4903_IredellCoMSWLF_Phase1and2and5October2024GWMR_FID1924407_20250130

Semi-Annual Monitoring Report – October 2024 Iredell County Lined Landfill Phases 1,2, 5 & 6 Page 1
Introduction
On behalf of Iredell County, Municipal Engineering, Inc. (MESCO) is pleased to present this Semi-
Annual Water Quality Report for an event performed at the Iredell County Lined Municipal Solid
Waste Landfill (MSWLF), Phases 1, 2, 5 & 6 on October 2-4, 2024. North Carolina Department of
Environmental Quality (NCDEQ) Solid Waste Section (SWS) rules at Title 15A, North Carolina
Administrative Code, Subchapter 13B, Rule .1632 requires Iredell County to report the quality of the
groundwater, surface waters and untreated leachate to the SWS on a semi-annual basis. Laboratory
analytical results indicate samples collected from MW-13B and MW-44 contained between 1 and 2
constituents above Groundwater Quality Standards at Title 15A, North Carolina Administrative Code,
Subchapter 2L (2L Standards). No constituents were detected in surface water samples in concentrations
above Surface Water Quality Standards (2B Standards). Leachate samples collected from the lined
lagoon contained elevated concentrations of several parameters.
Background
The Iredell County Lined MSWLF, permit #49-03, is located at 354 Twin Oaks Road, Statesville, North
Carolina. The site location topographic map is depicted in the attached Figure 1. Two sets of contiguous
Lined landfills (Phases 1 & 2) and (Phases 5 & 6) are combined and treated as a single unit in this report.
Phase 6 received permission to operate on April 23, 2021 and began waste deposition around June 1,
2021.
Water quality at this facility has been monitored at least semi-annually since prior to commencement of
operations in 1993 with all historical data available for comparisons. Most recent laboratory data was
compared to historical data from all previous events compiled since 1993.

This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A
NCAC 13B and as a condition of the permit to operate. A portion of the facility, in close proximity to
Phase 2, has been under assessment monitoring since July 2009. MESCO submitted a Request for
Appendix II Groundwater Monitoring Modification (DIN 20505) dated January 15, 2014 which was
formally approved by the SWS on February 7, 2014 (DIN 20528). Appendix II monitoring was last
performed during the July 2016 event and is planned for the Fall of 2024. On January 13, 2020 the
Section also approved a request to reduce the number of locations that Iredell County must target 1,4-
dioxane (FID:1387339). A Water Quality Monitoring Plan (WQMP) (DIN:1258476), which includes
installation of three new monitoring wells downgradient of Phase 2 along the compliance boundary,
construction of three new monitoring wells downgradient of Phase 6, removal of wells from the
monitoring network and a change in Appendix II frequency, was approved by the SWS on January 28,
2020 (DIN: 1388461).
An Alternative Source Demonstration Addendum (ASD-Add) which established Site Maximum
Allowable Contaminate (SMAC) regulatory compliance levels for five (5) metals (cadmium, chromium,
cobalt, thallium and vanadium) was approved by the SWS on January 30, 2020 (FID:1388745).This
report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization information as specified within 15A NCAC 13B.1632(i), the SWS Environmental
Monitoring Report Form and SWS memorandums.

Semi-Annual Monitoring Report – October 2024 Iredell County Lined Landfill Phases 1,2, 5 & 6 Page 2
Tables concerning well construction, field observations, field parameter data, sampling and analysis
summary, detections compared to Standards, as well as a potentiometric map, quality assurance/quality
control data, and laboratory analytical data results are also enclosed.
Sampling Procedure
MESCO performed this sampling event utilizing portable monitoring methodology in general accordance
with the site-specific WQMP. During this event water samples were collected from thirteen (13)
downgradient monitoring wells (MW-3A, MW-4B, MW-6A, MW-7, MW-8, MW-13B, MW-13BR,
MW-14B, MW-39, MW-40, MW-41, MW-43, MW-44), two (2) background wells (MW-32, MW-37),
and a leachate sample (LAGOON). The unnamed tributaries of Fourth Creek, which serve as the local
discharge feature, were monitored at two (2) locations (SW-2, SW-6). Quality control measures were
implemented during this event including submittal of an equipment (EB). Water level elevations were
determined from other wells located around the site to improve potentiometric contouring. Monitoring
locations are shown on Figure 2.
A summary detailing the construction of the groundwater monitoring wells is presented in Table 1. The
function and integrity of all monitoring locations was visually evaluated as documented in Table 2. The
depth to water in each well was electronically gaged prior to purging to quantify the static water level
elevation. Electrical submersible pumps or bailing was utilized to purge the wells a minimum of three (3)
times the volume of standing water in the well or until dry. Surface water samples were dipped from the
surface of the creeks at previously designated locations. Samples were then placed into laboratory-
prepared, pre-preserved containers. Samples were kept on ice and transported to a NC-certified
laboratory under proper chain of custody (C-O-C) protocols within the specified hold times for each
analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, specific
conductivity, temperature and surface water hardness. Field parameter data is presented in Table 3
and the field sampling data sheets are included in Appendix A.
Laboratory Results
Pace Analytical Laboratories (PACE) (NC Cert # 12, 40 & 677), performed the lab analysis. Groundwater
and surface water samples were analyzed for the constituents listed in 40CFR 258 Appendix I and 1,4-
dioxane. Samples collected from MW-13B and MW-14B were tested for parameters listed in Appendix
II. A leachate sample collected from the lagoon invert (LAGOON) which serves Phases 1-6, was
analyzed for the SWS required leachate specific list and 1,4-dioxane. The Quality control blanks
included an EB which was tested for Appendix I constituents, 1,4-dioxane and tetrahydrofuran. A
sampling and analysis table summarizing the locations, target parameters and laboratory methods is
presented as Table 4. Laboratory results and C-O-Cs are presented in Appendix B.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL) and any
value between the MDL and laboratory-established Reporting Limit (RL) is qualified with a “J” by the
laboratory as an estimated concentration. Estimated concentrations are considered non-quantifiable and

Semi-Annual Monitoring Report – October 2024 Iredell County Lined Landfill Phases 1,2, 5 & 6 Page 3
discretion should be made prior to making decisions based solely on a value that the laboratory flags as an
estimate.

Table 5 summarizes constituents detected in groundwater and QC samples compared to the 2L Standards
and Site Specific Maximum Allowable Contaminant Levels (SMAC), which have been recognized by the
SWS as groundwater compliance Standards. Although not applicable for regulatory compliance purposes
the detections were also compared to the Maximum Contaminant Level (MCL) commonly referenced as
the Federal “Drinking Water Standard”. The groundwater 2L Standards presented are current as of April
1, 2022. Table 6 lists the constituents detected in surface water samples compared with the NC Division
of Water Resources 2B Standards, modified July 26, 2021.
Quality Control Samples
No constituents were detected in the Equipment Blank (EB).
Groundwater Samples Above Standards
Groundwater sample MW-13B contained 1,4-dioxane at a concentration of 4.6 micrograms per liter,
which is above the RL and the NC 2L Standard of 3.0 ug/L. Wells MW-13B and MW-44 contained
benzene at a concentration of 1.6 ug/L and 1.2 ug/L respectively, which is above the RL and the NC 2L
Standard of 1.0 ug/L. Barium was detected in MW-13B at a concentration of 1,020 ug/L, which is above
the 2L Standard of 700 ug/L. Cobalt was also detected in well MW-4B at a concentration of 27.2 ug/L,
which is above the RL and the NC 2L SMAC alternate compliance standard (22 ug/L). No constituents
listed in Appendix II that are not also listed in Appendix I were detected during this event.
Surface Water Samples Above Standards
Neither surface water sample locations (SW-2, SW-6) contained contaminants above allowable 2B
Standards.
Leachate Samples
The leachate sample (LAGOON) contained concentrations of 10 metals and 7 VOCs at or above their RL
as presented in Table 5. Four (4) constituents have been noted with bold, red font to highlight the value
with respect to the 2L Standard, although the standards do not apply to the leachate as it is a wastewater.
The leachate sample collected at the influent of the lagoon originates from all lined Phases including 3&4.
The concentrations of analytes detected in the leachate samples are generally much lower than averages
of leachate from similar landfills as published by the EPA 1 which is generally consistent with historically
reported results.
The BOD and COD concentrations are low compared to typical domestic wastewater; however, the
BOD/COD ratio is very low (0.28). BOD/COD ratio below 0.3 may indicate that the majority of organic
matter is not biodegradable since either the organic matter is difficult to biodegrade or toxic substance(s)
are inhibiting microbial activities2.
1 1988 EPA document-Summary of Data on MSWLFLeachate Characteristics – EPA/530-SW-88-038
2 https://cgi.tu-harburg.de/~awwweb/wbt/emwater/lessons/lesson_a1/lm_pg_1068.html

Semi-Annual Monitoring Report – October 2024 Iredell County Lined Landfill Phases 1,2, 5 & 6 Page 4
Groundwater and Surface Water Characterization
A potentiometric map of the uppermost aquifer created from groundwater elevations measured during this
event is included as Figure 2. Groundwater flow directions and rates were calculated using modified
Darcy's equation and presented as Table 7. Groundwater in the uppermost aquifer typically flows in a
general northern direction towards the unnamed tributaries of Fourth Creek, which serves as the local
discharge feature. Streams located within the facility boundaries were visually observed to have elevated
volume, flow and turbidity likely as a result of the effects from Hurricane Helene. It should also be noted
that during the sampling event evidence suggested a significant number of wells had been inundated due
to the significant rains and flooding associated with Hurricane Helene. Water quality results, however,
are consistent with past sampling events suggesting the well integrity had not been compromised.
Findings
The only constituents detected above an established 2L Standard were benzene, 1,4-dioxane and barium
in MW-13B, benzene in MW-44 and cobalt in MW-4B. All concentrations remain within their own
respective historically identified range. MW-44 is located at the compliance boundary. This event marks
the third consecutive time since January 14, 2010 that VOCs have been below 2L Standards in samples
collected from MW-14B.
Iredell County owns the property and controls the groundwater resources located downgradient of the
plume. Analytical results from SW-2 indicate the local discharge feature downgradient of the known
impacted area remain unimpaired.
Closing
Semi-annual water quality monitoring, is planned to be performed again in the Spring of 2025. Keeping
with the WQMP testing of MW-13B and MW-14B for Appendix II constituents will be performed again
in the Fall of 2029.
Figures
SCALE:DATE:PROJECT NO.:
1/7/2020 G18118SEE SCALEBAR
UNLINED C&D
PHASE 1 CLOSED
UNLINED C&D
PHASE 2 CLOSED
LINED MSWLF INACTIVE (PHASE 2)
LINED MSWLF INACTIVE (PHASE 4)
LINED MSWLF INACTIVE (PHASE 3)
LAGOON
LINED MSWLF (PHASE 1)
UNLINED LANDFILL
CLOSED
FOU
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T
H

C
R
E
E
K
LINED MSWLF
INACTIVE (PHASE 5)
LINED MSWLF
ACTIVE (PHASE 6)
OPENED 6/1/21
GOLF COURSE
OU
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7
0
SW-SofConfluence
POND
SW
SW
SW
SW
APPROXIMATELY 2256' TO
PROPERTY BOUNDARY
1,4-Dioxane - 8.9 ug/L
850
805805
810
815
80
0
800
855
840
835
79
5
795
845
79
0
785
825
830
820
820
790
810
815
SW
860
MW GWE=789.42
MW-9RR
MW GWE=799.92
MW-10R
MW
GWE=783.23
MW-16
MW GWE=802.70
MW-22
MW
GWE=815.03
MW-23
MW GWE=809.79
MW-24S
MW
GWE=819.79
MW-26S
MW
GWE=788.05
MW-19SR
MW
GWE=817.37
MW-17
MW
GWE=793.63
MW-18
MW
GWE=789.91
MW-21SOWP-4
MW
GWE=796.48
MW-27S
MW
GWE=802.56
MW-28
MW
GWE=799.91
MW-29
OWP4-7S
MW
GWE=791.40
MW-30
MW MW-36S
MW GWE=786.42
MW-38
OW
P-86
OW
P-83
OW P-85
OW
MW-36D
MW
GWE=786.80
MW-19D*
MW
GWE=791.00
MW-21D*
MW MW-24D*
GWE=810.18
MW
MW-26D*
GWE=821.75
MW
GWE=796.47
MW-27D*
OW
P4-7D
MW
MW-2
MW
GWE=783.25
MW-3A
MW
GWE=774.15
MW-6A
MW
GWE=784.91
MW-7
MW
GWE=777.79
MW-8
MW
MW-11
MW
GWE=778.25
MW-13B
MW P2-10S
MW GWE=774.98
MW-13BR
MW
MW-15D
MW
MW-13A*MW
MW-15
OW
P2-19
OW
P2-10D
MW
MW-14A
MW
MW-4A
MW MW-6B
MW
MW-3B
MW
GWE=775.80
MW-43
MW GWE=776.32
MW-44
MW
MW-39
GWE:811.54
MW
MW-40
GWE:800.60
MW
MW-41
GWE:793.49
MW MW-4B
MW
GWE=776.96
MW-14B*
MW
GWE=857.85
MW-37
MW GWE=856.60
MW-32
780
MW
MW-12
FORCEMAIN
SW-3
SW-2
SW-5
Abandoned 10/12/19
GWE=791.48
SW-6
NOT TESTED
NOT TESTEDNOT TESTED
NOT TESTED
NOT TESTED
NOT TESTED
NOT TESTED NOT TESTED
NOT TESTED
NOT TESTED
NOT TESTED
NOT TESTED
NOT TESTED
MW-42
MW
GWE=796.96
MW-9R
MW
LINED MSWLF PHASE 5
INACTIVE PTO 11/18/14
LINED MSWLF
PHASE 2
INACTIVE
PTO 9/28/98
LINED MSWLF
PHASE 1
INACTIVE
BALER FACILITY
RECYCLING
TW
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O
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S

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SCALES
FOURTH CREEK TRIBUTARY-UNNAMED
FOURTH CREEK
TRIBUTARY-
UNNAMEDFOURTH CREEK
TRIBUTARY-UNNAMED
EXISTING COUNTY OWNED HOUSE
USED AS TRANSPORTATION HUB "ICATS"
FOURTH CREEK
TRIBUTARY-UNNAMED
LINED MSWLF
PHASE 4
INACTIVE
PTO 7/30/08
LINED MSWLF
PHASE 3
INACTIVE
PTO 7/26/02ACTIVE
GCCS
ACTIVE
GCCS
ACTIVE
GCCS
TWIN OAKS GOLF COURSE
OWNED BY IREDELL COUNTY
SHOP
GCCS
GENERATOR
AREA
LEACHATE LAGOON
MW-44
Benzene - 1.2 ug/L
UNLINED
CLOSED
C&D
FIGURE 2
OW
*MW-
ESTIMATED WASTE LIMITS UNLINED C&D LANDFILL
WASTE LIMITS OF UNLINED C&D LANDFILL
FACILITY OUTERMOST PROPERTY BOUNDARY
TOPOGRAPHIC CONTOURS-EXISTING
RELATIVE GROUNDWATER COMPLIANCE BOUNDARY
OBSERVATION WELL
MONITORING WELL
SURFACE WATER SAMPLING LOCATION
ROADS
STREAM/CREEK-LIKELY PERENNIAL
EQUIPOTENTIAL UPPERMOST GROUNDWATER CONTOUR (OCT. 2-3,2024)
APPROXIMATE EQUIPOTENTIAL GROUNDWATER CONTOUR
GROUNDWATER POTENTIOMETRIC ELEVATION
GROUNDWATER ELEVATION NOT USED FOR CONTOURING
LEGEND
960
GWE = 941.66
MW
SW
960
LINED MSWLF PHASE 6
ACTIVE APPROVAL TO OPERATE 4/23/21
ACTIVE
GCCS
SW
STREAM/CREEK-LIKELY INTERMITTENT
ACTIVE
GCCS
DA
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DRAWING NO.SHEET NO.
SCALE:
DATE:
DRWN. BY:
CHKD. BY:
PROJECT NUMBER
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MW-13B
1,4-Dioxane - 4.6 ug/L
Benzene - 1.6 ug/L
MW-4B
Cobalt - 27.2 ug/L
Tables
Table 1
Groundwater Monitoring Well Construction Table
October 1-2, 2024
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length
Top of
Casing
Elevation
Ground
Elevation Elevation
Depth to
Water
MW-32 2/21/08 2 23.90 8.90 15 Sandy Silt 874.75 871.82 855.60 19.15 35.7627 -80.8336
MW-37 4/12/10 2 44 29 15 Sandy Silt 895.26 892.26 857.85 37.41 35.7624 -80.8320
MW-3A 8/28/93 2 12 2 10 Silty Sand 792.10 790.80 783.25 8.85 35.7712 -80.8315
MW-4B 9/1/93 2 37 27 10 Weathered Rock 823.34 820.87 791.48 31.86 35.7713 -80.8295
MW-6A 8/28/93 2 23.5 8.5 15 Clayey Silt 793.00 791.50 774.15 18.85 35.7707 -80.8256
MW-7 8/30/93 2 23 8 15 Sandy Clay 798.23 796.43 784.91 13.32 35.7699 -80.8261
MW-8 8/31/93 2 27 12 15 Sandy Clay 797.40 795.10 777.79 19.61 35.7699 -80.8252
MW-13B 3/2/98 2 39.72 na na Silty Sand 818.10 815.44 778.25 39.85 35.7707 -80.8270
MW-13BR 6/30/06 2 43.56 28.56 15 Silty Sand 811.31 808.56 774.98 36.33 35.7709 -80.8266
MW-14B 3/3/98 2 58.50 na na Silty Sand 818.54 815.68 776.96 41.58 35.7711 -80.8271
MW-39 2/18/19 2 21 5 15 Silt 825.13 822.27 811.54 13.59 35.7656 -80.8250
MW-40 2/19/19 2 27 12 15 Silt 825.75 823.04 800.60 25.15 35.7676 -80.8347
MW-41 1/15/21 2 17 7 10 Silt 800.26 797.26 793.49 6.77 35.7683 -80.8338
MW-43 2/25/00 2 64 49 15 Competent rock 821.05 818.21 775.80 45.25 35.7718 -80.8276
MW-44 3/7/19 2 21 6 15 Silt 785.67 783.02 776.32 9.35 35.7714 -80.8269
NOTE:
na = not available
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Monitoring
Well
Date
Installed
Geology of
Screened Interval Latitude Longitude
Iredell County Lined Landfill, Phases 1, 2, 5 & 6 Page 1 of 1
Table 2
Field Observations of Monitoring Locations
October 2-3, 2024
Sample
Location
Viable
Location Tampering
Locked
After
Sampled Operates
Tagged
or
Labeled
Concrete
Surface Pad
Appears Comments
MW-32 Yes Yes Yes Yes Yes Yes Background well for Ph 1,2,5,6 & CDLF
MW-37 Yes Yes Yes Yes Yes Yes Background well for Ph 1,2,5,6 & CDLF
MW-3A Yes Yes Yes Yes Yes Yes Case hinge is poor. Needs additional screws
MW-4B Yes Yes Yes Yes Yes Yes
MW-6A Yes Yes Yes No Yes Yes Case hinge needs to be repaired
MW-7 Yes Yes Yes Yes Yes Yes Wasps in case. Adjacent basin was dry
MW-8 Yes Yes Yes Yes Yes Yes Case hinge is poor but functional
MW-13B Yes Yes Yes Yes Yes Yes Path blocked w/ soil from recent storm
MW-13BR Yes Yes Yes Yes Yes Yes
MW-14B Yes Yes Yes Yes Yes Yes
MW-39 Yes Yes Yes Yes Yes Yes Purge water very turbid
MW-40 Yes Yes Yes Yes Yes Yes Purge water moderately turbid
MW-41 Yes Yes Yes Yes Yes Yes
MW-43 Yes Yes Yes Yes Yes Yes
MW-44 Yes Yes Yes Yes Yes Yes Purge water is slightly turbid
SW-2 Yes -----High gage height, flow &turbidity.
SW-5 Yes -----High gage height, flow &turbidity.
SW-6 Yes -----High gage height, flow &turbidity.
LAGOON Yes -----Sample taken from Invert pipe (serves Ph 1-6)
Any unusual field conditions, observations, or events:
Stainless steel bailer told been stuck in MW-7 since ~2000. Believe presence has not compromised data.
Lined Phase 6, located between Ph 2 and 5, began operations on June 1, 2021.
Well field maintenance routinely performed by County.
Event occurred 6 days after Hurricane Helene (4.43 inches rain). Evidence that low lying areas had flooded.
Iredell County Lined Landfill, Phases 1,2, 5 & 6 Page 1 of 1
Table 3
Field Parameter Data Summary
October 1-3, 2024
Water Water Casing Specific
Ft (btoc)ft (amsl)ft (amsl)цs/cm mg/L
MW-32 19.15 855.60 874.75 17.9 6.37 49 NR
MW-37 37.41 857.85 895.26
MW-3A 8.85 783.25 792.10 18.1 6.12 133 NR
MW-4B 31.86 793.55 825.41
MW-6A 18.85 774.15 793.00 17.3 6.53 29 NR
MW-7 13.32 784.91 798.23
MW-8 19.61 777.79 797.40 17.5 6.51 71 NR
MW-13B 39.85 778.25 818.10
MW-13BR 36.33 774.98 811.31 17.5 6.19 197 NR
MW-14B 41.58 776.96 818.54 18.3 7.09 301 NR
MW-39 13.59 811.54 825.13 18.4 6.53 61 NR
MW-40 25.15 800.60 825.75 18.3 6.41 39 NR
MW-41 6.77 793.49 800.26
MW-43 45.25 776.90 822.15 17.1 6.47 28 NR
MW-44 9.35 776.32 785.67
Minimum 6.77 774.15 785.67 16.9 6.12 28 NR
Average 24.46 794.41 818.87 17.7 6.40 203 NR
Maximum 45.25 857.85 895.26 18.6 7.09 1025 NR
LAGOON ---
SW-2 ---18.7 7.03 77 51.3
SW-6 ---
NOTE:
NR = No Reading attempted
Iredell County Lined Landfill, Phases 1, 2, 5 & 6 Page 1 of 1
Table 4
Sampling and Analysis Summary
October 2-4, 2024
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MW-32 x x x x x x x
MW-37 x x x x x x x
MW-3A x x x x x x
MW-4B x x x x x x
MW-6A x x x x x x
MW-7 x x x x x x
MW-8 x x x x x x
MW-13B x x x x x x x x x x x x
MW-13BR x x x x x x
MW-14B x x x x x x x x x x x x
MW-39 x x x x x x
MW-40 x x x x x x
MW-41 x x x x x x
MW-43 x x x x x x
MW-44 x x x x x x x
SW-2 x x x x x x x x
SW-6 x x x x x x x x
EB x x x x
LAGOON x x x x x x x x x x x
App. I Field Parameters LeachateMisc.
Iredell County Lined Landfill, Phases 1,2,5 & 6 Page 1 of 1
Table 5
Groundwater, Leachate and Quality Control Sample Detections
October 2-4, 2024
SMAC VALUE*U U D D D D D D D D D D D D D LEACHATE QC
Antimony, total 0.5 1 1 6 8.3
Arsenic, total 0.17 1 10 10 0.2 J 0.51 J 2.7 0.77 J 29.5
Barium, total 0.5 1 700 2,000 62.2 84.4 71.5 123 95.4 207 154 1020 131 105 49 97.3 37.2 6.9 115 629
Beryllium, total 0.033 0.1 4 4 0.19 0.1 0.05 J 0.092 J 0.33 0.22 0.57 3.2 0.079 J 0.036 J 0.72 0.039 J 0.31 0.058 J
Cadmium, total 0.037 0.1 6*5 0.22 0.26 0.33 0.098 J 0.39 0.13 0.18 0.069 J 0.26 0.08 J 0.17
Chromium, total 0.39 1 66*100 2.2 0.42 J 1.6 0.74 J 4.9 1.3 12.1 0.58 J 0.79 J 8.2 4.5 3.2 10.7 37.2
Cobalt, total 0.14 1 22*NE 3.7 1.2 2 27.2 0.51 J 5.1 3 0.65 J 2.8 0.26 J 0.27 J 0.77 J 12.2
Copper, total 0.42 1 1,000 1,300 2.1 2.1 6.5 0.88 J 1.9 7.4 0.75 J 7.4 1.5 0.83 J 0.46 J 5.6
Lead, total 0.18 1 15 15 0.98 J 0.25 J 0.27 J 0.83 J 1.5 3.4 0.41 J 0.82 J 2.9
Nickel, total 0.26 1 100 NE 1.5 0.78 J 2.1 8.4 3 3.4 4.6 2.9 1.6 5.5 3.2 1.4 1.2 0.95 J 5.9 64.5
Selenium, total 0.2 2 20 50 0.46 J 0.82 J 0.23 J 0.63 J
Silver, total 0.028 0.5 20 NE 0.04 J 0.075 J
Thallium, total 0.11 1 2 2 0.032 J 0.071 J 0.17 J
Vanadium, total 0.064 1 89*NE 4.6 2.4 4.9 1.1 2 13 0.98 J 3.1 29.2 1.9 2.5 2.6 6.4 10.5
Zinc, total 0.93 10 1,000 NE 6.9 J 4.8 J 13.7 17.8 20.8 7.9 J 12.6 27 6.8 J 14.2
1,1-Dichloroethane 0.37 1 6 NE 0.38 J
1,4-Dichlorobenzene 0.33 1 6 75 0.79 J 0.67 J 0.4 J 3.8
1,4-Dioxane 38.7 150 3 NE
1,4-Dioxane 0.86 2 3 NE --------------4.6 --1 J --------2.5 30.7 --
2-Butanone (MEK)4 5 4,000 NE 6
Acetone 5.1 25 6,000 NE 16.7 J
Benzene 0.34 1 1 5 1.6 1.2 2.6
Chlorobenzene 0.28 1 50 100 0.78 J
cis-1,2-Dichloroethene 0.38 1 70 70 1.9 1.2 1.6 1.5 0.5 J
Ethylbenzene 0.3 1 600 700 24.5
Styrene 0.29 1 70 100 0.31 J
Tetrahydrofuran 3.5 10 NE NE ------------------------3.5 J --
Toluene 0.24 1 600 1,000 0.41 J 3.5
Vinyl chloride 0.39 1 0.03 2 0.56 J
Xylene (Total)0.34 1 500 10,000 23.4
BOD, 5 day 2,000 2,000 NE NE ------------------------------132,000 --
COD 12,500 25,000 NE NE ------------------------------466,000 --
Phosphorus 2.5 50 NE NE ------------------------------390 --
Sulfide 22 100 NE NE ------------------------------4,800 --
PH (Field) (SU)0.1 0.1 <6.5 or >8.5 NE ------------------------------6.81 --
Notes:
Bold Above RL and Established 2L/SMAC recognized by NC SWS as regulatory groundwater Standard
Highlighted Above Established MCL Drinking Water Std. (No regulatory significance)
U= Well Upgradient, D = Well Downgradient, QC = Quality Control Sample
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
2L = NC 2L Groundater Standard 15A NCAC 02L .0202
IMAC = Interim Maximum Allowable Concentration established via 15A NCAC 02L .0202
*SMAC = Site Maximum Allowable Concentration (Approved by NCDEQ via ASD in 2020)
MCL = Maximum Contaminant Level for drinking water established by the USEPA.
J = "J-qualified". Defined by the lab as "estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
MW-43 MW-44 LAGOONMW-13B MW-13BR MW-14B MW-39 MW-40 MW-41
Preliminary source of NC 2L Violations is believed to be anthropogenic with Landfill Gas &/or leachate as suspected transport mechanism. A definitive source of the detections was not determined as part of this report.
Units ug/L unless shown otherwise, Blank cells means not detected above MDL, - means parameter not analyzed, NE means not established.
RL = Reporting Limit defined by Pace laboratory as "The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific
analyte in a specific matrix."
Parameter Name MDL RL MCL MW-32 MW-37 MW-3A
VOCs (Targeted 40CFR 258 Appendix I, 1,4-Dioxane and THF)
Leachate Parameters
Outside Historically Observed Range
2L STANDARD EB
Metals (Targeted 40CFR 258 Appendix I)
MW-4B MW-6A MW-7 MW-8
Iredell County Lined Landfill, Phases 1, 2, 5 & 6 Page 1 of 1
Table 6
Surface Water Sample Detections
October 2, 2024
SW-2 SW-6
Downstream Downstream
Barium, total 0.5 1 NE NE 21,000 2000 27.3 66.2
Chromium, total 0.63 5 42.9C, 329.82A NE NE 100 0.73 J 1.3
Cobalt, total 0.14 1 NE NE 1.6C, 16A NE 0.42 J
Copper, total 0.42 1 5.06C, 7.17A NE NE 1300 1.1
Nickel, total 0.26 1 29.57C, 266.21A NE NE NE 0.61 J
Vanadium, total 0.91 1 NE NE NE NE 1.4 2.6
Zinc, total 3 10 66.56A, 67.11C NE NE NE 7.6 J
Hardness (mg/L)17.1 -NE NE NE NE 51.3 51.3
J = "J-qualified". Defined by the lab as "Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
Red Bold Above RL and Applicable 2B Std.
Above Established Federal MCL Primary Drinking Water Std.
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
2B Standards from All Waters (C & SC) or Class C.
Nationally Recommended Water Quality Criteria for which NC does not have a Water Quality Standard for one or more uses
Hardness as CaCo3 (Field Measured)
EPA
NRWQC2 NC ISTV3 MCL4Parameter Name MDL RL NC 2B STD1
Iredell County Lined Landfill, Phases 1,2,5 & 6 Page 1 of 1
Table 7
Hydrogeologic Properties at Monitoring Well Locations
October 2-3, 2024
Hydraulic Effective Hydraulic
Average
Linear
Velocity Depth to
Groundwater
Potentiometric
MW-32 3.21E-04 20 0.03 47 S68W 19.15 855.60 PWR
MW-37 5.18E-04 22 0.02 58 S80E 37.41 857.85 Sandy Silt
MW-3A 2.00E-04 20 0.07 77 N50W 8.85 783.25 Silty Sand
MW-4B 7.00E-05 20 0.05 16 N02E 31.86 793.55 Weathered Rock
MW-6A 7.00E-05 15 0.04 17 N04E 18.85 774.15 Clayey Silt
MW-7 2.00E-04 15 0.05 66 N01W 13.32 784.91 Sandy Clay
MW-8 1.00E-04 15 0.07 46 N75E 19.61 777.79 Sandy Clay
MW-13B 5.30E-06 21 0.02 1 N58E 39.85 778.25 Silty Sand
MW-13BR 9.24E-04 21 0.02 111 N58E 36.33 774.98 Silty Sand
MW-14B 1.20E-05 21 0.03 2 N56E 41.58 776.96 Silty Sand
MW-39 -18 0.06 -N60W 13.59 811.54 Sandy Silt
MW-40 3.77E-03 18 0.04 809 N32W 25.15 800.60 Sandy Silt
MW-41 1.26E-03 18 0.05 386 N25W 6.77 793.49 Sandy Silt
MW-43 --0.05 -N17E 45.25 775.80 Bedrock
MW-44 -18 0.03 -N57E 9.35 776.32 Sandy Silt
Minimum 5.30E-06 15 0.02 1 -6.77 774.15 -
Average 6.21E-04 19 0.04 136 -24.46 794.34 -
Maximum 3.77E-03 22 0.07 809 -45.25 857.85 -
NOTE:Hydrologic gradient calculated from groundwater elevations recorded on October 2-3, 2024.
Values for hydraulic conductivity determined via slug test by MESCO
Groundwater average linear velocity rate calculated from modified Darcy's equation:
where
K = hydraulic conductivity
e = effective porosity
dh = head difference
Monitoring Flow Screened Interval
dl
dh
n
KQ
e
⋅−=
Iredell County Lined Landfill, Phases 1, 2, 5 & 6 Page 1 of 1
Appendix A
Field Sampling Parameter Data Sheet(s)
Appendix B
Laboratory Analysis Reports
Chains of Custody
#=CL#
October 31, 2024
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92756913
92756913
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services, Inc.
68 Shipwash Dr.
Garner, NC 27529
Iredell Lined Ph 1,2,5,6
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between October 03, 2024 and October 04,
2024. The results relate only to the samples included in this report. Results reported herein conform to the applicable
TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the
report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole D'Oleo
[e-mail]
Project Manager
[phone]
Enclosures
cc:Accounts Payable, Municipal Engineering Services, Inc.
