7803_RobesonCoMSW_March2016_1stSemiAnnual_DIN26311_20160616

Robeson County Landfill
Water Quality Monitoring Report

March 2016 Semi-Annual Event

Prepared on Behalf of:

Robeson County Landfill
246 Landfill Rd
Lumberton, North Carolina 28360

Facility Permit No. 78-03

Dated:

June 16, 2016

Prepared by:

3430 Capuano St.
Lumberton NC, 28358

TRANSMITTAL LETTER

June 16, 2016

Mrs. Elizabeth Werner
Hydrogeologist
North Carolina Department of Environment and Natural Resources
Division of Waste Management - Solid Waste Section
217 W Jones St, Raleigh, North Carolina 27603

Subject: Robeson County Landfill Water Quality Monitoring Report
March 2016 Semi-Annual Event
Robeson County Landfill
St. Pauls, Robeson County, North Carolina

To: Mrs. Werner

Hunt Environmental Associates, PLLC has prepared this March 2016 Semi-Annual Water Quality
Monitoring Report for the Robeson County Landfill. This report summarizes the findings of
sampling data gathered at the site. The scope of work at the site was executed in order to fulfill the
NCDENR Solid Waste Section reporting requirements for environmental monitoring

We appreciate your consideration and review following the submission of this report. If you have-
any questions concerning this report, please don’t hesitate to contact us at [phone].

Respectfully Submitted,

______________________
Michael Cody Hunt, P.G., M.S.
Project Geologist

Table of Contents
1.0 INTRODUCTION ............................................................................................................... 1
2.0 SITE BACKGROUND AND MONITORING NETWORK .............................................. 1
3.0 SITE HYDROGEOLOGY................................................................................................... 1
4.0 FIELD ACTIVITIES ........................................................................................................... 2
5.0 ANALYTICAL RESULTS ................................................................................................. 2
5.1 Groundwater ..................................................................................................................... 2
5.2 Surface Water ................................................................................................................... 5
5.3 Leachate ........................................................................................................................... 5
6.0 STATISTICAL PROCEDURES ......................................................................................... 5
6.1 STATISTICAL RESULTS SUMMARY ........................................................................ 6
7.0 CONCLUSIONS AND RECOMMENDATIONS .............................................................. 6

Figures

Figure 1: Groundwater Potentiometric Map

Tables

Table 1: Groundwater Monitoring Program
Table 2: Ground Water Elevations & Flow Velocities
Table 3: Analytical Results
Table 4: Statistical Analysis Summary

Appendices

Appendix A: Laboratory Analytical Results
Appendix B: Time Series Graphs
Appendix C: Non-Parametric Prediction Interval Inter-Well Comparisons

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1.0 INTRODUCTION

The Robeson County Landfill, operating under North Carolina Department of Environment and
Natural Resources (NCDENR) Solid Waste Permit #78-03, is required to submit semi-annual
groundwater monitoring reports for detection monitoring of the Phase 2, Phase 3, and Phase 4
lined landfills and assessment monitoring of the Phase 1 unlined landfill. This report presents the
results of the first semi-annual monitoring event for 2016, conducted in March of 2016. Also
included in this report are the results of the surface water and leachate monitoring that was
performed in conjunction with the groundwater monitoring event.

The Robeson County Landfill is currently accepting construction and demolition debris (C&D)
waste over the closed Phase 1 Municipal Solid Waste (MSW) unlined landfill. Currently, all MSW
is being disposed in the Phase 4 lined landfill. The Phase 1 unlined landfill has been closed per
NCDENR Solid Waste Regulations, and the C&D disposal will bring the landfill to final closure
contours.
2.0 SITE BACKGROUND AND MONITORING NETWORK

Currently twenty-nine groundwater monitoring wells are located around the perimeter of the Phase
1, Phase 2, Phase 3, Phase 4 and C&D landfill cells (Figure 1). Table 1 lists the currently
monitored wells associated with each Phase of the landfill. Twenty-two groundwater monitoring
wells were monitored during this sampling event. Seven monitoring wells have been damaged
and were approved for closure by NCDENR Solid Waste Section correspondence from Ms.
Werner on March 22 of 2011, three wells were approved for closure and replacement on January
3, 2013 and therefore, none of them were sampled for this event.

Two surface water samples (SW-1 & SW-2) were collected as shown in Figure 1. Leachate
samples were also collected during this monitoring event for Phases 2, 3, and 4. Phase 2 and 3
leachate samples were collected from the respective line valves linked to the generator. The Phase
4 leachate sample was collected from the line pump station.

This report includes summaries of the field procedures, and field, laboratory, and statistical results
from the March 2016 semi-annual groundwater sampling event. Field and laboratory results of
the surface water and leachate sampling are also presented. Summary tables of the monitoring
network, groundwater characteristics, field measurements, laboratory and statistical analysis
results, as well as graphs of groundwater analytical data over time are included at the end of the
report.
3.0 SITE HYDROGEOLOGY

The site is located in the Coastal Plain Physiographic province within the Cretaceous-age Black
Creek Formation. In general, the lithology of the site is composed of sandy soils with clay. As a
result, the direction of groundwater flow should be largely controlled by site topography.

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Figure 1 provides potentiometric surface maps and groundwater flow calculations for the shallow
aquifer utilizing groundwater level data from the First Semi-Annual 2016 event. Groundwater flow
direction for the First Semi-Annual 2016 event was to the southeast towards the Big Marsh
Swamp, consistent with past events. Groundwater velocity for the First Semi-Annual 2016 event
was calculated utilizing Darcy’s law: V = Ki/n, where K = hydraulic conductivity, i = groundwater
gradient, n = porosity. Based on the fall dataset, groundwater velocities are estimated to range
from 0.18 feet/year (MW-24) to 91.39 feet/year (MW-9a).
4.0 FIELD ACTIVITIES

Groundwater, surface water, and leachate samples from the Robeson County Landfill were
collected on March 15 and 16, 2016. Twenty two (22) groundwater samples were collected by use
of a disposable, laboratory decontaminated polyethylene bailer. Sampling locations are presented
on Figure 1. Groundwater elevations were measured at each well prior to sampling and are
presented in Table 2. These groundwater elevations were used to construct the potentiometric
contours for this sampling event as shown on Figure 1. The groundwater elevations and
potentiometric contours were used to estimate groundwater velocities at each well presented in
Table 2. After depth to groundwater was measured, water was purged from each well to provide
fresh formation water within the well water column prior to sampling. All samples were collected
in clean laboratory prepared containers for the specified analytical methods. Groundwater samples
were properly preserved, placed on ice, and transported to the laboratory via overnight delivery.
The samples were transported to ESC Lab Sciences Inc., a North Carolina certified laboratory (NC
DW #21704). Laboratory analyses consisted of those noted in Table 1 and were reported
according to the laboratory’s Method Detection Limits (MDLs). The laboratory analytical reports
are included in Appendix A.

Trip and equipment blanks were used for quality assurance/quality control (QA/QC). Trip blanks
were prepared by the laboratory and accompanied the coolers during the sampling event. One
equipment blank was prepared by pouring distilled water over a bailer and collecting the water in
containers provided by the laboratory. Sampling methods followed the protocol outlined in
NCDENR’s Guidelines for Groundwater, Soil, and Surface Water Sampling (NCDENR 2008) and
in accordance with the approved Sampling and Analysis Plan (Water Quality Monitoring Plan,
David Garrett and Associates, Raleigh, NC, 2009).
5.0 ANALYTICAL RESULTS
5.1 Groundwater

ESC Lab Sciences, Inc. located in Lebanon, Tennesse analyzed samples for the North Carolina
Appendix I volatile organic compounds (VOCs) and metals. In accordance with SWS guidelines
the analytical results were reported to the laboratory specific method detection limit (MDL) and
are quantifiable at or below Solid Waste Section Limits (SWSLs). The following list indicates
which analytes were detected above the SWSL at each sampling location. Underlined analytes
exceeded the North Carolina 2L Standard (NC 2L), the Groundwater Protection Standard, or the
North Carolina Surface Water Standards for Class C Waters. A complete summary of all detected

3 | P a g e
and estimated concentrations for this sampling event is presented in Table 3. Copies of the
laboratory analytical data reports are provided in Appendix A.

MW-3R
Volatile Organic Compounds: None Detected
Metals: Barium, Chromium, Vanadium, Lead, Selenium

MW-5
Volatile Organic Compounds: Chlorobenzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane,
Vinyl Chloride
Metals: Barium

MW-6
Volatile Organic Compounds: None Detected
Metals: Barium, Lead

MW-8
Volatile Organic Compounds: 1,4-Dichlorobenzene, 1,1-Dichloroethane
Metals: Barium, Arsenic, Lead

MW-9A
Volatile Organic Compounds: Chlorobenzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane
Metals: Barium

MW-10
Volatile Organic Compounds: 1,1-Dichloroethane
Metals: Barium, Chromium, Vanadium, Beryllium, Cadmium,
Arsenic, Copper, Lead, Zinc

MW-11
Volatile Organic Compounds: None Detected
Metals: Barium, Lead

MW-12
Volatile Organic Compounds: None Detected
Metals: Barium

MW-13R
Volatile Organic Compounds: Acetone, Benzene, 1,4-Dichlorobenzene
Metals: Barium, Arsenic, Lead

MW-14
Volatile Organic Compounds: Acetone, Chlorobenzene, 1,4-Dichlorobenzene
Metals: Barium

4 | P a g e
MW-15
Volatile Organic Compounds: Acetone, Benzene, Chlorobenzene, 1,4-Dichlorobenzene,
1,1-Dichloroethane
Metals: Barium, Arsenic, Copper

MW-16
Volatile Organic Compounds: None Detected
Metals: Barium, Cobalt, Arsenic

MW-17R
Volatile Organic Compounds: None Detected
Metals: Barium

MW-18
Volatile Organic Compounds: None Detected
Metals: Barium, Lead

MW-19
Volatile Organic Compounds: None Detected
Metals: Barium, Chromium, Vanadium, Copper, Lead, Zinc

MW-20
Volatile Organic Compounds: None Detected
Metals: Barium, Lead

MW-21R
Volatile Organic Compounds: Acetone, 2-Butanone
Metals: Barium, Cobalt, Nickle, Arsenic, Copper, Lead

MW-22
Volatile Organic Compounds: None Detected
Metals: Barium, Lead

MW-23
Volatile Organic Compounds: None Detected
Metals: Barium

MW-24R
Volatile Organic Compounds: None Detected
Metals: Barium, Chromium, Vanadium, Lead

MW-25R
Volatile Organic Compounds: None Detected
Metals: Barium, Copper, Lead

5 | P a g e
MW-26
Volatile Organic Compounds: Acetone
Metals: Barium
5.2 Surface Water

HEA personnel sampled two surface water bodies in the vicinity of the Phase 1, 2, 3 and Phase 4
landfills (Figure 1). Surface water sampling point SW-1 is located below the outflow from the
existing sediment basin southwest of the Phase 1 cell. Surface water sampling point SW-2 is
located in a drainage ditch, southeast of the Phase 2 cell. The following list indicates which
analytes were detected above the SWSL at each sampling location. Underlined analytes exceeded
the North Carolina 2L Standard (NC 2L), the Groundwater Protection Standard, or the North
Carolina Surface Water Standards for Class C Waters.

SW-1
Volatile Organic Compounds: None Detected
Metals: Barium, Arsenic

SW-2
Volatile Organic Compounds: Acetone, Carbon Disulfide, 2-Butanone (Mek)
Metals: Barium, Nickle, Antimony, Arsenic, Zinc
5.3 Leachate

HEA personnel sampled three leachate drainage lines in the vicinity of the Phase 2, 3 and 4 landfill
cells. Two leachate sampling locations are east of the Phase 2 and 3 cells; one is located east of
the Phase 4 cell. Analytical results are presented in Table 3.
6.0 STATISTICAL PROCEDURES

The laboratory data from the sampling event were reviewed and analyzed by HEA in order to
evaluate trends and changes in the results and to identify statistically significant differences
between compliance and background wells. Data entry and analysis were performed using the
Chemstat statistical software package developed by Starpoint Software, Cincinnati, OH. Chemstat
follows the EPA document, Statistical Analysis of Ground-Water Monitoring Data at RCRA
Facilities – Unified Guidance (March 2009), as well as NCDENR guidelines.

The data were reviewed to evaluate the most appropriate analysis methods. Initial analysis
consisted of a basic review of the data and of the time vs. concentration graphs (included in
Appendix B) to determine any major changes or trends in the data. Individual compliance well
historical means were compared to the pooled background historical means for MW-6 and MW-
12 to determine if detected constituents were statistically significantly different from general
background groundwater quality.

The statistical analysis results are summarized in Table 4 and provided in Appendix C.

6 | P a g e
6.1 STATISTICAL RESULTS SUMMARY

For the First Semi-Annual 2016 event, statistically significant differences from background
concentrations and above SWSLs, shown in Table 4, were found for VOCs and Metals as detailed
below:

VOCs

 1,4-Dichlorobenzene – MW-9A, MW-13R, MW-15
 1,1-Dichloroethane – MW-9A
 Acetone – MW-21R

Metals

 Arsenic – MW-16, MW-21R
 Chromium – MW-10, MW-11, MW -17R
 Zinc – MW-11
 Cobalt – MW-17R, MW-21R
7.0 CONCLUSIONS AND RECOMMENDATIONS

For the First Semi-Annual 2016 groundwater monitoring event, concentrations that were
detected above an NC SWSL and NC GWPS/NC 2L were also determined to statistically exceed
the background concentrations. Based on the statistical evaluations:

No groundwater detections were identified as statistically significant increases for the First Semi-
Annual 2016 event.

The following groundwater detections were identified appearing to decrease sitewide:

 Acetone
 Benzene
 Cadmium
 Selenium

The following groundwater detections were identified appearing to remain relatively constant
sitewide:

 1,4-Dichlorobenzene
 1,1-Dichloroethane
 Arsenic
 Chromium
 Zinc
 Cobalt
 Selenium

7 | P a g e
During the First Semi-Annual 2016 event, one Appendix I VOCs and two Appendix I inorganic
constituents were detected in surface water samples at quantified concentrations above their
respective NC SWSLs at SW-2: Acetone, Barium, and Zinc. These constituents do not have a
NC 2B Surface Water Standard established for swamp waters (status of discharge locations).

The First Semi-Annual 2016 concentrations of acetone (0.14 mg/L), Barium (0.20 mg/L), and
Zinc (0.043 mg/L) at surface water location SW-2 are all below the NC 2L Groundwater
Standard 6 mg/L, 4 mg/L, 0.7 mg/L, and 1 mg/L respectively.

The site will continue monitoring in accordance with the requirements for Detection Monitoring
as outlined in Title 15A NCAC 13B .1633. The next semi-annual event is tentatively scheduled
for October 2016.

FIGURES

TABLES

Location Phase Gradient Current Use Zone
Monitored
Laboratory
Analysis
MW-1 Phase 1 Up Background Shallow N/A
MW-2 Phase 1 Down Compliance Shallow N/A
MW-3r Phase 1 Down Compliance Shallow Appendix I +
MW-4a Phase 1 Up Background Shallow N/A
MW-5 Phase 1 Down Compliance Shallow Appendix I +
MW-5a Phase 1 Down Compliance Deep N/A
MW-6 Phase 1 Up Background Shallow Appendix I +
MW-7 Phase 1 Cross Compliance Shallow N/A
MW-8 Phase 1 Down Compliance Shallow Appendix I +
MW-9 Phase 1 Down Compliance Shallow N/A
MW-9a Phase 1 Down Compliance Shallow Appendix I +
MW-9b Phase 1 Down Compliance Deep N/A
MW-10 Phase 1 Down Compliance Shallow Appendix I
MW-11 Phase 1 Down Compliance Shallow Appendix I
MW-12 Phase 2 Up Background Shallow Appendix I
MW-13r Phase 2 Down Compliance Shallow Appendix I
MW-14 Phase 2 Down Compliance Shallow Appendix I
MW-15 Phase 2 Down Compliance Shallow Appendix I
MW-16 Phase 2 Down Compliance Shallow Appendix I
MW-17r Phase 2 Down Compliance Shallow Appendix I
MW-18 Phase 2 Down Compliance Shallow Appendix I
MW-19 C & D Down Not used Shallow Metals & VOC
MW-20 C & D Down Not used Shallow Metals & VOC
MW-21 Phase 3 Down Compliance Shallow Appendix I
MW-22 Phase 3 Down Compliance Shallow Appendix I
MW-23 Phase 3 Cross Compliance Shallow Appendix I
MW-24R Phase 4 Cross Compliance Shallow Appendix I
MW-25R Phase 4 Down Compliance Shallow Appendix I
MW-26 Phase 4 Up Compliance Shallow Appendix I
Notes:
Appendix 1 = Appendix I constituents were analyzed.
N/A = Not Analyzed
Table 1
Groundwater Monitoring Program
Monitoring wells MW-1, MW-2, MW-4a, MW-5a, MW-7, MW-9, and MW-9b
were not analyzed per GNRA's request approved by NCDENR on July 14, 2000.
Appendix 1 + = Appendix I plus previously detected Appendix II constituents
were analyzed.
Well TOC Elevation
(ft)
DTW
(ft)
WTE
(ft)
Hyd Cond*
(ft/day)
Porosity**
(%)
Gradient***
(ft/ft)
Velocity****
(ft/day)(ft/year)
MW-1 151.14 nm NA 0.877 0.18 0.005 NA NA
MW-2 136.53 nm NA 0.822 0.16 0.005 NA NAMW-4a 153.02 nm NA 0.959 0.18 0.005 NA NAMW-7 155.89 nm NA 0.493 0.16 0.005 NA NA
MW-9 131.18 nm NA 0.466 0.20 0.005 NA NAMW-9a 131.60 4.36 127.24 9.589 0.18 0.005 0.250 91.39
MW-16 149.64 14.00 135.64 8.506 0.18 0.005 0.222 81.07MW-20 139.88 8.25 131.63 7.140 0.18 0.005 0.186 68.05MW-8 131.01 4.80 126.21 5.479 0.20 0.005 0.129 47.00
MW-6 150.73 8.94 141.79 2.000 0.15 0.005 0.063 22.87MW-12 157.79 15.65 142.14 2.041 0.18 0.005 0.053 19.45
MW-11 135.30 6.05 129.25 0.874 0.16 0.005 0.026 9.37MW-10 133.33 5.20 128.13 0.603 0.18 0.005 0.016 5.75MW-17r 150.31 12.92 137.39 0.257 0.15 0.005 0.008 2.94
MW-14 156.11 17.75 138.36 0.271 0.18 0.005 0.007 2.58MW-18 151.17 12.35 138.82 0.246 0.18 0.005 0.006 2.34
MW-13r 154.98 18.00 136.98 0.237 0.18 0.005 0.006 2.26MW-15a 151.91 15.30 136.61 0.183 0.16 0.005 0.005 1.96MW-3r 137.38 9.31 128.07 0.142 0.20 0.005 0.0033 1.22
MW-21 150.88 13.33 137.55 0.065 0.18 0.005 0.002 0.62MW-22 152.28 15.05 137.23 0.057 0.18 0.005 0.001 0.54
MW-26 154.59 13.60 140.99 0.05 0.18 0.005 0.00131 0.48MW-5 130.50 3.55 126.95 0.036 0.18 0.005 0.0009 0.34MW-23 151.75 11.49 140.26 0.028 0.18 0.005 0.001 0.27
MW-25R 154.25 14.61 139.64 0.025 0.18 0.005 0.00065 0.24MW-19 146.95 14.75 132.20 0.020 0.18 0.005 0.001 0.19
MW-24 154.58 12.43 142.15 0.019 0.18 0.005 0.00049 0.18
Notes TOC = Top of casing elevation NA = not available
DTW = Depth to Water from TOC nm = not measured
WTE = Water Table Elevation ft = feet
Hyd Cond = Hydraulic Conductivity % = percent
* Hydraulic Conductivity values from previous slug tests
** Effective Porosity from Groundwater & Wells (Driscoll, 1986)
***Average gradient for the October 2011 sampling event
****Velocity calculated by HEA using V=KI/n where
V = Ground water velocity
K = Hydraulic conductivity
I = Ground water gradient
n = Effective porosity
Table 2
Ground Water Elevations & Flow Velocities
M
W
-
3
R
M
W
-
5
M
W
-
6
M
W
-
8
M
W
-
9
A
M
W
-
1
0
M
W
-
1
1
M
W
-
1
2
M
W
-
1
3
R
M
W
-
1
4
M
W
-
1
5
M
W
-
1
6
M
W
-
1
7
R
M
W
-
1
8
M
W
-
1
9
M
W
-
2
0
M
W
-
2
1
R
M
W
-
2
2
M
W
-
2
3
M
W
-
2
4
R
M
W
-
2
5
R
M
W
-
2
6
S
W
-
1
S
W
-
2
L
E
A
C
H
A
T
E

