benzene 5.00 4.95 0.20995.00 4.96 99 76.0-124 30.00
1,2-Dichloroethane 5.00 4.80 0.63965.00 4.77 95 76.0-119 30.00
Trichloroethene 5.00 5.05 0.201015.00 5.04 101 74.0-121 30.00
1,2-Dichloropropane 5.00 4.58 0.0925.00 4.58 92 74.0-124 30.00
Dibromomethane 5.00 4.75 3.5955.00 4.92 98 71.0-128 30.00
Bromodichloromethane 5.00 4.74 0.63955.00 4.71 94 72.0-120 30.00
cis-1,3-Dichloropropene 5.00 5.02 2.21005.00 4.91 98 73.0-122 30.00
4-Methyl-2-pentanone 25.0 19.8 0.507925.0 19.9 79 65.0-124 30.00
Toluene 5.00 4.61 0.22925.00 4.62 92 75.0-123 30.00
Methyl iodide 5.00 3.91 0.26785.00 3.92 78 55.0-123 30.00
trans-1,3-Dichloropropene 5.00 4.74 0.84955.00 4.78 96 70.0-125 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 77 of 102
Blank Spike ID: LCS for HBN 69413 [VXX/5587]
Blank Spike Lab ID: 162068
Date Analyzed: 03/13/2015 09:23
Spike Duplicate ID: LCSD for HBN 69413 [VXX/5587]
Spike Duplicate Lab ID: 162069
Date Analyzed: 03/13/2015 09:48
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500424002, 31500424003, 31500424005, 31500424006, 31500424007, 31500424008, 31500424009,
31500424013, 31500424015, 31500424016
QC for Samples:
Carbon disulfide 5.00 5.22 0.381045.00 5.20 104 65.0-132 30.00
1,1,2-Trichloroethane 5.00 4.97 0.0995.00 4.97 99 76.0-121 30.00
Tetrachloroethene 5.00 5.01 1.21005.00 4.95 99 59.0-112 30.00
1,3-Dichloropropane 5.00 4.58 1.5925.00 4.51 90 74.0-120 30.00
2-Hexanone 25.0 21.7 1.48725.0 21.4 85 56.0-133 30.00
Dibromochloromethane 5.00 4.86 0.62975.00 4.83 97 67.0-122 30.00
1,2-Dibromoethane 5.00 4.57 2.4915.00 4.68 94 74.0-119 30.00
Chlorobenzene 5.00 4.73 0.64955.00 4.70 94 74.0-120 30.00
1,1,1,2-Tetrachloroethane 5.00 5.14 1.81035.00 5.05 101 73.0-119 30.00
Bromoform 5.00 5.16 6.61035.00 4.83 97 62.0-127 30.00
Bromobenzene 5.00 5.05 5.31015.00 4.79 96 75.0-120 30.00
1,1,2,2-Tetrachloroethane 5.00 4.96 4.5995.00 4.74 95 68.0-129 30.00
1,2,3-Trichloropropane 5.00 4.91 5.7985.00 4.64 93 67.0-126 30.00
Ethyl Benzene 5.00 4.32 2.1865.00 4.23 85 76.0-123 30.00
m,p-Xylene 10.0 8.86 2.38910.0 8.66 87 76.0-124 30.00
Styrene 5.00 4.13 1.2835.00 4.08 82 76.0-121 30.00
o-Xylene 5.00 3.90 1.8785.00 3.97 79 75.0-124 30.00
Isopropylbenzene (Cumene)5.00 4.14 1.5835.00 4.08 82 77.0-120 30.00
n-Propylbenzene 5.00 4.46 2.7895.00 4.34 87 77.0-123 30.00
2-Chlorotoluene 5.00 4.57 2.2915.00 4.47 89 74.0-127 30.00
4-Chlorotoluene 5.00 4.71 2.9945.00 4.85 97 77.0-123 30.00
1,3,5-Trimethylbenzene 5.00 4.43 2.1895.00 4.34 87 76.0-122 30.00
tert-Butylbenzene 5.00 4.22 0.24845.00 4.23 85 67.0-122 30.00
1,2,4-Trimethylbenzene 5.00 4.53 1.8915.00 4.45 89 76.0-124 30.00
sec-Butylbenzene 5.00 4.50 0.66905.00 4.53 91 78.0-121 30.00
1,3-Dichlorobenzene 5.00 4.83 2.3975.00 4.72 94 75.0-120 30.00
4-Isopropyltoluene 5.00 4.36 2.6875.00 4.25 85 77.0-120 30.00
1,4-Dichlorobenzene 5.00 4.76 3.2955.00 4.61 92 70.0-125 30.00
1,2-Dichlorobenzene 5.00 4.78 0.21965.00 4.77 95 76.0-118 30.00
n-Butylbenzene 5.00 4.34 2.8875.00 4.22 84 78.0-118 30.00
1,2-Dibromo-3-chloropropane 30.0 25.8 4.48630.0 24.7 82 62.0-130 30.00
1,2,4-Trichlorobenzene 5.00 4.19 0.0845.00 4.19 84 72.0-119 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 78 of 102
Blank Spike ID: LCS for HBN 69413 [VXX/5587]
Blank Spike Lab ID: 162068
Date Analyzed: 03/13/2015 09:23
Spike Duplicate ID: LCSD for HBN 69413 [VXX/5587]
Spike Duplicate Lab ID: 162069
Date Analyzed: 03/13/2015 09:48
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500424002, 31500424003, 31500424005, 31500424006, 31500424007, 31500424008, 31500424009,
31500424013, 31500424015, 31500424016
QC for Samples:
Hexachlorobutadiene 5.00 4.76 3.2955.00 4.61 92 69.0-121 30.00
Naphthalene 5.00 3.79 1.9765.00 3.72 74 67.0-122 30.00
trans-1,4-Dichloro-2-butene 25.0 22.2 1.48925.0 21.9 88 61.0-132 30.00
1,2,3-Trichlorobenzene 5.00 4.42 3.0885.00 4.29 86 68.0-123 30.00
Surrogates
1,2-Dichloroethane-d4 101 102 64.0-140
Toluene d8 99 98 82.0-117
4-Bromofluorobenzene 104 105 85.0-115
Batch Information
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 08:20
Spike Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Dupe Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 79 of 102
Batch Summary
SW-846 8260B SW-846 5030BAnalytical Method:Prep Method:
VXX5590
03/17/2015 10:26
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
LCS for HBN 69651 [VXX/5590]03/17/2015 13:47 MSD8 JHL162198VMS3554
LCSD for HBN 69651 [VXX/5590]03/17/2015 14:12 MSD8 JHL162199VMS3554
MB for HBN 69651 [VXX/5590]03/17/2015 15:02 MSD8 JHL162200VMS3554
FNW-4A 03/17/2015 17:58 MSD8 JHL31500424010VMS3554
OSW-2 03/17/2015 21:18 MSD8 JHL31500424014VMS3554
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 80 of 102
Blank ID: MB for HBN 69651 [VXX/5590]
Blank Lab ID: 162200
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500424010, 31500424014
Dichlorodifluoromethane ND 5.00 ug/L 1
Chloromethane ND 1.00 ug/L 1
Vinyl chloride ND 1.00 ug/L 1
Bromomethane ND 1.00 ug/L 1
Chloroethane ND 1.00 ug/L 1
Trichlorofluoromethane ND 1.00 ug/L 1
Acetone ND 25.0 ug/L 1
Methylene chloride ND 5.00 ug/L 1
trans-1,2-Dichloroethene ND 1.00 ug/L 1
tert-Butyl methyl ether (MTBE) ND 1.00 ug/L 1
1,1-Dichloroethane ND 1.00 ug/L 1
Diisopropyl Ether ND 1.00 ug/L 1
2,2-Dichloropropane ND 1.00 ug/L 1
2-Butanone ND 25.0 ug/L 1
Bromochloromethane ND 1.00 ug/L 1
Chloroform ND 1.00 ug/L 1
1,1,1-Trichloroethane ND 1.00 ug/L 1
Carbon tetrachloride ND 1.00 ug/L 1
1,1-Dichloropropene ND 1.00 ug/L 1
Benzene ND 1.00 ug/L 1
1,2-Dichloroethane ND 1.00 ug/L 1
Trichloroethene ND 1.00 ug/L 1
1,2-Dichloropropane ND 1.00 ug/L 1
Dibromomethane ND 1.00 ug/L 1
Bromodichloromethane ND 1.00 ug/L 1
cis-1,3-Dichloropropene ND 1.00 ug/L 1
4-Methyl-2-pentanone ND 5.00 ug/L 1
Toluene ND 1.00 ug/L 1
Methyl iodide ND 1.00 ug/L 1
trans-1,3-Dichloropropene ND 1.00 ug/L 1
Carbon disulfide ND 1.00 ug/L 1
1,1,2-Trichloroethane ND 1.00 ug/L 1
Tetrachloroethene ND 1.00 ug/L 1
1,3-Dichloropropane ND 1.00 ug/L 1
2-Hexanone ND 5.00 ug/L 1
Dibromochloromethane ND 1.00 ug/L 1
1,2-Dibromoethane ND 1.00 ug/L 1
Chlorobenzene ND 1.00 ug/L 1
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 1
Bromoform ND 1.00 ug/L 1
Bromobenzene ND 1.00 ug/L 1
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 81 of 102
Blank ID: MB for HBN 69651 [VXX/5590]
Blank Lab ID: 162200
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500424010, 31500424014
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 1
1,2,3-Trichloropropane ND 1.00 ug/L 1
Ethyl Benzene ND 1.00 ug/L 1
m,p-Xylene ND 2.00 ug/L 1
Styrene ND 1.00 ug/L 1
o-Xylene ND 1.00 ug/L 1
Xylene (total)ND 2.00 ug/L 1
Isopropylbenzene (Cumene) ND 1.00 ug/L 1
n-Propylbenzene ND 1.00 ug/L 1
2-Chlorotoluene ND 1.00 ug/L 1
4-Chlorotoluene ND 1.00 ug/L 1
1,3,5-Trimethylbenzene ND 1.00 ug/L 1
tert-Butylbenzene ND 1.00 ug/L 1
1,2,4-Trimethylbenzene ND 1.00 ug/L 1
sec-Butylbenzene ND 1.00 ug/L 1
1,3-Dichlorobenzene ND 1.00 ug/L 1
4-Isopropyltoluene ND 1.00 ug/L 1
1,4-Dichlorobenzene ND 1.00 ug/L 1
1,2-Dichlorobenzene ND 1.00 ug/L 1
n-Butylbenzene ND 1.00 ug/L 1
1,2-Dibromo-3-chloropropane ND 5.00 ug/L 1
1,2,4-Trichlorobenzene ND 1.00 ug/L 1
Hexachlorobutadiene ND 1.00 ug/L 1
Naphthalene ND 1.00 ug/L 1
trans-1,4-Dichloro-2-butene ND 5.00 ug/L 1
1,2,3-Trichlorobenzene ND 1.00 ug/L 1
Surrogates
1,2-Dichloroethane-d4 105 64.0-140 %1
Toluene d8 91.0 82.0-117 %1
4-Bromofluorobenzene 96.0 85.0-115 %1
Batch Information
Prep Batch: VXX5590
Prep Method: SW-846 5030B
Prep Date/Time: 3/17/2015 10:26:26AM
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3554
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 82 of 102
Blank Spike ID: LCS for HBN 69651 [VXX/5590]
Blank Spike Lab ID: 162198
Date Analyzed: 03/17/2015 13:47
Spike Duplicate ID: LCSD for HBN 69651 [VXX/5590]
Spike Duplicate Lab ID: 162199
Date Analyzed: 03/17/2015 14:12
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500424010, 31500424014QC for Samples:
Dichlorodifluoromethane 5.00 5.72 0.171145.00 5.73 115 33.0-170 30.00
Chloromethane 5.00 5.74 3.01155.00 5.57 111 57.0-132 30.00
Vinyl chloride 5.00 5.96 4.51195.00 5.70 114 59.0-138 30.00
Bromomethane 5.00 5.12 0.581025.00 5.15 103 51.0-134 30.00
Chloroethane 5.00 4.82 20965.00 5.89 118 64.0-145 30.00
Trichlorofluoromethane 5.00 6.21 0.481245.00 6.24 125 64.0-133 30.00
Acetone 25.0 32.6 5.013025.0 31.0 124 52.0-140 30.00
Methylene chloride 5.00 5.96 0.17119*5.00 5.95 119*70.0-113 30.00
trans-1,2-Dichloroethene 5.00 6.04 0.501215.00 6.07 121 57.0-138 30.00
tert-Butyl methyl ether (MTBE)5.00 6.00 6.01205.00 5.65 113 47.0-142 30.00
1,1-Dichloroethane 5.00 6.13 1.51235.00 6.04 121 68.0-133 30.00
Diisopropyl Ether 5.00 5.75 1.21155.00 5.68 114 66.0-132 30.00
2,2-Dichloropropane 5.00 6.56 2.8131*5.00 6.38 128*74.0-125 30.00
2-Butanone 25.0 31.3 4.612525.0 29.9 120 58.0-134 30.00
Bromochloromethane 5.00 6.22 3.91245.00 5.98 120 73.0-128 30.00
Chloroform 5.00 5.92 0.511185.00 5.95 119 74.0-124 30.00
1,1,1-Trichloroethane 5.00 6.13 2.1123*5.00 6.00 120*76.0-119 30.00
Carbon tetrachloride 5.00 6.38 1.7128*5.00 6.27 125*75.0-120 30.00
1,1-Dichloropropene 5.00 5.81 0.691165.00 5.77 115 76.0-124 30.00
Benzene 5.00 5.86 1.41175.00 5.78 116 76.0-124 30.00
1,2-Dichloroethane 5.00 5.97 0.331195.00 5.99 120*76.0-119 30.00
Trichloroethene 5.00 4.65 24935.00 5.91 118 74.0-121 30.00
1,2-Dichloropropane 5.00 5.24 1.11055.00 5.30 106 74.0-124 30.00
Dibromomethane 5.00 5.60 1.41125.00 5.68 114 71.0-128 30.00
Bromodichloromethane 5.00 5.55 2.71115.00 5.70 114 72.0-120 30.00
cis-1,3-Dichloropropene 5.00 6.11 1.81225.00 6.00 120 73.0-122 30.00
4-Methyl-2-pentanone 25.0 28.3 7.311325.0 26.3 105 65.0-124 30.00
Toluene 5.00 5.42 1.51085.00 5.34 107 75.0-123 30.00
Methyl iodide 5.00 4.28 1.2865.00 4.23 85 55.0-123 30.00
trans-1,3-Dichloropropene 5.00 5.81 0.521165.00 5.84 117 70.0-125 30.00
Carbon disulfide 5.00 5.99 0.01205.00 5.99 120 65.0-132 30.00
1,1,2-Trichloroethane 5.00 5.76 4.41155.00 6.02 120 76.0-121 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 83 of 102
Blank Spike ID: LCS for HBN 69651 [VXX/5590]
Blank Spike Lab ID: 162198
Date Analyzed: 03/17/2015 13:47
Spike Duplicate ID: LCSD for HBN 69651 [VXX/5590]
Spike Duplicate Lab ID: 162199
Date Analyzed: 03/17/2015 14:12
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500424010, 31500424014QC for Samples:
Tetrachloroethene 5.00 5.39 4.91085.00 5.66 113*59.0-112 30.00
1,3-Dichloropropane 5.00 5.29 3.31065.00 5.47 109 74.0-120 30.00
2-Hexanone 25.0 28.1 0.3611225.0 28.0 112 56.0-133 30.00
Dibromochloromethane 5.00 5.51 8.81105.00 6.02 120 67.0-122 30.00
1,2-Dibromoethane 5.00 5.50 2.21105.00 5.62 112 74.0-119 30.00
Chlorobenzene 5.00 5.08 9.01025.00 5.56 111 74.0-120 30.00
1,1,1,2-Tetrachloroethane 5.00 5.70 111145.00 6.37 127*73.0-119 30.00
Bromoform 5.00 5.68 9.91145.00 6.27 125 62.0-127 30.00
Bromobenzene 5.00 5.33 9.61075.00 5.87 117 75.0-120 30.00
1,1,2,2-Tetrachloroethane 5.00 5.75 4.61155.00 6.02 120 68.0-129 30.00
1,2,3-Trichloropropane 5.00 5.82 3.31165.00 5.63 113 67.0-126 30.00
Ethyl Benzene 5.00 4.52 6.4905.00 4.82 96 76.0-123 30.00
m,p-Xylene 10.0 9.27 8.69310.0 10.1 101 76.0-124 30.00
Styrene 5.00 4.44 8.4895.00 4.83 97 76.0-121 30.00
o-Xylene 5.00 4.22 6.2845.00 4.49 90 75.0-124 30.00
Isopropylbenzene (Cumene)5.00 4.39 7.2885.00 4.72 94 77.0-120 30.00
n-Propylbenzene 5.00 4.69 7.2945.00 5.04 101 77.0-123 30.00
2-Chlorotoluene 5.00 4.78 5.7965.00 5.06 101 74.0-127 30.00
4-Chlorotoluene 5.00 4.81 14965.00 5.54 111 77.0-123 30.00
1,3,5-Trimethylbenzene 5.00 4.69 8.2945.00 5.09 102 76.0-122 30.00
tert-Butylbenzene 5.00 4.56 5.5915.00 4.82 96 67.0-122 30.00
1,2,4-Trimethylbenzene 5.00 4.77 6.9955.00 5.11 102 76.0-124 30.00
sec-Butylbenzene 5.00 4.78 8.0965.00 5.18 104 78.0-121 30.00
1,3-Dichlorobenzene 5.00 5.12 6.61025.00 5.47 109 75.0-120 30.00
4-Isopropyltoluene 5.00 4.63 8.3935.00 5.03 101 77.0-120 30.00
1,4-Dichlorobenzene 5.00 5.01 7.31005.00 5.39 108 70.0-125 30.00
1,2-Dichlorobenzene 5.00 5.18 5.81045.00 5.49 110 76.0-118 30.00
n-Butylbenzene 5.00 4.69 6.4945.00 5.00 100 78.0-118 30.00
1,2-Dibromo-3-chloropropane 30.0 32.5 0.9210830.0 32.8 109 62.0-130 30.00
1,2,4-Trichlorobenzene 5.00 4.62 4.4925.00 4.83 97 72.0-119 30.00
Hexachlorobutadiene 5.00 5.02 111005.00 5.58 112 69.0-121 30.00
Naphthalene 5.00 4.53 1.1915.00 4.58 92 67.0-122 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 84 of 102
Blank Spike ID: LCS for HBN 69651 [VXX/5590]
Blank Spike Lab ID: 162198
Date Analyzed: 03/17/2015 13:47
Spike Duplicate ID: LCSD for HBN 69651 [VXX/5590]
Spike Duplicate Lab ID: 162199
Date Analyzed: 03/17/2015 14:12
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500424010, 31500424014QC for Samples:
trans-1,4-Dichloro-2-butene 25.0 27.2 3.310925.0 28.1 112 61.0-132 30.00
1,2,3-Trichlorobenzene 5.00 4.92 5.5985.00 5.20 104 68.0-123 30.00
Surrogates
1,2-Dichloroethane-d4 114 105 64.0-140
Toluene d8 107 98 82.0-117
4-Bromofluorobenzene 103 104 85.0-115
Batch Information
Analytical Batch: VMS3554
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: JHL
Prep Batch: VXX5590
Prep Method: SW-846 5030B
Prep Date/Time: 03/17/2015 10:26
Spike Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Dupe Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 85 of 102
Batch Summary
SW-846 8270D SW-846 3520C 1L/1mLAnalytical Method:Prep Method:
XXX4630
03/12/2015 16:00
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
MB for HBN 69407 [XXX/4630]03/17/2015 11:18 MSD10 DTF162008XMS2258
LCS for HBN 69407 [XXX/4630]03/17/2015 11:39 MSD10 DTF162009XMS2258
CAM-1R 03/17/2015 12:01 MSD10 DTF31500424001XMS2258
CAM-1R(161778DUP)03/17/2015 12:23 MSD10 DTF162010XMS2258
FNW-4A 03/17/2015 13:30 MSD10 DTF31500424010XMS2258
OSW-5C 03/17/2015 16:37 MSD10 DTF31500424005XMS2258
OSW-5C(161782MS)03/17/2015 16:58 MSD10 DTF162011XMS2258
OSW-4 03/17/2015 17:20 MSD10 DTF31500424013XMS2258
OSW-2 03/17/2015 17:42 MSD10 DTF31500424014XMS2258
FW-1C 03/17/2015 18:04 MSD10 DTF31500424015XMS2258
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 86 of 102
Blank ID: MB for HBN 69407 [XXX/4630]
Blank Lab ID: 162008
Matrix: Water
Results by SW-846 8270D
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500424001, 31500424005, 31500424010, 31500424013, 31500424014, 31500424015
1,4 Dioxane ND 2.00 ug/L 1
Surrogates
Nitrobenzene-d5 71.0 50.0-150 %1
Batch Information
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 3/12/2015 4:00:05PM
Prep Initial Wt./Vol.: 1000 mL
Prep Extract Vol: 1 mL
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 87 of 102
Blank Spike ID: LCS for HBN 69407 [XXX/4630]
Blank Spike Lab ID: 162009
Date Analyzed: 03/17/2015 11:39
Results by SW-846 8270D
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)CL
Blank Spike (ug/L)
31500424001, 31500424005, 31500424010, 31500424013, 31500424014, 31500424015QC for Samples:
1,4 Dioxane 10.0 4.09 41 2.29-102
Surrogates
Nitrobenzene-d5 75.1 46.0-117
Batch Information
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Spike Init Wt./Vol.: 1000 mL Extract Vol: 1 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 88 of 102
Original Sample ID: 31500424005 (OSW-5C)
MS Sample ID: 162011
MSD Sample ID:
Analysis Date: 03/17/2015 16:37
Analysis Date: 03/17/2015 16:58
Analysis Date:
Matrix: Water
Results by SW-846 8270D
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/L)Spike Duplicate (ug/L)
CL RPD CL
QC for Samples:31500424001, 31500424005, 31500424010, 31500424013, 31500424014, 31500424015
1,4 Dioxane 80.4 11.1 98.6 164 *2.29-102
Surrogates
Nitrobenzene-d5 80.5 46.0-117
Batch Information
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
MS Init Wt./Vol.: 902 mL Extract Vol.: 1 mL
MSD Init Wt./Vol.: Extract Vol.:
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 89 of 102
Original Sample ID: 31500424001-D
Duplicate Sample ID: 162010
Analysis Date: 03/17/2015 12:01
Analysis Date: 03/17/2015 12:23
Matrix: Water
Results by SW-846 8270D
Duplicate Sample Summary
PARAMETER Original (ug/L)Duplicate (ug/L)RPD (%)RPD CL
QC for Samples:31500424001, 31500424005, 31500424010, 31500424013, 31500424014, 31500424015
Qual Qual
1,4 Dioxane ND ND 30.00
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Batch Information
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 90 of 102
Batch Summary
EPA 300.0 EPA 300.0Analytical Method:Prep Method:
INO3705
03/11/2015 11:40
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
OSW-5C 03/11/2015 11:40 IC2 PSW31500424005INO3705
OSW-6C 03/11/2015 11:54 IC2 PSW31500424002INO3705
OSW-4 03/11/2015 12:08 IC2 PSW31500424013INO3705
OSW-2 03/11/2015 12:22 IC2 PSW31500424014INO3705
FW-1C 03/11/2015 12:36 IC2 PSW31500424015INO3705
OSW-1 03/11/2015 12:50 IC2 PSW31500424008INO3705
FNW-3A 03/11/2015 13:04 IC2 PSW31500424009INO3705
FNW-4A 03/11/2015 13:18 IC2 PSW31500424010INO3705
MB for HBN 69356 [INO/3705]03/11/2015 14:01 IC2 PSW161825INO3705
LCS for HBN 69356 [INO/3705]03/11/2015 14:29 IC2 PSW161826INO3705
OSW-4(161790MS)03/11/2015 14:43 IC2 PSW161873INO3705
OSW-4(161790MSD)03/11/2015 14:57 IC2 PSW161874INO3705
FW-1C(161792DUP)03/11/2015 15:12 IC2 PSW161827INO3705
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 91 of 102
Blank ID: MB for HBN 69356 [INO/3705]
Blank Lab ID: 161825
Matrix: Water
Results by EPA 300.0
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500424002, 31500424005, 31500424008, 31500424009, 31500424010, 31500424013, 31500424014, 31500424015
Nitrate as N ND 0.300 mg/L 1
Sulfate ND 1.00 mg/L 1
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 3/11/2015 2:01:24PM
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 92 of 102
Blank Spike ID: LCS for HBN 69356 [INO/3705]
Blank Spike Lab ID: 161826
Date Analyzed: 03/11/2015 14:29
Results by EPA 300.0
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)CL
Blank Spike (mg/L)
31500424002, 31500424005, 31500424008, 31500424009, 31500424010, 31500424013, 31500424014,
31500424015
QC for Samples:
Nitrate as N 4.00 4.27 107 90.0-110
Sulfate 20.0 21.5 107 90.0-110
Batch Information
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 14:29
Spike Init Wt./Vol.: 10 mL Extract Vol: 10 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 93 of 102
Original Sample ID: 31500424013 (OSW-4)
MS Sample ID: 161873
MSD Sample ID: 161874
Analysis Date: 03/11/2015 12:08
Analysis Date: 03/11/2015 14:43
Analysis Date: 03/11/2015 14:57
Matrix: Water
Results by EPA 300.0
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (mg/L)Spike Duplicate (mg/L)
CL RPD CL
QC for Samples:31500424002, 31500424005, 31500424008, 31500424009, 31500424010, 31500424013, 31500424014,
31500424015
Sulfate 17.3 20.0 35.8 20.0 36.4 96 1.792 20.0090.0-110
Nitrate as N ND 4.00 3.95 4.00 4.02 101 1.899 20.0090.0-110
Batch Information
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 12:08
MS Init Wt./Vol.: 10 mL Extract Vol.: 10 mL
MSD Init Wt./Vol.: 10 mL Extract Vol.: 10 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 94 of 102
Original Sample ID: 31500424015-F
Duplicate Sample ID: 161827
Analysis Date: 03/11/2015 12:36
Analysis Date: 03/11/2015 15:12
Matrix: Water
Results by EPA 300.0
Duplicate Sample Summary
PARAMETER Original (mg/L)Duplicate (mg/L)RPD (%)RPD CL
QC for Samples:31500424002, 31500424005, 31500424008, 31500424009, 31500424010, 31500424013, 31500424014,
31500424015
Qual Qual
Sulfate 14.2 14.6 2.8 10.00
Nitrate as N ND ND 10.00
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Batch Information
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 95 of 102
Batch Summary
EPA 300.0 EPA 300.0Analytical Method:Prep Method:
INO3710
03/13/2015 15:43
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
MB for HBN 69420 [INO/3710]03/13/2015 15:43 IC2 PSW162117INO3710
LCS for HBN 69420 [INO/3710]03/13/2015 15:57 IC2 PSW162118INO3710
FNW-3A 03/13/2015 16:11 IC2 PSW31500424009INO3710
FNW-3A(161786MS)03/13/2015 16:25 IC2 PSW162119INO3710
FNW-3A(161786MSD)03/13/2015 16:39 IC2 PSW162120INO3710
AM-OU3B-SW2-099(162028DUP)03/13/2015 17:22 IC2 PSW162121INO3710
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 96 of 102
Blank ID: MB for HBN 69420 [INO/3710]
Blank Lab ID: 162117
Matrix: Water
Results by EPA 300.0
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500424009
Sulfate ND 1.00 mg/L 1
Batch Information
Prep Batch: INO3710
Prep Method: EPA 300.0
Prep Date/Time: 3/13/2015 3:43:09PM
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3710
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 97 of 102
Blank Spike ID: LCS for HBN 69420 [INO/3710]
Blank Spike Lab ID: 162118
Date Analyzed: 03/13/2015 15:57
Results by EPA 300.0
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)CL
Blank Spike (mg/L)
31500424009QC for Samples:
Sulfate 20.0 19.7 98 90.0-110
Batch Information
Analytical Batch: INO3710
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Prep Batch: INO3710
Prep Method: EPA 300.0
Prep Date/Time: 03/13/2015 15:57
Spike Init Wt./Vol.: 10 mL Extract Vol: 10 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 98 of 102
Original Sample ID: 31500424009 (FNW-3A)
MS Sample ID: 162119
MSD Sample ID: 162120
Analysis Date: 03/13/2015 16:11
Analysis Date: 03/13/2015 16:25
Analysis Date: 03/13/2015 16:39
Matrix: Water
Results by EPA 300.0
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (mg/L)Spike Duplicate (mg/L)
CL RPD CL
QC for Samples:31500424009
Sulfate 82.3 200 277 200 276 97 0.3697 20.0090.0-110
Batch Information
Analytical Batch: INO3710
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Prep Batch: INO3710
Prep Method: EPA 300.0
Prep Date/Time: 03/13/2015 16:11
MS Init Wt./Vol.: 10 mL Extract Vol.: 10 mL
MSD Init Wt./Vol.: 10 mL Extract Vol.: 10 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500424 Page 99 of 102
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Report Number:31500427
Client Project:HeatCraft
Laboratory Report of Analysis
Ray Roblin
CORR ENVIRONMENTAL
4609 Candlestick Drive
Garland, TX 75043
Dear Ray Roblin,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be
retained in our files for a period of five years in the event they are required for future reference. All results are
intended to be used in their entirety and SGS is not responsible for use of less than the complete report. Any
samples submitted to our laboratory will be retained for a maximum of thirty (30) days from the date of this report
unless other arrangements are requested.