Jonathan Pfohl, Municipal Engineering Services
Jay Zimmerman, PG, Municipal Engineering Services, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 63
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
California Certification# 3096
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Utah
Utah FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 63
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Lab ID Sample ID Matrix Date Collected Date Received
92756913001 LAGOON Water 10/03/24 07:01 10/03/24 13:50
92756913002 MW-3A Water 10/03/24 10:21 10/04/24 14:08
92756913003 MW-6A Water 10/03/24 08:55 10/04/24 14:08
92756913004 MW-7 Water 10/03/24 09:12 10/04/24 14:08
92756913005 MW-8 Water 10/03/24 09:30 10/04/24 14:08
92756913006 MW-40 Water 10/03/24 15:17 10/04/24 14:08
92756913007 MW-13BR Water 10/03/24 09:51 10/04/24 14:08
92756913008 MW-41 Water 10/03/24 17:03 10/04/24 14:08
92756913009 MW-43 Water 10/03/24 16:23 10/04/24 14:08
92756913010 MW-4B Water 10/03/24 10:36 10/04/24 14:08
92756913011 MW-39 Water 10/03/24 15:03 10/04/24 14:08
92756913012 MW-44 Water 10/03/24 17:36 10/04/24 14:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 63
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92756913001 LAGOON EPA 353.2 Rev 2.0 1993 1 PASI-EJMM
SM 5210B-2016 1 PASI-EVLG
EPA 6020 15 PASI-OADS, BSL
EPA 8260D 51 PASI-CTMH
EPA 8260D Mod.3 PASI-CTEG
SM 4500-S2F 1 PASI-OJJB
EPA 365.4 1 PASI-OAGS
EPA 410.4 1 PASI-OJH
92756913002 MW-3A EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CTMH
92756913003 MW-6A EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CLMB
92756913004 MW-7 EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CLMB
92756913005 MW-8 EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CLMB
92756913006 MW-40 EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CLMB
92756913007 MW-13BR EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CLMB
92756913008 MW-41 EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CLMB
92756913009 MW-43 EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CLMB
92756913010 MW-4B EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CLMB
92756913011 MW-39 EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CLMB
92756913012 MW-44 EPA 6020 15 PASI-OADS
EPA 8260D 51 PASI-CLMB
EPA 8260D Mod.3 PASI-CTEG
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:LAGOON Lab ID:92756913001 Collected:10/03/24 07:01 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
353.2 NO2/NO3 unpres EDN
Nitrogen, Nitrate ND mg/L 10/04/24 11:33 14797-55-80.040 0.029 1
Analytical Method: SM 5210B-2016 Preparation Method: SM 5210B-2016
Pace Analytical Services - Eden
5210B BOD, 5 day EDN
BOD, 5 day 132 mg/L 10/09/24 16:19 B210/04/24 13:572.0 2.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony 8.3 ug/L 10/22/24 22:15 7440-36-010/13/24 16:341.0 0.50 1
Arsenic 29.5 ug/L 10/22/24 22:15 7440-38-210/13/24 16:341.0 0.50 1
Barium 629 ug/L 10/24/24 11:10 7440-39-310/13/24 16:342.0 1.0 2
Beryllium 0.058J ug/L 10/22/24 22:15 7440-41-710/13/24 16:340.10 0.033 1
Cadmium ND ug/L 10/22/24 22:15 7440-43-910/13/24 16:340.10 0.067 1
Chromium 37.2 ug/L 10/22/24 22:15 7440-47-310/13/24 16:341.0 0.50 1
Cobalt 12.2 ug/L 10/22/24 22:15 7440-48-410/13/24 16:341.0 0.24 1
Copper 5.6 ug/L 10/22/24 22:15 7440-50-810/13/24 16:341.0 0.42 1
Lead 2.9 ug/L 10/22/24 22:15 7439-92-110/13/24 16:341.0 0.22 1
Nickel 64.5 ug/L 10/24/24 11:10 7440-02-010/13/24 16:342.0 0.53 2
Selenium 0.63J ug/L 10/24/24 11:10 7782-49-210/13/24 16:344.0 0.40 2
Silver ND ug/L 10/22/24 22:15 7440-22-410/13/24 16:340.50 0.028 1
Thallium ND ug/L 10/22/24 22:15 7440-28-010/13/24 16:341.0 0.11 1
Vanadium 10.5 ug/L 10/22/24 22:15 7440-62-210/13/24 16:341.0 0.91 1
Zinc 14.2 ug/L 10/22/24 22:15 7440-66-610/13/24 16:3410.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone 16.7J ug/L 10/11/24 20:08 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/11/24 20:08 107-13-110.0 1.8 1
Benzene 2.6 ug/L 10/11/24 20:08 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/11/24 20:08 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/11/24 20:08 75-27-41.0 0.31 1
Bromoform ND ug/L 10/11/24 20:08 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/11/24 20:08 74-83-9 v22.0 1.7 1
2-Butanone (MEK)6.0 ug/L 10/11/24 20:08 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/11/24 20:08 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/11/24 20:08 56-23-51.0 0.33 1
Chlorobenzene 0.78J ug/L 10/11/24 20:08 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/11/24 20:08 75-00-31.0 0.65 1
Chloroform ND ug/L 10/11/24 20:08 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/11/24 20:08 74-87-3 v21.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/11/24 20:08 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/11/24 20:08 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/11/24 20:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/11/24 20:08 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/11/24 20:08 95-50-11.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:LAGOON Lab ID:92756913001 Collected:10/03/24 07:01 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
1,4-Dichlorobenzene 3.8 ug/L 10/11/24 20:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/11/24 20:08 110-57-61.0 0.56 1
1,1-Dichloroethane ND ug/L 10/11/24 20:08 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/11/24 20:08 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/11/24 20:08 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 0.50J ug/L 10/11/24 20:08 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/11/24 20:08 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/11/24 20:08 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/11/24 20:08 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/11/24 20:08 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/11/24 20:08 123-91-115038.7 1
Ethylbenzene 24.5 ug/L 10/11/24 20:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/11/24 20:08 591-78-6 v25.0 0.48 1
Iodomethane ND ug/L 10/11/24 20:08 74-88-4 L2,v220.0 9.7 1
Methylene Chloride ND ug/L 10/11/24 20:08 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/11/24 20:08 108-10-15.0 2.7 1
Styrene 0.31J ug/L 10/11/24 20:08 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/11/24 20:08 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/11/24 20:08 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/11/24 20:08 127-18-41.0 0.29 1
Toluene 3.5 ug/L 10/11/24 20:08 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/11/24 20:08 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/11/24 20:08 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/11/24 20:08 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/11/24 20:08 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/11/24 20:08 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/11/24 20:08 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 10/11/24 20:08 75-01-41.0 0.39 1
Xylene (Total)23.4 ug/L 10/11/24 20:08 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)101 %10/11/24 20:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %10/11/24 20:08 17060-07-070-130 1
Toluene-d8 (S)103 %10/11/24 20:08 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
1,4-Dioxane (p-Dioxane)30.7 ug/L 10/08/24 22:58 123-91-12.0 0.86 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %10/08/24 22:58 17060-07-070-130 1
Toluene-d8 (S)90 %10/08/24 22:58 2037-26-570-130 1
Analytical Method: SM 4500-S2F
Pace Analytical Services - Ormond Beach
4500S2F Sulfide
Sulfide 4.8 mg/L 10/18/24 11:12 18496-25-8 H10.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:LAGOON Lab ID:92756913001 Collected:10/03/24 07:01 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 365.4 Preparation Method: EPA 365.4
Pace Analytical Services - Ormond Beach
365.4 Phosphorus, Total
Phosphorus, Total (as P)0.39 mg/L 10/22/24 13:10 7723-14-010/22/24 07:300.10 0.070 1
Analytical Method: EPA 410.4 Preparation Method: EPA 410.4
Pace Analytical Services - Ormond Beach
410.4 COD
Chemical Oxygen Demand 466 mg/L 10/15/24 15:5510/14/24 13:1840.0 25.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-3A Lab ID:92756913002 Collected:10/03/24 10:21 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 10:34 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic 0.51J ug/L 10/24/24 10:34 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 71.5 ug/L 10/24/24 10:34 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium 0.050J ug/L 10/24/24 10:34 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium 0.33 ug/L 10/26/24 17:52 7440-43-910/25/24 23:090.10 0.067 1
Chromium 1.6 ug/L 10/24/24 10:34 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt 2.0 ug/L 10/24/24 10:34 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper 2.1 ug/L 10/24/24 10:34 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead 0.25J ug/L 10/24/24 10:34 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 2.1 ug/L 10/24/24 10:34 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium ND ug/L 10/24/24 10:34 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/24/24 10:34 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 10:34 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 2.4 ug/L 10/24/24 10:34 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc ND ug/L 10/24/24 10:34 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/11/24 17:28 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/11/24 17:28 107-13-110.0 1.8 1
Benzene ND ug/L 10/11/24 17:28 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/11/24 17:28 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/11/24 17:28 75-27-41.0 0.31 1
Bromoform ND ug/L 10/11/24 17:28 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/11/24 17:28 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 10/11/24 17:28 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/11/24 17:28 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/11/24 17:28 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/11/24 17:28 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/11/24 17:28 75-00-31.0 0.65 1
Chloroform ND ug/L 10/11/24 17:28 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/11/24 17:28 74-87-3 v21.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/11/24 17:28 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/11/24 17:28 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/11/24 17:28 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/11/24 17:28 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/11/24 17:28 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/11/24 17:28 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/11/24 17:28 110-57-61.0 0.56 1
1,1-Dichloroethane ND ug/L 10/11/24 17:28 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/11/24 17:28 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/11/24 17:28 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/11/24 17:28 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/11/24 17:28 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/11/24 17:28 78-87-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-3A Lab ID:92756913002 Collected:10/03/24 10:21 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/11/24 17:28 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/11/24 17:28 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/11/24 17:28 123-91-115038.7 1
Ethylbenzene ND ug/L 10/11/24 17:28 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/11/24 17:28 591-78-6 v25.0 0.48 1
Iodomethane ND ug/L 10/11/24 17:28 74-88-4 L2,v220.0 9.7 1
Methylene Chloride ND ug/L 10/11/24 17:28 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/11/24 17:28 108-10-15.0 2.7 1
Styrene ND ug/L 10/11/24 17:28 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/11/24 17:28 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/11/24 17:28 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/11/24 17:28 127-18-41.0 0.29 1
Toluene ND ug/L 10/11/24 17:28 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/11/24 17:28 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/11/24 17:28 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/11/24 17:28 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/11/24 17:28 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/11/24 17:28 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/11/24 17:28 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 10/11/24 17:28 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/11/24 17:28 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %10/11/24 17:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %10/11/24 17:28 17060-07-070-130 1
Toluene-d8 (S)106 %10/11/24 17:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-6A Lab ID:92756913003 Collected:10/03/24 08:55 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 10:37 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic ND ug/L 10/24/24 10:37 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 95.4 ug/L 10/24/24 10:37 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium 0.33 ug/L 10/24/24 10:37 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium ND ug/L 10/24/24 10:37 7440-43-9 1g10/16/24 06:070.10 0.067 1
Chromium 4.9 ug/L 10/24/24 10:37 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt ND ug/L 10/24/24 10:37 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper 0.88J ug/L 10/24/24 10:37 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead ND ug/L 10/24/24 10:37 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 3.0 ug/L 10/24/24 10:37 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium ND ug/L 10/24/24 10:37 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/24/24 10:37 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 10:37 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 1.1 ug/L 10/24/24 10:37 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc 13.7 ug/L 10/24/24 10:37 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 04:33 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 04:33 107-13-110.0 1.8 1
Benzene ND ug/L 10/12/24 04:33 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 04:33 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 04:33 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 04:33 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 04:33 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 04:33 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 04:33 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 04:33 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 04:33 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 04:33 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 04:33 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 04:33 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 04:33 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 04:33 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/24 04:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/12/24 04:33 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 04:33 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/12/24 04:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 04:33 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/12/24 04:33 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 04:33 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 04:33 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/12/24 04:33 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 04:33 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 04:33 78-87-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-6A Lab ID:92756913003 Collected:10/03/24 08:55 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/12/24 04:33 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 04:33 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 04:33 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 04:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 04:33 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 04:33 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 04:33 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 04:33 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 04:33 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 04:33 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 04:33 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 04:33 127-18-41.0 0.29 1
Toluene ND ug/L 10/12/24 04:33 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 04:33 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 04:33 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 04:33 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 04:33 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 04:33 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 04:33 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 04:33 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 04:33 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %10/12/24 04:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)86 %10/12/24 04:33 17060-07-070-130 1
Toluene-d8 (S)111 %10/12/24 04:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-7 Lab ID:92756913004 Collected:10/03/24 09:12 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 10:39 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic ND ug/L 10/24/24 10:39 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 207 ug/L 10/24/24 10:39 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium 0.22 ug/L 10/24/24 10:39 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium 0.39 ug/L 10/26/24 17:55 7440-43-910/25/24 23:090.10 0.067 1
Chromium 1.3 ug/L 10/24/24 10:39 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt 0.51J ug/L 10/24/24 10:39 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper 1.9 ug/L 10/24/24 10:39 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead 0.83J ug/L 10/24/24 10:39 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 3.4 ug/L 10/24/24 10:39 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium ND ug/L 10/24/24 10:39 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/24/24 10:39 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 10:39 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 2.0 ug/L 10/24/24 10:39 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc 17.8 ug/L 10/24/24 10:39 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 04:51 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 04:51 107-13-110.0 1.8 1
Benzene ND ug/L 10/12/24 04:51 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 04:51 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 04:51 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 04:51 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 04:51 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 04:51 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 04:51 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 04:51 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 04:51 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 04:51 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 04:51 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 04:51 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 04:51 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 04:51 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/24 04:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/12/24 04:51 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 04:51 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/12/24 04:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 04:51 110-57-6 v1,v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/12/24 04:51 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 04:51 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 04:51 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/12/24 04:51 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 04:51 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 04:51 78-87-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-7 Lab ID:92756913004 Collected:10/03/24 09:12 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/12/24 04:51 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 04:51 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 04:51 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 04:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 04:51 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 04:51 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 04:51 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 04:51 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 04:51 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 04:51 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 04:51 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 04:51 127-18-41.0 0.29 1
Toluene ND ug/L 10/12/24 04:51 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 04:51 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 04:51 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 04:51 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 04:51 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 04:51 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 04:51 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 04:51 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 04:51 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %10/12/24 04:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)85 %10/12/24 04:51 17060-07-070-130 1
Toluene-d8 (S)111 %10/12/24 04:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-8 Lab ID:92756913005 Collected:10/03/24 09:30 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 10:42 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic ND ug/L 10/24/24 10:42 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 154 ug/L 10/24/24 10:42 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium 0.57 ug/L 10/24/24 10:42 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium 0.13 ug/L 10/26/24 17:57 7440-43-910/25/24 23:090.10 0.067 1
Chromium 12.1 ug/L 10/24/24 10:42 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt 5.1 ug/L 10/24/24 10:42 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper 7.4 ug/L 10/24/24 10:42 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead 1.5 ug/L 10/24/24 10:42 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 4.6 ug/L 10/24/24 10:42 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium 0.46J ug/L 10/24/24 10:42 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/24/24 10:42 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 10:42 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 13.0 ug/L 10/24/24 10:42 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc 20.8 ug/L 10/24/24 10:42 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 05:09 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 05:09 107-13-110.0 1.8 1
Benzene ND ug/L 10/12/24 05:09 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 05:09 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 05:09 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 05:09 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 05:09 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 05:09 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 05:09 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 05:09 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 05:09 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 05:09 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 05:09 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 05:09 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 05:09 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 05:09 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/24 05:09 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/12/24 05:09 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 05:09 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/12/24 05:09 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 05:09 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/12/24 05:09 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 05:09 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 05:09 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/12/24 05:09 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 05:09 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 05:09 78-87-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-8 Lab ID:92756913005 Collected:10/03/24 09:30 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/12/24 05:09 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 05:09 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 05:09 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 05:09 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 05:09 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 05:09 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 05:09 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 05:09 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 05:09 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 05:09 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 05:09 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 05:09 127-18-41.0 0.29 1
Toluene ND ug/L 10/12/24 05:09 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 05:09 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 05:09 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 05:09 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 05:09 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 05:09 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 05:09 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 05:09 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 05:09 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %10/12/24 05:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)86 %10/12/24 05:09 17060-07-070-130 1
Toluene-d8 (S)111 %10/12/24 05:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-40 Lab ID:92756913006 Collected:10/03/24 15:17 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 10:45 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic ND ug/L 10/24/24 10:45 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 97.3 ug/L 10/24/24 10:45 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium 0.039J ug/L 10/24/24 10:45 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium 0.17 ug/L 10/26/24 18:00 7440-43-910/25/24 23:090.10 0.067 1
Chromium 4.5 ug/L 10/24/24 10:45 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt 0.26J ug/L 10/24/24 10:45 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper 1.5 ug/L 10/24/24 10:45 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead 0.41J ug/L 10/24/24 10:45 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 1.4 ug/L 10/24/24 10:45 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium ND ug/L 10/24/24 10:45 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/24/24 10:45 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 10:45 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 1.9 ug/L 10/24/24 10:45 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc 27.0 ug/L 10/24/24 10:45 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 05:28 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 05:28 107-13-110.0 1.8 1
Benzene ND ug/L 10/12/24 05:28 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 05:28 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 05:28 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 05:28 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 05:28 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 05:28 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 05:28 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 05:28 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 05:28 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 05:28 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 05:28 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 05:28 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 05:28 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 05:28 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/24 05:28 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/12/24 05:28 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 05:28 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/12/24 05:28 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 05:28 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/12/24 05:28 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 05:28 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 05:28 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/12/24 05:28 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 05:28 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 05:28 78-87-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-40 Lab ID:92756913006 Collected:10/03/24 15:17 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/12/24 05:28 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 05:28 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 05:28 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 05:28 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 05:28 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 05:28 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 05:28 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 05:28 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 05:28 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 05:28 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 05:28 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 05:28 127-18-41.0 0.29 1
Toluene ND ug/L 10/12/24 05:28 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 05:28 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 05:28 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 05:28 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 05:28 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 05:28 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 05:28 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 05:28 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 05:28 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %10/12/24 05:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %10/12/24 05:28 17060-07-070-130 1
Toluene-d8 (S)109 %10/12/24 05:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-13BR Lab ID:92756913007 Collected:10/03/24 09:51 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 10:47 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic ND ug/L 10/24/24 10:47 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 131 ug/L 10/24/24 10:47 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium 0.079J ug/L 10/24/24 10:47 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium 0.069J ug/L 10/26/24 18:03 7440-43-910/25/24 23:090.10 0.067 1
Chromium 0.79J ug/L 10/24/24 10:47 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt ND ug/L 10/24/24 10:47 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper ND ug/L 10/24/24 10:47 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead ND ug/L 10/24/24 10:47 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 1.6 ug/L 10/24/24 10:47 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium ND ug/L 10/24/24 10:47 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver 0.040J ug/L 10/24/24 10:47 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 10:47 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 0.98J ug/L 10/24/24 10:47 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc ND ug/L 10/24/24 10:47 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 05:46 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 05:46 107-13-110.0 1.8 1
Benzene ND ug/L 10/12/24 05:46 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 05:46 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 05:46 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 05:46 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 05:46 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 05:46 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 05:46 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 05:46 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 05:46 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 05:46 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 05:46 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 05:46 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 05:46 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 05:46 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/24 05:46 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/12/24 05:46 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 05:46 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/12/24 05:46 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 05:46 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/12/24 05:46 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 05:46 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 05:46 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/12/24 05:46 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 05:46 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 05:46 78-87-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-13BR Lab ID:92756913007 Collected:10/03/24 09:51 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/12/24 05:46 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 05:46 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 05:46 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 05:46 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 05:46 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 05:46 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 05:46 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 05:46 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 05:46 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 05:46 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 05:46 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 05:46 127-18-41.0 0.29 1
Toluene ND ug/L 10/12/24 05:46 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 05:46 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 05:46 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 05:46 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 05:46 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 05:46 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 05:46 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 05:46 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 05:46 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)92 %10/12/24 05:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)86 %10/12/24 05:46 17060-07-070-130 1
Toluene-d8 (S)107 %10/12/24 05:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-41 Lab ID:92756913008 Collected:10/03/24 17:03 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 10:55 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic ND ug/L 10/24/24 10:55 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 37.2 ug/L 10/24/24 10:55 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium ND ug/L 10/24/24 10:55 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium ND ug/L 10/24/24 10:55 7440-43-9 1g10/16/24 06:070.10 0.067 1
Chromium 3.2 ug/L 10/24/24 10:55 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt 0.27J ug/L 10/24/24 10:55 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper 0.83J ug/L 10/24/24 10:55 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead ND ug/L 10/24/24 10:55 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 1.2 ug/L 10/24/24 10:55 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium ND ug/L 10/24/24 10:55 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/24/24 10:55 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 10:55 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 2.5 ug/L 10/24/24 10:55 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc 6.8J ug/L 10/24/24 10:55 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 06:04 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 06:04 107-13-110.0 1.8 1
Benzene ND ug/L 10/12/24 06:04 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 06:04 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 06:04 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 06:04 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 06:04 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 06:04 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 06:04 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 06:04 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 06:04 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 06:04 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 06:04 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 06:04 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 06:04 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 06:04 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/24 06:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/12/24 06:04 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 06:04 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/12/24 06:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 06:04 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/12/24 06:04 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 06:04 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 06:04 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/12/24 06:04 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 06:04 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 06:04 78-87-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-41 Lab ID:92756913008 Collected:10/03/24 17:03 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/12/24 06:04 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 06:04 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 06:04 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 06:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 06:04 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 06:04 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 06:04 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 06:04 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 06:04 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 06:04 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 06:04 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 06:04 127-18-41.0 0.29 1
Toluene ND ug/L 10/12/24 06:04 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 06:04 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 06:04 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 06:04 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 06:04 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 06:04 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 06:04 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 06:04 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 06:04 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %10/12/24 06:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %10/12/24 06:04 17060-07-070-130 1
Toluene-d8 (S)110 %10/12/24 06:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-43 Lab ID:92756913009 Collected:10/03/24 16:23 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 10:57 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic ND ug/L 10/24/24 10:57 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 6.9 ug/L 10/24/24 10:57 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium ND ug/L 10/24/24 10:57 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium ND ug/L 10/24/24 10:57 7440-43-9 1g10/16/24 06:070.10 0.067 1
Chromium ND ug/L 10/24/24 10:57 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt ND ug/L 10/24/24 10:57 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper 0.46J ug/L 10/24/24 10:57 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead ND ug/L 10/24/24 10:57 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 0.95J ug/L 10/24/24 10:57 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium ND ug/L 10/24/24 10:57 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/24/24 10:57 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 10:57 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 2.6 ug/L 10/24/24 10:57 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc ND ug/L 10/24/24 10:57 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 06:23 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 06:23 107-13-110.0 1.8 1
Benzene ND ug/L 10/12/24 06:23 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 06:23 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 06:23 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 06:23 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 06:23 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 06:23 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 06:23 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 06:23 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 06:23 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 06:23 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 06:23 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 06:23 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 06:23 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 06:23 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/24 06:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/12/24 06:23 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 06:23 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/12/24 06:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 06:23 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/12/24 06:23 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 06:23 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 06:23 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 1.6 ug/L 10/12/24 06:23 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 06:23 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 06:23 78-87-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-43 Lab ID:92756913009 Collected:10/03/24 16:23 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/12/24 06:23 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 06:23 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 06:23 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 06:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 06:23 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 06:23 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 06:23 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 06:23 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 06:23 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 06:23 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 06:23 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 06:23 127-18-41.0 0.29 1
Toluene ND ug/L 10/12/24 06:23 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 06:23 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 06:23 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 06:23 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 06:23 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 06:23 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 06:23 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 06:23 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 06:23 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %10/12/24 06:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)85 %10/12/24 06:23 17060-07-070-130 1
Toluene-d8 (S)111 %10/12/24 06:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-4B Lab ID:92756913010 Collected:10/03/24 10:36 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 11:00 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic 2.7 ug/L 10/24/24 11:00 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 123 ug/L 10/24/24 11:00 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium 0.092J ug/L 10/24/24 11:00 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium 0.098J ug/L 10/26/24 18:05 7440-43-910/25/24 23:090.10 0.067 1
Chromium 0.74J ug/L 10/24/24 11:00 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt 27.2 ug/L 10/24/24 11:00 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper 6.5 ug/L 10/24/24 11:00 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead 0.27J ug/L 10/24/24 11:00 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 8.4 ug/L 10/24/24 11:00 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium ND ug/L 10/24/24 11:00 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/24/24 11:00 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 11:00 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 4.9 ug/L 10/24/24 11:00 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc ND ug/L 10/24/24 11:00 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 06:41 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 06:41 107-13-110.0 1.8 1
