319 SO WEST_Limited Phase II Report

LIMITED PHASE II ENVIRONMENTAL
SITE ASSESSMENT REPORT
0.28 ACRE COMMERCIAL TRACT
319 SOUTH WEST STREET
RALEIGH, NORTH CAROLINA

Mid-Atlantic Associates Job No. 000R2615.01

January 27, 2015

Prepared For: Prepared By:

Mr. Jason Widen MID-ATLANTIC ASSOCIATES, INC.
319 West, LLC
310 South Harrington Street
Raleigh, NC 27603

Wes Blaylock
Project Scientist

Daniel H. Nielsen, P.E.
Principal Engineer

TABLE OF CONTENTS

1.0 INTRODUCTION ..................................................................................................... 1

2.0 SUMMARY OF SOIL SAMPLING ACTIVITIES ....................................................... 1

3.0 SUMMARY OF LABORATORY TEST RESULTS ................................................... 2

4.0 CONCLUSIONS AND RECOMMENDATIONS ....................................................... 2

DRAWINGS

Drawing 1 Topographic Site Map
Drawing 2 Soil Boring Location Map

TABLE

Table 1 Soil Sampling Test Results

APPENDICES

Appendix A Soil Boring Logs
Appendix B Laboratory Analytical Reports and Chain-of-Custody Records

1.0 INTRODUCTION

In accordance with proposal No. P14R-7068, dated December 11, 2014, Mid-Atlantic
Associates, Inc. (Mid-Atlantic) has prepared this Limited Phase II Environmental Site
Assessment Report for the property located at 319 South West Street in Raleigh, North
Carolina (Drawing 1). This work was conducted based on the initial findings of a Phase I
Environmental Site Assessment (Mid-Atlantic’s Phase I Environmental Site Assessment
Report dated October 24, 2014), which identified recognized environmental conditions
(RECs) associated with the historical uses of the subject site including: a woodworking
shop with glue and varnish rooms; the storage of laundry and dry cleaning supplies; and
the historical presence of an oil tank on the subject site. The objective of our scope of
services was to evaluate if the conditions noted above had adversely-impacted the site.

2.0 SUMMARY OF SOIL SAMPLING ACTIVITIES

On December 31, 2014 and January 5, 2015, Mid-Atlantic mobilized to the site to
advance of six soil borings (SB-1 through SB-6, Drawing 2). Soil borings were hand-
augered by Mid-Atlantic personnel. Soil boring locations are summarized in the table
below:

Soil Boring Area of Concern
SB-1 Former varnish room
SB-2 Paint booth and approximate location of former oil tank
SB-3 Paint booth
SB-4 Approximate former location of dry-cleaning supplies storage
SB-5 Approximate former location of dry-cleaning supplies storage
SB-6 Approximate former location of dry-cleaning supplies storage

The locations of the varnish room and dry-cleaning supplies storage were identified on
the historical Sanborn fire insurance map from 1950 during Mid-Atlantic’s Phase I
Environmental Site Assessment. The location of the oil tank was identified on the 1914
Sanborn map.

Mid-Atlantic personnel used a concrete coring machine to core through the approximately
six-inch concrete floor of the on-site warehouse. A hand-auger was then used to advance
the six borings. Soil borings SB-1, SB-4, SB-5 and SB-6 were advanced to five feet below
land surface. Auger refusal, due to the presence of rocky material, was encountered at
three feet at SB-3 and four feet at SB-2. In general, the lithology (below concrete and
base course) at the site consisted of fine sandy silty clays and clayey silts. Soil boring
logs are provided in Appendix A.

Limited Phase II Environmental Site Assessment Report January 27, 2015
319 South West Street Page 2
Raleigh, North Carolina

Soil samples were collected in laboratory-supplied containers, packed into an ice-filled
cooler and transported under chain-of-custody from the subject site to Prism Laboratories,
Inc. (Prism) in Charlotte, North Carolina by Prism’s courier. The soil samples were
analyzed for volatile organic compounds (VOCs) according to EPA Method 8260 and
semi-volatile organic compounds (SVOCs) according to EPA Method 8270.

3.0 SUMMARY OF LABORATORY TEST RESULTS

The laboratory analytical reports and chain-of-custody records for the samples collected at
the site are provided in Appendix B. As summarized in Table 1, multiple chemical
constituents were detected in soil samples taken from soil borings SB-1, SB-2 and SB-4.
Constituents detected with concentrations that exceeded one or more North Carolina
Department of Environment and Natural Resources (NCDENR) Inactive Hazardous Sites
Branch (IHSB) Protection of Groundwater Preliminary Soil Remediation Goal (PSRG)
(Residential Health-Based Goal, Industrial Health-Based Goal, Protection of Groundwater
Goal) included benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene,
dibenzo(a,h)anthracene and indeno(1,2,3-cd)pyrene. These chemical constituents are
polycyclic aromatic hydrocarbons (PAHs). The compounds are common in “heavy” oils
such as motor oils and gear oils. They are also common in creosotes, charred wood,
asphalt and coal. During field sampling activities, Mid-Atlantic personnel observed a layer
of crumbled asphalt and/or clinkers (term used to describe solid waste that results from
burning fossil fuels) directly below the warehouse concrete slab floor. This layer of base
material beneath the warehouse floor may be the source of the chemical compounds listed
above. Although, there does not appear to be a correlation between the presence of
compounds exceeding PSRGs and the presence of clinkers/asphalt observed in the
borings. There does appear to be a correlation that the samples exceeding PSRGs for
PAHs were all detected in samples collected from the western portion of the site which
was developed later than the eastern portion of the site.

The dry-cleaning solvent tetrachloroethylene, also known as perchloroethylene or “perc”,
was detected in samples acquired from SB-4 and SB-6 at concentrations exceeding the
Protection of Groundwater PSRG of 0.005 milligrams per kilogram (mg/kg). The
concentrations (0.0059 and 0.0073, respectively) are likely the result of the historical
storage of dry-cleaning supplies at the subject site.

4.0 CONCLUSIONS AND RECOMMENDATIONS

Based on the results of this investigation, soil contaminants are present beneath the
subject site at concentrations above PSRGs. PAH compounds were detected in the soil
samples from SB-1, SB-2 and SB-4 above PSRGs. Benzo(a)pyrene in particular was
detected at levels exceeding the Industrial Health-Based PSRG. The detection of
Limited Phase II Environmental Site Assessment Report January 27, 2015
319 South West Street Page 3
Raleigh, North Carolina

tetrachloroethylene in samples from SB-4 and SB-6 at levels exceeding the Protection
of Groundwater PSRG indicates that an historical release of dry-cleaning chemicals
likely occurred on the subject site.

Since the data suggest that several compounds were detected in soil at concentrations
that exceed PSRGs, we recommend that this report be provided to the property owner
and that the property owner evaluate if any regulatory reporting obligations apply.

DRAWINGS
´
TOPOGRAPHIC SITE MAP0.28 ACRE COMMERCIAL TRACT319 SOUTH WEST STREETRALEIGH, NORTH CAROLINA
DRAWN BY:DATE:
ENG. CHECK:
JOB NO:
APPROVAL:
DRAFTCHECK:GIS NO:
DWG NO:
REFERENCES:SCALE:
WAKE
JOHNSTON
NASH
HARNETT
LEE
FRANKLINDURHAM
CHATHAM
ORANGE
WAYNE
WILSON
GRANVILLE
§¨¦I95
§¨¦I40
§¨¦I440
AREA SHOWNWITHIN WAKE COUNTY
JANUARY 2015
000R2615.01
02G-R2615.01-11
1. RALEIGH WEST, NC DIGITAL RASTER GRAPHIC, USGS. SCANNED FROM 1:24,000-SCALE RALEIGH WEST, NC TOPOGRAPHIC MAP, PUBLISHED 1993, USGS.2. INSET MAP DIGITAL DATA FROM 2002 NATIONAL TRANSPORTATION ATLAS, BUREAU OF TRANSPORTATION STATISTICS, WASHINGTON, D.C.3. PROPERTY BOUNDARY DATA FROM WAKE COUNTY GIS.
CONTOUR INTERVAL = 10 FEET
0 1,000 2,000500Feet
SITE
1:12,000
!U
!U
!U !U
!U
!U
´
SOIL BORING SAMPLE LOCATIONS0.28 ACRE COMMERCIAL TRACT319 SOUTH WEST STREETRALEIGH, NORTH CAROLINA
DRAWN BY:DATE:
ENG. CHECK:
JOB NO:
APPROVAL:
DRAFTCHECK:GIS NO:
DWG NO:
REFERENCES:SCALE:
JANUARY 2015
000R2615.01
02G-R2615.01-22
1. SAMPLE LOCATION ARE APPROXIMATE.2. PARCEL BOUNDARY AND ROAD DATA FROM WAKE COUNTY GIS.3. 2013 AERIAL IMAGERY FROM NC CGIA.4. MID-ATLANTIC FIELD NOTES.0 30 6015Feet1:360
SB-1
SB-2 SB-3
SB-5SB-4
SB-6

TABLE
SB
-
1

S
B
-
2

S
B
-
3

S
B
-
4

S
B
-
5

S
B
-
6
1.
0
'

-

2
.
0
'

1
.
0
'

-

2
.
0
'

2
.
0
'

-

3
.
0
'

1
.
0
'

-

2
.
0
'

2
.
0
'

-

3
.
0
'

1
.
5
'

-

2
.
5
'
12
/
3
1
/
2
0
1
4

1
/
5
/
2
0
1
5

1
2
/
3
1
/
2
0
1
4

1
2
/
3
1
/
2
0
1
4

1
2
/
3
1
/
2
0
1
4

1
2
/
3
1
/
2
0
1
4
Ac
e
n
a
p
h
t
h
e
n
e

8
2
7
0
D

0
.
1
4

J

<

0
.
4
4

<

0
.
4
3

0
.
2
3

J

<

0
.
4
6

<

0
.
5
2
70
0
9,000 8.4
An
t
h
r
a
c
e
n
e
82
7
0
D

0
.
3
5

J

0
.
1
6

J

<

0
.
4
3

0
.
5
3

<

0
.
4
6

<

0
.
5
2
3,
4
0
0
46,000 660
Be
n
z
o
(
a
)
a
n
t
h
r
a
c
e
n
e
82
7
0
D
0.
8
4

0
.
5
4
<
0
.
4
3
1.
3
<
0
.
4
6

<

0
.
5
2
0.
1
5
2.9 0.18
Be
n
z
o
(
a
)
p
y
r
e
n
e
82
7
0
D
0.
7
2

0
.
4
5
<
0
.
4
3
1.
1
<
0
.
4
6

<

0
.
5
2
0.
0
1
5
0.29 0.059
Be
n
z
o
(
b
)
f
l
u
o
r
a
n
t
h
e
n
e
82
7
0
D
0.
9
5

0
.
5
5
<
0
.
4
3
1.
5
<
0
.
4
6

<

0
.
5
2
0.
1
5
2.9 0.6
Be
n
z
o
(
g
,
h
,
i
)
p
e
r
y
l
e
n
e
82
7
0
D

0
.
4
2

J

0
.
2
7

J

<

0
.
4
3

0
.
6
7

<

0
.
4
6

<

0
.
5
2
NA
NA 7,800
Be
n
z
o
(
k
)
f
l
u
o
r
a
n
t
h
e
n
e
82
7
0
D

0
.
3
2

J

0
.
2
0

J

<

0
.
4
3

0
.
5
4

<

0
.
4
6

<

0
.
5
2
1.
5
29 5.9
Ch
r
y
s
e
n
e
82
7
0
D

0
.
8
8

0
.
4
9

0
.
1
1

J

1
.
4

<

0
.
4
6

<

0
.
5
2
15
290 18
Di
b
e
n
z
o
(
a
,
h
)
a
n
t
h
r
a
c
e
n
e
82
7
0
D
0.
1
2

J
<
0
.
4
4

<

0
.
4
3
0.
1
8

J
<
0
.
4
6

<

0
.
5
2
0.
0
1
5
0.29 0.19
Di
b
e
n
z
o
f
u
r
a
n
82
7
0
D

<

0
.
4
3

<

0
.
4
4

<

0
.
4
3

0
.
2
0

J

<

0
.
4
6

<

0
.
5
2
14
200 5.2
Fl
u
o
r
a
n
t
h
e
n
e
82
7
0
D

1
.
9
1.
1

0
.
1
7

J

3
.
1

<

0
.
4
6

<

0
.
5
2
46
0
6,000 330
Fl
u
o
r
e
n
e
82
7
0
D

0
.
1
5

J

<

0
.
4
4

<

0
.
4
3

0
.
2
1

J

<

0
.
4
6

<

0
.
5
2
46
0
6,000 56
In
d
e
n
o
(
1
,
2
,
3
-
c
d
)
p
y
r
e
n
e
82
7
0
D
0.
4
9

0
.
3
1

J
<
0
.
4
3
0.
7
8
<
0
.
4
6

<

0
.
5
2
0.
1
5
2.9 2.0
Na
p
h
t
h
a
l
e
n
e
82
7
0
D

<

0
.
4
3

<

0
.
4
4

<

0
.
4
3

0
.
1
2

J

<

0
.
4
6

<

0
.
5
2
3.
8
17 0.21
Ph
e
n
a
n
t
h
r
e
n
e
82
7
0
D

1
.
7

0
.
6
2

0
.
1
8

J

2
.
6

<

0
.
4
6

<

0
.
5
2
NA
NA 68
Py
r
e
n
e
82
7
0
D

1
.
4

0
.
9
5

0
.
1
5

J

2
.
3

<

0
.
4
6

<

0
.
5
2
34
0
4,600 220
Ac
e
t
o
n
e
82
6
0
B

0
.
0
8
6

0
.
0
3
2

J

0
.
0
2
3

J

0
.
1
8

0
.
0
2
1

J

0
.
0
3
7

J
12
,
0
0
0
100,000 24
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
82
6
0
B

<

0
.
0
0
4
1

<

0
.
0
0
5
3

0
.
0
1
2

0
.
0
0
3
0

J

<

0
.
0
0
4
7

<

0
.
0
0
6
57
640 0.023
Me
t
h
y
l

E
t
h
y
l

K
e
t
o
n
e

(
2
-
B
u
t
a
n
o
n
e
)

8
2
6
0
B

<

0
.
0
8
2

0
.
0
0
2
1

J

<

0
.
0
8
9

<

0
.
0
8
7

<

0
.
0
9
4

<

0
.
1
2
5,
4
0
0
28,000 16
Te
t
r
a
c
h
l
o
r
o
e
t
h
y
l
e
n
e
82
6
0
B

0
.
0
0
2
3

J

<

0
.
0
0
5
3

0
.
0
0
2
6

J

0
.
0
0
5
9

0
.
0
0
2
5

J

0
.
0
0
7
3
16
78 0.005
NC
D
E
N
R

I
H
S
B

=

N
o
r
t
h

C
a
r
o
l
i
n
a

D
e
p
a
r
t
m
e
n
t

o
f

E
n
v
i
o
n
m
e
n
t

a
n
d

N
a
t
u
r
a
l

R
e
s
o
u
r
c
e
s

I
n
a
c
t
i
v
e

H
a
z
a
r
d
o
u
s

S
i
t
e
s

B
r
a
n
c
h
Bo
l
d
-

C
o
n
c
e
n
t
r
a
t
i
o
n

e
x
c
e
e
d
s

R
e
s
i
d
e
n
t
i
a
l

H
e
a
l
t
h
-
B
a
s
e
d

P
S
R
G
Sh
a
d
e
d

-

C
o
n
c
e
n
t
r
a
t
i
o
n

e
x
c
e
e
d
s

P
r
o
t
e
c
t
i
o
n

o
f

G
r
o
u
n
d
w
a
t
e
r

P
S
R
G
Bo
l
d
&

S
h
a
d
e
d

-

C
o
n
c
e
n
t
r
a
t
i
o
n

e
x
c
e
e
d
s

R
e
s
i
d
e
n
t
i
a
l

H
e
a
l
t
h
-
B
a
s
e
d

a
n
d

P
r
o
t
e
c
t
i
o
n

o
f

G
r
o
u
n
d
w
a
t
e
r

P
S
R
G
s
Bo
l
d
,
S
h
a
d
e
d

w
i
t
h

D
o
u
b
l
e

B
o
r
d
e
r

-

C
o
n
c
e
n
t
r
a
t
i
o
n

e
x
c
e
e
d
s

R
e
s
i
d
e
n
t
i
a
l

H
e
a
l
t
h
-
B
a
s
e
d
,

P
r
o
t
e
c
t
i
o
n

o
f

G
r
o
u
n
d
w
a
t
e
r

a
n
d

I
n
d
u
s
t
r
i
a
l

H
e
a
l
t
h
-
B
a
s
e
d

P
S
R
G
s

CO
N
C
E
N
T
R
A
T
I
O
N

(
m
g
/
k
g
)
CH
E
M
I
C
A
L

C
O
N
S
T
I
T
U
E
N
T
AN
A
L
Y
S
I
S

ME
T
H
O
D
TA
B
L
E

1
SO
I
L

S
A
M
P
L
I
N
G

T
E
S
T

R
E
S
U
L
T
S
0.
2
8

A
C
R
E

C
O
M
M
E
R
C
I
A
L

T
R
A
C
T
31
9

S
O
U
T
H

W
E
S
T

S
T
R
E
E
T
RA
L
E
I
G
H
,

N
O
R
T
H

C
A
R
O
L
I
N
A
MI
D
-
A
T
L
A
N
T
I
C

J
O
B

N
O
.

