HomeMy WebLinkAboutIII.F. Environmental Reports - 2014-12-19 Terracon LSI-OCRLimited Site Investigation Report
Proposed Durham Police Headquarters
113 S. Elizabeth Street, 601 E. Ramseur Street, 605 E. Ramseur Street,
101 S. Elizabeth Street, 616 E. Main Street, and 102 Hood Street
Durham, Durham County,North Carolina
December 19, 2014
Terracon Project No. 70147828
Prepared for:
City of Durham
Durham, North Carolina
Prepared by:
Terracon Consultants, Inc.
Raleigh, North Carolina
ii
TABLE OF CONTENTS
1.0 SITE DESCRIPTION ....................................................................................................... 3
2.0 SCOPE OF SERVICES ................................................................................................... 4
2.1 Standard of Care.................................................................................................. 5
2.2 Additional Scope Limitations ................................................................................ 5
2.3 Reliance ............................................................................................................... 5
3.0 FIELD INVESTIGATION METHODS ............................................................................... 6
3.1 Soil Borings.......................................................................................................... 6
3.2 Temporary Monitoring Well Installation and Sampling .......................................... 7
3.3 Abandonment Activities........................................................................................ 8
4.0 DATA EVALUATION ...................................................................................................... 8
4.1 Soil Analytical Results .......................................................................................... 8
4.2 Groundwater Analytical Results ........................................................................... 9
5.0 SUMMARY AND CONCLUSIONS ................................................................................ 10
6.0 RECOMMENDATIONS ................................................................................................. 11
7.0 REFERENCES .............................................................................................................. 11
ATTACHMENTS
Appendix A: Exhibit 1 – Topographic Vicinity Diagram
Exhibit 2 – Boring Location Diagram
Appendix B: Table 1 – Summary of Groundwater Monitoring Well Construction Details
Table 2 – Summary of Compounds Detected in Soil Samples
Table 3 – Summary of Compounds Detected in Groundwater Samples
Appendix C: Soil Boring Logs
Appendix D: Analytical Report and Chain of Custody
Responsive ■Resourceful ■Reliable
LIMITED SITE INVESTIGATION REPORT
PROPOSED DURHAM POLICE HEADQUARTERS
113 S. ELIZABETH STREET, 601 E. RAMSEUR STREET, 605 E. RAMSEUR STREET,
101 S. ELIZABETH STREET, 616 E. MAIN STREET, and 102 HOOD STREET
DURHAM, DURHAM COUNTY, VIRGINIA
Terracon Project No. 70147828
December 19, 2014
1.0 SITE DESCRIPTION
The site consists of six parcels totaling 4.523 acres located in downtown Durham, Durham
County, North Carolina, within the city block formed by S. Elizabeth Street to the north, E. Main
Street to the east, Hood Street to the south, and Ramseur Street to the west. Walker Street
bisects the east end of the site. Walker Street is included in the site as it is owned by the current
site owner and not a public street. The site encompasses the following addresses:
n 113 S. Elizabeth Street;
n 601 E. Ramseur Street;
n 605 E. Ramseur Street;
n 101 S. Elizabeth Street;
n 616 E. Main Street; and
n 102 Hood Street.
The site location is depicted on a Topographic Vicinity Diagram (Exhibit 1) of Appendix A, which
was reproduced from a portion of the USGS 7.5-minute series topographic map. A Boring
Location Diagram is included as Exhibit 2 of Appendix A.
Based on a review of the historical information, the site was originally developed with multiple
residences from the early 1900s until the 1920s when the site was developed with auto dealership
with repair/service operations, and a truck parts/repair operation in the late 1940s
The following site features and/or historical uses were identified during completion of a Phase I
ESA (Terracon Project No. 70147828 dated December 19, 2014)
Underground Storage Tanks (101 S. Elizabeth Street & 616 E. Main Street)
A former on-site filling station at the corner of S Elizabeth Street & Walker Street, presently 101
S. Elizabeth St) operated during the 1930s until at least the 1950s. Two former underground
storage tanks (USTs) are depicted on historical Sanborn fire insurance maps along S Elizabeth
St. and one UST is depicted along Walker St. Terracon did not observe evidence of current USTs
and the status of the three USTs is unknown. Auto service/repair operations also occurred on-
site since the late 1920s which included operation of a paint booth within the building since at
least the 1930s.
Limited Site Investigation Report
Proposed Durham Police Headquarters ■Durham,North Carolina
December 19, 2014 ■Terracon Project No.70147828
Responsive ■Resourceful ■Reliable 3
A former filling station operated at 616 E. Main Street during the 1930s and undocumented
removal of up to three 250-gallon USTs in 1988 constitute a REC to the site. Additionally, an auto
sales and service building is depicted on the historical Sanborn fire insurance maps during the
1930s and 1950s. Prior reports depict two 1,000-gallon fuel oil USTs on the parcel. The reported
use was associated with fueling building furnaces. The tanks (listed below as Tanks 4 and 5)
were reportedly removed in 1988, and closure reports are not available as this pre-dates UST
closure reporting requirements.
Sumps, cisterns, catch basins and/or dry wells (113 S. Elizabeth Street)
Based on site observations and interviews with Mr. Mark Carpenter, Terracon observed and/or
understands the following belowground pits/structures are located at the site:
n One former belowground truck repair pit within the Ciderworks space at 113 S. Elizabeth
St. The pit was covered by a refrigeration unit at the time of the site reconnaissance.
According to Mr. Carpenter, the pit had a ladder or stairs to access the pit and allowed for
large trucks to be parked over the pit while employees worked on trucks from within the
pit. He was unaware of any drains within the pit and indicated the pit was mostly filled
with concrete years ago.
n One sump pit (or possible oil/water separator) located along the southern wall within the
former auto repair area. According to Mr. Carpenter, the trench drains that run the length
of the former auto repair area drain to the sump pit.
Hydraulic Lifts & Floor Drains (113 S. Elizabeth Street)
Terracon observed evidence of numerous former in-ground hydraulic lifts within the former auto
service area at 113 S. Elizabeth Street. Terracon estimates approximately 15 former lifts,
however, an exact number could not be determined due to the presence of objects stored within
the building at the time of the site reconnaissance. Each lift contained a small hydraulic oil tank
contained in sub-grade concrete vaults. According to Mr. Mark Carpenter the lifts have been
abandoned by filling the vaults with sand and covering the vaults with concrete.
Drums, barrels, and/or containers >5 gallons (113 S. Elizabeth Street & 218 Hood Street)
Within the Carolina Auto Masters tenant space at 113 S. Elizabeth Street and Durham Auto
Center at 218 Hood St, Terracon observed numerous containers including five 55-gallon plastic
drums of used oil, one 55-gallon plastic drum of antifreeze, five 19-gallon drums of racing fuel, a
parts washer with petroleum solvent, and several smaller containers of petroleum products
including hydraulic fluid, transmission fluid, new and used oil, fuel additives, etc. The containers
were observed to be stored on the concrete floor of the buildings. Surficial staining was observed
on the concrete floor beneath the containers.
Limited Site Investigation Report
Proposed Durham Police Headquarters ■Durham,North Carolina
December 19, 2014 ■Terracon Project No.70147828
Responsive ■Resourceful ■Reliable 4
Oil/water separators (113 S. Elizabeth Street)
One oil/water separator was observed within the Ciderworks space at 113 S. Elizabeth St. The
building was originally constructed in 1948. According to Mr. Carpenter the oil/water separator
was formerly associated with the truck repair operations and had not been utilized for many years.
He indicated the unit drained to a stormwater drain north of the building.
Interior Floor Drains (101 S. Elizabeth Street)
Interior floor drains were observed within the former service bay areas associated with auto repair
operations in the buildings located at 101 S. Elizabeth Street and 113 S. Elizabeth Street. The
floor drains reportedly discharge to the municipal sewer or stormwater system.
Stained pavement or similar surface (101 S. Elizabeth Street & 113 S. Elizabeth Street)
Numerous areas of stained concrete were observed within the current and former service bay
areas associated with auto repair operations in the buildings located at 101 S. Elizabeth Street
and 113 S. Elizabeth Street. The staining appeared to be contained on the concrete floor within
the building.
Previous Site Usage
101 S. Elizabeth Street and 113 S. Elizabeth Street were formerly operated as automotive repair
including the use and/or disposal of petroleum products and/or solvents. Site usage included an
oil/water separator, sump pit, floor drains, and truck repair pit.
Terracon observed evidence of numerous former in-ground hydraulic lifts within the former auto
service area at 113 S. Elizabeth Street. Each lift contained a small hydraulic oil tank contained
in sub-grade concrete vaults. The vaults have reportedly been filled with sand and the vaults
covered with concrete.
601 E Ramseur Street was formerly occupied by P&H Engineering & Mfg. Co. who manufactured
and assembled airplane and electronic components during the 1980s. Additionally, a former
tenant during the 2000s included auto detailing and collision repair.
2.0 SCOPE OF SERVICES
Based on the findings of the Phase I assessment and at the request of the City of Durham, the
objective of the LSI is to evaluate the presence of volatile organic compounds (VOC) and semi-
volatile organic compounds (SVOCs) above relevant laboratory reporting limits in the on-site soils
and groundwater as a result of potential releases from historic site uses.
Terracon conducted this Limited Site Investigation (LSI) in conjunction with our geotechnical
investigation which is provided under separate cover.
Limited Site Investigation Report
Proposed Durham Police Headquarters ■Durham,North Carolina
December 19, 2014 ■Terracon Project No.70147828
Responsive ■Resourceful ■Reliable 5
2.1 Standard of Care
Terracon’s services were performed in a manner consistent with generally accepted practices of
the profession undertaken in similar studies in the same geographical area during the same time.
Terracon makes no warranties, either expressed or implied, regarding the findings, conclusions,
or recommendations. Please note that Terracon does not warrant the work of laboratories,
regulatory agencies, or other third parties supplying information used in the preparation of the
report. These LSI services were performed in accordance with the scope of work authorized by
you, our client, as reflected in our proposal and were not performed in strict conformance of ASTM
E1903-11.
2.2 Additional Scope Limitations
Findings, conclusions and recommendations resulting from these services are based upon
information derived from the on-site activities and other services performed under this scope of
work; such information is subject to change over time. Certain indicators of the presence of
hazardous substances, petroleum products, or other constituents may have been latent,
inaccessible, unobservable, not detected or not present during these assessment activities; thus,
we cannot represent that the site is free of hazardous substances, toxic materials, petroleum
products, or other latent conditions beyond those identified during this LSI. Subsurface conditions
may vary from those encountered at specific borings or wells or during other surveys, tests,
assessments, investigations or exploratory services; the data, interpretations, findings, and our
recommendations are based solely upon data obtained at the time and within the scope of these
services.
2.3 Reliance
This report has been prepared for the exclusive use of the City of Durham, and their successors
and assigns. Any authorization for use or reliance by any other party (except a governmental
entity having jurisdiction over the site) is prohibited without the expressed written authorization of
the City of Durham and Terracon. Any unauthorized distribution or reuse is at the City of Durham’s
sole risk. Reliance by authorized parties will be subject to the terms, conditions, and limitations
stated in Terracon’s Proposal No. P70140466R , dated October 27, 2014, and the Agreement for
Services between the City of Durham and Terracon. The limitation of liability defined in the terms
and conditions is the aggregate limit of Terracon’s liability to the City of Durham and all relying
parties unless otherwise agreed in writing.
Limited Site Investigation Report
Proposed Durham Police Headquarters ■Durham,North Carolina
December 19, 2014 ■Terracon Project No.70147828
Responsive ■Resourceful ■Reliable 6
3.0 FIELD INVESTIGATION METHODS
Field activities were conducted from December 2 through 5, 2014. Activities included boring
layout, a ground penetrating radar (GPR) and electromagnetic (EM) survey, request for public
utility locate by NC811, advancement of four soil borings, and installation of temporary
groundwater monitoring wells. The GPR and EM surveys were conducted on December 2, 2014
and the boring layout and boring advancement were conducted on December 3 and 4, 2014.
Groundwater sampling of temporary monitoring wells was conducted on December 5, 2014.
Exhibit 2 depicts the layout of the site and boring locations.
The GPR and EM survey did not identify sub-grade objects that appeared to correspond to USTs
or associated piping that were identified in historical review of the site.
3.1 Soil Borings
Terracon advanced four hollow-stem auger borings to depths between 38.9 feet below land
surface (bls) and 48.8 feet bls with a North Carolina licensed well driller utilizing a track-mounted
Diedrich D-50 track mounted drill rig in the following locations:
n Boring B-1 - located in the northwest corner of the overall parcel adjacent to the former
electrical component manufacturer at 601 E. Ramseur Street. The boring was advanced
to an approximate depth of 39.3 feet bls;
n Boring B-7 – located in the parking lot of Bull City Ciderworks at 113 S. Elizabeth Street
adjacent to the former UST and storm drain connected to an oil/water separator. The
boring was advanced to a depth of 48.8 feet bls;
n Boring B-8 – located near the center of the overall parcel and adjacent to the western wing
of 101 S. Elizabeth Street adjacent to former paint booth. The boring was advanced to a
depth of 40 feet bls;
n Boring B-9 – located along the eastern edge of the overall parcel and near the center of
the undeveloped property at 616 E. Main Street near the suspected location of a former
UST. The boring was advanced to a depth of 38.9 feet bls;
Discreet soil samples were collected from the hollow-stem auger soil borings via split-spoon
samplers to document soil type, relative moisture content, and other lithologic characteristics. Soil
from four of the borings (B-1, B-7, B-8, and B-9) was visually observed and field-screened. Each
soil sample was placed into a dedicated, re-sealable plastic bag and screened for organic vapors
using an 11.7 eV photoionization detector (PID). The PID data were collected in order to
corroborate laboratory data and assist in selection of sample intervals for laboratory analysis. PID
readings from the borings ranged from 0.6 parts per million (ppm) to 12.8 ppm. Odors were not
noted in soil samples during site reconnaissance. A summary of PID readings is included on the
soil boring logs in Appendix C.
Limited Site Investigation Report
Proposed Durham Police Headquarters ■Durham,North Carolina
December 19, 2014 ■Terracon Project No.70147828
Responsive ■Resourceful ■Reliable 7
The site lithology is classified as the Triassic Basin Formation. Soils at the site were generally
characterized as 3 to 26 feet of residual, soft to stiff sandy silt and clay soils overlying partially
weathered rock (PWR) comprised of sandstone with interbedded siltstone. Hollow-stem auger
refusal was encountered in partially weathered rock (PWR) materials at approximate depths of
28.8, 56.2 and 47-feet bls in borings B-2, B-4 and B-10, respectively.
Groundwater was encountered during drilling operations at depths between 30.6 and 32 feet bls.
The borings were converted into temporary groundwater monitoring wells and subsequently
purged and sampled. The depths to groundwater in temporary monitoring wells B-1, B-7, B-8,
and B-9 were approximately 9.6 feet bls, 11.3 feet bls, 10.5 feet, and 9.4 feet bls, respectively.
One soil sample was collected from each of the borings. Sample intervals were based on field
observations and PID readings. Four soil samples were collected for laboratory analysis at the
following depths:
n B-1 (33.5-35.0’)n B-8 (6.0-7.5’)
n B-7 (18.5-20.0’)n B-9 (6.0-7.5’)
Soil samples were packed in sample containers provided by Shealy Environmental Services, Inc.
(Shealy). The sample containers were packed in ice and shipped via FedEx along with chain of
custody documentation to Shealy in West Columbia, South Carolina for analysis of:
n volatile organic compounds (VOCs) by EPA Method 8260; and,
n polyaromatic hydrocarbons (PAHs) by EPA Method 8270.
All non-dedicated sampling equipment was decontaminated using a Liquinox®/water wash
followed by a distilled water rinse prior to use and between borings.
3.2 Temporary Monitoring Well Installation and Sampling
Terracon constructed four temporary groundwater sampling points, B-1, B-7, B-8, and B-9 with
the following materials:
n Installation of a 10 to 15-foot section of 1-inch diameter, 0.010-inch machine slotted
PVC well screen;
n Installation of a 1-inch diameter, threaded, flush-joint PVC riser pipe to the ground
surface and;
n Placement of sand in the borehole annulus to one-foot above the screen followed by
a one-foot layer of hydrated bentonite seal.