Benzene ND ug/L 10/12/24 06:41 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 06:41 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 06:41 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 06:41 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 06:41 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 06:41 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 06:41 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 06:41 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 06:41 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 06:41 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 06:41 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 06:41 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 06:41 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 06:41 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/24 06:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/12/24 06:41 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 06:41 95-50-11.0 0.34 1
1,4-Dichlorobenzene 0.79J ug/L 10/12/24 06:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 06:41 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/12/24 06:41 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 06:41 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 06:41 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/12/24 06:41 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 06:41 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 06:41 78-87-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-4B Lab ID:92756913010 Collected:10/03/24 10:36 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/12/24 06:41 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 06:41 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 06:41 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 06:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 06:41 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 06:41 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 06:41 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 06:41 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 06:41 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 06:41 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 06:41 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 06:41 127-18-41.0 0.29 1
Toluene ND ug/L 10/12/24 06:41 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 06:41 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 06:41 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 06:41 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 06:41 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 06:41 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 06:41 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 06:41 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 06:41 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %10/12/24 06:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %10/12/24 06:41 17060-07-070-130 1
Toluene-d8 (S)110 %10/12/24 06:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-39 Lab ID:92756913011 Collected:10/03/24 15:03 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 11:03 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic 0.77J ug/L 10/24/24 11:03 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 49.0 ug/L 10/24/24 11:03 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium 0.72 ug/L 10/24/24 11:03 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium 0.080J ug/L 10/26/24 18:13 7440-43-910/25/24 23:090.10 0.067 1
Chromium 8.2 ug/L 10/24/24 11:03 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt 2.8 ug/L 10/24/24 11:03 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper 7.4 ug/L 10/24/24 11:03 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead 3.4 ug/L 10/24/24 11:03 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 3.2 ug/L 10/24/24 11:03 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium 0.82J ug/L 10/24/24 11:03 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/24/24 11:03 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 11:03 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 29.2 ug/L 10/24/24 11:03 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc 12.6 ug/L 10/24/24 11:03 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 06:59 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 06:59 107-13-110.0 1.8 1
Benzene ND ug/L 10/12/24 06:59 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 06:59 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 06:59 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 06:59 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 06:59 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 06:59 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 06:59 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 06:59 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 06:59 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 06:59 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 06:59 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 06:59 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 06:59 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 06:59 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/24 06:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/12/24 06:59 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 06:59 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/12/24 06:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 06:59 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/12/24 06:59 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 06:59 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 06:59 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/12/24 06:59 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 06:59 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 06:59 78-87-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-39 Lab ID:92756913011 Collected:10/03/24 15:03 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/12/24 06:59 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 06:59 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 06:59 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 06:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 06:59 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 06:59 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 06:59 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 06:59 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 06:59 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 06:59 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 06:59 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 06:59 127-18-41.0 0.29 1
Toluene ND ug/L 10/12/24 06:59 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 06:59 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 06:59 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 06:59 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 06:59 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 06:59 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 06:59 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 06:59 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 06:59 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %10/12/24 06:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %10/12/24 06:59 17060-07-070-130 1
Toluene-d8 (S)109 %10/12/24 06:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-44 Lab ID:92756913012 Collected:10/03/24 17:36 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/24/24 11:05 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic ND ug/L 10/24/24 11:05 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 115 ug/L 10/24/24 11:05 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium 0.31 ug/L 10/24/24 11:05 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium ND ug/L 10/24/24 11:05 7440-43-9 1g10/16/24 06:070.10 0.067 1
Chromium 10.7 ug/L 10/24/24 11:05 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt 0.77J ug/L 10/24/24 11:05 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper ND ug/L 10/24/24 11:05 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead 0.82J ug/L 10/24/24 11:05 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 5.9 ug/L 10/24/24 11:05 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium 0.23J ug/L 10/24/24 11:05 7782-49-2 1g10/16/24 06:072.0 0.20 1
Silver 0.075J ug/L 10/24/24 11:05 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/24/24 11:05 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 6.4 ug/L 10/24/24 11:05 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc ND ug/L 10/24/24 11:05 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 07:17 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 07:17 107-13-110.0 1.8 1
Benzene 1.2 ug/L 10/12/24 07:17 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 07:17 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 07:17 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 07:17 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 07:17 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 07:17 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 07:17 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 07:17 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 07:17 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 07:17 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 07:17 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 07:17 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 07:17 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 07:17 124-48-11.0 0.36 1
Dibromomethane ND ug/L 10/12/24 07:17 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 07:17 95-50-11.0 0.34 1
1,4-Dichlorobenzene 0.40J ug/L 10/12/24 07:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 07:17 110-57-6 v21.0 0.56 1
1,1-Dichloroethane 0.38J ug/L 10/12/24 07:17 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 07:17 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 07:17 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 1.5 ug/L 10/12/24 07:17 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 07:17 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 07:17 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/12/24 07:17 10061-01-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Sample:MW-44 Lab ID:92756913012 Collected:10/03/24 17:36 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 10/12/24 07:17 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 07:17 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 07:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 07:17 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 07:17 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 07:17 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 07:17 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 07:17 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 07:17 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 07:17 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 07:17 127-18-41.0 0.29 1
Tetrahydrofuran 3.5J ug/L 10/12/24 07:17 109-99-910.0 3.5 1
Toluene ND ug/L 10/12/24 07:17 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 07:17 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 07:17 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 07:17 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 07:17 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 07:17 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 07:17 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 07:17 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 07:17 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %10/12/24 07:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %10/12/24 07:17 17060-07-070-130 1
Toluene-d8 (S)110 %10/12/24 07:17 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
1,4-Dioxane (p-Dioxane)2.5 ug/L 10/07/24 19:05 123-91-12.0 0.86 1
Surrogates
1,2-Dichloroethane-d4 (S)91 %10/07/24 19:05 17060-07-070-130 1
Toluene-d8 (S)95 %10/07/24 19:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
886834
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite, Unpres. EDN
Laboratory:Pace Analytical Services - Eden
Associated Lab Samples:92756913001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4567269
Associated Lab Samples:92756913001
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate mg/L ND 0.040 10/04/24 11:290.029
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4567270LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 1.51.5 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4567271MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92756913001
4567272
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 93 90-11092 1 101.5ND 1.4 1.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
886869
SM 5210B-2016
SM 5210B-2016
5210B BOD, 5 day Final EDN
Laboratory:Pace Analytical Services - Eden
Associated Lab Samples:92756913001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4567493
Associated Lab Samples:92756913001
Matrix:Water
AnalyzedMDL
BOD, 5 day mg/L ND 2.0 10/09/24 15:422.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4567494LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day mg/L 191198 96 84.6-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756807001
4567496SAMPLE DUPLICATE:
BOD, 5 day mg/L 142 R6325138
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1047472
EPA 3010
EPA 6020
6020 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92756913001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5757861
Associated Lab Samples:92756913001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 1.0 10/22/24 21:060.50
Arsenic ug/L ND 1.0 10/22/24 21:060.50
Barium ug/L ND 1.0 10/22/24 21:060.50
Beryllium ug/L ND 0.10 10/22/24 21:060.033
Cadmium ug/L ND 0.10 10/22/24 21:060.067
Chromium ug/L ND 1.0 10/22/24 21:060.50
Cobalt ug/L ND 1.0 10/22/24 21:060.24
Copper ug/L ND 1.0 10/22/24 21:060.42
Lead ug/L ND 1.0 10/22/24 21:060.22
Nickel ug/L ND 1.0 10/22/24 21:060.26
Selenium ug/L ND 2.0 10/22/24 21:060.20
Silver ug/L ND 0.50 10/22/24 21:060.028
Thallium ug/L ND 1.0 10/22/24 21:060.11
Vanadium ug/L ND 1.0 10/22/24 21:060.91
Zinc ug/L ND 10.0 10/22/24 21:066.7
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5757862LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 162150 108 80-120
Arsenic ug/L 109100 109 80-120
Barium ug/L 109100 109 80-120
Beryllium ug/L 11.210 112 80-120
Cadmium ug/L 10.910 109 80-120
Chromium ug/L 55.150 110 80-120
Cobalt ug/L 109100 109 80-120
Copper ug/L 57.750 115 80-120
Lead ug/L 105100 105 80-120
Nickel ug/L 56.350 113 80-120
Selenium ug/L 165150 110 80-120
Silver ug/L 50.450 101 80-120
Thallium ug/L 163150 109 80-120
Vanadium ug/L 105100 105 80-120
Zinc ug/L 222200 111 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5757863MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35910115001
5757864
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 150 111 75-125112 1 201501.1 168 170
Arsenic ug/L 100 111 75-125111 0 201005.8 116 116
Barium ug/L 100 111 75-125116 3 2010083.7 195 200
Beryllium ug/L 10 111 75-125113 1 20100.033U 11.1 11.3
Cadmium ug/L 10 106 75-125107 1 20100.067U 10.6 10.7
Chromium ug/L 50 114 75-125115 0 20500.50U 57.7 57.7
Cobalt ug/L 100 111 75-125111 0 201000.24U 111 111
Copper ug/L 50 116 75-125115 0 20500.43J 58.3 58.2
Lead ug/L 100 114 75-125114 0 201000.31J 114 114
Nickel ug/L 50 112 75-125113 1 20504.9 60.9 61.3
Selenium ug/L M11503975-12539 1 201500.37J 58.5 59.1
Silver ug/L E5010875-125108 0 20500.028U 53.9 54.1
Thallium ug/L 150 109 75-125112 2 201500.11U 164 168
Vanadium ug/L 100 111 75-125112 0 201001.3 113 113
Zinc ug/L 200 113 75-125113 0 202006.7U 227 227
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1048094
EPA 3010
EPA 6020
6020 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92756913002, 92756913003, 92756913004, 92756913005, 92756913006, 92756913007, 92756913008,
92756913009, 92756913010, 92756913011, 92756913012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5762053
Associated Lab Samples:92756913002, 92756913003, 92756913004, 92756913005, 92756913006, 92756913007, 92756913008,
92756913009, 92756913010, 92756913011, 92756913012
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 1.0 1g10/24/24 10:240.50
Arsenic ug/L ND 1.0 1g10/24/24 10:240.50
Barium ug/L ND 1.0 1g10/24/24 10:240.50
Beryllium ug/L ND 0.10 1g10/24/24 10:240.033
Cadmium ug/L 0.11 0.10 1g10/24/24 10:240.067
Chromium ug/L ND 1.0 1g10/24/24 10:240.50
Cobalt ug/L ND 1.0 1g10/24/24 10:240.24
Copper ug/L ND 1.0 1g10/24/24 10:240.42
Lead ug/L ND 1.0 1g10/24/24 10:240.22
Nickel ug/L ND 1.0 1g10/24/24 10:240.26
Selenium ug/L ND 2.0 1g10/24/24 10:240.20
Silver ug/L ND 0.50 1g10/24/24 10:240.028
Thallium ug/L ND 1.0 1g10/24/24 10:240.11
Vanadium ug/L ND 1.0 1g10/24/24 10:240.91
Zinc ug/L ND 10.0 1g10/24/24 10:246.7
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5762054LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 54.3 1g5010980-120
Arsenic ug/L 50.3 1g5010180-120
Barium ug/L 55.5 1g5011180-120
Beryllium ug/L 5.4 1g510880-120
Cadmium ug/L 5.6 1g511280-120
Chromium ug/L 53.0 1g5010680-120
Cobalt ug/L 57.0 1g5011480-120
Copper ug/L 53.4 1g5010780-120
Lead ug/L 52.1 1g5010480-120
Nickel ug/L 52.4 1g5010580-120
Selenium ug/L 53.6 1g5010780-120
Silver ug/L 5.8 1g511680-120
Thallium ug/L 56.1 1g5011280-120
Vanadium ug/L 53.2 1g5010680-120
Zinc ug/L 253 1g25010180-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5762055MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35911307005
5762056
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 1g5010775-125108 0 20500.50U 53.7 53.8
Arsenic ug/L 1g5011375-125113 0 20500.50U 56.7 56.7
Barium ug/L 1g5010875-125110 1 205010.5 64.8 65.3
Beryllium ug/L 1g511175-125111 0 2050.033U 5.6 5.6
Cadmium ug/L 1g511175-125112 1 2050.067U 5.6 5.6
Chromium ug/L 1g5011275-125111 1 20500.50U 56.4 55.9
Cobalt ug/L 1g5011275-125113 1 20500.24U 56.3 56.9
Copper ug/L 1g5011375-125113 0 20500.42U 56.9 56.9
Lead ug/L 1g5011175-125110 1 20500.22U 55.6 55.3
Nickel ug/L 1g,CH5011775-125116 0 20500.26U 58.6 58.4
Selenium ug/L 1g,CH5011375-125113 0 20500.62J 57.2 57.1
Silver ug/L 1g511575-125116 1 2050.028U 5.8 5.8
Thallium ug/L 1g5011275-125112 0 20500.11U 55.8 55.8
Vanadium ug/L 1g5010975-125108 2 20500.91U 54.9 54.1
Zinc ug/L 1g25010675-125108 1 202506.7U 266 270
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1051146
EPA 3010
EPA 6020
6020 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92756913002, 92756913004, 92756913005, 92756913006, 92756913007, 92756913010, 92756913011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5778883
Associated Lab Samples:92756913002, 92756913004, 92756913005, 92756913006, 92756913007, 92756913010, 92756913011
Matrix:Water
AnalyzedMDL
Cadmium ug/L ND 0.10 10/26/24 17:290.067
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5778884LABORATORY CONTROL SAMPLE:
LCSSpike
Cadmium ug/L 5.55 110 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5778885MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92756911001
5778886
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cadmium ug/L 5 108 75-125107 2 2050.12 5.5 5.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
888072
EPA 8260D
EPA 8260D
8260D MSV Low Level Landfill
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92756913001, 92756913002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4573319
Associated Lab Samples:92756913001, 92756913002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/11/24 13:550.31
1,1,1-Trichloroethane ug/L ND 1.0 10/11/24 13:550.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/11/24 13:550.22
1,1,2-Trichloroethane ug/L ND 1.0 10/11/24 13:550.32
1,1-Dichloroethane ug/L ND 1.0 10/11/24 13:550.37
1,1-Dichloroethene ug/L ND 1.0 10/11/24 13:550.35
1,2,3-Trichloropropane ug/L ND 1.0 10/11/24 13:550.26
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/11/24 13:550.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/11/24 13:550.27
1,2-Dichlorobenzene ug/L ND 1.0 10/11/24 13:550.34
1,2-Dichloroethane ug/L ND 1.0 10/11/24 13:550.32
1,2-Dichloropropane ug/L ND 1.0 10/11/24 13:550.36
1,4-Dichlorobenzene ug/L ND 1.0 10/11/24 13:550.33
1,4-Dioxane (p-Dioxane)ug/L ND 150 10/11/24 13:5538.7
2-Butanone (MEK)ug/L ND 5.0 10/11/24 13:554.0
2-Hexanone ug/L ND 5.0 v210/11/24 13:550.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/11/24 13:552.7
Acetone ug/L ND 25.0 10/11/24 13:555.1
Acrylonitrile ug/L ND 10.0 10/11/24 13:551.8
Benzene ug/L ND 1.0 10/11/24 13:550.34
Bromochloromethane ug/L ND 1.0 10/11/24 13:550.47
Bromodichloromethane ug/L ND 1.0 10/11/24 13:550.31
Bromoform ug/L ND 1.0 10/11/24 13:550.34
Bromomethane ug/L ND 2.0 v210/11/24 13:551.7
Carbon disulfide ug/L ND 2.0 10/11/24 13:550.36
Carbon tetrachloride ug/L ND 1.0 10/11/24 13:550.33
Chlorobenzene ug/L ND 1.0 10/11/24 13:550.28
Chloroethane ug/L ND 1.0 10/11/24 13:550.65
Chloroform ug/L ND 1.0 10/11/24 13:550.43
Chloromethane ug/L ND 1.0 v210/11/24 13:550.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/11/24 13:550.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/11/24 13:550.36
Dibromochloromethane ug/L ND 1.0 10/11/24 13:550.36
Dibromomethane ug/L ND 1.0 10/11/24 13:550.39
Ethylbenzene ug/L ND 1.0 10/11/24 13:550.30
Iodomethane ug/L ND 20.0 v210/11/24 13:559.7
Methylene Chloride ug/L ND 5.0 10/11/24 13:552.0
Styrene ug/L ND 1.0 10/11/24 13:550.29
Tetrachloroethene ug/L ND 1.0 10/11/24 13:550.29
Toluene ug/L ND 1.0 10/11/24 13:550.24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4573319
Associated Lab Samples:92756913001, 92756913002
Matrix:Water
AnalyzedMDL
trans-1,2-Dichloroethene ug/L ND 1.0 10/11/24 13:550.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/11/24 13:550.36
trans-1,4-Dichloro-2-butene ug/L ND 1.0 10/11/24 13:550.56
Trichloroethene ug/L ND 1.0 10/11/24 13:550.38
Trichlorofluoromethane ug/L ND 1.0 10/11/24 13:550.30
Vinyl acetate ug/L ND 2.0 10/11/24 13:551.3
Vinyl chloride ug/L ND 1.0 10/11/24 13:550.39
Xylene (Total)ug/L ND 1.0 10/11/24 13:550.34
1,2-Dichloroethane-d4 (S)%102 70-130 10/11/24 13:55
4-Bromofluorobenzene (S)%100 70-130 10/11/24 13:55
Toluene-d8 (S)%103 70-130 10/11/24 13:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573320LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 18.220 91 70-130
1,1,1-Trichloroethane ug/L 18.120 90 70-130
1,1,2,2-Tetrachloroethane ug/L 17.920 90 70-130
1,1,2-Trichloroethane ug/L 18.820 94 70-130
1,1-Dichloroethane ug/L 20.820 104 70-130
1,1-Dichloroethene ug/L 21.320 107 69-131
1,2,3-Trichloropropane ug/L 17.720 89 70-130
1,2-Dibromo-3-chloropropane ug/L 18.820 94 70-130
1,2-Dibromoethane (EDB)ug/L 18.120 91 70-130
1,2-Dichlorobenzene ug/L 19.520 98 70-130
1,2-Dichloroethane ug/L 19.220 96 70-130
1,2-Dichloropropane ug/L 21.020 105 70-130
1,4-Dichlorobenzene ug/L 19.020 95 70-130
1,4-Dioxane (p-Dioxane)ug/L 372400 93 70-132
2-Butanone (MEK)ug/L 33.840 84 67-133
2-Hexanone ug/L 32.0 v3408070-133
4-Methyl-2-pentanone (MIBK)ug/L 32.240 81 70-130
Acetone ug/L 34.140 85 67-130
Acrylonitrile ug/L 89.2100 89 70-130
Benzene ug/L 20.220 101 70-130
Bromochloromethane ug/L 18.120 90 70-130
Bromodichloromethane ug/L 19.220 96 70-130
Bromoform ug/L 17.120 85 70-133
Bromomethane ug/L 8.6 v3204341-148
Carbon disulfide ug/L 19.320 97 70-131
Carbon tetrachloride ug/L 19.220 96 70-130
Chlorobenzene ug/L 18.620 93 70-130
Chloroethane ug/L 17.620 88 41-157
Chloroform ug/L 18.920 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573320LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 15.8 v3207959-141
cis-1,2-Dichloroethene ug/L 20.020 100 70-130
cis-1,3-Dichloropropene ug/L 19.020 95 70-130
Dibromochloromethane ug/L 18.420 92 70-130
Dibromomethane ug/L 19.820 99 70-130
Ethylbenzene ug/L 19.020 95 70-130
Iodomethane ug/L 16.6J L2,v3404257-140
Methylene Chloride ug/L 19.520 97 62-130
Styrene ug/L 18.820 94 70-130
Tetrachloroethene ug/L 18.620 93 70-130
Toluene ug/L 19.120 95 70-130
trans-1,2-Dichloroethene ug/L 21.320 107 70-130
trans-1,3-Dichloropropene ug/L 18.720 93 70-130
trans-1,4-Dichloro-2-butene ug/L 18.120 91 57-149
Trichloroethene ug/L 20.020 100 70-130
Trichlorofluoromethane ug/L 18.920 95 57-130
Vinyl acetate ug/L 36.240 90 70-141
Vinyl chloride ug/L 18.920 95 66-140
Xylene (Total)ug/L 55.560 92 70-130
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4573321MATRIX SPIKE SAMPLE:
MSSpike
Result
92756912001
1,1,1,2-Tetrachloroethane ug/L 13.6 M1206870-146ND
1,1,1-Trichloroethane ug/L 15.120 75 70-150ND
1,1,2,2-Tetrachloroethane ug/L 11.5 M1205866-144ND
1,1,2-Trichloroethane ug/L 12.1 M1206070-142ND
1,1-Dichloroethane ug/L 13.3 M1206668-150ND
1,1-Dichloroethene ug/L 14.220 71 64-162ND
1,2,3-Trichloropropane ug/L 11.4 M1205766-144ND
1,2-Dibromo-3-chloropropane ug/L 11.0 M1205562-146ND
1,2-Dibromoethane (EDB)ug/L 12.2 M1206170-143ND
1,2-Dichlorobenzene ug/L 13.0 M1206570-142ND
1,2-Dichloroethane ug/L 14.020 70 68-145ND
1,2-Dichloropropane ug/L 12.9 M1206570-144ND
1,4-Dichlorobenzene ug/L 13.2 M1206670-140ND
1,4-Dioxane (p-Dioxane)ug/L 208 M14005266-151ND
2-Butanone (MEK)ug/L 22.3 M1405657-156ND
2-Hexanone ug/L 21.5 M1405462-153ND
4-Methyl-2-pentanone (MIBK)ug/L 22.1 M1405565-144ND
Acetone ug/L 24.2J40 60 49-162ND
Acrylonitrile ug/L 60.2100 60 59-155ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4573321MATRIX SPIKE SAMPLE:
MSSpike
Result
92756912001
Benzene ug/L 13.520 68 68-144ND
Bromochloromethane ug/L 6.5 M1203370-148ND
Bromodichloromethane ug/L 13.7 M1206870-141ND
Bromoform ug/L 12.020 60 59-144ND
Bromomethane ug/L 15.220 76 23-190ND
Carbon disulfide ug/L 13.120 66 64-160ND
Carbon tetrachloride ug/L 15.820 79 70-147ND
Chlorobenzene ug/L 12.8 M1206470-143ND
Chloroethane ug/L 14.320 72 55-190ND
Chloroform ug/L 13.520 67 67-148ND
Chloromethane ug/L 14.020 70 38-180ND
cis-1,2-Dichloroethene ug/L 13.3 M1206667-151ND
cis-1,3-Dichloropropene ug/L 12.5 M1206270-142ND
Dibromochloromethane ug/L 12.7 M1206468-140ND
Dibromomethane ug/L 14.120 70 70-142ND
Ethylbenzene ug/L 13.2 M1206670-145ND
Iodomethane ug/L 30.5 v3407637-160ND
Methylene Chloride ug/L 13.820 69 54-149ND
Styrene ug/L 13.0 M1206570-147ND
Tetrachloroethene ug/L 13.8 M1206970-145ND
Toluene ug/L 12.9 M1206465-146ND
trans-1,2-Dichloroethene ug/L 13.820 69 69-155ND
trans-1,3-Dichloropropene ug/L 13.1 M1206570-142ND
trans-1,4-Dichloro-2-butene ug/L 10.020 50 39-149ND
Trichloroethene ug/L 13.920 70 70-152ND
Trichlorofluoromethane ug/L 16.420 82 60-158ND
Vinyl acetate ug/L 25.040 62 56-157ND
Vinyl chloride ug/L 14.820 74 51-178ND
Xylene (Total)ug/L 40.4 MS606770-146ND
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756912002
4573322SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756912002
4573322SAMPLE DUPLICATE:
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
1,4-Dioxane (p-Dioxane)ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND v230ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 0.54J 300.56J
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%11098
4-Bromofluorobenzene (S)%99101
Toluene-d8 (S)%98103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
888074
EPA 8260D
EPA 8260D
8260D MSV Low Level Landfill
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92756913003, 92756913004, 92756913005, 92756913006, 92756913007, 92756913008, 92756913009,
92756913010, 92756913011, 92756913012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4573332
Associated Lab Samples:92756913003, 92756913004, 92756913005, 92756913006, 92756913007, 92756913008, 92756913009,
92756913010, 92756913011, 92756913012
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/12/24 00:160.31
1,1,1-Trichloroethane ug/L ND 1.0 10/12/24 00:160.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/12/24 00:160.22
1,1,2-Trichloroethane ug/L ND 1.0 10/12/24 00:160.32
1,1-Dichloroethane ug/L ND 1.0 10/12/24 00:160.37
1,1-Dichloroethene ug/L ND 1.0 10/12/24 00:160.35
1,2,3-Trichloropropane ug/L ND 1.0 10/12/24 00:160.26
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/12/24 00:160.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/12/24 00:160.27
1,2-Dichlorobenzene ug/L ND 1.0 10/12/24 00:160.34
1,2-Dichloroethane ug/L ND 1.0 10/12/24 00:160.32
1,2-Dichloropropane ug/L ND 1.0 10/12/24 00:160.36
1,4-Dichlorobenzene ug/L ND 1.0 10/12/24 00:160.33
1,4-Dioxane (p-Dioxane)ug/L ND 150 10/12/24 00:1638.7
2-Butanone (MEK)ug/L ND 5.0 10/12/24 00:164.0
2-Hexanone ug/L ND 5.0 10/12/24 00:160.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/12/24 00:162.7
Acetone ug/L ND 25.0 10/12/24 00:165.1
Acrylonitrile ug/L ND 10.0 10/12/24 00:161.8
Benzene ug/L ND 1.0 10/12/24 00:160.34
Bromochloromethane ug/L ND 1.0 10/12/24 00:160.47
Bromodichloromethane ug/L ND 1.0 10/12/24 00:160.31
Bromoform ug/L ND 1.0 10/12/24 00:160.34
Bromomethane ug/L ND 2.0 10/12/24 00:161.7
Carbon disulfide ug/L ND 2.0 10/12/24 00:160.36
Carbon tetrachloride ug/L ND 1.0 10/12/24 00:160.33
Chlorobenzene ug/L ND 1.0 10/12/24 00:160.28
Chloroethane ug/L ND 1.0 10/12/24 00:160.65
Chloroform ug/L ND 1.0 10/12/24 00:160.43
Chloromethane ug/L ND 1.0 10/12/24 00:160.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/12/24 00:160.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/12/24 00:160.36
Dibromochloromethane ug/L ND 1.0 10/12/24 00:160.36
Dibromomethane ug/L ND 1.0 10/12/24 00:160.39
Ethylbenzene ug/L ND 1.0 10/12/24 00:160.30
Iodomethane ug/L ND 20.0 v210/12/24 00:169.7
Methylene Chloride ug/L ND 5.0 10/12/24 00:162.0
Styrene ug/L ND 1.0 10/12/24 00:160.29
Tetrachloroethene ug/L ND 1.0 10/12/24 00:160.29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4573332
Associated Lab Samples:92756913003, 92756913004, 92756913005, 92756913006, 92756913007, 92756913008, 92756913009,
92756913010, 92756913011, 92756913012
Matrix:Water
AnalyzedMDL
Tetrahydrofuran ug/L ND 10.0 10/12/24 00:163.5
Toluene ug/L ND 1.0 10/12/24 00:160.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/12/24 00:160.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/12/24 00:160.36
trans-1,4-Dichloro-2-butene ug/L ND 1.0 v210/12/24 00:160.56
Trichloroethene ug/L ND 1.0 10/12/24 00:160.38
Trichlorofluoromethane ug/L ND 1.0 10/12/24 00:160.30
Vinyl acetate ug/L ND 2.0 v210/12/24 00:161.3
Vinyl chloride ug/L ND 1.0 10/12/24 00:160.39
Xylene (Total)ug/L ND 1.0 10/12/24 00:160.34
1,2-Dichloroethane-d4 (S)%88 70-130 10/12/24 00:16
4-Bromofluorobenzene (S)%100 70-130 10/12/24 00:16
Toluene-d8 (S)%110 70-130 10/12/24 00:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573333LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 17.720 89 70-130
1,1,1-Trichloroethane ug/L 18.620 93 70-130
1,1,2,2-Tetrachloroethane ug/L 17.520 88 70-130
1,1,2-Trichloroethane ug/L 18.520 93 70-130
1,1-Dichloroethane ug/L 18.220 91 70-130
1,1-Dichloroethene ug/L 18.820 94 69-131
1,2,3-Trichloropropane ug/L 18.320 91 70-130
1,2-Dibromo-3-chloropropane ug/L 17.320 87 70-130
1,2-Dibromoethane (EDB)ug/L 18.520 92 70-130
1,2-Dichlorobenzene ug/L 19.120 96 70-130
1,2-Dichloroethane ug/L 18.720 93 70-130
1,2-Dichloropropane ug/L 19.620 98 70-130
1,4-Dichlorobenzene ug/L 18.220 91 70-130
1,4-Dioxane (p-Dioxane)ug/L 374400 94 70-132
2-Butanone (MEK)ug/L 33.440 84 67-133
2-Hexanone ug/L 31.340 78 70-133
4-Methyl-2-pentanone (MIBK)ug/L 32.640 81 70-130
Acetone ug/L 35.040 87 67-130
Acrylonitrile ug/L 87.7100 88 70-130
Benzene ug/L 20.420 102 70-130
Bromochloromethane ug/L 18.420 92 70-130
Bromodichloromethane ug/L 18.020 90 70-130
Bromoform ug/L 16.920 85 70-133
Bromomethane ug/L 18.820 94 41-148
Carbon disulfide ug/L 18.520 93 70-131
Carbon tetrachloride ug/L 19.020 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573333LABORATORY CONTROL SAMPLE:
LCSSpike
Chlorobenzene ug/L 18.820 94 70-130
Chloroethane ug/L 19.820 99 41-157
Chloroform ug/L 19.420 97 70-130
Chloromethane ug/L 17.220 86 59-141
cis-1,2-Dichloroethene ug/L 18.220 91 70-130
cis-1,3-Dichloropropene ug/L 18.220 91 70-130
Dibromochloromethane ug/L 17.320 86 70-130
Dibromomethane ug/L 19.720 98 70-130
Ethylbenzene ug/L 18.520 92 70-130
Iodomethane ug/L 27.8 v3406957-140
Methylene Chloride ug/L 17.520 88 62-130
Styrene ug/L 18.920 94 70-130
Tetrachloroethene ug/L 18.720 93 70-130
Tetrahydrofuran ug/L 179200 89 70-131
Toluene ug/L 19.020 95 70-130
trans-1,2-Dichloroethene ug/L 18.320 91 70-130
trans-1,3-Dichloropropene ug/L 18.020 90 70-130
trans-1,4-Dichloro-2-butene ug/L 22.3 v32011157-149
Trichloroethene ug/L 20.420 102 70-130
Trichlorofluoromethane ug/L 20.720 103 57-130
Vinyl acetate ug/L 29.8 v3407570-141
Vinyl chloride ug/L 17.220 86 66-140
Xylene (Total)ug/L 56.660 94 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4573334MATRIX SPIKE SAMPLE:
MSSpike
Result
92756913003
1,1,1,2-Tetrachloroethane ug/L 22.220 111 70-146ND
1,1,1-Trichloroethane ug/L 25.820 129 70-150ND
1,1,2,2-Tetrachloroethane ug/L 21.820 109 66-144ND
1,1,2-Trichloroethane ug/L 23.420 117 70-142ND
1,1-Dichloroethane ug/L 25.220 126 68-150ND
1,1-Dichloroethene ug/L 26.020 130 64-162ND
1,2,3-Trichloropropane ug/L 22.620 113 66-144ND
1,2-Dibromo-3-chloropropane ug/L 19.520 98 62-146ND
1,2-Dibromoethane (EDB)ug/L 22.620 113 70-143ND
1,2-Dichlorobenzene ug/L 23.220 116 70-142ND
1,2-Dichloroethane ug/L 24.920 125 68-145ND
1,2-Dichloropropane ug/L 25.420 127 70-144ND
1,4-Dichlorobenzene ug/L 23.420 117 70-140ND
1,4-Dioxane (p-Dioxane)ug/L 452400 113 66-151ND
2-Butanone (MEK)ug/L 42.040 105 57-156ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4573334MATRIX SPIKE SAMPLE:
MSSpike
Result
92756913003
2-Hexanone ug/L 36.940 92 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 39.540 99 65-144ND
Acetone ug/L 43.440 108 49-162ND
Acrylonitrile ug/L 111100 111 59-155ND
Benzene ug/L 26.420 132 68-144ND
Bromochloromethane ug/L 24.820 124 70-148ND
Bromodichloromethane ug/L 23.120 115 70-141ND
Bromoform ug/L 20.920 104 59-144ND
Bromomethane ug/L 23.120 116 23-190ND
Carbon disulfide ug/L 26.920 134 64-160ND
Carbon tetrachloride ug/L 25.520 128 70-147ND
Chlorobenzene ug/L 23.020 115 70-143ND
Chloroethane ug/L 26.720 134 55-190ND
Chloroform ug/L 25.520 128 67-148ND
Chloromethane ug/L 22.920 115 38-180ND
cis-1,2-Dichloroethene ug/L 24.620 123 67-151ND
cis-1,3-Dichloropropene ug/L 23.520 118 70-142ND
Dibromochloromethane ug/L 21.620 108 68-140ND
Dibromomethane ug/L 25.220 126 70-142ND
Ethylbenzene ug/L 23.220 116 70-145ND
Iodomethane ug/L 47.440 117 37-160ND
Methylene Chloride ug/L 23.120 116 54-149ND
Styrene ug/L 23.020 115 70-147ND
Tetrachloroethene ug/L 22.920 115 70-145ND
Tetrahydrofuran ug/L 221200 111 48-160ND
Toluene ug/L 24.420 122 65-146ND
trans-1,2-Dichloroethene ug/L 26.320 131 69-155ND
trans-1,3-Dichloropropene ug/L 23.720 119 70-142ND
trans-1,4-Dichloro-2-butene ug/L 18.6 v1209339-149ND
Trichloroethene ug/L 26.320 132 70-152ND
Trichlorofluoromethane ug/L 29.020 145 60-158ND
Vinyl acetate ug/L 40.540 101 56-157ND
Vinyl chloride ug/L 24.420 122 51-178ND
Xylene (Total)ug/L 71.360 119 70-146ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756913004
4573335SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756913004
4573335SAMPLE DUPLICATE:
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
1,4-Dioxane (p-Dioxane)ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND v130ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9285
4-Bromofluorobenzene (S)%9899
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756913004
4573335SAMPLE DUPLICATE:
Toluene-d8 (S)%110111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
887074
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92756913012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4568469
Associated Lab Samples:92756913012
Matrix:Water
AnalyzedMDL
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 10/07/24 17:090.86
1,2-Dichloroethane-d4 (S)%89 70-130 10/07/24 17:09
Toluene-d8 (S)%93 70-130 10/07/24 17:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4568470LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 18.520 93 67-130
1,2-Dichloroethane-d4 (S)%90 70-130
Toluene-d8 (S)%93 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4568471MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92756909001
4568472
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 91 10-17095 3 30201.3J 19.5 20.2
1,2-Dichloroethane-d4 (S)%90 70-13092 30
Toluene-d8 (S)%94 70-13094 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
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Huntersville, NC 28078
[phone]
Page 48 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
887323
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92756913001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4569421
Associated Lab Samples:92756913001
Matrix:Water
AnalyzedMDL
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 10/08/24 15:180.86
1,2-Dichloroethane-d4 (S)%83 70-130 10/08/24 15:18
Toluene-d8 (S)%90 70-130 10/08/24 15:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4569422LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 19.620 98 67-130
1,2-Dichloroethane-d4 (S)%83 70-130
Toluene-d8 (S)%91 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4569423MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92757091002
4569424
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 94 10-17096 2 3020ND18.9 19.2
1,2-Dichloroethane-d4 (S)%85 70-13085 30
Toluene-d8 (S)%88 70-13089 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
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Huntersville, NC 28078
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Page 49 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1048897
SM 4500-S2F
SM 4500-S2F
4500S2F Sulfide
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92756913001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5766725
Associated Lab Samples:92756913001
Matrix:Water
AnalyzedMDL
Sulfide mg/L ND 0.10 10/18/24 09:500.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5766726LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide mg/L 5.86 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
5766728MATRIX SPIKE SAMPLE:
MSSpike
Result
35911594001
Sulfide mg/L 5.96 96 80-1200.16
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
35911596001
5766727SAMPLE DUPLICATE:
Sulfide mg/L ND 200.10U
REPORT OF LABORATORY ANALYSIS
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Page 50 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1049466
EPA 365.4
EPA 365.4
365.4 Phosphorus
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92756913001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5769599
Associated Lab Samples:92756913001
Matrix:Water
AnalyzedMDL
Phosphorus, Total (as P)mg/L ND 0.10 10/22/24 12:390.070
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5769600LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus, Total (as P)mg/L 3.94 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5769602MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92756793003
5769601
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus, Total (as P)mg/L 40 108 80-120106 2 20402.0 45.1 44.5
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5769604MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35910434002
5769603
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus, Total (as P)mg/L 4 103 80-120104 1 2040.57 4.7 4.7
REPORT OF LABORATORY ANALYSIS
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Page 51 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1047568
EPA 410.4
EPA 410.4
410.4 COD
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92756913001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5758160
Associated Lab Samples:92756913001
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand mg/L ND 20.0 10/15/24 15:5512.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5758161LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand mg/L 504500 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5758163MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35911043002
5758162
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand mg/L 500 95 90-11096 1 2050028.6 501 509
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5758165MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92755811002
5758164
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand mg/L 500 96 90-11096 1 2050020.9 501 498
REPORT OF LABORATORY ANALYSIS
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Page 52 of 63
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
BATCH QUALIFIERS
Batch: 1048296
Samples 92756911001, 92754732012, 92756913-(2, 4, 5, 6, 7, 10, 11) were sent back to reprep for Cd hit in blank[1]
ANALYTE QUALIFIERS
Samples 92756911001, 92754732012, 92756913-(2, 4, 5, 6, 7, 10, 11) were sent back to reprep for Cd hit in blank1g
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.B2
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.CH
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analysis conducted outside the EPA method holding time.H1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The RPD between valid sample dilutions exceeded 30%.R6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
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Page 53 of 63
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
ANALYTE QUALIFIERS
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
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Page 54 of 63
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92756913001 886834LAGOONEPA 353.2 Rev 2.0 1993
92756913001 886869 887174LAGOONSM 5210B-2016 SM 5210B-2016
92756913001 1047472 1047534LAGOONEPA 3010 EPA 6020
92756913002 1048094 1048296MW-3A EPA 3010 EPA 6020
92756913002 1051146 1051157MW-3A EPA 3010 EPA 6020
92756913003 1048094 1048296MW-6A EPA 3010 EPA 6020
92756913004 1048094 1048296MW-7 EPA 3010 EPA 6020
92756913004 1051146 1051157MW-7 EPA 3010 EPA 6020
92756913005 1048094 1048296MW-8 EPA 3010 EPA 6020
92756913005 1051146 1051157MW-8 EPA 3010 EPA 6020
92756913006 1048094 1048296MW-40 EPA 3010 EPA 6020
92756913006 1051146 1051157MW-40 EPA 3010 EPA 6020
92756913007 1048094 1048296MW-13BR EPA 3010 EPA 6020
92756913007 1051146 1051157MW-13BR EPA 3010 EPA 6020
92756913008 1048094 1048296MW-41 EPA 3010 EPA 6020
92756913009 1048094 1048296MW-43 EPA 3010 EPA 6020
92756913010 1048094 1048296MW-4B EPA 3010 EPA 6020
92756913010 1051146 1051157MW-4B EPA 3010 EPA 6020
92756913011 1048094 1048296MW-39 EPA 3010 EPA 6020
92756913011 1051146 1051157MW-39 EPA 3010 EPA 6020
92756913012 1048094 1048296MW-44 EPA 3010 EPA 6020
92756913001 888072LAGOONEPA 8260D
92756913002 888072MW-3A EPA 8260D
92756913003 888074MW-6A EPA 8260D
92756913004 888074MW-7 EPA 8260D
92756913005 888074MW-8 EPA 8260D
92756913006 888074MW-40 EPA 8260D
92756913007 888074MW-13BR EPA 8260D
92756913008 888074MW-41 EPA 8260D
92756913009 888074MW-43 EPA 8260D
92756913010 888074MW-4B EPA 8260D
92756913011 888074MW-39 EPA 8260D
92756913012 888074MW-44 EPA 8260D
92756913001 887323LAGOONEPA 8260D Mod.
92756913012 887074MW-44 EPA 8260D Mod.
92756913001 1048897LAGOONSM 4500-S2F
92756913001 1049466 1049889LAGOONEPA 365.4 EPA 365.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2024 04:37 PM
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Page 55 of 63
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92756913
Iredell Lined Ph 1,2,5,6
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92756913001 1047568 1048300LAGOONEPA 410.4 EPA 410.4
REPORT OF LABORATORY ANALYSIS
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Page 56 of 63
Page 57 of 63
Page 58 of 63
Page 59 of 63
Page 60 of 63
Page 61 of 63
Page 62 of 63
Page 63 of 63
#=CL#
November 05, 2024
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92757074
92757074
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services, Inc.
68 Shipwash Dr.
Garner, NC 27529
Iredell Lined Ph 1,2,5+6
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on October 04, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole D'Oleo
[e-mail]
Project Manager
[phone]
Enclosures
cc:Accounts Payable, Municipal Engineering Services, Inc.
Jonathan Pfohl, Municipal Engineering Services
Jay Zimmerman, PG, Municipal Engineering Services, Inc.