P
H
A
S
E

2
L
E
A
C
H
A
T
E

P
H
A
S
E

3
L
E
A
C
H
A
T
E

P
H
A
S
E

4
Analyte Solid Waste
Selection Limits
Alkalinity BDL BDL NM
Dissolved Solids 108 77 NM
Phosphorus,Total NM 0.18 2.07 0.34
Cod NM 592 672 907
Bod NM 32.5 43.9 30.6
Barium 0.1 0.067 0.016 0.013 0.063 0.078 0.087 0.17 0.11 0.14 0.24 0.076 0.28 0.13 0.12 0.052 0.13 0.16 0.053 0.0091 0.041 0.029 NM 0.062 0.20 0.13 0.21 0.095
Chromium 0.01 0.012 BDL BDL BDL BDL 0.017 0.12 BDL BDL BDL BDL BDL 0.011 BDL 0.012 0.024 BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Cobalt 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.015 0.013 BDL BDL BDL 0.017 BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Nickel 0.05 BDL BDL BDL BDL BDL BDL 0.034 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL 0.017 BDL BDL 0.11
Silver 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Vanadium 0.025 0.026 BDL BDL BDL BDL 0.029 0.20 BDL BDL BDL BDL BDL BDL BDL 0.022 0.042 BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Antimony 0.006 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL 0.0041 BDL BDL BDL
Arsenic 0.01 BDL 0.002 BDL 0.0035 BDL 0.0023 0.0053 BDL BDL BDL BDL 0.011 BDL BDL BDL 0.0023 0.053 BDL BDL BDL 0.0022 NM 0.0021 0.0095 0.034 0.035 0.05
Beryllium 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Cadmium 0.001 BDL BDL BDL BDL BDL BDL 0.0051 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Copper 0.01 BDL BDL BDL BDL BDL BDL 0.043 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.019 0.0051 BDL BDL 0.01 NM BDL BDL 0.60 0.24 BDL
Lead 0.01 0.0043 BDL 0.0021 BDL BDL 0.0091 0.036 0.0026 0.0037 0.0024 BDL BDL 0.0048 0.0039 0.0078 0.01 0.0090 BDL BDL 0.0021 0.0033 NM BDL BDL 0.15 0.019 BDL
Selenium 0.01 0.023 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Thallium 0.0055 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Zinc 0.01 BDL BDL BDL BDL BDL BDL 0.30 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL 0.043 BDL BDL BDL
Acetone 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 2.95 BDL BDL BDL BDL NM BDL 0.14 0.092 BDL BDL
Acrylonitrile 0.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Benzene 0.001 BDL BDL BDL BDL 0.0011 BDL BDL BDL 0.002 BDL 0.0015 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL 0.0072 0.0059 0.01
Bromochloromethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Bromodichloromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Bromoform 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Bromomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Carbon Disulfide 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0014 NM BDL 0.013 BDL BDL BDL
Carbon Tetrachloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Chlorobenzene 0.003 BDL 0.0014 BDL BDL 0.0014 BDL BDL BDL BDL BDL 0.0021 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL 0.0021 0.0015 0.0012
Chlorodibromomethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Chloroethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Chloroform 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Chloromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Dibromomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
1,2-Dichlorobenzene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
1,4-Dichlorobenzene 0.001 BDL 0.0049 BDL 0.0016 0.0076 BDL BDL BDL 0.0011 BDL 0.0054 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL 0.018 0.009 0.0034
Project Sample ID
Table 3
Analytical Results
Trans-1,4-Dichloro-2-Butene 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
1,1-Dichloroethane 0.005 BDL 0.0038 BDL 0.0033 0.0093 0.0014 BDL BDL BDL BDL 0.0033 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
1,2-Dichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL 0.0022
1,1-Dichloroethene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Cis-1,2-Dichloroethene 0.005 BDL 0.0016 BDL BDL 0.0013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Trans-1,2-Dichloroethene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
1,2-Dichloropropane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Cis-1,3-Dichloropropene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Trans-1,3-Dichloropropene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Ethylbenzene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL 0.0063 0.0012 0.015
2-Hexanone 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Iodomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
2-Butanone (Mek)0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.076 BDL BDL BDL BDL NM BDL 0.068 0.11 BDL BDL
Methylene Chloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
4-Methyl-2-Pentanone (Mibk)0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Styrene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL 0.0017
1,1,1,2-Tetrachloroethane 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
1,1,2,2-Tetrachloroethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Tetrachloroethene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Toluene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL 0.017
1,1,1-Trichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
1,1,2-Trichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Trichloroethene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Trichlorofluoromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
1,2,3-Trichloropropane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Vinyl Acetate 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL BDL BDL
Vinyl Chloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL 0.0013 0.0015 0.0027
Xylenes, Total 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL 0.038 0.041 0.029
Chloride 1.2 4.2 NM
Nitrate 10 NM 0.54 0.90 BDL
Sulfate 250 8.1 14.7 NM 28.5 8.64 BDL
Notes:BDL = Below Detection Limit
* All units mg/L
NM - Not Measured / Well Dry at Time of Sampling
Location Parameter Detected
Concentration
Detection
Limit
Units %ND Test Statistically
Significant?
Above
2L/MCL
MW-3R Chromium 0.012 <0.0100 mg/L 0 NPPL N Y
MW-3R Vanadium 0.026 <0.0200 mg/L 50.3989 NPPL N Y
MW-3R Selenium 0.023 <0.00200 mg/L 57.6923 NPPL N Y
MW-5 1,4-Dichlorobenzene 0.0049 <0.00100 mg/L 60.425 NPPL N N
MW-8 1,4-Dichlorobenzene 0.002 <0.00100 mg/L 60.425 NPPL N N
MW-9A Benzene 0.001 <0.00100 mg/L 63.0667 NPPL N Y
MW-9A 1,4-Dichlorobenzene 0.0076 <0.00100 mg/L 60.425 NPPL Y Y
MW-9A 1,1-Dichloroethane 0.009 <0.00100 mg/L 41.1765 NPPL Y Y
MW-10 Chromium 0.017 <0.0100 mg/L 0 NPPL Y Y
MW-10 Vanadium 0.029 <0.0200 mg/L 50.3989 NPPL N Y
MW-11 Barium 0.1670 <0.00500 mg/L 50.9259 NPPL N N
MW-11 Chromium 0.1150 <0.0100 mg/L 0 NPPL Y Y
MW-11 Vanadium 0.2010 <0.0200 mg/L 50.3989 NPPL N Y
MW-11 Cadmium 0.0051 <0.00100 mg/L 51.4628 NPPL N Y
MW-11 Copper 0.043 <0.005 mg/L 53.7061 NPPL N Y
MW-11 Lead 0.0361 <0.00200 mg/L 47.2703 NPPL N Y
MW-11 Zinc 0.301 <0.0250 mg/L 43.9689 NPPL Y Y
MW-12 Barium 0.11 <0.00500 mg/L 50.9259 NPPL N Y
MW-13R Barium 0.140 <0.00500 mg/L 50.9259 NPPL N Y
MW-13R Benzene 0.00197 <0.00100 mg/L 63.0667 NPPL N Y
MW-13R 1,4-Dichlorobenzene 0.001 <0.00100 mg/L 60.425 NPPL Y N
MW-14 Barium 0.238 <0.00500 mg/L 50.9259 NPPL N N
MW-15 Benzene 0.002 <0.00100 mg/L 63.0667 NPPL N Y
MW-15 1,4-Dichlorobenzene 0.005 <0.00100 mg/L 60.425 NPPL Y N
MW-16 Barium 0.282 <0.00500 mg/L 50.9259 NPPL N N
MW-16 Cobalt 0.015 <0.0100 mg/L 54.244 NPPL F Y
MW-16 Arsenic 0.011 <0.002 mg/L 53.6521 NPPL Y Y
MW-17R Barium 0.128 <0.00500 mg/L 50.9259 NPPL N N
MW-17R Chromium 0.011 <0.0100 mg/L 0 NPPL Y Y
MW-17R Cobalt 0.013 <0.0100 mg/L 54.244 NPPL Y Y
MW-18 Barium 0.123 <0.00500 mg/L 50.9259 NPPL N N
MW-19 Chromium 0.012 <0.0100 mg/L 0 NPPL N Y
MW-20 Barium 0.130 <0.00500 mg/L 50.9259 NPPL N N
MW-20 Chromium 0.024 <0.0100 mg/L 0 NPPL N Y
MW-20 Vanadium 0.042 <0.0200 mg/L 50.3989 NPPL N Y
MW-20 Lead 0.010 <0.00200 mg/L 47.2703 NPPL N N
MW-21R Barium 0.161 <0.00500 mg/L 50.9259 NPPL N N
MW-21R Cobalt 0.017 <0.0100 mg/L 54.244 NPPL Y Y
MW-21R Arsenic 0.053 <0.002 mg/L 53.6521 NPPL Y Y
MW-21R Copper 0.019 <0.005 mg/L 53.7061 NPPL N Y
MW-21R Acetone 2.950 <0.05 mg/L 68.8172 NPPL Y Y
MW-25R Copper 0.010 <0.005 mg/L 53.7061 NPPL N Y
Notes:
MW-1 (historical data only), MW-6 and MW-12 were used as background wells. Wells not listed did not have any detected constituents.
% ND = percent non-detect
NPPL = Non-Parametric Prediction Limit (Inter-Well)
mg/L = milligrams per Liter
NA = Not available
Table 4
Statistical Analysis Summary

