WS-29804_48908_CA_UST61_20230308

#=CL#
March 03, 2023
LIMS USE: FR - JOE BEST
LIMS OBJECT ID: 92653415
92653415
Project:
Pace Project No.:
RE:
Mr. Joe Best
Best Geological & Environmental Consulting
1009 Hayfield Lane
Greensboro, NC 27410
Best Geo - Last Minute Market
Dear Mr. Best:
Enclosed are the analytical results for sample(s) received by the laboratory on February 22, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
Project Manager
704-977-0981
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 38
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 38
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92653415001 W1 EPA 504.1 2 PASI-CHH
MADEP EPH 7 PASI-CBAJ
EPA 200.8 Rev 5.4 1 PASI-ACRW
EPA 625.1 58 PASI-CPKS
SM 6200B 64 PASI-CSAS
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Sample:W1 Lab ID:92653415001 Collected:02/21/23 10:10 Received:02/22/23 11:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)0.092 ug/L 03/02/23 03:55 106-93-403/01/23 11:100.020 1
Surrogates
1-Chloro-2-bromopropane (S)99 %03/02/23 03:55 301-79-5603/01/23 11:1070-130 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 02/27/23 15:11 N202/24/23 16:201001
Aliphatic (C19-C36)ND ug/L 02/27/23 15:11 N202/24/23 16:201001
Aromatic (C11-C22)ND ug/L 02/27/23 15:11 N202/24/23 16:201001
Surrogates
1-Chlorooctadecane (S)55 %02/27/23 15:11 3386-33-202/24/23 16:2040-140 1
o-Terphenyl (S)72 %02/27/23 15:11 84-15-102/24/23 16:2040-140 1
2-Fluorobiphenyl (S)89 %02/27/23 15:11 321-60-802/24/23 16:2040-140 1
2-Bromonaphthalene (S)90 %02/27/23 15:11 580-13-202/24/23 16:2040-140 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4
Pace Analytical Services - Asheville
200.8 MET ICPMS
Lead 1.2 ug/L 02/26/23 21:14 7439-92-102/25/23 10:241.0 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 02/25/23 15:59 83-32-902/24/23 16:164.2 1
Acenaphthylene ND ug/L 02/25/23 15:59 208-96-802/24/23 16:164.2 1
Anthracene ND ug/L 02/25/23 15:59 120-12-702/24/23 16:164.2 1
Benzo(a)anthracene ND ug/L 02/25/23 15:59 56-55-302/24/23 16:164.2 1
Benzo(a)pyrene ND ug/L 02/25/23 15:59 50-32-802/24/23 16:164.2 1
Benzo(b)fluoranthene ND ug/L 02/25/23 15:59 205-99-202/24/23 16:164.2 1
Benzo(g,h,i)perylene ND ug/L 02/25/23 15:59 191-24-202/24/23 16:164.2 1
Benzo(k)fluoranthene ND ug/L 02/25/23 15:59 207-08-902/24/23 16:164.2 1
4-Bromophenylphenyl ether ND ug/L 02/25/23 15:59 101-55-302/24/23 16:164.2 1
Butylbenzylphthalate ND ug/L 02/25/23 15:59 85-68-702/24/23 16:164.2 1
4-Chloro-3-methylphenol ND ug/L 02/25/23 15:59 59-50-702/24/23 16:164.2 1
bis(2-Chloroethoxy)methane ND ug/L 02/25/23 15:59 111-91-102/24/23 16:168.3 1
bis(2-Chloroethyl) ether ND ug/L 02/25/23 15:59 111-44-402/24/23 16:164.2 1
2-Chloronaphthalene ND ug/L 02/25/23 15:59 91-58-702/24/23 16:164.2 1
2-Chlorophenol ND ug/L 02/25/23 15:59 95-57-802/24/23 16:164.2 1
4-Chlorophenylphenyl ether ND ug/L 02/25/23 15:59 7005-72-302/24/23 16:164.2 1
Chrysene ND ug/L 02/25/23 15:59 218-01-902/24/23 16:164.2 1
Dibenz(a,h)anthracene ND ug/L 02/25/23 15:59 53-70-302/24/23 16:164.2 1
3,3'-Dichlorobenzidine ND ug/L 02/25/23 15:59 91-94-102/24/23 16:168.3 1
2,4-Dichlorophenol ND ug/L 02/25/23 15:59 120-83-202/24/23 16:164.2 1
Diethylphthalate ND ug/L 02/25/23 15:59 84-66-202/24/23 16:164.2 1
2,4-Dimethylphenol ND ug/L 02/25/23 15:59 105-67-9 L102/24/23 16:168.3 1
Dimethylphthalate ND ug/L 02/25/23 15:59 131-11-302/24/23 16:164.2 1
Di-n-butylphthalate ND ug/L 02/25/23 15:59 84-74-202/24/23 16:164.2 1
4,6-Dinitro-2-methylphenol ND ug/L 02/25/23 15:59 534-52-102/24/23 16:168.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Sample:W1 Lab ID:92653415001 Collected:02/21/23 10:10 Received:02/22/23 11:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
2,4-Dinitrophenol ND ug/L 02/25/23 15:59 51-28-502/24/23 16:1641.7 1
2,4-Dinitrotoluene ND ug/L 02/25/23 15:59 121-14-202/24/23 16:164.2 1
2,6-Dinitrotoluene ND ug/L 02/25/23 15:59 606-20-202/24/23 16:164.2 1
Di-n-octylphthalate ND ug/L 02/25/23 15:59 117-84-002/24/23 16:164.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 02/25/23 15:59 117-81-702/24/23 16:164.2 1
Fluoranthene ND ug/L 02/25/23 15:59 206-44-002/24/23 16:164.2 1
Fluorene ND ug/L 02/25/23 15:59 86-73-702/24/23 16:164.2 1
Hexachloro-1,3-butadiene ND ug/L 02/25/23 15:59 87-68-302/24/23 16:164.2 1
Hexachlorobenzene ND ug/L 02/25/23 15:59 118-74-102/24/23 16:164.2 1
Hexachlorocyclopentadiene ND ug/L 02/25/23 15:59 77-47-402/24/23 16:168.3 1
Hexachloroethane ND ug/L 02/25/23 15:59 67-72-102/24/23 16:164.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 02/25/23 15:59 193-39-502/24/23 16:164.2 1
Isophorone ND ug/L 02/25/23 15:59 78-59-102/24/23 16:168.3 1
2-Methylnaphthalene ND ug/L 02/25/23 15:59 91-57-602/24/23 16:164.2 1
Naphthalene ND ug/L 02/25/23 15:59 91-20-302/24/23 16:164.2 1
Nitrobenzene ND ug/L 02/25/23 15:59 98-95-302/24/23 16:164.2 1
