4504_Henderson_TRANSFER_TCLResults_DIN26265_20160615

#=CL#
June 07, 2016
LIMS USE: FR - PRIVATE CLIENT
LIMS OBJECT ID: 92298776
92298776
Project:
Pace Project No.:
RE:
Private Client
Private Client
Private Client
Asheville, NC 28804
Mills River Waste Yard
Dear Private Client:
Enclosed are the analytical results for sample(s) received by the laboratory on May 20, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Denise Trantham
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 11
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92298776
Mills River Waste Yard
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
Asheville Certification IDs2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 11
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92298776
Mills River Waste Yard
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92298776001 Potting Soil EPA 6010 7 PASI-ACDF
EPA 7470 1 PASI-AANB
EPA 8260 14 PASI-CDLK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 11
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298776
Mills River Waste Yard
Sample:Potting Soil Lab ID:92298776001 Collected:05/19/16 15:00 Received:05/20/16 11:39 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 05/24/16 17:00 Initial pH: 6.9; Final pH: 5.3
6010 MET ICP, TCLP
Arsenic ND mg/L 05/26/16 11:29 7440-38-205/25/16 15:000.050 1
Barium ND mg/L 05/26/16 11:29 7440-39-305/25/16 15:000.25 1
Cadmium ND mg/L 05/26/16 11:29 7440-43-905/25/16 15:000.0050 1
Chromium ND mg/L 05/26/16 11:29 7440-47-305/25/16 15:000.025 1
Lead ND mg/L 05/26/16 11:29 7439-92-105/25/16 15:000.025 1
Selenium ND mg/L 05/26/16 11:29 7782-49-205/25/16 15:000.10 1
Silver ND mg/L 05/26/16 11:29 7440-22-405/25/16 15:000.025 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 05/24/16 17:00 Initial pH: 6.9; Final pH: 5.3
7470 Mercury, TCLP
Mercury ND mg/L 05/26/16 10:37 7439-97-605/25/16 15:000.00020 1
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 05/29/16 11:148260 MSV TCLP
Benzene ND ug/L 05/31/16 18:20 71-43-219238.5
2-Butanone (MEK)ND ug/L 05/31/16 18:20 78-93-338538.5
Carbon tetrachloride ND ug/L 05/31/16 18:20 56-23-519238.5
Chlorobenzene ND ug/L 05/31/16 18:20 108-90-719238.5
Chloroform ND ug/L 05/31/16 18:20 67-66-319238.5
1,4-Dichlorobenzene ND ug/L 05/31/16 18:20 106-46-719238.5
1,2-Dichloroethane ND ug/L 05/31/16 18:20 107-06-219238.5
1,1-Dichloroethene ND ug/L 05/31/16 18:20 75-35-419238.5
Tetrachloroethene ND ug/L 05/31/16 18:20 127-18-419238.5
Trichloroethene ND ug/L 05/31/16 18:20 79-01-619238.5
Vinyl chloride ND ug/L 05/31/16 18:20 75-01-419238.5
Surrogates
1,2-Dichloroethane-d4 (S)94 %05/31/16 18:20 17060-07-0 1g70-130 38.5
Toluene-d8 (S)100 %05/31/16 18:20 2037-26-567-135 38.5
4-Bromofluorobenzene (S)91 %05/31/16 18:20 460-00-470-130 38.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/07/2016 01:32 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298776
Mills River Waste Yard
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/9489
EPA 7470
EPA 7470
7470 Mercury TCLP
Associated Lab Samples:92298776001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1741987
Associated Lab Samples:92298776001
Matrix:Water
Analyzed
Mercury mg/L ND 0.00020 05/26/16 10:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1741988LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/L 0.0025.0025 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1741989MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92298076001
1741990
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/L .0025 102 75-12596 6.0025ND 0.0026 0.0024
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/07/2016 01:32 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298776
Mills River Waste Yard
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/21831
EPA 3010A
EPA 6010
6010 MET TCLP
Associated Lab Samples:92298776001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1741893
Associated Lab Samples:92298776001
Matrix:Water
Analyzed
Arsenic mg/L ND 0.050 05/26/16 11:03
Barium mg/L ND 0.25 05/26/16 11:03
Cadmium mg/L ND 0.0050 05/26/16 11:03
Chromium mg/L ND 0.025 05/26/16 11:03
Lead mg/L ND 0.025 05/26/16 11:03
Selenium mg/L ND 0.10 05/26/16 11:03
Silver mg/L ND 0.025 05/26/16 11:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1741894LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 2.52.5 102 80-120
Barium mg/L 2.42.5 96 80-120
Cadmium mg/L 2.52.5 101 80-120
Chromium mg/L 2.52.5 99 80-120
Lead mg/L 2.42.5 97 80-120
Selenium mg/L 2.62.5 103 80-120
Silver mg/L 1.11.2 89 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1741895MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92298496001
1741896
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/L 2.5 115 75-12597 172.5ND 2.9 2.4
Barium mg/L 2.5 108 75-12585 162.51.2 3.9 3.3
