5301_LeeCounty_MSWLF_Oct15_GWMReport.pdf

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 
100 E. RUFFIN ST., MEBANE, NC 27302 
(919)‐563‐9091 PHONE 
(919)‐563‐9095 FAX 

October 29, 2015 

Jaclynne Drummond 
Compliance Hydrogeologist 
NCDEQ, Division of Waste Management  
Solid Waste Section, Asheville Regional Office 
2090 US Highway 70, Swannanoa, NC 28778 

Re: Semi‐Annual Groundwater Monitoring Event (October 2015) 
 Lee County Landfill ‐ Sanford, NC 
 NCDWM – Solid Waste Section Permit # 53‐01 
 Terraquest Project No. 02296 

Dear Ms. Drummond: 

On behalf of the Lee County Department of Public Works, Terraquest Environmental 
Consultants, P.C. is reporting the results of a biannual ground and surface water sampling event 
that took pace at the Lee County Landfill in Sanford, NC on October 19, 2015.  In accordance 
with NCDWM‐SW’s reporting requirements, a Solid Waste Section Environmental Monitoring 
Reporting Form is attached.  The data from the event including analytical results, groundwater 
elevations, and field measured groundwater parameter data is summarized on the attached 
Table 1.  The location of the site is shown of Figure 1, the vicinity of the site on Figure 2, and 
site’s layout on Figure 3.  Figure 4 presents the recent potentiometric surface.  The full 
analytical report is also attached.  The following summarizes the event: 

On October 19, 2015, Terraquest personnel sampled monitoring wells MW5, MW6, MW9, 
MW10, MW12, and MW14, and collected one surface water sample, SW2.  An attempt was 
made to sample the SW1 location, however, no water was available.  All water samples were 
analyzed per SW‐846 8260B (VOCs) and SW‐846 7470A (mercury) and 6010C (RCRA Metals).  A 
trip blank was provided with the samples throughout the process.  The blank was analyzed for 
8260B Appendix I.  All water samples were collected following technical methods and standard 
procedures as outlined on the enclosed sheets.  Terraquest personnel also collected dissolved 
oxygen, pH, temperature, and conductivity measurements from each of the sampled 
monitoring wells following purging of the well and directly from the surface water body at the 
SW2 location.  These measurements are listed on the attached Table 1.   

The analytical results revealed detectable concentrations of petroleum‐type compounds in 
monitoring well MW12 only.  Benzene was reported at a concentration in excess of the 

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 
100 E. RUFFIN ST., MEBANE, NC 27302 
(919)‐563‐9091 PHONE 
(919)‐563‐9095 FAX 
standard set forth under Title 15A of the North Carolina Administrative Code Subchapter 2L 
.0202(g).  Results of the RCRA Metals analysis indicate that all of the monitoring wells and the 
surface water sample had a detection of at least one metal.  The analytical results are 
summarized in Table 1.   

A potentiometric surface map (Figure 4) depicting an interpreted groundwater flow direction at 
the site as measured on October 19, 2015 is attached.  Based upon the water levels in 
monitoring wells, the groundwater flow direction is to the southeast toward Mare Brand Creek.  
This flow direction conforms with historical flow directions.  Table 1 lists the groundwater 
elevations for the monitoring wells. 

If you have any questions regarding the sampling event or analytical report, please contact 
Ryan Kerins at (919)‐563‐9091 or Mr. Joseph Cherry of the Lee County Public Works 
Department at (919)‐774‐8440.  Thank you. 

Sincerely, 

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 

Ryan D. Kerins         Michael J. Brown P.G.    
Project Manager       President 

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E
T
E
R

R
E
S
U
L
T

U
N
I
T
S

Q
U
A
L
I
F
I
E
R
DI
L
U
T
I
O
N

FA
C
T
O
R
CO
L
L
E
C
T
 DA
T
E
EX
T
R
A
C
T
I
O
N
 DATE*ANALYSIS  DATE
53
‐01

M
W
9

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
8
4
.
2

f
e
e
t
53
‐01

M
W
9

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

6
.
3
8

f
e
e
t
53
‐01

M
W
9

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

37
7
.
8

f
e
e
t
53
‐01

M
W
9

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

3
.
9
1
53
‐01

M
W
9

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

5
.
0
9

m
g
/
L
53
‐01

M
W
9

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
7
.
8

d
e
g
.
 C
53
‐01

M
W
9

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

9
3

m
i
c
r
o
S
/
s
e
c
53
‐01

M
W
9

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
9

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
9

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
9

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
7
1

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
9

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

<
0
.
0
6
7

u
g
/
L

B
J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
7
/
1
5
53
‐01

M
W
9

7
4
4
0
‐38
‐2

1
4

A
r
s
e
n
i
c

<
1
0

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
9

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

1
5
6

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
9

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

<
0
.
0
5
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
9

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

2
.
2
4

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
9

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

2
.
5
6

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
9

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

3
.
2

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
9

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
0
.
2
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
0

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
7
7
.
0

f
e
e
t
53
‐01

M
W
1
0

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

9
.
0
4

f
e
e
t
53
‐01

M
W
1
0

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
6
8
.
0

f
e
e
t
53
‐01

M
W
1
0

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

3
.
8
5
53
‐01

M
W
1
0

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

3
.
2
6

m
g
/
L
53
‐01

M
W
1
0

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
8
.
1

d
e
g
.
 C
53
‐01

M
W
1
0

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

1
1
0

m
i
c
r
o
S
/
s
e
c
53
‐01

M
W
1
0

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
0

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
0

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
0

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
7
1

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
0

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

0
.
1
1
6

u
g
/
L

B
J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
7
/
1
5
53
‐01

M
W
1
0

7
4
4
0
‐38
‐2

1
4

A
r
s
e
n
i
c

<
2
.
6
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
0

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

1
8
7

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
0

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

<
0
.
0
5
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
0

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

4
.
3
2

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
0

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

1
.
5
6

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
0

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

3
.
0
9

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
0

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
0
.
2
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
1

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
9
9
.
6

f
e
e
t
53
‐01

M
W
1
1

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

1
0
.
4
0

f
e
e
t
53
‐01

M
W
1
1

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
8
9
.
2

f
e
e
t
53
‐01

M
W
1
2

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
3
7
.
4

f
e
e
t
53
‐01

M
W
1
2

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

3
.
3
8

f
e
e
t
53
‐01

M
W
1
2

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
3
4

f
e
e
t
53
‐01

M
W
1
2

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

5
.
7
5
53
‐01

M
W
1
2

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

1
.
0
8

m
g
/
L
53
‐01

M
W
1
2

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
8
.
3

d
e
g
.
 C
53
‐01

M
W
1
2

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

1
,
7
3
8

m
i
c
r
o
S
/
s
e
c
53
‐01

M
W
1
2

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

3
.
5
9

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
7
1

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

1
0
8
‐90
‐7

3
9

C
h
l
o
r
o
b
e
n
z
e
n
e

2
2
.
1

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

7
5
‐00
‐3

4
1

C
h
l
o
r
o
e
t
h
a
n
e

3
0
.
8

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

1
0
8
‐20
‐3

3
6
6

I
s
o
p
r
o
p
y
l
 et
h
e
r

0
.
3
9

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

9
8
‐82
‐8

3
6
7

I
s
o
p
r
o
p
y
l
b
e
n
z
e
n
e

0
.
8
4

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

1
6
3
4
‐04
‐4

3
6
9

M
e
t
h
y
l
 te
r
t
‐bu
t
y
l
 et
h
e
r

0
.
4
3

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

1
0
6
‐46
‐77
1

1
,
4
‐Di
c
h
l
o
r
o
b
e
n
z
e
n
e

4
.
7
3

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

7
5
‐34
‐37
5

1
,
1
‐Di
c
h
l
o
r
o
e
t
h
a
n
e

3
.
2
2

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

0
.
0
4
7

u
g
/
L

B
J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
7
/
1
5
53
‐01

M
W
1
2

7
4
4
0
‐38
‐2

1
4

A
r
s
e
n
i
c

7
.
9
2

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
2

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

1
4
0

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
2

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

2
.
2
4

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
2

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

2
.
9
6

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
2

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

2
2
.
7

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
2

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

<
0
.
3
0
9

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
2

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
0
.
2
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
No
t
e
:
1.
  * Te
c
h
n
i
c
a
l
l
y
,
 th
i
s
 sa
m
p
l
e
 se
t
 di
d
n
'
t
 ha
v
e
 an
y
 ex
t
r
a
c
t
i
o
n
s
.
  Th
e
 me
t
a
l
s
 we
r
e
 pr
e
p
p
e
d
 an
d
 dig
e
s
t
e
d
.
  Th
e
 vo
l
a
t
i
l
e
s
 ar
e
n
'
t
 in
v
o
l
v
e
d
 in
 an
y
 ex
t
r
a
c
t
i
o
n
 pr
o
c
e
s
s
.
  Th
e
y
 ar
e
 lo
a
d
e
d
 di
r
e
c
t
l
y
 on
t
o
 th
e
 in
s
t
r
u
m
e
n
t
.