If there are any questions about the report or services performed during this project, please call Amy J. Boehm at
[phone]. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America Inc.
__________________________________________________________________
Amy J. Boehm Date
Project Manager
[e-mail]
To:
Print Date: 03/24/2015 N.C. Certification # 481
This document is issued by the Company under its General Conditions of Service accessible at http://www.sgs.com/en/Terms-and-Conditions.htm. Attention is drawn
to the limitation of liability, indemnification and jurisdiction issues defined therein.
Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of
Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their
rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful
and offenders may be prosecuted to the fullest extent of the law.
WO# 31500427 Page 1 of 77
Laboratory Qualifiers
Report Definitions
DL Method, Instrument, or Estimated Detection Limit per Analytical Method
CL Control Limits for the recovery result of a parameter
LOQ Reporting Limit
DF Dilution Factor
RPD Relative Percent Difference
LCS(D) Laboratory Control Spike (Duplicate)
MS(D) Matrix Spike (Duplicate)
MB Method Blank
Qualifier Definitions
* Recovery or RPD outside of control limits
B Analyte was detected in the Lab Method Blank at a level above the LOQ
U Undetected (Reported as ND or < DL)
J Estimated Concentration.
E Amount detected is greater than the Upper Calibration Limit
TIC Tentatively Identified Compound
ND Not Detected
P RPD > 40% between results of dual columns
D Spike or surrogate was diluted out in order to achieve a parameter result within instrument calibration
range
Samples requiring manual integrations for various congeners and/or standards are marked and dated by the analyst. A
code definition is provided below:
M1 Mis-identified peak
M2 Software did not integrate peak
M3 Incorrect baseline construction (i.e. not all of peak included; two peaks integrated as one)
M4 Pattern integration required (i.e. DRO, GRO, PCB, Toxaphene and Technical Chlordane)
M5 Other - Explained in case narrative
Note Results pages that include a value for "Solids (%)" have been adjusted for moisture content.
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 2 of 77
Sample Summary
Client Sample ID Lab Sample ID Collected Received Matrix
OSW-7C 31500427001 03/11/2015 09:40 03/11/2015 15:20 Water
OSW-7B 31500427002 03/11/2015 10:00 03/11/2015 15:20 Water
OSW-7A 31500427003 03/11/2015 10:20 03/11/2015 15:20 Water
CR-4 31500427004 03/11/2015 10:45 03/11/2015 15:20 Water
CR-3 Water 31500427005 03/11/2015 11:00 03/11/2015 15:20 Water
CR-3 Soil 31500427006 03/11/2015 11:00 03/11/2015 15:20 Soil-Solid as dry weight
CR-2 Water 31500427007 03/11/2015 11:20 03/11/2015 15:20 Water
CR-2 Soil 31500427008 03/11/2015 11:20 03/11/2015 15:20 Soil-Solid as dry weight
CR-1 Water 31500427009 03/11/2015 11:30 03/11/2015 15:20 Water
CR-1 Soil 31500427010 03/11/2015 11:30 03/11/2015 15:20 Soil-Solid as dry weight
MW-2A 31500427011 03/11/2015 13:30 03/11/2015 15:20 Water
MW-2B 31500427012 03/11/2015 13:35 03/11/2015 15:20 Water
EW-6 31500427013 03/11/2015 13:50 03/11/2015 15:20 Water
EW-4 31500427014 03/11/2015 14:20 03/11/2015 15:20 Water
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 3 of 77
Case Narrative
CR-3 Soil(161904MSD)
Bad purge caused elevated analyte recoveries for early eluting/purging compounds.
EW-4
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
EW-6
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
LCS for HBN 69651 [VXX/5590]
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
LCSD for HBN 69651 [VXX/5590]
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
MB for HBN 69651 [VXX/5590]
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
MW-2A
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
MW-2B
Carbon Tetrachloride; 2,2-Dichloropropane; 1,1,1-Trichloroethane; Methylene Chloride were above QC acceptance limits
in LCS/LCSD. All reported samples were non-detect for these analytes.
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 4 of 77
Detectable Results Summary
Client Sample ID: CR-4
Lab Sample ID: 31500427004-A UnitsParameterResult
Trichloroethene ug/LSW-846 8260B 2.99
Vinyl chloride ug/L1.34
cis-1,2-Dichloroethene ug/L9.58
Client Sample ID: CR-3 Water
Lab Sample ID: 31500427005-A UnitsParameterResult
1,1-Dichloroethane ug/LSW-846 8260B 1.94
1,1-Dichloroethene ug/L1.41
Trichloroethene ug/L13.4
Vinyl chloride ug/L14.0
cis-1,2-Dichloroethene ug/L39.0
Client Sample ID: CR-2 Water
Lab Sample ID: 31500427007-A UnitsParameterResult
1,1-Dichloroethane ug/LSW-846 8260B 2.29
1,1-Dichloroethene ug/L1.74
Trichloroethene ug/L14.7
Vinyl chloride ug/L20.1
cis-1,2-Dichloroethene ug/L46.1
1,4 Dioxane ug/LSW-846 8270D 2.43
Client Sample ID: CR-1 Water
Lab Sample ID: 31500427009-A UnitsParameterResult
1,1-Dichloroethane ug/LSW-846 8260B 2.65
1,1-Dichloroethene ug/L2.16
Trichloroethene ug/L16.8
Vinyl chloride ug/L17.3
cis-1,2-Dichloroethene ug/L54.9
Client Sample ID: MW-2A
Lab Sample ID: 31500427011-F UnitsParameterResult
Sulfate mg/LEPA 300.0 3.82
1,1-Dichloroethane ug/LSW-846 8260B 92.4
1,1-Dichloroethene ug/L93.6
Chloroethane ug/L1.06
cis-1,2-Dichloroethene ug/L98.8
Client Sample ID: MW-2B
Lab Sample ID: 31500427012 UnitsParameterResult
1,1-Dichloroethane ug/LSW-846 8260B 92.6
1,1-Dichloroethene ug/L93.7
Chloroethane ug/L1.04
cis-1,2-Dichloroethene ug/L98.0
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 5 of 77
Detectable Results Summary
Client Sample ID: EW-6
Lab Sample ID: 31500427013 UnitsParameterResult
1,1,1-Trichloroethane ug/LSW-846 8260B 330
1,1-Dichloroethane ug/L60.6
1,1-Dichloroethene ug/L18.1
Trichloroethene ug/L10.5
Vinyl chloride ug/L74.2
cis-1,2-Dichloroethene ug/L321
trans-1,2-Dichloroethene ug/L3.12
Client Sample ID: EW-4
Lab Sample ID: 31500427014 UnitsParameterResult
1,1,1-Trichloroethane ug/LSW-846 8260B 1500
1,1-Dichloroethane ug/L540
1,1-Dichloroethene ug/L1520
Chloroethane ug/L10.2
Toluene ug/L8.72
Trichloroethene ug/L541
Vinyl chloride ug/L333
cis-1,2-Dichloroethene ug/L8780
trans-1,2-Dichloroethene ug/L77.8
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 6 of 77
Client Sample ID: OSW-7C
Client Project ID: HeatCraft
Lab Sample ID: 31500427001-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 09:40
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-7C
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 18:44
1,1,1-Trichloroethane ND ug/L 11.00 03/12/2015 18:44
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 18:44
1,1,2-Trichloroethane ND ug/L 11.00 03/12/2015 18:44
1,1-Dichloroethane ND ug/L 11.00 03/12/2015 18:44
1,1-Dichloroethene ND ug/L 11.00 03/12/2015 18:44
1,1-Dichloropropene ND ug/L 11.00 03/12/2015 18:44
1,2,3-Trichlorobenzene ND ug/L 11.00 03/12/2015 18:44
1,2,3-Trichloropropane ND ug/L 11.00 03/12/2015 18:44
1,2,4-Trichlorobenzene ND ug/L 11.00 03/12/2015 18:44
1,2,4-Trimethylbenzene ND ug/L 11.00 03/12/2015 18:44
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/12/2015 18:44
1,2-Dibromoethane ND ug/L 11.00 03/12/2015 18:44
1,2-Dichlorobenzene ND ug/L 11.00 03/12/2015 18:44
1,2-Dichloroethane ND ug/L 11.00 03/12/2015 18:44
1,2-Dichloropropane ND ug/L 11.00 03/12/2015 18:44
1,3,5-Trimethylbenzene ND ug/L 11.00 03/12/2015 18:44
1,3-Dichlorobenzene ND ug/L 11.00 03/12/2015 18:44
1,3-Dichloropropane ND ug/L 11.00 03/12/2015 18:44
1,4-Dichlorobenzene ND ug/L 11.00 03/12/2015 18:44
2,2-Dichloropropane ND ug/L 11.00 03/12/2015 18:44
2-Butanone ND ug/L 125.0 03/12/2015 18:44
2-Chlorotoluene ND ug/L 11.00 03/12/2015 18:44
2-Hexanone ND ug/L 15.00 03/12/2015 18:44
4-Chlorotoluene ND ug/L 11.00 03/12/2015 18:44
4-Isopropyltoluene ND ug/L 11.00 03/12/2015 18:44
4-Methyl-2-pentanone ND ug/L 15.00 03/12/2015 18:44
Acetone ND ug/L 125.0 03/12/2015 18:44
Benzene ND ug/L 11.00 03/12/2015 18:44
Bromobenzene ND ug/L 11.00 03/12/2015 18:44
Bromochloromethane ND ug/L 11.00 03/12/2015 18:44
Bromodichloromethane ND ug/L 11.00 03/12/2015 18:44
Bromoform ND ug/L 11.00 03/12/2015 18:44
Bromomethane ND ug/L 11.00 03/12/2015 18:44
n-Butylbenzene ND ug/L 11.00 03/12/2015 18:44
Carbon disulfide ND ug/L 11.00 03/12/2015 18:44
Carbon tetrachloride ND ug/L 11.00 03/12/2015 18:44
Chlorobenzene ND ug/L 11.00 03/12/2015 18:44
Chloroethane ND ug/L 11.00 03/12/2015 18:44
Chloroform ND ug/L 11.00 03/12/2015 18:44
Chloromethane ND ug/L 11.00 03/12/2015 18:44
Dibromochloromethane ND ug/L 11.00 03/12/2015 18:44
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 7 of 77
Client Sample ID: OSW-7C
Client Project ID: HeatCraft
Lab Sample ID: 31500427001-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 09:40
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-7C
Date Analyzed
Dibromomethane ND ug/L 11.00 03/12/2015 18:44
Dichlorodifluoromethane ND ug/L 15.00 03/12/2015 18:44
cis-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 18:44
trans-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 18:44
Diisopropyl Ether ND ug/L 11.00 03/12/2015 18:44
Ethyl Benzene ND ug/L 11.00 03/12/2015 18:44
Hexachlorobutadiene ND ug/L 11.00 03/12/2015 18:44
Isopropylbenzene (Cumene) ND ug/L 11.00 03/12/2015 18:44
Methyl iodide ND ug/L 11.00 03/12/2015 18:44
Methylene chloride ND ug/L 15.00 03/12/2015 18:44
Naphthalene ND ug/L 11.00 03/12/2015 18:44
Styrene ND ug/L 11.00 03/12/2015 18:44
Tetrachloroethene ND ug/L 11.00 03/12/2015 18:44
Toluene ND ug/L 11.00 03/12/2015 18:44
Trichloroethene ND ug/L 11.00 03/12/2015 18:44
Trichlorofluoromethane ND ug/L 11.00 03/12/2015 18:44
Vinyl chloride ND ug/L 11.00 03/12/2015 18:44
Xylene (total)ND ug/L 12.00 03/12/2015 18:44
cis-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 18:44
m,p-Xylene ND ug/L 12.00 03/12/2015 18:44
n-Propylbenzene ND ug/L 11.00 03/12/2015 18:44
o-Xylene ND ug/L 11.00 03/12/2015 18:44
sec-Butylbenzene ND ug/L 11.00 03/12/2015 18:44
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/12/2015 18:44
tert-Butylbenzene ND ug/L 11.00 03/12/2015 18:44
trans-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 18:44
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/12/2015 18:44
Surrogates
1,2-Dichloroethane-d4 102 % 164.0-140 03/12/2015 18:44
4-Bromofluorobenzene 96.0 % 185.0-115 03/12/2015 18:44
Toluene d8 94.0 % 182.0-117 03/12/2015 18:44
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/12/2015 16:18
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 8 of 77
Client Sample ID: OSW-7B
Client Project ID: HeatCraft
Lab Sample ID: 31500427002-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 10:00
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-7B
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 19:09
1,1,1-Trichloroethane ND ug/L 11.00 03/12/2015 19:09
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/12/2015 19:09
1,1,2-Trichloroethane ND ug/L 11.00 03/12/2015 19:09
1,1-Dichloroethane ND ug/L 11.00 03/12/2015 19:09
1,1-Dichloroethene ND ug/L 11.00 03/12/2015 19:09
1,1-Dichloropropene ND ug/L 11.00 03/12/2015 19:09
1,2,3-Trichlorobenzene ND ug/L 11.00 03/12/2015 19:09
1,2,3-Trichloropropane ND ug/L 11.00 03/12/2015 19:09
1,2,4-Trichlorobenzene ND ug/L 11.00 03/12/2015 19:09
1,2,4-Trimethylbenzene ND ug/L 11.00 03/12/2015 19:09
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/12/2015 19:09
1,2-Dibromoethane ND ug/L 11.00 03/12/2015 19:09
1,2-Dichlorobenzene ND ug/L 11.00 03/12/2015 19:09
1,2-Dichloroethane ND ug/L 11.00 03/12/2015 19:09
1,2-Dichloropropane ND ug/L 11.00 03/12/2015 19:09
1,3,5-Trimethylbenzene ND ug/L 11.00 03/12/2015 19:09
1,3-Dichlorobenzene ND ug/L 11.00 03/12/2015 19:09
1,3-Dichloropropane ND ug/L 11.00 03/12/2015 19:09
1,4-Dichlorobenzene ND ug/L 11.00 03/12/2015 19:09
2,2-Dichloropropane ND ug/L 11.00 03/12/2015 19:09
2-Butanone ND ug/L 125.0 03/12/2015 19:09
2-Chlorotoluene ND ug/L 11.00 03/12/2015 19:09
2-Hexanone ND ug/L 15.00 03/12/2015 19:09
4-Chlorotoluene ND ug/L 11.00 03/12/2015 19:09
4-Isopropyltoluene ND ug/L 11.00 03/12/2015 19:09
4-Methyl-2-pentanone ND ug/L 15.00 03/12/2015 19:09
Acetone ND ug/L 125.0 03/12/2015 19:09
Benzene ND ug/L 11.00 03/12/2015 19:09
Bromobenzene ND ug/L 11.00 03/12/2015 19:09
Bromochloromethane ND ug/L 11.00 03/12/2015 19:09
Bromodichloromethane ND ug/L 11.00 03/12/2015 19:09
Bromoform ND ug/L 11.00 03/12/2015 19:09
Bromomethane ND ug/L 11.00 03/12/2015 19:09
n-Butylbenzene ND ug/L 11.00 03/12/2015 19:09
Carbon disulfide ND ug/L 11.00 03/12/2015 19:09
Carbon tetrachloride ND ug/L 11.00 03/12/2015 19:09
Chlorobenzene ND ug/L 11.00 03/12/2015 19:09
Chloroethane ND ug/L 11.00 03/12/2015 19:09
Chloroform ND ug/L 11.00 03/12/2015 19:09
Chloromethane ND ug/L 11.00 03/12/2015 19:09
Dibromochloromethane ND ug/L 11.00 03/12/2015 19:09
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 9 of 77
Client Sample ID: OSW-7B
Client Project ID: HeatCraft
Lab Sample ID: 31500427002-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 10:00
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-7B
Date Analyzed
Dibromomethane ND ug/L 11.00 03/12/2015 19:09
Dichlorodifluoromethane ND ug/L 15.00 03/12/2015 19:09
cis-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 19:09
trans-1,3-Dichloropropene ND ug/L 11.00 03/12/2015 19:09
Diisopropyl Ether ND ug/L 11.00 03/12/2015 19:09
Ethyl Benzene ND ug/L 11.00 03/12/2015 19:09
Hexachlorobutadiene ND ug/L 11.00 03/12/2015 19:09
Isopropylbenzene (Cumene) ND ug/L 11.00 03/12/2015 19:09
Methyl iodide ND ug/L 11.00 03/12/2015 19:09
Methylene chloride ND ug/L 15.00 03/12/2015 19:09
Naphthalene ND ug/L 11.00 03/12/2015 19:09
Styrene ND ug/L 11.00 03/12/2015 19:09
Tetrachloroethene ND ug/L 11.00 03/12/2015 19:09
Toluene ND ug/L 11.00 03/12/2015 19:09
Trichloroethene ND ug/L 11.00 03/12/2015 19:09
Trichlorofluoromethane ND ug/L 11.00 03/12/2015 19:09
Vinyl chloride ND ug/L 11.00 03/12/2015 19:09
Xylene (total)ND ug/L 12.00 03/12/2015 19:09
cis-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 19:09
m,p-Xylene ND ug/L 12.00 03/12/2015 19:09
n-Propylbenzene ND ug/L 11.00 03/12/2015 19:09
o-Xylene ND ug/L 11.00 03/12/2015 19:09
sec-Butylbenzene ND ug/L 11.00 03/12/2015 19:09
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/12/2015 19:09
tert-Butylbenzene ND ug/L 11.00 03/12/2015 19:09
trans-1,2-Dichloroethene ND ug/L 11.00 03/12/2015 19:09
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/12/2015 19:09
Surrogates
1,2-Dichloroethane-d4 101 % 164.0-140 03/12/2015 19:09
4-Bromofluorobenzene 96.0 % 185.0-115 03/12/2015 19:09
Toluene d8 94.0 % 182.0-117 03/12/2015 19:09
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/12/2015 16:18
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 10 of 77
Client Sample ID: OSW-7A
Client Project ID: HeatCraft
Lab Sample ID: 31500427003-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 10:20
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-7A
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 11:27
1,1,1-Trichloroethane ND ug/L 11.00 03/13/2015 11:27
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 11:27
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 11:27
1,1-Dichloroethane ND ug/L 11.00 03/13/2015 11:27
1,1-Dichloroethene ND ug/L 11.00 03/13/2015 11:27
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 11:27
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 11:27
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 11:27
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 11:27
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 11:27
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 11:27
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 11:27
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 11:27
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 11:27
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 11:27
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 11:27
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 11:27
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 11:27
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 11:27
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 11:27
2-Butanone ND ug/L 125.0 03/13/2015 11:27
2-Chlorotoluene ND ug/L 11.00 03/13/2015 11:27
2-Hexanone ND ug/L 15.00 03/13/2015 11:27
4-Chlorotoluene ND ug/L 11.00 03/13/2015 11:27
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 11:27
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 11:27
Acetone ND ug/L 125.0 03/13/2015 11:27
Benzene ND ug/L 11.00 03/13/2015 11:27
Bromobenzene ND ug/L 11.00 03/13/2015 11:27
Bromochloromethane ND ug/L 11.00 03/13/2015 11:27
Bromodichloromethane ND ug/L 11.00 03/13/2015 11:27
Bromoform ND ug/L 11.00 03/13/2015 11:27
Bromomethane ND ug/L 11.00 03/13/2015 11:27
n-Butylbenzene ND ug/L 11.00 03/13/2015 11:27
Carbon disulfide ND ug/L 11.00 03/13/2015 11:27
Carbon tetrachloride ND ug/L 11.00 03/13/2015 11:27