R
2
6
1
5
.
0
1
PROTECTION OF GROUNDWATER
NC
D
E
N
R

I
H
S
B

P
R
E
L
I
M
I
N
A
R
Y

S
O
I
L

R
E
M
E
D
I
A
T
I
O
N

G
O
A
L
S

(
P
S
R
G
)

-

S
E
P
T
E
M
B
E
R

2
0
1
4
J
=

E
s
t
i
m
a
t
e
d

c
o
n
c
e
n
t
r
a
t
i
o
n

d
e
t
e
c
t
e
d

b
u
t

b
e
l
o
w

t
h
e

r
e
p
o
r
t
i
n
g

l
i
m
i
t
.
NA

=

N
o
t

A
p
p
l
i
c
a
b
l
e
mg
/
K
g

-

M
i
l
l
i
g
r
a
m
s

p
e
r

K
i
l
o
g
r
a
m
RE
S
I
D
E
N
T
I
A
L

H
E
A
L
T
H
-
BA
S
E
D
INDUSTRIAL HEALTH-BASED

APPENDIX A

SOIL BORING LOGS
ft
-
B
L
S
Odors SOIL DESCRIPTION (color, texture, moisture, etc.)Comments
NOTES:
COMMENTS:
in - indicates inches
ft - indicates depth in feet
ft BLS - indicates feet below land surface
N/A - indicates not applicable to this boring
Hand auger terminated at 5.0 feet
Sample taken from 1.0 - 2.0 feet
Reddish-brown fine sandy micaceous silty CLAY
Reddish-orange clayey micaceaus SILT
409 Rogers View Court
Raleigh, NC 27610
Ph: 1-800-486-7568
Raleigh, NC
Site Name:
Project Number:
Location:
R2615.01
Drilling/Boring Method:
12/31/2014
2
Date Completed:
4
SB-1LOG OF BORING:
G. Fischer
Longitude:
Geologist/Engineer:None
Total Boring Depth (ft):
N/A
5.0Concrete Coring Machine
1
N/A
Latitude:
N/A
Page: 1
ft
-
B
L
S
1
2
Date Started:
1
Re
c
o
v
e
r
y

(f
t
.
)
None 5
of
N/A
12/31/2014
319 S. West Street
Sampling Method:
Subcontractor/Drillers:
Monitoring Equipment:
Driller :
Top of Casing Elev. (ft):Hand Auger N/A
3
4
3
5
6" Concrete Pad with gravel beneath
5
ft
-
B
L
S
Odors SOIL DESCRIPTION (color, texture, moisture, etc.)Comments
NOTES:
COMMENTS:
in - indicates inches
ft - indicates depth in feet
ft BLS - indicates feet below land surface
N/A - indicates not applicable to this boring
SB-2LOG OF BORING:
G. Fischer
Longitude:
Geologist/Engineer:None
Total Boring Depth (ft):
N/A
N/A
1
N/A
Latitude:
Page: 1 of
Date Started:
Top of Casing Elev. (ft):
Concrete Coring Machine
Hand Auger
N/A
319 S. West Street
Sampling Method:
Subcontractor/Drillers:
R2615.01
1/5/2015
409 Rogers View Court
Raleigh, NC 27610
Ph: 1-800-486-7568
Raleigh, NC
4.0
Monitoring Equipment:
Driller :
Hand auger terminated at 4.0 feet
2
3
4
1
N/A
Date Completed:
1
1/5/2015
Site Name:
Project Number:
Location:
Drilling/Boring Method:
2
3
Sample taken from 1.0 - 2.0 feet
4
ft
-
B
L
S
Re
c
o
v
e
r
y

(f
t
.
)
None 4
6" Concrete Pad with gravel beneath
Brown fine sandy micaceous silty CLAY
ft
-
B
L
S
Odors SOIL DESCRIPTION (color, texture, moisture, etc.)Comments
NOTES:
COMMENTS:
in - indicates inches
ft - indicates depth in feet
ft BLS - indicates feet below land surface
N/A - indicates not applicable to this boring
Hand auger terminated at 3.0 feet
Sample taken from 2.0 - 3.0 feet
3
Light brown fine sandy SILT with gravel
Reddish-brown fine sandy micacaceous silty CLAY
1
Top of Casing Elev. (ft):Hand Auger
N/A
Latitude:
N/A
Monitoring Equipment:
Driller :
2
ft
-
B
L
S
Date Started: 1/5/2015
Re
c
o
v
e
r
y

(f
t
.
)
None 3
6" Concrete Pad with gravel/clinkers beneath
2
3
Date Completed:
1
1/5/2015
SB-3LOG OF BORING:
G. Fischer
Longitude:
Geologist/Engineer:None
Total Boring Depth (ft):
N/A
N/A
1 of
N/A
3.0Concrete Coring Machine
1Page:
409 Rogers View Court
Raleigh, NC 27610
Ph: 1-800-486-7568
Raleigh, NC
Site Name:
Project Number:
Location:
Drilling/Boring Method:
R2615.01
319 S. West Street
Sampling Method:
Subcontractor/Drillers:
ft
-
B
L
S
Odors SOIL DESCRIPTION (color, texture, moisture, etc.)Comments
NOTES:
COMMENTS:
in - indicates inches
ft - indicates depth in feet
ft BLS - indicates feet below land surface
N/A - indicates not applicable to this boring
4
5
319 S. West Street
Sampling Method:
Subcontractor/Drillers:
R2615.01
Drilling/Boring Method:
Re
c
o
v
e
r
y

(f
t
.
)
6" Concrete Pad with gravel beneath
5
Reddish-brown fine sandy micaceous silty CLAY
3
ft
-
B
L
S
1
2
1
N/A
SB-4
Page: 1 of
N/A
5.0Concrete Coring Machine
Hand Auger N/A
Latitude:
N/A
Top of Casing Elev. (ft):
G. Fischer
Longitude:
Geologist/Engineer:None
Total Boring Depth (ft):
N/A
LOG OF BORING:
Date Completed:
1
2
4
None
Hand auger terminated at 5.0 feet
Sample taken from 1.0 - 2.0 feet
409 Rogers View Court
Raleigh, NC 27610
Ph: 1-800-486-7568
Raleigh, NC
Site Name:
Project Number:
Location:
3
12/31/2014
12/31/2014Date Started:
Monitoring Equipment:
Driller :
5
ft
-
B
L
S
Odors SOIL DESCRIPTION (color, texture, moisture, etc.)Comments
NOTES:
COMMENTS:
in - indicates inches
ft - indicates depth in feet
ft BLS - indicates feet below land surface
N/A - indicates not applicable to this boring
5.0
409 Rogers View Court
Raleigh, NC 27610
Ph: 1-800-486-7568
LOG OF BORING: SB-5
Page: 1 of 1
Site Name: 319 S. West Street Drilling/Boring Method:Concrete Coring Machine Total Boring Depth (ft):
N/A
Project Number:R2615.01 Sampling Method:Hand Auger Top of Casing Elev. (ft):N/A
Location: Raleigh, NC Subcontractor/Drillers: N/A Latitude:
G. Fischer
Date Started:12/31/2014 Driller :N/A Longitude:N/A
Date Completed:12/31/2014 Monitoring Equipment:None Geologist/Engineer:
ft
-
B
L
S
Re
c
o
v
e
r
y

(f
t
.
)
None 5
6" Concrete Pad with clinkers/ground asphalt beneath
Reddish-brown fine sandy micaceous silty CLAY
1 1
2 2
3 3
4 4
5
Hand auger terminated at 5.0 feet
Sample taken from 2.0 - 3.0 feet
5
ft
-
B
L
S
Odors SOIL DESCRIPTION (color, texture, moisture, etc.)Comments
NOTES:
COMMENTS:
in - indicates inches
ft - indicates depth in feet
ft BLS - indicates feet below land surface
N/A - indicates not applicable to this boring
Sample taken from 1.5 - 2.5 feet
1 1
2 2
3 3
4 4
5 5
Hand auger terminated at 5.0 feet
Re
c
o
v
e
r
y

(f
t
.
)
ft
-
B
L
S
None 5
6" Concrete Pad with clinkers/ground asphalt beneath
Reddish-brown fine sandy micaceous silty CLAY
G. Fischer
Date Started:12/31/2014 Driller :N/A Longitude:N/A
Date Completed:12/31/2014 Monitoring Equipment:None Geologist/Engineer:
N/A
Project Number:R2615.01 Sampling Method:Hand Auger Top of Casing Elev. (ft):N/A
Location: Raleigh, NC Subcontractor/Drillers: N/A Latitude:
5.0
409 Rogers View Court
Raleigh, NC 27610
Ph: 1-800-486-7568
LOG OF BORING: SB-6
Page: 1 of 1
Site Name: 319 S. West Street Drilling/Boring Method:Concrete Coring Machine Total Boring Depth (ft):