A summary of groundwater monitoring well construction details is presented in Table 1.
Limited Site Investigation Report
Proposed Durham Police Headquarters ■Durham,North Carolina
December 19, 2014 ■Terracon Project No.70147828
Responsive ■Resourceful ■Reliable 8
Each temporary monitoring well was purged with a peristaltic pump using low flow sampling
techniques (i.e., <200 milliliters per minute) prior to sampling. A groundwater sample was
collected directly into laboratory supplied containers at low flow sampling rates. The following
parameters were measured after sampling: pH, temperature, oxidation reduction potential (ORP),
dissolved oxygen (DO), and conductivity. The groundwater samples were packed on ice and
shipped via FedEx along with chain of custody documentation to Shealy in West Columbia, South
Carolina for analysis of:
n VOCs by EPA Method 8260; and,
n PAHs by EPA Method 8270.
The drilling equipment used in the field at the site was thoroughly decontaminated prior to use
and between the advancement of each boring. Non-dedicated sampling equipment was
decontaminated using a Liquinox®/water wash followed by a distilled water rinse.
Investigation derived waste (IDW) was containerized in eleven 55-gallon drums, which were
sealed and left on the site pending off-site disposal.
3.3 Abandonment Activities
Following sampling activities, above grade well materials were removed from temporary
monitoring wells B-1, B-7, B-8, and B-9. The well borings were filled with bentonite pellets and
hydrated. Borings completed within the on-site asphalt pavement were patched.
4.0 DATA EVALUATION
The following sections discuss the field and laboratory results. Laboratory analytical reports from
Shealy Environmental Services, Inc. and field data associated with samples collected by Terracon
personnel were reviewed to ensure that specific data-quality objectives were met. Laboratory
analytical reports are provided in Appendix D.
4.1 Soil Analytical Results
Reported VOC and PAH concentrations from the soil samples were compared to the North
Carolina Department of Environment and Natural Resources (NCDENR) Industrial/Commercial
Soil Cleanup Level and Soil-to-Water Maximum Soil Contaminant Concentrations (MSCCs).
The laboratory results reported a concentration of acetone at 48 milligrams per kilogram (mg/kg)
in soil sample B-9 (6.0-7.5), which exceeded its Soil-to-Water MSCC of 24 mg/kg but was below
its NCDENR Industrial/Commercial Soil Cleanup Level of 360,000 mg/kg.
Limited Site Investigation Report
Proposed Durham Police Headquarters ■Durham,North Carolina
December 19, 2014 ■Terracon Project No.70147828
Responsive ■Resourceful ■Reliable 9
According to laboratory results, PAH constituents were not reported above method detection limits
from soil samples obtained on-site.
A summary of the constituents detected in the soils is included on Table 2.
4.2 Groundwater Analytical Results
Reported concentrations from the groundwater samples were compared to the NCDENR North
Carolina Administrative Code (NCAC) 2L Groundwater Quality Standards (GWQS) and the
NCDENR Division of Waste Management (DWM) Non-Residential Vapor Intrusion Screening
Levels (June 2014).
The following VOC was detected above their respective NCAC 2L GWQS but below their DWM
Non-Residential Vapor Screening Level:
n Benzene was detected in two samples (B-1 and B-7) at concentrations of 1.1 and
31 micrograms per liter (µg/L), respectively, compared to its NCAC 2L GWQS of
1.0 µg/L and their DWM Non-Residential Vapor Screening Levels of 69.3 µg/L.
The following VOCs did not exceed their respective NCAC 2L GWQS or DWM Non-Residential
Vapor Screening Levels, but were detected above the laboratory’s reporting limit.
n Acetone was detected in sample B-9.
n Benzene was detected in sample B-8.
n Chloroform was detected in samples B-1 and B-7.
n Ethylbenzene was detected in sample B-7.
n Isopropylbenzene was detected in sample B-7.
n Methyl tertiary butyl ether (MTBE) was detected in samples B-1 and B-7.
n Styrene was detected in sample B-7.
n Toluene was detected in sample B-7.
n Xylenes (total) was detected in sample B-7.
The following PAH was detected at or above its respective NCAC 2L GWQS but below its DWM
Non-Residential Vapor Screening Level:
n Naphthalene was detected in one sample (B-7) at a concentration of 6.0 µg/L compared
to its NCAC 2L GWQS of 6.0 µg/L and its DWM Non-Residential Vapor Screening Levels
of 146 µg/L.
Detected constituents are generally consistent with a release of gasoline and/or diesel fuel. A
summary of the constituents detected in the groundwater is included on Table 3.
Limited Site Investigation Report
Proposed Durham Police Headquarters ■Durham,North Carolina
December 19, 2014 ■Terracon Project No.70147828
Responsive ■Resourceful ■Reliable 10
5.0 SUMMARY AND CONCLUSIONS
The findings and conclusions of this investigation are discussed below.
n The site lithology is classified as Triassic Basin Formation. Site soils were generally
characterized as residual sandy silt and clay underlain by partially weathered rock (PWR).
n Low to moderate PID readings were noted in soil samples collected from the borings
performed at the site.
n Groundwater was encountered during drilling operations at depths between 30.6 and 32
feet bls. The borings were converted into temporary groundwater monitoring wells and
subsequently purged and sampled. Groundwater was encountered in temporary
monitoring wells B-1, B-7, B-8, and B-9 at approximate depths of 9.6 feet bls, 11.3 feet
bls, 10.5 feet, and 9.4 feet bls, respectively
n According to laboratory analytical results, a single constituent, acetone, was detected at
a concentration above its respective Soil-to-Groundwater MSCC.
n According to laboratory analytical results, a single petroleum constituent, benzene, was
detected at a concentration above its respective NCAC 2L GWQS.
n Data does not indicate a potential for vapor intrusion.
n Detected constituents are consistent with a release of gasoline and/or diesel fuel.
Limited Site Investigation Report
Proposed Durham Police Headquarters ■Durham,North Carolina
December 19, 2014 ■Terracon Project No.70147828
Responsive ■Resourceful ■Reliable 11
6.0 RECOMMENDATIONS
The results of this investigation confirmed the presence of petroleum impacts at the site above
regulatory standards, but did not confirm the magnitude, extent, and/or source of the impacts.
Based on the results of this investigation, Terracon recommends that if the client should elect to
pursue development of the site, this report should be provided to the NCDENR. Sufficient data
was not collected to determine if releases were associated with closed UST incidents.
The potential exists for the soil at the site to have been impacted by petroleum and/or solvent
releases not investigated by our limited soil and groundwater sampling. Based on the scope of
services, limitations, and findings of this investigation, Terracon recommends the following
options for dealing with impacted soil:
n Terracon recommends conducting limited soil sampling in the vicinity of likely
impacted areas (former UST locations, floor drains, sump pit, oil/water separator,
back doors, etc.) in an effort to define extent of soil impacts to be encountered
during construction activities. It is recommended the buildings be
unoccupied/vacant at the time of our sampling activities to allow for complete
access to relevant site features.
n Terracon recommends anticipation of impacted soil during construction activities.
Prior to excavation, a Soil Management Plan (SMP) should be developed to outline
worker protection procedures, impacted soil handling and segregation procedures,
and disposal options. The SMP and coordination with the contractor would
minimize schedule delays and costs associated with encountered impacted soils.
7.0 REFERENCES
n Phase I Environmental Site Assessment,Proposed Durham Police Headquarters, dated
December 19, 2014 prepared by Terracon (Terracon Project No. 70147828)
n ASTM E1903-11 Standard Practice for Environmental Site Assessments: Phase II
Environmental Site Assessment Process
n Geologic Map of North Carolina, Department of Natural Resources and Community
Development, S. Thomas Rhodes Secretary, 1985
APPENDIX A
Exhibit 1 – Topographic Vicinity Diagram
Exhibit 2 – Boring Location Diagram
TOPOGRAPHIC MAP IMAGE COURTESY OF THE U.S. GEOLOGICAL SURVEY
QUADRANGLES INCLUDE: NORTHWEST DURHAM, NC (1/1/1999), NORTHEAST DURHAM, NC (1/1/1999), SOUTHWEST DURHAM, NC (1/1/2002) and SOUTHEAST DURHAM, NC(1/1/2002).
2401 Brentwood Rd. Suite 107
Raleigh, NC
Project Manager:
Drawn by:
Checked by:
Approved by:
TOPOGRAPHIC VICINITY DIAGRAM
Proposed Durham Police Headquarters
113 S Elizabeth Street
Durham, NC
70147828
MHF
MTJ
MTJ
1:24,000
Exhibit 1
12/12/14
1
ExhibitMTJ
Project No.
Scale:
File Name:
Date:
Project Mngr:
Approved By:
Checked By:
Drawn By:
Project No.
Scale:
Date:
File No.Consulting Engineers and Scientists
Exhibit No.
2401 Brentwood Road, Ste. 107 Raleigh, North Carolina
FAX. (919) 873-9555PH. (919) 873-2211
MTJ
MHF
MTJ
MTJ
70147828
AS SHOWN
Exhibits.dwg
December 2014
BORING LOCATION DIAGRAM
Proposed Durham Police Headquarters
Durham, North Carolina
113 S Elizabeth Street 2
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Approximate Boring Location - Analytical Testing
APPENDIX B
Table 1 – Summary of Groundwater Monitoring Well Construction Details
Table 2 – Summary of Compounds Detected in Soil Samples
Table 3 – Summary of Compounds Detected in Groundwater Samples
Table 1
B-1 12/4/2014 38 28-38 9.6
B-7 12/4/2014 48 33-48 11.3
B-8 12/4/2014 40 25-40 10.5
B-9 12/3/2014 38 23-38 9.4
Notes: 1)ft bls - feet below land surface
2)
Summary of Groundwater Monitoring Well Construction Details
Proposed Durham Police Headquarters
Durham, Durham County, North Carolina
Terracon Project No. 70147828
Depth to Water
Measurement (ft bls)Well ID Date Installed Well Depth (ft bls)Screen Interval
(ft bls)
Wells abandoned on 12/4/14 in accordance with 15 NCAC 2C .0100 Well Construction Rules after sampling
Sample ID:
Sample Date:Sample Depth (ft bls):
Volatile Organic Compounds (EPA Method 8260)
Acetone 24 360,000 48
2) Concentrations are reported in milligrams per kilogram (mg/kg)
7) Detections highlighted in grey exceed their respective Soil-to-Groundwater MSCCs and/or
Industrial/Commercial Soil Cleanup Levels
Terracon Project No. 70147828
Analyte Industrial/ Commercial Soil
Cleanup Levels (mg/kg)
Soil-to-Groundwater MSCCs
(mg/kg)
B-9 (6.0-7.5)
Notes: 1) Only detected compounds are shown in the table
3) MSCCs - Maximum Soil Contaminant Concentrations (4/2012)
4) ft bls - feet below land surface
Table 2
Summary of Compounds Detected in Soil Samples
Proposed Durham Police Headquarters
Durham, Durham County, North Carolina
12/04/14
6.0-7.5
Sample ID:
Sample Date:
Screen Interval:
Volatile Organic Compounds (EPA Method 8260)
Acetone 6,000 1.90E+07 <10.0 <10.0 <10.0 3.5J
Benzene 1.0 6.93E+01 1.1 31 0.63 <0.50
Chloroform 70 3.55E+01 0.99 0.60 <0.50 <0.50
Ethylbenzene 600 1.52E+02 <0.50 1.3 <0.50 0.76
Isopropylbenzene 70 NS <0.50 1.6 <0.50 <0.50
Methyl tertiary butyl ether (MTBE)20 1.97E+04 0.58 9.5 <0.50 <0.50
Styrene 70 7.79E+03 <0.50 0.61 <0.50 <0.50
Toluene 600 1.61E+04 <0.50 0.40 J <0.50 <0.50
Xylenes (total)500 4.14E+02 <0.50 54 <0.50 <0.50
Polycyclic Aromatic Hydrocarbons (EPA Method 8270)
Naphthalene 6 1.46E+02 <5.0 6.0 <5.0 <5.0
2) Concentrations are reported in micrograms per liter (μg/L)
5) DWM Non-Residential Screening Levels - NCDENR Division of Waste Management Non-Residential Vapor Intrusion Screening Levels (June 2014)
12/05/14
23-38 (ft bls)
Table 3
Summary of Compounds Detected in Groundwater Samples
Proposed Durham Police Headquarters
Durham, Durham County, North Carolina
DWM Non-Residential
Vapor Screening Levels
(µg/L)
Terracon Project No. 70147828
Analyte NCAC 2L GWQS
(µg/L)28-38 (ft bls)
B-7
12/05/14
B-9
33-48 (ft bls)
12/05/14
B-1 B-8
12/05/14
25-40 (ft bls)
6) NS - no standard
Notes: 1) Only detected compounds are shown in the table
3) J - compound was detected at an estimated concentration above the method detection limit and below the reporting limit
4) NCAC 2L GWQS - North Carolina Administrative Code Subchapter 2L Groundwater Quality Standards (April 1, 2013)
APPENDIX C
Soil Boring Logs
0.20.7
22.5
28.5
32.5
39.3
ASPHALT, 2"
AGGREGATE BASE, 6"
SANDY FAT CLAY (CH),triassic basin formation,, residual
material, purple to orange, softto stiff, mottled coloring,
considerable variation inconsistency
PARTIALLY WEATHEREDROCK (PWR), purple to pale
olive with orange seams, hard,claystone, blocky structure
SILTY SAND, residual material,
tan to pale yellowish brown,medium dense
PARTIALLY WEATHEREDROCK (PWR), fine grained, tanto pale yellowish brown, hard to
very hard, sandstone
Boring Terminated at 39.3 Feet
Analytical Sample Taken at 33.5'
2.1
3.1
3.1
3.2
3.8
4.3
4.5
5.5
6.9
6.4
25 66-26-40
Open to the
ground
surface
Bentonitechips
10x20 sandfilter pack
10 feet wellscreen
18
18
18
18
16
18
3
16
4
8
406405.5
383.5
377.5
373.5
366.5
2-2-2N=4
3-4-4N=8
3-3-6N=9
0-2-1
N=3
18-29-29
N=58
10-18-23
N=41
50/3"
3-9-18N=27
50/4"
40-50/4"
Stratification lines are approximate. In-situ, the transition may be gradual.
Temporary Monitoring Well Installed
DEPTH
LOCATION:See Exhibit A-2
GR
A
P
H
I
C
L
O
G
Hammer Type: Automatic
TH
I
S
B
O
R
I
N
G
L
O
G
I
S
N
O
T
V
A
L
I
D
I
F
S
E
P
A
R
A
T
E
D
F
R
O
M
O
R
I
G
I
N
A
L
R
E
P
O
R
T
.
G
E
O
S
M
A
R
T
L
O
G
-
W
E
L
L
7
0
1
4
5
8
2
8
.
G
P
J
T
E
R
R
A
C
O
N
2
0
1
2
.
G
D
T
1
2
/
1
9
/
1
4
S/W/C E Main Street & S Elizabeth Street
Durham, North Carolina
SITE:
Page 1 of 1
Advancement Method:HSA
Abandonment Method:Borings backfilled with bentonite chips upon completion.
2401 Brentwood Road, Suite 107Raleigh, North Carolina
Notes:
Project No.: 70147828
Drill Rig: D-50T
Boring Started: 12/4/2014
BORING LOG NO. B-1
City of DurhamCLIENT:
Driller: M. Eklund
Boring Completed: 12/4/2014
Exhibit:A-1
See Exhibit A-3 for description of fieldprocedures.
See Appendix B for description of laboratoryprocedures and additional data (if any).
See Appendix C for explanation of symbols and
abbreviations.
PROJECT: Proposed City of Durham Headquarters
PID
WA
T
E
R
CO
N
T
E
N
T
(
%
)
DR
Y
U
N
I
T
WE
I
G
H
T
(
p
c
f
)
LL-PL-PI
ATTERBERGLIMITS
WA
T
E
R
L
E
V
E
L
OB
S
E
R
V
A
T
I
O
N
S
INSTALLATIONDETAILS
SA
M
P
L
E
T
Y
P
E
DE
P
T
H
(
F
t
.