2-Nitrophenol ND ug/L 02/25/23 15:59 88-75-502/24/23 16:164.2 1
4-Nitrophenol ND ug/L 02/25/23 15:59 100-02-702/24/23 16:168.3 1
N-Nitrosodimethylamine ND ug/L 02/25/23 15:59 62-75-902/24/23 16:164.2 1
N-Nitroso-di-n-propylamine ND ug/L 02/25/23 15:59 621-64-702/24/23 16:164.2 1
N-Nitrosodiphenylamine ND ug/L 02/25/23 15:59 86-30-602/24/23 16:168.3 1
Pentachlorophenol ND ug/L 02/25/23 15:59 87-86-502/24/23 16:168.3 1
Phenanthrene ND ug/L 02/25/23 15:59 85-01-802/24/23 16:164.2 1
Phenol ND ug/L 02/25/23 15:59 108-95-202/24/23 16:164.2 1
Pyrene ND ug/L 02/25/23 15:59 129-00-002/24/23 16:164.2 1
1,2,4-Trichlorobenzene ND ug/L 02/25/23 15:59 120-82-102/24/23 16:164.2 1
2,4,6-Trichlorophenol ND ug/L 02/25/23 15:59 88-06-202/24/23 16:168.3 1
Surrogates
Nitrobenzene-d5 (S)99 %02/25/23 15:59 4165-60-002/24/23 16:1610-120 1
2-Fluorobiphenyl (S)80 %02/25/23 15:59 321-60-802/24/23 16:1615-120 1
Terphenyl-d14 (S)114 %02/25/23 15:59 1718-51-002/24/23 16:1611-131 1
Phenol-d6 (S)55 %02/25/23 15:59 13127-88-302/24/23 16:1610-120 1
2-Fluorophenol (S)62 %02/25/23 15:59 367-12-402/24/23 16:1610-120 1
2,4,6-Tribromophenol (S)91 %02/25/23 15:59 118-79-602/24/23 16:1610-137 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/24/23 21:33 71-43-20.50 1
Bromobenzene ND ug/L 02/24/23 21:33 108-86-10.50 1
Bromochloromethane ND ug/L 02/24/23 21:33 74-97-50.50 1
Bromodichloromethane ND ug/L 02/24/23 21:33 75-27-40.50 1
Bromoform ND ug/L 02/24/23 21:33 75-25-20.50 1
Bromomethane ND ug/L 02/24/23 21:33 74-83-95.0 1
n-Butylbenzene ND ug/L 02/24/23 21:33 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/24/23 21:33 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/24/23 21:33 98-06-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Sample:W1 Lab ID:92653415001 Collected:02/21/23 10:10 Received:02/22/23 11:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Carbon tetrachloride ND ug/L 02/24/23 21:33 56-23-50.50 1
Chlorobenzene ND ug/L 02/24/23 21:33 108-90-70.50 1
Chloroethane ND ug/L 02/24/23 21:33 75-00-31.0 1
Chloroform ND ug/L 02/24/23 21:33 67-66-30.50 1
Chloromethane ND ug/L 02/24/23 21:33 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/24/23 21:33 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/24/23 21:33 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/24/23 21:33 96-12-81.0 1
Dibromochloromethane ND ug/L 02/24/23 21:33 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/24/23 21:33 106-93-40.50 1
Dibromomethane ND ug/L 02/24/23 21:33 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/24/23 21:33 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/24/23 21:33 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/24/23 21:33 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/24/23 21:33 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/24/23 21:33 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/24/23 21:33 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/24/23 21:33 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/24/23 21:33 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/24/23 21:33 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/24/23 21:33 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/24/23 21:33 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/24/23 21:33 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/24/23 21:33 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/24/23 21:33 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/24/23 21:33 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/24/23 21:33 108-20-30.50 1
Ethylbenzene ND ug/L 02/24/23 21:33 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/24/23 21:33 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/24/23 21:33 98-82-80.50 1
p-Isopropyltoluene ND ug/L 02/24/23 21:33 99-87-60.50 1
Methylene Chloride ND ug/L 02/24/23 21:33 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/24/23 21:33 1634-04-40.50 1
Naphthalene ND ug/L 02/24/23 21:33 91-20-32.0 1
n-Propylbenzene ND ug/L 02/24/23 21:33 103-65-10.50 1
Styrene ND ug/L 02/24/23 21:33 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/24/23 21:33 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/24/23 21:33 79-34-50.50 1
Tetrachloroethene ND ug/L 02/24/23 21:33 127-18-40.50 1
Toluene ND ug/L 02/24/23 21:33 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/24/23 21:33 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/24/23 21:33 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/24/23 21:33 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/24/23 21:33 79-00-50.50 1
Trichloroethene ND ug/L 02/24/23 21:33 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/24/23 21:33 75-69-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Sample:W1 Lab ID:92653415001 Collected:02/21/23 10:10 Received:02/22/23 11:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,3-Trichloropropane ND ug/L 02/24/23 21:33 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/24/23 21:33 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/24/23 21:33 108-67-80.50 1
