6004_DukeMcGuireLF1_Jan2016_1stSemiAnnual_DIN26335_20160418

McGuire Nuclear Station – Landfill #1
(Unlined) Permit No. 6004
Semiannual Groundwater
Monitoring Report
January 2016 Sampling Event

April 14, 2016

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
January 2016 Sampling Event
CONTENTS

ii

Contents
Page
Report Verification ......................................................................................................................... i
Contents ........................................................................................................................................ ii
Section 1 - Background ................................................................................................................. 1
Section 2 - Methods ...................................................................................................................... 3
2.1 Sampling and Analysis Methods .................................................................................... 3
2.2 Statement of Work .......................................................................................................... 4
Section 3 - Results ........................................................................................................................ 5
3.1 Site Groundwater Flow ................................................................................................... 5
3.2 Analytical Results ........................................................................................................... 5

FIGURES
1. Site Location Map
2. Sample Locations
3. Generalized Groundwater Surface Contours
TABLES
1. Well Construction Information
2. Groundwater Flow Velocities
3. Field Data Parameters
4. Groundwater Field and Analytical Results
5. Field and Analytical Results that Equal or Exceed 15A NCAC 2L Groundwater Quality
Standards
6. Surface Water Field and Analytical Results
7. Field and Analytical Results that Equal or Exceed 15A NCAC 2B Surface Water Quality
Standards
8. Radiological Analytical Results
APPENDICES
A. Field Sampling Forms
B. Laboratory Report and Chain-of-Custody Forms
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
January 2016 Sampling Event
SECTION 1 - BACKGROUND

1

Section 1 - Background
The McGuire Nuclear Station Landfill #1 (Unlined)1 is located at the Duke Energy Carolinas,
LLC (Duke Energy) McGuire Nuclear Station in Mecklenburg County, North Carolina. The
landfill is closed and no longer accepts waste. The landfill and nearby area are depicted on
Figure 1. The approximate limit of waste is shown on Figure 2.
The landfill is located south of NC Highway 73, east of the Catawba River, and to the west of
Cashion Road. Cashion Road runs along a topographic divide with topography sloping away
from Cashion Road to the northwest and to the southeast. Surface water to the northwest of
Cashion Road drains towards the Catawba River. There are two surface water drainage
features adjacent to the landfill. The surface water drainage feature located to the north of the
landfill contains an unnamed perennial stream that drains to the northwest towards another
perennial unnamed stream that flows to the Catawba River. The surface water drainage feature
located to the south and west of the landfill also drains to an unnamed stream that flows to the
Catawba River.
As described in the Sampling and Analysis Plan2 (SAP), the monitoring system at the landfill
consists of the following:
Monitoring Wells:MW-1
MW-1D
MW-2A
MW-2D
MW-3
MW-3D
MW-4
MW-4D
MW-11
MW-11D
MW-12
MW-12D
MW-4R
MW-4DR

Surface Water Sample Location:SW-1

The monitoring wells and the surface water sample location are shown on Figure 2. The wells
were installed as well pairs with one shallow well and one deeper well adjacent to each other.
The well with the “D” designation is the deeper well in each well pair. The shallow wells are
1 In response to the North Carolina Division of Public Health, Radiation Protection Section, November 17,
2006, letter to Duke Energy, LLC, Duke Energy offered to indicate the McGuire Nuclear Station Landfill
#1 as (Unlined) in reports.
2 McGuire Nuclear Station Landfill #1, Permit Number 60-04, Ground-Water Monitoring Program
Sampling and Analysis Plan (SAP), September 14, 1996, Revised, November 24, 1997, March 9, 2001.

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
January 2016 Sampling Event
SECTION 1 - BACKGROUND

2

screened to intercept the water table. The deep wells are constructed so that the bottom of the
screen is located in residual material just above auger refusal. Monitoring wells MW-1 and
MW-1D are located upgradient of the landfill.
Monitoring wells MW-4R and MW-4DR are not included in the SAP. These wells were installed
in December 2013 as replacement wells for MW-4 and MW-4D, respectively. Monitoring wells
MW-4 and MW-4D are approximately 15 feet outside of the waste boundary. The replacement
wells were installed in the vicinity of MW-4 and MW-4D and are located near the review
boundary. Replacement monitoring well MW-4R was installed with the well screen from 43 feet
to 28 feet below ground surface to intercept the water table. Monitoring well MW-4DR was
installed with the well screen from 87.6 feet to 72.6 feet below ground surface. Table 1 presents
well construction information for the landfill monitoring wells.
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
January 2016 Sampling Event
SECTION 2 - METHODS

3

Section 2 - Methods
2.1 Sampling and Analysis Methods
The collection of samples and documentation of sampling was performed by Duke Energy
personnel (Field Certification #5193) according to the North Carolina Solid Waste Management
Guidelines. Copies of the field sampling forms are included in Appendix A. The parameters and
constituents reported were selected by Duke Energy and the North Carolina Department of
Environmental Quality (NCDEQ) Division of Solid Waste and were analyzed by TestAmerica
Laboratories, Inc. (North Carolina Laboratory Certification #358) and the Duke Energy Analytical
Laboratory (North Carolina Laboratory Certification #248).
The groundwater and surface water samples were analyzed for the following constituents in
accordance with the SAP:
 Barium, chromium, and silver using Solid Waste (SW) Method/6010C
 Arsenic, cadmium, lead, and selenium using SW Method 6020A
 Mercury using US Environmental Protection Agency (EPA) Method 7470
 Sulfate using EPA Method 9056A
 Volatile organic compounds (VOCs) using SW846 Method 8260B
Surface water sample SW-1 was field-filtered and analyzed for the dissolved fraction of the
following constituents:
 Barium, chromium, and silver using SW Method/6010C
 Arsenic, cadmium, and lead using SW Method 6020A
In addition, the following analyses were performed in accordance with the requirements of the
Radioactive Materials License No. 060-0379-7 issued by the North Carolina Department of
Health and Human Services Radiation Protection Section:
 Gross alpha radioactivity using EPA Method 900
 Gross beta radioactivity using EPA Method 900
 Tritium using EPA Method 906.0 Modified
 Gamma radioactivity for select isotopes

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
January 2016 Sampling Event
SECTION 2 - METHODS

4

2.2 Statement of Work
HDR completed the following tasks:
 Received field sampling information provided by Duke Energy (performed by Duke
Energy personnel) for monitoring wells MW-1, MW-1D, MW-2A, MW-2D, MW-3, MW-3D,
MW-4, MW-4R, MW-4D, MW-4DR, MW-11, MW-11D, MW-12, and MW-12D. Data was
also received for surface water sample location SW-1. The samples were collected on
January 14, 2016, and HDR received the data on February 11, 2016. The field sampling
forms are included in Appendix A.
 Reviewed the laboratory analytical results for the samples. The Electronic Data
Deliverable (EDD) provided by Duke Energy was adapted to conform to the format
requirements of the NCDEQ EDD template. HDR added an italicized J’ data qualifier (J’)
to indicate a measured concentration that is equal to or greater than the laboratory’s
method reporting limit (MRL) but is less than the Solid Waste Section Limit3 (SWSL). A
copy of the original EDD is retained in HDR’s files.
 Developed a generalized groundwater surface contour map using map data and
groundwater elevation data supplied by Duke Energy. Calculated groundwater flow
velocities based on groundwater surface contours.
 Prepared and submitted this Semiannual Groundwater Monitoring Report to Duke
Energy.
3 The Solid Waste Section Limit (SWSL) is defined by NCDEQ as the lowest amount of analyte in a
sample that can be quantitatively determined with suitable precision and accuracy. The SWSL is the
concentration below which reported results must be qualified as estimated. NCDEQ Division of Waste
Management Memorandum dated February 23, 2007.
Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
January 2016 Sampling Event
SECTION 3 - RESULTS

5

Section 3 - Results
3.1 Site Groundwater Flow
Generalized groundwater surface contours and groundwater flow direction arrows for the site
are shown on Figure 3. These contours were developed using groundwater elevations
measured at the shallow wells on the date of sampling. Calculated flow velocities are presented
in Table 2.
Groundwater flow in the area of the landfill is generally from the southeast near MW-1/MW-1D
and Cashion Road, toward the northwest, toward MW-3/MW-3D, MW-4/MW-4D, and
MW-4R/MW-4DR. The discrepancy between water levels at MW-12/12D has been verified by
Duke Energy.
3.2 Analytical Results
A summary of the field data is presented in Table 3.
The field and analytical results of groundwater samples collected from the monitoring wells are
summarized in Table 4. The analytical results for these samples are compared to the
groundwater standards found in Title 15A NCAC 02L .0202 (g) (2L Standards). Concentrations
with values that attain or exceed the 2L Standards are noted on Table 4 by bold font. A
summary of the field and analytical results that attain or exceed the 2L Standards and a
preliminary analysis of the cause and significance of the exceedances are presented in Table 5.
Surface water sample location SW-1 is located on an unnamed stream. The unnamed stream is
a tributary to the Catawba River which is classified by the NCDEQ Division of Water Quality as
Class WS-IV water at its confluence with the unnamed stream. As a result, the field and
analytical results from this location are compared to Title 15A, North Carolina Administrative
Code (NCAC), Subchapter 2B Standards (2B Standards) for Class WS-IV water. The field and
analytical results of surface water sampling are summarized in Table 6. Concentrations with
values that attain or exceed the 2B Standards are noted on Table 6 by bold font. A summary of
the field and analytical results that attain or exceed the 2B Standards and a preliminary analysis
of the cause and significance of the exceedances are presented in Table 7.
The minimum detection limit (MDL) was greater than the respective 2L Standard for the
following constituents:
 1,2,3-Trichloropropane
 1,2-Dibromo-3-chloropropane
 1,2-Dibromoethane (EDB)
 Vinyl chloride

Duke Energy Carolinas, LLC | Semiannual Groundwater Monitoring Report
McGuire Nuclear Station – Landfill #1 (Unlined) Permit No. 6004
January 2016 Sampling Event
SECTION 3 - RESULTS

6

The MDL was greater than the respective 2B Standard for the following constituents:
 Mercury
 Silver, dissolved
The MDLs for the listed constituents were all below their corresponding SWSLs as required by
the February 23, 2007, NCDEQ memo4. With the exception of the vinyl chloride concentration in
the sample collected from monitoring well MW-4D and the dissolved silver concentration at SW-
1, these constituents were not detected above the MDL in the analyzed samples and are not
considered to exceed their respective 2L or 2B Standards.
Analytical results with values that equal or are greater than the SWSLs are noted in Table 4 by
gray cells.
The results of the radiological analysis are presented in Table 8. A copy of this report has been
submitted to the North Carolina Department of Health and Human Services Radiation Protection
Section for reference. HDR did not evaluate this data.
Select samples were diluted, as is normal laboratory practice, to bring samples within the
calibrated range of the analysis. Specifics regarding the samples that were diluted, including the
dilution amount, are reported in the EDD. The laboratory reports and chain-of-custody forms can
be found in Appendix B.

4 The Solid Waste Section Limit (SWSL) is defined by NCDEQ as the lowest amount of analyte in a
sample that can be quantitatively determined with suitable precision and accuracy. The SWSL is the
concentration below which reported results must be qualified as estimated. NCDEQ Division of Waste
Management Memorandum dated February 23, 2007.

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a
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h
e
r
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d

r
o
c
k
.
6
.

H
o
r
i
z
o
n
t
a
l

d
a
t
u
m

N
A
D
8
3
.
7
.

V
e
r
t
i
c
a
l

d
a
t
u
m

i
s

N
A
V
D

8
8
.
8
.

D
e
p
t
h

t
o

g
r
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d
w
a
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g
a
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d

o
n

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r
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1
4
,

2
0
1
6
.
9
.

I
n
f
o
r
m
a
t
i
o
n

p
r
o
v
i
d
e
d

b
y

D
u
k
e

E
n
e
r
g
y
.
10
.

T
o
t
a
l

w
e
l
l

d
e
p
t
h
s

f
r
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m

2
0
1
5

w
e
l
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d
e
p
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h

c
o
n
f
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m
a
t
i
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n
.
11
.

T
o
p

o
f

C
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s
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n
g

a
n
d

G
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o
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n
d

S
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a
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E
l
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v
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t
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s

f
r
o
m

J
a
n
u
a
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y

2
0
1
5

r
e
-
s
u
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v
e
y

b
y

P
r
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v
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d
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n
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L
a
n
d

G
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p
.
Co
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d
i
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a
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s
We
l
l

I
D
We
l
l

In
s
t
a
l
l
a
t
i
o
n

Da
t
e
W
e
l
l

T
O
C

Ele
v
a
t
i
o
n

(
f
t
.
)
Gr
o
u
n
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S
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f
a
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Ele
v
a
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(f
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.
)
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r
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e
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I
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t
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r
v
a
l

be
l
o
w

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C
(f
t
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)
Casing TypeWell Diameter (in.)Geology of Screened Interval
We
l
l

S
t
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c
k
-
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p

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i
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h
t

A
b
o
v
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Gr
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d

S
u
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f
a
c
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(f
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)
Gr
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d
w
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r

Ele
v
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o
n
(ft
.
)
De
p
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h

t
o

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a
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be
l
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w

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C
(ft
.
)
To
t
a
l

W
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l
l

De
p
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b
e
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C
(f
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.
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De
p
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t
o

T
o
p

o
f

Sc
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e
n

f
r
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m

T
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C
(ft
.
)
Page  1  of  1
Ta
b
l
e

2

-

G
r
o
u
n
d
w
a
t
e
r

F
l
o
w

V
e
l
o
c
i
t
i
e
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
We
l
l

I
D

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p
g
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d
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t

Gr
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w
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t
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r

Co
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t
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r

El
e
v
a
t
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o
n
(f
t
)
D
o
w
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g
r
a
d
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t

Gr
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w
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Co
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t
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E
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v
a
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(f
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t
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th
r
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(f
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)
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d
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a
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c

Gr
a
d
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(f
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/
f
t
)
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d
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a
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d
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v
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y

(f
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/
d
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)
Ef
f
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c
t
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e

Po
r
o
s
i
t
y

(%
/
1
0
0
)
Groundwater Velocity (ft/day)
MW
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1
70
2
70
0
55

0
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0
4

0
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4
1
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2
5
9

0
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6
MW
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8
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7
MW
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2
67
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72

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3

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4
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4
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6
67
6
21

0
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0
2

0
.
4
1
0.
2
5
9

0
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3
MW
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1
69
4
69
2
62

0
.
0
3

0
.
4
1
0.
2
5
9

0
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5
MW
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3
71
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35

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.
1
0

0
.
4
1
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2
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9

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5
MW
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76

0
.
0
1

0
.
4
1
0.
2
5
9

0
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0
1
No
t
e
s
:
1
.

L
i
n
e
a
r

d
i
s
t
a
n
c
e

m
e
a
s
u
r
e
d

t
h
r
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u
g
h

m
o
n
i
t
o
r
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n
g

w
e
l
l
s

i
s

g
e
n
e
r
a
l
l
y

p
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r
p
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n
d
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c
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l
a
r

t
o

g
r
o
u
n
d
w
a
t
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r

c
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n
t
o
u
r
s
.
2
.

A
t

m
o
n
i
t
o
r
i
n
g

w
e
l
l

l
o
c
a
t
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o
n
s

w
h
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r
e

d
o
w
n
g
r
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d
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e
n
t

c
o
n
t
o
u
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s

a
r
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n
o
t

p
r
e
s
e
n
t
,

t
h
e

g
r
o
u
n
d
w
a
t
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r

e
l
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v
a
t
i
o
n

a
t

t
h
e

m
o
n
i
t
o
r
i
n
g

w
e
l
l

i
s

u
s
e
d

a
s

t
h
e

d
o
w
n
g
r
a
d
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n
t

g
r
o
u
n
d
w
a
t
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r

e
l
e
v
a
t
i
o
n
.
3
.

A
t

m
o
n
i
t
o
r
i
n
g

w
e
l
l

l
o
c
a
t
i
o
n
s

w
h
e
r
e

u
p
g
r
a
d
i
e
n
t

c
o
n
t
o
u
r
s

a
r
e

n
o
t

p
r
e
s
e
n
t
,

t
h
e

g
r
o
u
n
d
w
a
t
e
r

e
l
e
v
a
t
i
o
n

a
t

t
h
e

m
o
n
i
t
o
r
i
n
g

w
e
l
l

i
s

u
s
e
d

a
s

t
h
e

u
p
g
r
a
d
i
e
n
t

g
r
o
u
n
d
w
a
t
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r

e
l
e
v
a
t
i
o
n
.
4
.

M
o
n
i
t
o
r
i
n
g

w
e
l
l
s

a
r
e

n
o
t

l
i
s
t
e
d

w
h
e
r
e

i
n
s
u
f
f
i
c
i
e
n
t

g
r
o
u
n
d
w
a
t
e
r

c
o
n
t
o
u
r

i
n
f
o
r
m
a
t
i
o
n

i
s

a
v
a
i
l
a
b
l
e

t
o

c
a
l
c
u
l
a
t
e

v
e
l
o
c
i
t
y
.
5
.

H
y
d
r
a
u
l
i
c

g
r
a
d
i
e
n
t
s

a
n
d

g
r
o
u
n
d
w
a
t
e
r

v
e
l
o
c
i
t
i
e
s

a
r
e

a
p
p
r
o
x
i
m
a
t
e
.
6
.

H
y
d
r
a
u
l
i
c

c
o
n
d
u
c
t
i
v
i
t
y

p
r
e
s
e
n
t
e
d

i
s

t
h
e

g
e
o
m
e
t
r
i
c

m
e
a
n

o
f

t
h
e

c
o
n
d
u
c
t
i
v
i
t
y

d
a
t
a

f
o
r

t
h
e

a
l
l
u
v
i
u
m
/
s
o
i
l
/
s
a
p
r
o
l
i
t
e

a
n
d

P
W
R

h
y
d
r
o
s
t
r
a
t
i
g
r
a
p
h
i
c

l
a
y
e
r

i
n

t
h
e

H
D
R

C
o
n
d
u
c
t
i
v
i
t
y

D
a
t
a
b
a
s
e

(
u
n
p
u
b
l
i
s
h
e
d

d
a
t
a

f
r
o
m

P
i
e
d
m
o
n
t

C
a
r
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l
i
n
a

s
i
t
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s

w
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t
h

f
o
l
i
a
t
e
d
/
l
a
y
e
r
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d

b
e
d
r
o
c
k
)
.
7
.

E
f
f
e
c
t
i
v
e

p
o
r
o
s
i
t
y

p
r
e
s
e
n
t
e
d

i
s

t
h
e

m
e
a
n

v
a
l
u
e

o
f

t
h
e

a
l
l
u
v
i
u
m
/
s
o
i
l
/
s
a
p
r
o
l
i
t
e

a
n
d

P
W
R

h
y
d
r
o
s
t
r
a
t
i
g
r
a
p
h
i
c

l
a
y
e
r

e
s
t
i
m
a
t
e
d

f
r
o
m

s
o
i
l

t
e
s
t
i
n
g

u
s
i
n
g

F
e
t
t
e
r
/
B
e
a
r

D
i
a
g
r
a
m
s
.

8
.

H
y
d
r
a
u
l
i
c

g
r
a
d
i
e
n
t

a
n
d

g
r
o
u
n
d
w
a
t
e
r

v
e
l
o
c
i
t
i
e
s

a
r
e

b
a
s
e
d

o
n

J
a
n
u
a
r
y

1
4
,

2
0
1
6

m
e
a
s
u
r
e
d

w
a
t
e
r

e
l
e
v
a
t
i
o
n
s
.
Page 1 of 1
Ta
b
l
e

3

-

F
i
e
l
d

D
a
t
a

P
a
r
a
m
e
t
e
r
s
Du
k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
i
t

N
o
.

6
0
0
4
DA
T
E
SA
M
P
L
E

I
D
WE
L
L
DE
P
T
H
(f
e
e
t
)
DE
P
T
H

T
O
WA
T
E
R
(f
e
e
t
)
WA
T
E
R
EL
E
V
.
(f
e
e
t
)

A
P
P
E
A
R
A
N
C
E
OD
O
R
PU
R
G
E
ME
T
H
O
D

PU
M
P

RA
T
E
(m
L
/
m
i
n
)
WE
L
L
VO
L
U
M
E
(g
a
l
)
EV
A
C
VO
L
U
M
E
(g
a
l
)
EV
A
C
(y
e
s
/
n
o
)
TE
M
P
(d
e
g

C
)
SP
E
C
I
F
I
C
CO
N
D
U
C
T
A
N
C
E
(µ
Լ /c
m
)
pH
(S
U
)
TURBIDITY (NTU)ORP (mV-NHE)DO (mg/L)
1/
1
4
/
2
0
1
6

M
W
-
1

6
8
.
5
5

2
7
.
7
5

7
0
2
.
4
8

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A
6.
6
5

2
0
.
2
5

N
O

1
5
.
2
0

1
1
4
6.1

6
.
6

2
2
8

0
.
0
0
1/
1
4
/
2
0
1
6

M
W
-
1
D

8
8
.
2
2

2
8
.
8
4

7
0
1
.
7
7

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A
9.
6
8

2
9
.
2
5

N
O

1
5
.
4
7

1
0
5
6.1

2
.
8

2
2
6

0
.
0
0
1/
1
4
/
2
0
1
6

M
W
-
2
A

7
7
.
5
7

5
3
.
1
9

6
8
6
.
4
8

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A
3.
9
8

6
.
5
0

N
O

1
6
.
5
2

8
6
6.4

2
.
1

3
9
0

4
.
4
9
1/
1
4
/
2
0
1
6

M
W
-
2
D

1
0
8
.
8
2

5
4
.
4
0

6
8
6
.
3
7

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A
8.
8
8

1
8
.
5
0

N
O

1
6
.
4
0

6
1
7.0

2
.
4

3
2
9

9
.
6
9
1/
1
4
/
2
0
1
6

M
W
-
3

7
3
.
6
4

5
7
.
1
3

6
7
1
.
3
0

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A
2.
6
9

1
3
.
7
5

N
O

1
4
.
9
2

8
1
6.4

1
.
6

3
8
6

5
.
6
1
1/
1
4
/
2
0
1
6

M
W
-
3
D

9
0
.
1
9

5
7
.
0
8

6
7
1
.
3
1

N
o
r
m
a
l

N
o
n
e

C
P

N
/
A
5.
4
0

1
6
.
5
0

N
O

1
5
.
0
6

1
2
7
6.6

1
.
1

3
4
3

1
.
7
2
1/
1
4
/
2
0
1
6

M
W
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4

7
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1
5

6
5
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5
3

6
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6
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o
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l

N
o
n
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N
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0
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3
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1
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P

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1
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5

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6
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6
1

6
9
5
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9
9

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l

N
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9
3

7
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5
0

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O

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9
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9
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1
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5

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N
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P

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/
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0
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2
9
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0
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O

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4
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4
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3
.
3
5

N
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m
a
l

N
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n
e

C
P

N
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2.
9
4

9
.
0
0

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O

1
3
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5
2

2
1
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6
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9

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8
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4
2

2
3
.
9
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7
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0
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8
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m
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l

N
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n
e

C
P

N
/
A
7.
2
5

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4
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7
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O

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5
0

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3

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1
5

8
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1
0
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4
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2
0
1
6

S
W
-
1

N
/
A
N/
A
N/
A
No
r
m
a
l

N
o
n
e

N
/
A
N/
A
N/
A
N/
A
N/
A
8.5
4
87
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2
5
.
6

2
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1

1
0
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6

M
W
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4
R

4
5
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7
3

3
8
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4
8

6
7
5
.
3
9

N
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r
m
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l

N
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P

N
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1.
1
8

6
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2
5

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O

1
4
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4
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6

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R

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4
0

3
7
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8
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5
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9
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N
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/
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5
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7
5

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O

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5
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2
1

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0
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2

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4
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5
4
No
t
e
s
:
1
.

P
u
r
g
e

M
e
t
h
o
d
s
;

L
F
=
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o
w

F
l
o
w
,

C
P
=
C
o
n
v
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n
t
i
o
n
a
l

P
u
r
g
e

(
3
-
5

w
e
l
l

v
o
l
u
m
e
s
)
,

N
P
=
N
o

P
u
r
g
e

(
H
y
d
r
a
S
l
e
e
v
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)
,

E
O
P
=
E
q
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p
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O
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l
y

P
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.