)
5
10
15
20
25
30
35
RE
C
O
V
E
R
Y
(
I
n
.
)
Surface Elev.: 406 (Ft.)
ELEVATION (Ft.)
FI
E
L
D
T
E
S
T
RE
S
U
L
T
S
31' While Drilling
21' After Boring Completion
9.6' BGS in Temporary Monitoring Well (12/5/14)
WATER LEVEL OBSERVATIONS
0.50.9
11.0
29.329.6
38.0
41.0
48.8
CONCRETE, 6"
AGGREGATE BASE, 5"
FAT CLAY (CH), triassic basinformation, tan to purple mottled
with olive and orange, soft tohard, residual material
SANDY SILT (ML), paleyellowish brown to olive, medium
hard to hard, residual material
SILTY SAND (SM), black,
medium dense, residual material
SANDY SILT (ML), paleyellowish brown to olive, stiff,
residual material
FAT CLAY (CH), greenish blackto greenish gray, very stiff,
residual material
PARTIALLY WEATHEREDROCK (PWR), purple to orange
with pale olive mottling, veryhard, claystone/mudstone,blocky structure
Boring Terminated at 48.8 Feet
Analytical Sample Taken at 18.5'
2.5
3.3
3.7
4.7
4.8
1.9
3.7
2.4
4.7
4.5
4.3
Open to the
ground
surface
Bentonitechips
10x20 sandfilter pack
15 feet wellscreen
16
0
18
18
18
14
16
14
16
18
4
3
417416.5
406.5
388388
379.5
376.5
368.5
1-1-1N=2
1-2-4N=6
7-19-20N=39
10-12-18
N=30
15-17-24
N=41
9-16-18
N=34
8-14-20
N=34
5-10-11N=21
3-3-5N=8
5-6-10N=16
50/5"
50/3"
Stratification lines are approximate. In-situ, the transition may be gradual.
Temporary Monitoring Well Installed
DEPTH
LOCATION:See Exhibit A-2
GR
A
P
H
I
C
L
O
G
Hammer Type: Automatic
TH
I
S
B
O
R
I
N
G
L
O
G
I
S
N
O
T
V
A
L
I
D
I
F
S
E
P
A
R
A
T
E
D
F
R
O
M
O
R
I
G
I
N
A
L
R
E
P
O
R
T
.
G
E
O
S
M
A
R
T
L
O
G
-
W
E
L
L
7
0
1
4
5
8
2
8
.
G
P
J
T
E
R
R
A
C
O
N
2
0
1
2
.
G
D
T
1
2
/
1
9
/
1
4
S/W/C E Main Street & S Elizabeth Street
Durham, North Carolina
SITE:
Page 1 of 1
Advancement Method:HSA
Abandonment Method:Borings backfilled with bentonite chips upon completion.
2401 Brentwood Road, Suite 107Raleigh, North Carolina
Notes:
Project No.: 70147828
Drill Rig: D-50T
Boring Started: 12/4/2014
BORING LOG NO. B-7
City of DurhamCLIENT:
Driller: M. Eklund
Boring Completed: 12/4/2014
Exhibit:A-7
See Exhibit A-3 for description of fieldprocedures.
See Appendix B for description of laboratoryprocedures and additional data (if any).
See Appendix C for explanation of symbols and
abbreviations.
PROJECT: Proposed City of Durham Headquarters
PID
WA
T
E
R
CO
N
T
E
N
T
(
%
)
DR
Y
U
N
I
T
WE
I
G
H
T
(
p
c
f
)
LL-PL-PI
ATTERBERGLIMITS
WA
T
E
R
L
E
V
E
L
OB
S
E
R
V
A
T
I
O
N
S
INSTALLATIONDETAILS
SA
M
P
L
E
T
Y
P
E
DE
P
T
H
(
F
t
.
)
5
10
15
20
25
30
35
40
45
RE
C
O
V
E
R
Y
(
I
n
.
)
Surface Elev.: 417.5 (Ft.)
ELEVATION (Ft.)
FI
E
L
D
T
E
S
T
RE
S
U
L
T
S
32' While Drilling
22.5' After Boring Completion
11.3' BGS in Temporary Monitoring Well (12/5/14)
WATER LEVEL OBSERVATIONS
0.20.8
10.0
17.0
22.5
40.0
ASPHALT, 2"
AGGREGATE BASE, 7"
SANDY LEAN CLAY (CL),triassic basin formation, gray
mottled with orange, mediumstiff to stiff, residual material
PARTIALLY WEATHEREDROCK (PWR),claystone/mudstone, purple to
purpleish beige, hard to veryhard, mottled coloring,considerable variation in
consistency related toweathering, blocky structure
FAT CLAY (CH), residual
material, purple to pale yellowishbrown mottled with orange, hard
PARTIALLY WEATHERED
ROCK (PWR), tan to gray, veryhard, siltstone/sandstone
Boring Terminated at 40 Feet
Analytical Sample Taken at 6'
1.2
3.3
12.8
2.0
3.7
4.2
7.4
6.5
7.3
9.1
27 43-26-17
Open to thegroundsurface
Bentonite
chips
10x20 sandfilter pack
15 feet wellscreen
10
16
15
16
14
12
10
6
12
10
417416
407
400
394.5
377
2-4-2N=6
4-4-4N=8
3-5-6N=11
1-4-8
N=12
8-40-50/5"
12-20-27
N=47
7-45-50/2"
50/6"
18-45-50/3"
41-39-46N=85
Stratification lines are approximate. In-situ, the transition may be gradual.
Temporary Monitoring Well Installed
DEPTH
LOCATION:See Exhibit A-2
GR
A
P
H
I
C
L
O
G
Hammer Type: Automatic
TH
I
S
B
O
R
I
N
G
L
O
G
I
S
N
O
T
V
A
L
I
D
I
F
S
E
P
A
R
A
T
E
D
F
R
O
M
O
R
I
G
I
N
A
L
R
E
P
O
R
T
.
G
E
O
S
M
A
R
T
L
O
G
-
W
E
L
L
7
0
1
4
5
8
2
8
.
G
P
J
T
E
R
R
A
C
O
N
2
0
1
2
.
G
D
T
1
2
/
1
9
/
1
4
S/W/C E Main Street & S Elizabeth Street
Durham, North Carolina
SITE:
Page 1 of 1
Advancement Method:HSA
Abandonment Method:Borings backfilled with bentonite chips upon completion.
2401 Brentwood Road, Suite 107Raleigh, North Carolina
Notes:
Project No.: 70147828
Drill Rig: D-50T
Boring Started: 12/4/2014
BORING LOG NO. B-8
City of DurhamCLIENT:
Driller: M. Eklund
Boring Completed: 12/4/2014
Exhibit:A-8
See Exhibit A-3 for description of fieldprocedures.
See Appendix B for description of laboratoryprocedures and additional data (if any).
See Appendix C for explanation of symbols and
abbreviations.
PROJECT: Proposed City of Durham Headquarters
PID
WA
T
E
R
CO
N
T
E
N
T
(
%
)
DR
Y
U
N
I
T
WE
I
G
H
T
(
p
c
f
)
LL-PL-PI
ATTERBERGLIMITS
WA
T
E
R
L
E
V
E
L
OB
S
E
R
V
A
T
I
O
N
S
INSTALLATIONDETAILS
SA
M
P
L
E
T
Y
P
E
DE
P
T
H
(
F
t
.
)
5
10
15
20
25
30
35
40
RE
C
O
V
E
R
Y
(
I
n
.
)
Surface Elev.: 417 (Ft.)
ELEVATION (Ft.)
FI
E
L
D
T
E
S
T
RE
S
U
L
T
S
30.6' While Drilling
20.7' After Boring Completion
10.5' BGS in Temporary Monitoring Well (12/5/14)
WATER LEVEL OBSERVATIONS
0.50.8
6.0
22.5
38.9
CONCRETE, 6"
AGGREGATE BASE, 3"
FAT CLAY (CH), triassic basinformation, with sand, dark brown
to brown, very soft, residualmaterial
SILTY CLAY (CL-ML), gray to
pale gray mottled with orange,medium stiff to very stiff,residual material
PARTIALLY WEATHEREDROCK (PWR),
claystone/mudstone, purple todark purpleish gray, hard to veryhard, mottled coloring,
considerable variation inconsistency related toweathering, blocky structure
Boring Terminated at 38.9 Feet
Analytical Sample Taken at 6'
0.6
4.2
9.4
3.2
8.4
6.1
5.1
4.6
1.4
2.1
Open to the
ground
surface
Bentonitechips
10x20 sandfilter pack
15 feet wellscreen
2
4
18
18
18
18
15
8
5
5
408407.5
402.5
386
369.5
0-0-0N=0
0-0-0N=0
2-3-4N=7
3-5-8
N=13
4-9-16
N=25
8-16-24
N=40
8-30-50/3"
40-50/5"
50/6"
50/5"
Stratification lines are approximate. In-situ, the transition may be gradual.
Temporary Monitoring Well Installed
DEPTH
LOCATION:See Exhibit A-2
GR
A
P
H
I
C
L
O
G
Hammer Type: Automatic
TH
I
S
B
O
R
I
N
G
L
O
G
I
S
N
O
T
V
A
L
I
D
I
F
S
E
P
A
R
A
T
E
D
F
R
O
M
O
R
I
G
I
N
A
L
R
E
P
O
R
T
.
G
E
O
S
M
A
R
T
L
O
G
-
W
E
L
L
7
0
1
4
5
8
2
8
.
G
P
J
T
E
R
R
A
C
O
N
2
0
1
2
.
G
D
T
1
2
/
1
9
/
1
4
S/W/C E Main Street & S Elizabeth Street
Durham, North Carolina
SITE:
Page 1 of 1
Advancement Method:HSA
Abandonment Method:Borings backfilled with bentonite chips upon completion.
2401 Brentwood Road, Suite 107Raleigh, North Carolina
Notes:
Project No.: 70147828
Drill Rig: D-50T
Boring Started: 12/3/2014
BORING LOG NO. B-9
City of DurhamCLIENT:
Driller: M. Eklund
Boring Completed: 12/3/2014
Exhibit:A-9
See Exhibit A-3 for description of fieldprocedures.
See Appendix B for description of laboratoryprocedures and additional data (if any).
See Appendix C for explanation of symbols and
abbreviations.
PROJECT: Proposed City of Durham Headquarters
PID
WA
T
E
R
CO
N
T
E
N
T
(
%
)
DR
Y
U
N
I
T
WE
I
G
H
T
(
p
c
f
)
LL-PL-PI
ATTERBERGLIMITS
WA
T
E
R
L
E
V
E
L
OB
S
E
R
V
A
T
I
O
N
S
INSTALLATIONDETAILS
SA
M
P
L
E
T
Y
P
E
DE
P
T
H
(
F
t
.
)
5
10
15
20
25
30
35
RE
C
O
V
E
R
Y
(
I
n
.
)
Surface Elev.: 408.5 (Ft.)
ELEVATION (Ft.)
FI
E
L
D
T
E
S
T
RE
S
U
L
T
S
9.4' BGS in Temporary Monitoring Well (12/5/14)
WATER LEVEL OBSERVATIONS
APPENDIX D
Laboratory Analytical Report and Chain of Custody Records
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Terracon Consultants, Inc.
2401 Brentwood Road
Suite 107 I
Raleigh, NC 27604
Attention: Michael Jordan
PL06010Lot Number:
70147828Project Number:
Durham Police HeadquartersProject Name:
12/15/2014Date Completed:
Nisreen Saikaly
Project Manager
*PL06010*
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Terracon Consultants, Inc.
Lot Number: PL06010
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, Inc.
Lot Number: PL06010
Sample Number Sample ID Matrix Date Sampled Date Received
001 12/03/2014 1610B-9(6.0-7.5)Solid 12/06/2014
002 12/04/2014 0930B-8(6.0-7.5)Solid 12/06/2014
003 12/04/2014 1215B-7(18.5-20.0)Solid 12/06/2014
004 12/04/2014 1534B-1(33.5-33.9)Solid 12/06/2014
005 12/05/2014 0905B-9 Aqueous 12/06/2014
006 12/05/2014 0945B-1 Aqueous 12/06/2014
007 12/05/2014 1230B-8 Aqueous 12/06/2014
008 12/05/2014 1315B-7 Aqueous 12/06/2014
009 12/05/2014 1330TRIP BLANK Aqueous 12/06/2014
(9 samples)
Page: 3 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Terracon Consultants, Inc.
