Elkin Chrysler Redev_2007.02.28_Mangum Street - Phase 2-OCR

409 Rogers View Court / Raleigh / North Carolina / 27610
800-486-7568 / 919-250-9918 / 919-250-9950 Facsimile
www.maaonline.com

February 28, 2007

Dr. Andrew Rothschild
Scientific Properties, Inc.
411 West Chapel Hill Street, Suite 906
Durham, North Carolina 27701

Subject: LETTER REPORT OF ENVIRONMENTAL SERVICES
PHASE II ENVIRONMENTAL SAMPLING
ELKINS CHRYSLER MITSUBISHI
DURHAM, NORTH CAROLINA
MID-ATLANTIC JOB NO. 000R1816.01

Dear Dr. Rothschild:

In accordance with your acceptance of our Proposal No. P07R-4251 dated January 9,
2007, Mid-Atlantic Associates, Inc. (Mid-Atlantic) is pleased to present this report of
environmental services for the Elkins Chrysler Mitsubishi site located at 925 Jackie
Robinson Drive (East-West Expressway) in Durham, North Carolina (Drawing 1). The
purpose of our services, as described in the attached report, was to perform a Phase II
assessment for the above referenced location. Specifically, our scope of services
included installing and sampling temporary monitoring wells, sampling existing
monitoring wells, advancing soil borings and collecting soil samples in potentially
contaminated areas located on-site. Our findings are presented below.

SUMMARY OF ACTIVITIES

Soil Boring Installation

On February 5-6, 2007, Ms. Katie Lippard of Mid-Atlantic mobilized to the site to oversee
the installation of soil borings and temporary monitoring wells on site, as shown on
Drawing 2. Boring and well installation services were provided by Subsurface
Environmental Investigations (SEI, Inc.) of Statesville, North Carolina (NC Driller’s
registration number 3393). Borings were advanced with a Geoprobe “macrocore”
sampler, and five-foot length cores of soil were scanned for the presence of volatile
organic compounds with a toxic vapor analyzer (TVA). In general, borings at the site
encountered silty fine sand to fine sandy silt with partially-weathered rock fragments
(Attachment A).
Letter Report of Environmental Services February 28, 2007
Phase II Assessment – Elkins Chrysler Mitsubishi Site Page 2
Durham, North Carolina

Ms. Lippard collected two samples (SB-1 and SB-2) in the vicinity of the waste oil
aboveground storage tank (AST), one sample (SB-3) in the former location of the
gasoline pump island, one sample (SB-4) in the vicinity of the former hydraulic lift in the
body shop, two samples (SB-5 and SB-6) on north and south sides of the oil/water
separator, thirteen samples (SB-7 through SB-9 and SB-12 through SB-21) in the vicinity
of the former hydraulic lifts in the service department and three soil samples (SB-10, SB-
11 and SB-22) in the vicinity of the former waste oil UST delivery line. The boring depths
ranged from 5 to 15 feet below land surface (BLS). Soil samples were collected at
approximately 2-foot intervals and screened with the TVA. Based on screening results
and field observations, one soil sample for each boring was selected for laboratory testing
except for SB-23 and SB-24 which were advanced for delineation purposes and not
sampled. Soil samples SB-1, SB-2, SB-4, SB-7 and SB-8 through SB-22 were analyzed
for oil and grease using EPA Method 9071. Soil samples SB-4, SB-8, SB-11, SB-13, SB-
17 and SB-22 were subsequently run by EPA 9071 with a silica gel cleanup to filter out
natural oils and greases. Soil sample SB-3 was analyzed for volatile petroleum
hydrocarbons using MADEP VPH and for volatiles using EPA Method 8260. Soil samples
SB-5 and SB-6 were also analyzed for volatiles using EPA Method 8260 along with semi-
volatiles using EPA Method 8270. Ms. Lippard wore new nitrile gloves during the
collection of each sample, and each sample was placed into laboratory-prepared, pre-
labeled bottles. The samples were packed in ice and shipped under chain-of-custody
control to SGS Environmental Services, Inc. (SGS) in Wilmington, North Carolina.

Hand auger borings were advanced by Ms. Lippard in the vicinity of the former solvent
(paint thinner) USTs formerly located north of the body shop (Drawing No. 2). Ms. Lippard
collected samples HA-1, HA-2 and HA-3 at depth of 6 feet below land surface (BLS),
2 feet BLS and 5 feet BLS, respectively. Ms. Lippard wore new nitrile gloves during the
collection of each sample, and each sample was placed into laboratory-prepared, pre-
labeled bottles. The samples were packed in ice and shipped under chain-of-custody
control to SGS for analysis. The samples were analyzed for volatiles using EPA Method
8260.

Soil Sampling Results

Laboratory analytical reports and chain of custody records are included in Attachment B
and summarized in Table 1. Soil samples SB-8, SB-11, SB-13, SB-17 and SB-22
exhibited oil and grease concentrations in excess of the regulatory action level of 250
milligrams per kilogram (mg/Kg). Samples SB-8, SB-13 and SB-17 were collected in the
vicinity of hydraulic lift systems in the service department. Samples SB-11 and SB-22
were detected in the vicinity of the former waste oil UST and associated delivery line.
Fourteen additional samples exhibited detectable levels of oil and grease below the 250
mg/Kg action level.
Letter Report of Environmental Services February 28, 2007
Phase II Assessment – Elkins Chrysler Mitsubishi Site Page 3
Durham, North Carolina

When analyzed using a silica gel clean up to filter out natural oils and greases, the
concentrations of oil and grease in samples SB-4 and SB-17 decreased to 37.2 mg/Kg
and none detected, respectively. Soil samples SB-8, SB-11, SB-13 and SB-22 exhibited
similar concentrations of oil and grease after being analyzed using a silica gel cleanup.

Volatile and semi-volatile organic compounds were detected in samples SB-5 and SB-6
at concentrations in excess of their respective soil-to-groundwater maximum soil
contaminant concentration (MSCC).

Temporary Monitoring Well Installation

On February 5, 2006, Ms. Katie Lippard oversaw the installation of two temporary
monitoring wells on site (TMW-1 and TMW-2), as shown on Drawing 2. An attempt was
made to install one temporary well at the northwest corner of the site. However, refusal
was encountered at approximately six-feet BLS. The borings were advanced until the
water table was penetrated and temporary, one-inch diameter Schedule 40 PVC
monitoring wells were installed. The wells were constructed such that the well screen
intersected the water table at the time of construction. A sand filter pack was placed
around the well screens to a depth approximately two feet above the top of the screened
interval. Each well was developed with a new, dedicated, polyethylene bailer upon
completion to remove sediment from the water column and was then equipped with a
locking cap.

Temporary and Permanent Monitoring Well Sampling

From February 5 through 7, 2007, Ms. Lippard sampled permanent monitoring well MW-1
and temporary monitoring wells TMW-1 and TMW-2. Prior to sampling, the depth to water
in each well was measured using an electronic water level indicator. The depth to water in
wells MW-1, TMW-1 and TMW-2 was measured at approximately 12.25, 15.50 and 11.95
feet BLS, respectively. The well’s dedicated bailer was then used to purge approximately
three well volumes of water (or until the well went dry) prior to sample collection. The
sampler donned new, nitrile gloves for purging and sampling activities. A groundwater
sample was collected from each well using the bailer. The samples were decanted into
laboratory-prepared, pre-labeled sampling bottles, packed in ice, and delivered under
chain-of-custody record to SGS for analysis. The samples were analyzed for volatiles and
semi-volatiles using EPA Methods 6210D and 625, respectively. Monitoring well sample
TMW-1 was also sampled for formaldehyde using EPA Method 8315.

Ms. Lippard attempted to collect a sample from permanent monitoring well MW-2.
However, due to lack of groundwater recovery after purging a sample could not be
collected.

Letter Report of Environmental Services February 28, 2007
Phase II Assessment – Elkins Chrysler Mitsubishi Site Page 4
Durham, North Carolina

Groundwater Sampling Results

A laboratory analytical report and chain of custody record is attached and the laboratory
results are shown on Table 2. Each of the groundwater samples collected at the site
exhibited detectable concentrations of volatile and semi-volatile contaminants. However,
only the samples collected from temporary monitoring wells TMW-1 and TMW-2 exhibited
concentrations in excess of their respective North Carolina Groundwater Quality Standard
(NCGQS). Sample TMW-1 exhibited concentrations of benzene [11.8 micrograms per
liter (ug/L)], 4-isopropyltoluene (3.03 ug/L), and Bis(2-ethylhexyl)phthalate (107 ug/L) in
excess of their respective NCGQS. The sample collected from TMW-2 exhibited Bis(2-
ethylhexyl)phthalate at a concentration (18.3 ug/L) in excess of the NCGQS. Benzene
and 4-isopropyltoluene are typically associated with releases of petroleum. Bis(2-
ethylhexyl)phthalate is a plasticizer that may have been introduced to the samples
through degradation of the plastic well casings or bailers. It is also a common laboratory
contaminant.

Formaldehyde was detected in the sample collected from temporary monitoring well
TMW-1 at an estimated value of 130 ug/L. Formaldehyde is typically used in embalming
fluids.

CONCLUSIONS AND RECOMMENDATIONS

Based on the results of this investigation, Mid-Atlantic concludes the following.

• Contaminants consistent with the historic use of the property were detected in the
majority of samples collected at the site.
• Releases appear to have occurred from the majority of the hydraulic systems
present at the site. Soil in the vicinity of the lifts associated with samples SB-8 and
SB-13 appears to be impacted with oil and grease concentrations in excess of the
action level of 250 mg/Kg. Although other samples collected in the vicinity of
hydraulic lifts (SB-4, SB-7, SB-9, SB-12 and SB-14 through SB-21) did not exhibit
concentrations of oil and grease in excess of the action level, contaminated soil
may still be present but undetected in these areas due to the limitations of this
investigation.
• Contaminated soil remains in the vicinity of the former waste oil UST and delivery
lines. The actual extent of contamination has not been delineated.
• A release(s) appears to have occurred from the on-site oil/water separator. Soil
samples collected in the vicinity of the separator exhibited concentrations of target
compounds in excess of their respective soil-to-groundwater maximum soil
contaminant concentrations. Based on the depth that these samples were
collected and the measured depth to groundwater at the site, it is reasonable to
suspect that groundwater in the vicinity of the separator may be adversely-
impacted by the release(s) from the separator.
Letter Report of Environmental Services February 28, 2007
Phase II Assessment – Elkins Chrysler Mitsubishi Site Page 5
Durham, North Carolina

• Groundwater at the northern portion of the site has been adversely-impacted by
petroleum constituents and formaldehyde resulting from documented releases at
nearby and/or adjacent sites.

Mid-Atlantic recommends that a copy of this report be submitted to the property owner with
a recommendation that a copy be submitted to the North Carolina Department of
Environment and Natural Resources. We also recommend that the historical operations at
the site, results of this investigation, and the potential for additional, currently undetected
areas of contamination be considered during the design and implementation of
redevelopment activities.

We appreciate the opportunity to provide these services to Carter. If you have any
questions, please contact me at 800-486-7568.

Sincerely,

MID-ATLANTIC ASSOCIATES, INC.
Katie A. Lippard Darin M. McClure, P.E.
Environmental Scientist Principal Engineer

Attachments: Drawings
Tables
A: Soil Boring/Monitoring Well Logs
B: Laboratory Analytical Reports

2-28-07 Elkins Chrysler Mitsubishi Site letter report/KAL/aso

DRAWINGS

TABLES
SB
-
1

S
B
-
2

S
B
-
3

S
B
-
4

S
B
-
5
2'

B
L
S

1
0
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B
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S

9
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5
'
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1
0
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B
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S

1
3
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B
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S

8
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9
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B
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5
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2
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2
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2
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Action Level (mg/Kg)
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e
s
s

o
f

S
o
i
l
-
t
o
-
G
r
o
u
n
d
w
a
t
e
r

M
S
C
C

o
r

A
c
t
i
o
n

L
e
v
e
l
NE

-

N
o
t

E
s
t
a
b
l
i
s
h
e
d
MS
C
C

-

M
a
x
i
m
u
m

S
o
i
l

C
o
n
t
a
m
i
n
a
n
t

C
o
n
c
e
n
t
r
a
t
i
o
n
90
7
1
*

-

A
n
a
l
y
s
i
s

w
i
t
h

s
i
l
i
c
a

g
e
l

c
l
e
a
n

u
p
.
CO
N
C
E
N
T
R
A
T
I
O
N

(
m
g
/
K
g

o
r

P
P
M
)
Na
p
h
t
h
a
l
e
n
e
Soil-to-Groundwater MSCC
AN
A
L
Y
T
I
C
A
L

ME
T
H
O
D
CH
E
M
I
C
A
L

C
O
N
S
T
I
T
U
E
N
T
MSCC (mg/Kg)
CO
N
C
E
N
T
R
A
T
I
O
N

(
m
g
/
K
g

o
r

P
P
M
)
SB
-
6

8.
5
'
-
9
.
5
'

B
L
S

2/
5
/
0
7
SB
-
7

8'

B
L
S

2/
5
/
0
7
SB
-
8

2'

B
L
S

2/
6
/
0
7
MI
D
-
A
T
L
A
N
T
I
C

J
O
B

N
O
.

0
0
0
R
1
8
1
6
.
0
1
TA
B
L
E

1

(
P
a
g
e

1

o
f

3
)
SU
M
M
A
R
Y

O
F

C
H
E
M
I
C
A
L

C
O
N
S
T
I
T
U
E
N
T
S

D
E
T
E
C
T
E
D

I
N

S
O
I
L

EL
K
I
N
S

C
H
R
Y
S
L
E
R

M
I
T
S
U
B
I
S
H
I

-

9
2
5

J
A
C
K
I
E

R
O
B
I
N
S
O
N

D
R
I
V
E
DU
R
H
A
M
,

N
O
R
T
H

C
A
R
O
L
I
N
A
Ac
e
t
o
n
e
50
3
0
/
8
2
6
0

N
S

N
S
NS

N
S

N
S

N
S

N
S

N
S
2.81
2-
B
u
t
a
n
o
n
e
50
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
0.69
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
50
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
3
Et
h
y
l
b
e
n
z
e
n
e
50
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
0.2
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e

(
C
u
m
e
n
e
)

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
2.0
4-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
50
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
NE
50
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
0.58
82
7
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
0.58
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
50
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
2.0
To
l
u
e
n
e
50
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
7.0
To
t
a
l

X
y
l
e
n
e
s
50
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
5
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
8
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S
NS

N
S

N
S

N
S

N
S
7
1,
2
,
3
-
T
r
i
c
h
l
o
r
o
b
e
n
z
e
n
e
82
6
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
NE
Be
n
z
o
[
a
]
a
n
t
h
r
a
c
e
n
e
82
7
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
0.34
Be
n
z
o
[
a
]
p
y
r
e
n
e
82
7
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
0.091
Be
n
z
o
[
b
]
f
l
u
o
r
a
n
t
h
e
n
e
82
7
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
1.2
Be
n
z
o
[
k
]
f
l
u
o
r
a
n
t
h
e
n
e
82
7
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
12
Bi
s
(
2
-
e
t
h
y
l
h
e
x
y
l
)
p
h
t
h
a
l
a
t
e

8
2
7
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
6.67
Ch
y
r
s
e
n
e
82
7
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
38
Fl
u
o
r
a
n
t
h
e
n
e
82
7
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
276
Ph
e
n
a
n
t
h
r
e
n
e
82
7
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
60
Py
r
e
n
e
82
7
0
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
286
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
VP
H
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
72
C9
-
C
1
8

A
l
i
p
h
a
t
i
c
s
VP
H
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
3255
C9
-
C
2
2

A
r
o
m
a
t
i
c
s
VP
H
NS

N
S

N
S
NS

N
S

N
S

N
S

N
S
34
CO
N
S
T
I
T
U
E
N
T
AN
A
L
Y
T
I
C
A
L

ME
T
H
O
D
Action Level (mg/Kg)
TV
A

R
e
a
d
i
n
g

(
P
P
M
)
NA
1.
2
6

1
.
6
5

2
.
1
1

1
.
0
8

2
.
3
2

3
.
0
6

2
.
9
6

2
.
8
6
NA
Oi
l

a
n
d

G
r
e
a
s
e

(
m
g
/
K
g
)

9
0
7
1

/

9
0
7
1
*

2
2
4

2
2
5
2,
2
8
0

/

2
,
4
0
0
14
0
2,
3
3
0

/

2
,
8
9
0
92
.
3

1
7
5

1
6
2
250
BL
S

-

B
e
l
o
w

L
a
n
d

S
u
r
f
a
c
e
NS

-

N
o
t

A
n
a
l
y
z
e
d

f
o
r

t
h
i
s

p
a
r
a
m
e
t
e
r
mg
/
K
g

-

M
i
l
l
i
g
r
a
m
s

p
e
r

K
i
l
o
g
r
a
m
NA

-

N
o
t

A
p
p
l
i
c
a
b
l
e
J
-

E
s
t
i
m
a
t
e
d

V
a
l
u
e
PP
M

-

P
a
r
t
s

p
e
r

m
i
l
l
i
o
n
ND

-

N
o
n
e

D
e
t
e
c
t
e
d

A
b
o
v
e

L
a
b
o
r
a
t
o
r
y

Q
u
a
n
t
i
t
a
t
i
o
n

L
i
m
i
t
Bo
l
d
e
d

v
a
l
u
e
s

i
n

e
x
c
e
s
s

o
f

S
o
i
l
-
t
o
-
G
r
o
u
n
d
w
a
t
e
r

M
S
C
C

o
r

A
c
t
i
o
n

L
e
v
e
l
NE

-

N
o
t

E
s
t
a
b
l
i
s
h
e
d
MS
C
C

-

M
a
x
i
m
u
m

S
o
i
l

C
o
n
t
a
m
i
n
a
n
t

C
o
n
c
e
n
t
r
a
t
i
o
n
90
7
1
*

-

A
n
a
l
y
s
i
s

w
i
t
h

s
i
l
i
c
a

g
e
l

c
l
e
a
n

u
p
.
SB
-
1
6

8'

B
L
S

2/
6
/
0
7
SB
-
1
0

4'
B
L
S

2/
6
/
0
7
SB
-
1
2

12
'

B
L
S

2/
6
/
0
7
SB
-
1
3
2'

B
L
S

2/
6
/
0
7
SB
-
1
4

10
'

B
L
S

2/
6
/
0
7
MI
D
-
A
T
L
A
N
T
I
C

J
O
B

N
O
.