REPORT OF LABORATORY ANALYSIS
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Page 1 of 49
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
California Certification# 3096
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Utah
Utah FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
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#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Pace Analytical Services National
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Lab ID Sample ID Matrix Date Collected Date Received
92757074001 MW-13B Water 10/03/24 16:31 10/04/24 14:08
92757074002 MW-14B Water 10/03/24 16:18 10/04/24 14:08
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92757074001 MW-13B EPA 8151A 5 PANNWH
EPA 8081B 21 PASI-CSEM
EPA 8082A 8 PASI-CSEM
EPA 6010 1 PASI-OJMP2
EPA 6020 15 PASI-OADS, BSL
EPA 7470 1 PASI-OJNK
EPA 8270E 111 PASI-CPKS
EPA 8260D 65 PASI-CLMB
EPA 8260D Mod.3 PASI-CTEG
SM 4500-S2D-2011 1 PASI-AMDW
EPA 335.4 1 PASI-OJH2
92757074002 MW-14B EPA 8151A 5 PANNWH
EPA 8081B 21 PASI-CSEM
EPA 8082A 8 PASI-CSEM
EPA 6010 1 PASI-OJMP2
EPA 6020 15 PASI-OBSL
EPA 7470 1 PASI-OJNK
EPA 8270E 111 PASI-CPKS
EPA 8260D 65 PASI-CLMB
EPA 8260D Mod.3 PASI-CTEG
SM 4500-S2D-2011 1 PASI-AMDW
EPA 335.4 1 PASI-OJH2
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-13B Lab ID:92757074001 Collected:10/03/24 16:31 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151A Preparation Method: 8151A
Pace National - Mt. Juliet
Chlorinated Herb. (GC) 8151A
2,4,5-T ND ug/L 10/16/24 00:16 93-76-5 H310/11/24 09:282.00 0.258 1
2,4,5-TP (Silvex)ND ug/L 10/16/24 00:16 93-72-1 H310/11/24 09:282.00 0.335 1
2,4-D ND ug/L 10/16/24 00:16 94-75-7 H3,L010/11/24 09:282.00 0.547 1
Dinoseb ND ug/L 10/16/24 00:16 88-85-7 H310/11/24 09:282.00 0.250 1
Surrogates
2,4-DCAA (S)142 %10/16/24 00:16 19719-28-910/11/24 09:2814.0-158 1
Analytical Method: EPA 8081B Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8081 OC Pesticides RVE
Aldrin ND ug/L 10/07/24 07:09 309-00-210/06/24 06:240.042 0.012 1
alpha-BHC ND ug/L 10/07/24 07:09 319-84-610/06/24 06:240.042 0.010 1
beta-BHC ND ug/L 10/07/24 07:09 319-85-710/06/24 06:240.042 0.041 1
delta-BHC ND ug/L 10/07/24 07:09 319-86-810/06/24 06:240.042 0.012 1
gamma-BHC (Lindane)ND ug/L 10/07/24 07:09 58-89-910/06/24 06:240.042 0.010 1
Chlordane (Technical)ND ug/L 10/07/24 07:09 57-74-910/06/24 06:240.42 0.13 1
4,4'-DDD ND ug/L 10/07/24 07:09 72-54-810/06/24 06:240.042 0.014 1
4,4'-DDE ND ug/L 10/07/24 07:09 72-55-910/06/24 06:240.042 0.020 1
4,4'-DDT ND ug/L 10/07/24 07:09 50-29-310/06/24 06:240.042 0.022 1
Dieldrin ND ug/L 10/07/24 07:09 60-57-110/06/24 06:240.042 0.012 1
Endosulfan I ND ug/L 10/07/24 07:09 959-98-810/06/24 06:240.042 0.014 1
Endosulfan II ND ug/L 10/07/24 07:09 33213-65-910/06/24 06:240.042 0.013 1
Endosulfan sulfate ND ug/L 10/07/24 07:09 1031-07-810/06/24 06:240.042 0.012 1
Endrin ND ug/L 10/07/24 07:09 72-20-810/06/24 06:240.042 0.015 1
Endrin aldehyde ND ug/L 10/07/24 07:09 7421-93-410/06/24 06:240.042 0.014 1
Heptachlor ND ug/L 10/07/24 07:09 76-44-810/06/24 06:240.042 0.016 1
Heptachlor epoxide ND ug/L 10/07/24 07:09 1024-57-310/06/24 06:240.042 0.024 1
Methoxychlor ND ug/L 10/07/24 07:09 72-43-510/06/24 06:240.12 0.035 1
Toxaphene ND ug/L 10/07/24 07:09 8001-35-210/06/24 06:240.42 0.18 1
Surrogates
Tetrachloro-m-xylene (S)175 %10/07/24 07:09 877-09-810/06/24 06:2410-190 1
Decachlorobiphenyl (S)103 %10/07/24 07:09 2051-24-310/06/24 06:2410-200 1
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8082 GCS PCB RVE
PCB-1016 (Aroclor 1016)ND ug/L 10/07/24 12:51 12674-11-210/06/24 06:240.42 0.18 1
PCB-1221 (Aroclor 1221)ND ug/L 10/07/24 12:51 11104-28-210/06/24 06:240.42 0.19 1
PCB-1232 (Aroclor 1232)ND ug/L 10/07/24 12:51 11141-16-510/06/24 06:240.42 0.19 1
PCB-1242 (Aroclor 1242)ND ug/L 10/07/24 12:51 53469-21-910/06/24 06:240.42 0.21 1
PCB-1248 (Aroclor 1248)ND ug/L 10/07/24 12:51 12672-29-610/06/24 06:240.42 0.24 1
PCB-1254 (Aroclor 1254)ND ug/L 10/07/24 12:51 11097-69-110/06/24 06:240.42 0.18 1
PCB-1260 (Aroclor 1260)ND ug/L 10/07/24 12:51 11096-82-510/06/24 06:240.42 0.13 1
Surrogates
Decachlorobiphenyl (S)75 %10/07/24 12:51 2051-24-310/06/24 06:2410-200 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-13B Lab ID:92757074001 Collected:10/03/24 16:31 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Tin ND ug/L 10/24/24 11:17 7440-31-510/18/24 09:4650.0 16.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/25/24 21:24 7440-36-010/18/24 09:461.0 0.50 1
Arsenic ND ug/L 10/25/24 21:24 7440-38-210/18/24 09:461.0 0.50 1
Barium 1020 ug/L 10/26/24 17:50 7440-39-310/18/24 09:465.0 2.5 5
Beryllium 3.2 ug/L 10/25/24 21:24 7440-41-710/18/24 09:460.10 0.033 1
Cadmium 0.18 ug/L 10/25/24 21:24 7440-43-910/18/24 09:460.10 0.067 1
Chromium 0.58J ug/L 10/25/24 21:24 7440-47-310/18/24 09:461.0 0.50 1
Cobalt 3.0 ug/L 10/25/24 21:24 7440-48-410/18/24 09:461.0 0.24 1
Copper 0.75J ug/L 10/25/24 21:24 7440-50-810/18/24 09:461.0 0.42 1
Lead ND ug/L 10/25/24 21:24 7439-92-110/18/24 09:461.0 0.22 1
Nickel 2.9 ug/L 10/25/24 21:24 7440-02-010/18/24 09:461.0 0.26 1
Selenium ND ug/L 10/25/24 21:24 7782-49-210/18/24 09:462.0 0.20 1
Silver ND ug/L 10/25/24 21:24 7440-22-410/18/24 09:460.50 0.028 1
Thallium 0.17J ug/L 10/25/24 21:24 7440-28-010/18/24 09:461.0 0.11 1
Vanadium ND ug/L 10/25/24 21:24 7440-62-210/18/24 09:461.0 0.91 1
Zinc 7.9J ug/L 10/25/24 21:24 7440-66-610/18/24 09:4610.0 6.7 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/22/24 15:06 7439-97-610/22/24 09:170.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 10/07/24 14:10 83-32-910/06/24 04:0210.0 2.0 1
Acenaphthylene ND ug/L 10/07/24 14:10 208-96-810/06/24 04:0210.0 2.0 1
Acetophenone ND ug/L 10/07/24 14:10 98-86-210/06/24 04:0210.0 1.5 1
2-Acetylaminofluorene ND ug/L 10/07/24 14:10 53-96-3 v2,v310/06/24 04:0210.0 4.1 1
4-Aminobiphenyl ND ug/L 10/07/24 14:10 92-67-1 R110/06/24 04:0210.0 4.7 1
Anthracene ND ug/L 10/07/24 14:10 120-12-710/06/24 04:0210.0 2.3 1
Benzo(a)anthracene ND ug/L 10/07/24 14:10 56-55-310/06/24 04:0210.0 2.7 1
Benzo(a)pyrene ND ug/L 10/07/24 14:10 50-32-810/06/24 04:0210.0 2.8 1
Benzo(b)fluoranthene ND ug/L 10/07/24 14:10 205-99-210/06/24 04:0210.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 10/07/24 14:10 191-24-210/06/24 04:0210.0 2.8 1
Benzo(k)fluoranthene ND ug/L 10/07/24 14:10 207-08-910/06/24 04:0210.0 2.7 1
Benzyl alcohol ND ug/L 10/07/24 14:10 100-51-610/06/24 04:0220.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 10/07/24 14:10 101-55-310/06/24 04:0210.0 1.8 1
Butylbenzylphthalate ND ug/L 10/07/24 14:10 85-68-710/06/24 04:0210.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 10/07/24 14:10 59-50-710/06/24 04:0210.0 3.3 1
4-Chloroaniline ND ug/L 10/07/24 14:10 106-47-810/06/24 04:0220.0 3.6 1
Chlorobenzilate ND ug/L 10/07/24 14:10 510-15-610/06/24 04:0210.0 3.8 1
bis(2-Chloroethoxy)methane ND ug/L 10/07/24 14:10 111-91-110/06/24 04:0210.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 10/07/24 14:10 111-44-410/06/24 04:0210.0 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-13B Lab ID:92757074001 Collected:10/03/24 16:31 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2-Chloronaphthalene ND ug/L 10/07/24 14:10 91-58-710/06/24 04:0210.0 1.7 1
2-Chlorophenol ND ug/L 10/07/24 14:10 95-57-810/06/24 04:0210.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 10/07/24 14:10 7005-72-310/06/24 04:0210.0 2.0 1
Chrysene ND ug/L 10/07/24 14:10 218-01-910/06/24 04:0210.0 2.8 1
Diallate ND ug/L 10/07/24 14:10 2303-16-4 v2,v310/06/24 04:0210.0 3.4 1
Dibenz(a,h)anthracene ND ug/L 10/07/24 14:10 53-70-310/06/24 04:0210.0 3.0 1
Dibenzofuran ND ug/L 10/07/24 14:10 132-64-910/06/24 04:0210.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 10/07/24 14:10 91-94-1 R110/06/24 04:0220.0 8.1 1
2,4-Dichlorophenol ND ug/L 10/07/24 14:10 120-83-210/06/24 04:0210.0 1.4 1
2,6-Dichlorophenol ND ug/L 10/07/24 14:10 87-65-010/06/24 04:0210.0 4.2 1
Diethylphthalate ND ug/L 10/07/24 14:10 84-66-210/06/24 04:0210.0 2.0 1
Dimethoate ND ug/L 10/07/24 14:10 60-51-510/06/24 04:0210.0 3.7 1
P-Dimethylaminoazobenzene ND ug/L 10/07/24 14:10 60-11-7 R110/06/24 04:025.0 2.4 1
7,12-Dimethylbenz(a)anthracene ND ug/L 10/07/24 14:10 57-97-610/06/24 04:0210.0 3.0 1
3,3'-Dimethylbenzidine ND ug/L 10/07/24 14:10 119-93-7 M110/06/24 04:0250.0 31.1 1
2,4-Dimethylphenol ND ug/L 10/07/24 14:10 105-67-910/06/24 04:0210.0 1.7 1
Dimethylphthalate ND ug/L 10/07/24 14:10 131-11-310/06/24 04:0210.0 2.1 1
Di-n-butylphthalate ND ug/L 10/07/24 14:10 84-74-210/06/24 04:0210.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 10/07/24 14:10 534-52-110/06/24 04:0220.0 7.8 1
1,3-Dinitrobenzene ND ug/L 10/07/24 14:10 99-65-010/06/24 04:0210.0 3.8 1
2,4-Dinitrophenol ND ug/L 10/07/24 14:10 51-28-5 R110/06/24 04:0250.0 26.0 1
2,4-Dinitrotoluene ND ug/L 10/07/24 14:10 121-14-2 v110/06/24 04:0210.0 1.6 1
2,6-Dinitrotoluene ND ug/L 10/07/24 14:10 606-20-210/06/24 04:0210.0 1.7 1
Di-n-octylphthalate ND ug/L 10/07/24 14:10 117-84-010/06/24 04:0210.0 3.9 1
Diphenylamine ND ug/L 10/07/24 14:10 122-39-410/06/24 04:0210.0 3.0 1
Disulfoton ND ug/L 10/07/24 14:10 298-04-410/06/24 04:0210.0 4.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/07/24 14:10 117-81-710/06/24 04:026.0 3.7 1
Ethyl methanesulfonate ND ug/L 10/07/24 14:10 62-50-010/06/24 04:0220.0 3.0 1
Famphur ND ug/L 10/07/24 14:10 52-85-710/06/24 04:0210.0 6.1 1
Fluoranthene ND ug/L 10/07/24 14:10 206-44-010/06/24 04:0210.0 2.2 1
Fluorene ND ug/L 10/07/24 14:10 86-73-710/06/24 04:0210.0 2.1 1
Hexachlorobenzene ND ug/L 10/07/24 14:10 118-74-110/06/24 04:0210.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 10/07/24 14:10 77-47-410/06/24 04:0210.0 1.6 1
Hexachloroethane ND ug/L 10/07/24 14:10 67-72-110/06/24 04:0210.0 1.4 1
Hexachloropropene ND ug/L 10/07/24 14:10 1888-71-710/06/24 04:0210.0 2.7 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/07/24 14:10 193-39-510/06/24 04:0210.0 2.9 1
Isodrin ND ug/L 10/07/24 14:10 465-73-610/06/24 04:0210.0 2.8 1
Isophorone ND ug/L 10/07/24 14:10 78-59-110/06/24 04:0210.0 1.7 1
Isosafrole ND ug/L 10/07/24 14:10 120-58-110/06/24 04:0210.0 2.5 1
Kepone ND ug/L 10/07/24 14:10 143-50-010/06/24 04:0220.0 14.1 1
Methapyrilene ND ug/L 10/07/24 14:10 91-80-5 L2,M010/06/24 04:0250.0 17.0 1
3-Methylcholanthrene ND ug/L 10/07/24 14:10 56-49-510/06/24 04:0210.0 3.7 1
Methyl methanesulfonate ND ug/L 10/07/24 14:10 66-27-310/06/24 04:025.0 3.1 1
2-Methylnaphthalene ND ug/L 10/07/24 14:10 91-57-610/06/24 04:0210.0 1.9 1
Methyl parathion ND ug/L 10/07/24 14:10 298-00-010/06/24 04:0210.0 3.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-13B Lab ID:92757074001 Collected:10/03/24 16:31 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2-Methylphenol(o-Cresol)ND ug/L 10/07/24 14:10 95-48-710/06/24 04:0210.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/07/24 14:10 15831-10-410/06/24 04:0210.0 1.2 1
1-Naphthalenamine ND ug/L 10/07/24 14:10 134-32-7 L2,M010/06/24 04:0210.0 6.0 1
2-Naphthalenamine ND ug/L 10/07/24 14:10 91-59-8 M110/06/24 04:0210.0 5.4 1
1,4-Naphthoquinone ND ug/L 10/07/24 14:10 130-15-410/06/24 04:025.0 4.4 1
2-Nitroaniline ND ug/L 10/07/24 14:10 88-74-410/06/24 04:0220.0 3.0 1
3-Nitroaniline ND ug/L 10/07/24 14:10 99-09-210/06/24 04:0220.0 3.8 1
4-Nitroaniline ND ug/L 10/07/24 14:10 100-01-610/06/24 04:0220.0 5.1 1
Nitrobenzene ND ug/L 10/07/24 14:10 98-95-310/06/24 04:0210.0 1.9 1
2-Nitrophenol ND ug/L 10/07/24 14:10 88-75-510/06/24 04:0210.0 1.4 1
4-Nitrophenol ND ug/L 10/07/24 14:10 100-02-710/06/24 04:0250.0 6.6 1
5-Nitro-o-toluidine ND ug/L 10/07/24 14:10 99-55-810/06/24 04:0210.0 3.8 1
N-Nitrosodiethylamine ND ug/L 10/07/24 14:10 55-18-510/06/24 04:0210.0 2.3 1
N-Nitrosodimethylamine ND ug/L 10/07/24 14:10 62-75-910/06/24 04:0210.0 1.9 1
N-Nitroso-di-n-butylamine ND ug/L 10/07/24 14:10 924-16-310/06/24 04:0210.0 2.0 1
N-Nitroso-di-n-propylamine ND ug/L 10/07/24 14:10 621-64-710/06/24 04:0210.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 10/07/24 14:10 86-30-610/06/24 04:0210.0 3.0 1
N-Nitrosomethylethylamine ND ug/L 10/07/24 14:10 10595-95-610/06/24 04:0210.0 7.5 1
N-Nitrosopiperidine ND ug/L 10/07/24 14:10 100-75-410/06/24 04:0210.0 2.5 1
N-Nitrosopyrrolidine ND ug/L 10/07/24 14:10 930-55-2 v2,v310/06/24 04:0210.0 3.1 1
O,O,O-Triethylphosphorothioate ND ug/L 10/07/24 14:10 126-68-110/06/24 04:0210.0 2.6 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/07/24 14:10 108-60-110/06/24 04:0210.0 1.2 1
Parathion (Ethyl parathion)ND ug/L 10/07/24 14:10 56-38-210/06/24 04:0210.0 3.9 1
Pentachlorobenzene ND ug/L 10/07/24 14:10 608-93-510/06/24 04:0210.0 3.4 1
Pentachloronitrobenzene ND ug/L 10/07/24 14:10 82-68-810/06/24 04:0210.0 3.3 1
Pentachlorophenol ND ug/L 10/07/24 14:10 87-86-510/06/24 04:0220.0 3.8 1
Phenacetin ND ug/L 10/07/24 14:10 62-44-210/06/24 04:0210.0 3.6 1
Phenanthrene ND ug/L 10/07/24 14:10 85-01-810/06/24 04:0210.0 2.0 1
Phenol ND ug/L 10/07/24 14:10 108-95-210/06/24 04:0210.0 1.4 1
p-Phenylenediamine ND ug/L 10/07/24 14:10 106-50-310/06/24 04:0210.0 10.0 1
Phorate ND ug/L 10/07/24 14:10 298-02-2 R110/06/24 04:0210.0 3.6 1
Pronamide ND ug/L 10/07/24 14:10 23950-58-510/06/24 04:0210.0 3.1 1
Pyrene ND ug/L 10/07/24 14:10 129-00-010/06/24 04:0210.0 2.2 1
Safrole ND ug/L 10/07/24 14:10 94-59-710/06/24 04:0210.0 2.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 10/07/24 14:10 95-94-310/06/24 04:0210.0 4.5 1
2,3,4,6-Tetrachlorophenol ND ug/L 10/07/24 14:10 58-90-210/06/24 04:0210.0 1.5 1
Thionazin ND ug/L 10/07/24 14:10 297-97-210/06/24 04:0210.0 2.9 1
O-Toluidine ND ug/L 10/07/24 14:10 95-53-410/06/24 04:0210.0 2.6 1
2,4,5-Trichlorophenol ND ug/L 10/07/24 14:10 95-95-410/06/24 04:0210.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 10/07/24 14:10 88-06-210/06/24 04:0210.0 1.6 1
1,3,5-Trinitrobenzene ND ug/L 10/07/24 14:10 99-35-410/06/24 04:0210.0 5.5 1
Surrogates
Nitrobenzene-d5 (S)28 %10/07/24 14:10 4165-60-010/06/24 04:0210-133 1
2-Fluorobiphenyl (S)29 %10/07/24 14:10 321-60-810/06/24 04:0210-130 1
Terphenyl-d14 (S)49 %10/07/24 14:10 1718-51-010/06/24 04:0210-193 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-13B Lab ID:92757074001 Collected:10/03/24 16:31 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Surrogates
Phenol-d6 (S)14 %10/07/24 14:10 13127-88-310/06/24 04:0210-130 1
2-Fluorophenol (S)21 %10/07/24 14:10 367-12-410/06/24 04:0210-130 1
2,4,6-Tribromophenol (S)42 %10/07/24 14:10 118-79-610/06/24 04:0210-166 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 10:21 67-64-125.0 5.1 1
Acetonitrile ND ug/L 10/12/24 10:21 75-05-850.0 24.8 1
Acrolein ND ug/L 10/12/24 10:21 107-02-8 AC10.0 8.5 1
Acrylonitrile ND ug/L 10/12/24 10:21 107-13-110.0 1.8 1
Allyl chloride ND ug/L 10/12/24 10:21 107-05-12.0 0.50 1
Benzene 1.6 ug/L 10/12/24 10:21 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 10:21 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 10:21 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 10:21 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 10:21 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 10:21 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 10:21 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 10:21 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 10:21 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 10:21 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 10:21 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 10:21 74-87-31.0 0.54 1
Chloroprene ND ug/L 10/12/24 10:21 126-99-85.0 1.6 1
Dibromochloromethane ND ug/L 10/12/24 10:21 124-48-11.0 0.36 1
Dibromomethane ND ug/L 10/12/24 10:21 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 10:21 95-50-11.0 0.34 1
1,4-Dichlorobenzene 0.67J ug/L 10/12/24 10:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 10:21 110-57-6 v21.0 0.56 1
Dichlorodifluoromethane ND ug/L 10/12/24 10:21 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/12/24 10:21 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 10:21 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 10:21 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 1.9 ug/L 10/12/24 10:21 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 10:21 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 10:21 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/12/24 10:21 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/12/24 10:21 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 10/12/24 10:21 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/12/24 10:21 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 10:21 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 10/12/24 10:21 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 10/12/24 10:21 97-63-21.0 0.28 1
Hexachloro-1,3-butadiene ND ug/L 10/12/24 10:21 87-68-32.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-13B Lab ID:92757074001 Collected:10/03/24 16:31 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
2-Hexanone ND ug/L 10/12/24 10:21 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 10:21 74-88-4 v220.0 9.7 1
Isobutanol ND ug/L 10/12/24 10:21 78-83-1 v210052.3 1
Methacrylonitrile ND ug/L 10/12/24 10:21 126-98-710.0 4.2 1
Methylene Chloride ND ug/L 10/12/24 10:21 75-09-25.0 2.0 1
Methyl methacrylate ND ug/L 10/12/24 10:21 80-62-62.0 0.32 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 10:21 108-10-15.0 2.7 1
Naphthalene ND ug/L 10/12/24 10:21 91-20-31.0 0.64 1
Propionitrile ND ug/L 10/12/24 10:21 107-12-020.0 3.6 1
Styrene ND ug/L 10/12/24 10:21 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 10:21 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 10:21 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 10:21 127-18-41.0 0.29 1
Toluene 0.41J ug/L 10/12/24 10:21 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/12/24 10:21 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/12/24 10:21 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/12/24 10:21 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 10:21 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 10:21 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 10:21 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 10:21 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 10:21 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 10:21 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 10:21 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %10/12/24 10:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %10/12/24 10:21 17060-07-070-130 1
Toluene-d8 (S)111 %10/12/24 10:21 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
1,4-Dioxane (p-Dioxane)4.6 ug/L 10/07/24 19:24 123-91-12.0 0.86 1
Surrogates
1,2-Dichloroethane-d4 (S)90 %10/07/24 19:24 17060-07-070-130 1
Toluene-d8 (S)95 %10/07/24 19:24 2037-26-570-130 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND ug/L 10/09/24 17:02 18496-25-8 D35001105
Analytical Method: EPA 335.4 Preparation Method: EPA 335.4
Pace Analytical Services - Ormond Beach
335.4 Cyanide, Total
Cyanide ND mg/L 10/17/24 13:54 57-12-510/17/24 09:430.010 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-14B Lab ID:92757074002 Collected:10/03/24 16:18 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151A Preparation Method: 8151A
Pace National - Mt. Juliet
Chlorinated Herb. (GC) 8151A
2,4,5-T ND ug/L 10/16/24 00:26 93-76-5 H310/11/24 09:282.00 0.258 1
2,4,5-TP (Silvex)ND ug/L 10/16/24 00:26 93-72-1 H310/11/24 09:282.00 0.335 1
2,4-D ND ug/L 10/16/24 00:26 94-75-7 H3,L010/11/24 09:282.00 0.547 1
Dinoseb ND ug/L 10/16/24 00:26 88-85-7 H310/11/24 09:282.00 0.250 1
Surrogates
2,4-DCAA (S)103 %10/16/24 00:26 19719-28-910/11/24 09:2814.0-158 1
Analytical Method: EPA 8081B Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8081 OC Pesticides RVE
Aldrin ND ug/L 10/07/24 07:22 309-00-210/06/24 06:240.045 0.013 1
alpha-BHC ND ug/L 10/07/24 07:22 319-84-610/06/24 06:240.045 0.011 1
beta-BHC ND ug/L 10/07/24 07:22 319-85-710/06/24 06:240.045 0.044 1
delta-BHC ND ug/L 10/07/24 07:22 319-86-810/06/24 06:240.045 0.013 1
gamma-BHC (Lindane)ND ug/L 10/07/24 07:22 58-89-910/06/24 06:240.045 0.011 1
Chlordane (Technical)ND ug/L 10/07/24 07:22 57-74-910/06/24 06:240.45 0.14 1
4,4'-DDD ND ug/L 10/07/24 07:22 72-54-810/06/24 06:240.045 0.015 1
4,4'-DDE ND ug/L 10/07/24 07:22 72-55-910/06/24 06:240.045 0.022 1
4,4'-DDT ND ug/L 10/07/24 07:22 50-29-310/06/24 06:240.045 0.023 1
Dieldrin ND ug/L 10/07/24 07:22 60-57-110/06/24 06:240.045 0.014 1
Endosulfan I ND ug/L 10/07/24 07:22 959-98-810/06/24 06:240.045 0.016 1
Endosulfan II ND ug/L 10/07/24 07:22 33213-65-910/06/24 06:240.045 0.014 1
Endosulfan sulfate ND ug/L 10/07/24 07:22 1031-07-810/06/24 06:240.045 0.013 1
Endrin ND ug/L 10/07/24 07:22 72-20-810/06/24 06:240.045 0.016 1
Endrin aldehyde ND ug/L 10/07/24 07:22 7421-93-410/06/24 06:240.045 0.015 1
Heptachlor ND ug/L 10/07/24 07:22 76-44-810/06/24 06:240.045 0.018 1
Heptachlor epoxide ND ug/L 10/07/24 07:22 1024-57-310/06/24 06:240.045 0.026 1
Methoxychlor ND ug/L 10/07/24 07:22 72-43-510/06/24 06:240.14 0.038 1
Toxaphene ND ug/L 10/07/24 07:22 8001-35-210/06/24 06:240.45 0.20 1
Surrogates
Tetrachloro-m-xylene (S)81 %10/07/24 07:22 877-09-810/06/24 06:2410-190 1
Decachlorobiphenyl (S)108 %10/07/24 07:22 2051-24-310/06/24 06:2410-200 1
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8082 GCS PCB RVE
PCB-1016 (Aroclor 1016)ND ug/L 10/07/24 13:04 12674-11-210/06/24 06:240.45 0.19 1
PCB-1221 (Aroclor 1221)ND ug/L 10/07/24 13:04 11104-28-210/06/24 06:240.45 0.21 1
PCB-1232 (Aroclor 1232)ND ug/L 10/07/24 13:04 11141-16-510/06/24 06:240.45 0.21 1
PCB-1242 (Aroclor 1242)ND ug/L 10/07/24 13:04 53469-21-910/06/24 06:240.45 0.23 1
PCB-1248 (Aroclor 1248)ND ug/L 10/07/24 13:04 12672-29-610/06/24 06:240.45 0.26 1
PCB-1254 (Aroclor 1254)ND ug/L 10/07/24 13:04 11097-69-110/06/24 06:240.45 0.19 1
PCB-1260 (Aroclor 1260)ND ug/L 10/07/24 13:04 11096-82-510/06/24 06:240.45 0.14 1
Surrogates
Decachlorobiphenyl (S)93 %10/07/24 13:04 2051-24-310/06/24 06:2410-200 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-14B Lab ID:92757074002 Collected:10/03/24 16:18 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6010 MET ICP
Tin ND ug/L 10/24/24 11:22 7440-31-510/18/24 09:4650.0 16.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/25/24 21:32 7440-36-010/18/24 09:461.0 0.50 1
Arsenic ND ug/L 10/25/24 21:32 7440-38-210/18/24 09:461.0 0.50 1
Barium 105 ug/L 10/25/24 21:32 7440-39-310/18/24 09:461.0 0.50 1
Beryllium 0.036J ug/L 10/25/24 21:32 7440-41-710/18/24 09:460.10 0.033 1
Cadmium 0.26 ug/L 10/25/24 21:32 7440-43-910/18/24 09:460.10 0.067 1
Chromium ND ug/L 10/25/24 21:32 7440-47-310/18/24 09:461.0 0.50 1
Cobalt 0.65J ug/L 10/25/24 21:32 7440-48-410/18/24 09:461.0 0.24 1
Copper ND ug/L 10/25/24 21:32 7440-50-810/18/24 09:461.0 0.42 1
Lead ND ug/L 10/25/24 21:32 7439-92-110/18/24 09:461.0 0.22 1
Nickel 5.5 ug/L 10/25/24 21:32 7440-02-010/18/24 09:461.0 0.26 1
Selenium ND ug/L 10/25/24 21:32 7782-49-210/18/24 09:462.0 0.20 1
Silver ND ug/L 10/25/24 21:32 7440-22-410/18/24 09:460.50 0.028 1
Thallium ND ug/L 10/25/24 21:32 7440-28-010/18/24 09:461.0 0.11 1
Vanadium 3.1 ug/L 10/25/24 21:32 7440-62-210/18/24 09:461.0 0.91 1
Zinc ND ug/L 10/25/24 21:32 7440-66-610/18/24 09:4610.0 6.7 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury ND ug/L 10/22/24 15:08 7439-97-610/22/24 09:170.20 0.14 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Acenaphthene ND ug/L 10/07/24 14:36 83-32-910/06/24 04:028.3 1.7 1
Acenaphthylene ND ug/L 10/07/24 14:36 208-96-810/06/24 04:028.3 1.6 1
Acetophenone ND ug/L 10/07/24 14:36 98-86-210/06/24 04:028.3 1.2 1
2-Acetylaminofluorene ND ug/L 10/07/24 14:36 53-96-3 v210/06/24 04:028.3 3.4 1
4-Aminobiphenyl ND ug/L 10/07/24 14:36 92-67-110/06/24 04:028.3 4.0 1
Anthracene ND ug/L 10/07/24 14:36 120-12-710/06/24 04:028.3 1.9 1
Benzo(a)anthracene ND ug/L 10/07/24 14:36 56-55-310/06/24 04:028.3 2.2 1
Benzo(a)pyrene ND ug/L 10/07/24 14:36 50-32-810/06/24 04:028.3 2.3 1
Benzo(b)fluoranthene ND ug/L 10/07/24 14:36 205-99-210/06/24 04:028.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 10/07/24 14:36 191-24-210/06/24 04:028.3 2.4 1
Benzo(k)fluoranthene ND ug/L 10/07/24 14:36 207-08-910/06/24 04:028.3 2.3 1
Benzyl alcohol ND ug/L 10/07/24 14:36 100-51-610/06/24 04:0216.7 2.4 1
4-Bromophenylphenyl ether ND ug/L 10/07/24 14:36 101-55-310/06/24 04:028.3 1.5 1
Butylbenzylphthalate ND ug/L 10/07/24 14:36 85-68-710/06/24 04:028.3 2.6 1
4-Chloro-3-methylphenol ND ug/L 10/07/24 14:36 59-50-710/06/24 04:028.3 2.8 1
4-Chloroaniline ND ug/L 10/07/24 14:36 106-47-810/06/24 04:0216.7 3.0 1
Chlorobenzilate ND ug/L 10/07/24 14:36 510-15-610/06/24 04:028.3 3.2 1
bis(2-Chloroethoxy)methane ND ug/L 10/07/24 14:36 111-91-110/06/24 04:028.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 10/07/24 14:36 111-44-410/06/24 04:028.3 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-14B Lab ID:92757074002 Collected:10/03/24 16:18 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2-Chloronaphthalene ND ug/L 10/07/24 14:36 91-58-710/06/24 04:028.3 1.4 1
2-Chlorophenol ND ug/L 10/07/24 14:36 95-57-810/06/24 04:028.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 10/07/24 14:36 7005-72-310/06/24 04:028.3 1.7 1
Chrysene ND ug/L 10/07/24 14:36 218-01-910/06/24 04:028.3 2.3 1
Diallate ND ug/L 10/07/24 14:36 2303-16-4 v210/06/24 04:028.3 2.8 1
Dibenz(a,h)anthracene ND ug/L 10/07/24 14:36 53-70-310/06/24 04:028.3 2.5 1
Dibenzofuran ND ug/L 10/07/24 14:36 132-64-910/06/24 04:028.3 1.8 1
3,3'-Dichlorobenzidine ND ug/L 10/07/24 14:36 91-94-110/06/24 04:0216.7 6.8 1
2,4-Dichlorophenol ND ug/L 10/07/24 14:36 120-83-210/06/24 04:028.3 1.2 1
2,6-Dichlorophenol ND ug/L 10/07/24 14:36 87-65-010/06/24 04:028.3 3.5 1
Diethylphthalate ND ug/L 10/07/24 14:36 84-66-210/06/24 04:028.3 1.7 1
Dimethoate ND ug/L 10/07/24 14:36 60-51-510/06/24 04:028.3 3.0 1
P-Dimethylaminoazobenzene ND ug/L 10/07/24 14:36 60-11-710/06/24 04:024.2 2.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 10/07/24 14:36 57-97-610/06/24 04:028.3 2.5 1
3,3'-Dimethylbenzidine ND ug/L 10/07/24 14:36 119-93-710/06/24 04:0241.7 25.9 1
2,4-Dimethylphenol ND ug/L 10/07/24 14:36 105-67-910/06/24 04:028.3 1.4 1
Dimethylphthalate ND ug/L 10/07/24 14:36 131-11-310/06/24 04:028.3 1.8 1
Di-n-butylphthalate ND ug/L 10/07/24 14:36 84-74-210/06/24 04:028.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 10/07/24 14:36 534-52-110/06/24 04:0216.7 6.5 1