Cadmium mg/L 2.5 112 75-12584 162.52.0 4.8 4.1
Chromium mg/L 2.5 106 75-12591 152.5ND 2.7 2.3
Lead mg/L 2.5 104 75-12581 152.51.5 4.1 3.6
Selenium mg/L 2.5 114 75-12598 152.5ND 2.9 2.5
Silver mg/L 1.2 111 75-12595 161.2ND 1.4 1.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/07/2016 01:32 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298776
Mills River Waste Yard
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/37074
EPA 8260
EPA 8260
8260 MSV TCLP
Associated Lab Samples:92298776001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1745399
Associated Lab Samples:92298776001
Matrix:Water
Analyzed
1,1-Dichloroethene ug/L ND 5.0 05/31/16 13:50
1,2-Dichloroethane ug/L ND 5.0 05/31/16 13:50
1,4-Dichlorobenzene ug/L ND 5.0 05/31/16 13:50
2-Butanone (MEK)ug/L ND 10.0 05/31/16 13:50
Benzene ug/L ND 5.0 05/31/16 13:50
Carbon tetrachloride ug/L ND 5.0 05/31/16 13:50
Chlorobenzene ug/L ND 5.0 05/31/16 13:50
Chloroform ug/L ND 5.0 05/31/16 13:50
Tetrachloroethene ug/L ND 5.0 05/31/16 13:50
Trichloroethene ug/L ND 5.0 05/31/16 13:50
Vinyl chloride ug/L ND 5.0 05/31/16 13:50
1,2-Dichloroethane-d4 (S)%105 70-130 05/31/16 13:50
4-Bromofluorobenzene (S)%97 70-130 05/31/16 13:50
Toluene-d8 (S)%101 67-135 05/31/16 13:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1745400LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1745401
1,1-Dichloroethene ug/L 59.850 120 66-13511658.2 3 30
1,2-Dichloroethane ug/L 52.050 104 67-12810451.9 0 30
1,4-Dichlorobenzene ug/L 51.150 102 78-13010351.4 1 30
2-Butanone (MEK)ug/L 108100 108 61-1449998.9 9 30
Benzene ug/L 52.150 104 80-12510452.1 0 30
Carbon tetrachloride ug/L 51.850 104 69-13110753.6 3 30
Chlorobenzene ug/L 52.050 104 81-12210552.5 1 30
Chloroform ug/L 54.950 110 73-12710854.2 1 30
Tetrachloroethene ug/L 38.950 78 78-1227939.7 2 30
Trichloroethene ug/L 49.950 100 78-1229848.9 2 30
Vinyl chloride ug/L 60.450 121 58-13711959.3 2 30
1,2-Dichloroethane-d4 (S)%103 70-130108
4-Bromofluorobenzene (S)%96 70-130101
Toluene-d8 (S)%100 67-135102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/07/2016 01:32 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 11
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92298776
Mills River Waste Yard
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
8260 results are from a total analysis which show that analytes are not present or that they are present but at such low
levels that the appropriate regulatory levels could not possibly be exceeded, per Section 1.2 of Method 1311.1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/07/2016 01:32 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 11
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92298776
Mills River Waste Yard
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92298776001 MPRP/21831 ICP/19570Potting Soil EPA 3010A EPA 6010
92298776001 MERP/9489 MERC/9126Potting Soil EPA 7470 EPA 7470
92298776001 MSV/37074Potting Soil EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/07/2016 01:32 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 11
Page 10 of 11
Page 11 of 11
1
Frost, Larry
From:Aja, Deborah
Sent:Monday, June 13, 2016 5:10 PM
To:Chip Gould; [e-mail]
Cc:Watkins, Jason; Gallagher, Tony; Frost, Larry; Hill, Lee; Drummond, Jaclynne
Subject:RE: tclp results for potting soil
Chip and Marcus,   
We have reviewed the June 7, 2016 TCLP results.  Based on the information provided there are no hazardous concerns 
with the materials tested.  The next step is to work with Larry Frost to submit your proposal to process the plant pots 
and soil at the Henderson County solid waste facilities. 
Thank you both again for your efforts to conduct this site clean‐up. 
Deb 
Deborah Aja
Western District Supervisor
Division of Waste Management - Solid Waste Section
North Carolina Department of Environmental Quality

828 296-4702 office
919 208-0184 mobile
[e-mail]

2090 U.S. Highway 70
Swannanoa, NC 28778

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Chip Gould [mailto:[e-mail]]  
Sent: Thursday, June 09, 2016 1:33 PM 
To: [e-mail]; Aja, Deborah <[e-mail]> 
Subject: FW: tclp results for potting soil 

Here are the results. Let me know if I need to forward to anyone else. Chip 
2

From: Denise Trantham [mailto:[e-mail]]  
Sent: Wednesday, June 08, 2016 8:54 AM 
To: [e-mail] 
Subject: tclp results for potting soil 

Dear Chip,
Enclosed you will find the potting soil results you were looking for. Please note that your actual results are on page four.
You will notice that it came back ND which stands for non detect. If there is anything else we can help you with please
feel free to give us a call.
Thanks,
Denise

Denise Trantham
Project Coordinator
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Ext. 23

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