Vinyl chloride ND ug/L 02/24/23 21:33 75-01-41.0 1
m&p-Xylene ND ug/L 02/24/23 21:33 179601-23-11.0 1
o-Xylene ND ug/L 02/24/23 21:33 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %02/24/23 21:33 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %02/24/23 21:33 460-00-470-130 1
Toluene-d8 (S)104 %02/24/23 21:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
758119
EPA 200.8 Rev 5.4
EPA 200.8 Rev 5.4
200.8 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92653415001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3938239
Associated Lab Samples:92653415001
Matrix:Water
Analyzed
Lead ug/L ND 1.0 02/26/23 20:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3938240LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 52.050 104 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3938241MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92645044001
3938242
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L 50 105 70-130107 150ND52.8 53.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
757939
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653415001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3937273
Associated Lab Samples:92653415001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/24/23 16:08
1,1,1-Trichloroethane ug/L ND 0.50 02/24/23 16:08
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/24/23 16:08
1,1,2-Trichloroethane ug/L ND 0.50 02/24/23 16:08
1,1-Dichloroethane ug/L ND 0.50 02/24/23 16:08
1,1-Dichloroethene ug/L ND 0.50 02/24/23 16:08
1,1-Dichloropropene ug/L ND 0.50 02/24/23 16:08
1,2,3-Trichlorobenzene ug/L ND 2.0 02/24/23 16:08
1,2,3-Trichloropropane ug/L ND 0.50 02/24/23 16:08
1,2,4-Trichlorobenzene ug/L ND 2.0 02/24/23 16:08
1,2,4-Trimethylbenzene ug/L ND 0.50 02/24/23 16:08
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/24/23 16:08
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/24/23 16:08
1,2-Dichlorobenzene ug/L ND 0.50 02/24/23 16:08
1,2-Dichloroethane ug/L ND 0.50 02/24/23 16:08
1,2-Dichloropropane ug/L ND 0.50 02/24/23 16:08
1,3,5-Trimethylbenzene ug/L ND 0.50 02/24/23 16:08
1,3-Dichlorobenzene ug/L ND 0.50 02/24/23 16:08
1,3-Dichloropropane ug/L ND 0.50 02/24/23 16:08
1,4-Dichlorobenzene ug/L ND 0.50 02/24/23 16:08
2,2-Dichloropropane ug/L ND 0.50 02/24/23 16:08
2-Chlorotoluene ug/L ND 0.50 02/24/23 16:08
4-Chlorotoluene ug/L ND 0.50 02/24/23 16:08
Benzene ug/L ND 0.50 02/24/23 16:08
Bromobenzene ug/L ND 0.50 02/24/23 16:08
Bromochloromethane ug/L ND 0.50 02/24/23 16:08
Bromodichloromethane ug/L ND 0.50 02/24/23 16:08
Bromoform ug/L ND 0.50 02/24/23 16:08
Bromomethane ug/L ND 5.0 02/24/23 16:08
Carbon tetrachloride ug/L ND 0.50 02/24/23 16:08
Chlorobenzene ug/L ND 0.50 02/24/23 16:08
Chloroethane ug/L ND 1.0 02/24/23 16:08
Chloroform ug/L ND 0.50 02/24/23 16:08
Chloromethane ug/L ND 1.0 02/24/23 16:08
cis-1,2-Dichloroethene ug/L ND 0.50 02/24/23 16:08
cis-1,3-Dichloropropene ug/L ND 0.50 02/24/23 16:08
Dibromochloromethane ug/L ND 0.50 02/24/23 16:08
Dibromomethane ug/L ND 0.50 02/24/23 16:08
Dichlorodifluoromethane ug/L ND 0.50 02/24/23 16:08
Diisopropyl ether ug/L ND 0.50 02/24/23 16:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3937273
Associated Lab Samples:92653415001
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 02/24/23 16:08
Hexachloro-1,3-butadiene ug/L ND 2.0 02/24/23 16:08
Isopropylbenzene (Cumene)ug/L ND 0.50 02/24/23 16:08
m&p-Xylene ug/L ND 1.0 02/24/23 16:08
Methyl-tert-butyl ether ug/L ND 0.50 02/24/23 16:08
Methylene Chloride ug/L ND 2.0 02/24/23 16:08
n-Butylbenzene ug/L ND 0.50 02/24/23 16:08
n-Propylbenzene ug/L ND 0.50 02/24/23 16:08
Naphthalene ug/L ND 2.0 02/24/23 16:08
o-Xylene ug/L ND 0.50 02/24/23 16:08
p-Isopropyltoluene ug/L ND 0.50 02/24/23 16:08
sec-Butylbenzene ug/L ND 0.50 02/24/23 16:08
Styrene ug/L ND 0.50 02/24/23 16:08
tert-Butylbenzene ug/L ND 0.50 02/24/23 16:08
Tetrachloroethene ug/L ND 0.50 02/24/23 16:08
Toluene ug/L ND 0.50 02/24/23 16:08
trans-1,2-Dichloroethene ug/L ND 0.50 02/24/23 16:08
trans-1,3-Dichloropropene ug/L ND 0.50 02/24/23 16:08
Trichloroethene ug/L ND 0.50 02/24/23 16:08
Trichlorofluoromethane ug/L ND 1.0 02/24/23 16:08
Vinyl chloride ug/L ND 1.0 02/24/23 16:08
1,2-Dichloroethane-d4 (S)%99 70-130 02/24/23 16:08
4-Bromofluorobenzene (S)%97 70-130 02/24/23 16:08
Toluene-d8 (S)%101 70-130 02/24/23 16:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3937274LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.220 101 60-140
1,1,1-Trichloroethane ug/L 23.620 118 60-140
1,1,2,2-Tetrachloroethane ug/L 20.420 102 60-140
1,1,2-Trichloroethane ug/L 21.320 107 60-140