Da
t
e
:
 10
/
3
0
/
1
5
Fa
c
i
l
i
t
y
 Na
m
e
:
  Le
e
 Co
u
n
t
y
 La
n
d
f
i
l
l
Ta
b
l
e
 1  ‐

CO
N
T
I
N
U
E
D
GR
O
U
N
D
W
A
T
E
R
 DA
T
A
 10
/
1
9
/
1
5
Pa
g
e
 3  of
 3
FA
C
I
L
I
T
Y
 PE
R
M
I
T

W
E
L
L
 ID

C
A
S
 Nu
m
b
e
r

S
W
S
 ID

P
A
R
A
M
E
T
E
R

R
E
S
U
L
T

U
N
I
T
S

Q
U
A
L
I
F
I
E
R
DI
L
U
T
I
O
N

FA
C
T
O
R
CO
L
L
E
C
T
 DA
T
E
EX
T
R
A
C
T
I
O
N
 DATE*ANALYSIS  DATE
53
‐01

M
W
1
3

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
6
3
.
9
3

f
e
e
t
53
‐01

M
W
1
3

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

9
.
6
9

f
e
e
t
53
‐01

M
W
1
3

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
5
4
.
2

f
e
e
t
53
‐01

M
W
1
4

S
W
3
2
8

3
2
8

T
o
p
 Of
 Ca
s
i
n
g

3
5
8
.
6
1

f
e
e
t
53
‐01

M
W
1
4

S
W
3
1
8

3
1
8

D
e
p
t
h
 To
 Wa
t
e
r

7
.
4
1

f
e
e
t
53
‐01

M
W
1
4

4
2
7

G
r
o
u
n
d
w
a
t
e
r
 Ele
v
a
t
i
o
n

3
5
1
.
2

f
e
e
t
53
‐01

M
W
1
4

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

5
.
8
5
53
‐01

M
W
1
4

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

0
.
9
7

m
g
/
L
53
‐01

M
W
1
4

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
6
.
5

d
e
g
.
 C
53
‐01

M
W
1
4

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

1
1
0

m
i
c
r
o
S
/
s
e
c
53
‐01

M
W
1
4

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
4

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
4

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
4

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
7
1

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
4

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

0
.
0
7
4
8

u
g
/
L

B
J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
7
/
1
5
53
‐01

M
W
1
4

7
4
4
0
‐38
‐2

1
4

A
r
s
e
n
i
c

4
.
3
2

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
4

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

2
0
7

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
4

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

0
.
5
2

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
4

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

1
1
.
2

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
4

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

7
5
.
7

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
4

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

<
3
.
0
9

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

M
W
1
4

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
0
.
2
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

S
W
2

S
W
3
2
0

3
2
0

p
H
 (f
i
e
l
d
)

5
.
7
3
53
‐01

S
W
2

S
W
3
5
6

3
5
6

D
i
s
s
o
l
v
e
d
 Ox
y
g
e
n

6
.
5
9

m
g
/
L
53
‐01

S
W
2

S
W
3
2
5

3
2
5

T
e
m
p
e
r
a
t
u
r
e

1
3
.
1

d
e
g
.
 C
53
‐01

S
W
2

S
W
3
2
4

3
2
4

C
o
n
d
u
c
t
i
v
i
t
y

1
1
8

m
i
c
r
o
S
/
s
e
c
53
‐01

S
W
2

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

S
W
2

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

S
W
2

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

S
W
2

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
7
1

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

S
W
2

7
4
3
9
‐97
‐6

1
3
2

M
e
r
c
u
r
y

0
.
0
6
0
8

u
g
/
L

B
J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
7
/
1
5
53
‐01

S
W
2

7
4
4
0
‐38
‐2

1
4

A
r
s
e
n
i
c

<
2
.
6
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

S
W
2

7
4
4
0
‐39
‐3

1
5

B
a
r
i
u
m

8
0
.
3

u
g
/
L

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

S
W
2

7
4
4
0
‐43
‐9

3
4

C
a
d
m
i
u
m

0
.
2
8

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

S
W
2

7
4
4
0
‐47
‐3

5
1

C
h
r
o
m
i
u
m

1
.
1
6

u
g
/
L

J

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

S
W
2

7
4
3
9
‐92
‐1

1
3
1

L
e
a
d

<
0
.
7
4
4

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

S
W
2

7
7
8
2
‐49
‐2

1
8
3

S
e
l
e
n
i
u
m

<
3
.
0
9

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

S
W
2

7
4
4
0
‐22
‐4

1
8
4

S
i
l
v
e
r

<
0
.
2
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
8
/
1
5
53
‐01

T
R
I
P
 BL
A
N
K

7
1
‐43
‐2

1
6

B
e
n
z
e
n
e

<
0
.
1
6

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

T
R
I
P
 BL
A
N
K

1
0
8
‐88
‐3

1
9
6

T
o
l
u
e
n
e

<
0
.
1
4

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

T
R
I
P
 BL
A
N
K

1
0
0
‐41
‐4

1
1
0

E
t
h
y
l
b
e
n
z
e
n
e

<
0
.
1
9

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

T
R
I
P
 BL
A
N
K

1
3
3
0
‐20
‐7

3
4
6

T
o
t
a
l
 Xy
l
e
n
e
s

<
0
.
7
1

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
53
‐01

M
W
1
2

1
6
3
4
‐04
‐4

3
6
9

M
e
t
h
y
l
 te
r
t
‐bu
t
y
l
 et
h
e
r

<
0
.
1
8

u
g
/
L

U

1

1
0
/
1
9
/
1
5

*

1
0
/
2
6
/
1
5
No
t
e
:
Da
t
e
:
 10
/
3
0
/
1
5
Fa
c
i
l
i
t
y
 Na
m
e
:
  Le
e
 Co
u
n
t
y
 La
n
d
f
i
l
l
Ta
b
l
e
 1  ‐

CO
N
T
I
N
U
E
D
GR
O
U
N
D
W
A
T
E
R
 DA
T
A
 10
/
1
9
/
1
5
1.
  * Te
c
h
n
i
c
a
l
l
y
,
 th
i
s
 sa
m
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 TECHNICAL METHODS/STANDARD PROCEDURES 

Groundwater Sampling 

Groundwater samples are collected from temporary or permanent monitoring wells according to 
established sampling protocol.  When multiple monitoring wells or sampling points are sampled, 
sampling is completed beginning with the least contaminated well to the most contaminated well, 
if it is known.  When permanent monitoring wells for petroleum sites are sampled, the well is 
purged of a minimum of three well‐bore volumes prior to sample collection in order to assure that 
sampled water is representative of aquifer conditions.  In temporary wells, the first water which 
migrates into the open borehole is sampled.  Samples from both temporary and permanent 
monitoring wells are collected using individually wrapped disposable polyethylene bailers by field 
personnel wearing disposable nitrile gloves.  Only one well is sampled with a given bailer in order to 
prevent sample cross‐contamination.  During both well purging and sampling, proper protective 
clothing and equipment is used and is dependent upon the type and level of contaminants present. 
Also, field personnel change gloves between different samples to reduce the chance of cross‐
contamination. Water samples are transferred from the bailer to laboratory‐prepared sampling 
containers using slow emptying devices to reduce the chance of contamination loss through 
volatilization.  Preservatives, such as acids, are provided by the laboratory in pre‐prepared 
containers in which collected samples are placed if in‐field preservation is necessary.  The samples 
are labeled with the project name, project number, sample identification, required analysis, and 
date and time of collection.  The samples are placed on ice, shipped to a certified laboratory, and 
analyzed before the expiration of an analytical method’s prescribed holding time.  Chain‐of‐custody 
documentation is maintained for each sample collected in the field.   