APPENDIX B

LABORATORY ANALYTICAL REPORTS AND
CHAIN-OF-CUSTODY RECORDS
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
01/13/2015
Mid-Atlantic Associates, Inc. - Raleigh
Wes Blaylock
409 Rogers View Court
Raleigh, NC 27610
Project: Phase II 319 S. West Street
Lab Submittal Date: 01/06/2015
Prism Work Order: 5010035
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
Data Qualifiers Key Reference:
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 19
Sample Receipt Summary
01/13/2015
Prism Work Order: 5010035
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
5010035-01 01/05/15SB-2 (1-2)01/06/15Solid
Samples were received in good condition at 0.5 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 19
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5010035
01/13/2015
Summary of Detections
0.16 J mg/kg dry5010035-01 SB-2 (1-2)Anthracene 8270D
0.54 mg/kg dry5010035-01 SB-2 (1-2)Benzo(a)anthracene 8270D
0.45 mg/kg dry5010035-01 SB-2 (1-2)Benzo(a)pyrene 8270D
0.55 mg/kg dry5010035-01 SB-2 (1-2)Benzo(b)fluoranthene 8270D
0.27 J mg/kg dry5010035-01 SB-2 (1-2)Benzo(g,h,i)perylene 8270D
0.20 J mg/kg dry5010035-01 SB-2 (1-2)Benzo(k)fluoranthene 8270D
0.49 mg/kg dry5010035-01 SB-2 (1-2)Chrysene 8270D
1.1 mg/kg dry5010035-01 SB-2 (1-2)Fluoranthene 8270D
0.31 J mg/kg dry5010035-01 SB-2 (1-2)Indeno(1,2,3-cd)pyrene 8270D
0.62 mg/kg dry5010035-01 SB-2 (1-2)Phenanthrene 8270D
0.95 mg/kg dry5010035-01 SB-2 (1-2)Pyrene 8270D
0.032 J mg/kg dry5010035-01 SB-2 (1-2)Acetone 8260B
0.0021 J mg/kg dry5010035-01 SB-2 (1-2)Methyl Ethyl Ketone (2-Butanone)8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 19
Laboratory Report
01/13/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-2 (1-2)
Prism Sample ID: 5010035-01
Prism Work Order: 5010035
Time Collected: 01/05/15 11:30
Time Submitted: 01/06/15 08:30
General Chemistry Parameters
75.5 *SM2540 G P5A007110.100 1/7/15 16:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0681,2,4-Trichlorobenzene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0661,2-Dichlorobenzene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0621,3-Dichlorobenzene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0641,4-Dichlorobenzene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0841-Methylnaphthalene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0822,4,6-Trichlorophenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0842,4-Dichlorophenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0672,4-Dimethylphenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0612,4-Dinitrophenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0532,4-Dinitrotoluene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0582,6-Dinitrotoluene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0632-Chloronaphthalene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0622-Chlorophenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0702-Methylnaphthalene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0562-Methylphenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0802-Nitrophenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0863,3'-Dichlorobenzidine
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0543/4-Methylphenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0664,6-Dinitro-2-methylphenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0754-Bromophenyl phenyl ether
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0614-Chloro-3-methylphenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0534-Chloroaniline
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0574-Chlorophenyl phenyl ether
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.0674-Nitrophenol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.059Acenaphthene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.063Acenaphthylene
0.16 8270D P5A006210.44 1/8/15 16:04 KCJmg/kg dry 0.070Anthracene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.058Azobenzene
0.54 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.057Benzo(a)anthracene
0.45 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.047Benzo(a)pyrene
0.55 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.051Benzo(b)fluoranthene
0.27 8270D P5A006210.44 1/8/15 16:04 KCJmg/kg dry 0.048Benzo(g,h,i)perylene
0.20 8270D P5A006210.44 1/8/15 16:04 KCJmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.037Benzoic Acid
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.058Benzyl alcohol
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.076bis(2-Chloroethoxy)methane
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.062Bis(2-Chloroethyl)ether
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.075Bis(2-chloroisopropyl)ether
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.065Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 19
Laboratory Report
01/13/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-2 (1-2)
Prism Sample ID: 5010035-01
Prism Work Order: 5010035
Time Collected: 01/05/15 11:30
Time Submitted: 01/06/15 08:30
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.062Butyl benzyl phthalate
0.49 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.055Chrysene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.053Dibenzo(a,h)anthracene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.066Dibenzofuran
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.060Diethyl phthalate
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.058Dimethyl phthalate
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.062Di-n-butyl phthalate
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.054Di-n-octyl phthalate
1.1 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.056Fluoranthene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.063Fluorene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.069Hexachlorobenzene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.079Hexachlorobutadiene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.078Hexachlorocyclopentadiene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.073Hexachloroethane
0.31 8270D P5A006210.44 1/8/15 16:04 KCJmg/kg dry 0.050Indeno(1,2,3-cd)pyrene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.059Isophorone
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.070Naphthalene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.062Nitrobenzene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.069N-Nitroso-di-n-propylamine
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.066N-Nitrosodiphenylamine
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.052Pentachlorophenol
0.62 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.057Phenanthrene
BRL 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.064Phenol
0.95 8270D P5A006210.44 1/8/15 16:04 KCmg/kg dry 0.058Pyrene
Surrogate Recovery Control Limits
39-132105 %2,4,6-Tribromophenol
44-11596 %2-Fluorobiphenyl
35-11588 %2-Fluorophenol
37-12288 %Nitrobenzene-d5
34-12183 %Phenol-d5
54-127107 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000321,1,1,2-Tetrachloroethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000171,1,1-Trichloroethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000871,1,2,2-Tetrachloroethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000441,1,2-Trichloroethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000441,1-Dichloroethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000321,1-Dichloroethylene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000551,1-Dichloropropylene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000791,2,3-Trichloropropane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000311,2,4-Trichlorobenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00101,2,4-Trimethylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 19
Laboratory Report
01/13/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-2 (1-2)
Prism Sample ID: 5010035-01
Prism Work Order: 5010035
Time Collected: 01/05/15 11:30
Time Submitted: 01/06/15 08:30
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000611,2-Dibromoethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000241,2-Dichlorobenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000851,2-Dichloroethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000331,2-Dichloropropane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000251,3,5-Trimethylbenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.0000731,3-Dichlorobenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000571,3-Dichloropropane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000391,4-Dichlorobenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000254-Chlorotoluene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.000334-Isopropyltoluene
0.032 8260B P5A006110.053 1/7/15 12:45 MSCJmg/kg dry 0.0028Acetone
BRL 8260B P5A006110.0032 1/7/15 12:45 MSCmg/kg dry 0.00032Benzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00022Bromobenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00077Bromochloromethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00024Bromodichloromethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00093Bromoform
BRL 8260B P5A006110.011 1/7/15 12:45 MSCmg/kg dry 0.0015Bromomethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00029Carbon Tetrachloride
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00025Chlorobenzene
BRL 8260B P5A006110.011 1/7/15 12:45 MSCmg/kg dry 0.0040Chloroethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00022Chloroform
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.0027Chloromethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00043cis-1,2-Dichloroethylene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00026cis-1,3-Dichloropropylene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00036Dibromochloromethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00056Dichlorodifluoromethane
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00034Ethylbenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00026Isopropylbenzene (Cumene)
BRL 8260B P5A006110.011 1/7/15 12:45 MSCmg/kg dry 0.00068m,p-Xylenes
BRL 8260B P5A006110.053 1/7/15 12:45 MSCmg/kg dry 0.0011Methyl Butyl Ketone (2-Hexanone)
0.0021 8260B P5A006110.11 1/7/15 12:45 MSCJmg/kg dry 0.0019Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5A006110.053 1/7/15 12:45 MSCmg/kg dry 0.0014Methyl Isobutyl Ketone
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00038Methylene Chloride
BRL 8260B P5A006110.011 1/7/15 12:45 MSCmg/kg dry 0.00040Methyl-tert-Butyl Ether
BRL 8260B P5A006110.011 1/7/15 12:45 MSCmg/kg dry 0.00039Naphthalene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00023n-Butylbenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00030n-Propylbenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00033o-Xylene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00021sec-Butylbenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00023Styrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 19
Laboratory Report
01/13/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-2 (1-2)
Prism Sample ID: 5010035-01
Prism Work Order: 5010035
Time Collected: 01/05/15 11:30
Time Submitted: 01/06/15 08:30
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00027tert-Butylbenzene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00037Tetrachloroethylene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00031Toluene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00061trans-1,2-Dichloroethylene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00025trans-1,3-Dichloropropylene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00049Trichloroethylene
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00043Trichlorofluoromethane
BRL 8260B P5A006110.026 1/7/15 12:45 MSCmg/kg dry 0.0015Vinyl acetate
BRL 8260B P5A006110.0053 1/7/15 12:45 MSCmg/kg dry 0.00068Vinyl chloride
BRL 8260B P5A006110.016 1/7/15 12:45 MSCmg/kg dry 0.00099Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-129101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0061 - 5035
Blank (P5A0061-BLK1)Prepared & Analyzed: 01/07/15
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0061 - 5035
Blank (P5A0061-BLK1)Prepared & Analyzed: 01/07/15
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 980.0491
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 990.0494
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 1010.0507
LCS (P5A0061-BS1)Prepared & Analyzed: 01/07/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0530 0.0050 0.05000 72-115106
1,1,1-Trichloroethane mg/kg wet0.0492 0.0050 0.05000 67-13198
1,1,2,2-Tetrachloroethane mg/kg wet0.0545 0.0050 0.05000 56-126109
1,1,2-Trichloroethane mg/kg wet0.0521 0.0050 0.05000 70-133104
1,1-Dichloroethane mg/kg wet0.0488 0.0050 0.05000 74-12797
1,1-Dichloroethylene mg/kg wet0.0466 0.0050 0.05000 67-14993
1,1-Dichloropropylene mg/kg wet0.0490 0.0050 0.05000 71-13098
1,2,3-Trichlorobenzene mg/kg wet0.0541 0.0050 0.05000 68-130108
1,2,3-Trichloropropane mg/kg wet0.0508 0.0050 0.05000 60-137102
1,2,4-Trichlorobenzene mg/kg wet0.0524 0.0050 0.05000 66-125105
1,2,4-Trimethylbenzene mg/kg wet0.0531 0.0050 0.05000 69-129106
1,2-Dibromoethane mg/kg wet0.0527 0.0050 0.05000 70-132105
1,2-Dichlorobenzene mg/kg wet0.0516 0.0050 0.05000 72-123103
1,2-Dichloroethane mg/kg wet0.0493 0.0050 0.05000 68-12899
1,2-Dichloropropane mg/kg wet0.0486 0.0050 0.05000 73-13097
1,3,5-Trimethylbenzene mg/kg wet0.0523 0.0050 0.05000 69-128105
1,3-Dichlorobenzene mg/kg wet0.0502 0.0050 0.05000 71-120100
1,3-Dichloropropane mg/kg wet0.0509 0.0050 0.05000 75-124102
1,4-Dichlorobenzene mg/kg wet0.0511 0.0050 0.05000 71-123102
2,2-Dichloropropane mg/kg wet0.0491 0.0050 0.05000 50-14298
2-Chlorotoluene mg/kg wet0.0514 0.0050 0.05000 67-124103
4-Chlorotoluene mg/kg wet0.0521 0.0050 0.05000 71-126104
4-Isopropyltoluene mg/kg wet0.0525 0.0050 0.05000 68-129105
Acetone mg/kg wet0.102 0.050 0.1000 29-198102
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0061 - 5035
LCS (P5A0061-BS1)Prepared & Analyzed: 01/07/15
Benzene mg/kg wet0.0504 0.0030 0.05000 74-127101
Bromobenzene mg/kg wet0.0518 0.0050 0.05000 73-125104
Bromochloromethane mg/kg wet0.0502 0.0050 0.05000 72-134100
Bromodichloromethane mg/kg wet0.0518 0.0050 0.05000 75-122104
Bromoform mg/kg wet0.0560 0.0050 0.05000 66-135112
Bromomethane mg/kg wet0.0508 0.010 0.05000 20-180102
Carbon Tetrachloride mg/kg wet0.0514 0.0050 0.05000 64-143103
Chlorobenzene mg/kg wet0.0509 0.0050 0.05000 74-118102
Chloroethane mg/kg wet0.0515 0.010 0.05000 33-149103
Chloroform mg/kg wet0.0493 0.0050 0.05000 73-12799
Chloromethane mg/kg wet0.0497 0.0050 0.05000 45-14399
cis-1,2-Dichloroethylene mg/kg wet0.0505 0.0050 0.05000 76-134101
cis-1,3-Dichloropropylene mg/kg wet0.0496 0.0050 0.05000 71-12599
Dibromochloromethane mg/kg wet0.0551 0.0050 0.05000 73-122110
Dichlorodifluoromethane mg/kg wet0.0471 0.0050 0.05000 26-14694
Ethylbenzene mg/kg wet0.0513 0.0050 0.05000 74-128103
Isopropyl Ether mg/kg wet0.0480 0.0050 0.05000 59-15996
Isopropylbenzene (Cumene)mg/kg wet0.0515 0.0050 0.05000 68-126103
m,p-Xylenes mg/kg wet0.102 0.010 0.1000 75-124102
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0600 0.050 0.05000 61-157120
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0543 0.10 0.05000 J63-149109
Methyl Isobutyl Ketone mg/kg wet0.0547 0.050 0.05000 57-162109
Methylene Chloride mg/kg wet0.0465 0.0050 0.05000 74-12993
Methyl-tert-Butyl Ether mg/kg wet0.0540 0.010 0.05000 70-130108
Naphthalene mg/kg wet0.0558 0.010 0.05000 57-157112
n-Butylbenzene mg/kg wet0.0538 0.0050 0.05000 65-135108
n-Propylbenzene mg/kg wet0.0506 0.0050 0.05000 67-130101
o-Xylene mg/kg wet0.0500 0.0050 0.05000 74-126100
sec-Butylbenzene mg/kg wet0.0515 0.0050 0.05000 66-131103
Styrene mg/kg wet0.0556 0.0050 0.05000 77-121111
tert-Butylbenzene mg/kg wet0.0504 0.0050 0.05000 67-132101
Tetrachloroethylene mg/kg wet0.0507 0.0050 0.05000 68-130101
Toluene mg/kg wet0.0504 0.0050 0.05000 71-129101
trans-1,2-Dichloroethylene mg/kg wet0.0483 0.0050 0.05000 73-13297
trans-1,3-Dichloropropylene mg/kg wet0.0519 0.0050 0.05000 68-123104
Trichloroethylene mg/kg wet0.0496 0.0050 0.05000 75-13399
Trichlorofluoromethane mg/kg wet0.0590 0.0050 0.05000 44-146118
Vinyl acetate mg/kg wet0.0608 0.025 0.05000 85-161122
Vinyl chloride mg/kg wet0.0520 0.0050 0.05000 48-147104
Xylenes, total mg/kg wet0.152 0.015 0.1500 74-126102
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1010.0503
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 1000.0498
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 1020.0509
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0061 - 5035
LCS Dup (P5A0061-BSD1)Prepared & Analyzed: 01/07/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0510 0.0050 0.05000 2072-115102 4
1,1,1-Trichloroethane mg/kg wet0.0456 0.0050 0.05000 2067-13191 7
1,1,2,2-Tetrachloroethane mg/kg wet0.0532 0.0050 0.05000 2056-126106 2
1,1,2-Trichloroethane mg/kg wet0.0514 0.0050 0.05000 2070-133103 1
1,1-Dichloroethane mg/kg wet0.0470 0.0050 0.05000 2074-12794 4
1,1-Dichloroethylene mg/kg wet0.0435 0.0050 0.05000 2067-14987 7
1,1-Dichloropropylene mg/kg wet0.0458 0.0050 0.05000 2071-13092 7
1,2,3-Trichlorobenzene mg/kg wet0.0534 0.0050 0.05000 2068-130107 1
1,2,3-Trichloropropane mg/kg wet0.0515 0.0050 0.05000 2060-137103 1
1,2,4-Trichlorobenzene mg/kg wet0.0505 0.0050 0.05000 2066-125101 4
1,2,4-Trimethylbenzene mg/kg wet0.0509 0.0050 0.05000 2069-129102 4
1,2-Dibromoethane mg/kg wet0.0512 0.0050 0.05000 2070-132102 3
1,2-Dichlorobenzene mg/kg wet0.0499 0.0050 0.05000 2072-123100 3
1,2-Dichloroethane mg/kg wet0.0479 0.0050 0.05000 2068-12896 3
1,2-Dichloropropane mg/kg wet0.0471 0.0050 0.05000 2073-13094 3
1,3,5-Trimethylbenzene mg/kg wet0.0494 0.0050 0.05000 2069-12899 6
1,3-Dichlorobenzene mg/kg wet0.0483 0.0050 0.05000 2071-12097 4
1,3-Dichloropropane mg/kg wet0.0500 0.0050 0.05000 2075-124100 2
1,4-Dichlorobenzene mg/kg wet0.0488 0.0050 0.05000 2071-12397 5
2,2-Dichloropropane mg/kg wet0.0469 0.0050 0.05000 2050-14294 5
2-Chlorotoluene mg/kg wet0.0487 0.0050 0.05000 2067-12497 5
4-Chlorotoluene mg/kg wet0.0494 0.0050 0.05000 2071-12699 5
4-Isopropyltoluene mg/kg wet0.0496 0.0050 0.05000 2068-12999 6
Acetone mg/kg wet0.0976 0.050 0.1000 2029-19898 4
Benzene mg/kg wet0.0487 0.0030 0.05000 2074-12797 3
Bromobenzene mg/kg wet0.0504 0.0050 0.05000 2073-125101 3
Bromochloromethane mg/kg wet0.0485 0.0050 0.05000 2072-13497 3
Bromodichloromethane mg/kg wet0.0493 0.0050 0.05000 2075-12299 5
Bromoform mg/kg wet0.0548 0.0050 0.05000 2066-135110 2
Bromomethane mg/kg wet0.0490 0.010 0.05000 2020-18098 4
Carbon Tetrachloride mg/kg wet0.0479 0.0050 0.05000 2064-14396 7