1,3-Dinitrobenzene ND ug/L 10/07/24 14:36 99-65-010/06/24 04:028.3 3.1 1
2,4-Dinitrophenol ND ug/L 10/07/24 14:36 51-28-510/06/24 04:0241.7 21.7 1
2,4-Dinitrotoluene ND ug/L 10/07/24 14:36 121-14-2 v110/06/24 04:028.3 1.4 1
2,6-Dinitrotoluene ND ug/L 10/07/24 14:36 606-20-210/06/24 04:028.3 1.4 1
Di-n-octylphthalate ND ug/L 10/07/24 14:36 117-84-010/06/24 04:028.3 3.3 1
Diphenylamine ND ug/L 10/07/24 14:36 122-39-410/06/24 04:028.3 2.5 1
Disulfoton ND ug/L 10/07/24 14:36 298-04-410/06/24 04:028.3 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/07/24 14:36 117-81-710/06/24 04:025.0 3.1 1
Ethyl methanesulfonate ND ug/L 10/07/24 14:36 62-50-010/06/24 04:0216.7 2.5 1
Famphur ND ug/L 10/07/24 14:36 52-85-710/06/24 04:028.3 5.1 1
Fluoranthene ND ug/L 10/07/24 14:36 206-44-010/06/24 04:028.3 1.8 1
Fluorene ND ug/L 10/07/24 14:36 86-73-710/06/24 04:028.3 1.7 1
Hexachlorobenzene ND ug/L 10/07/24 14:36 118-74-110/06/24 04:028.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 10/07/24 14:36 77-47-410/06/24 04:028.3 1.3 1
Hexachloroethane ND ug/L 10/07/24 14:36 67-72-110/06/24 04:028.3 1.2 1
Hexachloropropene ND ug/L 10/07/24 14:36 1888-71-710/06/24 04:028.3 2.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/07/24 14:36 193-39-510/06/24 04:028.3 2.4 1
Isodrin ND ug/L 10/07/24 14:36 465-73-610/06/24 04:028.3 2.3 1
Isophorone ND ug/L 10/07/24 14:36 78-59-110/06/24 04:028.3 1.4 1
Isosafrole ND ug/L 10/07/24 14:36 120-58-110/06/24 04:028.3 2.1 1
Kepone ND ug/L 10/07/24 14:36 143-50-010/06/24 04:0216.7 11.8 1
Methapyrilene ND ug/L 10/07/24 14:36 91-80-5 L210/06/24 04:0241.7 14.2 1
3-Methylcholanthrene ND ug/L 10/07/24 14:36 56-49-510/06/24 04:028.3 3.1 1
Methyl methanesulfonate ND ug/L 10/07/24 14:36 66-27-310/06/24 04:024.2 2.6 1
2-Methylnaphthalene ND ug/L 10/07/24 14:36 91-57-610/06/24 04:028.3 1.6 1
Methyl parathion ND ug/L 10/07/24 14:36 298-00-010/06/24 04:028.3 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-14B Lab ID:92757074002 Collected:10/03/24 16:18 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
2-Methylphenol(o-Cresol)ND ug/L 10/07/24 14:36 95-48-710/06/24 04:028.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/07/24 14:36 15831-10-410/06/24 04:028.3 1.0 1
1-Naphthalenamine ND ug/L 10/07/24 14:36 134-32-7 L210/06/24 04:028.3 5.0 1
2-Naphthalenamine ND ug/L 10/07/24 14:36 91-59-810/06/24 04:028.3 4.5 1
1,4-Naphthoquinone ND ug/L 10/07/24 14:36 130-15-410/06/24 04:024.2 3.7 1
2-Nitroaniline ND ug/L 10/07/24 14:36 88-74-410/06/24 04:0216.7 2.5 1
3-Nitroaniline ND ug/L 10/07/24 14:36 99-09-210/06/24 04:0216.7 3.1 1
4-Nitroaniline ND ug/L 10/07/24 14:36 100-01-610/06/24 04:0216.7 4.2 1
Nitrobenzene ND ug/L 10/07/24 14:36 98-95-310/06/24 04:028.3 1.6 1
2-Nitrophenol ND ug/L 10/07/24 14:36 88-75-510/06/24 04:028.3 1.2 1
4-Nitrophenol ND ug/L 10/07/24 14:36 100-02-710/06/24 04:0241.7 5.5 1
5-Nitro-o-toluidine ND ug/L 10/07/24 14:36 99-55-810/06/24 04:028.3 3.2 1
N-Nitrosodiethylamine ND ug/L 10/07/24 14:36 55-18-510/06/24 04:028.3 1.9 1
N-Nitrosodimethylamine ND ug/L 10/07/24 14:36 62-75-910/06/24 04:028.3 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 10/07/24 14:36 924-16-310/06/24 04:028.3 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 10/07/24 14:36 621-64-710/06/24 04:028.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 10/07/24 14:36 86-30-610/06/24 04:028.3 2.5 1
N-Nitrosomethylethylamine ND ug/L 10/07/24 14:36 10595-95-610/06/24 04:028.3 6.2 1
N-Nitrosopiperidine ND ug/L 10/07/24 14:36 100-75-410/06/24 04:028.3 2.1 1
N-Nitrosopyrrolidine ND ug/L 10/07/24 14:36 930-55-2 v210/06/24 04:028.3 2.6 1
O,O,O-Triethylphosphorothioate ND ug/L 10/07/24 14:36 126-68-110/06/24 04:028.3 2.1 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/07/24 14:36 108-60-110/06/24 04:028.3 0.96 1
Parathion (Ethyl parathion)ND ug/L 10/07/24 14:36 56-38-210/06/24 04:028.3 3.2 1
Pentachlorobenzene ND ug/L 10/07/24 14:36 608-93-510/06/24 04:028.3 2.8 1
Pentachloronitrobenzene ND ug/L 10/07/24 14:36 82-68-810/06/24 04:028.3 2.7 1
Pentachlorophenol ND ug/L 10/07/24 14:36 87-86-510/06/24 04:0216.7 3.1 1
Phenacetin ND ug/L 10/07/24 14:36 62-44-210/06/24 04:028.3 3.0 1
Phenanthrene ND ug/L 10/07/24 14:36 85-01-810/06/24 04:028.3 1.7 1
Phenol ND ug/L 10/07/24 14:36 108-95-210/06/24 04:028.3 1.1 1
p-Phenylenediamine ND ug/L 10/07/24 14:36 106-50-310/06/24 04:028.3 8.3 1
Phorate ND ug/L 10/07/24 14:36 298-02-210/06/24 04:028.3 3.0 1
Pronamide ND ug/L 10/07/24 14:36 23950-58-510/06/24 04:028.3 2.6 1
Pyrene ND ug/L 10/07/24 14:36 129-00-010/06/24 04:028.3 1.8 1
Safrole ND ug/L 10/07/24 14:36 94-59-710/06/24 04:028.3 1.9 1
1,2,4,5-Tetrachlorobenzene ND ug/L 10/07/24 14:36 95-94-310/06/24 04:028.3 3.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 10/07/24 14:36 58-90-210/06/24 04:028.3 1.3 1
Thionazin ND ug/L 10/07/24 14:36 297-97-210/06/24 04:028.3 2.4 1
O-Toluidine ND ug/L 10/07/24 14:36 95-53-410/06/24 04:028.3 2.2 1
2,4,5-Trichlorophenol ND ug/L 10/07/24 14:36 95-95-410/06/24 04:028.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 10/07/24 14:36 88-06-210/06/24 04:028.3 1.3 1
1,3,5-Trinitrobenzene ND ug/L 10/07/24 14:36 99-35-410/06/24 04:028.3 4.6 1
Surrogates
Nitrobenzene-d5 (S)40 %10/07/24 14:36 4165-60-010/06/24 04:0210-133 1
2-Fluorobiphenyl (S)42 %10/07/24 14:36 321-60-810/06/24 04:0210-130 1
Terphenyl-d14 (S)57 %10/07/24 14:36 1718-51-010/06/24 04:0210-193 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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Page 15 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-14B Lab ID:92757074002 Collected:10/03/24 16:18 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E APP9 RV
Surrogates
Phenol-d6 (S)17 %10/07/24 14:36 13127-88-310/06/24 04:0210-130 1
2-Fluorophenol (S)27 %10/07/24 14:36 367-12-410/06/24 04:0210-130 1
2,4,6-Tribromophenol (S)54 %10/07/24 14:36 118-79-610/06/24 04:0210-166 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 08:31 67-64-125.0 5.1 1
Acetonitrile ND ug/L 10/12/24 08:31 75-05-850.0 24.8 1
Acrolein ND ug/L 10/12/24 08:31 107-02-8 AC10.0 8.5 1
Acrylonitrile ND ug/L 10/12/24 08:31 107-13-110.0 1.8 1
Allyl chloride ND ug/L 10/12/24 08:31 107-05-12.0 0.50 1
Benzene ND ug/L 10/12/24 08:31 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 08:31 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 08:31 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 08:31 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 08:31 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 08:31 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 08:31 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 08:31 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 08:31 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 08:31 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 08:31 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 08:31 74-87-31.0 0.54 1
Chloroprene ND ug/L 10/12/24 08:31 126-99-85.0 1.6 1
Dibromochloromethane ND ug/L 10/12/24 08:31 124-48-11.0 0.36 1
Dibromomethane ND ug/L 10/12/24 08:31 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 08:31 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/12/24 08:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 08:31 110-57-6 v21.0 0.56 1
Dichlorodifluoromethane ND ug/L 10/12/24 08:31 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 10/12/24 08:31 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 08:31 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 08:31 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 1.2 ug/L 10/12/24 08:31 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 08:31 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 08:31 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 10/12/24 08:31 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 10/12/24 08:31 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 10/12/24 08:31 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/12/24 08:31 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/12/24 08:31 10061-02-61.0 0.36 1
Ethylbenzene ND ug/L 10/12/24 08:31 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 10/12/24 08:31 97-63-21.0 0.28 1
Hexachloro-1,3-butadiene ND ug/L 10/12/24 08:31 87-68-32.0 1.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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Page 16 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Sample:MW-14B Lab ID:92757074002 Collected:10/03/24 16:18 Received:10/04/24 14:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
2-Hexanone ND ug/L 10/12/24 08:31 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 08:31 74-88-4 v220.0 9.7 1
Isobutanol ND ug/L 10/12/24 08:31 78-83-1 v210052.3 1
Methacrylonitrile ND ug/L 10/12/24 08:31 126-98-710.0 4.2 1
Methylene Chloride ND ug/L 10/12/24 08:31 75-09-25.0 2.0 1
Methyl methacrylate ND ug/L 10/12/24 08:31 80-62-62.0 0.32 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 08:31 108-10-15.0 2.7 1
Naphthalene ND ug/L 10/12/24 08:31 91-20-31.0 0.64 1
Propionitrile ND ug/L 10/12/24 08:31 107-12-020.0 3.6 1
Styrene ND ug/L 10/12/24 08:31 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 08:31 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 08:31 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 08:31 127-18-41.0 0.29 1
Toluene ND ug/L 10/12/24 08:31 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/12/24 08:31 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/12/24 08:31 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/12/24 08:31 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 08:31 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 08:31 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 08:31 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 08:31 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 08:31 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 08:31 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 08:31 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)101 %10/12/24 08:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)85 %10/12/24 08:31 17060-07-070-130 1
Toluene-d8 (S)112 %10/12/24 08:31 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
1,4-Dioxane (p-Dioxane)1.0J ug/L 10/07/24 19:43 123-91-12.0 0.86 1
Surrogates
1,2-Dichloroethane-d4 (S)90 %10/07/24 19:43 17060-07-070-130 1
Toluene-d8 (S)94 %10/07/24 19:43 2037-26-570-130 1
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services - Asheville
4500S2D Sulfide Water
Sulfide ND ug/L 10/09/24 17:04 18496-25-810022.0 1
Analytical Method: EPA 335.4 Preparation Method: EPA 335.4
Pace Analytical Services - Ormond Beach
335.4 Cyanide, Total
Cyanide ND mg/L 10/17/24 13:53 57-12-510/17/24 09:430.010 0.0050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2380060
8151A
EPA 8151A
Chlorinated Herb. (GC) 8151A
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4133658-1
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 2.00 10/15/24 20:550.258
2,4,5-TP (Silvex)ug/L ND 2.00 10/15/24 20:550.335
2,4-D ug/L ND 2.00 10/15/24 20:550.547
Dinoseb ug/L ND 2.00 10/15/24 20:550.250
2,4-DCAA (S)%138 14.0-158 10/15/24 20:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4133658-2LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 2.442.50 97.6 54.0-120
2,4,5-TP (Silvex)ug/L 2.682.50 107 50.0-125
2,4-D ug/L 3.53 L0,P92.50 141 50.0-120
Dinoseb ug/L 2.532.50 101 36.0-134
2,4-DCAA (S)%109 14.0-158
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4133658-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1785304-02
R4133658-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L P92.50 109 54.0-120120 9.76 202.50ND 2.73 3.01
2,4,5-TP (Silvex)ug/L MH,P92.50 115 50.0-125126 8.64 202.50ND 2.88 3.14
2,4-D ug/L MH,P92.50 138 50.0-120150 8.60 202.50ND 3.45 3.76
Dinoseb ug/L MH,P92.50 129 36.0-134138 6.90 202.50ND 3.22 3.45
2,4-DCAA (S)%125 14.0-158135
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1049808
EPA 7470
EPA 7470
7470 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5771317
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/22/24 14:030.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5771318LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 1.92 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5771319MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35913219002
5771320
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2 98 75-12599 1 2020.14U 2.0 2.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1048973
EPA 3010
EPA 6010
6010 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5766985
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
Tin ug/L ND 50.0 10/24/24 10:3116.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5766986LABORATORY CONTROL SAMPLE:
LCSSpike
Tin ug/L 12601250 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5766987MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35912075001
5766988
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Tin ug/L 1250 99 75-12598 1 20125016.0U 1240 1230
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1048974
EPA 3010
EPA 6020
6020 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5766989
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 1.0 10/26/24 17:460.50
Arsenic ug/L ND 1.0 10/26/24 17:460.50
Barium ug/L ND 1.0 10/26/24 17:460.50
Beryllium ug/L ND 0.10 10/25/24 21:010.033
Cadmium ug/L ND 0.10 10/26/24 17:460.067
Chromium ug/L ND 1.0 10/26/24 17:460.50
Cobalt ug/L ND 1.0 10/26/24 17:460.24
Copper ug/L ND 1.0 10/26/24 17:460.42
Lead ug/L ND 1.0 10/26/24 17:460.22
Nickel ug/L ND 1.0 10/26/24 17:460.26
Selenium ug/L ND 2.0 10/26/24 17:460.20
Silver ug/L ND 0.50 10/26/24 17:460.028
Thallium ug/L ND 1.0 10/25/24 21:010.11
Vanadium ug/L ND 1.0 10/26/24 17:460.91
Zinc ug/L ND 10.0 10/25/24 21:016.7
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5766990LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 52.650 105 80-120
Arsenic ug/L 50.050 100 80-120
Barium ug/L 53.750 107 80-120
Beryllium ug/L 5.25 104 80-120
Cadmium ug/L 4.65 93 80-120
Chromium ug/L 51.050 102 80-120
Cobalt ug/L 52.050 104 80-120
Copper ug/L 50.050 100 80-120
Lead ug/L 51.550 103 80-120
Nickel ug/L 52.950 106 80-120
Selenium ug/L 50.750 101 80-120
Silver ug/L 4.85 96 80-120
Thallium ug/L 53.550 107 80-120
Vanadium ug/L 49.150 98 80-120
Zinc ug/L 246250 98 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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Huntersville, NC 28078
[phone]
Page 21 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5766991MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35912298001
5766992
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 50 105 75-125104 1 20500.50U 52.4 52.0
Arsenic ug/L 50 101 75-125100 1 20503.8 54.5 54.0
Barium ug/L 50 106 75-125110 1 2050192245247
Beryllium ug/L 5 105 75-125102 3 2050.033U 5.3 5.1
Cadmium ug/L 5 93 75-12591 2 2050.067U 4.7 4.5
Chromium ug/L 50 103 75-125103 0 20500.77J 52.0 52.1
Cobalt ug/L 50 103 75-125103 0 20500.51J 51.9 51.9
Copper ug/L 50 100 75-12598 2 20500.97J 50.8 49.9
Lead ug/L 50 99 75-12598 1 20500.22U 49.9 49.3
Nickel ug/L 50 104 75-125104 0 20500.68J 52.6 52.5
Selenium ug/L 50 99 75-12599 1 20500.43J 50.1 49.8
Silver ug/L 5 95 75-12594 1 2050.028U 4.8 4.7
Thallium ug/L 50 104 75-125103 1 20500.11U 52.1 51.5
Vanadium ug/L 50 102 75-125101 1 20500.91U 51.1 50.8
Zinc ug/L 250 95 75-12594 2 202507.2J 246 242
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
888074
EPA 8260D
EPA 8260D
8260D MSV Low Level Landfill
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4573332
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/12/24 00:160.31
1,1,1-Trichloroethane ug/L ND 1.0 10/12/24 00:160.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/12/24 00:160.22
1,1,2-Trichloroethane ug/L ND 1.0 10/12/24 00:160.32
1,1-Dichloroethane ug/L ND 1.0 10/12/24 00:160.37
1,1-Dichloroethene ug/L ND 1.0 10/12/24 00:160.35
1,1-Dichloropropene ug/L ND 1.0 10/12/24 00:160.43
1,2,3-Trichlorobenzene ug/L ND 1.0 10/12/24 00:160.81
1,2,3-Trichloropropane ug/L ND 1.0 10/12/24 00:160.26
1,2,4-Trichlorobenzene ug/L ND 1.0 10/12/24 00:160.64
1,2-Dichlorobenzene ug/L ND 1.0 10/12/24 00:160.34
1,2-Dichloroethane ug/L ND 1.0 10/12/24 00:160.32
1,2-Dichloropropane ug/L ND 1.0 10/12/24 00:160.36
1,3-Dichloropropane ug/L ND 1.0 10/12/24 00:160.28
1,4-Dichlorobenzene ug/L ND 1.0 10/12/24 00:160.33
2,2-Dichloropropane ug/L ND 1.0 10/12/24 00:160.39
2-Butanone (MEK)ug/L ND 5.0 10/12/24 00:164.0
2-Hexanone ug/L ND 5.0 10/12/24 00:160.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/12/24 00:162.7
Acetone ug/L ND 25.0 10/12/24 00:165.1
Acetonitrile ug/L ND 50.0 10/12/24 00:1624.8
Acrolein ug/L ND 10.0 10/12/24 00:168.5
Acrylonitrile ug/L ND 10.0 10/12/24 00:161.8
Allyl chloride ug/L ND 2.0 10/12/24 00:160.50
Benzene ug/L ND 1.0 10/12/24 00:160.34
Bromochloromethane ug/L ND 1.0 10/12/24 00:160.47
Bromodichloromethane ug/L ND 1.0 10/12/24 00:160.31
Bromoform ug/L ND 1.0 10/12/24 00:160.34
Bromomethane ug/L ND 2.0 10/12/24 00:161.7
Carbon disulfide ug/L ND 2.0 10/12/24 00:160.36
Carbon tetrachloride ug/L ND 1.0 10/12/24 00:160.33
Chlorobenzene ug/L ND 1.0 10/12/24 00:160.28
Chloroethane ug/L ND 1.0 10/12/24 00:160.65
Chloroform ug/L ND 1.0 10/12/24 00:160.43
Chloromethane ug/L ND 1.0 10/12/24 00:160.54
Chloroprene ug/L ND 5.0 10/12/24 00:161.6
cis-1,2-Dichloroethene ug/L ND 1.0 10/12/24 00:160.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/12/24 00:160.36
Dibromochloromethane ug/L ND 1.0 10/12/24 00:160.36
Dibromomethane ug/L ND 1.0 10/12/24 00:160.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4573332
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 10/12/24 00:160.35
Ethyl methacrylate ug/L ND 1.0 10/12/24 00:160.28
Ethylbenzene ug/L ND 1.0 10/12/24 00:160.30
Hexachloro-1,3-butadiene ug/L ND 2.0 10/12/24 00:161.5
Iodomethane ug/L ND 20.0 v210/12/24 00:169.7
Isobutanol ug/L ND 100 v210/12/24 00:1652.3
Methacrylonitrile ug/L ND 10.0 10/12/24 00:164.2
Methyl methacrylate ug/L ND 2.0 10/12/24 00:160.32
Methylene Chloride ug/L ND 5.0 10/12/24 00:162.0
Naphthalene ug/L ND 1.0 10/12/24 00:160.64
Propionitrile ug/L ND 20.0 10/12/24 00:163.6
Styrene ug/L ND 1.0 10/12/24 00:160.29
Tetrachloroethene ug/L ND 1.0 10/12/24 00:160.29
Toluene ug/L ND 1.0 10/12/24 00:160.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/12/24 00:160.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/12/24 00:160.36
trans-1,4-Dichloro-2-butene ug/L ND 1.0 v210/12/24 00:160.56
Trichloroethene ug/L ND 1.0 10/12/24 00:160.38
Trichlorofluoromethane ug/L ND 1.0 10/12/24 00:160.30
Vinyl acetate ug/L ND 2.0 v210/12/24 00:161.3
Vinyl chloride ug/L ND 1.0 10/12/24 00:160.39
Xylene (Total)ug/L ND 1.0 10/12/24 00:160.34
1,2-Dichloroethane-d4 (S)%88 70-130 10/12/24 00:16
4-Bromofluorobenzene (S)%100 70-130 10/12/24 00:16
Toluene-d8 (S)%110 70-130 10/12/24 00:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573333LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 17.720 89 70-130
1,1,1-Trichloroethane ug/L 18.620 93 70-130
1,1,2,2-Tetrachloroethane ug/L 17.520 88 70-130
1,1,2-Trichloroethane ug/L 18.520 93 70-130
1,1-Dichloroethane ug/L 18.220 91 70-130
1,1-Dichloroethene ug/L 18.820 94 69-131
1,1-Dichloropropene ug/L 18.920 94 70-132
1,2,3-Trichlorobenzene ug/L 18.120 91 70-132
1,2,3-Trichloropropane ug/L 18.320 91 70-130
1,2,4-Trichlorobenzene ug/L 18.320 91 70-130
1,2-Dichlorobenzene ug/L 19.120 96 70-130
1,2-Dichloroethane ug/L 18.720 93 70-130
1,2-Dichloropropane ug/L 19.620 98 70-130
1,3-Dichloropropane ug/L 18.520 92 70-130
1,4-Dichlorobenzene ug/L 18.220 91 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573333LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 17.020 85 69-130
2-Butanone (MEK)ug/L 33.440 84 67-133
2-Hexanone ug/L 31.340 78 70-133
4-Methyl-2-pentanone (MIBK)ug/L 32.640 81 70-130
Acetone ug/L 35.040 87 67-130
Acetonitrile ug/L 195200 97 70-130
Acrolein ug/L 97.9100 98 53-166
Acrylonitrile ug/L 87.7100 88 70-130
Allyl chloride ug/L 18.420 92 69-130
Benzene ug/L 20.420 102 70-130
Bromochloromethane ug/L 18.420 92 70-130
Bromodichloromethane ug/L 18.020 90 70-130
Bromoform ug/L 16.920 85 70-133
Bromomethane ug/L 18.820 94 41-148
Carbon disulfide ug/L 18.520 93 70-131
Carbon tetrachloride ug/L 19.020 95 70-130
Chlorobenzene ug/L 18.820 94 70-130
Chloroethane ug/L 19.820 99 41-157
Chloroform ug/L 19.420 97 70-130
Chloromethane ug/L 17.220 86 59-141
Chloroprene ug/L 16.920 84 70-130
cis-1,2-Dichloroethene ug/L 18.220 91 70-130
cis-1,3-Dichloropropene ug/L 18.220 91 70-130
Dibromochloromethane ug/L 17.320 86 70-130
Dibromomethane ug/L 19.720 98 70-130
Dichlorodifluoromethane ug/L 16.020 80 54-147
Ethyl methacrylate ug/L 16.220 81 70-130
Ethylbenzene ug/L 18.520 92 70-130
Hexachloro-1,3-butadiene ug/L 17.220 86 70-134
Iodomethane ug/L 27.8 v3406957-140
Isobutanol ug/L 289 v34007267-136
Methacrylonitrile ug/L 178200 89 70-130
Methyl methacrylate ug/L 16.820 84 70-130
Methylene Chloride ug/L 17.520 88 62-130
Naphthalene ug/L 18.620 93 70-135
Propionitrile ug/L 183200 91 70-130
Styrene ug/L 18.920 94 70-130
Tetrachloroethene ug/L 18.720 93 70-130
Toluene ug/L 19.020 95 70-130
trans-1,2-Dichloroethene ug/L 18.320 91 70-130
trans-1,3-Dichloropropene ug/L 18.020 90 70-130
trans-1,4-Dichloro-2-butene ug/L 22.3 v32011157-149
Trichloroethene ug/L 20.420 102 70-130
Trichlorofluoromethane ug/L 20.720 103 57-130
Vinyl acetate ug/L 29.8 v3407570-141
Vinyl chloride ug/L 17.220 86 66-140
Xylene (Total)ug/L 56.660 94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573333LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4573334MATRIX SPIKE SAMPLE:
MSSpike
Result
92756913003
1,1,1,2-Tetrachloroethane ug/L 22.220 111 70-146ND
1,1,1-Trichloroethane ug/L 25.820 129 70-150ND
1,1,2,2-Tetrachloroethane ug/L 21.820 109 66-144ND
1,1,2-Trichloroethane ug/L 23.420 117 70-142ND
1,1-Dichloroethane ug/L 25.220 126 68-150ND
1,1-Dichloroethene ug/L 26.020 130 64-162ND
1,1-Dichloropropene ug/L 26.320 131 70-160ND
1,2,3-Trichlorobenzene ug/L 23.920 120 66-151ND
1,2,3-Trichloropropane ug/L 22.620 113 66-144ND
1,2,4-Trichlorobenzene ug/L 25.320 127 69-147ND
1,2-Dichlorobenzene ug/L 23.220 116 70-142ND
1,2-Dichloroethane ug/L 24.920 125 68-145ND
1,2-Dichloropropane ug/L 25.420 127 70-144ND
1,3-Dichloropropane ug/L 22.420 112 70-141ND
1,4-Dichlorobenzene ug/L 23.420 117 70-140ND
2,2-Dichloropropane ug/L 26.720 134 58-160ND
2-Butanone (MEK)ug/L 42.040 105 57-156ND
2-Hexanone ug/L 36.940 92 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 39.540 99 65-144ND
Acetone ug/L 43.440 108 49-162ND
Acetonitrile ug/L 236200 118 69-145ND
Acrolein ug/L 127100 127 10-200ND
Acrylonitrile ug/L 111100 111 59-155ND
Allyl chloride ug/L 25.120 126 70-146ND
Benzene ug/L 26.420 132 68-144ND
Bromochloromethane ug/L 24.820 124 70-148ND
Bromodichloromethane ug/L 23.120 115 70-141ND
Bromoform ug/L 20.920 104 59-144ND
Bromomethane ug/L 23.120 116 23-190ND
Carbon disulfide ug/L 26.920 134 64-160ND
Carbon tetrachloride ug/L 25.520 128 70-147ND
Chlorobenzene ug/L 23.020 115 70-143ND
Chloroethane ug/L 26.720 134 55-190ND
Chloroform ug/L 25.520 128 67-148ND
Chloromethane ug/L 22.920 115 38-180ND
Chloroprene ug/L 23.920 119 70-148ND
cis-1,2-Dichloroethene ug/L 24.620 123 67-151ND
cis-1,3-Dichloropropene ug/L 23.520 118 70-142ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4573334MATRIX SPIKE SAMPLE:
MSSpike
Result
92756913003
Dibromochloromethane ug/L 21.620 108 68-140ND
Dibromomethane ug/L 25.220 126 70-142ND
Dichlorodifluoromethane ug/L 21.220 106 15-200ND
Ethyl methacrylate ug/L 20.020 100 68-139ND
Ethylbenzene ug/L 23.220 116 70-145ND
Hexachloro-1,3-butadiene ug/L 26.320 132 64-164ND
Iodomethane ug/L 47.440 117 37-160ND
Isobutanol ug/L 357 v34008953-152ND
Methacrylonitrile ug/L 225200 113 70-137ND
Methyl methacrylate ug/L 20.520 103 69-134ND
Methylene Chloride ug/L 23.120 116 54-149ND
Naphthalene ug/L 22.320 111 62-154ND
Propionitrile ug/L 227200 113 70-136ND
Styrene ug/L 23.020 115 70-147ND
Tetrachloroethene ug/L 22.920 115 70-145ND
Toluene ug/L 24.420 122 65-146ND
trans-1,2-Dichloroethene ug/L 26.320 131 69-155ND
trans-1,3-Dichloropropene ug/L 23.720 119 70-142ND
trans-1,4-Dichloro-2-butene ug/L 18.6 v1209339-149ND
Trichloroethene ug/L 26.320 132 70-152ND
Trichlorofluoromethane ug/L 29.020 145 60-158ND
Vinyl acetate ug/L 40.540 101 56-157ND
Vinyl chloride ug/L 24.420 122 51-178ND
Xylene (Total)ug/L 71.360 119 70-146ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756913004
4573335SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756913004
4573335SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND v230ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND v130ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756913004
4573335SAMPLE DUPLICATE:
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9285
4-Bromofluorobenzene (S)%9899
Toluene-d8 (S)%110111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
887074
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4568469
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 10/07/24 17:090.86
1,2-Dichloroethane-d4 (S)%89 70-130 10/07/24 17:09
Toluene-d8 (S)%93 70-130 10/07/24 17:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4568470LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 18.520 93 67-130
1,2-Dichloroethane-d4 (S)%90 70-130
Toluene-d8 (S)%93 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4568471MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92756909001
4568472
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 91 10-17095 3 30201.3J 19.5 20.2
1,2-Dichloroethane-d4 (S)%90 70-13092 30
Toluene-d8 (S)%94 70-13094 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
886992
EPA 3510C
EPA 8081B
8081 OC Pesticides Red Vol
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4568309
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.050 10/07/24 08:250.017
4,4'-DDE ug/L ND 0.050 10/07/24 08:250.024
4,4'-DDT ug/L ND 0.050 10/07/24 08:250.026
Aldrin ug/L ND 0.050 10/07/24 08:250.014
alpha-BHC ug/L ND 0.050 10/07/24 08:250.012
beta-BHC ug/L ND 0.050 10/07/24 08:250.049
Chlordane (Technical)ug/L ND 0.50 10/07/24 08:250.16
delta-BHC ug/L ND 0.050 10/07/24 08:250.014
Dieldrin ug/L ND 0.050 10/07/24 08:250.015
Endosulfan I ug/L ND 0.050 10/07/24 08:250.017
Endosulfan II ug/L ND 0.050 10/07/24 08:250.016
Endosulfan sulfate ug/L ND 0.050 10/07/24 08:250.015
Endrin ug/L ND 0.050 10/07/24 08:250.018