1,1-Dichloroethane ug/L 21.820 109 60-140
1,1-Dichloroethene ug/L 23.920 120 60-140
1,1-Dichloropropene ug/L 24.720 123 60-140
1,2,3-Trichlorobenzene ug/L 18.920 94 60-140
1,2,3-Trichloropropane ug/L 19.220 96 60-140
1,2,4-Trichlorobenzene ug/L 17.820 89 60-140
1,2,4-Trimethylbenzene ug/L 20.220 101 60-140
1,2-Dibromo-3-chloropropane ug/L 18.620 93 60-140
1,2-Dibromoethane (EDB)ug/L 20.220 101 60-140
1,2-Dichlorobenzene ug/L 19.320 96 60-140
1,2-Dichloroethane ug/L 23.120 115 60-140
1,2-Dichloropropane ug/L 21.720 108 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3937274LABORATORY CONTROL SAMPLE:
LCSSpike
1,3,5-Trimethylbenzene ug/L 19.520 98 60-140
1,3-Dichlorobenzene ug/L 19.220 96 60-140
1,3-Dichloropropane ug/L 20.220 101 60-140
1,4-Dichlorobenzene ug/L 19.420 97 60-140
2,2-Dichloropropane ug/L 24.320 122 60-140
2-Chlorotoluene ug/L 20.120 101 60-140
4-Chlorotoluene ug/L 19.320 97 60-140
Benzene ug/L 20.520 102 60-140
Bromobenzene ug/L 18.920 94 60-140
Bromochloromethane ug/L 22.820 114 60-140
Bromodichloromethane ug/L 21.820 109 60-140
Bromoform ug/L 20.620 103 60-140
Bromomethane ug/L 16.420 82 60-140
Carbon tetrachloride ug/L 21.720 108 60-140
Chlorobenzene ug/L 20.020 100 60-140
Chloroethane ug/L 24.320 121 60-140
Chloroform ug/L 23.020 115 60-140
Chloromethane ug/L 19.420 97 60-140
cis-1,2-Dichloroethene ug/L 23.420 117 60-140
cis-1,3-Dichloropropene ug/L 21.420 107 60-140
Dibromochloromethane ug/L 20.220 101 60-140
Dibromomethane ug/L 21.820 109 60-140
Dichlorodifluoromethane ug/L 14.920 74 60-140
Diisopropyl ether ug/L 20.220 101 60-140
Ethylbenzene ug/L 19.320 96 60-140
Hexachloro-1,3-butadiene ug/L 18.120 90 60-140
Isopropylbenzene (Cumene)ug/L 19.420 97 60-140
m&p-Xylene ug/L 40.140 100 60-140
Methyl-tert-butyl ether ug/L 22.020 110 60-140
Methylene Chloride ug/L 23.120 115 60-140
n-Butylbenzene ug/L 20.320 102 60-140
n-Propylbenzene ug/L 19.420 97 60-140
Naphthalene ug/L 19.220 96 60-140
o-Xylene ug/L 20.220 101 60-140
p-Isopropyltoluene ug/L 20.320 101 60-140
sec-Butylbenzene ug/L 19.420 97 60-140
Styrene ug/L 21.120 106 60-140
tert-Butylbenzene ug/L 15.920 79 60-140
Tetrachloroethene ug/L 17.920 89 60-140
Toluene ug/L 20.420 102 60-140
trans-1,2-Dichloroethene ug/L 24.020 120 60-140
trans-1,3-Dichloropropene ug/L 21.420 107 60-140
Trichloroethene ug/L 21.520 107 60-140
Trichlorofluoromethane ug/L 19.520 97 60-140
Vinyl chloride ug/L 20.820 104 60-140
1,2-Dichloroethane-d4 (S)%111 70-130
4-Bromofluorobenzene (S)%106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3937274LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3937275MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653764004
3937276
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 96 60-140109 1220ND19.3 21.7
1,1,1-Trichloroethane ug/L 20 95 60-140114 1820ND19.0 22.7
1,1,2,2-Tetrachloroethane ug/L 20 87 60-140106 2020ND17.4 21.2
1,1,2-Trichloroethane ug/L 20 87 60-140106 2020ND17.3 21.3
1,1-Dichloroethane ug/L 20 87 60-140103 1720ND17.4 20.7
1,1-Dichloroethene ug/L 20 96 60-140117 1920ND19.3 23.3
1,1-Dichloropropene ug/L 20 104 60-140127 1920ND20.9 25.4
1,2,3-Trichlorobenzene ug/L 20 89 60-140111 2220ND17.8 22.2
1,2,3-Trichloropropane ug/L 20 75 60-14087 1420ND15.1 17.4
1,2,4-Trichlorobenzene ug/L 20 89 60-140107 1720ND17.9 21.3
1,2,4-Trimethylbenzene ug/L 20 95 60-140111 15201.9 20.9 24.2
1,2-Dibromo-3-chloropropane ug/L 20 92 60-140109 1720ND18.3 21.7
1,2-Dibromoethane (EDB)ug/L 20 93 60-140102 1020ND18.5 20.4
1,2-Dichlorobenzene ug/L 20 90 60-140105 1620ND17.9 21.1
1,2-Dichloroethane ug/L 20 87 60-140104 1720ND17.5 20.7
1,2-Dichloropropane ug/L 20 90 60-140109 1920ND18.0 21.8
1,3,5-Trimethylbenzene ug/L 20 95 60-140109 1320ND19.1 21.8
1,3-Dichlorobenzene ug/L 20 90 60-140106 1720ND18.0 21.2
1,3-Dichloropropane ug/L 20 89 60-140106 1820ND17.8 21.3
1,4-Dichlorobenzene ug/L 20 88 60-140105 1820ND17.6 21.0
2,2-Dichloropropane ug/L 20 96 60-140116 2020ND19.1 23.3
2-Chlorotoluene ug/L 20 88 60-140105 1820ND17.6 21.1
4-Chlorotoluene ug/L 20 92 60-140107 1620ND18.3 21.4
Benzene ug/L 20 91 60-140106 13204.5 22.6 25.8
Bromobenzene ug/L 20 90 60-140104 1520ND17.9 20.8
Bromochloromethane ug/L 20 87 60-140104 1820ND17.4 20.9
Bromodichloromethane ug/L 20 90 60-140109 1920ND18.0 21.8
Bromoform ug/L 20 93 60-140113 1920ND18.6 22.5
Bromomethane ug/L M1205960-14069 1620ND11.7 13.7
Carbon tetrachloride ug/L 20 104 60-140116 1120ND20.8 23.1
Chlorobenzene ug/L 20 90 60-140105 1620ND17.9 21.0
Chloroethane ug/L 20 94 60-140117 2220ND18.8 23.4
Chloroform ug/L 20 90 60-140107 1720ND18.0 21.4
Chloromethane ug/L 20 79 60-14092 1620ND15.8 18.4
cis-1,2-Dichloroethene ug/L 20 90 60-140107 1720ND18.1 21.5
cis-1,3-Dichloropropene ug/L 20 92 60-140110 1720ND18.5 22.0
Dibromochloromethane ug/L 20 95 60-140106 1020ND19.1 21.1
Dibromomethane ug/L 20 90 60-140102 1320ND17.9 20.4