Chlorobenzene mg/kg wet0.0495 0.0050 0.05000 2074-11899 3
Chloroethane mg/kg wet0.0501 0.010 0.05000 2033-149100 3
Chloroform mg/kg wet0.0475 0.0050 0.05000 2073-12795 4
Chloromethane mg/kg wet0.0470 0.0050 0.05000 2045-14394 6
cis-1,2-Dichloroethylene mg/kg wet0.0485 0.0050 0.05000 2076-13497 4
cis-1,3-Dichloropropylene mg/kg wet0.0481 0.0050 0.05000 2071-12596 3
Dibromochloromethane mg/kg wet0.0544 0.0050 0.05000 2073-122109 1
Dichlorodifluoromethane mg/kg wet0.0431 0.0050 0.05000 2026-14686 9
Ethylbenzene mg/kg wet0.0483 0.0050 0.05000 2074-12897 6
Isopropyl Ether mg/kg wet0.0465 0.0050 0.05000 2059-15993 3
Isopropylbenzene (Cumene)mg/kg wet0.0494 0.0050 0.05000 2068-12699 4
m,p-Xylenes mg/kg wet0.0974 0.010 0.1000 2075-12497 5
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0586 0.050 0.05000 2061-157117 2
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0518 0.10 0.05000 20 J63-149104 5
Methyl Isobutyl Ketone mg/kg wet0.0534 0.050 0.05000 2057-162107 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0061 - 5035
LCS Dup (P5A0061-BSD1)Prepared & Analyzed: 01/07/15
Methylene Chloride mg/kg wet0.0454 0.0050 0.05000 2074-12991 2
Methyl-tert-Butyl Ether mg/kg wet0.0530 0.010 0.05000 2070-130106 2
Naphthalene mg/kg wet0.0562 0.010 0.05000 2057-157112 0.6
n-Butylbenzene mg/kg wet0.0502 0.0050 0.05000 2065-135100 7
n-Propylbenzene mg/kg wet0.0484 0.0050 0.05000 2067-13097 5
o-Xylene mg/kg wet0.0476 0.0050 0.05000 2074-12695 5
sec-Butylbenzene mg/kg wet0.0484 0.0050 0.05000 2066-13197 6
Styrene mg/kg wet0.0525 0.0050 0.05000 2077-121105 6
tert-Butylbenzene mg/kg wet0.0476 0.0050 0.05000 2067-13295 6
Tetrachloroethylene mg/kg wet0.0472 0.0050 0.05000 2068-13094 7
Toluene mg/kg wet0.0480 0.0050 0.05000 2071-12996 5
trans-1,2-Dichloroethylene mg/kg wet0.0461 0.0050 0.05000 2073-13292 5
trans-1,3-Dichloropropylene mg/kg wet0.0502 0.0050 0.05000 2068-123100 3
Trichloroethylene mg/kg wet0.0468 0.0050 0.05000 2075-13394 6
Trichlorofluoromethane mg/kg wet0.0539 0.0050 0.05000 2044-146108 9
Vinyl acetate mg/kg wet0.0598 0.025 0.05000 2085-161120 2
Vinyl chloride mg/kg wet0.0476 0.0050 0.05000 2048-14795 9
Xylenes, total mg/kg wet0.145 0.015 0.1500 2074-12697 5
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1040.0521
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 1040.0520
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 1060.0528
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5A0062 - 3546
Blank (P5A0062-BLK1)Prepared: 01/07/15 Analyzed: 01/08/15
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3'-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5A0062 - 3546
Blank (P5A0062-BLK1)Prepared: 01/07/15 Analyzed: 01/08/15
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.327 39-132Surrogate: 2,4,6-Tribromophenol 983.26
mg/kg wet 1.663 44-115Surrogate: 2-Fluorobiphenyl 891.48
mg/kg wet 3.327 35-115Surrogate: 2-Fluorophenol 892.95
mg/kg wet 1.663 37-122Surrogate: Nitrobenzene-d5 841.39
mg/kg wet 3.327 34-121Surrogate: Phenol-d5 842.80
mg/kg wet 1.663 54-127Surrogate: Terphenyl-d14 1091.81
LCS (P5A0062-BS1)Prepared: 01/07/15 Analyzed: 01/08/15
1,2,4-Trichlorobenzene mg/kg wet1.39 0.33 1.662 34-11884
1,2-Dichlorobenzene mg/kg wet1.30 0.33 1.662 33-11778
1,3-Dichlorobenzene mg/kg wet1.27 0.33 1.662 30-11576
1,4-Dichlorobenzene mg/kg wet1.26 0.33 1.662 31-11576
1-Methylnaphthalene mg/kg wet1.49 0.33 1.662 40-11990
2,4,6-Trichlorophenol mg/kg wet1.57 0.33 1.662 39-12694
2,4-Dichlorophenol mg/kg wet1.52 0.33 1.662 40-12292
2,4-Dimethylphenol mg/kg wet1.53 0.33 1.662 30-12792
2,4-Dinitrophenol mg/kg wet1.60 0.33 1.662 27-12996
2,4-Dinitrotoluene mg/kg wet1.54 0.33 1.662 48-12693
2,6-Dinitrotoluene mg/kg wet1.49 0.33 1.662 46-12490
2-Chloronaphthalene mg/kg wet2.06 0.33 1.662 L141-114124
2-Chlorophenol mg/kg wet1.37 0.33 1.662 34-12182
2-Methylnaphthalene mg/kg wet1.41 0.33 1.662 38-12285
2-Methylphenol mg/kg wet1.45 0.33 1.662 32-12287
2-Nitrophenol mg/kg wet1.42 0.33 1.662 36-12385
3,3'-Dichlorobenzidine mg/kg wet1.10 0.33 1.662 22-12166
3/4-Methylphenol mg/kg wet1.49 0.33 1.662 34-11989
4,6-Dinitro-2-methylphenol mg/kg wet1.79 0.33 1.662 29-132107
4-Bromophenyl phenyl ether mg/kg wet1.42 0.33 1.662 46-12485
4-Chloro-3-methylphenol mg/kg wet1.60 0.33 1.662 45-12296
4-Chloroaniline mg/kg wet1.19 0.33 1.662 17-10672
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5A0062 - 3546
LCS (P5A0062-BS1)Prepared: 01/07/15 Analyzed: 01/08/15
4-Chlorophenyl phenyl ether mg/kg wet1.43 0.33 1.662 45-12186
4-Nitrophenol mg/kg wet1.71 0.33 1.662 30-132103
Acenaphthene mg/kg wet1.50 0.33 1.662 40-12390
Acenaphthylene mg/kg wet1.49 0.33 1.662 32-13290
Anthracene mg/kg wet1.56 0.33 1.662 47-12394
Azobenzene mg/kg wet1.49 0.33 1.662 39-12590
Benzo(a)anthracene mg/kg wet1.62 0.33 1.662 49-12697
Benzo(a)pyrene mg/kg wet1.63 0.33 1.662 45-12998
Benzo(b)fluoranthene mg/kg wet1.58 0.33 1.662 45-13295
Benzo(g,h,i)perylene mg/kg wet1.58 0.33 1.662 43-13495
Benzo(k)fluoranthene mg/kg wet1.61 0.33 1.662 47-13297
Benzoic Acid mg/kg wet1.39 0.33 1.662 L110-8384
Benzyl alcohol mg/kg wet1.24 0.33 1.662 29-12274
bis(2-Chloroethoxy)methane mg/kg wet1.28 0.33 1.662 36-12177
Bis(2-Chloroethyl)ether mg/kg wet1.15 0.33 1.662 31-12069
Bis(2-chloroisopropyl)ether mg/kg wet1.16 0.33 1.662 33-13170
Bis(2-Ethylhexyl)phthalate mg/kg wet1.54 0.33 1.662 51-13392
Butyl benzyl phthalate mg/kg wet1.52 0.33 1.662 48-13292
Chrysene mg/kg wet1.58 0.33 1.662 50-12495
Dibenzo(a,h)anthracene mg/kg wet1.61 0.33 1.662 45-13497
Dibenzofuran mg/kg wet1.48 0.33 1.662 44-12089
Diethyl phthalate mg/kg wet1.57 0.33 1.662 50-12494
Dimethyl phthalate mg/kg wet1.57 0.33 1.662 48-12495
Di-n-butyl phthalate mg/kg wet1.56 0.33 1.662 51-12894
Di-n-octyl phthalate mg/kg wet1.51 0.33 1.662 45-14091
Fluoranthene mg/kg wet1.59 0.33 1.662 50-12795
Fluorene mg/kg wet1.55 0.33 1.662 43-12593
Hexachlorobenzene mg/kg wet1.62 0.33 1.662 45-12297
Hexachlorobutadiene mg/kg wet1.41 0.33 1.662 32-12385
Hexachlorocyclopentadiene mg/kg wet1.71 0.33 1.662 32-117103
Hexachloroethane mg/kg wet1.32 0.33 1.662 28-11779
Indeno(1,2,3-cd)pyrene mg/kg wet1.67 0.33 1.662 45-133100
Isophorone mg/kg wet1.44 0.33 1.662 30-12286
Naphthalene mg/kg wet1.36 0.33 1.662 35-12382
Nitrobenzene mg/kg wet1.29 0.33 1.662 34-12277
N-Nitroso-di-n-propylamine mg/kg wet1.41 0.33 1.662 36-12085
N-Nitrosodiphenylamine mg/kg wet1.50 0.33 1.662 38-12790
Pentachlorophenol mg/kg wet1.47 0.33 1.662 25-13389
Phenanthrene mg/kg wet1.51 0.33 1.662 50-12191
Phenol mg/kg wet1.40 0.33 1.662 34-12184
Pyrene mg/kg wet1.57 0.33 1.662 47-12794
mg/kg wet 3.324 39-132Surrogate: 2,4,6-Tribromophenol 963.19
mg/kg wet 1.662 44-115Surrogate: 2-Fluorobiphenyl 891.47
mg/kg wet 3.324 35-115Surrogate: 2-Fluorophenol 852.83
mg/kg wet 1.662 37-122Surrogate: Nitrobenzene-d5 821.37
mg/kg wet 3.324 34-121Surrogate: Phenol-d5 822.72
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5A0062 - 3546
LCS (P5A0062-BS1)Prepared: 01/07/15 Analyzed: 01/08/15
mg/kg wet 1.662 54-127Surrogate: Terphenyl-d14 1011.67
LCS Dup (P5A0062-BSD1)Prepared: 01/07/15 Analyzed: 01/08/15
1,2,4-Trichlorobenzene mg/kg wet1.31 0.33 1.666 2034-11878 7
1,2-Dichlorobenzene mg/kg wet1.23 0.33 1.666 2033-11774 5
1,3-Dichlorobenzene mg/kg wet1.20 0.33 1.666 2030-11572 6
1,4-Dichlorobenzene mg/kg wet1.19 0.33 1.666 2031-11572 5
1-Methylnaphthalene mg/kg wet1.38 0.33 1.666 2040-11983 7
2,4,6-Trichlorophenol mg/kg wet1.46 0.33 1.666 2039-12687 7
2,4-Dichlorophenol mg/kg wet1.40 0.33 1.666 2040-12284 8
2,4-Dimethylphenol mg/kg wet1.41 0.33 1.666 2030-12785 8
2,4-Dinitrophenol mg/kg wet1.55 0.33 1.666 2027-12993 3
2,4-Dinitrotoluene mg/kg wet1.46 0.33 1.666 2048-12688 5
2,6-Dinitrotoluene mg/kg wet1.41 0.33 1.666 2046-12484 6
2-Chloronaphthalene mg/kg wet1.84 0.33 1.666 2041-114111 11
2-Chlorophenol mg/kg wet1.28 0.33 1.666 2034-12177 7
2-Methylnaphthalene mg/kg wet1.31 0.33 1.666 2038-12279 7
2-Methylphenol mg/kg wet1.30 0.33 1.666 2032-12278 11
2-Nitrophenol mg/kg wet1.31 0.33 1.666 2036-12379 8
3,3'-Dichlorobenzidine mg/kg wet1.05 0.33 1.666 2022-12163 5
3/4-Methylphenol mg/kg wet1.40 0.33 1.666 2034-11984 6
4,6-Dinitro-2-methylphenol mg/kg wet1.71 0.33 1.666 2029-132103 4
4-Bromophenyl phenyl ether mg/kg wet1.34 0.33 1.666 2046-12480 6
4-Chloro-3-methylphenol mg/kg wet1.49 0.33 1.666 2045-12289 7
4-Chloroaniline mg/kg wet1.09 0.33 1.666 2017-10666 9
4-Chlorophenyl phenyl ether mg/kg wet1.34 0.33 1.666 2045-12181 6
4-Nitrophenol mg/kg wet1.64 0.33 1.666 2030-13298 4
Acenaphthene mg/kg wet1.35 0.33 1.666 2040-12381 10
Acenaphthylene mg/kg wet1.38 0.33 1.666 2032-13283 8
Anthracene mg/kg wet1.46 0.33 1.666 2047-12387 7
Azobenzene mg/kg wet1.39 0.33 1.666 2039-12584 7
Benzo(a)anthracene mg/kg wet1.52 0.33 1.666 2049-12691 6
Benzo(a)pyrene mg/kg wet1.57 0.33 1.666 2045-12994 4
Benzo(b)fluoranthene mg/kg wet1.59 0.33 1.666 2045-13295 0.4
Benzo(g,h,i)perylene mg/kg wet1.52 0.33 1.666 2043-13491 4
Benzo(k)fluoranthene mg/kg wet1.54 0.33 1.666 2047-13292 5
Benzoic Acid mg/kg wet1.32 0.33 1.666 2010-8379 5
Benzyl alcohol mg/kg wet1.12 0.33 1.666 2029-12267 10
bis(2-Chloroethoxy)methane mg/kg wet1.21 0.33 1.666 2036-12172 6
Bis(2-Chloroethyl)ether mg/kg wet1.08 0.33 1.666 2031-12065 6
Bis(2-chloroisopropyl)ether mg/kg wet1.08 0.33 1.666 2033-13165 7
Bis(2-Ethylhexyl)phthalate mg/kg wet1.46 0.33 1.666 2051-13387 5
Butyl benzyl phthalate mg/kg wet1.44 0.33 1.666 2048-13287 5
Chrysene mg/kg wet1.48 0.33 1.666 2050-12489 6
Dibenzo(a,h)anthracene mg/kg wet1.53 0.33 1.666 2045-13492 5
Dibenzofuran mg/kg wet1.38 0.33 1.666 2044-12083 7
Diethyl phthalate mg/kg wet1.47 0.33 1.666 2050-12488 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5A0062 - 3546
LCS Dup (P5A0062-BSD1)Prepared: 01/07/15 Analyzed: 01/08/15
Dimethyl phthalate mg/kg wet1.46 0.33 1.666 2048-12488 7
Di-n-butyl phthalate mg/kg wet1.51 0.33 1.666 2051-12891 3
Di-n-octyl phthalate mg/kg wet1.47 0.33 1.666 2045-14088 3
Fluoranthene mg/kg wet1.52 0.33 1.666 2050-12791 4
Fluorene mg/kg wet1.43 0.33 1.666 2043-12586 8
Hexachlorobenzene mg/kg wet1.54 0.33 1.666 2045-12293 5
Hexachlorobutadiene mg/kg wet1.37 0.33 1.666 2032-12382 3
Hexachlorocyclopentadiene mg/kg wet1.62 0.33 1.666 2032-11797 5
Hexachloroethane mg/kg wet1.21 0.33 1.666 2028-11773 9
Indeno(1,2,3-cd)pyrene mg/kg wet1.64 0.33 1.666 2045-13398 2
Isophorone mg/kg wet1.32 0.33 1.666 2030-12279 9
Naphthalene mg/kg wet1.26 0.33 1.666 2035-12375 8
Nitrobenzene mg/kg wet1.22 0.33 1.666 2034-12273 6
N-Nitroso-di-n-propylamine mg/kg wet1.29 0.33 1.666 2036-12077 9
N-Nitrosodiphenylamine mg/kg wet1.41 0.33 1.666 2038-12784 7
Pentachlorophenol mg/kg wet1.46 0.33 1.666 2025-13388 0.9
Phenanthrene mg/kg wet1.46 0.33 1.666 2050-12188 3
Phenol mg/kg wet1.27 0.33 1.666 2034-12176 10
Pyrene mg/kg wet1.46 0.33 1.666 2047-12788 7
mg/kg wet 3.332 39-132Surrogate: 2,4,6-Tribromophenol 923.06
mg/kg wet 1.666 44-115Surrogate: 2-Fluorobiphenyl 841.39
mg/kg wet 3.332 35-115Surrogate: 2-Fluorophenol 792.64
mg/kg wet 1.666 37-122Surrogate: Nitrobenzene-d5 781.30
mg/kg wet 3.332 34-121Surrogate: Phenol-d5 752.49
mg/kg wet 1.666 54-127Surrogate: Terphenyl-d14 961.61
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 19
1/13/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010035
Time Submitted: 1/6/2015 8:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P5A0071 - Solids, Dry Weight
Blank (P5A0071-BLK1)Prepared & Analyzed: 01/07/15
% Solids % by Weight99.9 0.100
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P5A00715010035-01 01/07/15 16:103030gg
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P5A00625010035-01 01/07/15 12:5030.01 1g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P5A00615010035-01 01/07/15 12:066.29 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 19
Page 19 of 19
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
01/12/2015
Mid-Atlantic Associates, Inc. - Raleigh
Wes Blaylock
409 Rogers View Court
Raleigh, NC 27610
Project: Phase II 319 S. West Street
Lab Submittal Date: 01/05/2015
Prism Work Order: 5010020
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
M Matrix spike outside of the control limits.
MI Matrix spike outside of the control limits. Matrix interference suspected.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 39
Sample Receipt Summary
01/12/2015
Prism Work Order: 5010020
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
5010020-01 12/31/14SB-1 (1-2)01/05/15Solid
5010020-02 12/31/14SB-3 (2-3)01/05/15Solid
5010020-03 12/31/14SB-4 (1-2)01/05/15Solid
5010020-04 12/31/14SB-5 (2-3)01/05/15Solid
5010020-05 12/31/14SB-6 (1.5-2.5)01/05/15Solid
Samples were received in good condition at 2.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 39
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5010020
01/12/2015
Summary of Detections
0.14 J mg/kg dry5010020-01 SB-1 (1-2)Acenaphthene 8270D
0.35 J mg/kg dry5010020-01 SB-1 (1-2)Anthracene 8270D
0.84 mg/kg dry5010020-01 SB-1 (1-2)Benzo(a)anthracene 8270D
0.72 mg/kg dry5010020-01 SB-1 (1-2)Benzo(a)pyrene 8270D
0.95 mg/kg dry5010020-01 SB-1 (1-2)Benzo(b)fluoranthene 8270D
0.42 J mg/kg dry5010020-01 SB-1 (1-2)Benzo(g,h,i)perylene 8270D
0.32 J mg/kg dry5010020-01 SB-1 (1-2)Benzo(k)fluoranthene 8270D
0.88 mg/kg dry5010020-01 SB-1 (1-2)Chrysene 8270D
0.12 J mg/kg dry5010020-01 SB-1 (1-2)Dibenzo(a,h)anthracene 8270D
1.9 mg/kg dry5010020-01 SB-1 (1-2)Fluoranthene 8270D
0.15 J mg/kg dry5010020-01 SB-1 (1-2)Fluorene 8270D
0.49 mg/kg dry5010020-01 SB-1 (1-2)Indeno(1,2,3-cd)pyrene 8270D
1.7 mg/kg dry5010020-01 SB-1 (1-2)Phenanthrene 8270D
1.4 mg/kg dry5010020-01 SB-1 (1-2)Pyrene 8270D
0.086 mg/kg dry5010020-01 SB-1 (1-2)Acetone 8260B
0.0023 J mg/kg dry5010020-01 SB-1 (1-2)Tetrachloroethylene 8260B
0.11 J mg/kg dry5010020-02 SB-3 (2-3)Chrysene 8270D
0.17 J mg/kg dry5010020-02 SB-3 (2-3)Fluoranthene 8270D
0.18 J mg/kg dry5010020-02 SB-3 (2-3)Phenanthrene 8270D
0.15 J mg/kg dry5010020-02 SB-3 (2-3)Pyrene 8270D
0.023 J mg/kg dry5010020-02 SB-3 (2-3)Acetone 8260B
0.012 mg/kg dry5010020-02 SB-3 (2-3)Methylene Chloride 8260B
0.0026 J mg/kg dry5010020-02 SB-3 (2-3)Tetrachloroethylene 8260B
0.23 J mg/kg dry5010020-03 SB-4 (1-2)Acenaphthene 8270D
0.53 mg/kg dry5010020-03 SB-4 (1-2)Anthracene 8270D
1.3 mg/kg dry5010020-03 SB-4 (1-2)Benzo(a)anthracene 8270D
1.1 mg/kg dry5010020-03 SB-4 (1-2)Benzo(a)pyrene 8270D
1.5 mg/kg dry5010020-03 SB-4 (1-2)Benzo(b)fluoranthene 8270D
0.67 mg/kg dry5010020-03 SB-4 (1-2)Benzo(g,h,i)perylene 8270D
0.54 mg/kg dry5010020-03 SB-4 (1-2)Benzo(k)fluoranthene 8270D
1.4 mg/kg dry5010020-03 SB-4 (1-2)Chrysene 8270D
0.18 J mg/kg dry5010020-03 SB-4 (1-2)Dibenzo(a,h)anthracene 8270D
0.20 J mg/kg dry5010020-03 SB-4 (1-2)Dibenzofuran 8270D
3.1 mg/kg dry5010020-03 SB-4 (1-2)Fluoranthene 8270D
0.21 J mg/kg dry5010020-03 SB-4 (1-2)Fluorene 8270D
0.78 mg/kg dry5010020-03 SB-4 (1-2)Indeno(1,2,3-cd)pyrene 8270D
0.12 J mg/kg dry5010020-03 SB-4 (1-2)Naphthalene 8270D
2.6 mg/kg dry5010020-03 SB-4 (1-2)Phenanthrene 8270D
2.3 mg/kg dry5010020-03 SB-4 (1-2)Pyrene 8270D
0.18 mg/kg dry5010020-03 SB-4 (1-2)Acetone 8260B
0.0030 J mg/kg dry5010020-03 SB-4 (1-2)Methylene Chloride 8260B
0.0059 mg/kg dry5010020-03 SB-4 (1-2)Tetrachloroethylene 8260B
0.021 J mg/kg dry5010020-04 SB-5 (2-3)Acetone 8260B
0.0025 J mg/kg dry5010020-04 SB-5 (2-3)Tetrachloroethylene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 39
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5010020
01/12/2015
Summary of Detections
0.037 J mg/kg dry5010020-05 SB-6 (1.5-2.5)Acetone 8260B
0.0073 mg/kg dry5010020-05 SB-6 (1.5-2.5)Tetrachloroethylene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-1 (1-2)
Prism Sample ID: 5010020-01
Prism Work Order: 5010020
Time Collected: 12/31/14 13:45
Time Submitted: 01/05/15 08:00
General Chemistry Parameters
76.4 *SM2540 G P5A003110.100 1/5/15 14:30 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0651,2-Dichlorobenzene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0631,4-Dichlorobenzene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0812,4,6-Trichlorophenol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0832,4-Dichlorophenol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0612-Chlorophenol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0552-Methylphenol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0782-Nitrophenol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0853,3'-Dichlorobenzidine
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0654,6-Dinitro-2-methylphenol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0604-Chloro-3-methylphenol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0524-Chloroaniline
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.0664-Nitrophenol
0.14 8270D P5A004610.43 1/7/15 20:14 KCJmg/kg dry 0.059Acenaphthene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.062Acenaphthylene
0.35 8270D P5A004610.43 1/7/15 20:14 KCJmg/kg dry 0.069Anthracene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.057Azobenzene
0.84 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.056Benzo(a)anthracene
0.72 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.047Benzo(a)pyrene
0.95 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.050Benzo(b)fluoranthene
0.42 8270D P5A004610.43 1/7/15 20:14 KCJmg/kg dry 0.047Benzo(g,h,i)perylene
0.32 8270D P5A004610.43 1/7/15 20:14 KCJmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.036Benzoic Acid
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.057Benzyl alcohol
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.075bis(2-Chloroethoxy)methane
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.061Bis(2-Chloroethyl)ether
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.074Bis(2-chloroisopropyl)ether
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-1 (1-2)
Prism Sample ID: 5010020-01
Prism Work Order: 5010020
Time Collected: 12/31/14 13:45
Time Submitted: 01/05/15 08:00
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.061Butyl benzyl phthalate
0.88 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.054Chrysene
0.12 8270D P5A004610.43 1/7/15 20:14 KCJmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.066Dibenzofuran
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.059Diethyl phthalate
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.053Di-n-octyl phthalate
1.9 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.055Fluoranthene
0.15 8270D P5A004610.43 1/7/15 20:14 KCJmg/kg dry 0.062Fluorene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.068Hexachlorobenzene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.077Hexachlorobutadiene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.077Hexachlorocyclopentadiene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.072Hexachloroethane