Lot Number: PL06010
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 B-9(6.0-7.5)Solid Acetone 8260B 48 ug/kg 5
005 B-9 Aqueous Acetone 8260B 3.5 J ug/L 21
005 B-9 Aqueous Ethylbenzene 8260B 0.76 ug/L 21
006 B-1 Aqueous Benzene 8260B 1.1 ug/L 25
006 B-1 Aqueous Chloroform 8260B 0.99 ug/L 25
006 B-1 Aqueous Methyl tertiary butyl ether (MTBE)8260B 0.58 ug/L 25
007 B-8 Aqueous Benzene 8260B 0.63 ug/L 29
008 B-7 Aqueous Benzene 8260B 31 ug/L 33
008 B-7 Aqueous Chloroform 8260B 0.60 ug/L 33
008 B-7 Aqueous Ethylbenzene 8260B 1.3 ug/L 33
008 B-7 Aqueous Isopropylbenzene 8260B 1.6 ug/L 33
008 B-7 Aqueous Methyl tertiary butyl ether (MTBE)8260B 9.5 ug/L 33
008 B-7 Aqueous Styrene 8260B 0.61 ug/L 33
008 B-7 Aqueous Toluene 8260B 0.40 J ug/L 33
008 B-7 Aqueous Xylenes (total)8260B 54 ug/L 34
008 B-7 Aqueous Naphthalene 8270D 6.0 ug/L 36
(16 detections)
Page: 4 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-9(6.0-7.5)
PL06010-001
12/03/2014 1610
12/06/2014
Solid
% Solids:80.8 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 12/09/2014 1147 DCS 62647 6.92
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 48 1ug/kg6.018
Benzene 71-43-2 8260B ND 1ug/kg0.984.5
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.54.5
Bromoform 75-25-2 8260B ND 1ug/kg0.634.5
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg1.64.5
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.18.9
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.24.5
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.64.5
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.54.5
Chloroethane 75-00-3 8260B ND 1ug/kg1.24.5
Chloroform 67-66-3 8260B ND 1ug/kg0.744.5
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg0.894.5
Cyclohexane 110-82-7 8260B ND 1ug/kg0.604.5
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.34.5
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.54.5
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.764.5
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.54.5
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.54.5
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.54.5
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.44.5
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.654.5
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg0.894.5
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.54.5
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.684.5
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.34.5
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.814.5
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.614.5
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.734.5
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.54.5
2-Hexanone 591-78-6 8260B ND 1ug/kg1.28.9
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.214.5
Methyl acetate 79-20-9 8260B ND 1ug/kg0.884.5
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.364.5
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.38.9
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.374.5
Methylene chloride 75-09-2 8260B ND 1ug/kg2.34.5
Styrene 100-42-5 8260B ND 1ug/kg0.984.5
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.424.5
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.454.5
Toluene 108-88-3 8260B ND 1ug/kg1.54.5
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.564.5
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.54.5
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.764.5
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.714.5
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-9(6.0-7.5)
PL06010-001
12/03/2014 1610
12/06/2014
Solid
% Solids:80.8 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 12/09/2014 1147 DCS 62647 6.92
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg1.74.5
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.34.5
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.774.5
Xylenes (total)1330-20-7 8260B ND 1ug/kg2.64.5
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 53-142
Bromofluorobenzene 94 47-138
Toluene-d8 102 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-9(6.0-7.5)
PL06010-001
12/03/2014 1610
12/06/2014
Solid
% Solids:80.8 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 12/10/2014 1926 RBH 12/08/2014 1620 62573
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/kg13410
Acenaphthylene 208-96-8 8270D ND 1ug/kg16410
Acetophenone 98-86-2 8270D ND 1ug/kg24410
Anthracene 120-12-7 8270D ND 1ug/kg18410
Atrazine 1912-24-9 8270D ND 1ug/kg120410
Benzaldehyde 100-52-7 8270D ND 1ug/kg331000
Benzo(a)anthracene 56-55-3 8270D ND 1ug/kg13410
Benzo(a)pyrene 50-32-8 8270D ND 1ug/kg30410
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/kg28410
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/kg28410
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg34410
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg38410
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg17410
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg140410
Caprolactam 105-60-2 8270D ND 1ug/kg301000
Carbazole 86-74-8 8270D ND 1ug/kg12410
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg23410
4-Chloroaniline 106-47-8 8270D ND 1ug/kg21410
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg18410
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg17410
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 1ug/kg16410
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg20410
2-Chlorophenol 95-57-8 8270D ND 1ug/kg17410
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg16410
Chrysene 218-01-9 8270D ND 1ug/kg13410
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg140410
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg140410
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg27410
Dibenzofuran 132-64-9 8270D ND 1ug/kg16410
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg701000
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg17410
Diethylphthalate 84-66-2 8270D ND 1ug/kg140410
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg140410
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg21410
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg471000
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg8.21000
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg30410
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg36410
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg140410
Fluoranthene 206-44-0 8270D ND 1ug/kg13410
Fluorene 86-73-7 8270D ND 1ug/kg16410
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg16410
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg17410
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg791000
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-9(6.0-7.5)
PL06010-001
12/03/2014 1610
12/06/2014
Solid
% Solids:80.8 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 12/10/2014 1926 RBH 12/08/2014 1620 62573
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Hexachloroethane 67-72-1 8270D ND 1ug/kg20410
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/kg37410
Isophorone 78-59-1 8270D ND 1ug/kg19410
2-Methylnaphthalene 91-57-6 8270D ND 1ug/kg15410
2-Methylphenol 95-48-7 8270D ND 1ug/kg23410
3 & 4-Methylphenol 106-44-5 8270D ND 1ug/kg39830
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg21410
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg14410
Naphthalene 91-20-3 8270D ND 1ug/kg17410
2-Nitroaniline 88-74-4 8270D ND 1ug/kg29410
3-Nitroaniline 99-09-2 8270D ND 1ug/kg29410
4-Nitroaniline 100-01-6 8270D ND 1ug/kg24410
Nitrobenzene 98-95-3 8270D ND 1ug/kg19410
2-Nitrophenol 88-75-5 8270D ND 1ug/kg44410
4-Nitrophenol 100-02-7 8270D ND 1ug/kg1801000
Pentachlorophenol 87-86-5 8270D ND 1ug/kg431000
Phenanthrene 85-01-8 8270D ND 1ug/kg17410
Phenol 108-95-2 8270D ND 1ug/kg20410
Pyrene 129-00-0 8270D ND 1ug/kg18410
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg21410
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg23410
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,4,6-Tribromophenol 78 30-117
2-Fluorobiphenyl 67 33-102
2-Fluorophenol 70 28-104
Nitrobenzene-d5 71 22-109
Phenol-d5 76 27-103
Terphenyl-d14 94 41-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-8(6.0-7.5)
PL06010-002
12/04/2014 0930
12/06/2014
Solid
% Solids:78.6 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 12/09/2014 1208 DCS 62647 5.62
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg7.623
Benzene 71-43-2 8260B ND 1ug/kg1.25.7
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.95.7
Bromoform 75-25-2 8260B ND 1ug/kg0.795.7
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.05.7
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.711
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.55.7
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.05.7
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.95.7
Chloroethane 75-00-3 8260B ND 1ug/kg1.55.7
Chloroform 67-66-3 8260B ND 1ug/kg0.945.7
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.15.7
Cyclohexane 110-82-7 8260B ND 1ug/kg0.765.7
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.75.7
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.95.7
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.965.7
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.95.7
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.95.7
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.95.7
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.85.7
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.835.7
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.15.7
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.95.7
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.865.7
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.75.7
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.05.7
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.775.7
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.935.7
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.95.7
2-Hexanone 591-78-6 8260B ND 1ug/kg1.511
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.265.7
Methyl acetate 79-20-9 8260B ND 1ug/kg1.15.7
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.455.7
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.711
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.465.7
Methylene chloride 75-09-2 8260B ND 1ug/kg2.95.7
Styrene 100-42-5 8260B ND 1ug/kg1.25.7
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.535.7
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.575.7
Toluene 108-88-3 8260B ND 1ug/kg1.95.7
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.715.7
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.95.7
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.965.7
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.895.7
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-8(6.0-7.5)
PL06010-002
12/04/2014 0930
12/06/2014
Solid
% Solids:78.6 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 12/09/2014 1208 DCS 62647 5.62
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.25.7
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.75.7
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.975.7
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.35.7
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 53-142
Bromofluorobenzene 93 47-138
Toluene-d8 100 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-8(6.0-7.5)
PL06010-002
12/04/2014 0930
12/06/2014
Solid
% Solids:78.6 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 12/10/2014 1949 RBH 12/08/2014 1620 62573
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/kg13420
Acenaphthylene 208-96-8 8270D ND 1ug/kg17420
Acetophenone 98-86-2 8270D ND 1ug/kg25420
Anthracene 120-12-7 8270D ND 1ug/kg19420
Atrazine 1912-24-9 8270D ND 1ug/kg130420
Benzaldehyde 100-52-7 8270D ND 1ug/kg341100
Benzo(a)anthracene 56-55-3 8270D ND 1ug/kg14420
Benzo(a)pyrene 50-32-8 8270D ND 1ug/kg31420
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/kg28420
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/kg29420
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg35420
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg39420
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg18420
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg140420
Caprolactam 105-60-2 8270D ND 1ug/kg311100
Carbazole 86-74-8 8270D ND 1ug/kg12420
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg23420
4-Chloroaniline 106-47-8 8270D ND 1ug/kg22420
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg19420
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg18420
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 1ug/kg16420
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg20420
2-Chlorophenol 95-57-8 8270D ND 1ug/kg18420
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg17420
Chrysene 218-01-9 8270D ND 1ug/kg13420
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg140420
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg140420
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg28420
Dibenzofuran 132-64-9 8270D ND 1ug/kg17420
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg721100
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg17420
Diethylphthalate 84-66-2 8270D ND 1ug/kg140420
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg140420
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg22420
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg491100
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg8.41100
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg31420
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg37420
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg140420
Fluoranthene 206-44-0 8270D ND 1ug/kg13420
Fluorene 86-73-7 8270D ND 1ug/kg16420
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg17420
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg17420
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg821100
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-8(6.0-7.5)
PL06010-002
12/04/2014 0930
12/06/2014
Solid
% Solids:78.6 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 12/10/2014 1949 RBH 12/08/2014 1620 62573
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Hexachloroethane 67-72-1 8270D ND 1ug/kg21420
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/kg38420
Isophorone 78-59-1 8270D ND 1ug/kg20420
2-Methylnaphthalene 91-57-6 8270D ND 1ug/kg15420
2-Methylphenol 95-48-7 8270D ND 1ug/kg24420
3 & 4-Methylphenol 106-44-5 8270D ND 1ug/kg40850
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg22420
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg14420
Naphthalene 91-20-3 8270D ND 1ug/kg18420
2-Nitroaniline 88-74-4 8270D ND 1ug/kg30420
3-Nitroaniline 99-09-2 8270D ND 1ug/kg30420
4-Nitroaniline 100-01-6 8270D ND 1ug/kg25420
Nitrobenzene 98-95-3 8270D ND 1ug/kg19420
2-Nitrophenol 88-75-5 8270D ND 1ug/kg45420
4-Nitrophenol 100-02-7 8270D ND 1ug/kg1801100
Pentachlorophenol 87-86-5 8270D ND 1ug/kg451100
Phenanthrene 85-01-8 8270D ND 1ug/kg17420
Phenol 108-95-2 8270D ND 1ug/kg20420
Pyrene 129-00-0 8270D ND 1ug/kg18420
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg22420
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg23420
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,4,6-Tribromophenol 87 30-117
2-Fluorobiphenyl 77 33-102
2-Fluorophenol 79 28-104
Nitrobenzene-d5 81 22-109
Phenol-d5 87 27-103
Terphenyl-d14 94 41-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-7(18.5-20.0)
PL06010-003
12/04/2014 1215
12/06/2014
Solid
% Solids:86.0 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 12/09/2014 1229 DCS 62647 6.74
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg5.817
Benzene 71-43-2 8260B ND 1ug/kg0.954.3
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.54.3
Bromoform 75-25-2 8260B ND 1ug/kg0.604.3
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg1.64.3
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.18.6
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.14.3
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.64.3
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.54.3
Chloroethane 75-00-3 8260B ND 1ug/kg1.14.3
Chloroform 67-66-3 8260B ND 1ug/kg0.724.3
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg0.864.3
Cyclohexane 110-82-7 8260B ND 1ug/kg0.584.3
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.34.3
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.54.3
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.734.3
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.54.3
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.54.3
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.54.3
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.44.3
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.634.3
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg0.864.3
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.54.3
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.664.3
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.34.3
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.784.3
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.594.3
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.714.3
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.54.3
2-Hexanone 591-78-6 8260B ND 1ug/kg1.18.6