APPENDIX A: LABORATORY ANALYTICAL RESULTS

ANALYTICAL REPORT
March 25, 2016
Hunt Environmental Associates
Sample Delivery Group:L824012
Samples Received:03/17/2016
Project Number:14-011550
Description:Robeson Co Solid Waste Semi-Annual Env Monitoring
Report To:Cody Hunt
3430 Capuano Street
Lumberton, NC 28358
Entire Report Reviewed By:
March 25, 2016
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
March 25, 2016
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 7
⁵Sr: Sample Results 8
MW-3R L824012-01 8
MW-5 L824012-02 10
MW-6 L824012-03 12
MW-8 L824012-04 14
MW-9A L824012-05 16
MW-10 L824012-06 18
MW-11 L824012-07 20
MW-12 L824012-08 22
MW-13R L824012-09 24
MW-14 L824012-10 26
MW-15 L824012-11 28
MW-16 L824012-12 30
MW-17R L824012-13 32
MW-18 L824012-14 34
MW-19 L824012-15 36
MW-20 L824012-16 38
MW-21R L824012-17 40
MW-22 L824012-18 42
MW-23 L824012-19 44
MW-24R L824012-20 46
⁶Qc: Quality Control Summary 48
Gravimetric Analysis by Method 2540 C-2011 48
Wet Chemistry by Method 2320 B-2011 49
Wet Chemistry by Method 9056A 50
Metals (ICP) by Method 6010C 52
Metals (ICPMS) by Method 6020 53
Volatile Organic Compounds (GC/MS) by Method 8260B 55
⁷Gl: Glossary of Terms 61
⁸Al: Accreditations & Locations 62
⁹Sc: Chain of Custody 63
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-3R L824012-01 GW 03/16/16 12:00 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 17:50 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 19:43 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 14:52 03/23/16 14:52 BMB
Collected by Collected date/time Received date/time
MW-5 L824012-02 GW 03/16/16 13:40 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 17:54 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 19:45 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 15:10 03/23/16 15:10 BMB
Collected by Collected date/time Received date/time
MW-6 L824012-03 GW 03/16/16 08:45 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 17:38 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 19:47 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 15:28 03/23/16 15:28 BMB
Collected by Collected date/time Received date/time
MW-8 L824012-04 GW 03/16/16 14:08 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 17:57 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 18:51 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 15:47 03/23/16 15:47 BMB
Collected by Collected date/time Received date/time
MW-9A L824012-05 GW 03/16/16 13:50 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:06 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 19:50 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 16:05 03/23/16 16:05 BMB
Collected by Collected date/time Received date/time
MW-10 L824012-06 GW 03/16/16 13:20 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:09 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 19:52 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 16:23 03/23/16 16:23 BMB
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-11 L824012-07 GW 03/16/16 13:05 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:12 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 19:55 VSS
Metals (ICPMS) by Method 6020 WG857406 5 03/18/16 11:38 03/20/16 20:58 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 16:42 03/23/16 16:42 BMB
Collected by Collected date/time Received date/time
MW-12 L824012-08 GW 03/16/16 09:00 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:15 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 19:57 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 17:00 03/23/16 17:00 BMB
Collected by Collected date/time Received date/time
MW-13R L824012-09 GW 03/16/16 10:30 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:18 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 19:59 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 17:18 03/23/16 17:18 BMB
Collected by Collected date/time Received date/time
MW-14 L824012-10 GW 03/16/16 10:40 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:21 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:01 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 17:36 03/23/16 17:36 BMB
Collected by Collected date/time Received date/time
MW-15 L824012-11 GW 03/16/16 10:50 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:24 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:04 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 17:55 03/23/16 17:55 BMB
Collected by Collected date/time Received date/time
MW-16 L824012-12 GW 03/16/16 11:10 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:28 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:36 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 18:13 03/23/16 18:13 BMB
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-17R L824012-13 GW 03/16/16 11:50 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:31 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:39 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 18:31 03/23/16 18:31 BMB
Collected by Collected date/time Received date/time
MW-18 L824012-14 GW 03/16/16 11:40 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:34 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:42 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 18:49 03/23/16 18:49 BMB
Collected by Collected date/time Received date/time
MW-19 L824012-15 GW 03/16/16 12:30 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG857757 1 03/21/16 16:28 03/21/16 17:35 MF
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:43 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:44 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 19:08 03/23/16 19:08 BMB
Wet Chemistry by Method 2320 B-2011 WG858403 1 03/25/16 09:29 03/25/16 09:29 MCG
Wet Chemistry by Method 9056A WG857779 1 03/21/16 14:42 03/21/16 14:42 DJD
Collected by Collected date/time Received date/time
MW-20 L824012-16 GW 03/16/16 12:45 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG857757 1 03/21/16 16:28 03/21/16 17:35 MF
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:46 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:46 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 19:26 03/23/16 19:26 BMB
Wet Chemistry by Method 2320 B-2011 WG858403 1 03/25/16 09:36 03/25/16 09:36 MCG
Wet Chemistry by Method 9056A WG857779 1 03/21/16 14:59 03/21/16 14:59 DJD
Collected by Collected date/time Received date/time
MW-21R L824012-17 GW 03/16/16 10:00 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:49 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:49 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 19:45 03/23/16 19:45 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG858884 10 03/24/16 06:02 03/24/16 06:02 BMB
Collected by Collected date/time Received date/time
MW-22 L824012-18 GW 03/16/16 10:15 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:52 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:51 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 20:03 03/23/16 20:03 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG858884 1 03/24/16 06:25 03/24/16 06:25 BMB
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-23 L824012-19 GW 03/16/16 09:40 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:55 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:54 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 20:21 03/23/16 20:21 BMB
Collected by Collected date/time Received date/time
MW-24R L824012-20 GW 03/16/16 09:20 03/17/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG857404 1 03/18/16 11:35 03/18/16 18:59 WBD
Metals (ICPMS) by Method 6020 WG857406 1 03/18/16 11:38 03/20/16 20:56 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG858088 1 03/23/16 14:34 03/23/16 14:34 BMB
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Jimmy Hunt
Technical Service Representative
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L824012
MW-3R
Collected date/time: 03/16/16 12:00
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0666 0.00500 1 03/18/2016 17:50 WG857404
Chromium 0.0121 0.0100 1 03/18/2016 17:50 WG857404
Cobalt ND 0.0100 1 03/18/2016 17:50 WG857404
Nickel ND 0.0100 1 03/18/2016 17:50 WG857404
Silver ND 0.00500 1 03/18/2016 17:50 WG857404
Vanadium 0.0262 0.0200 1 03/18/2016 17:50 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 19:43 WG857406
Arsenic ND 0.00200 1 03/20/2016 19:43 WG857406
Beryllium ND 0.00200 1 03/20/2016 19:43 WG857406
Cadmium ND 0.00100 1 03/20/2016 19:43 WG857406
Copper ND 0.00500 1 03/20/2016 19:43 WG857406
Lead 0.00426 0.00200 1 03/20/2016 19:43 WG857406
Selenium 0.0226 0.00200 1 03/20/2016 19:43 WG857406
Thallium ND 0.00200 1 03/20/2016 19:43 WG857406
Zinc ND 0.0250 1 03/20/2016 19:43 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 14:52 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 14:52 WG858088
Benzene ND 0.00100 1 03/23/2016 14:52 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 14:52 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 14:52 WG858088
Bromoform ND 0.00100 1 03/23/2016 14:52 WG858088
Bromomethane ND 0.00500 1 03/23/2016 14:52 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 14:52 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 14:52 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 14:52 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 14:52 WG858088
Chloroethane ND 0.00500 1 03/23/2016 14:52 WG858088
Chloroform ND 0.00500 1 03/23/2016 14:52 WG858088
Chloromethane ND 0.00250 1 03/23/2016 14:52 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 14:52 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 14:52 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 14:52 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 14:52 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 14:52 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 14:52 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 14:52 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 14:52 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 14:52 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 14:52 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 14:52 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 14:52 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 14:52 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 14:52 WG858088
Iodomethane ND 0.0100 1 03/23/2016 14:52 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 14:52 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 14:52 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 14:52 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L824012
MW-3R
Collected date/time: 03/16/16 12:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 14:52 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 14:52 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 14:52 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 14:52 WG858088
Toluene ND 0.00500 1 03/23/2016 14:52 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 14:52 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 14:52 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 14:52 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 14:52 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 14:52 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 14:52 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 14:52 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 14:52 WG858088
(S) Toluene-d8 101 90.0-115 03/23/2016 14:52 WG858088
(S) Dibromofluoromethane 102 79.0-121 03/23/2016 14:52 WG858088
(S) a,a,a-Trifluorotoluene 99.8 90.4-116 03/23/2016 14:52 WG858088
(S) 4-Bromofluorobenzene 93.9 80.1-120 03/23/2016 14:52 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L824012
MW-5
Collected date/time: 03/16/16 13:40
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0162 0.00500 1 03/18/2016 17:54 WG857404
Chromium ND 0.0100 1 03/18/2016 17:54 WG857404
Cobalt ND 0.0100 1 03/18/2016 17:54 WG857404
Nickel ND 0.0100 1 03/18/2016 17:54 WG857404
Silver ND 0.00500 1 03/18/2016 17:54 WG857404
Vanadium ND 0.0200 1 03/18/2016 17:54 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 19:45 WG857406
Arsenic 0.00202 0.00200 1 03/20/2016 19:45 WG857406
Beryllium ND 0.00200 1 03/20/2016 19:45 WG857406
Cadmium ND 0.00100 1 03/20/2016 19:45 WG857406
Copper ND 0.00500 1 03/20/2016 19:45 WG857406
Lead ND 0.00200 1 03/20/2016 19:45 WG857406
Selenium ND 0.00200 1 03/20/2016 19:45 WG857406
Thallium ND 0.00200 1 03/20/2016 19:45 WG857406
Zinc ND 0.0250 1 03/20/2016 19:45 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 15:10 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 15:10 WG858088
Benzene ND 0.00100 1 03/23/2016 15:10 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 15:10 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 15:10 WG858088
Bromoform ND 0.00100 1 03/23/2016 15:10 WG858088
Bromomethane ND 0.00500 1 03/23/2016 15:10 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 15:10 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 15:10 WG858088
Chlorobenzene 0.00139 0.00100 1 03/23/2016 15:10 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 15:10 WG858088
Chloroethane ND 0.00500 1 03/23/2016 15:10 WG858088
Chloroform ND 0.00500 1 03/23/2016 15:10 WG858088
Chloromethane ND 0.00250 1 03/23/2016 15:10 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 15:10 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 15:10 WG858088
1,4-Dichlorobenzene 0.00490 0.00100 1 03/23/2016 15:10 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 15:10 WG858088
1,1-Dichloroethane 0.00379 0.00100 1 03/23/2016 15:10 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 15:10 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 15:10 WG858088
cis-1,2-Dichloroethene 0.00155 0.00100 1 03/23/2016 15:10 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 15:10 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 15:10 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 15:10 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 15:10 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 15:10 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 15:10 WG858088
Iodomethane ND 0.0100 1 03/23/2016 15:10 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 15:10 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 15:10 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 15:10 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L824012
MW-5
Collected date/time: 03/16/16 13:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 15:10 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 15:10 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 15:10 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 15:10 WG858088
Toluene ND 0.00500 1 03/23/2016 15:10 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 15:10 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 15:10 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 15:10 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 15:10 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 15:10 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 15:10 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 15:10 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 15:10 WG858088
(S) Toluene-d8 99.4 90.0-115 03/23/2016 15:10 WG858088
(S) Dibromofluoromethane 105 79.0-121 03/23/2016 15:10 WG858088
(S) a,a,a-Trifluorotoluene 102 90.4-116 03/23/2016 15:10 WG858088
(S) 4-Bromofluorobenzene 103 80.1-120 03/23/2016 15:10 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L824012
MW-6
Collected date/time: 03/16/16 08:45
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0126 0.00500 1 03/18/2016 17:38 WG857404
Chromium ND 0.0100 1 03/18/2016 17:38 WG857404
Cobalt ND 0.0100 1 03/18/2016 17:38 WG857404
Nickel ND 0.0100 1 03/18/2016 17:38 WG857404
Silver ND 0.00500 1 03/18/2016 17:38 WG857404
Vanadium ND 0.0200 1 03/18/2016 17:38 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 19:47 WG857406
Arsenic ND 0.00200 1 03/20/2016 19:47 WG857406
Beryllium ND 0.00200 1 03/20/2016 19:47 WG857406
Cadmium ND 0.00100 1 03/20/2016 19:47 WG857406
Copper ND 0.00500 1 03/20/2016 19:47 WG857406
Lead 0.00208 0.00200 1 03/20/2016 19:47 WG857406
Selenium ND 0.00200 1 03/20/2016 19:47 WG857406
Thallium ND 0.00200 1 03/20/2016 19:47 WG857406
Zinc ND 0.0250 1 03/20/2016 19:47 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 15:28 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 15:28 WG858088
Benzene ND 0.00100 1 03/23/2016 15:28 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 15:28 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 15:28 WG858088
Bromoform ND 0.00100 1 03/23/2016 15:28 WG858088
Bromomethane ND 0.00500 1 03/23/2016 15:28 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 15:28 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 15:28 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 15:28 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 15:28 WG858088
Chloroethane ND 0.00500 1 03/23/2016 15:28 WG858088
Chloroform ND 0.00500 1 03/23/2016 15:28 WG858088
Chloromethane ND 0.00250 1 03/23/2016 15:28 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 15:28 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 15:28 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 15:28 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 15:28 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 15:28 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 15:28 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 15:28 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 15:28 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 15:28 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 15:28 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 15:28 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 15:28 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 15:28 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 15:28 WG858088
Iodomethane ND 0.0100 1 03/23/2016 15:28 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 15:28 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 15:28 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 15:28 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L824012
MW-6
Collected date/time: 03/16/16 08:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 15:28 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 15:28 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 15:28 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 15:28 WG858088
Toluene ND 0.00500 1 03/23/2016 15:28 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 15:28 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 15:28 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 15:28 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 15:28 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 15:28 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 15:28 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 15:28 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 15:28 WG858088
(S) Toluene-d8 105 90.0-115 03/23/2016 15:28 WG858088
(S) Dibromofluoromethane 102 79.0-121 03/23/2016 15:28 WG858088
(S) a,a,a-Trifluorotoluene 107 90.4-116 03/23/2016 15:28 WG858088
(S) 4-Bromofluorobenzene 98.6 80.1-120 03/23/2016 15:28 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L824012
MW-8
Collected date/time: 03/16/16 14:08
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0632 0.00500 1 03/18/2016 17:57 WG857404
Chromium ND 0.0100 1 03/18/2016 17:57 WG857404
Cobalt ND 0.0100 1 03/18/2016 17:57 WG857404
Nickel ND 0.0100 1 03/18/2016 17:57 WG857404
Silver ND 0.00500 1 03/18/2016 17:57 WG857404
Vanadium ND 0.0200 1 03/18/2016 17:57 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 18:51 WG857406
Arsenic 0.00347 0.00200 1 03/20/2016 18:51 WG857406
Beryllium ND 0.00200 1 03/20/2016 18:51 WG857406
Cadmium ND 0.00100 1 03/20/2016 18:51 WG857406
Copper ND 0.00500 1 03/20/2016 18:51 WG857406
Lead ND 0.00200 1 03/20/2016 18:51 WG857406
Selenium ND 0.00200 1 03/20/2016 18:51 WG857406
Thallium ND 0.00200 1 03/20/2016 18:51 WG857406
Zinc ND 0.0250 1 03/20/2016 18:51 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 15:47 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 15:47 WG858088
Benzene ND 0.00100 1 03/23/2016 15:47 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 15:47 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 15:47 WG858088
Bromoform ND 0.00100 1 03/23/2016 15:47 WG858088
Bromomethane ND 0.00500 1 03/23/2016 15:47 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 15:47 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 15:47 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 15:47 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 15:47 WG858088
Chloroethane ND 0.00500 1 03/23/2016 15:47 WG858088
Chloroform ND 0.00500 1 03/23/2016 15:47 WG858088
Chloromethane ND 0.00250 1 03/23/2016 15:47 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 15:47 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 15:47 WG858088
1,4-Dichlorobenzene 0.00163 0.00100 1 03/23/2016 15:47 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 15:47 WG858088
1,1-Dichloroethane 0.00328 0.00100 1 03/23/2016 15:47 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 15:47 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 15:47 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 15:47 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 15:47 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 15:47 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 15:47 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 15:47 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 15:47 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 15:47 WG858088
Iodomethane ND 0.0100 1 03/23/2016 15:47 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 15:47 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 15:47 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 15:47 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 14 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 14 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L824012
MW-8
Collected date/time: 03/16/16 14:08
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 15:47 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 15:47 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 15:47 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 15:47 WG858088
Toluene ND 0.00500 1 03/23/2016 15:47 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 15:47 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 15:47 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 15:47 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 15:47 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 15:47 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 15:47 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 15:47 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 15:47 WG858088
(S) Toluene-d8 98.9 90.0-115 03/23/2016 15:47 WG858088
(S) Dibromofluoromethane 104 79.0-121 03/23/2016 15:47 WG858088
(S) a,a,a-Trifluorotoluene 104 90.4-116 03/23/2016 15:47 WG858088
(S) 4-Bromofluorobenzene 97.2 80.1-120 03/23/2016 15:47 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 15 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 15 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L824012
MW-9A
Collected date/time: 03/16/16 13:50
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0777 0.00500 1 03/18/2016 18:06 WG857404
Chromium ND 0.0100 1 03/18/2016 18:06 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:06 WG857404
Nickel ND 0.0100 1 03/18/2016 18:06 WG857404
Silver ND 0.00500 1 03/18/2016 18:06 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:06 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 19:50 WG857406
Arsenic ND 0.00200 1 03/20/2016 19:50 WG857406
Beryllium ND 0.00200 1 03/20/2016 19:50 WG857406
Cadmium ND 0.00100 1 03/20/2016 19:50 WG857406
Copper ND 0.00500 1 03/20/2016 19:50 WG857406
Lead ND 0.00200 1 03/20/2016 19:50 WG857406
Selenium ND 0.00200 1 03/20/2016 19:50 WG857406
Thallium ND 0.00200 1 03/20/2016 19:50 WG857406
Zinc ND 0.0250 1 03/20/2016 19:50 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 16:05 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 16:05 WG858088
Benzene 0.00113 0.00100 1 03/23/2016 16:05 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 16:05 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 16:05 WG858088
Bromoform ND 0.00100 1 03/23/2016 16:05 WG858088
Bromomethane ND 0.00500 1 03/23/2016 16:05 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 16:05 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 16:05 WG858088
Chlorobenzene 0.00143 0.00100 1 03/23/2016 16:05 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 16:05 WG858088
Chloroethane ND 0.00500 1 03/23/2016 16:05 WG858088
Chloroform ND 0.00500 1 03/23/2016 16:05 WG858088
Chloromethane ND 0.00250 1 03/23/2016 16:05 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 16:05 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 16:05 WG858088
1,4-Dichlorobenzene 0.00762 0.00100 1 03/23/2016 16:05 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 16:05 WG858088
1,1-Dichloroethane 0.00931 0.00100 1 03/23/2016 16:05 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 16:05 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 16:05 WG858088
cis-1,2-Dichloroethene 0.00129 0.00100 1 03/23/2016 16:05 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 16:05 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 16:05 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 16:05 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 16:05 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 16:05 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 16:05 WG858088
Iodomethane ND 0.0100 1 03/23/2016 16:05 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 16:05 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 16:05 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 16:05 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 16 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 16 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L824012
MW-9A
Collected date/time: 03/16/16 13:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 16:05 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 16:05 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 16:05 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 16:05 WG858088
Toluene ND 0.00500 1 03/23/2016 16:05 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 16:05 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 16:05 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 16:05 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 16:05 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 16:05 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 16:05 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 16:05 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 16:05 WG858088
(S) Toluene-d8 103 90.0-115 03/23/2016 16:05 WG858088
(S) Dibromofluoromethane 103 79.0-121 03/23/2016 16:05 WG858088
(S) a,a,a-Trifluorotoluene 101 90.4-116 03/23/2016 16:05 WG858088
(S) 4-Bromofluorobenzene 98.5 80.1-120 03/23/2016 16:05 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 17 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 17 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L824012
MW-10
Collected date/time: 03/16/16 13:20
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0868 0.00500 1 03/18/2016 18:09 WG857404
Chromium 0.0167 0.0100 1 03/18/2016 18:09 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:09 WG857404
Nickel ND 0.0100 1 03/18/2016 18:09 WG857404
Silver ND 0.00500 1 03/18/2016 18:09 WG857404
Vanadium 0.0290 0.0200 1 03/18/2016 18:09 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 19:52 WG857406
Arsenic 0.00233 0.00200 1 03/20/2016 19:52 WG857406
Beryllium ND 0.00200 1 03/20/2016 19:52 WG857406
Cadmium ND 0.00100 1 03/20/2016 19:52 WG857406
Copper ND 0.00500 1 03/20/2016 19:52 WG857406
Lead 0.00909 0.00200 1 03/20/2016 19:52 WG857406
Selenium ND 0.00200 1 03/20/2016 19:52 WG857406
Thallium ND 0.00200 1 03/20/2016 19:52 WG857406
Zinc ND 0.0250 1 03/20/2016 19:52 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 16:23 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 16:23 WG858088
Benzene ND 0.00100 1 03/23/2016 16:23 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 16:23 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 16:23 WG858088
Bromoform ND 0.00100 1 03/23/2016 16:23 WG858088
Bromomethane ND 0.00500 1 03/23/2016 16:23 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 16:23 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 16:23 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 16:23 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 16:23 WG858088
Chloroethane ND 0.00500 1 03/23/2016 16:23 WG858088
Chloroform ND 0.00500 1 03/23/2016 16:23 WG858088
Chloromethane ND 0.00250 1 03/23/2016 16:23 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 16:23 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 16:23 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 16:23 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 16:23 WG858088
1,1-Dichloroethane 0.00141 0.00100 1 03/23/2016 16:23 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 16:23 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 16:23 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 16:23 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 16:23 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 16:23 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 16:23 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 16:23 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 16:23 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 16:23 WG858088
Iodomethane ND 0.0100 1 03/23/2016 16:23 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 16:23 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 16:23 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 16:23 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 18 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 18 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L824012
MW-10
Collected date/time: 03/16/16 13:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 16:23 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 16:23 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 16:23 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 16:23 WG858088
Toluene ND 0.00500 1 03/23/2016 16:23 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 16:23 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 16:23 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 16:23 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 16:23 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 16:23 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 16:23 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 16:23 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 16:23 WG858088