Chlorobenzene ND ug/L 11.00 03/13/2015 11:27
Chloroethane ND ug/L 11.00 03/13/2015 11:27
Chloroform ND ug/L 11.00 03/13/2015 11:27
Chloromethane ND ug/L 11.00 03/13/2015 11:27
Dibromochloromethane ND ug/L 11.00 03/13/2015 11:27
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 11 of 77
Client Sample ID: OSW-7A
Client Project ID: HeatCraft
Lab Sample ID: 31500427003-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 10:20
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of OSW-7A
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 11:27
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 11:27
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 11:27
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 11:27
Diisopropyl Ether ND ug/L 11.00 03/13/2015 11:27
Ethyl Benzene ND ug/L 11.00 03/13/2015 11:27
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 11:27
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 11:27
Methyl iodide ND ug/L 11.00 03/13/2015 11:27
Methylene chloride ND ug/L 15.00 03/13/2015 11:27
Naphthalene ND ug/L 11.00 03/13/2015 11:27
Styrene ND ug/L 11.00 03/13/2015 11:27
Tetrachloroethene ND ug/L 11.00 03/13/2015 11:27
Toluene ND ug/L 11.00 03/13/2015 11:27
Trichloroethene ND ug/L 11.00 03/13/2015 11:27
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 11:27
Vinyl chloride ND ug/L 11.00 03/13/2015 11:27
Xylene (total)ND ug/L 12.00 03/13/2015 11:27
cis-1,2-Dichloroethene ND ug/L 11.00 03/13/2015 11:27
m,p-Xylene ND ug/L 12.00 03/13/2015 11:27
n-Propylbenzene ND ug/L 11.00 03/13/2015 11:27
o-Xylene ND ug/L 11.00 03/13/2015 11:27
sec-Butylbenzene ND ug/L 11.00 03/13/2015 11:27
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 11:27
tert-Butylbenzene ND ug/L 11.00 03/13/2015 11:27
trans-1,2-Dichloroethene ND ug/L 11.00 03/13/2015 11:27
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 11:27
Surrogates
1,2-Dichloroethane-d4 100 % 164.0-140 03/13/2015 11:27
4-Bromofluorobenzene 96.0 % 185.0-115 03/13/2015 11:27
Toluene d8 91.0 % 182.0-117 03/13/2015 11:27
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 12 of 77
Client Sample ID: CR-4
Client Project ID: HeatCraft
Lab Sample ID: 31500427004-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 10:45
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-4
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 11:52
1,1,1-Trichloroethane ND ug/L 11.00 03/13/2015 11:52
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 11:52
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 11:52
1,1-Dichloroethane ND ug/L 11.00 03/13/2015 11:52
1,1-Dichloroethene ND ug/L 11.00 03/13/2015 11:52
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 11:52
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 11:52
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 11:52
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 11:52
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 11:52
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 11:52
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 11:52
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 11:52
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 11:52
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 11:52
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 11:52
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 11:52
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 11:52
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 11:52
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 11:52
2-Butanone ND ug/L 125.0 03/13/2015 11:52
2-Chlorotoluene ND ug/L 11.00 03/13/2015 11:52
2-Hexanone ND ug/L 15.00 03/13/2015 11:52
4-Chlorotoluene ND ug/L 11.00 03/13/2015 11:52
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 11:52
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 11:52
Acetone ND ug/L 125.0 03/13/2015 11:52
Benzene ND ug/L 11.00 03/13/2015 11:52
Bromobenzene ND ug/L 11.00 03/13/2015 11:52
Bromochloromethane ND ug/L 11.00 03/13/2015 11:52
Bromodichloromethane ND ug/L 11.00 03/13/2015 11:52
Bromoform ND ug/L 11.00 03/13/2015 11:52
Bromomethane ND ug/L 11.00 03/13/2015 11:52
n-Butylbenzene ND ug/L 11.00 03/13/2015 11:52
Carbon disulfide ND ug/L 11.00 03/13/2015 11:52
Carbon tetrachloride ND ug/L 11.00 03/13/2015 11:52
Chlorobenzene ND ug/L 11.00 03/13/2015 11:52
Chloroethane ND ug/L 11.00 03/13/2015 11:52
Chloroform ND ug/L 11.00 03/13/2015 11:52
Chloromethane ND ug/L 11.00 03/13/2015 11:52
Dibromochloromethane ND ug/L 11.00 03/13/2015 11:52
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 13 of 77
Client Sample ID: CR-4
Client Project ID: HeatCraft
Lab Sample ID: 31500427004-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 10:45
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-4
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 11:52
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 11:52
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 11:52
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 11:52
Diisopropyl Ether ND ug/L 11.00 03/13/2015 11:52
Ethyl Benzene ND ug/L 11.00 03/13/2015 11:52
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 11:52
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 11:52
Methyl iodide ND ug/L 11.00 03/13/2015 11:52
Methylene chloride ND ug/L 15.00 03/13/2015 11:52
Naphthalene ND ug/L 11.00 03/13/2015 11:52
Styrene ND ug/L 11.00 03/13/2015 11:52
Tetrachloroethene ND ug/L 11.00 03/13/2015 11:52
Toluene ND ug/L 11.00 03/13/2015 11:52
Trichloroethene 2.99 ug/L 11.00 03/13/2015 11:52
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 11:52
Vinyl chloride 1.34 ug/L 11.00 03/13/2015 11:52
Xylene (total)ND ug/L 12.00 03/13/2015 11:52
cis-1,2-Dichloroethene 9.58 ug/L 11.00 03/13/2015 11:52
m,p-Xylene ND ug/L 12.00 03/13/2015 11:52
n-Propylbenzene ND ug/L 11.00 03/13/2015 11:52
o-Xylene ND ug/L 11.00 03/13/2015 11:52
sec-Butylbenzene ND ug/L 11.00 03/13/2015 11:52
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 11:52
tert-Butylbenzene ND ug/L 11.00 03/13/2015 11:52
trans-1,2-Dichloroethene ND ug/L 11.00 03/13/2015 11:52
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 11:52
Surrogates
1,2-Dichloroethane-d4 102 % 164.0-140 03/13/2015 11:52
4-Bromofluorobenzene 96.0 % 185.0-115 03/13/2015 11:52
Toluene d8 91.0 % 182.0-117 03/13/2015 11:52
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 14 of 77
Client Sample ID: CR-3 Water
Client Project ID: HeatCraft
Lab Sample ID: 31500427005-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:00
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-3 Water
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 12:17
1,1,1-Trichloroethane ND ug/L 11.00 03/13/2015 12:17
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 12:17
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 12:17
1,1-Dichloroethane 1.94 ug/L 11.00 03/13/2015 12:17
1,1-Dichloroethene 1.41 ug/L 11.00 03/13/2015 12:17
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 12:17
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 12:17
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 12:17
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 12:17
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 12:17
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 12:17
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 12:17
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 12:17
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 12:17
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 12:17
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 12:17
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 12:17
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 12:17
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 12:17
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 12:17
2-Butanone ND ug/L 125.0 03/13/2015 12:17
2-Chlorotoluene ND ug/L 11.00 03/13/2015 12:17
2-Hexanone ND ug/L 15.00 03/13/2015 12:17
4-Chlorotoluene ND ug/L 11.00 03/13/2015 12:17
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 12:17
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 12:17
Acetone ND ug/L 125.0 03/13/2015 12:17
Benzene ND ug/L 11.00 03/13/2015 12:17
Bromobenzene ND ug/L 11.00 03/13/2015 12:17
Bromochloromethane ND ug/L 11.00 03/13/2015 12:17
Bromodichloromethane ND ug/L 11.00 03/13/2015 12:17
Bromoform ND ug/L 11.00 03/13/2015 12:17
Bromomethane ND ug/L 11.00 03/13/2015 12:17
n-Butylbenzene ND ug/L 11.00 03/13/2015 12:17
Carbon disulfide ND ug/L 11.00 03/13/2015 12:17
Carbon tetrachloride ND ug/L 11.00 03/13/2015 12:17
Chlorobenzene ND ug/L 11.00 03/13/2015 12:17
Chloroethane ND ug/L 11.00 03/13/2015 12:17
Chloroform ND ug/L 11.00 03/13/2015 12:17
Chloromethane ND ug/L 11.00 03/13/2015 12:17
Dibromochloromethane ND ug/L 11.00 03/13/2015 12:17
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 15 of 77
Client Sample ID: CR-3 Water
Client Project ID: HeatCraft
Lab Sample ID: 31500427005-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:00
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-3 Water
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 12:17
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 12:17
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 12:17
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 12:17
Diisopropyl Ether ND ug/L 11.00 03/13/2015 12:17
Ethyl Benzene ND ug/L 11.00 03/13/2015 12:17
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 12:17
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 12:17
Methyl iodide ND ug/L 11.00 03/13/2015 12:17
Methylene chloride ND ug/L 15.00 03/13/2015 12:17
Naphthalene ND ug/L 11.00 03/13/2015 12:17
Styrene ND ug/L 11.00 03/13/2015 12:17
Tetrachloroethene ND ug/L 11.00 03/13/2015 12:17
Toluene ND ug/L 11.00 03/13/2015 12:17
Trichloroethene 13.4 ug/L 11.00 03/13/2015 12:17
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 12:17
Vinyl chloride 14.0 ug/L 11.00 03/13/2015 12:17
Xylene (total)ND ug/L 12.00 03/13/2015 12:17
cis-1,2-Dichloroethene 39.0 ug/L 11.00 03/13/2015 12:17
m,p-Xylene ND ug/L 12.00 03/13/2015 12:17
n-Propylbenzene ND ug/L 11.00 03/13/2015 12:17
o-Xylene ND ug/L 11.00 03/13/2015 12:17
sec-Butylbenzene ND ug/L 11.00 03/13/2015 12:17
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 12:17
tert-Butylbenzene ND ug/L 11.00 03/13/2015 12:17
trans-1,2-Dichloroethene ND ug/L 11.00 03/13/2015 12:17
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 12:17
Surrogates
1,2-Dichloroethane-d4 103 % 164.0-140 03/13/2015 12:17
4-Bromofluorobenzene 96.0 % 185.0-115 03/13/2015 12:17
Toluene d8 91.0 % 182.0-117 03/13/2015 12:17
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 16 of 77
Client Sample ID: CR-3 Soil
Client Project ID: HeatCraft
Lab Sample ID: 31500427006-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:00
Received Date: 03/11/2015 15:20
Matrix: Soil-Solid as dry weight
Solids (%): 78.30
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-3 Soil
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 15.04 03/16/2015 16:06
1,1,1-Trichloroethane ND ug/Kg 15.04 03/16/2015 16:06
1,1,2,2-Tetrachloroethane ND ug/Kg 15.04 03/16/2015 16:06
1,1,2-Trichloroethane ND ug/Kg 15.04 03/16/2015 16:06
1,1-Dichloroethane ND ug/Kg 15.04 03/16/2015 16:06
1,1-Dichloroethene ND ug/Kg 15.04 03/16/2015 16:06
1,1-Dichloropropene ND ug/Kg 15.04 03/16/2015 16:06
1,2,3-Trichlorobenzene ND ug/Kg 15.04 03/16/2015 16:06
1,2,3-Trichloropropane ND ug/Kg 15.04 03/16/2015 16:06
1,2,4-Trichlorobenzene ND ug/Kg 15.04 03/16/2015 16:06
1,2,4-Trimethylbenzene ND ug/Kg 15.04 03/16/2015 16:06
1,2-Dibromo-3-chloropropane ND ug/Kg 130.3 03/16/2015 16:06
1,2-Dibromoethane ND ug/Kg 15.04 03/16/2015 16:06
1,2-Dichlorobenzene ND ug/Kg 15.04 03/16/2015 16:06
1,2-Dichloroethane ND ug/Kg 15.04 03/16/2015 16:06
1,2-Dichloropropane ND ug/Kg 15.04 03/16/2015 16:06
1,3,5-Trimethylbenzene ND ug/Kg 15.04 03/16/2015 16:06
1,3-Dichlorobenzene ND ug/Kg 15.04 03/16/2015 16:06
1,3-Dichloropropane ND ug/Kg 15.04 03/16/2015 16:06
1,4-Dichlorobenzene ND ug/Kg 15.04 03/16/2015 16:06
2,2-Dichloropropane ND ug/Kg 15.04 03/16/2015 16:06
2-Butanone ND ug/Kg 125.2 03/16/2015 16:06
2-Chlorotoluene ND ug/Kg 15.04 03/16/2015 16:06
2-Hexanone ND ug/Kg 112.6 03/16/2015 16:06
4-Chlorotoluene ND ug/Kg 15.04 03/16/2015 16:06
4-Isopropyltoluene ND ug/Kg 15.04 03/16/2015 16:06
4-Methyl-2-pentanone ND ug/Kg 112.6 03/16/2015 16:06
Acetone ND ug/Kg 150.4 03/16/2015 16:06
Benzene ND ug/Kg 15.04 03/16/2015 16:06
Bromobenzene ND ug/Kg 15.04 03/16/2015 16:06
Bromochloromethane ND ug/Kg 15.04 03/16/2015 16:06
Bromodichloromethane ND ug/Kg 15.04 03/16/2015 16:06
Bromoform ND ug/Kg 15.04 03/16/2015 16:06
Bromomethane ND ug/Kg 15.04 03/16/2015 16:06
n-Butylbenzene ND ug/Kg 15.04 03/16/2015 16:06
Carbon disulfide ND ug/Kg 15.04 03/16/2015 16:06
Carbon tetrachloride ND ug/Kg 15.04 03/16/2015 16:06
Chlorobenzene ND ug/Kg 15.04 03/16/2015 16:06
Chloroethane ND ug/Kg 15.04 03/16/2015 16:06
Chloroform ND ug/Kg 15.04 03/16/2015 16:06
Chloromethane ND ug/Kg 15.04 03/16/2015 16:06
Dibromochloromethane ND ug/Kg 15.04 03/16/2015 16:06
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 17 of 77
Client Sample ID: CR-3 Soil
Client Project ID: HeatCraft
Lab Sample ID: 31500427006-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:00
Received Date: 03/11/2015 15:20
Matrix: Soil-Solid as dry weight
Solids (%): 78.30
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-3 Soil
Date Analyzed
Dibromomethane ND ug/Kg 15.04 03/16/2015 16:06
Dichlorodifluoromethane ND ug/Kg 15.04 03/16/2015 16:06
cis-1,3-Dichloropropene ND ug/Kg 15.04 03/16/2015 16:06
trans-1,3-Dichloropropene ND ug/Kg 15.04 03/16/2015 16:06
Diisopropyl Ether ND ug/Kg 15.04 03/16/2015 16:06
Ethyl Benzene ND ug/Kg 15.04 03/16/2015 16:06
Hexachlorobutadiene ND ug/Kg 15.04 03/16/2015 16:06
Isopropylbenzene (Cumene) ND ug/Kg 15.04 03/16/2015 16:06
Methyl iodide ND ug/Kg 15.04 03/16/2015 16:06
Methylene chloride ND ug/Kg 120.2 03/16/2015 16:06
Naphthalene ND ug/Kg 15.04 03/16/2015 16:06
Styrene ND ug/Kg 15.04 03/16/2015 16:06
Tetrachloroethene ND ug/Kg 15.04 03/16/2015 16:06
Toluene ND ug/Kg 15.04 03/16/2015 16:06
Trichloroethene ND ug/Kg 15.04 03/16/2015 16:06
Trichlorofluoromethane ND ug/Kg 15.04 03/16/2015 16:06
Vinyl chloride ND ug/Kg 15.04 03/16/2015 16:06
Xylene (total)ND ug/Kg 110.1 03/16/2015 16:06
cis-1,2-Dichloroethene ND ug/Kg 15.04 03/16/2015 16:06
m,p-Xylene ND ug/Kg 110.1 03/16/2015 16:06
n-Propylbenzene ND ug/Kg 15.04 03/16/2015 16:06
o-Xylene ND ug/Kg 15.04 03/16/2015 16:06
sec-Butylbenzene ND ug/Kg 15.04 03/16/2015 16:06
tert-Butyl methyl ether (MTBE) ND ug/Kg 15.04 03/16/2015 16:06
tert-Butylbenzene ND ug/Kg 15.04 03/16/2015 16:06
trans-1,2-Dichloroethene ND ug/Kg 15.04 03/16/2015 16:06
trans-1,4-Dichloro-2-butene ND ug/Kg 125.2 03/16/2015 16:06
Surrogates
1,2-Dichloroethane-d4 118 % 155.0-173 03/16/2015 16:06
4-Bromofluorobenzene 102 % 123.0-141 03/16/2015 16:06
Toluene d8 106 % 157.0-134 03/16/2015 16:06
Batch Information
Prep Batch: VXX5589
Prep Method: SW-846 5030B SL
Prep Date/Time: 03/17/2015 11:33
Prep Initial Wt./Vol.: 6.33 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3553
Analytical Method: SW-846 8260B
Instrument: MSD2
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 18 of 77
Client Sample ID: CR-2 Water
Client Project ID: HeatCraft
Lab Sample ID: 31500427007-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:20
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-2 Water
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 12:42
1,1,1-Trichloroethane ND ug/L 11.00 03/13/2015 12:42
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 12:42
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 12:42
1,1-Dichloroethane 2.29 ug/L 11.00 03/13/2015 12:42
1,1-Dichloroethene 1.74 ug/L 11.00 03/13/2015 12:42
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 12:42
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 12:42
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 12:42
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 12:42
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 12:42
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 12:42
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 12:42
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 12:42
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 12:42
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 12:42
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 12:42
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 12:42
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 12:42
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 12:42
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 12:42
2-Butanone ND ug/L 125.0 03/13/2015 12:42
2-Chlorotoluene ND ug/L 11.00 03/13/2015 12:42
