9801_WilsonCountyMSWLF_GWMR_26302_20160511

May 12, 2016

Mr. Ervin Lane, Hydrogeologist
NC Division of Waste Management
Solid Waste Section
Mail Service Center 1646
Raleigh, NC 27699-1646

Re: 2016 First Semi-Annual Water Quality Monitoring Results
Closed Wilson County Landfill
Wilson, North Carolina
Permit #98-01

Dear Ervin:

Babb & Associates, P.A. has completed the 2016 first semi-annual sampling event at the closed Wilson
County Landfill. On April 29, 2016, nine groundwater monitoring wells and five surface water monitoring
stations were sampled and analyzed for volatile organic compounds (VOCs) by EPA Method 8260 and
Appendix I inorganic compounds.

A site map is provided with this report which shows the groundwater and surface water sample locations
and shallow potentiometric surface. Additional attachments to this report include tables summarizing the
groundwater and surface water analytical results (Tables 1 & 2), field parameters collected during the
monitoring event (Table 3), well construction information (Table 4), and groundwater flow rates (Table 5).
The laboratory analytical report, in pdf and EDD formats, is included as Appendix A.

If there are any questions regarding the attached information, please contact me at [phone].

Respectfully,

Babb & Associates, P.A.

Gary D. Babb, P.G.
President

Enclosures

cc: Mr. Andy Davis, Director
Wilson County Solid Waste

Water Quality Monitoring Report

Wilson County Municipal Solid Waste Landfill
4537 Landfill Road
Wilson, North Carolina
Permit No. 98-01

Prepared for:

Wilson County Solid Waste
P.O. Box 1728
Wilson, North Carolina 27894

Prepared by:

Babb & Associates, P.A.
P.O. Box 37697
Raleigh, North Carolina 27627

April 2016

___________________________________
Gary D. Babb, Licensed Geologist

Table of Contents

1.0 Introduction 1
1.1 Site Information
1.2 Site Geology
1.3 Site Hydrogeology

2.0 Water Quality Monitoring Program 5
2.1 Groundwater Monitoring Network
2.2 Surface Water Monitoring Network

3.0 Water Quality Sample Collection 7
3.1 Field Sample Procedures
3.2 Field Quality Assurance
3.3 Sample Delivery/Chain-of-Custody

4.0 Laboratory Analysis 9

5.0 Hydrogeological Conditions 10

6.0 Laboratory Analytical Results 11
6.1 Groundwater Analytical Results
6.2 Surface Water Analytical Results
6.3 Quality Control Sample

7.0 Conclusions 13

Figure 1 Water Quality Monitoring Sample Locations/Potentiometric Map

Table 1 Groundwater Analytical Results
Table 2 Surface Water Analytical Results
Table 3 Field Parameter Measurements
Table 4 Well Construction Information/Elevations
Table 5 Groundwater Flow Rates

Appendix A ENCO Laboratory Analytical Report

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 1

1.0 Introduction

1.1 Site Information

The closed Wilson County Landfill is located approximately 3.5 miles east of downtown
Wilson, NC at the intersection of NC 42 and Tucker Court. Originally, the site
containing the closed Wilson County Landfill facility was dominated by a hill
(approximately 108 feet above msl) located in the central portion of the present site.
Several residential/farm houses were located in the northeast portion of the site. An
intermittent stream originating in the northern portion of the site flowed southeastward
eventually flowing into an unnamed stream southeast of the site. This unnamed stream
flowed westward becoming part of the southern site boundary and traversed the
southwestern most portion of the site and emptied into the Toisnot Swamp Canal. The
remainder of the site contained drainage features that radiated outward from the dominant
hill and discharged into these streams or with other drainage features located to the
northwest of the site. Wetland areas were associated with streams and the Toisnot
Swamp. Prior to construction of the landfill facility, agriculture was the primary land use
in this area of Wilson County.

Surrounding properties within 1,500 feet of the site are currently being used for farming,
residential, or solid waste management purposes. Land south of the site is mostly
farmland with a mobile home park located approximately 1,200 feet to the south. Land
immediately west of the site is owned by Wilson County and used for construction and
demolition debris disposal, recycling/reclaimation, and other solid waste management
activities. Land north of the site is mostly used for farmland with wooded areas. Land
east of the site is mostly farmland with wooded areas and light residential use.

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 2

1.2 Site Geology

The closed Wilson County Landfill is located in the western portion of the Carolina
Coastal Plain near the Fall Line. The Fall Line is the province boundary between the
Piedmont and the Coastal Plain provinces. It represents a significant change in lithology,
which in turn reflects a change in stream gradients. Lithology of the Piedmont province
is primarily igneous and metamorphic while the Coastal Plain province is primarily
sedimentary. In general, rivers and streams in the Piedmont Province have higher flow
rates with well defined channels while Coastal Plain rivers and streams are meandering
with lesser defined channels resulting in swamps and bays. These streams, swamps, and
bays are the major discharge point of the uppermost aquifer.

The Carolina Coastal Plain is underlain by flat-lying to very gently eastward dipping
sedimentary strata which overlay a foundation of crystalline rocks. These sediments
were deposited during repeated marine transgressive and regressive cycles due to
fluctuations in sea level caused by expansion and recession of glacial ice caps during the
Pliocene and early Pleistocene epochs (approximately 2 to 5 million years ago).

Sediments in the area of the closed Wilson County Landfill facility are classified as being
in the Yorktown Formation. Information gathered from the Geologic Map of North
Carolina, 1985 and The Geology of the Carolina, 1991, cites that sediments of the
Yorktown Formation are fossiliferous clay with varying amounts of fine-grained sand,
silty sand, sandy silt, silty clay, and bluish gray shell material. These types of deposits
are found mainly north of the Neuse River and are commonly concentrated in lenses and
vary in vertical and horizontal dimensions. The topography of the Coastal Plain is
characterized by flat to gently undulating relief.

The local geology is characterized by relatively thin layers (0.5 - 7.0 feet) of clays, silts,
and sands in varying textures and colors that overlie a gray/black silty clay/sand that is
found throughout the area. The drainage canals located on the northwest and southeast
Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 3

property boundaries expose these silty clay and sand layers. The original soils at the site
were excavated to create capacity for waste disposal.

1.3 Site Hydrogeology

The major groundwater discharge features influencing groundwater flow direction at the
site are the Toisnot Swamp and drainage ditches located to the southeast and northwest of
the site. Groundwater level measurements collected on April 20, 2016 indicate that the
general groundwater flow direction on the facility is to the south-southeast towards the
Toisnot Swamp Canal. However, the presence of drainage ditches have an impact on
localized groundwater flow. Groundwater flow near the southeastern drainage ditch
tends to be in a more southerly direction towards the drainage ditch. A Potentiometric
Map indicating groundwater flow directions is provided as Figure 1.

Aquifer hydraulic conductivity testing was performed in June 1997 on five of the site
monitoring wells and consisted of rising and falling head tests (slug tests). The results of
the slug test data was analyzed using the Bouwer and Rice method and are summarized
on the table below:

WELL ID HYDRAULIC
CONDUCTIVITY
(centimeters/second)
TYPE OF TEST FORMATION
MW-3A 3.80 x 10-5 Falling Yorktown
P-3 1.27 x 10-4 Rising Alluvium/Yorktown
MW-4 1.01 x 10-4 Rising Alluvium
MW-4 5.89 x 10-4 Falling Alluvium
MW-5 8.50 x 10-5 Rising Alluvium
MW-5 2.06 x 10-4 Falling Alluvium
MW-6 1.85 x 10-4 Rising Yorktown
MW-6 6.53 x 10-4 Falling Yorktown
MW-7 1.66 x 10-4 Rising Alluvium
MW-7 1.95 x 10-4 Falling Alluvium

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 4

The geometric average of the shallow water table aquifer hydraulic conductivity is 2.56 x
10-4 cm/sec (0.73 feet per day). This value may be considered a reasonable estimate of
the hydraulic conductivity of the shallow water table aquifer at the closed Wilson County
Landfill site.

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 5

2.0 Water Quality Monitoring Program

The water quality monitoring network at the closed Wilson County Landfill is evaluated on a
semi-annual basis. The location of the groundwater and surface water samples collected during
the semi-annual monitoring events is shown on the attached Figure 1.

2.1 Groundwater Monitoring Network

There are nine groundwater monitoring wells located at the facility that comprise the
existing groundwater monitoring system (Figure 1). Monitoring well MW-1A is located
to the northwest of the landfill area and serves as the sidegradient groundwater
monitoring well. This well is situated on the northwest edge of the drainage ditch that
separates the former fill and borrow areas. Monitoring well MW-2 is located at the
entrance to the landfill at Landfill Road (SR 1503) and serves as the upgradient
groundwater monitoring well providing background water quality. Monitoring well
MW-3 is located on the landfill side of the drainage ditch on the southeast property
boundary of the landfill. Monitoring well MW-3A, added in 2004, is also located on the
southeastern side of the landfill but on the opposite side of the drainage ditch.
Monitoring wells MW-4 and MW-5 are both located to the southwest and downgradient
of the landfill but hydraulically upgradient of the Toisnot Swamp Canal. Monitoring
wells MW-6 and MW-7 are located on the southeast border of the landfill. Monitoring
well MW-8 is considered a side-gradient monitoring well to the west of the former
landfill area.

Table 4 provides monitoring well construction information including installation date,
well depth/screened interval, survey elevations, and lat/long for each well location. Table
5 provides the estimated hydraulic conductivity values for select monitoring wells based
on falling/rising head slug tests.

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 6

2.2 Surface Water Monitoring Network

There are presently five surface water monitoring stations associated with the closed
Wilson County Landfill. Surface water monitoring stations SW-1 and SW-2 are both
located on the Toisnot Swamp Canal. The upstream sampling location (SW-1) is located
approximately 400 feet northwest of the landfill property boundary. The downstream
sampling location (SW-2) is located approximately 1,100 feet southeast of the landfill
property boundary. The drainage canal located along the southeastern boundary of the
landfill is monitored with surface water stations SW-3 and SW-4. The drainage canal
located on the northwestern boundary of the landfill is monitoring with surface water
station SW-5. These surface water monitoring locations are shown on Figure 1.

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 7

3.0 Water Quality Sample Collection

Samples of groundwater and surface water were collected in accordance with the approved
Wilson County 1996 Water Quality Monitoring Plan and the 2008 NC Solid Waste Section
Guidelines for Groundwater, Soil, and Surface Water Sampling Guidance Document. A brief
description of the sample collection procedure is provided below.

3.1 Field Sample Procedures

Prior to groundwater sampling, water levels were obtained from each well using an
electric water level meter capable of measuring the depth to water to the nearest 0.01 feet.
This information was later used to determine the elevation of the water table in each
monitoring well relative to surveyed datum (Table 3). The depth to water in each well
was also used to determine the volume of standing water in the well casing. This
information allowed for the purging of a minimum of three casing volumes from each
well prior to sample collection to assure a fresh groundwater sample was collected. New
disposable laboratory gloves were worn by sampling personnel and each well was purged
and sampled with a new disposable bailer which was discarded after use.