0
0
0
R
1
8
1
6
.
0
1
TA
B
L
E

1

(
P
a
g
e

2

o
f

3
)
SU
M
M
A
R
Y

O
F

C
H
E
M
I
C
A
L

C
O
N
S
T
I
T
U
E
N
T
S

D
E
T
E
C
T
E
D

I
N

S
O
I
L

EL
K
I
N
S

C
H
R
Y
S
L
E
R

M
I
T
S
U
B
I
S
H
I

-

9
2
5

J
A
C
K
I
E

R
O
B
I
N
S
O
N

D
R
I
V
E
DU
R
H
A
M
,

N
O
R
T
H

C
A
R
O
L
I
N
A
Na
p
h
t
h
a
l
e
n
e
Soil-to-Groundwater MSCC
AN
A
L
Y
T
I
C
A
L

ME
T
H
O
D
CH
E
M
I
C
A
L

C
O
N
S
T
I
T
U
E
N
T
MSCC (mg/Kg)
SB
-
1
1
2'

B
L
S

2/
6
/
0
7
CO
N
C
E
N
T
R
A
T
I
O
N

(
m
g
/
K
g

o
r

P
P
M
)
SB
-
9

10
'

B
L
S

2/
6
/
0
7
SB
-
1
5

6'

B
L
S

2/
6
/
0
7
Ac
e
t
o
n
e
50
3
0
/
8
2
6
0

N
S

N
S

N
S

N
S

N
S

N
S
0.
0
2
2
3

J

0
.
0
2
7
6

J

0
.
0
0
9
1
0

J
2.81
2-
B
u
t
a
n
o
n
e

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S

N
S

N
S

N
S

<
0
.
0
2
3
3

0
.
0
0
4
3

J

<
0
.
0
2
5
9

0
.
6
9
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S

N
S

N
S

N
S

<
0
.
0
0
4
6
6

<
0
.
0
0
4
9
1

<
0
.
0
0
5
1
7

3
Et
h
y
l
b
e
n
z
e
n
e

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S

N
S

N
S

N
S

<
0
.
0
0
4
6
6

<
0
.
0
0
4
9
1

<
0
.
0
0
5
1
7

0
.
2
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e

(
C
u
m
e
n
e
)

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S

N
S

N
S

N
S

<
0
.
0
0
4
6
6

<
0
.
0
0
4
9
1

<
0
.
0
0
5
1
7

2
.
0
4-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S

N
S

N
S

N
S

<
0
.
0
0
4
6
6

<
0
.
0
0
4
9
1

<
0
.
0
0
5
1
7

N
E
50
3
0
/
8
2
6
0

N
S

N
S

N
S

N
S

N
S

N
S

<
0
.
0
0
4
6
6

<
0
.
0
0
4
9
1

<
0
.
0
0
5
1
7

0
.
5
8
82
7
0

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

0
.
5
8
n-
P
r
o
p
y
l
b
e
n
z
e
n
e

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S

N
S

N
S

N
S

<
0
.
0
0
4
6
6

<
0
.
0
0
4
9
1

<
0
.
0
0
5
1
7

2
.
0
To
l
u
e
n
e

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S

N
S

N
S

N
S

<
0
.
0
0
4
6
6

<
0
.
0
0
4
9
1

<
0
.
0
0
5
1
7

7
.
0
To
t
a
l

X
y
l
e
n
e
s

5
0
3
0
/
8
2
6
0

N
S

N
S

N
S

N
S

N
S

N
S

<
0
.
0
1
4
0

<
0
.
0
1
4
7

<
0
.
0
1
5
5

5
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
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N
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N
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N
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N
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N
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N
S

1
.
2
Be
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k
]
f
l
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N
S

N
S

N
S

N
S

N
S

N
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N
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N
S

N
S

1
2
Bi
s
(
2
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t
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y
l
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x
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l
)
p
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8
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N
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N
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N
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6
.
6
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Ch
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8
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N
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N
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N
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N
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N
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N
S

N
S

3
8
Fl
u
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r
a
n
t
h
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8
2
7
0

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

2
7
6
Ph
e
n
a
n
t
h
r
e
n
e

8
2
7
0

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

6
0
Py
r
e
n
e

8
2
7
0

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

2
8
6
C5
-
C
8

A
l
i
p
h
a
t
i
c
s

V
P
H

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

7
2
C9
-
C
1
8

A
l
i
p
h
a
t
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s

V
P
H

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

3
2
5
5
C9
-
C
2
2

A
r
o
m
a
t
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c
s

V
P
H

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

N
S

3
4
CO
N
S
T
I
T
U
E
N
T
AN
A
L
Y
T
I
C
A
L

ME
T
H
O
D
Action Level (mg/Kg)
TV
A

R
e
a
d
i
n
g

(
P
P
M
)

N
A

3
.
1
5

4
.
9
9

4
.
4
0

4
.
9
2

3
.
2
4

2
.
6
0

5
.
3
7

7
.
5
2

4
.
6
5

N
A
Oi
l

a
n
d

G
r
e
a
s
e

(
m
g
/
K
g
)

9
0
7
1

/

9
0
7
1
*
28
0

/

ND
11
0

1
7
7

1
1
0

9
1
.
7
1,
9
1
0

/

1
,
8
0
0
NS

N
S

N
S

2
5
0
BL
S

-

B
e
l
o
w

L
a
n
d

S
u
r
f
a
c
e
NS

-

N
o
t

A
n
a
l
y
z
e
d

f
o
r

t
h
i
s

p
a
r
a
m
e
t
e
r
mg
/
K
g

-

M
i
l
l
i
g
r
a
m
s

p
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r

K
i
l
o
g
r
a
m
NA

-

N
o
t

A
p
p
l
i
c
a
b
l
e
J
-

E
s
t
i
m
a
t
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d

V
a
l
u
e
PP
M

-

P
a
r
t
s

p
e
r

m
i
l
l
i
o
n
ND

-

N
o
n
e

D
e
t
e
c
t
e
d

A
b
o
v
e

L
a
b
o
r
a
t
o
r
y

Q
u
a
n
t
i
t
a
t
i
o
n

L
i
m
i
t

B
o
l
d
e
d

v
a
l
u
e
s

i
n

e
x
c
e
s
s

o
f

S
o
i
l
-
t
o
-
G
r
o
u
n
d
w
a
t
e
r

M
S
C
C

o
r

A
c
t
i
o
n

L
e
v
e
l
NE

-

N
o
t

E
s
t
a
b
l
i
s
h
e
d
MS
C
C

-

M
a
x
i
m
u
m

S
o
i
l

C
o
n
t
a
m
i
n
a
n
t

C
o
n
c
e
n
t
r
a
t
i
o
n
90
7
1
*

-

A
n
a
l
y
s
i
s

w
i
t
h

s
i
l
i
c
a

g
e
l

c
l
e
a
n

u
p
.
Na
p
h
t
h
a
l
e
n
e
Soil-to-Groundwater MSCC
AN
A
L
Y
T
I
C
A
L

ME
T
H
O
D
CH
E
M
I
C
A
L

C
O
N
S
T
I
T
U
E
N
T
MSCC (mg/Kg)
CO
N
C
E
N
T
R
A
T
I
O
N

(
m
g
/
K
g

o
r

P
P
M
)
SB
-
1
7

4'

B
L
S

2/
6
/
0
7
SB
-
2
1

2'

B
L
S

2/
6
/
0
7
SB
-
2
2
2'

B
L
S

2/
6
/
0
7
TA
B
L
E

2

(
P
a
g
e

3

o
f

3
)
SU
M
M
A
R
Y

O
F

C
H
E
M
I
C
A
L

C
O
N
S
T
I
T
U
E
N
T
S

D
E
T
E
C
T
E
D

I
N

S
O
I
L

EL
K
I
N
S

C
H
R
Y
S
L
E
R

M
I
T
S
U
B
I
S
H
I

-

9
2
5

J
A
C
K
I
E

R
O
B
I
N
S
O
N

D
R
I
V
E
DU
R
H
A
M
,

N
O
R
T
H

C
A
R
O
L
I
N
A
MI
D
-
A
T
L
A
N
T
I
C

J
O
B

N
O
.

0
0
0
R
1
8
1
6
.
0
1
HA
-
1

6'

B
L
S

2/
7
/
0
7
HA
-
2

2'

B
L
S

2/
8
/
0
7
HA
-
3

5'

B
L
S

2/
8
/
0
7
SB
-
1
8

2'
B
L
S

2/
6
/
0
7
SB
-
1
9

8'

B
L
S

2/
6
/
0
7
SB
-
2
0

12
'

B
L
S

2/
6
/
0
7
Benzene <1.0 11.8 <0.5 1
sec-Butylbenzene <1.0 3.66 <0.5 70
tert-Butylbenzene <1.0 0.54 <0.5 70
1,1-Dichloroethane 1.16 <0.5 <0.5 70
Diisopropyl ether (DIPE)<1.0 0.8 <0.5 70
Ethylbenzene <1.0 3.61 <0.5 550
Isopropylbenzene <1.0 7.36 <0.5 70
4-Isopropyltoluene <1.0 3.03 <0.5 NE
Methyl-tert-butyl ether (MTBE)5.83 <0.5 3.73 200
n-Propylbenzene <1.0 8.08 <0.5 70
Toluene <1.0 1.6 0.350 J 1,000
1,2,4-Trimethylbenzene <1.0 2.94 <0.5 350
1,3,5-Trimethylbenzene <1.0 7.44 <0.5 350
Total Xylenes <3.0 9.12 <1.5 530
Bis(2-ethylhexyl)phthalate 1.70 J 107 18.3 2.5
Diethylphthalate 1.50 J 1.6 J <1.48 5,000
Formaldehyde NS 130 J NS NE
NOTES:
ug/L - micrograms per liter Bold Values exceed NCGQS
NS - Not analyzed for this parameter NE - Not Established. Concentration in excess of the
NR - laboratory analysis not requested laboratory practical quantitation limit is
J - Estimated value below practical quantitation limit considered a violation.
TMW-1MW-1
COMPOUNDS
CONCENTRATION (ug/L)
TMW-2
Volatile Organic Compounds (6210D)
Formaldehyde (8315)
Semi-Volatile Organic Compounds (625)
TABLE 2
SUMMARY OF GROUNDWATER QUALITY DATA - FEBRUARY 2007
ELKINS CHRYSLER MITSUBISHI
925 JACKIE ROBINSON DRIVE
DURHAM, NORTH CAROLINA
MID-ATLANTIC JOB NO. 000R1816.01
NCGQS
2-13-07 Elkins Chrysler site tablesGW - Table 2 Page 1 of 1

ATTACHMENT A

SOIL BORING/MONITORING WELL LOGS
Temporary Wells
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 0.08
4' - 0.01
5 - 10 6' - 0.71
8' - 0.42
10 - 11 10' - 0.19 Orangish brown silty fine SAND with
rock fragments dry, no odor
11 - 11.5 11.5' - 0.06 Black rock fragments moist, no odor
11.5 - 15 12' - 3.08
14' - 2.42 dry, petroleum odor
15 - 17 16' - 2.29
17' - 45.01 moist, petroleum odor
Screened Interval: 15'
Bentonite Interval: None
Outer Casing Interval: None
Sand Interval: 2" above screen
Grout Interval: None
Outer Casing Diameter: None
Well Diameter: 1"
Orangish brown silty fine SAND dry, no odor
Grayish fine sandy SILT
Note: *TMW-1 removed on 2/8/07 and borehole closed with grout to grade.
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: TMW-1 Date: 2/5/07
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 17'
Temporary Wells
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 36.01
4' - 2.90
5 - 10 6' - 1.60
8' - 1.40
10 - 15
10' - 1.53
12' - 1.46
14' - 1.48
Orangish brown silty fine SAND
(10' - 14')
Silty medium SAND
(14' - 15')
dry, no odor
15 - 20
16' - 1.37
18' - 1.59
20' - 1.83
Orangish brown fine to medium sandy
SILT dry, no odor
*TMW-2 removed on 2/6/07 and borehole filled with Bentonite to grade.
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: TMW-2 Date: 2/5/07
Installation Method: Geoprobe Borehole Diameter: 2"
Screened Interval: 15'
Bentonite Interval: None
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 20' Well Diameter: 1"
Orangish brown silty fine SAND dry, no odor
Outer Casing Interval: None
Sand Interval: 2" above screen
Grout Interval: None
Outer Casing Diameter: None
Temporary Wells
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Installation Method: Geoprobe Borehole Diameter: 2"
Screened Interval:
Bentonite Interval:
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth:
Attempted to install in 2 locations approximately 10 feet apart. Refusal encountered at 6 feet BLS.
Unable to install.
Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: TMW-3 Date: 2/5/07
Former Solvent USTs
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
2' - 0.26
4' - 0.66
6' - 5.37
8' - 4.79
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: HA-1 Date: 2/7/07
Installation Method: Hand Auger Borehole Diameter: 4"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 8.5' Well Diameter:
Silty fine SAND to fine sandy SILT (0 -
7.5' BLS). Clayey SILT with sand (7.5' -
8.5' BLS); very tight material.
Unable to determine
moisture content due to
water in borehole from
coring. No odor.
Hand Auger
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Former Solvent USTs
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
2 - 7.52
4 - 2.51
5 - 4.08
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Installation Method: Hand Auger Borehole Diameter: 4"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 5'Well Diameter:
Silty fine SAND to fine sandy SILT
(0 - 3' BLS).
Clayey SILT to silty CLAY
(3' - 5' BLS)
dry, no odorHand Auger
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: HA-2 Date: 2/8/07
Former Solvent USTs
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
2' - 3.01
4' - 3.02
5' - 4.65
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: HA-3 Date: 2/8/07
Installation Method: Hand Auger Borehole Diameter: 4"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 5' Well Diameter:
Silty fine SAND to fine sandy SILT
(0 - 3' BLS).
Clayey SILT to silty CLAY
(3' - 5' BLS)
dry, no odorHand Auger
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
AST
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 14.01
4' - -0.03 Orangish brown silty fine SAND 0 - 2' = dry, petroleum odor
2 - 5' = dry, no odor
5 - 10
6' - 10.81
8' - -0.32
10' - 0.10
Orangish brown silty fine SAND
(5' - 8' BLS)
Fine sandy SILT
(8' - 10')
dry, no odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 10'Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-1 Date: 2/5/07
Installation Method: Geoprobe Borehole Diameter: 2"
AST
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 1.37
4' - 1.14 Orangish brown silty fine SAND dry, no odor
5 - 10
6' - 1.01
8' - 1.43
10' - 1.51
Fine sandy SILT
(5' - 9' BLS)
Black fine medium SAND with silt
(9' - 9.5' BLS)
Fine sandy SILT
(9.5' - 10' BLS)
dry, no odor
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 10'Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-2 Date: 2/5/07
Installation Method: Geoprobe Borehole Diameter: 2"
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Pump Island
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 0.31
4' - 0.47 Dark brown fine sandy SILT dry, no odor
5 - 10
6' - 0.60
8' - 0.99
10' - 1.15
Dark brown orange fine sandy SILT
(5' - 7' BLS)
Orange silty fine SAND
(7' - 10' BLS)
5' - 7' = moist, no odor
8' - 10' = dry, light odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 10'Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-3 Date: 2/5/07
Installation Method: Geoprobe Borehole Diameter: 2"
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 0.02
4' - 0.07 Orangish brown to tan fine sandy SILT dry, no odor
5 - 10 6' - 0.22
8' - 0.27 Orangish brown to tan fine sandy SILT dry, light odor
10 - 15
10' - 0.27
12' - 0.31
14' - 0.31
Orangish brown to tan fine sandy SILT
(10' - 13' BLS)
Fine medium silty SAND
(13' - 15')
10' - 13' = dry, light odor
13' - 15' = moist, light odor
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 15' Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-4 Date: 2/5/07
Installation Method: Geoprobe Borehole Diameter: 2"
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Oil/Water Separator
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 1.00
4' - 1.60 Orange fine sandy SILT dry, no odor
5 - 9 6' - 0.68
8' - 0.75 Gray fine sandy SILT 5' - 8' = dry, no odor
8' - 9' = moist, light odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 9'Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-5 Date: 2/5/07
Installation Method: Geoprobe Borehole Diameter: 2"
Oil/Water Separator
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 0.72
4' - 0.79 Orange fine sandy SILT dry, no odor
5 - 9.5 6' - 0.71
8' - 0.71
Gray fine sandy SILT
(5' - 7' BLS)
Dark gray SILT with fine sand
(7' - 9' BLS)
5' - 8' = dry, no odor
8' - 9.5' = moist, light odor
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 9.5'Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-6 Date: 2/5/07
Installation Method: Geoprobe Borehole Diameter: 2"
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Service Bay/Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 6.85
4' - 6.48 0 - 7.5' = dry, no odor
5 - 10 6' - 7.56
8' - 9.36 7.5' - 8.5' = dry, light odor
10 - 12 10' - 7.20
12' - 7.00 8.5' - 12' = dry, no odor
Orangish brown fine sandy SILT
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
Installation Method: Geoprobe Borehole Diameter: 2"
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-7 Date: 2/5/07
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 0.41
4' - 0.41
Brown silty fine SAND
(0 - 9.5' BLS)
5 - 10 6' - 0.76
8' - 0.88
10 - 12 10' - 0.00
12' - 0.40
Installation Method: Geoprobe Borehole Diameter: 2"
dry, no odor
Orangish brown silty fine SAND
(9.5' - 12' BLS)
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-8 Date: 2/6/07
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
Screened Interval:
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 1.53
4' - 1.17 0 - 5': Brownish orange silty fine SAND dry, no odor
5 - 10 6' - 1.21
8' - 1.12
5' - 10': Orangish yellow silty fine
SAND dry, no odor
10 - 12 10' - 1.26
12' - 1.08
10' - 11': Red rock fragments and fine
sand SILT
11' - 12': Orange silty fine SAND
dry, no odor
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-9 Date: 2/6/07
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
UST Lines - Inside Bay
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 1.53
4' - 1.65 0 - 5': Brownish orange silty fine SAND dry, no odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 5' Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-10 Date: 2/6/07
UST Lines - Inside Bay
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 2.11
4' - 1.73 0 - 5': Brownish orange silty fine SAND dry, no odor
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-11 Date: 2/6/07
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 5' Well Diameter:
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 1.52
4' - 1.54 0 - 7': Brownish orange silty fine SAND dry, no odor
5 - 10
6' - 1.47
7' - 1.87
8' - 1.90
7' - 7.5': Black silty fine SAND dry, no odor
10 - 12 10' - 1.26
12' - 1.08
7.5' - 12': Brownish orange silty fine
SAND dry, no odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-12 Date: 2/6/07
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 2.32
4' - 2.00 Brownish orange silty fine SAND dry, no odor
5 - 10 6' - 1.76
8' - 1.96 Brownish orange silty fine SAND dry, no odor
10 - 12 10' - 1.78
12' - 1.76 Brownish orange silty fine SAND dry, no odor
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-13 Date: 2/6/07
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 2.25
4' - 2.11
0 - 5': Brownish orange silty fine
SAND dry, no odor
5 - 10 6' - 2.17
8' - 2.18 5' - 7': Gray fine sandy SILT dry, no odor
10 - 12 10' - 3.06
12' - 2.79 7' - 12': Orange silt fine SAND dry, no odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-14 Date: 2/6/07
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 2.22
4' - 2.19 Brownish orange silty fine SAND dry, no odor
5 - 10 6' - 2.96
8' - 2.23 Brownish orange silty fine SAND dry, no odor
10 - 12 10' - 2.19
12' - 2.24 Brownish orange silty fine SAND dry, no odor
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-15 Date: 2/6/07
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5
2' - not enough
recovery
4' - 2.81
Brownish orange silty fine SAND dry, no odor
5 - 10 6' - 2.84
8' - 2.86 Brownish orange silty fine SAND dry, no odor
10 - 12 10' - 2.76
12' - 2.64 Brownish orange silty fine SAND dry, no odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-16 Date: 2/6/07
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 2.98
4' - 3.15 Brownish orange silty fine SAND dry, no odor
5 - 10 6' - 3.00
8' - 2.86 Brownish orange silty fine SAND dry, no odor
10 - 12 10' - 2.32
12' - 2.31 Brownish orange silty fine SAND dry, no odor
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-17 Date: 2/6/07
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 4.99
4' - 3.08 0 - 9': Brownish orange silty fine SAND 0 - 10': dry, no odor
5 - 10 6' - 3.00
8' - 4.26 9' - 12': Orange fine sandy SILT 10' - 11': moist, no odor
10 - 12 10' - 3.15
12' - 3.76 9' - 12': Orange fine sandy SILT 11' - 12': dry, no odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-18 Date: 2/6/07
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 3.06
4' - 2.86
0 - 5': Brownish orange fine sandy
SILT dry, no odor
5 - 10 6' - 4.06
8' - 4.40 5' - 12': Orange brown silty fine SAND dry, no odor
10 - 12 10' - 3.54
12' - 3.90 5' - 12': Orange brown silty fine SAND dry, no odor
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-19 Date: 2/6/07
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 4.64
4' - 2.84 Brownish orange silty fine SAND dry, no odor
5 - 10 6' - 3.13
8' - 3.74 Brownish orange silty fine SAND dry, no odor
10 - 12 10' - 5.01
12' - 4.92 Brownish orange silty fine SAND dry, no odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-20 Date: 2/6/07
Hydraulic Lift
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 3.24
4' - 3.10 Brownish orange silty fine SAND dry, no odor
5 - 10 6' - 2.92
8' - 2.90 Brownish orange silty fine SAND dry, no odor
10 - 12 10' - 2.89
12' - 2.75 Brownish orange silty fine SAND dry, no odor
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-21 Date: 2/6/07
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 12' Well Diameter:
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Former UST Lines - Outside
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 2.60
4' - 2.60 Brownish orange silty fine SAND moist, petroleum odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 5'Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-22 Date: 2/6/07
Former UST Lines - Outside
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 2.33
4' - 2.45 Brownish orange silty fine SAND dry, petroleum odor
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-23 Date: 2/6/07
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 5' Well Diameter:
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Former UST Lines - Outside
Split Spoon
Interval (ft.)
Field Screening
Results (ppm)Lithology (soil type, color, etc.)Soil Conditions (dry,
moist, petroleum odor)
0 - 5 2' - 2.47
4' - 2.50 Brownish orange silty fine SAND dry, petroleum odor
Screened Interval:
Bentonite Interval:
Outer Casing Interval:
Sand Interval:
Grout Interval:
Outer Casing Diameter:
Installation Method: Geoprobe Borehole Diameter: 2"
WELL CONSTRUCTION DETAILS (if applicable)
Total Depth: 5'Well Diameter:
SOIL BORING/MONITORING WELL LOG
Project Name: Elkins Project No.: 000R1816.01
Boring/MW No.: SB-24 Date: 2/6/07