Surface Water Sampling 

Surface water samples, specifically samples from creeks or streams, are collected from a 
moving/flowing portion of the creek or stream to ensure that stagnant water is not collected.  Field 
personnel are careful to collect samples from flowing areas that are not so turbulent as to cause a 
loss of volatile contaminants which might have been contained in the creek’s/stream’s water.  
Samples are collected by field personnel wearing disposable nitrile gloves.  Field personnel change 
gloves between different locations to reduce the chance of cross‐contamination.  Samples are 
collected directly from the appropriate creek or stream location and placed into the appropriate 
laboratory‐prepared containers.  Preservatives, such as acids, are provided by the laboratory in pre‐
prepared containers in which collected samples are placed if in‐field preservation is necessary. The 
samples are labeled with the project name, project number, sample identification, required 
analysis, and date and time of collection.  The samples are cooled on ice to approximately four 
degrees centigrade, shipped to a certified laboratory, and analyzed before the expiration of an 
analytical method’s prescribed holding time.  Chain‐of‐custody documentation is maintained for 
each sample collected in the field.    

Field Measurements 

Field measurements taken to determine the pH, conductivity, temperature, and dissolved oxygen 
concentration of a particular groundwater sample are taken directly after a particular monitoring 
well has been adequately purged.  This ensures that the groundwater parameter data collected is 
representative of the aquifer conditions at a given location.  Once purging of the monitoring well is 
complete, the decontaminated probe head and cord of the appropriate unit is lowered into the 
required monitoring well.  If the depth to water in a specific monitoring well is greater than the 
length of cord for a particular unit, a new, disposable bailer is slowly lowered into the appropriate 
monitoring well and a representative groundwater sample is retrieved.  A slow pouring device is 
fitted onto the end of the disposable bailer and the sample is slowly poured into a new, disposable 
plastic cup.  Groundwater parameter data are then collected from the groundwater in the cup 
using the required unit.   

For pH, conductivity, and temperature, a Hanna Instruments Model 991300 portable meter is 
utilized.  This unit is periodically calibrated and maintained in accordance with the unit’s operations 
manual by field personnel.  Prior to data collection, the unit is properly decontaminated to prevent 
cross‐contamination.  The unit is decontaminated between each sample.  The procedure used for 
sample measurement involves lowering the meter’s probe into the new, disposable cup containing 
the groundwater sample to be measured and slowly stirring the probe to force groundwater across 
the probe’s membrane.  The measurements displayed by the meter are then recorded.   

For dissolved oxygen concentration measurements, a YSI® Model 55 Handheld Dissolved Oxygen 
System is utilized.  This unit is periodically calibrated and maintained in accordance with the unit’s 
operations manual by field personnel.  Prior to data collection, the unit is properly decontaminated 
to prevent cross‐contamination.  The unit is decontaminated between each sample.  The procedure 
used for sample measurement involves adjusting the unit for the correct altitude where the 
sampling will take place and adjusting the reported units desired.  Once this is done, the unit’s 
probe is inserted into the groundwater sample to be measured and the probe is slowly stirred to 
force the groundwater across the probe’s membrane.  The measurements displayed by the unit are 
then recorded.   
Analytical Report 517846
for
Terraquest Environmental Consultants, P.C.
Project Manager: Ryan Kerins
Lee Co. Landfill
28-OCT-15
02296
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (T104704215-15-19), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
Oklahoma (9218)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Texas (T104704477), Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)
Collected By: Client
Page 1 of 45 Final 1.000

Page 2 of 45 Final 1.000
Table of Contents
Cover Page 1
Cover Letter 3
Sample ID Cross Reference 4
Explanation of Qualifiers (Flags) 5
Hits Summary 6
Certificate of Analysis (Detailed Report) 10
Summary of Quality control 33
Blank Summary 39
Chain of Custody 43
Sample Receipt Conformance Report 45
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Project Manager: Ryan Kerins
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302

Reference: XENCO Report No(s): 517846
Lee Co. Landfill
Project Address: NC
Ryan Kerins:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 517846. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 517846 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
28-OCT-15
Project Manager
Debbie Simmons
Page 3 of 45 Final 1.000
Sample Cross Reference 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
Sample Id
MW5
MW6
MW9
MW10
MW12
MW14
SW2
Trip Blank
10-19-15 13:45
10-19-15 12:05
10-19-15 11:15
10-19-15 11:35
10-19-15 13:15
10-19-15 10:50
10-19-15 14:30
10-19-15 00:00
Date Collected Lab Sample Id
517846-001
517846-002
517846-003
517846-004
517846-005
517846-006
517846-007
517846-008

Sample DepthMatrix
W
W
W
W
W
W
W
W
Page 4 of 45 Final 1.000
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4143 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd , Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
2505 North Falkenburg Rd, Tampa, FL 33619
12600 West I-20 East, Odessa, TX 79765
6017 Financial Drive, Norcross, GA 30071
3725 E. Atlanta Ave, Phoenix, AZ 85040
Phone Fax
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone]
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non-Calculable
+ NELAC certification not offered for this compound.

* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Page 5 of 45 Final 1.000
Hits Summary 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50
10.21.15 09.50
Date Received :
Date Received :
% Moisture :
% Moisture :
10.19.15 13.45
10.19.15 12.05
Date Collected :
Date Collected :
517846-001
517846-002
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW5
MW6
Sample Id :
Sample Id :
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method :
Analytical Method :
Analytical Method :
Analytical Method :
SW7470P
SW3010A_LL
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
10.23.15 10.33
10.28.15 12.48
Date Prep:
Date Prep:
Date Prep:
Date Prep:
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Barium
Chromium
Parameter
Parameter
Parameter
Parameter
Result
Result
Result
Result
BJ
J
J
BJ
J
J
Flag
Flag
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
Units
Units
1
1
1
1
1
1
1
1
1
Dil
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
Cas Number
7439-97-6
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7439-97-6
7440-39-3
7440-47-3
0.0000882
0.0135
0.431
0.000840
0.0113
0.0304
0.0000188
0.0450
0.000440
979955
980071
979955
980071
Seq Number
Seq Number
Seq Number
Seq Number
10.27.15 07.57
10.28.15 14.15
10.28.15 14.15
10.28.15 14.15
10.28.15 14.15
10.28.15 14.15
10.27.15 08.15
10.28.15 14.32
10.28.15 14.32
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Page 6 of 45 Final 1.000
Hits Summary 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50
10.21.15 09.50
Date Received :
Date Received :
% Moisture :
% Moisture :
10.19.15 11.15
10.19.15 11.35
Date Collected :
Date Collected :
517846-003
517846-004
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW9
MW10
Sample Id :
Sample Id :
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method :
Analytical Method :
Analytical Method :
Analytical Method :
SW7470P
SW3010A_LL
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
10.23.15 10.33
10.28.15 12.48
Date Prep:
Date Prep:
Date Prep:
Date Prep:
Mercury
Barium
Chromium
Lead
Selenium
Mercury
Barium
Chromium
Lead
Parameter
Parameter
Parameter
Parameter
Result
Result
Result
Result
BJ
J
J
J
BJ
J
J
Flag
Flag
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
Units
Units
1
1
1
1
1
1
1
1
1
Dil
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
Cas Number
7439-97-6
7440-39-3
7440-47-3
7439-92-1
7782-49-2
7439-97-6
7440-39-3
7440-47-3
7439-92-1
0.0000670
0.156
0.00224
0.00256
0.00320
0.000116
0.187
0.00432
0.00156
979955
980071
979955
980071
Seq Number
Seq Number
Seq Number
Seq Number
10.27.15 08.18
10.28.15 14.39
10.28.15 14.39
10.28.15 14.39
10.28.15 14.39
10.27.15 08.21
10.28.15 14.41
10.28.15 14.41
10.28.15 14.41
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Page 7 of 45 Final 1.000
Hits Summary 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received :
% Moisture :
10.19.15 13.15 Date Collected : 517846-005Lab Sample Id :
Ground WaterMatrix : MW12Sample Id :
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
VOCs by SW-846 8260B
Analytical Method :
Analytical Method :
Analytical Method :
SW7470P
SW3010A_LL
SW5030B
Prep Method:
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
10.26.15 12.48
Date Prep:
Date Prep:
Date Prep:
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
1,1-Dichloroethane
1,4-Dichlorobenzene
Benzene
Chlorobenzene
Chloroethane
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether
Parameter
Parameter
Parameter
Result
Result
Result
BJ
J
J
J
J
J
J
Flag
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7439-97-6
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
75-34-3
106-46-7
71-43-2
108-90-7
75-00-3
108-20-3
98-82-8
1634-04-4
0.0000474
0.00792
1.40
0.00224
0.00296
0.0227
3.22
4.73
3.59
22.1
30.8
0.390
0.840
0.430
979955
980071
979967
Seq Number
Seq Number
Seq Number
10.27.15 08.24
10.28.15 14.43
10.28.15 14.43
10.28.15 14.43
10.28.15 14.43
10.28.15 14.43
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
Analysis Date
Analysis Date
Analysis Date
Page 8 of 45 Final 1.000
Hits Summary 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50
10.21.15 09.50
Date Received :
Date Received :
% Moisture :
% Moisture :
10.19.15 10.50
10.19.15 14.30
Date Collected :
Date Collected :
517846-006
517846-007
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW14
SW2
Sample Id :
Sample Id :
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method :
Analytical Method :
Analytical Method :
Analytical Method :
SW7470P
SW3010A_LL
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
10.23.15 10.33
10.28.15 12.48
Date Prep:
Date Prep:
Date Prep:
Date Prep:
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Barium
Cadmium
Chromium
Parameter
Parameter
Parameter
Parameter
Result
Result
Result
Result
BJ
J
J
J
BJ
J
J
Flag
Flag
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
Units
Units
1
1
1
1
1
1
1
1
1
1
Dil
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
Cas Number
7439-97-6
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7439-97-6
7440-39-3
7440-43-9
7440-47-3
0.0000748
0.00432
0.207
0.000520
0.0112
0.0757
0.0000608
0.0803
0.000280
0.00116
979955
980071
979955
980071
Seq Number
Seq Number
Seq Number
Seq Number
10.27.15 08.27
10.28.15 14.44
10.28.15 14.44
10.28.15 14.44
10.28.15 14.44
10.28.15 14.44
10.27.15 08.30
10.28.15 14.46
10.28.15 14.46
10.28.15 14.46
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Page 9 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 13.45 Date Collected:517846-001Lab Sample Id:
Ground WaterMatrix: MW5Sample Id:
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method:
Analytical Method:
ABA
ABA
Analyst:
Analyst:
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
Date Prep:
Date Prep:
HAP
ABA
Tech:
Tech:
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
Parameter
0.0000101
0.00266
0.000916
0.0000560
0.000160
0.000744
0.00309
0.000260
Result
Result
BJ
J
J
U
U
0.00200
0.0100
0.0500
0.00500
0.0500
0.0100
0.0500
0.0200
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
1
1
1
1
1
1
1
1
Dil
Dil
Cas Number
Cas Number
7439-97-6
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
0.0000882
0.0135
0.431
0.000840
0.0113
0.0304
U
U
979955
980071
Seq Number:
Seq Number:
RL
RL
MDL
MDL
10.27.15 07.57
10.28.15 14.15
10.28.15 14.15
10.28.15 14.15
10.28.15 14.15
10.28.15 14.15
10.28.15 14.15
10.28.15 14.15
Analysis Date
Analysis Date
% Moisture:
% Moisture:
Page 10 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 13.45 Date Collected:517846-001Lab Sample Id:
Ground WaterMatrix: MW5Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.160
0.180
0.250
0.110
0.200
0.100
0.250
0.210
0.170
0.140
0.180
0.140
0.180
0.150
0.170
0.170
0.190
0.170
0.210
0.280
0.190
0.320
0.130
0.130
0.260
0.350
0.160
0.210
0.200
0.250
0.170
0.250
0.330
0.150
0.150
0.260
0.160
0.250
0.210
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
UX
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2.00
1.00
2.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
Analysis Date
% Moisture:
Page 11 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 13.45 Date Collected:517846-001Lab Sample Id:
Ground WaterMatrix: MW5Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter
0.100
0.220
8.00
0.190
0.0800
0.150
0.510
0.180
0.420
0.220
0.170
0.180
0.200
0.210
0.180
0.180
0.160
0.140
0.210
0.110
0.190
0.530
0.720
0.190
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
20.0
1.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
179601-23-1
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
Analysis Date
Surrogate
53-159
30-186
70-130
%
Recovery Flag
%
%
%
86
98
96
10.26.15 15.47