After the monitoring wells had been allowed to recover from purging, samples were
collected in the following order:

 Volatile organic compounds
 Inorganic compounds
 Field Parameters (pH, Conductivity, Temperature)

The samples are collected directly in the laboratory-supplied containers which are pre-
filled with the appropriate preservative. No filtering of the samples is performed prior to
collection. After collection, the samples are placed in a cooler on ice for overnight
shipment to the analytical laboratory.

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 8

Surface water samples are collected directly into the laboratory-supplied containers as
grab samples. Sampling personnel wear new disposable laboratory gloves for each
surface water sample collected. As with the groundwater samples, these samples are
stored in a cooler on ice prior to overnight delivery to the analytical laboratory.

3.2 Field Quality Assurance

One trip blank sample was prepared by the analytical laboratory and accompanied the
sample shipment until receipt back at the laboratory. The trip blank sample was analyzed
for volatile organic compounds only. Temperature blanks are also provided with the
sample shipments to assure the proper temperature is maintained until delivery to the
analytical laboratory.

3.3 Sample Delivery/Chain of Custody

All groundwater and surface water samples are stored in coolers on ice immediately after
collection. Individual sample containers for each well or surface water sample are placed
in zip lock plastic bags to reduce the potential for cross contamination. Chain-of-Custody
control documents are prepared and shipped with each cooler. Custody seals are also
used for each cooler to maintain sample integrity until delivery to the analytical
laboratory. The sample coolers are shipped via Federal Express for next morning
delivery to the analytical laboratory.

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 9

4.0 Laboratory Analysis

The samples were analyzed for parameters specified by the Solid Waste Section for Detection
Monitoring at permitted solid waste facilities. The standard Detection Monitoring Program for
groundwater and surface water samples consists of the Appendix I parameters. The Appendix I
analysis consists of volatile organic compounds by EPA Method 8260B and inorganic
compounds by EPA Methods 6010C/6020A.

The laboratory performing the water quality analysis is Environmental Conservation
Laboratories, Inc. (ENCO) of Cary, North Carolina, which is a NC Certified Laboratory.
Internal quality control samples, including matrix spikes/matrix spike duplicates, are performed
by ENCO for each set of samples. The ENCO laboratory report, including internal quality
control samples, is provided with this report in Appendix A.

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 10

5.0 Hydrogeological Conditions

The depth to groundwater was measured in the nine compliance monitoring wells during the
April 20, 2016 monitoring event. The groundwater elevations were calculated relative to the
surveyed measuring point (top of casing) for each monitoring well. The groundwater elevations
are summarized on Table 3 and the potentiometric surface of the shallow water table is shown on
Figure 1.

The general direction of groundwater flow, based on the water level information collected during
this monitoring event, is also shown on Figure 1. Groundwater flow direction is generally to the
south-southwest, toward the Toisnot Swamp Canal.

Based on the results of prior hydrologic tests conducted at the site, the groundwater flow rate in
the shallow saprolite ranges from 0.108 ft/day to 1.85 ft/day. The average hydraulic conductivity
and transmissivity values for the site are provided on Table 5.

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 11

6.0 Laboratory Analytical Results

Final laboratory analytical results for the samples collected on April 20, 2016 were received
from the analytical laboratory on May 5, 2016. A summary of the analytical results are provided
on Table 1 (groundwater), Table 2 (surface water), and Table 3 (field parameters).

6.1 Groundwater Analytical Results

During this monitoring event, no volatile organic compounds (VOCs) were detected at
concentrations exceeding the Solid Waste Section Limits (SWSLs) or the 2L
Groundwater Standards in any of the nine groundwater monitoring wells.

Only two inorganic compounds were detected at a concentration that exceeded the 2L
Groundwater Standards. The concentration of barium in monitoring well MW-5 (700
ug/l) equaled the 2L Groundwater Standard of 700 ug/l. The concentration of arsenic in
monitoring well MW-4 (10.0 ug/l) also equaled the 2L Groundwater Standard of 10 ug/l.
No other inorganic compounds were detected above the 2L Groundwater Standards in
any of the other seven groundwater monitoring wells sampled during this monitoring
event.

The inorganic compound barium was reported above the laboratory detection limit and
SWSL in monitoring wells MW-1A, MW-3, MW-3A, MW-4, and MW-7; however, the
concentrations did not exceed the established 2L Groundwater Standard. Monitoring
wells MW-3, MW-6, and MW-8 reported detectable concentrations of zinc, although the
concentrations were well below the established 2L Groundwater Standard. Monitoring
wells MW-3 and MW-6 reported detectable concentrations of beryllium, both of which
were below the established 2L Groundwater Standard. Monitoring well MW-6 also
reported a detectable concentration of cobalt, which does not have an established 2L
Groundwater Standard. A summary of the groundwater laboratory analytical results is
provided on Table 1.

Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 12

6.2 Surface Water Analytical Results

During sampling of the five surface water monitoring stations, no VOCs were reported in
any of the surface water samples collected above the SWSLs, laboratory detection limits,
or 2B Surface Water Standards.

The inorganic compound zinc was reported above the laboratory detection limit in four of
the five surface water samples with the reported concentration in SW-3 (64.7 ug/l)
slightly above the 2B Surface Water Standard for zinc of 50 ug/l. The inorganic
compound cobalt was reported in SW-3 (16.1 ug/l), SW-4 (15.3 ug/l), and SW-5 (37.0
ug/l) at concentrations which exceed the 2B Surface Water Standard for cobalt of 3.0
ug/l. The inorganic compound lead was reported in surface water sample SW-3 at a
concentration of 26.5 ug/l which slightly exceeds the 2B Surface Water Standard for lead
of 25.0 ug/l.

The inorganic compound barium was reported above the laboratory detection limit in
SW-2, SW-3, SW-4, and SW-5; however, the reported concentrations were well below
the established 2B Surface Water Standard for barium. The inorganic compound
beryllium was reported in surface water sample SW-3 at a concentration of 1.17 ug/l
which is below the 2B Surface Water Standard for beryllium of 6.5 ug/l. No other
inorganic compounds were reported above the laboratory detection limits or 2B Surface
Water Standards in the samples collected from the five surface water monitoring stations.
A summary of the surface water analytical results for the five surface water samples is
provided on Table 2.

6.3 Quality Control Sample

One trip blank was submitted and analyzed for quality assurance purposes. No VOCs
were detected at a concentration equaling or exceeding laboratory quantitation limits in
the trip blank.
Wilson County Closed Landfill Water Quality Monitoring Report
April 2016 Page 13

7.0 Conclusions

The results of this monitoring event report only minor variants from the established 2L
Groundwater Standards and 2B Surface Water Standards. Based on the results of this water
quality monitoring event, the closed Wilson County Landfill will remain in Detection
Monitoring in accordance with Title 15A NACA 13B .0601. The 2016 fall semi-annual water
quality monitoring event is tentatively scheduled for October 2016.

Attachments to this report include tables summarizing the groundwater and surface water
analytical results (Tables 1 & 2), field parameters collected during the monitoring event (Table
3), well construction information (Table 4), and hydrologic test results (Table 5). A copy of the
laboratory analytical report in pdf and EDD formats is included with this report in Appendix A.

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MW
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MW
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7
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MW
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7
8

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8
MW
-
4

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7

2
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6

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1
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MW
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8

4
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7
8

8
2
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3
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6
7
8

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5
.
7

6
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4
MW
-
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6

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1
0
6

2
1
.
7
0

8
7
.
7
6

5
4
9

1
7
.
6

5
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4
MW
-
7

4
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3
7

7
.
5
3

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3
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SW
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7

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A

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4
7

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7
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1

7
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6
SW
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2

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8

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SW
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2
SW
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0

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SW
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#
9
8
-
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1
We
l
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D
Da
t
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Dr
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We
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Di
a
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To
t
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De
p
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De
p
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Sc
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In
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El
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El
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Gr
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De
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La
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y
MW
-
1
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4

2
"

3
0
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0
'

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5
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0
'

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5
'

-

3
0
'

1
0
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1
0

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3
9

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5
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7
3
0
5
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1

N

23
4
0
1
4
6
.
2
1

E
silty sandy CLAY
MW
-
2

4
/
2
6
/
8
9

2
"

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4
.
0
'

4
.
0
'

4
'

-

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4
'

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1
8
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3
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1
3
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6
8
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7
5
7
5
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7
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23
4
2
7
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6
.
0
1

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silty sandy CLAY
MW
-
3

6
/
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2
"

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5
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'

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7
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6
6
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5
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8
6

N

23
4
1
6
8
6
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9
9

E
fine SAND
MW
-
3
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5
/
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9
7

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4
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4
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4
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23
4
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9
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med. grey SILT
MW
-
4

4
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6
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8
9

2
"

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3
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.
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3
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3
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8
2
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8
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4
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2
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5
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1
7

N

23
3
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4
3
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8
5

E
silty sandy CLAY
MW
-
5

4
/
2
6
/
8
9

2
"

1
3
.
0
'

3
.
0
'

3
'

-

1
3
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8
5
.
4
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7
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4
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9
5
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8
2

N

23
3
9
0
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8
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9
8

E
silty sandy CLAY
MW
-
6

5
/
1
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/
9
7

2
"

2
8
.
0
'

1
8
.
0
'

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8
'

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2
8
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1
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0
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4
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7
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7
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6
1
6
9
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9
0

N

23
4
1
2
8
5
.
5
5

E
f. to coarse SAND
MW
-
7

5
/
1
5
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9
7

2
"

1
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6
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8
3
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5
9

N

23
4
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2
7
8
.
9
1

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silty sandy CLAY
MW
-
8

6
/
3
/
0
4

2
"

2
0
.
0
'

5
.
0
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5
'

-

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8
9
.
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9
2
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2
6

8
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8
3
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5
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71
6
7
0
7
.
9
7

N

23
3
9
5
4
5
.
8
9

E
coarse SAND
TO
S

-

T
o
p

o
f

S
c
r
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n
TO
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T
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5
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1
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t
y

M
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L
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f
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,

N
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t
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C
a
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a
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m
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t

#
9
8
-
0
1
Te
s
t

P
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2
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(c
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)
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t
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v
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t
y

(f
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t
/
d
a
y
)
Geologic Material
MW
-
3
A

F
a
l
l
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n
g

H
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d

3
.
8
0

x

1
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0.
1
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8

m
e
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.

g
r
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S
I
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T
MW
-
4

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1
.
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1

x

1
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2
2
7

s
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t
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s
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-
4

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5
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9

x

1
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6
7

s
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t
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s
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C
L
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5

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x

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4

s
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MW
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5

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2
.
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x

1
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5
8
5

s
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t
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s
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C
L
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MW
-
6

R
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1
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5

x

1
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-4
0.
5
2
4

f
.

t
o

c
o
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s
e

S
A
N
D
MW
-
6

F
a
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g

H
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6
.
5
3

x

1
0
-4
1.
8
5

f
.