ATTACHMENT B

LABORATORY ANALYTICAL REPORTS
Client Sample ID: HA-1 @ 6 BLS
SGS ENVIRONMENTAL SERVICES, INC.
Results for Volatiles
by GCMS 8260-5030
Analyzed By: MJC
Client Project ID: Elkins Chrysler Mitsubishi Date Collected: 02-07-2007 14:28
Lab Sample ID G122-2913-1A Date Received: 2/9/2007
Lab Project ID: G122-2913 Matrix: Soil
Report Basis: Dry Weight %Solids: 88.2
Report Name Result Quantitation MDL Dilution Date
Compound UG/KG Limit UG/KG UG/KG Factor Analyzed Flag
Acetone 22.3 46.6 2.59 1 2/10/2007 J
Benzene BQL 4.66 2.81 1 2/10/2007
Bromobenzene BQL 4.66 3.02 1 2/10/2007
Bromochloromethane BQL 4.66 2.06 1 2/10/2007
Bromodichloromethane BQL 4.66 2.46 1 2/10/2007
Bromoform BQL 4.66 2.11 1 2/10/2007
Bromomethane BQL 4.66 4.47 2/10/2007
2-Butanone BQL 23.3 2.99 2/10/2007
n-Butylbenzene BQL 4.66 2.55 2/10/2007
sec-Butyl benzene BQL 4.66 3.61 2/10/2007
tert-Butylbenzene BQL 4.66 3.43 2/10/2007
Carbon disulfide BQL 4.66 2.43 2/10/2007
Carbon tetrachloride BQL 4.66 3.27 2/10/2007
Chlorobenzene BQL 4.66 3.27 2/10/2007
Chloroethane BQL 4.66 4.13 2/10/2007
Chloroform BQL 4.66 2.71 2/10/2007
Chloromethane BQL 4.66 2.90 2/10/2007
2-Chlorotoluene BQL 4.66 3.22 2/10/2007
4-Chlorotoluene BQL 4.66 3.37 2/10/2007
Dibromochloromethane BQL 4.66 2.35 2/10/2007
1,2-Dibromo-3-chloropropane BQL 4.66 6.76 2/10/2007
Dibromomethane BQL 4.66 1.66 2/10/2007
1,2-Dibromoethane (EDB) BQL 4.66 1.73 2/10/2007
1,2-Dichlorobenzene BQL 4.66 2.81 2/10/2007
1,3-Dichlorobenzene BQL 4.66 3.06 2/10/2007
1,4-Dichlorobenzene BQL 4.66 2.97 2/10/2007
trans-1,4-Dichloro-2-butene BQL 4.66 6.14 2/10/2007
1, 1-Dichloroethane BQL 4.66 3.23 2/10/2007
1, 1-Dichloroethene BQL 4.66 3.33 2/10/2007
1,2-Dichloroethane BQL 4.66 2.23 2/10/2007
cis-1,2-Dichloroethene BQL 4.66 2.95 2/10/2007
trans-1,2-dichloroethene BQL 4.66 3.33 2/10/2007
1,2-Dichloropropane BQL 4.66 2.58 2/10/2007
1,3-Dichloropropane BQL 4.66 1.91 2/10/2007
2,2-Dichloropropane BQL 4.66 2.69 2/10/2007
1, 1-Dichloropropene BQL 4.66 3.26 2/10/2007
cis-1,3-Dichloropropene BQL 4.66 2.18 1 2/10/2007
trans-1,3-Dichloropropene BQL 4.66 1.85 1 2/10/2007
Dichlorodifluoromethane BQL 4.66 3.36 1 2/10/2007
Diisopropyl ether (DIPE) BQL 4.66 2.73 1 2/10/2007
Ethyl benzene BQL 4.66 3.32 1 2/10/2007
Hexachlorobutadiene BQL 4.66 3.34 1 2/10/2007
Page 1 of 2 GCMS_LIMS_SOLO_V1 .74
N.C. CERTIFICATION #481 2of14
Client Sample ID: HA-1 @ 6 BLS
SGS ENVIRONMENTAL SERVICES, INC.
Results for Volatiles
by GCMS 8260-5030
Analyzed By: MJC
Client Project ID: Elkins Chrysler Mitsubishi Date Collected: 02-07-2007 14:28
Lab Sample ID G122-2913-1A Date Received: 2/9/2007
Lab Project ID: G122-2913 Matrix: Soil
Report Basis: Dry Weight %Solids: 88.2
Report Name Result Quantitation MDL Dilution Date
Compound UG/KG Limit UG/KG UG/KG Factor Analyzed Flag
2-Hexanone BQL 4.66 1.66 1 2/10/2007
lodomethane BQL 4.66 3.36 1 2/10/2007
lsopropylbenzene BQL 4.66 3.53 1 2/10/2007
4-lsopropyltoluene BQL 4.66 3.43 1 2/10/2007
Methylene chloride BQL 18.6 2.87 1 2/10/2007
4-Methyl-2-pentanone BQL 4.66 1 .11 1 2/10/2007
Methyl-tert-butyl ether (MTBE) BQL 4.66 2.12 2/10/2007
Naphthalene BQL 4.66 2.22 2/10/2007
n-Propyl benzene BQL 4.66 3.47 1 2/10/2007
Styrene BQL 4.66 4.40 1 2/10/2007
1 , 1, 1 ,2-Tetrachloroethane BQL 4.66 2.71 1 2/10/2007
1, 1,2,2-Tetrachloroethane BQL 4.66 1.69 1 2/10/2007
Tetrachloroethene BQL 4.66 3.56 2/10/2007
Toluene BQL 4.66 3.01 2/10/2007
1,2,3-Trichlorobenzene BQL 4.66 2.45 2/10/2007
1,2,4-Trichlorobenzene BQL 4.66 2.17 2/10/2007
Trichloroethane BQL 4.66 3.24 1 2/10/2007
1, 1 , 1-Trichloroethane BQL 4.66 3.26 1 2/10/2007
1, 1,2-Trichloroethane BQL 4.66 1.87 1 2/10/2007
Trichlorofluoromethane BQL 4.66 3.66 1 2/10/2007
1,2,3-Trichloropropane BQL 4.66 1.73 2/10/2007
1,2,4-Trimethylbenzene BQL 4.66 3.37 2/10/2007
1,3,5-Trimethylbenzene BQL 4.66 3.45 2/10/2007
Vinyl chloride BQL 4.66 3.21 2/10/2007
m-,p-Xylene BQL 9.32 6.85 2/10/2007
a-Xylene BQL 4.66 3.31 2/10/2007
Spike Spike Percent
Added Result Recovered
4-Bromofluorobenzene 50 37.4 75
1,2-Dichloroethane-d4 50 63.3 127
Toluene-dB 50 42.8 86
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Reviewed By: w
Page 2 of 2
N.C. CERTIFICATION #481
GCMS_LIMS_SOLO_V1 .74
3of14
Client Sample ID: HA-2 @ 2 BLS
SGS ENVIRONMENTAL SERVICES, INC.
Results for Volatiles
by GCMS 8260-5030
Analyzed By: MJC
Client Project ID: Elkins Chrysler Mitsubishi Date Collected: 02-08-2007 12:17
Lab Sample ID G122-2913-2A Date Received: 2/9/2007
Lab Project ID: G122-2913 Matrix: Soil
Report Basis: Dry Weight %Solids: 83.2
Report Name Result Quantitation MDL Dilution Date
Compound UG/KG Limit UG/KG UG/KG Factor Analyzed Flag
Acetone 27.6 49.1 2.73 1 2/10/2007 J
Benzene BQL 4.91 2.97 2/10/2007
Bromobenzene BQL 4.91 3.18 2/10/2007
Bromochloromethane BQL 4.91 2.17 2/10/2007
Bromodichloromethane BQL 4.91 2.59 2/10/2007
Bromoform BQL 4.91 2.22 2/10/2007
Bromomethane BQL 4.91 4.71 2/10/2007
2-Butanone 4.30 24.6 3.15 2/10/2007 J
n-Butylbenzene BQL 4.91 2.69 2/10/2007
sec-Butyl benzene BQL 4.91 3.80 2/10/2007
tert-Butylbenzene BQL 4.91 3.61 1 2/10/2007
Carbon disulfide BQL 4.91 2.56 1 2/10/2007
Carbon tetrachloride BQL 4.91 3.45 2/10/2007
Chlorobenzene BQL 4.91 3.45 2/10/2007
Chloroethane BQL 4.91 4.35 2/10/2007
Chloroform BQL 4.91 2.86 2/10/2007
Chloromethane BQL 4.91 3.05 2/10/2007
2-Chlorotoluene BQL 4.91 3.40 2/10/2007
4-Chlorotoluene BQL 4.91 3.56 2/10/2007
Dibromochloromethane BQL 4.91 2.47 2/10/2007
1,2-Dibromo-3-chloropropane BQL 4.91 7.12 1 2/10/2007
Dibromomethane BQL 4.91 1.75 1 2/10/2007
1,2-Dibromoethane (EDB) BQL 4.91 1.83 1 2/10/2007
1,2-Dichlorobenzene BQL 4.91 2.97 1 2/10/2007
1,3-Dichlorobenzene BQL 4.91 3.22 1 2/10/2007
1,4-Dichlorobenzene BQL 4.91 3.13 2/10/2007
trans-1,4-Dichloro-2-butene BQL 4.91 6.47 2/10/2007
1, 1-Dichloroethane BQL 4.91 3.41 2/10/2007
1, 1-Dichloroethene BQL 4.91 3.51 2/10/2007
1,2-Dichloroethane BQL 4.91 2.35 2/10/2007
cis-1,2-Dichloroethene BQL 4.91 3.11 1 2/10/2007
trans-1,2-dichloroethene BQL 4.91 3.51 1 2/10/2007
1,2-Dichloropropane BQL 4.91 2.72 1 2/10/2007
1,3-Dichloropropane BQL 4.91 2.01 1 2/10/2007
2,2-Dichloropropane BQL 4.91 2.84 1 2/10/2007
1, 1-Dichloropropene BQL 4.91 3.44 2/10/2007
cis-1,3-Dichloropropene BQL 4.91 2.30 2/10/2007
trans-1,3-Dichloropropene BQL 4.91 1.94 2/10/2007
Dichlorodifluoromethane BQL 4.91 3.54 2/10/2007
Diisopropyl ether (DIPE) BQL 4.91 2.88 1 2/10/2007
Ethyl benzene BQL 4.91 3.50 1 2/10/2007
Hexach lorobutad iene BQL 4.91 3.52 1 2/10/2007
Pafe 1of2 N.C. CER IFICATION #481 GCMS_LIMS_SOLO_V14 Qf 14
Client Sample ID: HA-2@ 2 BLS
SGS ENVIRONMENTAL SERVICES, INC.
Results for Volatiles
by GCMS 8260-5030
Analyzed By: MJC
Client Project ID: Elkins Chrysler Mitsubishi Date Collected: 02-08-2007 12: 17
Lab Sample ID G122-2913-2A Date Received: 2/9/2007
Lab Project ID: G122-2913 Matrix: Soil
Report Basis: Dry Weight %Solids: 83.2
Report Name Result Quantitation MDL Dilution Date
Compound UG/KG Limit UG/KG UG/KG Factor Analyzed Flag
2-Hexanone BQL 4.91 1.75 1 2/10/2007
lodomethane BQL 4.91 3.54 1 2/10/2007
lsopropylbenzene BQL 4.91 3.72 1 2/10/2007
4-lsopropyltoluene BQL 4.91 3.61 1 2/10/2007
Methylene chloride BQL 19.6 3.02 2/10/2007
4-Methyl-2-pentanone BQL 4.91 1.17 2/10/2007
Methyl-tert-butyl ether (MTBE) BQL 4.91 2.23 2/10/2007
Naphthalene BQL 4.91 2.34 2/10/2007
n-Propyl benzene BQL 4.91 3.65 2/10/2007
Styrene BQL 4.91 4.64 2/10/2007
1, 1, 1,2-Tetrachloroethane BQL 4.91 2.86 2/10/2007
1, 1,2,2-Tetrachloroethane BQL 4.91 1.78 2/10/2007
Tetrachloroethene BQL 4.91 3.75 2/10/2007
Toluene 6.89 4.91 3.17 2/10/2007
1,2,3-Trichlorobenzene BQL 4.91 2.58 2/10/2007
1,2,4-Trichlorobenzene BQL 4.91 2.29 2/10/2007
Trichloroethane BQL 4.91 3.42 2/10/2007
1, 1, 1-Trichloroethane BQL 4.91 3.44 2/10/2007
1, 1,2-Trichloroethane BQL 4.91 1.97 2/10/2007
Trichlorofluoromethane BQL 4.91 3.86 2/10/2007
1,2,3-Trichloropropane BQL 4.91 1.83 2/10/2007
1,2,4-Trimethylbenzene BQL 4.91 3.56 2/10/2007
1,3,5-Trimethylbenzene BQL 4.91 3.63 2/10/2007
Vinyl chloride BQL 4.91 3.38 2/10/2007
m-,p-Xylene BQL 9.82 7.22 2/10/2007
a-Xylene BQL 4.91 3.49 2/10/2007
Spike Spike Percent
Added Result Recovered
4-Bromofluorobenzene 50 37.1 74
1,2-Dichloroethane-d4 50 67.2 134
Toluene-dB 50 43.2 86
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Reviewed By: N..f
Pag_e 2 of 2 N.C. CERTIFICATION #481
GCMS LIMS SOLO V1.74 ---5 of 14
Client Sample ID: HA-3 @ 5 BLS
SGS ENVIRONMENTAL SERVICES, INC.
Results for Volatiles
by GCMS 8260-5030
Analyzed By: MJC
Client Project ID: Elkins Chrysler Mitsubishi Date Collected: 02-08-2007 12:23
Lab Sample ID G122-2913-3A Date Received: 2/9/2007
Lab Project ID: G122-2913 Matrix: Soil
Report Basis: Dry Weight %Solids: 85.1
Report Name Result Quantitation MDL Dilution Date
Compound UG/KG Limit UG/KG UG/KG Factor Analyzed Flag
Acetone 9.10 51.7 2.88 1 2/10/2007 J
Benzene BQL 5.17 3.12 2/10/2007
Bromobenzene BQL 5.17 3.35 2/10/2007
Bromochloromethane BQL 5.17 2.29 1 2/10/2007
Bromodichloromethane BQL 5.17 2.73 1 2/10/2007
Bromoform BQL 5.17 2.34 1 2/10/2007
Bromomethane BQL 5.17 4.97 1 2/10/2007
2-Butanone BQL 25.9 3.32 1 2/10/2007
n-Butylbenzene BQL 5.17 2.83 2/10/2007
sec-Butyl benzene BQL 5.17 4.00 2/10/2007
tert-Butylbenzene BQL 5.17 3.81 2/10/2007
Carbon disulfide BQL 5.17 2.70 2/10/2007
Carbon tetrachloride BQL 5.17 3.63 2/10/2007
Chlorobenzene BQL 5.17 3.63 2/10/2007
Chloroethane BQL 5.17 4.58 2/10/2007
Chloroform BQL 5.17 3.01 2/10/2007
Chloromethane BQL 5.17 3.22 2/10/2007
2-Chlorotoluene BQL 5.17 3.58 2/10/2007
4-Chlorotoluene BQL 5.17 3.74 2/10/2007
Dibromochloromethane BQL 5.17 2.61 2/10/2007
1,2-Dibromo-3-chloropropane BQL 5.17 7.50 2/10/2007
Dibromomethane BQL 5.17 1.84 2/10/2007
1,2-Dibromoethane (EDS) BQL 5.17 1.92 2/10/2007
1,2-Dichlorobenzene BQL 5.17 3.12 2/10/2007
1,3-Dichlorobenzene BQL 5.17 3.39 2/10/2007
1,4-Dichlorobenzene BQL 5.17 3.30 2/10/2007
trans-1,4-Dichloro-2-butene BQL 5.17 6.82 2/10/2007
1, 1-Dichloroethane BQL 5.17 3.59 2/10/2007
1, 1-Dichloroethene BQL 5.17 3.69 2/10/2007
1,2-Dichloroethane BQL 5.17 2.47 2/10/2007
cis-1,2-Dichloroethene BQL 5.17 3.28 2/10/2007
trans-1,2-dichloroethene BQL 5.17 3.69 2/10/2007
1,2-Dichloropropane BQL 5.17 2.87 2/10/2007
1,3-Dichloropropane BQL 5.17 2.12 2/10/2007
2,2-Dichloropropane BQL 5.17 2.99 2/10/2007
1, 1-Dichloropropene BQL 5.17 3.62 2/10/2007
cis-1,3-Dichloropropene BQL 5.17 2.42 2/10/2007
trans-1,3-Dichloropropene BQL 5.17 2.05 2/10/2007
Dichlorodifluoromethane BQL 5.17 3.72 2/10/2007
Diisopropyl ether (DIPE) BQL 5.17 3.03 2/10/2007
Ethyl benzene BQL 5.17 3.68 2/10/2007
Hexachlorobutadiene BQL 5.17 3.70 2/10/2007
PlTe 1 of 2 GCMS_LIMS_SOLO_V1 .74 N.C. CER FICATION #481 6Of14
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: HA-3 @ 5 BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID G122-2913-3A
Lab Project ID: G122-2913
Report Basis: Dry Weight
Report Name Result
Compound UG/KG
2-Hexanone BQL
lodomethane BQL
lsopropylbenzene BQL
4-lsopropyltoluene BQL
Methylene chloride BQL
4-Methyl-2-pentanone BQL
Methyl-tert-butyl ether (MTBE) BQL
Naphthalene BQL
n-Propyl benzene BQL
Styrene BQL
1, 1, 1,2-Tetrachloroethane BQL
1, 1,2,2-Tetrachloroethane BQL
Tetrachloroethene BQL
Toluene BQL
1,2,3-Trichlorobenzene BQL
1,2,4-Trichlorobenzene BQL
Trichloroethane BQL
1, 1 , 1-Trichloroethane BQL
1, 1,2-Trichloroethane BQL
Trichlorofluoromethane BQL
1,2,3-Trichloropropane BQL
1,2,4-Trimethylbenzene BQL
1,3,5-Trimethylbenzene BQL
Vinyl chloride BQL
m-,p-Xylene BQL
a-Xylene BQL
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Results for Volatiles
by GCMS 8260-5030
Quantitation MDL
Limit UG/KG UG/KG
5.17 1.84
5.17 3.72
5.17 3.92
5.17 3.81
20.7 3.19
5.17 1.23
5.17 2.35
5.17 2.46
5.17 3.85
5.17 4.88
5.17 3.01
5.17 1.87
5.17 3.95
5.17 3.34
5.17 2.72
5.17 2.41
5.17 3.60
5.17 3.62
5.17 2.08
5.17 4.07
5.17 1.92
5.17 3.74
5.17 3.83
5.17 3.56
10.3 7.60
5.17 3.67
Spike Spike
Added Result
50 33.2
50 68.5
50 41.9
Page 2 of 2
N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected: 02-08-2007 12:23
Date Received: 2/9/2007
Matrix: Soil
%Solids: 85.1
Dilution Date
Factor Analyzed Flag
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
Percent
Recovered
66
137
84
Reviewed By: <c_....j!
GCMS_LIMS_SOLO_V1 .74
7of14
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID VBLK9021007B
Lab Project ID:
Report Basis: Dry Weight
Report Name
Compound
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
n-Butylbenzene
sec-Butyl benzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromo-3-chloropropane
Dibromomethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1 , 1-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloroethane
cis-1,2-Dichloroethene
trans-1,2-dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Dichlorodifluoromethane
Diisopropyl ether (DIPE)
Ethyl benzene
Hexachlorobutadiene
SGS ENVIRONMENTAL SERVICES, INC.
Result
UG/KG
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 8260-5030
Quantitation MDL
Limit UG/KG UG/KG
50.0 2.78
5.00 3.02
5.00 3.24
5.00 2.21
5.00 2.64
5.00 2.26
5.00 4.80
25.0 3.21
5.00 2.74
5.00 3.87
5.00 3.68
5.00 2.61
5.00 3.51
5.00 3.51
5.00 4.43
5.00 2.91
5.00 3.11
5.00 3.46
5.00 3.62
5.00 2.52
5.00 7.25
5.00 1.78
5.00 1.86
5.00 3.02
5.00 3.28
5.00 3.19
5.00 6.59
5.00 3.47
5.00 3.57
5.00 2.39
5.00 3.17
5.00 3.57
5.00 2.77
5.00 2.05
5.00 2.89
5.00 3.50
5.00 2.34
5.00 1.98
5.00 3.60
5.00 2.93
5.00 3.56
5.00 3.58
Paf1{ 1 of 2 N.C. CER IFICATION #481
Analyzed By: MJC
Date Collected:
Date Received:
Matrix: Soil
%Solids: 100.0
Dilution Date
Factor Analyzed Flag
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
GCMS_LIMS_SOLO_V1.78 Qf 14
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID VBLK9021007B
Lab Project ID:
Report Basis: Dry Weight
Report Name
Compound
2-Hexanone
lodomethane
lsopropylbenzene
4-lsopropyltoluene
Methylene chloride
4-Methyl-2-pentanone
Methyl-tert-butyl ether (MTBE)
Naphthalene
n-Propyl benzene
Styrene
1, 1, 1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Trichloroethane
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-,p-Xylene
a-Xylene
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
Comments:
Flags:
BQL =Below Quantitation Limits.
J = Detected below the quantitation limit.
SGS ENVIRONMENTAL SERVICES, INC.
Result
UG/KG
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 8260-5030
Quantitation MDL
Limit UG/KG UG/KG
5.00 1.78
5.00 3.60
5.00 3.79
5.00 3.68
20.0 3.08
5.00 1.19
5.00 2.27
5.00 2.38
5.00 3.72
5.00 4.72
5.00 2.91
5.00 1.81
5.00 3.82
5.00 3.23
5.00 2.63
5.00 2.33
5.00 3.48
5.00 3.50
5.00 2.01