0.49 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.058Isophorone
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.069Naphthalene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.061Nitrobenzene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.068N-Nitroso-di-n-propylamine
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.066N-Nitrosodiphenylamine
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.051Pentachlorophenol
1.7 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.056Phenanthrene
BRL 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.064Phenol
1.4 8270D P5A004610.43 1/7/15 20:14 KCmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13299 %2,4,6-Tribromophenol
44-11589 %2-Fluorobiphenyl
35-11581 %2-Fluorophenol
37-12283 %Nitrobenzene-d5
34-12177 %Phenol-d5
54-127108 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000251,1,1,2-Tetrachloroethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000131,1,1-Trichloroethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000681,1,2,2-Tetrachloroethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000351,1,2-Trichloroethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000351,1-Dichloroethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000431,1-Dichloropropylene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000301,2,3-Trichlorobenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000621,2,3-Trichloropropane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000241,2,4-Trichlorobenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000801,2,4-Trimethylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-1 (1-2)
Prism Sample ID: 5010020-01
Prism Work Order: 5010020
Time Collected: 12/31/14 13:45
Time Submitted: 01/05/15 08:00
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000471,2-Dibromoethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000191,2-Dichlorobenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000661,2-Dichloroethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000261,2-Dichloropropane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000201,3,5-Trimethylbenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.0000561,3-Dichlorobenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000441,3-Dichloropropane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000301,4-Dichlorobenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000262,2-Dichloropropane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000252-Chlorotoluene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000194-Chlorotoluene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.000264-Isopropyltoluene
0.086 8260B P5A002910.041 1/5/15 16:58 MSCmg/kg dry 0.0022Acetone
BRL 8260B P5A002910.0025 1/5/15 16:58 MSCmg/kg dry 0.00025Benzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00017Bromobenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00060Bromochloromethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00019Bromodichloromethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00072Bromoform
BRL 8260B P5A002910.0082 1/5/15 16:58 MSCmg/kg dry 0.0012Bromomethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00022Carbon Tetrachloride
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00019Chlorobenzene
BRL 8260B P5A002910.0082 1/5/15 16:58 MSCmg/kg dry 0.0031Chloroethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00017Chloroform
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.0021Chloromethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00033cis-1,2-Dichloroethylene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00044Dichlorodifluoromethane
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00026Ethylbenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00018Isopropyl Ether
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00020Isopropylbenzene (Cumene)
BRL 8260B P5A002910.0082 1/5/15 16:58 MSCmg/kg dry 0.00053m,p-Xylenes
BRL 8260B P5A002910.041 1/5/15 16:58 MSCmg/kg dry 0.00084Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5A002910.082 1/5/15 16:58 MSCmg/kg dry 0.0015Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5A002910.041 1/5/15 16:58 MSCmg/kg dry 0.0011Methyl Isobutyl Ketone
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00030Methylene Chloride
BRL 8260B P5A002910.0082 1/5/15 16:58 MSCmg/kg dry 0.00031Methyl-tert-Butyl Ether
BRL 8260B P5A002910.0082 1/5/15 16:58 MSCmg/kg dry 0.00030Naphthalene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00018n-Butylbenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00023n-Propylbenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00026o-Xylene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00017sec-Butylbenzene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00018Styrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-1 (1-2)
Prism Sample ID: 5010020-01
Prism Work Order: 5010020
Time Collected: 12/31/14 13:45
Time Submitted: 01/05/15 08:00
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00021tert-Butylbenzene
0.0023 8260B P5A002910.0041 1/5/15 16:58 MSCJmg/kg dry 0.00028Tetrachloroethylene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00024Toluene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00047trans-1,2-Dichloroethylene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00020trans-1,3-Dichloropropylene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00038Trichloroethylene
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00033Trichlorofluoromethane
BRL 8260B P5A002910.020 1/5/15 16:58 MSCmg/kg dry 0.0012Vinyl acetate
BRL 8260B P5A002910.0041 1/5/15 16:58 MSCmg/kg dry 0.00053Vinyl chloride
BRL 8260B P5A002910.012 1/5/15 16:58 MSCmg/kg dry 0.00077Xylenes, total
Surrogate Recovery Control Limits
70-130116 %4-Bromofluorobenzene
84-123115 %Dibromofluoromethane
76-12993 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-3 (2-3)
Prism Sample ID: 5010020-02
Prism Work Order: 5010020
Time Collected: 12/31/14 14:20
Time Submitted: 01/05/15 08:00
General Chemistry Parameters
76.4 *SM2540 G P5A003110.100 1/5/15 14:30 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0661,2-Dichlorobenzene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0631,4-Dichlorobenzene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0812,4,6-Trichlorophenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0832,4-Dichlorophenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0612-Chlorophenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0552-Methylphenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0792-Nitrophenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0853,3'-Dichlorobenzidine
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0654,6-Dinitro-2-methylphenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0614-Chloro-3-methylphenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0524-Chloroaniline
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.0674-Nitrophenol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.059Acenaphthene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.062Acenaphthylene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.070Anthracene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.057Azobenzene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.056Benzo(a)anthracene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.047Benzo(a)pyrene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.036Benzoic Acid
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.057Benzyl alcohol
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.075bis(2-Chloroethoxy)methane
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.061Bis(2-Chloroethyl)ether
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.074Bis(2-chloroisopropyl)ether
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-3 (2-3)
Prism Sample ID: 5010020-02
Prism Work Order: 5010020
Time Collected: 12/31/14 14:20
Time Submitted: 01/05/15 08:00
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.061Butyl benzyl phthalate
0.11 8270D P5A004610.43 1/7/15 20:35 KCJmg/kg dry 0.054Chrysene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.053Dibenzo(a,h)anthracene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.066Dibenzofuran
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.059Diethyl phthalate
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.053Di-n-octyl phthalate
0.17 8270D P5A004610.43 1/7/15 20:35 KCJmg/kg dry 0.055Fluoranthene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.062Fluorene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.069Hexachlorobenzene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.078Hexachlorobutadiene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.077Hexachlorocyclopentadiene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.072Hexachloroethane
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.050Indeno(1,2,3-cd)pyrene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.058Isophorone
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.069Naphthalene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.061Nitrobenzene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.068N-Nitroso-di-n-propylamine
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.066N-Nitrosodiphenylamine
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.051Pentachlorophenol
0.18 8270D P5A004610.43 1/7/15 20:35 KCJmg/kg dry 0.056Phenanthrene
BRL 8270D P5A004610.43 1/7/15 20:35 KCmg/kg dry 0.064Phenol
0.15 8270D P5A004610.43 1/7/15 20:35 KCJmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-132106 %2,4,6-Tribromophenol
44-115101 %2-Fluorobiphenyl
35-11593 %2-Fluorophenol
37-12292 %Nitrobenzene-d5
34-12188 %Phenol-d5
54-127116 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000271,1,1,2-Tetrachloroethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000151,1,1-Trichloroethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000741,1,2,2-Tetrachloroethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000381,1,2-Trichloroethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000381,1-Dichloroethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000471,1-Dichloropropylene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000331,2,3-Trichlorobenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000671,2,3-Trichloropropane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000261,2,4-Trichlorobenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000881,2,4-Trimethylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-3 (2-3)
Prism Sample ID: 5010020-02
Prism Work Order: 5010020
Time Collected: 12/31/14 14:20
Time Submitted: 01/05/15 08:00
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000511,2-Dibromoethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000201,2-Dichlorobenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000721,2-Dichloroethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000281,2-Dichloropropane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000211,3,5-Trimethylbenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.0000611,3-Dichlorobenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000481,3-Dichloropropane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000331,4-Dichlorobenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000282,2-Dichloropropane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000272-Chlorotoluene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000214-Chlorotoluene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.000284-Isopropyltoluene
0.023 8260B P5A002910.045 1/5/15 17:30 MSCJmg/kg dry 0.0024Acetone
BRL 8260B P5A002910.0027 1/5/15 17:30 MSCmg/kg dry 0.00027Benzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00019Bromobenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00065Bromochloromethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00020Bromodichloromethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00079Bromoform
BRL 8260B P5A002910.0089 1/5/15 17:30 MSCmg/kg dry 0.0013Bromomethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00024Carbon Tetrachloride
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00021Chlorobenzene
BRL 8260B P5A002910.0089 1/5/15 17:30 MSCmg/kg dry 0.0034Chloroethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00019Chloroform
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.0023Chloromethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00036cis-1,2-Dichloroethylene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00030Dibromochloromethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00048Dichlorodifluoromethane
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00029Ethylbenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00019Isopropyl Ether
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00022Isopropylbenzene (Cumene)
BRL 8260B P5A002910.0089 1/5/15 17:30 MSCmg/kg dry 0.00057m,p-Xylenes
BRL 8260B P5A002910.045 1/5/15 17:30 MSCmg/kg dry 0.00092Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5A002910.089 1/5/15 17:30 MSCmg/kg dry 0.0016Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5A002910.045 1/5/15 17:30 MSCmg/kg dry 0.0012Methyl Isobutyl Ketone
0.012 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00032Methylene Chloride
BRL 8260B P5A002910.0089 1/5/15 17:30 MSCmg/kg dry 0.00034Methyl-tert-Butyl Ether
BRL 8260B P5A002910.0089 1/5/15 17:30 MSCmg/kg dry 0.00033Naphthalene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00020n-Butylbenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00025n-Propylbenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00028o-Xylene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00018sec-Butylbenzene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00019Styrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-3 (2-3)
Prism Sample ID: 5010020-02
Prism Work Order: 5010020
Time Collected: 12/31/14 14:20
Time Submitted: 01/05/15 08:00
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00023tert-Butylbenzene
0.0026 8260B P5A002910.0045 1/5/15 17:30 MSCJmg/kg dry 0.00031Tetrachloroethylene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00026Toluene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00052trans-1,2-Dichloroethylene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00021trans-1,3-Dichloropropylene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00041Trichloroethylene
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00036Trichlorofluoromethane
BRL 8260B P5A002910.022 1/5/15 17:30 MSCmg/kg dry 0.0013Vinyl acetate
BRL 8260B P5A002910.0045 1/5/15 17:30 MSCmg/kg dry 0.00058Vinyl chloride
BRL 8260B P5A002910.013 1/5/15 17:30 MSCmg/kg dry 0.00083Xylenes, total
Surrogate Recovery Control Limits
70-130117 %4-Bromofluorobenzene
84-123110 %Dibromofluoromethane
76-12994 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-4 (1-2)
Prism Sample ID: 5010020-03
Prism Work Order: 5010020
Time Collected: 12/31/14 13:15
Time Submitted: 01/05/15 08:00
General Chemistry Parameters
70.3 *SM2540 G P5A003110.100 1/5/15 14:30 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0731,2,4-Trichlorobenzene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0711,2-Dichlorobenzene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0661,3-Dichlorobenzene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0691,4-Dichlorobenzene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0901-Methylnaphthalene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0882,4,6-Trichlorophenol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0912,4-Dichlorophenol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0722,4-Dimethylphenol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0662,4-Dinitrophenol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0572,4-Dinitrotoluene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0622,6-Dinitrotoluene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0682-Chloronaphthalene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0672-Chlorophenol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0752-Methylnaphthalene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0602-Methylphenol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0852-Nitrophenol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0933,3'-Dichlorobenzidine
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0583/4-Methylphenol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0704,6-Dinitro-2-methylphenol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0814-Bromophenyl phenyl ether
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0664-Chloro-3-methylphenol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0564-Chloroaniline
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0614-Chlorophenyl phenyl ether
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.0724-Nitrophenol
0.23 8270D P5A004610.47 1/7/15 20:56 KCJmg/kg dry 0.064Acenaphthene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.068Acenaphthylene
0.53 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.076Anthracene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.062Azobenzene
1.3 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.061Benzo(a)anthracene
1.1 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.051Benzo(a)pyrene
1.5 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.054Benzo(b)fluoranthene
0.67 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.051Benzo(g,h,i)perylene
0.54 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.062Benzo(k)fluoranthene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.040Benzoic Acid
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.062Benzyl alcohol
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.081bis(2-Chloroethoxy)methane
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.066Bis(2-Chloroethyl)ether
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.080Bis(2-chloroisopropyl)ether
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.070Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-4 (1-2)
Prism Sample ID: 5010020-03
Prism Work Order: 5010020
Time Collected: 12/31/14 13:15
Time Submitted: 01/05/15 08:00
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.067Butyl benzyl phthalate
1.4 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.059Chrysene
0.18 8270D P5A004610.47 1/7/15 20:56 KCJmg/kg dry 0.057Dibenzo(a,h)anthracene
0.20 8270D P5A004610.47 1/7/15 20:56 KCJmg/kg dry 0.071Dibenzofuran
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.065Diethyl phthalate