t
o

c
o
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r
s
e

S
A
N
D
MW
-
7

R
i
s
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n
g

H
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1
.
6
6

x

1
0
-4
0.
4
7
1

s
i
l
t
y

s
a
n
d
y

C
L
A
Y
MW
-
7

F
a
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n
g

H
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1
.
9
5

x

1
0
-4
0.
5
5
3

s
i
l
t
y

s
a
n
d
y

C
L
A
Y
1
D
a
t
a

f
r
o
m

J
u
n
e

2
0
0
3

G
r
o
u
n
d
w
a
t
e
r

a
n
d

S
u
r
f
a
c
e

W
a
t
e
r

A
s
s
e
s
s
m
e
n
t

Re
p
o
r
t
2

A
q
u
i
f
e
r

T
e
s
t
i
n
g

b
y

f
a
l
l
i
n
g
/
r
i
s
i
n
g

h
e
a
d

s
l
u
g

t
e
s
t
s
,

a
n
a
l
y
z
e
d

us
i
n
g

B
o
u
w
e
r

a
n
d

R
i
c
e

m
e
t
h
o
d

LAB REPORT

102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): CZ05055
Raleigh, NC 27606
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Wilson County MSWLF
Attn: Gary Babb
Babb & Associates (BA024)
3605 Country Cove Lane
Bill Scott
Project Manager
Thursday, May 5, 2016
RE: Laboratory Results for
Dear Gary Babb,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, April 21, 2016.
The total number of pages in this report, including this page is 64.
Page 1 of 67
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
9801-MW1A CZ05055-01 Sampled:04/20/16 08:39 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 12:55
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 13:07
EPA 8260B 05/04/16 05/01/16 12:15 5/2/2016 13:31
9801-MW2 CZ05055-02 Sampled:04/20/16 11:49 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 12:58
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 13:41
EPA 8260B 05/04/16 05/01/16 12:15 5/2/2016 14:01
9801-MW3 CZ05055-03 Sampled:04/20/16 11:26 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:01
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 13:45
EPA 8260B 05/04/16 05/01/16 12:15 5/2/2016 15:00
9801-MW3A CZ05055-04 Sampled:04/20/16 11:33 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:03
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 13:48
EPA 8260B 05/04/16 05/01/16 12:15 5/2/2016 15:32
9801-MW4 CZ05055-05 Sampled:04/20/16 09:27 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:18
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 13:52
EPA 8260B 05/04/16 05/03/16 11:13 5/3/2016 18:45
9801-MW5 CZ05055-06 Sampled:04/20/16 09:48 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:21
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 13:55
EPA 8260B 05/04/16 05/03/16 11:13 5/3/2016 19:14
9801-MW6 CZ05055-07 Sampled:04/20/16 11:06 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:24
EPA 8260B 05/04/16 05/01/16 12:15 5/2/2016 17:07
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9801-MW6 CZ05055-07RE1 Sampled:04/20/16 11:06 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 14:41
9801-MW7 CZ05055-08 Sampled:04/20/16 10:37 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:27
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 14:03
EPA 8260B 05/04/16 05/02/16 12:38 5/3/2016 10:12
9801-MW8 CZ05055-09 Sampled:04/20/16 08:50 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:29
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 14:06
EPA 8260B 05/04/16 05/03/16 11:13 5/3/2016 19:43
9801-SW1 CZ05055-10 Sampled:04/20/16 09:57 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:32
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 14:10
EPA 8260B 05/04/16 05/02/16 12:38 5/3/2016 11:10
9801-SW2 CZ05055-11 Sampled:04/20/16 09:39 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:35
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 14:14
EPA 8260B 05/04/16 05/03/16 12:01 5/4/2016 04:49
9801-SW3 CZ05055-12 Sampled:04/20/16 11:20 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:37
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 14:30
EPA 8260B 05/04/16 05/03/16 12:01 5/4/2016 05:19
9801-SW4 CZ05055-13 Sampled:04/20/16 09:34 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:40
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 14:34
EPA 8260B 05/04/16 05/03/16 12:01 5/4/2016 05:49
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9801-SW5 CZ05055-14 Sampled:04/20/16 10:03 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/17/16 04/26/16 10:39 4/27/2016 13:43
EPA 6020B 10/17/16 04/26/16 14:23 4/28/2016 14:37
EPA 8260B 05/04/16 05/03/16 12:01 5/4/2016 06:19
9801-Tripblank CZ05055-15 Sampled:04/20/16 09:34 Received:04/21/16 10:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 05/04/16 05/02/16 12:38 5/3/2016 03:12
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW1A CZ05055-01
Flag NotesMDLNC SWSLMRLDF
147 ug/L EPA 6010D 10010.01.001Barium - Total
3.89 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
6.06 ug/L EPA 6010DJ 5010.02.201Nickel - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW2 CZ05055-02
Flag NotesMDLNC SWSLMRLDF
0.285 ug/L EPA 6020BJ 62.000.2201Antimony - Total
82.5 ug/L EPA 6010DJ 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW3 CZ05055-03
Flag NotesMDLNC SWSLMRLDF
115 ug/L EPA 6010D 10010.01.001Barium - Total
1.23 ug/L EPA 6010D 11.000.1001Beryllium - Total
2.31 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
6.12 ug/L EPA 6010DJ 5010.02.201Nickel - Total
15.8 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW3A CZ05055-04
Flag NotesMDLNC SWSLMRLDF
312 ug/L EPA 6010D 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW4 CZ05055-05
Flag NotesMDLNC SWSLMRLDF
10.0 ug/L EPA 6010D 1010.06.801Arsenic - Total
603 ug/L EPA 6010D 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW5 CZ05055-06
Flag NotesMDLNC SWSLMRLDF
10 ug/L EPA 8260BJ 1005.01.21Acetone
700 ug/L EPA 6010D 10010.01.001Barium - Total
2.00 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
4.00 ug/L EPA 6010DJ 5010.02.201Nickel - Total
2.17 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW6 CZ05055-07
Flag NotesMDLNC SWSLMRLDF
37.3 ug/L EPA 6010DJ 10010.01.001Barium - Total
2.26 ug/L EPA 6010D 11.000.1001Beryllium - Total
0.515 ug/L EPA 6010DJ 11.000.3601Cadmium - Total
25.4 ug/L EPA 6010D 1010.01.101Cobalt - Total
43.9 ug/L EPA 6010DJ 5010.02.201Nickel - Total
4.20 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
57.3 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW7 CZ05055-08
Flag NotesMDLNC SWSLMRLDF
106 ug/L EPA 6010D 10010.01.001Barium - Total
4.63 ug/L EPA 6010DJ 1010.04.401Zinc - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW8 CZ05055-09
Flag NotesMDLNC SWSLMRLDF
70.3 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.273 ug/L EPA 6010DJ 11.000.1001Beryllium - Total
4.35 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
3.18 ug/L EPA 6010DJ 5010.02.201Nickel - Total
15.9 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW1 CZ05055-10
Flag NotesMDLNC SWSLMRLDF
52.2 ug/L EPA 6010DJ 10010.01.001Barium - Total
5.64 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
3.07 ug/L EPA 6010DJ 5010.02.201Nickel - Total
3.48 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
5.55 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW2 CZ05055-11
Flag NotesMDLNC SWSLMRLDF
102 ug/L EPA 6010D 10010.01.001Barium - Total
1.2 ug/L EPA 8260BJ 51.00.151cis-1,2-Dichloroethene
3.14 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
8.10 ug/L EPA 6010DJ 1010.01.601Copper - Total
4.92 ug/L EPA 6010DJ 5010.02.201Nickel - Total
1.99 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
11.5 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW3 CZ05055-12
Flag NotesMDLNC SWSLMRLDF
3.6 ug/L EPA 8260BJ 1005.01.21Acetone
7.02 ug/L EPA 6010DJ 1010.06.801Arsenic - Total
257 ug/L EPA 6010D 10010.01.001Barium - Total
1.17 ug/L EPA 6010D 11.000.1001Beryllium - Total
7.36 ug/L EPA 6010DJ 1010.01.401Chromium - Total
16.1 ug/L EPA 6010D 1010.01.101Cobalt - Total
7.98 ug/L EPA 6010DJ 1010.01.601Copper - Total
26.5 ug/L EPA 6010D 1010.03.101Lead - Total
12.7 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.53 ug/L EPA 8260BJ 11.00.141Toluene
24.5 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
64.7 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW4 CZ05055-13
Flag NotesMDLNC SWSLMRLDF
137 ug/L EPA 6010D 10010.01.001Barium - Total
1.5 ug/L EPA 8260BJ 51.00.151cis-1,2-Dichloroethene
15.3 ug/L EPA 6010D 1010.01.101Cobalt - Total
3.15 ug/L EPA 6010DJ 5010.02.201Nickel - Total
1.72 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
13.3 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW5 CZ05055-14
Flag NotesMDLNC SWSLMRLDF
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Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW5 CZ05055-14
Flag NotesMDLNC SWSLMRLDF
102 ug/L EPA 6010D 10010.01.001Barium - Total
37.0 ug/L EPA 6010D 1010.01.101Cobalt - Total
10.6 ug/L EPA 6010DJ 5010.02.201Nickel - Total
48.5 ug/L EPA 6010D 1010.04.401Zinc - Total
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ANALYTICAL RESULTS
9801-MW1ADescription:Lab Sample ID:CZ05055-01 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 08:39 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/02/16 13:311,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/02/16 13:311,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/02/16 13:311,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/02/16 13:311,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/02/16 13:311,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/02/16 13:311,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/02/16 13:311,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/02/16 13:311,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/02/16 13:311,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/02/16 13:311,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/02/16 13:311,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/02/16 13:311,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/02/16 13:311,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/02/16 13:312-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/02/16 13:312-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/02/16 13:314-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/02/16 13:31Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/02/16 13:31Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/02/16 13:31Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 13:31Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/02/16 13:31Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 13:31Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/02/16 13:31Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/02/16 13:31Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/02/16 13:31Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 13:31Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/02/16 13:31Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/02/16 13:31Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/02/16 13:31Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/02/16 13:31cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/02/16 13:31cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/02/16 13:31Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/02/16 13:31Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/02/16 13:31Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/02/16 13:31Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/02/16 13:31m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/02/16 13:31Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/02/16 13:31o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/02/16 13:31Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/02/16 13:31Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 13:31Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/02/16 13:31trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/02/16 13:31trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 13:31trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/02/16 13:31Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 13:31Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/02/16 13:31Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/02/16 13:31Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
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9801-MW1ADescription:Lab Sample ID:CZ05055-01 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 08:39 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/02/16 13:31Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136101 %MSZEPA 8260B 05/02/16 13:316E010025050.0 1
Dibromofluoromethane 67-129104 %MSZEPA 8260B 05/02/16 13:316E010025250.0 1
Toluene-d8 59-13499 %MSZEPA 8260B 05/02/16 13:316E010024950.0 1
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9801-MW1ADescription:Lab Sample ID:CZ05055-01 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 08:39 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 13:07Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 12:55Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 12:55Barium [7440-39-3] ^1.00 JDH10.0147 1001
ug/L EPA 6010D 04/27/16 12:55Beryllium [7440-41-7] ^0.100 JDH1.000.100 U 11
ug/L EPA 6010D 04/27/16 12:55Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 12:55Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 12:55Cobalt [7440-48-4] ^1.10 JDH10.03.89 J 101
ug/L EPA 6010D 04/27/16 12:55Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 12:55Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 12:55Nickel [7440-02-0] ^2.20 JDH10.06.06 J 501
ug/L EPA 6020B 04/28/16 13:07Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 12:55Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 13:07Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 12:55Vanadium [7440-62-2] ^1.40 JDH10.01.40 U 251
ug/L EPA 6010D 04/27/16 12:55Zinc [7440-66-6] ^4.40 JDH10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW2Description:Lab Sample ID:CZ05055-02 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:49 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/02/16 14:011,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/02/16 14:011,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/02/16 14:011,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/02/16 14:011,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/02/16 14:011,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/02/16 14:011,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/02/16 14:011,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/02/16 14:011,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/02/16 14:011,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/02/16 14:011,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/02/16 14:011,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/02/16 14:011,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/02/16 14:011,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/02/16 14:012-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/02/16 14:012-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/02/16 14:014-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/02/16 14:01Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/02/16 14:01Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/02/16 14:01Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 14:01Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/02/16 14:01Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 14:01Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/02/16 14:01Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/02/16 14:01Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/02/16 14:01Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 14:01Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/02/16 14:01Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/02/16 14:01Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/02/16 14:01Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/02/16 14:01cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/02/16 14:01cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/02/16 14:01Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/02/16 14:01Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/02/16 14:01Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/02/16 14:01Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/02/16 14:01m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/02/16 14:01Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/02/16 14:01o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/02/16 14:01Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/02/16 14:01Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 14:01Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/02/16 14:01trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/02/16 14:01trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 14:01trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/02/16 14:01Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 14:01Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/02/16 14:01Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/02/16 14:01Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/02/16 14:01Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW2Description:Lab Sample ID:CZ05055-02 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:49 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136104 %MSZEPA 8260B 05/02/16 14:016E010025250.0 1