P
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p

r
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a
p
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a
b
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t
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L
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p
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o
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.
2
.

F
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s
a
m
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p
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b
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D
u
k
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E
n
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y

C
a
r
o
l
i
n
a
s
,

L
L
C

p
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s
o
n
n
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l
.
3
.

E
V
A
C

i
n
d
i
c
a
t
e
s

w
h
e
t
h
e
r

t
h
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w
a
t
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r

l
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v
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l

i
n

t
h
e

w
e
l
l

w
a
s

d
r
a
w
n

d
o
w
n

t
o

t
h
e

l
e
v
e
l

o
f

t
h
e

p
u
m
p

d
u
r
i
n
g

p
u
r
g
i
n
g
.
4
.

µ
Լ /c
m

i
n
d
i
c
a
t
e
s

m
i
c
r
o

m
h
o
s

p
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r

c
e
n
t
i
m
e
t
e
r
.
5
.

S
U

i
n
d
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c
a
t
e
s

S
t
a
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d
a
r
d

U
n
i
t
s
.
6
.

N
T
U

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n
d
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c
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N
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p
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m
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T
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b
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y

U
n
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t
s
.
7
.

m
V
-
N
H
E

i
n
d
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c
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s

m
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l
l
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s
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N
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m
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d
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n

E
l
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c
t
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d
e
.
8
.

m
g
/
L

i
n
d
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c
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t
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s

m
i
l
l
i
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r
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m
s

p
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l
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r
.
9
.

N
/
A

i
n
d
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c
a
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s

n
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t

a
p
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l
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c
a
b
l
e
.
10
.

I
n
f
o
r
m
a
t
i
o
n

p
r
o
v
i
d
e
d

b
y

T
i
m

H
u
n
s
u
c
k
e
r

o
f

D
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k
e

E
n
e
r
g
y

C
a
r
o
l
i
n
a
s
,

L
L
C

o
n

F
e
b
r
u
a
r
y

1
1
,

2
0
1
6
.
Page 1 of 1
Ta
b
l
e

4

-

G
r
o
u
n
d
w
a
t
e
r

F
i
e
l
d

a
n
d

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
Du
k
e

E
n
e
r
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y

C
a
r
o
l
i
n
a
s
,

L
L
C
/
M
c
G
u
i
r
e

N
u
c
l
e
a
r

S
t
a
t
i
o
n
La
n
d
f
i
l
l

#
1

(
U
n
l
i
n
e
d
)

-

P
e
r
m
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t

N
o
.

6
0
0
4
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l
d

p
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32
0

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1
9
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6
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5
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µ
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5
1
9
3
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N
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m
p
e
r
a
t
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e

3
2
5

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5
1
9
3
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o
f

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g

3
2
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t

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t
o

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r

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l
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1
1

f
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t

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E

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E

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Ar
s
e
n
i
c

1
4
µg/
L
24
8

0
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1
7
7
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3
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1
4
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0
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0
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0
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0.
0
7
8

1
0
10
10
Ba
r
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u
m
15
µg/
L
24
8
21
8
10
3
26
.
4
J'
15
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4
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38
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2
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0.1

1
0
0

7
0
0
2,000
Ca
d
m
i
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m
34
µg/
L
24
8
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1
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1

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1
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1

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Ch
r
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m
51
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L
24
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5

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5

1
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100
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a
d
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1
µg/
L
24
8
0.
0
6
5

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5

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6
5

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15
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r
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u
r
y

1
3
2
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L
24
8

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0
3
3
4

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0
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0
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3
4

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3
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n
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m
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L
24
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0
9
2

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2

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0
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1
1
4
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0
9
2

1
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20
50
Si
l
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r
18
4
µg/
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24
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0.7

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0.
7

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0.7

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7

U
0.7

U

0
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7

1
0
20
100*
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l
f
a
t
e
31
5
µg/
L
24
8
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0
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34
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43
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37
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2
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5
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0
0
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2
5
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0
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n
e
16

µ
g
/
L

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2

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2

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0
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2

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c
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7
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µ
g
/
L

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4

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2
4

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0
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2
4

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2
4

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2
4

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s
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2
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c
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t
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8
µg/
L

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8
0.2
1

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0
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2
1

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0
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2
1

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2
1

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0
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2
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2
1

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tr
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n
s
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c
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l
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e
t
h
y
l
e
n
e

7
9

µ
g
/
L

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5
8
0.2
3

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0
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2
3

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0
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2
3

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0
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2
3

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0
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2
3

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2
3

5
10
0
100
Dic
h
l
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m
e
t
h
a
n
e

1
4
0
µg/
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3
5
8
1U
1U
1U
1U
1U
11

5

5
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t
r
a
c
h
l
o
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e
t
h
y
l
e
n
e

1
9
2
µg/
L

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8
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4

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1
4

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0
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1
4

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0
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1
4

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0
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1
4

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1
4

1
0.7
5
To
l
u
e
n
e
19
6
µg/
L

3
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7

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0
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1
7

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0
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1
7

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0
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1
7

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1
7

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1
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1,000
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c
h
l
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e
t
h
y
l
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n
e

2
0
1
µg/
L

3
5
8
0.2

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2

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0.2

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0.
2

U
0.2

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0.2

1
3
5
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l

C
h
l
o
r
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d
e
21
1
µg/
L

3
5
8
0.1
8

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0
.
1
8

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0
.
1
8

U

0
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1
8

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1
8

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1
8

1
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0
3
2
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n
e

(
t
o
t
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l
)
34
6

µ
g
/
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3
5
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8

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0
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5
8

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0
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5
8

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0
.
5
8

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0
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5
8

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5
8

5
50
0
10,000
No
t
e
s
:
1
.

C
o
n
c
e
n
t
r
a
t
i
o
n
s

p
r
e
s
e
n
t
e
d

i
n

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r

(
µ
g
/
L
)
.
2
.

S
U

i
n
d
i
c
a
t
e
s

S
t
a
n
d
a
r
d

U
n
i
t
s
.
3
.

µ
Լ /c
m

i
n
d
i
c
a
t
e
s

m
i
c
r
o
m
h
o
s

p
e
r

c
e
n
t
i
m
e
t
e
r
.
4
.

S
W
S

I
D

i
s

t
h
e

S
o
l
i
d

W
a
s
t
e

S
e
c
t
i
o
n

I
d
e
n
t
i
f
i
c
a
t
i
o
n

N
u
m
b
e
r
.
5
.

M
D
L

i
s

t
h
e

l
a
b
o
r
a
t
o
r
y

m
e
t
h
o
d

d
e
t
e
c
t
i
o
n

l
i
m
i
t
.

T
h
e

M
D
L

v
a
lu
e
s

p
r
e
s
e
n
t
e
d

a
r
e

f
o
r

s
a
m
p
l
e
s

n
o
t

d
i
l
u
t
e
d

b
y

t
h
e

l
a
b
o
r
a
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Page 2 of 3
Ta
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1
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5
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Page 3 of 3
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Ta
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6

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Page 1 of 1

A
Appendix A
Field Sampling Forms

ANALYZER SERIAL #:
WEATHER CONDITIONS:
DATE:TIME:DATE:TIME:
Calibation Instrument Standard Instrument Standard
Standard Value Value Value Value
SS 0.0 ▬▬►0.0 0.0 ▬/▬►0.0
SS 223.7 ▬▬►227 229.6 ▬/▬►227
SS 74.8 ▬/▬►75 75.7 ▬/▬►75
SS ▬/▬►▬/▬►
B (7.00)6.97 ▬▬►7.02 7.08 ▬/▬►7.02
B (4.00)4.04 ▬▬►4.00 4.04 ▬/▬►4.00
B (10.00)10.09 ▬/▬►10.06 10.16 ▬/▬►10.06
20.08 20.14
pH Check B (7.00)▬▬►
Time:
SS (7.00)442 ▬▬►441 441 ▬/▬►440
SS (4.00)N/A ▬/▬►N/A N/A ▬/▬►N/A
Zobell's 20.09 20.24
W 9.00 8.90
W 9.00 9.00
AW 9.00 ▬▬►9.00 8.96 ▬/▬►8.95
SS 54.9 ▬/▬►54.3 54.6 ▬/▬►54.3
NIST N/A ▬/▬►N/A N/A ▬/▬►N/A
KEY:
NOTES:
SS = Standard solution AW = Average Winkler ▬/▬►= Not Adjusted To
(mmHg)
B = Buffer W = Winkler ▬▬► = Adjusted To N/A = Not Applicable
Replaced DO electrolyte See Notes
Field Barometric Pressure
Beginning BP 743.7 (mmHg)Ending BP 743.7
Tested - OK See Notes Tested - OK See Notes
Dissolved Oxygen Subsystem
Replaced Teflon Membrane Cleaned Electrode
Tested - OK See Notes
Oxidation Reduction Subsystem Temperature Subsystem
Cleaned Electrode Cleaned Electrode
Tested - OK Replaced ref Electrode KCL
See Notes Replaced Ref. Electrode Tip
INSTRUMENT MAINTENANCE DATE / TIME
Conductance Subsystem pH Subsystem
Cleaned Electrodes Cleaned Electrodes
Temp Cert Device #
TEMP
(deg C)Adjustment Not Available Adjustment Not Available
ORP Temp.ORP Temp.
Calibration Pass
TURB
(ntu)Calibration Accepted Calibration Accepted
DO
(mg/L)Calibration Accepted
Buffer Temp.
ORP
(mV)
Calibration Accepted Calibration Pass
pH
(units)
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Buffer Temp.Buffer Temp.
Parameter Calibration Results Calibration Results
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
CHECK (uS/cm)
SPEC. COND.
(uS/cm)
Instrument Zeroed Zero Pass
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Calibration Date / Time 14-Jan-16 5:35 15-Jan-16 5:35
CALIBRATION BP (mmHg)743.9 CALIBRATION BP (mmHg)741.2
COLLECTORS:LDC, PSP, CMF SURFACE UNIT SERIAL #:0662
ANALYZER MODEL#:HL4 400437
PROCEDURE #:HYDROLAB 3210.5 VALIDATED BY:
FIELD SAMPLING CALIBRATION FORM
STUDY:McGUIRE NUCLEAR STATION - LANDFILL 1 GROUNDWATER MONITORING
DATE (s):January 14, 2016 SURFACE UNIT READER:LDC
OTHER EQUIPMENT:TURBIDIMETER NO.2 - 3260-GW Clear, calm, 25 to 60 deg F.
ANALYZER SERIAL #:
WEATHER CONDITIONS:
DATE:TIME:DATE:TIME:
Calibation Instrument Standard Instrument Standard
Standard Value Value Value Value
SS 0.0 ▬/▬►0.0 0.0 ▬/▬►0.0
SS 227.7 ▬▬►227 226.1 ▬/▬►227
SS 73.2 ▬/▬►75 72.8 ▬/▬►75
SS ▬/▬►▬/▬►
B (7.00)6.92 ▬▬►7.02 7.01 ▬/▬►7.02
B (4.00)4.01 ▬▬►4.00 3.97 ▬/▬►4.00
B (10.00)10.18 ▬/▬►10.06 10.16 ▬/▬►10.06
20.18 20.26
pH Check B (7.00)▬▬►
Time:
SS (7.00)441 ▬▬►441 439 ▬/▬►440
SS (4.00)N/A ▬/▬►N/A N/A ▬/▬►N/A
Zobell's 20.17 20.24
W 9.00 8.90
W 9.00 9.00
AW 8.95 ▬▬►9.00 9.02 ▬/▬►8.95
SS 54.1 ▬/▬►54.1 54.6 ▬/▬►54.1
NIST N/A ▬/▬►N/A N/A ▬/▬►N/A
KEY:
NOTES:
SS = Standard solution AW = Average Winkler ▬/▬►= Not Adjusted To
(mmHg)
B = Buffer W = Winkler ▬▬► = Adjusted To N/A = Not Applicable
Replaced DO electrolyte See Notes
Field Barometric Pressure
Beginning BP 743.7 (mmHg)Ending BP 743.7
Tested - OK See Notes Tested - OK See Notes
Dissolved Oxygen Subsystem
Replaced Teflon Membrane Cleaned Electrode
Tested - OK See Notes
Oxidation Reduction Subsystem Temperature Subsystem
Cleaned Electrode Cleaned Electrode
Tested - OK Replaced ref Electrode KCL
See Notes Replaced Ref. Electrode Tip
INSTRUMENT MAINTENANCE DATE / TIME
Conductance Subsystem pH Subsystem
Cleaned Electrodes Cleaned Electrodes
Temp Cert Device #
TEMP
(deg C)Adjustment Not Available Adjustment Not Available
ORP Temp.ORP Temp.
Calibration Pass
TURB
(ntu)Calibration Accepted Calibration Accepted
DO
(mg/L)Calibration Accepted
Buffer Temp.
ORP
(mV)
Calibration Accepted Calibration Pass
pH
(units)
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Buffer Temp.Buffer Temp.
Parameter Calibration Results Calibration Results
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
CHECK (uS/cm)
SPEC. COND.
(uS/cm)
Instrument Zeroed Zero Pass
Calibration Accepted Calibration Pass
Calibration Accepted Calibration Pass
Calibration Date / Time 14-Jan-16 5:20 15-Jan-16 5:25
CALIBRATION BP (mmHg)743.9 CALIBRATION BP (mmHg)741.2
COLLECTORS:LDC, PSP, CMF SURFACE UNIT SERIAL #:S05042
ANALYZER MODEL#:MS5 66120
PROCEDURE #:HYDROLAB 3210.5 VALIDATED BY:
FIELD SAMPLING CALIBRATION FORM
STUDY:McGUIRE NUCLEAR STATION - LANDFILL 1 GROUNDWATER MONITORING
DATE (s):January 14, 2016 SURFACE UNIT READER:PSP
OTHER EQUIPMENT:TURBIDIMETER NO.1 - 3260-GW Clear, calm, 25 to 60 deg F.
58.55 68.55
35 (psi)9 (sec)(sec)
(gal)
6.65 (gal)
@
QC By:< 2.0
DATE TIME
DISSOLVED
OXYGEN
6.6 228 0.00
0.00230
1/14/2016 0850
Sample preservation verified to pH
(units)
ORP
(ft)(YES/NO)
6.75 NO 15.11 114 6.07
15.24
VOLUME EVACUATION COND.
PURGE METHOD
Conventional
DISCHARGERECHARGEPRESSURE 6
PUMP CONTROLLER SETTINGS
0.1631CONVERSION FACTOR
Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
6.65WELL VOLUME
(gal)
FIELD CREW LDC, PSP, CMF
MONITORING WELL INFORMATION
2
N/A
PROCEDURE NO 3175.2DUKE ENERGY
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING
SAMPLING DATE(s)14-Jan-2016
63.55
68.05PUMP INTAKE DEPTH (ft TOC)68.55
TOC ELEV (ft msl)
GS ELEV (ft msl)
730.23
729.58
WELL/LOCATION NAME MW-1
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88
WELL DEPTH (ft TOC)
WELL DIAMETER (in)MIDDLE OF WETTED SCREEN (ft toc)
WELL VOL
SCREEN INTERVAL (ft TOC)TO
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)27.75 WATER COLUMN (ft)40.80
EQUIPMENT INFORMATION
LEVEL METER SERIAL#26055 SAMPLING EQUIPMENT
TUBING DIAMETER (in)1/2 OD
QED T1200
PURGE COMPLETE TEMP SPECIFIC pH TURBIDITY
WATER ELEVATION (ft msl)702.48
APPEARANCE
DETECTED ODOR None
Normal
WATER LEVEL
AFTER PURGE *(recalculates on
current water
level)(deg C)(umho/cm)(SU)(NTU)(mV-NHE)(mg/L)
21.2 235 0.00
6.75 NO
6.75 NO 15.20 114 6.10
114 6.08 7.0
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY
LDC 0
TOTAL PURGE
VOLUME
20.25
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
WELL CASING
WELL CONDITION
PROTECTIVE CASING
WELL PAD
WELL TAG
Good Condition
Good Condition
Good Condition
SAMPLING NOTES
QC for rad collected
ADDITIONAL WELL CONDITION NOTES
Good Tag
78.22 88.22
42 (psi)8 (sec)(sec)
(gal)
9.68 (gal)
@
QC By:
SAMPLING NOTES
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
29.25 LDC 1/14/2016 0905 0
9.75 NO 15.47 105 6.08 2.8 226 0.00
9.75 NO 15.47 105 6.10 4.1 228 0.00
OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
9.75 NO 15.38 104 6.07 7.3 229
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
0.00
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.
(gal)
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)28.84 WATER COLUMN (ft)59.38 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)701.77 WELL VOLUME 9.68
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 7
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)730.61 MIDDLE OF WETTED SCREEN (ft toc)83.22
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)88.22 GS ELEV (ft msl)729.75 PUMP INTAKE DEPTH (ft TOC)87.72
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-1D
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
67.57 77.57
48 (psi)10 (sec)(sec)
(gal)
3.98 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-2A
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)739.67 MIDDLE OF WETTED SCREEN (ft toc)72.57
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)77.57 GS ELEV (ft msl)736.96 PUMP INTAKE DEPTH (ft TOC)77.07
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
28651 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)53.19 WATER COLUMN (ft)24.38 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)686.48 WELL VOLUME 3.98
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
4.00 70.47 NO 16.35 85 6.41 2.5 387
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
6.63 1.16
1.25 NO 16.52 86 6.38 2.1 390 4.49
1.25 NO 16.37 88 6.36 4.2 381 5.30
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
6.50 PSP / CMF 1/14/2016 1330 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
98.82 108.82
50 (psi)5 (sec)(sec)
(gal)
8.88 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-2D
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)740.77 MIDDLE OF WETTED SCREEN (ft toc)103.82
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)108.82 GS ELEV (ft msl)737.41 PUMP INTAKE DEPTH (ft TOC)108.32
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
28651 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)54.40 WATER COLUMN (ft)54.42 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)686.37 WELL VOLUME 8.88
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
9.00 80.03 NO 16.42 63 6.98 5.8 339
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
11.44 4.70
4.75 NO 16.40 61 6.98 2.4 329 9.69
4.75 NO 16.57 61 7.03 3.0 331 10.19
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
18.50 PSP / CMF 1/14/2016 1425 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
63.64 73.64
38 (psi)10 (sec)(sec)
(gal)
2.69 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-3
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)728.43 MIDDLE OF WETTED SCREEN (ft toc)68.64
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)73.64 GS ELEV (ft msl)724.98 PUMP INTAKE DEPTH (ft TOC)73.14
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
28651 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)57.13 WATER COLUMN (ft)16.51 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)671.30 WELL VOLUME 2.69
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
2.75 NO 14.97 94 6.30 2.6 356
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
5.40
2.75 NO 14.99 82 6.37 1.5 387 5.51
2.75 NO 15.03 87 6.40 2.7 386 5.35
2.75 NO 14.92 81 6.38 1.6 386 5.61
2.75 NO 15.02 81 6.37 1.3 388 5.52
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
13.75 PSP / CMF 1/14/2016 1000 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
80.19 90.19
48 (psi)14 (sec)(sec)
(gal)
5.40 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-3D
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)728.39 MIDDLE OF WETTED SCREEN (ft toc)85.19
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)90.19 GS ELEV (ft msl)724.98 PUMP INTAKE DEPTH (ft TOC)89.69
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 6
28651 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)57.08 WATER COLUMN (ft)33.11 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)671.31 WELL VOLUME 5.40
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
5.50 NO 14.81 128 6.63 340
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
1.36
5.50 NO 15.06 127 6.61 1.1 343 1.72
5.50 NO 15.03 128 6.63 1.1 350 1.49
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
16.50 PSP / CMF 1/14/2016 1020 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
64.15 74.15
45 (psi)45 (sec)(sec)
(gal)
1600 (ml)
495 (ml)
2095 (ml)=0.55 (gal)@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR EQUIPMENT PURGE ONLY SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-4
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)741.13 MIDDLE OF WETTED SCREEN (ft toc)69.84
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)74.15 GS ELEV (ft msl)738.40 PUMP INTAKE DEPTH (ft TOC)73.65
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 15
28651 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Equip. Only Purge
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)65.53 WATER COLUMN (ft)8.62 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)675.60 WELL VOLUME 1.41
INITIAL FLOW FINAL TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
(ft)(ml/min)(ft)(deg C)(umho/cm)(SU)(NTU)(mV-NHE)(mg/L)
WATER LEVEL RATE WATER LEVEL COND.OXYGEN
1.3 432 0.52 N/A
Tubing Volume Purged 0.75 GAL.EQUIPMENT PURGE ONLY SAMPLE CHLORINE
(mg/l)Pump (Bladder) Volume
65.53 N/A 15.32 194 5.59
0
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
SAMPLE COLLECTED BY DATE TIME
Total Purge Volume PSP /CMF 1/14/2016 0750
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
92.24 102.24
60 (psi)10 (sec)(sec)
(gal)
6.16 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-4D
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)740.58 MIDDLE OF WETTED SCREEN (ft toc)97.24
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)102.24 GS ELEV (ft msl)738.25 PUMP INTAKE DEPTH (ft TOC)101.74
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
28651 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)64.48 WATER COLUMN (ft)37.76 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)676.10 WELL VOLUME 6.16
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
6.25 NO 15.72 165 6.33 7.4 252
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
0.40
6.25 NO 15.75 171 6.38 3.0 223 0.25
6.25 NO 15.75 171 6.36 7.6 231 0.26
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
18.75 PSP / CMF 1/14/2016 0835 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
28.00 43.00
30 (psi)13 (sec)(sec)
(gal)
1.18 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-4R
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)713.87 MIDDLE OF WETTED SCREEN (ft toc)42.11
SCREEN LENGTH (ft)15.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)45.73 GS ELEV (ft msl)711.15 PUMP INTAKE DEPTH (ft TOC)45.23
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 7
28651 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
1.18
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)38.48 WATER COLUMN (ft)7.25 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)675.39 WELL VOLUME
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV -NEH)(mg/L)
1.25 NO 14.82 142 6.15 20.6 310
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
4.12
1.25 NO 14.83 130 6.09 29.5 317 4.93
1.25 NO 14.89 140 6.13 12.9 320 4.01
1.25 NO 14.46 134 6.12 8.8 311 4.27
1.25 NO 14.58 130 6.09 9.5 318 4.34
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
6.25 PSP / CMF 1/14/2016 1120 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
72.60 87.60
60 (psi)10 (sec)(sec)
(gal)
8.57 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-4DR
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)713.75 MIDDLE OF WETTED SCREEN (ft toc)82.90
SCREEN LENGTH (ft)15.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)90.40 GS ELEV (ft msl)711.15 PUMP INTAKE DEPTH (ft TOC)89.90
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 5
28651 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
8.57
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)37.84 WATER COLUMN (ft)52.56 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)675.91 WELL VOLUME
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV -NEH)(mg/L)
8.75 53.34 NO 15.19 131 6.89 5.1 300
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
4.44 6.04
6.00 NO 15.21 130 6.86 4.2 319 4.54
6.00 NO 15.18 129 6.82 4.3 298 4.44
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
20.75 PSP / CMF 1/14/2016 1145 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
23.45 38.45
25 (psi)13 (sec)(sec)
(gal)
1.93 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-11
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)722.60 MIDDLE OF WETTED SCREEN (ft toc)32.53
SCREEN LENGTH (ft)15.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)38.45 GS ELEV (ft msl)720.10 PUMP INTAKE DEPTH (ft TOC)37.95
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 7
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)26.61 WATER COLUMN (ft)11.84 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)695.99 WELL VOLUME 1.93
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
2.00 NO 14.39 19 5.03 15.0 515
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
4.32
2.00 35.28 NO 13.82 19 5.06 28.8 533 5.66 0.52
2.00 NO 14.34 21 5.01 9.8 534 2.99
0.75 NO 13.90 19 5.06 11.7 543 5.74
0.75 NO 13.87 19 5.07 22.2 536 5.71
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
7.50 LDC 1/14/2016 1045 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
91.55 101.55
50 (psi)8 (sec)(sec)
(gal)
12.02 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-11D
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)723.14 MIDDLE OF WETTED SCREEN (ft toc)96.55
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)101.55 GS ELEV (ft msl)720.84 PUMP INTAKE DEPTH (ft TOC)101.05
See note below PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 7
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)27.87 WATER COLUMN (ft)73.68 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)695.27 WELL VOLUME 12.02
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
12.50 49.85 NO 14.66 32 5.74 10.0 517
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
6.43 8.43
7.79
8.00 NO 14.79 32 5.70 4.9 520 6.59
8.50 53.81 NO 14.77 32 5.71 5.2 517 6.54
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
29.00 LDC 1/14/2016 1130 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
After initial well volume is removed - WL drops to 65 ft - recalculate well volume and use for subsequent readings.
14.49 29.49
18 (psi)14 (sec)(sec)
(gal)
2.94 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-12
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)724.81 MIDDLE OF WETTED SCREEN (ft toc)21.99
SCREEN LENGTH (ft)15.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)29.49 GS ELEV (ft msl)722.21 PUMP INTAKE DEPTH (ft TOC)28.99
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 6
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)11.46 WATER COLUMN (ft)18.03 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)713.35 WELL VOLUME 2.94
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
3.00 14.81 NO 13.51 21 4.96 6.1 566
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
5.91 2.39
3.00 NO 13.52 21 4.94 6.9 575 6.50
3.00 NO 13.50 20 4.94 7.0 564 6.04
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
9.00 LDC 1/14/2016 1250 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
58.42 68.42
35 (psi)10 (sec)(sec)
(gal)
7.25 (gal)
@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR CONVENTIONAL SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME MW-12D
MONITORING WELL INFORMATION
WELL DIAMETER (in)2 TOC ELEV (ft msl)724.77 MIDDLE OF WETTED SCREEN (ft toc)63.42
SCREEN LENGTH (ft)10.00 ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)68.42 GS ELEV (ft msl)722.21 PUMP INTAKE DEPTH (ft TOC)67.92
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE 10
26055 SAMPLING EQUIPMENT QED T1200 PURGE METHOD
TUBING DIAMETER (in)1/2 OD Conventional
7.25
DETECTED ODOR None CONVERSION FACTOR 0.1631
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)23.95 WATER COLUMN (ft)44.47 Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)700.82 WELL VOLUME
(gal)
PURGE WATER LEVEL
AFTER PURGE *
COMPLETE TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED WELL VOL
VOLUME EVACUATION COND.OXYGEN (recalculates on
current water
level)(mV-NHE)(mg/L)
7.25 45.78 NO 14.60 78 6.28 14.6 518
(ft)(YES/NO)(deg C)(umho/cm)(SU)(NTU)
8.17 3.69
3.75 NO 14.50 78 6.28 6.3 515 8.10
3.75 NO 14.63 78 6.23 15.3 515 8.13
CHLORINE (mg/l)SAMPLE COLLECTED BY DATE TIME
14.75 LDC 1/14/2016 1310 0
TOTAL PURGE
VOLUME
* Optional measurement to recalculate well
volume when purging results in substantial
drawdown of water column
COLLECT SAMPLE - SAMPLE CRITERIA SATISFIED
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING Good Condition
WELL PAD Good Condition
WELL CASING Good Condition
WELL TAG Good Tag
SAMPLING NOTES
0.00 0.00
N/A (psi)N/A (sec)(sec)
(gal)
(ft)=(in)@
QC By:
SITE NAME McGUIRE NUCLEAR STATION PERMIT #60-04 SITE ID N/A
DUKE ENERGY PROCEDURE NO 3175.2
GROUNDWATER MONITORING DATA SHEET
FOR NO PURGE SAMPLING
PROJECT NAME LANDFILL 1 GROUNDWATER MONITORING FIELD CREW LDC, PSP, CMF
SAMPLING DATE(s)14-Jan-2016 WELL/LOCATION NAME SW-1
MONITORING WELL INFORMATION
WELL DIAMETER (in)TOC ELEV (ft msl)N/A MIDDLE OF WETTED SCREEN (ft toc)
SCREEN LENGTH (ft)ELEV REF NAVD 88 SCREEN INTERVAL (ft TOC)TO
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
WELL DEPTH (ft TOC)GS ELEV (ft msl)PUMP INTAKE DEPTH (ft TOC)N/A
PUMP CONTROLLER SETTINGS
PRESSURE RECHARGE DISCHARGE N/A
N/A SAMPLING EQUIPMENT PERISTALTIC PUMP PURGE METHOD
TUBING DIAMETER (in)3/8 OD No Purge
DETECTED ODOR None CONVERSION FACTOR
APPEARANCE Normal
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)N/A WATER COLUMN (ft)Well Volume = water column X conversion factor
(Conversion factor dependent on well diameter
and selected well volume units)
WATER ELEVATION (ft msl)WELL VOLUME
TEMP SPECIFIC pH TURBIDITY ORP DISSOLVED
TIME
PSP / CMF 1/14/2016
LENGTH DEPTH (top)DEPLOYED COND.OXYGEN
(inches)(ft TOC)(deg C)(umho/cm)(SU)
HYDRASLEEVE DEPLOYED DATE
(NTU)(mV-NHE)(mg/L)
N/A N/A N/A 8.54 87 6.54 25.6
1220
211 10.17
0
N/A
Deployed Water Column In Screen
Above Top Of Hydrasleeve
NO PURGE SAMPLE CHLORINE
(mg/l)Top Weight SAMPLE COLLECTED BY DATE
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
Sample preservation verified to pH
(units)< 2.0
PROTECTIVE CASING
WELL PAD
WELL CASING
WELL TAG
SAMPLING NOTES
PERMIT #
MW-1 MW-1D MW-2 MW-2D MW-3 MW-3D MW-4 MW-4D MW-11 MW-11D MW-12 MW-12D SW-1 MW-4R MW-4PR
YES YES YES YES YES YES YES YES YES YES YES YES YES YES YES
YES YES YES YES YES YES YES YES YES YES YES YES YES YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
YES YES YES YES YES YES YES YES YES YES YES YES N/A YES YES
Lacks required information - Total well depth
Lacks required information - Depth to screen
Lacks required information - Non potable tag
NOTE:
Lacks required information - Completion date
FLUSH MOUNT WELLS
Vault in good condition
Water inside vault
Vault bolt holes broken or stripped
Bolts stripped
Vault lid cracked or broken
WELL ID TAGS
Well tag in good condition
Well tag missing
Well tag damaged / illegible
Lacks required information - Driller Reg #
Replaced damaged well cap
Fire ants around concrete pad
WELL PROTECTIVE CASINGS
Casing in good condition
Damaged casing / still functional
Damaged casing / repair required
Broken hinge on protective lid
Wasp nest inside protective casing
Ants inside protective casing
WELL CAPS
Well cap in good conditon
Damaged / needs replacement
Undermined / washing out
Lock in good condition
Lock rusted, difficult to open / needs replacing
Replaced damaged lock
WELL CASINGS
Casing in good condition
Damaged casing / still functional
Damaged casing / repair required
CONCRETE PADS
Pad in good condition
Minor cracks
Major cracks / broken / repair required
WELL LOCK CONDITION
PAGE 1 OF 1
ACCESS TO WELLS
Access cleared into well
Access cleared around well
Tall grass or weeds - needs mowing
Road washing out / muddy / needs grading
Fallen tree blocking access
WELL SECURITY
Well found locked
Well found unlocked
SITE CONTACT John Williamson, Bill Spencer FIELD CREW LDC, PSP, CMF
WEATHER Clear, calm, 25 to 60 deg F.
NORTH CAROLINA GROUNDWATER SAMPLING SITE CHECKLIST
LOCATION / SITE McGUIRE NUCLEAR STATION - LANDFILL #1 GROUNDWATER MONITORING 60-04 SAMPLE DATE January 14, 2016
WELL DEPTH TO WATER Purge AVG *WELL EVAC SPECIFIC
WELL DEPTH WATER ELEV.Method PMP RATE VOL VOL EVAC TEMP CONDUCTANCE pH TURBIDITY ORP DODATENO.(feet-toc)(feet-toc)(feet)APPEARANCE ODOR (ml/min)(gal)(gal)(yes/no)(deg C)(umho/cm)(units)(NTU)(mV-NHE)(mg/l)
1/14/2016 MW-1 68.55 27.75 702.48 Normal None C N/A 6.65 20.25 NO 15.20 114 6.1 6.6 228 0.00
1/14/2016 MW-1D 88.22 28.84 701.77 Normal None C N/A 9.68 29.25 NO 15.47 105 6.1 2.8 226 0.00
1/14/2016 MW-2A 77.57 53.19 686.48 Normal None C N/A 3.98 6.50 NO 16.52 86 6.4 2.1 390 4.49
1/14/2016 MW-2D 108.82 54.40 686.37 Normal None C N/A 8.88 18.50 NO 16.40 61 7.0 2.4 329 9.69
1/14/2016 MW-3 73.64 57.13 671.30 Normal None C N/A 2.69 13.75 NO 14.92 81 6.4 1.6 386 5.61
1/14/2016 MW-3D 90.19 57.08 671.31 Normal None C N/A 5.40 16.50 NO 15.06 127 6.6 1.1 343 1.72
1/14/2016 MW-4 74.15 65.53 675.60 Normal None EOP N/A 1.41 0.55 N/A 15.32 194 5.6 1.3 432 0.52
1/14/2016 MW-4D 102.24 64.48 676.10 Normal None C N/A 6.16 18.75 NO 15.75 171 6.4 3.0 223 0.25
1/14/2016 MW-11 38.45 26.61 695.99 Normal None C N/A 1.93 7.50 NO 13.90 19 5.1 11.7 543 5.74
1/14/2016 MW-11D 101.55 27.87 695.27 Normal None C N/A 12.02 29.00 NO 14.79 32 5.7 4.9 520 6.59
1/14/2016 MW-12 29.49 11.46 713.35 Normal None C N/A 2.94 9.00 NO 13.52 21 4.9 6.9 575 6.50
1/14/2016 MW-12D 68.42 23.95 700.82 Normal None C N/A 7.25 14.75 NO 14.50 78 6.3 6.3 515 8.10
1/14/2016 SW-1 N/A N/A N/A Normal None NP N/A N/A N/A N/A 8.54 87 6.5 25.6 211 10.17
1/14/2016 MW-4R 45.73 38.48 675.39 Normal None C N/A 1.18 6.25 NO 14.46 134 6.1 8.8 311 4.27
1/14/2016 MW-4DR 90.40 37.84 675.91 Normal None C N/A 8.57 20.75 NO 15.21 130 6.9 4.2 319 4.54
Purge Methods
LF = Low Flow
LF(M) = Low Flow (Mod.)
C = Connventional
NP = No Purge
EOP = Equip. Only Purge
LO = Level Only
* = Applicable to LF & LF(M) Purging Only
McGUIRE NUCLEAR STATION
LANDFILL 1 GROUNDWATER MONITORING
GROUNDWATER MONITORING FIELD DATA
PERMIT #60-04