5.00 3.93
5.00 1.86
5.00 3.62
5.00 3.70
5.00 3.44
10.0 7.35
5.00 3.55
Spike Spike
Added Result
50 44.3
50 43.6
50 42.1
Page 2 of 2
Analyzed By: MJC
Date Collected:
Date Received:
Matrix: Soil
%Solids: 100.0
Dilution Date
Factor Analyzed Flag
1 2/10/2007
1 2/10/2007
2/10/2007
2/10/2007
2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
2/10/2007
2/10/2007
2/10/2007
Percent
Recovered
89
87
84
Reviewed By: i-..J
N.C. CERTIFICATION #481
GCMS_LIMS_SOLO_V1 .749 Qf 14
SGS ENVIRONMENTAL SERVICES, INC.
List of Reporting Abbreviations
and Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantitation Limit (RL or MDL)
DF =Dilution Factor
Dup = Duplicate
D = Detected, but RPO is > 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL= Method Detection Limit
MS(D) =Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL = Reporting Limit
RPO = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
N.C. CERTIFICATION #481
M134.030606.3
13 of 14
Mr. Darin McClure
Mid-Atlantic Associates
409 Rogersview Ct.
Raleigh NC 27610
Report Number: G 122-2908
SGS ENVIRONMENTAL SERVICES, INC.
Client Project: Elkins Chrysler Mitsubishi
Dear Mr. McClure:
Enclosed are the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
lfthere are any questions about the report or the services performed during this project,
please call SGS/Paradigm at [phone]. We will be happy to answer any questions
or concerns which you may have.
Thank you for using SGS/Paradigm Analytical Labs for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Analytical Laboratories, Inc.
N.C. CERTIFICATION #481 1 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-8@2' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G 122-2908-1 B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 34.8
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
2/6/2007 10:47
21712007
86.24
Result
MG/KG
731
Reviewed By: 'b-i1
9071 LIMS v1 .35 - - 2 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-8@2' BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: g122-2908-1 D
Lab Project ID: G122-2908
Matrix: Soil
Parameter Method RL
MG/KG
Oil & Grease 9071 35.7
Comments:
Silica Gel Clean-up performed.
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
Date Analyzed:
Analyzed By:
Date Collected:
Date Received:
Solids:
2/19/2007
alt
21612007 10:47
21712007
86.24
Result
MG/KG
3540
Reviewed By: ~
9071 LIMS v1 .35 - - 3 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-9@10' BLS Date Analyzed: 2/13/2007
Client Project ID: Elkins Chysler Mitsubishi Analyzed By: alt
Lab Sample ID: G122-2908-2B Date Collected: 21612007 11 : 18
Lab Project ID: G122-2908 Date Received: 21712007
Matrix: Soil Solids: 84.94
Parameter Method RL Result
MG/KG MG/KG
Oil & Grease 9071 35.6 224
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
Reviewed By: ~?
9071 LIMS v1 .35
N.C. CERTIFICATION #481 --4 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-10@4' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-3B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 36.4
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21612007 11 :26
21712007
83.76
Result
MG/KG
225
Reviewed By: \'2..Jl
9071 LIMS v1 .35 --5 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-11@2' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-4B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 36.2
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21612007 11 :34
21712007
85.59
Result
MG/KG
2280
Reviewed By: N
9071 LIMS v1 .35 - - 6 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-11@2' BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: g 122-2908-4D
Lab Project ID: G122-2908
Matrix: Soil
Parameter Method RL
MG/KG
Oil & Grease 9071 36
Comments:
Silica Gel Clean-up performed.
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
Date Analyzed:
Analyzed By:
Date Collected:
Date Received:
Solids:
2/19/2007
alt
21612007 11 :34
21712007
85.59
Result
MG/KG
2400
Reviewed By: M__
9071 LIMS v1 .35 - - 7 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-12@12' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-5B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 35
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
2/6/2007 11 :59
21712007
85.46
Result
MG/KG
140
Reviewed By: hf!
9071 LIMS v1 .35 - - 8 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-13@2' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-6B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 37.8
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21612007 12:20
21712007
82.25
Result
MG/KG
2330
Reviewed By: U
9071 LIMS v1 .35 - - 9 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-13@2' BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: g122-2908-6D
Lab Project ID: G122-2908
Matrix: Soil
Parameter Method RL
MG/KG
Oil & Grease 9071 35.9
Comments:
Silica Gel Clean-up performed.
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
Date Analyzed:
Analyzed By:
Date Collected:
Date Received:
Solids:
2/19/2007
alt
2/6/2007 12:20
21712007
82.25
Result
MG/KG
2890
Reviewed By: M..-
9071 _LIMS_ v1 .35
10 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-14@10' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-7B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 35.5
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21612007 12:33
21712007
86.06
Result
MG/KG
92.3
Reviewed By: H
9071 LIMS v1 .35 - -11 Of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-15@6' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-8B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 34.9
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
2/6/2007 12:52
21712007
85.12
Result
MG/KG
175
Reviewed By: ~
9071 LIMS v1 .35 - -12 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-16@8' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-9B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 36.9
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21612007 13:06
21712007
82.25
Result
MG/KG
162
Reviewed By: _'lhl~-
9071 LIMS v1 .35
- -13 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-17@4' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G 122-2908-1 OB Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 35.1
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21612007 13: 19
21712007
86.90
Result
MG/KG
280
Reviewed By: q_.JI
9071 LIMS v1 .35 - -14 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-17@4' BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: g122-2908-10D
Lab Project ID: G122-2908
Matrix: Soil
Parameter Method RL
MG/KG
Oil & Grease 9071 35.6
Comments:
Silica Gel Clean-up performed.
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
Date Analyzed:
Analyzed By:
Date Collected:
Date Received:
Solids:
2/19/2007
alt
21612007 13: 19
21712007
86.90
Result
MG/KG
BQL
Reviewed By: RA.u_
9071 LIMS v1 .35 - -15 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-18@2' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-11 B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 35.4
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21612007 13:52
21712007
85.15
Result
MG/KG
110
Reviewed By: \J..s:-Q
9071 LIMS v1 .35
- -16 Of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-19@8' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-12B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 36.2
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
2/6/2007 14: 10
21712007
82.68
Result
MG/KG
177
Reviewed By: <4fJ
9071 LIMS v1 .35 - -17 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-20@12' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-13B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 34.4
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21612007 14:41
21712007
85.81
Result
MG/KG
110
Reviewed By: (t'"tf
9071 LIMS v1 .35 - -18 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-21@2' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2908-14B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 36.7
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21612007 15:05
21712007
84.36
Result
MG/KG
91.7
Reviewed By: !b---41
9071 LIMS v1 .35 - -19 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-22@2' BLS Date Analyzed:
Client Project ID: Elkins Chysler Mitsubishi Analyzed By:
Lab Sample ID: G 122-2908-15B Date Collected:
Lab Project ID: G122-2908 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 38.7
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21612007 15:40
21712007
78.53
Result
MG/KG
1910
Reviewed By: N
9071 LIMS v1 .35 - -20 of 26
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-22@2' BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: g122-2908-15D
Lab Project ID: G122-2908
Matrix: Soil
Parameter Method RL
MG/KG
Oil & Grease 9071 37.9
Comments:
Silica Gel Clean-up performed.
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
Date Analyzed:
Analyzed By:
Date Collected:
Date Received:
Solids:
2/19/2007
alt
21612007 15:40
21712007
78.53
Result
MG/KG
1800
Reviewed By: KML
9071 LIMS v1 .35 --21 Of 26
SGS ENVIRONMENTAL SERVICES, INC.
List of Reporting Abbreviations
and Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantitation Limit (RL or MDL}
OF= Dilution Factor
Dup = Duplicate
D =Detected, but RPO is> 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) =Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL = Reporting Limit
RPD = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
N.C. CERTIFICATION #481
Ml34.030606.3
24 of 26
Mr. Darin McClure
Mid-Atlantic Associates
409 Rogersview Ct.
Raleigh NC 27610
Report Number: G 122-2909
SGS ENVIRONMENTAL SERVICES, INC.
Client Project: Elkins Chrysler Mitsubishi
Dear Mr. McClure:
Enclosed are the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call SGS/Paradigm at [phone]. We will be happy to answer any questions
or concerns which you may have.
Thank you for using SGS/Paradigm Analytical Labs for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely,
SGS/Paradigm Analytical Laboratories, Inc.
__ 1:-t~_l-l Lauoratory Director _;zjJY /~ -----bate
J. Patrick Weaver
N.C. CERTIFICATION #481 1 of 35
Client Sample ID: SB-3 @ 9.5 to 10 BLS
SGS ENVIRONMENTAL SERVICES, INC.
Results for Volatiles
by GCMS 8260-5030
Analyzed By: MJC
Client Project ID: Elkins Chrysler Mitsubishi Date Collected: 02-05-2007 15:55
Lab Sample ID G 122-2909-3B Date Received: 2/7/2007
Lab Project ID: G122-2909 Matrix: Soil
Report Basis: Dry Weight %Solids: 82.2
Report Name Result Quantitation MDL Dilution Date
Compound UG/KG Limit UG/KG UG/KG Factor Analyzed Flag
Acetone 4.80 47.2 2.63 1 21912007 J
Benzene BQL 4.72 2.85 1 2/9/2007
Bromobenzene BQL 4.72 3.06 1 2/9/2007
Bromochloromethane BQL 4.72 2.09 1 2/9/2007
Bromodichloromethane BQL 4.72 2.49 1 2/9/2007
Bromoform BQL 4.72 2.13 1 2/9/2007
Bromomethane BQL 4.72 4.53 1 2/9/2007
2-Butanone BQL 23.6 3.03 1 2/9/2007
n-Butylbenzene BQL 4.72 2.59 1 21912007
sec-Butyl benzene BQL 4.72 3.66 1 2/9/2007
tert-Butylbenzene BQL 4.72 3.48 1 21912007
Carbon disulfide BQL 4.72 2.47 1 2/9/2007
Carbon tetrachloride BQL 4.72 3.32 1 21912007
Chlorobenzene BQL 4.72 3.32 1 21912007
Chloroethane BQL 4.72 4.18 2/9/2007
Chloroform BQL 4.72 2.75 21912007
Chloromethane BQL 4.72 2.94 2/9/2007
2-Chlorotoluene BQL 4.72 3.27 21912007
4-Chlorotoluene BQL 4.72 3.42 21912007
Dibromochloromethane BQL 4.72 2.38 2/9/2007
1,2-Dibromo-3-chloropropane BQL 4.72 6.85 21912007
Dibromomethane BQL 4.72 1.68 1 21912007
1,2-Dibromoethane (EDB) BQL 4.72 1.76 1 21912007
1,2-Dichlorobenzene BQL 4.72 2.85 1 21912007
1,3-Dichlorobenzene BQL 4.72 3.10 1 2/9/2007
1,4-Dichlorobenzene BQL 4.72 3.01 1 2/9/2007
trans-1,4-Dichloro-2-butene BQL 4.72 6.22 1 21912007
1, 1-Dichloroethane BQL 4.72 3.28 2/9/2007
1, 1-Dichloroethene BQL 4.72 3.37 2/9/2007
1,2-Dichloroethane BQL 4.72 2.26 21912007
cis-1,2-Dichloroethene BQL 4.72 2.99 2/9/2007
trans-1,2-dichloroethene BQL 4.72 3.37 2/9/2007
1,2-Dichloropropane BQL 4.72 2.62 21912007
1,3-Dichloropropane BQL 4.72 1.94 2/9/2007
2,2-Dichloropropane BQL 4.72 2.73 21912007
1, 1-Dichloropropene BQL 4.72 3.31 21912007
cis-1,3-Dichloropropene BQL 4.72 2.21 2/9/2007
trans-1,3-Dichloropropene BQL 4.72 1.87 2/9/2007
Dichlorodifluoromethane BQL 4.72 3.40 2/9/2007
Diisopropyl ether (DIPE) BQL 4.72 2.77 2/9/2007
Ethyl benzene BQL 4.72 3.36 21912007
Hexachlorobutadiene BQL 4.72 3.38 21912007
Page 1 of 2 GCMS_LIMS_SOLO_V1 .74
N.C. CERTIFICATION #481 2of35
Client Sample ID: SB-5 @ 8 to 9 BLS
SGS ENVIRONMENTAL SERVICES, INC.
Results for Volatiles
by GCMS 82608/5035
Analyzed By: MJC
Client Project ID: Elkins Chrysler Mitsubishi Date Collected: 2/5/2007 17:06
Lab Sample ID: G122-2909-5E Date Received: 2/7/2007
Lab Project ID: G122-2909 Matrix: Soil
Report Basis: Dry Weight %Solids: 78.9
Result Quantitation MDL Dilution Date
Compound UG/KG Limit UG/KG UG/KG Factor Analyzed Flag
Acetone BQL 21100 2850 800 2/10/2007
Benzene BQL 845 137 800 2/10/2007
Bromobenzene BQL 845 189 800 2/10/2007
Bromochloromethane BQL 845 264 800 2/10/2007
Bromodichloromethane BQL 845 156 800 2/10/2007
Bromoform BQL 845 81.2 800 2/10/2007
Bromomethane BQL 845 87.9 800 2/10/2007
2-Butanone BQL 21100 922 800 2/10/2007
n-Butylbenzene BQL 845 230 800 2/10/2007
sec-Butyl benzene 524 845 199 ·800 2/10/2007 J
tert-Butylbenzene BQL 845 154 800 2/10/2007
Carbon disulfide BQL 845 174 800 2/10/2007
Carbon tetrachloride BQL 845 153 800 2/10/2007
Chlorobenzene BQL 845 150 800 2/10/2007
Chloroethane BQL 845 352 800 2/10/2007
Chloroform BQL 845 186 800 2/10/2007
Chloromethane BQL 845 238 800 2/10/2007
2-Chlorotoluene BQL 845 173 800 2/10/2007
4-Chlorotoluene BQL 845 174 800 2/10/2007
Dibromochloromethane BQL 845 176 800 2/10/2007
1,2-Dibromo-3-chloropropane BQL 4230 1650 800 2/10/2007
Dibromomethane BQL 845 233 800 2/10/2007
1,2-Dibromoethane (EDB) BQL 845 223 800 2/10/2007
1,2-Dichlorobenzene BQL 845 161 800 2/10/2007
1,3-Dichlorobenzene BQL 845 198 800 2/10/2007
1,4-Dichlorobenzene BQL 845 154 800 2/10/2007
trans-1,4-Dichloro-2-butene BQL 4230 1200 800 2/10/2007
1, 1-Dichloroethane BQL 845 182 800 2/10/2007
1, 1-Dichloroethene BQL 845 139 800 2/10/2007
1,2-Dichloroethane BQL 845 206 800 2/10/2007
cis-1,2-Dichloroethene BQL 845 149 800 2/10/2007
trans-1,2-dichloroethene BQL 845 194 800 2/10/2007
1,2-Dichloropropane BQL 845 140 800 2/10/2007
1,3-Dichloropropane BQL 845 143 800 2/10/2007
2,2-Dichloropropane BQL 845 202 800 2/10/2007
1, 1-Dichloropropene BQL 845 149 800 2/10/2007
cis-1,3-Dichloropropene BQL 845 171 800 2/10/2007
trans-1,3-Dichloropropene BQL 845 101 800 2/10/2007