Dibromofluoromethane 67-129106 %MSZEPA 8260B 05/02/16 14:016E010025350.0 1
Toluene-d8 59-13499 %MSZEPA 8260B 05/02/16 14:016E010025050.0 1
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9801-MW2Description:Lab Sample ID:CZ05055-02 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:49 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 13:41Antimony [7440-36-0] ^0.220 VLO2.000.285 J 61
ug/L EPA 6010D 04/27/16 12:58Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 12:58Barium [7440-39-3] ^1.00 JDH10.082.5 J 1001
ug/L EPA 6010D 04/27/16 12:58Beryllium [7440-41-7] ^0.100 JDH1.000.100 U 11
ug/L EPA 6010D 04/27/16 12:58Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 12:58Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 12:58Cobalt [7440-48-4] ^1.10 JDH10.01.10 U 101
ug/L EPA 6010D 04/27/16 12:58Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 12:58Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 12:58Nickel [7440-02-0] ^2.20 JDH10.02.20 U 501
ug/L EPA 6020B 04/28/16 13:41Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 12:58Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 13:41Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 12:58Vanadium [7440-62-2] ^1.40 JDH10.01.40 U 251
ug/L EPA 6010D 04/27/16 12:58Zinc [7440-66-6] ^4.40 JDH10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW3Description:Lab Sample ID:CZ05055-03 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:26 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/02/16 15:001,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/02/16 15:001,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/02/16 15:001,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/02/16 15:001,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/02/16 15:001,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/02/16 15:001,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/02/16 15:001,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/02/16 15:001,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/02/16 15:001,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/02/16 15:001,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/02/16 15:001,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/02/16 15:001,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/02/16 15:001,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/02/16 15:002-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/02/16 15:002-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/02/16 15:004-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/02/16 15:00Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/02/16 15:00Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/02/16 15:00Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 15:00Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/02/16 15:00Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 15:00Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/02/16 15:00Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/02/16 15:00Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/02/16 15:00Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 15:00Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/02/16 15:00Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/02/16 15:00Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/02/16 15:00Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/02/16 15:00cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/02/16 15:00cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/02/16 15:00Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/02/16 15:00Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/02/16 15:00Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/02/16 15:00Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/02/16 15:00m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/02/16 15:00Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/02/16 15:00o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/02/16 15:00Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/02/16 15:00Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 15:00Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/02/16 15:00trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/02/16 15:00trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 15:00trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/02/16 15:00Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 15:00Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/02/16 15:00Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/02/16 15:00Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/02/16 15:00Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW3Description:Lab Sample ID:CZ05055-03 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:26 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136105 %MSZEPA 8260B 05/02/16 15:006E010025250.0 1
Dibromofluoromethane 67-129104 %MSZEPA 8260B 05/02/16 15:006E010025250.0 1
Toluene-d8 59-134101 %MSZEPA 8260B 05/02/16 15:006E010025150.0 1
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9801-MW3Description:Lab Sample ID:CZ05055-03 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:26 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 13:45Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:01Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 13:01Barium [7440-39-3] ^1.00 JDH10.0115 1001
ug/L EPA 6010D 04/27/16 13:01Beryllium [7440-41-7] ^0.100 JDH1.001.23 11
ug/L EPA 6010D 04/27/16 13:01Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:01Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:01Cobalt [7440-48-4] ^1.10 JDH10.02.31 J 101
ug/L EPA 6010D 04/27/16 13:01Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 13:01Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:01Nickel [7440-02-0] ^2.20 JDH10.06.12 J 501
ug/L EPA 6020B 04/28/16 13:45Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:01Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 13:45Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:01Vanadium [7440-62-2] ^1.40 JDH10.01.40 U 251
ug/L EPA 6010D 04/27/16 13:01Zinc [7440-66-6] ^4.40 JDH10.015.8 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW3ADescription:Lab Sample ID:CZ05055-04 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:33 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/02/16 15:321,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/02/16 15:321,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/02/16 15:321,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/02/16 15:321,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/02/16 15:321,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/02/16 15:321,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/02/16 15:321,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/02/16 15:321,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/02/16 15:321,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/02/16 15:321,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/02/16 15:321,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/02/16 15:321,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/02/16 15:321,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/02/16 15:322-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/02/16 15:322-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/02/16 15:324-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/02/16 15:32Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/02/16 15:32Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/02/16 15:32Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 15:32Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/02/16 15:32Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 15:32Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/02/16 15:32Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/02/16 15:32Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/02/16 15:32Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 15:32Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/02/16 15:32Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/02/16 15:32Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/02/16 15:32Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/02/16 15:32cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/02/16 15:32cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/02/16 15:32Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/02/16 15:32Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/02/16 15:32Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/02/16 15:32Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/02/16 15:32m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/02/16 15:32Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/02/16 15:32o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/02/16 15:32Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/02/16 15:32Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 15:32Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/02/16 15:32trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/02/16 15:32trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 15:32trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/02/16 15:32Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 15:32Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/02/16 15:32Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/02/16 15:32Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/02/16 15:32Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW3ADescription:Lab Sample ID:CZ05055-04 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:33 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136105 %MSZEPA 8260B 05/02/16 15:326E010025350.0 1
Dibromofluoromethane 67-129107 %MSZEPA 8260B 05/02/16 15:326E010025350.0 1
Toluene-d8 59-134100 %MSZEPA 8260B 05/02/16 15:326E010025050.0 1
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9801-MW3ADescription:Lab Sample ID:CZ05055-04 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:33 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 13:48Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:03Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 13:03Barium [7440-39-3] ^1.00 JDH10.0312 1001
ug/L EPA 6010D 04/27/16 13:03Beryllium [7440-41-7] ^0.100 JDH1.000.100 U 11
ug/L EPA 6010D 04/27/16 13:03Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:03Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:03Cobalt [7440-48-4] ^1.10 JDH10.01.10 U 101
ug/L EPA 6010D 04/27/16 13:03Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 13:03Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:03Nickel [7440-02-0] ^2.20 JDH10.02.20 U 501
ug/L EPA 6020B 04/28/16 13:48Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:03Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 13:48Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:03Vanadium [7440-62-2] ^1.40 JDH10.01.40 U 251
ug/L EPA 6010D 04/27/16 13:03Zinc [7440-66-6] ^4.40 JDH10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW4Description:Lab Sample ID:CZ05055-05 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:27 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/03/16 18:451,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/03/16 18:451,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/03/16 18:451,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/03/16 18:451,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 18:451,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/03/16 18:451,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 18:451,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 18:451,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/03/16 18:451,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/03/16 18:451,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/03/16 18:451,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/03/16 18:451,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/03/16 18:451,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/03/16 18:452-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/03/16 18:452-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/03/16 18:454-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/03/16 18:45Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/03/16 18:45Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/03/16 18:45Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 18:45Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/03/16 18:45Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 18:45Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/03/16 18:45Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/03/16 18:45Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/03/16 18:45Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 18:45Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 18:45Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/03/16 18:45Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/03/16 18:45Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 18:45cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/03/16 18:45cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/03/16 18:45Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 18:45Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/03/16 18:45Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 18:45Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/03/16 18:45m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/03/16 18:45Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 18:45o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/03/16 18:45Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/03/16 18:45Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 18:45Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 18:45trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 18:45trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 18:45trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/03/16 18:45Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 18:45Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/03/16 18:45Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/03/16 18:45Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/03/16 18:45Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW4Description:Lab Sample ID:CZ05055-05 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:27 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13682 %MSZEPA 8260B 05/03/16 18:456E030174150.0 1