2-Hexanone ND ug/L 15.00 03/13/2015 12:42
4-Chlorotoluene ND ug/L 11.00 03/13/2015 12:42
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 12:42
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 12:42
Acetone ND ug/L 125.0 03/13/2015 12:42
Benzene ND ug/L 11.00 03/13/2015 12:42
Bromobenzene ND ug/L 11.00 03/13/2015 12:42
Bromochloromethane ND ug/L 11.00 03/13/2015 12:42
Bromodichloromethane ND ug/L 11.00 03/13/2015 12:42
Bromoform ND ug/L 11.00 03/13/2015 12:42
Bromomethane ND ug/L 11.00 03/13/2015 12:42
n-Butylbenzene ND ug/L 11.00 03/13/2015 12:42
Carbon disulfide ND ug/L 11.00 03/13/2015 12:42
Carbon tetrachloride ND ug/L 11.00 03/13/2015 12:42
Chlorobenzene ND ug/L 11.00 03/13/2015 12:42
Chloroethane ND ug/L 11.00 03/13/2015 12:42
Chloroform ND ug/L 11.00 03/13/2015 12:42
Chloromethane ND ug/L 11.00 03/13/2015 12:42
Dibromochloromethane ND ug/L 11.00 03/13/2015 12:42
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 19 of 77
Client Sample ID: CR-2 Water
Client Project ID: HeatCraft
Lab Sample ID: 31500427007-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:20
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-2 Water
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 12:42
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 12:42
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 12:42
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 12:42
Diisopropyl Ether ND ug/L 11.00 03/13/2015 12:42
Ethyl Benzene ND ug/L 11.00 03/13/2015 12:42
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 12:42
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 12:42
Methyl iodide ND ug/L 11.00 03/13/2015 12:42
Methylene chloride ND ug/L 15.00 03/13/2015 12:42
Naphthalene ND ug/L 11.00 03/13/2015 12:42
Styrene ND ug/L 11.00 03/13/2015 12:42
Tetrachloroethene ND ug/L 11.00 03/13/2015 12:42
Toluene ND ug/L 11.00 03/13/2015 12:42
Trichloroethene 14.7 ug/L 11.00 03/13/2015 12:42
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 12:42
Vinyl chloride 20.1 ug/L 11.00 03/13/2015 12:42
Xylene (total)ND ug/L 12.00 03/13/2015 12:42
cis-1,2-Dichloroethene 46.1 ug/L 11.00 03/13/2015 12:42
m,p-Xylene ND ug/L 12.00 03/13/2015 12:42
n-Propylbenzene ND ug/L 11.00 03/13/2015 12:42
o-Xylene ND ug/L 11.00 03/13/2015 12:42
sec-Butylbenzene ND ug/L 11.00 03/13/2015 12:42
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 12:42
tert-Butylbenzene ND ug/L 11.00 03/13/2015 12:42
trans-1,2-Dichloroethene ND ug/L 11.00 03/13/2015 12:42
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 12:42
Surrogates
1,2-Dichloroethane-d4 103 % 164.0-140 03/13/2015 12:42
4-Bromofluorobenzene 95.0 % 185.0-115 03/13/2015 12:42
Toluene d8 91.0 % 182.0-117 03/13/2015 12:42
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 20 of 77
Client Sample ID: CR-2 Water
Client Project ID: HeatCraft
Lab Sample ID: 31500427007-D
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:20
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of CR-2 Water
Date Analyzed
1,4 Dioxane 2.43 ug/L 12.13 03/17/2015 14:57
Surrogates
Nitrobenzene-d5 71.9 % 150.0-150 03/17/2015 14:57
Batch Information
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Prep Initial Wt./Vol.: 939 mL
Prep Extract Vol: 1 mL
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 21 of 77
Client Sample ID: CR-2 Soil
Client Project ID: HeatCraft
Lab Sample ID: 31500427008-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:20
Received Date: 03/11/2015 15:20
Matrix: Soil-Solid as dry weight
Solids (%): 74.40
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-2 Soil
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 15.52 03/16/2015 16:33
1,1,1-Trichloroethane ND ug/Kg 15.52 03/16/2015 16:33
1,1,2,2-Tetrachloroethane ND ug/Kg 15.52 03/16/2015 16:33
1,1,2-Trichloroethane ND ug/Kg 15.52 03/16/2015 16:33
1,1-Dichloroethane ND ug/Kg 15.52 03/16/2015 16:33
1,1-Dichloroethene ND ug/Kg 15.52 03/16/2015 16:33
1,1-Dichloropropene ND ug/Kg 15.52 03/16/2015 16:33
1,2,3-Trichlorobenzene ND ug/Kg 15.52 03/16/2015 16:33
1,2,3-Trichloropropane ND ug/Kg 15.52 03/16/2015 16:33
1,2,4-Trichlorobenzene ND ug/Kg 15.52 03/16/2015 16:33
1,2,4-Trimethylbenzene ND ug/Kg 15.52 03/16/2015 16:33
1,2-Dibromo-3-chloropropane ND ug/Kg 133.1 03/16/2015 16:33
1,2-Dibromoethane ND ug/Kg 15.52 03/16/2015 16:33
1,2-Dichlorobenzene ND ug/Kg 15.52 03/16/2015 16:33
1,2-Dichloroethane ND ug/Kg 15.52 03/16/2015 16:33
1,2-Dichloropropane ND ug/Kg 15.52 03/16/2015 16:33
1,3,5-Trimethylbenzene ND ug/Kg 15.52 03/16/2015 16:33
1,3-Dichlorobenzene ND ug/Kg 15.52 03/16/2015 16:33
1,3-Dichloropropane ND ug/Kg 15.52 03/16/2015 16:33
1,4-Dichlorobenzene ND ug/Kg 15.52 03/16/2015 16:33
2,2-Dichloropropane ND ug/Kg 15.52 03/16/2015 16:33
2-Butanone ND ug/Kg 127.6 03/16/2015 16:33
2-Chlorotoluene ND ug/Kg 15.52 03/16/2015 16:33
2-Hexanone ND ug/Kg 113.8 03/16/2015 16:33
4-Chlorotoluene ND ug/Kg 15.52 03/16/2015 16:33
4-Isopropyltoluene ND ug/Kg 15.52 03/16/2015 16:33
4-Methyl-2-pentanone ND ug/Kg 113.8 03/16/2015 16:33
Acetone ND ug/Kg 155.2 03/16/2015 16:33
Benzene ND ug/Kg 15.52 03/16/2015 16:33
Bromobenzene ND ug/Kg 15.52 03/16/2015 16:33
Bromochloromethane ND ug/Kg 15.52 03/16/2015 16:33
Bromodichloromethane ND ug/Kg 15.52 03/16/2015 16:33
Bromoform ND ug/Kg 15.52 03/16/2015 16:33
Bromomethane ND ug/Kg 15.52 03/16/2015 16:33
n-Butylbenzene ND ug/Kg 15.52 03/16/2015 16:33
Carbon disulfide ND ug/Kg 15.52 03/16/2015 16:33
Carbon tetrachloride ND ug/Kg 15.52 03/16/2015 16:33
Chlorobenzene ND ug/Kg 15.52 03/16/2015 16:33
Chloroethane ND ug/Kg 15.52 03/16/2015 16:33
Chloroform ND ug/Kg 15.52 03/16/2015 16:33
Chloromethane ND ug/Kg 15.52 03/16/2015 16:33
Dibromochloromethane ND ug/Kg 15.52 03/16/2015 16:33
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 22 of 77
Client Sample ID: CR-2 Soil
Client Project ID: HeatCraft
Lab Sample ID: 31500427008-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:20
Received Date: 03/11/2015 15:20
Matrix: Soil-Solid as dry weight
Solids (%): 74.40
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-2 Soil
Date Analyzed
Dibromomethane ND ug/Kg 15.52 03/16/2015 16:33
Dichlorodifluoromethane ND ug/Kg 15.52 03/16/2015 16:33
cis-1,3-Dichloropropene ND ug/Kg 15.52 03/16/2015 16:33
trans-1,3-Dichloropropene ND ug/Kg 15.52 03/16/2015 16:33
Diisopropyl Ether ND ug/Kg 15.52 03/16/2015 16:33
Ethyl Benzene ND ug/Kg 15.52 03/16/2015 16:33
Hexachlorobutadiene ND ug/Kg 15.52 03/16/2015 16:33
Isopropylbenzene (Cumene) ND ug/Kg 15.52 03/16/2015 16:33
Methyl iodide ND ug/Kg 15.52 03/16/2015 16:33
Methylene chloride ND ug/Kg 122.1 03/16/2015 16:33
Naphthalene ND ug/Kg 15.52 03/16/2015 16:33
Styrene ND ug/Kg 15.52 03/16/2015 16:33
Tetrachloroethene ND ug/Kg 15.52 03/16/2015 16:33
Toluene ND ug/Kg 15.52 03/16/2015 16:33
Trichloroethene ND ug/Kg 15.52 03/16/2015 16:33
Trichlorofluoromethane ND ug/Kg 15.52 03/16/2015 16:33
Vinyl chloride ND ug/Kg 15.52 03/16/2015 16:33
Xylene (total)ND ug/Kg 111.0 03/16/2015 16:33
cis-1,2-Dichloroethene ND ug/Kg 15.52 03/16/2015 16:33
m,p-Xylene ND ug/Kg 111.0 03/16/2015 16:33
n-Propylbenzene ND ug/Kg 15.52 03/16/2015 16:33
o-Xylene ND ug/Kg 15.52 03/16/2015 16:33
sec-Butylbenzene ND ug/Kg 15.52 03/16/2015 16:33
tert-Butyl methyl ether (MTBE) ND ug/Kg 15.52 03/16/2015 16:33
tert-Butylbenzene ND ug/Kg 15.52 03/16/2015 16:33
trans-1,2-Dichloroethene ND ug/Kg 15.52 03/16/2015 16:33
trans-1,4-Dichloro-2-butene ND ug/Kg 127.6 03/16/2015 16:33
Surrogates
1,2-Dichloroethane-d4 120 % 155.0-173 03/16/2015 16:33
4-Bromofluorobenzene 103 % 123.0-141 03/16/2015 16:33
Toluene d8 105 % 157.0-134 03/16/2015 16:33
Batch Information
Prep Batch: VXX5589
Prep Method: SW-846 5030B SL
Prep Date/Time: 03/17/2015 11:33
Prep Initial Wt./Vol.: 6.09 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3553
Analytical Method: SW-846 8260B
Instrument: MSD2
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 23 of 77
Client Sample ID: CR-1 Water
Client Project ID: HeatCraft
Lab Sample ID: 31500427009-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:30
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-1 Water
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 13:06
1,1,1-Trichloroethane ND ug/L 11.00 03/13/2015 13:06
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/13/2015 13:06
1,1,2-Trichloroethane ND ug/L 11.00 03/13/2015 13:06
1,1-Dichloroethane 2.65 ug/L 11.00 03/13/2015 13:06
1,1-Dichloroethene 2.16 ug/L 11.00 03/13/2015 13:06
1,1-Dichloropropene ND ug/L 11.00 03/13/2015 13:06
1,2,3-Trichlorobenzene ND ug/L 11.00 03/13/2015 13:06
1,2,3-Trichloropropane ND ug/L 11.00 03/13/2015 13:06
1,2,4-Trichlorobenzene ND ug/L 11.00 03/13/2015 13:06
1,2,4-Trimethylbenzene ND ug/L 11.00 03/13/2015 13:06
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/13/2015 13:06
1,2-Dibromoethane ND ug/L 11.00 03/13/2015 13:06
1,2-Dichlorobenzene ND ug/L 11.00 03/13/2015 13:06
1,2-Dichloroethane ND ug/L 11.00 03/13/2015 13:06
1,2-Dichloropropane ND ug/L 11.00 03/13/2015 13:06
1,3,5-Trimethylbenzene ND ug/L 11.00 03/13/2015 13:06
1,3-Dichlorobenzene ND ug/L 11.00 03/13/2015 13:06
1,3-Dichloropropane ND ug/L 11.00 03/13/2015 13:06
1,4-Dichlorobenzene ND ug/L 11.00 03/13/2015 13:06
2,2-Dichloropropane ND ug/L 11.00 03/13/2015 13:06
2-Butanone ND ug/L 125.0 03/13/2015 13:06
2-Chlorotoluene ND ug/L 11.00 03/13/2015 13:06
2-Hexanone ND ug/L 15.00 03/13/2015 13:06
4-Chlorotoluene ND ug/L 11.00 03/13/2015 13:06
4-Isopropyltoluene ND ug/L 11.00 03/13/2015 13:06
4-Methyl-2-pentanone ND ug/L 15.00 03/13/2015 13:06
Acetone ND ug/L 125.0 03/13/2015 13:06
Benzene ND ug/L 11.00 03/13/2015 13:06
Bromobenzene ND ug/L 11.00 03/13/2015 13:06
Bromochloromethane ND ug/L 11.00 03/13/2015 13:06
Bromodichloromethane ND ug/L 11.00 03/13/2015 13:06
Bromoform ND ug/L 11.00 03/13/2015 13:06
Bromomethane ND ug/L 11.00 03/13/2015 13:06
n-Butylbenzene ND ug/L 11.00 03/13/2015 13:06
Carbon disulfide ND ug/L 11.00 03/13/2015 13:06
Carbon tetrachloride ND ug/L 11.00 03/13/2015 13:06
Chlorobenzene ND ug/L 11.00 03/13/2015 13:06
Chloroethane ND ug/L 11.00 03/13/2015 13:06
Chloroform ND ug/L 11.00 03/13/2015 13:06
Chloromethane ND ug/L 11.00 03/13/2015 13:06
Dibromochloromethane ND ug/L 11.00 03/13/2015 13:06
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 24 of 77
Client Sample ID: CR-1 Water
Client Project ID: HeatCraft
Lab Sample ID: 31500427009-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:30
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-1 Water
Date Analyzed
Dibromomethane ND ug/L 11.00 03/13/2015 13:06
Dichlorodifluoromethane ND ug/L 15.00 03/13/2015 13:06
cis-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 13:06
trans-1,3-Dichloropropene ND ug/L 11.00 03/13/2015 13:06
Diisopropyl Ether ND ug/L 11.00 03/13/2015 13:06
Ethyl Benzene ND ug/L 11.00 03/13/2015 13:06
Hexachlorobutadiene ND ug/L 11.00 03/13/2015 13:06
Isopropylbenzene (Cumene) ND ug/L 11.00 03/13/2015 13:06
Methyl iodide ND ug/L 11.00 03/13/2015 13:06
Methylene chloride ND ug/L 15.00 03/13/2015 13:06
Naphthalene ND ug/L 11.00 03/13/2015 13:06
Styrene ND ug/L 11.00 03/13/2015 13:06
Tetrachloroethene ND ug/L 11.00 03/13/2015 13:06
Toluene ND ug/L 11.00 03/13/2015 13:06
Trichloroethene 16.8 ug/L 11.00 03/13/2015 13:06
Trichlorofluoromethane ND ug/L 11.00 03/13/2015 13:06
Vinyl chloride 17.3 ug/L 11.00 03/13/2015 13:06
Xylene (total)ND ug/L 12.00 03/13/2015 13:06
cis-1,2-Dichloroethene 54.9 ug/L 11.00 03/13/2015 13:06
m,p-Xylene ND ug/L 12.00 03/13/2015 13:06
n-Propylbenzene ND ug/L 11.00 03/13/2015 13:06
o-Xylene ND ug/L 11.00 03/13/2015 13:06
sec-Butylbenzene ND ug/L 11.00 03/13/2015 13:06
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/13/2015 13:06
tert-Butylbenzene ND ug/L 11.00 03/13/2015 13:06
trans-1,2-Dichloroethene ND ug/L 11.00 03/13/2015 13:06
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/13/2015 13:06
Surrogates
1,2-Dichloroethane-d4 102 % 164.0-140 03/13/2015 13:06
4-Bromofluorobenzene 95.0 % 185.0-115 03/13/2015 13:06
Toluene d8 90.0 % 182.0-117 03/13/2015 13:06
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 11:32
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 25 of 77
Client Sample ID: CR-1 Soil
Client Project ID: HeatCraft
Lab Sample ID: 31500427010-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:30
Received Date: 03/11/2015 15:20
Matrix: Soil-Solid as dry weight
Solids (%): 82.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-1 Soil
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 15.82 03/16/2015 16:59
1,1,1-Trichloroethane ND ug/Kg 15.82 03/16/2015 16:59
1,1,2,2-Tetrachloroethane ND ug/Kg 15.82 03/16/2015 16:59
1,1,2-Trichloroethane ND ug/Kg 15.82 03/16/2015 16:59
1,1-Dichloroethane ND ug/Kg 15.82 03/16/2015 16:59
1,1-Dichloroethene ND ug/Kg 15.82 03/16/2015 16:59
1,1-Dichloropropene ND ug/Kg 15.82 03/16/2015 16:59
1,2,3-Trichlorobenzene ND ug/Kg 15.82 03/16/2015 16:59
1,2,3-Trichloropropane ND ug/Kg 15.82 03/16/2015 16:59
1,2,4-Trichlorobenzene ND ug/Kg 15.82 03/16/2015 16:59
1,2,4-Trimethylbenzene ND ug/Kg 15.82 03/16/2015 16:59
1,2-Dibromo-3-chloropropane ND ug/Kg 134.9 03/16/2015 16:59
1,2-Dibromoethane ND ug/Kg 15.82 03/16/2015 16:59
1,2-Dichlorobenzene ND ug/Kg 15.82 03/16/2015 16:59
1,2-Dichloroethane ND ug/Kg 15.82 03/16/2015 16:59
1,2-Dichloropropane ND ug/Kg 15.82 03/16/2015 16:59
1,3,5-Trimethylbenzene ND ug/Kg 15.82 03/16/2015 16:59
1,3-Dichlorobenzene ND ug/Kg 15.82 03/16/2015 16:59
1,3-Dichloropropane ND ug/Kg 15.82 03/16/2015 16:59
1,4-Dichlorobenzene ND ug/Kg 15.82 03/16/2015 16:59
2,2-Dichloropropane ND ug/Kg 15.82 03/16/2015 16:59
2-Butanone ND ug/Kg 129.1 03/16/2015 16:59
2-Chlorotoluene ND ug/Kg 15.82 03/16/2015 16:59
2-Hexanone ND ug/Kg 114.6 03/16/2015 16:59
4-Chlorotoluene ND ug/Kg 15.82 03/16/2015 16:59
4-Isopropyltoluene ND ug/Kg 15.82 03/16/2015 16:59
4-Methyl-2-pentanone ND ug/Kg 114.6 03/16/2015 16:59
Acetone ND ug/Kg 158.2 03/16/2015 16:59
Benzene ND ug/Kg 15.82 03/16/2015 16:59
Bromobenzene ND ug/Kg 15.82 03/16/2015 16:59
Bromochloromethane ND ug/Kg 15.82 03/16/2015 16:59
Bromodichloromethane ND ug/Kg 15.82 03/16/2015 16:59
Bromoform ND ug/Kg 15.82 03/16/2015 16:59
Bromomethane ND ug/Kg 15.82 03/16/2015 16:59
n-Butylbenzene ND ug/Kg 15.82 03/16/2015 16:59
Carbon disulfide ND ug/Kg 15.82 03/16/2015 16:59
Carbon tetrachloride ND ug/Kg 15.82 03/16/2015 16:59
Chlorobenzene ND ug/Kg 15.82 03/16/2015 16:59
Chloroethane ND ug/Kg 15.82 03/16/2015 16:59
Chloroform ND ug/Kg 15.82 03/16/2015 16:59
Chloromethane ND ug/Kg 15.82 03/16/2015 16:59
Dibromochloromethane ND ug/Kg 15.82 03/16/2015 16:59
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 26 of 77
Client Sample ID: CR-1 Soil
Client Project ID: HeatCraft
Lab Sample ID: 31500427010-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 11:30
Received Date: 03/11/2015 15:20
Matrix: Soil-Solid as dry weight
Solids (%): 82.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of CR-1 Soil
Date Analyzed
Dibromomethane ND ug/Kg 15.82 03/16/2015 16:59
Dichlorodifluoromethane ND ug/Kg 15.82 03/16/2015 16:59
cis-1,3-Dichloropropene ND ug/Kg 15.82 03/16/2015 16:59
trans-1,3-Dichloropropene ND ug/Kg 15.82 03/16/2015 16:59
Diisopropyl Ether ND ug/Kg 15.82 03/16/2015 16:59
Ethyl Benzene ND ug/Kg 15.82 03/16/2015 16:59
Hexachlorobutadiene ND ug/Kg 15.82 03/16/2015 16:59
Isopropylbenzene (Cumene) ND ug/Kg 15.82 03/16/2015 16:59
Methyl iodide ND ug/Kg 15.82 03/16/2015 16:59
Methylene chloride ND ug/Kg 123.3 03/16/2015 16:59
Naphthalene ND ug/Kg 15.82 03/16/2015 16:59
Styrene ND ug/Kg 15.82 03/16/2015 16:59
Tetrachloroethene ND ug/Kg 15.82 03/16/2015 16:59
Toluene ND ug/Kg 15.82 03/16/2015 16:59
Trichloroethene ND ug/Kg 15.82 03/16/2015 16:59
Trichlorofluoromethane ND ug/Kg 15.82 03/16/2015 16:59
Vinyl chloride ND ug/Kg 15.82 03/16/2015 16:59
Xylene (total)ND ug/Kg 111.6 03/16/2015 16:59
cis-1,2-Dichloroethene ND ug/Kg 15.82 03/16/2015 16:59
m,p-Xylene ND ug/Kg 111.6 03/16/2015 16:59
n-Propylbenzene ND ug/Kg 15.82 03/16/2015 16:59
o-Xylene ND ug/Kg 15.82 03/16/2015 16:59
sec-Butylbenzene ND ug/Kg 15.82 03/16/2015 16:59
tert-Butyl methyl ether (MTBE) ND ug/Kg 15.82 03/16/2015 16:59
tert-Butylbenzene ND ug/Kg 15.82 03/16/2015 16:59
trans-1,2-Dichloroethene ND ug/Kg 15.82 03/16/2015 16:59
trans-1,4-Dichloro-2-butene ND ug/Kg 129.1 03/16/2015 16:59
Surrogates
1,2-Dichloroethane-d4 118 % 155.0-173 03/16/2015 16:59
4-Bromofluorobenzene 101 % 123.0-141 03/16/2015 16:59
Toluene d8 108 % 157.0-134 03/16/2015 16:59
Batch Information
Prep Batch: VXX5589
Prep Method: SW-846 5030B SL
Prep Date/Time: 03/17/2015 11:33
Prep Initial Wt./Vol.: 5.19 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3553
Analytical Method: SW-846 8260B
Instrument: MSD2
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 27 of 77
Client Sample ID: MW-2A
Client Project ID: HeatCraft
Lab Sample ID: 31500427011-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:30