B
Appendix B
Laboratory Report and
Chain-of-Custody Forms

13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J16010006
Project Name:MCGUIRE - GW LF1
Lab Contact:Peggy Kendall
Date:2/5/2016
Customer Address:13225 Hagers Ferry Rd
Customer Name(s):TIM HUNSUCKER, CHUCK CAMPBELL
Mail Code: MG01CH
Huntersville, NC 28078-8985
Phone:
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Peggy Kendall) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Peggy Kendall
Page 1 of 90
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2016000037 MCGUIRE 14-Jan-16 5:35 AM LDC TRIP BLANK
2016000038 MCGUIRE 14-Jan-16 8:50 AM LDC MW-1
2016000039 MCGUIRE 14-Jan-16 9:05 AM LDC MW-1D
2016000040 MCGUIRE 14-Jan-16 1:30 PM PSP MW-2A
2016000041 MCGUIRE 14-Jan-16 2:25 PM PSP MW-2D
2016000042 MCGUIRE 14-Jan-16 10:00 AM PSP MW-3
2016000043 MCGUIRE 14-Jan-16 10:20 AM PSP MW-3D
2016000044 MCGUIRE 14-Jan-16 7:50 AM PSP MW-4
2016000045 MCGUIRE 14-Jan-16 8:35 AM PSP MW-4D
2016000046 MCGUIRE 14-Jan-16 10:45 AM LDC MW-11
2016000047 MCGUIRE 14-Jan-16 11:30 AM LDC MW-11D
2016000048 MCGUIRE 14-Jan-16 12:50 PM LDC MW-12
2016000049 MCGUIRE 14-Jan-16 1:10 PM LDC MW-12D
2016000050 MCGUIRE 14-Jan-16 12:20 PM PSP SW-1
2016000051 MCGUIRE 14-Jan-16 11:20 AM PSP MW-4R
2016000052 MCGUIRE 14-Jan-16 11:45 AM PSP MW-4DR
2016000053 MCGUIRE 14-Jan-16 2:45 PM PSP FIELD BLANK
17 Total Samples
Page 2 of 90
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:2/5/2016
Electronic Data Deliverable (EDD) Sent Separatel
Page 3 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000037
Collection Date:14-Jan-16 5:35 AM
Site:TRIP BLANK
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 4 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000038
Collection Date:14-Jan-16 8:50 AM
Site:MW-1
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)54 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 1.8 mg/L EPA 9056A 01/25/2016 22:54 BGN90340.1 1
Sulfate 0.31 mg/L EPA 9056A 01/25/2016 22:54 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/28/2016 11:24 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.218 mg/L SW 6010C 01/19/2016 13:01 MHH71310.005 1
Calcium (Ca)6.81 mg/L SW 6010C 01/19/2016 13:01 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 13:01 MHH71310.005 1
Magnesium (Mg)3.13 mg/L SW 6010C 01/19/2016 13:01 MHH71310.005 1
Potassium (K)1.15 mg/L SW 6010C 01/19/2016 13:01 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 13:01 MHH71310.005 1
Sodium (Na)5.96 mg/L SW 6010C 01/19/2016 13:01 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 15:13 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 15:13 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 15:13 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 15:13 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 5 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000039
Collection Date:14-Jan-16 9:05 AM
Site:MW-1D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)50 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 1.6 mg/L EPA 9056A 01/25/2016 23:45 BGN90340.1 1
Sulfate 0.34 mg/L EPA 9056A 01/25/2016 23:45 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/28/2016 11:34 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.103 mg/L SW 6010C 01/19/2016 13:14 MHH71310.005 1
Calcium (Ca)7.31 mg/L SW 6010C 01/19/2016 13:14 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 13:14 MHH71310.005 1
Magnesium (Mg)2.54 mg/L SW 6010C 01/19/2016 13:14 MHH71310.005 1
Potassium (K)1.08 mg/L SW 6010C 01/19/2016 13:14 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 13:14 MHH71310.005 1
Sodium (Na)6.60 mg/L SW 6010C 01/19/2016 13:14 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 14:43 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 14:43 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 14:43 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 14:43 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 6 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000040
Collection Date:14-Jan-16 1:30 PM
Site:MW-2A
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)37 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 1.4 mg/L EPA 9056A 01/26/2016 00:02 BGN90340.1 1
Sulfate 0.44 mg/L EPA 9056A 01/26/2016 00:02 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/29/2016 13:21 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.026 mg/L SW 6010C 01/19/2016 13:18 MHH71310.005 1
Calcium (Ca)8.27 mg/L SW 6010C 01/19/2016 13:18 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 13:18 MHH71310.005 1
Magnesium (Mg)2.36 mg/L SW 6010C 01/19/2016 13:18 MHH71310.005 1
Potassium (K)0.401 mg/L SW 6010C 01/19/2016 13:18 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 13:18 MHH71310.005 1
Sodium (Na)5.79 mg/L SW 6010C 01/19/2016 13:18 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 15:17 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 15:17 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 15:17 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 15:17 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 7 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000041
Collection Date:14-Jan-16 2:25 PM
Site:MW-2D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)25 mg/L
(CaCO3)
SM 2320B4d 01/19/2016 11:28 GHUTCHI51
INORGANIC IONS BY IC
Chloride 1.2 mg/L EPA 9056A 01/26/2016 00:19 BGN90340.1 1
Sulfate 0.38 mg/L EPA 9056A 01/26/2016 00:19 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/29/2016 13:23 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.015 mg/L SW 6010C 01/19/2016 13:22 MHH71310.005 1
Calcium (Ca)5.24 mg/L SW 6010C 01/19/2016 13:22 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 13:22 MHH71310.005 1
Magnesium (Mg)1.53 mg/L SW 6010C 01/19/2016 13:22 MHH71310.005 1
Potassium (K)0.650 mg/L SW 6010C 01/19/2016 13:22 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 13:22 MHH71310.005 1
Sodium (Na)5.25 mg/L SW 6010C 01/19/2016 13:22 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 15:22 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 15:22 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 15:22 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 15:22 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 8 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000042
Collection Date:14-Jan-16 10:00 AM
Site:MW-3
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)39 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 1.5 mg/L EPA 9056A 01/26/2016 00:36 BGN90340.1 1
Sulfate 0.52 mg/L EPA 9056A 01/26/2016 00:36 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/28/2016 11:41 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.038 mg/L SW 6010C 01/19/2016 13:26 MHH71310.005 1
Calcium (Ca)7.36 mg/L SW 6010C 01/19/2016 13:26 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 13:26 MHH71310.005 1
Magnesium (Mg)3.08 mg/L SW 6010C 01/19/2016 13:26 MHH71310.005 1
Potassium (K)0.773 mg/L SW 6010C 01/19/2016 13:26 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 13:26 MHH71310.005 1
Sodium (Na)4.03 mg/L SW 6010C 01/19/2016 13:26 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 15:27 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 15:27 MHALL311
Lead (Pb)1.10 ug/L SW 6020A 01/17/2016 15:27 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 15:27 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 9 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000043
Collection Date:14-Jan-16 10:20 AM
Site:MW-3D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)63 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 1.6 mg/L EPA 9056A 01/26/2016 00:53 BGN90340.1 1
Sulfate 1.0 mg/L EPA 9056A 01/26/2016 00:53 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/29/2016 13:25 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.027 mg/L SW 6010C 01/19/2016 13:30 MHH71310.005 1
Calcium (Ca)13.1 mg/L SW 6010C 01/19/2016 13:30 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 13:30 MHH71310.005 1
Magnesium (Mg)4.45 mg/L SW 6010C 01/19/2016 13:30 MHH71310.005 1
Potassium (K)0.839 mg/L SW 6010C 01/19/2016 13:30 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 13:30 MHH71310.005 1
Sodium (Na)6.26 mg/L SW 6010C 01/19/2016 13:30 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 15:32 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 15:32 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 15:32 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 15:32 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 10 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000044
Collection Date:14-Jan-16 7:50 AM
Site:MW-4
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)83 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 1.8 mg/L EPA 9056A 01/26/2016 01:10 BGN90340.1 1
Sulfate 0.94 mg/L EPA 9056A 01/26/2016 01:10 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/29/2016 13:28 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.074 mg/L SW 6010C 01/19/2016 13:34 MHH71310.005 1
Calcium (Ca)13.3 mg/L SW 6010C 01/19/2016 13:34 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 13:34 MHH71310.005 1
Magnesium (Mg)12.3 mg/L SW 6010C 01/19/2016 13:34 MHH71310.005 1
Potassium (K)0.750 mg/L SW 6010C 01/19/2016 13:34 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 13:34 MHH71310.005 1
Sodium (Na)2.28 mg/L SW 6010C 01/19/2016 13:34 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 15:37 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 15:37 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 15:37 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 15:37 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 11 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000045
Collection Date:14-Jan-16 8:35 AM
Site:MW-4D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)88 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 1.7 mg/L EPA 9056A 01/27/2016 11:31 BGN90340.1 1
Sulfate 0.24 mg/L EPA 9056A 01/27/2016 11:31 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/29/2016 13:30 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.045 mg/L SW 6010C 01/19/2016 13:38 MHH71310.005 1
Calcium (Ca)17.7 mg/L SW 6010C 01/19/2016 13:38 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 13:38 MHH71310.005 1
Magnesium (Mg)7.91 mg/L SW 6010C 01/19/2016 13:38 MHH71310.005 1
Potassium (K)0.589 mg/L SW 6010C 01/19/2016 13:38 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 13:38 MHH71310.005 1
Sodium (Na)4.09 mg/L SW 6010C 01/19/2016 13:38 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 15:42 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 15:42 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 15:42 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 15:42 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 12 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000046
Collection Date:14-Jan-16 10:45 AM
Site:MW-11
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)< 5 mg/L
(CaCO3)
SM 2320B4d 01/19/2016 11:28 GHUTCHI51
INORGANIC IONS BY IC
Chloride 1.4 mg/L EPA 9056A 01/27/2016 11:48 BGN90340.1 1
Sulfate 0.42 mg/L EPA 9056A 01/27/2016 11:48 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/29/2016 13:51 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.006 mg/L SW 6010C 01/19/2016 13:42 MHH71310.005 1
Calcium (Ca)0.861 mg/L SW 6010C 01/19/2016 13:42 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 13:42 MHH71310.005 1
Magnesium (Mg)0.722 mg/L SW 6010C 01/19/2016 13:42 MHH71310.005 1
Potassium (K)< 0.1 mg/L SW 6010C 01/19/2016 13:42 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 13:42 MHH71310.005 1
Sodium (Na)1.08 mg/L SW 6010C 01/19/2016 13:42 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 15:47 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 15:47 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 15:47 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 15:47 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 13 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000047
Collection Date:14-Jan-16 11:30 AM
Site:MW-11D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)10 mg/L
(CaCO3)
SM 2320B4d 01/19/2016 11:28 GHUTCHI51
INORGANIC IONS BY IC
Chloride 1.4 mg/L EPA 9056A 01/27/2016 12:06 BGN90340.1 1
Sulfate 0.81 mg/L EPA 9056A 01/27/2016 12:06 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/28/2016 11:39 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.011 mg/L SW 6010C 01/19/2016 13:55 MHH71310.005 1
Calcium (Ca)1.55 mg/L SW 6010C 01/19/2016 13:55 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 13:55 MHH71310.005 1
Magnesium (Mg)0.931 mg/L SW 6010C 01/19/2016 13:55 MHH71310.005 1
Potassium (K)0.160 mg/L SW 6010C 01/19/2016 13:55 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 13:55 MHH71310.005 1
Sodium (Na)3.45 mg/L SW 6010C 01/19/2016 13:55 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 16:21 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 16:21 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 16:21 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 16:21 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 14 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000048
Collection Date:14-Jan-16 12:50 PM
Site:MW-12
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)< 5 mg/L
(CaCO3)
SM 2320B4d 01/19/2016 11:28 GHUTCHI51
INORGANIC IONS BY IC
Chloride 3.9 mg/L EPA 9056A 01/27/2016 12:24 BGN90340.1 1
Sulfate 0.15 mg/L EPA 9056A 01/27/2016 12:24 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/28/2016 11:46 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.007 mg/L SW 6010C 01/19/2016 14:07 MHH71310.005 1
Calcium (Ca)0.580 mg/L SW 6010C 01/19/2016 14:07 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 14:07 MHH71310.005 1
Magnesium (Mg)0.415 mg/L SW 6010C 01/19/2016 14:07 MHH71310.005 1
Potassium (K)0.332 mg/L SW 6010C 01/19/2016 14:07 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 14:07 MHH71310.005 1
Sodium (Na)1.52 mg/L SW 6010C 01/19/2016 14:07 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 15:52 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 15:52 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 15:52 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 15:52 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 15 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000049
Collection Date:14-Jan-16 1:10 PM
Site:MW-12D
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)36 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 2.8 mg/L EPA 9056A 01/27/2016 12:42 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 9056A 01/27/2016 12:42 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/28/2016 11:51 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.009 mg/L SW 6010C 01/19/2016 14:11 MHH71310.005 1
Calcium (Ca)7.65 mg/L SW 6010C 01/19/2016 14:11 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 14:11 MHH71310.005 1
Magnesium (Mg)1.22 mg/L SW 6010C 01/19/2016 14:11 MHH71310.005 1
Potassium (K)0.291 mg/L SW 6010C 01/19/2016 14:11 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 14:11 MHH71310.005 1
Sodium (Na)7.62 mg/L SW 6010C 01/19/2016 14:11 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 16:26 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 16:26 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 16:26 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 16:26 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 16 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000050
Collection Date:14-Jan-16 12:20 PM
Site:SW-1
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)37 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 2.5 mg/L EPA 9056A 01/27/2016 13:00 BGN90340.1 1
Sulfate 2.9 mg/L EPA 9056A 01/27/2016 13:00 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/28/2016 11:36 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.034 mg/L SW 6010C 01/19/2016 14:15 MHH71310.005 1
Calcium (Ca)7.70 mg/L SW 6010C 01/19/2016 14:15 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 14:15 MHH71310.005 1
Magnesium (Mg)3.30 mg/L SW 6010C 01/19/2016 14:15 MHH71310.005 1
Potassium (K)1.02 mg/L SW 6010C 01/19/2016 14:15 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 14:15 MHH71310.005 1
Sodium (Na)4.54 mg/L SW 6010C 01/19/2016 14:15 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 16:31 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 16:31 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 16:31 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 16:31 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 17 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000051
Collection Date:14-Jan-16 11:20 AM
Site:MW-4R
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)67 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 2.2 mg/L EPA 9056A 01/27/2016 13:18 BGN90340.1 1
Sulfate 0.34 mg/L EPA 9056A 01/27/2016 13:18 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/28/2016 11:48 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.013 mg/L SW 6010C 01/19/2016 14:19 MHH71310.005 1
Calcium (Ca)11.6 mg/L SW 6010C 01/19/2016 14:19 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 14:19 MHH71310.005 1
Magnesium (Mg)8.82 mg/L SW 6010C 01/19/2016 14:19 MHH71310.005 1
Potassium (K)0.351 mg/L SW 6010C 01/19/2016 14:19 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 14:19 MHH71310.005 1
Sodium (Na)2.82 mg/L SW 6010C 01/19/2016 14:19 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 16:36 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 16:36 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 16:36 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 16:36 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 18 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000052
Collection Date:14-Jan-16 11:45 AM
Site:MW-4DR
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY (FIXED END POINT 4.5)
Alkalinity (mg/L CaCO3)65 mg/L
(CaCO3)
SM 2320B 01/16/2016 10:52 GHUTCHI201
INORGANIC IONS BY IC
Chloride 1.8 mg/L EPA 9056A 01/27/2016 13:36 BGN90340.1 1
Sulfate 1.5 mg/L EPA 9056A 01/27/2016 13:36 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/29/2016 13:35 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)0.013 mg/L SW 6010C 01/19/2016 14:23 MHH71310.005 1
Calcium (Ca)14.2 mg/L SW 6010C 01/19/2016 14:23 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 14:23 MHH71310.005 1
Magnesium (Mg)4.40 mg/L SW 6010C 01/19/2016 14:23 MHH71310.005 1
Potassium (K)0.829 mg/L SW 6010C 01/19/2016 14:23 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 14:23 MHH71310.005 1
Sodium (Na)6.61 mg/L SW 6010C 01/19/2016 14:23 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 16:41 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 16:41 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 16:41 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 16:41 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 19 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
2016000053
Collection Date:14-Jan-16 2:45 PM
Site:FIELD BLANK
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
LOW LEVEL ALKALINITY (FIXED END POINT)
Alkalinity (mg/L CaCO3)< 5 mg/L
(CaCO3)
SM 2320B4d 01/19/2016 11:28 GHUTCHI51
INORGANIC IONS BY IC
Chloride < 0.1 mg/L EPA 9056A 01/27/2016 13:54 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 9056A 01/27/2016 13:54 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 7470 01/28/2016 11:44 ACPAYNE0.05 1
TOTAL RECOVERABLE METALS BY ICP
Barium (Ba)< 0.005 mg/L SW 6010C 01/19/2016 14:27 MHH71310.005 1
Calcium (Ca)0.013 mg/L SW 6010C 01/19/2016 14:27 MHH71310.01 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/19/2016 14:27 MHH71310.005 1
Magnesium (Mg)< 0.005 mg/L SW 6010C 01/19/2016 14:27 MHH71310.005 1
Potassium (K)< 0.1 mg/L SW 6010C 01/19/2016 14:27 MHH71310.1 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/19/2016 14:27 MHH71310.005 1
Sodium (Na)< 0.05 mg/L SW 6010C 01/19/2016 14:27 MHH71310.05 1
TOTAL RECOVERABLE METALS BY ICP-MS
Arsenic (As)< 1 ug/L SW 6020A 01/17/2016 16:45 MHALL311
Cadmium (Cd)< 1 ug/L SW 6020A 01/17/2016 16:45 MHALL311
Lead (Pb)< 1 ug/L SW 6020A 01/17/2016 16:45 MHALL311
Selenium (Se)< 1 ug/L SW 6020A 01/17/2016 16:45 MHALL311
VOLATILES - (Analysis Performed by Test America)
Vendor Parameter Complete Vendor Method V_T. America
Page 20 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
Q16010352 ALK_FIX4.5 ALKALINITY (FIXED END POINT 4.5)
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Duplicate # 1
RPD
Parent Sample: J16010006 -- 2016000038
Alkalinity (mg/L CaCO3)0.492mg/L
(CaCO3)
-154.2
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Alkalinity (mg/L CaCO3)81.6 100mg/L
(CaCO3)
-12080181.7
Page 21 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
Q16010399 ALK_LL_Fix LOW LEVEL ALKALINITY (FIXED END POINT)
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Duplicate # 1
RPD
Parent Sample: J16010004 -- 2016000005
Alkalinity (mg/L CaCO3)7.29mg/L
(CaCO3)
-112.8
Final QualifierDilMeasuredUnits:Parameter
Duplicate # 2
RPD
Parent Sample: J16010004 -- 2016000020
Alkalinity (mg/L CaCO3)4mg/L
(CaCO3)
-19.09
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Alkalinity (mg/L CaCO3)8.16 94.6mg/L
(CaCO3)
-1208017.72
Final QualifierDilMeasuredUnits:Parameter
LCS # 2
% Recovery LCL UCLSpike
Alkalinity (mg/L CaCO3)8.16 85mg/L
(CaCO3)
-1208016.94
Page 22 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
Q16010494 Dionex INORGANIC IONS BY IC
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Chloride 0.0155 mg/L -10.0155 0.1 < 1/2 RDL
Sulfate -0.0406 mg/L -1-0.0406 0.1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
IS # 1
% Recovery LCL UCLSpike
Chloride 8.89 5 98.4mg/L -1208018.89
Sulfate 7.34 5 96.8mg/L -1208017.34
Final QualifierDilMeasuredUnits:Parameter
ISD # 1
RPD% Recovery LCL UCLSpike
Chloride 8.89 5 98.4 0.0752mg/L -1208018.89
Sulfate 7.34 5 96.9 0.109mg/L -1208017.34
Final QualifierDilMeasuredUnits:Parameter
IS # 2
% Recovery LCL UCLSpike
Chloride 9.26 5 99.8mg/L -1208019.26
Sulfate 7.61 5 102mg/L -1208017.61
Final QualifierDilMeasuredUnits:Parameter
ISD # 2
RPD% Recovery LCL UCLSpike
Chloride 9.26 5 99.7 0.114mg/L -1208019.26
Sulfate 7.63 5 103 0.3mg/L -1208017.63
Final QualifierDilMeasuredUnits:Parameter
IS # 3
% Recovery LCL UCLSpike
Chloride 7.06 5 105mg/L -1208017.06
Sulfate 5.72 5 108mg/L -1208015.72
Final QualifierDilMeasuredUnits:Parameter
ISD # 3
RPD% Recovery LCL UCLSpike
Chloride 7.02 5 104 0.655mg/L -1208017.02
Sulfate 5.73 5 108 0.166mg/L -1208015.73
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Chloride 4.94 5 98.9mg/L -1208014.94
Sulfate 5.08 5 102mg/L -1208015.08
Page 23 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
Q16010563 Dionex INORGANIC IONS BY IC
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Chloride 0.0174 mg/L -10.0174 0.1 < 1/2 RDL
Sulfate -0.0417 mg/L -1-0.0417 0.1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
IS # 1
% Recovery LCL UCLSpike
Chloride 8.71 5 100mg/L -1208018.71
Sulfate 7.76 5 101mg/L -1208017.76
Final QualifierDilMeasuredUnits:Parameter
ISD # 1
RPD% Recovery LCL UCLSpike
Chloride 8.75 5 101 0.789mg/L -1208018.75