Dibromofluoromethane 67-12992 %MSZEPA 8260B 05/03/16 18:456E030174650.0 1
Toluene-d8 59-13495 %MSZEPA 8260B 05/03/16 18:456E030174750.0 1
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9801-MW4Description:Lab Sample ID:CZ05055-05 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:27 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 13:52Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:18Arsenic [7440-38-2] ^6.80 JDH10.010.0 101
ug/L EPA 6010D 04/27/16 13:18Barium [7440-39-3] ^1.00 JDH10.0603 1001
ug/L EPA 6010D 04/27/16 13:18Beryllium [7440-41-7] ^0.100 JDH1.000.100 U 11
ug/L EPA 6010D 04/27/16 13:18Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:18Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:18Cobalt [7440-48-4] ^1.10 JDH10.01.10 U 101
ug/L EPA 6010D 04/27/16 13:18Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 13:18Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:18Nickel [7440-02-0] ^2.20 JDH10.02.20 U 501
ug/L EPA 6020B 04/28/16 13:52Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:18Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 13:52Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:18Vanadium [7440-62-2] ^1.40 JDH10.01.40 U 251
ug/L EPA 6010D 04/27/16 13:18Zinc [7440-66-6] ^4.40 JDH10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW5Description:Lab Sample ID:CZ05055-06 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:48 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/03/16 19:141,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/03/16 19:141,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/03/16 19:141,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/03/16 19:141,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 19:141,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/03/16 19:141,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 19:141,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 19:141,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/03/16 19:141,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/03/16 19:141,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/03/16 19:141,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/03/16 19:141,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/03/16 19:141,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/03/16 19:142-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/03/16 19:142-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/03/16 19:144-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/03/16 19:14Acetone [67-64-1] ^1.2 MSZ5.010J 1001
ug/L EPA 8260B 05/03/16 19:14Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/03/16 19:14Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 19:14Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/03/16 19:14Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 19:14Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/03/16 19:14Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/03/16 19:14Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/03/16 19:14Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 19:14Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 19:14Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/03/16 19:14Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/03/16 19:14Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 19:14cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/03/16 19:14cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/03/16 19:14Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 19:14Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/03/16 19:14Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 19:14Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/03/16 19:14m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/03/16 19:14Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 19:14o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/03/16 19:14Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/03/16 19:14Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 19:14Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 19:14trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 19:14trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 19:14trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/03/16 19:14Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 19:14Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/03/16 19:14Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/03/16 19:14Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/03/16 19:14Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW5Description:Lab Sample ID:CZ05055-06 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:48 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13685 %MSZEPA 8260B 05/03/16 19:146E030174250.0 1
Dibromofluoromethane 67-12992 %MSZEPA 8260B 05/03/16 19:146E030174650.0 1
Toluene-d8 59-13497 %MSZEPA 8260B 05/03/16 19:146E030174850.0 1
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9801-MW5Description:Lab Sample ID:CZ05055-06 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:48 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 13:55Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:21Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 13:21Barium [7440-39-3] ^1.00 JDH10.0700 1001
ug/L EPA 6010D 04/27/16 13:21Beryllium [7440-41-7] ^0.100 JDH1.000.100 U 11
ug/L EPA 6010D 04/27/16 13:21Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:21Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:21Cobalt [7440-48-4] ^1.10 JDH10.02.00 J 101
ug/L EPA 6010D 04/27/16 13:21Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 13:21Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:21Nickel [7440-02-0] ^2.20 JDH10.04.00 J 501
ug/L EPA 6020B 04/28/16 13:55Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:21Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 13:55Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:21Vanadium [7440-62-2] ^1.40 JDH10.02.17 J 251
ug/L EPA 6010D 04/27/16 13:21Zinc [7440-66-6] ^4.40 JDH10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW6Description:Lab Sample ID:CZ05055-07 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:06 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/02/16 17:071,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/02/16 17:071,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/02/16 17:071,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/02/16 17:071,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/02/16 17:071,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/02/16 17:071,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/02/16 17:071,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/02/16 17:071,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/02/16 17:071,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/02/16 17:071,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/02/16 17:071,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/02/16 17:071,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/02/16 17:071,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/02/16 17:072-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/02/16 17:072-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/02/16 17:074-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/02/16 17:07Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/02/16 17:07Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/02/16 17:07Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 17:07Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/02/16 17:07Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 17:07Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/02/16 17:07Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/02/16 17:07Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/02/16 17:07Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 17:07Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/02/16 17:07Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/02/16 17:07Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/02/16 17:07Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/02/16 17:07cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/02/16 17:07cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/02/16 17:07Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/02/16 17:07Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/02/16 17:07Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/02/16 17:07Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/02/16 17:07m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/02/16 17:07Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/02/16 17:07o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/02/16 17:07Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/02/16 17:07Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/02/16 17:07Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/02/16 17:07trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/02/16 17:07trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 17:07trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/02/16 17:07Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/02/16 17:07Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/02/16 17:07Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/02/16 17:07Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/02/16 17:07Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW6Description:Lab Sample ID:CZ05055-07 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:06 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136101 %MSZEPA 8260B 05/02/16 17:076E010025050.0 1
Dibromofluoromethane 67-129104 %MSZEPA 8260B 05/02/16 17:076E010025250.0 1
Toluene-d8 59-13499 %MSZEPA 8260B 05/02/16 17:076E010024950.0 1
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9801-MW6Description:Lab Sample ID:CZ05055-07 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:06 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 14:41Antimony [7440-36-0] ^2.20 VLO20.02.20 UD QI-03610
ug/L EPA 6010D 04/27/16 13:24Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 13:24Barium [7440-39-3] ^1.00 JDH10.037.3 J 1001
ug/L EPA 6010D 04/27/16 13:24Beryllium [7440-41-7] ^0.100 JDH1.002.26 11
ug/L EPA 6010D 04/27/16 13:24Cadmium [7440-43-9] ^0.360 JDH1.000.515 J 11
ug/L EPA 6010D 04/27/16 13:24Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:24Cobalt [7440-48-4] ^1.10 JDH10.025.4 101
ug/L EPA 6010D 04/27/16 13:24Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 13:24Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:24Nickel [7440-02-0] ^2.20 JDH10.043.9 J 501
ug/L EPA 6020B 04/28/16 14:41Selenium [7782-49-2] ^9.10 VLO30.09.10 UD QI-031010
ug/L EPA 6010D 04/27/16 13:24Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 14:41Thallium [7440-28-0] ^1.10 VLO10.01.10 UD QI-035.510
ug/L EPA 6010D 04/27/16 13:24Vanadium [7440-62-2] ^1.40 JDH10.04.20 J 251
ug/L EPA 6010D 04/27/16 13:24Zinc [7440-66-6] ^4.40 JDH10.057.3 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW7Description:Lab Sample ID:CZ05055-08 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 10:37 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/03/16 10:121,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/03/16 10:121,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/03/16 10:121,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/03/16 10:121,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 10:121,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/03/16 10:121,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 10:121,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 10:121,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/03/16 10:121,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/03/16 10:121,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/03/16 10:121,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/03/16 10:121,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/03/16 10:121,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/03/16 10:122-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/03/16 10:122-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/03/16 10:124-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/03/16 10:12Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/03/16 10:12Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/03/16 10:12Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 10:12Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/03/16 10:12Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 10:12Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/03/16 10:12Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/03/16 10:12Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/03/16 10:12Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 10:12Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 10:12Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/03/16 10:12Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/03/16 10:12Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 10:12cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/03/16 10:12cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/03/16 10:12Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 10:12Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/03/16 10:12Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 10:12Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/03/16 10:12m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/03/16 10:12Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 10:12o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/03/16 10:12Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/03/16 10:12Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 10:12Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 10:12trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 10:12trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 10:12trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/03/16 10:12Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 10:12Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/03/16 10:12Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/03/16 10:12Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/03/16 10:12Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW7Description:Lab Sample ID:CZ05055-08 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 10:37 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13688 %MSZEPA 8260B 05/03/16 10:126E020284450.0 1
Dibromofluoromethane 67-12991 %MSZEPA 8260B 05/03/16 10:126E020284650.0 1
Toluene-d8 59-13495 %MSZEPA 8260B 05/03/16 10:126E020284850.0 1
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9801-MW7Description:Lab Sample ID:CZ05055-08 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 10:37 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 14:03Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:27Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 13:27Barium [7440-39-3] ^1.00 JDH10.0106 1001
ug/L EPA 6010D 04/27/16 13:27Beryllium [7440-41-7] ^0.100 JDH1.000.100 U 11
ug/L EPA 6010D 04/27/16 13:27Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:27Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:27Cobalt [7440-48-4] ^1.10 JDH10.01.10 U 101