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of MW-2A
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/17/2015 20:53
1,1,1-Trichloroethane ND ug/L 11.00 03/17/2015 20:53
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/17/2015 20:53
1,1,2-Trichloroethane ND ug/L 11.00 03/17/2015 20:53
1,1-Dichloroethane 92.4 ug/L 55.00 03/13/2015 13:56
1,1-Dichloroethene 93.6 ug/L 55.00 03/13/2015 13:56
1,1-Dichloropropene ND ug/L 11.00 03/17/2015 20:53
1,2,3-Trichlorobenzene ND ug/L 11.00 03/17/2015 20:53
1,2,3-Trichloropropane ND ug/L 11.00 03/17/2015 20:53
1,2,4-Trichlorobenzene ND ug/L 11.00 03/17/2015 20:53
1,2,4-Trimethylbenzene ND ug/L 11.00 03/17/2015 20:53
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/17/2015 20:53
1,2-Dibromoethane ND ug/L 11.00 03/17/2015 20:53
1,2-Dichlorobenzene ND ug/L 11.00 03/17/2015 20:53
1,2-Dichloroethane ND ug/L 11.00 03/17/2015 20:53
1,2-Dichloropropane ND ug/L 11.00 03/17/2015 20:53
1,3,5-Trimethylbenzene ND ug/L 11.00 03/17/2015 20:53
1,3-Dichlorobenzene ND ug/L 11.00 03/17/2015 20:53
1,3-Dichloropropane ND ug/L 11.00 03/17/2015 20:53
1,4-Dichlorobenzene ND ug/L 11.00 03/17/2015 20:53
2,2-Dichloropropane ND ug/L 11.00 03/17/2015 20:53
2-Butanone ND ug/L 125.0 03/17/2015 20:53
2-Chlorotoluene ND ug/L 11.00 03/17/2015 20:53
2-Hexanone ND ug/L 15.00 03/17/2015 20:53
4-Chlorotoluene ND ug/L 11.00 03/17/2015 20:53
4-Isopropyltoluene ND ug/L 11.00 03/17/2015 20:53
4-Methyl-2-pentanone ND ug/L 15.00 03/17/2015 20:53
Acetone ND ug/L 125.0 03/17/2015 20:53
Benzene ND ug/L 11.00 03/17/2015 20:53
Bromobenzene ND ug/L 11.00 03/17/2015 20:53
Bromochloromethane ND ug/L 11.00 03/17/2015 20:53
Bromodichloromethane ND ug/L 11.00 03/17/2015 20:53
Bromoform ND ug/L 11.00 03/17/2015 20:53
Bromomethane ND ug/L 11.00 03/17/2015 20:53
n-Butylbenzene ND ug/L 11.00 03/17/2015 20:53
Carbon disulfide ND ug/L 11.00 03/17/2015 20:53
Carbon tetrachloride ND ug/L 11.00 03/17/2015 20:53
Chlorobenzene ND ug/L 11.00 03/17/2015 20:53
Chloroethane 1.06 ug/L 11.00 03/17/2015 20:53
Chloroform ND ug/L 11.00 03/17/2015 20:53
Chloromethane ND ug/L 11.00 03/17/2015 20:53
Dibromochloromethane ND ug/L 11.00 03/17/2015 20:53
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 28 of 77
Client Sample ID: MW-2A
Client Project ID: HeatCraft
Lab Sample ID: 31500427011-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:30
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of MW-2A
Date Analyzed
Dibromomethane ND ug/L 11.00 03/17/2015 20:53
Dichlorodifluoromethane ND ug/L 15.00 03/17/2015 20:53
cis-1,3-Dichloropropene ND ug/L 11.00 03/17/2015 20:53
trans-1,3-Dichloropropene ND ug/L 11.00 03/17/2015 20:53
Diisopropyl Ether ND ug/L 11.00 03/17/2015 20:53
Ethyl Benzene ND ug/L 11.00 03/17/2015 20:53
Hexachlorobutadiene ND ug/L 11.00 03/17/2015 20:53
Isopropylbenzene (Cumene) ND ug/L 11.00 03/17/2015 20:53
Methyl iodide ND ug/L 11.00 03/17/2015 20:53
Methylene chloride ND ug/L 15.00 03/17/2015 20:53
Naphthalene ND ug/L 11.00 03/17/2015 20:53
Styrene ND ug/L 11.00 03/17/2015 20:53
Tetrachloroethene ND ug/L 11.00 03/17/2015 20:53
Toluene ND ug/L 11.00 03/17/2015 20:53
Trichloroethene ND ug/L 11.00 03/17/2015 20:53
Trichlorofluoromethane ND ug/L 11.00 03/17/2015 20:53
Vinyl chloride ND ug/L 11.00 03/17/2015 20:53
Xylene (total)ND ug/L 12.00 03/17/2015 20:53
cis-1,2-Dichloroethene 98.8 ug/L 55.00 03/13/2015 13:56
m,p-Xylene ND ug/L 12.00 03/17/2015 20:53
n-Propylbenzene ND ug/L 11.00 03/17/2015 20:53
o-Xylene ND ug/L 11.00 03/17/2015 20:53
sec-Butylbenzene ND ug/L 11.00 03/17/2015 20:53
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/17/2015 20:53
tert-Butylbenzene ND ug/L 11.00 03/17/2015 20:53
trans-1,2-Dichloroethene ND ug/L 11.00 03/17/2015 20:53
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/17/2015 20:53
Surrogates
1,2-Dichloroethane-d4 106 % 164.0-140 03/17/2015 20:53
4-Bromofluorobenzene 95.0 % 185.0-115 03/17/2015 20:53
Toluene d8 90.0 % 182.0-117 03/17/2015 20:53
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 29 of 77
Client Sample ID: MW-2A
Client Project ID: HeatCraft
Lab Sample ID: 31500427011-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:30
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of MW-2A
Date Analyzed
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:12
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5590
Prep Method: SW-846 5030B
Prep Date/Time: 03/17/2015 13:37
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3554
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 30 of 77
Client Sample ID: MW-2A
Client Project ID: HeatCraft
Lab Sample ID: 31500427011-D
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:30
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of MW-2A
Date Analyzed
1,4 Dioxane ND ug/L 12.07 03/17/2015 15:18
Surrogates
Nitrobenzene-d5 67.0 % 150.0-150 03/17/2015 15:18
Batch Information
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Prep Initial Wt./Vol.: 965 mL
Prep Extract Vol: 1 mL
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 31 of 77
Client Sample ID: MW-2A
Client Project ID: HeatCraft
Lab Sample ID: 31500427011-F
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:30
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by EPA 300.0
Results of MW-2A
Date Analyzed
Sulfate 3.82 mg/L 11.00 03/11/2015 15:28
Nitrate as N ND mg/L 10.300 03/11/2015 15:28
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 15:28
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 32 of 77
Client Sample ID: MW-2B
Client Project ID: HeatCraft
Lab Sample ID: 31500427012-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:35
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of MW-2B
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/17/2015 20:28
1,1,1-Trichloroethane ND ug/L 11.00 03/17/2015 20:28
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/17/2015 20:28
1,1,2-Trichloroethane ND ug/L 11.00 03/17/2015 20:28
1,1-Dichloroethane 92.6 ug/L 44.00 03/13/2015 13:31
1,1-Dichloroethene 93.7 ug/L 44.00 03/13/2015 13:31
1,1-Dichloropropene ND ug/L 11.00 03/17/2015 20:28
1,2,3-Trichlorobenzene ND ug/L 11.00 03/17/2015 20:28
1,2,3-Trichloropropane ND ug/L 11.00 03/17/2015 20:28
1,2,4-Trichlorobenzene ND ug/L 11.00 03/17/2015 20:28
1,2,4-Trimethylbenzene ND ug/L 11.00 03/17/2015 20:28
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/17/2015 20:28
1,2-Dibromoethane ND ug/L 11.00 03/17/2015 20:28
1,2-Dichlorobenzene ND ug/L 11.00 03/17/2015 20:28
1,2-Dichloroethane ND ug/L 11.00 03/17/2015 20:28
1,2-Dichloropropane ND ug/L 11.00 03/17/2015 20:28
1,3,5-Trimethylbenzene ND ug/L 11.00 03/17/2015 20:28
1,3-Dichlorobenzene ND ug/L 11.00 03/17/2015 20:28
1,3-Dichloropropane ND ug/L 11.00 03/17/2015 20:28
1,4-Dichlorobenzene ND ug/L 11.00 03/17/2015 20:28
2,2-Dichloropropane ND ug/L 11.00 03/17/2015 20:28
2-Butanone ND ug/L 125.0 03/17/2015 20:28
2-Chlorotoluene ND ug/L 11.00 03/17/2015 20:28
2-Hexanone ND ug/L 15.00 03/17/2015 20:28
4-Chlorotoluene ND ug/L 11.00 03/17/2015 20:28
4-Isopropyltoluene ND ug/L 11.00 03/17/2015 20:28
4-Methyl-2-pentanone ND ug/L 15.00 03/17/2015 20:28
Acetone ND ug/L 125.0 03/17/2015 20:28
Benzene ND ug/L 11.00 03/17/2015 20:28
Bromobenzene ND ug/L 11.00 03/17/2015 20:28
Bromochloromethane ND ug/L 11.00 03/17/2015 20:28
Bromodichloromethane ND ug/L 11.00 03/17/2015 20:28
Bromoform ND ug/L 11.00 03/17/2015 20:28
Bromomethane ND ug/L 11.00 03/17/2015 20:28
n-Butylbenzene ND ug/L 11.00 03/17/2015 20:28
Carbon disulfide ND ug/L 11.00 03/17/2015 20:28
Carbon tetrachloride ND ug/L 11.00 03/17/2015 20:28
Chlorobenzene ND ug/L 11.00 03/17/2015 20:28
Chloroethane 1.04 ug/L 11.00 03/17/2015 20:28
Chloroform ND ug/L 11.00 03/17/2015 20:28
Chloromethane ND ug/L 11.00 03/17/2015 20:28
Dibromochloromethane ND ug/L 11.00 03/17/2015 20:28
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 33 of 77
Client Sample ID: MW-2B
Client Project ID: HeatCraft
Lab Sample ID: 31500427012-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:35
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of MW-2B
Date Analyzed
Dibromomethane ND ug/L 11.00 03/17/2015 20:28
Dichlorodifluoromethane ND ug/L 15.00 03/17/2015 20:28
cis-1,3-Dichloropropene ND ug/L 11.00 03/17/2015 20:28
trans-1,3-Dichloropropene ND ug/L 11.00 03/17/2015 20:28
Diisopropyl Ether ND ug/L 11.00 03/17/2015 20:28
Ethyl Benzene ND ug/L 11.00 03/17/2015 20:28
Hexachlorobutadiene ND ug/L 11.00 03/17/2015 20:28
Isopropylbenzene (Cumene) ND ug/L 11.00 03/17/2015 20:28
Methyl iodide ND ug/L 11.00 03/17/2015 20:28
Methylene chloride ND ug/L 15.00 03/17/2015 20:28
Naphthalene ND ug/L 11.00 03/17/2015 20:28
Styrene ND ug/L 11.00 03/17/2015 20:28
Tetrachloroethene ND ug/L 11.00 03/17/2015 20:28
Toluene ND ug/L 11.00 03/17/2015 20:28
Trichloroethene ND ug/L 11.00 03/17/2015 20:28
Trichlorofluoromethane ND ug/L 11.00 03/17/2015 20:28
Vinyl chloride ND ug/L 11.00 03/17/2015 20:28
Xylene (total)ND ug/L 12.00 03/17/2015 20:28
cis-1,2-Dichloroethene 98.0 ug/L 44.00 03/13/2015 13:31
m,p-Xylene ND ug/L 12.00 03/17/2015 20:28
n-Propylbenzene ND ug/L 11.00 03/17/2015 20:28
o-Xylene ND ug/L 11.00 03/17/2015 20:28
sec-Butylbenzene ND ug/L 11.00 03/17/2015 20:28
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/17/2015 20:28
tert-Butylbenzene ND ug/L 11.00 03/17/2015 20:28
trans-1,2-Dichloroethene ND ug/L 11.00 03/17/2015 20:28
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/17/2015 20:28
Surrogates
1,2-Dichloroethane-d4 105 % 164.0-140 03/17/2015 20:28
4-Bromofluorobenzene 95.0 % 185.0-115 03/17/2015 20:28
Toluene d8 89.0 % 182.0-117 03/17/2015 20:28
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 34 of 77
Client Sample ID: MW-2B
Client Project ID: HeatCraft
Lab Sample ID: 31500427012-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:35
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of MW-2B
Date Analyzed
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:12
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5590
Prep Method: SW-846 5030B
Prep Date/Time: 03/17/2015 13:37
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3554
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 35 of 77
Client Sample ID: EW-6
Client Project ID: HeatCraft
Lab Sample ID: 31500427013-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:50
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of EW-6
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 11.00 03/17/2015 18:48
1,1,1-Trichloroethane 330 ug/L 2020.0 03/13/2015 14:21
1,1,2,2-Tetrachloroethane ND ug/L 11.00 03/17/2015 18:48
1,1,2-Trichloroethane ND ug/L 11.00 03/17/2015 18:48
1,1-Dichloroethane 60.6 ug/L 2020.0 03/13/2015 14:21
1,1-Dichloroethene 18.1 ug/L 11.00 03/17/2015 18:48
1,1-Dichloropropene ND ug/L 11.00 03/17/2015 18:48
1,2,3-Trichlorobenzene ND ug/L 11.00 03/17/2015 18:48
1,2,3-Trichloropropane ND ug/L 11.00 03/17/2015 18:48
1,2,4-Trichlorobenzene ND ug/L 11.00 03/17/2015 18:48
1,2,4-Trimethylbenzene ND ug/L 11.00 03/17/2015 18:48
1,2-Dibromo-3-chloropropane ND ug/L 15.00 03/17/2015 18:48
1,2-Dibromoethane ND ug/L 11.00 03/17/2015 18:48
1,2-Dichlorobenzene ND ug/L 11.00 03/17/2015 18:48
1,2-Dichloroethane ND ug/L 11.00 03/17/2015 18:48
1,2-Dichloropropane ND ug/L 11.00 03/17/2015 18:48
1,3,5-Trimethylbenzene ND ug/L 11.00 03/17/2015 18:48
1,3-Dichlorobenzene ND ug/L 11.00 03/17/2015 18:48
1,3-Dichloropropane ND ug/L 11.00 03/17/2015 18:48
1,4-Dichlorobenzene ND ug/L 11.00 03/17/2015 18:48
2,2-Dichloropropane ND ug/L 11.00 03/17/2015 18:48
2-Butanone ND ug/L 125.0 03/17/2015 18:48
2-Chlorotoluene ND ug/L 11.00 03/17/2015 18:48
2-Hexanone ND ug/L 15.00 03/17/2015 18:48
4-Chlorotoluene ND ug/L 11.00 03/17/2015 18:48
4-Isopropyltoluene ND ug/L 11.00 03/17/2015 18:48
4-Methyl-2-pentanone ND ug/L 15.00 03/17/2015 18:48
Acetone ND ug/L 125.0 03/17/2015 18:48
Benzene ND ug/L 11.00 03/17/2015 18:48
Bromobenzene ND ug/L 11.00 03/17/2015 18:48
Bromochloromethane ND ug/L 11.00 03/17/2015 18:48
Bromodichloromethane ND ug/L 11.00 03/17/2015 18:48
Bromoform ND ug/L 11.00 03/17/2015 18:48
Bromomethane ND ug/L 11.00 03/17/2015 18:48
n-Butylbenzene ND ug/L 11.00 03/17/2015 18:48
Carbon disulfide ND ug/L 11.00 03/17/2015 18:48
Carbon tetrachloride ND ug/L 11.00 03/17/2015 18:48
Chlorobenzene ND ug/L 11.00 03/17/2015 18:48
Chloroethane ND ug/L 11.00 03/17/2015 18:48
Chloroform ND ug/L 11.00 03/17/2015 18:48
Chloromethane ND ug/L 11.00 03/17/2015 18:48
Dibromochloromethane ND ug/L 11.00 03/17/2015 18:48
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 36 of 77
Client Sample ID: EW-6
Client Project ID: HeatCraft
Lab Sample ID: 31500427013-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:50
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of EW-6
Date Analyzed
Dibromomethane ND ug/L 11.00 03/17/2015 18:48
Dichlorodifluoromethane ND ug/L 15.00 03/17/2015 18:48
cis-1,3-Dichloropropene ND ug/L 11.00 03/17/2015 18:48
trans-1,3-Dichloropropene ND ug/L 11.00 03/17/2015 18:48
Diisopropyl Ether ND ug/L 11.00 03/17/2015 18:48
Ethyl Benzene ND ug/L 11.00 03/17/2015 18:48
Hexachlorobutadiene ND ug/L 11.00 03/17/2015 18:48
Isopropylbenzene (Cumene) ND ug/L 11.00 03/17/2015 18:48
Methyl iodide ND ug/L 11.00 03/17/2015 18:48
Methylene chloride ND ug/L 15.00 03/17/2015 18:48
Naphthalene ND ug/L 11.00 03/17/2015 18:48
Styrene ND ug/L 11.00 03/17/2015 18:48
Tetrachloroethene ND ug/L 11.00 03/17/2015 18:48
Toluene ND ug/L 11.00 03/17/2015 18:48
Trichloroethene 10.5 ug/L 11.00 03/17/2015 18:48
Trichlorofluoromethane ND ug/L 11.00 03/17/2015 18:48
Vinyl chloride 74.2 ug/L 2020.0 03/13/2015 14:21
Xylene (total)ND ug/L 12.00 03/17/2015 18:48
cis-1,2-Dichloroethene 321 ug/L 2020.0 03/13/2015 14:21
m,p-Xylene ND ug/L 12.00 03/17/2015 18:48
n-Propylbenzene ND ug/L 11.00 03/17/2015 18:48
o-Xylene ND ug/L 11.00 03/17/2015 18:48
sec-Butylbenzene ND ug/L 11.00 03/17/2015 18:48
tert-Butyl methyl ether (MTBE) ND ug/L 11.00 03/17/2015 18:48
tert-Butylbenzene ND ug/L 11.00 03/17/2015 18:48
trans-1,2-Dichloroethene 3.12 ug/L 11.00 03/17/2015 18:48
trans-1,4-Dichloro-2-butene ND ug/L 15.00 03/17/2015 18:48
Surrogates
1,2-Dichloroethane-d4 113 % 164.0-140 03/17/2015 18:48
4-Bromofluorobenzene 96.0 % 185.0-115 03/17/2015 18:48
Toluene d8 101 % 182.0-117 03/17/2015 18:48
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 37 of 77
Client Sample ID: EW-6
Client Project ID: HeatCraft
Lab Sample ID: 31500427013-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 13:50
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of EW-6
Date Analyzed
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:12
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5590
Prep Method: SW-846 5030B
Prep Date/Time: 03/17/2015 13:37
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3554
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 38 of 77
Client Sample ID: EW-4
Client Project ID: HeatCraft
Lab Sample ID: 31500427014-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 14:20
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of EW-4
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/L 88.00 03/17/2015 18:22
1,1,1-Trichloroethane 1500 ug/L 400400 03/13/2015 15:11
1,1,2,2-Tetrachloroethane ND ug/L 88.00 03/17/2015 18:22
1,1,2-Trichloroethane ND ug/L 88.00 03/17/2015 18:22
1,1-Dichloroethane 540 ug/L 88.00 03/17/2015 18:22
1,1-Dichloroethene 1520 ug/L 400400 03/13/2015 15:11
1,1-Dichloropropene ND ug/L 88.00 03/17/2015 18:22
1,2,3-Trichlorobenzene ND ug/L 88.00 03/17/2015 18:22
1,2,3-Trichloropropane ND ug/L 88.00 03/17/2015 18:22
1,2,4-Trichlorobenzene ND ug/L 88.00 03/17/2015 18:22
1,2,4-Trimethylbenzene ND ug/L 88.00 03/17/2015 18:22
1,2-Dibromo-3-chloropropane ND ug/L 840.0 03/17/2015 18:22
1,2-Dibromoethane ND ug/L 88.00 03/17/2015 18:22
1,2-Dichlorobenzene ND ug/L 88.00 03/17/2015 18:22
1,2-Dichloroethane ND ug/L 88.00 03/17/2015 18:22
1,2-Dichloropropane ND ug/L 88.00 03/17/2015 18:22
1,3,5-Trimethylbenzene ND ug/L 88.00 03/17/2015 18:22
1,3-Dichlorobenzene ND ug/L 88.00 03/17/2015 18:22
1,3-Dichloropropane ND ug/L 88.00 03/17/2015 18:22
1,4-Dichlorobenzene ND ug/L 88.00 03/17/2015 18:22
2,2-Dichloropropane ND ug/L 88.00 03/17/2015 18:22
2-Butanone ND ug/L 8200 03/17/2015 18:22
2-Chlorotoluene ND ug/L 88.00 03/17/2015 18:22
2-Hexanone ND ug/L 840.0 03/17/2015 18:22
4-Chlorotoluene ND ug/L 88.00 03/17/2015 18:22
4-Isopropyltoluene ND ug/L 88.00 03/17/2015 18:22
4-Methyl-2-pentanone ND ug/L 840.0 03/17/2015 18:22
Acetone ND ug/L 8200 03/17/2015 18:22
Benzene ND ug/L 88.00 03/17/2015 18:22
Bromobenzene ND ug/L 88.00 03/17/2015 18:22
Bromochloromethane ND ug/L 88.00 03/17/2015 18:22
Bromodichloromethane ND ug/L 88.00 03/17/2015 18:22
Bromoform ND ug/L 88.00 03/17/2015 18:22
Bromomethane ND ug/L 88.00 03/17/2015 18:22
n-Butylbenzene ND ug/L 88.00 03/17/2015 18:22