(S) Toluene-d8 102 90.0-115 03/23/2016 16:23 WG858088
(S) Dibromofluoromethane 105 79.0-121 03/23/2016 16:23 WG858088
(S) a,a,a-Trifluorotoluene 103 90.4-116 03/23/2016 16:23 WG858088
(S) 4-Bromofluorobenzene 101 80.1-120 03/23/2016 16:23 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 19 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 19 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L824012
MW-11
Collected date/time: 03/16/16 13:05
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.167 0.00500 1 03/18/2016 18:12 WG857404
Chromium 0.115 0.0100 1 03/18/2016 18:12 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:12 WG857404
Nickel 0.0339 0.0100 1 03/18/2016 18:12 WG857404
Silver ND 0.00500 1 03/18/2016 18:12 WG857404
Vanadium 0.201 0.0200 1 03/18/2016 18:12 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 19:55 WG857406
Arsenic 0.00532 0.00200 1 03/20/2016 19:55 WG857406
Beryllium ND 0.00200 1 03/20/2016 19:55 WG857406
Cadmium 0.00508 0.00100 1 03/20/2016 19:55 WG857406
Copper 0.0425 0.00500 1 03/20/2016 19:55 WG857406
Lead 0.0361 0.00200 1 03/20/2016 19:55 WG857406
Selenium ND 0.00200 1 03/20/2016 19:55 WG857406
Thallium ND 0.00200 1 03/20/2016 19:55 WG857406
Zinc 0.301 0.125 5 03/20/2016 20:58 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 16:42 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 16:42 WG858088
Benzene ND 0.00100 1 03/23/2016 16:42 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 16:42 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 16:42 WG858088
Bromoform ND 0.00100 1 03/23/2016 16:42 WG858088
Bromomethane ND 0.00500 1 03/23/2016 16:42 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 16:42 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 16:42 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 16:42 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 16:42 WG858088
Chloroethane ND 0.00500 1 03/23/2016 16:42 WG858088
Chloroform ND 0.00500 1 03/23/2016 16:42 WG858088
Chloromethane ND 0.00250 1 03/23/2016 16:42 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 16:42 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 16:42 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 16:42 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 16:42 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 16:42 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 16:42 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 16:42 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 16:42 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 16:42 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 16:42 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 16:42 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 16:42 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 16:42 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 16:42 WG858088
Iodomethane ND 0.0100 1 03/23/2016 16:42 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 16:42 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 16:42 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 16:42 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 20 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 20 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L824012
MW-11
Collected date/time: 03/16/16 13:05
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 16:42 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 16:42 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 16:42 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 16:42 WG858088
Toluene ND 0.00500 1 03/23/2016 16:42 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 16:42 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 16:42 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 16:42 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 16:42 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 16:42 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 16:42 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 16:42 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 16:42 WG858088
(S) Toluene-d8 100 90.0-115 03/23/2016 16:42 WG858088
(S) Dibromofluoromethane 103 79.0-121 03/23/2016 16:42 WG858088
(S) a,a,a-Trifluorotoluene 102 90.4-116 03/23/2016 16:42 WG858088
(S) 4-Bromofluorobenzene 102 80.1-120 03/23/2016 16:42 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 21 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 21 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L824012
MW-12
Collected date/time: 03/16/16 09:00
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.106 0.00500 1 03/18/2016 18:15 WG857404
Chromium ND 0.0100 1 03/18/2016 18:15 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:15 WG857404
Nickel ND 0.0100 1 03/18/2016 18:15 WG857404
Silver ND 0.00500 1 03/18/2016 18:15 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:15 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 19:57 WG857406
Arsenic ND 0.00200 1 03/20/2016 19:57 WG857406
Beryllium ND 0.00200 1 03/20/2016 19:57 WG857406
Cadmium ND 0.00100 1 03/20/2016 19:57 WG857406
Copper ND 0.00500 1 03/20/2016 19:57 WG857406
Lead 0.00263 0.00200 1 03/20/2016 19:57 WG857406
Selenium ND 0.00200 1 03/20/2016 19:57 WG857406
Thallium ND 0.00200 1 03/20/2016 19:57 WG857406
Zinc ND 0.0250 1 03/20/2016 19:57 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 17:00 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 17:00 WG858088
Benzene ND 0.00100 1 03/23/2016 17:00 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 17:00 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 17:00 WG858088
Bromoform ND 0.00100 1 03/23/2016 17:00 WG858088
Bromomethane ND 0.00500 1 03/23/2016 17:00 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 17:00 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 17:00 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 17:00 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 17:00 WG858088
Chloroethane ND 0.00500 1 03/23/2016 17:00 WG858088
Chloroform ND 0.00500 1 03/23/2016 17:00 WG858088
Chloromethane ND 0.00250 1 03/23/2016 17:00 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 17:00 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 17:00 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 17:00 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 17:00 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 17:00 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 17:00 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 17:00 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 17:00 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 17:00 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 17:00 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 17:00 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 17:00 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 17:00 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 17:00 WG858088
Iodomethane ND 0.0100 1 03/23/2016 17:00 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 17:00 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 17:00 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 17:00 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 22 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 22 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L824012
MW-12
Collected date/time: 03/16/16 09:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 17:00 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 17:00 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 17:00 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 17:00 WG858088
Toluene ND 0.00500 1 03/23/2016 17:00 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 17:00 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 17:00 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 17:00 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 17:00 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 17:00 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 17:00 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 17:00 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 17:00 WG858088
(S) Toluene-d8 99.3 90.0-115 03/23/2016 17:00 WG858088
(S) Dibromofluoromethane 109 79.0-121 03/23/2016 17:00 WG858088
(S) a,a,a-Trifluorotoluene 103 90.4-116 03/23/2016 17:00 WG858088
(S) 4-Bromofluorobenzene 94.2 80.1-120 03/23/2016 17:00 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 23 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 23 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L824012
MW-13R
Collected date/time: 03/16/16 10:30
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.140 0.00500 1 03/18/2016 18:18 WG857404
Chromium ND 0.0100 1 03/18/2016 18:18 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:18 WG857404
Nickel ND 0.0100 1 03/18/2016 18:18 WG857404
Silver ND 0.00500 1 03/18/2016 18:18 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:18 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 19:59 WG857406
Arsenic ND 0.00200 1 03/20/2016 19:59 WG857406
Beryllium ND 0.00200 1 03/20/2016 19:59 WG857406
Cadmium ND 0.00100 1 03/20/2016 19:59 WG857406
Copper ND 0.00500 1 03/20/2016 19:59 WG857406
Lead 0.00373 0.00200 1 03/20/2016 19:59 WG857406
Selenium ND 0.00200 1 03/20/2016 19:59 WG857406
Thallium ND 0.00200 1 03/20/2016 19:59 WG857406
Zinc ND 0.0250 1 03/20/2016 19:59 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 17:18 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 17:18 WG858088
Benzene 0.00197 0.00100 1 03/23/2016 17:18 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 17:18 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 17:18 WG858088
Bromoform ND 0.00100 1 03/23/2016 17:18 WG858088
Bromomethane ND 0.00500 1 03/23/2016 17:18 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 17:18 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 17:18 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 17:18 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 17:18 WG858088
Chloroethane ND 0.00500 1 03/23/2016 17:18 WG858088
Chloroform ND 0.00500 1 03/23/2016 17:18 WG858088
Chloromethane ND 0.00250 1 03/23/2016 17:18 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 17:18 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 17:18 WG858088
1,4-Dichlorobenzene 0.00107 0.00100 1 03/23/2016 17:18 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 17:18 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 17:18 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 17:18 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 17:18 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 17:18 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 17:18 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 17:18 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 17:18 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 17:18 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 17:18 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 17:18 WG858088
Iodomethane ND 0.0100 1 03/23/2016 17:18 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 17:18 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 17:18 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 17:18 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 24 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 24 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L824012
MW-13R
Collected date/time: 03/16/16 10:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 17:18 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 17:18 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 17:18 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 17:18 WG858088
Toluene ND 0.00500 1 03/23/2016 17:18 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 17:18 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 17:18 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 17:18 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 17:18 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 17:18 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 17:18 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 17:18 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 17:18 WG858088
(S) Toluene-d8 103 90.0-115 03/23/2016 17:18 WG858088
(S) Dibromofluoromethane 106 79.0-121 03/23/2016 17:18 WG858088
(S) a,a,a-Trifluorotoluene 102 90.4-116 03/23/2016 17:18 WG858088
(S) 4-Bromofluorobenzene 99.4 80.1-120 03/23/2016 17:18 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 25 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 25 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L824012
MW-14
Collected date/time: 03/16/16 10:40
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.238 0.00500 1 03/18/2016 18:21 WG857404
Chromium ND 0.0100 1 03/18/2016 18:21 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:21 WG857404
Nickel ND 0.0100 1 03/18/2016 18:21 WG857404
Silver ND 0.00500 1 03/18/2016 18:21 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:21 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:01 WG857406
Arsenic ND 0.00200 1 03/20/2016 20:01 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:01 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:01 WG857406
Copper ND 0.00500 1 03/20/2016 20:01 WG857406
Lead 0.00243 0.00200 1 03/20/2016 20:01 WG857406
Selenium ND 0.00200 1 03/20/2016 20:01 WG857406
Thallium ND 0.00200 1 03/20/2016 20:01 WG857406
Zinc ND 0.0250 1 03/20/2016 20:01 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 17:36 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 17:36 WG858088
Benzene ND 0.00100 1 03/23/2016 17:36 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 17:36 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 17:36 WG858088
Bromoform ND 0.00100 1 03/23/2016 17:36 WG858088
Bromomethane ND 0.00500 1 03/23/2016 17:36 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 17:36 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 17:36 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 17:36 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 17:36 WG858088
Chloroethane ND 0.00500 1 03/23/2016 17:36 WG858088
Chloroform ND 0.00500 1 03/23/2016 17:36 WG858088
Chloromethane ND 0.00250 1 03/23/2016 17:36 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 17:36 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 17:36 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 17:36 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 17:36 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 17:36 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 17:36 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 17:36 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 17:36 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 17:36 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 17:36 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 17:36 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 17:36 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 17:36 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 17:36 WG858088
Iodomethane ND 0.0100 1 03/23/2016 17:36 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 17:36 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 17:36 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 17:36 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 26 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 26 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L824012
MW-14
Collected date/time: 03/16/16 10:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 17:36 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 17:36 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 17:36 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 17:36 WG858088
Toluene ND 0.00500 1 03/23/2016 17:36 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 17:36 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 17:36 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 17:36 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 17:36 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 17:36 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 17:36 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 17:36 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 17:36 WG858088
(S) Toluene-d8 101 90.0-115 03/23/2016 17:36 WG858088
(S) Dibromofluoromethane 106 79.0-121 03/23/2016 17:36 WG858088
(S) a,a,a-Trifluorotoluene 105 90.4-116 03/23/2016 17:36 WG858088
(S) 4-Bromofluorobenzene 95.8 80.1-120 03/23/2016 17:36 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 16:06 27 of 64
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L824012 03/25/16 19:38 27 of 64
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L824012
MW-15
Collected date/time: 03/16/16 10:50
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0760 0.00500 1 03/18/2016 18:24 WG857404
Chromium ND 0.0100 1 03/18/2016 18:24 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:24 WG857404
Nickel ND 0.0100 1 03/18/2016 18:24 WG857404
Silver ND 0.00500 1 03/18/2016 18:24 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:24 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:04 WG857406
Arsenic ND 0.00200 1 03/20/2016 20:04 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:04 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:04 WG857406
Copper ND 0.00500 1 03/20/2016 20:04 WG857406
Lead ND 0.00200 1 03/20/2016 20:04 WG857406
Selenium ND 0.00200 1 03/20/2016 20:04 WG857406
Thallium ND 0.00200 1 03/20/2016 20:04 WG857406
Zinc ND 0.0250 1 03/20/2016 20:04 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 17:55 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 17:55 WG858088
Benzene 0.00153 0.00100 1 03/23/2016 17:55 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 17:55 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 17:55 WG858088
Bromoform ND 0.00100 1 03/23/2016 17:55 WG858088
Bromomethane ND 0.00500 1 03/23/2016 17:55 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 17:55 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 17:55 WG858088
Chlorobenzene 0.00205 0.00100 1 03/23/2016 17:55 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 17:55 WG858088
Chloroethane ND 0.00500 1 03/23/2016 17:55 WG858088
Chloroform ND 0.00500 1 03/23/2016 17:55 WG858088
Chloromethane ND 0.00250 1 03/23/2016 17:55 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 17:55 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 17:55 WG858088
1,4-Dichlorobenzene 0.00544 0.00100 1 03/23/2016 17:55 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 17:55 WG858088
1,1-Dichloroethane 0.00326 0.00100 1 03/23/2016 17:55 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 17:55 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 17:55 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 17:55 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 17:55 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 17:55 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 17:55 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 17:55 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 17:55 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 17:55 WG858088
Iodomethane ND 0.0100 1 03/23/2016 17:55 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 17:55 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 17:55 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 17:55 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L824012
MW-15
Collected date/time: 03/16/16 10:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 17:55 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 17:55 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 17:55 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 17:55 WG858088
Toluene ND 0.00500 1 03/23/2016 17:55 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 17:55 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 17:55 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 17:55 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 17:55 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 17:55 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 17:55 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 17:55 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 17:55 WG858088
(S) Toluene-d8 103 90.0-115 03/23/2016 17:55 WG858088
(S) Dibromofluoromethane 104 79.0-121 03/23/2016 17:55 WG858088
(S) a,a,a-Trifluorotoluene 103 90.4-116 03/23/2016 17:55 WG858088
(S) 4-Bromofluorobenzene 100 80.1-120 03/23/2016 17:55 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L824012
MW-16
Collected date/time: 03/16/16 11:10
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.282 0.00500 1 03/18/2016 18:28 WG857404
Chromium ND 0.0100 1 03/18/2016 18:28 WG857404
Cobalt 0.0150 0.0100 1 03/18/2016 18:28 WG857404
Nickel ND 0.0100 1 03/18/2016 18:28 WG857404
Silver ND 0.00500 1 03/18/2016 18:28 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:28 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:36 WG857406
Arsenic 0.0114 0.00200 1 03/20/2016 20:36 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:36 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:36 WG857406
Copper ND 0.00500 1 03/20/2016 20:36 WG857406
Lead ND 0.00200 1 03/20/2016 20:36 WG857406
Selenium ND 0.00200 1 03/20/2016 20:36 WG857406
Thallium ND 0.00200 1 03/20/2016 20:36 WG857406
Zinc ND 0.0250 1 03/20/2016 20:36 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 18:13 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 18:13 WG858088
Benzene ND 0.00100 1 03/23/2016 18:13 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 18:13 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 18:13 WG858088
Bromoform ND 0.00100 1 03/23/2016 18:13 WG858088
Bromomethane ND 0.00500 1 03/23/2016 18:13 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 18:13 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 18:13 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 18:13 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 18:13 WG858088
Chloroethane ND 0.00500 1 03/23/2016 18:13 WG858088
Chloroform ND 0.00500 1 03/23/2016 18:13 WG858088
Chloromethane ND 0.00250 1 03/23/2016 18:13 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 18:13 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 18:13 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 18:13 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 18:13 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 18:13 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 18:13 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 18:13 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 18:13 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 18:13 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 18:13 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 18:13 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 18:13 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 18:13 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 18:13 WG858088
Iodomethane ND 0.0100 1 03/23/2016 18:13 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 18:13 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 18:13 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 18:13 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L824012
MW-16
Collected date/time: 03/16/16 11:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 18:13 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 18:13 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 18:13 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 18:13 WG858088
Toluene ND 0.00500 1 03/23/2016 18:13 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 18:13 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 18:13 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 18:13 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 18:13 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 18:13 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 18:13 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 18:13 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 18:13 WG858088
(S) Toluene-d8 101 90.0-115 03/23/2016 18:13 WG858088
(S) Dibromofluoromethane 106 79.0-121 03/23/2016 18:13 WG858088
(S) a,a,a-Trifluorotoluene 105 90.4-116 03/23/2016 18:13 WG858088
(S) 4-Bromofluorobenzene 95.4 80.1-120 03/23/2016 18:13 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L824012
MW-17R
Collected date/time: 03/16/16 11:50
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.128 0.00500 1 03/18/2016 18:31 WG857404
Chromium 0.0109 0.0100 1 03/18/2016 18:31 WG857404
Cobalt 0.0130 0.0100 1 03/18/2016 18:31 WG857404
Nickel ND 0.0100 1 03/18/2016 18:31 WG857404
Silver ND 0.00500 1 03/18/2016 18:31 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:31 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:39 WG857406
Arsenic ND 0.00200 1 03/20/2016 20:39 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:39 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:39 WG857406
Copper ND 0.00500 1 03/20/2016 20:39 WG857406
Lead 0.00480 0.00200 1 03/20/2016 20:39 WG857406
Selenium ND 0.00200 1 03/20/2016 20:39 WG857406
Thallium ND 0.00200 1 03/20/2016 20:39 WG857406
Zinc ND 0.0250 1 03/20/2016 20:39 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 18:31 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 18:31 WG858088
Benzene ND 0.00100 1 03/23/2016 18:31 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 18:31 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 18:31 WG858088
Bromoform ND 0.00100 1 03/23/2016 18:31 WG858088
Bromomethane ND 0.00500 1 03/23/2016 18:31 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 18:31 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 18:31 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 18:31 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 18:31 WG858088
Chloroethane ND 0.00500 1 03/23/2016 18:31 WG858088
Chloroform ND 0.00500 1 03/23/2016 18:31 WG858088
Chloromethane ND 0.00250 1 03/23/2016 18:31 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 18:31 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 18:31 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 18:31 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 18:31 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 18:31 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 18:31 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 18:31 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 18:31 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 18:31 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 18:31 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 18:31 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 18:31 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 18:31 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 18:31 WG858088
Iodomethane ND 0.0100 1 03/23/2016 18:31 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 18:31 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 18:31 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 18:31 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L824012
MW-17R
Collected date/time: 03/16/16 11:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 18:31 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 18:31 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 18:31 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 18:31 WG858088
Toluene ND 0.00500 1 03/23/2016 18:31 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 18:31 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 18:31 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 18:31 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 18:31 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 18:31 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 18:31 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 18:31 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 18:31 WG858088
(S) Toluene-d8 99.3 90.0-115 03/23/2016 18:31 WG858088
(S) Dibromofluoromethane 104 79.0-121 03/23/2016 18:31 WG858088
(S) a,a,a-Trifluorotoluene 103 90.4-116 03/23/2016 18:31 WG858088
(S) 4-Bromofluorobenzene 97.7 80.1-120 03/23/2016 18:31 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L824012
MW-18
Collected date/time: 03/16/16 11:40
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.123 0.00500 1 03/18/2016 18:34 WG857404
Chromium ND 0.0100 1 03/18/2016 18:34 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:34 WG857404
Nickel ND 0.0100 1 03/18/2016 18:34 WG857404
Silver ND 0.00500 1 03/18/2016 18:34 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:34 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:42 WG857406
Arsenic ND 0.00200 1 03/20/2016 20:42 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:42 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:42 WG857406
Copper ND 0.00500 1 03/20/2016 20:42 WG857406
Lead 0.00391 0.00200 1 03/20/2016 20:42 WG857406
Selenium ND 0.00200 1 03/20/2016 20:42 WG857406
Thallium ND 0.00200 1 03/20/2016 20:42 WG857406
Zinc ND 0.0250 1 03/20/2016 20:42 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 18:49 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 18:49 WG858088
Benzene ND 0.00100 1 03/23/2016 18:49 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 18:49 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 18:49 WG858088
Bromoform ND 0.00100 1 03/23/2016 18:49 WG858088
Bromomethane ND 0.00500 1 03/23/2016 18:49 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 18:49 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 18:49 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 18:49 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 18:49 WG858088
Chloroethane ND 0.00500 1 03/23/2016 18:49 WG858088
Chloroform ND 0.00500 1 03/23/2016 18:49 WG858088
Chloromethane ND 0.00250 1 03/23/2016 18:49 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 18:49 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 18:49 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 18:49 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 18:49 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 18:49 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 18:49 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 18:49 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 18:49 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 18:49 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 18:49 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 18:49 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 18:49 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 18:49 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 18:49 WG858088