ug/L EPA 6010D 04/27/16 13:27Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 13:27Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:27Nickel [7440-02-0] ^2.20 JDH10.02.20 U 501
ug/L EPA 6020B 04/28/16 14:03Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:27Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 14:03Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:27Vanadium [7440-62-2] ^1.40 JDH10.01.40 U 251
ug/L EPA 6010D 04/27/16 13:27Zinc [7440-66-6] ^4.40 JDH10.04.63 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW8Description:Lab Sample ID:CZ05055-09 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 08:50 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/03/16 19:431,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/03/16 19:431,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/03/16 19:431,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/03/16 19:431,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 19:431,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/03/16 19:431,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 19:431,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 19:431,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/03/16 19:431,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/03/16 19:431,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/03/16 19:431,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/03/16 19:431,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/03/16 19:431,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/03/16 19:432-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/03/16 19:432-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/03/16 19:434-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/03/16 19:43Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/03/16 19:43Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/03/16 19:43Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 19:43Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/03/16 19:43Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 19:43Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/03/16 19:43Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/03/16 19:43Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/03/16 19:43Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 19:43Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 19:43Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/03/16 19:43Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/03/16 19:43Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 19:43cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/03/16 19:43cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/03/16 19:43Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 19:43Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/03/16 19:43Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 19:43Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/03/16 19:43m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/03/16 19:43Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 19:43o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/03/16 19:43Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/03/16 19:43Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 19:43Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 19:43trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 19:43trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 19:43trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/03/16 19:43Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 19:43Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/03/16 19:43Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/03/16 19:43Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/03/16 19:43Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW8Description:Lab Sample ID:CZ05055-09 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 08:50 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13687 %MSZEPA 8260B 05/03/16 19:436E030174450.0 1
Dibromofluoromethane 67-12993 %MSZEPA 8260B 05/03/16 19:436E030174650.0 1
Toluene-d8 59-13494 %MSZEPA 8260B 05/03/16 19:436E030174750.0 1
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www.encolabs.com
9801-MW8Description:Lab Sample ID:CZ05055-09 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 08:50 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 14:06Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:29Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 13:29Barium [7440-39-3] ^1.00 JDH10.070.3 J 1001
ug/L EPA 6010D 04/27/16 13:29Beryllium [7440-41-7] ^0.100 JDH1.000.273 J 11
ug/L EPA 6010D 04/27/16 13:29Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:29Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:29Cobalt [7440-48-4] ^1.10 JDH10.04.35 J 101
ug/L EPA 6010D 04/27/16 13:29Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 13:29Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:29Nickel [7440-02-0] ^2.20 JDH10.03.18 J 501
ug/L EPA 6020B 04/28/16 14:06Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:29Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 14:06Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:29Vanadium [7440-62-2] ^1.40 JDH10.01.40 U 251
ug/L EPA 6010D 04/27/16 13:29Zinc [7440-66-6] ^4.40 JDH10.015.9 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW1Description:Lab Sample ID:CZ05055-10 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:57 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/03/16 11:101,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/03/16 11:101,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/03/16 11:101,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/03/16 11:101,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 11:101,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/03/16 11:101,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 11:101,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 11:101,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/03/16 11:101,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/03/16 11:101,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/03/16 11:101,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/03/16 11:101,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/03/16 11:101,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/03/16 11:102-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/03/16 11:102-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/03/16 11:104-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/03/16 11:10Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/03/16 11:10Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/03/16 11:10Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 11:10Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/03/16 11:10Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 11:10Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/03/16 11:10Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/03/16 11:10Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/03/16 11:10Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 11:10Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 11:10Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/03/16 11:10Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/03/16 11:10Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 11:10cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/03/16 11:10cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/03/16 11:10Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 11:10Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/03/16 11:10Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 11:10Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/03/16 11:10m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/03/16 11:10Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 11:10o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/03/16 11:10Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/03/16 11:10Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 11:10Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 11:10trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 11:10trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 11:10trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/03/16 11:10Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 11:10Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/03/16 11:10Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/03/16 11:10Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/03/16 11:10Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW1Description:Lab Sample ID:CZ05055-10 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:57 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13690 %MSZEPA 8260B 05/03/16 11:106E020284550.0 1
Dibromofluoromethane 67-12987 %MSZEPA 8260B 05/03/16 11:106E020284350.0 1
Toluene-d8 59-13493 %MSZEPA 8260B 05/03/16 11:106E020284750.0 1
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www.encolabs.com
9801-SW1Description:Lab Sample ID:CZ05055-10 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:57 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 14:10Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:32Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 13:32Barium [7440-39-3] ^1.00 JDH10.052.2 J 1001
ug/L EPA 6010D 04/27/16 13:32Beryllium [7440-41-7] ^0.100 JDH1.000.100 U 11
ug/L EPA 6010D 04/27/16 13:32Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:32Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:32Cobalt [7440-48-4] ^1.10 JDH10.05.64 J 101
ug/L EPA 6010D 04/27/16 13:32Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 13:32Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:32Nickel [7440-02-0] ^2.20 JDH10.03.07 J 501
ug/L EPA 6020B 04/28/16 14:10Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:32Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 14:10Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:32Vanadium [7440-62-2] ^1.40 JDH10.03.48 J 251
ug/L EPA 6010D 04/27/16 13:32Zinc [7440-66-6] ^4.40 JDH10.05.55 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW2Description:Lab Sample ID:CZ05055-11 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:39 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/04/16 04:491,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/04/16 04:491,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/04/16 04:491,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/04/16 04:491,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/04/16 04:491,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/04/16 04:491,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/04/16 04:491,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/04/16 04:491,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/04/16 04:491,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/04/16 04:491,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/04/16 04:491,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/04/16 04:491,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/04/16 04:491,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/04/16 04:492-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/04/16 04:492-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/04/16 04:494-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/04/16 04:49Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/04/16 04:49Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/04/16 04:49Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 04:49Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/04/16 04:49Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 04:49Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/04/16 04:49Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/04/16 04:49Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/04/16 04:49Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 04:49Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/04/16 04:49Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/04/16 04:49Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/04/16 04:49Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/04/16 04:49cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.01.2 J 51
ug/L EPA 8260B 05/04/16 04:49cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/04/16 04:49Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/04/16 04:49Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/04/16 04:49Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/04/16 04:49Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/04/16 04:49m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/04/16 04:49Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/04/16 04:49o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/04/16 04:49Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/04/16 04:49Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 04:49Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/04/16 04:49trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/04/16 04:49trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 04:49trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/04/16 04:49Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 04:49Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/04/16 04:49Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/04/16 04:49Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/04/16 04:49Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW2Description:Lab Sample ID:CZ05055-11 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:39 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136106 %MSZEPA 8260B 05/04/16 04:496E030205350.0 1
Dibromofluoromethane 67-129108 %MSZEPA 8260B 05/04/16 04:496E030205450.0 1
Toluene-d8 59-134100 %MSZEPA 8260B 05/04/16 04:496E030205050.0 1
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9801-SW2Description:Lab Sample ID:CZ05055-11 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:39 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 14:14Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:35Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 13:35Barium [7440-39-3] ^1.00 JDH10.0102 1001
ug/L EPA 6010D 04/27/16 13:35Beryllium [7440-41-7] ^0.100 JDH1.000.100 U 11
ug/L EPA 6010D 04/27/16 13:35Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:35Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:35Cobalt [7440-48-4] ^1.10 JDH10.03.14 J 101
ug/L EPA 6010D 04/27/16 13:35Copper [7440-50-8] ^1.60 JDH10.08.10 J 101
ug/L EPA 6010D 04/27/16 13:35Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:35Nickel [7440-02-0] ^2.20 JDH10.04.92 J 501
ug/L EPA 6020B 04/28/16 14:14Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:35Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 14:14Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:35Vanadium [7440-62-2] ^1.40 JDH10.01.99 J 251
ug/L EPA 6010D 04/27/16 13:35Zinc [7440-66-6] ^4.40 JDH10.011.5 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW3Description:Lab Sample ID:CZ05055-12 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:20 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/04/16 05:191,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/04/16 05:191,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/04/16 05:191,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/04/16 05:191,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/04/16 05:191,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/04/16 05:191,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/04/16 05:191,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/04/16 05:191,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/04/16 05:191,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/04/16 05:191,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/04/16 05:191,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/04/16 05:191,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/04/16 05:191,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/04/16 05:192-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/04/16 05:192-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/04/16 05:194-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/04/16 05:19Acetone [67-64-1] ^1.2 MSZ5.03.6 J 1001