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.204.3
Methyl acetate 79-20-9 8260B ND 1ug/kg0.854.3
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.344.3
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.38.6
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.354.3
Methylene chloride 75-09-2 8260B ND 1ug/kg2.24.3
Styrene 100-42-5 8260B ND 1ug/kg0.954.3
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.414.3
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.434.3
Toluene 108-88-3 8260B ND 1ug/kg1.54.3
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.544.3
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.54.3
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.734.3
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.684.3
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-7(18.5-20.0)
PL06010-003
12/04/2014 1215
12/06/2014
Solid
% Solids:86.0 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 12/09/2014 1229 DCS 62647 6.74
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg1.64.3
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.34.3
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.744.3
Xylenes (total)1330-20-7 8260B ND 1ug/kg2.54.3
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 100 53-142
Bromofluorobenzene 93 47-138
Toluene-d8 99 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-7(18.5-20.0)
PL06010-003
12/04/2014 1215
12/06/2014
Solid
% Solids:86.0 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 12/10/2014 2012 RBH 12/08/2014 1620 62573
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/kg12380
Acenaphthylene 208-96-8 8270D ND 1ug/kg15380
Acetophenone 98-86-2 8270D ND 1ug/kg23380
Anthracene 120-12-7 8270D ND 1ug/kg17380
Atrazine 1912-24-9 8270D ND 1ug/kg120380
Benzaldehyde 100-52-7 8270D ND 1ug/kg31960
Benzo(a)anthracene 56-55-3 8270D ND 1ug/kg13380
Benzo(a)pyrene 50-32-8 8270D ND 1ug/kg28380
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/kg26380
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/kg26380
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg32380
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg35380
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg16380
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg130380
Caprolactam 105-60-2 8270D ND 1ug/kg28960
Carbazole 86-74-8 8270D ND 1ug/kg11380
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg21380
4-Chloroaniline 106-47-8 8270D ND 1ug/kg20380
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg17380
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg16380
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 1ug/kg15380
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg18380
2-Chlorophenol 95-57-8 8270D ND 1ug/kg16380
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg15380
Chrysene 218-01-9 8270D ND 1ug/kg12380
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg130380
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg130380
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg25380
Dibenzofuran 132-64-9 8270D ND 1ug/kg15380
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg66960
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg16380
Diethylphthalate 84-66-2 8270D ND 1ug/kg130380
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg130380
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg20380
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg45960
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg7.7960
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg28380
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg33380
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg130380
Fluoranthene 206-44-0 8270D ND 1ug/kg12380
Fluorene 86-73-7 8270D ND 1ug/kg15380
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg15380
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg16380
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg75960
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-7(18.5-20.0)
PL06010-003
12/04/2014 1215
12/06/2014
Solid
% Solids:86.0 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 12/10/2014 2012 RBH 12/08/2014 1620 62573
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Hexachloroethane 67-72-1 8270D ND 1ug/kg19380
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/kg35380
Isophorone 78-59-1 8270D ND 1ug/kg18380
2-Methylnaphthalene 91-57-6 8270D ND 1ug/kg14380
2-Methylphenol 95-48-7 8270D ND 1ug/kg22380
3 & 4-Methylphenol 106-44-5 8270D ND 1ug/kg36780
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg20380
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg13380
Naphthalene 91-20-3 8270D ND 1ug/kg16380
2-Nitroaniline 88-74-4 8270D ND 1ug/kg27380
3-Nitroaniline 99-09-2 8270D ND 1ug/kg28380
4-Nitroaniline 100-01-6 8270D ND 1ug/kg23380
Nitrobenzene 98-95-3 8270D ND 1ug/kg18380
2-Nitrophenol 88-75-5 8270D ND 1ug/kg41380
4-Nitrophenol 100-02-7 8270D ND 1ug/kg170960
Pentachlorophenol 87-86-5 8270D ND 1ug/kg41960
Phenanthrene 85-01-8 8270D ND 1ug/kg16380
Phenol 108-95-2 8270D ND 1ug/kg18380
Pyrene 129-00-0 8270D ND 1ug/kg17380
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg20380
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg21380
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,4,6-Tribromophenol 80 30-117
2-Fluorobiphenyl 76 33-102
2-Fluorophenol 78 28-104
Nitrobenzene-d5 80 22-109
Phenol-d5 86 27-103
Terphenyl-d14 93 41-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-1(33.5-33.9)
PL06010-004
12/04/2014 1534
12/06/2014
Solid
% Solids:76.1 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 12/09/2014 1250 DCS 62647 5.81
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg7.623
Benzene 71-43-2 8260B ND 1ug/kg1.25.7
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.95.7
Bromoform 75-25-2 8260B ND 1ug/kg0.795.7
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.05.7
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.711
Carbon disulfide 75-15-0 8260B ND 1ug/kg1.55.7
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.05.7
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.95.7
Chloroethane 75-00-3 8260B ND 1ug/kg1.55.7
Chloroform 67-66-3 8260B ND 1ug/kg0.945.7
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg1.15.7
Cyclohexane 110-82-7 8260B ND 1ug/kg0.765.7
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg1.75.7
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.95.7
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.965.7
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.95.7
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.95.7
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.95.7
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.85.7
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.835.7
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg1.15.7
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.95.7
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.865.7
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.75.7
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg1.05.7
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.775.7
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.935.7
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.95.7
2-Hexanone 591-78-6 8260B ND 1ug/kg1.511
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.265.7
Methyl acetate 79-20-9 8260B ND 1ug/kg1.15.7
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg0.455.7
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.711
Methylcyclohexane 108-87-2 8260B ND 1ug/kg0.465.7
Methylene chloride 75-09-2 8260B ND 1ug/kg2.95.7
Styrene 100-42-5 8260B ND 1ug/kg1.25.7
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.535.7
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.575.7
Toluene 108-88-3 8260B ND 1ug/kg1.95.7
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg0.715.7
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.95.7
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.965.7
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.895.7
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-1(33.5-33.9)
PL06010-004
12/04/2014 1534
12/06/2014
Solid
% Solids:76.1 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 12/09/2014 1250 DCS 62647 5.81
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.7
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.75.7
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.975.7
Xylenes (total)1330-20-7 8260B ND 1ug/kg3.35.7
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 53-142
Bromofluorobenzene 92 47-138
Toluene-d8 99 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-1(33.5-33.9)
PL06010-004
12/04/2014 1534
12/06/2014
Solid
% Solids:76.1 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 12/10/2014 2036 RBH 12/08/2014 1620 62573
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/kg13430
Acenaphthylene 208-96-8 8270D ND 1ug/kg17430
Acetophenone 98-86-2 8270D ND 1ug/kg26430
Anthracene 120-12-7 8270D ND 1ug/kg19430
Atrazine 1912-24-9 8270D ND 1ug/kg130430
Benzaldehyde 100-52-7 8270D ND 1ug/kg341100
Benzo(a)anthracene 56-55-3 8270D ND 1ug/kg14430
Benzo(a)pyrene 50-32-8 8270D ND 1ug/kg31430
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/kg29430
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/kg29430
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg35430
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg40430
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg18430
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg140430
Caprolactam 105-60-2 8270D ND 1ug/kg321100
Carbazole 86-74-8 8270D ND 1ug/kg13430
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg24430
4-Chloroaniline 106-47-8 8270D ND 1ug/kg22430
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg19430
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg18430
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 1ug/kg16430
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg21430
2-Chlorophenol 95-57-8 8270D ND 1ug/kg18430
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg17430
Chrysene 218-01-9 8270D ND 1ug/kg13430
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg140430
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg140430
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg29430
Dibenzofuran 132-64-9 8270D ND 1ug/kg17430
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg741100
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg17430
Diethylphthalate 84-66-2 8270D ND 1ug/kg140430
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg140430
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg22430
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg501100
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg8.61100
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg32430
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg37430
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg140430
Fluoranthene 206-44-0 8270D ND 1ug/kg14430
Fluorene 86-73-7 8270D ND 1ug/kg17430
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg17430
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg18430
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg841100
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-1(33.5-33.9)
PL06010-004
12/04/2014 1534
12/06/2014
Solid
% Solids:76.1 12/06/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8270D 1 12/10/2014 2036 RBH 12/08/2014 1620 62573
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Hexachloroethane 67-72-1 8270D ND 1ug/kg21430
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/kg39430
Isophorone 78-59-1 8270D ND 1ug/kg20430
2-Methylnaphthalene 91-57-6 8270D ND 1ug/kg16430
2-Methylphenol 95-48-7 8270D ND 1ug/kg24430
3 & 4-Methylphenol 106-44-5 8270D ND 1ug/kg41870
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg22430
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg14430
Naphthalene 91-20-3 8270D ND 1ug/kg18430
2-Nitroaniline 88-74-4 8270D ND 1ug/kg30430
3-Nitroaniline 99-09-2 8270D ND 1ug/kg31430
4-Nitroaniline 100-01-6 8270D ND 1ug/kg26430
Nitrobenzene 98-95-3 8270D ND 1ug/kg20430
2-Nitrophenol 88-75-5 8270D ND 1ug/kg46430
4-Nitrophenol 100-02-7 8270D ND 1ug/kg1901100
Pentachlorophenol 87-86-5 8270D ND 1ug/kg461100
Phenanthrene 85-01-8 8270D ND 1ug/kg17430
Phenol 108-95-2 8270D ND 1ug/kg21430
Pyrene 129-00-0 8270D ND 1ug/kg19430
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg22430
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg24430
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,4,6-Tribromophenol 80 30-117
2-Fluorobiphenyl 69 33-102
2-Fluorophenol 74 28-104
Nitrobenzene-d5 75 22-109
Phenol-d5 80 27-103
Terphenyl-d14 96 41-120
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 20 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-9
PL06010-005
12/05/2014 0905
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 12/13/2014 1637 ALL 63005
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 3.5 J 1ug/L3.310
Benzene 71-43-2 8260B ND 1ug/L0.0270.50
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.170.50
Bromoform 75-25-2 8260B ND 1ug/L0.0100.50
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.200.50
2-Butanone (MEK)78-93-3 8260B ND 1ug/L2.010
Carbon disulfide 75-15-0 8260B ND 1ug/L0.0970.50
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.0850.50
Chlorobenzene 108-90-7 8260B ND 1ug/L0.170.50
Chloroethane 75-00-3 8260B ND 1ug/L0.170.50
Chloroform 67-66-3 8260B ND 1ug/L0.170.50
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.170.50
Cyclohexane 110-82-7 8260B ND 1ug/L0.300.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.0690.50
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.170.50
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.0610.50
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.170.50
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.170.50
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.170.50
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.0710.50
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.0540.50
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.0230.50
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.0790.50
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.0940.50
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.0870.50
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.0810.50
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.180.50
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.0900.50
Ethylbenzene 100-41-4 8260B 0.76 1ug/L0.170.50
2-Hexanone 591-78-6 8260B ND 1ug/L0.2710
Isopropylbenzene 98-82-8 8260B ND 1ug/L0.0290.50
Methyl acetate 79-20-9 8260B ND 1ug/L0.301.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.0190.50
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L0.3110
Methylcyclohexane 108-87-2 8260B ND 1ug/L0.955.0
Methylene chloride 75-09-2 8260B ND 1ug/L0.170.50
Styrene 100-42-5 8260B ND 1ug/L0.0150.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.0130.50
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.0140.50
Toluene 108-88-3 8260B ND 1ug/L0.170.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L0.300.50
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.170.50
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.0290.50
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.0310.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 21 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-9
PL06010-005
12/05/2014 0905
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 12/13/2014 1637 ALL 63005
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/L0.0240.50
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.0510.50
Vinyl chloride 75-01-4 8260B ND 1ug/L0.0650.50
Xylenes (total)1330-20-7 8260B ND 1ug/L0.170.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 100 70-130
Bromofluorobenzene 113 70-130
Toluene-d8 110 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 22 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-9
PL06010-005
12/05/2014 0905
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 12/11/2014 1458 RBH 12/08/2014 1820 62580
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/L1.25.0
Acenaphthylene 208-96-8 8270D ND 1ug/L1.25.0
Acetophenone 98-86-2 8270D ND 1ug/L0.905.0
Anthracene 120-12-7 8270D ND 1ug/L1.15.0
Atrazine 1912-24-9 8270D ND 1ug/L4.25.0
Benzaldehyde 100-52-7 8270D ND 1ug/L3.025
Benzo(a)anthracene 56-55-3 8270D ND 1ug/L0.605.0
Benzo(a)pyrene 50-32-8 8270D ND 1ug/L0.505.0
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/L0.605.0
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/L0.805.0
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/L1.05.0
1,1'-Biphenyl 92-52-4 8270D ND 1ug/L1.35.0
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/L1.25.0
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/L3.310
Caprolactam 105-60-2 8270D ND 1ug/L1.225
Carbazole 86-74-8 8270D ND 1ug/L1.75.0
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/L1.65.0
4-Chloroaniline 106-47-8 8270D ND 1ug/L0.815.0
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/L1.55.0
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/L1.25.0
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 1ug/L1.35.0
2-Chloronaphthalene 91-58-7 8270D ND 1ug/L1.35.0
2-Chlorophenol 95-57-8 8270D ND 1ug/L1.45.0