Sulfate 7.78 5 101 0.367mg/L -1208017.78
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Chloride 5.01 5 100mg/L -1208015.01
Sulfate 5.14 5 103mg/L -1208015.14
Page 24 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
Q16010557 HG 7470 MERCURY (COLD VAPOR) IN WATER
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Mercury (Hg) 0.016 ug/L -10.016 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Mercury (Hg) 2.03 2 102ug/L -1158512.03
Mercury (Hg) 2.03 2 102ug/L -1208012.03
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16010004 -- 2016000008
Mercury (Hg) 1.03 1 100ug/L -1307011.03
Mercury (Hg) 1.03 1 100ug/L -1257511.03
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16010004 -- 2016000008
Mercury (Hg) 1.03 1 101 0.797ug/L -1307011.03
Mercury (Hg) 1.03 1 101 0.797ug/L -1257511.03
Final QualifierDilMeasuredUnits:Parameter
MS # 2
% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000038
Mercury (Hg) 0.993 1 97.9ug/L -1257510.993
Mercury (Hg) 0.993 1 97.9ug/L -1307010.993
Final QualifierDilMeasuredUnits:Parameter
MSD # 2
RPD% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000038
Mercury (Hg) 0.999 1 98.5 0.611ug/L -1257510.999
Mercury (Hg) 0.999 1 98.5 0.611ug/L -1307010.999
Page 25 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
Q16010608 HG 7470 MERCURY (COLD VAPOR) IN WATER
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Mercury (Hg)ug/L -10.002 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Mercury (Hg)2 92.2ug/L -1208011.84
Mercury (Hg)2 92.2ug/L -1158511.84
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16010004 -- 2016000024
Mercury (Hg)1 91.3ug/L -1307010.93
Mercury (Hg)1 91.3ug/L -1257510.93
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16010004 -- 2016000024
Mercury (Hg)1 95.3 4.29ug/L -1257510.97
Mercury (Hg)1 95.3 4.29ug/L -1307010.97
Page 26 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
Q16010330 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Barium (Ba) -0.000063 mg/L -1-0.000063 0.005 < 1/2 RDL
Calcium (Ca) 0.00289 mg/L -10.00289 0.01 < 1/2 RDL
Chromium (Cr) -0.000024 mg/L -1-0.000024 0.005 < 1/2 RDL
Magnesium (Mg) 0.000403 mg/L -10.000403 0.005 < 1/2 RDL
Potassium (K) -0.00872 mg/L -1-0.00872 0.1 < 1/2 RDL
Silver (Ag) -0.000011 mg/L -1-0.000011 0.005 < 1/2 RDL
Sodium (Na) -0.00902 mg/L -1-0.00902 0.05 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Barium (Ba) 5.05 5 101mg/L -1208015.05
Calcium (Ca) 4.91 5 98.2mg/L -1208014.91
Chromium (Cr) 4.93 5 98.5mg/L -1208014.93
Magnesium (Mg) 4.98 5 99.6mg/L -1208014.98
Potassium (K) 4.89 5 97.9mg/L -1208014.89
Silver (Ag) 0.476 0.5 95.2mg/L -1208010.476
Sodium (Na) 4.91 5 98.2mg/L -1208014.91
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000038
Barium (Ba) 5.16 5 98.9mg/L -1257515.16
Calcium (Ca) 11.5 5 93.8mg/L -12575111.5
Chromium (Cr) 4.81 5 96.3mg/L -1257514.81
Magnesium (Mg) 7.84 5 94.3mg/L -1257517.84
Potassium (K) 5.96 5 96.1mg/L -1257515.96
Silver (Ag) 0.462 0.5 92.4mg/L -1257510.462
Sodium (Na) 10.8 5 97.4mg/L -12575110.8
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000038
Barium (Ba) 5.2 5 99.7 0.826mg/L -1257515.2
Calcium (Ca) 11.8 5 98.9 5.25mg/L -12575111.8
Chromium (Cr) 4.88 5 97.6 1.4mg/L -1257514.88
Magnesium (Mg) 7.99 5 97.3 3.15mg/L -1257517.99
Potassium (K) 6.05 5 98 1.94mg/L -1257516.05
Silver (Ag) 0.469 0.5 93.9 1.64mg/L -1257510.469
Sodium (Na) 11 5 101 3.55mg/L -12575111
Final QualifierDilMeasuredUnits:Parameter
MS # 2
% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000047
Barium (Ba) 5.06 5 101mg/L -1257515.06
Page 27 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
Q16010330 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
MS # 2
% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000047
Calcium (Ca) 6.58 5 101mg/L -1257516.58
Chromium (Cr) 5 5 100mg/L -1257515
Magnesium (Mg) 5.95 5 100mg/L -1257515.95
Potassium (K) 5.12 5 99.2mg/L -1257515.12
Silver (Ag) 0.477 0.5 95.4mg/L -1257510.477
Sodium (Na) 8.45 5 100mg/L -1257518.45
Final QualifierDilMeasuredUnits:Parameter
MSD # 2
RPD% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000047
Barium (Ba) 5.12 5 102 1.1mg/L -1257515.12
Calcium (Ca) 6.62 5 101 0.693mg/L -1257516.62
Chromium (Cr) 5.02 5 100 0.259mg/L -1257515.02
Magnesium (Mg) 5.96 5 101 0.298mg/L -1257515.96
Potassium (K) 5.17 5 100 0.903mg/L -1257515.17
Silver (Ag) 0.482 0.5 96.4 1.02mg/L -1257510.482
Sodium (Na) 8.61 5 103 3.13mg/L -1257518.61
Page 28 of 90
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010006
Q16010334 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Arsenic (As) 0.0056 ug/L -10.0056 1 < 1/2 RDL
Cadmium (Cd) 0.0016 ug/L -10.0016 1 < 1/2 RDL
Lead (Pb) -0.0005 ug/L -1-0.0005 1 < 1/2 RDL
Selenium (Se) 0.0138 ug/L -10.0138 1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Arsenic (As) 52.2 50 104ug/L -12080152.2
Cadmium (Cd) 50.5 50 101ug/L -12080150.5
Lead (Pb) 48.2 50 96.4ug/L -12080148.2
Selenium (Se) 52.3 50 105ug/L -12080152.3
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000039
Arsenic (As) 51.6 50 103ug/L -12080151.6
Cadmium (Cd) 50.1 50 100ug/L -12080150.1
Lead (Pb) 48.3 50 96.5ug/L -12080148.3
Selenium (Se) 51.7 50 103ug/L -12080151.7
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000039
Arsenic (As) 52.8 50 105 2.34ug/L -12080152.8
Cadmium (Cd) 51.5 50 103 2.81ug/L -12080151.5
Lead (Pb) 49.4 50 98.8 2.39ug/L -12080149.4
Selenium (Se) 48.8 50 97.6 5.81ug/L -12080148.8
Final QualifierDilMeasuredUnits:Parameter
MS # 2
% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000048
Arsenic (As) 50.7 50 101ug/L -12080150.7
Cadmium (Cd) 49.9 50 99.8ug/L -12080149.9
Lead (Pb) 48.4 50 96.6ug/L -12080148.4
Selenium (Se) 49.5 50 98.9ug/L -12080149.5
Final QualifierDilMeasuredUnits:Parameter
MSD # 2
RPD% Recovery LCL UCLSpike
Parent Sample: J16010006 -- 2016000048
Arsenic (As) 51.2 50 102 0.942ug/L -12080151.2
Cadmium (Cd) 50.3 50 101 0.81ug/L -12080150.3
Lead (Pb) 49.2 50 98.3 1.68ug/L -12080149.2
Selenium (Se) 50 50 100 1.03ug/L -12080150
Page 29 of 90
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-95901-1
Client Project/Site: MNS Landfill #1 J16010006
For:
Duke Energy Corporation
13339 Hagers Ferry Road
Huntersville, North Carolina 28078
Attn: Lab Customer
Authorized for release by:
1/29/2016 3:28:50 PM
Shali Brown, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
TestAmerica Job ID: 490-95901-1
Page 2 of 60 TestAmerica Nashville1/29/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .56
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .57
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .60
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Sample Summary
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-95901-1 TRIPBLANK Water 01/14/16 05:35 01/16/16 09:20
490-95901-2 MW-1 Water 01/14/16 08:50 01/16/16 09:20
490-95901-3 MW-1D Water 01/14/16 09:05 01/16/16 09:20
490-95901-4 MW-2A Water 01/14/16 13:30 01/16/16 09:20
490-95901-5 MW-2D Water 01/14/16 14:25 01/16/16 09:20
490-95901-6 MW-3 Water 01/14/16 10:00 01/16/16 09:20
490-95901-7 MW-3D Water 01/14/16 10:20 01/16/16 09:20
490-95901-8 MW-4 Water 01/14/16 07:50 01/16/16 09:20
490-95901-9 MW-4D Water 01/14/16 08:35 01/16/16 09:20
490-95901-10 MW-11 Water 01/14/16 10:45 01/16/16 09:20
490-95901-11 MW-11D Water 01/14/16 11:30 01/16/16 09:20
490-95901-12 MW-12 Water 01/14/16 12:50 01/16/16 09:20
490-95901-13 MW-12D Water 01/14/16 13:10 01/16/16 09:20
490-95901-14 SW-1 Water 01/14/16 12:20 01/16/16 09:20
490-95901-15 MW-4R Water 01/14/16 11:20 01/16/16 09:20
490-95901-16 MW-4DR Water 01/14/16 11:45 01/16/16 09:20
490-95901-17 FIELDBLANK Water 01/14/16 14:45 01/16/16 09:20
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Case Narrative
Client: Duke Energy Corporation TestAmerica Job ID: 490-95901-1
Project/Site: MNS Landfill #1 J16010006
Job ID: 490-95901-1
Laboratory: TestAmerica Nashville
Narrative
CASE NARRATIVE
Client: Duke Energy Corporation
Project: MNS Landfill #1
Report Number: 490-95901-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
TestAmerica Nashville attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses
performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the
application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data
have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions
to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written
approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
All solid sample results are reported on an "as received" basis unless otherwise indicated by the presence of a % solids value in the
method header.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT
The samples were received on 01/16/2016; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 0.4 C.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples TRIPBLANK (490-95901-1), MW-1 (490-95901-2), MW-1D (490-95901-3), MW-2A (490-95901-4), MW-2D (490-95901-5), MW-3
(490-95901-6), MW-3D (490-95901-7), MW-4 (490-95901-8), MW-4D (490-95901-9), MW-11 (490-95901-10), MW-11D (490-95901-11),
MW-12 (490-95901-12), MW-12D (490-95901-13), SW-1 (490-95901-14), MW-4R (490-95901-15), MW-4DR (490-95901-16) and
FIELDBLANK (490-95901-17) were analyzed for volatile organic compounds (GC-MS) in accordance with EPA SW-846 Method 8260B. The
samples were analyzed on 01/21/2016 and 01/22/2016.
Trichlorofluoromethane failed the recovery criteria high for LCS 490-314019/4. Trichlorofluoromethane failed the recovery criteria high for
LCS 490-314254/3. Trichlorofluoromethane failed the recovery criteria high for LCSD 490-314019/5. Trichlorofluoromethane failed the
recovery criteria high for LCSD 490-314254/4. These analytes were biased high in the LCS and were not detected in the associated
samples; therefore, the data have been reported.
1,2-Dibromo-3-Chloropropane failed the recovery criteria low for the MS of sample MW-1MS (490-95901-2) in batch 490-314019.
1,2-Dibromo-3-Chloropropane failed the recovery criteria low for the MSD of sample MW-1MSD (490-95901-2) in batch 490-314019.
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Case Narrative
Client: Duke Energy Corporation TestAmerica Job ID: 490-95901-1
Project/Site: MNS Landfill #1 J16010006
Job ID: 490-95901-1 (Continued)
Laboratory: TestAmerica Nashville (Continued)
Trichlorofluoromethane failed the recovery criteria high. Refer to the QC report for details.
The preservative used in the sample containers provided is not compatible with one of the Method 8260 analytes requested. The following
samples was received preserved with hydrochloric acid: MW-1 (490-95901-2), MW-1D (490-95901-3), MW-2A (490-95901-4), MW-2D
(490-95901-5), MW-3 (490-95901-6), MW-3D (490-95901-7), MW-4 (490-95901-8), MW-4D (490-95901-9), MW-11 (490-95901-10),
MW-11D (490-95901-11), MW-12 (490-95901-12), MW-12D (490-95901-13), SW-1 (490-95901-14), MW-4R (490-95901-15), MW-4DR
(490-95901-16) and FIELDBLANK (490-95901-17). The requested target analyte list includes acrylonitrile, an acid-labile compound that
degrades in an acidic medium.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated
with analytical batch 490-314254.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Qualifiers
GC/MS VOA
Qualifier Description
*LCS or LCSD is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
F1 MS and/or MSD Recovery is outside acceptance limits.
E Result exceeded calibration range.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-1Client Sample ID: TRIPBLANK
Matrix: WaterDate Collected: 01/14/16 05:35
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/22/16 00:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/22/16 00:44 1AcrylonitrileND
1.00 0.200 ug/L 01/22/16 00:44 1BenzeneND
1.00 0.150 ug/L 01/22/16 00:44 1BromochloromethaneND
1.00 0.170 ug/L 01/22/16 00:44 1BromodichloromethaneND
1.00 0.290 ug/L 01/22/16 00:44 1BromoformND
1.00 0.350 ug/L 01/22/16 00:44 1BromomethaneND
50.0 2.64 ug/L 01/22/16 00:44 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/22/16 00:44 1Carbon disulfide ND
1.00 0.180 ug/L 01/22/16 00:44 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/22/16 00:44 1ChlorobenzeneND
1.00 0.250 ug/L 01/22/16 00:44 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/22/16 00:44 1ChloroethaneND
1.00 0.230 ug/L 01/22/16 00:44 1ChloroformND
1.00 0.360 ug/L 01/22/16 00:44 1ChloromethaneND
1.00 0.210 ug/L 01/22/16 00:44 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/22/16 00:44 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/22/16 00:44 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/22/16 00:44 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/22/16 00:44 1DibromomethaneND
1.00 0.190 ug/L 01/22/16 00:44 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/22/16 00:44 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/22/16 00:44 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/22/16 00:44 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/22/16 00:44 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/22/16 00:44 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/22/16 00:44 1EthylbenzeneND
10.0 1.28 ug/L 01/22/16 00:44 12-Hexanone ND
10.0 1.50 ug/L 01/22/16 00:44 1IodomethaneND
1.00 1.00 ug/L 01/22/16 00:44 1Methylene Chloride ND
10.0 0.810 ug/L 01/22/16 00:44 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/22/16 00:44 1StyreneND
1.00 0.150 ug/L 01/22/16 00:44 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/22/16 00:44 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/22/16 00:44 1TetrachloroetheneND
1.00 0.170 ug/L 01/22/16 00:44 1TolueneND
5.00 0.460 ug/L 01/22/16 00:44 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/22/16 00:44 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/22/16 00:44 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/22/16 00:44 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/22/16 00:44 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/22/16 00:44 1TrichloroetheneND
1.00 0.210 ug/L 01/22/16 00:44 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/22/16 00:44 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/22/16 00:44 1Vinyl acetate ND
1.00 0.180 ug/L 01/22/16 00:44 1Vinyl chloride ND
3.00 0.580 ug/L 01/22/16 00:44 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-1Client Sample ID: TRIPBLANK
Matrix: WaterDate Collected: 01/14/16 05:35
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)90 70-130 01/22/16 00:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)100 01/22/16 00:44 170-130
1,2-Dichloroethane-d4 (Surr)97 01/22/16 00:44 170-130
Toluene-d8 (Surr)96 01/22/16 00:44 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-2Client Sample ID: MW-1
Matrix: WaterDate Collected: 01/14/16 08:50
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 14:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 14:21 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 14:21 1BenzeneND
1.00 0.150 ug/L 01/21/16 14:21 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 14:21 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 14:21 1BromoformND
1.00 0.350 ug/L 01/21/16 14:21 1BromomethaneND
50.0 2.64 ug/L 01/21/16 14:21 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 14:21 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 14:21 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 14:21 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 14:21 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 14:21 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 14:21 1ChloroformND
1.00 0.360 ug/L 01/21/16 14:21 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 14:21 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 14:21 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 14:21 11,2-Dibromo-3-Chloropropane ND F1
1.00 0.210 ug/L 01/21/16 14:21 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 14:21 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 14:21 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 14:21 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 14:21 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 14:21 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 14:21 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 14:21 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 14:21 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 14:21 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 14:21 1IodomethaneND
1.00 1.00 ug/L 01/21/16 14:21 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 14:21 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 14:21 1StyreneND
1.00 0.150 ug/L 01/21/16 14:21 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 14:21 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 14:21 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 14:21 1TolueneND
5.00 0.460 ug/L 01/21/16 14:21 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 14:21 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 14:21 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 14:21 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 14:21 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 14:21 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 14:21 1TrichlorofluoromethaneND * F1
1.00 0.230 ug/L 01/21/16 14:21 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 14:21 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 14:21 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 14:21 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-2Client Sample ID: MW-1
Matrix: WaterDate Collected: 01/14/16 08:50
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)92 70-130 01/21/16 14:21 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 01/21/16 14:21 170-130
1,2-Dichloroethane-d4 (Surr)97 01/21/16 14:21 170-130
Toluene-d8 (Surr)98 01/21/16 14:21 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-3Client Sample ID: MW-1D
Matrix: WaterDate Collected: 01/14/16 09:05
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 14:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 14:48 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 14:48 1BenzeneND
1.00 0.150 ug/L 01/21/16 14:48 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 14:48 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 14:48 1BromoformND
1.00 0.350 ug/L 01/21/16 14:48 1BromomethaneND
50.0 2.64 ug/L 01/21/16 14:48 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 14:48 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 14:48 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 14:48 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 14:48 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 14:48 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 14:48 1ChloroformND
1.00 0.360 ug/L 01/21/16 14:48 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 14:48 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 14:48 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 14:48 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 14:48 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 14:48 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 14:48 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 14:48 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 14:48 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 14:48 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 14:48 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 14:48 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 14:48 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 14:48 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 14:48 1IodomethaneND
1.00 1.00 ug/L 01/21/16 14:48 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 14:48 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 14:48 1StyreneND
1.00 0.150 ug/L 01/21/16 14:48 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 14:48 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 14:48 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 14:48 1TolueneND
5.00 0.460 ug/L 01/21/16 14:48 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 14:48 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 14:48 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 14:48 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 14:48 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 14:48 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 14:48 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 14:48 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 14:48 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 14:48 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 14:48 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-3Client Sample ID: MW-1D
Matrix: WaterDate Collected: 01/14/16 09:05
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)92 70-130 01/21/16 14:48 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)102 01/21/16 14:48 170-130
1,2-Dichloroethane-d4 (Surr)99 01/21/16 14:48 170-130
Toluene-d8 (Surr)101 01/21/16 14:48 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-4Client Sample ID: MW-2A
Matrix: WaterDate Collected: 01/14/16 13:30
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 15:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 15:15 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 15:15 1BenzeneND
1.00 0.150 ug/L 01/21/16 15:15 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 15:15 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 15:15 1BromoformND
1.00 0.350 ug/L 01/21/16 15:15 1BromomethaneND
50.0 2.64 ug/L 01/21/16 15:15 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 15:15 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 15:15 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 15:15 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 15:15 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 15:15 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 15:15 1ChloroformND
1.00 0.360 ug/L 01/21/16 15:15 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 15:15 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 15:15 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 15:15 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 15:15 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 15:15 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 15:15 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 15:15 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 15:15 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 15:15 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 15:15 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 15:15 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 15:15 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 15:15 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 15:15 1IodomethaneND
1.00 1.00 ug/L 01/21/16 15:15 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 15:15 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 15:15 1StyreneND
1.00 0.150 ug/L 01/21/16 15:15 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 15:15 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 15:15 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 15:15 1TolueneND