Dichlorodifluoromethane BQL 4230 326 800 2/10/2007
Diisopropyl ether (DIPE) BQL 845 199 800 2/10/2007
Ethyl benzene 2940 845 174 800 2/10/2007
Hexachlorobutadiene BQL 845 346 800 2/10/2007
Pa..pe 1 of 2 OGCMS_LIMS v2.70
N.C. CER IFICATION #481 - 4 of 35
Client Sample ID: SB-5 @ 8 to 9 BLS
SGS ENVIRONMENTAL SERVICES, INC.
Results for Volatiles
by GCMS 82608/5035
Analyzed By: MJC
Client Project ID: Elkins Chrysler Mitsubishi Date Collected: 2/5/2007 17:06
Lab Sample ID: G122-2909-5E Date Received: 2/7/2007
Lab Project ID: G122-2909 Matrix: Soil
Report Basis: Dry Weight %Solids: 78.9
Result Quantitation MDL Dilution Date
Compound UG/KG Limit UG/KG UG/KG Factor Analyzed Flag
2-Hexanone BQL 4230 739 800 2/10/2007
lodomethane BQL 845 109 800 2/10/2007
lsopropylbenzene 913 845 146 800 2/10/2007
4-lsopropyltoluene 330 845 169 800 2/10/2007 J
Methylene chloride BQL 4230 159 800 2/10/2007
4-Methyl-2-pentanone BQL 4230 419 800 2/10/2007
Methyl-tert-butyl ether (MTBE) BQL 845 181 800 2/10/2007
Naphthalene 4610 845 237 800 2/10/2007
n-Propyl benzene 3900 845 178 800 2/10/2007
Styrene BQL 845 202 800 2/10/2007
1, 1, 1,2-Tetrachloroethane BQL 845 244 800 2/10/2007
1, 1,2,2-Tetrachloroethane BQL 845 216 800 2/10/2007
Tetrachloroethene BQL 845 257 800 2/10/2007
Toluene 271 845 148 800 2/10/2007 J
1,2,3-Trichlorobenzene BQL 845 168 800 2/10/2007
1,2,4-Trichlorobenzene BQL 845 206 800 2/10/2007
Trichloroethane BQL 845 177 800 2/10/2007
1, 1, 1-Trichloroethane BQL 845 167 800 2/10/2007
1, 1,2-Trichloroethane BQL 845 226 800 2/10/2007
Trichlorofluoromethane BQL 845 362 800 2/10/2007
1,2,3-Trichloropropane BQL 845 198 800 2/10/2007
1,2,4-Trimethylbenzene 23400 845 169 800 2/10/2007
1,3,5-Trimethylbenzene 6700 845 158 800 2/10/2007
Vinyl chloride BQL 845 338 800 2/10/2007
m-,p-Xylene 11900 1690 326 800 2/10/2007
o-Xylene 4720 845 141 800 2/10/2007
Spike Spike Percent
Added Result Recovered
4-Bromofluorobenzene 10 9.37 94
1,2-Dichloroethane-d4 10 9.83 98
Toluene-dB 10 9.9 99
Comments:
Flags:
BQL = Below Quantitation Limits.
Reviewed By: w
Page 2 of 2
N.C. CERTIFICATION #481
OGCMS LIMS v2.70 - - 5 of 35
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: SB-6@ 8.5 to 9.5 BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID G122-2909-6B
Lab Project ID: 8122-2909
Report Basis: Dry Weight
Report Name Result
Compound UG/KG
Results for Volatiles
by GCMS 8260-5030
Quantitation MDL
Limit UG/KG UG/KG
Acetone 7.58 56.2 3.13
Benzene BQL 5.62 3.39
Bromobenzene BQL 5.62 3.64
Bromochloromethane BQL 5.62 2.48
Bromodichloromethane BQL 5.62 2.97
Bromoform BQL 5.62 2.54
Bromomethane BQL 5.62 5.40
2-Butanone BQL 28.1 3.61
n-Butylbenzene BQL 5.62 3.08
sec-Butyl benzene BQL 5.62 4.35
tert-Butylbenzene BQL 5.62 4.14
Carbon disulfide BQL 5.62 2.93
Carbon tetrachloride BQL 5.62 3.95
Chlorobenzene BQL 5.62 3.95
Chloroethane BQL 5.62 4.98
Chloroform BQL 5.62 3.27
Chloromethane BQL 5.62 3.50
2-Chlorotoluene BQL 5.62 3.89
4-Chlorotoluene BQL 5.62 4.07
Dibromochloromethane BQL 5.62 2.83
1,2-Dibromo-3-chloropropane BQL 5.62 8.15
Dibromomethane BQL 5.62 2.00
1,2-Dibromoethane (EDB) BQL 5.62 2.09
1,2-Dichlorobenzene BQL 5.62 3.39
1,3-Dichlorobenzene BQL 5.62 3.69
1,4-Dichlorobenzene BQL 5.62 3.59
trans-1,4-Dichloro-2-butene BQL 5.62 7.41
1, 1-Dichloroethane BQL 5.62 3.90
1, 1-Dichloroethene BQL 5.62 4.01
1,2-Dichloroethane BQL 5.62 2.69
cis-1,2-Dichloroethene BQL 5.62 3.56
trans-1,2-dichloroethene BQL 5.62 4.01
1,2-Dichloropropane BQL 5.62 3.11
1,3-Dichloropropane BQL 5.62 2.30
2,2-Dichloropropane BQL 5.62 3.25
1, 1-Dichloropropene BQL 5.62 3.93
cis-1,3-Dichloropropene BQL 5.62 2.63
trans-1,3-Dichloropropene BQL 5.62 2.23
Dichlorodifluoromethane BQL 5.62 4.05
Diisopropyl ether (DIPE) BQL 5.62 3.29
Ethyl benzene BQL 5.62 4.00
Hexachlorobutadiene BQL 5.62 4.02
Page 1 of 2
N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected: 02-05-2007 17:11
Date Received: 21712007
Matrix: Soil
%Solids: 76.8
Dilution Date
Factor Analyzed Flag
1 21912007 J
1 21912007
1 21912007
2/9/2007
21912007
21912007
21912007
21912007
21912007
2/9/2007
2/9/2007
21912007
21912007
2/9/2007
21912007
21912007
2/9/2007
21912007
21912007
2/9/2007
21912007
21912007
21912007
21912007
2/9/2007
21912007
2/9/2007
21912007
2/9/2007
21912007
21912007
2/9/2007
21912007
21912007
2/9/2007
2/9/2007
21912007
21912007
21912007
2/9/2007
21912007
21912007
GCMS_LIMS_SOLO_V1 .74
6of35
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: VBLK4021007B
Lab Project ID:
Compound
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
n-Butyl benzene
sec-Butyl benzene
tert-Butyl benzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromo-3-chloropropane
Dibromomethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1, 1-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloroethane
cis-1,2-Dichloroethene
trans-1,2-dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Dichlorodifluoromethane
Diisopropyl ether (DIPE)
Ethyl benzene
Hexachlorobutadiene
SGS ENVIRONMENTAL SERVICES, INC.
Result
UG/L
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 82608
Quantitation MDL
Limit UG/L UG/L
25.0 3.37
1.00 0.162
1.00 0.224
1.00 0.312
1.00 0.185
1.00 0.0960
1.00 0.104
25.0 1.09
1.00 0.272
1.00 0.235
1.00 0.182
1.00 0.206
1.00 0.181
1.00 0.177
1.00 0.416
1.00 0.220
1.00 0.282
1.00 0.205
1.00 0.206
1.00 0.208
5.00 1.95
1.00 0.275
1.00 0.264
1.00 0.190
1.00 0.234
1.00 0.182
5.00 1.42
1.00 0.215
1.00 0.164
1.00 0.244
1.00 0.176
1.00 0.230
1.00 0.166
1.00 0.169
1.00 0.239
1.00 0.176
1.00 0.202
1.00 0.119
5.00 0.385
1.00 0.235
1.00 0.206
1.00 0.409
Page 1 of 2
N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected:
Date Received:
Matrix: Water
Dilution Date
Factor Analyzed
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
1 2/10/2007
1 2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
Flag
OGCMS LIMS v2.70 -- 8 of 35
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: VBLK4021007B
Lab Project ID:
Compound
2-Hexanone
lodomethane
lsopropylbenzene
4-lsopropyltoluene
Methylene chloride
4-Methyl-2-pentanone
Methyl-tert-butyl ether (MTBE)
Naphthalene
n-Propyl benzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Trichloroethene
1, 1, 1-Trichloroethane
1 , 1,2-Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-,p-Xylene
a-Xylene
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
Comments:
Flags:
BQL = Below Quantitation Limits.
SGS ENVIRONMENTAL SERVICES, INC.
Result
UG/L
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.550
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 82608
Quantitation MDL
Limit UG/L UG/L
5.00 0.874
1.00 0.129
1.00 0.173
1.00 0.200
5.00 0.188
5.00 0.495
1.00 0.214
1.00 0.280
1.00 0.211
1.00 0.239
1.00 0.288
1.00 0.256
1.00 0.304
1.00 0.175
1.00 0.199
1.00 0.244
1.00 0.209
1.00 0.197
1.00 0.267
1.00 0.428
1.00 0.234
1.00 0.200
1.00 0.187
1.00 0.400
2.00 0.386
1.00 0.167
Spike Spike
Added Result
10 9.92
10 9.77
10 10
PaJJe 2 of 2 N.C. CER 1 IFICATION #481
Analyzed By: MJC
Date Collected:
Date Received:
Matrix: Water
Dilution Date
Factor Analyzed
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
1 2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
2/10/2007
Percent
Recovered
99
98
100
Reviewed By: <!c.i1
Flag
j
DGCMS_LIMS_v290 Qf 35
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID VBLK9020907B
Lab Project ID:
Report Basis: Dry Weight
Report Name
Compound
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
n-Butylbenzene
sec-Butyl benzene
tert-Butylbenzene
Carbon di~ulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromo-3-chloropropane
Dibromomethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1, 1-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloroethane
cis-1,2-Dichloroethene
trans-1,2-dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Dichlorodifluoromethane
Diisopropyl ether (DIPE)
Ethyl benzene
Hexachlorobutadiene
SGS ENVIRONMENTAL SERVICES, INC.
Result
UG/KG
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 8260-5030
Quantitation MDL
Limit UG/KG UG/KG
50.0 2.78
5.00 3.02
5.00 3.24
5.00 2.21
5.00 2.64
5.00 2.26
5.00 4.80
25.0 3.21
5.00 2.74
5.00 3.87
5.00 3.68
5.00 2.61
5.00 3.51
5.00 3.51
5.00 4.43
5.00 2.91
5.00 3.11
5.00 3.46
5.00 3.62
5.00 2.52
5.00 7.25
5.00 1.78
5.00 1.86
5.00 3.02
5.00 3.28
5.00 3.19
5.00 6.59
5.00 3.47
5.00 3.57
5.00 2.39
5.00 3.17
5.00 3.57
5.00 2.77
5.00 2.05
5.00 2.89
5.00 3.50
5.00 2.34
5.00 1.98
5.00 3.60
5.00 2.93
5.00 3.56
5.00 3.58
Page 1 of 2
N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected:
Date Received:
Matrix: Soil
%Solids: 100.0
Dilution Date
Factor Analyzed Flag
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
GCMS_LIMS_SOLO_V1 .74
13 of 35
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID VBLK9020907B
Lab Project ID:
Report Basis: Dry Weight
Report Name
Compound
2-Hexanone
lodomethane
lsopropylbenzene
4-lsopropyltoluene
Methylene chloride
4-Methyl-2-pentanone
Methyl-tert-butyl ether (MTBE)
Naphthalene
n-Propyl benzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Trichloroethene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-,p-Xylene
a-Xylene
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
SGS ENVIRONMENTAL SERVICES, INC.
Result
UG/KG
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 8260-5030
Quantitation MDL
Limit UG/KG UG/KG
5.00 1.78
5.00 3.60
5.00 3.79
5.00 3.68
20.0 3.08
5.00 1.19
5.00 2.27
5.00 2.38
5.00 3.72
5.00 4.72
5.00 2.91
5.00 1.81
5.00 3.82
5.00 3.23
5.00 2.63
5.00 2.33
5.00 3.48
5.00 3.50
5.00 2.01
5.00 3.93
5.00 1.86
5.00 3.62
5.00 3.70
5.00 3.44
10.0 7.35
5.00 3.55
Spike Spike
Added Result
50 48.8
50 43.9
50 42.9
Page 2 of 2
N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected:
Date Received:
Matrix: Soil
%Solids: 100.0
Dilution Date
Factor Analyzed Flag
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Percent
Recovered
98
88
86
Reviewed By: w
GCMS LIMS SOLO V1.74 - - -14 of 35
SGS ENVIRONMENTAL SERVICES, INC.
Results for Semivolatiles
by GCMS 8270
Client Sample ID: SB-5 @ 8 to 9 BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2909-5G
Lab Project ID: G122-2909
Report Basis: Dry weight
Result RL MDL
Compound ug/Kg ug/Kg ug/Kg
Acenaphthene BQL 388 55.5
Acenaphthylene BQL 388 51.7
Anthracene BQL 388 56.3
Benzo[a]anthracene 105 388 67.2
Benzo[a]pyrene 93.2 388 59.4
Benzo[b ]fluoranthene 109 388 68.0
Benzo[g,h,i]perylene BQL 388 106
Benzo[k]fluoranthene BQL 388 75.0
Benzoic Acid BQL 777 777
Bis(2-chloroethoxy)methane BQL 388 57.9
Bis(2-chloroethyl)ether BQL 388 47.0
Bis(2-chloroisopropyl )ether BQL 388 48.6
Bis(2-ethylhexyl)phthalate 221 388 52.0
4-bromophenyl phenyl ether BQL 388 65.6
Butylbenzylphthalate BQL 388 59.8
2-Chloronaphthalene BQL 388 61.0
2-Chlorophenol BQL 388 122
4-Chloro-3-methylphenol BQL 388 121
4-Chloroaniline BQL 1940 296
4-Chlorophenyl phenyl ether BQL 388 57.1
Chrysene 109 388 42.0
Dibenzo[a,h]anthracene BQL 388 109
Dibenzofuran BQL 388 70.7
Di-n-Butylphthalate BQL 388 46.2
1,2-Dichlorobenzene BQL 388 43.1
1,3-Dichlorobenzene BQL 388 42.3
1,4-Dichlorobenzene BQL 388 43.9
3,3'-Dichlorobenzidine BQL 777 97.9
2,4-Dichlorophenol BQL 388 140
Diethylphthalate BQL 388 50.1
Dimethylphthalate BQL 388 47.0
2 ,4-Dimethylphenol BQL 388 278
Di-n-octylphthalate BQL 388 64.1
4,6-Dinitro-2-methylphenol BQL 1940 229
2 ,4-Dinitrophenol BQL 1940 855
2,4-Dinitrotoluene BQL 388 50.5
2,6-Dinitrotoluene BQL 388 70.7
Diphenylamine * BQL 388 38.1
Fluoranthene 237 388 54.4
Fluorene BQL 388 48.2
Hexachlorobenzene BQL 388 59.8
Hexachlorobutadiene BQL 388 62.1
Hexachlorocyclopentadiene BQL 777 40.0
Hexachloroethane BQL 388 35.0
lndeno(1,2,3-c,d)pyrene BQL 388 99.4
lsophorone BQL 388 57.1
Page 1 of 2
N.C. CERTIFICATION #481
Analyzed By: EAW
Date Collected: 2/5/2007 17:06
Date Received: 2/7/2007
Date Extracted: 2/9/2007
Matrix: Soil
% Solids: 78.85
Dilution Date
Factor Analyzed
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
Flag
J
J
J
J
J
J
8270.xls
18 of 35
SGS ENVIRONMENTAL SERVICES, INC.
Results for Semivolatiles
by GCMS 8270
Client Sample ID: SB-5 @ 8 to 9 BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2909-5G
Lab Project ID: G122-2909
Report Basis: Dry weight
Result RL MDL
Compound ug/Kg ug/Kg ug/Kg
2-Methylnaphthalene BQL 388 113
2-Methylphenol BQL 388 137
3-& 4-Methylphenol BQL 388 132
Naphthalene 171 388 31.5
2-Nitroaniline BQL 388 61.0
3-Nitroaniline BQL 1940 400
4-Nitroaniline BQL 1940 120
Nitrobenzene BQL 388 52.4
2-Nitrophenol BQL 388 120
4-Nitrophenol BQL 1940 108
N-Nitrosodi-n-propylamine BQL 388 49.3
Pentachlorophenol BQL 1940 101
Phenanthrene 206 388 44.3
Phenol BQL 388 106
Pyrene 148 388 74.6
1,2,4-Trichlorobenzene BQL 388 48.6
2 ,4,5-Trichlorophenol BQL 388 150
2,4,6-Trichlorophenol BQL 388 138
Spike Spike
Added Result
2-Fluorobiphenyl 10 9.2
2-Fluorophenol 10 9.8
Nitrobenzene-d5 10 10.2
Phenol-d6 10 9.5
2,4,6-Tribromophenol 10 10.2
4-Terphenyl-d 14 10 8.5
Comments:
Analyzed By: EAW
Date Collected: 2/5/2007 17:06
Date Received: 2/7/2007
Date Extracted: 2/9/2007
Matrix: Soil
% Solids: 78.85
Dilution Date
Factor Analyzed
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
Percent
Recovered
92
98
102
95
102
85
* N-Nitrosodiphenylamine is reported as the breakdown product Diphenylamine.
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Reviewed By: (I....>/
Page 2 of 2
N.C. CERTIFICATION #481
Flag
J
J
J
8270.xls
19 of 35
SGS ENVIRONMENTAL SERVICES, INC.
Results for Semivolatiles
by GCMS 8270
Client Sample ID: SB-6 @ 8.5 to 9.5 BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2909-6G
Lab Project ID: G122-2909
Report Basis: Dry weight
Result RL MDL
Compound ug/Kg ug/Kg ug/Kg
Acenaphthene BQL 401 57.3
Acenaphthylene BQL 401 53.3
Anthracene BQL 401 58.1
Benzo[a]anthracene 144 401 69.3
Benzo[a]pyrene 164 401 61.3
Benzo[b]fluoranthene 160 401 70.1
Benzo[g,h,i]perylene BQL 401 109
Benzo[k]fluoranthene 92.1 401 77.3
Benzoic Acid BQL 801 801
Bis(2-chloroethoxy)methane BQL 401 59.7
Bis(2-chloroethyl)ether BQL 401 48.5
Bis(2-chloroisopropyl )ether BQL 401 50.1
Bis(2-ethylhexyl}phthalate BQL 401 53.7
4-bromophenyl phenyl ether BQL 401 67.7
Butylbenzylphthalate BQL 401 61.7
2-Chloronaphthalene BQL 401 62.9
2-Chlorophenol BQL 401 125
4-Chloro-3-methylphenol BQL 401 125
4-Chloroaniline BQL 2000 305
4-Chlorophenyl phenyl ether BQL 401 58.9
Chrysene 156 401 43.3
Dibenzo[a,h]anthracene BQL 401 112
Dibenzofuran BQL 401 72.9
Di-n-Butylphthalate BQL 401 47.7
1,2-Dichlorobenzene BQL 401 44.5
1,3-Dichlorobenzene BQL 401 43.7
1,4-Dichlorobenzene BQL 401 45.3
3,3'-Dichlorobenzidine BQL 801 101