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/L1.65.0
Chrysene 218-01-9 8270D ND 1ug/L0.705.0
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/L1.75.0
Di-n-octylphthalate 117-84-0 8270D ND 1ug/L1.75.0
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/L1.35.0
Dibenzofuran 132-64-9 8270D ND 1ug/L1.25.0
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/L2.625
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/L1.25.0
Diethylphthalate 84-66-2 8270D ND 1ug/L1.95.0
Dimethyl phthalate 131-11-3 8270D ND 1ug/L1.75.0
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/L1.45.0
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/L8.125
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/L4.825
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/L3.810
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/L3.410
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/L1.75.0
Fluoranthene 206-44-0 8270D ND 1ug/L1.45.0
Fluorene 86-73-7 8270D ND 1ug/L1.45.0
Hexachlorobenzene 118-74-1 8270D ND 1ug/L1.25.0
Hexachlorobutadiene 87-68-3 8270D ND 1ug/L1.45.0
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/L4.025
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 23 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-9
PL06010-005
12/05/2014 0905
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 12/11/2014 1458 RBH 12/08/2014 1820 62580
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Hexachloroethane 67-72-1 8270D ND 1ug/L1.25.0
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/L2.35.0
Isophorone 78-59-1 8270D ND 1ug/L1.45.0
2-Methylnaphthalene 91-57-6 8270D ND 1ug/L1.55.0
2-Methylphenol 95-48-7 8270D ND 1ug/L1.15.0
3 & 4-Methylphenol 106-44-5 8270D ND 1ug/L2.710
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/L1.45.0
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/L1.05.0
Naphthalene 91-20-3 8270D ND 1ug/L1.35.0
2-Nitroaniline 88-74-4 8270D ND 1ug/L2.110
3-Nitroaniline 99-09-2 8270D ND 1ug/L3.010
4-Nitroaniline 100-01-6 8270D ND 1ug/L4.210
Nitrobenzene 98-95-3 8270D ND 1ug/L1.65.0
2-Nitrophenol 88-75-5 8270D ND 1ug/L2.910
4-Nitrophenol 100-02-7 8270D ND 1ug/L9.025
Pentachlorophenol 87-86-5 8270D ND 1ug/L5.125
Phenanthrene 85-01-8 8270D ND 1ug/L1.25.0
Phenol 108-95-2 8270D ND 1ug/L1.25.0
Pyrene 129-00-0 8270D ND 1ug/L3.15.0
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/L1.25.0
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/L1.35.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,4,6-Tribromophenol 90 41-144
2-Fluorobiphenyl 89 37-129
2-Fluorophenol 88 24-127
Nitrobenzene-d5 97 38-127
Phenol-d5 94 28-128
Terphenyl-d14 97 10-148
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 24 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-1
PL06010-006
12/05/2014 0945
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 12/13/2014 1659 ALL 63005
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/L3.310
Benzene 71-43-2 8260B 1.1 1ug/L0.0270.50
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.170.50
Bromoform 75-25-2 8260B ND 1ug/L0.0100.50
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.200.50
2-Butanone (MEK)78-93-3 8260B ND 1ug/L2.010
Carbon disulfide 75-15-0 8260B ND 1ug/L0.0970.50
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.0850.50
Chlorobenzene 108-90-7 8260B ND 1ug/L0.170.50
Chloroethane 75-00-3 8260B ND 1ug/L0.170.50
Chloroform 67-66-3 8260B 0.99 1ug/L0.170.50
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.170.50
Cyclohexane 110-82-7 8260B ND 1ug/L0.300.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.0690.50
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.170.50
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.0610.50
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.170.50
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.170.50
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.170.50
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.0710.50
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.0540.50
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.0230.50
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.0790.50
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.0940.50
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.0870.50
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.0810.50
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.180.50
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.0900.50
Ethylbenzene 100-41-4 8260B ND 1ug/L0.170.50
2-Hexanone 591-78-6 8260B ND 1ug/L0.2710
Isopropylbenzene 98-82-8 8260B ND 1ug/L0.0290.50
Methyl acetate 79-20-9 8260B ND 1ug/L0.301.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 0.58 1ug/L0.0190.50
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L0.3110
Methylcyclohexane 108-87-2 8260B ND 1ug/L0.955.0
Methylene chloride 75-09-2 8260B ND 1ug/L0.170.50
Styrene 100-42-5 8260B ND 1ug/L0.0150.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.0130.50
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.0140.50
Toluene 108-88-3 8260B ND 1ug/L0.170.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L0.300.50
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.170.50
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.0290.50
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.0310.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 25 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-1
PL06010-006
12/05/2014 0945
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 12/13/2014 1659 ALL 63005
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/L0.0240.50
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.0510.50
Vinyl chloride 75-01-4 8260B ND 1ug/L0.0650.50
Xylenes (total)1330-20-7 8260B ND 1ug/L0.170.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 70-130
Bromofluorobenzene 110 70-130
Toluene-d8 110 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 26 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-1
PL06010-006
12/05/2014 0945
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 12/11/2014 1545 RBH 12/08/2014 1820 62580
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/L1.25.0
Acenaphthylene 208-96-8 8270D ND 1ug/L1.25.0
Acetophenone 98-86-2 8270D ND 1ug/L0.905.0
Anthracene 120-12-7 8270D ND 1ug/L1.15.0
Atrazine 1912-24-9 8270D ND 1ug/L4.25.0
Benzaldehyde 100-52-7 8270D ND 1ug/L3.025
Benzo(a)anthracene 56-55-3 8270D ND 1ug/L0.605.0
Benzo(a)pyrene 50-32-8 8270D ND 1ug/L0.505.0
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/L0.605.0
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/L0.805.0
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/L1.05.0
1,1'-Biphenyl 92-52-4 8270D ND 1ug/L1.35.0
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/L1.25.0
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/L3.310
Caprolactam 105-60-2 8270D ND 1ug/L1.225
Carbazole 86-74-8 8270D ND 1ug/L1.75.0
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/L1.65.0
4-Chloroaniline 106-47-8 8270D ND 1ug/L0.815.0
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/L1.55.0
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/L1.25.0
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 1ug/L1.35.0
2-Chloronaphthalene 91-58-7 8270D ND 1ug/L1.35.0
2-Chlorophenol 95-57-8 8270D ND 1ug/L1.45.0
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/L1.65.0
Chrysene 218-01-9 8270D ND 1ug/L0.705.0
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/L1.75.0
Di-n-octylphthalate 117-84-0 8270D ND 1ug/L1.75.0
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/L1.35.0
Dibenzofuran 132-64-9 8270D ND 1ug/L1.25.0
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/L2.625
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/L1.25.0
Diethylphthalate 84-66-2 8270D ND 1ug/L1.95.0
Dimethyl phthalate 131-11-3 8270D ND 1ug/L1.75.0
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/L1.45.0
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/L8.125
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/L4.825
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/L3.810
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/L3.410
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/L1.75.0
Fluoranthene 206-44-0 8270D ND 1ug/L1.45.0
Fluorene 86-73-7 8270D ND 1ug/L1.45.0
Hexachlorobenzene 118-74-1 8270D ND 1ug/L1.25.0
Hexachlorobutadiene 87-68-3 8270D ND 1ug/L1.45.0
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/L4.025
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 27 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-1
PL06010-006
12/05/2014 0945
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 12/11/2014 1545 RBH 12/08/2014 1820 62580
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Hexachloroethane 67-72-1 8270D ND 1ug/L1.25.0
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/L2.35.0
Isophorone 78-59-1 8270D ND 1ug/L1.45.0
2-Methylnaphthalene 91-57-6 8270D ND 1ug/L1.55.0
2-Methylphenol 95-48-7 8270D ND 1ug/L1.15.0
3 & 4-Methylphenol 106-44-5 8270D ND 1ug/L2.710
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/L1.45.0
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/L1.05.0
Naphthalene 91-20-3 8270D ND 1ug/L1.35.0
2-Nitroaniline 88-74-4 8270D ND 1ug/L2.110
3-Nitroaniline 99-09-2 8270D ND 1ug/L3.010
4-Nitroaniline 100-01-6 8270D ND 1ug/L4.210
Nitrobenzene 98-95-3 8270D ND 1ug/L1.65.0
2-Nitrophenol 88-75-5 8270D ND 1ug/L2.910
4-Nitrophenol 100-02-7 8270D ND 1ug/L9.025
Pentachlorophenol 87-86-5 8270D ND 1ug/L5.125
Phenanthrene 85-01-8 8270D ND 1ug/L1.25.0
Phenol 108-95-2 8270D ND 1ug/L1.25.0
Pyrene 129-00-0 8270D ND 1ug/L3.15.0
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/L1.25.0
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/L1.35.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,4,6-Tribromophenol 78 41-144
2-Fluorobiphenyl 87 37-129
2-Fluorophenol 74 24-127
Nitrobenzene-d5 100 38-127
Phenol-d5 86 28-128
Terphenyl-d14 46 10-148
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 28 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-8
PL06010-007
12/05/2014 1230
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 12/13/2014 1721 ALL 63005
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/L3.310
Benzene 71-43-2 8260B 0.63 1ug/L0.0270.50
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.170.50
Bromoform 75-25-2 8260B ND 1ug/L0.0100.50
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.200.50
2-Butanone (MEK)78-93-3 8260B ND 1ug/L2.010
Carbon disulfide 75-15-0 8260B ND 1ug/L0.0970.50
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.0850.50
Chlorobenzene 108-90-7 8260B ND 1ug/L0.170.50
Chloroethane 75-00-3 8260B ND 1ug/L0.170.50
Chloroform 67-66-3 8260B ND 1ug/L0.170.50
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.170.50
Cyclohexane 110-82-7 8260B ND 1ug/L0.300.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.0690.50
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.170.50
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.0610.50
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.170.50
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.170.50
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.170.50
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.0710.50
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.0540.50
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.0230.50
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.0790.50
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.0940.50
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.0870.50
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.0810.50
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.180.50
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.0900.50
Ethylbenzene 100-41-4 8260B ND 1ug/L0.170.50
2-Hexanone 591-78-6 8260B ND 1ug/L0.2710
Isopropylbenzene 98-82-8 8260B ND 1ug/L0.0290.50
Methyl acetate 79-20-9 8260B ND 1ug/L0.301.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.0190.50
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L0.3110
Methylcyclohexane 108-87-2 8260B ND 1ug/L0.955.0
Methylene chloride 75-09-2 8260B ND 1ug/L0.170.50
Styrene 100-42-5 8260B ND 1ug/L0.0150.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.0130.50
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.0140.50
Toluene 108-88-3 8260B ND 1ug/L0.170.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L0.300.50
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.170.50
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.0290.50
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.0310.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 29 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-8
PL06010-007
12/05/2014 1230
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 12/13/2014 1721 ALL 63005
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/L0.0240.50
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.0510.50
Vinyl chloride 75-01-4 8260B ND 1ug/L0.0650.50
Xylenes (total)1330-20-7 8260B ND 1ug/L0.170.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Bromofluorobenzene 112 70-130
Toluene-d8 111 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 30 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-8
PL06010-007
12/05/2014 1230
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 12/11/2014 1608 RBH 12/08/2014 1820 62580
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/L1.25.0
Acenaphthylene 208-96-8 8270D ND 1ug/L1.25.0
Acetophenone 98-86-2 8270D ND 1ug/L0.905.0
Anthracene 120-12-7 8270D ND 1ug/L1.15.0
Atrazine 1912-24-9 8270D ND 1ug/L4.25.0
Benzaldehyde 100-52-7 8270D ND 1ug/L3.025
Benzo(a)anthracene 56-55-3 8270D ND 1ug/L0.605.0
Benzo(a)pyrene 50-32-8 8270D ND 1ug/L0.505.0
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/L0.605.0
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/L0.805.0
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/L1.05.0
1,1'-Biphenyl 92-52-4 8270D ND 1ug/L1.35.0
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/L1.25.0
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/L3.310
Caprolactam 105-60-2 8270D ND 1ug/L1.225
Carbazole 86-74-8 8270D ND 1ug/L1.75.0
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/L1.65.0
4-Chloroaniline 106-47-8 8270D ND 1ug/L0.815.0
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/L1.55.0
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/L1.25.0
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 1ug/L1.35.0
2-Chloronaphthalene 91-58-7 8270D ND 1ug/L1.35.0
2-Chlorophenol 95-57-8 8270D ND 1ug/L1.45.0
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/L1.65.0
Chrysene 218-01-9 8270D ND 1ug/L0.705.0
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/L1.75.0
Di-n-octylphthalate 117-84-0 8270D ND 1ug/L1.75.0
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/L1.35.0
Dibenzofuran 132-64-9 8270D ND 1ug/L1.25.0
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/L2.625
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/L1.25.0
Diethylphthalate 84-66-2 8270D ND 1ug/L1.95.0
Dimethyl phthalate 131-11-3 8270D ND 1ug/L1.75.0
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/L1.45.0
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/L8.125
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/L4.825
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/L3.810
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/L3.410
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/L1.75.0
Fluoranthene 206-44-0 8270D ND 1ug/L1.45.0
Fluorene 86-73-7 8270D ND 1ug/L1.45.0
Hexachlorobenzene 118-74-1 8270D ND 1ug/L1.25.0
Hexachlorobutadiene 87-68-3 8270D ND 1ug/L1.45.0
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/L4.025
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 31 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-8
PL06010-007
12/05/2014 1230
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 12/11/2014 1608 RBH 12/08/2014 1820 62580
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Hexachloroethane 67-72-1 8270D ND 1ug/L1.25.0
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/L2.35.0
Isophorone 78-59-1 8270D ND 1ug/L1.45.0
2-Methylnaphthalene 91-57-6 8270D ND 1ug/L1.55.0
2-Methylphenol 95-48-7 8270D ND 1ug/L1.15.0
3 & 4-Methylphenol 106-44-5 8270D ND 1ug/L2.710
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/L1.45.0
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/L1.05.0
Naphthalene 91-20-3 8270D ND 1ug/L1.35.0
2-Nitroaniline 88-74-4 8270D ND 1ug/L2.110
3-Nitroaniline 99-09-2 8270D ND 1ug/L3.010
4-Nitroaniline 100-01-6 8270D ND 1ug/L4.210
Nitrobenzene 98-95-3 8270D ND 1ug/L1.65.0
2-Nitrophenol 88-75-5 8270D ND 1ug/L2.910
4-Nitrophenol 100-02-7 8270D ND 1ug/L9.025
Pentachlorophenol 87-86-5 8270D ND 1ug/L5.125
Phenanthrene 85-01-8 8270D ND 1ug/L1.25.0
Phenol 108-95-2 8270D ND 1ug/L1.25.0
Pyrene 129-00-0 8270D ND 1ug/L3.15.0
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/L1.25.0
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/L1.35.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,4,6-Tribromophenol 84 41-144
2-Fluorobiphenyl 89 37-129
2-Fluorophenol 89 24-127
Nitrobenzene-d5 96 38-127
Phenol-d5 93 28-128
Terphenyl-d14 85 10-148
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 32 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-7
PL06010-008
12/05/2014 1315
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 12/13/2014 1742 ALL 63005