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.062Dimethyl phthalate
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.067Di-n-butyl phthalate
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.058Di-n-octyl phthalate
3.1 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.060Fluoranthene
0.21 8270D P5A004610.47 1/7/15 20:56 KCJmg/kg dry 0.067Fluorene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.074Hexachlorobenzene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.084Hexachlorobutadiene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.084Hexachlorocyclopentadiene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.079Hexachloroethane
0.78 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.054Indeno(1,2,3-cd)pyrene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.064Isophorone
0.12 8270D P5A004610.47 1/7/15 20:56 KCJmg/kg dry 0.075Naphthalene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.067Nitrobenzene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.074N-Nitroso-di-n-propylamine
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.071N-Nitrosodiphenylamine
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.055Pentachlorophenol
2.6 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.061Phenanthrene
BRL 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.069Phenol
2.3 8270D P5A004610.47 1/7/15 20:56 KCmg/kg dry 0.062Pyrene
Surrogate Recovery Control Limits
39-13298 %2,4,6-Tribromophenol
44-11592 %2-Fluorobiphenyl
35-11582 %2-Fluorophenol
37-12282 %Nitrobenzene-d5
34-12178 %Phenol-d5
54-127104 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000261,1,1,2-Tetrachloroethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000141,1,1-Trichloroethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000721,1,2,2-Tetrachloroethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000371,1,2-Trichloroethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000371,1-Dichloroethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000261,1-Dichloroethylene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000461,1-Dichloropropylene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000651,2,3-Trichloropropane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000261,2,4-Trichlorobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-4 (1-2)
Prism Sample ID: 5010020-03
Prism Work Order: 5010020
Time Collected: 12/31/14 13:15
Time Submitted: 01/05/15 08:00
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000851,2,4-Trimethylbenzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000501,2-Dibromoethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000201,2-Dichlorobenzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000701,2-Dichloroethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000271,2-Dichloropropane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000211,3,5-Trimethylbenzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.0000601,3-Dichlorobenzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000471,3-Dichloropropane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000321,4-Dichlorobenzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000272-Chlorotoluene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000204-Chlorotoluene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.000274-Isopropyltoluene
0.18 8260B P5A002910.043 1/5/15 18:01 MSCmg/kg dry 0.0023Acetone
BRL 8260B P5A002910.0026 1/5/15 18:01 MSCmg/kg dry 0.00026Benzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00018Bromobenzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00063Bromochloromethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00020Bromodichloromethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00077Bromoform
BRL 8260B P5A002910.0087 1/5/15 18:01 MSCmg/kg dry 0.0012Bromomethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00024Carbon Tetrachloride
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00020Chlorobenzene
BRL 8260B P5A002910.0087 1/5/15 18:01 MSCmg/kg dry 0.0033Chloroethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00018Chloroform
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.0022Chloromethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00035cis-1,2-Dichloroethylene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00029Dibromochloromethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00046Dichlorodifluoromethane
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00028Ethylbenzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00019Isopropyl Ether
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00022Isopropylbenzene (Cumene)
BRL 8260B P5A002910.0087 1/5/15 18:01 MSCmg/kg dry 0.00056m,p-Xylenes
BRL 8260B P5A002910.043 1/5/15 18:01 MSCmg/kg dry 0.00089Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5A002910.087 1/5/15 18:01 MSCmg/kg dry 0.0015Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5A002910.043 1/5/15 18:01 MSCmg/kg dry 0.0011Methyl Isobutyl Ketone
0.0030 8260B P5A002910.0043 1/5/15 18:01 MSCJmg/kg dry 0.00032Methylene Chloride
BRL 8260B P5A002910.0087 1/5/15 18:01 MSCmg/kg dry 0.00033Methyl-tert-Butyl Ether
BRL 8260B P5A002910.0087 1/5/15 18:01 MSCmg/kg dry 0.00032Naphthalene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00019n-Butylbenzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00025n-Propylbenzene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00027o-Xylene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00018sec-Butylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-4 (1-2)
Prism Sample ID: 5010020-03
Prism Work Order: 5010020
Time Collected: 12/31/14 13:15
Time Submitted: 01/05/15 08:00
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00019Styrene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00022tert-Butylbenzene
0.0059 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00030Tetrachloroethylene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00026Toluene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00050trans-1,2-Dichloroethylene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00021trans-1,3-Dichloropropylene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00040Trichloroethylene
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00035Trichlorofluoromethane
BRL 8260B P5A002910.022 1/5/15 18:01 MSCmg/kg dry 0.0012Vinyl acetate
BRL 8260B P5A002910.0043 1/5/15 18:01 MSCmg/kg dry 0.00056Vinyl chloride
BRL 8260B P5A002910.013 1/5/15 18:01 MSCmg/kg dry 0.00081Xylenes, total
Surrogate Recovery Control Limits
70-130113 %4-Bromofluorobenzene
84-123114 %Dibromofluoromethane
76-12993 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-5 (2-3)
Prism Sample ID: 5010020-04
Prism Work Order: 5010020
Time Collected: 12/31/14 15:00
Time Submitted: 01/05/15 08:00
General Chemistry Parameters
72.2 *SM2540 G P5A003110.100 1/5/15 14:30 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0711,2,4-Trichlorobenzene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0691,2-Dichlorobenzene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0641,3-Dichlorobenzene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0671,4-Dichlorobenzene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0881-Methylnaphthalene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0862,4,6-Trichlorophenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0882,4-Dichlorophenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0702,4-Dimethylphenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0642,4-Dinitrophenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0552,4-Dinitrotoluene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0612,6-Dinitrotoluene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0662-Chloronaphthalene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0652-Chlorophenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0732-Methylnaphthalene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0592-Methylphenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0832-Nitrophenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0903,3'-Dichlorobenzidine
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0563/4-Methylphenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0694,6-Dinitro-2-methylphenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0784-Bromophenyl phenyl ether
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0644-Chloro-3-methylphenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0554-Chloroaniline
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0594-Chlorophenyl phenyl ether
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.0704-Nitrophenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.062Acenaphthene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.066Acenaphthylene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.074Anthracene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.060Azobenzene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.060Benzo(a)anthracene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.049Benzo(a)pyrene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.053Benzo(b)fluoranthene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.050Benzo(g,h,i)perylene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.060Benzo(k)fluoranthene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.038Benzoic Acid
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.060Benzyl alcohol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.079bis(2-Chloroethoxy)methane
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.064Bis(2-Chloroethyl)ether
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.078Bis(2-chloroisopropyl)ether
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.068Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-5 (2-3)
Prism Sample ID: 5010020-04
Prism Work Order: 5010020
Time Collected: 12/31/14 15:00
Time Submitted: 01/05/15 08:00
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.065Butyl benzyl phthalate
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.058Chrysene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.056Dibenzo(a,h)anthracene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.069Dibenzofuran
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.063Diethyl phthalate
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.060Dimethyl phthalate
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.065Di-n-butyl phthalate
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.056Di-n-octyl phthalate
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.058Fluoranthene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.066Fluorene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.072Hexachlorobenzene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.082Hexachlorobutadiene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.081Hexachlorocyclopentadiene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.076Hexachloroethane
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.052Indeno(1,2,3-cd)pyrene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.062Isophorone
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.073Naphthalene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.065Nitrobenzene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.072N-Nitroso-di-n-propylamine
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.069N-Nitrosodiphenylamine
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.054Pentachlorophenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.059Phenanthrene
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.067Phenol
BRL 8270D P5A004610.46 1/8/15 12:52 KCmg/kg dry 0.060Pyrene
Surrogate Recovery Control Limits
39-132107 %2,4,6-Tribromophenol
44-11598 %2-Fluorobiphenyl
35-11594 %2-Fluorophenol
37-12289 %Nitrobenzene-d5
34-12189 %Phenol-d5
54-127113 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000281,1,1,2-Tetrachloroethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000151,1,1-Trichloroethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000781,1,2,2-Tetrachloroethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000401,1,2-Trichloroethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000401,1-Dichloroethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000291,1-Dichloroethylene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000491,1-Dichloropropylene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000351,2,3-Trichlorobenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000711,2,3-Trichloropropane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000281,2,4-Trichlorobenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000921,2,4-Trimethylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-5 (2-3)
Prism Sample ID: 5010020-04
Prism Work Order: 5010020
Time Collected: 12/31/14 15:00
Time Submitted: 01/05/15 08:00
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000541,2-Dibromoethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000211,2-Dichlorobenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000761,2-Dichloroethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000301,2-Dichloropropane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000221,3,5-Trimethylbenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.0000651,3-Dichlorobenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000511,3-Dichloropropane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000341,4-Dichlorobenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000302,2-Dichloropropane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000292-Chlorotoluene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000224-Chlorotoluene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.000304-Isopropyltoluene
0.021 8260B P5A002910.047 1/5/15 18:33 MSCJmg/kg dry 0.0025Acetone
BRL 8260B P5A002910.0028 1/5/15 18:33 MSCmg/kg dry 0.00028Benzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00020Bromobenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00068Bromochloromethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00022Bromodichloromethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00083Bromoform
BRL 8260B P5A002910.0094 1/5/15 18:33 MSCmg/kg dry 0.0013Bromomethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00026Carbon Tetrachloride
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00022Chlorobenzene
BRL 8260B P5A002910.0094 1/5/15 18:33 MSCmg/kg dry 0.0036Chloroethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00020Chloroform
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.0024Chloromethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00038cis-1,2-Dichloroethylene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00032Dibromochloromethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00050Dichlorodifluoromethane
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00030Ethylbenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00020Isopropyl Ether
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00023Isopropylbenzene (Cumene)
BRL 8260B P5A002910.0094 1/5/15 18:33 MSCmg/kg dry 0.00060m,p-Xylenes
BRL 8260B P5A002910.047 1/5/15 18:33 MSCmg/kg dry 0.00097Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5A002910.094 1/5/15 18:33 MSCmg/kg dry 0.0017Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5A002910.047 1/5/15 18:33 MSCmg/kg dry 0.0012Methyl Isobutyl Ketone
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00034Methylene Chloride
BRL 8260B P5A002910.0094 1/5/15 18:33 MSCmg/kg dry 0.00036Methyl-tert-Butyl Ether
BRL 8260B P5A002910.0094 1/5/15 18:33 MSCmg/kg dry 0.00034Naphthalene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00021n-Butylbenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00027n-Propylbenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00030o-Xylene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00019sec-Butylbenzene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00020Styrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-5 (2-3)
Prism Sample ID: 5010020-04
Prism Work Order: 5010020
Time Collected: 12/31/14 15:00
Time Submitted: 01/05/15 08:00
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00024tert-Butylbenzene
0.0025 8260B P5A002910.0047 1/5/15 18:33 MSCJmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00028Toluene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00054trans-1,2-Dichloroethylene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00023trans-1,3-Dichloropropylene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00043Trichloroethylene
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00038Trichlorofluoromethane
BRL 8260B P5A002910.023 1/5/15 18:33 MSCmg/kg dry 0.0013Vinyl acetate
BRL 8260B P5A002910.0047 1/5/15 18:33 MSCmg/kg dry 0.00061Vinyl chloride
BRL 8260B P5A002910.014 1/5/15 18:33 MSCmg/kg dry 0.00088Xylenes, total
Surrogate Recovery Control Limits
70-130112 %4-Bromofluorobenzene
84-123118 %Dibromofluoromethane
76-12993 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-6 (1.5-2.5)
Prism Sample ID: 5010020-05
Prism Work Order: 5010020
Time Collected: 12/31/14 16:00
Time Submitted: 01/05/15 08:00
General Chemistry Parameters
63.6 *SM2540 G P5A003110.100 1/5/15 14:30 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0811,2,4-Trichlorobenzene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0791,2-Dichlorobenzene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0731,3-Dichlorobenzene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0761,4-Dichlorobenzene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.101-Methylnaphthalene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0972,4,6-Trichlorophenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.102,4-Dichlorophenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0802,4-Dimethylphenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0722,4-Dinitrophenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0632,4-Dinitrotoluene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0692,6-Dinitrotoluene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0752-Chloronaphthalene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0742-Chlorophenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0832-Methylnaphthalene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0662-Methylphenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0942-Nitrophenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.103,3'-Dichlorobenzidine
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0643/4-Methylphenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0784,6-Dinitro-2-methylphenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0894-Bromophenyl phenyl ether