ug/L EPA 8260B 05/04/16 05:19Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/04/16 05:19Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 05:19Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/04/16 05:19Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 05:19Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/04/16 05:19Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/04/16 05:19Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/04/16 05:19Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 05:19Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/04/16 05:19Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/04/16 05:19Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/04/16 05:19Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/04/16 05:19cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/04/16 05:19cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/04/16 05:19Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/04/16 05:19Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/04/16 05:19Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/04/16 05:19Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/04/16 05:19m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/04/16 05:19Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/04/16 05:19o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/04/16 05:19Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/04/16 05:19Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 05:19Toluene [108-88-3] ^0.14 MSZ1.00.53 J 11
ug/L EPA 8260B 05/04/16 05:19trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/04/16 05:19trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 05:19trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/04/16 05:19Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 05:19Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/04/16 05:19Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/04/16 05:19Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/04/16 05:19Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW3Description:Lab Sample ID:CZ05055-12 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:20 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136107 %MSZEPA 8260B 05/04/16 05:196E030205350.0 1
Dibromofluoromethane 67-129107 %MSZEPA 8260B 05/04/16 05:196E030205450.0 1
Toluene-d8 59-13499 %MSZEPA 8260B 05/04/16 05:196E030205050.0 1
Page 42 of 64
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www.encolabs.com
9801-SW3Description:Lab Sample ID:CZ05055-12 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 11:20 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 14:30Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:37Arsenic [7440-38-2] ^6.80 JDH10.07.02 J 101
ug/L EPA 6010D 04/27/16 13:37Barium [7440-39-3] ^1.00 JDH10.0257 1001
ug/L EPA 6010D 04/27/16 13:37Beryllium [7440-41-7] ^0.100 JDH1.001.17 11
ug/L EPA 6010D 04/27/16 13:37Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:37Chromium [7440-47-3] ^1.40 JDH10.07.36 J 101
ug/L EPA 6010D 04/27/16 13:37Cobalt [7440-48-4] ^1.10 JDH10.016.1 101
ug/L EPA 6010D 04/27/16 13:37Copper [7440-50-8] ^1.60 JDH10.07.98 J 101
ug/L EPA 6010D 04/27/16 13:37Lead [7439-92-1] ^3.10 JDH10.026.5 101
ug/L EPA 6010D 04/27/16 13:37Nickel [7440-02-0] ^2.20 JDH10.012.7 J 501
ug/L EPA 6020B 04/28/16 14:30Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:37Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 14:30Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:37Vanadium [7440-62-2] ^1.40 JDH10.024.5 J 251
ug/L EPA 6010D 04/27/16 13:37Zinc [7440-66-6] ^4.40 JDH10.064.7 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW4Description:Lab Sample ID:CZ05055-13 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:34 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/04/16 05:491,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/04/16 05:491,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/04/16 05:491,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/04/16 05:491,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/04/16 05:491,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/04/16 05:491,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/04/16 05:491,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/04/16 05:491,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/04/16 05:491,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/04/16 05:491,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/04/16 05:491,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/04/16 05:491,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/04/16 05:491,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/04/16 05:492-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/04/16 05:492-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/04/16 05:494-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/04/16 05:49Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/04/16 05:49Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/04/16 05:49Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 05:49Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/04/16 05:49Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 05:49Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/04/16 05:49Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/04/16 05:49Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/04/16 05:49Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 05:49Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/04/16 05:49Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/04/16 05:49Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/04/16 05:49Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/04/16 05:49cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.01.5 J 51
ug/L EPA 8260B 05/04/16 05:49cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/04/16 05:49Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/04/16 05:49Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/04/16 05:49Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/04/16 05:49Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/04/16 05:49m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/04/16 05:49Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/04/16 05:49o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/04/16 05:49Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/04/16 05:49Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 05:49Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/04/16 05:49trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/04/16 05:49trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 05:49trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/04/16 05:49Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 05:49Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/04/16 05:49Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/04/16 05:49Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/04/16 05:49Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW4Description:Lab Sample ID:CZ05055-13 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:34 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136107 %MSZEPA 8260B 05/04/16 05:496E030205450.0 1
Dibromofluoromethane 67-129107 %MSZEPA 8260B 05/04/16 05:496E030205450.0 1
Toluene-d8 59-13499 %MSZEPA 8260B 05/04/16 05:496E030204950.0 1
Page 45 of 64
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9801-SW4Description:Lab Sample ID:CZ05055-13 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:34 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 14:34Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:40Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 13:40Barium [7440-39-3] ^1.00 JDH10.0137 1001
ug/L EPA 6010D 04/27/16 13:40Beryllium [7440-41-7] ^0.100 JDH1.000.100 U 11
ug/L EPA 6010D 04/27/16 13:40Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:40Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:40Cobalt [7440-48-4] ^1.10 JDH10.015.3 101
ug/L EPA 6010D 04/27/16 13:40Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 13:40Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:40Nickel [7440-02-0] ^2.20 JDH10.03.15 J 501
ug/L EPA 6020B 04/28/16 14:34Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:40Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 14:34Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:40Vanadium [7440-62-2] ^1.40 JDH10.01.72 J 251
ug/L EPA 6010D 04/27/16 13:40Zinc [7440-66-6] ^4.40 JDH10.013.3 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW5Description:Lab Sample ID:CZ05055-14 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 10:03 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/04/16 06:191,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/04/16 06:191,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/04/16 06:191,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/04/16 06:191,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/04/16 06:191,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/04/16 06:191,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/04/16 06:191,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/04/16 06:191,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/04/16 06:191,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/04/16 06:191,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/04/16 06:191,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/04/16 06:191,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/04/16 06:191,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/04/16 06:192-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/04/16 06:192-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/04/16 06:194-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/04/16 06:19Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/04/16 06:19Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/04/16 06:19Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 06:19Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/04/16 06:19Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 06:19Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/04/16 06:19Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/04/16 06:19Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/04/16 06:19Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 06:19Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/04/16 06:19Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/04/16 06:19Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/04/16 06:19Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/04/16 06:19cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/04/16 06:19cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/04/16 06:19Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/04/16 06:19Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/04/16 06:19Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/04/16 06:19Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/04/16 06:19m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/04/16 06:19Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/04/16 06:19o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/04/16 06:19Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/04/16 06:19Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/04/16 06:19Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/04/16 06:19trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/04/16 06:19trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 06:19trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/04/16 06:19Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/04/16 06:19Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/04/16 06:19Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/04/16 06:19Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/04/16 06:19Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW5Description:Lab Sample ID:CZ05055-14 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 10:03 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136110 %MSZEPA 8260B 05/04/16 06:196E030205550.0 1
Dibromofluoromethane 67-129107 %MSZEPA 8260B 05/04/16 06:196E030205350.0 1
Toluene-d8 59-134102 %MSZEPA 8260B 05/04/16 06:196E030205150.0 1
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9801-SW5Description:Lab Sample ID:CZ05055-14 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 10:03 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ROBERT WELDY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 04/28/16 14:37Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 04/27/16 13:43Arsenic [7440-38-2] ^6.80 JDH10.06.80 U 101
ug/L EPA 6010D 04/27/16 13:43Barium [7440-39-3] ^1.00 JDH10.0102 1001
ug/L EPA 6010D 04/27/16 13:43Beryllium [7440-41-7] ^0.100 JDH1.000.100 U 11
ug/L EPA 6010D 04/27/16 13:43Cadmium [7440-43-9] ^0.360 JDH1.000.360 U 11
ug/L EPA 6010D 04/27/16 13:43Chromium [7440-47-3] ^1.40 JDH10.01.40 U 101
ug/L EPA 6010D 04/27/16 13:43Cobalt [7440-48-4] ^1.10 JDH10.037.0 101
ug/L EPA 6010D 04/27/16 13:43Copper [7440-50-8] ^1.60 JDH10.01.60 U 101
ug/L EPA 6010D 04/27/16 13:43Lead [7439-92-1] ^3.10 JDH10.03.10 U 101
ug/L EPA 6010D 04/27/16 13:43Nickel [7440-02-0] ^2.20 JDH10.010.6 J 501
ug/L EPA 6020B 04/28/16 14:37Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 04/27/16 13:43Silver [7440-22-4] ^1.90 JDH10.01.90 U 101
ug/L EPA 6020B 04/28/16 14:37Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 04/27/16 13:43Vanadium [7440-62-2] ^1.40 JDH10.01.40 U 251
ug/L EPA 6010D 04/27/16 13:43Zinc [7440-66-6] ^4.40 JDH10.048.5 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-TripblankDescription:Lab Sample ID:CZ05055-15 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:34 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/03/16 03:121,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MSZ1.00.17 U 51
ug/L EPA 8260B 05/03/16 03:121,1,1-Trichloroethane [71-55-6] ^0.12 MSZ1.00.12 U 11
ug/L EPA 8260B 05/03/16 03:121,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MSZ1.00.28 U 31
ug/L EPA 8260B 05/03/16 03:121,1,2-Trichloroethane [79-00-5] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 03:121,1-Dichloroethane [75-34-3] ^0.13 MSZ1.00.13 U 51
ug/L EPA 8260B 05/03/16 03:121,1-Dichloroethene [75-35-4] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 03:121,2,3-Trichloropropane [96-18-4] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 03:121,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MSZ1.00.48 U 131
ug/L EPA 8260B 05/03/16 03:121,2-Dibromoethane [106-93-4] ^0.66 MSZ1.00.66 U 11
ug/L EPA 8260B 05/03/16 03:121,2-Dichlorobenzene [95-50-1] ^0.19 MSZ1.00.19 U 51
ug/L EPA 8260B 05/03/16 03:121,2-Dichloroethane [107-06-2] ^0.21 MSZ1.00.21 U 11
ug/L EPA 8260B 05/03/16 03:121,2-Dichloropropane [78-87-5] ^0.10 MSZ1.00.10 U 11
ug/L EPA 8260B 05/03/16 03:121,4-Dichlorobenzene [106-46-7] ^0.19 MSZ1.00.19 U 11
ug/L EPA 8260B 05/03/16 03:122-Butanone [78-93-3] ^1.3 MSZ5.01.3 U 1001
ug/L EPA 8260B 05/03/16 03:122-Hexanone [591-78-6] ^0.88 MSZ5.00.88 U 501
ug/L EPA 8260B 05/03/16 03:124-Methyl-2-pentanone [108-10-1] ^1.1 MSZ5.01.1 U 1001