10.26.15 15.47
10.26.15 15.47
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 12 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 12.05 Date Collected:517846-002Lab Sample Id:
Ground WaterMatrix: MW6Sample Id:
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method:
Analytical Method:
ABA
ABA
Analyst:
Analyst:
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
Date Prep:
Date Prep:
HAP
ABA
Tech:
Tech:
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
Parameter
0.0000101
0.00266
0.000916
0.0000560
0.000160
0.000744
0.00309
0.000260
Result
Result
BJ
U
J
U
J
U
U
U
0.00200
0.0100
0.0500
0.00500
0.0500
0.0100
0.0500
0.0200
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
1
1
1
1
1
1
1
1
Dil
Dil
Cas Number
Cas Number
7439-97-6
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
0.0000188
U
0.0450
U
0.000440
U
U
U
979955
980071
Seq Number:
Seq Number:
RL
RL
MDL
MDL
10.27.15 08.15
10.28.15 14.32
10.28.15 14.32
10.28.15 14.32
10.28.15 14.32
10.28.15 14.32
10.28.15 14.32
10.28.15 14.32
Analysis Date
Analysis Date
% Moisture:
% Moisture:
Page 13 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 12.05 Date Collected:517846-002Lab Sample Id:
Ground WaterMatrix: MW6Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.160
0.180
0.250
0.110
0.200
0.100
0.250
0.210
0.170
0.140
0.180
0.140
0.180
0.150
0.170
0.170
0.190
0.170
0.210
0.280
0.190
0.320
0.130
0.130
0.260
0.350
0.160
0.210
0.200
0.250
0.170
0.250
0.330
0.150
0.150
0.260
0.160
0.250
0.210
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2.00
1.00
2.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
Analysis Date
% Moisture:
Page 14 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 12.05 Date Collected:517846-002Lab Sample Id:
Ground WaterMatrix: MW6Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter
0.100
0.220
8.00
0.190
0.0800
0.150
0.510
0.180
0.420
0.220
0.170
0.180
0.200
0.210
0.180
0.180
0.160
0.140
0.210
0.110
0.190
0.530
0.720
0.190
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
20.0
1.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
179601-23-1
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
Analysis Date
Surrogate
53-159
30-186
70-130
%
Recovery Flag
%
%
%
88
97
98
10.26.15 16.11
10.26.15 16.11
10.26.15 16.11
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 15 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 11.15 Date Collected:517846-003Lab Sample Id:
Ground WaterMatrix: MW9Sample Id:
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method:
Analytical Method:
ABA
ABA
Analyst:
Analyst:
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
Date Prep:
Date Prep:
HAP
ABA
Tech:
Tech:
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
Parameter
0.0000101
0.00266
0.000916
0.0000560
0.000160
0.000744
0.00309
0.000260
Result
Result
BJ
U
U
J
J
J
U
0.00200
0.0100
0.0500
0.00500
0.0500
0.0100
0.0500
0.0200
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
1
1
1
1
1
1
1
1
Dil
Dil
Cas Number
Cas Number
7439-97-6
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
0.0000670
U
0.156
U
0.00224
0.00256
0.00320
U
979955
980071
Seq Number:
Seq Number:
RL
RL
MDL
MDL
10.27.15 08.18
10.28.15 14.39
10.28.15 14.39
10.28.15 14.39
10.28.15 14.39
10.28.15 14.39
10.28.15 14.39
10.28.15 14.39
Analysis Date
Analysis Date
% Moisture:
% Moisture:
Page 16 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 11.15 Date Collected:517846-003Lab Sample Id:
Ground WaterMatrix: MW9Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.160
0.180
0.250
0.110
0.200
0.100
0.250
0.210
0.170
0.140
0.180
0.140
0.180
0.150
0.170
0.170
0.190
0.170
0.210
0.280
0.190
0.320
0.130
0.130
0.260
0.350
0.160
0.210
0.200
0.250
0.170
0.250
0.330
0.150
0.150
0.260
0.160
0.250
0.210
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2.00
1.00
2.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
Analysis Date
% Moisture:
Page 17 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 11.15 Date Collected:517846-003Lab Sample Id:
Ground WaterMatrix: MW9Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter
0.100
0.220
8.00
0.190
0.0800
0.150
0.510
0.180
0.420
0.220
0.170
0.180
0.200
0.210
0.180
0.180
0.160
0.140
0.210
0.110
0.190
0.530
0.720
0.190
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
20.0
1.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
179601-23-1
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
Analysis Date
Surrogate
53-159
30-186
70-130
%
Recovery Flag
%
%
%
87
99
97
10.26.15 16.35
10.26.15 16.35
10.26.15 16.35
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 18 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 11.35 Date Collected:517846-004Lab Sample Id:
Ground WaterMatrix: MW10Sample Id:
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method:
Analytical Method:
ABA
ABA
Analyst:
Analyst:
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
Date Prep:
Date Prep:
HAP
ABA
Tech:
Tech:
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
Parameter
0.0000101
0.00266
0.000916
0.0000560
0.000160
0.000744
0.00309
0.000260
Result
Result
BJ
U
U
J
J
U
U
0.00200
0.0100
0.0500
0.00500
0.0500
0.0100
0.0500
0.0200
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
1
1
1
1
1
1
1
1
Dil
Dil
Cas Number
Cas Number
7439-97-6
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
0.000116
U
0.187
U
0.00432
0.00156
U
U
979955
980071
Seq Number:
Seq Number:
RL
RL
MDL
MDL
10.27.15 08.21
10.28.15 14.41
10.28.15 14.41
10.28.15 14.41
10.28.15 14.41
10.28.15 14.41
10.28.15 14.41
10.28.15 14.41
Analysis Date
Analysis Date
% Moisture:
% Moisture:
Page 19 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 11.35 Date Collected:517846-004Lab Sample Id:
Ground WaterMatrix: MW10Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.160
0.180
0.250
0.110
0.200
0.100
0.250
0.210
0.170
0.140
0.180
0.140
0.180
0.150
0.170
0.170
0.190
0.170
0.210
0.280
0.190
0.320
0.130
0.130
0.260
0.350
0.160
0.210
0.200
0.250
0.170
0.250
0.330
0.150
0.150
0.260
0.160
0.250
0.210
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2.00
1.00
2.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
Analysis Date
% Moisture:
Page 20 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 11.35 Date Collected:517846-004Lab Sample Id:
Ground WaterMatrix: MW10Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter
0.100
0.220
8.00
0.190
0.0800
0.150
0.510
0.180
0.420
0.220
0.170
0.180
0.200
0.210
0.180
0.180
0.160
0.140
0.210
0.110
0.190
0.530
0.720
0.190
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
20.0
1.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
179601-23-1
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
Analysis Date
Surrogate
53-159
30-186
70-130
%
Recovery Flag
%
%
%
90
100
99
10.26.15 16.58
10.26.15 16.58
10.26.15 16.58
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 21 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 13.15 Date Collected:517846-005Lab Sample Id:
Ground WaterMatrix: MW12Sample Id:
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method:
Analytical Method:
ABA
ABA
Analyst:
Analyst:
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
Date Prep:
Date Prep:
HAP
ABA
Tech:
Tech:
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
Parameter
0.0000101
0.00266
0.000916
0.0000560
0.000160
0.000744
0.00309
0.000260
Result
Result
BJ
J
J
J
U
U
0.00200
0.0100
0.0500
0.00500
0.0500
0.0100
0.0500
0.0200
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
1
1
1
1
1
1
1
1
Dil
Dil
Cas Number
Cas Number
7439-97-6
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
0.0000474
0.00792
1.40
0.00224
0.00296
0.0227
U
U
979955
980071