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0734-Chloro-3-methylphenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0624-Chloroaniline
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0674-Chlorophenyl phenyl ether
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.0804-Nitrophenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.071Acenaphthene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.075Acenaphthylene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.084Anthracene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.069Azobenzene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.068Benzo(a)anthracene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.056Benzo(a)pyrene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.060Benzo(b)fluoranthene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.057Benzo(g,h,i)perylene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.068Benzo(k)fluoranthene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.044Benzoic Acid
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.068Benzyl alcohol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.090bis(2-Chloroethoxy)methane
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.073Bis(2-Chloroethyl)ether
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.089Bis(2-chloroisopropyl)ether
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.077Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-6 (1.5-2.5)
Prism Sample ID: 5010020-05
Prism Work Order: 5010020
Time Collected: 12/31/14 16:00
Time Submitted: 01/05/15 08:00
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.074Butyl benzyl phthalate
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.065Chrysene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.063Dibenzo(a,h)anthracene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.079Dibenzofuran
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.072Diethyl phthalate
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.069Dimethyl phthalate
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.074Di-n-butyl phthalate
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.064Di-n-octyl phthalate
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.066Fluoranthene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.074Fluorene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.082Hexachlorobenzene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.093Hexachlorobutadiene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.093Hexachlorocyclopentadiene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.087Hexachloroethane
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.060Indeno(1,2,3-cd)pyrene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.070Isophorone
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.083Naphthalene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.074Nitrobenzene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.082N-Nitroso-di-n-propylamine
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.079N-Nitrosodiphenylamine
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.061Pentachlorophenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.067Phenanthrene
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.077Phenol
BRL 8270D P5A004610.52 1/8/15 13:14 KCmg/kg dry 0.069Pyrene
Surrogate Recovery Control Limits
39-132107 %2,4,6-Tribromophenol
44-115100 %2-Fluorobiphenyl
35-11598 %2-Fluorophenol
37-12293 %Nitrobenzene-d5
34-12192 %Phenol-d5
54-127113 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000371,1,1,2-Tetrachloroethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000201,1,1-Trichloroethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00101,1,2,2-Tetrachloroethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000511,1,2-Trichloroethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000511,1-Dichloroethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000371,1-Dichloroethylene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000641,1-Dichloropropylene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000451,2,3-Trichlorobenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000911,2,3-Trichloropropane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000361,2,4-Trichlorobenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00121,2,4-Trimethylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-6 (1.5-2.5)
Prism Sample ID: 5010020-05
Prism Work Order: 5010020
Time Collected: 12/31/14 16:00
Time Submitted: 01/05/15 08:00
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000701,2-Dibromoethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000271,2-Dichlorobenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000981,2-Dichloroethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000381,2-Dichloropropane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000291,3,5-Trimethylbenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.0000831,3-Dichlorobenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000651,3-Dichloropropane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000441,4-Dichlorobenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000382,2-Dichloropropane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000372-Chlorotoluene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000284-Chlorotoluene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.000384-Isopropyltoluene
0.037 8260B P5A002910.060 1/5/15 19:04 MSCJmg/kg dry 0.0032Acetone
BRL 8260B P5A002910.0036 1/5/15 19:04 MSCmg/kg dry 0.00037Benzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00026Bromobenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00088Bromochloromethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00028Bromodichloromethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.0011Bromoform
BRL 8260B P5A002910.012 1/5/15 19:04 MSCmg/kg dry 0.0017Bromomethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00033Carbon Tetrachloride
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00028Chlorobenzene
BRL 8260B P5A002910.012 1/5/15 19:04 MSCmg/kg dry 0.0046Chloroethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00025Chloroform
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.0031Chloromethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00049cis-1,2-Dichloroethylene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00030cis-1,3-Dichloropropylene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00041Dibromochloromethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00065Dichlorodifluoromethane
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00039Ethylbenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00026Isopropyl Ether
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00030Isopropylbenzene (Cumene)
BRL 8260B P5A002910.012 1/5/15 19:04 MSCmg/kg dry 0.00078m,p-Xylenes
BRL 8260B P5A002910.060 1/5/15 19:04 MSCmg/kg dry 0.0012Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5A002910.12 1/5/15 19:04 MSCmg/kg dry 0.0022Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P5A002910.060 1/5/15 19:04 MSCmg/kg dry 0.0016Methyl Isobutyl Ketone
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00044Methylene Chloride
BRL 8260B P5A002910.012 1/5/15 19:04 MSCmg/kg dry 0.00046Methyl-tert-Butyl Ether
BRL 8260B P5A002910.012 1/5/15 19:04 MSCmg/kg dry 0.00044Naphthalene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00027n-Butylbenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00034n-Propylbenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00038o-Xylene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00024sec-Butylbenzene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00026Styrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 39
Laboratory Report
01/12/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Sample Matrix: Solid
Client Sample ID: SB-6 (1.5-2.5)
Prism Sample ID: 5010020-05
Prism Work Order: 5010020
Time Collected: 12/31/14 16:00
Time Submitted: 01/05/15 08:00
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00031tert-Butylbenzene
0.0073 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00042Tetrachloroethylene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00036Toluene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00070trans-1,2-Dichloroethylene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00029trans-1,3-Dichloropropylene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00056Trichloroethylene
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00049Trichlorofluoromethane
BRL 8260B P5A002910.030 1/5/15 19:04 MSCmg/kg dry 0.0017Vinyl acetate
BRL 8260B P5A002910.0060 1/5/15 19:04 MSCmg/kg dry 0.00078Vinyl chloride
BRL 8260B P5A002910.018 1/5/15 19:04 MSCmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130109 %4-Bromofluorobenzene
84-123117 %Dibromofluoromethane
76-12995 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0029 - 5035
Blank (P5A0029-BLK1)Prepared & Analyzed: 01/05/15
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0029 - 5035
Blank (P5A0029-BLK1)Prepared & Analyzed: 01/05/15
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1140.0570
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 1050.0526
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 950.0475
LCS (P5A0029-BS1)Prepared & Analyzed: 01/05/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0482 0.0050 0.05000 72-11596
1,1,1-Trichloroethane mg/kg wet0.0501 0.0050 0.05000 67-131100
1,1,2,2-Tetrachloroethane mg/kg wet0.0422 0.0050 0.05000 56-12684
1,1,2-Trichloroethane mg/kg wet0.0474 0.0050 0.05000 70-13395
1,1-Dichloroethane mg/kg wet0.0432 0.0050 0.05000 74-12786
1,1-Dichloroethylene mg/kg wet0.0512 0.0050 0.05000 67-149102
1,1-Dichloropropylene mg/kg wet0.0457 0.0050 0.05000 71-13091
1,2,3-Trichlorobenzene mg/kg wet0.0492 0.0050 0.05000 68-13098
1,2,3-Trichloropropane mg/kg wet0.0458 0.0050 0.05000 60-13792
1,2,4-Trichlorobenzene mg/kg wet0.0485 0.0050 0.05000 66-12597
1,2,4-Trimethylbenzene mg/kg wet0.0503 0.0050 0.05000 69-129101
1,2-Dibromoethane mg/kg wet0.0463 0.0050 0.05000 70-13293
1,2-Dichlorobenzene mg/kg wet0.0450 0.0050 0.05000 72-12390
1,2-Dichloroethane mg/kg wet0.0491 0.0050 0.05000 68-12898
1,2-Dichloropropane mg/kg wet0.0408 0.0050 0.05000 73-13082
1,3,5-Trimethylbenzene mg/kg wet0.0486 0.0050 0.05000 69-12897
1,3-Dichlorobenzene mg/kg wet0.0450 0.0050 0.05000 71-12090
1,3-Dichloropropane mg/kg wet0.0433 0.0050 0.05000 75-12487
1,4-Dichlorobenzene mg/kg wet0.0455 0.0050 0.05000 71-12391
2,2-Dichloropropane mg/kg wet0.0495 0.0050 0.05000 50-14299
2-Chlorotoluene mg/kg wet0.0466 0.0050 0.05000 67-12493
4-Chlorotoluene mg/kg wet0.0478 0.0050 0.05000 71-12696
4-Isopropyltoluene mg/kg wet0.0492 0.0050 0.05000 68-12998
Acetone mg/kg wet0.130 0.050 0.1000 29-198130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0029 - 5035
LCS (P5A0029-BS1)Prepared & Analyzed: 01/05/15
Benzene mg/kg wet0.0416 0.0030 0.05000 74-12783
Bromobenzene mg/kg wet0.0465 0.0050 0.05000 73-12593
Bromochloromethane mg/kg wet0.0528 0.0050 0.05000 72-134106
Bromodichloromethane mg/kg wet0.0503 0.0050 0.05000 75-122101
Bromoform mg/kg wet0.0497 0.0050 0.05000 66-13599
Bromomethane mg/kg wet0.0552 0.010 0.05000 20-180110
Carbon Tetrachloride mg/kg wet0.0515 0.0050 0.05000 64-143103
Chlorobenzene mg/kg wet0.0457 0.0050 0.05000 74-11891
Chloroethane mg/kg wet0.0551 0.010 0.05000 33-149110
Chloroform mg/kg wet0.0540 0.0050 0.05000 73-127108
Chloromethane mg/kg wet0.0438 0.0050 0.05000 45-14388
cis-1,2-Dichloroethylene mg/kg wet0.0486 0.0050 0.05000 76-13497
cis-1,3-Dichloropropylene mg/kg wet0.0466 0.0050 0.05000 71-12593
Dibromochloromethane mg/kg wet0.0502 0.0050 0.05000 73-122100
Dichlorodifluoromethane mg/kg wet0.0514 0.0050 0.05000 26-146103
Ethylbenzene mg/kg wet0.0466 0.0050 0.05000 74-12893
Isopropyl Ether mg/kg wet0.0422 0.0050 0.05000 59-15984
Isopropylbenzene (Cumene)mg/kg wet0.0443 0.0050 0.05000 68-12689
m,p-Xylenes mg/kg wet0.0956 0.010 0.1000 75-12496
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0486 0.050 0.05000 J61-15797
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0516 0.10 0.05000 J63-149103
Methyl Isobutyl Ketone mg/kg wet0.0480 0.050 0.05000 J57-16296
Methylene Chloride mg/kg wet0.0530 0.0050 0.05000 74-129106
Methyl-tert-Butyl Ether mg/kg wet0.0569 0.010 0.05000 70-130114
Naphthalene mg/kg wet0.0509 0.010 0.05000 57-157102
n-Butylbenzene mg/kg wet0.0485 0.0050 0.05000 65-13597
n-Propylbenzene mg/kg wet0.0472 0.0050 0.05000 67-13094
o-Xylene mg/kg wet0.0474 0.0050 0.05000 74-12695
sec-Butylbenzene mg/kg wet0.0469 0.0050 0.05000 66-13194
Styrene mg/kg wet0.0492 0.0050 0.05000 77-12198
tert-Butylbenzene mg/kg wet0.0472 0.0050 0.05000 67-13294
Tetrachloroethylene mg/kg wet0.0449 0.0050 0.05000 68-13090
Toluene mg/kg wet0.0441 0.0050 0.05000 71-12988
trans-1,2-Dichloroethylene mg/kg wet0.0470 0.0050 0.05000 73-13294
trans-1,3-Dichloropropylene mg/kg wet0.0497 0.0050 0.05000 68-12399
Trichloroethylene mg/kg wet0.0499 0.0050 0.05000 75-133100
Trichlorofluoromethane mg/kg wet0.0609 0.0050 0.05000 44-146122
Vinyl acetate mg/kg wet0.0559 0.025 0.05000 85-161112
Vinyl chloride mg/kg wet0.0425 0.0050 0.05000 48-14785
Xylenes, total mg/kg wet0.143 0.015 0.1500 74-12695
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 960.0481
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 1020.0512
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 930.0466
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0029 - 5035
LCS Dup (P5A0029-BSD1)Prepared & Analyzed: 01/05/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0479 0.0050 0.05000 2072-11596 0.7
1,1,1-Trichloroethane mg/kg wet0.0477 0.0050 0.05000 2067-13195 5
1,1,2,2-Tetrachloroethane mg/kg wet0.0423 0.0050 0.05000 2056-12685 0.2
1,1,2-Trichloroethane mg/kg wet0.0469 0.0050 0.05000 2070-13394 1
1,1-Dichloroethane mg/kg wet0.0435 0.0050 0.05000 2074-12787 0.6
1,1-Dichloroethylene mg/kg wet0.0502 0.0050 0.05000 2067-149100 2
1,1-Dichloropropylene mg/kg wet0.0446 0.0050 0.05000 2071-13089 2
1,2,3-Trichlorobenzene mg/kg wet0.0486 0.0050 0.05000 2068-13097 1
1,2,3-Trichloropropane mg/kg wet0.0437 0.0050 0.05000 2060-13787 5
1,2,4-Trichlorobenzene mg/kg wet0.0477 0.0050 0.05000 2066-12595 2
1,2,4-Trimethylbenzene mg/kg wet0.0493 0.0050 0.05000 2069-12999 2
1,2-Dibromoethane mg/kg wet0.0485 0.0050 0.05000 2070-13297 5
1,2-Dichlorobenzene mg/kg wet0.0435 0.0050 0.05000 2072-12387 3
1,2-Dichloroethane mg/kg wet0.0496 0.0050 0.05000 2068-12899 1
1,2-Dichloropropane mg/kg wet0.0419 0.0050 0.05000 2073-13084 3
1,3,5-Trimethylbenzene mg/kg wet0.0446 0.0050 0.05000 2069-12889 8
1,3-Dichlorobenzene mg/kg wet0.0430 0.0050 0.05000 2071-12086 5
1,3-Dichloropropane mg/kg wet0.0450 0.0050 0.05000 2075-12490 4
1,4-Dichlorobenzene mg/kg wet0.0445 0.0050 0.05000 2071-12389 2
2,2-Dichloropropane mg/kg wet0.0480 0.0050 0.05000 2050-14296 3
2-Chlorotoluene mg/kg wet0.0429 0.0050 0.05000 2067-12486 8
4-Chlorotoluene mg/kg wet0.0453 0.0050 0.05000 2071-12691 5
4-Isopropyltoluene mg/kg wet0.0451 0.0050 0.05000 2068-12990 9
Acetone mg/kg wet0.141 0.050 0.1000 2029-198141 8
Benzene mg/kg wet0.0438 0.0030 0.05000 2074-12788 5
Bromobenzene mg/kg wet0.0436 0.0050 0.05000 2073-12587 6
Bromochloromethane mg/kg wet0.0515 0.0050 0.05000 2072-134103 3
Bromodichloromethane mg/kg wet0.0503 0.0050 0.05000 2075-122101 0
Bromoform mg/kg wet0.0507 0.0050 0.05000 2066-135101 2
Bromomethane mg/kg wet0.0567 0.010 0.05000 2020-180113 3
Carbon Tetrachloride mg/kg wet0.0496 0.0050 0.05000 2064-14399 4
Chlorobenzene mg/kg wet0.0467 0.0050 0.05000 2074-11893 2
Chloroethane mg/kg wet0.0500 0.010 0.05000 2033-149100 10
Chloroform mg/kg wet0.0520 0.0050 0.05000 2073-127104 4
Chloromethane mg/kg wet0.0469 0.0050 0.05000 2045-14394 7
cis-1,2-Dichloroethylene mg/kg wet0.0472 0.0050 0.05000 2076-13494 3
cis-1,3-Dichloropropylene mg/kg wet0.0468 0.0050 0.05000 2071-12594 0.4
Dibromochloromethane mg/kg wet0.0516 0.0050 0.05000 2073-122103 3
Dichlorodifluoromethane mg/kg wet0.0505 0.0050 0.05000 2026-146101 2
Ethylbenzene mg/kg wet0.0466 0.0050 0.05000 2074-12893 0
Isopropyl Ether mg/kg wet0.0422 0.0050 0.05000 2059-15984 0.07
Isopropylbenzene (Cumene)mg/kg wet0.0426 0.0050 0.05000 2068-12685 4
m,p-Xylenes mg/kg wet0.0913 0.010 0.1000 2075-12491 5
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0502 0.050 0.05000 2061-157100 3
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0513 0.10 0.05000 20 J63-149103 0.6
Methyl Isobutyl Ketone mg/kg wet0.0487 0.050 0.05000 20 J57-16297 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0029 - 5035
LCS Dup (P5A0029-BSD1)Prepared & Analyzed: 01/05/15
Methylene Chloride mg/kg wet0.0583 0.0050 0.05000 2074-129117 9
Methyl-tert-Butyl Ether mg/kg wet0.0588 0.010 0.05000 2070-130118 3
Naphthalene mg/kg wet0.0518 0.010 0.05000 2057-157104 2
n-Butylbenzene mg/kg wet0.0466 0.0050 0.05000 2065-13593 4
n-Propylbenzene mg/kg wet0.0434 0.0050 0.05000 2067-13087 8
o-Xylene mg/kg wet0.0474 0.0050 0.05000 2074-12695 0.06
sec-Butylbenzene mg/kg wet0.0449 0.0050 0.05000 2066-13190 4
Styrene mg/kg wet0.0489 0.0050 0.05000 2077-12198 0.6
tert-Butylbenzene mg/kg wet0.0454 0.0050 0.05000 2067-13291 4
Tetrachloroethylene mg/kg wet0.0464 0.0050 0.05000 2068-13093 3
Toluene mg/kg wet0.0449 0.0050 0.05000 2071-12990 2
trans-1,2-Dichloroethylene mg/kg wet0.0505 0.0050 0.05000 2073-132101 7
trans-1,3-Dichloropropylene mg/kg wet0.0507 0.0050 0.05000 2068-123101 2
Trichloroethylene mg/kg wet0.0478 0.0050 0.05000 2075-13396 4
Trichlorofluoromethane mg/kg wet0.0616 0.0050 0.05000 2044-146123 1
Vinyl acetate mg/kg wet0.0610 0.025 0.05000 2085-161122 9
Vinyl chloride mg/kg wet0.0471 0.0050 0.05000 2048-14794 10
Xylenes, total mg/kg wet0.139 0.015 0.1500 2074-12692 3
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 940.0468
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 1020.0512
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 960.0481
Matrix Spike (P5A0029-MS1)Prepared & Analyzed: 01/05/15 Source: 5010020-02
1,1,1,2-Tetrachloroethane mg/kg dry0.0254 0.0047 0.04737 BRL MI60-12054
1,1,1-Trichloroethane mg/kg dry0.0277 0.0047 0.04737 BRL 52-13959
1,1,2,2-Tetrachloroethane mg/kg dry0.0271 0.0047 0.04737 BRL 39-13557
1,1,2-Trichloroethane mg/kg dry0.0263 0.0047 0.04737 BRL 44-14056
1,1-Dichloroethane mg/kg dry0.0311 0.0047 0.04737 BRL 59-13766
1,1-Dichloroethylene mg/kg dry0.0285 0.0047 0.04737 BRL 54-16260
1,1-Dichloropropylene mg/kg dry0.0254 0.0047 0.04737 BRL MI55-13754
1,2,3-Trichlorobenzene mg/kg dry0.00981 0.0047 0.04737 BRL MI34-12021
1,2,3-Trichloropropane mg/kg dry0.0236 0.0047 0.04737 BRL 45-13950