2 ,4-Dichlorophenol BQL 401 144
Diethylphthalate BQL 401 51.7
Dimethylphthalate BQL 401 48.5
2,4-Dimethylphenol BQL 401 286
Di-n-octylphthalate BQL 401 66.1
4,6-Dinitro-2-methylphenol BQL 2000 236
2,4-Dinitrophenol BQL 2000 882
2,4-Dinitrotoluene BQL 401 52.1
2,6-Dinitrotoluene BQL 401 72.9
Diphenylamine * BQL 401 39.3
Fluoranthene 328 401 56.1
Fluorene BQL 401 49.7
Hexachlorobenzene BQL 401 61.7
Hexachlorobutadiene BQL 401 64.1
Hexachlorocyclopentadiene BQL 801 41.3
Hexachloroethane BQL 401 36.0
lndeno(1,2,3-c,d)pyrene BQL 401 103
lsophorone BQL 401 58.9
Page 1of2
N.C. CERTIFICATION #481
Analyzed By: EAW
Date Collected: 2/5/2007 17: 11
Date Received: 2/7/2007
Date Extracted: 2/9/2007
Matrix: Soil
% Solids: 76.82
Dilution Date
Factor Analyzed
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
Flag
J
J
J
J
J
J
8270.xls
20 of 35
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: PB7297
Lab Project ID:
Report Basis: Dry Weight
Compound
Acenaphthene
Acenaphthylene
Anthracene
Benzo[a]anthracene
Benzo[a]pyrene
Benzo[b ]fluoranthene
Benzo[g,h,i]perylene
Benzo[k]fluoranthene
Benzoic Acid
Bis(2-chloroethoxy )methane
Bis(2-chloroethyl}ether
Bis(2-chloroisopropyl )ether
Bis(2-ethylhexyl)phthalate
4-bromophenyl phenyl ether
Butylbenzylphthalate
2-Chloronaphthalene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo[a,h]anthracene
Dibenzofuran
Di-n-Butylphthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethylphthalate
2,4-Dimethylphenol
Di-n-octylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diphenylamine *
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
SGS ENVIRONMENTAL SERVICES, INC.
Results for Semivolatiles
by GCMS 8270
Result RL MDL
ug/Kg ug/Kg ug/Kg
BQL 313 44.7
BQL 313 41.6
BQL 313 45.3
BQL 313 54.1
BQL 313 47.8
BQL 313 54.7
BQL 313 85.0
BQL 313 60.3
BQL 625 625
BQL 313 46.6
BQL 313 37.8
BQL 313 39.1
BQL 313 41.9
BQL 313 52.8
BQL 313 48.1
BQL 313 49.1
BQL 313 97.8
BQL 313 97.5
BQL 1560 238
BQL 313 45.9
BQL 313 33.8
BQL 313 87.5
BQL 313 56.9
BQL 313 37.2
BQL 313 34.7
BQL 313 34.1
BQL 313 35.3
BQL 625 78.8
BQL 313 113
BQL 313 40.3
BQL 313 37.8
BQL 313 223
BQL 313 51.6
BQL 1560 184
BQL 1560 688
BQL 313 40.6
BQL 313 56.9
BQL 313 30.6
BQL 313 43.7
BQL 313 38.8
BQL 313 48.1
BQL 313 50.0
BQL 625 32.2
BQL 313 28.1
BQL 313 80.0
BQL 313 45.9
Page 1 of 2
N.C. CERTIFICATION #481
Analyzed By: EAW
Date Collected:
Date Received:
Date Extracted: 2/9/2007
Matrix: SOIL
% Solids: 100
Dilution Date
Factor Analyzed
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
1 2/11/2007
Flag
8270.xls
22 of 35
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-1 @2 BLS Date Analyzed:
Client Project ID: Elkins Chrysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2909-1B Date Collected:
Lab Project ID: G122-2909 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 34.8
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
2/5/2007 15: 17
21712007
86.33
Result
MG/KG
157
Reviewed By: 'bf
9071 LIMS v1 .35 - -27 of 35
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-2@ 10 BLS Date Analyzed:
Client Project ID: Elkins Chrysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2909-2B Date Collected:
Lab Project ID: G122-2909 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 34.4
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
21512007 15:20
21712007
86.27
Result
MG/KG
216
Reviewed By: "41
9071_LIMS_v1 .35
28 Of 35
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-4@ 13 BLS Date Analyzed:
Client Project ID: Elkins Chrysler Mitsubishi Analyzed By:
Lab Sample ID: G122-2909-4B Date Collected:
Lab Project ID: G122-2909 Date Received:
Matrix: Soil Solids:
Parameter Method RL
MG/KG
Oil & Grease 9071 33
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
2/13/2007
alt
2/5/2007 16:05
21712007
90.32
Result
MG/KG
244
Reviewed By: <:pf!
9071 LIMS v1 .35 - -29 of 35
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-7@ 8 BLS Date Analyzed: 2/13/2007
Client Project ID: Elkins Chrysler Mitsubishi Analyzed By: alt
Lab Sample ID: G122-2909-7B Date Collected: 2/5/2007 17:37
Lab Project ID: G122-2909 Date Received: 21712007
Matrix: Soil Solids: 86.90
Parameter Method RL Result
MG/KG MG/KG
Oil & Grease 9071 35.6 203
Comments:
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
Reviewed By: (2.......___;/
9071 LIMS v1 .35
N.C. CERTIFICATION #481 - -30 of 35
SGS ENVIRONMENTAL SERVICES, INC.
Results for Oil and Grease
Client Sample ID: SB-4@ 13 BLS
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: g122-2909-4F
Lab Project ID: G122-2909
Matrix: Soil
Parameter Method RL
MG/KG
Oil & Grease 9071 33.8
Comments:
Silica Gel Clean-up performed.
BQL = Below Quantitation Limit
All soils are corrected for percent solids.
N.C. CERTIFICATION #481
Date Analyzed:
Analyzed By:
Date Collected:
Date Received:
Solids:
2/19/2007
alt
2/5/2007 16:05
21712007
90.32
Result
MG/KG
37.2
Reviewed By: __ _
9071 LIMS v1 .35 - -32 of 35
SGS ENVIRONMENTAL SERVICES, INC.
List of Reporting Abbreviations
and Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantitation Limit (RL or MDL}
OF = Dilution Factor
Dup = Duplicate
D =Detected, but RPO is> 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D} =Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) =Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL = Reporting Limit
RPO = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
N.C. CERTIFICATION #481
Ml34.030606.3
34 of 35
Mr. Darin McClure
Mid-Atlantic Associates
409 Rogersview Ct.
Raleigh NC 27610
Report Number: G 122-2912
SGS ENVIRONMENTAL SERVICES, INC.
Client Project: Elkins Chyrsler Mitsubishi
Dear Mr. McClure:
Enclosed are the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call SGS/Paradigm at [phone]. We will be happy to answer any questions
or concerns which you may have.
Thank you for using SGS/Paradigm Analytical Labs for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Analytical Laboratories, Inc.
o atory Dired6r--
trick Weaver
N.C. CERTIFICATION #481 1 of 11
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: TMW-1
Results for Organics
by EPA 8315
Client Project ID: Elkins Chyrsler Mitusbishi
Lab Sample ID: G122-2912-1B
Lab Project ID: G122-2912
Compound
Formaldehyde
Result
mg/L
0.130
Quantitation
Limit mg/L
0.250
Analyzed By: CLP
Date Collected: 2/7/2007 8:13
Date Received: 2/9/2007
Matrix: Water
MDL
mg/L
0.0212
Dilution
Factor
1
Date
Analyzed Flag
2/12/2007 J
Reviewed By: \L-.;;
8315.XLS
N.C. CERTIFICATION #481 2of11
Client Sample ID: TMW-1
SGS ENVIRONMENTAL SERVICES, INC.
Results for Semivolatiles
by GCMS 625
Analyzed By: EAW
Client Project ID: Elkins Chyrsler Mitsubishi Date Collected: 2/7/2007 8:13
Lab Sample ID: G122-2912-1C Date Received: 2/9/2007
Lab Project ID: G122-2912 Date Extracted: 2/13/2007
Matrix: Water
Result RL MDL Dilution Date
Compound ug/L ug/L ug/L Factor Analyzed
Acenaphthene BQL 10.0 1.22 1 2/15/2007
Acenaphthylene BQL 10.0 1.12 1 2/15/2007
Anthracene BQL 10.0 1.75 1 2/15/2007
Benzo[a]anthracene BQL 10.0 1.36 1 2115/2007
Benzo[a]pyrene BQL 10.0 1.27 1 2/15/2007
Benzo[b ]fluoranthene BQL 10.0 1.43 1 2/15/2007
Benzo[g, h, i]perylene BQL 10.0 4.57 1 2/15/2007
Benzo[k]fluoranthene BQL 10.0 1.09 1 2/15/2007
Bis(2-chloroethoxy)methane BQL 10.0 1.11 1 2/15/2007
Bis(2-chloroethyl)ether BQL 10.0 1.09 1 2/15/2007
Bis(2-chloroisopropyl)ether BQL 10.0 1.57 1 2/15/2007
Bis(2-ethylhexyl)phthalate 107 10.0 1.33 1 2/15/2007
4-bromophenyl phenyl ether BQL 10.0 1.99 1 2/15/2007
Butylbenzylphthalate BQL 10.0 1.53 1 2/15/2007
2-Chloronaphthalene BQL 10.0 1.25 1 2/15/2007
2-Chlorophenol BQL 10.0 4.22 1 2/15/2007
4-Chloro-3-methylphenol BQL 10.0 3.26 1 2/15/2007
4-Chlorophenyl phenyl ether BQL 10.0 1.42 1 2/15/2007
Chrysene BQL 10.0 1.11 1 2/15/2007
Dibenzo[ a, h]anth racene BQL 10.0 4.87 1 2/15/2007
Di-n-Butylphthalate BQL 10.0 1.65 1 2/15/2007
1,2-Dichlorobenzene BQL 10.0 1.25 1 2/15/2007
1,3-Dichlorobenzene BQL 10.0 1.24 1 2/15/2007
1,4-Dichlorobenzene BQL 10.0 1.20 1 2/15/2007
3,3'-Dichlorobenzidine BQL 20.0 4.10 1 2/15/2007
2,4-Dichlorophenol BQL 10.0 3.75 1 2/15/2007
Diethylphthalate 1.60 10.0 1.48 1 2/15/2007
Dimethylphthalate BQL 10.0 1.04 1 2/15/2007
2,4-Dimethylphenol BQL 10.0 9.25 1 2/15/2007
Di-n-octylphthalate BQL 10.0 1.16 1 2/15/2007
4,6-Dinitro-2-methylphenol BQL 50.0 3.71 1 2/15/2007
2,4-Dinitrophenol BQL 50.0 4.20 1 2/15/2007
2,4-Dinitrotoluene BQL 10.0 1.52 1 2/15/2007
2,6-Dinitrotoluene BQL 10.0 1.41 1 2/15/2007
Diphenylamine * BQL 10.0 1.53 1 2/15/2007
Fluoranthene BQL 10.0 1.41 1 2/15/2007
Fluorene BQL 10.0 1.22 1 2/15/2007
Hexachlorobenzene BQL 10.0 1.22 1 2/15/2007
Hexachlorobutadiene BQL 10.0 1.58 1 2/15/2007
Hexachlorocyclopentadiene BQL 20.0 20.0 1 2/15/2007
Hexachloroethane BQL 10.0 1.58 1 2/15/2007
lndeno(1,2,3-c,d)pyrene BQL 10.0 4.57 1 2/15/2007
lsophorone BQL 10.0 1.27 1 2/15/2007
Naphthalene BQL 10.0 1.08 1 2/15/2007
Nitrobenzene BQL 10.0 1.32 1 2/15/2007
2-Nitrophenol BQL 10.0 3.52 1 2/15/2007
4-Nitrophenol BQL 50.0 3.17 1 2/15/2007
Page 1of2
N.C. CERTIFICATION #481
Flag
J
8270.xls
4of11
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: TMW-1
Results for Semivolatiles
by GCMS 625
Client Project ID: Elkins Chyrsler Mitsubishi
Lab Sample ID: G122-2912-1C
Lab Project ID: G122-2912
Compound
N-Nitrosodi-n-propylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d6
2,4,6-Tribromophenol
4-Terphenyl-d 14
Comments:
Result
ug/L
BQL
BQL
BQL
BQL
BQL
BQL
BQL
RL
ug/L
10.0
50.0
10.0
10.0
10.0
10.0
10.0
Spike
Added
10
10
10
10
10
10
MDL
ug/L
1.87
2.83
1.38
3.38
2.08
1.33
2.92
Spike
Result
8.4
8.4
8.9
9
10.9
10.7
Analyzed By: EAW
Date Collected: 2/7/2007 8:13
Date Received: 2/9/2007
Date Extracted: 2/13/2007
Matrix: Water
Dilution
Factor
1
1
1
1
1
1
1
Percent
Recovered
84
84
89
90
109
107
Date
Analyzed
2/15/2007
2/15/2007
2/15/2007
2/15/2007
2/15/2007
2/15/2007
2/15/2007
* N-Nitrosodiphenylamine is reported as the breakdown product Diphenylamine.
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Reviewed By: f-.,_ir?
Flag
Page 2 of 2 8270.xls
N.C. CERTIFICATION #481 5 of 11
Client Sample ID: TMW-2
SGS ENVIRONMENTAL SERVICES, INC.
Results for Semivolatiles
by GCMS 625
Analyzed By: EAW
Client Project ID: Elkins Chyrsler Mitsubishi Date Collected: 2/6/2007 0:00
Lab Sample ID: G122-2912-2C Date Received: 2/9/2007
Lab Project ID: G122-2912 Date Extracted: 2/13/2007
Matrix: Water
Result RL MDL Dilution Date
Compound ug/L ug/L ug/L Factor Analyzed
Acenaphthene BQL 10.0 1.22 1 2/15/2007
Acenaphthylene BQL 10.0 1.12 1 2/15/2007
Anthracene BQL 10.0 1.75 1 2/15/2007
Benzo[a]anthracene BQL 10.0 1.36 1 2/15/2007
Benzo[a]pyrene BQL 10.0 1.27 1 2/15/2007
Benzo[b]fluoranthene BQL 10.0 1.43 1 2/15/2007
Benzo[g,h,i]perylene BQL 10.0 4.57 1 2/15/2007
Benzo[k]fluoranthene BQL 10.0 1.09 1 2/15/2007
Bis(2-chloroethoxy)methane BQL 10.0 1.11 1 2/15/2007
Bis(2-chloroethyl)ether BQL 10.0 1.09 1 2/15/2007
Bis(2-chloroisopropyl)ether BQL 10.0 1.57 1 2/15/2007
Bis(2-ethylhexyl)phthalate 18.3 10.0 1.33 1 2/15/2007
4-bromophenyl phenyl ether BQL 10.0 1.99 1 2/15/2007
Butylbenzylphthalate BQL 10.0 1.53 1 2/15/2007
2-Chloronaphthalene BQL 10.0 1.25 1 2/15/2007
2-Chlorophenol BQL 10.0 4.22 1 2/15/2007
4-Chloro-3-methylphenol BQL 10.0 3.26 1 2/15/2007
4-Chlorophenyl phenyl ether BQL 10.0 1.42 1 2/15/2007
Chrysene BQL 10.0 1.11 1 2/15/2007
Dibenzo[a,h]anthracene BQL 10.0 4.87 1 2/15/2007
Di-n-Butylphthalate BQL 10.0 1.65 1 2/15/2007
1,2-Dichlorobenzene BQL 10.0 1.25 1 2/15/2007
1,3-Dichlorobenzene BQL 10.0 1.24 1 2/15/2007
1,4-Dichlorobenzene BQL 10.0 1.20 1 2/15/2007
3,3'-Dichlorobenzidine BQL 20.0 4.10 1 2/15/2007
2 ,4-Dichlorophenol BQL 10.0 3.75 1 2/15/2007
Diethylphthalate BQL 10.0 1.48 1 2/15/2007
Dimethylphthalate BQL 10.0 1.04 1 2/15/2007
2,4-Dimethylphenol BQL 10.0 9.25 1 2/15/2007
Di-n-octylphthalate BQL 10.0 1.16 1 2/15/2007
4,6-Dinitro-2-methylphenol BQL 50.0 3.71 1 2/15/2007
2,4-Dinitrophenol BQL 50.0 4.20 1 2/15/2007
2,4-Dinitrotoluene BQL 10.0 1.52 1 2/15/2007
2,6-Dinitrotoluene BQL 10.0 1.41 1 2/15/2007
Diphenylamine * BQL 10.0 1.53 1 2/15/2007
Fluoranthene BQL 10.0 1.41 1 2/15/2007
Fluorene BQL 10.0 1.22 1 2/15/2007
Hexachlorobenzene BQL 10.0 1.22 1 2/15/2007
Hexachlorobutadiene BQL 10.0 1.58 1 2/15/2007
Hexachlorocyclopentadiene BQL 20.0 20.0 1 2/15/2007
Hexachloroethane BQL 10.0 1.58 1 2/15/2007
lndeno(1,2,3-c,d)pyrene BQL 10.0 4.57 1 2/15/2007
lsophorone BQL 10.0 1.27 1 2/15/2007
Naphthalene BQL 10.0 1.08 1 2/15/2007
Nitrobenzene BQL 10.0 1.32 1 2/15/2007
2-Nitrophenol BQL 10.0 3.52 1 2/15/2007
4-Nitrophenol BQL 50.0 3.17 1 2/15/2007
Page 1of2
N.C. CERTIFICATION #481
Flag
8270.xls
6of11
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: TMW-2
Results for Semivolatiles
by GCMS 625
Client Project ID: Elkins Chyrsler Mitsubishi
Lab Sample ID: G122-2912-2C
Lab Project ID: G122-2912
Compound
N-Nitrosodi-n-propylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d6
2,4,6-Tribromophenol
4-Terphenyl-d 14
Comments:
Result
ug/L
BQL
BQL
BQL
BQL
BQL
BQL
BQL
RL
ug/L
10.0
50.0
10.0
10.0
10.0
10.0
10.0
Spike
Added
10
10
10
10
10
10
MDL
ug/L
1.87
2.83
1.38
3.38
2.08
1.33
2.92
Spike
Result
9.2
9
9.6
9.7
11
10.1
Analyzed By: EAW
Date Collected: 2/6/2007 0:00
Date Received: 2/9/2007
Date Extracted: 2/13/2007
Matrix: Water
Dilution
Factor
1
1
1
1
1
1
1
Percent
Recovered
92
90
96
97
110
101
Date
Analyzed
2/15/2007
2/15/2007
2/15/2007
2/15/2007
2/15/2007
2/15/2007
2/15/2007
* N-Nitrosodiphenylamine is reported as the breakdown product Diphenylamine.
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Reviewed By: f..=,.-J
Flag
Page 2 of 2 8270.xls
N.C. CERTIFICATION #481 7 of 11
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: PB7323
Lab Project ID:
Compound
Acenaphthene
Acenaphthylene
Anthracene
Benzo[a]anthracene
Benzo[a]pyrene
Benzo[b]fluoranthene
Benzo[g, h, i]perylene
Benzo[k]fluoranthene
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl}ether
Bis(2-ethylhexyl}phthalate
4-bromophenyl phenyl ether
Butylbenzylphthalate
2-Chloronaphthalene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo[a,h]anthracene
Di-n-Butylphthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethylphthalate
2,4-Dimethylphenol
Di-n-octylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diphenylamine *
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
Naphthalene
SGS ENVIRONMENTAL SERVICES, INC.
Results for Semivolatiles
by GCMS 625
Result RL MDL
ug/L ug/L ug/L
BQL 10.0 1.22
BQL 10.0 1.12
BQL 10.0 1.75
BQL 10.0 1.36
BQL 10.0 1.27
BQL 10.0 1.43
BQL 10.0 4.57
BQL 10.0 1.09
BQL 10.0 1.11
BQL 10.0 1.09