Carbon disulfide ND ug/L 88.00 03/17/2015 18:22
Carbon tetrachloride ND ug/L 88.00 03/17/2015 18:22
Chlorobenzene ND ug/L 88.00 03/17/2015 18:22
Chloroethane 10.2 ug/L 88.00 03/17/2015 18:22
Chloroform ND ug/L 88.00 03/17/2015 18:22
Chloromethane ND ug/L 88.00 03/17/2015 18:22
Dibromochloromethane ND ug/L 88.00 03/17/2015 18:22
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 39 of 77
Client Sample ID: EW-4
Client Project ID: HeatCraft
Lab Sample ID: 31500427014-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 14:20
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of EW-4
Date Analyzed
Dibromomethane ND ug/L 88.00 03/17/2015 18:22
Dichlorodifluoromethane ND ug/L 840.0 03/17/2015 18:22
cis-1,3-Dichloropropene ND ug/L 88.00 03/17/2015 18:22
trans-1,3-Dichloropropene ND ug/L 88.00 03/17/2015 18:22
Diisopropyl Ether ND ug/L 88.00 03/17/2015 18:22
Ethyl Benzene ND ug/L 88.00 03/17/2015 18:22
Hexachlorobutadiene ND ug/L 88.00 03/17/2015 18:22
Isopropylbenzene (Cumene) ND ug/L 88.00 03/17/2015 18:22
Methyl iodide ND ug/L 88.00 03/17/2015 18:22
Methylene chloride ND ug/L 840.0 03/17/2015 18:22
Naphthalene ND ug/L 88.00 03/17/2015 18:22
Styrene ND ug/L 88.00 03/17/2015 18:22
Tetrachloroethene ND ug/L 88.00 03/17/2015 18:22
Toluene 8.72 ug/L 88.00 03/17/2015 18:22
Trichloroethene 541 ug/L 88.00 03/17/2015 18:22
Trichlorofluoromethane ND ug/L 88.00 03/17/2015 18:22
Vinyl chloride 333 ug/L 88.00 03/17/2015 18:22
Xylene (total)ND ug/L 816.0 03/17/2015 18:22
cis-1,2-Dichloroethene 8780 ug/L 400400 03/13/2015 15:11
m,p-Xylene ND ug/L 816.0 03/17/2015 18:22
n-Propylbenzene ND ug/L 88.00 03/17/2015 18:22
o-Xylene ND ug/L 88.00 03/17/2015 18:22
sec-Butylbenzene ND ug/L 88.00 03/17/2015 18:22
tert-Butyl methyl ether (MTBE) ND ug/L 88.00 03/17/2015 18:22
tert-Butylbenzene ND ug/L 88.00 03/17/2015 18:22
trans-1,2-Dichloroethene 77.8 ug/L 88.00 03/17/2015 18:22
trans-1,4-Dichloro-2-butene ND ug/L 840.0 03/17/2015 18:22
Surrogates
1,2-Dichloroethane-d4 103 % 864.0-140 03/17/2015 18:22
4-Bromofluorobenzene 96.0 % 885.0-115 03/17/2015 18:22
Toluene d8 92.0 % 882.0-117 03/17/2015 18:22
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 40 of 77
Client Sample ID: EW-4
Client Project ID: HeatCraft
Lab Sample ID: 31500427014-A
Lab Project ID: 31500427
Collection Date: 03/11/2015 14:20
Received Date: 03/11/2015 15:20
Matrix: Water
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of EW-4
Date Analyzed
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/18/2015 14:12
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5590
Prep Method: SW-846 5030B
Prep Date/Time: 03/17/2015 13:37
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3554
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 41 of 77
Batch Summary
SW-846 8260B SW-846 5030BAnalytical Method:Prep Method:
VXX5581
03/12/2015 07:56
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
LCS for HBN 69384 [VXX/5581]03/12/2015 15:00 MSD8 BWS161921VMS3548
LCSD for HBN 69384 [VXX/5581]03/12/2015 15:25 MSD8 BWS161922VMS3548
MB for HBN 69384 [VXX/5581]03/12/2015 16:15 MSD8 BWS161923VMS3548
OSW-7C 03/12/2015 18:44 MSD8 BWS31500427001VMS3548
OSW-7B 03/12/2015 19:09 MSD8 BWS31500427002VMS3548
FNW-3A(161786MS)03/13/2015 00:56 MSD8 BWS162355VMS3548
FNW-3A(161786MSD)03/13/2015 01:21 MSD8 BWS162356VMS3548
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 42 of 77
Blank ID: MB for HBN 69384 [VXX/5581]
Blank Lab ID: 161923
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500427001, 31500427002
Dichlorodifluoromethane ND 5.00 ug/L 1
Chloromethane ND 1.00 ug/L 1
Vinyl chloride ND 1.00 ug/L 1
Bromomethane ND 1.00 ug/L 1
Chloroethane ND 1.00 ug/L 1
Trichlorofluoromethane ND 1.00 ug/L 1
1,1-Dichloroethene ND 1.00 ug/L 1
Acetone ND 25.0 ug/L 1
Methylene chloride ND 5.00 ug/L 1
trans-1,2-Dichloroethene ND 1.00 ug/L 1
tert-Butyl methyl ether (MTBE) ND 1.00 ug/L 1
1,1-Dichloroethane ND 1.00 ug/L 1
Diisopropyl Ether ND 1.00 ug/L 1
2,2-Dichloropropane ND 1.00 ug/L 1
cis-1,2-Dichloroethene ND 1.00 ug/L 1
2-Butanone ND 25.0 ug/L 1
Bromochloromethane ND 1.00 ug/L 1
Chloroform ND 1.00 ug/L 1
1,1,1-Trichloroethane ND 1.00 ug/L 1
Carbon tetrachloride ND 1.00 ug/L 1
1,1-Dichloropropene ND 1.00 ug/L 1
Benzene ND 1.00 ug/L 1
1,2-Dichloroethane ND 1.00 ug/L 1
Trichloroethene ND 1.00 ug/L 1
1,2-Dichloropropane ND 1.00 ug/L 1
Dibromomethane ND 1.00 ug/L 1
Bromodichloromethane ND 1.00 ug/L 1
cis-1,3-Dichloropropene ND 1.00 ug/L 1
4-Methyl-2-pentanone ND 5.00 ug/L 1
Toluene ND 1.00 ug/L 1
Methyl iodide ND 1.00 ug/L 1
trans-1,3-Dichloropropene ND 1.00 ug/L 1
Carbon disulfide ND 1.00 ug/L 1
1,1,2-Trichloroethane ND 1.00 ug/L 1
Tetrachloroethene ND 1.00 ug/L 1
1,3-Dichloropropane ND 1.00 ug/L 1
2-Hexanone ND 5.00 ug/L 1
Dibromochloromethane ND 1.00 ug/L 1
1,2-Dibromoethane ND 1.00 ug/L 1
Chlorobenzene ND 1.00 ug/L 1
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 1
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 43 of 77
Blank ID: MB for HBN 69384 [VXX/5581]
Blank Lab ID: 161923
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500427001, 31500427002
Bromoform ND 1.00 ug/L 1
Bromobenzene ND 1.00 ug/L 1
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 1
1,2,3-Trichloropropane ND 1.00 ug/L 1
Ethyl Benzene ND 1.00 ug/L 1
m,p-Xylene ND 2.00 ug/L 1
Styrene ND 1.00 ug/L 1
o-Xylene ND 1.00 ug/L 1
Xylene (total)ND 2.00 ug/L 1
Isopropylbenzene (Cumene) ND 1.00 ug/L 1
n-Propylbenzene ND 1.00 ug/L 1
2-Chlorotoluene ND 1.00 ug/L 1
4-Chlorotoluene ND 1.00 ug/L 1
1,3,5-Trimethylbenzene ND 1.00 ug/L 1
tert-Butylbenzene ND 1.00 ug/L 1
1,2,4-Trimethylbenzene ND 1.00 ug/L 1
sec-Butylbenzene ND 1.00 ug/L 1
1,3-Dichlorobenzene ND 1.00 ug/L 1
4-Isopropyltoluene ND 1.00 ug/L 1
1,4-Dichlorobenzene ND 1.00 ug/L 1
1,2-Dichlorobenzene ND 1.00 ug/L 1
n-Butylbenzene ND 1.00 ug/L 1
1,2-Dibromo-3-chloropropane ND 5.00 ug/L 1
1,2,4-Trichlorobenzene ND 1.00 ug/L 1
Hexachlorobutadiene ND 1.00 ug/L 1
Naphthalene ND 1.00 ug/L 1
trans-1,4-Dichloro-2-butene ND 5.00 ug/L 1
1,2,3-Trichlorobenzene ND 1.00 ug/L 1
Surrogates
1,2-Dichloroethane-d4 102 64.0-140 %1
Toluene d8 96.0 82.0-117 %1
4-Bromofluorobenzene 95.0 85.0-115 %1
Batch Information
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 3/12/2015 7:56:33AM
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 44 of 77
Blank Spike ID: LCS for HBN 69384 [VXX/5581]
Blank Spike Lab ID: 161921
Date Analyzed: 03/12/2015 15:00
Spike Duplicate ID: LCSD for HBN 69384 [VXX/5581]
Spike Duplicate Lab ID: 161922
Date Analyzed: 03/12/2015 15:25
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500427001, 31500427002QC for Samples:
Dichlorodifluoromethane 5.00 5.30 5.21065.00 5.03 101 33.0-170 30.00
Chloromethane 5.00 5.11 0.201025.00 5.10 102 57.0-132 30.00
Vinyl chloride 5.00 5.30 3.81065.00 5.10 102 59.0-138 30.00
Bromomethane 5.00 5.42 0.921085.00 5.47 109 51.0-134 30.00
Chloroethane 5.00 4.38 6.6885.00 4.68 94 64.0-145 30.00
Trichlorofluoromethane 5.00 5.36 1.11075.00 5.30 106 64.0-133 30.00
1,1-Dichloroethene 5.00 5.29 2.51065.00 5.16 103 71.0-128 30.00
Acetone 25.0 ND 0.527725.0 ND 77 52.0-140 30.00
Methylene chloride 5.00 5.32 2.71065.00 5.18 104 70.0-113 30.00
trans-1,2-Dichloroethene 5.00 5.47 2.61095.00 5.33 107 57.0-138 30.00
tert-Butyl methyl ether (MTBE)5.00 5.17 5.21035.00 4.91 98 47.0-142 30.00
1,1-Dichloroethane 5.00 5.23 1.91055.00 5.13 103 68.0-133 30.00
Diisopropyl Ether 5.00 5.04 3.01015.00 4.89 98 66.0-132 30.00
2,2-Dichloropropane 5.00 5.33 6.41075.00 5.00 100 74.0-125 30.00
cis-1,2-Dichloroethene 5.00 5.24 2.51055.00 5.11 102 73.0-128 30.00
2-Butanone 25.0 ND 4.19025.0 ND 86 58.0-134 30.00
Bromochloromethane 5.00 5.55 2.01115.00 5.44 109 73.0-128 30.00
Chloroform 5.00 5.25 1.71055.00 5.16 103 74.0-124 30.00
1,1,1-Trichloroethane 5.00 5.19 0.01045.00 5.19 104 76.0-119 30.00
Carbon tetrachloride 5.00 5.16 0.971035.00 5.11 102 75.0-120 30.00
1,1-Dichloropropene 5.00 5.05 2.01015.00 4.95 99 76.0-124 30.00
Benzene 5.00 5.14 0.191035.00 5.15 103 76.0-124 30.00
1,2-Dichloroethane 5.00 5.17 2.21035.00 5.06 101 76.0-119 30.00
Trichloroethene 5.00 4.61 8.5925.00 5.02 100 74.0-121 30.00
1,2-Dichloropropane 5.00 4.74 0.21955.00 4.73 95 74.0-124 30.00
Dibromomethane 5.00 5.22 3.31045.00 5.05 101 71.0-128 30.00
Bromodichloromethane 5.00 4.93 0.0995.00 4.93 99 72.0-120 30.00
cis-1,3-Dichloropropene 5.00 5.08 2.61025.00 4.95 99 73.0-122 30.00
4-Methyl-2-pentanone 25.0 23.6 6.69425.0 22.1 88 65.0-124 30.00
Toluene 5.00 5.05 1.21015.00 4.99 100 75.0-123 30.00
Methyl iodide 5.00 5.02 1.61005.00 4.94 99 55.0-123 30.00
trans-1,3-Dichloropropene 5.00 5.01 2.81005.00 4.87 97 70.0-125 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 45 of 77
Blank Spike ID: LCS for HBN 69384 [VXX/5581]
Blank Spike Lab ID: 161921
Date Analyzed: 03/12/2015 15:00
Spike Duplicate ID: LCSD for HBN 69384 [VXX/5581]
Spike Duplicate Lab ID: 161922
Date Analyzed: 03/12/2015 15:25
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500427001, 31500427002QC for Samples:
Carbon disulfide 5.00 5.12 1.41025.00 5.05 101 65.0-132 30.00
1,1,2-Trichloroethane 5.00 5.10 2.01025.00 5.00 100 76.0-121 30.00
Tetrachloroethene 5.00 5.18 0.191045.00 5.17 103 59.0-112 30.00
1,3-Dichloropropane 5.00 5.03 7.41015.00 4.67 93 74.0-120 30.00
2-Hexanone 25.0 22.5 2.79025.0 21.9 88 56.0-133 30.00
Dibromochloromethane 5.00 4.91 2.9985.00 4.77 95 67.0-122 30.00
1,2-Dibromoethane 5.00 4.98 2.41005.00 4.86 97 74.0-119 30.00
Chlorobenzene 5.00 5.09 3.01025.00 4.94 99 74.0-120 30.00
1,1,1,2-Tetrachloroethane 5.00 4.89 2.5985.00 4.77 95 73.0-119 30.00
Bromoform 5.00 5.11 4.81025.00 4.87 97 62.0-127 30.00
Bromobenzene 5.00 5.28 3.31065.00 5.11 102 75.0-120 30.00
1,1,2,2-Tetrachloroethane 5.00 5.17 5.61035.00 4.89 98 68.0-129 30.00
1,2,3-Trichloropropane 5.00 5.28 6.01065.00 4.97 99 67.0-126 30.00
Ethyl Benzene 5.00 4.69 0.43945.00 4.67 93 76.0-123 30.00
m,p-Xylene 10.0 9.57 0.429610.0 9.61 96 76.0-124 30.00
Styrene 5.00 4.60 0.0925.00 4.60 92 76.0-121 30.00
o-Xylene 5.00 4.36 2.0875.00 4.45 89 75.0-124 30.00
Isopropylbenzene (Cumene)5.00 4.56 0.44915.00 4.58 92 77.0-120 30.00
n-Propylbenzene 5.00 4.75 0.0955.00 4.75 95 77.0-123 30.00
2-Chlorotoluene 5.00 4.90 0.61985.00 4.93 99 74.0-127 30.00
4-Chlorotoluene 5.00 5.06 0.201015.00 5.07 101 77.0-123 30.00
1,3,5-Trimethylbenzene 5.00 4.77 1.0955.00 4.82 96 76.0-122 30.00
tert-Butylbenzene 5.00 4.66 0.85935.00 4.70 94 67.0-122 30.00
1,2,4-Trimethylbenzene 5.00 4.81 0.42965.00 4.79 96 76.0-124 30.00
sec-Butylbenzene 5.00 4.81 0.83965.00 4.85 97 78.0-121 30.00
1,3-Dichlorobenzene 5.00 5.07 1.61015.00 5.15 103 75.0-120 30.00
4-Isopropyltoluene 5.00 4.70 0.85945.00 4.74 95 77.0-120 30.00
1,4-Dichlorobenzene 5.00 4.99 0.401005.00 4.97 99 70.0-125 30.00
1,2-Dichlorobenzene 5.00 5.05 1.81015.00 4.96 99 76.0-118 30.00
n-Butylbenzene 5.00 4.67 0.21935.00 4.66 93 78.0-118 30.00
1,2-Dibromo-3-chloropropane 30.0 27.9 6.79330.0 26.1 87 62.0-130 30.00
1,2,4-Trichlorobenzene 5.00 4.76 2.3955.00 4.65 93 72.0-119 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 46 of 77
Blank Spike ID: LCS for HBN 69384 [VXX/5581]
Blank Spike Lab ID: 161921
Date Analyzed: 03/12/2015 15:00
Spike Duplicate ID: LCSD for HBN 69384 [VXX/5581]
Spike Duplicate Lab ID: 161922
Date Analyzed: 03/12/2015 15:25
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500427001, 31500427002QC for Samples:
Hexachlorobutadiene 5.00 5.19 7.01045.00 4.84 97 69.0-121 30.00
Naphthalene 5.00 4.47 4.8895.00 4.26 85 67.0-122 30.00
trans-1,4-Dichloro-2-butene 25.0 23.6 6.19425.0 22.2 89 61.0-132 30.00
1,2,3-Trichlorobenzene 5.00 4.96 3.3995.00 4.80 96 68.0-123 30.00
Surrogates
1,2-Dichloroethane-d4 104 99 64.0-140
Toluene d8 102 101 82.0-117
4-Bromofluorobenzene 103 102 85.0-115
Batch Information
Analytical Batch: VMS3548
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5581
Prep Method: SW-846 5030B
Prep Date/Time: 03/12/2015 07:56
Spike Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Dupe Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 47 of 77
Batch Summary
SW-846 8260B SW-846 5030BAnalytical Method:Prep Method:
VXX5587
03/13/2015 08:20
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
LCS for HBN 69413 [VXX/5587]03/13/2015 09:23 MSD8 BWS162068VMS3552
LCSD for HBN 69413 [VXX/5587]03/13/2015 09:48 MSD8 BWS162069VMS3552
MB for HBN 69413 [VXX/5587]03/13/2015 10:37 MSD8 BWS162070VMS3552
OSW-7A 03/13/2015 11:27 MSD8 BWS31500427003VMS3552
CR-4 03/13/2015 11:52 MSD8 BWS31500427004VMS3552
CR-3 Water 03/13/2015 12:17 MSD8 BWS31500427005VMS3552
CR-2 Water 03/13/2015 12:42 MSD8 BWS31500427007VMS3552
CR-1 Water 03/13/2015 13:06 MSD8 BWS31500427009VMS3552
MW-2B 03/13/2015 13:31 MSD8 BWS31500427012VMS3552
MW-2A 03/13/2015 13:56 MSD8 BWS31500427011VMS3552
EW-6 03/13/2015 14:21 MSD8 BWS31500427013VMS3552
EW-4 03/13/2015 15:11 MSD8 BWS31500427014VMS3552
RW-2(161981MS)03/13/2015 19:44 MSD8 BWS162388VMS3552
RW-2(161981MSD)03/13/2015 20:09 MSD8 BWS162389VMS3552
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 48 of 77
Blank ID: MB for HBN 69413 [VXX/5587]
Blank Lab ID: 162070
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500427003, 31500427004, 31500427005, 31500427007, 31500427009, 31500427011, 31500427012, 31500427013, 31500427014
Dichlorodifluoromethane ND 5.00 ug/L 1
Chloromethane ND 1.00 ug/L 1
Vinyl chloride ND 1.00 ug/L 1
Bromomethane ND 1.00 ug/L 1
Chloroethane ND 1.00 ug/L 1
Trichlorofluoromethane ND 1.00 ug/L 1
1,1-Dichloroethene ND 1.00 ug/L 1
Acetone ND 25.0 ug/L 1
Methylene chloride ND 5.00 ug/L 1
trans-1,2-Dichloroethene ND 1.00 ug/L 1
tert-Butyl methyl ether (MTBE) ND 1.00 ug/L 1
1,1-Dichloroethane ND 1.00 ug/L 1
Diisopropyl Ether ND 1.00 ug/L 1
2,2-Dichloropropane ND 1.00 ug/L 1
cis-1,2-Dichloroethene ND 1.00 ug/L 1
2-Butanone ND 25.0 ug/L 1
Bromochloromethane ND 1.00 ug/L 1
Chloroform ND 1.00 ug/L 1
1,1,1-Trichloroethane ND 1.00 ug/L 1
Carbon tetrachloride ND 1.00 ug/L 1
1,1-Dichloropropene ND 1.00 ug/L 1
Benzene ND 1.00 ug/L 1
1,2-Dichloroethane ND 1.00 ug/L 1
Trichloroethene ND 1.00 ug/L 1
1,2-Dichloropropane ND 1.00 ug/L 1
Dibromomethane ND 1.00 ug/L 1
Bromodichloromethane ND 1.00 ug/L 1
cis-1,3-Dichloropropene ND 1.00 ug/L 1
4-Methyl-2-pentanone ND 5.00 ug/L 1
Toluene ND 1.00 ug/L 1
Methyl iodide ND 1.00 ug/L 1
trans-1,3-Dichloropropene ND 1.00 ug/L 1
Carbon disulfide ND 1.00 ug/L 1
1,1,2-Trichloroethane ND 1.00 ug/L 1
Tetrachloroethene ND 1.00 ug/L 1
1,3-Dichloropropane ND 1.00 ug/L 1
2-Hexanone ND 5.00 ug/L 1
Dibromochloromethane ND 1.00 ug/L 1
1,2-Dibromoethane ND 1.00 ug/L 1
Chlorobenzene ND 1.00 ug/L 1
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 1
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 49 of 77
Blank ID: MB for HBN 69413 [VXX/5587]
Blank Lab ID: 162070
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500427003, 31500427004, 31500427005, 31500427007, 31500427009, 31500427011, 31500427012, 31500427013, 31500427014
Bromoform ND 1.00 ug/L 1
Bromobenzene ND 1.00 ug/L 1
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 1
1,2,3-Trichloropropane ND 1.00 ug/L 1
Ethyl Benzene ND 1.00 ug/L 1
m,p-Xylene ND 2.00 ug/L 1
Styrene ND 1.00 ug/L 1
o-Xylene ND 1.00 ug/L 1
Xylene (total)ND 2.00 ug/L 1
Isopropylbenzene (Cumene) ND 1.00 ug/L 1
n-Propylbenzene ND 1.00 ug/L 1
2-Chlorotoluene ND 1.00 ug/L 1
4-Chlorotoluene ND 1.00 ug/L 1
1,3,5-Trimethylbenzene ND 1.00 ug/L 1
tert-Butylbenzene ND 1.00 ug/L 1
1,2,4-Trimethylbenzene ND 1.00 ug/L 1
sec-Butylbenzene ND 1.00 ug/L 1
1,3-Dichlorobenzene ND 1.00 ug/L 1
4-Isopropyltoluene ND 1.00 ug/L 1
1,4-Dichlorobenzene ND 1.00 ug/L 1
1,2-Dichlorobenzene ND 1.00 ug/L 1
n-Butylbenzene ND 1.00 ug/L 1
1,2-Dibromo-3-chloropropane ND 5.00 ug/L 1
1,2,4-Trichlorobenzene ND 1.00 ug/L 1
Hexachlorobutadiene ND 1.00 ug/L 1
Naphthalene ND 1.00 ug/L 1
trans-1,4-Dichloro-2-butene ND 5.00 ug/L 1
1,2,3-Trichlorobenzene ND 1.00 ug/L 1
Surrogates
1,2-Dichloroethane-d4 102 64.0-140 %1
Toluene d8 93.0 82.0-117 %1
4-Bromofluorobenzene 96.0 85.0-115 %1
Batch Information
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 3/13/2015 8:20:39AM
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 50 of 77
Blank Spike ID: LCS for HBN 69413 [VXX/5587]
Blank Spike Lab ID: 162068
Date Analyzed: 03/13/2015 09:23
Spike Duplicate ID: LCSD for HBN 69413 [VXX/5587]
Spike Duplicate Lab ID: 162069
Date Analyzed: 03/13/2015 09:48
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500427003, 31500427004, 31500427005, 31500427007, 31500427009, 31500427011, 31500427012,
31500427013, 31500427014
QC for Samples:
Dichlorodifluoromethane 5.00 5.15 6.41035.00 ND 97 33.0-170 30.00
Chloromethane 5.00 5.09 4.41025.00 4.87 97 57.0-132 30.00
Vinyl chloride 5.00 5.16 4.61035.00 4.93 99 59.0-138 30.00
Bromomethane 5.00 4.77 2.3955.00 4.66 93 51.0-134 30.00
Chloroethane 5.00 5.04 3.51015.00 5.22 104 64.0-145 30.00
Trichlorofluoromethane 5.00 5.51 4.61105.00 5.26 105 64.0-133 30.00