5.00 0.460 ug/L 01/21/16 15:15 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 15:15 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 15:15 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 15:15 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 15:15 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 15:15 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 15:15 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 15:15 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 15:15 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 15:15 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 15:15 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-4Client Sample ID: MW-2A
Matrix: WaterDate Collected: 01/14/16 13:30
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)91 70-130 01/21/16 15:15 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 01/21/16 15:15 170-130
1,2-Dichloroethane-d4 (Surr)97 01/21/16 15:15 170-130
Toluene-d8 (Surr)100 01/21/16 15:15 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-5Client Sample ID: MW-2D
Matrix: WaterDate Collected: 01/14/16 14:25
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 15:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 15:42 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 15:42 1BenzeneND
1.00 0.150 ug/L 01/21/16 15:42 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 15:42 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 15:42 1BromoformND
1.00 0.350 ug/L 01/21/16 15:42 1BromomethaneND
50.0 2.64 ug/L 01/21/16 15:42 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 15:42 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 15:42 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 15:42 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 15:42 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 15:42 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 15:42 1ChloroformND
1.00 0.360 ug/L 01/21/16 15:42 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 15:42 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 15:42 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 15:42 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 15:42 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 15:42 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 15:42 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 15:42 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 15:42 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 15:42 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 15:42 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 15:42 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 15:42 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 15:42 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 15:42 1IodomethaneND
1.00 1.00 ug/L 01/21/16 15:42 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 15:42 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 15:42 1StyreneND
1.00 0.150 ug/L 01/21/16 15:42 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 15:42 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 15:42 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 15:42 1TolueneND
5.00 0.460 ug/L 01/21/16 15:42 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 15:42 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 15:42 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 15:42 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 15:42 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 15:42 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 15:42 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 15:42 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 15:42 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 15:42 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 15:42 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-5Client Sample ID: MW-2D
Matrix: WaterDate Collected: 01/14/16 14:25
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)93 70-130 01/21/16 15:42 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)101 01/21/16 15:42 170-130
1,2-Dichloroethane-d4 (Surr)98 01/21/16 15:42 170-130
Toluene-d8 (Surr)100 01/21/16 15:42 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-6Client Sample ID: MW-3
Matrix: WaterDate Collected: 01/14/16 10:00
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 16:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 16:10 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 16:10 1BenzeneND
1.00 0.150 ug/L 01/21/16 16:10 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 16:10 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 16:10 1BromoformND
1.00 0.350 ug/L 01/21/16 16:10 1BromomethaneND
50.0 2.64 ug/L 01/21/16 16:10 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 16:10 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 16:10 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 16:10 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 16:10 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 16:10 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 16:10 1ChloroformND
1.00 0.360 ug/L 01/21/16 16:10 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 16:10 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 16:10 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 16:10 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 16:10 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 16:10 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 16:10 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 16:10 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 16:10 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 16:10 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 16:10 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 16:10 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 16:10 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 16:10 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 16:10 1IodomethaneND
1.00 1.00 ug/L 01/21/16 16:10 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 16:10 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 16:10 1StyreneND
1.00 0.150 ug/L 01/21/16 16:10 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 16:10 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 16:10 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 16:10 1TolueneND
5.00 0.460 ug/L 01/21/16 16:10 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 16:10 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 16:10 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 16:10 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 16:10 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 16:10 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 16:10 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 16:10 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 16:10 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 16:10 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 16:10 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-6Client Sample ID: MW-3
Matrix: WaterDate Collected: 01/14/16 10:00
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)91 70-130 01/21/16 16:10 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)100 01/21/16 16:10 170-130
1,2-Dichloroethane-d4 (Surr)96 01/21/16 16:10 170-130
Toluene-d8 (Surr)100 01/21/16 16:10 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-7Client Sample ID: MW-3D
Matrix: WaterDate Collected: 01/14/16 10:20
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 16:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 16:37 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 16:37 1BenzeneND
1.00 0.150 ug/L 01/21/16 16:37 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 16:37 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 16:37 1BromoformND
1.00 0.350 ug/L 01/21/16 16:37 1BromomethaneND
50.0 2.64 ug/L 01/21/16 16:37 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 16:37 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 16:37 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 16:37 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 16:37 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 16:37 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 16:37 1ChloroformND
1.00 0.360 ug/L 01/21/16 16:37 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 16:37 1cis-1,2-Dichloroethene 0.673 J
1.00 0.170 ug/L 01/21/16 16:37 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 16:37 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 16:37 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 16:37 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 16:37 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 16:37 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 16:37 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 16:37 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 16:37 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 16:37 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 16:37 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 16:37 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 16:37 1IodomethaneND
1.00 1.00 ug/L 01/21/16 16:37 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 16:37 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 16:37 1StyreneND
1.00 0.150 ug/L 01/21/16 16:37 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 16:37 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 16:37 1Tetrachloroethene0.336 J
1.00 0.170 ug/L 01/21/16 16:37 1TolueneND
5.00 0.460 ug/L 01/21/16 16:37 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 16:37 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 16:37 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 16:37 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 16:37 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 16:37 1Trichloroethene0.709 J
1.00 0.210 ug/L 01/21/16 16:37 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 16:37 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 16:37 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 16:37 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 16:37 1Xylenes, Total 2.43 J
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-7Client Sample ID: MW-3D
Matrix: WaterDate Collected: 01/14/16 10:20
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)92 70-130 01/21/16 16:37 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)96 01/21/16 16:37 170-130
1,2-Dichloroethane-d4 (Surr)101 01/21/16 16:37 170-130
Toluene-d8 (Surr)99 01/21/16 16:37 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-8Client Sample ID: MW-4
Matrix: WaterDate Collected: 01/14/16 07:50
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 17:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 17:04 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 17:04 1BenzeneND
1.00 0.150 ug/L 01/21/16 17:04 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 17:04 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 17:04 1BromoformND
1.00 0.350 ug/L 01/21/16 17:04 1BromomethaneND
50.0 2.64 ug/L 01/21/16 17:04 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 17:04 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 17:04 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 17:04 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 17:04 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 17:04 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 17:04 1ChloroformND
1.00 0.360 ug/L 01/21/16 17:04 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 17:04 1cis-1,2-Dichloroethene 2.23
1.00 0.170 ug/L 01/21/16 17:04 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 17:04 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 17:04 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 17:04 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 17:04 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 17:04 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 17:04 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 17:04 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 17:04 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 17:04 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 17:04 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 17:04 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 17:04 1IodomethaneND
1.00 1.00 ug/L 01/21/16 17:04 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 17:04 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 17:04 1StyreneND
1.00 0.150 ug/L 01/21/16 17:04 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 17:04 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 17:04 1Tetrachloroethene1.84
1.00 0.170 ug/L 01/21/16 17:04 1TolueneND
5.00 0.460 ug/L 01/21/16 17:04 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 17:04 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 17:04 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 17:04 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 17:04 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 17:04 1Trichloroethene1.12
1.00 0.210 ug/L 01/21/16 17:04 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 17:04 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 17:04 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 17:04 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 17:04 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-8Client Sample ID: MW-4
Matrix: WaterDate Collected: 01/14/16 07:50
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)99 70-130 01/21/16 17:04 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)102 01/21/16 17:04 170-130
1,2-Dichloroethane-d4 (Surr)96 01/21/16 17:04 170-130
Toluene-d8 (Surr)99 01/21/16 17:04 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-9Client Sample ID: MW-4D
Matrix: WaterDate Collected: 01/14/16 08:35
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 17:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 17:31 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 17:31 1Benzene0.837 J
1.00 0.150 ug/L 01/21/16 17:31 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 17:31 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 17:31 1BromoformND
1.00 0.350 ug/L 01/21/16 17:31 1BromomethaneND
50.0 2.64 ug/L 01/21/16 17:31 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 17:31 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 17:31 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 17:31 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 17:31 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 17:31 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 17:31 1ChloroformND
1.00 0.360 ug/L 01/21/16 17:31 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 17:31 1cis-1,2-Dichloroethene 12.1
1.00 0.170 ug/L 01/21/16 17:31 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 17:31 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 17:31 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 17:31 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 17:31 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 17:31 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 17:31 11,1-Dichloroethane 0.302 J
1.00 0.200 ug/L 01/21/16 17:31 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 17:31 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 17:31 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 17:31 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 17:31 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 17:31 1IodomethaneND
1.00 1.00 ug/L 01/21/16 17:31 1Methylene Chloride 7.01
10.0 0.810 ug/L 01/21/16 17:31 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 17:31 1StyreneND
1.00 0.150 ug/L 01/21/16 17:31 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 17:31 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 17:31 1Tetrachloroethene1.34
1.00 0.170 ug/L 01/21/16 17:31 1Toluene0.184 J
5.00 0.460 ug/L 01/21/16 17:31 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 17:31 1trans-1,2-Dichloroethene 0.384 J
1.00 0.170 ug/L 01/21/16 17:31 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 17:31 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 17:31 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 17:31 1Trichloroethene4.08
1.00 0.210 ug/L 01/21/16 17:31 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 17:31 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 17:31 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 17:31 1Vinyl chloride 0.473 J
3.00 0.580 ug/L 01/21/16 17:31 1Xylenes, Total 34.2
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-9Client Sample ID: MW-4D
Matrix: WaterDate Collected: 01/14/16 08:35
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)92 70-130 01/21/16 17:31 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)102 01/21/16 17:31 170-130
1,2-Dichloroethane-d4 (Surr)101 01/21/16 17:31 170-130
Toluene-d8 (Surr)97 01/21/16 17:31 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-10Client Sample ID: MW-11
Matrix: WaterDate Collected: 01/14/16 10:45
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 17:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 17:58 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 17:58 1BenzeneND
1.00 0.150 ug/L 01/21/16 17:58 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 17:58 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 17:58 1BromoformND
1.00 0.350 ug/L 01/21/16 17:58 1BromomethaneND
50.0 2.64 ug/L 01/21/16 17:58 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 17:58 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 17:58 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 17:58 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 17:58 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 17:58 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 17:58 1ChloroformND
1.00 0.360 ug/L 01/21/16 17:58 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 17:58 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 17:58 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 17:58 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 17:58 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 17:58 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 17:58 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 17:58 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 17:58 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 17:58 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 17:58 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 17:58 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 17:58 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 17:58 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 17:58 1IodomethaneND
1.00 1.00 ug/L 01/21/16 17:58 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 17:58 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 17:58 1StyreneND
1.00 0.150 ug/L 01/21/16 17:58 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 17:58 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 17:58 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 17:58 1TolueneND
5.00 0.460 ug/L 01/21/16 17:58 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 17:58 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 17:58 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 17:58 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 17:58 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 17:58 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 17:58 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 17:58 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 17:58 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 17:58 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 17:58 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-10Client Sample ID: MW-11
Matrix: WaterDate Collected: 01/14/16 10:45
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)99 70-130 01/21/16 17:58 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 01/21/16 17:58 170-130
1,2-Dichloroethane-d4 (Surr)98 01/21/16 17:58 170-130
Toluene-d8 (Surr)101 01/21/16 17:58 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-11Client Sample ID: MW-11D
Matrix: WaterDate Collected: 01/14/16 11:30
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 18:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 18:25 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 18:25 1BenzeneND
1.00 0.150 ug/L 01/21/16 18:25 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 18:25 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 18:25 1BromoformND
1.00 0.350 ug/L 01/21/16 18:25 1BromomethaneND
50.0 2.64 ug/L 01/21/16 18:25 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 18:25 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 18:25 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 18:25 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 18:25 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 18:25 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 18:25 1ChloroformND
1.00 0.360 ug/L 01/21/16 18:25 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 18:25 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 18:25 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 18:25 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 18:25 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 18:25 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 18:25 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 18:25 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 18:25 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 18:25 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 18:25 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 18:25 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 18:25 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 18:25 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 18:25 1IodomethaneND
1.00 1.00 ug/L 01/21/16 18:25 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 18:25 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 18:25 1StyreneND
1.00 0.150 ug/L 01/21/16 18:25 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 18:25 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 18:25 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 18:25 1TolueneND
5.00 0.460 ug/L 01/21/16 18:25 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 18:25 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 18:25 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 18:25 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 18:25 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 18:25 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 18:25 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 18:25 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 18:25 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 18:25 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 18:25 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-11Client Sample ID: MW-11D
Matrix: WaterDate Collected: 01/14/16 11:30
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)104 70-130 01/21/16 18:25 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 01/21/16 18:25 170-130