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/L3.310
Benzene 71-43-2 8260B 31 1ug/L0.0270.50
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.170.50
Bromoform 75-25-2 8260B ND 1ug/L0.0100.50
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.200.50
2-Butanone (MEK)78-93-3 8260B ND 1ug/L2.010
Carbon disulfide 75-15-0 8260B ND 1ug/L0.0970.50
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.0850.50
Chlorobenzene 108-90-7 8260B ND 1ug/L0.170.50
Chloroethane 75-00-3 8260B ND 1ug/L0.170.50
Chloroform 67-66-3 8260B 0.60 1ug/L0.170.50
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.170.50
Cyclohexane 110-82-7 8260B ND 1ug/L0.300.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.0690.50
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.170.50
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.0610.50
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.170.50
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.170.50
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.170.50
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.0710.50
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.0540.50
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.0230.50
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.0790.50
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.0940.50
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.0870.50
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.0810.50
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.180.50
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.0900.50
Ethylbenzene 100-41-4 8260B 1.3 1ug/L0.170.50
2-Hexanone 591-78-6 8260B ND 1ug/L0.2710
Isopropylbenzene 98-82-8 8260B 1.6 1ug/L0.0290.50
Methyl acetate 79-20-9 8260B ND 1ug/L0.301.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 9.5 1ug/L0.0190.50
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L0.3110
Methylcyclohexane 108-87-2 8260B ND 1ug/L0.955.0
Methylene chloride 75-09-2 8260B ND 1ug/L0.170.50
Styrene 100-42-5 8260B 0.61 1ug/L0.0150.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.0130.50
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.0140.50
Toluene 108-88-3 8260B 0.40 J 1ug/L0.170.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L0.300.50
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.170.50
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.0290.50
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.0310.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 33 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-7
PL06010-008
12/05/2014 1315
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 12/13/2014 1742 ALL 63005
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichloroethene 79-01-6 8260B ND 1ug/L0.0240.50
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.0510.50
Vinyl chloride 75-01-4 8260B ND 1ug/L0.0650.50
Xylenes (total)1330-20-7 8260B 54 1ug/L0.170.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 105 70-130
Bromofluorobenzene 123 70-130
Toluene-d8 117 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 34 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-7
PL06010-008
12/05/2014 1315
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 12/11/2014 1632 RBH 12/08/2014 1820 62580
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/L1.25.0
Acenaphthylene 208-96-8 8270D ND 1ug/L1.25.0
Acetophenone 98-86-2 8270D ND 1ug/L0.905.0
Anthracene 120-12-7 8270D ND 1ug/L1.15.0
Atrazine 1912-24-9 8270D ND 1ug/L4.25.0
Benzaldehyde 100-52-7 8270D ND 1ug/L3.025
Benzo(a)anthracene 56-55-3 8270D ND 1ug/L0.605.0
Benzo(a)pyrene 50-32-8 8270D ND 1ug/L0.505.0
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/L0.605.0
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/L0.805.0
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/L1.05.0
1,1'-Biphenyl 92-52-4 8270D ND 1ug/L1.35.0
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/L1.25.0
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/L3.310
Caprolactam 105-60-2 8270D ND 1ug/L1.225
Carbazole 86-74-8 8270D ND 1ug/L1.75.0
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/L1.65.0
4-Chloroaniline 106-47-8 8270D ND 1ug/L0.815.0
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/L1.55.0
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/L1.25.0
bis(2-Chloroisopropyl)ether 108-60-1 8270D ND 1ug/L1.35.0
2-Chloronaphthalene 91-58-7 8270D ND 1ug/L1.35.0
2-Chlorophenol 95-57-8 8270D ND 1ug/L1.45.0
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/L1.65.0
Chrysene 218-01-9 8270D ND 1ug/L0.705.0
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/L1.75.0
Di-n-octylphthalate 117-84-0 8270D ND 1ug/L1.75.0
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/L1.35.0
Dibenzofuran 132-64-9 8270D ND 1ug/L1.25.0
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/L2.625
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/L1.25.0
Diethylphthalate 84-66-2 8270D ND 1ug/L1.95.0
Dimethyl phthalate 131-11-3 8270D ND 1ug/L1.75.0
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/L1.45.0
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/L8.125
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/L4.825
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/L3.810
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/L3.410
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/L1.75.0
Fluoranthene 206-44-0 8270D ND 1ug/L1.45.0
Fluorene 86-73-7 8270D ND 1ug/L1.45.0
Hexachlorobenzene 118-74-1 8270D ND 1ug/L1.25.0
Hexachlorobutadiene 87-68-3 8270D ND 1ug/L1.45.0
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/L4.025
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 35 of 53
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Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
B-7
PL06010-008
12/05/2014 1315
12/06/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 12/11/2014 1632 RBH 12/08/2014 1820 62580
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Hexachloroethane 67-72-1 8270D ND 1ug/L1.25.0
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/L2.35.0
Isophorone 78-59-1 8270D ND 1ug/L1.45.0
2-Methylnaphthalene 91-57-6 8270D ND 1ug/L1.55.0
2-Methylphenol 95-48-7 8270D ND 1ug/L1.15.0
3 & 4-Methylphenol 106-44-5 8270D ND 1ug/L2.710
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/L1.45.0
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/L1.05.0
Naphthalene 91-20-3 8270D 6.0 1ug/L1.35.0
2-Nitroaniline 88-74-4 8270D ND 1ug/L2.110
3-Nitroaniline 99-09-2 8270D ND 1ug/L3.010
4-Nitroaniline 100-01-6 8270D ND 1ug/L4.210
Nitrobenzene 98-95-3 8270D ND 1ug/L1.65.0
2-Nitrophenol 88-75-5 8270D ND 1ug/L2.910
4-Nitrophenol 100-02-7 8270D ND 1ug/L9.025
Pentachlorophenol 87-86-5 8270D ND 1ug/L5.125
Phenanthrene 85-01-8 8270D ND 1ug/L1.25.0
Phenol 108-95-2 8270D ND 1ug/L1.25.0
Pyrene 129-00-0 8270D ND 1ug/L3.15.0
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/L1.25.0
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/L1.35.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,4,6-Tribromophenol 83 41-144
2-Fluorobiphenyl 87 37-129
2-Fluorophenol 87 24-127
Nitrobenzene-d5 100 38-127
Phenol-d5 95 28-128
Terphenyl-d14 49 10-148
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 36 of 53
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Level 1 Report v2.1
QC Summary
Page: 37 of 53
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ62647-001
62647 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 12/09/2014 1051206.7 ug/kg1
Benzene ND 12/09/2014 10515.0 1.1 ug/kg1
Bromodichloromethane ND 12/09/2014 10515.0 1.7 ug/kg1
Bromoform ND 12/09/2014 10515.0 0.70 ug/kg1
Bromomethane (Methyl bromide)ND 12/09/2014 10515.0 1.8 ug/kg1
2-Butanone (MEK)ND 12/09/2014 1051102.4 ug/kg1
Carbon disulfide ND 12/09/2014 10515.0 1.3 ug/kg1
Carbon tetrachloride ND 12/09/2014 10515.0 1.8 ug/kg1
Chlorobenzene ND 12/09/2014 10515.0 1.7 ug/kg1
Chloroethane ND 12/09/2014 10515.0 1.3 ug/kg1
Chloroform ND 12/09/2014 10515.0 0.83 ug/kg1
Chloromethane (Methyl chloride)ND 12/09/2014 10515.0 1.0 ug/kg1
Cyclohexane ND 12/09/2014 10515.0 0.67 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 12/09/2014 10515.0 1.5 ug/kg1
Dibromochloromethane ND 12/09/2014 10515.0 1.7 ug/kg1
1,2-Dibromoethane (EDB)ND 12/09/2014 10515.0 0.85 ug/kg1
1,4-Dichlorobenzene ND 12/09/2014 10515.0 1.7 ug/kg1
1,3-Dichlorobenzene ND 12/09/2014 10515.0 1.7 ug/kg1
1,2-Dichlorobenzene ND 12/09/2014 10515.0 1.7 ug/kg1
Dichlorodifluoromethane ND 12/09/2014 10515.0 1.6 ug/kg1
1,2-Dichloroethane ND 12/09/2014 10515.0 1.0 ug/kg1
1,1-Dichloroethane ND 12/09/2014 10515.0 0.73 ug/kg1
trans-1,2-Dichloroethene ND 12/09/2014 10515.0 1.5 ug/kg1
cis-1,2-Dichloroethene ND 12/09/2014 10515.0 0.76 ug/kg1
1,1-Dichloroethene ND 12/09/2014 10515.0 1.7 ug/kg1
1,2-Dichloropropane ND 12/09/2014 10515.0 0.91 ug/kg1
trans-1,3-Dichloropropene ND 12/09/2014 10515.0 0.82 ug/kg1
cis-1,3-Dichloropropene ND 12/09/2014 10515.0 0.68 ug/kg1
Ethylbenzene ND 12/09/2014 10515.0 1.7 ug/kg1
2-Hexanone ND 12/09/2014 1051101.3 ug/kg1
Isopropylbenzene ND 12/09/2014 10515.0 0.23 ug/kg1
Methyl acetate ND 12/09/2014 10515.0 0.98 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 12/09/2014 10515.0 0.40 ug/kg1
4-Methyl-2-pentanone ND 12/09/2014 1051101.5 ug/kg1
Methylcyclohexane ND 12/09/2014 10515.0 0.41 ug/kg1
Methylene chloride ND 12/09/2014 10515.0 2.6 ug/kg1
Styrene ND 12/09/2014 10515.0 1.1 ug/kg1
1,1,2,2-Tetrachloroethane ND 12/09/2014 10515.0 0.47 ug/kg1
Tetrachloroethene ND 12/09/2014 10515.0 0.50 ug/kg1
Toluene ND 12/09/2014 10515.0 1.7 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 12/09/2014 10515.0 0.63 ug/kg1
1,2,4-Trichlorobenzene ND 12/09/2014 10515.0 1.7 ug/kg1
1,1,2-Trichloroethane ND 12/09/2014 10515.0 0.79 ug/kg1
1,1,1-Trichloroethane ND 12/09/2014 10515.0 0.85 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 38 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ62647-001
62647 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Trichloroethene ND 12/09/2014 10515.0 1.9 ug/kg1
Trichlorofluoromethane ND 12/09/2014 10515.0 1.5 ug/kg1
Vinyl chloride ND 12/09/2014 10515.0 0.86 ug/kg1
Xylenes (total)ND 12/09/2014 10515.0 2.9 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 93 47-138
1,2-Dichloroethane-d4 100 53-142
Toluene-d8 98 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 39 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ62647-002
62647 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 100 12/09/2014 094910310060-1401
Benzene 44 12/09/2014 0949885069-1231
Bromodichloromethane 45 12/09/2014 0949915069-1211
Bromoform 46 12/09/2014 0949935061-1191
Bromomethane (Methyl bromide)44 12/09/2014 0949895010-1681
2-Butanone (MEK)99 12/09/2014 09499910057-1481
Carbon disulfide 46 12/09/2014 0949935058-1221
Carbon tetrachloride 47 12/09/2014 0949945058-1361
Chlorobenzene 43 12/09/2014 0949875059-1291
Chloroethane 44 12/09/2014 0949875042-1631
Chloroform 45 12/09/2014 0949915071-1251
Chloromethane (Methyl chloride)43 12/09/2014 0949865034-1341
Cyclohexane 50 12/09/2014 09491015053-1391
1,2-Dibromo-3-chloropropane (DBCP)50 12/09/2014 0949995055-1251
Dibromochloromethane 46 12/09/2014 0949935066-1191
1,2-Dibromoethane (EDB)44 12/09/2014 0949885074-1241
1,4-Dichlorobenzene 42 12/09/2014 0949835052-1331
1,3-Dichlorobenzene 42 12/09/2014 0949845051-1341
1,2-Dichlorobenzene 42 12/09/2014 0949845057-1311
Dichlorodifluoromethane 45 12/09/2014 0949905010-1571
1,2-Dichloroethane 48 12/09/2014 0949965067-1291
1,1-Dichloroethane 46 12/09/2014 0949935071-1271
trans-1,2-Dichloroethene 45 12/09/2014 0949915068-1311
cis-1,2-Dichloroethene 45 12/09/2014 0949905070-1221
1,1-Dichloroethene 48 12/09/2014 0949955069-1381
1,2-Dichloropropane 45 12/09/2014 0949905072-1241
trans-1,3-Dichloropropene 45 12/09/2014 0949905070-1241
cis-1,3-Dichloropropene 46 12/09/2014 0949915070-1261
Ethylbenzene 43 12/09/2014 0949855059-1281
2-Hexanone 95 12/09/2014 09499510054-1371
Isopropylbenzene 41 12/09/2014 0949825050-1361
Methyl acetate 58 12/09/2014 09491165059-1371
Methyl tertiary butyl ether (MTBE)48 12/09/2014 0949975070-1301
4-Methyl-2-pentanone 100 12/09/2014 094910210060-1341
Methylcyclohexane 46 12/09/2014 0949925041-1441
Methylene chloride 46 12/09/2014 0949915070-1301
Styrene 43 12/09/2014 0949865054-1361
1,1,2,2-Tetrachloroethane 45 12/09/2014 0949905069-1321
Tetrachloroethene 45 12/09/2014 0949905045-1501
Toluene 42 12/09/2014 0949855061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 50 12/09/2014 09491005049-1361
1,2,4-Trichlorobenzene 43 12/09/2014 0949875034-1451
1,1,2-Trichloroethane 44 12/09/2014 0949875055-1281
1,1,1-Trichloroethane 47 12/09/2014 0949945063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 40 of 53
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ62647-002
62647 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 45 12/09/2014 0949895062-1261
Trichlorofluoromethane 46 12/09/2014 0949935045-1381
Vinyl chloride 43 12/09/2014 0949865042-1321
Xylenes (total)87 12/09/2014 09498710058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 94 47-138
1,2-Dichloroethane-d4 100 53-142
Toluene-d8 98 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 41 of 53
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ63005-001
63005 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 12/13/2014 1235103.3 ug/L1
Benzene ND 12/13/2014 12350.50 0.027 ug/L1
Bromodichloromethane ND 12/13/2014 12350.50 0.17 ug/L1
Bromoform ND 12/13/2014 12350.50 0.010 ug/L1
Bromomethane (Methyl bromide)ND 12/13/2014 12350.50 0.20 ug/L1
2-Butanone (MEK)ND 12/13/2014 1235102.0 ug/L1
Carbon disulfide ND 12/13/2014 12350.50 0.097 ug/L1
Carbon tetrachloride ND 12/13/2014 12350.50 0.085 ug/L1
Chlorobenzene ND 12/13/2014 12350.50 0.17 ug/L1
Chloroethane ND 12/13/2014 12350.50 0.17 ug/L1
Chloroform ND 12/13/2014 12350.50 0.17 ug/L1
Chloromethane (Methyl chloride)ND 12/13/2014 12350.50 0.17 ug/L1
Cyclohexane ND 12/13/2014 12350.50 0.30 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 12/13/2014 12350.50 0.069 ug/L1
Dibromochloromethane ND 12/13/2014 12350.50 0.17 ug/L1
1,2-Dibromoethane (EDB)ND 12/13/2014 12350.50 0.061 ug/L1
1,4-Dichlorobenzene ND 12/13/2014 12350.50 0.17 ug/L1
1,3-Dichlorobenzene ND 12/13/2014 12350.50 0.17 ug/L1
1,2-Dichlorobenzene ND 12/13/2014 12350.50 0.17 ug/L1
Dichlorodifluoromethane ND 12/13/2014 12350.50 0.071 ug/L1
1,2-Dichloroethane ND 12/13/2014 12350.50 0.023 ug/L1
1,1-Dichloroethane ND 12/13/2014 12350.50 0.054 ug/L1
trans-1,2-Dichloroethene ND 12/13/2014 12350.50 0.079 ug/L1
cis-1,2-Dichloroethene ND 12/13/2014 12350.50 0.087 ug/L1
1,1-Dichloroethene ND 12/13/2014 12350.50 0.094 ug/L1
1,2-Dichloropropane ND 12/13/2014 12350.50 0.081 ug/L1
trans-1,3-Dichloropropene ND 12/13/2014 12350.50 0.18 ug/L1
cis-1,3-Dichloropropene ND 12/13/2014 12350.50 0.090 ug/L1
Ethylbenzene ND 12/13/2014 12350.50 0.17 ug/L1
2-Hexanone ND 12/13/2014 1235100.27 ug/L1
Isopropylbenzene ND 12/13/2014 12350.50 0.029 ug/L1
Methyl acetate ND 12/13/2014 12351.0 0.30 ug/L1
Methyl tertiary butyl ether (MTBE)ND 12/13/2014 12350.50 0.019 ug/L1
4-Methyl-2-pentanone ND 12/13/2014 1235100.31 ug/L1
Methylcyclohexane ND 12/13/2014 12355.0 0.95 ug/L1
Methylene chloride ND 12/13/2014 12350.50 0.17 ug/L1
Styrene ND 12/13/2014 12350.50 0.015 ug/L1
1,1,2,2-Tetrachloroethane ND 12/13/2014 12350.50 0.013 ug/L1
Tetrachloroethene ND 12/13/2014 12350.50 0.014 ug/L1
Toluene ND 12/13/2014 12350.50 0.17 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 12/13/2014 12350.50 0.30 ug/L1
1,2,4-Trichlorobenzene ND 12/13/2014 12350.50 0.17 ug/L1
1,1,2-Trichloroethane ND 12/13/2014 12350.50 0.031 ug/L1
1,1,1-Trichloroethane ND 12/13/2014 12350.50 0.029 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 42 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ63005-001
63005 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Trichloroethene ND 12/13/2014 12350.50 0.024 ug/L1
Trichlorofluoromethane ND 12/13/2014 12350.50 0.051 ug/L1
Vinyl chloride ND 12/13/2014 12350.50 0.065 ug/L1
Xylenes (total)ND 12/13/2014 12350.50 0.17 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 115 70-130
1,2-Dichloroethane-d4 103 70-130
Toluene-d8 108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 43 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ63005-002
63005 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 77 12/13/2014 11167710060-1401
Benzene 52 12/13/2014 11161035070-1301
Bromodichloromethane 56 12/13/2014 11161125070-1301
Bromoform 52 12/13/2014 11161055070-1301
Bromomethane (Methyl bromide)46 12/13/2014 1116935060-1401
2-Butanone (MEK)97 12/13/2014 11169710060-1401
Carbon disulfide 53 12/13/2014 11161065060-1401
Carbon tetrachloride 50 12/13/2014 11161005070-1301
Chlorobenzene 54 12/13/2014 11161075070-1301
Chloroethane 46 12/13/2014 1116925042-1631
Chloroform 50 12/13/2014 11161015070-1301
Chloromethane (Methyl chloride)56 12/13/2014 11161135020-1581
Cyclohexane 48 12/13/2014 1116975070-1301
1,2-Dibromo-3-chloropropane (DBCP)49 12/13/2014 1116975070-1301
Dibromochloromethane 51 12/13/2014 11161035070-1301
1,2-Dibromoethane (EDB)52 12/13/2014 11161035070-1301
1,4-Dichlorobenzene 54 12/13/2014 11161095070-1301
1,3-Dichlorobenzene 56 12/13/2014 11161115070-1301
1,2-Dichlorobenzene 54 12/13/2014 11161085070-1301
Dichlorodifluoromethane 58 12/13/2014 11161165060-1401
1,2-Dichloroethane 52 12/13/2014 11161045070-1301