Iodomethane ND 0.0100 1 03/23/2016 18:49 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 18:49 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 18:49 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 18:49 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L824012
MW-18
Collected date/time: 03/16/16 11:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 18:49 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 18:49 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 18:49 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 18:49 WG858088
Toluene ND 0.00500 1 03/23/2016 18:49 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 18:49 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 18:49 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 18:49 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 18:49 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 18:49 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 18:49 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 18:49 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 18:49 WG858088
(S) Toluene-d8 102 90.0-115 03/23/2016 18:49 WG858088
(S) Dibromofluoromethane 100 79.0-121 03/23/2016 18:49 WG858088
(S) a,a,a-Trifluorotoluene 102 90.4-116 03/23/2016 18:49 WG858088
(S) 4-Bromofluorobenzene 96.4 80.1-120 03/23/2016 18:49 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L824012
MW-19
Collected date/time: 03/16/16 12:30
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 108 10.0 1 03/21/2016 17:35 WG857757
Wet Chemistry by Method 2320 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Alkalinity ND 20.0 1 03/25/2016 09:29 WG858403
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chloride 1.20 1.00 1 03/21/2016 14:42 WG857779
Sulfate 8.12 5.00 1 03/21/2016 14:42 WG857779
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0520 0.00500 1 03/18/2016 18:43 WG857404
Chromium 0.0118 0.0100 1 03/18/2016 18:43 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:43 WG857404
Nickel ND 0.0100 1 03/18/2016 18:43 WG857404
Silver ND 0.00500 1 03/18/2016 18:43 WG857404
Vanadium 0.0215 0.0200 1 03/18/2016 18:43 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:44 WG857406
Arsenic ND 0.00200 1 03/20/2016 20:44 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:44 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:44 WG857406
Copper ND 0.00500 1 03/20/2016 20:44 WG857406
Lead 0.00778 0.00200 1 03/20/2016 20:44 WG857406
Selenium ND 0.00200 1 03/20/2016 20:44 WG857406
Thallium ND 0.00200 1 03/20/2016 20:44 WG857406
Zinc ND 0.0250 1 03/20/2016 20:44 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 19:08 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 19:08 WG858088
Benzene ND 0.00100 1 03/23/2016 19:08 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 19:08 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 19:08 WG858088
Bromoform ND 0.00100 1 03/23/2016 19:08 WG858088
Bromomethane ND 0.00500 1 03/23/2016 19:08 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 19:08 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 19:08 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 19:08 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 19:08 WG858088
Chloroethane ND 0.00500 1 03/23/2016 19:08 WG858088
Chloroform ND 0.00500 1 03/23/2016 19:08 WG858088
Chloromethane ND 0.00250 1 03/23/2016 19:08 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L824012
MW-19
Collected date/time: 03/16/16 12:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dibromomethane ND 0.00100 1 03/23/2016 19:08 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 19:08 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 19:08 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 19:08 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 19:08 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 19:08 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 19:08 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 19:08 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 19:08 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 19:08 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 19:08 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 19:08 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 19:08 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 19:08 WG858088
Iodomethane ND 0.0100 1 03/23/2016 19:08 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 19:08 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 19:08 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 19:08 WG858088
Styrene ND 0.00100 1 03/23/2016 19:08 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 19:08 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 19:08 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 19:08 WG858088
Toluene ND 0.00500 1 03/23/2016 19:08 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 19:08 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 19:08 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 19:08 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 19:08 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 19:08 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 19:08 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 19:08 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 19:08 WG858088
(S) Toluene-d8 102 90.0-115 03/23/2016 19:08 WG858088
(S) Dibromofluoromethane 106 79.0-121 03/23/2016 19:08 WG858088
(S) a,a,a-Trifluorotoluene 100 90.4-116 03/23/2016 19:08 WG858088
(S) 4-Bromofluorobenzene 93.2 80.1-120 03/23/2016 19:08 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L824012
MW-20
Collected date/time: 03/16/16 12:45
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 77.0 10.0 1 03/21/2016 17:35 WG857757
Wet Chemistry by Method 2320 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Alkalinity ND 20.0 1 03/25/2016 09:36 WG858403
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chloride 4.19 1.00 1 03/21/2016 14:59 WG857779
Sulfate 14.7 5.00 1 03/21/2016 14:59 WG857779
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.130 0.00500 1 03/18/2016 18:46 WG857404
Chromium 0.0243 0.0100 1 03/18/2016 18:46 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:46 WG857404
Nickel ND 0.0100 1 03/18/2016 18:46 WG857404
Silver ND 0.00500 1 03/18/2016 18:46 WG857404
Vanadium 0.0416 0.0200 1 03/18/2016 18:46 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:46 WG857406
Arsenic 0.00230 0.00200 1 03/20/2016 20:46 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:46 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:46 WG857406
Copper ND 0.00500 1 03/20/2016 20:46 WG857406
Lead 0.0102 0.00200 1 03/20/2016 20:46 WG857406
Selenium ND 0.00200 1 03/20/2016 20:46 WG857406
Thallium ND 0.00200 1 03/20/2016 20:46 WG857406
Zinc ND 0.0250 1 03/20/2016 20:46 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 19:26 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 19:26 WG858088
Benzene ND 0.00100 1 03/23/2016 19:26 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 19:26 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 19:26 WG858088
Bromoform ND 0.00100 1 03/23/2016 19:26 WG858088
Bromomethane ND 0.00500 1 03/23/2016 19:26 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 19:26 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 19:26 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 19:26 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 19:26 WG858088
Chloroethane ND 0.00500 1 03/23/2016 19:26 WG858088
Chloroform ND 0.00500 1 03/23/2016 19:26 WG858088
Chloromethane ND 0.00250 1 03/23/2016 19:26 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L824012
MW-20
Collected date/time: 03/16/16 12:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dibromomethane ND 0.00100 1 03/23/2016 19:26 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 19:26 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 19:26 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 19:26 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 19:26 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 19:26 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 19:26 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 19:26 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 19:26 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 19:26 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 19:26 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 19:26 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 19:26 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 19:26 WG858088
Iodomethane ND 0.0100 1 03/23/2016 19:26 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 19:26 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 19:26 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 19:26 WG858088
Styrene ND 0.00100 1 03/23/2016 19:26 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 19:26 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 19:26 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 19:26 WG858088
Toluene ND 0.00500 1 03/23/2016 19:26 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 19:26 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 19:26 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 19:26 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 19:26 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 19:26 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 19:26 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 19:26 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 19:26 WG858088
(S) Toluene-d8 98.1 90.0-115 03/23/2016 19:26 WG858088
(S) Dibromofluoromethane 107 79.0-121 03/23/2016 19:26 WG858088
(S) a,a,a-Trifluorotoluene 101 90.4-116 03/23/2016 19:26 WG858088
(S) 4-Bromofluorobenzene 94.7 80.1-120 03/23/2016 19:26 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L824012
MW-21R
Collected date/time: 03/16/16 10:00
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.161 0.00500 1 03/18/2016 18:49 WG857404
Chromium ND 0.0100 1 03/18/2016 18:49 WG857404
Cobalt 0.0172 0.0100 1 03/18/2016 18:49 WG857404
Nickel ND 0.0100 1 03/18/2016 18:49 WG857404
Silver ND 0.00500 1 03/18/2016 18:49 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:49 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:49 WG857406
Arsenic 0.0533 0.00200 1 03/20/2016 20:49 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:49 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:49 WG857406
Copper 0.0192 0.00500 1 03/20/2016 20:49 WG857406
Lead 0.00895 0.00200 1 03/20/2016 20:49 WG857406
Selenium ND 0.00200 1 03/20/2016 20:49 WG857406
Thallium ND 0.00200 1 03/20/2016 20:49 WG857406
Zinc ND 0.0250 1 03/20/2016 20:49 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone 2.95 0.500 10 03/24/2016 06:02 WG858884
Acrylonitrile ND 0.0100 1 03/23/2016 19:45 WG858088
Benzene ND 0.00100 1 03/23/2016 19:45 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 19:45 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 19:45 WG858088
Bromoform ND 0.00100 1 03/23/2016 19:45 WG858088
Bromomethane ND 0.00500 1 03/23/2016 19:45 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 19:45 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 19:45 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 19:45 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 19:45 WG858088
Chloroethane ND 0.00500 1 03/23/2016 19:45 WG858088
Chloroform ND 0.00500 1 03/23/2016 19:45 WG858088
Chloromethane ND 0.00250 1 03/23/2016 19:45 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 19:45 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 19:45 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 19:45 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 19:45 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 19:45 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 19:45 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 19:45 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 19:45 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 19:45 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 19:45 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 19:45 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 19:45 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 19:45 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 19:45 WG858088
Iodomethane ND 0.0100 1 03/23/2016 19:45 WG858088
2-Butanone (MEK)0.0763 0.0100 1 03/23/2016 19:45 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 19:45 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 19:45 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L824012
MW-21R
Collected date/time: 03/16/16 10:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 19:45 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 19:45 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 19:45 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 19:45 WG858088
Toluene ND 0.00500 1 03/23/2016 19:45 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 19:45 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 19:45 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 19:45 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 19:45 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 19:45 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 19:45 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 19:45 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 19:45 WG858088
(S) Toluene-d8 100 90.0-115 03/23/2016 19:45 WG858088
(S) Dibromofluoromethane 102 79.0-121 03/23/2016 19:45 WG858088
(S) a,a,a-Trifluorotoluene 100 90.4-116 03/23/2016 19:45 WG858088
(S) 4-Bromofluorobenzene 102 80.1-120 03/23/2016 19:45 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L824012
MW-22
Collected date/time: 03/16/16 10:15
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0534 0.00500 1 03/18/2016 18:52 WG857404
Chromium ND 0.0100 1 03/18/2016 18:52 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:52 WG857404
Nickel ND 0.0100 1 03/18/2016 18:52 WG857404
Silver ND 0.00500 1 03/18/2016 18:52 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:52 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:51 WG857406
Arsenic ND 0.00200 1 03/20/2016 20:51 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:51 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:51 WG857406
Copper 0.00511 0.00500 1 03/20/2016 20:51 WG857406
Lead ND 0.00200 1 03/20/2016 20:51 WG857406
Selenium ND 0.00200 1 03/20/2016 20:51 WG857406
Thallium ND 0.00200 1 03/20/2016 20:51 WG857406
Zinc ND 0.0250 1 03/20/2016 20:51 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/24/2016 06:25 WG858884
Acrylonitrile ND 0.0100 1 03/23/2016 20:03 WG858088
Benzene ND 0.00100 1 03/23/2016 20:03 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 20:03 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 20:03 WG858088
Bromoform ND 0.00100 1 03/23/2016 20:03 WG858088
Bromomethane ND 0.00500 1 03/23/2016 20:03 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 20:03 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 20:03 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 20:03 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 20:03 WG858088
Chloroethane ND 0.00500 1 03/23/2016 20:03 WG858088
Chloroform ND 0.00500 1 03/23/2016 20:03 WG858088
Chloromethane ND 0.00250 1 03/23/2016 20:03 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 20:03 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 20:03 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 20:03 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 20:03 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 20:03 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 20:03 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 20:03 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 20:03 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 20:03 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 20:03 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 20:03 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 20:03 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 20:03 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 20:03 WG858088
Iodomethane ND 0.0100 1 03/23/2016 20:03 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 20:03 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 20:03 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 20:03 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L824012
MW-22
Collected date/time: 03/16/16 10:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 20:03 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 20:03 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 20:03 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 20:03 WG858088
Toluene ND 0.00500 1 03/23/2016 20:03 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 20:03 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 20:03 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 20:03 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 20:03 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 20:03 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 20:03 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 20:03 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 20:03 WG858088
(S) Toluene-d8 103 90.0-115 03/23/2016 20:03 WG858088
(S) Dibromofluoromethane 105 79.0-121 03/23/2016 20:03 WG858088
(S) a,a,a-Trifluorotoluene 102 90.4-116 03/23/2016 20:03 WG858088
(S) 4-Bromofluorobenzene 95.0 80.1-120 03/23/2016 20:03 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L824012
MW-23
Collected date/time: 03/16/16 09:40
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.00907 0.00500 1 03/18/2016 18:55 WG857404
Chromium ND 0.0100 1 03/18/2016 18:55 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:55 WG857404
Nickel ND 0.0100 1 03/18/2016 18:55 WG857404
Silver ND 0.00500 1 03/18/2016 18:55 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:55 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:54 WG857406
Arsenic ND 0.00200 1 03/20/2016 20:54 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:54 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:54 WG857406
Copper ND 0.00500 1 03/20/2016 20:54 WG857406
Lead ND 0.00200 1 03/20/2016 20:54 WG857406
Selenium ND 0.00200 1 03/20/2016 20:54 WG857406
Thallium ND 0.00200 1 03/20/2016 20:54 WG857406
Zinc ND 0.0250 1 03/20/2016 20:54 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 20:21 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 20:21 WG858088
Benzene ND 0.00100 1 03/23/2016 20:21 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 20:21 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 20:21 WG858088
Bromoform ND 0.00100 1 03/23/2016 20:21 WG858088
Bromomethane ND 0.00500 1 03/23/2016 20:21 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 20:21 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 20:21 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 20:21 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 20:21 WG858088
Chloroethane ND 0.00500 1 03/23/2016 20:21 WG858088
Chloroform ND 0.00500 1 03/23/2016 20:21 WG858088
Chloromethane ND 0.00250 1 03/23/2016 20:21 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 20:21 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 20:21 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 20:21 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 20:21 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 20:21 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 20:21 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 20:21 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 20:21 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 20:21 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 20:21 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 20:21 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 20:21 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 20:21 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 20:21 WG858088
Iodomethane ND 0.0100 1 03/23/2016 20:21 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 20:21 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 20:21 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 20:21 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L824012
MW-23
Collected date/time: 03/16/16 09:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 20:21 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 20:21 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 20:21 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 20:21 WG858088
Toluene ND 0.00500 1 03/23/2016 20:21 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 20:21 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 20:21 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 20:21 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 20:21 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 20:21 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 20:21 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 20:21 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 20:21 WG858088
(S) Toluene-d8 102 90.0-115 03/23/2016 20:21 WG858088
(S) Dibromofluoromethane 108 79.0-121 03/23/2016 20:21 WG858088
(S) a,a,a-Trifluorotoluene 101 90.4-116 03/23/2016 20:21 WG858088
(S) 4-Bromofluorobenzene 96.2 80.1-120 03/23/2016 20:21 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L824012
MW-24R
Collected date/time: 03/16/16 09:20
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0414 0.00500 1 03/18/2016 18:59 WG857404
Chromium ND 0.0100 1 03/18/2016 18:59 WG857404
Cobalt ND 0.0100 1 03/18/2016 18:59 WG857404
Nickel ND 0.0100 1 03/18/2016 18:59 WG857404
Silver ND 0.00500 1 03/18/2016 18:59 WG857404
Vanadium ND 0.0200 1 03/18/2016 18:59 WG857404
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/20/2016 20:56 WG857406
Arsenic ND 0.00200 1 03/20/2016 20:56 WG857406
Beryllium ND 0.00200 1 03/20/2016 20:56 WG857406
Cadmium ND 0.00100 1 03/20/2016 20:56 WG857406
Copper ND 0.00500 1 03/20/2016 20:56 WG857406
Lead 0.00207 0.00200 1 03/20/2016 20:56 WG857406
Selenium ND 0.00200 1 03/20/2016 20:56 WG857406
Thallium ND 0.00200 1 03/20/2016 20:56 WG857406
Zinc ND 0.0250 1 03/20/2016 20:56 WG857406
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/23/2016 14:34 WG858088
Acrylonitrile ND 0.0100 1 03/23/2016 14:34 WG858088
Benzene ND 0.00100 1 03/23/2016 14:34 WG858088
Bromochloromethane ND 0.00100 1 03/23/2016 14:34 WG858088
Bromodichloromethane ND 0.00100 1 03/23/2016 14:34 WG858088
Bromoform ND 0.00100 1 03/23/2016 14:34 WG858088
Bromomethane ND 0.00500 1 03/23/2016 14:34 WG858088
Carbon disulfide ND 0.00100 1 03/23/2016 14:34 WG858088
Carbon tetrachloride ND 0.00100 1 03/23/2016 14:34 WG858088
Chlorobenzene ND 0.00100 1 03/23/2016 14:34 WG858088
Chlorodibromomethane ND 0.00100 1 03/23/2016 14:34 WG858088
Chloroethane ND 0.00500 1 03/23/2016 14:34 WG858088
Chloroform ND 0.00500 1 03/23/2016 14:34 WG858088
Chloromethane ND 0.00250 1 03/23/2016 14:34 WG858088
Dibromomethane ND 0.00100 1 03/23/2016 14:34 WG858088
1,2-Dichlorobenzene ND 0.00100 1 03/23/2016 14:34 WG858088
1,4-Dichlorobenzene ND 0.00100 1 03/23/2016 14:34 WG858088
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/23/2016 14:34 WG858088
1,1-Dichloroethane ND 0.00100 1 03/23/2016 14:34 WG858088
1,2-Dichloroethane ND 0.00100 1 03/23/2016 14:34 WG858088
1,1-Dichloroethene ND 0.00100 1 03/23/2016 14:34 WG858088
cis-1,2-Dichloroethene ND 0.00100 1 03/23/2016 14:34 WG858088
trans-1,2-Dichloroethene ND 0.00100 1 03/23/2016 14:34 WG858088
1,2-Dichloropropane ND 0.00100 1 03/23/2016 14:34 WG858088
cis-1,3-Dichloropropene ND 0.00100 1 03/23/2016 14:34 WG858088
trans-1,3-Dichloropropene ND 0.00100 1 03/23/2016 14:34 WG858088
Ethylbenzene ND 0.00100 1 03/23/2016 14:34 WG858088
2-Hexanone ND 0.0100 1 03/23/2016 14:34 WG858088
Iodomethane ND 0.0100 1 03/23/2016 14:34 WG858088
2-Butanone (MEK)ND 0.0100 1 03/23/2016 14:34 WG858088
Methylene Chloride ND 0.00500 1 03/23/2016 14:34 WG858088
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/23/2016 14:34 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L824012
MW-24R
Collected date/time: 03/16/16 09:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/23/2016 14:34 WG858088
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/23/2016 14:34 WG858088
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/23/2016 14:34 WG858088
Tetrachloroethene ND 0.00100 1 03/23/2016 14:34 WG858088
Toluene ND 0.00500 1 03/23/2016 14:34 WG858088
1,1,1-Trichloroethane ND 0.00100 1 03/23/2016 14:34 WG858088
1,1,2-Trichloroethane ND 0.00100 1 03/23/2016 14:34 WG858088
Trichloroethene ND 0.00100 1 03/23/2016 14:34 WG858088
Trichlorofluoromethane ND 0.00500 1 03/23/2016 14:34 WG858088
1,2,3-Trichloropropane ND 0.00250 1 03/23/2016 14:34 WG858088
Vinyl acetate ND 0.0100 1 03/23/2016 14:34 WG858088
Vinyl chloride ND 0.00100 1 03/23/2016 14:34 WG858088
Xylenes, Total ND 0.00300 1 03/23/2016 14:34 WG858088
(S) Toluene-d8 104 90.0-115 03/23/2016 14:34 WG858088
(S) Dibromofluoromethane 107 79.0-121 03/23/2016 14:34 WG858088
(S) a,a,a-Trifluorotoluene 105 90.4-116 03/23/2016 14:34 WG858088
(S) 4-Bromofluorobenzene 102 80.1-120 03/23/2016 14:34 WG858088
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857757
Gravimetric Analysis by Method 2540 C-2011 L824012-15,16
Method Blank (MB)
(MB) R3123047-1 03/21/16 17:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Dissolved Solids U 2.82 10.0
Original Sample (OS) • Duplicate (DUP)
(OS) L823925-01 03/21/16 17:35 • (DUP) R3123047-4 03/21/16 17:35
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Dissolved Solids 183 187 1 2.16 5
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3123047-2 03/21/16 17:35 • (LCSD) R3123047-3 03/21/16 17:35
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Dissolved Solids 8800 8810 8790 100 99.9 85.0-115 0.227 5
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG858403
Wet Chemistry by Method 2320 B-2011 L824012-15,16
Method Blank (MB)
(MB) R3123815-3 03/25/16 08:48
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Alkalinity U 2.61 20.0
Original Sample (OS) • Duplicate (DUP)
(OS) L823430-01 03/25/16 08:55 • (DUP) R3123815-4 03/25/16 09:03
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Alkalinity 53.5 54.5 1 1.85 20
Original Sample (OS) • Duplicate (DUP)
(OS) L823867-03 03/25/16 10:55 • (DUP) R3123815-6 03/25/16 11:01
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Alkalinity 348 352 1 1.14 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3123815-5 03/25/16 09:55 • (LCSD) R3123815-7 03/25/16 11:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Alkalinity 100 96.7 97.7 96.7 97.7 85.0-115 1.01 20
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L823914-01 03/25/16 12:21 • (MS) R3123815-8 03/25/16 12:33 • (MSD) R3123815-9 03/25/16 12:43
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Alkalinity 100 1530 1470 1470 -57.5 59.2 1 80.0-120 V V 0.114 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857779
Wet Chemistry by Method 9056A L824012-15,16
Method Blank (MB)
(MB) R3122814-1 03/21/16 12:44
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Chloride U 0.0519 1.00
Sulfate U 0.0774 5.00
Original Sample (OS) • Duplicate (DUP)
(OS) L824225-02 03/21/16 16:07 • (DUP) R3122814-5 03/21/16 16:24
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Chloride 100 99.0 10 1 15
Sulfate 21.5 81.2 10 116 P1 15
Original Sample (OS) • Duplicate (DUP)
(OS) L824282-05 03/21/16 18:39 • (DUP) R3122814-6 03/21/16 18:56
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Chloride 0.993 1.00 1 1 15
Sulfate 0.329 0.314 1 0 J 15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3122814-2 03/21/16 13:01 • (LCSD) R3122814-3 03/21/16 13:18
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Chloride 40.0 39.7 39.8 99 99 80-120 0 15
Sulfate 40.0 37.8 37.9 94 95 80-120 0 15
Original Sample (OS) • Matrix Spike (MS)
(OS) L824225-01 03/21/16 15:33 • (MS) R3122814-4 03/21/16 15:50
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Chloride 50.0 18.8 68.7 100 1 80-120
Sulfate 50.0 8.20 54.1 92 1 80-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857779
Wet Chemistry by Method 9056A L824012-15,16
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L824282-06 03/21/16 19:13 • (MS) R3122814-7 03/21/16 19:30 • (MSD) R3122814-8 03/21/16 19:47
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Chloride 50.0 1.55 51.9 51.8 101 100 1 80-120 0 15
Sulfate 50.0 2.08 52.9 52.5 102 101 1 80-120 1 15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857404
Metals (ICP) by Method 6010C L824012-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3122238-1 03/18/16 17:29
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Barium U 0.0017 0.00500
Chromium U 0.0014 0.0100
Cobalt U 0.0023 0.0100
Nickel U 0.0049 0.0100
Silver U 0.0028 0.00500
Vanadium U 0.0024 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3122238-2 03/18/16 17:32 • (LCSD) R3122238-3 03/18/16 17:35
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Barium 1.00 1.04 1.04 104 104 80-120 0 20
Chromium 1.00 1.06 1.07 106 107 80-120 0 20
Cobalt 1.00 1.07 1.06 107 106 80-120 0 20
Nickel 1.00 1.06 1.06 106 106 80-120 0 20
Silver 1.00 0.997 1.00 100 100 80-120 0 20
Vanadium 1.00 1.07 1.07 107 107 80-120 0 20
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L824012-03 03/18/16 17:38 • (MS) R3122238-5 03/18/16 17:44 • (MSD) R3122238-6 03/18/16 17:47
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Barium 1.00 0.0126 1.07 1.06 106 105 1 75-125 1 20
Chromium 1.00 0.00172 1.10 1.10 110 110 1 75-125 0 20
Cobalt 1.00 0.00137 1.08 1.07 108 107 1 75-125 1 20
Nickel 1.00 0.000539 1.08 1.07 108 107 1 75-125 1 20
Silver 1.00 0.000190 1.02 1.02 102 102 1 75-125 1 20
Vanadium 1.00 0.00247 1.06 1.05 106 105 1 75-125 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857406
Metals (ICPMS) by Method 6020 L824012-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3122331-1 03/20/16 18:44
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.00021 0.00200
Arsenic U 0.00025 0.00200
Beryllium U 0.00012 0.00200
Cadmium U 0.00016 0.00100
Copper 0.00106 0.00052 0.00500
Lead U 0.00024 0.00200
Selenium U 0.00038 0.00200
Thallium U 0.00019 0.00200
Zinc U 0.00256 0.0250
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3122331-2 03/20/16 18:46 • (LCSD) R3122331-3 03/20/16 18:48
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Antimony 0.0500 0.0512 0.0532 102 106 80-120 4 20
Arsenic 0.0500 0.0508 0.0490 102 98 80-120 4 20
Beryllium 0.0500 0.0504 0.0502 101 100 80-120 0 20
Cadmium 0.0500 0.0515 0.0500 103 100 80-120 3 20
Copper 0.0500 0.0528 0.0529 106 106 80-120 0 20