1,2,4-Trichlorobenzene mg/kg dry0.00773 0.0047 0.04737 BRL MI35-11616
1,2,4-Trimethylbenzene mg/kg dry0.0237 0.0047 0.04737 BRL 38-14250
1,2-Dibromoethane mg/kg dry0.0203 0.0047 0.04737 BRL MI49-13243
1,2-Dichlorobenzene mg/kg dry0.0157 0.0047 0.04737 BRL MI42-13033
1,2-Dichloroethane mg/kg dry0.0234 0.0047 0.04737 BRL MI51-13149
1,2-Dichloropropane mg/kg dry0.0311 0.0047 0.04737 BRL 55-13866
1,3,5-Trimethylbenzene mg/kg dry0.0256 0.0047 0.04737 BRL 44-14054
1,3-Dichlorobenzene mg/kg dry0.0127 0.0047 0.04737 BRL MI41-12927
1,3-Dichloropropane mg/kg dry0.0236 0.0047 0.04737 BRL MI53-12950
1,4-Dichlorobenzene mg/kg dry0.0108 0.0047 0.04737 BRL MI44-13423
2,2-Dichloropropane mg/kg dry0.0302 0.0047 0.04737 BRL 30-14764
2-Chlorotoluene mg/kg dry0.0212 0.0047 0.04737 BRL MI46-13245
4-Chlorotoluene mg/kg dry0.0154 0.0047 0.04737 BRL MI44-13533
4-Isopropyltoluene mg/kg dry0.0230 0.0047 0.04737 BRL 32-14449
Acetone mg/kg dry0.0900 0.047 0.09474 0.0234 34-14370
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0029 - 5035
Matrix Spike (P5A0029-MS1)Prepared & Analyzed: 01/05/15 Source: 5010020-02
Benzene mg/kg dry0.0303 0.0028 0.04737 BRL 60-13564
Bromobenzene mg/kg dry0.0193 0.0047 0.04737 BRL MI45-13541
Bromochloromethane mg/kg dry0.0256 0.0047 0.04737 BRL MI55-13654
Bromodichloromethane mg/kg dry0.0251 0.0047 0.04737 BRL MI55-12753
Bromoform mg/kg dry0.0230 0.0047 0.04737 BRL 40-13649
Bromomethane mg/kg dry0.0278 0.0095 0.04737 BRL 30-13759
Carbon Tetrachloride mg/kg dry0.0275 0.0047 0.04737 BRL 48-15358
Chlorobenzene mg/kg dry0.0187 0.0047 0.04737 BRL MI57-12539
Chloroethane mg/kg dry0.0293 0.0095 0.04737 BRL 16-17762
Chloroform mg/kg dry0.0296 0.0047 0.04737 BRL 56-13762
Chloromethane mg/kg dry0.0303 0.0047 0.04737 BRL 40-14564
cis-1,2-Dichloroethylene mg/kg dry0.0272 0.0047 0.04737 BRL MI58-14057
cis-1,3-Dichloropropylene mg/kg dry0.0211 0.0047 0.04737 BRL 42-13545
Dibromochloromethane mg/kg dry0.0235 0.0047 0.04737 BRL 49-12750
Dichlorodifluoromethane mg/kg dry0.0292 0.0047 0.04737 BRL 25-15162
Ethylbenzene mg/kg dry0.0222 0.0047 0.04737 BRL 44-14447
Isopropyl Ether mg/kg dry0.0380 0.0047 0.04737 BRL 51-15580
Isopropylbenzene (Cumene)mg/kg dry0.0278 0.0047 0.04737 BRL 41-14059
m,p-Xylenes mg/kg dry0.0421 0.0095 0.09474 BRL 36-14844
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0288 0.047 0.04737 BRL J30-14761
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0362 0.095 0.04737 BRL J24-16076
Methyl Isobutyl Ketone mg/kg dry0.0328 0.047 0.04737 BRL J25-16369
Methylene Chloride mg/kg dry0.0392 0.0047 0.04737 0.0119 53-14458
Methyl-tert-Butyl Ether mg/kg dry0.0390 0.0095 0.04737 BRL 49-13582
Naphthalene mg/kg dry0.0144 0.0095 0.04737 BRL MI32-12730
n-Butylbenzene mg/kg dry0.0161 0.0047 0.04737 BRL 23-14834
n-Propylbenzene mg/kg dry0.0212 0.0047 0.04737 BRL 35-14445
o-Xylene mg/kg dry0.0242 0.0047 0.04737 BRL 43-14351
sec-Butylbenzene mg/kg dry0.0244 0.0047 0.04737 BRL 34-14451
Styrene mg/kg dry0.0177 0.0047 0.04737 BRL MI42-13237
tert-Butylbenzene mg/kg dry0.0279 0.0047 0.04737 BRL 36-15059
Tetrachloroethylene mg/kg dry0.0257 0.0047 0.04737 0.00263 47-14249
Toluene mg/kg dry0.0245 0.0047 0.04737 BRL MI57-13552
trans-1,2-Dichloroethylene mg/kg dry0.0270 0.0047 0.04737 BRL MI58-14157
trans-1,3-Dichloropropylene mg/kg dry0.0162 0.0047 0.04737 BRL MI41-12434
Trichloroethylene mg/kg dry0.0250 0.0047 0.04737 BRL 38-16453
Trichlorofluoromethane mg/kg dry0.0305 0.0047 0.04737 BRL 30-15764
Vinyl acetate mg/kg dry0.00798 0.024 0.04737 BRL MI, J61-15417
Vinyl chloride mg/kg dry0.0276 0.0047 0.04737 BRL 40-15658
Xylenes, total mg/kg dry0.0663 0.014 0.1421 BRL 36-14847
mg/kg dry 0.04737 70-130Surrogate: 4-Bromofluorobenzene 1120.0529
mg/kg dry 0.04737 84-123Surrogate: Dibromofluoromethane 910.0432
mg/kg dry 0.04737 76-129Surrogate: Toluene-d8 970.0458
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0029 - 5035
Matrix Spike Dup (P5A0029-MSD1)Prepared & Analyzed: 01/05/15 Source: 5010020-02
1,1,1,2-Tetrachloroethane mg/kg dry0.0255 0.0046 0.04578 BRL 15 MI60-12056 0.1
1,1,1-Trichloroethane mg/kg dry0.0268 0.0046 0.04578 BRL 2152-13958 4
1,1,2,2-Tetrachloroethane mg/kg dry0.0260 0.0046 0.04578 BRL 2239-13557 4
1,1,2-Trichloroethane mg/kg dry0.0250 0.0046 0.04578 BRL 2144-14055 5
1,1-Dichloroethane mg/kg dry0.0298 0.0046 0.04578 BRL 2159-13765 4
1,1-Dichloroethylene mg/kg dry0.0258 0.0046 0.04578 BRL 2254-16256 10
1,1-Dichloropropylene mg/kg dry0.0234 0.0046 0.04578 BRL 19 MI55-13751 8
1,2,3-Trichlorobenzene mg/kg dry0.00856 0.0046 0.04578 BRL 41 MI34-12019 14
1,2,3-Trichloropropane mg/kg dry0.0220 0.0046 0.04578 BRL 2545-13948 7
1,2,4-Trichlorobenzene mg/kg dry0.00705 0.0046 0.04578 BRL 62 MI35-11615 9
1,2,4-Trimethylbenzene mg/kg dry0.0220 0.0046 0.04578 BRL 2438-14248 8
1,2-Dibromoethane mg/kg dry0.0187 0.0046 0.04578 BRL 15 MI49-13241 8
1,2-Dichlorobenzene mg/kg dry0.0146 0.0046 0.04578 BRL 21 MI42-13032 7
1,2-Dichloroethane mg/kg dry0.0224 0.0046 0.04578 BRL 13 MI51-13149 5
1,2-Dichloropropane mg/kg dry0.0303 0.0046 0.04578 BRL 1655-13866 3
1,3,5-Trimethylbenzene mg/kg dry0.0246 0.0046 0.04578 BRL 2944-14054 4
1,3-Dichlorobenzene mg/kg dry0.0118 0.0046 0.04578 BRL 24 MI41-12926 7
1,3-Dichloropropane mg/kg dry0.0221 0.0046 0.04578 BRL 15 MI53-12948 7
1,4-Dichlorobenzene mg/kg dry0.00979 0.0046 0.04578 BRL 21 MI44-13421 10
2,2-Dichloropropane mg/kg dry0.0291 0.0046 0.04578 BRL 2030-14763 4
2-Chlorotoluene mg/kg dry0.0202 0.0046 0.04578 BRL 29 MI46-13244 5
4-Chlorotoluene mg/kg dry0.0144 0.0046 0.04578 BRL 23 MI44-13531 7
4-Isopropyltoluene mg/kg dry0.0221 0.0046 0.04578 BRL 2232-14448 4
Acetone mg/kg dry0.0849 0.046 0.09156 0.0234 4934-14367 6
Benzene mg/kg dry0.0287 0.0027 0.04578 BRL 2060-13563 6
Bromobenzene mg/kg dry0.0175 0.0046 0.04578 BRL 25 MI45-13538 10
Bromochloromethane mg/kg dry0.0249 0.0046 0.04578 BRL 18 MI55-13654 3
Bromodichloromethane mg/kg dry0.0243 0.0046 0.04578 BRL 17 MI55-12753 3
Bromoform mg/kg dry0.0224 0.0046 0.04578 BRL 3540-13649 3
Bromomethane mg/kg dry0.0274 0.0092 0.04578 BRL 3030-13760 1
Carbon Tetrachloride mg/kg dry0.0268 0.0046 0.04578 BRL 2348-15358 3
Chlorobenzene mg/kg dry0.0173 0.0046 0.04578 BRL 14 MI57-12538 7
Chloroethane mg/kg dry0.0291 0.0092 0.04578 BRL 4716-17763 0.8
Chloroform mg/kg dry0.0291 0.0046 0.04578 BRL 1856-13764 2
Chloromethane mg/kg dry0.0273 0.0046 0.04578 BRL 2640-14560 10
cis-1,2-Dichloroethylene mg/kg dry0.0256 0.0046 0.04578 BRL 28 MI58-14056 6
cis-1,3-Dichloropropylene mg/kg dry0.0196 0.0046 0.04578 BRL 3242-13543 7
Dibromochloromethane mg/kg dry0.0238 0.0046 0.04578 BRL 2449-12752 1
Dichlorodifluoromethane mg/kg dry0.0272 0.0046 0.04578 BRL 3725-15160 7
Ethylbenzene mg/kg dry0.0207 0.0046 0.04578 BRL 1944-14445 7
Isopropyl Ether mg/kg dry0.0316 0.0046 0.04578 BRL 13 D51-15569 18
Isopropylbenzene (Cumene)mg/kg dry0.0266 0.0046 0.04578 BRL 2741-14058 4
m,p-Xylenes mg/kg dry0.0395 0.0092 0.09156 BRL 2036-14843 7
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0291 0.046 0.04578 BRL 42 J30-14763 0.9
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0341 0.092 0.04578 BRL 42 J24-16075 6
Methyl Isobutyl Ketone mg/kg dry0.0291 0.046 0.04578 BRL 44 J25-16363 12
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5A0029 - 5035
Matrix Spike Dup (P5A0029-MSD1)Prepared & Analyzed: 01/05/15 Source: 5010020-02
Methylene Chloride mg/kg dry0.0346 0.0046 0.04578 0.0119 14 M53-14449 13
Methyl-tert-Butyl Ether mg/kg dry0.0357 0.0092 0.04578 BRL 2249-13578 9
Naphthalene mg/kg dry0.0127 0.0092 0.04578 BRL 44 MI32-12728 12
n-Butylbenzene mg/kg dry0.0148 0.0046 0.04578 BRL 3923-14832 8
n-Propylbenzene mg/kg dry0.0193 0.0046 0.04578 BRL 2735-14442 9
o-Xylene mg/kg dry0.0232 0.0046 0.04578 BRL 1743-14351 4
sec-Butylbenzene mg/kg dry0.0228 0.0046 0.04578 BRL 2834-14450 7
Styrene mg/kg dry0.0165 0.0046 0.04578 BRL 28 MI42-13236 7
tert-Butylbenzene mg/kg dry0.0274 0.0046 0.04578 BRL 2936-15060 2
Tetrachloroethylene mg/kg dry0.0259 0.0046 0.04578 0.00263 2647-14251 1
Toluene mg/kg dry0.0230 0.0046 0.04578 BRL 22 MI57-13550 7
trans-1,2-Dichloroethylene mg/kg dry0.0239 0.0046 0.04578 BRL 18 MI58-14152 12
trans-1,3-Dichloropropylene mg/kg dry0.0140 0.0046 0.04578 BRL 20 MI41-12431 14
Trichloroethylene mg/kg dry0.0231 0.0046 0.04578 BRL 1838-16450 8
Trichlorofluoromethane mg/kg dry0.0286 0.0046 0.04578 BRL 2730-15762 6
Vinyl acetate mg/kg dry0.00450 0.023 0.04578 BRL 35 D, MI, J61-15410 56
Vinyl chloride mg/kg dry0.0240 0.0046 0.04578 BRL 3540-15652 14
Xylenes, total mg/kg dry0.0627 0.014 0.1373 BRL 2036-14846 6
mg/kg dry 0.04578 70-130Surrogate: 4-Bromofluorobenzene 1150.0526
mg/kg dry 0.04578 84-123Surrogate: Dibromofluoromethane 930.0426
mg/kg dry 0.04578 76-129Surrogate: Toluene-d8 970.0446
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5A0046 - 3546
Blank (P5A0046-BLK1)Prepared: 01/06/15 Analyzed: 01/07/15
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3'-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5A0046 - 3546
Blank (P5A0046-BLK1)Prepared: 01/06/15 Analyzed: 01/07/15
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.327 39-132Surrogate: 2,4,6-Tribromophenol 892.96
mg/kg wet 1.663 44-115Surrogate: 2-Fluorobiphenyl 861.44
mg/kg wet 3.327 35-115Surrogate: 2-Fluorophenol 832.77
mg/kg wet 1.663 37-122Surrogate: Nitrobenzene-d5 791.31
mg/kg wet 3.327 34-121Surrogate: Phenol-d5 772.55
mg/kg wet 1.663 54-127Surrogate: Terphenyl-d14 1011.68
LCS (P5A0046-BS1)Prepared: 01/06/15 Analyzed: 01/07/15
1,2,4-Trichlorobenzene mg/kg wet1.33 0.33 1.666 34-11880
1,2-Dichlorobenzene mg/kg wet1.22 0.33 1.666 33-11773
1,3-Dichlorobenzene mg/kg wet1.19 0.33 1.666 30-11572
1,4-Dichlorobenzene mg/kg wet1.18 0.33 1.666 31-11571
1-Methylnaphthalene mg/kg wet1.40 0.33 1.666 40-11984
2,4,6-Trichlorophenol mg/kg wet1.52 0.33 1.666 39-12691
2,4-Dichlorophenol mg/kg wet1.41 0.33 1.666 40-12285
2,4-Dimethylphenol mg/kg wet1.43 0.33 1.666 30-12786
2,4-Dinitrophenol mg/kg wet1.25 0.33 1.666 27-12975
2,4-Dinitrotoluene mg/kg wet1.52 0.33 1.666 48-12691
2,6-Dinitrotoluene mg/kg wet1.48 0.33 1.666 46-12489
2-Chloronaphthalene mg/kg wet1.74 0.33 1.666 41-114105
2-Chlorophenol mg/kg wet1.30 0.33 1.666 34-12178
2-Methylnaphthalene mg/kg wet1.31 0.33 1.666 38-12279
2-Methylphenol mg/kg wet1.30 0.33 1.666 32-12278
2-Nitrophenol mg/kg wet1.32 0.33 1.666 36-12379
3,3'-Dichlorobenzidine mg/kg wet1.29 0.33 1.666 22-12178
3/4-Methylphenol mg/kg wet1.35 0.33 1.666 34-11981
4,6-Dinitro-2-methylphenol mg/kg wet1.56 0.33 1.666 29-13294
4-Bromophenyl phenyl ether mg/kg wet1.41 0.33 1.666 46-12485
4-Chloro-3-methylphenol mg/kg wet1.49 0.33 1.666 45-12290
4-Chloroaniline mg/kg wet1.23 0.33 1.666 17-10674
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5A0046 - 3546
LCS (P5A0046-BS1)Prepared: 01/06/15 Analyzed: 01/07/15
4-Chlorophenyl phenyl ether mg/kg wet1.42 0.33 1.666 45-12185
4-Nitrophenol mg/kg wet1.63 0.33 1.666 30-13298
Acenaphthene mg/kg wet1.48 0.33 1.666 40-12389
Acenaphthylene mg/kg wet1.48 0.33 1.666 32-13289
Anthracene mg/kg wet1.55 0.33 1.666 47-12393
Azobenzene mg/kg wet1.50 0.33 1.666 39-12590
Benzo(a)anthracene mg/kg wet1.62 0.33 1.666 49-12698
Benzo(a)pyrene mg/kg wet1.61 0.33 1.666 45-12997
Benzo(b)fluoranthene mg/kg wet1.62 0.33 1.666 45-13297
Benzo(g,h,i)perylene mg/kg wet1.57 0.33 1.666 43-13494
Benzo(k)fluoranthene mg/kg wet1.52 0.33 1.666 47-13291
Benzoic Acid mg/kg wet1.34 0.33 1.666 10-8380
Benzyl alcohol mg/kg wet1.15 0.33 1.666 29-12269
bis(2-Chloroethoxy)methane mg/kg wet1.24 0.33 1.666 36-12174
Bis(2-Chloroethyl)ether mg/kg wet1.15 0.33 1.666 31-12069
Bis(2-chloroisopropyl)ether mg/kg wet1.12 0.33 1.666 33-13167
Bis(2-Ethylhexyl)phthalate mg/kg wet1.62 0.33 1.666 51-13397
Butyl benzyl phthalate mg/kg wet1.56 0.33 1.666 48-13294
Chrysene mg/kg wet1.57 0.33 1.666 50-12495
Dibenzo(a,h)anthracene mg/kg wet1.61 0.33 1.666 45-13497
Dibenzofuran mg/kg wet1.48 0.33 1.666 44-12089
Diethyl phthalate mg/kg wet1.52 0.33 1.666 50-12491
Dimethyl phthalate mg/kg wet1.54 0.33 1.666 48-12492
Di-n-butyl phthalate mg/kg wet1.53 0.33 1.666 51-12892
Di-n-octyl phthalate mg/kg wet1.52 0.33 1.666 45-14091
Fluoranthene mg/kg wet1.56 0.33 1.666 50-12794
Fluorene mg/kg wet1.52 0.33 1.666 43-12591
Hexachlorobenzene mg/kg wet1.61 0.33 1.666 45-12297
Hexachlorobutadiene mg/kg wet1.30 0.33 1.666 32-12378
Hexachlorocyclopentadiene mg/kg wet1.39 0.33 1.666 32-11784
Hexachloroethane mg/kg wet1.19 0.33 1.666 28-11772
Indeno(1,2,3-cd)pyrene mg/kg wet1.69 0.33 1.666 45-133101
Isophorone mg/kg wet1.34 0.33 1.666 30-12280
Naphthalene mg/kg wet1.27 0.33 1.666 35-12376
Nitrobenzene mg/kg wet1.24 0.33 1.666 34-12274
N-Nitroso-di-n-propylamine mg/kg wet1.25 0.33 1.666 36-12075
N-Nitrosodiphenylamine mg/kg wet1.51 0.33 1.666 38-12791
Pentachlorophenol mg/kg wet1.60 0.33 1.666 25-13396
Phenanthrene mg/kg wet1.52 0.33 1.666 50-12191
Phenol mg/kg wet1.34 0.33 1.666 34-12181
Pyrene mg/kg wet1.56 0.33 1.666 47-12794
mg/kg wet 3.332 39-132Surrogate: 2,4,6-Tribromophenol 923.07
mg/kg wet 1.666 44-115Surrogate: 2-Fluorobiphenyl 891.48
mg/kg wet 3.332 35-115Surrogate: 2-Fluorophenol 812.71
mg/kg wet 1.666 37-122Surrogate: Nitrobenzene-d5 781.31
mg/kg wet 3.332 34-121Surrogate: Phenol-d5 782.59
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5A0046 - 3546
LCS (P5A0046-BS1)Prepared: 01/06/15 Analyzed: 01/07/15
mg/kg wet 1.666 54-127Surrogate: Terphenyl-d14 1011.68
LCS Dup (P5A0046-BSD1)Prepared: 01/06/15 Analyzed: 01/07/15
1,2,4-Trichlorobenzene mg/kg wet1.37 0.33 1.665 2034-11882 3
1,2-Dichlorobenzene mg/kg wet1.31 0.33 1.665 2033-11779 7
1,3-Dichlorobenzene mg/kg wet1.28 0.33 1.665 2030-11577 7
1,4-Dichlorobenzene mg/kg wet1.28 0.33 1.665 2031-11577 8
1-Methylnaphthalene mg/kg wet1.42 0.33 1.665 2040-11985 1
2,4,6-Trichlorophenol mg/kg wet1.54 0.33 1.665 2039-12693 1
2,4-Dichlorophenol mg/kg wet1.44 0.33 1.665 2040-12286 2
2,4-Dimethylphenol mg/kg wet1.48 0.33 1.665 2030-12789 3
2,4-Dinitrophenol mg/kg wet1.27 0.33 1.665 2027-12976 2
2,4-Dinitrotoluene mg/kg wet1.51 0.33 1.665 2048-12691 0.6
2,6-Dinitrotoluene mg/kg wet1.47 0.33 1.665 2046-12488 0.5
2-Chloronaphthalene mg/kg wet1.77 0.33 1.665 2041-114106 1
2-Chlorophenol mg/kg wet1.37 0.33 1.665 2034-12182 5
2-Methylnaphthalene mg/kg wet1.34 0.33 1.665 2038-12280 2
2-Methylphenol mg/kg wet1.41 0.33 1.665 2032-12285 8
2-Nitrophenol mg/kg wet1.39 0.33 1.665 2036-12383 5
3,3'-Dichlorobenzidine mg/kg wet1.32 0.33 1.665 2022-12179 2
3/4-Methylphenol mg/kg wet1.47 0.33 1.665 2034-11988 9
4,6-Dinitro-2-methylphenol mg/kg wet1.66 0.33 1.665 2029-13299 6
4-Bromophenyl phenyl ether mg/kg wet1.41 0.33 1.665 2046-12485 0.1
4-Chloro-3-methylphenol mg/kg wet1.49 0.33 1.665 2045-12289 0.4
4-Chloroaniline mg/kg wet1.28 0.33 1.665 2017-10677 4
4-Chlorophenyl phenyl ether mg/kg wet1.39 0.33 1.665 2045-12184 2
4-Nitrophenol mg/kg wet1.64 0.33 1.665 2030-13298 0.5
Acenaphthene mg/kg wet1.47 0.33 1.665 2040-12389 0.5
Acenaphthylene mg/kg wet1.48 0.33 1.665 2032-13289 0.5
Anthracene mg/kg wet1.56 0.33 1.665 2047-12394 0.9
Azobenzene mg/kg wet1.47 0.33 1.665 2039-12588 2
Benzo(a)anthracene mg/kg wet1.63 0.33 1.665 2049-12698 0.04
Benzo(a)pyrene mg/kg wet1.62 0.33 1.665 2045-12997 0.4
Benzo(b)fluoranthene mg/kg wet1.56 0.33 1.665 2045-13294 4
Benzo(g,h,i)perylene mg/kg wet1.62 0.33 1.665 2043-13497 3
Benzo(k)fluoranthene mg/kg wet1.65 0.33 1.665 2047-13299 8
Benzoic Acid mg/kg wet1.40 0.33 1.665 20 L210-8384 4
Benzyl alcohol mg/kg wet1.22 0.33 1.665 2029-12273 5
bis(2-Chloroethoxy)methane mg/kg wet1.27 0.33 1.665 2036-12176 2
Bis(2-Chloroethyl)ether mg/kg wet1.26 0.33 1.665 2031-12075 9
Bis(2-chloroisopropyl)ether mg/kg wet1.20 0.33 1.665 2033-13172 7
Bis(2-Ethylhexyl)phthalate mg/kg wet1.57 0.33 1.665 2051-13395 3
Butyl benzyl phthalate mg/kg wet1.55 0.33 1.665 2048-13293 1
Chrysene mg/kg wet1.59 0.33 1.665 2050-12495 0.9
Dibenzo(a,h)anthracene mg/kg wet1.65 0.33 1.665 2045-13499 3
Dibenzofuran mg/kg wet1.47 0.33 1.665 2044-12088 0.7
Diethyl phthalate mg/kg wet1.51 0.33 1.665 2050-12491 0.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5A0046 - 3546
LCS Dup (P5A0046-BSD1)Prepared: 01/06/15 Analyzed: 01/07/15
Dimethyl phthalate mg/kg wet1.54 0.33 1.665 2048-12492 0.3
Di-n-butyl phthalate mg/kg wet1.54 0.33 1.665 2051-12892 0.8
Di-n-octyl phthalate mg/kg wet1.54 0.33 1.665 2045-14092 1
Fluoranthene mg/kg wet1.59 0.33 1.665 2050-12795 2
Fluorene mg/kg wet1.49 0.33 1.665 2043-12589 2
Hexachlorobenzene mg/kg wet1.59 0.33 1.665 2045-12295 1
Hexachlorobutadiene mg/kg wet1.38 0.33 1.665 2032-12383 6
Hexachlorocyclopentadiene mg/kg wet1.42 0.33 1.665 2032-11785 2
Hexachloroethane mg/kg wet1.24 0.33 1.665 2028-11774 4
Indeno(1,2,3-cd)pyrene mg/kg wet1.73 0.33 1.665 2045-133104 3
Isophorone mg/kg wet1.40 0.33 1.665 2030-12284 4
Naphthalene mg/kg wet1.31 0.33 1.665 2035-12379 3
Nitrobenzene mg/kg wet1.28 0.33 1.665 2034-12277 3
N-Nitroso-di-n-propylamine mg/kg wet1.36 0.33 1.665 2036-12082 8
N-Nitrosodiphenylamine mg/kg wet1.51 0.33 1.665 2038-12791 0.09
Pentachlorophenol mg/kg wet1.58 0.33 1.665 2025-13395 0.9
Phenanthrene mg/kg wet1.52 0.33 1.665 2050-12191 0.4
Phenol mg/kg wet1.39 0.33 1.665 2034-12183 3
Pyrene mg/kg wet1.56 0.33 1.665 2047-12794 0.1
mg/kg wet 3.330 39-132Surrogate: 2,4,6-Tribromophenol 923.06
mg/kg wet 1.665 44-115Surrogate: 2-Fluorobiphenyl 921.53
mg/kg wet 3.330 35-115Surrogate: 2-Fluorophenol 872.90
mg/kg wet 1.665 37-122Surrogate: Nitrobenzene-d5 831.38
mg/kg wet 3.330 34-121Surrogate: Phenol-d5 822.73
mg/kg wet 1.665 54-127Surrogate: Terphenyl-d14 1021.71
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 39
1/12/15
Level II QC Report
409 Rogers View Court
Project: Phase II 319 S. West StreetMid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Wes Blaylock
Prism Work Order: 5010020
Time Submitted: 1/5/2015 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P5A0031 - Solids, Dry Weight
Blank (P5A0031-BLK1)Prepared & Analyzed: 01/05/15
% Solids % by Weight1000.100
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P5A00315010020-01 01/05/15 14:303030gg
P5A00315010020-02 01/05/15 14:303030gg
P5A00315010020-03 01/05/15 14:303030gg
P5A00315010020-04 01/05/15 14:303030gg
P5A00315010020-05 01/05/15 14:303030gg
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P5A00465010020-01 01/06/15 15:3530.06 1g mL
P5A00465010020-02 01/06/15 15:3530.04 1g mL
P5A00465010020-03 01/06/15 15:3530.03 1g mL
P5A00465010020-04 01/06/15 15:3530.04 1g mL
P5A00465010020-05 01/06/15 15:3530.01 1g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P5A00295010020-01 01/05/15 14:177.99 5g mL
P5A00295010020-02 01/05/15 14:177.35 5g mL
P5A00295010020-03 01/05/15 14:178.2 5g mL
P5A00295010020-04 01/05/15 14:177.38 5g mL
P5A00295010020-05 01/05/15 14:176.5 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 39
Page 39 of 39