Dichlorodifluoromethane ug/L M1205760-14068 1720ND11.4 13.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3937275MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653764004
3937276
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diisopropyl ether ug/L 20 81 60-140100 112014.8 31.1 34.7
Ethylbenzene ug/L 20 90 60-140103 9209.1 27.2 29.8
Hexachloro-1,3-butadiene ug/L 20 106 60-140116 920ND21.2 23.2
Isopropylbenzene (Cumene)ug/L 20 96 60-140109 1320ND19.2 21.8
m&p-Xylene ug/L 40 93 60-140105 11405.1 42.3 47.0
Methyl-tert-butyl ether ug/L 20 93 60-140115 15208.3 27.0 31.3
Methylene Chloride ug/L 20 82 60-140101 2120ND16.3 20.2
n-Butylbenzene ug/L 20 102 60-140119 1520ND20.4 23.8
n-Propylbenzene ug/L 20 95 60-140109 13200.54 19.5 22.3
Naphthalene ug/L 20 90 60-140110 19201.7J 19.6 23.6
o-Xylene ug/L 20 92 60-140107 15200.38J 18.9 21.9
p-Isopropyltoluene ug/L 20 102 60-140115 1220ND20.4 23.0
sec-Butylbenzene ug/L 20 98 60-140111 1320ND19.6 22.3
Styrene ug/L 20 94 60-140111 1720ND18.8 22.2
tert-Butylbenzene ug/L 20 80 60-14095 1720ND16.0 18.9
Tetrachloroethene ug/L 20 91 60-140108 1620ND18.3 21.5
Toluene ug/L 20 86 60-140102 1720ND17.2 20.3
trans-1,2-Dichloroethene ug/L 20 96 60-140112 1620ND19.2 22.5
trans-1,3-Dichloropropene ug/L 20 91 60-140109 1820ND18.1 21.8
Trichloroethene ug/L 20 99 60-140119 1820ND19.7 23.7
Trichlorofluoromethane ug/L 20 87 60-140102 1620ND17.4 20.4
Vinyl chloride ug/L 20 85 60-14098 1420ND16.9 19.5
1,2-Dichloroethane-d4 (S)%99 70-130100
4-Bromofluorobenzene (S)%97 70-130101
Toluene-d8 (S)%95 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
758661
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653415001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3940602
Associated Lab Samples:92653415001
Matrix:Water
Analyzed
1,2-Dibromoethane (EDB)ug/L ND 0.020 03/02/23 03:12
1-Chloro-2-bromopropane (S)%94 70-130 03/02/23 03:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3940603LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3940604
1,2-Dibromoethane (EDB)ug/L 0.230.25 91 70-130950.24 5 20
1-Chloro-2-bromopropane (S)%93 70-13097
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3940606MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92654121003
3940607
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2-Dibromoethane (EDB)ug/L 0.25 91 65-13595 40.25ND 0.23 0.23
1-Chloro-2-bromopropane (S)%92 70-13096
Parameter Units
Dup
Result QualifiersRPDResult
92654121001
3940605SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L NDND
1-Chloro-2-bromopropane (S)%8993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
757737
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653415001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3936243
Associated Lab Samples:92653415001
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 02/23/23 21:44
2,4,6-Trichlorophenol ug/L ND 10.0 02/23/23 21:44
2,4-Dichlorophenol ug/L ND 5.0 02/23/23 21:44
2,4-Dimethylphenol ug/L ND 10.0 02/23/23 21:44
2,4-Dinitrophenol ug/L ND 50.0 02/23/23 21:44
2,4-Dinitrotoluene ug/L ND 5.0 02/23/23 21:44
2,6-Dinitrotoluene ug/L ND 5.0 02/23/23 21:44
2-Chloronaphthalene ug/L ND 5.0 02/23/23 21:44
2-Chlorophenol ug/L ND 5.0 02/23/23 21:44
2-Methylnaphthalene ug/L ND 5.0 02/23/23 21:44
2-Nitrophenol ug/L ND 5.0 02/23/23 21:44
3,3'-Dichlorobenzidine ug/L ND 10.0 02/23/23 21:44
4,6-Dinitro-2-methylphenol ug/L ND 10.0 02/23/23 21:44
4-Bromophenylphenyl ether ug/L ND 5.0 02/23/23 21:44
4-Chloro-3-methylphenol ug/L ND 5.0 02/23/23 21:44
4-Chlorophenylphenyl ether ug/L ND 5.0 02/23/23 21:44
4-Nitrophenol ug/L ND 10.0 02/23/23 21:44
Acenaphthene ug/L ND 5.0 02/23/23 21:44
Acenaphthylene ug/L ND 5.0 02/23/23 21:44
Anthracene ug/L ND 5.0 02/23/23 21:44
Benzo(a)anthracene ug/L ND 5.0 02/23/23 21:44
Benzo(a)pyrene ug/L ND 5.0 02/23/23 21:44
Benzo(b)fluoranthene ug/L ND 5.0 02/23/23 21:44
Benzo(g,h,i)perylene ug/L ND 5.0 02/23/23 21:44
Benzo(k)fluoranthene ug/L ND 5.0 02/23/23 21:44
bis(2-Chloroethoxy)methane ug/L ND 10.0 02/23/23 21:44
bis(2-Chloroethyl) ether ug/L ND 5.0 02/23/23 21:44
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 02/23/23 21:44
Butylbenzylphthalate ug/L ND 5.0 02/23/23 21:44
Chrysene ug/L ND 5.0 02/23/23 21:44
Di-n-butylphthalate ug/L ND 5.0 02/23/23 21:44
Di-n-octylphthalate ug/L ND 5.0 02/23/23 21:44
Dibenz(a,h)anthracene ug/L ND 5.0 02/23/23 21:44
Diethylphthalate ug/L ND 5.0 02/23/23 21:44
Dimethylphthalate ug/L ND 5.0 02/23/23 21:44
Fluoranthene ug/L ND 5.0 02/23/23 21:44
Fluorene ug/L ND 5.0 02/23/23 21:44
Hexachloro-1,3-butadiene ug/L ND 5.0 02/23/23 21:44
Hexachlorobenzene ug/L ND 5.0 02/23/23 21:44
Hexachlorocyclopentadiene ug/L ND 10.0 02/23/23 21:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3936243
Associated Lab Samples:92653415001
Matrix:Water
Analyzed
Hexachloroethane ug/L ND 5.0 02/23/23 21:44