Lead 0.0500 0.0494 0.0498 99 100 80-120 1 20
Selenium 0.0500 0.0512 0.0507 102 101 80-120 1 20
Thallium 0.0500 0.0491 0.0494 98 99 80-120 1 20
Zinc 0.0500 0.0498 0.0478 100 96 80-120 4 20
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L824012-04 03/20/16 18:51 • (MS) R3122331-5 03/20/16 18:56 • (MSD) R3122331-6 03/20/16 18:58
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 0.0500 0.000298 0.0529 0.0546 105 109 1 75-125 3 20
Arsenic 0.0500 0.00347 0.0525 0.0526 98 98 1 75-125 0 20
Beryllium 0.0500 0.000115 0.0474 0.0499 95 100 1 75-125 5 20
Cadmium 0.0500 0.00000982 0.0496 0.0493 99 99 1 75-125 1 20
Copper 0.0500 0.000893 0.0490 0.0497 96 98 1 75-125 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857406
Metals (ICPMS) by Method 6020 L824012-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L824012-04 03/20/16 18:51 • (MS) R3122331-5 03/20/16 18:56 • (MSD) R3122331-6 03/20/16 18:58
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Lead 0.0500 0.00134 0.0510 0.0533 99 104 1 75-125 4 20
Selenium 0.0500 0.00103 0.0502 0.0524 98 103 1 75-125 4 20
Thallium 0.0500 0.000419 0.0489 0.0508 97 101 1 75-125 4 20
Zinc 0.0500 0.00266 0.0496 0.0491 94 93 1 75-125 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG858088
Volatile Organic Compounds (GC/MS) by Method 8260B L824012-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3123285-3 03/23/16 12:32
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00187 0.0100
Benzene U 0.000331 0.00100
Bromodichloromethane U 0.000380 0.00100
Bromochloromethane U 0.000520 0.00100
Bromoform U 0.000469 0.00100
Bromomethane U 0.000866 0.00500
Carbon disulfide U 0.000275 0.00100
Carbon tetrachloride U 0.000379 0.00100
Chlorobenzene U 0.000348 0.00100
Chlorodibromomethane U 0.000327 0.00100
Chloroethane U 0.000453 0.00500
Chloroform U 0.000324 0.00500
Chloromethane U 0.000276 0.00250
Dibromomethane U 0.000346 0.00100
1,2-Dichlorobenzene U 0.000349 0.00100
1,4-Dichlorobenzene U 0.000274 0.00100
trans-1,4-Dichloro-2-butene U 0.000866 0.00250
1,1-Dichloroethane U 0.000259 0.00100
1,2-Dichloroethane U 0.000361 0.00100
1,1-Dichloroethene U 0.000398 0.00100
cis-1,2-Dichloroethene U 0.000260 0.00100
trans-1,2-Dichloroethene U 0.000396 0.00100
1,2-Dichloropropane U 0.000306 0.00100
cis-1,3-Dichloropropene U 0.000418 0.00100
trans-1,3-Dichloropropene U 0.000419 0.00100
Ethylbenzene U 0.000384 0.00100
2-Hexanone U 0.00382 0.0100
Iodomethane U 0.00171 0.0100
2-Butanone (MEK)U 0.00393 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100
Styrene U 0.000307 0.00100
1,1,1,2-Tetrachloroethane U 0.000385 0.00100
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
Tetrachloroethene U 0.000372 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG858088
Volatile Organic Compounds (GC/MS) by Method 8260B L824012-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3123285-3 03/23/16 12:32
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Toluene U 0.000780 0.00500
1,1,1-Trichloroethane U 0.000319 0.00100
1,1,2-Trichloroethane U 0.000383 0.00100
Trichloroethene U 0.000398 0.00100
Trichlorofluoromethane U 0.00120 0.00500
1,2,3-Trichloropropane U 0.000807 0.00250
Vinyl acetate U 0.00163 0.0100
Vinyl chloride U 0.000259 0.00100
Xylenes, Total U 0.00106 0.00300
(S) Toluene-d8 102 90.0-115
(S) Dibromofluoromethane 104 79.0-121
(S) a,a,a-Trifluorotoluene 101 90.4-116
(S) 4-Bromofluorobenzene 98.8 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3123285-1 03/23/16 11:00 • (LCSD) R3123285-2 03/23/16 11:19
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.125 0.0714 0.0771 57.1 61.7 28.7-175 7.67 20.9
Acrylonitrile 0.125 0.136 0.112 108 89.9 58.2-145 18.7 20
Benzene 0.0250 0.0225 0.0225 90.0 89.9 73.0-122 0.0500 20
Bromodichloromethane 0.0250 0.0239 0.0236 95.7 94.5 75.5-121 1.28 20
Bromochloromethane 0.0250 0.0242 0.0237 96.7 94.9 78.9-123 1.89 20
Bromoform 0.0250 0.0230 0.0234 92.1 93.6 71.5-131 1.70 20
Bromomethane 0.0250 0.0386 0.0365 154 146 22.4-187 5.66 20
Carbon disulfide 0.0250 0.0253 0.0242 101 96.9 53.0-134 4.54 20
Carbon tetrachloride 0.0250 0.0218 0.0217 87.1 86.8 70.9-129 0.400 20
Chlorobenzene 0.0250 0.0222 0.0221 88.9 88.6 79.7-122 0.350 20
Chlorodibromomethane 0.0250 0.0236 0.0242 94.6 96.7 78.2-124 2.23 20
Chloroethane 0.0250 0.0302 0.0287 121 115 41.2-153 5.11 20
Chloroform 0.0250 0.0239 0.0240 95.4 95.9 73.2-125 0.500 20
Chloromethane 0.0250 0.0245 0.0246 97.9 98.3 55.8-134 0.470 20
Dibromomethane 0.0250 0.0251 0.0243 100 97.4 79.5-118 3.00 20
1,2-Dichlorobenzene 0.0250 0.0233 0.0218 93.0 87.1 84.7-118 6.61 20
1,4-Dichlorobenzene 0.0250 0.0224 0.0225 89.7 89.9 82.2-114 0.220 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG858088
Volatile Organic Compounds (GC/MS) by Method 8260B L824012-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3123285-1 03/23/16 11:00 • (LCSD) R3123285-2 03/23/16 11:19
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
trans-1,4-Dichloro-2-butene 0.0250 0.0255 0.0250 102 99.8 58.3-129 2.21 20
1,1-Dichloroethane 0.0250 0.0236 0.0231 94.2 92.5 71.7-127 1.81 20
1,2-Dichloroethane 0.0250 0.0250 0.0242 100 96.7 65.3-126 3.44 20
1,1-Dichloroethene 0.0250 0.0259 0.0253 104 101 59.9-137 2.42 20
cis-1,2-Dichloroethene 0.0250 0.0233 0.0233 93.3 93.1 77.3-122 0.260 20
trans-1,2-Dichloroethene 0.0250 0.0244 0.0239 97.7 95.5 72.6-125 2.31 20
1,2-Dichloropropane 0.0250 0.0233 0.0229 93.1 91.5 77.4-125 1.72 20
cis-1,3-Dichloropropene 0.0250 0.0249 0.0246 99.8 98.6 77.7-124 1.21 20
trans-1,3-Dichloropropene 0.0250 0.0262 0.0249 105 99.8 73.5-127 4.77 20
Ethylbenzene 0.0250 0.0215 0.0215 86.0 86.0 80.9-121 0.0100 20
2-Hexanone 0.125 0.128 0.127 102 102 59.4-151 0.500 20
Iodomethane 0.125 0.130 0.125 104 100 64.6-137 3.66 20
2-Butanone (MEK)0.125 0.112 0.109 89.6 86.9 46.4-155 3.05 20
Methylene Chloride 0.0250 0.0223 0.0225 89.1 89.9 69.5-120 0.890 20
4-Methyl-2-pentanone (MIBK)0.125 0.135 0.132 108 106 63.3-138 1.96 20
Styrene 0.0250 0.0222 0.0227 88.8 90.7 79.9-124 2.21 20
1,1,1,2-Tetrachloroethane 0.0250 0.0230 0.0228 92.0 91.1 78.5-125 1.02 20
1,1,2,2-Tetrachloroethane 0.0250 0.0224 0.0231 89.4 92.6 79.3-123 3.50 20
Tetrachloroethene 0.0250 0.0217 0.0211 86.8 84.5 73.5-130 2.70 20
Toluene 0.0250 0.0219 0.0222 87.6 88.9 77.9-116 1.45 20
1,1,1-Trichloroethane 0.0250 0.0233 0.0228 93.4 91.3 71.1-129 2.21 20
1,1,2-Trichloroethane 0.0250 0.0244 0.0234 97.7 93.8 81.6-120 4.09 20
Trichloroethene 0.0250 0.0233 0.0233 93.2 93.2 79.5-121 0.0100 20
Trichlorofluoromethane 0.0250 0.0240 0.0250 96.0 99.9 49.1-157 4.00 20
1,2,3-Trichloropropane 0.0250 0.0235 0.0244 94.0 97.8 74.9-124 3.90 20
Vinyl acetate 0.125 0.112 0.109 90.0 87.3 41.7-159 3.01 20
Vinyl chloride 0.0250 0.0274 0.0270 110 108 61.5-134 1.54 20
Xylenes, Total 0.0750 0.0662 0.0673 88.2 89.7 79.2-122 1.69 20
(S) Toluene-d8 103 105 90.0-115
(S) Dibromofluoromethane 104 102 79.0-121
(S) a,a,a-Trifluorotoluene 101 102 90.4-116
(S) 4-Bromofluorobenzene 93.4 96.5 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG858088
Volatile Organic Compounds (GC/MS) by Method 8260B L824012-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L824012-20 03/23/16 14:34 • (MS) R3123285-4 03/23/16 13:16 • (MSD) R3123285-5 03/23/16 13:35
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Acetone 0.125 0.00209 0.0585 0.0483 45.1 37.0 1 25.0-156 19.1 21.5
Acrylonitrile 0.125 ND 0.128 0.117 103 93.4 1 55.9-161 9.41 20
Benzene 0.0250 ND 0.0201 0.0215 80.3 86.0 1 58.6-133 6.87 20
Bromodichloromethane 0.0250 ND 0.0227 0.0244 90.9 97.7 1 69.2-127 7.27 20
Bromochloromethane 0.0250 ND 0.0219 0.0225 87.7 90.1 1 74.4-128 2.65 20
Bromoform 0.0250 ND 0.0231 0.0245 92.5 98.1 1 66.3-140 5.83 20
Bromomethane 0.0250 ND 0.0269 0.0295 107 118 1 16.6-183 9.54 20.5
Carbon disulfide 0.0250 0.000175 0.0155 0.0171 61.4 67.9 1 34.9-138 9.93 20
Carbon tetrachloride 0.0250 ND 0.0204 0.0221 81.5 88.3 1 60.6-139 8.01 20
Chlorobenzene 0.0250 ND 0.0215 0.0233 86.1 93.0 1 70.1-130 7.76 20
Chlorodibromomethane 0.0250 ND 0.0240 0.0256 95.9 102 1 71.6-132 6.54 20
Chloroethane 0.0250 ND 0.0227 0.0250 90.9 100 1 33.3-155 9.64 20
Chloroform 0.0250 ND 0.0220 0.0237 88.2 94.7 1 66.1-133 7.13 20
Chloromethane 0.0250 ND 0.0166 0.0182 66.4 72.9 1 40.7-139 9.22 20
Dibromomethane 0.0250 ND 0.0230 0.0241 92.0 96.3 1 72.8-127 4.53 20
1,2-Dichlorobenzene 0.0250 ND 0.0212 0.0240 84.8 96.0 1 77.4-127 12.4 20
1,4-Dichlorobenzene 0.0250 ND 0.0215 0.0233 85.9 93.2 1 74.4-123 8.23 20
trans-1,4-Dichloro-2-butene 0.0250 ND 0.0261 0.0278 104 111 1 57.6-136 6.39 20
1,1-Dichloroethane 0.0250 ND 0.0212 0.0233 84.7 93.1 1 64.0-134 9.46 20
1,2-Dichloroethane 0.0250 ND 0.0223 0.0229 89.4 91.5 1 60.7-132 2.37 20
1,1-Dichloroethene 0.0250 ND 0.0221 0.0243 88.2 97.3 1 48.8-144 9.80 20
cis-1,2-Dichloroethene 0.0250 ND 0.0212 0.0223 84.6 89.4 1 60.6-136 5.43 20
trans-1,2-Dichloroethene 0.0250 ND 0.0201 0.0219 80.6 87.8 1 61.0-132 8.56 20
1,2-Dichloropropane 0.0250 ND 0.0219 0.0234 87.5 93.4 1 69.7-130 6.57 20
cis-1,3-Dichloropropene 0.0250 ND 0.0225 0.0236 89.9 94.6 1 71.1-129 5.08 20
trans-1,3-Dichloropropene 0.0250 ND 0.0245 0.0247 98.0 98.7 1 66.3-136 0.710 20
Ethylbenzene 0.0250 ND 0.0210 0.0230 84.1 92.1 1 62.7-136 9.09 20
2-Hexanone 0.125 ND 0.109 0.114 87.2 90.8 1 59.4-154 4.11 20.1
Iodomethane 0.125 ND 0.107 0.116 85.8 92.5 1 55.2-140 7.46 20
2-Butanone (MEK)0.125 ND 0.0875 0.0818 70.0 65.4 1 45.0-156 6.67 20.8
Methylene Chloride 0.0250 ND 0.0208 0.0216 83.3 86.5 1 61.5-125 3.73 20
4-Methyl-2-pentanone (MIBK)0.125 ND 0.133 0.139 106 112 1 60.7-150 4.74 20
Styrene 0.0250 ND 0.0219 0.0237 87.4 95.0 1 68.2-133 8.30 20
1,1,1,2-Tetrachloroethane 0.0250 ND 0.0227 0.0245 90.8 98.0 1 70.5-132 7.58 20
1,1,2,2-Tetrachloroethane 0.0250 ND 0.0244 0.0256 97.7 103 1 64.9-145 4.80 20
Tetrachloroethene 0.0250 ND 0.0200 0.0216 80.1 86.2 1 57.4-141 7.33 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG858088
Volatile Organic Compounds (GC/MS) by Method 8260B L824012-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L824012-20 03/23/16 14:34 • (MS) R3123285-4 03/23/16 13:16 • (MSD) R3123285-5 03/23/16 13:35
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Toluene 0.0250 ND 0.0201 0.0219 80.3 87.6 1 67.8-124 8.75 20
1,1,1-Trichloroethane 0.0250 ND 0.0222 0.0237 88.8 94.9 1 58.7-134 6.66 20
1,1,2-Trichloroethane 0.0250 ND 0.0231 0.0251 92.5 100 1 74.1-130 8.10 20
Trichloroethene 0.0250 ND 0.0206 0.0220 82.4 88.1 1 48.9-148 6.76 20
Trichlorofluoromethane 0.0250 ND 0.0235 0.0254 93.9 102 1 39.9-165 7.95 20
1,2,3-Trichloropropane 0.0250 ND 0.0253 0.0263 101 105 1 71.5-134 3.58 20
Vinyl acetate 0.125 ND 0.131 0.134 105 107 1 42.8-181 1.89 20
Vinyl chloride 0.0250 ND 0.0201 0.0218 80.5 87.3 1 44.3-143 8.05 20
Xylenes, Total 0.0750 ND 0.0620 0.0681 82.7 90.9 1 65.6-133 9.46 20
(S) Toluene-d8 103 104 90.0-115
(S) Dibromofluoromethane 105 102 79.0-121
(S) a,a,a-Trifluorotoluene 102 105 90.4-116
(S) 4-Bromofluorobenzene 99.2 102 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG858884
Volatile Organic Compounds (GC/MS) by Method 8260B L824012-17,18
Method Blank (MB)
(MB) R3123440-1 03/24/16 00:39
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0100 0.0500
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3123440-2 03/24/16 01:47 • (LCSD) R3123440-3 03/24/16 02:09
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.125 0.123 0.121 98.6 97.1 28.7-175 1.58 20.9
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND,U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
SDL Sample Detection Limit.
MQL Method Quantitation Limit.
Unadj. MQL Unadjusted Method Quantitation Limit.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry. The most significant benefit to our “one location” design is the design of our laboratory campus. The model is conducive to accelerated productivity,
decreasing turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
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* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
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ANALYTICAL REPORT
March 28, 2016
Hunt Environmental Associates
Sample Delivery Group:L823634
Samples Received:03/16/2016
Project Number:14-011550
Description:Robeson Co Solid Waste Semi-Annual Env Monitoring
Report To:Cody Hunt
3430 Capuano Street
Lumberton, NC 28358
Entire Report Reviewed By:
March 28, 2016
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
March 28, 2016
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 5
⁵Sr: Sample Results 6
MW-25R 14.61FT L823634-01 6
SW-1 L823634-02 8
SW-2 L823634-03 10
LEACHATE PHASE 2 L823634-04 12
LEACHATE PHASE 3 L823634-05 14
LEACHATE PHASE 4 L823634-06 16
⁶Qc: Quality Control Summary 18
Wet Chemistry by Method 365.4 18
Wet Chemistry by Method 410.4 19
Wet Chemistry by Method 5210 B-2011 20
Wet Chemistry by Method 9056A 24
Metals (ICP) by Method 6010C 26
Metals (ICPMS) by Method 6020 27
Volatile Organic Compounds (GC/MS) by Method 8260B 29
⁷Gl: Glossary of Terms 34
⁸Al: Accreditations & Locations 35
⁹Sc: Chain of Custody 36
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-25R 14.61FT L823634-01 GW 03/15/16 12:59 03/16/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG856921 1 03/16/16 17:56 03/17/16 12:48 CCE
Metals (ICPMS) by Method 6020 WG856922 1 03/16/16 16:47 03/17/16 12:27 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG857667 1 03/20/16 03:28 03/20/16 03:28 BMB
Collected by Collected date/time Received date/time
SW-1 L823634-02 GW 03/15/16 12:30 03/16/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG856921 1 03/16/16 17:56 03/17/16 13:00 LTB
Metals (ICPMS) by Method 6020 WG856922 1 03/16/16 16:47 03/17/16 13:11 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG857667 1 03/20/16 03:48 03/20/16 03:48 BMB
Collected by Collected date/time Received date/time
SW-2 L823634-03 GW 03/15/16 12:20 03/16/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG856921 1 03/16/16 17:56 03/17/16 13:03 LTB
Metals (ICPMS) by Method 6020 WG856922 1 03/16/16 16:47 03/17/16 13:14 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG857667 1 03/20/16 04:08 03/20/16 04:08 BMB
Collected by Collected date/time Received date/time
LEACHATE PHASE 2 L823634-04 GW 03/15/16 11:26 03/16/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG856921 9 03/16/16 17:56 03/17/16 13:06 LTB
Metals (ICPMS) by Method 6020 WG856922 9 03/16/16 16:47 03/17/16 13:17 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG857667 1 03/20/16 04:28 03/20/16 04:28 BMB
Wet Chemistry by Method 365.4 WG857030 1 03/17/16 10:51 03/22/16 23:51 ASK
Wet Chemistry by Method 410.4 WG857015 1 03/18/16 12:17 03/18/16 17:27 SJM
Wet Chemistry by Method 5210 B-2011 WG856835 1 03/16/16 14:38 03/21/16 09:58 BBM
Wet Chemistry by Method 9056A WG856814 1 03/16/16 18:25 03/16/16 18:25 CM
Collected by Collected date/time Received date/time
LEACHATE PHASE 3 L823634-05 GW 03/15/16 11:30 03/16/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG856921 9 03/16/16 17:56 03/17/16 13:15 LTB
Metals (ICPMS) by Method 6020 WG856922 9 03/16/16 16:47 03/17/16 13:19 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG857667 1 03/20/16 04:48 03/20/16 04:48 BMB
Wet Chemistry by Method 365.4 WG857030 1 03/17/16 10:51 03/22/16 23:52 ASK
Wet Chemistry by Method 410.4 WG857015 1 03/18/16 12:17 03/18/16 17:28 SJM
Wet Chemistry by Method 5210 B-2011 WG856835 1 03/16/16 14:41 03/21/16 10:00 BBM
Wet Chemistry by Method 9056A WG856814 1 03/16/16 18:41 03/16/16 18:41 CM
Collected by Collected date/time Received date/time
LEACHATE PHASE 4 L823634-06 GW 03/15/16 11:40 03/16/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG856921 9 03/16/16 17:56 03/17/16 13:18 LTB
Metals (ICPMS) by Method 6020 WG856922 9 03/16/16 16:47 03/17/16 13:22 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG857667 1 03/20/16 05:08 03/20/16 05:08 BMB
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
LEACHATE PHASE 4 L823634-06 GW 03/15/16 11:40 03/16/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Wet Chemistry by Method 365.4 WG857030 1 03/17/16 10:51 03/22/16 23:53 ASK
Wet Chemistry by Method 410.4 WG857015 1 03/18/16 12:17 03/18/16 17:28 SJM
Wet Chemistry by Method 5210 B-2011 WG858345 1 03/22/16 13:34 03/27/16 10:58 RTB
Wet Chemistry by Method 9056A WG856814 1 03/16/16 18:57 03/16/16 18:57 CM
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the
dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria
except where addressed in this case narrative, a non-conformance form or properly qualified within the
sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Sample Handling and Receiving
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
ESC Sample ID Project Sample ID Method
L823634-04 LEACHATE PHASE 2 6010C, 6020
L823634-05 LEACHATE PHASE 3 6010C, 6020
L823634-06 LEACHATE PHASE 4 6010C, 6020
The following samples were prepared and/or analyzed past recommended holding time. Concentrations should be
considered minimum values.
ESC Sample ID Project Sample ID Method
L823634-06 LEACHATE PHASE 4 5210 B-2011
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Jimmy Hunt
Technical Service Representative
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L823634
MW-25R 14.61FT
Collected date/time: 03/15/16 12:59
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0294 0.00500 1 03/17/2016 12:48 WG856921
Chromium ND 0.0100 1 03/17/2016 12:48 WG856921
Cobalt ND 0.0100 1 03/17/2016 12:48 WG856921
Nickel ND 0.0100 1 03/17/2016 12:48 WG856921
Silver ND 0.00500 1 03/17/2016 12:48 WG856921
Vanadium ND 0.0200 1 03/17/2016 12:48 WG856921
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/17/2016 12:27 WG856922
Arsenic 0.00223 0.00200 1 03/17/2016 12:27 WG856922
Beryllium ND 0.00200 1 03/17/2016 12:27 WG856922
Cadmium ND 0.00100 1 03/17/2016 12:27 WG856922
Copper 0.0103 0.00500 1 03/17/2016 12:27 WG856922
Lead 0.00334 0.00200 1 03/17/2016 12:27 WG856922
Selenium ND 0.00200 1 03/17/2016 12:27 WG856922
Thallium ND 0.00200 1 03/17/2016 12:27 WG856922
Zinc ND 0.0250 1 03/17/2016 12:27 WG856922
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/20/2016 03:28 WG857667
Acrylonitrile ND 0.0100 1 03/20/2016 03:28 WG857667
Benzene ND 0.00100 1 03/20/2016 03:28 WG857667
Bromochloromethane ND 0.00100 1 03/20/2016 03:28 WG857667
Bromodichloromethane ND 0.00100 1 03/20/2016 03:28 WG857667
Bromoform ND 0.00100 1 03/20/2016 03:28 WG857667
Bromomethane ND 0.00500 1 03/20/2016 03:28 WG857667
Carbon disulfide 0.00140 0.00100 1 03/20/2016 03:28 WG857667
Carbon tetrachloride ND 0.00100 1 03/20/2016 03:28 WG857667
Chlorobenzene ND 0.00100 1 03/20/2016 03:28 WG857667
Chlorodibromomethane ND 0.00100 1 03/20/2016 03:28 WG857667
Chloroethane ND 0.00500 1 03/20/2016 03:28 WG857667
Chloroform ND 0.00500 1 03/20/2016 03:28 WG857667
Chloromethane ND 0.00250 1 03/20/2016 03:28 WG857667
Dibromomethane ND 0.00100 1 03/20/2016 03:28 WG857667
1,2-Dichlorobenzene ND 0.00100 1 03/20/2016 03:28 WG857667
1,4-Dichlorobenzene ND 0.00100 1 03/20/2016 03:28 WG857667
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/20/2016 03:28 WG857667
1,1-Dichloroethane ND 0.00100 1 03/20/2016 03:28 WG857667
1,2-Dichloroethane ND 0.00100 1 03/20/2016 03:28 WG857667
1,1-Dichloroethene ND 0.00100 1 03/20/2016 03:28 WG857667
cis-1,2-Dichloroethene ND 0.00100 1 03/20/2016 03:28 WG857667
trans-1,2-Dichloroethene ND 0.00100 1 03/20/2016 03:28 WG857667
1,2-Dichloropropane ND 0.00100 1 03/20/2016 03:28 WG857667
cis-1,3-Dichloropropene ND 0.00100 1 03/20/2016 03:28 WG857667
trans-1,3-Dichloropropene ND 0.00100 1 03/20/2016 03:28 WG857667
Ethylbenzene ND 0.00100 1 03/20/2016 03:28 WG857667
2-Hexanone ND 0.0100 1 03/20/2016 03:28 WG857667
Iodomethane ND 0.0100 1 03/20/2016 03:28 WG857667
2-Butanone (MEK)ND 0.0100 1 03/20/2016 03:28 WG857667
Methylene Chloride ND 0.00500 1 03/20/2016 03:28 WG857667
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/20/2016 03:28 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L823634
MW-25R 14.61FT
Collected date/time: 03/15/16 12:59
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/20/2016 03:28 WG857667
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/20/2016 03:28 WG857667
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/20/2016 03:28 WG857667
Tetrachloroethene ND 0.00100 1 03/20/2016 03:28 WG857667
Toluene ND 0.00500 1 03/20/2016 03:28 WG857667
1,1,1-Trichloroethane ND 0.00100 1 03/20/2016 03:28 WG857667
1,1,2-Trichloroethane ND 0.00100 1 03/20/2016 03:28 WG857667
Trichloroethene ND 0.00100 1 03/20/2016 03:28 WG857667
Trichlorofluoromethane ND 0.00500 1 03/20/2016 03:28 WG857667
1,2,3-Trichloropropane ND 0.00250 1 03/20/2016 03:28 WG857667
Vinyl acetate ND 0.0100 1 03/20/2016 03:28 WG857667
Vinyl chloride ND 0.00100 1 03/20/2016 03:28 WG857667
Xylenes, Total ND 0.00300 1 03/20/2016 03:28 WG857667
(S) Toluene-d8 106 90.0-115 03/20/2016 03:28 WG857667
(S) Dibromofluoromethane 101 79.0-121 03/20/2016 03:28 WG857667
(S) a,a,a-Trifluorotoluene 100 90.4-116 03/20/2016 03:28 WG857667
(S) 4-Bromofluorobenzene 97.4 80.1-120 03/20/2016 03:28 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L823634
SW-1
Collected date/time: 03/15/16 12:30
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0622 0.00500 1 03/17/2016 13:00 WG856921
Chromium ND 0.0100 1 03/17/2016 13:00 WG856921
Cobalt ND 0.0100 1 03/17/2016 13:00 WG856921
Nickel ND 0.0100 1 03/17/2016 13:00 WG856921
Silver ND 0.00500 1 03/17/2016 13:00 WG856921
Vanadium ND 0.0200 1 03/17/2016 13:00 WG856921
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 03/17/2016 13:11 WG856922
Arsenic 0.00208 0.00200 1 03/17/2016 13:11 WG856922
Beryllium ND 0.00200 1 03/17/2016 13:11 WG856922
Cadmium ND 0.00100 1 03/17/2016 13:11 WG856922
Copper ND 0.00500 1 03/17/2016 13:11 WG856922
Lead ND 0.00200 1 03/17/2016 13:11 WG856922
Selenium ND 0.00200 1 03/17/2016 13:11 WG856922
Thallium ND 0.00200 1 03/17/2016 13:11 WG856922
Zinc ND 0.0250 1 03/17/2016 13:11 WG856922
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/20/2016 03:48 WG857667
Acrylonitrile ND 0.0100 1 03/20/2016 03:48 WG857667
Benzene ND 0.00100 1 03/20/2016 03:48 WG857667
Bromochloromethane ND 0.00100 1 03/20/2016 03:48 WG857667
Bromodichloromethane ND 0.00100 1 03/20/2016 03:48 WG857667
Bromoform ND 0.00100 1 03/20/2016 03:48 WG857667
Bromomethane ND 0.00500 1 03/20/2016 03:48 WG857667
Carbon disulfide ND 0.00100 1 03/20/2016 03:48 WG857667
Carbon tetrachloride ND 0.00100 1 03/20/2016 03:48 WG857667
Chlorobenzene ND 0.00100 1 03/20/2016 03:48 WG857667
Chlorodibromomethane ND 0.00100 1 03/20/2016 03:48 WG857667
Chloroethane ND 0.00500 1 03/20/2016 03:48 WG857667
Chloroform ND 0.00500 1 03/20/2016 03:48 WG857667
Chloromethane ND 0.00250 1 03/20/2016 03:48 WG857667
Dibromomethane ND 0.00100 1 03/20/2016 03:48 WG857667
1,2-Dichlorobenzene ND 0.00100 1 03/20/2016 03:48 WG857667
1,4-Dichlorobenzene ND 0.00100 1 03/20/2016 03:48 WG857667
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/20/2016 03:48 WG857667
1,1-Dichloroethane ND 0.00100 1 03/20/2016 03:48 WG857667
1,2-Dichloroethane ND 0.00100 1 03/20/2016 03:48 WG857667
1,1-Dichloroethene ND 0.00100 1 03/20/2016 03:48 WG857667
cis-1,2-Dichloroethene ND 0.00100 1 03/20/2016 03:48 WG857667
trans-1,2-Dichloroethene ND 0.00100 1 03/20/2016 03:48 WG857667
1,2-Dichloropropane ND 0.00100 1 03/20/2016 03:48 WG857667
cis-1,3-Dichloropropene ND 0.00100 1 03/20/2016 03:48 WG857667
trans-1,3-Dichloropropene ND 0.00100 1 03/20/2016 03:48 WG857667
Ethylbenzene ND 0.00100 1 03/20/2016 03:48 WG857667
2-Hexanone ND 0.0100 1 03/20/2016 03:48 WG857667
Iodomethane ND 0.0100 1 03/20/2016 03:48 WG857667
2-Butanone (MEK)ND 0.0100 1 03/20/2016 03:48 WG857667
Methylene Chloride ND 0.00500 1 03/20/2016 03:48 WG857667
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/20/2016 03:48 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L823634
SW-1
Collected date/time: 03/15/16 12:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/20/2016 03:48 WG857667
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/20/2016 03:48 WG857667
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/20/2016 03:48 WG857667
Tetrachloroethene ND 0.00100 1 03/20/2016 03:48 WG857667
Toluene ND 0.00500 1 03/20/2016 03:48 WG857667
1,1,1-Trichloroethane ND 0.00100 1 03/20/2016 03:48 WG857667
1,1,2-Trichloroethane ND 0.00100 1 03/20/2016 03:48 WG857667
Trichloroethene ND 0.00100 1 03/20/2016 03:48 WG857667
Trichlorofluoromethane ND 0.00500 1 03/20/2016 03:48 WG857667
1,2,3-Trichloropropane ND 0.00250 1 03/20/2016 03:48 WG857667
Vinyl acetate ND 0.0100 1 03/20/2016 03:48 WG857667
Vinyl chloride ND 0.00100 1 03/20/2016 03:48 WG857667
Xylenes, Total ND 0.00300 1 03/20/2016 03:48 WG857667
(S) Toluene-d8 105 90.0-115 03/20/2016 03:48 WG857667
(S) Dibromofluoromethane 103 79.0-121 03/20/2016 03:48 WG857667
(S) a,a,a-Trifluorotoluene 101 90.4-116 03/20/2016 03:48 WG857667
(S) 4-Bromofluorobenzene 97.2 80.1-120 03/20/2016 03:48 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L823634
SW-2
Collected date/time: 03/15/16 12:20
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.202 0.00500 1 03/17/2016 13:03 WG856921
Chromium ND 0.0100 1 03/17/2016 13:03 WG856921
Cobalt ND 0.0100 1 03/17/2016 13:03 WG856921
Nickel 0.0174 B 0.0100 1 03/17/2016 13:03 WG856921
Silver ND 0.00500 1 03/17/2016 13:03 WG856921
Vanadium ND 0.0200 1 03/17/2016 13:03 WG856921
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony 0.00413 0.00200 1 03/17/2016 13:14 WG856922
Arsenic 0.00951 0.00200 1 03/17/2016 13:14 WG856922
Beryllium ND 0.00200 1 03/17/2016 13:14 WG856922
Cadmium ND 0.00100 1 03/17/2016 13:14 WG856922
Copper ND 0.00500 1 03/17/2016 13:14 WG856922
Lead ND 0.00200 1 03/17/2016 13:14 WG856922
Selenium ND 0.00200 1 03/17/2016 13:14 WG856922
Thallium ND 0.00200 1 03/17/2016 13:14 WG856922
Zinc 0.0433 0.0250 1 03/17/2016 13:14 WG856922
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone 0.140 0.0500 1 03/20/2016 04:08 WG857667
Acrylonitrile ND 0.0100 1 03/20/2016 04:08 WG857667
Benzene ND 0.00100 1 03/20/2016 04:08 WG857667
Bromochloromethane ND 0.00100 1 03/20/2016 04:08 WG857667
Bromodichloromethane ND 0.00100 1 03/20/2016 04:08 WG857667
Bromoform ND 0.00100 1 03/20/2016 04:08 WG857667
Bromomethane ND 0.00500 1 03/20/2016 04:08 WG857667
Carbon disulfide 0.0131 0.00100 1 03/20/2016 04:08 WG857667
Carbon tetrachloride ND 0.00100 1 03/20/2016 04:08 WG857667
Chlorobenzene ND 0.00100 1 03/20/2016 04:08 WG857667
Chlorodibromomethane ND 0.00100 1 03/20/2016 04:08 WG857667
Chloroethane ND 0.00500 1 03/20/2016 04:08 WG857667
Chloroform ND 0.00500 1 03/20/2016 04:08 WG857667
Chloromethane ND 0.00250 1 03/20/2016 04:08 WG857667
Dibromomethane ND 0.00100 1 03/20/2016 04:08 WG857667
1,2-Dichlorobenzene ND 0.00100 1 03/20/2016 04:08 WG857667
1,4-Dichlorobenzene ND 0.00100 1 03/20/2016 04:08 WG857667
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/20/2016 04:08 WG857667
1,1-Dichloroethane ND 0.00100 1 03/20/2016 04:08 WG857667
1,2-Dichloroethane ND 0.00100 1 03/20/2016 04:08 WG857667
1,1-Dichloroethene ND 0.00100 1 03/20/2016 04:08 WG857667
cis-1,2-Dichloroethene ND 0.00100 1 03/20/2016 04:08 WG857667
trans-1,2-Dichloroethene ND 0.00100 1 03/20/2016 04:08 WG857667
1,2-Dichloropropane ND 0.00100 1 03/20/2016 04:08 WG857667
cis-1,3-Dichloropropene ND 0.00100 1 03/20/2016 04:08 WG857667
trans-1,3-Dichloropropene ND 0.00100 1 03/20/2016 04:08 WG857667
Ethylbenzene ND 0.00100 1 03/20/2016 04:08 WG857667
2-Hexanone ND 0.0100 1 03/20/2016 04:08 WG857667
Iodomethane ND 0.0100 1 03/20/2016 04:08 WG857667
2-Butanone (MEK)0.0677 0.0100 1 03/20/2016 04:08 WG857667
Methylene Chloride ND 0.00500 1 03/20/2016 04:08 WG857667
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/20/2016 04:08 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L823634
SW-2
Collected date/time: 03/15/16 12:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 03/20/2016 04:08 WG857667
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/20/2016 04:08 WG857667
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/20/2016 04:08 WG857667
Tetrachloroethene ND 0.00100 1 03/20/2016 04:08 WG857667
Toluene ND 0.00500 1 03/20/2016 04:08 WG857667
1,1,1-Trichloroethane ND 0.00100 1 03/20/2016 04:08 WG857667
1,1,2-Trichloroethane ND 0.00100 1 03/20/2016 04:08 WG857667
Trichloroethene ND 0.00100 1 03/20/2016 04:08 WG857667
Trichlorofluoromethane ND 0.00500 1 03/20/2016 04:08 WG857667
1,2,3-Trichloropropane ND 0.00250 1 03/20/2016 04:08 WG857667
Vinyl acetate ND 0.0100 1 03/20/2016 04:08 WG857667
Vinyl chloride ND 0.00100 1 03/20/2016 04:08 WG857667
Xylenes, Total ND 0.00300 1 03/20/2016 04:08 WG857667
(S) Toluene-d8 107 90.0-115 03/20/2016 04:08 WG857667
(S) Dibromofluoromethane 105 79.0-121 03/20/2016 04:08 WG857667
(S) a,a,a-Trifluorotoluene 101 90.4-116 03/20/2016 04:08 WG857667
(S) 4-Bromofluorobenzene 99.0 80.1-120 03/20/2016 04:08 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L823634 03/28/16 17:02 11 of 36
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L823634
LEACHATE PHASE 2
Collected date/time: 03/15/16 11:26
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Phosphorus,Total 0.179 0.100 1 03/22/2016 23:51 WG857030
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 592 10.0 1 03/18/2016 17:27 WG857015
Wet Chemistry by Method 5210 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
BOD 32.5 10.0 1 03/21/2016 09:58 WG856835
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Nitrate 0.540 0.100 1 03/16/2016 18:25 WG856814
Sulfate 28.5 5.00 1 03/16/2016 18:25 WG856814
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.133 0.0450 9 03/17/2016 13:06 WG856921
Chromium ND 0.0900 9 03/17/2016 13:06 WG856921
Cobalt ND 0.0900 9 03/17/2016 13:06 WG856921
Nickel ND 0.0900 9 03/17/2016 13:06 WG856921
Silver ND 0.0450 9 03/17/2016 13:06 WG856921
Vanadium ND 0.180 9 03/17/2016 13:06 WG856921
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0180 9 03/17/2016 13:17 WG856922
Arsenic 0.0342 0.0180 9 03/17/2016 13:17 WG856922
Beryllium ND 0.0180 9 03/17/2016 13:17 WG856922
Cadmium ND 0.00900 9 03/17/2016 13:17 WG856922
Copper 0.603 0.0450 9 03/17/2016 13:17 WG856922
Lead 0.147 0.0180 9 03/17/2016 13:17 WG856922
Selenium ND 0.0180 9 03/17/2016 13:17 WG856922
Thallium ND 0.0180 9 03/17/2016 13:17 WG856922
Zinc ND 0.225 9 03/17/2016 13:17 WG856922
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone 0.0918 0.0500 1 03/20/2016 04:28 WG857667
Acrylonitrile ND 0.0100 1 03/20/2016 04:28 WG857667
Benzene 0.00717 0.00100 1 03/20/2016 04:28 WG857667
Bromochloromethane ND 0.00100 1 03/20/2016 04:28 WG857667
Bromodichloromethane ND 0.00100 1 03/20/2016 04:28 WG857667
Bromoform ND 0.00100 1 03/20/2016 04:28 WG857667
Bromomethane ND 0.00500 1 03/20/2016 04:28 WG857667
Carbon disulfide ND 0.00100 1 03/20/2016 04:28 WG857667
Carbon tetrachloride ND 0.00100 1 03/20/2016 04:28 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L823634 03/28/16 17:02 12 of 36
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L823634
LEACHATE PHASE 2
Collected date/time: 03/15/16 11:26