1,1-Dichloroethane 51 12/13/2014 11161025070-1301
trans-1,2-Dichloroethene 55 12/13/2014 11161105070-1301
cis-1,2-Dichloroethene 54 12/13/2014 11161095070-1301
1,1-Dichloroethene 51 12/13/2014 11161015070-1301
1,2-Dichloropropane 51 12/13/2014 11161025070-1301
trans-1,3-Dichloropropene 54 12/13/2014 11161095070-1301
cis-1,3-Dichloropropene 53 12/13/2014 11161055070-1301
Ethylbenzene 55 12/13/2014 11161105070-1301
2-Hexanone 98 12/13/2014 11169810060-1401
Isopropylbenzene 54 12/13/2014 11161085070-1301
Methyl acetate 52 12/13/2014 11161045060-1401
Methyl tertiary butyl ether (MTBE)50 12/13/2014 11161015070-1301
4-Methyl-2-pentanone 96 12/13/2014 11169610060-1401
Methylcyclohexane 53 12/13/2014 11161065070-1301
Methylene chloride 47 12/13/2014 1116955070-1301
Styrene 56 12/13/2014 11161125070-1301
1,1,2,2-Tetrachloroethane 57 12/13/2014 11161145070-1301
Tetrachloroethene 60 12/13/2014 11161215070-1301
Toluene 56 12/13/2014 11161125070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 54 12/13/2014 11161085070-1301
1,2,4-Trichlorobenzene 55 12/13/2014 11161105070-1301
1,1,2-Trichloroethane 53 12/13/2014 11161065070-1301
1,1,1-Trichloroethane 50 12/13/2014 11161005070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 44 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ63005-002
63005 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Trichloroethene 52 12/13/2014 11161055070-1301
Trichlorofluoromethane 52 12/13/2014 11161055060-1401
Vinyl chloride 57 12/13/2014 11161145060-1401
Xylenes (total)110 12/13/2014 111611110070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 121 70-130
1,2-Dichloroethane-d4 101 70-130
Toluene-d8 110 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 45 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:PQ62573-001
62573 3550C
12/08/2014 1620Analytical Method:8270D
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
1,1'-Biphenyl ND 12/09/2014 144633031ug/kg1
2,4,5-Trichlorophenol ND 12/09/2014 144633017ug/kg1
2,4,6-Trichlorophenol ND 12/09/2014 144633018ug/kg1
2,4-Dichlorophenol ND 12/09/2014 144633013ug/kg1
2,4-Dimethylphenol ND 12/09/2014 144633017ug/kg1
2,4-Dinitrophenol ND 12/09/2014 14468306.6 ug/kg1
2,4-Dinitrotoluene ND 12/09/2014 144633024ug/kg1
2,6-Dinitrotoluene ND 12/09/2014 144633029ug/kg1
2-Chloronaphthalene ND 12/09/2014 144633016ug/kg1
2-Chlorophenol ND 12/09/2014 144633014ug/kg1
2-Methylnaphthalene ND 12/09/2014 144633012ug/kg1
2-Methylphenol ND 12/09/2014 144633019ug/kg1
2-Nitroaniline ND 12/09/2014 144633023ug/kg1
2-Nitrophenol ND 12/09/2014 144633036ug/kg1
3 & 4-Methylphenol ND 12/09/2014 144667031ug/kg1
3,3'-Dichlorobenzidine ND 12/09/2014 144683057ug/kg1
3-Nitroaniline ND 12/09/2014 144633024ug/kg1
4,6-Dinitro-2-methylphenol ND 12/09/2014 144683038ug/kg1
4-Bromophenyl phenyl ether ND 12/09/2014 144633014ug/kg1
4-Chloro-3-methyl phenol ND 12/09/2014 144633018ug/kg1
4-Chloroaniline ND 12/09/2014 144633017ug/kg1
4-Chlorophenyl phenyl ether ND 12/09/2014 144633013ug/kg1
4-Nitroaniline ND 12/09/2014 144633020ug/kg1
4-Nitrophenol ND 12/09/2014 1446830140ug/kg1
Acenaphthene ND 12/09/2014 144633010ug/kg1
Acenaphthylene ND 12/09/2014 144633013ug/kg1
Acetophenone ND 12/09/2014 144633020ug/kg1
Anthracene ND 12/09/2014 144633015ug/kg1
Atrazine ND 12/09/2014 1446330100ug/kg1
Benzaldehyde ND 12/09/2014 144683026ug/kg1
Benzo(a)anthracene ND 12/09/2014 144633011ug/kg1
Benzo(a)pyrene ND 12/09/2014 144633024ug/kg1
Benzo(b)fluoranthene ND 12/09/2014 144633022ug/kg1
Benzo(g,h,i)perylene ND 12/09/2014 144633023ug/kg1
Benzo(k)fluoranthene ND 12/09/2014 144633027ug/kg1
bis(2-Chloroethoxy)methane ND 12/09/2014 144633015ug/kg1
bis(2-Chloroethyl)ether ND 12/09/2014 144633014ug/kg1
bis(2-Chloroisopropyl)ether ND 12/09/2014 144633013ug/kg1
bis(2-Ethylhexyl)phthalate ND 12/09/2014 1446330110ug/kg1
Butyl benzyl phthalate ND 12/09/2014 1446330110ug/kg1
Caprolactam ND 12/09/2014 144683024ug/kg1
Carbazole ND 12/09/2014 14463309.8 ug/kg1
Chrysene ND 12/09/2014 144633010ug/kg1
Di-n-butyl phthalate ND 12/09/2014 1446330110ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 46 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:PQ62573-001
62573 3550C
12/08/2014 1620Analytical Method:8270D
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Di-n-octylphthalate ND 12/09/2014 1446330110ug/kg1
Dibenzo(a,h)anthracene ND 12/09/2014 144633022ug/kg1
Dibenzofuran ND 12/09/2014 144633013ug/kg1
Diethylphthalate ND 12/09/2014 1446330110ug/kg1
Dimethyl phthalate ND 12/09/2014 1446330110ug/kg1
Fluoranthene ND 12/09/2014 144633010ug/kg1
Fluorene ND 12/09/2014 144633013ug/kg1
Hexachlorobenzene ND 12/09/2014 144633013ug/kg1
Hexachlorobutadiene ND 12/09/2014 144633014ug/kg1
Hexachlorocyclopentadiene ND 12/09/2014 144683064ug/kg1
Hexachloroethane ND 12/09/2014 144633016ug/kg1
Indeno(1,2,3-c,d)pyrene ND 12/09/2014 144633030ug/kg1
Isophorone ND 12/09/2014 144633016ug/kg1
N-Nitrosodi-n-propylamine ND 12/09/2014 144633017ug/kg1
N-Nitrosodiphenylamine (Diphenylamine)ND 12/09/2014 144633011ug/kg1
Naphthalene ND 12/09/2014 144633014ug/kg1
Nitrobenzene ND 12/09/2014 144633015ug/kg1
Pentachlorophenol ND 12/09/2014 144683035ug/kg1
Phenanthrene ND 12/09/2014 144633013ug/kg1
Phenol ND 12/09/2014 144633016ug/kg1
Pyrene ND 12/09/2014 144633014ug/kg1
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 65 30-117
2-Fluorobiphenyl 82 33-102
2-Fluorophenol 73 28-104
Nitrobenzene-d5 71 22-109
Phenol-d5 77 27-103
Terphenyl-d14 91 41-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 47 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:PQ62573-002
62573 3550C
12/08/2014 1620Analytical Method:8270D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
1,1'-Biphenyl 2700 12/09/2014 151381330049-1101
2,4,5-Trichlorophenol 2900 12/09/2014 151387330046-1221
2,4,6-Trichlorophenol 2700 12/09/2014 151381330038-1151
2,4-Dichlorophenol 2800 12/09/2014 151383330041-1131
2,4-Dimethylphenol 3400 12/09/2014 1513103330033-1231
2,4-Dinitrophenol 17000 12/09/2014 15131011700045-1271
2,4-Dinitrotoluene 6100 12/09/2014 151392670048-1241
2,6-Dinitrotoluene 6100 12/09/2014 151391670047-1251
2-Chloronaphthalene 2400 12/09/2014 151373330031-1271
2-Chlorophenol 2400 12/09/2014 151373330037-1061
2-Methylnaphthalene 2800 12/09/2014 151383330040-1061
2-Methylphenol 2700 12/09/2014 151380330032-1071
2-Nitroaniline 5900 12/09/2014 151389670045-1231
2-Nitrophenol 5300 12/09/2014 151379670035-1081
3 & 4-Methylphenol 5200 12/09/2014 151378670039-1081
3,3'-Dichlorobenzidine 5800 12/09/2014 151387670046-1131
3-Nitroaniline 5400 12/09/2014 151382670024-1271
4,6-Dinitro-2-methylphenol 15000 12/09/2014 1513931700040-1301
4-Bromophenyl phenyl ether 2700 12/09/2014 151381330046-1181
4-Chloro-3-methyl phenol 2900 12/09/2014 151386330049-1181
4-Chloroaniline 3000 12/09/2014 151389330010-1251
4-Chlorophenyl phenyl ether 2800 12/09/2014 151383330047-1161
4-Nitroaniline 6500 12/09/2014 151398670048-1271
4-Nitrophenol 14000 12/09/2014 1513851700018-1541
Acenaphthene 2600 12/09/2014 151379330046-1141
Acenaphthylene 3400 12/09/2014 1513103330044-1221
Acetophenone 2500 12/09/2014 151375330048-1111
Anthracene 3000 12/09/2014 151389330050-1191
Atrazine 2400 12/09/2014 151373330048-1161
Benzaldehyde 1800 12/09/2014 151355330040-1171
Benzo(a)anthracene 2900 12/09/2014 151386330047-1211
Benzo(a)pyrene 3400 12/09/2014 1513102330055-1341
Benzo(b)fluoranthene 3300 12/09/2014 151398330028-1391
Benzo(g,h,i)perylene 2700 12/09/2014 151382330036-1251
Benzo(k)fluoranthene 3400 12/09/2014 1513102330047-1301
bis(2-Chloroethoxy)methane 2400 12/09/2014 151372330039-1081
bis(2-Chloroethyl)ether 2000 12/09/2014 151361330032-1051
bis(2-Chloroisopropyl)ether 1900 12/09/2014 151356330031-1021
bis(2-Ethylhexyl)phthalate 3200 12/09/2014 151397330045-1281
Butyl benzyl phthalate 3300 12/09/2014 151399330046-1281
Caprolactam 3700 12/09/2014 1513110330043-1211
Carbazole 3200 12/09/2014 151395330047-1281
Chrysene 2900 12/09/2014 151387330045-1261
Di-n-butyl phthalate 3000 12/09/2014 151389330051-1291
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 48 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:PQ62573-002
62573 3550C
12/08/2014 1620Analytical Method:8270D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Di-n-octylphthalate 3300 12/09/2014 151398330049-1421
Dibenzo(a,h)anthracene 2900 12/09/2014 151387330045-1221
Dibenzofuran 2800 12/09/2014 151383330045-1121
Diethylphthalate 2800 12/09/2014 151383330049-1231
Dimethyl phthalate 2900 12/09/2014 151387330048-1201
Fluoranthene 3100 12/09/2014 151392330050-1231
Fluorene 2800 12/09/2014 151384330048-1171
Hexachlorobenzene 2600 12/09/2014 151379330044-1221
Hexachlorobutadiene 2400 12/09/2014 151373330033-1031
Hexachlorocyclopentadiene 14000 12/09/2014 1513831700018-1211
Hexachloroethane 2000 12/09/2014 151359330030-961
Indeno(1,2,3-c,d)pyrene 2900 12/09/2014 151387330045-1231
Isophorone 2600 12/09/2014 151377330041-1131
N-Nitrosodi-n-propylamine 2400 12/09/2014 151372330032-1151
N-Nitrosodiphenylamine (Diphenylamine)3300 12/09/2014 151398330053-1501
Naphthalene 2400 12/09/2014 151373330036-1101
Nitrobenzene 2300 12/09/2014 151369330033-1141
Pentachlorophenol 14000 12/09/2014 1513861700027-1381
Phenanthrene 2800 12/09/2014 151385330049-1171
Phenol 2400 12/09/2014 151373330036-1081
Pyrene 3000 12/09/2014 151389330047-1191
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 93 30-117
2-Fluorobiphenyl 81 33-102
2-Fluorophenol 73 28-104
Nitrobenzene-d5 75 22-109
Phenol-d5 78 27-103
Terphenyl-d14 94 41-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 49 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:PQ62580-001
62580 3520C
12/08/2014 1820Analytical Method:8270D
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
1,1'-Biphenyl ND 12/10/2014 10515.0 1.3 ug/L1
2,4,5-Trichlorophenol ND 12/10/2014 10515.0 1.2 ug/L1
2,4,6-Trichlorophenol ND 12/10/2014 10515.0 1.3 ug/L1
2,4-Dichlorophenol ND 12/10/2014 10515.0 1.2 ug/L1
2,4-Dimethylphenol ND 12/10/2014 10515.0 1.4 ug/L1
2,4-Dinitrophenol ND 12/10/2014 1051254.8 ug/L1
2,4-Dinitrotoluene ND 12/10/2014 1051103.8 ug/L1
2,6-Dinitrotoluene ND 12/10/2014 1051103.4 ug/L1
2-Chloronaphthalene ND 12/10/2014 10515.0 1.3 ug/L1
2-Chlorophenol ND 12/10/2014 10515.0 1.4 ug/L1
2-Methylnaphthalene ND 12/10/2014 10515.0 1.5 ug/L1
2-Methylphenol ND 12/10/2014 10515.0 1.1 ug/L1
2-Nitroaniline ND 12/10/2014 1051102.1 ug/L1
2-Nitrophenol ND 12/10/2014 1051102.9 ug/L1
3 & 4-Methylphenol ND 12/10/2014 1051102.7 ug/L1
3,3'-Dichlorobenzidine ND 12/10/2014 1051252.6 ug/L1
3-Nitroaniline ND 12/10/2014 1051103.0 ug/L1
4,6-Dinitro-2-methylphenol ND 12/10/2014 1051258.1 ug/L1
4-Bromophenyl phenyl ether ND 12/10/2014 10515.0 1.2 ug/L1
4-Chloro-3-methyl phenol ND 12/10/2014 10515.0 1.6 ug/L1
4-Chloroaniline ND 12/10/2014 10515.0 0.81 ug/L1
4-Chlorophenyl phenyl ether ND 12/10/2014 10515.0 1.6 ug/L1
4-Nitroaniline ND 12/10/2014 1051104.2 ug/L1
4-Nitrophenol ND 12/10/2014 1051259.0 ug/L1
Acenaphthene ND 12/10/2014 10515.0 1.2 ug/L1
Acenaphthylene ND 12/10/2014 10515.0 1.2 ug/L1
Acetophenone ND 12/10/2014 10515.0 0.90 ug/L1
Anthracene ND 12/10/2014 10515.0 1.1 ug/L1
Atrazine ND 12/10/2014 10515.0 4.2 ug/L1
Benzaldehyde ND 12/10/2014 1051253.0 ug/L1
Benzo(a)anthracene ND 12/10/2014 10515.0 0.60 ug/L1
Benzo(a)pyrene ND 12/10/2014 10515.0 0.50 ug/L1
Benzo(b)fluoranthene ND 12/10/2014 10515.0 0.60 ug/L1
Benzo(g,h,i)perylene ND 12/10/2014 10515.0 0.80 ug/L1
Benzo(k)fluoranthene ND 12/10/2014 10515.0 1.0 ug/L1
bis(2-Chloroethoxy)methane ND 12/10/2014 10515.0 1.5 ug/L1
bis(2-Chloroethyl)ether ND 12/10/2014 10515.0 1.2 ug/L1
bis(2-Chloroisopropyl)ether ND 12/10/2014 10515.0 1.3 ug/L1
bis(2-Ethylhexyl)phthalate ND 12/10/2014 10515.0 1.7 ug/L1
Butyl benzyl phthalate ND 12/10/2014 1051103.3 ug/L1
Caprolactam ND 12/10/2014 1051251.2 ug/L1
Carbazole ND 12/10/2014 10515.0 1.7 ug/L1
Chrysene ND 12/10/2014 10515.0 0.70 ug/L1
Di-n-butyl phthalate ND 12/10/2014 10515.0 1.7 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 50 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:PQ62580-001
62580 3520C
12/08/2014 1820Analytical Method:8270D
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Di-n-octylphthalate ND 12/10/2014 10515.0 1.7 ug/L1
Dibenzo(a,h)anthracene ND 12/10/2014 10515.0 1.3 ug/L1
Dibenzofuran ND 12/10/2014 10515.0 1.2 ug/L1
Diethylphthalate ND 12/10/2014 10515.0 1.9 ug/L1
Dimethyl phthalate ND 12/10/2014 10515.0 1.7 ug/L1
Fluoranthene ND 12/10/2014 10515.0 1.4 ug/L1
Fluorene ND 12/10/2014 10515.0 1.4 ug/L1
Hexachlorobenzene ND 12/10/2014 10515.0 1.2 ug/L1
Hexachlorobutadiene ND 12/10/2014 10515.0 1.4 ug/L1
Hexachlorocyclopentadiene ND 12/10/2014 1051254.0 ug/L1
Hexachloroethane ND 12/10/2014 10515.0 1.2 ug/L1
Indeno(1,2,3-c,d)pyrene ND 12/10/2014 10515.0 2.3 ug/L1
Isophorone ND 12/10/2014 10515.0 1.4 ug/L1
N-Nitrosodi-n-propylamine ND 12/10/2014 10515.0 1.4 ug/L1
N-Nitrosodiphenylamine (Diphenylamine)ND 12/10/2014 10515.0 1.0 ug/L1
Naphthalene ND 12/10/2014 10515.0 1.3 ug/L1
Nitrobenzene ND 12/10/2014 10515.0 1.6 ug/L1
Pentachlorophenol ND 12/10/2014 1051255.1 ug/L1
Phenanthrene ND 12/10/2014 10515.0 1.2 ug/L1
Phenol ND 12/10/2014 10515.0 1.2 ug/L1
Pyrene ND 12/10/2014 10515.0 3.1 ug/L1
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 87 41-144
2-Fluorobiphenyl 89 37-129
2-Fluorophenol 96 24-127
Nitrobenzene-d5 96 38-127
Phenol-d5 105 28-128
Terphenyl-d14 90 10-148
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 51 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:PQ62580-002
62580 3520C
12/08/2014 1820Analytical Method:8270D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,1'-Biphenyl 91 12/10/2014 11159110030-1301
2,4,5-Trichlorophenol 88 12/10/2014 11158810030-1301
2,4,6-Trichlorophenol 91 12/10/2014 11159110030-1301
2,4-Dichlorophenol 91 12/10/2014 11159110030-1301
2,4-Dimethylphenol 110 12/10/2014 111511210030-1301
2,4-Dinitrophenol 490 12/10/2014 11159850030-1301
2,4-Dinitrotoluene 200 12/10/2014 111510020030-1301
2,6-Dinitrotoluene 190 12/10/2014 11159520030-1301
2-Chloronaphthalene 81 12/10/2014 11158110030-1301
2-Chlorophenol 94 12/10/2014 11159410030-1301
2-Methylnaphthalene 95 12/10/2014 11159510040-1321
2-Methylphenol 95 12/10/2014 11159510030-1301
2-Nitroaniline 190 12/10/2014 11159720030-1301
2-Nitrophenol 180 12/10/2014 11159220030-1301
3 & 4-Methylphenol 200 12/10/2014 11159820030-1301
3,3'-Dichlorobenzidine 150 12/10/2014 11157720030-1301
3-Nitroaniline 180 12/10/2014 11158920030-1301
4,6-Dinitro-2-methylphenol 500 12/10/2014 111510050030-1301
4-Bromophenyl phenyl ether 87 12/10/2014 11158710030-1301
4-Chloro-3-methyl phenol 100 12/10/2014 111510010030-1301
4-Chloroaniline 36 12/10/2014 11153610010-1301
4-Chlorophenyl phenyl ether 88 12/10/2014 11158810030-1301
4-Nitroaniline 210 12/10/2014 111510520030-1301
4-Nitrophenol 560 12/10/2014 111511350030-1301
Acenaphthene 97 12/10/2014 11159710030-1301
Acenaphthylene 110 12/10/2014 111511310030-1301
Acetophenone 96 12/10/2014 11159610030-1301
Anthracene 97 12/10/2014 11159710030-1301
Atrazine 75 12/10/2014 11157510030-1301
Benzaldehyde 85 12/10/2014 11158510030-1301
Benzo(a)anthracene 88 12/10/2014 11158810030-1301
Benzo(a)pyrene 110 12/10/2014 111511310030-1301
Benzo(b)fluoranthene 120 12/10/2014 111511710030-1301
Benzo(g,h,i)perylene 100 12/10/2014 111510310030-1301
Benzo(k)fluoranthene 120 12/10/2014 111512510030-1301
bis(2-Chloroethoxy)methane 95 12/10/2014 11159510030-1301
bis(2-Chloroethyl)ether 100 12/10/2014 111510510030-1301
bis(2-Chloroisopropyl)ether 110 12/10/2014 111510810030-1301
bis(2-Ethylhexyl)phthalate 92 12/10/2014 11159210030-1301
Butyl benzyl phthalate 96 12/10/2014 11159610030-1301
Caprolactam 110 12/10/2014 111511010030-1301
Carbazole 100 12/10/2014 111510110030-1301
Chrysene 88 12/10/2014 11158810030-1301
Di-n-butyl phthalate 97 12/10/2014 11159710030-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 52 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:PQ62580-002
62580 3520C
12/08/2014 1820Analytical Method:8270D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Di-n-octylphthalate 120 12/10/2014 111511610030-1301
Dibenzo(a,h)anthracene 120 12/10/2014 111511610030-1301
Dibenzofuran 89 12/10/2014 11158910030-1301
Diethylphthalate 98 12/10/2014 11159810030-1301
Dimethyl phthalate 95 12/10/2014 11159510030-1301
Fluoranthene 91 12/10/2014 11159110030-1301
Fluorene 91 12/10/2014 11159110030-1301
Hexachlorobenzene 92 12/10/2014 11159210030-1301
Hexachlorobutadiene 88 12/10/2014 11158810030-1301
Hexachlorocyclopentadiene 430 12/10/2014 11158550030-1301
Hexachloroethane 86 12/10/2014 11158610030-1301
Indeno(1,2,3-c,d)pyrene 110 12/10/2014 111510710030-1301
Isophorone 100 12/10/2014 111510110030-1301
N-Nitrosodi-n-propylamine 110 12/10/2014 111510910030-1301
N-Nitrosodiphenylamine (Diphenylamine)110 12/10/2014 111510610018-1801
Naphthalene 85 12/10/2014 11158510030-1301
Nitrobenzene 99 12/10/2014 11159910030-1301
Pentachlorophenol 470 12/10/2014 11159350030-1301
Phenanthrene 93 12/10/2014 11159310030-1301
Phenol 96 12/10/2014 11159610030-1301
Pyrene 88 12/10/2014 11158810030-1301
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 99 41-144
2-Fluorobiphenyl 92 37-129
2-Fluorophenol 90 24-127
Nitrobenzene-d5 98 38-127
Phenol-d5 98 28-128
Terphenyl-d14 96 10-148
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 53 of 53
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1