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 02/23/23 21:44
Isophorone ug/L ND 10.0 02/23/23 21:44
N-Nitroso-di-n-propylamine ug/L ND 5.0 02/23/23 21:44
N-Nitrosodimethylamine ug/L ND 5.0 02/23/23 21:44
N-Nitrosodiphenylamine ug/L ND 10.0 02/23/23 21:44
Naphthalene ug/L ND 5.0 02/23/23 21:44
Nitrobenzene ug/L ND 5.0 02/23/23 21:44
Pentachlorophenol ug/L ND 10.0 02/23/23 21:44
Phenanthrene ug/L ND 5.0 02/23/23 21:44
Phenol ug/L ND 5.0 02/23/23 21:44
Pyrene ug/L ND 5.0 02/23/23 21:44
2,4,6-Tribromophenol (S)%71 10-137 02/23/23 21:44
2-Fluorobiphenyl (S)%55 15-120 02/23/23 21:44
2-Fluorophenol (S)%51 10-120 02/23/23 21:44
Nitrobenzene-d5 (S)%65 10-120 02/23/23 21:44
Phenol-d6 (S)%41 10-120 02/23/23 21:44
Terphenyl-d14 (S)%92 11-131 02/23/23 21:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3936244LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 46.950 94 44-142
2,4,6-Trichlorophenol ug/L 57.250 114 37-144
2,4-Dichlorophenol ug/L 58.150 116 1-191
2,4-Dimethylphenol ug/L 70.5 L15014132-119
2,4-Dinitrophenol ug/L 294250 117 1-181
2,4-Dinitrotoluene ug/L 58.950 118 39-139
2,6-Dinitrotoluene ug/L 60.150 120 50-158
2-Chloronaphthalene ug/L 54.350 109 60-118
2-Chlorophenol ug/L 47.250 94 23-134
2-Methylnaphthalene ug/L 52.450 105 25-150
2-Nitrophenol ug/L 56.150 112 29-182
3,3'-Dichlorobenzidine ug/L 118100 118 1-262
4,6-Dinitro-2-methylphenol ug/L 116100 116 1-181
4-Bromophenylphenyl ether ug/L 54.150 108 53-127
4-Chloro-3-methylphenol ug/L 100100 100 22-147
4-Chlorophenylphenyl ether ug/L 53.450 107 25-158
4-Nitrophenol ug/L 163250 65 1-132
Acenaphthene ug/L 50.050 100 47-145
Acenaphthylene ug/L 51.150 102 33-145
Anthracene ug/L 46.750 93 1-166
Benzo(a)anthracene ug/L 54.850 110 33-143
Benzo(a)pyrene ug/L 54.650 109 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3936244LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 56.550 113 24-159
Benzo(g,h,i)perylene ug/L 51.750 103 1-219
Benzo(k)fluoranthene ug/L 52.450 105 11-162
bis(2-Chloroethoxy)methane ug/L 54.550 109 33-184
bis(2-Chloroethyl) ether ug/L 49.850 100 12-158
bis(2-Ethylhexyl)phthalate ug/L 61.650 123 8-158
Butylbenzylphthalate ug/L 63.550 127 1-152
Chrysene ug/L 50.450 101 17-168
Di-n-butylphthalate ug/L 58.450 117 1-118
Di-n-octylphthalate ug/L 67.150 134 4-146
Dibenz(a,h)anthracene ug/L 55.550 111 1-227
Diethylphthalate ug/L 54.150 108 1-114
Dimethylphthalate ug/L 53.450 107 1-112
Fluoranthene ug/L 55.050 110 26-137
Fluorene ug/L 53.050 106 59-121
Hexachloro-1,3-butadiene ug/L 42.150 84 24-116
Hexachlorobenzene ug/L 51.450 103 1-152
Hexachlorocyclopentadiene ug/L 48.850 98 25-150
Hexachloroethane ug/L 37.650 75 40-113
Indeno(1,2,3-cd)pyrene ug/L 55.450 111 1-171
Isophorone ug/L 52.950 106 21-196
N-Nitroso-di-n-propylamine ug/L 53.750 107 1-230
N-Nitrosodimethylamine ug/L 51.650 103 25-150
N-Nitrosodiphenylamine ug/L 51.150 102 25-150
Naphthalene ug/L 45.750 91 21-133
Nitrobenzene ug/L 50.950 102 35-180
Pentachlorophenol ug/L 115100 115 14-176
Phenanthrene ug/L 50.550 101 54-120
Phenol ug/L 32.550 65 5-112
Pyrene ug/L 52.050 104 52-115
2,4,6-Tribromophenol (S)%132 10-137
2-Fluorobiphenyl (S)%111 15-120
2-Fluorophenol (S)%85 10-120
Nitrobenzene-d5 (S)%110 10-120
Phenol-d6 (S)%71 10-120
Terphenyl-d14 (S)%120 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3936543MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653424001
3936544
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 72 44-14291 2350ND36.0 45.3
2,4,6-Trichlorophenol ug/L 50 112 37-144114 250ND56.2 57.1
2,4-Dichlorophenol ug/L 50 114 1-191124 850ND56.8 61.9
2,4-Dimethylphenol ug/L M05016032-119184 1450ND80.0 92.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3936543MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653424001
3936544
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dinitrophenol ug/L 250 141 1-181145 3250ND351362
2,4-Dinitrotoluene ug/L 50 139 39-139134 450ND69.6 66.8
2,6-Dinitrotoluene ug/L 50 131 50-158130 150ND65.4 64.8
2-Chloronaphthalene ug/L 50 101 60-118109 850ND50.6 54.7
2-Chlorophenol ug/L 50 104 23-134118 1250ND52.1 58.8
2-Methylnaphthalene ug/L 50 103 25-150114 1050ND51.6 56.8
2-Nitrophenol ug/L 50 127 29-182135 650ND63.7 67.5
3,3'-Dichlorobenzidine ug/L 100 69 1-26271 3100ND69.0 70.8
4,6-Dinitro-2-methylphenol ug/L 100 155 1-181152 1100ND155152
4-Bromophenylphenyl ether ug/L 50 112 53-127111 150ND56.2 55.7
4-Chloro-3-methylphenol ug/L 100 129 22-147136 6100ND129136
4-Chlorophenylphenyl ether ug/L 50 103 25-158104 150ND51.3 51.9
4-Nitrophenol ug/L 250 81 1-13271 13250ND202177
Acenaphthene ug/L 50 107 47-145109 350ND53.3 54.7
Acenaphthylene ug/L 50 109 33-145112 350ND54.3 55.8
Anthracene ug/L 50 106 1-166105 050ND52.9 52.7
Benzo(a)anthracene ug/L 50 112 33-143113 150ND55.9 56.7
Benzo(a)pyrene ug/L 50 114 17-163118 450ND56.8 58.9
Benzo(b)fluoranthene ug/L 50 117 24-159120 250ND58.4 59.8