Seq Number:
Seq Number:
RL
RL
MDL
MDL
10.27.15 08.24
10.28.15 14.43
10.28.15 14.43
10.28.15 14.43
10.28.15 14.43
10.28.15 14.43
10.28.15 14.43
10.28.15 14.43
Analysis Date
Analysis Date
% Moisture:
% Moisture:
Page 22 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 13.15 Date Collected:517846-005Lab Sample Id:
Ground WaterMatrix: MW12Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.160
0.180
0.250
0.110
0.200
0.100
0.250
0.210
0.170
0.140
0.180
0.140
0.180
0.150
0.170
0.170
0.190
0.170
0.210
0.280
0.190
0.320
0.130
0.130
0.260
0.350
0.160
0.210
0.200
0.250
0.170
0.250
0.330
0.150
0.150
0.260
0.160
0.250
0.210
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2.00
1.00
2.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
3.22
U
U
U
U
U
U
U
U
U
U
U
U
U
4.73
U
U
U
U
U
U
U
U
3.59
U
U
U
U
U
U
22.1
U
30.8
U
U
U
979967Seq Number:
RL MDL
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
Analysis Date
% Moisture:
Page 23 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 13.15 Date Collected:517846-005Lab Sample Id:
Ground WaterMatrix: MW12Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter
0.100
0.220
8.00
0.190
0.0800
0.150
0.510
0.180
0.420
0.220
0.170
0.180
0.200
0.210
0.180
0.180
0.160
0.140
0.210
0.110
0.190
0.530
0.720
0.190
Result
U
U
U
U
J
J
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
20.0
1.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
179601-23-1
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
0.390
0.840
U
0.430
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
Analysis Date
Surrogate
53-159
30-186
70-130
%
Recovery Flag
%
%
%
90
100
95
10.26.15 17.22
10.26.15 17.22
10.26.15 17.22
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 24 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 10.50 Date Collected:517846-006Lab Sample Id:
Ground WaterMatrix: MW14Sample Id:
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method:
Analytical Method:
ABA
ABA
Analyst:
Analyst:
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
Date Prep:
Date Prep:
HAP
ABA
Tech:
Tech:
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
Parameter
0.0000101
0.00266
0.000916
0.0000560
0.000160
0.000744
0.00309
0.000260
Result
Result
BJ
J
J
J
U
U
0.00200
0.0100
0.0500
0.00500
0.0500
0.0100
0.0500
0.0200
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
1
1
1
1
1
1
1
1
Dil
Dil
Cas Number
Cas Number
7439-97-6
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
0.0000748
0.00432
0.207
0.000520
0.0112
0.0757
U
U
979955
980071
Seq Number:
Seq Number:
RL
RL
MDL
MDL
10.27.15 08.27
10.28.15 14.44
10.28.15 14.44
10.28.15 14.44
10.28.15 14.44
10.28.15 14.44
10.28.15 14.44
10.28.15 14.44
Analysis Date
Analysis Date
% Moisture:
% Moisture:
Page 25 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 10.50 Date Collected:517846-006Lab Sample Id:
Ground WaterMatrix: MW14Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.160
0.180
0.250
0.110
0.200
0.100
0.250
0.210
0.170
0.140
0.180
0.140
0.180
0.150
0.170
0.170
0.190
0.170
0.210
0.280
0.190
0.320
0.130
0.130
0.260
0.350
0.160
0.210
0.200
0.250
0.170
0.250
0.330
0.150
0.150
0.260
0.160
0.250
0.210
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2.00
1.00
2.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
Analysis Date
% Moisture:
Page 26 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 10.50 Date Collected:517846-006Lab Sample Id:
Ground WaterMatrix: MW14Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter
0.100
0.220
8.00
0.190
0.0800
0.150
0.510
0.180
0.420
0.220
0.170
0.180
0.200
0.210
0.180
0.180
0.160
0.140
0.210
0.110
0.190
0.530
0.720
0.190
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
20.0
1.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
179601-23-1
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
Analysis Date
Surrogate
53-159
30-186
70-130
%
Recovery Flag
%
%
%
91
101
97
10.26.15 17.46
10.26.15 17.46
10.26.15 17.46
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 27 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 14.30 Date Collected:517846-007Lab Sample Id:
Ground WaterMatrix: SW2Sample Id:
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method:
Analytical Method:
ABA
ABA
Analyst:
Analyst:
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
10.23.15 10.33
10.28.15 12.48
Date Prep:
Date Prep:
HAP
ABA
Tech:
Tech:
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
Parameter
0.0000101
0.00266
0.000916
0.0000560
0.000160
0.000744
0.00309
0.000260
Result
Result
BJ
U
J
J
U
U
U
0.00200
0.0100
0.0500
0.00500
0.0500
0.0100
0.0500
0.0200
Flag
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
1
1
1
1
1
1
1
1
Dil
Dil
Cas Number
Cas Number
7439-97-6
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
0.0000608
U
0.0803
0.000280
0.00116
U
U
U
979955
980071
Seq Number:
Seq Number:
RL
RL
MDL
MDL
10.27.15 08.30
10.28.15 14.46
10.28.15 14.46
10.28.15 14.46
10.28.15 14.46
10.28.15 14.46
10.28.15 14.46
10.28.15 14.46
Analysis Date
Analysis Date
% Moisture:
% Moisture:
Page 28 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 14.30 Date Collected:517846-007Lab Sample Id:
Ground WaterMatrix: SW2Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.160
0.180
0.250
0.110
0.200
0.100
0.250
0.210
0.170
0.140
0.180
0.140
0.180
0.150
0.170
0.170
0.190
0.170
0.210
0.280
0.190
0.320
0.130
0.130
0.260
0.350
0.160
0.210
0.200
0.250
0.170
0.250
0.330
0.150
0.150
0.260
0.160
0.250
0.210
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2.00
1.00
2.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
Analysis Date
% Moisture:
Page 29 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 14.30 Date Collected:517846-007Lab Sample Id:
Ground WaterMatrix: SW2Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter
0.100
0.220
8.00
0.190
0.0800
0.150
0.510
0.180
0.420
0.220
0.170
0.180
0.200
0.210
0.180
0.180
0.160
0.140
0.210
0.110
0.190
0.530
0.720
0.190
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
20.0
1.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
179601-23-1
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
Analysis Date
Surrogate
53-159
30-186
70-130
%
Recovery Flag
%
%
%
90
101
97
10.26.15 18.10
10.26.15 18.10
10.26.15 18.10
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 30 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 00.00 Date Collected:517846-008Lab Sample Id:
WaterMatrix: Trip BlankSample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.160
0.180
0.250
0.110
0.200
0.100
0.250
0.210
0.170
0.140
0.180
0.140
0.180
0.150
0.170
0.170
0.190
0.170
0.210
0.280
0.190
0.320
0.130
0.130
0.260
0.350
0.160
0.210
0.200
0.250
0.170
0.250
0.330
0.150
0.150
0.260
0.160
0.250
0.210
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2.00
1.00
2.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
Analysis Date
% Moisture:
Page 31 of 45 Final 1.000
Certificate of Analytical Results 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
10.21.15 09.50 Date Received:
10.19.15 00.00 Date Collected:517846-008Lab Sample Id:
WaterMatrix: Trip BlankSample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12.48 Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter
0.100
0.220
8.00
0.190
0.0800
0.150
0.510
0.180
0.420
0.220
0.170
0.180
0.200
0.210
0.180
0.180
0.160
0.140
0.210
0.110
0.190
0.530
0.720
0.190
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
20.0
1.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
179601-23-1
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
RL MDL
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
Analysis Date
Surrogate
53-159
30-186
70-130
%
Recovery Flag
%
%
%
86