1,2-Dichloroethane-d4 (Surr)97 01/21/16 18:25 170-130
Toluene-d8 (Surr)98 01/21/16 18:25 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-12Client Sample ID: MW-12
Matrix: WaterDate Collected: 01/14/16 12:50
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 18:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 18:52 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 18:52 1BenzeneND
1.00 0.150 ug/L 01/21/16 18:52 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 18:52 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 18:52 1BromoformND
1.00 0.350 ug/L 01/21/16 18:52 1BromomethaneND
50.0 2.64 ug/L 01/21/16 18:52 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 18:52 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 18:52 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 18:52 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 18:52 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 18:52 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 18:52 1ChloroformND
1.00 0.360 ug/L 01/21/16 18:52 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 18:52 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 18:52 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 18:52 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 18:52 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 18:52 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 18:52 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 18:52 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 18:52 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 18:52 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 18:52 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 18:52 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 18:52 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 18:52 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 18:52 1IodomethaneND
1.00 1.00 ug/L 01/21/16 18:52 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 18:52 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 18:52 1StyreneND
1.00 0.150 ug/L 01/21/16 18:52 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 18:52 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 18:52 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 18:52 1TolueneND
5.00 0.460 ug/L 01/21/16 18:52 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 18:52 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 18:52 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 18:52 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 18:52 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 18:52 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 18:52 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 18:52 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 18:52 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 18:52 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 18:52 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-12Client Sample ID: MW-12
Matrix: WaterDate Collected: 01/14/16 12:50
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)104 70-130 01/21/16 18:52 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)100 01/21/16 18:52 170-130
1,2-Dichloroethane-d4 (Surr)101 01/21/16 18:52 170-130
Toluene-d8 (Surr)99 01/21/16 18:52 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-13Client Sample ID: MW-12D
Matrix: WaterDate Collected: 01/14/16 13:10
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 19:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 19:19 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 19:19 1BenzeneND
1.00 0.150 ug/L 01/21/16 19:19 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 19:19 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 19:19 1BromoformND
1.00 0.350 ug/L 01/21/16 19:19 1BromomethaneND
50.0 2.64 ug/L 01/21/16 19:19 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 19:19 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 19:19 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 19:19 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 19:19 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 19:19 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 19:19 1ChloroformND
1.00 0.360 ug/L 01/21/16 19:19 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 19:19 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 19:19 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 19:19 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 19:19 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 19:19 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 19:19 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 19:19 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 19:19 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 19:19 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 19:19 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 19:19 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 19:19 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 19:19 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 19:19 1IodomethaneND
1.00 1.00 ug/L 01/21/16 19:19 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 19:19 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 19:19 1StyreneND
1.00 0.150 ug/L 01/21/16 19:19 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 19:19 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 19:19 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 19:19 1TolueneND
5.00 0.460 ug/L 01/21/16 19:19 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 19:19 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 19:19 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 19:19 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 19:19 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 19:19 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 19:19 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 19:19 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 19:19 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 19:19 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 19:19 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-13Client Sample ID: MW-12D
Matrix: WaterDate Collected: 01/14/16 13:10
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)98 70-130 01/21/16 19:19 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 01/21/16 19:19 170-130
1,2-Dichloroethane-d4 (Surr)96 01/21/16 19:19 170-130
Toluene-d8 (Surr)99 01/21/16 19:19 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-14Client Sample ID: SW-1
Matrix: WaterDate Collected: 01/14/16 12:20
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 19:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 19:46 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 19:46 1BenzeneND
1.00 0.150 ug/L 01/21/16 19:46 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 19:46 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 19:46 1BromoformND
1.00 0.350 ug/L 01/21/16 19:46 1BromomethaneND
50.0 2.64 ug/L 01/21/16 19:46 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 19:46 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 19:46 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 19:46 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 19:46 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 19:46 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 19:46 1ChloroformND
1.00 0.360 ug/L 01/21/16 19:46 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 19:46 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 19:46 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 19:46 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 19:46 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 19:46 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 19:46 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 19:46 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 19:46 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 19:46 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 19:46 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 19:46 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 19:46 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 19:46 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 19:46 1IodomethaneND
1.00 1.00 ug/L 01/21/16 19:46 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 19:46 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 19:46 1StyreneND
1.00 0.150 ug/L 01/21/16 19:46 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 19:46 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 19:46 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 19:46 1TolueneND
5.00 0.460 ug/L 01/21/16 19:46 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 19:46 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 19:46 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 19:46 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 19:46 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 19:46 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 19:46 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 19:46 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 19:46 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 19:46 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 19:46 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-14Client Sample ID: SW-1
Matrix: WaterDate Collected: 01/14/16 12:20
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)93 70-130 01/21/16 19:46 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)95 01/21/16 19:46 170-130
1,2-Dichloroethane-d4 (Surr)100 01/21/16 19:46 170-130
Toluene-d8 (Surr)97 01/21/16 19:46 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-15Client Sample ID: MW-4R
Matrix: WaterDate Collected: 01/14/16 11:20
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 20:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 20:13 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 20:13 1BenzeneND
1.00 0.150 ug/L 01/21/16 20:13 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 20:13 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 20:13 1BromoformND
1.00 0.350 ug/L 01/21/16 20:13 1BromomethaneND
50.0 2.64 ug/L 01/21/16 20:13 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 20:13 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 20:13 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 20:13 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 20:13 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 20:13 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 20:13 1ChloroformND
1.00 0.360 ug/L 01/21/16 20:13 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 20:13 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 20:13 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 20:13 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 20:13 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 20:13 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 20:13 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 20:13 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 20:13 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 20:13 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 20:13 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 20:13 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 20:13 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 20:13 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 20:13 1IodomethaneND
1.00 1.00 ug/L 01/21/16 20:13 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 20:13 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 20:13 1StyreneND
1.00 0.150 ug/L 01/21/16 20:13 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 20:13 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 20:13 1Tetrachloroethene0.502 J
1.00 0.170 ug/L 01/21/16 20:13 1TolueneND
5.00 0.460 ug/L 01/21/16 20:13 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 20:13 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 20:13 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 20:13 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 20:13 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 20:13 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 20:13 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 20:13 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 20:13 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 20:13 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 20:13 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-15Client Sample ID: MW-4R
Matrix: WaterDate Collected: 01/14/16 11:20
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)96 70-130 01/21/16 20:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)103 01/21/16 20:13 170-130
1,2-Dichloroethane-d4 (Surr)96 01/21/16 20:13 170-130
Toluene-d8 (Surr)96 01/21/16 20:13 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-16Client Sample ID: MW-4DR
Matrix: WaterDate Collected: 01/14/16 11:45
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 20:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 20:41 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 20:41 1BenzeneND
1.00 0.150 ug/L 01/21/16 20:41 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 20:41 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 20:41 1BromoformND
1.00 0.350 ug/L 01/21/16 20:41 1BromomethaneND
50.0 2.64 ug/L 01/21/16 20:41 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 20:41 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 20:41 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 20:41 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 20:41 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 20:41 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 20:41 1ChloroformND
1.00 0.360 ug/L 01/21/16 20:41 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 20:41 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 20:41 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 20:41 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 20:41 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 20:41 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 20:41 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 20:41 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 20:41 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 20:41 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 20:41 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 20:41 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 20:41 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 20:41 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 20:41 1IodomethaneND
1.00 1.00 ug/L 01/21/16 20:41 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 20:41 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 20:41 1StyreneND
1.00 0.150 ug/L 01/21/16 20:41 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 20:41 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 20:41 1Tetrachloroethene0.251 J
1.00 0.170 ug/L 01/21/16 20:41 1TolueneND
5.00 0.460 ug/L 01/21/16 20:41 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 20:41 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 20:41 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 20:41 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 20:41 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 20:41 1Trichloroethene0.202 J
1.00 0.210 ug/L 01/21/16 20:41 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 20:41 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 20:41 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 20:41 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 20:41 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-16Client Sample ID: MW-4DR
Matrix: WaterDate Collected: 01/14/16 11:45
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)97 70-130 01/21/16 20:41 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)100 01/21/16 20:41 170-130
1,2-Dichloroethane-d4 (Surr)99 01/21/16 20:41 170-130
Toluene-d8 (Surr)95 01/21/16 20:41 170-130
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-17Client Sample ID: FIELDBLANK
Matrix: WaterDate Collected: 01/14/16 14:45
Date Received: 01/16/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 13:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 01/21/16 13:54 1AcrylonitrileND
1.00 0.200 ug/L 01/21/16 13:54 1BenzeneND
1.00 0.150 ug/L 01/21/16 13:54 1BromochloromethaneND
1.00 0.170 ug/L 01/21/16 13:54 1BromodichloromethaneND
1.00 0.290 ug/L 01/21/16 13:54 1BromoformND
1.00 0.350 ug/L 01/21/16 13:54 1BromomethaneND
50.0 2.64 ug/L 01/21/16 13:54 12-Butanone (MEK)ND
1.00 0.220 ug/L 01/21/16 13:54 1Carbon disulfide ND
1.00 0.180 ug/L 01/21/16 13:54 1Carbon tetrachloride ND
1.00 0.180 ug/L 01/21/16 13:54 1ChlorobenzeneND
1.00 0.250 ug/L 01/21/16 13:54 1ChlorodibromomethaneND
1.00 0.360 ug/L 01/21/16 13:54 1ChloroethaneND
1.00 0.230 ug/L 01/21/16 13:54 1ChloroformND
1.00 0.360 ug/L 01/21/16 13:54 1ChloromethaneND
1.00 0.210 ug/L 01/21/16 13:54 1cis-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 13:54 1cis-1,3-Dichloropropene ND
10.0 0.940 ug/L 01/21/16 13:54 11,2-Dibromo-3-Chloropropane ND
1.00 0.210 ug/L 01/21/16 13:54 11,2-Dibromoethane (EDB)ND
1.00 0.450 ug/L 01/21/16 13:54 1DibromomethaneND
1.00 0.190 ug/L 01/21/16 13:54 11,2-Dichlorobenzene ND
1.00 0.170 ug/L 01/21/16 13:54 11,4-Dichlorobenzene ND
1.00 0.240 ug/L 01/21/16 13:54 11,1-Dichloroethane ND
1.00 0.200 ug/L 01/21/16 13:54 11,2-Dichloroethane ND
1.00 0.250 ug/L 01/21/16 13:54 11,1-Dichloroethene ND
1.00 0.250 ug/L 01/21/16 13:54 11,2-Dichloropropane ND
1.00 0.190 ug/L 01/21/16 13:54 1EthylbenzeneND
10.0 1.28 ug/L 01/21/16 13:54 12-Hexanone ND
10.0 1.50 ug/L 01/21/16 13:54 1IodomethaneND
1.00 1.00 ug/L 01/21/16 13:54 1Methylene Chloride ND
10.0 0.810 ug/L 01/21/16 13:54 14-Methyl-2-pentanone (MIBK)ND
1.00 0.280 ug/L 01/21/16 13:54 1StyreneND
1.00 0.150 ug/L 01/21/16 13:54 11,1,1,2-Tetrachloroethane ND
1.00 0.190 ug/L 01/21/16 13:54 11,1,2,2-Tetrachloroethane ND
1.00 0.140 ug/L 01/21/16 13:54 1TetrachloroetheneND
1.00 0.170 ug/L 01/21/16 13:54 1TolueneND
5.00 0.460 ug/L 01/21/16 13:54 1trans-1,4-Dichloro-2-butene ND
1.00 0.230 ug/L 01/21/16 13:54 1trans-1,2-Dichloroethene ND
1.00 0.170 ug/L 01/21/16 13:54 1trans-1,3-Dichloropropene ND
1.00 0.190 ug/L 01/21/16 13:54 11,1,1-Trichloroethane ND
1.00 0.190 ug/L 01/21/16 13:54 11,1,2-Trichloroethane ND
1.00 0.200 ug/L 01/21/16 13:54 1TrichloroetheneND
1.00 0.210 ug/L 01/21/16 13:54 1TrichlorofluoromethaneND *
1.00 0.230 ug/L 01/21/16 13:54 11,2,3-Trichloropropane ND
10.0 1.71 ug/L 01/21/16 13:54 1Vinyl acetate ND
1.00 0.180 ug/L 01/21/16 13:54 1Vinyl chloride ND
3.00 0.580 ug/L 01/21/16 13:54 1Xylenes, Total ND
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Client Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Lab Sample ID: 490-95901-17Client Sample ID: FIELDBLANK
Matrix: WaterDate Collected: 01/14/16 14:45
Date Received: 01/16/16 09:20
4-Bromofluorobenzene (Surr)94 70-130 01/21/16 13:54 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)102 01/21/16 13:54 170-130
1,2-Dichloroethane-d4 (Surr)97 01/21/16 13:54 170-130
Toluene-d8 (Surr)100 01/21/16 13:54 170-130
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QC Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-314019/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314019
RL MDL
Acetone ND 25.0 2.66 ug/L 01/21/16 11:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.50010.0 ug/L 01/21/16 11:38 1Acrylonitrile
ND 0.2001.00 ug/L 01/21/16 11:38 1Benzene
ND 0.1501.00 ug/L 01/21/16 11:38 1Bromochloromethane
ND 0.1701.00 ug/L 01/21/16 11:38 1Bromodichloromethane
ND 0.2901.00 ug/L 01/21/16 11:38 1Bromoform
ND 0.3501.00 ug/L 01/21/16 11:38 1Bromomethane
ND 2.6450.0 ug/L 01/21/16 11:38 12-Butanone (MEK)
ND 0.2201.00 ug/L 01/21/16 11:38 1Carbon disulfide
ND 0.1801.00 ug/L 01/21/16 11:38 1Carbon tetrachloride
ND 0.1801.00 ug/L 01/21/16 11:38 1Chlorobenzene
ND 0.2501.00 ug/L 01/21/16 11:38 1Chlorodibromomethane
ND 0.3601.00 ug/L 01/21/16 11:38 1Chloroethane
ND 0.2301.00 ug/L 01/21/16 11:38 1Chloroform
ND 0.3601.00 ug/L 01/21/16 11:38 1Chloromethane
ND 0.2101.00 ug/L 01/21/16 11:38 1cis-1,2-Dichloroethene
ND 0.1701.00 ug/L 01/21/16 11:38 1cis-1,3-Dichloropropene
ND 0.94010.0 ug/L 01/21/16 11:38 11,2-Dibromo-3-Chloropropane
ND 0.2101.00 ug/L 01/21/16 11:38 11,2-Dibromoethane (EDB)
ND 0.4501.00 ug/L 01/21/16 11:38 1Dibromomethane
ND 0.1901.00 ug/L 01/21/16 11:38 11,2-Dichlorobenzene
ND 0.1701.00 ug/L 01/21/16 11:38 11,4-Dichlorobenzene
ND 0.2401.00 ug/L 01/21/16 11:38 11,1-Dichloroethane
ND 0.2001.00 ug/L 01/21/16 11:38 11,2-Dichloroethane
ND 0.2501.00 ug/L 01/21/16 11:38 11,1-Dichloroethene
ND 0.2501.00 ug/L 01/21/16 11:38 11,2-Dichloropropane
ND 0.1901.00 ug/L 01/21/16 11:38 1Ethylbenzene
ND 1.2810.0 ug/L 01/21/16 11:38 12-Hexanone
ND 1.5010.0 ug/L 01/21/16 11:38 1Iodomethane
ND 1.001.00 ug/L 01/21/16 11:38 1Methylene Chloride
ND 0.81010.0 ug/L 01/21/16 11:38 14-Methyl-2-pentanone (MIBK)
ND 0.2801.00 ug/L 01/21/16 11:38 1Styrene
ND 0.1501.00 ug/L 01/21/16 11:38 11,1,1,2-Tetrachloroethane
ND 0.1901.00 ug/L 01/21/16 11:38 11,1,2,2-Tetrachloroethane
ND 0.1401.00 ug/L 01/21/16 11:38 1Tetrachloroethene
ND 0.1701.00 ug/L 01/21/16 11:38 1Toluene
ND 0.4605.00 ug/L 01/21/16 11:38 1trans-1,4-Dichloro-2-butene
ND 0.2301.00 ug/L 01/21/16 11:38 1trans-1,2-Dichloroethene
ND 0.1701.00 ug/L 01/21/16 11:38 1trans-1,3-Dichloropropene
ND 0.1901.00 ug/L 01/21/16 11:38 11,1,1-Trichloroethane
ND 0.1901.00 ug/L 01/21/16 11:38 11,1,2-Trichloroethane
ND 0.2001.00 ug/L 01/21/16 11:38 1Trichloroethene
ND 0.2101.00 ug/L 01/21/16 11:38 1Trichlorofluoromethane
ND 0.2301.00 ug/L 01/21/16 11:38 11,2,3-Trichloropropane
ND 1.7110.0 ug/L 01/21/16 11:38 1Vinyl acetate
ND 0.1801.00 ug/L 01/21/16 11:38 1Vinyl chloride
ND 0.5803.00 ug/L 01/21/16 11:38 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-314019/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314019
4-Bromofluorobenzene (Surr)93 70-130 01/21/16 11:38 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
95 01/21/16 11:38 1Dibromofluoromethane (Surr)70-130
94 01/21/16 11:38 11,2-Dichloroethane-d4 (Surr)70-130
99 01/21/16 11:38 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-314019/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314019
Acetone 100 66.84 ug/L 67 54-145
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 156.2 ug/L 78 61-140
Benzene 20.0 18.65 ug/L 93 80-121
Bromochloromethane 20.0 18.78 ug/L 94 78-129
Bromodichloromethane 20.0 20.35 ug/L 102 75-129
Bromoform 20.0 22.77 E ug/L 114 46-145
Bromomethane 20.0 25.52 ug/L 128 41-150
2-Butanone (MEK)100 77.24 ug/L 77 62-133
Carbon disulfide 20.0 20.46 ug/L 102 77-126
Carbon tetrachloride 20.0 24.54 ug/L 123 64-147
Chlorobenzene 20.0 19.20 ug/L 96 80-120
Chlorodibromomethane 20.0 21.75 ug/L 109 69-133
Chloroethane 20.0 18.54 ug/L 93 72-120
Chloroform 20.0 20.86 ug/L 104 73-129
Chloromethane 20.0 18.49 ug/L 92 12-150
cis-1,2-Dichloroethene 20.0 19.14 ug/L 96 76-125
cis-1,3-Dichloropropene 20.0 18.60 ug/L 93 74-140