1,1-Dichloroethene 5.00 5.16 0.971035.00 5.11 102 71.0-128 30.00
Acetone 25.0 ND 2.19525.0 ND 93 52.0-140 30.00
Methylene chloride 5.00 5.14 0.191035.00 5.13 103 70.0-113 30.00
trans-1,2-Dichloroethene 5.00 5.30 2.31065.00 5.18 104 57.0-138 30.00
tert-Butyl methyl ether (MTBE)5.00 4.62 2.2925.00 4.52 90 47.0-142 30.00
1,1-Dichloroethane 5.00 5.31 2.91065.00 5.16 103 68.0-133 30.00
Diisopropyl Ether 5.00 4.75 0.0955.00 4.75 95 66.0-132 30.00
2,2-Dichloropropane 5.00 5.57 0.721115.00 5.53 111 74.0-125 30.00
cis-1,2-Dichloroethene 5.00 5.00 0.401005.00 4.98 100 73.0-128 30.00
2-Butanone 25.0 ND 2.69325.0 ND 91 58.0-134 30.00
Bromochloromethane 5.00 5.11 1.61025.00 5.03 101 73.0-128 30.00
Chloroform 5.00 5.06 0.791015.00 5.02 100 74.0-124 30.00
1,1,1-Trichloroethane 5.00 5.17 1.21035.00 5.11 102 76.0-119 30.00
Carbon tetrachloride 5.00 5.18 0.961045.00 5.23 105 75.0-120 30.00
1,1-Dichloropropene 5.00 4.83 1.9975.00 4.74 95 76.0-124 30.00
Benzene 5.00 4.95 0.20995.00 4.96 99 76.0-124 30.00
1,2-Dichloroethane 5.00 4.80 0.63965.00 4.77 95 76.0-119 30.00
Trichloroethene 5.00 5.05 0.201015.00 5.04 101 74.0-121 30.00
1,2-Dichloropropane 5.00 4.58 0.0925.00 4.58 92 74.0-124 30.00
Dibromomethane 5.00 4.75 3.5955.00 4.92 98 71.0-128 30.00
Bromodichloromethane 5.00 4.74 0.63955.00 4.71 94 72.0-120 30.00
cis-1,3-Dichloropropene 5.00 5.02 2.21005.00 4.91 98 73.0-122 30.00
4-Methyl-2-pentanone 25.0 19.8 0.507925.0 19.9 79 65.0-124 30.00
Toluene 5.00 4.61 0.22925.00 4.62 92 75.0-123 30.00
Methyl iodide 5.00 3.91 0.26785.00 3.92 78 55.0-123 30.00
trans-1,3-Dichloropropene 5.00 4.74 0.84955.00 4.78 96 70.0-125 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 51 of 77
Blank Spike ID: LCS for HBN 69413 [VXX/5587]
Blank Spike Lab ID: 162068
Date Analyzed: 03/13/2015 09:23
Spike Duplicate ID: LCSD for HBN 69413 [VXX/5587]
Spike Duplicate Lab ID: 162069
Date Analyzed: 03/13/2015 09:48
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500427003, 31500427004, 31500427005, 31500427007, 31500427009, 31500427011, 31500427012,
31500427013, 31500427014
QC for Samples:
Carbon disulfide 5.00 5.22 0.381045.00 5.20 104 65.0-132 30.00
1,1,2-Trichloroethane 5.00 4.97 0.0995.00 4.97 99 76.0-121 30.00
Tetrachloroethene 5.00 5.01 1.21005.00 4.95 99 59.0-112 30.00
1,3-Dichloropropane 5.00 4.58 1.5925.00 4.51 90 74.0-120 30.00
2-Hexanone 25.0 21.7 1.48725.0 21.4 85 56.0-133 30.00
Dibromochloromethane 5.00 4.86 0.62975.00 4.83 97 67.0-122 30.00
1,2-Dibromoethane 5.00 4.57 2.4915.00 4.68 94 74.0-119 30.00
Chlorobenzene 5.00 4.73 0.64955.00 4.70 94 74.0-120 30.00
1,1,1,2-Tetrachloroethane 5.00 5.14 1.81035.00 5.05 101 73.0-119 30.00
Bromoform 5.00 5.16 6.61035.00 4.83 97 62.0-127 30.00
Bromobenzene 5.00 5.05 5.31015.00 4.79 96 75.0-120 30.00
1,1,2,2-Tetrachloroethane 5.00 4.96 4.5995.00 4.74 95 68.0-129 30.00
1,2,3-Trichloropropane 5.00 4.91 5.7985.00 4.64 93 67.0-126 30.00
Ethyl Benzene 5.00 4.32 2.1865.00 4.23 85 76.0-123 30.00
m,p-Xylene 10.0 8.86 2.38910.0 8.66 87 76.0-124 30.00
Styrene 5.00 4.13 1.2835.00 4.08 82 76.0-121 30.00
o-Xylene 5.00 3.90 1.8785.00 3.97 79 75.0-124 30.00
Isopropylbenzene (Cumene)5.00 4.14 1.5835.00 4.08 82 77.0-120 30.00
n-Propylbenzene 5.00 4.46 2.7895.00 4.34 87 77.0-123 30.00
2-Chlorotoluene 5.00 4.57 2.2915.00 4.47 89 74.0-127 30.00
4-Chlorotoluene 5.00 4.71 2.9945.00 4.85 97 77.0-123 30.00
1,3,5-Trimethylbenzene 5.00 4.43 2.1895.00 4.34 87 76.0-122 30.00
tert-Butylbenzene 5.00 4.22 0.24845.00 4.23 85 67.0-122 30.00
1,2,4-Trimethylbenzene 5.00 4.53 1.8915.00 4.45 89 76.0-124 30.00
sec-Butylbenzene 5.00 4.50 0.66905.00 4.53 91 78.0-121 30.00
1,3-Dichlorobenzene 5.00 4.83 2.3975.00 4.72 94 75.0-120 30.00
4-Isopropyltoluene 5.00 4.36 2.6875.00 4.25 85 77.0-120 30.00
1,4-Dichlorobenzene 5.00 4.76 3.2955.00 4.61 92 70.0-125 30.00
1,2-Dichlorobenzene 5.00 4.78 0.21965.00 4.77 95 76.0-118 30.00
n-Butylbenzene 5.00 4.34 2.8875.00 4.22 84 78.0-118 30.00
1,2-Dibromo-3-chloropropane 30.0 25.8 4.48630.0 24.7 82 62.0-130 30.00
1,2,4-Trichlorobenzene 5.00 4.19 0.0845.00 4.19 84 72.0-119 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 52 of 77
Blank Spike ID: LCS for HBN 69413 [VXX/5587]
Blank Spike Lab ID: 162068
Date Analyzed: 03/13/2015 09:23
Spike Duplicate ID: LCSD for HBN 69413 [VXX/5587]
Spike Duplicate Lab ID: 162069
Date Analyzed: 03/13/2015 09:48
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500427003, 31500427004, 31500427005, 31500427007, 31500427009, 31500427011, 31500427012,
31500427013, 31500427014
QC for Samples:
Hexachlorobutadiene 5.00 4.76 3.2955.00 4.61 92 69.0-121 30.00
Naphthalene 5.00 3.79 1.9765.00 3.72 74 67.0-122 30.00
trans-1,4-Dichloro-2-butene 25.0 22.2 1.48925.0 21.9 88 61.0-132 30.00
1,2,3-Trichlorobenzene 5.00 4.42 3.0885.00 4.29 86 68.0-123 30.00
Surrogates
1,2-Dichloroethane-d4 101 102 64.0-140
Toluene d8 99 98 82.0-117
4-Bromofluorobenzene 104 105 85.0-115
Batch Information
Analytical Batch: VMS3552
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: BWS
Prep Batch: VXX5587
Prep Method: SW-846 5030B
Prep Date/Time: 03/13/2015 08:20
Spike Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Dupe Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 53 of 77
Batch Summary
SW-846 8260B SW-846 5035 SLAnalytical Method:Prep Method:
VXX5589
03/17/2015 11:33
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
LCS-S for HBN 69561 [VXX/5589]03/16/2015 12:17 MSD2 JHL162185VMS3553
LCSD-S for HBN 69561 [VXX/5589 03/16/2015 12:43 MSD2 JHL162186VMS3553
MB-S for HBN 69561 [VXX/5589]03/16/2015 13:53 MSD2 JHL162187VMS3553
CR-3 Soil 03/16/2015 16:06 MSD2 JHL31500427006VMS3553
CR-2 Soil 03/16/2015 16:33 MSD2 JHL31500427008VMS3553
CR-1 Soil 03/16/2015 16:59 MSD2 JHL31500427010VMS3553
CR-3 Soil(161904MS)03/16/2015 20:13 MSD2 JHL162188VMS3553
CR-3 Soil(161904MSD)03/16/2015 20:40 MSD2 JHL162189VMS3553
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 54 of 77
Blank ID: MB-S for HBN 69561 [VXX/5589]
Blank Lab ID: 162187
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500427006, 31500427008, 31500427010
Dichlorodifluoromethane ND 5.00 ug/Kg 1
Chloromethane ND 5.00 ug/Kg 1
Vinyl chloride ND 5.00 ug/Kg 1
Bromomethane ND 5.00 ug/Kg 1
Chloroethane ND 5.00 ug/Kg 1
Trichlorofluoromethane ND 5.00 ug/Kg 1
1,1-Dichloroethene ND 5.00 ug/Kg 1
Acetone ND 50.0 ug/Kg 1
Methylene chloride ND 20.0 ug/Kg 1
trans-1,2-Dichloroethene ND 5.00 ug/Kg 1
tert-Butyl methyl ether (MTBE) ND 5.00 ug/Kg 1
1,1-Dichloroethane ND 5.00 ug/Kg 1
Diisopropyl Ether ND 5.00 ug/Kg 1
2,2-Dichloropropane ND 5.00 ug/Kg 1
cis-1,2-Dichloroethene ND 5.00 ug/Kg 1
2-Butanone ND 25.0 ug/Kg 1
Bromochloromethane ND 5.00 ug/Kg 1
Chloroform ND 5.00 ug/Kg 1
1,1,1-Trichloroethane ND 5.00 ug/Kg 1
Carbon tetrachloride ND 5.00 ug/Kg 1
1,1-Dichloropropene ND 5.00 ug/Kg 1
Benzene ND 5.00 ug/Kg 1
1,2-Dichloroethane ND 5.00 ug/Kg 1
Trichloroethene ND 5.00 ug/Kg 1
1,2-Dichloropropane ND 5.00 ug/Kg 1
Dibromomethane ND 5.00 ug/Kg 1
Bromodichloromethane ND 5.00 ug/Kg 1
cis-1,3-Dichloropropene ND 5.00 ug/Kg 1
4-Methyl-2-pentanone ND 12.5 ug/Kg 1
Toluene ND 5.00 ug/Kg 1
Methyl iodide ND 5.00 ug/Kg 1
trans-1,3-Dichloropropene ND 5.00 ug/Kg 1
Carbon disulfide ND 5.00 ug/Kg 1
1,1,2-Trichloroethane ND 5.00 ug/Kg 1
Tetrachloroethene ND 5.00 ug/Kg 1
1,3-Dichloropropane ND 5.00 ug/Kg 1
2-Hexanone ND 12.5 ug/Kg 1
Dibromochloromethane ND 5.00 ug/Kg 1
1,2-Dibromoethane ND 5.00 ug/Kg 1
Chlorobenzene ND 5.00 ug/Kg 1
1,1,1,2-Tetrachloroethane ND 5.00 ug/Kg 1
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 55 of 77
Blank ID: MB-S for HBN 69561 [VXX/5589]
Blank Lab ID: 162187
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500427006, 31500427008, 31500427010
Bromoform ND 5.00 ug/Kg 1
Bromobenzene ND 5.00 ug/Kg 1
1,1,2,2-Tetrachloroethane ND 5.00 ug/Kg 1
1,2,3-Trichloropropane ND 5.00 ug/Kg 1
Ethyl Benzene ND 5.00 ug/Kg 1
m,p-Xylene ND 10.0 ug/Kg 1
Styrene ND 5.00 ug/Kg 1
o-Xylene ND 5.00 ug/Kg 1
Xylene (total)ND 10.0 ug/Kg 1
Isopropylbenzene (Cumene) ND 5.00 ug/Kg 1
n-Propylbenzene ND 5.00 ug/Kg 1
2-Chlorotoluene ND 5.00 ug/Kg 1
4-Chlorotoluene ND 5.00 ug/Kg 1
1,3,5-Trimethylbenzene ND 5.00 ug/Kg 1
tert-Butylbenzene ND 5.00 ug/Kg 1
1,2,4-Trimethylbenzene ND 5.00 ug/Kg 1
sec-Butylbenzene ND 5.00 ug/Kg 1
1,3-Dichlorobenzene ND 5.00 ug/Kg 1
4-Isopropyltoluene ND 5.00 ug/Kg 1
1,4-Dichlorobenzene ND 5.00 ug/Kg 1
1,2-Dichlorobenzene ND 5.00 ug/Kg 1
n-Butylbenzene ND 5.00 ug/Kg 1
1,2-Dibromo-3-chloropropane ND 30.0 ug/Kg 1
1,2,4-Trichlorobenzene ND 5.00 ug/Kg 1
Hexachlorobutadiene ND 5.00 ug/Kg 1
Naphthalene ND 5.00 ug/Kg 1
trans-1,4-Dichloro-2-butene ND 25.0 ug/Kg 1
1,2,3-Trichlorobenzene ND 5.00 ug/Kg 1
Surrogates
1,2-Dichloroethane-d4 109 55.0-173 %1
Toluene d8 106 57.0-134 %1
4-Bromofluorobenzene 103 23.0-141 %1
Batch Information
Prep Batch: VXX5589
Prep Method: SW-846 5035 SL
Prep Date/Time: 3/17/2015 11:33:31AM
Prep Initial Wt./Vol.: 5 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3553
Analytical Method: SW-846 8260B
Instrument: MSD2
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 56 of 77
Blank Spike ID: LCS-S for HBN 69561 [VXX/5589]
Blank Spike Lab ID: 162185
Date Analyzed: 03/16/2015 12:17
Spike Duplicate ID: LCSD-S for HBN 69561 [VXX/5589
Spike Duplicate Lab ID: 162186
Date Analyzed: 03/16/2015 12:43
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31500427006, 31500427008, 31500427010QC for Samples:
Dichlorodifluoromethane 30.0 25.9 138630.0 29.4 98 52.0-133 30.00
Chloromethane 30.0 30.0 1410030.0 34.5 115 64.0-126 30.00
Vinyl chloride 30.0 30.4 1210130.0 34.4 115 69.0-120 30.00
Bromomethane 30.0 31.2 9.510430.0 34.3 114 41.0-160 30.00
Chloroethane 30.0 29.9 1410030.0 34.3 114 69.0-126 30.00
Trichlorofluoromethane 30.0 27.0 269030.0 34.9 116 72.0-123 30.00
1,1-Dichloroethene 30.0 29.1 149730.0 33.6 112 78.0-113 30.00
Acetone 75.0 91.5 0.012275.0 91.5 122 0.00-243 30.00
Methylene chloride 30.0 30.7 9.910230.0 33.9 113 40.0-156 30.00
trans-1,2-Dichloroethene 30.0 29.8 139930.0 33.9 113*78.0-111 30.00
tert-Butyl methyl ether (MTBE)30.0 32.6 4.810930.0 34.2 114 68.0-138 30.00
1,1-Dichloroethane 30.0 30.5 1310230.0 34.6 115 71.0-121 30.00
Diisopropyl Ether 30.0 29.4 129830.0 33.0 110 60.0-141 30.00
2,2-Dichloropropane 30.0 29.0 139730.0 32.9 110 79.0-127 30.00
cis-1,2-Dichloroethene 30.0 30.3 1010130.0 33.6 112 80.0-114 30.00
2-Butanone 75.0 100 1.013475.0 101 134 31.0-189 30.00
Bromochloromethane 30.0 31.2 1110430.0 34.7 116*81.0-115 30.00
Chloroform 30.0 30.5 1310230.0 34.6 115*76.0-114 30.00
1,1,1-Trichloroethane 30.0 28.9 149630.0 33.4 111 79.0-117 30.00
Carbon tetrachloride 30.0 29.3 149830.0 33.6 112 82.0-119 30.00
1,1-Dichloropropene 30.0 28.7 139630.0 32.7 109 82.0-114 30.00
Benzene 30.0 30.9 1210330.0 35.0 117*82.0-113 30.00
1,2-Dichloroethane 30.0 32.5 7.410830.0 35.0 117 72.0-126 30.00
Trichloroethene 30.0 30.0 1410030.0 34.4 115*82.0-108 30.00
1,2-Dichloropropane 30.0 31.6 1110530.0 35.3 118*78.0-116 30.00
Dibromomethane 30.0 33.5 6.111230.0 35.6 119 79.0-125 30.00
Bromodichloromethane 30.0 31.1 1010430.0 34.5 115 79.0-122 30.00
cis-1,3-Dichloropropene 30.0 31.2 9.810430.0 34.4 115 75.0-127 30.00
4-Methyl-2-pentanone 75.0 93.9 0.9512575.0 94.8 126 57.0-159 30.00
Toluene 30.0 29.7 139930.0 33.7 112*83.0-111 30.00
Methyl iodide 30.0 30.5 1310230.0 34.9 116 63.0-137 30.00
trans-1,3-Dichloropropene 30.0 32.1 6.310730.0 34.2 114 75.0-134 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 57 of 77
Blank Spike ID: LCS-S for HBN 69561 [VXX/5589]
Blank Spike Lab ID: 162185
Date Analyzed: 03/16/2015 12:17
Spike Duplicate ID: LCSD-S for HBN 69561 [VXX/5589
Spike Duplicate Lab ID: 162186
Date Analyzed: 03/16/2015 12:43
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31500427006, 31500427008, 31500427010QC for Samples:
Carbon disulfide 30.0 30.2 1310130.0 34.5 115 72.0-116 30.00
1,1,2-Trichloroethane 30.0 30.9 4.110330.0 32.2 107 73.0-121 30.00
Tetrachloroethene 30.0 26.4 138830.0 30.1 100 60.0-118 30.00
1,3-Dichloropropane 30.0 30.0 3.610030.0 31.1 104 76.0-121 30.00
2-Hexanone 75.0 84.5 2.211375.0 82.7 110 41.0-171 30.00
Dibromochloromethane 30.0 29.4 3.39830.0 30.4 101 77.0-126 30.00
1,2-Dibromoethane 30.0 30.2 1.610130.0 30.7 102 76.0-125 30.00
Chlorobenzene 30.0 28.4 7.89530.0 30.7 102 78.0-109 30.00
1,1,1,2-Tetrachloroethane 30.0 27.5 7.09230.0 29.5 98 81.0-117 30.00
Bromoform 30.0 30.6 2.610230.0 31.4 105 72.0-134 30.00
Bromobenzene 30.0 28.2 8.59430.0 30.7 102 76.0-113 30.00
1,1,2,2-Tetrachloroethane 30.0 33.3 0.3011130.0 33.2 111 76.0-129 30.00
1,2,3-Trichloropropane 30.0 32.3 0.6210830.0 32.5 108 70.0-145 30.00
Ethyl Benzene 30.0 26.0 118730.0 29.1 97 72.0-115 30.00
m,p-Xylene 60.0 51.5 118660.0 57.6 96 73.0-114 30.00
Styrene 30.0 25.7 8.68630.0 28.0 93 74.0-114 30.00
o-Xylene 30.0 25.7 108630.0 28.4 95 74.0-113 30.00
Isopropylbenzene (Cumene)30.0 24.8 128330.0 28.0 93 72.0-115 30.00
n-Propylbenzene 30.0 24.7 168230.0 29.0 97 71.0-117 30.00
2-Chlorotoluene 30.0 26.1 8.88730.0 28.5 95 76.0-111 30.00
4-Chlorotoluene 30.0 25.9 9.68630.0 28.5 95 75.0-113 30.00
1,3,5-Trimethylbenzene 30.0 25.3 118430.0 28.2 94 72.0-115 30.00
tert-Butylbenzene 30.0 25.6 128530.0 28.9 96 74.0-112 30.00
1,2,4-Trimethylbenzene 30.0 25.8 8.98630.0 28.2 94 73.0-114 30.00
sec-Butylbenzene 30.0 25.1 128430.0 28.3 94 72.0-115 30.00
1,3-Dichlorobenzene 30.0 27.5 7.49230.0 29.6 99 75.0-110 30.00
4-Isopropyltoluene 30.0 26.4 118830.0 29.5 98 73.0-114 30.00
1,4-Dichlorobenzene 30.0 27.7 5.39230.0 29.2 97 76.0-110 30.00
1,2-Dichlorobenzene 30.0 27.4 7.79130.0 29.6 99 77.0-109 30.00
n-Butylbenzene 30.0 25.8 128630.0 29.1 97 72.0-118 30.00
1,2-Dibromo-3-chloropropane 180 191 3.2106180 185 103 54.0-166 30.00
1,2,4-Trichlorobenzene 30.0 29.1 6.39730.0 31.0 103 76.0-115 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 58 of 77
Blank Spike ID: LCS-S for HBN 69561 [VXX/5589]
Blank Spike Lab ID: 162185
Date Analyzed: 03/16/2015 12:17
Spike Duplicate ID: LCSD-S for HBN 69561 [VXX/5589
Spike Duplicate Lab ID: 162186
Date Analyzed: 03/16/2015 12:43
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31500427006, 31500427008, 31500427010QC for Samples:
Hexachlorobutadiene 30.0 28.2 139430.0 32.0 107 70.0-111 30.00
Naphthalene 30.0 30.8 0.6510330.0 31.0 103 71.0-129 30.00
trans-1,4-Dichloro-2-butene 150 157 3.2105150 152 101 62.0-164 30.00
1,2,3-Trichlorobenzene 30.0 29.5 4.69830.0 30.9 103 78.0-115 30.00
Surrogates
1,2-Dichloroethane-d4 102 105 55.0-173
Toluene d8 104 108 57.0-134
4-Bromofluorobenzene 103 101 23.0-141
Batch Information
Analytical Batch: VMS3553
Analytical Method: SW-846 8260B
Instrument: MSD2
Analyst: JHL
Prep Batch: VXX5589
Prep Method: SW-846 5035 SL
Prep Date/Time: 03/17/2015 11:33
Spike Init Wt./Vol.: 5 g Extract Vol: 5 mL
Dupe Init Wt./Vol.: 5 g Extract Vol: 5 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 59 of 77
Original Sample ID: 31500427006 (CR-3 Soil)
MS Sample ID: 162188
MSD Sample ID: 162189
Analysis Date: 03/16/2015 16:06
Analysis Date: 03/16/2015 20:13
Analysis Date: 03/16/2015 20:40
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31500427006, 31500427008, 31500427010
1,1,1,2-Tetrachloroethane ND 31.0 28.2 30.4 51.7 170 *59*91 30.0069.0-120
1,1,1-Trichloroethane ND 31.0 32.0 30.4 61.2 202 *62*103 30.0078.0-121
1,1,2,2-Tetrachloroethane ND 31.0 42.7 30.4 80.4 265 *61*137 * 30.0076.0-136
1,1,2-Trichloroethane ND 31.0 36.1 30.4 69.7 230 *63*116 30.0065.0-128
1,1-Dichloroethane ND 31.0 34.8 30.4 67.9 224 *65*112 30.0072.0-139
1,1-Dichloroethene ND 31.0 33.6 30.4 64.7 213 *63*108 30.0072.0-135
1,1-Dichloropropene ND 31.0 30.6 30.4 58.5 193 *63*99 30.0069.0-137
1,2,3-Trichlorobenzene ND 31.0 17.8 30.4 18.8 62 5.657 * 30.0061.0-126
1,2,3-Trichloropropane ND 31.0 45.2 30.4 84.3 278 *60*146 30.0010.0-218
1,2,4-Trichlorobenzene ND 31.0 17.9 30.4 18.5 61 2.858 * 30.0061.0-125
1,2,4-Trimethylbenzene ND 31.0 21.5 30.4 30.1 99 33*69 30.0031.0-172
1,2-Dibromo-3-chloropropane ND 186 260 183 475 261 *58*140 30.0043.0-229
1,2-Dibromoethane ND 31.0 36.6 30.4 68.6 226 *61*118 30.0078.0-148
1,2-Dichlorobenzene ND 31.0 23.2 30.4 34.6 114 40*75 30.0058.0-148
1,2-Dichloroethane ND 31.0 38.7 30.4 75.0 247 *64*125 30.0073.0-146
1,2-Dichloropropane ND 31.0 35.1 30.4 68.6 226 *65*113 30.0076.0-136
1,3,5-Trimethylbenzene ND 31.0 21.1 30.4 28.8 95 31*68 30.0068.0-132
1,3-Dichlorobenzene ND 31.0 22.1 30.4 32.9 108 39*71 30.0055.0-145
1,3-Dichloropropane ND 31.0 34.7 30.4 65.9 217 *62*112 30.0033.0-137
1,4-Dichlorobenzene ND 31.0 22.8 30.4 34.0 112 39*74 30.0053.0-146
2,2-Dichloropropane ND 31.0 30.1 30.4 59.4 196 *66*97 30.0058.0-150
2-Butanone ND 77.7 134 75.9 253 333 *61*172 30.0041.0-256
2-Chlorotoluene ND 31.0 22.6 30.4 34.3 113 41*73 30.0060.0-144
2-Hexanone ND 77.7 140 75.9 267 352 *62*180 * 30.0042.0-111
4-Chlorotoluene ND 31.0 22.9 30.4 35.2 116 42*74 30.0059.0-141
4-Isopropyltoluene ND 31.0 20.0 30.4 22.5 74 *1264 * 30.0075.0-122