ug/L EPA 8260B 05/03/16 03:12Acetone [67-64-1] ^1.2 MSZ5.01.2 U 1001
ug/L EPA 8260B 05/03/16 03:12Acrylonitrile [107-13-1] ^3.5 MSZ103.5 U 2001
ug/L EPA 8260B 05/03/16 03:12Benzene [71-43-2] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 03:12Bromochloromethane [74-97-5] ^0.48 MSZ1.00.48 U 31
ug/L EPA 8260B 05/03/16 03:12Bromodichloromethane [75-27-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 03:12Bromoform [75-25-2] ^0.22 MSZ1.00.22 U 31
ug/L EPA 8260B 05/03/16 03:12Bromomethane [74-83-9] ^0.14 MSZ1.00.14 U 101
ug/L EPA 8260B 05/03/16 03:12Carbon disulfide [75-15-0] ^1.5 MSZ5.01.5 U 1001
ug/L EPA 8260B 05/03/16 03:12Carbon tetrachloride [56-23-5] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 03:12Chlorobenzene [108-90-7] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 03:12Chloroethane [75-00-3] ^0.23 MSZ1.00.23 U 101
ug/L EPA 8260B 05/03/16 03:12Chloroform [67-66-3] ^0.18 MSZ1.00.18 U 51
ug/L EPA 8260B 05/03/16 03:12Chloromethane [74-87-3] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 03:12cis-1,2-Dichloroethene [156-59-2] ^0.15 MSZ1.00.15 U 51
ug/L EPA 8260B 05/03/16 03:12cis-1,3-Dichloropropene [10061-01-5] ^0.20 MSZ1.00.20 U 11
ug/L EPA 8260B 05/03/16 03:12Dibromochloromethane [124-48-1] ^0.17 MSZ1.00.17 U 31
ug/L EPA 8260B 05/03/16 03:12Dibromomethane [74-95-3] ^0.27 MSZ1.00.27 U 101
ug/L EPA 8260B 05/03/16 03:12Ethylbenzene [100-41-4] ^0.13 MSZ1.00.13 U 11
ug/L EPA 8260B 05/03/16 03:12Iodomethane [74-88-4] ^1.7 MSZ5.01.7 U 101
ug/L EPA 8260B 05/03/16 03:12m,p-Xylenes [108-38-3/106-42-3] ^0.17 MSZ2.00.17 U NE1
ug/L EPA 8260B 05/03/16 03:12Methylene chloride [75-09-2] ^0.23 MSZ1.00.23 U 11
ug/L EPA 8260B 05/03/16 03:12o-Xylene [95-47-6] ^0.065 MSZ1.00.065 U NE1
ug/L EPA 8260B 05/03/16 03:12Styrene [100-42-5] ^0.11 MSZ1.00.11 U 11
ug/L EPA 8260B 05/03/16 03:12Tetrachloroethene [127-18-4] ^0.17 MSZ1.00.17 U 11
ug/L EPA 8260B 05/03/16 03:12Toluene [108-88-3] ^0.14 MSZ1.00.14 U 11
ug/L EPA 8260B 05/03/16 03:12trans-1,2-Dichloroethene [156-60-5] ^0.21 MSZ1.00.21 U 51
ug/L EPA 8260B 05/03/16 03:12trans-1,3-Dichloropropene [10061-02-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 03:12trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MSZ1.00.70 U 1001
ug/L EPA 8260B 05/03/16 03:12Trichloroethene [79-01-6] ^0.15 MSZ1.00.15 U 11
ug/L EPA 8260B 05/03/16 03:12Trichlorofluoromethane [75-69-4] ^0.24 MSZ1.00.24 U 11
ug/L EPA 8260B 05/03/16 03:12Vinyl acetate [108-05-4] ^0.95 MSZ5.00.95 U 501
ug/L EPA 8260B 05/03/16 03:12Vinyl chloride [75-01-4] ^0.32 MSZ1.00.32 U 11
ug/L EPA 8260B 05/03/16 03:12Xylenes (Total) [1330-20-7] ^0.45 MSZ3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-TripblankDescription:Lab Sample ID:CZ05055-15 04/21/16 10:30Received:
Matrix:Water Sampled:04/20/16 09:34 Work Order:CZ05055
Wilson County MSWLFProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13689 %MSZEPA 8260B 05/03/16 03:126E020284450.0 1
Dibromofluoromethane 67-12996 %MSZEPA 8260B 05/03/16 03:126E020284850.0 1
Toluene-d8 59-13494 %MSZEPA 8260B 05/03/16 03:126E020284750.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6E01002 - EPA 5030B_MS
Prepared: 05/01/2016 12:15 Analyzed: 05/02/2016 11:04Blank (6E01002-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6E01002 - EPA 5030B_MS
Prepared: 05/01/2016 12:15 Analyzed: 05/02/2016 11:04Blank (6E01002-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10251
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10552
ug/L 50.0 59-134Surrogate: Toluene-d8 9949
Prepared: 05/01/2016 12:15 Analyzed: 05/02/2016 16:38LCS (6E01002-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13310822 1,1-Dichloroethene
ug/L1.0 20.0 81-1348918 Benzene
ug/L1.0 20.0 83-1178717 Chlorobenzene
ug/L1.0 20.0 71-11810120 Toluene
ug/L1.0 20.0 74-11910421 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10251
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10553
ug/L 50.0 59-134Surrogate: Toluene-d8 9949
Prepared: 05/01/2016 12:15 Analyzed: 05/02/2016 12:03Matrix Spike (6E01002-MS1)
Source: CZ05877-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331060.21 U21 1,1-Dichloroethene
ug/L1.0 20.0 81-134930.15 U19 Benzene
ug/L1.0 20.0 83-117900.17 U18 Chlorobenzene
ug/L1.0 20.0 71-118850.14 U17 Toluene
ug/L1.0 20.0 74-1191240.15 U25 QM-07Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10552
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10452
ug/L 50.0 59-134Surrogate: Toluene-d8 10151
Prepared: 05/01/2016 12:15 Analyzed: 05/02/2016 12:32Matrix Spike Dup (6E01002-MSD1)
Source: CZ05877-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133106 0.30.21 U21 1,1-Dichloroethene
ug/L1.0 20.0 1781-13491 10.15 U18 Benzene
ug/L1.0 20.0 1683-11787 40.17 U17 Chlorobenzene
ug/L1.0 20.0 1771-11883 30.14 U17 Toluene
ug/L1.0 20.0 2274-119125 10.15 U25 QM-07Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10150
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10452
ug/L 50.0 59-134Surrogate: Toluene-d8 9950
Batch 6E02028 - EPA 5030B_MS
Prepared: 05/02/2016 12:38 Analyzed: 05/03/2016 00:47Blank (6E02028-BLK1)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6E02028 - EPA 5030B_MS
Prepared: 05/02/2016 12:38 Analyzed: 05/03/2016 00:47Blank (6E02028-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6E02028 - EPA 5030B_MS
Prepared: 05/02/2016 12:38 Analyzed: 05/03/2016 00:47Blank (6E02028-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 8744
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9045
ug/L 50.0 59-134Surrogate: Toluene-d8 9849
Prepared: 05/02/2016 12:38 Analyzed: 05/03/2016 01:16LCS (6E02028-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1337816 1,1-Dichloroethene
ug/L1.0 20.0 81-1349118 Benzene
ug/L1.0 20.0 83-11710120 Chlorobenzene
ug/L1.0 20.0 71-1189118 Toluene
ug/L1.0 20.0 74-11910421 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 8944
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 8743
ug/L 50.0 59-134Surrogate: Toluene-d8 9146
Prepared: 05/02/2016 12:38 Analyzed: 05/03/2016 01:45Matrix Spike (6E02028-MS1)
Source: CZ05877-05
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-133830.21 U17 1,1-Dichloroethene
ug/L1.0 20.0 81-134980.15 U20 Benzene
ug/L1.0 20.0 83-1171010.17 U20 Chlorobenzene
ug/L1.0 20.0 71-118920.14 U18 Toluene
ug/L1.0 20.0 74-1191080.15 U22 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 8844
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9347
ug/L 50.0 59-134Surrogate: Toluene-d8 9950
Prepared: 05/02/2016 12:38 Analyzed: 05/03/2016 02:14Matrix Spike Dup (6E02028-MSD1)
Source: CZ05877-05
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13381 20.21 U16 1,1-Dichloroethene
ug/L1.0 20.0 1781-13494 50.15 U19 Benzene
ug/L1.0 20.0 1683-117100 0.40.17 U20 Chlorobenzene
ug/L1.0 20.0 1771-11893 20.14 U19 Toluene
ug/L1.0 20.0 2274-119107 0.80.15 U21 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9145
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9347
ug/L 50.0 59-134Surrogate: Toluene-d8 9950
Batch 6E03017 - EPA 5030B_MS
Prepared: 05/03/2016 11:13 Analyzed: 05/03/2016 13:27Blank (6E03017-BLK1)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6E03017 - EPA 5030B_MS
Prepared: 05/03/2016 11:13 Analyzed: 05/03/2016 13:27Blank (6E03017-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6E03017 - EPA 5030B_MS
Prepared: 05/03/2016 11:13 Analyzed: 05/03/2016 13:27Blank (6E03017-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 8844
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9346
ug/L 50.0 59-134Surrogate: Toluene-d8 9749
Prepared: 05/03/2016 11:13 Analyzed: 05/03/2016 14:25LCS (6E03017-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1338617 1,1-Dichloroethene
ug/L1.0 20.0 81-13410321 Benzene
ug/L1.0 20.0 83-11710922 Chlorobenzene
ug/L1.0 20.0 71-11810020 Toluene
ug/L1.0 20.0 74-11911022 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9246
ug/L 50.0 59-134Surrogate: Toluene-d8 9749
Prepared: 05/03/2016 11:13 Analyzed: 05/03/2016 13:56Matrix Spike (6E03017-MS1)
Source: CZ05877-08
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-133830.21 U17 1,1-Dichloroethene
ug/L1.0 20.0 81-134960.15 U19 Benzene
ug/L1.0 20.0 83-1171090.17 U22 Chlorobenzene
ug/L1.0 20.0 71-1181000.14 U20 Toluene
ug/L1.0 20.0 74-1191080.15 U22 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9748
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9447
ug/L 50.0 59-134Surrogate: Toluene-d8 9648
Prepared: 05/03/2016 11:13 Analyzed: 05/03/2016 14:54Matrix Spike Dup (6E03017-MSD1)
Source: CZ05877-08
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13380 40.21 U16 1,1-Dichloroethene
ug/L1.0 20.0 1781-134100 40.15 U20 Benzene
ug/L1.0 20.0 1683-117104 50.17 U21 Chlorobenzene
ug/L1.0 20.0 1771-11895 50.14 U19 Toluene
ug/L1.0 20.0 2274-119104 30.15 U21 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 8844
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9146
ug/L 50.0 59-134Surrogate: Toluene-d8 9949
Batch 6E03020 - EPA 5030B_MS
Prepared: 05/03/2016 12:01 Analyzed: 05/04/2016 03:50Blank (6E03020-BLK1)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6E03020 - EPA 5030B_MS
Prepared: 05/03/2016 12:01 Analyzed: 05/04/2016 03:50Blank (6E03020-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L5.01.2 U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6E03020 - EPA 5030B_MS
Prepared: 05/03/2016 12:01 Analyzed: 05/04/2016 03:50Blank (6E03020-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10452
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10553
ug/L 50.0 59-134Surrogate: Toluene-d8 10050
Prepared: 05/03/2016 12:01 Analyzed: 05/04/2016 02:21LCS (6E03020-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13310621 1,1-Dichloroethene
ug/L1.0 20.0 81-1348818 Benzene
ug/L1.0 20.0 83-1178717 Chlorobenzene
ug/L1.0 20.0 71-1188116 Toluene
ug/L1.0 20.0 74-11911222 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10452
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10452
ug/L 50.0 59-134Surrogate: Toluene-d8 10150
Prepared: 05/03/2016 12:01 Analyzed: 05/04/2016 01:51Matrix Spike (6E03020-MS1)
Source: CZ05877-09
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331030.21 U21 1,1-Dichloroethene
ug/L1.0 20.0 81-134880.15 U18 Benzene
ug/L1.0 20.0 83-117820.17 U16 QM-07Chlorobenzene
ug/L1.0 20.0 71-118790.14 U16 Toluene
ug/L1.0 20.0 74-1191030.15 U21 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10552
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10754
ug/L 50.0 59-134Surrogate: Toluene-d8 9950
Prepared: 05/03/2016 12:01 Analyzed: 05/04/2016 02:51Matrix Spike Dup (6E03020-MSD1)
Source: CZ05877-09
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133101 20.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 1781-13488 0.060.15 U18 Benzene
ug/L1.0 20.0 1683-11785 30.17 U17 Chlorobenzene
ug/L1.0 20.0 1771-11880 10.14 U16 Toluene
ug/L1.0 20.0 2274-119112 80.15 U22 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10251
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10552
ug/L 50.0 59-134Surrogate: Toluene-d8 10050
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6D26020 - EPA 3005A
Prepared: 04/26/2016 10:39 Analyzed: 04/27/2016 12:18Blank (6D26020-BLK1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6D26020 - EPA 3005A
Prepared: 04/26/2016 10:39 Analyzed: 04/27/2016 12:18Blank (6D26020-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.100 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
ug/L10.03.10 U Lead
ug/L10.02.20 U Nickel
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.04.40 U Zinc
Prepared: 04/26/2016 10:39 Analyzed: 04/27/2016 12:22LCS (6D26020-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-120107214 Arsenic
ug/L10.0 200 80-120104208 Barium
ug/L1.00 20.0 80-12010420.7 Beryllium
ug/L1.00 20.0 80-12010521.0 Cadmium
ug/L10.0 200 80-120104207 Chromium
ug/L10.0 200 80-120104208 Cobalt
ug/L10.0 200 80-120101203 Copper
ug/L10.0 200 80-120102205 Lead
ug/L10.0 200 80-120107214 Nickel
ug/L10.0 200 80-120107214 Silver
ug/L10.0 200 80-120105211 Vanadium
ug/L10.0 200 80-120105210 Zinc
Prepared: 04/26/2016 10:39 Analyzed: 04/27/2016 12:29Matrix Spike (6D26020-MS1)
Source: CZ05054-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-1251096.80 U217 Arsenic
ug/L10.0 200 75-125103104309 Barium
ug/L1.00 20.0 75-1251060.98622.2 Beryllium
ug/L1.00 20.0 75-1251080.360 U21.6 Cadmium
ug/L10.0 200 75-1251061.40 U212 Chromium
ug/L10.0 200 75-1251078.31222 Cobalt
ug/L10.0 200 75-1251031.96207 Copper
ug/L10.0 200 75-1251053.10 U210 Lead
ug/L10.0 200 75-12510610.8223 Nickel
ug/L10.0 200 75-1251081.90 U216 Silver
ug/L10.0 200 75-1251081.40 U216 Vanadium
ug/L10.0 200 75-12510618.6231 Zinc
Prepared: 04/26/2016 10:39 Analyzed: 04/27/2016 12:39Matrix Spike Dup (6D26020-MSD1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6D26020 - EPA 3005A
Prepared: 04/26/2016 10:39 Analyzed: 04/27/2016 12:39Matrix Spike Dup (6D26020-MSD1) Continued
Source: CZ05054-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125108 0.86.80 U215 Arsenic
ug/L10.0 200 2075-125103 0.006104309 Barium
ug/L1.00 20.0 2075-125107 0.40.98622.3 Beryllium
ug/L1.00 20.0 2075-125107 0.80.360 U21.4 Cadmium
ug/L10.0 200 2075-125106 0.51.40 U213 Chromium
ug/L10.0 200 2075-125107 0.098.31221 Cobalt
ug/L10.0 200 2075-125102 0.11.96207 Copper
ug/L10.0 200 2075-125102 23.10 U205 Lead
ug/L10.0 200 2075-125106 0.0510.8223 Nickel
ug/L10.0 200 2075-125108 0.31.90 U217 Silver
ug/L10.0 200 2075-125108 0.31.40 U217 Vanadium
ug/L10.0 200 2075-125106 0.218.6231 Zinc
Prepared: 04/26/2016 10:39 Analyzed: 04/27/2016 12:42Post Spike (6D26020-PS1)
Source: CZ05054-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-1201030.00680 U0.207 Arsenic
mg/L0.0100 0.200 80-120970.00100 U0.297 Barium
mg/L0.00100 0.0200 80-1201010.000100 U0.0212 Beryllium
mg/L0.00100 0.0200 80-1201010.000360 U0.0203 Cadmium
mg/L0.0100 0.200 80-1201000.00140 U0.201 Chromium
mg/L0.0100 0.200 80-1201000.00110 U0.209 Cobalt
mg/L0.0100 0.200 80-120970.00160 U0.196 Copper
mg/L0.0100 0.200 80-120980.00310 U0.196 Lead
mg/L0.0100 0.200 80-1201010.00220 U0.212 Nickel
mg/L0.0100 0.200 80-1201020.00190 U0.204 Silver
mg/L0.0100 0.200 80-1201020.00140 U0.205 Vanadium
mg/L0.0100 0.200 80-1201030.00440 U0.224 Zinc
Batch 6D26040 - EPA 3005A
Prepared: 04/26/2016 14:23 Analyzed: 04/28/2016 13:03Blank (6D26040-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.220 U Antimony
ug/L3.000.910 U Selenium
ug/L1.000.110 U Thallium
Prepared: 04/26/2016 14:23 Analyzed: 04/28/2016 13:10LCS (6D26040-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120104208 Antimony
ug/L3.00 200 80-120112224 Selenium
ug/L1.00 200 80-120110221 Thallium
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6D26040 - EPA 3005A
Prepared: 04/26/2016 14:23 Analyzed: 04/28/2016 13:14Matrix Spike (6D26040-MS1)
Source: CZ05055-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-1251090.220 U218 Antimony
ug/L3.00 200 75-1251150.910 U230 Selenium
ug/L1.00 200 75-1251020.110 U204 Thallium
Prepared: 04/26/2016 14:23 Analyzed: 04/28/2016 13:18Matrix Spike Dup (6D26040-MSD1)
Source: CZ05055-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-125111 20.220 U222 Antimony
ug/L3.00 200 2075-125115 0.50.910 U231 Selenium
ug/L1.00 200 2075-125104 10.110 U207 Thallium
Prepared: 04/26/2016 14:23 Analyzed: 04/28/2016 13:21Post Spike (6D26040-PS1)
Source: CZ05055-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-1201090.220 U218 Antimony
ug/L3.00 200 80-1201160.910 U232 Selenium
ug/L1.00 200 80-1201060.110 U211 Thallium
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
The internal standard(s) for this sample were outside the acceptance limits due to sample
matrix interference. The sample was reanalyzed at a dilution.
QI-03
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-07
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