BQL 10.0 1.57
BQL 10.0 1.33
BQL 10.0 1.99
BQL 10.0 1.53
BQL 10.0 1.25
BQL 10.0 4.22
BQL 10.0 3.26
BQL 10.0 1.42
BQL 10.0 1 .11
BQL 10.0 4.87
BQL 10.0 1.65
BQL 10.0 1.25
BQL 10.0 1.24
BQL 10.0 1.20
BQL 20.0 4.10
BQL 10.0 3.75
2.60 10.0 1.48
BQL 10.0 1.04
BQL 10.0 9.25
BQL 10.0 1.16
BQL 50.0 3.71
BQL 50.0 4.20
BQL 10.0 1.52
BQL 10.0 1.41
BQL 10.0 1.53
BQL 10.0 1.41
BQL 10.0 1.22
BQL 10.0 1.22
BQL 10.0 1.58
BQL 20.0 20.0
BQL 10.0 1.58
BQL 10.0 4.57
BQL 10.0 1.27
BQL 10.0 1.08
Page 1 of 2
N.C. CERTIFICATION #481
Analyzed By: EAW
Date Collected:
Date Received:
Date Extracted: 2/13/2007
Matrix: WATER
Dilution Date
Factor Analyzed
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
Flag
J
8270.xls
8of11
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: PB7323
Lab Project ID:
Compound
Nitrobenzene
2-Nitrophenol
4-N itrophenol
N-Nitrosodi-n-propylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
2-Fluorobiphenyl
2-Fluorophenol
N itrobenzene-d5
Phenol-d6
2,4,6-Tribromophenol
4-T erphenyl-d 14
Comments:
Results for Semivolatiles
by GCMS 625
Result RL MDL
ug/L ug/L ug/L
BQL 10.0 1.32
BQL 10.0 3.52
BQL 50.0 3.17
BQL 10.0 1.87
BQL 50.0 2.83
BQL 10.0 1.38
BQL 10.0 3.38
BQL 10.0 2.08
BQL 10.0 1.33
BQL 10.0 2.92
Spike Spike
Added Result
10 9.1
10 8.2
10 10.3
10 8.9
10 9.7
10 11.3
Analyzed By: EAW
Date Collected:
Date Received:
Date Extracted: 2/13/2007
Matrix: WATER
Dilution Date
Factor Analyzed
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
1 2/15/2007
Percent
Recovered
91
82
103
89
97
113
* N-Nitrosodiphenylamine is reported as the breakdown product Diphenylamine.
Flags:
BQL =Below Quantitation Limits.
J = Detected below the quantitation limit.
Reviewed By: w
Page 2 of 2
N.C. CERTIFICATION #481
Flag
8270.xls
9of11
Mr. Darin McClure
Mid-Atlantic Associates
409 Rogersview Ct.
Raleigh NC 27610
Report Number: G 122-2906
SGS ENVIRONMENTAL SERVICES, INC.
Client Project: Elkins Chrysler Mitsubishi
Dear Mr. McClure:
Enclosed are the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call SGS/Paradigm at [phone]. We will be happy to answer any questions
or concerns which you may have.
Thank you for using SGS/Paradigm Analytical Labs for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely,
SGS/Paradigm Analytical Laboratories, Inc.
---t°Tl -&L . Laborato Director
J. Patrick Weaver
N.C. CERTIFICATION #481 1 of 15
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: MW-1
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2906-1A
Lab Project ID: 8122-2906
Result
Compound UG/L
Acetone BQL
Benzene BQL
Bromobenzene BQL
Bromochloromethane BQL
Bromodichloromethane BQL
Bromoform BQL
Bromomethane BQL
2-Butanone BQL
n-Butyl benzene BQL
sec-Butyl benzene BQL
tert-B utyl benzene BQL
Carbon disulfide BQL
Carbon tetrachloride BQL
Chlorobenzene BQL
Chloroethane BQL
Chloroform BQL
Chloromethane BQL
2-Chlorotoluene BQL
4-Chlorotoluene BQL
Dibromochloromethane BQL
1,2-Dibromo-3-chloropropane BQL
Dibromomethane BQL
1,2-Dibromoethane (EDB) BQL
1,2-Dichlorobenzene BQL
1,3-Dichlorobenzene BQL
1,4-Dichlorobenzene BQL
trans-1,4-Dichloro-2-butene BQL
Results for Volatiles
by GCMS 82608
Quantitation MDL
Limit UG/L UG/L
25.0 3.37
1.00 0.162
1.00 0.224
1.00 0.312
1.00 0.185
1.00 0.0960
1.00 0.104
25.0 1.09
1.00 0.272
1.00 0.235
1.00 0.182
1.00 0.206
1.00 0.181
1.00 0.177
1.00 0.416
1.00 0.220
1.00 0.282
1.00 0.205
1.00 0.206
1.00 0.208
5.00 1.95
1.00 0.275
1.00 0.264
1.00 0.190
1.00 0.234
1.00 0.182
5.00 1.42
1, 1-Dichloroethane 1.16 1.00 0.215
1, 1-Dichloroethene BQL 1.00 0.164
1,2-Dichloroethane BQL 1.00 0.244
cis-1,2-Dichloroethene BQL 1.00 0.176
trans-1,2-dichloroethene BQL 1.00 0.230
1,2-Dichloropropane BQL 1.00 0.166
1,3-Dichloropropane BQL 1.00 0.169
2,2-Dichloropropane BQL 1.00 0.239
1, 1-Dichloropropene BQL 1.00 0.176
cis-1,3-Dichloropropene BQL 1.00 0.202
trans-1,3-Dichloropropene BQL 1.00 0.119
Dichlorodifluoromethane BQL 5.00 0.385
Diisopropyl ether (DIPE) BQL 1.00 0.235
Ethyl benzene BQL 1.00 0.206
Hexachlorobutadiene BQL 1.00 0.409
Pare 1of2 N.C. CER IFICATION #481
Analyzed By: MJC
Date Collected: 2/5/2007 11 :31
Date Received: 2/6/2007
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
21912007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
21912007
1 21912007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
2/9/2007
21912007
2/9/2007
21912007
2/9/2007
1 2/9/2007
1 21912007
1 21912007
1 21912007
1 21912007
1 2/9/2007
1 21912007
1 21912007
1 21912007
1 2/9/2007
1 21912007
1 21912007
1 21912007
1 2/9/2007
1 21912007
1 21912007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 21912007
1 21912007
1 2/9/2007
Flag
OGCMS LIMS v2.70 -- 2 of 15
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: MW-1
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2906-1A
Lab Project ID: G122-2906
Result
Compound UG/L
2-Hexanone BQL
lodomethane BQL
lsopropylbenzene BQL
4-lsopropyltoluene BQL
Methylene chloride BQL
4-Methyl-2-pentanone BQL
Results for Volatiles
by GCMS 82608
Quantitation MDL
Limit UG/L UG/L
5.00 0.874
1.00 0.129
1.00 0.173
1.00 0.200
1.00 0.188
5.00 0.495
Methyl-tert-butyl ether {MTBE) 5.83 1.00 0.214
Naphthalene BQL 1.00 0.280
n-Propyl benzene BQL 1.00 0.211
Styrene BQL 1.00 0.239
1, 1, 1 ,2-Tetrachloroethane BQL 1.00 0.288
1, 1,2,2-Tetrachloroethane BQL 1.00 0.256
Tetrachloroethene BQL 1.00 0.304
Toluene BQL 1.00 0.175
1,2,3-Trichlorobenzene BQL 1.00 0.199
1,2,4-Trichlorobenzene BQL 1.00 0.244
Trichloroethene BQL 1.00 0.209
1, 1, 1-Trichloroethane BQL 1.00 0.197
1, 1,2-Trichloroethane BQL 1.00 0.267
Trichlorofluoromethane BQL 1.00 0.428
1,2,3-Trichloropropane BQL 1.00 0.234
1,2,4-Trimethylbenzene BQL 1.00 0.200
1,3,5-Trimethylbenzene BQL 1.00 0.187
Vinyl chloride BQL 1.00 0.400
m-,p-Xylene BQL 2.00 0.386
a-Xylene BQL 1.00 0.167
Spike Spike
Added Result
4-Bromofluorobenzene 10 9.81
1 ,2-Dichloroethane-d4 10 10.1
Toluene-dB 10 10.1
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
P~2of2 N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected: 2/5/2007 11 :31
Date Received: 2/6/2007
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Percent
Recovered
98
101
101
Reviewed By: N
Flag
OGCMS_LIMS_v2 7~ Qf 15
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: VBLK4020907B
Lab Project ID:
Compound
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
n-Butylbenzene
sec-Butyl benzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromo-3-chloropropane
Dibromomethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1 , 1-Dichloroethane
1 , 1-Dichloroethene
1 ,2-Dichloroethane
cis-1,2-Dichloroethene
trans-1,2-dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Dichlorodifluoromethane
Diisopropyl ether (DIPE)
Ethyl benzene
Hexachlorobutadiene
SGS ENVIRONMENTAL SERVICES, INC.
Result
UG/L
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 82608
Quantitation MDL
Limit UG/L UG/L
25.0 3.37
1.00 0.162
1.00 0.224
1.00 0.312
1.00 0.185
1.00 0.0960
1.00 0.104
25.0 1.09
1.00 0.272
1.00 0.235
1.00 0.182
1.00 0.206
1.00 0.181
1.00 0.177
1.00 0.416
1.00 0.220
1.00 0.282
1.00 0.205
1.00 0.206
1.00 0.208
5.00 1.95
1.00 0.275
1.00 0.264
1.00 0.190
1.00 0.234
1.00 0.182
5.00 1.42
1.00 0.215
1.00 0.164
1.00 0.244
1.00 0.176
1.00 0.230
1.00 0.166
1.00 0.169
1.00 0.239
1.00 0.176
1.00 0.202
1.00 0.119
5.00 0.385
1.00 0.235
1.00 0.206
1.00 0.409
Pare 1 of 2 N.C. CER IFICATION #481
Analyzed By: MJC
Date Collected:
Date Received:
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Flag
OGCMS LIMS v2.70 - - 4 of 15
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: VBLK4020907B
Lab Project ID:
Compound
2-Hexanone
lodomethane
lsopropylbenzene
4-lsopropyltoluene
Methylene chloride
4-Methyl-2-pentanone
Methyl-tert-butyl ether {MTBE)
Naphthalene
n-Propyl benzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Trichloroethene
1, 1, 1-Trichloroethane
1 , 1 ,2-Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-,p-Xylene
a-Xylene
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
SGS ENVIRONMENTAL SERVICES, INC.
Result
UG/L
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.480
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 82608
Quantitation MDL
Limit UG/L UG/L
5.00 0.874
1.00 0.129
1.00 0.173
1.00 0.200
1.00 0.188
5.00 0.495
1.00 0.214
1.00 0.280
1.00 0.211
1.00 0.239
1.00 0.288
1.00 0.256
1.00 0.304
1.00 0.175
1.00 0.199
1.00 0.244
1.00 0.209
1.00 0.197
1.00 0.267
1.00 0.428
1.00 0.234
1.00 0.200
1.00 0.187
1.00 0.400
2.00 0.386
1.00 0.167
Spike Spike
Added Result
10 9.79
10 9.73
10 9.9
Pa@2 of2 N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected:
Date Received:
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Percent
Recovered
98
97
99
Reviewed By: 'J.....--(1
Flag
J
OGCMS_LIMS_v2.7g Qf 15
Client Sample ID: MW-1
SGS ENVIRONMENTAL SERVICES, INC.
Results for Semivolatiles
by GCMS 625
Analyzed By: EAW
Client Project ID: Elkins Chrysler Mitsubishi Date Collected: 2/5/2007 11 :31
Date Received: 2/6/2007 Lab Sample ID: G122-2906-1F
Lab Project ID: G122-2906 Date Extracted: 2/7/2007
Matrix: Water
Result RL MDL Dilution Date
Compound ug/L ug/L ug/L Factor Analyzed
Acenaphthene BQL 10.0 1.22 1 2/8/2007
Acenaphthylene BQL 10.0 1.12 1 2/8/2007
Anthracene BQL 10.0 1.75 1 2/8/2007
Benzo[a]anthracene BQL 10.0 1.36 1 2/8/2007
Benzo[a]pyrene BQL 10.0 1.27 1 2/8/2007
Benzo[b ]fluoranthene BQL 10.0 1.43 1 2/8/2007
Benzo[g,h,i]perylene BQL 10.0 4.57 1 2/8/2007
Benzo[k]fluoranthene BQL 10.0 1.09 1 2/8/2007
Bis(2-chloroethoxy)methane BQL 10.0 1.11 1 2/8/2007
Bis(2-chloroethyl)ether BQL 10.0 1.09 1 2/8/2007
Bis(2-chloroisopropyl)ether BQL 10.0 1.57 1 2/8/2007
Bis(2-ethylhexyl }phthalate 1.70 10.0 1.33 1 2/8/2007
4-bromophenyl phenyl ether BQL 10.0 1.99 1 2/8/2007
Butylbenzylphthalate BQL 10.0 1.53 1 2/8/2007
2-Chloronaphthalene BQL 10.0 1.25 1 2/8/2007
2-Chlorophenol BQL 10.0 4.22 1 2/8/2007
4-Chloro-3-methylphenol BQL 10.0 3.26 1 2/8/2007
4-Chlorophenyl phenyl ether BQL 10.0 1.42 1 2/8/2007
Chrysene BQL 10.0 1.11 1 2/8/2007
Dibenzo[a,h]anthracene BQL 10.0 4.87 1 2/8/2007
Di-n-Butylphthalate BQL 10.0 1.65 1 2/8/2007
1,2-Dichlorobenzene BQL 10.0 1.25 1 2/8/2007
1,3-Dichlorobenzene BQL 10.0 1.24 1 2/8/2007
1,4-Dichlorobenzene BQL 10.0 1.20 1 2/8/2007
3,3'-Dichlorobenzidine BQL 20.0 4.10 1 2/8/2007
2,4-Dichlorophenol BQL 10.0 3.75 1 2/8/2007
Diethylphthalate 1.50 10.0 1.48 1 2/8/2007
Dimethylphthalate BQL 10.0 1.04 1 2/8/2007
2,4-Dimethylphenol BQL 10.0 9.25 1 2/8/2007
Di-n-octylphthalate BQL 10.0 1.16 1 2/8/2007
4,6-Dinitro-2-methylphenol BQL 50.0 3.71 1 2/8/2007
2,4-Dinitrophenol BQL 50.0 4.20 1 2/8/2007
2 ,4-Dinitrotoluene BQL 10.0 1.52 1 2/8/2007
2,6-Dinitrotoluene BQL 10.0 1.41 1 2/8/2007
Diphenylamine " BQL 10.0 1.53 1 2/8/2007
Fluoranthene BQL 10.0 1.41 1 2/8/2007
Fluorene BQL 10.0 1.22 1 2/8/2007
Hexachlorobenzene BQL 10.0 1.22 1 2/8/2007
Hexachlorobutadiene BQL 10.0 1.58 1 2/8/2007
Hexachlorocyclopentadiene BQL 20.0 20.0 1 2/8/2007
Hexachloroethane BQL 10.0 1.58 1 2/8/2007
lndeno(1,2,3-c,d)pyrene BQL 10.0 4.57 1 2/8/2007
lsophorone BQL 10.0 1.27 1 2/8/2007
Naphthalene BQL 10.0 1.08 1 2/8/2007
Nitrobenzene BQL 10.0 1.32 1 2/8/2007
2-Nitrophenol BQL 10.0 3.52 1 2/8/2007
Page 1of2
N.C. CERTIFICATION #481
Flag
J
J
8270.xls
9of15
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: MW-1
Results for Semivolatiles
byGCMS 625
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2906-1F
Lab Project ID: G122-2906
Compound
4-Nitrophenol
N-Nitrosodi-n-propylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d6
2,4,6-Tribromophenol
4-Terphenyl-d14
Comments:
Result
ug/L
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
RL
ug/L
50.0
10.0
50.0
10.0
10.0
10.0
10.0
10.0
Spike
Added
10
10
10
10
10
10
MDL
ug/L
3.17
1.87
2.83
1.38
3.38
2.08
1.33
2.92
Spike
Result
8.7
8.6
8.9
9
10.4
11.2
Analyzed By: EAW
Date Collected: 2/5/2007 11 :31
Date Received: 2/6/2007
Date Extracted: 2/7/2007
Matrix: Water
Dilution
Factor
1
1
1
1
1
1
1
1
Percent
Recovered
87
86
89
90
104
112
Date
Analyzed
2/8/2007
2/8/2007
2/8/2007
2/8/2007
2/8/2007
2/8/2007
2/8/2007
2/8/2007
.. N-Nitrosodiphenylamine is reported as the breakdown product Diphenylamine.
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Reviewed By: Rt
Page 2 of 2
N.C. CERTIFICATION #481
Flag
8270.xls
1Oof15
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: PB7284
Lab Project ID:
Compound
Acenaphthene
Acenaphthylene
Anthracene
Benzo[a]anthracene
Benzo(a]pyrene
Benzo[b ]fluoranthene
Benzo(g,h ,i]perylene
Benzo[k]fluoranthene
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl )ether
Bis(2-ethylhexyl)phthalate
4-bromophenyl phenyl ether
Butylbenzylphthalate
2-Chloronaphthalene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo[a,h]anthracene
Di-n-Butylphthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethylphthalate
2,4-Dimethylphenol
Di-n-octylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diphenylamine *
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
SGS ENVIRONMENTAL SERVICES, INC.
Results for Semivolatiles
by GCMS 625
Result RL MDL
ug/L ug/L ug/L
BQL 10.0 1.22
BQL 10.0 1.12
BQL 10.0 1.75
BQL 10.0 1.36
BQL 10.0 1.27
BQL 10.0 1.43
BQL 10.0 4.57
BQL 10.0 1.09
BQL 10.0 1.11
BQL 10.0 1.09
BQL 10.0 1.57
1.50 10.0 1.33
BQL 10.0 1.99
BQL 10.0 1.53
BQL 10.0 1.25
BQL 10.0 4.22
BQL 10.0 3.26
BQL 10.0 1.42
BQL 10.0 1.11
BQL 10.0 4.87
BQL 10.0 1.65
BQL 10.0 1.25
BQL 10.0 1.24
BQL 10.0 1.20
BQL 20.0 4.10
BQL 10.0 3.75
BQL 10.0 1.48
BQL 10.0 1.04
BQL 10.0 9.25
BQL 10.0 1.16
BQL 50.0 3.71
BQL 50.0 4.20
BQL 10.0 1.52
BQL 10.0 1.41
BQL 10.0 1.53
BQL 10.0 1.41
BQL 10.0 1.22
BQL 10.0 1.22
BQL 10.0 1.58
BQL 20.0 20.0
BQL 10.0 1.58
BQL 10.0 4.57
BQL 10.0 1.27
BQL 10.0 1.08
BQL 10.0 1.32
BQL 10.0 3.52
Page 1 of2
N.C. CERTIFICATION #481
Analyzed By: EAW
Date Collected:
Date Received:
Date Extracted: 2/7/2007
Matrix: WATER
Dilution Date
Factor Analyzed
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 21912007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
Flag
J
8270,xls
11 of 15
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: PB7284
Lab Project ID:
Compound
4-Nitrophenol
N-Nitrosodi-n-propylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d6
2,4,6-Tribromophenol
4-Terphenyl-d 14
Comments:
Results for Semivolatiles
by GCMS 625
Result RL MDL
ug/L ug/L ug/L
BQL 50.0 3.17
BQL 10.0 1.87
BQL 50.0 2.83
BQL 10.0 1.38
BQL 10.0 3.38
BQL 10.0 2.08
BQL 10.0 1.33
BQL 10.0 2.92
Spike Spike
Added Result
10 8.6
10 8
10 8.8
10 8.7
10 10
10 12.3
Analyzed By: EAW
Date Collected:
Date Received:
Date Extracted: 2/7/2007
Matrix: WATER
Dilution Date
Factor Analyzed