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chlorobenzene 0.00211 0.00100 1 03/20/2016 04:28 WG857667
Chlorodibromomethane ND 0.00100 1 03/20/2016 04:28 WG857667
Chloroethane ND 0.00500 1 03/20/2016 04:28 WG857667
Chloroform ND 0.00500 1 03/20/2016 04:28 WG857667
Chloromethane ND 0.00250 1 03/20/2016 04:28 WG857667
Dibromomethane ND 0.00100 1 03/20/2016 04:28 WG857667
1,2-Dichlorobenzene ND 0.00100 1 03/20/2016 04:28 WG857667
1,4-Dichlorobenzene 0.0180 0.00100 1 03/20/2016 04:28 WG857667
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/20/2016 04:28 WG857667
1,1-Dichloroethane ND 0.00100 1 03/20/2016 04:28 WG857667
1,2-Dichloroethane ND 0.00100 1 03/20/2016 04:28 WG857667
1,1-Dichloroethene ND 0.00100 1 03/20/2016 04:28 WG857667
cis-1,2-Dichloroethene ND 0.00100 1 03/20/2016 04:28 WG857667
trans-1,2-Dichloroethene ND 0.00100 1 03/20/2016 04:28 WG857667
1,2-Dichloropropane ND 0.00100 1 03/20/2016 04:28 WG857667
cis-1,3-Dichloropropene ND 0.00100 1 03/20/2016 04:28 WG857667
trans-1,3-Dichloropropene ND 0.00100 1 03/20/2016 04:28 WG857667
Ethylbenzene 0.00626 0.00100 1 03/20/2016 04:28 WG857667
2-Hexanone ND 0.0100 1 03/20/2016 04:28 WG857667
Iodomethane ND 0.0100 1 03/20/2016 04:28 WG857667
2-Butanone (MEK)0.114 0.0100 1 03/20/2016 04:28 WG857667
Methylene Chloride ND 0.00500 1 03/20/2016 04:28 WG857667
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/20/2016 04:28 WG857667
Styrene ND 0.00100 1 03/20/2016 04:28 WG857667
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/20/2016 04:28 WG857667
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/20/2016 04:28 WG857667
Tetrachloroethene ND 0.00100 1 03/20/2016 04:28 WG857667
Toluene ND 0.00500 1 03/20/2016 04:28 WG857667
1,1,1-Trichloroethane ND 0.00100 1 03/20/2016 04:28 WG857667
1,1,2-Trichloroethane ND 0.00100 1 03/20/2016 04:28 WG857667
Trichloroethene ND 0.00100 1 03/20/2016 04:28 WG857667
Trichlorofluoromethane ND 0.00500 1 03/20/2016 04:28 WG857667
1,2,3-Trichloropropane ND 0.00250 1 03/20/2016 04:28 WG857667
Vinyl acetate ND 0.0100 1 03/20/2016 04:28 WG857667
Vinyl chloride 0.00132 0.00100 1 03/20/2016 04:28 WG857667
Xylenes, Total 0.0379 0.00300 1 03/20/2016 04:28 WG857667
(S) Toluene-d8 103 90.0-115 03/20/2016 04:28 WG857667
(S) Dibromofluoromethane 102 79.0-121 03/20/2016 04:28 WG857667
(S) a,a,a-Trifluorotoluene 98.9 90.4-116 03/20/2016 04:28 WG857667
(S) 4-Bromofluorobenzene 97.3 80.1-120 03/20/2016 04:28 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L823634 03/28/16 17:02 13 of 36
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L823634
LEACHATE PHASE 3
Collected date/time: 03/15/16 11:30
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Phosphorus,Total 2.07 0.100 1 03/22/2016 23:52 WG857030
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 672 10.0 1 03/18/2016 17:28 WG857015
Wet Chemistry by Method 5210 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
BOD 43.9 10.0 1 03/21/2016 10:00 WG856835
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Nitrate 0.904 0.100 1 03/16/2016 18:41 WG856814
Sulfate 8.64 5.00 1 03/16/2016 18:41 WG856814
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.212 0.0450 9 03/17/2016 13:15 WG856921
Chromium ND 0.0900 9 03/17/2016 13:15 WG856921
Cobalt ND 0.0900 9 03/17/2016 13:15 WG856921
Nickel ND 0.0900 9 03/17/2016 13:15 WG856921
Silver ND 0.0450 9 03/17/2016 13:15 WG856921
Vanadium ND 0.180 9 03/17/2016 13:15 WG856921
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0180 9 03/17/2016 13:19 WG856922
Arsenic 0.0352 0.0180 9 03/17/2016 13:19 WG856922
Beryllium ND 0.0180 9 03/17/2016 13:19 WG856922
Cadmium ND 0.00900 9 03/17/2016 13:19 WG856922
Copper 0.243 0.0450 9 03/17/2016 13:19 WG856922
Lead 0.0187 0.0180 9 03/17/2016 13:19 WG856922
Selenium ND 0.0180 9 03/17/2016 13:19 WG856922
Thallium ND 0.0180 9 03/17/2016 13:19 WG856922
Zinc ND 0.225 9 03/17/2016 13:19 WG856922
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/20/2016 04:48 WG857667
Acrylonitrile ND 0.0100 1 03/20/2016 04:48 WG857667
Benzene 0.00594 0.00100 1 03/20/2016 04:48 WG857667
Bromochloromethane ND 0.00100 1 03/20/2016 04:48 WG857667
Bromodichloromethane ND 0.00100 1 03/20/2016 04:48 WG857667
Bromoform ND 0.00100 1 03/20/2016 04:48 WG857667
Bromomethane ND 0.00500 1 03/20/2016 04:48 WG857667
Carbon disulfide ND 0.00100 1 03/20/2016 04:48 WG857667
Carbon tetrachloride ND 0.00100 1 03/20/2016 04:48 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L823634 03/28/16 17:02 14 of 36
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L823634
LEACHATE PHASE 3
Collected date/time: 03/15/16 11:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chlorobenzene 0.00150 0.00100 1 03/20/2016 04:48 WG857667
Chlorodibromomethane ND 0.00100 1 03/20/2016 04:48 WG857667
Chloroethane ND 0.00500 1 03/20/2016 04:48 WG857667
Chloroform ND 0.00500 1 03/20/2016 04:48 WG857667
Chloromethane ND 0.00250 1 03/20/2016 04:48 WG857667
Dibromomethane ND 0.00100 1 03/20/2016 04:48 WG857667
1,2-Dichlorobenzene ND 0.00100 1 03/20/2016 04:48 WG857667
1,4-Dichlorobenzene 0.00896 0.00100 1 03/20/2016 04:48 WG857667
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/20/2016 04:48 WG857667
1,1-Dichloroethane ND 0.00100 1 03/20/2016 04:48 WG857667
1,2-Dichloroethane ND 0.00100 1 03/20/2016 04:48 WG857667
1,1-Dichloroethene ND 0.00100 1 03/20/2016 04:48 WG857667
cis-1,2-Dichloroethene ND 0.00100 1 03/20/2016 04:48 WG857667
trans-1,2-Dichloroethene ND 0.00100 1 03/20/2016 04:48 WG857667
1,2-Dichloropropane ND 0.00100 1 03/20/2016 04:48 WG857667
cis-1,3-Dichloropropene ND 0.00100 1 03/20/2016 04:48 WG857667
trans-1,3-Dichloropropene ND 0.00100 1 03/20/2016 04:48 WG857667
Ethylbenzene 0.00117 0.00100 1 03/20/2016 04:48 WG857667
2-Hexanone ND 0.0100 1 03/20/2016 04:48 WG857667
Iodomethane ND 0.0100 1 03/20/2016 04:48 WG857667
2-Butanone (MEK)ND 0.0100 1 03/20/2016 04:48 WG857667
Methylene Chloride ND 0.00500 1 03/20/2016 04:48 WG857667
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/20/2016 04:48 WG857667
Styrene ND 0.00100 1 03/20/2016 04:48 WG857667
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/20/2016 04:48 WG857667
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/20/2016 04:48 WG857667
Tetrachloroethene ND 0.00100 1 03/20/2016 04:48 WG857667
Toluene ND 0.00500 1 03/20/2016 04:48 WG857667
1,1,1-Trichloroethane ND 0.00100 1 03/20/2016 04:48 WG857667
1,1,2-Trichloroethane ND 0.00100 1 03/20/2016 04:48 WG857667
Trichloroethene ND 0.00100 1 03/20/2016 04:48 WG857667
Trichlorofluoromethane ND 0.00500 1 03/20/2016 04:48 WG857667
1,2,3-Trichloropropane ND 0.00250 1 03/20/2016 04:48 WG857667
Vinyl acetate ND 0.0100 1 03/20/2016 04:48 WG857667
Vinyl chloride 0.00149 0.00100 1 03/20/2016 04:48 WG857667
Xylenes, Total 0.0407 0.00300 1 03/20/2016 04:48 WG857667
(S) Toluene-d8 106 90.0-115 03/20/2016 04:48 WG857667
(S) Dibromofluoromethane 106 79.0-121 03/20/2016 04:48 WG857667
(S) a,a,a-Trifluorotoluene 99.0 90.4-116 03/20/2016 04:48 WG857667
(S) 4-Bromofluorobenzene 97.5 80.1-120 03/20/2016 04:48 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L823634 03/28/16 16:07 15 of 36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L823634 03/28/16 17:02 15 of 36
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L823634
LEACHATE PHASE 4
Collected date/time: 03/15/16 11:40
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Phosphorus,Total 0.336 0.100 1 03/22/2016 23:53 WG857030
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 907 10.0 1 03/18/2016 17:28 WG857015
Wet Chemistry by Method 5210 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
BOD 30.6 H 10.0 1 03/27/2016 10:58 WG858345
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Nitrate ND 0.100 1 03/16/2016 18:57 WG856814
Sulfate ND 5.00 1 03/16/2016 18:57 WG856814
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0951 0.0450 9 03/17/2016 13:18 WG856921
Chromium ND 0.0900 9 03/17/2016 13:18 WG856921
Cobalt ND 0.0900 9 03/17/2016 13:18 WG856921
Nickel 0.106 0.0900 9 03/17/2016 13:18 WG856921
Silver ND 0.0450 9 03/17/2016 13:18 WG856921
Vanadium ND 0.180 9 03/17/2016 13:18 WG856921
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0180 9 03/17/2016 13:22 WG856922
Arsenic 0.0503 0.0180 9 03/17/2016 13:22 WG856922
Beryllium ND 0.0180 9 03/17/2016 13:22 WG856922
Cadmium ND 0.00900 9 03/17/2016 13:22 WG856922
Copper ND 0.0450 9 03/17/2016 13:22 WG856922
Lead ND 0.0180 9 03/17/2016 13:22 WG856922
Selenium ND 0.0180 9 03/17/2016 13:22 WG856922
Thallium ND 0.0180 9 03/17/2016 13:22 WG856922
Zinc ND 0.225 9 03/17/2016 13:22 WG856922
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 03/20/2016 05:08 WG857667
Acrylonitrile ND 0.0100 1 03/20/2016 05:08 WG857667
Benzene 0.0103 0.00100 1 03/20/2016 05:08 WG857667
Bromochloromethane ND 0.00100 1 03/20/2016 05:08 WG857667
Bromodichloromethane ND 0.00100 1 03/20/2016 05:08 WG857667
Bromoform ND 0.00100 1 03/20/2016 05:08 WG857667
Bromomethane ND 0.00500 1 03/20/2016 05:08 WG857667
Carbon disulfide ND 0.00100 1 03/20/2016 05:08 WG857667
Carbon tetrachloride ND 0.00100 1 03/20/2016 05:08 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L823634
LEACHATE PHASE 4
Collected date/time: 03/15/16 11:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chlorobenzene 0.00116 0.00100 1 03/20/2016 05:08 WG857667
Chlorodibromomethane ND 0.00100 1 03/20/2016 05:08 WG857667
Chloroethane ND 0.00500 1 03/20/2016 05:08 WG857667
Chloroform ND 0.00500 1 03/20/2016 05:08 WG857667
Chloromethane ND 0.00250 1 03/20/2016 05:08 WG857667
Dibromomethane ND 0.00100 1 03/20/2016 05:08 WG857667
1,2-Dichlorobenzene ND 0.00100 1 03/20/2016 05:08 WG857667
1,4-Dichlorobenzene 0.00336 0.00100 1 03/20/2016 05:08 WG857667
trans-1,4-Dichloro-2-butene ND 0.00250 1 03/20/2016 05:08 WG857667
1,1-Dichloroethane ND 0.00100 1 03/20/2016 05:08 WG857667
1,2-Dichloroethane 0.00219 0.00100 1 03/20/2016 05:08 WG857667
1,1-Dichloroethene ND 0.00100 1 03/20/2016 05:08 WG857667
cis-1,2-Dichloroethene ND 0.00100 1 03/20/2016 05:08 WG857667
trans-1,2-Dichloroethene ND 0.00100 1 03/20/2016 05:08 WG857667
1,2-Dichloropropane ND 0.00100 1 03/20/2016 05:08 WG857667
cis-1,3-Dichloropropene ND 0.00100 1 03/20/2016 05:08 WG857667
trans-1,3-Dichloropropene ND 0.00100 1 03/20/2016 05:08 WG857667
Ethylbenzene 0.0148 0.00100 1 03/20/2016 05:08 WG857667
2-Hexanone ND 0.0100 1 03/20/2016 05:08 WG857667
Iodomethane ND 0.0100 1 03/20/2016 05:08 WG857667
2-Butanone (MEK)ND 0.0100 1 03/20/2016 05:08 WG857667
Methylene Chloride ND 0.00500 1 03/20/2016 05:08 WG857667
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 03/20/2016 05:08 WG857667
Styrene 0.00173 0.00100 1 03/20/2016 05:08 WG857667
1,1,1,2-Tetrachloroethane ND 0.00100 1 03/20/2016 05:08 WG857667
1,1,2,2-Tetrachloroethane ND 0.00100 1 03/20/2016 05:08 WG857667
Tetrachloroethene ND 0.00100 1 03/20/2016 05:08 WG857667
Toluene 0.0166 0.00500 1 03/20/2016 05:08 WG857667
1,1,1-Trichloroethane ND 0.00100 1 03/20/2016 05:08 WG857667
1,1,2-Trichloroethane ND 0.00100 1 03/20/2016 05:08 WG857667
Trichloroethene ND 0.00100 1 03/20/2016 05:08 WG857667
Trichlorofluoromethane ND 0.00500 1 03/20/2016 05:08 WG857667
1,2,3-Trichloropropane ND 0.00250 1 03/20/2016 05:08 WG857667
Vinyl acetate ND 0.0100 1 03/20/2016 05:08 WG857667
Vinyl chloride 0.00274 0.00100 1 03/20/2016 05:08 WG857667
Xylenes, Total 0.0292 0.00300 1 03/20/2016 05:08 WG857667
(S) Toluene-d8 106 90.0-115 03/20/2016 05:08 WG857667
(S) Dibromofluoromethane 107 79.0-121 03/20/2016 05:08 WG857667
(S) a,a,a-Trifluorotoluene 100 90.4-116 03/20/2016 05:08 WG857667
(S) 4-Bromofluorobenzene 98.0 80.1-120 03/20/2016 05:08 WG857667
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857030
Wet Chemistry by Method 365.4 L823634-04,05,06
Method Blank (MB)
(MB) 03/22/16 23:25
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Phosphorus,Total ND 0.100
L823615-03 Original Sample (OS) • Duplicate (DUP)
(OS) 03/23/16 00:06 • (DUP) 03/23/16 00:07
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Phosphorus,Total ND ND 1 0.000 20
L823699-01 Original Sample (OS) • Duplicate (DUP)
(OS) 03/23/16 00:09 • (DUP) 03/23/16 00:10
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Phosphorus,Total 19.4 20.3 10 5.00 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/22/16 23:26 • (LCSD) 03/22/16 23:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Phosphorus,Total 1.00 0.946 0.923 95.0 92.0 90.0-110 2.00 20
L823615-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/22/16 23:33 • (MS) 03/22/16 23:34 • (MSD) 03/22/16 23:35
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Phosphorus,Total 2.50 0.0347 2.13 2.11 84.0 83.0 1 90.0-110 J6 J6 1.00 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857015
Wet Chemistry by Method 410.4 L823634-04,05,06
Method Blank (MB)
(MB) 03/18/16 17:24
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
COD ND 10.0
L823624-01 Original Sample (OS) • Duplicate (DUP)
(OS) 03/18/16 17:25 • (DUP) 03/18/16 17:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
COD 139 139 1 0.000 20
L823816-01 Original Sample (OS) • Duplicate (DUP)
(OS) 03/18/16 17:31 • (DUP) 03/18/16 17:32
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
COD 21.0 19.8 1 6.00 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/18/16 17:24 • (LCSD) 03/18/16 17:24
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
COD 242 231 230 95.0 95.0 90.0-110 0.000 20
L823626-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/18/16 17:26 • (MS) 03/18/16 17:27 • (MSD) 03/18/16 17:27
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
COD 400 773 1150 1150 95.0 95.0 1 80.0-120 0.000 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856835
Wet Chemistry by Method 5210 B-2011 L823634-04,05
Method Blank (MB)
(MB) 03/21/16 12:05
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
BOD ND 1.00
L823554-01 Original Sample (OS) • Duplicate (DUP)
(OS) 03/21/16 08:57 • (DUP) 03/21/16 08:58
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
BOD 8.10 8.40 1 4 30
L823601-01 Original Sample (OS) • Duplicate (DUP)
(OS) 03/21/16 09:48 • (DUP) 03/21/16 09:50
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
BOD 28.9 28.2 1 2 30
L823575-01 Original Sample (OS) • Duplicate (DUP)
(OS) 03/21/16 10:56 • (DUP) 03/21/16 10:57
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
BOD 5.10 7.40 1 37 P1 30
L823673-01 Original Sample (OS) • Duplicate (DUP)
(OS) 03/21/16 11:55 • (DUP) 03/21/16 11:58
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
BOD 11.1 9.80 1 12 30
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856835
Wet Chemistry by Method 5210 B-2011 L823634-04,05
Laboratory Control Sample (LCS)
(LCS) 03/21/16 08:51
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
BOD 198 181 91.6 84.6-115
Laboratory Control Sample (LCS)
(LCS) 03/21/16 10:49
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
BOD 198 202 102 84.6-115
Laboratory Control Sample (LCS)
(LCS) 03/21/16 12:02
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
BOD 198 209 106 84.6-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG858345
Wet Chemistry by Method 5210 B-2011 L823634-06
Method Blank (MB)
(MB) 03/27/16 13:45
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
BOD ND 1.00
L824728-02 Original Sample (OS) • Duplicate (DUP)
(OS) 03/27/16 11:53 • (DUP) 03/27/16 11:54
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
BOD 1.70 0.000 1 0 30
L824750-06 Original Sample (OS) • Duplicate (DUP)
(OS) 03/27/16 12:38 • (DUP) 03/27/16 12:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
BOD ND 0.000 1 0 30
L824750-13 Original Sample (OS) • Duplicate (DUP)
(OS) 03/27/16 12:56 • (DUP) 03/27/16 12:57
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
BOD 0.140 0.000 1 0 30
L824816-01 Original Sample (OS) • Duplicate (DUP)
(OS) 03/27/16 13:35 • (DUP) 03/27/16 13:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
BOD 1.60 1.30 1 21 30
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG858345
Wet Chemistry by Method 5210 B-2011 L823634-06
Laboratory Control Sample (LCS)
(LCS) 03/27/16 10:45
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
BOD 198 180 90.7 84.6-115
Laboratory Control Sample (LCS)
(LCS) 03/27/16 12:46
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
BOD 198 181 91.4 84.6-115
Laboratory Control Sample (LCS)
(LCS) 03/27/16 13:43
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
BOD 198 170 85.7 84.6-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856814
Wet Chemistry by Method 9056A L823634-04,05,06
Method Blank (MB)
(MB) 03/16/16 07:03
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Nitrate ND 0.100
Sulfate ND 5.00
L823613-01 Original Sample (OS) • Duplicate (DUP)
(OS) 03/16/16 14:35 • (DUP) 03/16/16 14:51
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Nitrate 0.0532 0.0560 1 5 J 15
Sulfate 41.8 41.8 1 0 15
L823651-07 Original Sample (OS) • Duplicate (DUP)
(OS) 03/16/16 21:25 • (DUP) 03/16/16 21:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Nitrate ND 0.000 1 0 15
Sulfate ND 0.000 1 0 15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/16/16 07:19 • (LCSD) 03/16/16 07:36
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Nitrate 8.00 8.16 8.20 102 103 80-120 1 15
Sulfate 40.0 40.3 40.2 101 101 80-120 0 15
L823613-02 Original Sample (OS) • Matrix Spike (MS)
(OS) 03/16/16 15:08 • (MS) 03/16/16 15:24
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Nitrate 5.00 ND 4.82 96 1 80-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856814
Wet Chemistry by Method 9056A L823634-04,05,06
L823651-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/16/16 20:36 • (MS) 03/16/16 20:52 • (MSD) 03/16/16 21:09
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Nitrate 5.00 ND 4.99 4.76 100 95 1 80-120 5 15
Sulfate 50.0 54.4 103 101 97 93 1 80-120 2 15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856921
Metals (ICP) by Method 6010C L823634-01,02,03,04,05,06
Method Blank (MB)
(MB) 03/17/16 12:40
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Barium ND 0.00500
Chromium ND 0.0100
Cobalt ND 0.0100
Nickel ND 0.0100
Silver ND 0.00500
Vanadium ND 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/17/16 12:43 • (LCSD) 03/17/16 12:45
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Barium 1.00 1.02 1.02 102 102 80-120 0 20
Chromium 1.00 0.986 0.977 99 98 80-120 1 20
Cobalt 1.00 1.01 1.01 101 101 80-120 0 20
Nickel 1.00 0.987 0.983 99 98 80-120 0 20
Silver 1.00 1.02 1.01 102 101 80-120 1 20
Vanadium 1.00 1.03 1.01 103 101 80-120 2 20
L823634-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/17/16 12:48 • (MS) 03/17/16 12:54 • (MSD) 03/17/16 12:57
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Barium 1.00 0.0294 1.06 1.06 103 103 1 75-125 0 20
Chromium 1.00 0.00207 0.981 0.983 98 98 1 75-125 0 20
Cobalt 1.00 0.000982 1.02 1.02 102 102 1 75-125 0 20
Nickel 1.00 0.00184 0.990 0.991 99 99 1 75-125 0 20
Silver 1.00 0.000264 1.02 1.02 102 102 1 75-125 0 20
Vanadium 1.00 0.00155 1.03 1.03 102 103 1 75-125 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856922
Metals (ICPMS) by Method 6020 L823634-01,02,03,04,05,06
Method Blank (MB)
(MB) 03/17/16 12:18
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Antimony ND 0.00200
Arsenic ND 0.00200
Beryllium ND 0.00200
Cadmium ND 0.00100
Copper ND 0.00500
Lead ND 0.00200
Selenium ND 0.00200
Thallium ND 0.00200
Zinc ND 0.0250
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/17/16 12:21 • (LCSD) 03/17/16 12:24
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Antimony 0.0500 0.0517 0.0513 103 103 80-120 1 20
Arsenic 0.0500 0.0458 0.0467 92 93 80-120 2 20
Beryllium 0.0500 0.0458 0.0453 92 91 80-120 1 20
Cadmium 0.0500 0.0509 0.0515 102 103 80-120 1 20
Copper 0.0500 0.0506 0.0529 101 106 80-120 4 20
Lead 0.0500 0.0484 0.0484 97 97 80-120 0 20
Selenium 0.0500 0.0495 0.0502 99 100 80-120 1 20
Thallium 0.0500 0.0480 0.0477 96 95 80-120 0 20
Zinc 0.0500 0.0470 0.0511 94 102 80-120 8 20
L823634-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/17/16 12:27 • (MS) 03/17/16 12:32 • (MSD) 03/17/16 12:35
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 0.0500 0.000357 0.0500 0.0503 99 100 1 75-125 1 20
Arsenic 0.0500 0.00223 0.0480 0.0485 91 93 1 75-125 1 20
Beryllium 0.0500 0.0000562 0.0435 0.0450 87 90 1 75-125 3 20
Cadmium 0.0500 0.0000490 0.0511 0.0518 102 104 1 75-125 1 20
Copper 0.0500 0.0103 0.0518 0.0512 83 82 1 75-125 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856922
Metals (ICPMS) by Method 6020 L823634-01,02,03,04,05,06
L823634-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/17/16 12:27 • (MS) 03/17/16 12:32 • (MSD) 03/17/16 12:35
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Lead 0.0500 0.00334 0.0486 0.0505 91 94 1 75-125 4 20
Selenium 0.0500 0.000229 0.0490 0.0509 98 101 1 75-125 4 20
Thallium 0.0500 0.0000779 0.0465 0.0470 93 94 1 75-125 1 20
Zinc 0.0500 0.00152 0.0586 0.0528 114 103 1 75-125 10 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857667
Volatile Organic Compounds (GC/MS) by Method 8260B L823634-01,02,03,04,05,06
Method Blank (MB)
(MB) 03/20/16 01:35
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Acetone ND 0.0500
Acrylonitrile ND 0.0100
Benzene ND 0.00100
Bromodichloromethane ND 0.00100
Bromochloromethane ND 0.00100
Bromoform ND 0.00100
Bromomethane ND 0.00500
Carbon disulfide ND 0.00100
Carbon tetrachloride ND 0.00100
Chlorobenzene ND 0.00100
Chlorodibromomethane ND 0.00100
Chloroethane ND 0.00500
Chloroform ND 0.00500
Chloromethane ND 0.00250
Dibromomethane ND 0.00100
1,2-Dichlorobenzene ND 0.00100
1,4-Dichlorobenzene ND 0.00100
trans-1,4-Dichloro-2-butene ND 0.00250
1,1-Dichloroethane ND 0.00100
1,2-Dichloroethane ND 0.00100
1,1-Dichloroethene ND 0.00100
cis-1,2-Dichloroethene ND 0.00100
trans-1,2-Dichloroethene ND 0.00100
1,2-Dichloropropane ND 0.00100
cis-1,3-Dichloropropene ND 0.00100
trans-1,3-Dichloropropene ND 0.00100
Ethylbenzene ND 0.00100
2-Hexanone ND 0.0100
Iodomethane ND 0.0100
2-Butanone (MEK)ND 0.0100
Methylene Chloride ND 0.00500
4-Methyl-2-pentanone (MIBK)ND 0.0100
Styrene ND 0.00100
1,1,1,2-Tetrachloroethane ND 0.00100
1,1,2,2-Tetrachloroethane ND 0.00100
Tetrachloroethene ND 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857667
Volatile Organic Compounds (GC/MS) by Method 8260B L823634-01,02,03,04,05,06
Method Blank (MB)
(MB) 03/20/16 01:35
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Toluene ND 0.00500
1,1,1-Trichloroethane ND 0.00100
1,1,2-Trichloroethane ND 0.00100
Trichloroethene ND 0.00100
Trichlorofluoromethane ND 0.00500
1,2,3-Trichloropropane ND 0.00250
Vinyl acetate ND 0.0100
Vinyl chloride ND 0.00100
Xylenes, Total ND 0.00300
(S) Toluene-d8 103 90.0-115
(S) Dibromofluoromethane 101 79.0-121
(S) a,a,a-Trifluorotoluene 99.8 90.4-116
(S) 4-Bromofluorobenzene 98.7 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/19/16 23:55 • (LCSD) 03/20/16 00:15
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.125 0.120 0.123 96.3 98.2 28.7-175 1.88 20.9
Acrylonitrile 0.125 0.130 0.130 104 104 58.2-145 0.320 20
Benzene 0.0250 0.0252 0.0251 101 100 73.0-122 0.360 20
Bromodichloromethane 0.0250 0.0265 0.0261 106 105 75.5-121 1.42 20
Bromochloromethane 0.0250 0.0264 0.0249 105 99.4 78.9-123 5.88 20
Bromoform 0.0250 0.0253 0.0250 101 100 71.5-131 1.25 20
Bromomethane 0.0250 0.0274 0.0269 110 108 22.4-187 1.73 20
Carbon disulfide 0.0250 0.0265 0.0254 106 102 53.0-134 4.32 20
Carbon tetrachloride 0.0250 0.0252 0.0242 101 96.7 70.9-129 4.21 20
Chlorobenzene 0.0250 0.0248 0.0249 99.2 99.6 79.7-122 0.340 20
Chlorodibromomethane 0.0250 0.0263 0.0274 105 110 78.2-124 4.00 20
Chloroethane 0.0250 0.0258 0.0244 103 97.7 41.2-153 5.60 20
Chloroform 0.0250 0.0258 0.0247 103 98.8 73.2-125 4.17 20
Chloromethane 0.0250 0.0281 0.0264 112 106 55.8-134 5.98 20
Dibromomethane 0.0250 0.0259 0.0251 104 100 79.5-118 3.19 20
1,2-Dichlorobenzene 0.0250 0.0244 0.0243 97.7 97.1 84.7-118 0.550 20
1,4-Dichlorobenzene 0.0250 0.0234 0.0230 93.7 92.1 82.2-114 1.73 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857667
Volatile Organic Compounds (GC/MS) by Method 8260B L823634-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/19/16 23:55 • (LCSD) 03/20/16 00:15
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
trans-1,4-Dichloro-2-butene 0.0250 0.0256 0.0256 102 102 58.3-129 0.240 20
1,1-Dichloroethane 0.0250 0.0265 0.0254 106 102 71.7-127 4.08 20
1,2-Dichloroethane 0.0250 0.0254 0.0247 101 98.9 65.3-126 2.53 20
1,1-Dichloroethene 0.0250 0.0232 0.0220 93.0 88.2 59.9-137 5.35 20
cis-1,2-Dichloroethene 0.0250 0.0268 0.0257 107 103 77.3-122 4.21 20
trans-1,2-Dichloroethene 0.0250 0.0256 0.0242 103 96.9 72.6-125 5.68 20
1,2-Dichloropropane 0.0250 0.0267 0.0259 107 103 77.4-125 3.40 20
cis-1,3-Dichloropropene 0.0250 0.0269 0.0275 107 110 77.7-124 2.37 20
trans-1,3-Dichloropropene 0.0250 0.0287 0.0302 115 121 73.5-127 4.96 20
Ethylbenzene 0.0250 0.0245 0.0250 98.1 99.9 80.9-121 1.76 20
2-Hexanone 0.125 0.130 0.140 104 112 59.4-151 7.72 20
Iodomethane 0.125 0.119 0.117 94.9 93.4 64.6-137 1.56 20
2-Butanone (MEK)0.125 0.110 0.116 87.9 92.5 46.4-155 5.20 20
Methylene Chloride 0.0250 0.0261 0.0247 105 98.7 69.5-120 5.81 20
4-Methyl-2-pentanone (MIBK)0.125 0.127 0.131 102 105 63.3-138 3.23 20
Styrene 0.0250 0.0256 0.0251 102 100 79.9-124 1.99 20
1,1,1,2-Tetrachloroethane 0.0250 0.0245 0.0246 97.9 98.4 78.5-125 0.530 20
1,1,2,2-Tetrachloroethane 0.0250 0.0234 0.0230 93.6 92.0 79.3-123 1.76 20
Tetrachloroethene 0.0250 0.0239 0.0238 95.5 95.2 73.5-130 0.260 20
Toluene 0.0250 0.0243 0.0240 97.0 96.2 77.9-116 0.870 20
1,1,1-Trichloroethane 0.0250 0.0268 0.0255 107 102 71.1-129 4.89 20
1,1,2-Trichloroethane 0.0250 0.0246 0.0258 98.4 103 81.6-120 4.66 20
Trichloroethene 0.0250 0.0243 0.0240 97.2 95.9 79.5-121 1.37 20
Trichlorofluoromethane 0.0250 0.0253 0.0243 101 97.0 49.1-157 4.21 20
1,2,3-Trichloropropane 0.0250 0.0231 0.0229 92.5 91.7 74.9-124 0.900 20
Vinyl acetate 0.125 0.139 0.141 111 113 41.7-159 1.21 20
Vinyl chloride 0.0250 0.0260 0.0244 104 97.4 61.5-134 6.35 20
Xylenes, Total 0.0750 0.0722 0.0709 96.3 94.6 79.2-122 1.76 20
(S) Toluene-d8 102 103 90.0-115
(S) Dibromofluoromethane 103 98.8 79.0-121
(S) a,a,a-Trifluorotoluene 98.5 94.5 90.4-116
(S) 4-Bromofluorobenzene 99.2 95.5 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857667
Volatile Organic Compounds (GC/MS) by Method 8260B L823634-01,02,03,04,05,06
L823634-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/20/16 03:28 • (MS) 03/20/16 02:07 • (MSD) 03/20/16 02:27
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Acetone 0.125 0.00804 0.148 0.163 112 124 1 25.0-156 9.19 21.5
Acrylonitrile 0.125 ND 0.119 0.125 95.5 100 1 55.9-161 4.82 20
Benzene 0.0250 ND 0.0242 0.0250 96.8 100 1 58.6-133 3.38 20
Bromodichloromethane 0.0250 ND 0.0251 0.0251 100 100 1 69.2-127 0.100 20
Bromochloromethane 0.0250 ND 0.0246 0.0258 98.4 103 1 74.4-128 4.80 20
Bromoform 0.0250 ND 0.0240 0.0249 96.1 99.5 1 66.3-140 3.41 20
Bromomethane 0.0250 ND 0.0252 0.0263 101 105 1 16.6-183 4.31 20.5
Carbon disulfide 0.0250 0.00140 0.0268 0.0283 102 107 1 34.9-138 5.44 20
Carbon tetrachloride 0.0250 ND 0.0238 0.0247 95.4 98.7 1 60.6-139 3.42 20
Chlorobenzene 0.0250 ND 0.0243 0.0244 97.1 97.7 1 70.1-130 0.590 20
Chlorodibromomethane 0.0250 ND 0.0252 0.0259 101 104 1 71.6-132 2.64 20
Chloroethane 0.0250 ND 0.0245 0.0253 98.2 101 1 33.3-155 2.98 20
Chloroform 0.0250 ND 0.0247 0.0252 98.7 101 1 66.1-133 2.20 20
Chloromethane 0.0250 ND 0.0250 0.0253 100 101 1 40.7-139 1.19 20
Dibromomethane 0.0250 ND 0.0244 0.0245 97.4 98.0 1 72.8-127 0.560 20
1,2-Dichlorobenzene 0.0250 ND 0.0233 0.0236 93.2 94.3 1 77.4-127 1.17 20
1,4-Dichlorobenzene 0.0250 ND 0.0225 0.0226 90.1 90.3 1 74.4-123 0.260 20
trans-1,4-Dichloro-2-butene 0.0250 ND 0.0228 0.0239 91.0 95.6 1 57.6-136 4.86 20
1,1-Dichloroethane 0.0250 ND 0.0248 0.0262 99.1 105 1 64.0-134 5.77 20
1,2-Dichloroethane 0.0250 ND 0.0249 0.0257 99.5 103 1 60.7-132 3.11 20
1,1-Dichloroethene 0.0250 ND 0.0222 0.0230 88.8 91.9 1 48.8-144 3.40 20
cis-1,2-Dichloroethene 0.0250 ND 0.0251 0.0260 101 104 1 60.6-136 3.43 20
trans-1,2-Dichloroethene 0.0250 ND 0.0239 0.0251 95.6 100 1 61.0-132 4.78 20
1,2-Dichloropropane 0.0250 ND 0.0249 0.0255 99.4 102 1 69.7-130 2.56 20
cis-1,3-Dichloropropene 0.0250 ND 0.0254 0.0257 102 103 1 71.1-129 0.860 20
trans-1,3-Dichloropropene 0.0250 ND 0.0278 0.0279 111 112 1 66.3-136 0.340 20
Ethylbenzene 0.0250 ND 0.0240 0.0241 95.9 96.3 1 62.7-136 0.420 20
2-Hexanone 0.125 ND 0.135 0.145 108 116 1 59.4-154 7.15 20.1
Iodomethane 0.125 ND 0.113 0.122 90.7 97.4 1 55.2-140 7.17 20
2-Butanone (MEK)0.125 ND 0.120 0.133 96.0 107 1 45.0-156 10.6 20.8
Methylene Chloride 0.0250 0.000357 0.0243 0.0256 95.6 101 1 61.5-125 5.27 20
4-Methyl-2-pentanone (MIBK)0.125 ND 0.116 0.123 92.9 98.1 1 60.7-150 5.47 20
Styrene 0.0250 ND 0.0244 0.0250 97.5 100 1 68.2-133 2.66 20
1,1,1,2-Tetrachloroethane 0.0250 ND 0.0238 0.0241 95.0 96.5 1 70.5-132 1.48 20
1,1,2,2-Tetrachloroethane 0.0250 ND 0.0222 0.0231 88.7 92.6 1 64.9-145 4.26 20
Tetrachloroethene 0.0250 ND 0.0233 0.0233 93.3 93.1 1 57.4-141 0.210 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG857667
Volatile Organic Compounds (GC/MS) by Method 8260B L823634-01,02,03,04,05,06
L823634-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/20/16 03:28 • (MS) 03/20/16 02:07 • (MSD) 03/20/16 02:27
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Toluene 0.0250 ND 0.0232 0.0232 93.0 92.9 1 67.8-124 0.0900 20
1,1,1-Trichloroethane 0.0250 ND 0.0255 0.0264 102 106 1 58.7-134 3.56 20
1,1,2-Trichloroethane 0.0250 ND 0.0234 0.0240 93.7 96.0 1 74.1-130 2.43 20
Trichloroethene 0.0250 ND 0.0235 0.0238 94.2 95.3 1 48.9-148 1.21 20
Trichlorofluoromethane 0.0250 ND 0.0234 0.0245 93.5 98.1 1 39.9-165 4.77 20
1,2,3-Trichloropropane 0.0250 ND 0.0220 0.0225 87.9 90.0 1 71.5-134 2.32 20
Vinyl acetate 0.125 ND 0.139 0.148 111 118 1 42.8-181 6.28 20
Vinyl chloride 0.0250 ND 0.0240 0.0250 96.2 100 1 44.3-143 3.92 20
Xylenes, Total 0.0750 ND 0.0693 0.0712 92.4 95.0 1 65.6-133 2.70 20
(S) Toluene-d8 103 102 90.0-115
(S) Dibromofluoromethane 102 106 79.0-121
(S) a,a,a-Trifluorotoluene 99.2 98.0 90.4-116
(S) 4-Bromofluorobenzene 99.0 98.3 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND,U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
SDL Sample Detection Limit.
MQL Method Quantitation Limit.
Unadj. MQL Unadjusted Method Quantitation Limit.
Qualifier Description
B The same analyte is found in the associated blank.
H The indicated analytical results were generated from a reinjection of the same sample extract or
aliquot.
J The identification of the analyte is acceptable; the reported value is an estimate.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is
low.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Our Locations
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Indiana C-TN-01
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ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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APPENDIX B: TIME SERIES GRAPHS