101
98
10.26.15 15.24
10.26.15 15.24
10.26.15 15.24
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 32 of 45 Final 1.000
QC Summary 517846
Terraquest Environmental Consultants, P.C.
Lee Co. Landfill
699870-1-BLK
517846-001
517846-001
700082-1-BLK
MB Sample Id:
Parent Sample Id:
Parent Sample Id:
MB Sample Id:
Water
Ground Water
Ground Water
Water
Matrix:
Matrix:
Matrix:
Matrix:
Mercury by SW-846 7470A
Mercury by SW-846 7470A
Mercury by SW-846 7470A
RCRA Metals by SW846-6010C
Analytical Method:
Analytical Method:
Analytical Method:
Analytical Method:
SW7470P
SW7470P
SW7470P
SW3010A_LL
Prep Method:
Prep Method:
Prep Method:
Prep Method:
10.23.15
10.23.15
10.23.15
10.28.15
Date Prep:
Date Prep:
Date Prep:
Date Prep:
Mercury
Mercury
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
Parameter
Parameter
Parameter
%RPD
%RPD
%RPD
%RPD
J
Flag
Flag
Flag
Flag
20
20
20
20
20
20
20
20
20
20
RPD
Limit
RPD
Limit
RPD
Limit
RPD
Limit
3
9
4
0
1
0
1
1
0
1
979955
979955
979955
980071
Seq Number:
Seq Number:
Seq Number:
Seq Number:
10.27.15 07:51
10.27.15 08:00
10.27.15 08:03
10.28.15 14:11
10.28.15 14:11
10.28.15 14:11
10.28.15 14:11
10.28.15 14:11
10.28.15 14:11
10.28.15 14:11
Analysis
Date
Analysis
Date
Analysis
Date
Analysis
Date
Limits
Limits
Limits
85-115
85-115
75-125
75-125
75-125
75-125
75-125
75-125
75-125
LCSD
%Rec
MSD
%Rec
LCSD
%Rec
104
97
102
105
102
103
105
100
89
LCSD
Result
MSD
Result
LCSD
Result
0.00312
0.00300
0.408
0.419
0.408
0.413
0.418
0.401
0.0355
LCS
%Rec
MS
%Rec
LCS
%Rec
101
101
102
106
103
105
106
101
90
0.00303
0.0000807
0.00312
0.407
0.424
0.410
0.419
0.423
0.403
0.0358
Spike
Amount
Spike
Amount
Spike
Amount
0.00300
0.00300
0.400
0.400
0.400
0.400
0.400
0.400
0.0400
MB
Result
Parent
Result
Parent
Result
MB
Result
0.0000180
0.0000882
0.0000882
<0.00266
<0.000916
<0.0000560
0.000400
<0.000744
0.00320
<0.000260
699870-1-BKS
517846-001 D
517846-001 S
700082-1-BKS
LCS Sample Id:
MD Sample Id:
MS Sample Id:
LCS Sample Id:
699870-1-BSD
517846-001 SD
700082-1-BSD
LCSD Sample Id:
MSD Sample Id:
LCSD Sample Id:
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
Units
Units
LCS
Result
MD
Result
MS
Result
LCS
Result
Page 33 of 45 Final 1.000
QC Summary 517846
Terraquest Environmental Consultants, P.C.
Lee Co. Landfill
517846-001
517846-001
Parent Sample Id:
Parent Sample Id:
Ground Water
Ground Water
Matrix:
Matrix:
RCRA Metals by SW846-6010C
RCRA Metals by SW846-6010C
Analytical Method:
Analytical Method:
SW3010A_LL
SW3010A_LL
Prep Method:
Prep Method:
10.28.15
10.28.15
Date Prep:
Date Prep:
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
Parameter
%RPD
%RPD
J
FJ
U
U
Flag
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
RPD
Limit
3
3
5
26
10
0
0
0
1
0
0
0
1
1
980071
980071
Seq Number:
Seq Number:
10.28.15 14:17
10.28.15 14:17
10.28.15 14:17
10.28.15 14:17
10.28.15 14:17
10.28.15 14:17
10.28.15 14:17
10.28.15 14:19
10.28.15 14:19
10.28.15 14:19
10.28.15 14:19
10.28.15 14:19
10.28.15 14:19
10.28.15 14:19
Analysis
Date
Analysis
Date
Limits
75-125
75-125
75-125
75-125
75-125
75-125
75-125
MSD
%Rec
102
99
101
104
102
99
83
MSD
Result
0.423
0.827
0.404
0.427
0.439
0.394
0.0330
MS
%Rec
103
100
101
104
102
97
83
0.0139
0.446
0.000880
0.0147
0.0335
<0.00309
<0.000260
0.424
0.832
0.404
0.427
0.440
0.389
0.0333
Spike
Amount
0.400
0.400
0.400
0.400
0.400
0.400
0.0400
Parent
Result
Parent
Result
0.0135
0.431
0.000840
0.0113
0.0304
<0.00309
<0.000260
0.0135
0.431
0.000840
0.0113
0.0304
<0.00309
<0.000260
517846-001 D
517846-001 S
MD Sample Id:
MS Sample Id:517846-001 SDMSD Sample Id:
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
MD
Result
MS
Result
Page 34 of 45 Final 1.000
QC Summary 517846
Terraquest Environmental Consultants, P.C.
Lee Co. Landfill
700028-1-BLKMB Sample Id:
WaterMatrix:
VOCs by SW-846 8260BAnalytical Method:SW5030BPrep Method:
10.26.15Date Prep:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
3
1
1
3
4
3
2
1
3
3
1
0
2
1
4
2
1
5
4
3
3
4
3
4
4
3
0
1
1
1
0
1
4
4
2
4
1
2
0
2
7
6
3
2
3
4
2
3
2
6
4
2
979967Seq Number:
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
Analysis
Date
Limits
65-130
65-130
75-125
70-135
70-130
75-130
55-140
75-125
65-135
75-130
80-120
70-120
70-130
75-125
75-130
75-125
75-125
75-125
70-130
30-150
75-125
55-130
75-130
75-130
60-135
40-140
80-120
75-125
65-130
75-120
70-130
30-145
65-140
80-120
60-135
60-135
65-135
40-125
70-125
70-130
30-155
65-135
75-125
65-135
75-125
75-130
65-125
55-140
55-140
70-130
70-130
80-120
LCSD
%Rec
99
95
97
83
100
93
98
91
105
106
104
106
80
89
105
107
94
100
102
78
100
84
102
109
81
78
98
93
107
103
97
141
98
105
97
97
93
103
103
95
110
85
100
80
109
109
91
92
81
100
101
113
LCSD
Result
49.3
47.6
48.3
41.3
50.2
46.5
49.1
45.5
52.7
53.0
51.8
53.2
40.2
44.4
52.4
53.7
47.2
50.2
51.2
78.4
50.2
83.9
51.0
54.7
81.4
77.5
49.1
46.7
53.7
51.4
48.7
70.7
49.1
52.3
48.4
48.7
46.5
51.7
51.5
47.3
54.8
1690
49.8
40.1
54.5
109
90.9
46.0
40.7
49.9
50.6
56.3
LCS
%Rec
101
94
95
85
104
96
101
90
108
109
105
106
82
90
109
110
94
106
107
76
103
81
105
114
78
75
98
94
107
104
97
140
102
109
99
93
94
102
103
97
117
80
103
82
113
113
93
95
79
106
105
114
50.7
46.9
47.6
42.4
52.1
48.0
50.3
45.2
54.1
54.5
52.4
53.1
41.2
45.0
54.4
55.0
46.8
52.8
53.3
76.1
51.7
80.6
52.5
57.0
78.2
75.2
49.0
47.1
53.3
51.8
48.7
69.9
51.1
54.3
49.3
46.6
47.2
50.8
51.7
48.3
58.5
1590
51.3
41.0
56.3
113
92.8
47.6
39.7
53.1
52.7
57.2
Spike
Amount
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
100
50.0
100
50.0
50.0
100
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
2000
50.0
50.0
50.0
100
100
50.0
50.0
50.0
50.0
50.0
MB
Result
<0.160
<0.180
<0.250
<0.110
<0.200
<0.100
<0.250
<0.210
<0.170
<0.140
<0.180
<0.140
<0.180
<0.150
<0.170
<0.170
<0.190
<0.170
<0.210
<0.280
<0.190
<0.320
<0.130
<0.130
<0.260
<0.350
<0.160
<0.210
<0.200
<0.250
<0.170
<0.250
<0.330
<0.150
<0.150
<0.260
<0.160
<0.250
<0.210
<0.100
<0.220
<8.00
<0.190
<0.0800
<0.150
<0.510
<0.180
<0.420
<0.220
<0.170
<0.180
<0.200
700028-1-BKSLCS Sample Id:700028-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 35 of 45 Final 1.000
QC Summary 517846
Terraquest Environmental Consultants, P.C.
Lee Co. Landfill
700028-1-BLKMB Sample Id:
WaterMatrix:
VOCs by SW-846 8260BAnalytical Method:SW5030BPrep Method:
10.26.15Date Prep:
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
5
3
4
7
2
3
2
5
4
0
1
979967Seq Number:
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
Analysis
Date
Limits
70-125
65-135
70-130
45-150
75-120
60-140
55-140
70-125
60-145
65-135
50-145
LCSD
%Rec
106
113
111
104
98
100
91
97
94
77
106
LCSD
Result
53.2
56.6
55.7
52.0
49.2
49.8
45.5
48.7
46.9
38.5
53.0
LCS
%Rec
112
116
115
111
100
102
93
103
98
77
107
56.1
58.2
57.7
55.6
50.0
51.1
46.4
51.3
49.0
38.5
53.4
Spike
Amount
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
MB
Result
<0.210
<0.180
<0.180
<0.160
<0.140
<0.210
<0.110
<0.190
<0.530
<0.720
<0.190
700028-1-BKSLCS Sample Id:700028-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate LCSD
Flag
10.26.15 13:49
10.26.15 13:49
10.26.15 13:49
Analysis
Date
Limits
53-159
30-186
70-130
LCSD
%Rec
76
90
93
LCS
%Rec
78
90
94
MB
%Rec
85
99
97
%
%
%
UnitsLCS
Flag
MB
Flag
Page 36 of 45 Final 1.000
QC Summary 517846
Terraquest Environmental Consultants, P.C.
Lee Co. Landfill
517846-001Parent Sample Id:
Ground WaterMatrix:
VOCs by SW-846 8260BAnalytical Method:SW5030BPrep Method:
10.26.15Date Prep:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
Parameter %RPD
X
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
2
6
2
2
3
1
8
3
5
1
5
2
0
3
1
1
0
3
7
4
1
9
1
1
6
5
1
3
5
3
0
6
1
3
1
1
0
1
1
2
1
10
0
3
1
1
1
4
9
3
1
4