1,2-Dibromo-3-Chloropropane 20.0 11.83 ug/L 59 54-125
1,2-Dibromoethane (EDB)20.0 18.23 ug/L 91 80-129
Dibromomethane 20.0 20.07 ug/L 100 71-125
1,2-Dichlorobenzene 20.0 19.46 ug/L 97 80-121
1,4-Dichlorobenzene 20.0 20.64 ug/L 103 80-120
1,1-Dichloroethane 20.0 20.20 ug/L 101 78-125
1,2-Dichloroethane 20.0 21.11 ug/L 106 77-121
1,1-Dichloroethene 20.0 21.28 ug/L 106 79-124
1,2-Dichloropropane 20.0 19.05 ug/L 95 75-120
Ethylbenzene 20.0 18.82 ug/L 94 80-130
2-Hexanone 100 69.14 ug/L 69 60-142
Iodomethane 20.0 20.47 ug/L 102 40-150
Methylene Chloride 20.0 18.37 ug/L 92 79-123
4-Methyl-2-pentanone (MIBK)100 72.28 ug/L 72 60-137
Styrene 20.0 18.25 ug/L 91 80-127
1,1,1,2-Tetrachloroethane 20.0 20.96 ug/L 105 74-135
1,1,2,2-Tetrachloroethane 20.0 17.44 ug/L 87 69-131
Tetrachloroethene 20.0 21.22 ug/L 106 80-126
Toluene 20.0 18.83 ug/L 94 80-126
trans-1,4-Dichloro-2-butene 20.0 15.93 ug/L 80 41-147
trans-1,2-Dichloroethene 20.0 19.58 ug/L 98 79-126
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QC Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-314019/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314019
trans-1,3-Dichloropropene 20.0 16.99 ug/L 85 63-134
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 20.0 21.53 ug/L 108 78-135
1,1,2-Trichloroethane 20.0 19.29 ug/L 96 80-124
Trichloroethene 20.0 20.59 ug/L 103 80-123
Trichlorofluoromethane 20.0 25.78 * ug/L 129 65-124
1,2,3-Trichloropropane 20.0 19.11 ug/L 96 70-131
Vinyl acetate 40.0 30.40 ug/L 76 54-139
Vinyl chloride 20.0 19.07 ug/L 95 68-120
Xylenes, Total 40.0 37.41 ug/L 94 80-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
921,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-314019/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314019
Acetone 100 72.07 ug/L 72 54-145 8 21
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 154.5 ug/L 77 61-140 1 18
Benzene 20.0 18.61 ug/L 93 80-121 0 17
Bromochloromethane 20.0 19.06 ug/L 95 78-129 1 17
Bromodichloromethane 20.0 19.28 ug/L 96 75-129 5 18
Bromoform 20.0 22.61 E ug/L 113 46-145 1 16
Bromomethane 20.0 23.41 ug/L 117 41-150 9 50
2-Butanone (MEK)100 75.84 ug/L 76 62-133 2 19
Carbon disulfide 20.0 20.51 ug/L 103 77-126 0 21
Carbon tetrachloride 20.0 23.51 ug/L 118 64-147 4 19
Chlorobenzene 20.0 19.25 ug/L 96 80-120 0 14
Chlorodibromomethane 20.0 20.33 ug/L 102 69-133 7 15
Chloroethane 20.0 18.52 ug/L 93 72-120 0 20
Chloroform 20.0 20.59 ug/L 103 73-129 1 18
Chloromethane 20.0 19.38 ug/L 97 12-150 5 31
cis-1,2-Dichloroethene 20.0 19.20 ug/L 96 76-125 0 17
cis-1,3-Dichloropropene 20.0 17.49 ug/L 87 74-140 6 15
1,2-Dibromo-3-Chloropropane 20.0 12.53 ug/L 63 54-125 6 24
1,2-Dibromoethane (EDB)20.0 17.88 ug/L 89 80-129 2 15
Dibromomethane 20.0 18.56 ug/L 93 71-125 8 16
1,2-Dichlorobenzene 20.0 19.56 ug/L 98 80-121 1 15
1,4-Dichlorobenzene 20.0 19.58 ug/L 98 80-120 5 15
1,1-Dichloroethane 20.0 19.49 ug/L 97 78-125 4 17
1,2-Dichloroethane 20.0 20.48 ug/L 102 77-121 3 17
1,1-Dichloroethene 20.0 20.42 ug/L 102 79-124 4 17
1,2-Dichloropropane 20.0 18.98 ug/L 95 75-120 0 17
Ethylbenzene 20.0 18.25 ug/L 91 80-130 3 15
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QC Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-314019/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314019
2-Hexanone 100 70.06 ug/L 70 60-142 1 15
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Iodomethane 20.0 22.06 ug/L 110 40-150 7 23
Methylene Chloride 20.0 18.20 ug/L 91 79-123 1 17
4-Methyl-2-pentanone (MIBK)100 71.96 ug/L 72 60-137 0 17
Styrene 20.0 17.94 ug/L 90 80-127 2 24
1,1,1,2-Tetrachloroethane 20.0 20.04 ug/L 100 74-135 4 16
1,1,2,2-Tetrachloroethane 20.0 17.46 ug/L 87 69-131 0 20
Tetrachloroethene 20.0 20.45 ug/L 102 80-126 4 16
Toluene 20.0 18.74 ug/L 94 80-126 0 15
trans-1,4-Dichloro-2-butene 20.0 15.82 ug/L 79 41-147 1 26
trans-1,2-Dichloroethene 20.0 19.15 ug/L 96 79-126 2 16
trans-1,3-Dichloropropene 20.0 16.75 ug/L 84 63-134 1 14
1,1,1-Trichloroethane 20.0 21.52 ug/L 108 78-135 0 17
1,1,2-Trichloroethane 20.0 18.57 ug/L 93 80-124 4 15
Trichloroethene 20.0 20.95 ug/L 105 80-123 2 17
Trichlorofluoromethane 20.0 26.51 * ug/L 133 65-124 3 18
1,2,3-Trichloropropane 20.0 18.65 ug/L 93 70-131 2 19
Vinyl acetate 40.0 30.35 ug/L 76 54-139 0 21
Vinyl chloride 20.0 19.83 ug/L 99 68-120 4 17
Xylenes, Total 40.0 36.93 ug/L 92 80-132 1 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
93
LCSD LCSD
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
901,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Client Sample ID: MW-1Lab Sample ID: 490-95901-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314019
Acetone ND 250 154.9 ug/L 62 45-141
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile ND 500 345.7 ug/L 69 50-148
Benzene ND 50.0 42.90 ug/L 86 75-133
Bromochloromethane ND 50.0 45.67 ug/L 91 67-139
Bromodichloromethane ND 50.0 51.44 ug/L 103 70-140
Bromoform ND 50.0 58.13 E ug/L 116 42-147
Bromomethane ND 50.0 60.12 E ug/L 120 16-163
2-Butanone (MEK)ND 250 176.3 ug/L 71 50-138
Carbon disulfide ND 50.0 44.92 ug/L 90 48-152
Carbon tetrachloride ND 50.0 62.00 ug/L 124 62-164
Chlorobenzene ND 50.0 46.50 ug/L 93 80-129
Chlorodibromomethane ND 50.0 56.31 E ug/L 113 66-140
Chloroethane ND 50.0 46.03 ug/L 92 58-137
Chloroform ND 50.0 50.66 ug/L 101 66-138
Chloromethane ND 50.0 41.22 ug/L 82 10-169
cis-1,2-Dichloroethene ND 50.0 44.16 ug/L 88 68-138
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QC Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-1Lab Sample ID: 490-95901-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314019
cis-1,3-Dichloropropene ND 50.0 43.20 ug/L 86 71-141
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dibromo-3-Chloropropane ND F1 50.0 25.26 F1 ug/L 51 52-126
1,2-Dibromoethane (EDB)ND 50.0 43.70 ug/L 87 75-137
Dibromomethane ND 50.0 48.03 ug/L 96 58-140
1,2-Dichlorobenzene ND 50.0 45.07 ug/L 90 79-128
1,4-Dichlorobenzene ND 50.0 46.25 ug/L 93 78-126
1,1-Dichloroethane ND 50.0 47.38 ug/L 95 71-139
1,2-Dichloroethane ND 50.0 51.17 ug/L 102 64-136
1,1-Dichloroethene ND 50.0 46.96 ug/L 94 70-142
1,2-Dichloropropane ND 50.0 43.43 ug/L 87 67-131
Ethylbenzene ND 50.0 43.56 ug/L 87 79-139
2-Hexanone ND 250 162.3 ug/L 65 50-150
Iodomethane ND 50.0 50.64 ug/L 101 34-191
Methylene Chloride ND 50.0 42.10 ug/L 84 64-139
4-Methyl-2-pentanone (MIBK)ND 250 164.8 ug/L 66 50-147
Styrene ND 50.0 44.49 ug/L 89 61-148
1,1,1,2-Tetrachloroethane ND 50.0 53.80 ug/L 108 73-141
1,1,2,2-Tetrachloroethane ND 50.0 37.42 ug/L 75 56-143
Tetrachloroethene ND 50.0 50.24 ug/L 100 72-145
Toluene ND 50.0 43.45 ug/L 87 75-136
trans-1,4-Dichloro-2-butene ND 50.0 30.60 ug/L 61 29-156
trans-1,2-Dichloroethene ND 50.0 44.33 ug/L 89 66-143
trans-1,3-Dichloropropene ND 50.0 39.77 ug/L 80 59-135
1,1,1-Trichloroethane ND 50.0 53.52 ug/L 107 76-149
1,1,2-Trichloroethane ND 50.0 44.12 ug/L 88 74-134
Trichloroethene ND 50.0 49.41 ug/L 99 73-144
Trichlorofluoromethane ND * F1 50.0 64.28 ug/L 129 58-139
1,2,3-Trichloropropane ND 50.0 42.16 ug/L 84 53-144
Vinyl acetate ND 100 60.17 ug/L 60 37-154
Vinyl chloride ND 50.0 46.32 ug/L 93 56-129
Xylenes, Total ND 100 89.30 ug/L 89 74-141
4-Bromofluorobenzene (Surr)70 -130
Surrogate
85
MS MS
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
951,2-Dichloroethane-d4 (Surr)70 -130
97Toluene-d8 (Surr)70 -130
Client Sample ID: MW-1Lab Sample ID: 490-95901-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314019
Acetone ND 250 168.1 ug/L 67 45-141 8 21
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile ND 500 356.1 ug/L 71 50-148 3 18
Benzene ND 50.0 43.20 ug/L 86 75-133 1 17
Bromochloromethane ND 50.0 45.50 ug/L 91 67-139 0 17
Bromodichloromethane ND 50.0 50.60 ug/L 101 70-140 2 18
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QC Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-1Lab Sample ID: 490-95901-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314019
Bromoform ND 50.0 57.20 E ug/L 114 42-147 2 16
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromomethane ND 50.0 64.44 E ug/L 129 16-163 7 50
2-Butanone (MEK)ND 250 174.8 ug/L 70 50-138 1 19
Carbon disulfide ND 50.0 46.51 ug/L 93 48-152 3 21
Carbon tetrachloride ND 50.0 61.06 ug/L 122 62-164 2 19
Chlorobenzene ND 50.0 46.92 ug/L 94 80-129 1 14
Chlorodibromomethane ND 50.0 56.44 E ug/L 113 66-140 0 15
Chloroethane ND 50.0 47.40 ug/L 95 58-137 3 20
Chloroform ND 50.0 51.17 ug/L 102 66-138 1 18
Chloromethane ND 50.0 45.88 ug/L 92 10-169 11 31
cis-1,2-Dichloroethene ND 50.0 45.17 ug/L 90 68-138 2 17
cis-1,3-Dichloropropene ND 50.0 44.73 ug/L 89 71-141 3 15
1,2-Dibromo-3-Chloropropane ND F1 50.0 24.97 F1 ug/L 50 52-126 1 24
1,2-Dibromoethane (EDB)ND 50.0 45.05 ug/L 90 75-137 3 15
Dibromomethane ND 50.0 47.32 ug/L 95 58-140 1 16
1,2-Dichlorobenzene ND 50.0 45.28 ug/L 91 79-128 0 15
1,4-Dichlorobenzene ND 50.0 45.79 ug/L 92 78-126 1 15
1,1-Dichloroethane ND 50.0 48.85 ug/L 98 71-139 3 17
1,2-Dichloroethane ND 50.0 50.28 ug/L 101 64-136 2 17
1,1-Dichloroethene ND 50.0 51.29 ug/L 103 70-142 9 17
1,2-Dichloropropane ND 50.0 43.68 ug/L 87 67-131 1 17
Ethylbenzene ND 50.0 43.42 ug/L 87 79-139 0 15
2-Hexanone ND 250 165.1 ug/L 66 50-150 2 15
Iodomethane ND 50.0 57.13 ug/L 114 34-191 12 23
Methylene Chloride ND 50.0 43.09 ug/L 86 64-139 2 17
4-Methyl-2-pentanone (MIBK)ND 250 169.1 ug/L 68 50-147 3 17
Styrene ND 50.0 45.32 ug/L 91 61-148 2 24
1,1,1,2-Tetrachloroethane ND 50.0 53.47 ug/L 107 73-141 1 16
1,1,2,2-Tetrachloroethane ND 50.0 37.48 ug/L 75 56-143 0 20
Tetrachloroethene ND 50.0 51.21 ug/L 102 72-145 2 16
Toluene ND 50.0 44.45 ug/L 89 75-136 2 15
trans-1,4-Dichloro-2-butene ND 50.0 32.05 ug/L 64 29-156 5 26
trans-1,2-Dichloroethene ND 50.0 45.80 ug/L 92 66-143 3 16
trans-1,3-Dichloropropene ND 50.0 40.61 ug/L 81 59-135 2 14
1,1,1-Trichloroethane ND 50.0 53.40 ug/L 107 76-149 0 17
1,1,2-Trichloroethane ND 50.0 45.45 ug/L 91 74-134 3 15
Trichloroethene ND 50.0 50.08 ug/L 100 73-144 1 17
Trichlorofluoromethane ND * F1 50.0 71.98 F1 ug/L 144 58-139 11 18
1,2,3-Trichloropropane ND 50.0 41.12 ug/L 82 53-144 3 19
Vinyl acetate ND 100 62.14 ug/L 62 37-154 3 21
Vinyl chloride ND 50.0 49.01 ug/L 98 56-129 6 17
Xylenes, Total ND 100 89.84 ug/L 90 74-141 1 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
85
MSD MSD
Qualifier Limits%Recovery
107Dibromofluoromethane (Surr)70 -130
891,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Client Sample ID: Method BlankLab Sample ID: MB 490-314254/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314254
RL MDL
Acetone ND 25.0 2.66 ug/L 01/22/16 00:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.50010.0 ug/L 01/22/16 00:17 1Acrylonitrile
ND 0.2001.00 ug/L 01/22/16 00:17 1Benzene
ND 0.1501.00 ug/L 01/22/16 00:17 1Bromochloromethane
ND 0.1701.00 ug/L 01/22/16 00:17 1Bromodichloromethane
ND 0.2901.00 ug/L 01/22/16 00:17 1Bromoform
ND 0.3501.00 ug/L 01/22/16 00:17 1Bromomethane
ND 2.6450.0 ug/L 01/22/16 00:17 12-Butanone (MEK)
ND 0.2201.00 ug/L 01/22/16 00:17 1Carbon disulfide
ND 0.1801.00 ug/L 01/22/16 00:17 1Carbon tetrachloride
ND 0.1801.00 ug/L 01/22/16 00:17 1Chlorobenzene
ND 0.2501.00 ug/L 01/22/16 00:17 1Chlorodibromomethane
ND 0.3601.00 ug/L 01/22/16 00:17 1Chloroethane
ND 0.2301.00 ug/L 01/22/16 00:17 1Chloroform
ND 0.3601.00 ug/L 01/22/16 00:17 1Chloromethane
ND 0.2101.00 ug/L 01/22/16 00:17 1cis-1,2-Dichloroethene
ND 0.1701.00 ug/L 01/22/16 00:17 1cis-1,3-Dichloropropene
ND 0.94010.0 ug/L 01/22/16 00:17 11,2-Dibromo-3-Chloropropane
ND 0.2101.00 ug/L 01/22/16 00:17 11,2-Dibromoethane (EDB)
ND 0.4501.00 ug/L 01/22/16 00:17 1Dibromomethane
ND 0.1901.00 ug/L 01/22/16 00:17 11,2-Dichlorobenzene
ND 0.1701.00 ug/L 01/22/16 00:17 11,4-Dichlorobenzene
ND 0.2401.00 ug/L 01/22/16 00:17 11,1-Dichloroethane
ND 0.2001.00 ug/L 01/22/16 00:17 11,2-Dichloroethane
ND 0.2501.00 ug/L 01/22/16 00:17 11,1-Dichloroethene
ND 0.2501.00 ug/L 01/22/16 00:17 11,2-Dichloropropane
ND 0.1901.00 ug/L 01/22/16 00:17 1Ethylbenzene
ND 1.2810.0 ug/L 01/22/16 00:17 12-Hexanone
ND 1.5010.0 ug/L 01/22/16 00:17 1Iodomethane
ND 1.001.00 ug/L 01/22/16 00:17 1Methylene Chloride
ND 0.81010.0 ug/L 01/22/16 00:17 14-Methyl-2-pentanone (MIBK)
ND 0.2801.00 ug/L 01/22/16 00:17 1Styrene
ND 0.1501.00 ug/L 01/22/16 00:17 11,1,1,2-Tetrachloroethane
ND 0.1901.00 ug/L 01/22/16 00:17 11,1,2,2-Tetrachloroethane
ND 0.1401.00 ug/L 01/22/16 00:17 1Tetrachloroethene
ND 0.1701.00 ug/L 01/22/16 00:17 1Toluene
ND 0.4605.00 ug/L 01/22/16 00:17 1trans-1,4-Dichloro-2-butene
ND 0.2301.00 ug/L 01/22/16 00:17 1trans-1,2-Dichloroethene
ND 0.1701.00 ug/L 01/22/16 00:17 1trans-1,3-Dichloropropene
ND 0.1901.00 ug/L 01/22/16 00:17 11,1,1-Trichloroethane
ND 0.1901.00 ug/L 01/22/16 00:17 11,1,2-Trichloroethane
ND 0.2001.00 ug/L 01/22/16 00:17 1Trichloroethene
ND 0.2101.00 ug/L 01/22/16 00:17 1Trichlorofluoromethane
ND 0.2301.00 ug/L 01/22/16 00:17 11,2,3-Trichloropropane
ND 1.7110.0 ug/L 01/22/16 00:17 1Vinyl acetate
ND 0.1801.00 ug/L 01/22/16 00:17 1Vinyl chloride
ND 0.5803.00 ug/L 01/22/16 00:17 1Xylenes, Total
4-Bromofluorobenzene (Surr)94 70-130 01/22/16 00:17 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
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QC Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-314254/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314254
Dibromofluoromethane (Surr)98 70-130 01/22/16 00:17 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
94 01/22/16 00:17 11,2-Dichloroethane-d4 (Surr)70-130
99 01/22/16 00:17 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-314254/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314254
Acetone 100 79.81 ug/L 80 54-145
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 157.9 ug/L 79 61-140
Benzene 20.0 19.71 ug/L 99 80-121
Bromochloromethane 20.0 19.56 ug/L 98 78-129
Bromodichloromethane 20.0 19.99 ug/L 100 75-129
Bromoform 20.0 19.44 ug/L 97 46-145
Bromomethane 20.0 26.85 ug/L 134 41-150
2-Butanone (MEK)100 82.54 ug/L 83 62-133
Carbon disulfide 20.0 20.70 ug/L 103 77-126
Carbon tetrachloride 20.0 23.67 ug/L 118 64-147
Chlorobenzene 20.0 19.80 ug/L 99 80-120
Chlorodibromomethane 20.0 18.80 ug/L 94 69-133
Chloroethane 20.0 20.37 ug/L 102 72-120
Chloroform 20.0 21.67 ug/L 108 73-129
Chloromethane 20.0 18.65 ug/L 93 12-150
cis-1,2-Dichloroethene 20.0 19.52 ug/L 98 76-125
cis-1,3-Dichloropropene 20.0 15.77 ug/L 79 74-140
1,2-Dibromo-3-Chloropropane 20.0 10.86 ug/L 54 54-125
1,2-Dibromoethane (EDB)20.0 18.31 ug/L 92 80-129
Dibromomethane 20.0 20.36 ug/L 102 71-125
1,2-Dichlorobenzene 20.0 19.77 ug/L 99 80-121
1,4-Dichlorobenzene 20.0 20.23 ug/L 101 80-120
1,1-Dichloroethane 20.0 19.88 ug/L 99 78-125
1,2-Dichloroethane 20.0 22.08 ug/L 110 77-121
1,1-Dichloroethene 20.0 21.02 ug/L 105 79-124
1,2-Dichloropropane 20.0 19.52 ug/L 98 75-120
Ethylbenzene 20.0 18.95 ug/L 95 80-130
2-Hexanone 100 65.16 ug/L 65 60-142
Iodomethane 20.0 20.74 ug/L 104 40-150
Methylene Chloride 20.0 19.62 ug/L 98 79-123
4-Methyl-2-pentanone (MIBK)100 68.41 ug/L 68 60-137
Styrene 20.0 18.06 ug/L 90 80-127
1,1,1,2-Tetrachloroethane 20.0 19.25 ug/L 96 74-135
1,1,2,2-Tetrachloroethane 20.0 16.72 ug/L 84 69-131
Tetrachloroethene 20.0 20.93 ug/L 105 80-126
Toluene 20.0 19.11 ug/L 96 80-126
trans-1,4-Dichloro-2-butene 20.0 14.95 ug/L 75 41-147
trans-1,2-Dichloroethene 20.0 19.72 ug/L 99 79-126
trans-1,3-Dichloropropene 20.0 13.81 ug/L 69 63-134
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QC Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-314254/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314254
1,1,1-Trichloroethane 20.0 21.78 ug/L 109 78-135
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1,2-Trichloroethane 20.0 19.16 ug/L 96 80-124
Trichloroethene 20.0 21.45 ug/L 107 80-123
Trichlorofluoromethane 20.0 26.54 * ug/L 133 65-124
1,2,3-Trichloropropane 20.0 18.27 ug/L 91 70-131
Vinyl acetate 40.0 29.03 ug/L 73 54-139
Vinyl chloride 20.0 21.06 ug/L 105 68-120
Xylenes, Total 40.0 37.99 ug/L 95 80-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
941,2-Dichloroethane-d4 (Surr)70 -130
98Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-314254/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314254
Acetone 100 72.76 ug/L 73 54-145 9 21
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 151.6 ug/L 76 61-140 4 18
Benzene 20.0 18.77 ug/L 94 80-121 5 17
Bromochloromethane 20.0 17.96 ug/L 90 78-129 9 17
Bromodichloromethane 20.0 17.57 ug/L 88 75-129 13 18
Bromoform 20.0 18.53 ug/L 93 46-145 5 16
Bromomethane 20.0 22.53 ug/L 113 41-150 17 50
2-Butanone (MEK)100 71.13 ug/L 71 62-133 15 19
Carbon disulfide 20.0 19.28 ug/L 96 77-126 7 21
Carbon tetrachloride 20.0 22.44 ug/L 112 64-147 5 19
Chlorobenzene 20.0 19.01 ug/L 95 80-120 4 14
Chlorodibromomethane 20.0 18.24 ug/L 91 69-133 3 15
Chloroethane 20.0 18.12 ug/L 91 72-120 12 20
Chloroform 20.0 20.45 ug/L 102 73-129 6 18
Chloromethane 20.0 17.17 ug/L 86 12-150 8 31
cis-1,2-Dichloroethene 20.0 18.26 ug/L 91 76-125 7 17
cis-1,3-Dichloropropene 20.0 15.08 ug/L 75 74-140 4 15
1,2-Dibromo-3-Chloropropane 20.0 10.85 ug/L 54 54-125 0 24
1,2-Dibromoethane (EDB)20.0 16.72 ug/L 84 80-129 9 15
Dibromomethane 20.0 18.54 ug/L 93 71-125 9 16
1,2-Dichlorobenzene 20.0 19.01 ug/L 95 80-121 4 15
1,4-Dichlorobenzene 20.0 19.46 ug/L 97 80-120 4 15
1,1-Dichloroethane 20.0 19.42 ug/L 97 78-125 2 17
1,2-Dichloroethane 20.0 20.57 ug/L 103 77-121 7 17
1,1-Dichloroethene 20.0 20.02 ug/L 100 79-124 5 17
1,2-Dichloropropane 20.0 17.95 ug/L 90 75-120 8 17
Ethylbenzene 20.0 18.13 ug/L 91 80-130 4 15
2-Hexanone 100 63.19 ug/L 63 60-142 3 15
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QC Sample Results
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-314254/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 314254
Iodomethane 20.0 20.95 ug/L 105 40-150 1 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Methylene Chloride 20.0 17.47 ug/L 87 79-123 12 17
4-Methyl-2-pentanone (MIBK)100 67.97 ug/L 68 60-137 1 17
Styrene 20.0 17.54 ug/L 88 80-127 3 24
1,1,1,2-Tetrachloroethane 20.0 18.51 ug/L 93 74-135 4 16
1,1,2,2-Tetrachloroethane 20.0 15.66 ug/L 78 69-131 7 20
Tetrachloroethene 20.0 20.70 ug/L 103 80-126 1 16
Toluene 20.0 18.45 ug/L 92 80-126 4 15
trans-1,4-Dichloro-2-butene 20.0 14.40 ug/L 72 41-147 4 26
trans-1,2-Dichloroethene 20.0 18.81 ug/L 94 79-126 5 16
trans-1,3-Dichloropropene 20.0 13.05 ug/L 65 63-134 6 14
1,1,1-Trichloroethane 20.0 20.27 ug/L 101 78-135 7 17
1,1,2-Trichloroethane 20.0 17.46 ug/L 87 80-124 9 15
Trichloroethene 20.0 20.74 ug/L 104 80-123 3 17
Trichlorofluoromethane 20.0 25.76 * ug/L 129 65-124 3 18
1,2,3-Trichloropropane 20.0 17.88 ug/L 89 70-131 2 19
Vinyl acetate 40.0 27.18 ug/L 68 54-139 7 21
Vinyl chloride 20.0 19.71 ug/L 99 68-120 7 17
Xylenes, Total 40.0 36.45 ug/L 91 80-132 4 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
92
LCSD LCSD
Qualifier Limits%Recovery
102Dibromofluoromethane (Surr)70 -130
901,2-Dichloroethane-d4 (Surr)70 -130
96Toluene-d8 (Surr)70 -130
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QC Association Summary
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
GC/MS VOA
Analysis Batch: 314019
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-95901-2 MW-1 Total/NA
Water 8260B490-95901-2 MS MW-1 Total/NA
Water 8260B490-95901-2 MSD MW-1 Total/NA
Water 8260B490-95901-3 MW-1D Total/NA
Water 8260B490-95901-4 MW-2A Total/NA
Water 8260B490-95901-5 MW-2D Total/NA
Water 8260B490-95901-6 MW-3 Total/NA
Water 8260B490-95901-7 MW-3D Total/NA
Water 8260B490-95901-8 MW-4 Total/NA
Water 8260B490-95901-9 MW-4D Total/NA
Water 8260B490-95901-10 MW-11 Total/NA
Water 8260B490-95901-11 MW-11D Total/NA
Water 8260B490-95901-12 MW-12 Total/NA
Water 8260B490-95901-13 MW-12D Total/NA
Water 8260B490-95901-14 SW-1 Total/NA
Water 8260B490-95901-15 MW-4R Total/NA
Water 8260B490-95901-16 MW-4DR Total/NA
Water 8260B490-95901-17 FIELDBLANK Total/NA
Water 8260BLCS 490-314019/4 Lab Control Sample Total/NA
Water 8260BLCSD 490-314019/5 Lab Control Sample Dup Total/NA
Water 8260BMB 490-314019/7 Method Blank Total/NA
Analysis Batch: 314254
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-95901-1 TRIPBLANK Total/NA
Water 8260BLCS 490-314254/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-314254/4 Lab Control Sample Dup Total/NA
Water 8260BMB 490-314254/6 Method Blank Total/NA
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Lab Chronicle
Client: Duke Energy Corporation TestAmerica Job ID: 490-95901-1
Project/Site: MNS Landfill #1 J16010006
Client Sample ID: TRIPBLANK Lab Sample ID: 490-95901-1
Matrix: WaterDate Collected: 01/14/16 05:35
Date Received: 01/16/16 09:20
Analysis 8260B 01/22/16 00:44 JPH1 314254 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-1 Lab Sample ID: 490-95901-2
Matrix: WaterDate Collected: 01/14/16 08:50
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 14:21 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-1D Lab Sample ID: 490-95901-3
Matrix: WaterDate Collected: 01/14/16 09:05
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 14:48 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-2A Lab Sample ID: 490-95901-4
Matrix: WaterDate Collected: 01/14/16 13:30
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 15:15 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-2D Lab Sample ID: 490-95901-5
Matrix: WaterDate Collected: 01/14/16 14:25
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 15:42 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-3 Lab Sample ID: 490-95901-6
Matrix: WaterDate Collected: 01/14/16 10:00
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 16:10 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
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Lab Chronicle
Client: Duke Energy Corporation TestAmerica Job ID: 490-95901-1
Project/Site: MNS Landfill #1 J16010006
Client Sample ID: MW-3D Lab Sample ID: 490-95901-7
Matrix: WaterDate Collected: 01/14/16 10:20
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 16:37 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-4 Lab Sample ID: 490-95901-8
Matrix: WaterDate Collected: 01/14/16 07:50
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 17:04 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-4D Lab Sample ID: 490-95901-9
Matrix: WaterDate Collected: 01/14/16 08:35
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 17:31 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-11 Lab Sample ID: 490-95901-10
Matrix: WaterDate Collected: 01/14/16 10:45
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 17:58 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-11D Lab Sample ID: 490-95901-11
Matrix: WaterDate Collected: 01/14/16 11:30
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 18:25 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-12 Lab Sample ID: 490-95901-12
Matrix: WaterDate Collected: 01/14/16 12:50
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 18:52 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Nashville
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Lab Chronicle
Client: Duke Energy Corporation TestAmerica Job ID: 490-95901-1
Project/Site: MNS Landfill #1 J16010006
Client Sample ID: MW-12D Lab Sample ID: 490-95901-13
Matrix: WaterDate Collected: 01/14/16 13:10