Benzo(g,h,i)perylene ug/L 50 124 1-219121 350ND62.0 60.3
Benzo(k)fluoranthene ug/L 50 112 11-162111 150ND56.2 55.5
bis(2-Chloroethoxy)methane ug/L 50 122 33-184132 850ND60.9 66.2
bis(2-Chloroethyl) ether ug/L 50 128 12-158124 3507.43 71.4 69.3
bis(2-Ethylhexyl)phthalate ug/L 50 139 8-158144 450ND69.4 72.0
Butylbenzylphthalate ug/L 50 148 1-152147 050ND74.0 73.7
Chrysene ug/L 50 107 17-168111 450ND53.7 55.7
Di-n-butylphthalate ug/L M1501341-118129 350ND66.9 64.6
Di-n-octylphthalate ug/L M1501514-146153 150ND75.5 76.5
Dibenz(a,h)anthracene ug/L 50 113 1-227117 350ND56.5 58.4
Diethylphthalate ug/L M1501231-114119 450ND61.5 59.3
Dimethylphthalate ug/L M1501141-112116 250ND57.0 58.2
Fluoranthene ug/L 50 118 26-137112 550ND59.0 56.0
Fluorene ug/L 50 112 59-121111 150ND55.9 55.5
Hexachloro-1,3-butadiene ug/L 50 62 24-11678 2250ND31.0 38.8
Hexachlorobenzene ug/L 50 101 1-152101 050ND50.6 50.4
Hexachlorocyclopentadiene ug/L 50 68 25-15086 2350ND34.2 43.0
Hexachloroethane ug/L 50 60 40-11374 2050ND30.2 37.1
Indeno(1,2,3-cd)pyrene ug/L 50 124 1-171121 250ND62.1 60.6
Isophorone ug/L 50 132 21-196140 650ND65.8 70.1
N-Nitroso-di-n-propylamine ug/L 50 137 1-230150 950ND68.7 74.8
N-Nitrosodimethylamine ug/L 50 132 25-150135 350ND65.9 67.7
N-Nitrosodiphenylamine ug/L 50 117 25-150120 250ND58.7 60.0
Naphthalene ug/L 50 86 21-133102 1750ND43.1 51.0
Nitrobenzene ug/L 50 127 35-180133 450ND63.5 66.3
Pentachlorophenol ug/L 100 123 14-176130 5100ND123130
Phenanthrene ug/L 50 115 54-120111 350ND57.3 55.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3936543MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653424001
3936544
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol ug/L M150835-112113 3050ND41.5 56.3
Pyrene ug/L M15012452-115125 150ND62.0 62.3
2,4,6-Tribromophenol (S)%111 10-137122
2-Fluorobiphenyl (S)%91 15-120103
2-Fluorophenol (S)%85 10-120100
Nitrobenzene-d5 (S)%S011610-120131
Phenol-d6 (S)%75 10-120110
Terphenyl-d14 (S)%114 11-131124
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
758018
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653415001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3937626
Associated Lab Samples:92653415001
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N202/27/23 08:30
Aliphatic (C19-C36)ug/L ND 100 N202/27/23 08:30
Aromatic (C11-C22)ug/L ND 100 N202/27/23 08:30
1-Chlorooctadecane (S)%64 40-140 02/27/23 08:30
2-Bromonaphthalene (S)%81 40-140 02/27/23 08:30
2-Fluorobiphenyl (S)%80 40-140 02/27/23 08:30
o-Terphenyl (S)%71 40-140 02/27/23 08:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3937627LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3937628
Aliphatic (C09-C18)ug/L 161 N23005440-14050151 7 50
Aliphatic (C19-C36)ug/L 326 N24008140-14087350 7 50
Aromatic (C11-C22)ug/L 552 N28506540-14072614 11 50
1-Chlorooctadecane (S)%62 40-14066
2-Bromonaphthalene (S)%62 40-14077
2-Fluorobiphenyl (S)%62 40-14075
o-Terphenyl (S)%66 40-14075
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 38
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 38
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92653415
Best Geo - Last Minute Market
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92653415001 758661 758802W1EPA 504.1 EPA 504.1
92653415001 758018 758207W1MADEP EPH MADEP EPH
92653415001 758119 758142W1EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92653415001 757737 757852W1EPA 625.1 EPA 625.1
92653415001 757939W1SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/03/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 38
Page 23 of 38
Page 24 of 38
Page 25 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 3, 2023
Stephanie Knott
Pace Analytical Services - NC
1377 South Park Dr.
Kernersville, NC 27284
Project Location: Best Geo- Last Minute Market
Client Job Number:
Project Number: 92653415
Laboratory Work Order Number: 23B2550
Enclosed are results of analyses for samples as received by the laboratory on February 23, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 1 of 13
Table of Contents
Page 26 of 38
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23B2550-01 5
Sample Preparation Information 6
QC Data 7
Petroleum Hydrocarbons Analyses - VPH 7
B332563 7
Flag/Qualifier Summary 9
Certifications 10
Chain of Custody/Sample Receipt 11
Page 2 of 13
Table of Contents
Page 27 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/3/2023
Pace Analytical Services - NC
1377 South Park Dr.
Kernersville, NC 27284
ATTN: Stephanie Knott
92653415
23B2550
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Best Geo- Last Minute Market
W1 23B2550-01 Water MADEP-VPH-Feb
2018 Rev 2.1
[TOC_1]Sample Summary[TOC]
Page 3 of 13
Table of Contents
Page 28 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH, only hydrocarbon ranges were requested and reported.