Endrin aldehyde ug/L ND 0.050 10/07/24 08:250.016
gamma-BHC (Lindane)ug/L ND 0.050 10/07/24 08:250.012
Heptachlor ug/L ND 0.050 10/07/24 08:250.020
Heptachlor epoxide ug/L ND 0.050 10/07/24 08:250.028
Methoxychlor ug/L ND 0.15 10/07/24 08:250.042
Toxaphene ug/L ND 0.50 10/07/24 08:250.22
Decachlorobiphenyl (S)%152 10-200 10/07/24 08:25
Tetrachloro-m-xylene (S)%84 10-190 10/07/24 08:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4568310LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.340.25 137 46-200
4,4'-DDE ug/L 0.310.25 123 36-198
4,4'-DDT ug/L 0.300.25 121 35-200
Aldrin ug/L 0.270.25 106 10-154
alpha-BHC ug/L 0.320.25 127 24-168
beta-BHC ug/L 0.290.25 117 43-161
delta-BHC ug/L 0.260.25 102 32-153
Dieldrin ug/L 0.300.25 121 31-196
Endosulfan I ug/L 0.310.25 123 32-167
Endosulfan II ug/L 0.350.25 138 38-166
Endosulfan sulfate ug/L 0.330.25 134 45-169
Endrin ug/L 0.310.25 124 35-200
Endrin aldehyde ug/L 0.350.25 138 38-156
gamma-BHC (Lindane)ug/L 0.300.25 122 24-165
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4568310LABORATORY CONTROL SAMPLE:
LCSSpike
Heptachlor ug/L 0.270.25 110 18-183
Heptachlor epoxide ug/L 0.290.25 116 31-159
Methoxychlor ug/L 0.980.75 131 28-173
Decachlorobiphenyl (S)%175 10-200
Tetrachloro-m-xylene (S)%111 10-190
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4568311MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92742838015
4568312
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4,4'-DDD ug/L 0.5 160 18-200178 11 300.5ND 0.80 0.89
4,4'-DDE ug/L 0.5 108 10-200135 22 300.5ND 0.54 0.67
4,4'-DDT ug/L 0.5 144 12-200176 20 300.5ND 0.72 0.88
Aldrin ug/L 0.5 118 10-174155 27 300.5ND 0.59 0.77
alpha-BHC ug/L 0.5 120 10-191140 16 300.5ND 0.60 0.70
beta-BHC ug/L 0.5 112 13-193130 15 300.5ND 0.56 0.65
delta-BHC ug/L 0.5 97 10-184115 18 300.5ND 0.48 0.58
Dieldrin ug/L 0.5 104 10-200123 16 300.5ND 0.52 0.61
Endosulfan I ug/L 0.5 117 14-182136 15 300.5ND 0.58 0.68
Endosulfan II ug/L 0.5 163 10-192192 16 300.5ND 0.82 0.96
Endosulfan sulfate ug/L 0.5 122 19-195147 19 300.5ND 0.61 0.74
Endrin ug/L 0.5 110 10-200130 17 300.5ND 0.55 0.65
Endrin aldehyde ug/L 0.5 139 10-185161 15 300.5ND 0.70 0.81
gamma-BHC (Lindane)ug/L 0.5 103 10-188123 18 300.5ND 0.52 0.61
Heptachlor ug/L 0.5 92 10-200115 23 300.5ND 0.46 0.57
Heptachlor epoxide ug/L 0.5 116 10-186136 16 300.5ND 0.58 0.68
Methoxychlor ug/L 1.5 116 10-194137 17 301.5ND 1.7 2.1
Decachlorobiphenyl (S)%125 10-200131
Tetrachloro-m-xylene (S)%85 10-190102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
887010
EPA 3510C
EPA 8082A
8082 GCS PCB
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4568360
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 10/07/24 14:080.21
PCB-1221 (Aroclor 1221)ug/L ND 0.50 10/07/24 14:080.23
PCB-1232 (Aroclor 1232)ug/L ND 0.50 10/07/24 14:080.23
PCB-1242 (Aroclor 1242)ug/L ND 0.50 10/07/24 14:080.25
PCB-1248 (Aroclor 1248)ug/L ND 0.50 10/07/24 14:080.29
PCB-1254 (Aroclor 1254)ug/L ND 0.50 10/07/24 14:080.21
PCB-1260 (Aroclor 1260)ug/L ND 0.50 10/07/24 14:080.16
Decachlorobiphenyl (S)%131 10-200 10/07/24 14:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4568361LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 5.05 100 36-140
PCB-1260 (Aroclor 1260)ug/L 5.65 112 31-146
Decachlorobiphenyl (S)%102 10-200
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4568362MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92745548023
4568363
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
PCB-1016 (Aroclor 1016)ug/L 10 54 10-18168 24 3010ND5.4 6.8
PCB-1260 (Aroclor 1260)ug/L R1104010-16658 36 3010ND4.0 5.8
Decachlorobiphenyl (S)%43 10-20062
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
886988
EPA 3510C
EPA 8270E
8270E Water APP9 RV MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4568290
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 10/07/24 12:524.5
1,3,5-Trinitrobenzene ug/L ND 10.0 10/07/24 12:525.5
1,3-Dinitrobenzene ug/L ND 10.0 10/07/24 12:523.8
1,4-Naphthoquinone ug/L ND 5.0 10/07/24 12:524.4
1-Naphthalenamine ug/L ND 10.0 10/07/24 12:526.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 10/07/24 12:521.2
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 10/07/24 12:521.5
2,4,5-Trichlorophenol ug/L ND 10.0 10/07/24 12:521.4
2,4,6-Trichlorophenol ug/L ND 10.0 10/07/24 12:521.6
2,4-Dichlorophenol ug/L ND 10.0 10/07/24 12:521.4
2,4-Dimethylphenol ug/L ND 10.0 10/07/24 12:521.7
2,4-Dinitrophenol ug/L ND 50.0 10/07/24 12:5226.0
2,4-Dinitrotoluene ug/L ND 10.0 v110/07/24 12:521.6
2,6-Dichlorophenol ug/L ND 10.0 10/07/24 12:524.2
2,6-Dinitrotoluene ug/L ND 10.0 10/07/24 12:521.7
2-Acetylaminofluorene ug/L ND 10.0 v210/07/24 12:524.1
2-Chloronaphthalene ug/L ND 10.0 10/07/24 12:521.7
2-Chlorophenol ug/L ND 10.0 10/07/24 12:521.2
2-Methylnaphthalene ug/L ND 10.0 10/07/24 12:521.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 10/07/24 12:521.9
2-Naphthalenamine ug/L ND 10.0 10/07/24 12:525.4
2-Nitroaniline ug/L ND 20.0 10/07/24 12:523.0
2-Nitrophenol ug/L ND 10.0 10/07/24 12:521.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 10/07/24 12:521.2
3,3'-Dichlorobenzidine ug/L ND 20.0 10/07/24 12:528.1
3,3'-Dimethylbenzidine ug/L ND 50.0 10/07/24 12:5231.1
3-Methylcholanthrene ug/L ND 10.0 10/07/24 12:523.7
3-Nitroaniline ug/L ND 20.0 10/07/24 12:523.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 10/07/24 12:527.8
4-Aminobiphenyl ug/L ND 10.0 10/07/24 12:524.7
4-Bromophenylphenyl ether ug/L ND 10.0 10/07/24 12:521.8
4-Chloro-3-methylphenol ug/L ND 10.0 10/07/24 12:523.3
4-Chloroaniline ug/L ND 20.0 10/07/24 12:523.6
4-Chlorophenylphenyl ether ug/L ND 10.0 10/07/24 12:522.0
4-Nitroaniline ug/L ND 20.0 10/07/24 12:525.1
4-Nitrophenol ug/L ND 50.0 10/07/24 12:526.6
5-Nitro-o-toluidine ug/L ND 10.0 10/07/24 12:523.8
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 10/07/24 12:523.0
Acenaphthene ug/L ND 10.0 10/07/24 12:522.0
Acenaphthylene ug/L ND 10.0 10/07/24 12:522.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4568290
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
Acetophenone ug/L ND 10.0 10/07/24 12:521.5
Anthracene ug/L ND 10.0 10/07/24 12:522.3
Benzo(a)anthracene ug/L ND 10.0 10/07/24 12:522.7
Benzo(a)pyrene ug/L ND 10.0 10/07/24 12:522.8
Benzo(b)fluoranthene ug/L ND 10.0 10/07/24 12:522.6
Benzo(g,h,i)perylene ug/L ND 10.0 10/07/24 12:522.8
Benzo(k)fluoranthene ug/L ND 10.0 10/07/24 12:522.7
Benzyl alcohol ug/L ND 20.0 10/07/24 12:522.9
bis(2-Chloroethoxy)methane ug/L ND 10.0 10/07/24 12:521.8
bis(2-Chloroethyl) ether ug/L ND 10.0 10/07/24 12:521.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 10/07/24 12:523.7
Butylbenzylphthalate ug/L ND 10.0 10/07/24 12:523.1
Chlorobenzilate ug/L ND 10.0 10/07/24 12:523.8
Chrysene ug/L ND 10.0 10/07/24 12:522.8
Di-n-butylphthalate ug/L ND 10.0 10/07/24 12:522.2
Di-n-octylphthalate ug/L ND 10.0 10/07/24 12:523.9
Diallate ug/L ND 10.0 v210/07/24 12:523.4
Dibenz(a,h)anthracene ug/L ND 10.0 10/07/24 12:523.0
Dibenzofuran ug/L ND 10.0 10/07/24 12:522.1
Diethylphthalate ug/L ND 10.0 10/07/24 12:522.0
Dimethoate ug/L ND 10.0 10/07/24 12:523.7
Dimethylphthalate ug/L ND 10.0 10/07/24 12:522.1
Diphenylamine ug/L ND 10.0 10/07/24 12:523.0
Disulfoton ug/L ND 10.0 10/07/24 12:524.6
Ethyl methanesulfonate ug/L ND 20.0 10/07/24 12:523.0
Famphur ug/L ND 10.0 10/07/24 12:526.1
Fluoranthene ug/L ND 10.0 10/07/24 12:522.2
Fluorene ug/L ND 10.0 10/07/24 12:522.1
Hexachlorobenzene ug/L ND 10.0 10/07/24 12:522.2
Hexachlorocyclopentadiene ug/L ND 10.0 10/07/24 12:521.6
Hexachloroethane ug/L ND 10.0 10/07/24 12:521.4
Hexachloropropene ug/L ND 10.0 10/07/24 12:522.7
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 10/07/24 12:522.9
Isodrin ug/L ND 10.0 10/07/24 12:522.8
Isophorone ug/L ND 10.0 10/07/24 12:521.7
Isosafrole ug/L ND 10.0 10/07/24 12:522.5
Kepone ug/L ND 20.0 10/07/24 12:5214.1
Methapyrilene ug/L ND 50.0 10/07/24 12:5217.0
Methyl methanesulfonate ug/L ND 5.0 10/07/24 12:523.1
Methyl parathion ug/L ND 10.0 10/07/24 12:523.7
N-Nitroso-di-n-butylamine ug/L ND 10.0 10/07/24 12:522.0
N-Nitroso-di-n-propylamine ug/L ND 10.0 10/07/24 12:521.3
N-Nitrosodiethylamine ug/L ND 10.0 10/07/24 12:522.3
N-Nitrosodimethylamine ug/L ND 10.0 10/07/24 12:521.9
N-Nitrosodiphenylamine ug/L ND 10.0 10/07/24 12:523.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4568290
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
N-Nitrosomethylethylamine ug/L ND 10.0 10/07/24 12:527.5
N-Nitrosopiperidine ug/L ND 10.0 10/07/24 12:522.5
N-Nitrosopyrrolidine ug/L ND 10.0 v210/07/24 12:523.1
Nitrobenzene ug/L ND 10.0 10/07/24 12:521.9
O,O,O-Triethylphosphorothioate ug/L ND 10.0 10/07/24 12:522.6
O-Toluidine ug/L ND 10.0 10/07/24 12:522.6
P-Dimethylaminoazobenzene ug/L ND 5.0 10/07/24 12:522.4
p-Phenylenediamine ug/L ND 10.0 10/07/24 12:5210.0
Parathion (Ethyl parathion)ug/L ND 10.0 10/07/24 12:523.9
Pentachlorobenzene ug/L ND 10.0 10/07/24 12:523.4
Pentachloronitrobenzene ug/L ND 10.0 10/07/24 12:523.3
Pentachlorophenol ug/L ND 20.0 10/07/24 12:523.8
Phenacetin ug/L ND 10.0 10/07/24 12:523.6
Phenanthrene ug/L ND 10.0 10/07/24 12:522.0
Phenol ug/L ND 10.0 10/07/24 12:521.4
Phorate ug/L ND 10.0 10/07/24 12:523.6
Pronamide ug/L ND 10.0 10/07/24 12:523.1
Pyrene ug/L ND 10.0 10/07/24 12:522.2
Safrole ug/L ND 10.0 10/07/24 12:522.3
Thionazin ug/L ND 10.0 10/07/24 12:522.9
2,4,6-Tribromophenol (S)%11 10-166 10/07/24 12:52
2-Fluorobiphenyl (S)%32 10-130 10/07/24 12:52
2-Fluorophenol (S)%5 10-130 S010/07/24 12:52
Nitrobenzene-d5 (S)%36 10-133 10/07/24 12:52
Phenol-d6 (S)%11 10-130 10/07/24 12:52
Terphenyl-d14 (S)%54 10-193 10/07/24 12:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4568291LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 30.250 60 18-130
1,3,5-Trinitrobenzene ug/L 44.850 90 59-200
1,3-Dinitrobenzene ug/L 41.550 83 51-170
1,4-Naphthoquinone ug/L 34.450 69 32-132
1-Naphthalenamine ug/L 15.4 L2503135-140
2,2'-Oxybis(1-chloropropane)ug/L 27.250 54 23-130
2,3,4,6-Tetrachlorophenol ug/L 39.250 78 38-154
2,4,5-Trichlorophenol ug/L 39.950 80 36-150
2,4,6-Trichlorophenol ug/L 35.550 71 30-151
2,4-Dichlorophenol ug/L 33.850 68 36-140
2,4-Dimethylphenol ug/L 31.850 64 36-155
2,4-Dinitrophenol ug/L 165250 66 10-169
2,4-Dinitrotoluene ug/L 48.9 v1509846-160
2,6-Dichlorophenol ug/L 36.550 73 34-156
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4568291LABORATORY CONTROL SAMPLE:
LCSSpike
2,6-Dinitrotoluene ug/L 45.850 92 47-161
2-Acetylaminofluorene ug/L 31.2 v3506239-184
2-Chloronaphthalene ug/L 31.250 62 29-134
2-Chlorophenol ug/L 28.350 57 29-130
2-Methylnaphthalene ug/L 29.950 60 26-130
2-Methylphenol(o-Cresol)ug/L 25.950 52 32-130
2-Naphthalenamine ug/L 24.050 48 23-145
2-Nitroaniline ug/L 70.9100 71 41-150
2-Nitrophenol ug/L 31.350 63 31-145
3&4-Methylphenol(m&p Cresol)ug/L 25.250 50 29-130
3,3'-Dichlorobenzidine ug/L 85.1100 85 46-153
3,3'-Dimethylbenzidine ug/L 38.4J100 38 24-200
3-Methylcholanthrene ug/L 42.450 85 31-195
3-Nitroaniline ug/L 81.4100 81 47-156
4,6-Dinitro-2-methylphenol ug/L 66.5100 66 23-161
4-Aminobiphenyl ug/L 27.850 56 26-151
4-Bromophenylphenyl ether ug/L 40.550 81 45-143
4-Chloro-3-methylphenol ug/L 69.8100 70 42-143
4-Chloroaniline ug/L 59.2100 59 37-135
4-Chlorophenylphenyl ether ug/L 39.150 78 43-140
4-Nitroaniline ug/L 86.7100 87 47-157
4-Nitrophenol ug/L 131250 52 10-130
5-Nitro-o-toluidine ug/L 47.550 95 54-170
7,12-Dimethylbenz(a)anthracene ug/L 43.350 87 29-176
Acenaphthene ug/L 32.850 66 38-138
Acenaphthylene ug/L 33.650 67 39-139
Acetophenone ug/L 27.450 55 34-135
Anthracene ug/L 39.650 79 45-136
Benzo(a)anthracene ug/L 41.150 82 52-151
Benzo(a)pyrene ug/L 42.150 84 46-165
Benzo(b)fluoranthene ug/L 45.750 91 44-170
Benzo(g,h,i)perylene ug/L 46.050 92 39-171
Benzo(k)fluoranthene ug/L 42.550 85 43-168
Benzyl alcohol ug/L 48.7100 49 33-134
bis(2-Chloroethoxy)methane ug/L 28.950 58 37-140
bis(2-Chloroethyl) ether ug/L 27.750 55 33-136
bis(2-Ethylhexyl)phthalate ug/L 36.550 73 50-169
Butylbenzylphthalate ug/L 37.450 75 50-174
Chlorobenzilate ug/L 41.850 84 46-167
Chrysene ug/L 41.750 83 52-148
Di-n-butylphthalate ug/L 41.850 84 51-154
Di-n-octylphthalate ug/L 38.550 77 44-170
Diallate ug/L 32.2 v3506449-147
Dibenz(a,h)anthracene ug/L 44.450 89 41-171
Dibenzofuran ug/L 33.650 67 42-157
Diethylphthalate ug/L 42.750 85 50-149
Dimethoate ug/L 36.050 72 52-169
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4568291LABORATORY CONTROL SAMPLE:
LCSSpike
Dimethylphthalate ug/L 40.650 81 47-146
Diphenylamine ug/L 37.650 75 53-142
Disulfoton ug/L 29.650 59 45-135
Ethyl methanesulfonate ug/L 28.850 58 27-146
Famphur ug/L 37.150 74 13-130
Fluoranthene ug/L 44.850 90 51-152
Fluorene ug/L 37.150 74 46-143
Hexachlorobenzene ug/L 40.750 81 40-139
Hexachlorocyclopentadiene ug/L 27.250 54 10-130
Hexachloroethane ug/L 17.550 35 10-130
Hexachloropropene ug/L 15.750 31 10-130
Indeno(1,2,3-cd)pyrene ug/L 45.250 90 40-172
Isodrin ug/L 42.650 85 50-150
Isophorone ug/L 32.050 64 37-143
Isosafrole ug/L 31.550 63 35-130
Kepone ug/L 77.0100 77 12-130
Methapyrilene ug/L ND L250310-188
Methyl methanesulfonate ug/L 19.050 38 24-135
Methyl parathion ug/L 40.550 81 59-174
N-Nitroso-di-n-butylamine ug/L 22.150 44 33-130
N-Nitroso-di-n-propylamine ug/L 29.950 60 38-145
N-Nitrosodiethylamine ug/L 27.250 54 26-145
N-Nitrosodimethylamine ug/L 23.250 46 30-130
N-Nitrosodiphenylamine ug/L 37.650 75 46-144
N-Nitrosomethylethylamine ug/L 26.350 53 19-138
N-Nitrosopiperidine ug/L 30.650 61 35-147
N-Nitrosopyrrolidine ug/L 25.5 v3505131-142
Nitrobenzene ug/L 29.950 60 33-136
O,O,O-Triethylphosphorothioate ug/L 32.750 65 27-136
O-Toluidine ug/L 26.350 53 27-140
P-Dimethylaminoazobenzene ug/L 36.8100 37 23-130
p-Phenylenediamine ug/L ND
Parathion (Ethyl parathion)ug/L 46.050 92 59-171
Pentachlorobenzene ug/L 38.150 76 42-138
Pentachloronitrobenzene ug/L 52.850 106 64-185
Pentachlorophenol ug/L 75.7100 76 19-156
Phenacetin ug/L 42.350 85 57-174
Phenanthrene ug/L 39.050 78 49-143
Phenol ug/L 17.250 34 18-130
Phorate ug/L 36.450 73 41-200
Pronamide ug/L 45.550 91 59-174
Pyrene ug/L 36.550 73 48-156
Safrole ug/L 31.950 64 31-136
Thionazin ug/L 37.350 75 52-151
2,4,6-Tribromophenol (S)%75 10-166
2-Fluorobiphenyl (S)%48 10-130
2-Fluorophenol (S)%34 10-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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[phone]
Page 38 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4568291LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrobenzene-d5 (S)%50 10-133
Phenol-d6 (S)%26 10-130
Terphenyl-d14 (S)%65 10-193
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4568292MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92757074001
4568293
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4,5-Tetrachlorobenzene ug/L 90.9 42 10-13636 16 3090.9ND 38.1 32.6
1,3,5-Trinitrobenzene ug/L 90.9 74 32-20063 16 3090.9ND 67.4 57.3
1,3-Dinitrobenzene ug/L 90.9 60 30-17353 13 3090.9ND 54.6 48.0
1,4-Naphthoquinone ug/L 90.9 49 10-14443 13 3090.9ND 44.3 38.7
1-Naphthalenamine ug/L M090.9 23 10-1565 3090.9ND 20.7 ND
2,2'-Oxybis(1-
chloropropane)ug/L 90.9 35 10-13231 10 3090.9ND 31.7 28.6
2,3,4,6-Tetrachlorophenol ug/L 90.9 59 10-18551 15 3090.9ND 53.3 46.0
2,4,5-Trichlorophenol ug/L 90.9 60 10-17453 12 3090.9ND 54.6 48.2
2,4,6-Trichlorophenol ug/L 90.9 52 10-17345 14 3090.9ND 46.9 40.7
2,4-Dichlorophenol ug/L 90.9 45 10-15339 13 3090.9ND 41.0 35.9
2,4-Dimethylphenol ug/L 90.9 43 12-15736 20 3090.9ND 39.5 32.3
2,4-Dinitrophenol ug/L R14552110-16542 66 30455ND96.8 193
2,4-Dinitrotoluene ug/L v190.9 70 29-16860 15 3090.9ND 63.8 55.0
2,6-Dichlorophenol ug/L 90.9 51 10-17844 15 3090.9ND 45.9 39.6
2,6-Dinitrotoluene ug/L 90.9 66 28-16857 15 3090.9ND 59.9 51.6
2-Acetylaminofluorene ug/L v390.9 57 20-19449 17 3090.9ND 52.3 44.1
2-Chloronaphthalene ug/L 90.9 42 11-13637 14 3090.9ND 38.2 33.3
2-Chlorophenol ug/L 90.9 36 10-13432 13 3090.9ND 33.1 29.1
2-Methylnaphthalene ug/L 90.9 40 10-13135 11 3090.9ND 36.0 32.2
2-Methylphenol(o-Cresol)ug/L 90.9 35 10-13030 16 3090.9ND 31.7 26.8
2-Naphthalenamine ug/L M190.9 31 10-1473 3090.9ND 27.9 ND
2-Nitroaniline ug/L 182 51 19-15646 11 30182ND93.1 83.7
2-Nitrophenol ug/L 90.9 41 10-16037 9 3090.9ND 37.3 33.9
3&4-Methylphenol(m&p
Cresol)ug/L 90.9 35 10-13230 17 3090.9ND 32.2 27.1
3,3'-Dichlorobenzidine ug/L R11826610-17339 52 30182ND12070.7
3,3'-Dimethylbenzidine ug/L M11823610-2000 30182ND65.1J ND
3-Methylcholanthrene ug/L 90.9 67 10-20055 20 3090.9ND 61.3 50.1
3-Nitroaniline ug/L 182 59 19-16949 18 30182ND10789.9
4,6-Dinitro-2-methylphenol ug/L 182 44 10-17842 3 30182ND79.5 77.0
4-Aminobiphenyl ug/L R190.9 40 10-17021 62 3090.9ND 36.8 19.3
4-Bromophenylphenyl ether ug/L 90.9 59 28-14952 13 3090.9ND 54.1 47.3
4-Chloro-3-methylphenol ug/L 182 52 18-14845 15 30182ND95.3 82.2
4-Chloroaniline ug/L 182 43 10-14132 30 30182ND77.8 57.7
4-Chlorophenylphenyl ether ug/L 90.9 56 24-14448 16 3090.9ND 51.4 43.7
4-Nitroaniline ug/L 182 62 18-17052 18 30182ND11394.0
4-Nitrophenol ug/L 455 35 10-13034 2 30455ND159155
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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Page 39 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4568292MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92757074001
4568293
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
5-Nitro-o-toluidine ug/L 90.9 71 38-16757 21 3090.9ND 64.4 52.1
7,12-
Dimethylbenz(a)anthracene ug/L 90.9 69 10-18258 18 3090.9ND 62.7 52.4
Acenaphthene ug/L 90.9 45 18-14239 15 3090.9ND 41.0 35.3
Acenaphthylene ug/L 90.9 46 18-14340 15 3090.9ND 42.2 36.4
Acetophenone ug/L 90.9 36 10-14232 10 3090.9ND 32.4 29.3
Anthracene ug/L 90.9 61 32-13851 17 3090.9ND 55.4 46.7
Benzo(a)anthracene ug/L 90.9 65 41-15553 19 3090.9ND 58.9 48.6
Benzo(a)pyrene ug/L 90.9 66 10-16755 19 3090.9ND 60.3 49.9
Benzo(b)fluoranthene ug/L 90.9 70 31-17258 18 3090.9ND 63.4 52.7
Benzo(g,h,i)perylene ug/L 90.9 72 26-17758 21 3090.9ND 65.1 52.9
Benzo(k)fluoranthene ug/L 90.9 66 31-16858 14 3090.9ND 60.3 52.4
Benzyl alcohol ug/L 182 32 10-13629 10 30182ND57.7 52.3
bis(2-
Chloroethoxy)methane
ug/L 90.9 37 12-14334 8 3090.9ND 33.7 31.0
bis(2-Chloroethyl) ether ug/L 90.9 36 10-13932 10 3090.9ND 32.5 29.5
bis(2-Ethylhexyl)phthalate ug/L 90.9 56 41-17347 17 3090.9ND 51.1 43.1
Butylbenzylphthalate ug/L 90.9 57 38-18249 15 3090.9ND 52.2 44.9
Chlorobenzilate ug/L 90.9 67 33-17556 18 3090.9ND 60.7 50.8
Chrysene ug/L 90.9 66 41-15255 18 3090.9ND 60.1 50.3
Di-n-butylphthalate ug/L 90.9 62 37-16255 13 3090.9ND 56.7 49.7
Di-n-octylphthalate ug/L 90.9 59 36-17651 14 3090.9ND 53.2 46.2
Diallate ug/L v390.9 48 26-15542 12 3090.9ND 43.8 38.6
Dibenz(a,h)anthracene ug/L 90.9 69 29-17558 17 3090.9ND 62.5 52.7
Dibenzofuran ug/L 90.9 48 23-14441 16 3090.9ND 43.8 37.4
Diethylphthalate ug/L 90.9 63 33-15454 15 3090.9ND 57.0 49.1
Dimethoate ug/L 90.9 54 41-16946 17 3090.9ND 49.0 41.4
Dimethylphthalate ug/L 90.9 58 29-15049 16 3090.9ND 52.8 44.9
Diphenylamine ug/L 90.9 58 34-14648 18 3090.9ND 52.6 43.7
Disulfoton ug/L 90.9 48 36-13341 16 3090.9ND 43.7 37.2
Ethyl methanesulfonate ug/L 90.9 38 10-14735 3090.9ND 34.6J 31.8J
Famphur ug/L 90.9 53 10-13046 14 3090.9ND 48.1 42.0
Fluoranthene ug/L 90.9 68 40-15657 17 3090.9ND 62.1 52.2
Fluorene ug/L 90.9 53 26-14845 15 3090.9ND 47.9 41.1
Hexachlorobenzene ug/L 90.9 60 27-14553 13 3090.9ND 54.8 48.3
Hexachlorocyclopentadiene ug/L 90.9 32 10-13031 5 3090.9ND 29.4 28.0
Hexachloroethane ug/L 90.9 22 10-13019 3090.9ND 19.6 17.4J
Hexachloropropene ug/L 90.9 27 10-13020 3090.9ND 24.4 17.8J
Indeno(1,2,3-cd)pyrene ug/L 90.9 69 28-17657 19 3090.9ND 63.1 52.2
Isodrin ug/L 90.9 66 33-15358 13 3090.9ND 60.1 52.5
Isophorone ug/L 90.9 42 14-14539 8 3090.9ND 38.1 35.2
Isosafrole ug/L 90.9 43 13-13637 15 3090.9ND 39.1 33.6
Kepone ug/L 182 60 10-13056 7 30182ND110102
Methapyrilene ug/L M090.9 13 10-2000 3090.9ND ND ND
Methyl methanesulfonate ug/L 90.9 25 10-13822 12 3090.9ND 23.0 20.4
Methyl parathion ug/L 90.9 60 44-17752 14 3090.9ND 54.1 46.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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Huntersville, NC 28078
[phone]
Page 40 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4568292MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92757074001
4568293
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitroso-di-n-butylamine ug/L 90.9 39 14-13328 30 3090.9ND 35.0 25.8
N-Nitroso-di-n-propylamine ug/L 90.9 40 12-14937 10 3090.9ND 36.7 33.3
N-Nitrosodiethylamine ug/L 90.9 36 10-14833 7 3090.9ND 32.3 30.0
N-Nitrosodimethylamine ug/L 90.9 31 10-13027 13 3090.9ND 28.1 24.8
N-Nitrosodiphenylamine ug/L 90.9 58 29-14948 18 3090.9ND 52.6 43.7
N-Nitrosomethylethylamine ug/L 90.9 40 10-13932 22 3090.9ND 36.6 29.4
N-Nitrosopiperidine ug/L 90.9 41 14-15136 13 3090.9ND 36.9 32.3
N-Nitrosopyrrolidine ug/L v390.9 35 14-14332 11 3090.9ND 32.0 28.7
Nitrobenzene ug/L 90.9 41 10-14536 13 3090.9ND 37.3 32.8
O,O,O-
Triethylphosphorothioate
ug/L 90.9 44 10-14240 10 3090.9ND 40.1 36.4
O-Toluidine ug/L 90.9 37 10-13728 27 3090.9ND 33.7 25.7
P-
Dimethylaminoazobenzene ug/L R11823017-13017 55 30182ND54.2 30.9
p-Phenylenediamine ug/L 30NDNDND
Parathion (Ethyl parathion)ug/L 90.9 68 45-17458 15 3090.9ND 61.8 53.2
Pentachlorobenzene ug/L 90.9 54 20-14347 15 3090.9ND 49.3 42.5
Pentachloronitrobenzene ug/L 90.9 79 39-18670 12 3090.9ND 71.6 63.6
Pentachlorophenol ug/L 182 56 10-17852 7 30182ND10294.9
Phenacetin ug/L 90.9 63 36-18555 13 3090.9ND 57.1 50.1
Phenanthrene ug/L 90.9 59 36-14650 17 3090.9ND 53.8 45.5
Phenol ug/L 90.9 24 10-13019 3090.9ND 21.6 17.5J
Phorate ug/L R190.9 66 26-20047 34 3090.9ND 60.2 42.5
Pronamide ug/L 90.9 69 40-18158 16 3090.9ND 62.4 53.1
Pyrene ug/L 90.9 58 42-15649 17 3090.9ND 52.8 44.4
Safrole ug/L 90.9 44 10-14239 13 3090.9ND 40.2 35.3
Thionazin ug/L 90.9 58 31-15949 16 3090.9ND 52.3 44.4
2,4,6-Tribromophenol (S)%59 10-16649
2-Fluorobiphenyl (S)%35 10-13033
2-Fluorophenol (S)%23 10-13020
Nitrobenzene-d5 (S)%34 10-13331
Phenol-d6 (S)%18 10-13015
Terphenyl-d14 (S)%49 10-19337
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
887565
SM 4500-S2D-2011
SM 4500-S2D-2011
4500S2D Sulfide Water
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4570882
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 100 10/09/24 16:4222.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4570883LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 516500 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4570886MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92757074002
4570887
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 108 80-120108 0 10500ND539539
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4571846MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92757339001
4571847
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 112 80-120112 0 10500ND583583
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1048509
EPA 335.4
EPA 335.4
335.4 Cyanide, Total
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92757074001, 92757074002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5764429
Associated Lab Samples:92757074001, 92757074002
Matrix:Water
AnalyzedMDL
Cyanide mg/L ND 0.010 10/17/24 13:500.0050
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5764430LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/L 0.0500.05 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5765029MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35911747001
5765030
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L 0.025 93 90-11098 5 200.025ND 0.024 0.025
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5765031MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35911775001
5765032
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L M10.025 74 90-11084 13 200.025ND 0.019 0.021
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 43 of 49
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
WORKORDER QUALIFIERS
WO: 92757074
[1]
ANALYTE QUALIFIERS
Analysis of acrolein and/or acrylonitrile was performed from a sample that was field preserved to pH < 2, which is less
than the pH range of 4-5 specified in the test method and required for NPDES compliance per 40CFR Part 136.AC
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Sample was received or analysis requested beyond the recognized method holding time.H3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
RPD between the primary and confirmatory analysis exceeded 40%.P9
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 49
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
ANALYTE QUALIFIERS
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 49
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92757074
Iredell Lined Ph 1,2,5+6
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92757074001 2380060 2380060MW-13B 8151A EPA 8151A
92757074002 2380060 2380060MW-14B 8151A EPA 8151A
92757074001 886992 887021MW-13B EPA 3510C EPA 8081B
92757074002 886992 887021MW-14B EPA 3510C EPA 8081B
92757074001 887010 887023MW-13B EPA 3510C EPA 8082A
92757074002 887010 887023MW-14B EPA 3510C EPA 8082A
92757074001 1048973 1049051MW-13B EPA 3010 EPA 6010
92757074002 1048973 1049051MW-14B EPA 3010 EPA 6010
92757074001 1048974 1049052MW-13B EPA 3010 EPA 6020
92757074002 1048974 1049052MW-14B EPA 3010 EPA 6020
92757074001 1049808 1049843MW-13B EPA 7470 EPA 7470
92757074002 1049808 1049843MW-14B EPA 7470 EPA 7470
92757074001 886988 887028MW-13B EPA 3510C EPA 8270E
92757074002 886988 887028MW-14B EPA 3510C EPA 8270E
92757074001 888074MW-13B EPA 8260D
92757074002 888074MW-14B EPA 8260D
92757074001 887074MW-13B EPA 8260D Mod.
92757074002 887074MW-14B EPA 8260D Mod.
92757074001 887565MW-13B SM 4500-S2D-2011
92757074002 887565MW-14B SM 4500-S2D-2011
92757074001 1048509 1048637MW-13B EPA 335.4 EPA 335.4
92757074002 1048509 1048637MW-14B EPA 335.4 EPA 335.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2024 11:11 AM
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[phone]
Page 46 of 49
Page 47 of 49
Page 48 of 49
Page 49 of 49
#=CL#
October 25, 2024
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92756908
92756908
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services, Inc.
68 Shipwash Dr.
Garner, NC 27529
Iredell SW2_6
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on October 03, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole D'Oleo
[e-mail]
Project Manager
[phone]
Enclosures
cc:Accounts Payable, Municipal Engineering Services, Inc.