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 19:19 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: SW-1 Lab Sample ID: 490-95901-14
Matrix: WaterDate Collected: 01/14/16 12:20
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 19:46 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-4R Lab Sample ID: 490-95901-15
Matrix: WaterDate Collected: 01/14/16 11:20
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 20:13 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-4DR Lab Sample ID: 490-95901-16
Matrix: WaterDate Collected: 01/14/16 11:45
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 20:41 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: FIELDBLANK Lab Sample ID: 490-95901-17
Matrix: WaterDate Collected: 01/14/16 14:45
Date Received: 01/16/16 09:20
Analysis 8260B 01/21/16 13:54 JJR1 314019 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-95901-1Client: Duke Energy Corporation
Project/Site: MNS Landfill #1 J16010006
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Duke Energy Corporation TestAmerica Job ID: 490-95901-1
Project/Site: MNS Landfill #1 J16010006
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Duke Energy Corporation Job Number: 490-95901-1
Login Number: 95901
Question Answer Comment
Creator: Vest, Laura E
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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Page 89 of 90
Page 90 of 90
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J16010007
Project Name:MCGUIRE -
Lab Contact:Peggy Kendall
Date:2/6/2016
Customer Address:13225 Hagers Ferry Rd
Customer Name(s):TIM HUNSUCKER, CHUCK CAMPBELL
Mail Code: MG01CH
Huntersville, NC 28078-8985
Phone:
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Peggy Kendall) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Peggy Kendall
Page 1 of 7
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2016000054 MCGUIRE 14-Jan-16 12:20 PM PSP SW-1
1 Total Samples
Page 2 of 7
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:2/2/2016
Electronic Data Deliverable (EDD) Sent Separatel
Page 3 of 7
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010007
2016000054
Collection Date:14-Jan-16 12:20 PM
Site:SW-1
Matrix:GW_RCRA
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP
Barium (Ba)0.031 mg/L SW 6010C 01/21/2016 14:39 FCJORDA0.005 1
Chromium (Cr)< 0.005 mg/L SW 6010C 01/21/2016 14:39 FCJORDA0.005 1
Silver (Ag)< 0.005 mg/L SW 6010C 01/21/2016 14:39 FCJORDA0.005 1
DISSOLVED METALS BY ICP-MS
Arsenic (As)< 1 ug/L EPA 200.8 01/29/2016 14:03 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 01/29/2016 14:03 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 01/29/2016 14:03 JAHERMA11
Page 4 of 7
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010007
Q16010452 ICP Dissolved DISSOLVED METALS BY ICP
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Barium (Ba) 0.98 1 98mg/L -1158510.98
Chromium (Cr) 1.02 1 102mg/L -1158511.02
Silver (Ag) 0.975 1 97.5mg/L -1158510.975
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16010005 -- 2016000033
Barium (Ba) 5.66 5 113mg/L -1307015.66
Chromium (Cr) 5.5 5 110mg/L -1307015.5
Silver (Ag) 4.82 5 96.4mg/L -1307014.82
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16010005 -- 2016000033
Barium (Ba) 5.58 5 111 1.56mg/L -1307015.58
Chromium (Cr) 5.46 5 109 0.73mg/L -1307015.46
Silver (Ag) 4.77 5 95.5 0.938mg/L -1307014.77
Page 5 of 7
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J16010007
Q16010505 IMS Dissolved DISSOLVED METALS BY ICP-MS
Level II QC Summary
Final QualifierDilMeasuredUnits:Parameter
Blank # 1
RDL Relative Concentration
Arsenic (As) 0.007 ug/L -10.007 1 < 1/2 RDL
Cadmium (Cd) 0 ug/L -10 1 < 1/2 RDL
Lead (Pb) -0.006 ug/L -1-0.006 1 < 1/2 RDL
Final QualifierDilMeasuredUnits:Parameter
LCS # 1
% Recovery LCL UCLSpike
Arsenic (As) 83 80 104ug/L -11585183
Cadmium (Cd) 8.25 8 103ug/L -1158518.25
Lead (Pb) 82.2 80 103ug/L -11585182.2
Final QualifierDilMeasuredUnits:Parameter
MS # 1
% Recovery LCL UCLSpike
Parent Sample: J16010005 -- 2016000033
Arsenic (As) 50 50 99.8ug/L -13070150
Cadmium (Cd) 50.1 50 100ug/L -13070150.1
Lead (Pb) 50.3 50 101ug/L -13070150.3
Final QualifierDilMeasuredUnits:Parameter
MSD # 1
RPD% Recovery LCL UCLSpike
Parent Sample: J16010005 -- 2016000033
Arsenic (As) 46.6 50 93 7.08ug/L -13070146.6
Cadmium (Cd) 45.9 50 91.9 8.71ug/L -13070145.9
Lead (Pb) 46.6 50 93.1 7.83ug/L -13070146.6
Page 6 of 7
Page 7 of 7
Radiological Data for MCGUIRE
397997Sample #:Station:MCGUIRE
Collection End: 1/14/2016 08:50:00
Collection Start:1/14/2016 08:50:00Location:MW-1_ML1 [ MNS Landfill 1 / MW-1 ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha 6.36E-01 4.88E-01 7.02E-01
Beta 2.02E+00 7.57E-01 1.14E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.08E+00 0.00E+00 4.08E+00 <1000 LLD OK<15
Co-58 <5.57E+00 0.00E+00 5.57E+00 <1000 LLD OK<15
Fe-59 <8.95E+00 0.00E+00 8.95E+00 <400 LLD OK<30
Co-60 <5.36E+00 0.00E+00 5.36E+00 <300 LLD OK<15
Zn-65 <8.71E+00 0.00E+00 8.71E+00 <300 LLD OK<30
Zr-95 <1.10E+01 0.00E+00 1.10E+01 <400 LLD OK<15
Nb-95 <6.84E+00 0.00E+00 6.84E+00 <400 LLD OK<15
I-131 <7.16E+00 0.00E+00 7.16E+00 LLD OK<15
Cs-134 <7.28E+00 0.00E+00 7.28E+00 <30 LLD OK<15
Cs-137 <6.90E+00 0.00E+00 6.90E+00 <50 LLD OK<18
BaLa-140 <1.02E+01 0.00E+00 1.02E+01 <200 LLD OK<15
Be-7 <5.42E+01 0.00E+00 5.42E+01
K-40 <8.21E+01 0.00E+00 8.21E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <1.00E+01 0.00E+00 2.05E+02 <20000 LLD OK<250
397998Sample #:Station:MCGUIRE
Collection End: 1/14/2016 09:05:00
Collection Start:1/14/2016 09:05:00Location:MW-1D_ML1 [ MNS Landfill 1 / MW-1D ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-5.7E-03 0.00E+00 7.43E-01
Beta 1.05E+00 7.44E-01 1.21E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.45E+00 0.00E+00 5.45E+00 <1000 LLD OK<15
Co-58 <5.57E+00 0.00E+00 5.57E+00 <1000 LLD OK<15
Fe-59 <1.13E+01 0.00E+00 1.13E+01 <400 LLD OK<30
Page 1 of 12Report Generated @ 2/10/2016 16:20:56
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EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 1 of 13 02.10.2016
Radiological Data for MCGUIRE
397998Sample #:Station:MCGUIRE
Collection End: 1/14/2016 09:05:00
Collection Start:1/14/2016 09:05:00Location:MW-1D_ML1 [ MNS Landfill 1 / MW-1D ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <6.13E+00 0.00E+00 6.13E+00 <300 LLD OK<15
Zn-65 <1.15E+01 0.00E+00 1.15E+01 <300 LLD OK<30
Zr-95 <1.07E+01 0.00E+00 1.07E+01 <400 LLD OK<15
Nb-95 <6.33E+00 0.00E+00 6.33E+00 <400 LLD OK<15
I-131 <7.68E+00 0.00E+00 7.68E+00 LLD OK<15
Cs-134 <6.11E+00 0.00E+00 6.11E+00 <30 LLD OK<15
Cs-137 <6.90E+00 0.00E+00 6.90E+00 <50 LLD OK<18
BaLa-140 <9.03E+00 0.00E+00 9.03E+00 <200 LLD OK<15
Be-7 <5.33E+01 0.00E+00 5.33E+01
K-40 3.20E+01 4.95E+01 8.33E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-2.2E+01 0.00E+00 2.07E+02 <20000 LLD OK<250
397999Sample #:Station:MCGUIRE
Collection End: 1/14/2016 13:30:00
Collection Start:1/14/2016 13:30:00Location:MW-2A_ML1 [ MNS Landfill 1 / MW-2A ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <1.41E-01 0.00E+00 6.76E-01
Beta <5.02E-01 0.00E+00 1.13E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.94E+00 0.00E+00 4.94E+00 <1000 LLD OK<15
Co-58 <4.54E+00 0.00E+00 4.54E+00 <1000 LLD OK<15
Fe-59 <9.78E+00 0.00E+00 9.78E+00 <400 LLD OK<30
Co-60 <5.53E+00 0.00E+00 5.53E+00 <300 LLD OK<15
Zn-65 <1.18E+01 0.00E+00 1.18E+01 <300 LLD OK<30
Zr-95 <9.55E+00 0.00E+00 9.55E+00 <400 LLD OK<15
Nb-95 <6.08E+00 0.00E+00 6.08E+00 <400 LLD OK<15
I-131 <8.63E+00 0.00E+00 8.63E+00 LLD OK<15
Cs-134 <6.02E+00 0.00E+00 6.02E+00 <30 LLD OK<15
Cs-137 <6.14E+00 0.00E+00 6.14E+00 <50 LLD OK<18
BaLa-140 <7.06E+00 0.00E+00 7.06E+00 <200 LLD OK<15
Page 2 of 12Report Generated @ 2/10/2016 16:20:56
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EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 2 of 13 02.10.2016
Radiological Data for MCGUIRE
397999Sample #:Station:MCGUIRE
Collection End: 1/14/2016 13:30:00
Collection Start:1/14/2016 13:30:00Location:MW-2A_ML1 [ MNS Landfill 1 / MW-2A ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.71E+01 0.00E+00 4.71E+01
K-40 8.44E+01 6.06E+01 8.88E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-3.4E+01 0.00E+00 2.06E+02 <20000 LLD OK<250
398000Sample #:Station:MCGUIRE
Collection End: 1/14/2016 14:25:00
Collection Start:1/14/2016 14:25:00Location:MW-2D_ML1 [ MNS Landfill 1 / MW-2D ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <4.28E-02 0.00E+00 7.04E-01
Beta 7.52E-01 7.23E-01 1.20E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <4.59E+00 0.00E+00 4.59E+00 <1000 LLD OK<15
Co-58 <5.55E+00 0.00E+00 5.55E+00 <1000 LLD OK<15
Fe-59 <8.10E+00 0.00E+00 8.10E+00 <400 LLD OK<30
Co-60 <4.40E+00 0.00E+00 4.40E+00 <300 LLD OK<15
Zn-65 <1.15E+01 0.00E+00 1.15E+01 <300 LLD OK<30
Zr-95 <8.96E+00 0.00E+00 8.96E+00 <400 LLD OK<15
Nb-95 <5.36E+00 0.00E+00 5.36E+00 <400 LLD OK<15
I-131 <6.78E+00 0.00E+00 6.78E+00 LLD OK<15
Cs-134 <4.57E+00 0.00E+00 4.57E+00 <30 LLD OK<15
Cs-137 <5.83E+00 0.00E+00 5.83E+00 <50 LLD OK<18
BaLa-140 <7.57E+00 0.00E+00 7.57E+00 <200 LLD OK<15
Be-7 <4.97E+01 0.00E+00 4.97E+01
K-40 <7.95E+01 0.00E+00 7.95E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-8.1E+01 0.00E+00 2.02E+02 <20000 LLD OK<250
Page 3 of 12Report Generated @ 2/10/2016 16:20:56
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 3 of 13 02.10.2016
Radiological Data for MCGUIRE
398001Sample #:Station:MCGUIRE
Collection End: 1/14/2016 10:00:00
Collection Start:1/14/2016 10:00:00Location:MW-3_ML1 [ MNS Landfill 1 / MW-3 ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <2.79E-01 0.00E+00 7.06E-01
Beta 6.87E-01 7.22E-01 1.20E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.49E+00 0.00E+00 5.49E+00 <1000 LLD OK<15
Co-58 <5.40E+00 0.00E+00 5.40E+00 <1000 LLD OK<15
Fe-59 <9.64E+00 0.00E+00 9.64E+00 <400 LLD OK<30
Co-60 <4.46E+00 0.00E+00 4.46E+00 <300 LLD OK<15
Zn-65 <1.16E+01 0.00E+00 1.16E+01 <300 LLD OK<30
Zr-95 <1.01E+01 0.00E+00 1.01E+01 <400 LLD OK<15
Nb-95 <6.86E+00 0.00E+00 6.86E+00 <400 LLD OK<15
I-131 <6.95E+00 0.00E+00 6.95E+00 LLD OK<15
Cs-134 <4.91E+00 0.00E+00 4.91E+00 <30 LLD OK<15
Cs-137 <6.04E+00 0.00E+00 6.04E+00 <50 LLD OK<18
BaLa-140 <6.96E+00 0.00E+00 6.96E+00 <200 LLD OK<15
Be-7 <5.28E+01 0.00E+00 5.28E+01
K-40 6.33E+01 4.99E+01 7.32E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <3.15E+01 0.00E+00 2.02E+02 <20000 LLD OK<250
398002Sample #:Station:MCGUIRE
Collection End: 1/14/2016 10:20:00
Collection Start:1/14/2016 10:20:00Location:MW-3D_ML1 [ MNS Landfill 1 / MW-3D ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <4.45E-02 0.00E+00 7.26E-01
Beta 1.26E+00 7.21E-01 1.15E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <6.65E+00 0.00E+00 6.65E+00 <1000 LLD OK<15
Co-58 <6.26E+00 0.00E+00 6.26E+00 <1000 LLD OK<15
Fe-59 <1.16E+01 0.00E+00 1.16E+01 <400 LLD OK<30
Page 4 of 12Report Generated @ 2/10/2016 16:20:56
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 4 of 13 02.10.2016
Radiological Data for MCGUIRE
398002Sample #:Station:MCGUIRE
Collection End: 1/14/2016 10:20:00
Collection Start:1/14/2016 10:20:00Location:MW-3D_ML1 [ MNS Landfill 1 / MW-3D ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <6.69E+00 0.00E+00 6.69E+00 <300 LLD OK<15
Zn-65 <1.35E+01 0.00E+00 1.35E+01 <300 LLD OK<30
Zr-95 <9.92E+00 0.00E+00 9.92E+00 <400 LLD OK<15
Nb-95 <6.46E+00 0.00E+00 6.46E+00 <400 LLD OK<15
I-131 <8.16E+00 0.00E+00 8.16E+00 LLD OK<15
Cs-134 <6.88E+00 0.00E+00 6.88E+00 <30 LLD OK<15
Cs-137 <6.14E+00 0.00E+00 6.14E+00 <50 LLD OK<18
BaLa-140 <1.10E+01 0.00E+00 1.10E+01 <200 LLD OK<15
Be-7 <5.28E+01 0.00E+00 5.28E+01
K-40 <1.21E+02 0.00E+00 1.21E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-6.0E+00 0.00E+00 2.04E+02 <20000 LLD OK<250
398003Sample #:Station:MCGUIRE
Collection End: 1/14/2016 07:50:00
Collection Start:1/14/2016 07:50:00Location:MW-4_ML1 [ MNS Landfill 1 / MW-4 ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <3.20E-01 0.00E+00 8.25E-01
Beta 1.75E+00 7.96E-01 1.24E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.68E+00 0.00E+00 5.68E+00 <1000 LLD OK<15
Co-58 <5.19E+00 0.00E+00 5.19E+00 <1000 LLD OK<15
Fe-59 <1.19E+01 0.00E+00 1.19E+01 <400 LLD OK<30
Co-60 <4.97E+00 0.00E+00 4.97E+00 <300 LLD OK<15
Zn-65 <1.38E+01 0.00E+00 1.38E+01 <300 LLD OK<30
Zr-95 <1.04E+01 0.00E+00 1.04E+01 <400 LLD OK<15
Nb-95 <5.82E+00 0.00E+00 5.82E+00 <400 LLD OK<15
I-131 <7.55E+00 0.00E+00 7.55E+00 LLD OK<15
Cs-134 <6.15E+00 0.00E+00 6.15E+00 <30 LLD OK<15
Cs-137 <6.20E+00 0.00E+00 6.20E+00 <50 LLD OK<18
BaLa-140 <6.01E+00 0.00E+00 6.01E+00 <200 LLD OK<15
Page 5 of 12Report Generated @ 2/10/2016 16:20:56
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 5 of 13 02.10.2016
Radiological Data for MCGUIRE
398003Sample #:Station:MCGUIRE
Collection End: 1/14/2016 07:50:00
Collection Start:1/14/2016 07:50:00Location:MW-4_ML1 [ MNS Landfill 1 / MW-4 ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <3.77E+01 0.00E+00 3.77E+01
K-40 6.43E+01 5.31E+01 7.98E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <7.52E+01 0.00E+00 1.83E+02 <20000 LLD OK<250
398004Sample #:Station:MCGUIRE
Collection End: 1/14/2016 11:20:00
Collection Start:1/14/2016 11:20:00Location:MW-4R_ML1 [ MNS Landfill 1 / MW-4R ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.10E-02 0.00E+00 7.87E-01
Beta <2.59E-01 0.00E+00 1.23E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.79E+00 0.00E+00 5.79E+00 <1000 LLD OK<15
Co-58 <5.72E+00 0.00E+00 5.72E+00 <1000 LLD OK<15
Fe-59 <9.52E+00 0.00E+00 9.52E+00 <400 LLD OK<30
Co-60 <4.92E+00 0.00E+00 4.92E+00 <300 LLD OK<15
Zn-65 <6.72E+00 0.00E+00 6.72E+00 <300 LLD OK<30
Zr-95 <8.91E+00 0.00E+00 8.91E+00 <400 LLD OK<15
Nb-95 <6.27E+00 0.00E+00 6.27E+00 <400 LLD OK<15
I-131 <7.88E+00 0.00E+00 7.88E+00 LLD OK<15
Cs-134 <5.37E+00 0.00E+00 5.37E+00 <30 LLD OK<15
Cs-137 <6.41E+00 0.00E+00 6.41E+00 <50 LLD OK<18
BaLa-140 <7.73E+00 0.00E+00 7.73E+00 <200 LLD OK<15
Be-7 <5.00E+01 0.00E+00 5.00E+01
K-40 <1.03E+02 0.00E+00 1.03E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <7.52E+01 0.00E+00 1.83E+02 <20000 LLD OK<250
Page 6 of 12Report Generated @ 2/10/2016 16:20:56
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 6 of 13 02.10.2016
Radiological Data for MCGUIRE
398005Sample #:Station:MCGUIRE
Collection End: 1/14/2016 10:45:00
Collection Start:1/14/2016 10:45:00Location:MW-11_ML1 [ MNS Landfill 1 / MW-11 ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <1.17E-01 0.00E+00 5.98E-01
Beta <4.74E-01 0.00E+00 1.18E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.52E+00 0.00E+00 5.52E+00 <1000 LLD OK<15
Co-58 <5.39E+00 0.00E+00 5.39E+00 <1000 LLD OK<15
Fe-59 <1.11E+01 0.00E+00 1.11E+01 <400 LLD OK<30
Co-60 <5.37E+00 0.00E+00 5.37E+00 <300 LLD OK<15
Zn-65 <1.19E+01 0.00E+00 1.19E+01 <300 LLD OK<30
Zr-95 <1.06E+01 0.00E+00 1.06E+01 <400 LLD OK<15
Nb-95 <6.92E+00 0.00E+00 6.92E+00 <400 LLD OK<15
I-131 <8.39E+00 0.00E+00 8.39E+00 LLD OK<15
Cs-134 <7.14E+00 0.00E+00 7.14E+00 <30 LLD OK<15
Cs-137 <6.01E+00 0.00E+00 6.01E+00 <50 LLD OK<18
BaLa-140 <5.15E+00 0.00E+00 5.15E+00 <200 LLD OK<15
Be-7 <4.11E+01 0.00E+00 4.11E+01
K-40 <1.03E+02 0.00E+00 1.03E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <2.00E+01 0.00E+00 2.04E+02 <20000 LLD OK<250
398006Sample #:Station:MCGUIRE
Collection End: 1/14/2016 11:30:00
Collection Start:1/14/2016 11:30:00Location:MW-11D_ML1 [ MNS Landfill 1 / MW-11D ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <1.60E-01 0.00E+00 6.22E-01
Beta 1.16E+00 7.34E-01 1.18E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.77E+00 0.00E+00 5.77E+00 <1000 LLD OK<15
Co-58 <6.45E+00 0.00E+00 6.45E+00 <1000 LLD OK<15
Fe-59 <9.80E+00 0.00E+00 9.80E+00 <400 LLD OK<30
Page 7 of 12Report Generated @ 2/10/2016 16:20:56
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 7 of 13 02.10.2016
Radiological Data for MCGUIRE
398006Sample #:Station:MCGUIRE
Collection End: 1/14/2016 11:30:00
Collection Start:1/14/2016 11:30:00Location:MW-11D_ML1 [ MNS Landfill 1 / MW-11D ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <5.06E+00 0.00E+00 5.06E+00 <300 LLD OK<15
Zn-65 <1.05E+01 0.00E+00 1.05E+01 <300 LLD OK<30
Zr-95 <1.09E+01 0.00E+00 1.09E+01 <400 LLD OK<15
Nb-95 <6.29E+00 0.00E+00 6.29E+00 <400 LLD OK<15
I-131 <6.59E+00 0.00E+00 6.59E+00 LLD OK<15
Cs-134 <6.68E+00 0.00E+00 6.68E+00 <30 LLD OK<15
Cs-137 <6.30E+00 0.00E+00 6.30E+00 <50 LLD OK<18
BaLa-140 <7.12E+00 0.00E+00 7.12E+00 <200 LLD OK<15
Be-7 <3.56E+01 0.00E+00 3.56E+01
K-40 <1.15E+02 0.00E+00 1.15E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-3.6E+01 0.00E+00 2.06E+02 <20000 LLD OK<250
398007Sample #:Station:MCGUIRE
Collection End: 1/14/2016 12:50:00
Collection Start:1/14/2016 12:50:00Location:MW-12_ML1 [ MNS Landfill 1 / MW-12 ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <1.94E-01 0.00E+00 5.93E-01
Beta 6.44E-01 7.07E-01 1.18E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.08E+00 0.00E+00 5.08E+00 <1000 LLD OK<15
Co-58 <5.60E+00 0.00E+00 5.60E+00 <1000 LLD OK<15
Fe-59 <1.29E+01 0.00E+00 1.29E+01 <400 LLD OK<30
Co-60 <4.46E+00 0.00E+00 4.46E+00 <300 LLD OK<15
Zn-65 <1.10E+01 0.00E+00 1.10E+01 <300 LLD OK<30
Zr-95 <9.76E+00 0.00E+00 9.76E+00 <400 LLD OK<15
Nb-95 <6.35E+00 0.00E+00 6.35E+00 <400 LLD OK<15
I-131 <7.07E+00 0.00E+00 7.07E+00 LLD OK<15
Cs-134 <6.96E+00 0.00E+00 6.96E+00 <30 LLD OK<15
Cs-137 <6.66E+00 0.00E+00 6.66E+00 <50 LLD OK<18
BaLa-140 <9.09E+00 0.00E+00 9.09E+00 <200 LLD OK<15
Page 8 of 12Report Generated @ 2/10/2016 16:20:56
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 8 of 13 02.10.2016
Radiological Data for MCGUIRE
398007Sample #:Station:MCGUIRE
Collection End: 1/14/2016 12:50:00
Collection Start:1/14/2016 12:50:00Location:MW-12_ML1 [ MNS Landfill 1 / MW-12 ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.64E+01 0.00E+00 4.64E+01
K-40 <1.02E+02 0.00E+00 1.02E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-4.7E+01 0.00E+00 2.01E+02 <20000 LLD OK<250
398008Sample #:Station:MCGUIRE
Collection End: 1/14/2016 13:10:00
Collection Start:1/14/2016 13:10:00Location:MW-12D_ML1 [ MNS Landfill 1 / MW-12D ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <2.10E-01 0.00E+00 6.99E-01
Beta 4.27E+00 8.79E-01 1.20E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.01E+00 0.00E+00 5.01E+00 <1000 LLD OK<15
Co-58 <4.14E+00 0.00E+00 4.14E+00 <1000 LLD OK<15
Fe-59 <1.31E+01 0.00E+00 1.31E+01 <400 LLD OK<30
Co-60 <5.78E+00 0.00E+00 5.78E+00 <300 LLD OK<15
Zn-65 <9.48E+00 0.00E+00 9.48E+00 <300 LLD OK<30
Zr-95 <1.03E+01 0.00E+00 1.03E+01 <400 LLD OK<15
Nb-95 <4.90E+00 0.00E+00 4.90E+00 <400 LLD OK<15
I-131 <7.06E+00 0.00E+00 7.06E+00 LLD OK<15
Cs-134 <4.54E+00 0.00E+00 4.54E+00 <30 LLD OK<15
Cs-137 <4.43E+00 0.00E+00 4.43E+00 <50 LLD OK<18
BaLa-140 <9.07E+00 0.00E+00 9.07E+00 <200 LLD OK<15
Be-7 <5.09E+01 0.00E+00 5.09E+01
K-40 9.70E+01 5.63E+01 7.52E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <3.33E+01 0.00E+00 2.00E+02 <20000 LLD OK<250
Page 9 of 12Report Generated @ 2/10/2016 16:20:56
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 9 of 13 02.10.2016
Radiological Data for MCGUIRE
398009Sample #:Station:MCGUIRE
Collection End: 1/14/2016 12:20:00
Collection Start:1/14/2016 12:20:00Location:SW-1_ML1 [ MNS Landfill 1 / SW-1 ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <9.19E-02 0.00E+00 7.29E-01
Beta 9.55E-01 7.37E-01 1.21E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.28E+00 0.00E+00 5.28E+00 <1000 LLD OK<15
Co-58 <5.63E+00 0.00E+00 5.63E+00 <1000 LLD OK<15
Fe-59 <1.17E+01 0.00E+00 1.17E+01 <400 LLD OK<30
Co-60 <4.81E+00 0.00E+00 4.81E+00 <300 LLD OK<15
Zn-65 <1.44E+01 0.00E+00 1.44E+01 <300 LLD OK<30
Zr-95 <9.82E+00 0.00E+00 9.82E+00 <400 LLD OK<15
Nb-95 <5.64E+00 0.00E+00 5.64E+00 <400 LLD OK<15
I-131 <8.00E+00 0.00E+00 8.00E+00 LLD OK<15
Cs-134 <7.57E+00 0.00E+00 7.57E+00 <30 LLD OK<15
Cs-137 <7.10E+00 0.00E+00 7.10E+00 <50 LLD OK<18
BaLa-140 <5.11E+00 0.00E+00 5.11E+00 <200 LLD OK<15
Be-7 <4.61E+01 0.00E+00 4.61E+01
K-40 <1.10E+02 0.00E+00 1.10E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <3.33E+01 0.00E+00 1.85E+02 <20000 LLD OK<250
398010Sample #:Station:MCGUIRE
Collection End: 1/14/2016 08:35:00
Collection Start:1/14/2016 08:35:00Location:MW-4D_ML1 [ MNS Landfill 1 / MW-4D ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-1.1E-01 0.00E+00 8.35E-01
Beta <4.54E-01 0.00E+00 1.25E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.69E+00 0.00E+00 5.69E+00 <1000 LLD OK<15
Co-58 <6.18E+00 0.00E+00 6.18E+00 <1000 LLD OK<15
Fe-59 <1.03E+01 0.00E+00 1.03E+01 <400 LLD OK<30
Page 10 of 12Report Generated @ 2/10/2016 16:20:56
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 10 of 13 02.10.2016
Radiological Data for MCGUIRE
398010Sample #:Station:MCGUIRE
Collection End: 1/14/2016 08:35:00
Collection Start:1/14/2016 08:35:00Location:MW-4D_ML1 [ MNS Landfill 1 / MW-4D ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60 <5.43E+00 0.00E+00 5.43E+00 <300 LLD OK<15
Zn-65 <1.16E+01 0.00E+00 1.16E+01 <300 LLD OK<30
Zr-95 <8.66E+00 0.00E+00 8.66E+00 <400 LLD OK<15
Nb-95 <5.43E+00 0.00E+00 5.43E+00 <400 LLD OK<15
I-131 <6.91E+00 0.00E+00 6.91E+00 LLD OK<15
Cs-134 <4.61E+00 0.00E+00 4.61E+00 <30 LLD OK<15
Cs-137 <5.33E+00 0.00E+00 5.33E+00 <50 LLD OK<18
BaLa-140 <9.21E+00 0.00E+00 9.21E+00 <200 LLD OK<15
Be-7 <4.35E+01 0.00E+00 4.35E+01
K-40 4.96E+01 5.37E+01 8.58E+01
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <5.43E+01 0.00E+00 1.83E+02 <20000 LLD OK<250
398011Sample #:Station:MCGUIRE
Collection End: 1/14/2016 11:45:00
Collection Start:1/14/2016 11:45:00Location:MW-4DR_ML1 [ MNS Landfill 1 / MW-4DR ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis Waters
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <-5.8E-03 0.00E+00 7.73E-01
Beta 1.05E+00 7.50E-01 1.22E+00 LLD OK<4
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54 <5.52E+00 0.00E+00 5.52E+00 <1000 LLD OK<15
Co-58 <4.86E+00 0.00E+00 4.86E+00 <1000 LLD OK<15
Fe-59 <1.04E+01 0.00E+00 1.04E+01 <400 LLD OK<30
Co-60 <6.71E+00 0.00E+00 6.71E+00 <300 LLD OK<15
Zn-65 <1.44E+01 0.00E+00 1.44E+01 <300 LLD OK<30
Zr-95 <8.96E+00 0.00E+00 8.96E+00 <400 LLD OK<15
Nb-95 <6.93E+00 0.00E+00 6.93E+00 <400 LLD OK<15
I-131 <8.71E+00 0.00E+00 8.71E+00 LLD OK<15
Cs-134 <6.92E+00 0.00E+00 6.92E+00 <30 LLD OK<15
Cs-137 <5.14E+00 0.00E+00 5.14E+00 <50 LLD OK<18
BaLa-140 <8.42E+00 0.00E+00 8.42E+00 <200 LLD OK<15
Page 11 of 12Report Generated @ 2/10/2016 16:20:56
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 11 of 13 02.10.2016
Radiological Data for MCGUIRE
398011Sample #:Station:MCGUIRE
Collection End: 1/14/2016 11:45:00
Collection Start:1/14/2016 11:45:00Location:MW-4DR_ML1 [ MNS Landfill 1 / MW-4DR ( LANDFILL ) ]
MNS_7DEC2015_AJob:
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.24E+01 0.00E+00 4.24E+01
K-40 <1.03E+02 0.00E+00 1.03E+02
H3 Tritium Analysis of Water
Units:pCi/l Calculated MDA 2 Sigma Error Activity SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-3.7E+01 0.00E+00 1.82E+02 <20000 LLD OK<250
Page 12 of 12Report Generated @ 2/10/2016 16:20:56
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Hagers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratory Page 12 of 13 02.10.2016
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