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2/19/2013 3/16/2016
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9
1/30/2013 3/16/2016
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0510152025303540
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8/23/2000 9/11/2001
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APPENDIX C: NON-PARAMETRIC PREDICTION
INTERVAL INTER-WELL COMPARISONS
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Zinc
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 43.9689%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 105
Maximum Background Value = 260
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 2.56 FALSE
MW-2 3/24/2000 1 50 FALSE
MW-3 9/11/2001 1 50 FALSE
MW-7 3/24/2000 1 50 FALSE
MW-8 3/16/2016 1 2.56 FALSE
MW-9 9/11/2001 1 50 FALSE
MW-9A 3/16/2016 1 2.56 FALSE
MW-11 3/16/2016 1 301 TRUE
MW-5 3/16/2016 1 2.56 FALSE
MW-15A 10/2/2013 1 5.4 FALSE
MW-16 3/16/2016 1 2.56 FALSE
MW-17 6/12/1997 1 50 FALSE
MW-18 3/16/2016 1 2.56 FALSE
MW-14 3/16/2016 1 2.56 FALSE
MW-13R 3/16/2016 1 2.56 FALSE
MW-17R 3/16/2016 1 2.56 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 2.56 FALSE
MW-21 10/2/2013 1 8.4 FALSE
Page 2
MW-22 3/16/2016 1 2.56 FALSE
MW-23 3/16/2016 1 2.56 FALSE
MW-24 10/1/2013 1 2.4 FALSE
MW-25 3/10/2010 1 26 FALSE
MW-26 11/17/2015 1 2.56 FALSE
MW-25R 3/15/2016 1 2.56 FALSE
MW-15 3/16/2016 1 2.56 FALSE
MW-24R 3/16/2016 1 2.56 FALSE
MW-21R 3/16/2016 1 2.56 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Vanadium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 50.3989%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 210
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 29 FALSE
MW-2 3/24/2000 1 40 FALSE
MW-3 9/11/2001 1 40 FALSE
MW-7 3/24/2000 1 40 FALSE
MW-8 3/16/2016 1 2.4 FALSE
MW-9 9/11/2001 1 40 FALSE
MW-9A 3/16/2016 1 2.4 FALSE
MW-11 3/16/2016 1 201 FALSE
MW-5 3/16/2016 1 3.33 FALSE
MW-15A 10/2/2013 1 0.07 FALSE
MW-16 3/16/2016 1 2.4 FALSE
MW-17 6/12/1997 1 40 FALSE
MW-18 3/16/2016 1 7.6 FALSE
MW-14 3/16/2016 1 2.4 FALSE
MW-13R 3/16/2016 1 7.01 FALSE
MW-17R 3/16/2016 1 15.4 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 26.2 FALSE
MW-21 10/2/2013 1 0.07 FALSE
Page 2
MW-22 3/16/2016 1 2.4 FALSE
MW-23 3/16/2016 1 2.4 FALSE
MW-24 10/1/2013 1 0.91 FALSE
MW-25 3/10/2010 1 10.6 FALSE
MW-26 11/17/2015 1 45.9 FALSE
MW-25R 3/15/2016 1 2.4 FALSE
MW-15 3/16/2016 1 2.4 FALSE
MW-24R 3/16/2016 1 4.38 FALSE
MW-21R 3/16/2016 1 4.92 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Selenium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 57.6923%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 20
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 0.38 FALSE
MW-2 3/24/2000 1 20 FALSE
MW-3 9/11/2001 1 39 TRUE
MW-7 3/24/2000 1 20 FALSE
MW-8 3/16/2016 1 0.38 FALSE
MW-9 9/11/2001 1 20 FALSE
MW-9A 3/16/2016 1 0.38 FALSE
MW-11 3/16/2016 1 0.38 FALSE
MW-5 3/16/2016 1 0.38 FALSE
MW-15A 10/2/2013 1 2.1 FALSE
MW-16 3/16/2016 1 0.38 FALSE
MW-17 6/12/1997 1 20 FALSE
MW-18 3/16/2016 1 0.38 FALSE
MW-14 3/16/2016 1 0.38 FALSE
MW-13R 3/16/2016 1 0.38 FALSE
MW-17R 3/16/2016 1 0.38 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 22.6 TRUE
MW-21 10/2/2013 1 1.2 FALSE
Page 2
MW-22 3/16/2016 1 0.38 FALSE
MW-23 3/16/2016 1 0.38 FALSE
MW-24 10/1/2013 1 0.18 FALSE
MW-25 3/10/2010 1 0.4 FALSE
MW-26 11/17/2015 1 0.38 FALSE
MW-25R 3/15/2016 1 0.38 FALSE
MW-15 3/16/2016 1 0.38 FALSE
MW-24R 3/16/2016 1 0.38 FALSE
MW-21R 3/16/2016 1 0.38 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Lead
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 47.2703%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 41
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 9.09 FALSE
MW-2 3/24/2000 1 20 FALSE
MW-3 9/11/2001 1 20 FALSE
MW-7 3/24/2000 1 10 FALSE
MW-8 3/16/2016 1 0.24 FALSE
MW-9 9/11/2001 1 18 FALSE
MW-9A 3/16/2016 1 0.24 FALSE
MW-11 3/16/2016 1 36.1 FALSE
MW-5 3/16/2016 1 0.24 FALSE
MW-15A 10/2/2013 1 0.74 FALSE
MW-16 3/16/2016 1 0.24 FALSE
MW-17 6/12/1997 1 10 FALSE
MW-18 3/16/2016 1 3.91 FALSE
MW-14 3/16/2016 1 2.43 FALSE
MW-13R 3/16/2016 1 3.72 FALSE
MW-17R 3/16/2016 1 4.8 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 4.26 FALSE
MW-21 10/2/2013 1 0.3 FALSE
Page 2
MW-22 3/16/2016 1 0.24 FALSE
MW-23 3/16/2016 1 0.24 FALSE
MW-24 10/1/2013 1 1.1 FALSE
MW-25 3/10/2010 1 6.7 FALSE
MW-26 11/17/2015 1 8.96 FALSE
MW-25R 3/15/2016 1 3.34 FALSE
MW-15 3/16/2016 1 0.24 FALSE
MW-24R 3/16/2016 1 2.07 FALSE
MW-21R 3/16/2016 1 8.95 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Copper
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 53.7061%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 106
Maximum Background Value = 200
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 0.52 FALSE
MW-2 3/24/2000 1 200 FALSE
MW-3 9/11/2001 1 200 FALSE
MW-7 3/24/2000 1 200 FALSE
MW-8 3/16/2016 1 0.52 FALSE
MW-9 9/11/2001 1 200 FALSE
MW-9A 3/16/2016 1 0.52 FALSE
MW-11 3/16/2016 1 42.5 FALSE
MW-5 3/16/2016 1 0.52 FALSE
MW-15A 10/2/2013 1 8.8 FALSE
MW-16 3/16/2016 1 0.52 FALSE
MW-17 6/12/1997 1 200 FALSE
MW-18 3/16/2016 1 0.52 FALSE
MW-14 3/16/2016 1 0.52 FALSE
MW-13R 3/16/2016 1 0.52 FALSE
MW-17R 3/16/2016 1 0.52 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 0.52 FALSE
MW-21 10/2/2013 1 4.4 FALSE
Page 2
MW-22 3/16/2016 1 5.11 FALSE
MW-23 3/16/2016 1 0.52 FALSE
MW-24 10/1/2013 1 4.5 FALSE
MW-25 3/10/2010 1 4.2 FALSE
MW-26 11/17/2015 1 7.64 FALSE
MW-25R 3/15/2016 1 10.3 FALSE
MW-15 3/16/2016 1 0.52 FALSE
MW-24R 3/16/2016 1 0.52 FALSE
MW-21R 3/16/2016 1 19.2 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Cobalt
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 54.244%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 10
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 3.01 FALSE
MW-2 3/24/2000 1 10 FALSE
MW-3 9/11/2001 1 10 FALSE
MW-7 3/24/2000 1 10 FALSE
MW-8 3/16/2016 1 2.76 FALSE
MW-9 9/11/2001 1 10 FALSE
MW-9A 3/16/2016 1 2.3 FALSE
MW-11 3/16/2016 1 6.44 FALSE
MW-5 3/16/2016 1 2.3 FALSE
MW-15A 10/2/2013 1 3.3 FALSE
MW-16 3/16/2016 1 15 TRUE
MW-17 6/12/1997 1 11 TRUE
MW-18 3/16/2016 1 3.01 FALSE
MW-14 3/16/2016 1 4.21 FALSE
MW-13R 3/16/2016 1 4.64 FALSE
MW-17R 3/16/2016 1 13 TRUE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 2.3 FALSE
MW-21 10/2/2013 1 19 TRUE
Page 2
MW-22 3/16/2016 1 2.3 FALSE
MW-23 3/16/2016 1 2.3 FALSE
MW-24 10/1/2013 1 1.3 FALSE
MW-25 3/10/2010 1 1.6 FALSE
MW-26 11/17/2015 1 2.3 FALSE
MW-25R 3/15/2016 1 2.3 FALSE
MW-15 3/16/2016 1 3.58 FALSE
MW-24R 3/16/2016 1 2.3 FALSE
MW-21R 3/16/2016 1 17.2 TRUE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Chromium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 0%
Number of comparisons = 18
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 6
Maximum Background Value = 8.35
Confidence Level = 42.9%
False Positive Rate = 57.1%
Location Date Count Mean Significant
MW-9R 3/16/2016 1 12.1 TRUE
MW-5 3/16/2016 1 4 FALSE
MW-8 3/16/2016 1 1.44 FALSE
MW-9A 3/16/2016 1 1.4 FALSE
MW-10 3/16/2016 1 16.7 TRUE
MW-11 3/16/2016 1 114 TRUE
MW-13R 3/16/2016 1 2.45 FALSE
MW-14 3/16/2016 1 1.4 FALSE
MW-15 3/16/2016 1 1.4 FALSE
MW-16 3/16/2016 1 7.82 FALSE
MW-17R 3/16/2016 1 10.9 TRUE
MW-18 3/16/2016 1 6.94 FALSE
MW-21R 3/16/2016 1 2.9 FALSE
MW-22 3/16/2016 1 1.4 FALSE
MW-23 3/16/2016 1 1.66 FALSE
MW-24R 3/16/2016 1 5.79 FALSE
MW-25R 3/15/2016 1 2.07 FALSE
MW-26 11/17/2015 1 25.3 TRUE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Cadmium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 51.4628%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 6
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 0.16 FALSE
MW-2 3/24/2000 1 18 TRUE
MW-3 9/11/2001 1 1 FALSE
MW-7 3/24/2000 1 1 FALSE
MW-8 3/16/2016 1 0.16 FALSE
MW-9 9/11/2001 1 3 FALSE
MW-9A 3/16/2016 1 0.16 FALSE
MW-11 3/16/2016 1 5.08 FALSE
MW-5 3/16/2016 1 0.16 FALSE
MW-15A 10/2/2013 1 0.2 FALSE
MW-16 3/16/2016 1 0.16 FALSE
MW-17 6/12/1997 1 1 FALSE
MW-18 3/16/2016 1 0.16 FALSE
MW-14 3/16/2016 1 0.16 FALSE
MW-13R 3/16/2016 1 0.16 FALSE
MW-17R 3/16/2016 1 0.16 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 0.16 FALSE
MW-21 10/2/2013 1 0.19 FALSE
Page 2
MW-22 3/16/2016 1 0.16 FALSE
MW-23 3/16/2016 1 0.16 FALSE
MW-24 10/1/2013 1 0.05 FALSE
MW-25 3/10/2010 1 0.4 FALSE
MW-26 11/17/2015 1 0.16 FALSE
MW-25R 3/15/2016 1 0.16 FALSE
MW-15 3/16/2016 1 0.16 FALSE
MW-24R 3/16/2016 1 0.16 FALSE
MW-21R 3/16/2016 1 0.16 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Benzene
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 63.0667%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 101
Maximum Background Value = 5
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 0.331 FALSE
MW-2 3/24/2000 1 5 FALSE
MW-3 9/11/2001 1 5 FALSE
MW-7 3/24/2000 1 5 FALSE
MW-8 3/16/2016 1 0.331 FALSE
MW-9 9/11/2001 1 5 FALSE
MW-9A 3/16/2016 1 1.12 FALSE
MW-11 3/16/2016 1 0.331 FALSE
MW-5 3/16/2016 1 0.331 FALSE
MW-15A 10/2/2013 1 1.8 FALSE
MW-16 3/16/2016 1 0.331 FALSE
MW-17 6/12/1997 1 5 FALSE
MW-18 3/16/2016 1 0.331 FALSE
MW-14 3/16/2016 1 0.331 FALSE
MW-13R 3/16/2016 1 1.97 FALSE
MW-17R 3/16/2016 1 0.331 FALSE
MW-5A 10/21/2011 1 0.24 FALSE
MW-9B 3/24/2000 1 5 FALSE
MW-9R 3/16/2016 1 0.331 FALSE
MW-21 10/2/2013 1 0.9 FALSE
Page 2
MW-22 3/16/2016 1 0.331 FALSE
MW-23 3/16/2016 1 0.331 FALSE
MW-24 10/1/2013 1 0.24 FALSE
MW-25 3/10/2010 1 0 FALSE
MW-26 11/17/2015 1 0.331 FALSE
MW-25R 3/15/2016 1 0.331 FALSE
MW-15 3/16/2016 1 1.53 FALSE
MW-24R 3/16/2016 1 0.331 FALSE
MW-21R 3/16/2016 1 0.331 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Barium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 50.9259%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 500
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 86.8 FALSE
MW-2 3/24/2000 1 500 FALSE
MW-3 9/11/2001 1 500 FALSE
MW-7 3/24/2000 1 500 FALSE
MW-8 3/16/2016 1 63.2 FALSE
MW-9 9/11/2001 1 500 FALSE
MW-9A 3/16/2016 1 77.7 FALSE
MW-11 3/16/2016 1 167 FALSE
MW-5 3/16/2016 1 16.2 FALSE
MW-15A 10/2/2013 1 58.6 FALSE
MW-16 3/16/2016 1 282 FALSE
MW-17 6/12/1997 1 500 FALSE
MW-18 3/16/2016 1 123 FALSE
MW-14 3/16/2016 1 238 FALSE
MW-13R 3/16/2016 1 140 FALSE
MW-17R 3/16/2016 1 128 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 66.6 FALSE
MW-21 10/2/2013 1 32.1 FALSE
Page 2
MW-22 3/16/2016 1 53.4 FALSE
MW-23 3/16/2016 1 9.07 FALSE
MW-24 10/1/2013 1 38.2 FALSE
MW-25 3/10/2010 1 13.7 FALSE
MW-26 11/17/2015 1 97.5 FALSE
MW-25R 3/15/2016 1 29.4 FALSE
MW-15 3/16/2016 1 76 FALSE
MW-24R 3/16/2016 1 41.4 FALSE
MW-21R 3/16/2016 1 161 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Arsenic
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 53.6521%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 10
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 2.33 FALSE
MW-2 3/24/2000 1 35 TRUE
MW-3 9/11/2001 1 10 FALSE
MW-7 3/24/2000 1 10 FALSE
MW-8 3/16/2016 1 3.47 FALSE
MW-9 9/11/2001 1 10 FALSE
MW-9A 3/16/2016 1 0.25 FALSE
MW-11 3/16/2016 1 5.32 FALSE
MW-5 3/16/2016 1 2.02 FALSE
MW-15A 10/2/2013 1 6.2 FALSE
MW-16 3/16/2016 1 11.4 TRUE
MW-17 6/12/1997 1 10 FALSE
MW-18 3/16/2016 1 0.25 FALSE
MW-14 3/16/2016 1 0.25 FALSE
MW-13R 3/16/2016 1 0.25 FALSE
MW-17R 3/16/2016 1 0.25 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 0.25 FALSE
MW-21 10/2/2013 1 2.4 FALSE
Page 2
MW-22 3/16/2016 1 0.25 FALSE
MW-23 3/16/2016 1 0.25 FALSE
MW-24 10/1/2013 1 0.41 FALSE
MW-25 3/10/2010 1 3.3 FALSE
MW-26 11/17/2015 1 0.25 FALSE
MW-25R 3/15/2016 1 2.23 FALSE
MW-15 3/16/2016 1 0.25 FALSE
MW-24R 3/16/2016 1 0.25 FALSE
MW-21R 3/16/2016 1 53.3 TRUE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Acetone
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 68.8172%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 101
Maximum Background Value = 100
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 10 FALSE
MW-2 3/24/2000 1 100 FALSE
MW-3 9/11/2001 1 100 FALSE
MW-7 3/24/2000 1 100 FALSE
MW-8 3/16/2016 1 10 FALSE
MW-9 9/11/2001 1 100 FALSE
MW-9A 3/16/2016 1 10 FALSE
MW-11 3/16/2016 1 10 FALSE
MW-5 3/16/2016 1 10 FALSE
MW-15A 10/2/2013 1 52.7 FALSE
MW-16 3/16/2016 1 10 FALSE
MW-17 6/12/1997 1 100 FALSE
MW-18 3/16/2016 1 10 FALSE
MW-14 3/16/2016 1 10 FALSE
MW-13R 3/16/2016 1 10 FALSE
MW-17R 3/16/2016 1 10 FALSE
MW-5A 10/21/2011 1 9.06 FALSE
MW-9B 3/24/2000 1 100 FALSE
MW-9R 3/16/2016 1 10 FALSE
MW-21 10/2/2013 1 821 TRUE
Page 2
MW-22 3/16/2016 1 10 FALSE
MW-23 3/16/2016 1 10 FALSE
MW-24 10/1/2013 1 9.06 FALSE
MW-25 3/10/2010 1 65.1 FALSE
MW-26 11/17/2015 1 10 FALSE
MW-25R 3/15/2016 1 10 FALSE
MW-15 3/16/2016 1 10 FALSE
MW-24R 3/16/2016 1 10 FALSE
MW-21R 3/16/2016 1 2950 TRUE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: 1,4-Dichlorobenzene
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 60.425%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 101
Maximum Background Value = 5
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 0.274 FALSE
MW-2 3/24/2000 1 5 FALSE
MW-3 9/11/2001 1 5 FALSE
MW-7 3/24/2000 1 5 FALSE
MW-8 3/16/2016 1 1.63 FALSE
MW-9 9/11/2001 1 5 FALSE
MW-9A 3/16/2016 1 7.62 TRUE
MW-11 3/16/2016 1 0.274 FALSE
MW-5 3/16/2016 1 4.9 FALSE
MW-15A 10/2/2013 1 8.9 TRUE
MW-16 3/16/2016 1 0.274 FALSE
MW-17 6/12/1997 1 5 FALSE
MW-18 3/16/2016 1 0.274 FALSE
MW-14 3/16/2016 1 0.274 FALSE
MW-13R 3/16/2016 1 1.06 FALSE
MW-17R 3/16/2016 1 0.274 FALSE
MW-5A 10/21/2011 1 0.39 FALSE
MW-9B 3/24/2000 1 5 FALSE
MW-9R 3/16/2016 1 0.274 FALSE
MW-21 10/2/2013 1 0.6 FALSE
Page 2
MW-22 3/16/2016 1 0.274 FALSE
MW-23 3/16/2016 1 0.274 FALSE
MW-24 10/1/2013 1 0.39 FALSE
MW-25 3/10/2010 1 0 FALSE
MW-26 11/17/2015 1 0.274 FALSE
MW-25R 3/15/2016 1 0.274 FALSE
MW-15 3/16/2016 1 5.44 TRUE
MW-24R 3/16/2016 1 0.274 FALSE
MW-21R 3/16/2016 1 0.274 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: 1,1-Dichloroethane
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 41.1765%
Number of comparisons = 29
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 101
Maximum Background Value = 5
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 3/16/2016 1 1.41 FALSE
MW-2 3/24/2000 1 7 TRUE
MW-3 9/11/2001 1 5 FALSE
MW-7 3/24/2000 1 5 FALSE
MW-8 3/16/2016 1 3.28 FALSE
MW-9 9/11/2001 1 5 FALSE
MW-9A 3/16/2016 1 9.31 TRUE
MW-11 3/16/2016 1 0.259 FALSE
MW-5 3/16/2016 1 3.78 FALSE
MW-15A 10/2/2013 1 4.6 FALSE
MW-16 3/16/2016 1 0.259 FALSE
MW-17 6/12/1997 1 5 FALSE
MW-18 3/16/2016 1 0.259 FALSE
MW-14 3/16/2016 1 0.259 FALSE
MW-13R 3/16/2016 1 0.259 FALSE
MW-17R 3/16/2016 1 0.259 FALSE
MW-5A 10/21/2011 1 0.2 FALSE
MW-9B 3/24/2000 1 5 FALSE
MW-9R 3/16/2016 1 0.259 FALSE
MW-21 10/2/2013 1 0.3 FALSE
Page 2
MW-22 3/16/2016 1 0.259 FALSE
MW-23 3/16/2016 1 0.259 FALSE
MW-24 10/1/2013 1 0.2 FALSE
MW-25 3/10/2010 1 0 FALSE
MW-26 11/17/2015 1 0.259 FALSE
MW-25R 3/15/2016 1 0.259 FALSE
MW-15 3/16/2016 1 3.26 FALSE
MW-24R 3/16/2016 1 0.259 FALSE
MW-21R 3/16/2016 1 0.259 FALSE