Jonathan Pfohl, Municipal Engineering Services
Jay Zimmerman, PG, Municipal Engineering Services, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92756908
Iredell SW2_6
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
California Certification# 3096
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Utah
Utah FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92756908
Iredell SW2_6
Lab ID Sample ID Matrix Date Collected Date Received
92756908001 SW-2 Water 10/02/24 05:26 10/03/24 13:50
92756908002 SW-6 Water 10/02/24 04:30 10/03/24 13:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92756908
Iredell SW2_6
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92756908001 SW-2 EPA 6020 15 PASI-OBSL
EPA 8260D 51 PASI-CTMH
92756908002 SW-6 EPA 6020 15 PASI-OBSL
EPA 8260D 51 PASI-CTMH
PASI-C = Pace Analytical Services - Charlotte
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756908
Iredell SW2_6
Sample:SW-2 Lab ID:92756908001 Collected:10/02/24 05:26 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/22/24 22:50 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic ND ug/L 10/22/24 22:50 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 27.3 ug/L 10/22/24 22:50 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium ND ug/L 10/22/24 22:50 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium ND ug/L 10/22/24 22:50 7440-43-9 1g10/16/24 06:070.10 0.067 1
Chromium 0.73J ug/L 10/22/24 22:50 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt 0.42J ug/L 10/22/24 22:50 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper 1.1 ug/L 10/22/24 22:50 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead ND ug/L 10/22/24 22:50 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel 0.61J ug/L 10/22/24 22:50 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium ND ug/L 10/22/24 22:50 7782-49-2 1g,CU10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/22/24 22:50 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/22/24 22:50 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 1.4 ug/L 10/22/24 22:50 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc 7.6J ug/L 10/22/24 22:50 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/09/24 05:21 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/09/24 05:21 107-13-110.0 1.8 1
Benzene ND ug/L 10/09/24 05:21 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/09/24 05:21 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/09/24 05:21 75-27-41.0 0.31 1
Bromoform ND ug/L 10/09/24 05:21 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/09/24 05:21 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 10/09/24 05:21 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/09/24 05:21 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/09/24 05:21 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/09/24 05:21 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/09/24 05:21 75-00-31.0 0.65 1
Chloroform ND ug/L 10/09/24 05:21 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/09/24 05:21 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/24 05:21 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/09/24 05:21 124-48-11.0 0.36 1
Dibromomethane ND ug/L 10/09/24 05:21 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/09/24 05:21 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/09/24 05:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/09/24 05:21 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/09/24 05:21 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/09/24 05:21 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/09/24 05:21 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/09/24 05:21 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/09/24 05:21 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/09/24 05:21 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/09/24 05:21 10061-01-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/25/2024 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756908
Iredell SW2_6
Sample:SW-2 Lab ID:92756908001 Collected:10/02/24 05:26 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 10/09/24 05:21 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/09/24 05:21 123-91-115038.7 1
Ethylbenzene ND ug/L 10/09/24 05:21 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/09/24 05:21 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/09/24 05:21 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/09/24 05:21 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/24 05:21 108-10-15.0 2.7 1
Styrene ND ug/L 10/09/24 05:21 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/24 05:21 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/24 05:21 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/09/24 05:21 127-18-41.0 0.29 1
Tetrahydrofuran ND ug/L 10/09/24 05:21 109-99-910.0 3.5 1
Toluene ND ug/L 10/09/24 05:21 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/09/24 05:21 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/09/24 05:21 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/09/24 05:21 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/09/24 05:21 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/09/24 05:21 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/09/24 05:21 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 10/09/24 05:21 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/09/24 05:21 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %10/09/24 05:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %10/09/24 05:21 17060-07-070-130 1
Toluene-d8 (S)98 %10/09/24 05:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/25/2024 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756908
Iredell SW2_6
Sample:SW-6 Lab ID:92756908002 Collected:10/02/24 04:30 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020 Preparation Method: EPA 3010
Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Antimony ND ug/L 10/22/24 22:52 7440-36-0 1g10/16/24 06:071.0 0.50 1
Arsenic ND ug/L 10/22/24 22:52 7440-38-2 1g10/16/24 06:071.0 0.50 1
Barium 66.2 ug/L 10/22/24 22:52 7440-39-3 1g10/16/24 06:071.0 0.50 1
Beryllium 0.038J ug/L 10/22/24 22:52 7440-41-7 1g10/16/24 06:070.10 0.033 1
Cadmium ND ug/L 10/22/24 22:52 7440-43-9 1g10/16/24 06:070.10 0.067 1
Chromium 1.3 ug/L 10/22/24 22:52 7440-47-3 1g10/16/24 06:071.0 0.50 1
Cobalt ND ug/L 10/22/24 22:52 7440-48-4 1g10/16/24 06:071.0 0.24 1
Copper ND ug/L 10/22/24 22:52 7440-50-8 1g10/16/24 06:071.0 0.42 1
Lead ND ug/L 10/22/24 22:52 7439-92-1 1g10/16/24 06:071.0 0.22 1
Nickel ND ug/L 10/22/24 22:52 7440-02-0 1g10/16/24 06:071.0 0.26 1
Selenium ND ug/L 10/22/24 22:52 7782-49-2 1g,CU10/16/24 06:072.0 0.20 1
Silver ND ug/L 10/22/24 22:52 7440-22-4 1g10/16/24 06:070.50 0.028 1
Thallium ND ug/L 10/22/24 22:52 7440-28-0 1g10/16/24 06:071.0 0.11 1
Vanadium 2.6 ug/L 10/22/24 22:52 7440-62-2 1g10/16/24 06:071.0 0.91 1
Zinc ND ug/L 10/22/24 22:52 7440-66-6 1g10/16/24 06:0710.0 6.7 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/09/24 07:32 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/09/24 07:32 107-13-110.0 1.8 1
Benzene ND ug/L 10/09/24 07:32 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/09/24 07:32 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/09/24 07:32 75-27-41.0 0.31 1
Bromoform ND ug/L 10/09/24 07:32 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/09/24 07:32 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 10/09/24 07:32 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/09/24 07:32 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/09/24 07:32 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/09/24 07:32 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/09/24 07:32 75-00-31.0 0.65 1
Chloroform ND ug/L 10/09/24 07:32 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/09/24 07:32 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/24 07:32 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/09/24 07:32 124-48-11.0 0.36 1
Dibromomethane ND ug/L 10/09/24 07:32 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/09/24 07:32 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/09/24 07:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/09/24 07:32 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/09/24 07:32 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/09/24 07:32 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/09/24 07:32 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/09/24 07:32 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/09/24 07:32 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/09/24 07:32 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/09/24 07:32 10061-01-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/25/2024 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756908
Iredell SW2_6
Sample:SW-6 Lab ID:92756908002 Collected:10/02/24 04:30 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 10/09/24 07:32 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/09/24 07:32 123-91-115038.7 1
Ethylbenzene ND ug/L 10/09/24 07:32 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/09/24 07:32 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/09/24 07:32 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/09/24 07:32 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/24 07:32 108-10-15.0 2.7 1
Styrene ND ug/L 10/09/24 07:32 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/24 07:32 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/24 07:32 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/09/24 07:32 127-18-41.0 0.29 1
Tetrahydrofuran ND ug/L 10/09/24 07:32 109-99-910.0 3.5 1
Toluene ND ug/L 10/09/24 07:32 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/09/24 07:32 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/09/24 07:32 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/09/24 07:32 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/09/24 07:32 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/09/24 07:32 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/09/24 07:32 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 10/09/24 07:32 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/09/24 07:32 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %10/09/24 07:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/09/24 07:32 17060-07-070-130 1
Toluene-d8 (S)99 %10/09/24 07:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/25/2024 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756908
Iredell SW2_6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1048094
EPA 3010
EPA 6020
6020 MET
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92756908001, 92756908002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5762053
Associated Lab Samples:92756908001, 92756908002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 1.0 1g10/24/24 10:240.50
Arsenic ug/L ND 1.0 1g10/24/24 10:240.50
Barium ug/L ND 1.0 1g10/24/24 10:240.50
Beryllium ug/L ND 0.10 1g10/24/24 10:240.033
Cadmium ug/L 0.11 0.10 1g10/24/24 10:240.067
Chromium ug/L ND 1.0 1g10/24/24 10:240.50
Cobalt ug/L ND 1.0 1g10/24/24 10:240.24
Copper ug/L ND 1.0 1g10/24/24 10:240.42
Lead ug/L ND 1.0 1g10/24/24 10:240.22
Nickel ug/L ND 1.0 1g10/24/24 10:240.26
Selenium ug/L ND 2.0 1g10/24/24 10:240.20
Silver ug/L ND 0.50 1g10/24/24 10:240.028
Thallium ug/L ND 1.0 1g10/24/24 10:240.11
Vanadium ug/L ND 1.0 1g10/24/24 10:240.91
Zinc ug/L ND 10.0 1g10/24/24 10:246.7
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5762054LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 54.3 1g5010980-120
Arsenic ug/L 50.3 1g5010180-120
Barium ug/L 55.5 1g5011180-120
Beryllium ug/L 5.4 1g510880-120
Cadmium ug/L 5.6 1g511280-120
Chromium ug/L 53.0 1g5010680-120
Cobalt ug/L 57.0 1g5011480-120
Copper ug/L 53.4 1g5010780-120
Lead ug/L 52.1 1g5010480-120
Nickel ug/L 52.4 1g5010580-120
Selenium ug/L 53.6 1g5010780-120
Silver ug/L 5.8 1g511680-120
Thallium ug/L 56.1 1g5011280-120
Vanadium ug/L 53.2 1g5010680-120
Zinc ug/L 253 1g25010180-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/25/2024 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756908
Iredell SW2_6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5762055MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35911307005
5762056
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 1g5010775-125108 0 20500.50U 53.7 53.8
Arsenic ug/L 1g5011375-125113 0 20500.50U 56.7 56.7
Barium ug/L 1g5010875-125110 1 205010.5 64.8 65.3
Beryllium ug/L 1g511175-125111 0 2050.033U 5.6 5.6
Cadmium ug/L 1g511175-125112 1 2050.067U 5.6 5.6
Chromium ug/L 1g5011275-125111 1 20500.50U 56.4 55.9
Cobalt ug/L 1g5011275-125113 1 20500.24U 56.3 56.9
Copper ug/L 1g5011375-125113 0 20500.42U 56.9 56.9
Lead ug/L 1g5011175-125110 1 20500.22U 55.6 55.3
Nickel ug/L 1g,CH5011775-125116 0 20500.26U 58.6 58.4
Selenium ug/L 1g,CH5011375-125113 0 20500.62J 57.2 57.1
Silver ug/L 1g511575-125116 1 2050.028U 5.8 5.8
Thallium ug/L 1g5011275-125112 0 20500.11U 55.8 55.8
Vanadium ug/L 1g5010975-125108 2 20500.91U 54.9 54.1
Zinc ug/L 1g25010675-125108 1 202506.7U 266 270
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/25/2024 02:30 PM
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Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756908
Iredell SW2_6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
887486
EPA 8260D
EPA 8260D
8260D MSV Low Level Landfill
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92756908001, 92756908002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4570450
Associated Lab Samples:92756908001, 92756908002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/09/24 02:320.31
1,1,1-Trichloroethane ug/L ND 1.0 10/09/24 02:320.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/09/24 02:320.22
1,1,2-Trichloroethane ug/L ND 1.0 10/09/24 02:320.32
1,1-Dichloroethane ug/L ND 1.0 10/09/24 02:320.37
1,1-Dichloroethene ug/L ND 1.0 10/09/24 02:320.35
1,2,3-Trichloropropane ug/L ND 1.0 10/09/24 02:320.26
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/09/24 02:320.34
1,2-Dichlorobenzene ug/L ND 1.0 10/09/24 02:320.34
1,2-Dichloroethane ug/L ND 1.0 10/09/24 02:320.32
1,2-Dichloropropane ug/L ND 1.0 10/09/24 02:320.36
1,4-Dichlorobenzene ug/L ND 1.0 10/09/24 02:320.33
1,4-Dioxane (p-Dioxane)ug/L ND 150 10/09/24 02:3238.7
2-Butanone (MEK)ug/L ND 5.0 10/09/24 02:324.0
2-Hexanone ug/L ND 5.0 10/09/24 02:320.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/09/24 02:322.7
Acetone ug/L ND 25.0 10/09/24 02:325.1
Acrylonitrile ug/L ND 10.0 10/09/24 02:321.8
Benzene ug/L ND 1.0 10/09/24 02:320.34
Bromochloromethane ug/L ND 1.0 10/09/24 02:320.47
Bromodichloromethane ug/L ND 1.0 10/09/24 02:320.31
Bromoform ug/L ND 1.0 10/09/24 02:320.34
Bromomethane ug/L ND 2.0 v210/09/24 02:321.7
Carbon disulfide ug/L ND 2.0 10/09/24 02:320.36
Carbon tetrachloride ug/L ND 1.0 10/09/24 02:320.33
Chlorobenzene ug/L ND 1.0 10/09/24 02:320.28
Chloroethane ug/L ND 1.0 10/09/24 02:320.65
Chloroform ug/L ND 1.0 10/09/24 02:320.43
Chloromethane ug/L ND 1.0 10/09/24 02:320.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/09/24 02:320.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/09/24 02:320.36
Dibromochloromethane ug/L ND 1.0 10/09/24 02:320.36
Dibromomethane ug/L ND 1.0 10/09/24 02:320.39
Ethylbenzene ug/L ND 1.0 10/09/24 02:320.30
Iodomethane ug/L ND 20.0 v210/09/24 02:329.7
Methylene Chloride ug/L ND 5.0 10/09/24 02:322.0
Styrene ug/L ND 1.0 10/09/24 02:320.29
Tetrachloroethene ug/L ND 1.0 10/09/24 02:320.29
Tetrahydrofuran ug/L ND 10.0 10/09/24 02:323.5
Toluene ug/L ND 1.0 10/09/24 02:320.24
REPORT OF LABORATORY ANALYSIS
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Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756908
Iredell SW2_6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4570450
Associated Lab Samples:92756908001, 92756908002
Matrix:Water
AnalyzedMDL
trans-1,2-Dichloroethene ug/L ND 1.0 10/09/24 02:320.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/09/24 02:320.36
trans-1,4-Dichloro-2-butene ug/L ND 1.0 v210/09/24 02:320.56
Trichloroethene ug/L ND 1.0 10/09/24 02:320.38
Trichlorofluoromethane ug/L ND 1.0 10/09/24 02:320.30
Vinyl acetate ug/L ND 2.0 10/09/24 02:321.3
Vinyl chloride ug/L ND 1.0 10/09/24 02:320.39
Xylene (Total)ug/L ND 1.0 10/09/24 02:320.34
1,2-Dichloroethane-d4 (S)%93 70-130 10/09/24 02:32
4-Bromofluorobenzene (S)%98 70-130 10/09/24 02:32
Toluene-d8 (S)%98 70-130 10/09/24 02:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4570451LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.720 103 70-130
1,1,1-Trichloroethane ug/L 18.020 90 70-130
1,1,2,2-Tetrachloroethane ug/L 19.520 98 70-130
1,1,2-Trichloroethane ug/L 19.120 95 70-130
1,1-Dichloroethane ug/L 18.220 91 70-130
1,1-Dichloroethene ug/L 17.620 88 69-131
1,2,3-Trichloropropane ug/L 20.420 102 70-130
1,2-Dibromo-3-chloropropane ug/L 18.920 95 70-130
1,2-Dichlorobenzene ug/L 20.220 101 70-130
1,2-Dichloroethane ug/L 18.520 92 70-130
1,2-Dichloropropane ug/L 18.720 93 70-130
1,4-Dichlorobenzene ug/L 19.820 99 70-130
1,4-Dioxane (p-Dioxane)ug/L 377400 94 70-132
2-Butanone (MEK)ug/L 31.940 80 67-133
2-Hexanone ug/L 34.940 87 70-133
4-Methyl-2-pentanone (MIBK)ug/L 34.340 86 70-130
Acetone ug/L 34.040 85 67-130
Acrylonitrile ug/L 88.3100 88 70-130
Benzene ug/L 19.020 95 70-130
Bromochloromethane ug/L 20.420 102 70-130
Bromodichloromethane ug/L 19.020 95 70-130
Bromoform ug/L 19.420 97 70-133
Bromomethane ug/L 13.0 v3206541-148
Carbon disulfide ug/L 17.420 87 70-131
Carbon tetrachloride ug/L 18.520 93 70-130
Chlorobenzene ug/L 19.620 98 70-130
Chloroethane ug/L 17.020 85 41-157
Chloroform ug/L 17.720 88 70-130
Chloromethane ug/L 17.420 87 59-141
REPORT OF LABORATORY ANALYSIS
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Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756908
Iredell SW2_6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4570451LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 18.220 91 70-130
cis-1,3-Dichloropropene ug/L 19.220 96 70-130
Dibromochloromethane ug/L 20.120 100 70-130
Dibromomethane ug/L 20.120 101 70-130
Ethylbenzene ug/L 19.720 98 70-130
Iodomethane ug/L 33.2 v3408357-140
Methylene Chloride ug/L 17.420 87 62-130
Styrene ug/L 20.320 102 70-130
Tetrachloroethene ug/L 19.920 99 70-130
Tetrahydrofuran ug/L 168200 84 70-131
Toluene ug/L 19.120 96 70-130
trans-1,2-Dichloroethene ug/L 18.420 92 70-130
trans-1,3-Dichloropropene ug/L 19.520 97 70-130
trans-1,4-Dichloro-2-butene ug/L 19.8 v3209957-149
Trichloroethene ug/L 19.420 97 70-130
Trichlorofluoromethane ug/L 17.320 86 57-130
Vinyl acetate ug/L 36.540 91 70-141
Vinyl chloride ug/L 19.120 95 66-140
Xylene (Total)ug/L 61.760 103 70-130
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4570452MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92756775012
4570453
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 127 70-146133 4 3020ND25.4 26.5
1,1,1-Trichloroethane ug/L 20 137 70-150137 0 3020ND27.4 27.5
1,1,2,2-Tetrachloroethane ug/L 20 116 66-144126 9 3020ND23.1 25.2
1,1,2-Trichloroethane ug/L 20 129 70-142136 5 3020ND25.8 27.2
1,1-Dichloroethane ug/L 20 147 68-150149 2 3020ND29.3 29.9
1,1-Dichloroethene ug/L 20 152 64-162160 5 3020ND30.4 32.0
1,2,3-Trichloropropane ug/L 20 118 66-144129 9 3020ND23.6 25.8
1,2-Dibromo-3-
chloropropane ug/L 20 119 62-146127 6 3020ND23.8 25.4
1,2-Dichlorobenzene ug/L 20 118 70-142120 1 3020ND23.7 24.0
1,2-Dichloroethane ug/L M12014268-145150 5 3020ND28.4 30.0
1,2-Dichloropropane ug/L M12014670-144151 4 3020ND29.2 30.3
1,4-Dichlorobenzene ug/L 20 119 70-140118 0 3020ND23.8 23.7
1,4-Dioxane (p-Dioxane)ug/L 400 133 66-151127 5 30400ND532508
2-Butanone (MEK)ug/L 40 125 57-156144 14 3040ND50.1 57.6
2-Hexanone ug/L 40 121 62-153128 5 3040ND48.5 51.1
4-Methyl-2-pentanone
(MIBK)ug/L 40 119 65-144128 7 3040ND47.7 51.3
Acetone ug/L 40 118 49-162129 9 3040ND47.2 51.6
REPORT OF LABORATORY ANALYSIS
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Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756908
Iredell SW2_6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4570452MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92756775012
4570453
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acrylonitrile ug/L 100 123 59-155132 6 30100ND123132
Benzene ug/L M12014568-144154 6 3020ND29.0 30.9
Bromochloromethane ug/L 20 120 70-148131 9 3020ND24.0 26.2
Bromodichloromethane ug/L 20 137 70-141140 2 3020ND27.5 28.0
Bromoform ug/L 20 125 59-144122 3 3020ND25.0 24.4
Bromomethane ug/L 20 102 23-190114 11 3020ND20.5 22.8
Carbon disulfide ug/L 20 134 64-160138 4 3020ND26.7 27.7
Carbon tetrachloride ug/L 20 141 70-147145 3 3020ND28.2 29.0
Chlorobenzene ug/L 20 127 70-143131 4 3020ND25.3 26.2
Chloroethane ug/L 20 130 55-190139 6 3020ND26.1 27.7
Chloroform ug/L M12013567-148149 10 3020ND26.9 29.7
Chloromethane ug/L 20 135 38-180138 2 3020ND27.1 27.6
cis-1,2-Dichloroethene ug/L 20 144 67-151146 1 3020ND28.8 29.1
cis-1,3-Dichloropropene ug/L 20 130 70-142139 7 3020ND26.0 27.8
Dibromochloromethane ug/L 20 126 68-140132 5 3020ND25.1 26.3
Dibromomethane ug/L 20 123 70-142131 7 3020ND24.6 26.3
Ethylbenzene ug/L 20 126 70-145129 3 3020ND25.1 25.9
Iodomethane ug/L v3409337-160103 10 3040ND37.3 41.3
Methylene Chloride ug/L 20 135 54-149145 7 3020ND27.0 28.9
Styrene ug/L 20 124 70-147126 1 3020ND24.9 25.1
Tetrachloroethene ug/L 20 120 70-145121 1 3020ND24.0 24.3
Tetrahydrofuran ug/L 200 127 48-160133 5 30200ND254266
Toluene ug/L 20 132 65-146139 5 3020ND26.3 27.7
trans-1,2-Dichloroethene ug/L 20 147 69-155153 4 3020ND29.4 30.6
trans-1,3-Dichloropropene ug/L 20 123 70-142132 7 3020ND24.5 26.4
trans-1,4-Dichloro-2-butene ug/L 20 147 39-149123 18 3020ND29.4 24.5
Trichloroethene ug/L 20 142 70-152147 3 3020ND28.3 29.3
Trichlorofluoromethane ug/L 20 141 60-158151 7 3020ND28.1 30.2
Vinyl acetate ug/L 40 129 56-157142 10 3040ND51.5 56.8
Vinyl chloride ug/L 20 140 51-178149 6 3020ND27.9 29.7
Xylene (Total)ug/L 60 123 70-146128 4 3060ND73.6 76.8
1,2-Dichloroethane-d4 (S)%104 70-130105
4-Bromofluorobenzene (S)%99 70-13098
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
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Page 14 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92756908
Iredell SW2_6
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
BATCH QUALIFIERS
Batch: 1048296
Samples 92756911001, 92754732012, 92756913-(2, 4, 5, 6, 7, 10, 11) were sent back to reprep for Cd hit in blank[1]
ANALYTE QUALIFIERS
Samples 92756911001, 92754732012, 92756913-(2, 4, 5, 6, 7, 10, 11) were sent back to reprep for Cd hit in blank1g
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.CH
The continuing calibration for this analyte is above laboratory acceptance limits. Analyte was not detected above the
reporting limit in any of the associated samples.CU
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/25/2024 02:30 PM
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Page 15 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92756908
Iredell SW2_6
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92756908001 1048094 1048296SW-2 EPA 3010 EPA 6020
92756908002 1048094 1048296SW-6 EPA 3010 EPA 6020
92756908001 887486SW-2 EPA 8260D
92756908002 887486SW-6 EPA 8260D
REPORT OF LABORATORY ANALYSIS
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Page 16 of 19
Page 17 of 19
Page 18 of 19
Page 19 of 19
#=CL#
October 21, 2024
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92756912
92756912
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services, Inc.
68 Shipwash Dr.
Garner, NC 27529
Iredell Background
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on October 03, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole D'Oleo
[e-mail]
Project Manager
[phone]
Enclosures
cc:Accounts Payable, Municipal Engineering Services, Inc.
Jonathan Pfohl, Municipal Engineering Services
Jay Zimmerman, PG, Municipal Engineering Services, Inc.
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 1 of 20
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92756912
Iredell Background
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 20
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92756912
Iredell Background
Lab ID Sample ID Matrix Date Collected Date Received
92756912001 MW-32 Water 10/02/24 14:12 10/03/24 13:50
92756912002 MW-37 Water 10/02/24 13:57 10/03/24 13:50
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92756912
Iredell Background
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92756912001 MW-32 EPA 6020B 15 PASI-AKRL
EPA 8260D 51 PASI-CTMH
92756912002 MW-37 EPA 6020B 15 PASI-AKRL
EPA 8260D 51 PASI-CTMH
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756912
Iredell Background
Sample:MW-32 Lab ID:92756912001 Collected:10/02/24 14:12 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Antimony ND ug/L 10/20/24 19:46 7440-36-010/18/24 16:301.0 0.10 1
Arsenic 0.20J ug/L 10/20/24 19:46 7440-38-210/18/24 16:301.0 0.17 1
Barium 62.2 ug/L 10/20/24 19:46 7440-39-310/18/24 16:301.0 0.36 1
Beryllium 0.19 ug/L 10/20/24 19:46 7440-41-710/18/24 16:300.10 0.045 1
Cadmium 0.22 ug/L 10/20/24 19:46 7440-43-910/18/24 16:300.10 0.037 1
Chromium 2.2 ug/L 10/20/24 19:46 7440-47-310/18/24 16:301.0 0.39 1
Cobalt 3.7 ug/L 10/20/24 19:46 7440-48-410/18/24 16:301.0 0.14 1
Copper 2.1 ug/L 10/20/24 19:46 7440-50-810/18/24 16:302.0 0.55 1
Lead 0.98J ug/L 10/20/24 19:46 7439-92-110/18/24 16:301.0 0.18 1
Nickel 1.5 ug/L 10/20/24 19:46 7440-02-010/18/24 16:301.0 0.26 1
Selenium ND ug/L 10/20/24 19:46 7782-49-210/18/24 16:302.0 0.22 1
Silver ND ug/L 10/20/24 19:46 7440-22-410/18/24 16:300.40 0.046 1
Thallium 0.032J ug/L 10/20/24 19:46 7440-28-010/18/24 16:300.20 0.028 1
Vanadium 4.6 ug/L 10/20/24 19:46 7440-62-210/18/24 16:301.0 0.064 1
Zinc 6.9J ug/L 10/20/24 19:46 7440-66-610/18/24 16:3010.0 0.93 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/11/24 15:59 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/11/24 15:59 107-13-110.0 1.8 1
Benzene ND ug/L 10/11/24 15:59 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/11/24 15:59 74-97-5 M11.0 0.47 1
Bromodichloromethane ND ug/L 10/11/24 15:59 75-27-4 M11.0 0.31 1
Bromoform ND ug/L 10/11/24 15:59 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/11/24 15:59 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 10/11/24 15:59 78-93-3 M15.0 4.0 1
Carbon disulfide ND ug/L 10/11/24 15:59 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/11/24 15:59 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/11/24 15:59 108-90-7 M11.0 0.28 1
Chloroethane ND ug/L 10/11/24 15:59 75-00-31.0 0.65 1
Chloroform ND ug/L 10/11/24 15:59 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/11/24 15:59 74-87-3 v21.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/11/24 15:59 96-12-8 M12.0 0.34 1
Dibromochloromethane ND ug/L 10/11/24 15:59 124-48-1 M11.0 0.36 1
Dibromomethane ND ug/L 10/11/24 15:59 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/11/24 15:59 95-50-1 M11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/11/24 15:59 106-46-7 M11.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/11/24 15:59 110-57-61.0 0.56 1
1,1-Dichloroethane ND ug/L 10/11/24 15:59 75-34-3 M11.0 0.37 1
1,2-Dichloroethane ND ug/L 10/11/24 15:59 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/11/24 15:59 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/11/24 15:59 156-59-2 M11.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/11/24 15:59 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/11/24 15:59 78-87-5 M11.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/11/24 15:59 10061-01-5 M11.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2024 02:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756912
Iredell Background
Sample:MW-32 Lab ID:92756912001 Collected:10/02/24 14:12 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 10/11/24 15:59 10061-02-6 M11.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/11/24 15:59 123-91-1 M115038.7 1
Ethylbenzene ND ug/L 10/11/24 15:59 100-41-4 M11.0 0.30 1
2-Hexanone ND ug/L 10/11/24 15:59 591-78-6 M1,v25.0 0.48 1
Iodomethane ND ug/L 10/11/24 15:59 74-88-4 L2,v220.0 9.7 1
Methylene Chloride ND ug/L 10/11/24 15:59 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/11/24 15:59 108-10-1 M15.0 2.7 1
Styrene ND ug/L 10/11/24 15:59 100-42-5 M11.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/11/24 15:59 630-20-6 M11.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/11/24 15:59 79-34-5 M11.0 0.22 1
Tetrachloroethene ND ug/L 10/11/24 15:59 127-18-4 M11.0 0.29 1
Tetrahydrofuran ND ug/L 10/11/24 15:59 109-99-910.0 3.5 1
Toluene ND ug/L 10/11/24 15:59 108-88-3 M11.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/11/24 15:59 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/11/24 15:59 79-00-5 M11.0 0.32 1
Trichloroethene ND ug/L 10/11/24 15:59 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/11/24 15:59 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/11/24 15:59 96-18-4 M11.0 0.26 1
Vinyl acetate ND ug/L 10/11/24 15:59 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 10/11/24 15:59 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/11/24 15:59 1330-20-7 MS1.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %10/11/24 15:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %10/11/24 15:59 17060-07-070-130 1
Toluene-d8 (S)103 %10/11/24 15:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2024 02:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756912
Iredell Background
Sample:MW-37 Lab ID:92756912002 Collected:10/02/24 13:57 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Antimony ND ug/L 10/20/24 20:13 7440-36-010/18/24 16:301.0 0.10 1
Arsenic ND ug/L 10/20/24 20:13 7440-38-210/18/24 16:301.0 0.17 1
Barium 84.4 ug/L 10/20/24 20:13 7440-39-310/18/24 16:301.0 0.36 1
Beryllium 0.10 ug/L 10/20/24 20:13 7440-41-710/18/24 16:300.10 0.045 1
Cadmium 0.26 ug/L 10/20/24 20:13 7440-43-910/18/24 16:300.10 0.037 1
Chromium 0.42J ug/L 10/20/24 20:13 7440-47-310/18/24 16:301.0 0.39 1
Cobalt 1.2 ug/L 10/20/24 20:13 7440-48-410/18/24 16:301.0 0.14 1
Copper ND ug/L 10/20/24 20:13 7440-50-810/18/24 16:302.0 0.55 1
Lead ND ug/L 10/20/24 20:13 7439-92-110/18/24 16:301.0 0.18 1
Nickel 0.78J ug/L 10/20/24 20:13 7440-02-010/18/24 16:301.0 0.26 1
Selenium ND ug/L 10/20/24 20:13 7782-49-210/18/24 16:302.0 0.22 1
Silver ND ug/L 10/20/24 20:13 7440-22-410/18/24 16:300.40 0.046 1
Thallium 0.071J ug/L 10/20/24 20:13 7440-28-010/18/24 16:300.20 0.028 1
Vanadium ND ug/L 10/20/24 20:13 7440-62-210/18/24 16:301.0 0.064 1
Zinc 4.8J ug/L 10/20/24 20:13 7440-66-610/18/24 16:3010.0 0.93 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/11/24 16:17 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/11/24 16:17 107-13-110.0 1.8 1
Benzene ND ug/L 10/11/24 16:17 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/11/24 16:17 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/11/24 16:17 75-27-41.0 0.31 1
Bromoform ND ug/L 10/11/24 16:17 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/11/24 16:17 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 10/11/24 16:17 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/11/24 16:17 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/11/24 16:17 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/11/24 16:17 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/11/24 16:17 75-00-31.0 0.65 1
Chloroform ND ug/L 10/11/24 16:17 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/11/24 16:17 74-87-3 v21.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/11/24 16:17 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/11/24 16:17 124-48-11.0 0.36 1
Dibromomethane ND ug/L 10/11/24 16:17 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/11/24 16:17 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/11/24 16:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/11/24 16:17 110-57-61.0 0.56 1
1,1-Dichloroethane ND ug/L 10/11/24 16:17 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/11/24 16:17 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/11/24 16:17 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/11/24 16:17 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/11/24 16:17 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/11/24 16:17 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/11/24 16:17 10061-01-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2024 02:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92756912