REVISED REPORT: Project name updated. 3/3/23
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
Average of 3 markers passes
Analyte & Samples(s) Qualified:
Z-01
Decane
S083947-CCV2
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody
form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Rebecca Faust
Project Manager 1
Page 4 of 13
Table of Contents
Page 29 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/23/2023
Work Order: 23B2550Sample Description:Project Location: Best Geo- Last Minute Market
Sample ID: 23B2550-01
Field Sample #: W1
Sample Matrix: Water
Sampled: 2/21/2023 10:10
[TOC_2]23B2550-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 2/24/23 19:32 EEHµg/L 2/24/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 2/24/23 19:32 EEHµg/L 2/24/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 2/24/23 19:32 EEHµg/L 2/24/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 2/24/23 19:32 EEHµg/L 2/24/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 2/24/23 19:32 EEHµg/L 2/24/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)109 2/24/23 19:3270-130
2,5-Dibromotoluene (PID)105 2/24/23 19:3270-130
[TOC_1]Sample Results[TOC]
Page 5 of 13
Table of Contents
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B332563 02/24/235 5.0023B2550-01 [W1]
[TOC_1]Sample Preparation Information[TOC]
Page 6 of 13
Table of Contents
Page 31 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B332563 - MA VPH
[TOC_3]B332563[TOC]
Blank (B332563-BLK1) Prepared & Analyzed: 02/24/23
Unadjusted C5-C8 Aliphatics µg/L100ND
C5-C8 Aliphatics µg/L100ND
Unadjusted C9-C12 Aliphatics µg/L100ND
C9-C12 Aliphatics µg/L100ND
C9-C10 Aromatics µg/L100ND
Benzene µg/L1.0ND
Butylcyclohexane µg/L1.0ND
Decane µg/L1.0ND
Ethylbenzene µg/L1.0ND
Methyl tert-Butyl Ether (MTBE)µg/L1.0ND
2-Methylpentane µg/L1.0ND
Naphthalene µg/L5.0ND
Nonane µg/L1.0ND
Pentane µg/L1.0ND
Toluene µg/L1.0ND
1,2,4-Trimethylbenzene µg/L1.0ND
2,2,4-Trimethylpentane µg/L1.0ND
m+p Xylene µg/L2.0ND
o-Xylene µg/L1.0ND
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10642.5
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10441.7
LCS (B332563-BS1) Prepared & Analyzed: 02/24/23
Unadjusted C5-C8 Aliphatics µg/L100 150 70-130105158
Unadjusted C9-C12 Aliphatics µg/L100 150 70-13097.8147
C9-C10 Aromatics µg/L100 50.0 70-13010250.8
Benzene µg/L1.0 50.0 70-13010552.6
Butylcyclohexane µg/L1.0 50.0 70-13010753.3
Decane µg/L1.0 50.0 70-13079.539.8
Ethylbenzene µg/L1.0 50.0 70-13010451.9
Methyl tert-Butyl Ether (MTBE)µg/L1.0 50.0 70-13010954.6
2-Methylpentane µg/L1.0 50.0 70-13010954.5
Naphthalene µg/L5.0 50.0 70-13096.148.1
Nonane µg/L1.0 50.0 70-13010753.7
Pentane µg/L1.0 50.0 70-13011256.0
Toluene µg/L1.0 50.0 70-13010451.8
1,2,4-Trimethylbenzene µg/L1.0 50.0 70-13010250.8
2,2,4-Trimethylpentane µg/L1.0 50.0 70-13094.447.2
m+p Xylene µg/L2.0 100 70-130104104
o-Xylene µg/L1.0 50.0 70-13010552.6
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12349.1
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)12048.1
[TOC_1]QC Data[TOC]
Page 7 of 13
Table of Contents
Page 32 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B332563 - MA VPH
LCS Dup (B332563-BSD1) Prepared & Analyzed: 02/24/23
Unadjusted C5-C8 Aliphatics µg/L100 150 2570-130106 0.512159
Unadjusted C9-C12 Aliphatics µg/L100 150 2570-13099.1 1.24149
C9-C10 Aromatics µg/L100 50.0 2570-130102 0.49451.1
Benzene µg/L1.0 50.0 2570-130108 2.2753.8
Butylcyclohexane µg/L1.0 50.0 2570-130108 1.3954.0
Decane µg/L1.0 50.0 2570-13080.6 1.4140.3
Ethylbenzene µg/L1.0 50.0 2570-130105 1.6352.7
Methyl tert-Butyl Ether (MTBE)µg/L1.0 50.0 2570-130110 1.0155.2
2-Methylpentane µg/L1.0 50.0 2570-130111 2.1655.7
Naphthalene µg/L5.0 50.0 2570-13097.2 1.1448.6
Nonane µg/L1.0 50.0 2570-130108 0.95154.2
Pentane µg/L1.0 50.0 2570-130112 0.35255.8
Toluene µg/L1.0 50.0 2570-130105 1.6952.7
1,2,4-Trimethylbenzene µg/L1.0 50.0 2570-130102 0.49451.1
2,2,4-Trimethylpentane µg/L1.0 50.0 2570-13094.0 0.39147.0
m+p Xylene µg/L2.0 100 2570-130105 1.30105
o-Xylene µg/L1.0 50.0 2570-130107 1.5453.4
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)11847.1
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11646.5
Page 8 of 13
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Page 33 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
†Wide recovery limits established for difficult compound.
‡Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Average of 3 markers passesZ-01
[TOC_1]Flag/Qualifier Summary[TOC]
Page 9 of 13
Table of Contents
Page 34 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Water
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2023
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
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