4-Methyl-2-pentanone ND 77.7 152 75.9 302 398 *66*196 * 30.006.90-166
Acetone ND 77.7 101 75.9 203 267 67*130 30.006.80-355
Benzene ND 31.0 34.0 30.4 66.3 218 *64*110 30.0075.0-133
Bromobenzene ND 31.0 27.1 30.4 46.8 154 *53*87 30.0066.0-140
Bromochloromethane ND 31.0 36.1 30.4 71.1 234 *65*116 30.0085.0-136
Bromodichloromethane ND 31.0 34.2 30.4 66.8 220 *64*110 30.0077.0-140
Bromoform ND 31.0 35.5 30.4 67.2 222 *62*114 30.0075.0-151
Bromomethane ND 31.0 31.3 30.4 62.2 205 *66*101 30.0030.0-127
n-Butylbenzene ND 31.0 18.6 30.4 18.1 60 2.860 30.0041.0-147
Carbon disulfide ND 31.0 34.1 30.4 65.0 214 *62*110 30.0064.0-145
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 60 of 77
Original Sample ID: 31500427006 (CR-3 Soil)
MS Sample ID: 162188
MSD Sample ID: 162189
Analysis Date: 03/16/2015 16:06
Analysis Date: 03/16/2015 20:13
Analysis Date: 03/16/2015 20:40
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31500427006, 31500427008, 31500427010
Carbon tetrachloride ND 31.0 30.9 30.4 58.6 193 *62*100 30.0064.0-142
Chlorobenzene ND 31.0 27.6 30.4 50.2 166 *58*89 30.0066.0-135
Chloroethane ND 31.0 33.6 30.4 65.8 217 *65*108 30.0021.0-182
Chloroform ND 31.0 33.9 30.4 65.6 216 *64*109 30.0071.0-143
Chloromethane ND 31.0 32.8 30.4 63.9 210 *65*106 30.0069.0-138
Dibromochloromethane ND 31.0 32.1 30.4 60.5 199 *62*103 30.0078.0-141
Dibromomethane ND 31.0 40.9 30.4 78.4 258 *63*132 30.0080.0-150
Dichlorodifluoromethane ND 31.0 28.0 30.4 49.6 163 *55*90 30.0082.0-130
cis-1,3-Dichloropropene ND 31.0 33.0 30.4 63.2 208 *63*106 30.0072.0-146
trans-1,3-Dichloropropene ND 31.0 35.9 30.4 69.3 228 *64*116 30.0045.0-144
Diisopropyl Ether ND 31.0 33.0 30.4 66.6 219 *67*106 30.0079.0-122
Ethyl Benzene ND 31.0 25.1 30.4 43.0 142 *52*81 30.0074.0-126
Hexachlorobutadiene ND 31.0 15.1 30.4 9.87 33 *42*49 * 30.0052.0-134
Isopropylbenzene (Cumene) ND 31.0 22.2 30.4 33.5 110 40*72 * 30.0074.0-123
Methyl iodide ND 31.0 33.9 30.4 65.9 217 *64*109 30.0041.0-126
Methylene chloride ND 31.0 34.7 30.4 66.3 218 *62*112 30.0049.0-155
Naphthalene ND 31.0 23.7 30.4 31.2 103 2876 30.0055.0-140
Styrene ND 31.0 21.1 30.4 35.6 117 51*68 * 30.0073.0-123
Tetrachloroethene ND 31.0 26.3 30.4 43.5 143 49*85 30.0046.0-153
Toluene ND 31.0 31.4 30.4 59.9 197 *62*101 30.0066.0-128
Trichloroethene ND 31.0 32.2 30.4 61.5 203 *63*104 30.0035.0-136
Trichlorofluoromethane ND 31.0 30.8 30.4 57.7 190 *61*99 30.0077.0-132
Vinyl chloride ND 31.0 34.3 30.4 64.9 214 *62*110 30.0068.0-137
cis-1,2-Dichloroethene ND 31.0 34.1 30.4 65.0 214 *62*110 30.0077.0-134
m,p-Xylene ND 62.1 49.0 60.7 82.9 137 *51*79 * 30.0080.0-118
n-Propylbenzene ND 31.0 22.4 30.4 31.4 103 33*72 30.0072.0-128
o-Xylene ND 31.0 24.1 30.4 41.8 138 *53*78 * 30.0080.0-121
sec-Butylbenzene ND 31.0 19.4 30.4 22.1 73 1362 30.0057.0-138
tert-Butyl methyl ether (MTBE) ND 31.0 38.9 30.4 77.2 254 *66*125 30.0067.0-135
tert-Butylbenzene ND 31.0 21.2 30.4 26.9 89 2468 30.0061.0-142
trans-1,2-Dichloroethene ND 31.0 33.9 30.4 64.9 214 *63*109 30.0072.0-135
trans-1,4-Dichloro-2-butene ND 156 199 152 373 246 *61*128 30.0049.0-211
Surrogates
1,2-Dichloroethane-d4 119115 55.0-173
4-Bromofluorobenzene 106106 23.0-141
Toluene d8 108105 57.0-134
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 61 of 77
Original Sample ID: 31500427006 (CR-3 Soil)
MS Sample ID: 162188
MSD Sample ID: 162189
Analysis Date: 03/16/2015 16:06
Analysis Date: 03/16/2015 20:13
Analysis Date: 03/16/2015 20:40
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (%)Spike Duplicate (%)
CL RPD CL
QC for Samples:31500427006, 31500427008, 31500427010
Batch Information
Analytical Batch: VMS3553
Analytical Method: SW-846 8260B
Instrument: MSD2
Analyst: JHL
Prep Batch: VXX5589
Prep Method: SW-846 5030B SL
Prep Date/Time: 03/17/2015 11:33
MS Init Wt./Vol.: 6.17 g Extract Vol.: 5 mL
MSD Init Wt./Vol.: 6.31 g Extract Vol.: 5 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 62 of 77
Batch Summary
SW-846 8260B SW-846 5030BAnalytical Method:Prep Method:
VXX5590
03/17/2015 10:26
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
LCS for HBN 69651 [VXX/5590]03/17/2015 13:47 MSD8 JHL162198VMS3554
LCSD for HBN 69651 [VXX/5590]03/17/2015 14:12 MSD8 JHL162199VMS3554
MB for HBN 69651 [VXX/5590]03/17/2015 15:02 MSD8 JHL162200VMS3554
EW-4 03/17/2015 18:22 MSD8 JHL31500427014VMS3554
EW-6 03/17/2015 18:48 MSD8 JHL31500427013VMS3554
MW-2B 03/17/2015 20:28 MSD8 JHL31500427012VMS3554
MW-2A 03/17/2015 20:53 MSD8 JHL31500427011VMS3554
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 63 of 77
Blank ID: MB for HBN 69651 [VXX/5590]
Blank Lab ID: 162200
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500427011, 31500427012, 31500427013, 31500427014
Dichlorodifluoromethane ND 5.00 ug/L 1
Chloromethane ND 1.00 ug/L 1
Vinyl chloride ND 1.00 ug/L 1
Bromomethane ND 1.00 ug/L 1
Chloroethane ND 1.00 ug/L 1
Trichlorofluoromethane ND 1.00 ug/L 1
1,1-Dichloroethene ND 1.00 ug/L 1
Acetone ND 25.0 ug/L 1
Methylene chloride ND 5.00 ug/L 1
trans-1,2-Dichloroethene ND 1.00 ug/L 1
tert-Butyl methyl ether (MTBE) ND 1.00 ug/L 1
1,1-Dichloroethane ND 1.00 ug/L 1
Diisopropyl Ether ND 1.00 ug/L 1
2,2-Dichloropropane ND 1.00 ug/L 1
2-Butanone ND 25.0 ug/L 1
Bromochloromethane ND 1.00 ug/L 1
Chloroform ND 1.00 ug/L 1
1,1,1-Trichloroethane ND 1.00 ug/L 1
Carbon tetrachloride ND 1.00 ug/L 1
1,1-Dichloropropene ND 1.00 ug/L 1
Benzene ND 1.00 ug/L 1
1,2-Dichloroethane ND 1.00 ug/L 1
Trichloroethene ND 1.00 ug/L 1
1,2-Dichloropropane ND 1.00 ug/L 1
Dibromomethane ND 1.00 ug/L 1
Bromodichloromethane ND 1.00 ug/L 1
cis-1,3-Dichloropropene ND 1.00 ug/L 1
4-Methyl-2-pentanone ND 5.00 ug/L 1
Toluene ND 1.00 ug/L 1
Methyl iodide ND 1.00 ug/L 1
trans-1,3-Dichloropropene ND 1.00 ug/L 1
Carbon disulfide ND 1.00 ug/L 1
1,1,2-Trichloroethane ND 1.00 ug/L 1
Tetrachloroethene ND 1.00 ug/L 1
1,3-Dichloropropane ND 1.00 ug/L 1
2-Hexanone ND 5.00 ug/L 1
Dibromochloromethane ND 1.00 ug/L 1
1,2-Dibromoethane ND 1.00 ug/L 1
Chlorobenzene ND 1.00 ug/L 1
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 1
Bromoform ND 1.00 ug/L 1
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 64 of 77
Blank ID: MB for HBN 69651 [VXX/5590]
Blank Lab ID: 162200
Matrix: Water
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500427011, 31500427012, 31500427013, 31500427014
Bromobenzene ND 1.00 ug/L 1
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 1
1,2,3-Trichloropropane ND 1.00 ug/L 1
Ethyl Benzene ND 1.00 ug/L 1
m,p-Xylene ND 2.00 ug/L 1
Styrene ND 1.00 ug/L 1
o-Xylene ND 1.00 ug/L 1
Xylene (total)ND 2.00 ug/L 1
Isopropylbenzene (Cumene) ND 1.00 ug/L 1
n-Propylbenzene ND 1.00 ug/L 1
2-Chlorotoluene ND 1.00 ug/L 1
4-Chlorotoluene ND 1.00 ug/L 1
1,3,5-Trimethylbenzene ND 1.00 ug/L 1
tert-Butylbenzene ND 1.00 ug/L 1
1,2,4-Trimethylbenzene ND 1.00 ug/L 1
sec-Butylbenzene ND 1.00 ug/L 1
1,3-Dichlorobenzene ND 1.00 ug/L 1
4-Isopropyltoluene ND 1.00 ug/L 1
1,4-Dichlorobenzene ND 1.00 ug/L 1
1,2-Dichlorobenzene ND 1.00 ug/L 1
n-Butylbenzene ND 1.00 ug/L 1
1,2-Dibromo-3-chloropropane ND 5.00 ug/L 1
1,2,4-Trichlorobenzene ND 1.00 ug/L 1
Hexachlorobutadiene ND 1.00 ug/L 1
Naphthalene ND 1.00 ug/L 1
trans-1,4-Dichloro-2-butene ND 5.00 ug/L 1
1,2,3-Trichlorobenzene ND 1.00 ug/L 1
Surrogates
1,2-Dichloroethane-d4 105 64.0-140 %1
Toluene d8 91.0 82.0-117 %1
4-Bromofluorobenzene 96.0 85.0-115 %1
Batch Information
Prep Batch: VXX5590
Prep Method: SW-846 5030B
Prep Date/Time: 3/17/2015 10:26:26AM
Prep Initial Wt./Vol.: 40 mL
Prep Extract Vol: 40 mL
Analytical Batch: VMS3554
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: JHL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 65 of 77
Blank Spike ID: LCS for HBN 69651 [VXX/5590]
Blank Spike Lab ID: 162198
Date Analyzed: 03/17/2015 13:47
Spike Duplicate ID: LCSD for HBN 69651 [VXX/5590]
Spike Duplicate Lab ID: 162199
Date Analyzed: 03/17/2015 14:12
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500427011, 31500427012, 31500427013, 31500427014QC for Samples:
Dichlorodifluoromethane 5.00 5.72 0.171145.00 5.73 115 33.0-170 30.00
Chloromethane 5.00 5.74 3.01155.00 5.57 111 57.0-132 30.00
Vinyl chloride 5.00 5.96 4.51195.00 5.70 114 59.0-138 30.00
Bromomethane 5.00 5.12 0.581025.00 5.15 103 51.0-134 30.00
Chloroethane 5.00 4.82 20965.00 5.89 118 64.0-145 30.00
Trichlorofluoromethane 5.00 6.21 0.481245.00 6.24 125 64.0-133 30.00
1,1-Dichloroethene 5.00 5.97 1.31195.00 5.89 118 71.0-128 30.00
Acetone 25.0 32.6 5.013025.0 31.0 124 52.0-140 30.00
Methylene chloride 5.00 5.96 0.17119*5.00 5.95 119*70.0-113 30.00
trans-1,2-Dichloroethene 5.00 6.04 0.501215.00 6.07 121 57.0-138 30.00
tert-Butyl methyl ether (MTBE)5.00 6.00 6.01205.00 5.65 113 47.0-142 30.00
1,1-Dichloroethane 5.00 6.13 1.51235.00 6.04 121 68.0-133 30.00
Diisopropyl Ether 5.00 5.75 1.21155.00 5.68 114 66.0-132 30.00
2,2-Dichloropropane 5.00 6.56 2.8131*5.00 6.38 128*74.0-125 30.00
2-Butanone 25.0 31.3 4.612525.0 29.9 120 58.0-134 30.00
Bromochloromethane 5.00 6.22 3.91245.00 5.98 120 73.0-128 30.00
Chloroform 5.00 5.92 0.511185.00 5.95 119 74.0-124 30.00
1,1,1-Trichloroethane 5.00 6.13 2.1123*5.00 6.00 120*76.0-119 30.00
Carbon tetrachloride 5.00 6.38 1.7128*5.00 6.27 125*75.0-120 30.00
1,1-Dichloropropene 5.00 5.81 0.691165.00 5.77 115 76.0-124 30.00
Benzene 5.00 5.86 1.41175.00 5.78 116 76.0-124 30.00
1,2-Dichloroethane 5.00 5.97 0.331195.00 5.99 120*76.0-119 30.00
Trichloroethene 5.00 4.65 24935.00 5.91 118 74.0-121 30.00
1,2-Dichloropropane 5.00 5.24 1.11055.00 5.30 106 74.0-124 30.00
Dibromomethane 5.00 5.60 1.41125.00 5.68 114 71.0-128 30.00
Bromodichloromethane 5.00 5.55 2.71115.00 5.70 114 72.0-120 30.00
cis-1,3-Dichloropropene 5.00 6.11 1.81225.00 6.00 120 73.0-122 30.00
4-Methyl-2-pentanone 25.0 28.3 7.311325.0 26.3 105 65.0-124 30.00
Toluene 5.00 5.42 1.51085.00 5.34 107 75.0-123 30.00
Methyl iodide 5.00 4.28 1.2865.00 4.23 85 55.0-123 30.00
trans-1,3-Dichloropropene 5.00 5.81 0.521165.00 5.84 117 70.0-125 30.00
Carbon disulfide 5.00 5.99 0.01205.00 5.99 120 65.0-132 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 66 of 77
Blank Spike ID: LCS for HBN 69651 [VXX/5590]
Blank Spike Lab ID: 162198
Date Analyzed: 03/17/2015 13:47
Spike Duplicate ID: LCSD for HBN 69651 [VXX/5590]
Spike Duplicate Lab ID: 162199
Date Analyzed: 03/17/2015 14:12
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500427011, 31500427012, 31500427013, 31500427014QC for Samples:
1,1,2-Trichloroethane 5.00 5.76 4.41155.00 6.02 120 76.0-121 30.00
Tetrachloroethene 5.00 5.39 4.91085.00 5.66 113*59.0-112 30.00
1,3-Dichloropropane 5.00 5.29 3.31065.00 5.47 109 74.0-120 30.00
2-Hexanone 25.0 28.1 0.3611225.0 28.0 112 56.0-133 30.00
Dibromochloromethane 5.00 5.51 8.81105.00 6.02 120 67.0-122 30.00
1,2-Dibromoethane 5.00 5.50 2.21105.00 5.62 112 74.0-119 30.00
Chlorobenzene 5.00 5.08 9.01025.00 5.56 111 74.0-120 30.00
1,1,1,2-Tetrachloroethane 5.00 5.70 111145.00 6.37 127*73.0-119 30.00
Bromoform 5.00 5.68 9.91145.00 6.27 125 62.0-127 30.00
Bromobenzene 5.00 5.33 9.61075.00 5.87 117 75.0-120 30.00
1,1,2,2-Tetrachloroethane 5.00 5.75 4.61155.00 6.02 120 68.0-129 30.00
1,2,3-Trichloropropane 5.00 5.82 3.31165.00 5.63 113 67.0-126 30.00
Ethyl Benzene 5.00 4.52 6.4905.00 4.82 96 76.0-123 30.00
m,p-Xylene 10.0 9.27 8.69310.0 10.1 101 76.0-124 30.00
Styrene 5.00 4.44 8.4895.00 4.83 97 76.0-121 30.00
o-Xylene 5.00 4.22 6.2845.00 4.49 90 75.0-124 30.00
Isopropylbenzene (Cumene)5.00 4.39 7.2885.00 4.72 94 77.0-120 30.00
n-Propylbenzene 5.00 4.69 7.2945.00 5.04 101 77.0-123 30.00
2-Chlorotoluene 5.00 4.78 5.7965.00 5.06 101 74.0-127 30.00
4-Chlorotoluene 5.00 4.81 14965.00 5.54 111 77.0-123 30.00
1,3,5-Trimethylbenzene 5.00 4.69 8.2945.00 5.09 102 76.0-122 30.00
tert-Butylbenzene 5.00 4.56 5.5915.00 4.82 96 67.0-122 30.00
1,2,4-Trimethylbenzene 5.00 4.77 6.9955.00 5.11 102 76.0-124 30.00
sec-Butylbenzene 5.00 4.78 8.0965.00 5.18 104 78.0-121 30.00
1,3-Dichlorobenzene 5.00 5.12 6.61025.00 5.47 109 75.0-120 30.00
4-Isopropyltoluene 5.00 4.63 8.3935.00 5.03 101 77.0-120 30.00
1,4-Dichlorobenzene 5.00 5.01 7.31005.00 5.39 108 70.0-125 30.00
1,2-Dichlorobenzene 5.00 5.18 5.81045.00 5.49 110 76.0-118 30.00
n-Butylbenzene 5.00 4.69 6.4945.00 5.00 100 78.0-118 30.00
1,2-Dibromo-3-chloropropane 30.0 32.5 0.9210830.0 32.8 109 62.0-130 30.00
1,2,4-Trichlorobenzene 5.00 4.62 4.4925.00 4.83 97 72.0-119 30.00
Hexachlorobutadiene 5.00 5.02 111005.00 5.58 112 69.0-121 30.00
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 67 of 77
Blank Spike ID: LCS for HBN 69651 [VXX/5590]
Blank Spike Lab ID: 162198
Date Analyzed: 03/17/2015 13:47
Spike Duplicate ID: LCSD for HBN 69651 [VXX/5590]
Spike Duplicate Lab ID: 162199
Date Analyzed: 03/17/2015 14:12
Results by SW-846 8260B
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/L)
RPD CL
Spike Duplicate (ug/L)
31500427011, 31500427012, 31500427013, 31500427014QC for Samples:
Naphthalene 5.00 4.53 1.1915.00 4.58 92 67.0-122 30.00
trans-1,4-Dichloro-2-butene 25.0 27.2 3.310925.0 28.1 112 61.0-132 30.00
1,2,3-Trichlorobenzene 5.00 4.92 5.5985.00 5.20 104 68.0-123 30.00
Surrogates
1,2-Dichloroethane-d4 114 105 64.0-140
Toluene d8 107 98 82.0-117
4-Bromofluorobenzene 103 104 85.0-115
Batch Information
Analytical Batch: VMS3554
Analytical Method: SW-846 8260B
Instrument: MSD8
Analyst: JHL
Prep Batch: VXX5590
Prep Method: SW-846 5030B
Prep Date/Time: 03/17/2015 10:26
Spike Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Dupe Init Wt./Vol.: 40 mL Extract Vol: 40 mL
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 68 of 77
Batch Summary
SW-846 8270D SW-846 3520C 1L/1mLAnalytical Method:Prep Method:
XXX4630
03/12/2015 16:00
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
MB for HBN 69407 [XXX/4630]03/17/2015 11:18 MSD10 DTF162008XMS2258
LCS for HBN 69407 [XXX/4630]03/17/2015 11:39 MSD10 DTF162009XMS2258
CAM-1R(161778DUP)03/17/2015 12:23 MSD10 DTF162010XMS2258
CR-2 Water 03/17/2015 14:57 MSD10 DTF31500427007XMS2258
MW-2A 03/17/2015 15:18 MSD10 DTF31500427011XMS2258
OSW-5C(161782MS)03/17/2015 16:58 MSD10 DTF162011XMS2258
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 69 of 77
Blank ID: MB for HBN 69407 [XXX/4630]
Blank Lab ID: 162008
Matrix: Water
Results by SW-846 8270D
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500427007, 31500427011
1,4 Dioxane ND 2.00 ug/L 1
Surrogates
Nitrobenzene-d5 71.0 50.0-150 %1
Batch Information
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 3/12/2015 4:00:05PM
Prep Initial Wt./Vol.: 1000 mL
Prep Extract Vol: 1 mL
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 70 of 77
Blank Spike ID: LCS for HBN 69407 [XXX/4630]
Blank Spike Lab ID: 162009
Date Analyzed: 03/17/2015 11:39
Results by SW-846 8270D
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)CL
Blank Spike (ug/L)
31500427007, 31500427011QC for Samples:
1,4 Dioxane 10.0 4.09 41 -
Surrogates
Nitrobenzene-d5 75.1 -
Batch Information
Analytical Batch: XMS2258
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX4630
Prep Method: SW-846 3520C 1L/1mL
Prep Date/Time: 03/12/2015 16:00
Spike Init Wt./Vol.: 1000 mL Extract Vol: 1 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 71 of 77
Batch Summary
EPA 300.0 EPA 300.0Analytical Method:Prep Method:
INO3705
03/11/2015 14:01
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
MB for HBN 69356 [INO/3705]03/11/2015 14:01 IC2 PSW161825INO3705
LCS for HBN 69356 [INO/3705]03/11/2015 14:29 IC2 PSW161826INO3705
OSW-4(161790MS)03/11/2015 14:43 IC2 PSW161873INO3705
OSW-4(161790MSD)03/11/2015 14:57 IC2 PSW161874INO3705
FW-1C(161792DUP)03/11/2015 15:12 IC2 PSW161827INO3705
MW-2A 03/11/2015 15:28 IC2 PSW31500427011INO3705
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 72 of 77
Blank ID: MB for HBN 69356 [INO/3705]
Blank Lab ID: 161825
Matrix: Water
Results by EPA 300.0
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31500427011
Nitrate as N ND 0.300 mg/L 1
Sulfate ND 1.00 mg/L 1
Batch Information
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 3/11/2015 2:01:24PM
Prep Initial Wt./Vol.: 10 mL
Prep Extract Vol: 10 mL
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 73 of 77
Blank Spike ID: LCS for HBN 69356 [INO/3705]
Blank Spike Lab ID: 161826
Date Analyzed: 03/11/2015 14:29
Results by EPA 300.0
Blank Spike Summary
Matrix: Water
Parameter Spike Result Rec (%)CL
Blank Spike (mg/L)
31500427011QC for Samples:
Nitrate as N 4.00 4.27 107 90.0-110
Sulfate 20.0 21.5 107 90.0-110
Batch Information
Analytical Batch: INO3705
Analytical Method: EPA 300.0
Instrument: IC2
Analyst: PSW
Prep Batch: INO3705
Prep Method: EPA 300.0
Prep Date/Time: 03/11/2015 14:29
Spike Init Wt./Vol.: 10 mL Extract Vol: 10 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 03/24/2015 N.C. Certification # 481
WO# 31500427 Page 74 of 77
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WO# 31500427 Page 77 of 77