Iredell Background
Sample:MW-37 Lab ID:92756912002 Collected:10/02/24 13:57 Received:10/03/24 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 10/11/24 16:17 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/11/24 16:17 123-91-115038.7 1
Ethylbenzene ND ug/L 10/11/24 16:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/11/24 16:17 591-78-6 v25.0 0.48 1
Iodomethane ND ug/L 10/11/24 16:17 74-88-4 L2,v220.0 9.7 1
Methylene Chloride ND ug/L 10/11/24 16:17 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/11/24 16:17 108-10-15.0 2.7 1
Styrene ND ug/L 10/11/24 16:17 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/11/24 16:17 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/11/24 16:17 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/11/24 16:17 127-18-41.0 0.29 1
Tetrahydrofuran ND ug/L 10/11/24 16:17 109-99-910.0 3.5 1
Toluene ND ug/L 10/11/24 16:17 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/11/24 16:17 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/11/24 16:17 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/11/24 16:17 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/11/24 16:17 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/11/24 16:17 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/11/24 16:17 108-05-42.0 1.3 1
Vinyl chloride 0.56J ug/L 10/11/24 16:17 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/11/24 16:17 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)101 %10/11/24 16:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/11/24 16:17 17060-07-070-130 1
Toluene-d8 (S)103 %10/11/24 16:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2024 02:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756912
Iredell Background
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
889904
EPA 3010A
EPA 6020B
6020 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92756912001, 92756912002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4582404
Associated Lab Samples:92756912001, 92756912002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 1.0 10/20/24 19:380.10
Arsenic ug/L ND 1.0 10/20/24 19:380.17
Barium ug/L ND 1.0 10/20/24 19:380.36
Beryllium ug/L ND 0.10 10/20/24 19:380.045
Cadmium ug/L ND 0.10 10/20/24 19:380.037
Chromium ug/L ND 1.0 10/20/24 19:380.39
Cobalt ug/L ND 1.0 10/20/24 19:380.14
Copper ug/L ND 2.0 10/20/24 19:380.55
Lead ug/L ND 1.0 10/20/24 19:380.18
Nickel ug/L ND 1.0 10/20/24 19:380.26
Selenium ug/L ND 2.0 10/20/24 19:380.22
Silver ug/L ND 0.40 10/20/24 19:380.046
Thallium ug/L ND 0.20 10/20/24 19:380.028
Vanadium ug/L ND 1.0 10/20/24 19:380.064
Zinc ug/L ND 10.0 10/20/24 19:380.93
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4582405LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 50.350 101 80-120
Arsenic ug/L 50.150 100 80-120
Barium ug/L 50.450 101 80-120
Beryllium ug/L 50.950 102 80-120
Cadmium ug/L 52.550 105 80-120
Chromium ug/L 52.750 105 80-120
Cobalt ug/L 52.050 104 80-120
Copper ug/L 53.550 107 80-120
Lead ug/L 53.450 107 80-120
Nickel ug/L 53.550 107 80-120
Selenium ug/L 50.450 101 80-120
Silver ug/L 25.725 103 80-120
Thallium ug/L 26.325 105 80-120
Vanadium ug/L 53.550 107 80-120
Zinc ug/L 51.850 104 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2024 02:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756912
Iredell Background
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4582406MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92756912001
4582407
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 50 95 75-12597 2 2050ND47.7 48.5
Arsenic ug/L 50 99 75-125101 2 20500.20J 49.8 50.8
Barium ug/L 50 103 75-12594 4 205062.2 114 109
Beryllium ug/L 50 102 75-125102 0 20500.19 51.2 51.3
Cadmium ug/L 50 103 75-125104 2 20500.22 51.6 52.4
Chromium ug/L 50 106 75-125105 1 20502.2 55.2 54.7
Cobalt ug/L 50 105 75-125105 0 20503.7 56.0 56.0
Copper ug/L 50 109 75-125108 1 20502.1 56.5 55.9
Lead ug/L 50 103 75-125103 1 20500.98J 52.4 52.7
Nickel ug/L 50 107 75-125107 0 20501.5 55.3 55.1
Selenium ug/L 50 103 75-125101 1 2050ND51.3 50.8
Silver ug/L 25 101 75-125102 1 2025ND25.2 25.5
Thallium ug/L 25 104 75-125104 1 20250.032J 25.9 26.1
Vanadium ug/L 50 106 75-125105 1 20504.6 57.5 57.0
Zinc ug/L 50 102 75-125103 1 20506.9J 57.7 58.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2024 02:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756912
Iredell Background
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
888072
EPA 8260D
EPA 8260D
8260D MSV Low Level Landfill
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92756912001, 92756912002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4573319
Associated Lab Samples:92756912001, 92756912002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/11/24 13:550.31
1,1,1-Trichloroethane ug/L ND 1.0 10/11/24 13:550.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/11/24 13:550.22
1,1,2-Trichloroethane ug/L ND 1.0 10/11/24 13:550.32
1,1-Dichloroethane ug/L ND 1.0 10/11/24 13:550.37
1,1-Dichloroethene ug/L ND 1.0 10/11/24 13:550.35
1,2,3-Trichloropropane ug/L ND 1.0 10/11/24 13:550.26
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/11/24 13:550.34
1,2-Dichlorobenzene ug/L ND 1.0 10/11/24 13:550.34
1,2-Dichloroethane ug/L ND 1.0 10/11/24 13:550.32
1,2-Dichloropropane ug/L ND 1.0 10/11/24 13:550.36
1,4-Dichlorobenzene ug/L ND 1.0 10/11/24 13:550.33
1,4-Dioxane (p-Dioxane)ug/L ND 150 10/11/24 13:5538.7
2-Butanone (MEK)ug/L ND 5.0 10/11/24 13:554.0
2-Hexanone ug/L ND 5.0 v210/11/24 13:550.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/11/24 13:552.7
Acetone ug/L ND 25.0 10/11/24 13:555.1
Acrylonitrile ug/L ND 10.0 10/11/24 13:551.8
Benzene ug/L ND 1.0 10/11/24 13:550.34
Bromochloromethane ug/L ND 1.0 10/11/24 13:550.47
Bromodichloromethane ug/L ND 1.0 10/11/24 13:550.31
Bromoform ug/L ND 1.0 10/11/24 13:550.34
Bromomethane ug/L ND 2.0 v210/11/24 13:551.7
Carbon disulfide ug/L ND 2.0 10/11/24 13:550.36
Carbon tetrachloride ug/L ND 1.0 10/11/24 13:550.33
Chlorobenzene ug/L ND 1.0 10/11/24 13:550.28
Chloroethane ug/L ND 1.0 10/11/24 13:550.65
Chloroform ug/L ND 1.0 10/11/24 13:550.43
Chloromethane ug/L ND 1.0 v210/11/24 13:550.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/11/24 13:550.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/11/24 13:550.36
Dibromochloromethane ug/L ND 1.0 10/11/24 13:550.36
Dibromomethane ug/L ND 1.0 10/11/24 13:550.39
Ethylbenzene ug/L ND 1.0 10/11/24 13:550.30
Iodomethane ug/L ND 20.0 v210/11/24 13:559.7
Methylene Chloride ug/L ND 5.0 10/11/24 13:552.0
Styrene ug/L ND 1.0 10/11/24 13:550.29
Tetrachloroethene ug/L ND 1.0 10/11/24 13:550.29
Tetrahydrofuran ug/L ND 10.0 10/11/24 13:553.5
Toluene ug/L ND 1.0 10/11/24 13:550.24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/21/2024 02:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756912
Iredell Background
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4573319
Associated Lab Samples:92756912001, 92756912002
Matrix:Water
AnalyzedMDL
trans-1,2-Dichloroethene ug/L ND 1.0 10/11/24 13:550.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/11/24 13:550.36
trans-1,4-Dichloro-2-butene ug/L ND 1.0 10/11/24 13:550.56
Trichloroethene ug/L ND 1.0 10/11/24 13:550.38
Trichlorofluoromethane ug/L ND 1.0 10/11/24 13:550.30
Vinyl acetate ug/L ND 2.0 10/11/24 13:551.3
Vinyl chloride ug/L ND 1.0 10/11/24 13:550.39
Xylene (Total)ug/L ND 1.0 10/11/24 13:550.34
1,2-Dichloroethane-d4 (S)%102 70-130 10/11/24 13:55
4-Bromofluorobenzene (S)%100 70-130 10/11/24 13:55
Toluene-d8 (S)%103 70-130 10/11/24 13:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573320LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 18.220 91 70-130
1,1,1-Trichloroethane ug/L 18.120 90 70-130
1,1,2,2-Tetrachloroethane ug/L 17.920 90 70-130
1,1,2-Trichloroethane ug/L 18.820 94 70-130
1,1-Dichloroethane ug/L 20.820 104 70-130
1,1-Dichloroethene ug/L 21.320 107 69-131
1,2,3-Trichloropropane ug/L 17.720 89 70-130
1,2-Dibromo-3-chloropropane ug/L 18.820 94 70-130
1,2-Dichlorobenzene ug/L 19.520 98 70-130
1,2-Dichloroethane ug/L 19.220 96 70-130
1,2-Dichloropropane ug/L 21.020 105 70-130
1,4-Dichlorobenzene ug/L 19.020 95 70-130
1,4-Dioxane (p-Dioxane)ug/L 372400 93 70-132
2-Butanone (MEK)ug/L 33.840 84 67-133
2-Hexanone ug/L 32.0 v3408070-133
4-Methyl-2-pentanone (MIBK)ug/L 32.240 81 70-130
Acetone ug/L 34.140 85 67-130
Acrylonitrile ug/L 89.2100 89 70-130
Benzene ug/L 20.220 101 70-130
Bromochloromethane ug/L 18.120 90 70-130
Bromodichloromethane ug/L 19.220 96 70-130
Bromoform ug/L 17.120 85 70-133
Bromomethane ug/L 8.6 v3204341-148
Carbon disulfide ug/L 19.320 97 70-131
Carbon tetrachloride ug/L 19.220 96 70-130
Chlorobenzene ug/L 18.620 93 70-130
Chloroethane ug/L 17.620 88 41-157
Chloroform ug/L 18.920 95 70-130
Chloromethane ug/L 15.8 v3207959-141
REPORT OF LABORATORY ANALYSIS
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Page 12 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756912
Iredell Background
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573320LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 20.020 100 70-130
cis-1,3-Dichloropropene ug/L 19.020 95 70-130
Dibromochloromethane ug/L 18.420 92 70-130
Dibromomethane ug/L 19.820 99 70-130
Ethylbenzene ug/L 19.020 95 70-130
Iodomethane ug/L 16.6J L2,v3404257-140
Methylene Chloride ug/L 19.520 97 62-130
Styrene ug/L 18.820 94 70-130
Tetrachloroethene ug/L 18.620 93 70-130
Tetrahydrofuran ug/L 169200 84 70-131
Toluene ug/L 19.120 95 70-130
trans-1,2-Dichloroethene ug/L 21.320 107 70-130
trans-1,3-Dichloropropene ug/L 18.720 93 70-130
trans-1,4-Dichloro-2-butene ug/L 18.120 91 57-149
Trichloroethene ug/L 20.020 100 70-130
Trichlorofluoromethane ug/L 18.920 95 57-130
Vinyl acetate ug/L 36.240 90 70-141
Vinyl chloride ug/L 18.920 95 66-140
Xylene (Total)ug/L 55.560 92 70-130
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4573321MATRIX SPIKE SAMPLE:
MSSpike
Result
92756912001
1,1,1,2-Tetrachloroethane ug/L 13.6 M1206870-146ND
1,1,1-Trichloroethane ug/L 15.120 75 70-150ND
1,1,2,2-Tetrachloroethane ug/L 11.5 M1205866-144ND
1,1,2-Trichloroethane ug/L 12.1 M1206070-142ND
1,1-Dichloroethane ug/L 13.3 M1206668-150ND
1,1-Dichloroethene ug/L 14.220 71 64-162ND
1,2,3-Trichloropropane ug/L 11.4 M1205766-144ND
1,2-Dibromo-3-chloropropane ug/L 11.0 M1205562-146ND
1,2-Dichlorobenzene ug/L 13.0 M1206570-142ND
1,2-Dichloroethane ug/L 14.020 70 68-145ND
1,2-Dichloropropane ug/L 12.9 M1206570-144ND
1,4-Dichlorobenzene ug/L 13.2 M1206670-140ND
1,4-Dioxane (p-Dioxane)ug/L 208 M14005266-151ND
2-Butanone (MEK)ug/L 22.3 M1405657-156ND
2-Hexanone ug/L 21.5 M1405462-153ND
4-Methyl-2-pentanone (MIBK)ug/L 22.1 M1405565-144ND
Acetone ug/L 24.2J40 60 49-162ND
Acrylonitrile ug/L 60.2100 60 59-155ND
Benzene ug/L 13.520 68 68-144ND
REPORT OF LABORATORY ANALYSIS
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Page 13 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756912
Iredell Background
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4573321MATRIX SPIKE SAMPLE:
MSSpike
Result
92756912001
Bromochloromethane ug/L 6.5 M1203370-148ND
Bromodichloromethane ug/L 13.7 M1206870-141ND
Bromoform ug/L 12.020 60 59-144ND
Bromomethane ug/L 15.220 76 23-190ND
Carbon disulfide ug/L 13.120 66 64-160ND
Carbon tetrachloride ug/L 15.820 79 70-147ND
Chlorobenzene ug/L 12.8 M1206470-143ND
Chloroethane ug/L 14.320 72 55-190ND
Chloroform ug/L 13.520 67 67-148ND
Chloromethane ug/L 14.020 70 38-180ND
cis-1,2-Dichloroethene ug/L 13.3 M1206667-151ND
cis-1,3-Dichloropropene ug/L 12.5 M1206270-142ND
Dibromochloromethane ug/L 12.7 M1206468-140ND
Dibromomethane ug/L 14.120 70 70-142ND
Ethylbenzene ug/L 13.2 M1206670-145ND
Iodomethane ug/L 30.5 v3407637-160ND
Methylene Chloride ug/L 13.820 69 54-149ND
Styrene ug/L 13.0 M1206570-147ND
Tetrachloroethene ug/L 13.8 M1206970-145ND
Tetrahydrofuran ug/L 105200 53 48-160ND
Toluene ug/L 12.9 M1206465-146ND
trans-1,2-Dichloroethene ug/L 13.820 69 69-155ND
trans-1,3-Dichloropropene ug/L 13.1 M1206570-142ND
trans-1,4-Dichloro-2-butene ug/L 10.020 50 39-149ND
Trichloroethene ug/L 13.920 70 70-152ND
Trichlorofluoromethane ug/L 16.420 82 60-158ND
Vinyl acetate ug/L 25.040 62 56-157ND
Vinyl chloride ug/L 14.820 74 51-178ND
Xylene (Total)ug/L 40.4 MS606770-146ND
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756912002
4573322SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 14 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92756912
Iredell Background
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92756912002
4573322SAMPLE DUPLICATE:
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
1,4-Dioxane (p-Dioxane)ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND v230ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 0.54J 300.56J
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%11098
4-Bromofluorobenzene (S)%99101
Toluene-d8 (S)%98103
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92756912
Iredell Background
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 16 of 20
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92756912
Iredell Background
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92756912001 889904 889977MW-32 EPA 3010A EPA 6020B
92756912002 889904 889977MW-37 EPA 3010A EPA 6020B
92756912001 888072MW-32 EPA 8260D
92756912002 888072MW-37 EPA 8260D
REPORT OF LABORATORY ANALYSIS
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Page 17 of 20
Page 18 of 20
Page 19 of 20
Page 20 of 20
#=CL#
October 17, 2024
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92757092
92757092
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services, Inc.
68 Shipwash Dr.
Garner, NC 27529
Iredell Blanks
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on October 04, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole D'Oleo
[e-mail]
Project Manager
[phone]
Enclosures
cc:Accounts Payable, Municipal Engineering Services, Inc.
Jonathan Pfohl, Municipal Engineering Services
Jay Zimmerman, PG, Municipal Engineering Services, Inc.
REPORT OF LABORATORY ANALYSIS
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Page 1 of 18
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92757092
Iredell Blanks
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
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Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
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Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
DoD Certification via A2LA #: 2926.01
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
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Minnesota Dept of Ag Approval: via MN 027-053-137
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Mississippi Certification #: MN00064
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North Carolina WW Certification #: 530
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Ohio VAP Certification (1700) #: CL101
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Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
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West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification via A2LA #: 2926.01
USDA Permit #: P330-19-00208
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
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South Carolina Laboratory ID: 99006
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Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 18
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92757092
Iredell Blanks
Lab ID Sample ID Matrix Date Collected Date Received
92757092001 EB Water 10/04/24 14:39 10/04/24 16:00
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92757092
Iredell Blanks
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92757092001 EB EPA 6020B 15 PASI-MNN2
EPA 8260D 51 PASI-CLMB
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
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Page 4 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757092
Iredell Blanks
Sample:EB Lab ID:92757092001 Collected:10/04/24 14:39 Received:10/04/24 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3020A
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Antimony ND ug/L 10/14/24 12:18 7440-36-010/09/24 13:440.50 0.087 1
Arsenic ND ug/L 10/14/24 12:18 7440-38-210/09/24 13:440.50 0.12 1
Barium ND ug/L 10/14/24 12:18 7440-39-310/09/24 13:440.30 0.070 1
Beryllium ND ug/L 10/14/24 12:18 7440-41-710/09/24 13:440.20 0.084 1
Cadmium ND ug/L 10/14/24 12:18 7440-43-910/09/24 13:440.080 0.030 1
Chromium ND ug/L 10/14/24 12:18 7440-47-310/09/24 13:442.0 0.54 1
Cobalt ND ug/L 10/14/24 12:18 7440-48-410/09/24 13:440.50 0.095 1
Copper ND ug/L 10/14/24 12:18 7440-50-810/09/24 13:441.0 0.35 1
Lead ND ug/L 10/14/24 12:18 7439-92-110/09/24 13:440.50 0.18 1
Nickel ND ug/L 10/14/24 12:18 7440-02-010/09/24 13:440.50 0.15 1
Selenium ND ug/L 10/14/24 12:18 7782-49-210/09/24 13:440.50 0.074 1
Silver ND ug/L 10/14/24 12:18 7440-22-410/09/24 13:440.50 0.13 1
Thallium ND ug/L 10/14/24 12:18 7440-28-010/09/24 13:440.10 0.026 1
Vanadium ND ug/L 10/14/24 12:18 7440-62-210/09/24 13:441.0 0.20 1
Zinc ND ug/L 10/14/24 12:18 7440-66-610/09/24 13:445.0 2.0 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 10/12/24 00:53 67-64-125.0 5.1 1
Acrylonitrile ND ug/L 10/12/24 00:53 107-13-110.0 1.8 1
Benzene ND ug/L 10/12/24 00:53 71-43-21.0 0.34 1
Bromochloromethane ND ug/L 10/12/24 00:53 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 10/12/24 00:53 75-27-41.0 0.31 1
Bromoform ND ug/L 10/12/24 00:53 75-25-21.0 0.34 1
Bromomethane ND ug/L 10/12/24 00:53 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 10/12/24 00:53 78-93-35.0 4.0 1
Carbon disulfide ND ug/L 10/12/24 00:53 75-15-02.0 0.36 1
Carbon tetrachloride ND ug/L 10/12/24 00:53 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 10/12/24 00:53 108-90-71.0 0.28 1
Chloroethane ND ug/L 10/12/24 00:53 75-00-31.0 0.65 1
Chloroform ND ug/L 10/12/24 00:53 67-66-31.0 0.43 1
Chloromethane ND ug/L 10/12/24 00:53 74-87-31.0 0.54 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/24 00:53 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 10/12/24 00:53 124-48-11.0 0.36 1
Dibromomethane ND ug/L 10/12/24 00:53 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 10/12/24 00:53 95-50-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 10/12/24 00:53 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/12/24 00:53 110-57-6 v21.0 0.56 1
1,1-Dichloroethane ND ug/L 10/12/24 00:53 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 10/12/24 00:53 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 10/12/24 00:53 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/12/24 00:53 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/12/24 00:53 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 10/12/24 00:53 78-87-51.0 0.36 1
cis-1,3-Dichloropropene ND ug/L 10/12/24 00:53 10061-01-51.0 0.36 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
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Page 5 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92757092
Iredell Blanks
Sample:EB Lab ID:92757092001 Collected:10/04/24 14:39 Received:10/04/24 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 10/12/24 00:53 10061-02-61.0 0.36 1
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/24 00:53 123-91-115038.7 1
Ethylbenzene ND ug/L 10/12/24 00:53 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/12/24 00:53 591-78-65.0 0.48 1
Iodomethane ND ug/L 10/12/24 00:53 74-88-4 v220.0 9.7 1
Methylene Chloride ND ug/L 10/12/24 00:53 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/24 00:53 108-10-15.0 2.7 1
Styrene ND ug/L 10/12/24 00:53 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/24 00:53 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/24 00:53 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/12/24 00:53 127-18-41.0 0.29 1
Tetrahydrofuran ND ug/L 10/12/24 00:53 109-99-910.0 3.5 1
Toluene ND ug/L 10/12/24 00:53 108-88-31.0 0.24 1
1,1,1-Trichloroethane ND ug/L 10/12/24 00:53 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 10/12/24 00:53 79-00-51.0 0.32 1
Trichloroethene ND ug/L 10/12/24 00:53 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 10/12/24 00:53 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/12/24 00:53 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 10/12/24 00:53 108-05-4 v22.0 1.3 1
Vinyl chloride ND ug/L 10/12/24 00:53 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 10/12/24 00:53 1330-20-71.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)92 %10/12/24 00:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %10/12/24 00:53 17060-07-070-130 1
Toluene-d8 (S)105 %10/12/24 00:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
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Page 6 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757092
Iredell Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
972515
EPA 3020A
EPA 6020B
6020B Water UPD5
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92757092001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5082355
Associated Lab Samples:92757092001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 0.50 10/14/24 11:190.087
Arsenic ug/L ND 0.50 10/14/24 11:190.12
Barium ug/L 0.11J 0.30 10/14/24 11:190.070
Beryllium ug/L ND 0.20 10/14/24 11:190.084
Cadmium ug/L ND 0.080 10/14/24 11:190.030
Chromium ug/L ND 2.0 10/14/24 11:190.54
Cobalt ug/L ND 0.50 10/14/24 11:190.095
Copper ug/L ND 1.0 10/14/24 11:190.35
Lead ug/L ND 0.50 10/14/24 11:190.18
Nickel ug/L ND 0.50 10/14/24 11:190.15
Selenium ug/L ND 0.50 10/14/24 11:190.074
Silver ug/L ND 0.50 10/14/24 11:190.13
Thallium ug/L ND 0.10 10/14/24 11:190.026
Vanadium ug/L ND 1.0 10/14/24 11:190.20
Zinc ug/L ND 5.0 10/14/24 11:192.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5082356LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 91.7100 92 80-120
Arsenic ug/L 91.3100 91 80-120
Barium ug/L 94.6100 95 80-120
Beryllium ug/L 95.7100 96 80-120
Cadmium ug/L 93.6100 94 80-120
Chromium ug/L 96.9100 97 80-120
Cobalt ug/L 99.2100 99 80-120
Copper ug/L 99.8100 100 80-120
Lead ug/L 97.6100 98 80-120
Nickel ug/L 101100 101 80-120
Selenium ug/L 95.4100 95 80-120
Silver ug/L 49.250 98 80-120
Thallium ug/L 94.6100 95 80-120
Vanadium ug/L 100100 100 80-120
Zinc ug/L 98.4100 98 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
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Huntersville, NC 28078
[phone]
Page 7 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757092
Iredell Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5082357MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92757091001
5082358
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 100 104 75-125104 0 20100ND104104
Arsenic ug/L 100 102 75-125102 0 20100ND102102
Barium ug/L 100 93 75-12596 1 20100129222225
Beryllium ug/L 100 93 75-12598 6 201000.13J 93.2 98.4
Cadmium ug/L 100 92 75-12597 5 201000.54 92.7 97.3
Chromium ug/L 100 94 75-12599 5 201000.56J 94.2 99.2
Cobalt ug/L 100 95 75-125101 6 201000.36J 95.0 101
Copper ug/L 100 95 75-125102 7 201000.53J 95.9 102
Lead ug/L 100 95 75-125100 6 20100ND94.5 100
Nickel ug/L 100 97 75-125102 5 201001.2 98.2 103
Selenium ug/L 100 103 75-125103 1 201000.16J 103 104
Silver ug/L 50 94 75-125100 6 2050ND47.1 50.0
Thallium ug/L 100 92 75-12599 7 201000.34 92.7 99.8
Vanadium ug/L 100 96 75-125101 5 20100ND95.8 101
Zinc ug/L 100 97 75-12597 0 201006.1 103 103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 8 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757092
Iredell Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
888079
EPA 8260D
EPA 8260D
8260D MSV Low Level Landfill
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92757092001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4573347
Associated Lab Samples:92757092001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/12/24 00:350.31
1,1,1-Trichloroethane ug/L ND 1.0 10/12/24 00:350.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/12/24 00:350.22
1,1,2-Trichloroethane ug/L ND 1.0 10/12/24 00:350.32
1,1-Dichloroethane ug/L ND 1.0 10/12/24 00:350.37
1,1-Dichloroethene ug/L ND 1.0 10/12/24 00:350.35
1,2,3-Trichloropropane ug/L ND 1.0 10/12/24 00:350.26
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/12/24 00:350.34
1,2-Dichlorobenzene ug/L ND 1.0 10/12/24 00:350.34
1,2-Dichloroethane ug/L ND 1.0 10/12/24 00:350.32
1,2-Dichloropropane ug/L ND 1.0 10/12/24 00:350.36
1,4-Dichlorobenzene ug/L ND 1.0 10/12/24 00:350.33
1,4-Dioxane (p-Dioxane)ug/L ND 150 10/12/24 00:3538.7
2-Butanone (MEK)ug/L ND 5.0 10/12/24 00:354.0
2-Hexanone ug/L ND 5.0 10/12/24 00:350.48
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/12/24 00:352.7
Acetone ug/L ND 25.0 10/12/24 00:355.1
Acrylonitrile ug/L ND 10.0 10/12/24 00:351.8
Benzene ug/L ND 1.0 10/12/24 00:350.34
Bromochloromethane ug/L ND 1.0 10/12/24 00:350.47
Bromodichloromethane ug/L ND 1.0 10/12/24 00:350.31
Bromoform ug/L ND 1.0 10/12/24 00:350.34
Bromomethane ug/L ND 2.0 10/12/24 00:351.7
Carbon disulfide ug/L ND 2.0 10/12/24 00:350.36
Carbon tetrachloride ug/L ND 1.0 10/12/24 00:350.33
Chlorobenzene ug/L ND 1.0 10/12/24 00:350.28
Chloroethane ug/L ND 1.0 10/12/24 00:350.65
Chloroform ug/L ND 1.0 10/12/24 00:350.43
Chloromethane ug/L ND 1.0 10/12/24 00:350.54
cis-1,2-Dichloroethene ug/L ND 1.0 10/12/24 00:350.38
cis-1,3-Dichloropropene ug/L ND 1.0 10/12/24 00:350.36
Dibromochloromethane ug/L ND 1.0 10/12/24 00:350.36
Dibromomethane ug/L ND 1.0 10/12/24 00:350.39
Ethylbenzene ug/L ND 1.0 10/12/24 00:350.30
Iodomethane ug/L ND 20.0 v210/12/24 00:359.7
Methylene Chloride ug/L ND 5.0 10/12/24 00:352.0
Styrene ug/L ND 1.0 10/12/24 00:350.29
Tetrachloroethene ug/L ND 1.0 10/12/24 00:350.29
Tetrahydrofuran ug/L ND 10.0 10/12/24 00:353.5
Toluene ug/L ND 1.0 10/12/24 00:350.24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757092
Iredell Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4573347
Associated Lab Samples:92757092001
Matrix:Water
AnalyzedMDL
trans-1,2-Dichloroethene ug/L ND 1.0 10/12/24 00:350.40
trans-1,3-Dichloropropene ug/L ND 1.0 10/12/24 00:350.36
trans-1,4-Dichloro-2-butene ug/L ND 1.0 v210/12/24 00:350.56
Trichloroethene ug/L ND 1.0 10/12/24 00:350.38
Trichlorofluoromethane ug/L ND 1.0 10/12/24 00:350.30
Vinyl acetate ug/L ND 2.0 v210/12/24 00:351.3
Vinyl chloride ug/L ND 1.0 10/12/24 00:350.39
Xylene (Total)ug/L ND 1.0 10/12/24 00:350.34
1,2-Dichloroethane-d4 (S)%88 70-130 10/12/24 00:35
4-Bromofluorobenzene (S)%97 70-130 10/12/24 00:35
Toluene-d8 (S)%107 70-130 10/12/24 00:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573348LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 18.720 94 70-130
1,1,1-Trichloroethane ug/L 18.920 94 70-130
1,1,2,2-Tetrachloroethane ug/L 18.120 91 70-130
1,1,2-Trichloroethane ug/L 18.820 94 70-130
1,1-Dichloroethane ug/L 18.520 93 70-130
1,1-Dichloroethene ug/L 18.520 93 69-131
1,2,3-Trichloropropane ug/L 19.020 95 70-130
1,2-Dibromo-3-chloropropane ug/L 17.620 88 70-130
1,2-Dichlorobenzene ug/L 18.920 94 70-130
1,2-Dichloroethane ug/L 19.220 96 70-130
1,2-Dichloropropane ug/L 19.520 98 70-130
1,4-Dichlorobenzene ug/L 18.520 93 70-130
1,4-Dioxane (p-Dioxane)ug/L 373400 93 70-132
2-Butanone (MEK)ug/L 34.140 85 67-133
2-Hexanone ug/L 32.740 82 70-133
4-Methyl-2-pentanone (MIBK)ug/L 33.440 84 70-130
Acetone ug/L 37.440 94 67-130
Acrylonitrile ug/L 88.4100 88 70-130
Benzene ug/L 20.320 101 70-130
Bromochloromethane ug/L 19.120 95 70-130
Bromodichloromethane ug/L 18.220 91 70-130
Bromoform ug/L 17.220 86 70-133
Bromomethane ug/L 18.620 93 41-148
Carbon disulfide ug/L 18.520 93 70-131
Carbon tetrachloride ug/L 19.220 96 70-130
Chlorobenzene ug/L 19.120 95 70-130
Chloroethane ug/L 19.120 96 41-157
Chloroform ug/L 19.220 96 70-130
Chloromethane ug/L 17.320 87 59-141
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757092
Iredell Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4573348LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 18.220 91 70-130
cis-1,3-Dichloropropene ug/L 17.820 89 70-130
Dibromochloromethane ug/L 17.820 89 70-130
Dibromomethane ug/L 19.920 100 70-130
Ethylbenzene ug/L 18.920 94 70-130
Iodomethane ug/L 30.8 v3407757-140
Methylene Chloride ug/L 17.720 89 62-130
Styrene ug/L 19.120 95 70-130
Tetrachloroethene ug/L 19.520 97 70-130
Tetrahydrofuran ug/L 180200 90 70-131
Toluene ug/L 19.520 98 70-130
trans-1,2-Dichloroethene ug/L 18.820 94 70-130
trans-1,3-Dichloropropene ug/L 18.020 90 70-130
trans-1,4-Dichloro-2-butene ug/L 22.9 v32011457-149
Trichloroethene ug/L 20.620 103 70-130
Trichlorofluoromethane ug/L 20.620 103 57-130
Vinyl acetate ug/L 31.7 v3407970-141
Vinyl chloride ug/L 17.620 88 66-140
Xylene (Total)ug/L 57.260 95 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4573349MATRIX SPIKE SAMPLE:
MSSpike
Result
92757023007
1,1,1,2-Tetrachloroethane ug/L 18.220 91 70-146ND
1,1,1-Trichloroethane ug/L 21.520 107 70-150ND
1,1,2,2-Tetrachloroethane ug/L 18.520 93 66-144ND
1,1,2-Trichloroethane ug/L 19.820 99 70-142ND
1,1-Dichloroethane ug/L 21.720 109 68-150ND
1,1-Dichloroethene ug/L 22.220 111 64-162ND
1,2,3-Trichloropropane ug/L 20.120 100 66-144ND
1,2-Dibromo-3-chloropropane ug/L 16.720 84 62-146ND
1,2-Dichlorobenzene ug/L 20.520 102 70-142ND
1,2-Dichloroethane ug/L 21.420 107 68-145ND
1,2-Dichloropropane ug/L 20.320 101 70-144ND
1,4-Dichlorobenzene ug/L 19.920 100 70-140ND
1,4-Dioxane (p-Dioxane)ug/L 429400 107 66-151ND
2-Butanone (MEK)ug/L 36.440 91 57-156ND
2-Hexanone ug/L 32.940 82 62-153ND
4-Methyl-2-pentanone (MIBK)ug/L 34.040 85 65-144ND
Acetone ug/L 38.840 97 49-162ND
Acrylonitrile ug/L 98.5100 99 59-155ND
Benzene ug/L 22.220 111 68-144ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
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Page 11 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757092
Iredell Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4573349MATRIX SPIKE SAMPLE:
MSSpike
Result
92757023007
Bromochloromethane ug/L 21.320 106 70-148ND
Bromodichloromethane ug/L 19.720 98 70-141ND
Bromoform ug/L 17.620 88 59-144ND
Bromomethane ug/L 18.620 91 23-190ND
Carbon disulfide ug/L 23.120 115 64-160ND
Carbon tetrachloride ug/L 21.820 109 70-147ND
Chlorobenzene ug/L 19.720 98 70-143ND
Chloroethane ug/L 23.420 117 55-190ND
Chloroform ug/L 22.120 110 67-148ND
Chloromethane ug/L 19.320 96 38-180ND
cis-1,2-Dichloroethene ug/L 20.720 103 67-151ND
cis-1,3-Dichloropropene ug/L 19.820 99 70-142ND
Dibromochloromethane ug/L 18.920 95 68-140ND
Dibromomethane ug/L 20.720 103 70-142ND
Ethylbenzene ug/L 19.820 99 70-145ND
Iodomethane ug/L 38.340 94 37-160ND
Methylene Chloride ug/L 19.920 99 54-149ND
Styrene ug/L 19.220 96 70-147ND
Tetrachloroethene ug/L 19.420 97 70-145ND
Tetrahydrofuran ug/L 196200 98 48-160ND
Toluene ug/L 21.120 105 65-146ND
trans-1,2-Dichloroethene ug/L 22.420 112 69-155ND
trans-1,3-Dichloropropene ug/L 19.920 100 70-142ND
trans-1,4-Dichloro-2-butene ug/L 15.8 v1207939-149ND
Trichloroethene ug/L 22.020 110 70-152ND
Trichlorofluoromethane ug/L 24.920 125 60-158ND
Vinyl acetate ug/L 35.840 90 56-157ND
Vinyl chloride ug/L 20.820 104 51-178ND
Xylene (Total)ug/L 60.860 101 70-146ND
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92757091001
4573350SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 12 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92757092
Iredell Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92757091001
4573350SAMPLE DUPLICATE:
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
1,4-Dioxane (p-Dioxane)ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L 3.9J 303.6J
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND v130ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9286
4-Bromofluorobenzene (S)%9899
Toluene-d8 (S)%110110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92757092
Iredell Blanks
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 18
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92757092
Iredell Blanks
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92757092001 972515 972807EBEPA 3020A EPA 6020B
92757092001 888079EBEPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2024 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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