979967Seq Number:
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
Analysis
Date
Limits
59-138
63-126
72-115
69-132
62-131
74-123
48-122
59-119
34-131
47-139
66-125
58-124
55-141
78-121
53-129
62-120
66-123
64-114
40-159
50-152
60-129
55-136
64-124
62-121
65-132
40-140
77-118
66-121
64-130
68-125
53-112
63-137
56-138
71-114
53-125
60-137
65-131
48-151
22-185
67-113
38-145
38-162
66-127
59-148
58-127
65-126
58-141
63-150
30-148
63-122
64-127
64-123
MSD
%Rec
85
91
89
74
94
80
81
88
77
84
98
90
74
78
83
90
86
88
72
86
85
91
87
91
83
84
82
81
96
91
89
127
88
93
89
82
82
96
90
74
102
100
86
74
93
95
86
84
79
80
85
96
MSD
Result
42.6
45.7
44.6
36.8
46.8
39.9
40.4
43.8
38.6
42.2
49.0
45.1
37.0
39.1
41.5
45.2
42.8
43.9
35.9
85.7
42.7
90.6
43.3
45.6
83.0
83.5
41.1
40.6
48.1
45.3
44.3
63.6
43.8
46.3
44.3
41.1
41.1
48.1
45.2
36.9
51.0
2000
42.8
36.9
46.4
94.9
85.6
41.8
39.4
39.9
42.4
47.8
MS
%Rec
87
86
88
75
91
79
75
85
74
84
93
89
74
76
82
89
86
86
77
82
85
83
86
90
78
79
83
79
101
93
89
120
88
90
89
83
82
97
89
75
101
91
86
71
92
94
85
87
72
78
84
99
43.3
43.2
43.9
37.6
45.5
39.7
37.4
42.4
36.8
41.8
46.6
44.4
37.0
38.1
41.0
44.7
42.9
42.8
38.4
82.3
42.4
82.7
42.8
45.1
78.3
79.4
41.7
39.3
50.4
46.5
44.5
59.8
44.1
45.1
44.7
41.7
40.9
48.5
44.7
37.5
50.6
1810
42.9
35.7
46.1
94.0
84.9
43.3
36.1
38.8
42.0
49.7
Spike
Amount
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
100
50.0
100
50.0
50.0
100
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
2000
50.0
50.0
50.0
100
100
50.0
50.0
50.0
50.0
50.0
Parent
Result
<0.160
<0.180
<0.250
<0.110
<0.200
<0.100
<0.250
<0.210
<0.170
<0.140
<0.180
<0.140
<0.180
<0.150
<0.170
<0.170
<0.190
<0.170
<0.210
<0.280
<0.190
<0.320
<0.130
<0.130
<0.260
<0.350
<0.160
<0.210
<0.200
<0.250
<0.170
<0.250
<0.330
<0.150
<0.150
<0.260
<0.160
<0.250
<0.210
<0.100
<0.220
<8.00
<0.190
<0.0800
<0.150
<0.510
<0.180
<0.420
<0.220
<0.170
<0.180
<0.200
517846-001 SMS Sample Id:517846-001 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
Page 37 of 45 Final 1.000
QC Summary 517846
Terraquest Environmental Consultants, P.C.
Lee Co. Landfill
517846-001Parent Sample Id:
Ground WaterMatrix:
VOCs by SW-846 8260BAnalytical Method:SW5030BPrep Method:
10.26.15Date Prep:
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
2
2
2
3
0
5
1
3
1
1
4
979967Seq Number:
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
Analysis
Date
Limits
59-124
50-133
58-125
52-125
65-123
65-135
50-125
65-125
51-145
49-135
52-140
MSD
%Rec
91
98
95
88
85
86
78
86
97
61
100
MSD
Result
45.3
49.0
47.7
44.0
42.5
43.2
39.2
42.8
48.6
30.6
50.2
MS
%Rec
89
96
94
85
85
91
79
88
97
60
96
44.4
48.2
46.8
42.7
42.4
45.6
39.7
43.9
48.3
30.2
48.1
Spike
Amount
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
Parent
Result
<0.210
<0.180
<0.180
<0.160
<0.140
<0.210
<0.110
<0.190
<0.530
<0.720
<0.190
517846-001 SMS Sample Id:517846-001 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate MSD
Flag
10.26.15 23:19
10.26.15 23:19
10.26.15 23:19
Analysis
Date
Limits
53-159
30-186
70-130
MSD
%Rec
78
88
90
MS
%Rec
82
87
88
%
%
%
UnitsMS
Flag
Page 38 of 45 Final 1.000
Blank Summary 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
699870-1-BLKLab Sample Id:
WATERMatrix: 699870-1-BLK Sample Id:
Mercury by SW-846 7470A Analytical Method:
ABAAnalyst:
SW7470PPrep Method:
10.23.15 10:33Date Prep:
HAPTech:
Mercury
Parameter
0.0000101
Result
J0.00200
Flag
mg/L
Units
1
DilCas Number
7439-97-6 0.0000180
979955Seq Number:
MDLRL
10.27.15 07:48
Analysis
Date
Page 39 of 45 Final 1.000
Blank Summary 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
700028-1-BLKLab Sample Id:
WATERMatrix: 700028-1-BLK Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12:48Date Prep:
MWETech:
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Parameter
0.160
0.180
0.250
0.110
0.200
0.100
0.250
0.210
0.170
0.140
0.180
0.140
0.180
0.150
0.170
0.170
0.190
0.170
0.210
0.280
0.190
0.320
0.130
0.130
0.260
0.350
0.160
0.210
0.200
0.250
0.170
0.250
0.330
0.150
0.150
0.260
0.160
0.250
0.210
0.100
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2.00
1.00
2.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
MDLRL
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
Analysis
Date
Page 40 of 45 Final 1.000
Blank Summary 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
700028-1-BLKLab Sample Id:
WATERMatrix: 700028-1-BLK Sample Id:
VOCs by SW-846 8260B Analytical Method:
ZHOAnalyst:
SW5030BPrep Method:
10.26.15 12:48Date Prep:
MWETech:
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
m,p-Xylenes
Methyl tert-butyl ether
Methylene chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Parameter
0.220
8.00
0.190
0.0800
0.150
0.510
0.180
0.420
0.220
0.170
0.180
0.200
0.210
0.180
0.180
0.160
0.140
0.210
0.110
0.190
0.530
0.720
0.190
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
20.0
1.00
1.00
1.00
2.00
2.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
179601-23-1
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
979967Seq Number:
MDLRL
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
10.26.15 15:00
Analysis
Date
Page 41 of 45 Final 1.000
Blank Summary 517846
Terraquest Environmental Consultants, P.C., Mebane, NC
Lee Co. Landfill
700082-1-BLKLab Sample Id:
WATERMatrix: 700082-1-BLK Sample Id:
RCRA Metals by SW846-6010C Analytical Method:
ABAAnalyst:
SW3010A_LLPrep Method:
10.28.15 12:48Date Prep:
ABATech:
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
0.00266
0.000916
0.0000560
0.000160
0.000744
0.00309
0.000260
Result
U
U
U
J
U
J
U
0.0100
0.0500
0.00500
0.0500
0.0100
0.0500
0.0500
Flag
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
1
1
1
1
1
1
1
DilCas Number
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
U
U
U
0.000400
U
0.00320
U
980071Seq Number:
MDLRL
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Analysis
Date
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Prelogin/Nonconformance Report- Sample Log-In
XENCO Laboratories
517846Work Order #:
10/21/2015 09:50:00 AMDate/ Time Received:
Terraquest Environmental Consultants, PClient:
Sample Receipt Checklist
Checklist completed by: Date:
Checklist reviewed by:Date:
Debbie Simmons
10/21/2015
10/26/2015
#2 *Shipping container in good condition?
#3 *Samples received on ice?
#4 *Custody Seals intact on shipping container/ cooler?
#5 Custody Seals intact on sample bottles?
#6 *Custody Seals Signed and dated?
#7 *Chain of Custody present?
#8 Sample instructions complete on Chain of Custody?
#9 Any missing/extra samples?
#10 Chain of Custody signed when relinquished/ received?
#11 Chain of Custody agrees with sample label(s)?
#12 Container label(s) legible and intact?
#13 Sample matrix/ properties agree with Chain of Custody?
#14 Samples in proper container/ bottle?
#15 Samples properly preserved?
#16 Sample container(s) intact?
#17 Sufficient sample amount for indicated test(s)?
#18 All samples received within hold time?
#19 Subcontract of sample(s)?
#20 VOC samples have zero headspace (less than 1/4 inch bubble)?
#21 <2 for all samples preserved with HNO3,HCL, H2SO4? Except for
samples for the analysis of HEM or HEM-SGT which are verified by the
analysts.
#22 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH?
Yes
Yes
N/A
N/A
N/A
Yes
Yes
No
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
Yes
N/A

#1 *Temperature of cooler(s)?2.2
Acceptable Temperature Range: 0 - 6 degC
Air and Metal samples Acceptable Range: Ambient
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: PH Device/Lot#:DL I016662-9
Comments
Dario Lagunas
Temperature Measuring device used : #61
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