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
Percent
Recovered
86
80
88
87
100
123
* N-Nitrosodiphenylamine is reported as the breakdown product Diphenylamine.
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Reviewed By: Jl'N='---
Page 2 of 2
N.C. CERTIFICATION #481
Flag
8270.xls
12 of 15
SGS ENVIRONMENTAL SERVICES, INC.
List of Reporting Abbreviations
and Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantitation Limit (RL or MDL)
DF = Dilution Factor
Dup = Duplicate
D = Detected, but RPD is > 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL = Reporting Limit
RPO = Relative Percent Difference
mg/kg= milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
N.C. CERTIFICATION #481
Ml34.030606.3
14 of 15
z
0
() m ;:o
:::!
"Tl
0 ~ 0 z
:!;!:
00
.....>.
01
0 -.....>.
01
SGS
D 200 W. Potter Drive Anchorage, AK 99518 Tel: [phone] Fax: [phone]
D 5500 Business Drive Wilmington, NC 28405 Tel: [phone] Fax: [phone]
:J 1270 Greenbrier Street Charleston, WV 25311 Tel: [phone] Fax: [phone] White -Retained by Lab
Yellow -Returned with Report
Pink -Retained by Sampler
Mr. Darin McClure
Mid-Atlantic Associates
409 Rogersview Ct.
Raleigh NC 27610
Report Number: G 122-2910
SGS ENVIRONMENTAL SERVICES, INC.
Client Project: Elkins Chrysler Mitsubishi
Dear Mr. McClure:
Enclosed are the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call SGS/Paradigm at [phone]. We will be happy to answer any questions
or concerns which you may have.
Thank you for using SGS/Paradigm Analytical Labs for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely,
SGS/Paradigm Analytical Laboratories, Inc.
Lab~~~-
J. Patrick Weaver
-- -::J J I ?.) hJ.;sl ~e
N.C. CERTIFICATION #481 1 of 14
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: TMW-2
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2910-1A
Lab Project ID: G122-2910
Result
Compound UG/L
Benzene BQL
Bromobenzene BQL
Bromochloromethane BQL
Bromodichloromethane BQL
Bromoform BQL
Bromomethane BQL
n-Butylbenzene BQL
sec-Butyl benzene BQL
tert-Butylbenzene BQL
Carbon tetrachloride BQL
Chlorobenzene BQL
Chloroethane BQL
Chloroform BQL
Chloromethane BQL
2-Chlorotoluene BQL
4-Chlorotoluene BQL
Dibromochloromethane BQL
1,2-Dibromo-3-chloropropane BQL
Dibromomethane BQL
1,2-Dibromoethane (EDS) BQL
1,2-Dichlorobenzene BQL
1 ,3-Dichlorobenzene BQL
1 ,4-Dichlorobenzene BQL
1, 1-Dichloroethane BQL
1 , 1-Dichloroethene BQL
1 ,2-Dichloroethane BQL
cis-1,2-Dichloroethene BQL
trans-1,2-dichloroethene BQL
1 ,2-Dichloropropane BQL
1,3-Dichloropropane BQL
2,2-Dichloropropane BQL
1, 1-Dichloropropene BQL
Dichlorodifluoromethane BQL
Diisopropyl ether (DIPE) BQL
Ethyl benzene BQL
Hexachlorobutadiene BQL
lsopropylbenzene BQL
4-lsopropyltoluene BQL
Methylene chloride BQL
Results for Volatiles
by GCMS 621 OD
Quantitation MDL
Limit UG/L UG/L
0.500 0.152
0.500 0.199
0.500 0.312
0.500 0.195
0.500 0.116
0.500 0.398
0.500 0.262
0.500 0.234
0.500 0.181
0.500 0.150
0.500 0.178
0.500 0.373
0.500 0.195
0.500 0.457
0.500 0.204
0.500 0.198
0.500 0.198
5.00 1.89
0.500 0.276
0.500 0.269
0.500 0.187
0.500 0.242
0.500 0.177
0.500 0.201
0.500 0.159
0.500 0.223
0.500 0.161
0.500 0.230
0.500 0.132
0.500 0.163
0.500 0.263
0.500 0.176
5.00 0.459
0.500 0.204
0.500 0.183
0.500 0.406
0.500 0.163
0.500 0.203
5.00 0.176
Methyl-tert-butyl ether (MTBE) 3.73 0.500 0.201
Naphthalene BQL 0.500 0.259
n-Propyl benzene BQL 0.500 0.203
Page 1 of 2
N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected: 2/6/2007 8:01
Date Received: 2/7/2007
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Flag
OGCMS_LIMS_v2.70 2of14
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: TMW-2
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2910-1A
Lab Project ID: G122-2910
Result
Compound UG/L
Styrene BQL
1, 1, 1,2-Tetrachloroethane BQL
1, 1,2,2-Tetrachloroethane BQL
Tetrachloroethene BQL
Toluene 0.350
1,2,3-Trichlorobenzene BQL
1,2,4-Trichlorobenzene BQL
Trichloroethane BQL
1, 1, 1-Trichloroethane BQL
1, 1,2-Trichloroethane BQL
Trichlorofluoromethane BQL
1,2,3-Trichloropropane BQL
1,2,4-Trimethylbenzene BQL
1,3,5-Trimethylbenzene BQL
Vinyl chloride BQL
m-,p-Xylene BQL
a-Xylene BQL
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Results for Volatiles
by GCMS 621 OD
Quantitation MDL
Limit UG/L UG/L
0.500 0.235
0.500 0.298
0.500 0.217
0.500 0.219
0.500 0.154
0.500 0.206
0.500 0.271
0.500 0.201
0.500 0.168
0.500 0.231
0.500 0.481
0.500 0.214
0.500 0.205
0.500 0.179
0.500 0.464
1.00 0.388
0.500 0.156
Spike Spike
Added Result
10 9.93
10 10.2
10 9.91
Page 2 of 2 N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected: 2/6/2007 8:01
Date Received: 2/7/2007
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Percent
Recovered
99
102
99
Reviewed By: ~
Flag
j
OGCMS_LIMS_v2.73 Qf 14
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: TMW-1
Results for Volatiles
by GCMS 621 OD
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2910-2A
Lab Project ID: 8122-2910
Result Quantitation MDL
Compound UG/L Limit UG/L UG/L
Benzene 11.8 0.500 0.152
Bromobenzene BQL 0.500 0.199
Bromochloromethane BQL 0.500 0.312
Bromodichloromethane BQL 0.500 0.195
Bromoform BQL 0.500 0.116
Bromomethane BQL 0.500 0.398
n-Butylbenzene BQL 0.500 0.262
sec-Butyl benzene 3.66 0.500 0.234
tert-Butylbenzene 0.540 0.500 0.181
Carbon tetrachloride BQL 0.500 0.150
Chlorobenzene BQL 0.500 0.178
Chloroethane BQL 0.500 0.373
Chloroform BQL 0.500 0.195
Chloromethane BQL 0.500 0.457
2-Chlorotoluene BQL 0.500 0.204
4-Chlorotoluene BQL 0.500 0.198
Dibromochloromethane BQL 0.500 0.198
1,2-Dibromo-3-chloropropane BQL 5.00 1.89
Dibromomethane BQL 0.500 0.276
1,2-Dibromoethane (EDB) BQL 0.500 0.269
1,2-Dichlorobenzene BQL 0.500 0.187
1,3-Dichlorobenzene BQL 0.500 0.242
1,4-Dichlorobenzene BQL 0.500 0.177
1, 1-Dichloroethane BQL 0.500 0.201
1, 1-Dichloroethene BQL 0.500 0.159
1,2-Dichloroethane BQL 0.500 0.223
cis-1,2-Dichloroethene BQL 0.500 0.161
trans-1,2-dichloroethene BQL 0.500 0.230
1 ,2-Dichloropropane BQL 0.500 0.132
1 ,3-Dichloropropane BQL 0.500 0.163
2,2-Dichloropropane BQL 0.500 0.263
1, 1-Dichloropropene BQL 0.500 0.176
D ich lo rod ifluoromethane BQL 5.00 0.459
Diisopropyl ether (DIPE) 0.800 0.500 0.204
Ethyl benzene 3.61 0.500 0.183
Hexachlorobutadiene BQL 0.500 0.406
lsopropylbenzene 7.36 0.500 0.163
4-lsopropyltoluene 3.03 0.500 0.203
Methylene chloride BQL 5.00 0.176
Methyl-tert-butyl ether (MTBE) BQL 0.500 0.201
Naphthalene BQL 0.500 0.259
n-Propyl benzene 8.08 0.500 0.203
Page 1 of 2 N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected: 2/6/2007 9:00
Date Received: 2/7/2007
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Flag
OGCMS_LIMS_v2.74 Qf 14
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: TMW-1
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2910-2A
Lab Project ID: 8122-2910
Result
Compound UG/L
Styrene BQL
1, 1, 1,2-Tetrachloroethane BQL
1, 1,2,2-Tetrachloroethane BQL
Tetrachloroethene BQL
Toluene 1.60
1,2,3-Trichlorobenzene BQL
1,2,4-Trichlorobenzene BQL
Trichloroethene BQL
1, 1, 1-Trichloroethane BQL
1, 1,2-Trichloroethane BQL
Trichlorofluoromethane BQL
1,2,3-Trichloropropane BQL
1,2,4-Trimethylbenzene 2.94
1,3,5-Trimethylbenzene 7.44
Vinyl chloride BQL
m-,p-Xylene 8.22
a-Xylene 0.900
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Results for Volatiles
by GCMS 621 OD
Quantitation MDL
Limit UG/L UG/L
0.500 0.235
0.500 0.298
0.500 0.217
0.500 0.219
0.500 0.154
0.500 0.206
0.500 0.271
0.500 0.201
0.500 0.168
0.500 0.231
0.500 0.481
0.500 0.214
0.500 0.205
0.500 0.179
0.500 0.464
1.00 0.388
0.500 0.156
Spike Spike
Added Result
10 9.73
10 10.2
10 10.8
N.C. C~~t1f=ft~TION #481
Analyzed By: MJC
Date Collected: 2/6/2007 9:00
Date Received: 2/7/2007
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Percent
Recovered
97
102
108
Reviewed By'. 4
Flag
DGCMS_LIMS_v2.7cs of 14
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: TRIP BLANK
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2910-3A
Lab Project ID: G122-2910
Result
Compound UG/L
Benzene BQL
Bromobenzene BQL
Bromochloromethane BQL
Bromodichloromethane BQL
Bromoform BQL
Bromomethane BQL
n-Butylbenzene BQL
sec-Butyl benzene BQL
tert-Butylbenzene BQL
Carbon tetrachloride BQL
Chlorobenzene BQL
Chloroethane BQL
Chloroform BQL
Chloromethane BQL
2-Chlorotoluene BQL
4-Chlorotoluene BQL
Dibromochloromethane BQL
1,2-Dibromo-3-chloropropane BQL
Dibromomethane BQL
1,2-Dibromoethane (EDB) BQL
1,2-Dichlorobenzene BQL
1,3-Dichlorobenzene BQL
1,4-Dichlorobenzene BQL
1, 1-Dichloroethane BQL
1, 1-Dichloroethene BQL
1,2-Dichloroethane BQL
cis-1,2-Dichloroethene BQL
trans-1,2-dichloroethene BQL
1,2-Dichloropropane BQL
1,3-Dichloropropane BQL
2,2-Dichloropropane BQL
1, 1-Dichloropropene BQL
Dichlorodifluoromethane BQL
Diisopropyl ether (DIPE) BQL
Ethyl benzene BQL
Hexachlorobutadiene BQL
lsopropylbenzene BQL
4-lsopropyltoluene BQL
Methylene chloride BQL
Methyl-tert-butyl ether (MTBE) BQL
Naphthalene BQL
n-Propyl benzene BQL
Results for Volatiles
by GCMS 621 OD
Quantitation MDL
Limit UG/L UG/L
0.500 0.152
0.500 0.199
0.500 0.312
0.500 0.195
0.500 0.116
0.500 0.398
0.500 0.262
0.500 0.234
0.500 0.181
0.500 0.150
0.500 0.178
0.500 0.373
0.500 0.195
0.500 0.457
0.500 0.204
0.500 0.198
0.500 0.198
5.00 1.89
0.500 0.276
0.500 0.269
0.500 0.187
0.500 0.242
0.500 0.177
0.500 0.201
0.500 0.159
0.500 0.223
0.500 0.161
0.500 0.230
0.500 0.132
0.500 0.163
0.500 0.263
0.500 0.176
5.00 0.459
0.500 0.204
0.500 0.183
0.500 0.406
0.500 0.163
0.500 0.203
5.00 0.176
0.500 0.201
0.500 0.259
0.500 0.203
P~e 1of2 N.C. CE TIFICATION #481
Analyzed By: MJC
Date Collected: 2/6/2007 0:00
Date Received: 2/7/2007
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Flag
OGCMS_LIMS_v2 7~ Qf 14
SGS ENVIRONMENTAL SERVICES, INC.
Client Sample ID: TRIP BLANK
Client Project ID: Elkins Chrysler Mitsubishi
Lab Sample ID: G122-2910-3A
Lab Project ID: G122-2910
Result
Compound UG/L
Styrene BQL
1 , 1 , 1 ,2-Tetrachloroethane BQL
1, 1,2,2-Tetrachloroethane BQL
T etrach loroethene BQL
Toluene BQL
1,2,3-Trichlorobenzene BQL
1 ,2 ,4-Trichlorobenzene BQL
Trichloroethene BQL
1, 1, 1-Trichloroethane BQL
1, 1,2-Trichloroethane BQL
Trichlorofluoromethane BQL
1 ,2 ,3-Trichloropropane BQL
1,2,4-Trimethylbenzene BQL
1,3,5-Trimethylbenzene BQL
Vinyl chloride BQL
m-,p-Xylene BQL
a-Xylene BQL
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Results for Volatiles
by GCMS 621 OD
Quantitation MDL
Limit UG/L UG/L
0.500 0.235
0.500 0.298
0.500 0.217
0.500 0.219
0.500 0.154
0.500 0.206
0.500 0.271
0.500 0.201
0.500 0.168
0.500 0.231
0.500 0.481
0.500 0.214
0.500 0.205
0.500 0.179
0.500 0.464
1.00 0.388
0.500 0.156
Spike Spike
Added Result
10 9.96
10 9.95
10 9.95
Page 2 of 2
N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected: 2/6/2007 0:00
Date Received: 2/7/2007
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Percent
Recovered
100
99
99
Reviewed By: '5bfl
Flag
OGCMS_LIMS_v2.7°7 Qf 14
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: VBLK4020907B
Lab Project ID:
Compound
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butyl benzene
tert-Butyl benzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromo-3-chloropropane
Dibromomethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1, 1-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloroethane
cis-1,2-Dichloroethene
trans-1,2-dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichloropropene
Dichlorodifluoromethane
Diisopropyl ether (DIPE)
Ethyl benzene
Hexachlorobutadiene
lsopropylbenzene
4-lsopropyltoluene
Methylene chloride
Methyl-tert-butyl ether (MTBE)
Naphthalene
n-Propyl benzene
SGS ENVIRONMENTAL SERVICES, INC.
Result
UG/L
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 621 OD
Quantitation MDL
Limit UG/L UG/L
0.500 0.152
0.500 0.199
0.500 0.312
0.500 0.195
0.500 0.116
0.500 0.398
0.500 0.262
0.500 0.234
0.500 0.181
0.500 0.150
0.500 0.178
0.500 0.373
0.500 0.195
0.500 0.457
0.500 0.204
0.500 0.198
0.500 0.198
5.00 1.89
0.500 0.276
0.500 0.269
0.500 0.187
0.500 0.242
0.500 0.177
0.500 0.201
0.500 0.159
0.500 0.223
0.500 0.161
0.500 0.230
0.500 0.132
0.500 0.163
0.500 0.263
0.500 0.176
5.00 0.459
0.500 0.204
0.500 0.183
0.500 0.406
0.500 0.163
0.500 0.203
5.00 0.176
0.500 0.201
0.500 0.259
0.500 0.203
Pa~e 1of2 N.C. CE TIFICATION #481
Analyzed By: MJC
Date Collected:
Date Received:
Matrix: Water
Dilution Date
Factor Analyzed
1 2/9/2007
1 21912007
1 2/9/2007
1 2/9/2007
1 21912007
1 2/9/2007
1 21912007
2/9/2007
21912007
2/9/2007
21912007
21912007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
1 21912007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
21912007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
21912007
21912007
2/9/2007
2/9/2007
1 2/9/2007
1 2/9/2007
1 2/9/2007
21912007
21912007
2/9/2007
2/9/2007
Flag
OGCMS_LIMS_v2.7ig Qf 14
Client Sample ID: Method Blank
Client Project ID:
Lab Sample ID: VBLK4020907B
Lab Project ID:
Compound
Styrene
1, 1, 1 ,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetra ch loroethene
Toluene
1,2,3-Trichlorobenzene
1 ,2 ,4-Trichlorobenzene
Trichloroethane
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichlorofluoromethane
1 ,2 ,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-,p-Xylene
a-Xylene
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
SGS ENVIRONMENTAL SERVICES, INC.
Result
UG/L
BQL
BQL
BQL
BQL
BQL
0.480
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 621 OD
Quantitation MDL
Limit UG/L UG/L
0.500 0.235
0.500 0.298
0.500 0.217
0.500 0.219
0.500 0.154
0.500 0.206
0.500 0.271
0.500 0.201
0.500 0.168
0.500 0.231
0.500 0.481
0.500 0.214
0.500 0.205
0.500 0.179
0.500 0.464
1.00 0.388
0.500 0.156
Spike Spike
Added Result
10 9.79
10 9.73
10 9.9
Pa_ile 2 of 2 N.C. CERTIFICATION #481
Analyzed By: MJC
Date Collected:
Date Received:
Matrix: Water
Dilution Date
Factor Analyzed
1 21912007
1 21912007
1 21912007
21912007
21912007
21912007
21912007
2/9/2007
2/9/2007
2/9/2007
21912007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
2/9/2007
Percent
Recovered
98
97
99
Reviewed By: (L.,.f
Flag
J
OGCMS_LIMS_v2.7ig Qf 14
SGS ENVIRONMENTAL SERVICES, INC.
List of Reporting Abbreviations
and Data Qualifiers
8 = Compound also detected in batch blank
BQL = Below Quantitation Limit (RL or MDL)
OF= Dilution Factor
Dup = Duplicate
D = Detected, but RPO is > 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL = Reporting Limit
RPO = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
N.C. CERTIFICATION #481
Ml34.030606.3
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