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HomeMy WebLinkAboutMO-3182_7570_CA_FPR_20230228_Free Product Recovery & Groundwater Monitoring ReportREPARED FOR:
WBTV Television
One Julian Price Place
Charlotte, North Carolina
PREPARED BY:
S&ME, Inc.
2016 Ayrsley Town Boulevard, Suite 2-A
Charlotte, North Carolina 28273
February 28, 2023
February 28, 2023
WBTV Television
One Julian Price Place
Charlotte, North Carolina
Attention: Mr. Mike Guthrie
Reference: Groundwater Monitoring and Free Product Recovery Report
Jefferson Pilot Communications — WBTV (Incident No. 7570)
One Julian Price Place, Charlotte, North Carolina
S&ME Project No. 210963
Dear Mr. Guthrie:
S&ME, Inc. (S&ME) submits this Groundwater Monitoring and Free Product Recovery Report in general
accordance with our proposal No. 210963B dated July 26, 2022, and as authorized by the North Carolina
Department of Environmental Quality (NCDEQ) Task Authorization No. 7570-25 signed on July 29, 2022. The
services were based on the NCDEQ issued Notice of Regulatory Requirements (NORR) on March 14, 2022,
directing WBTV Television to continue free product recovery efforts. The NORR also required WBTV Television to
conduct an annual groundwater monitoring event at the site using monitoring wells that do not contain free
product.
An 8-hour Aggressive Fluid Vapor Recovery (AFVR) Event was completed on August 16, 2022, using monitoring
well MW-2, which contained 0.36 feet of free product (FP) before the AFVR event. No other monitoring wells
recorded FP during the AFVR event. A total of 227 gallons of fluids, including FP, were removed. Based on vapor
emissions calculated by S&ME, an additional estimated five gallons of vapor phase hydrocarbons were removed.
From August 30, 2022, and January 10, 2023, S&ME performed monthly removal and installation of new product
absorbent socks (if necessary) in wells with measurable FP thicknesses. Free product was observed in monitoring
well MW-2 on August 30, 2022, October 7, 2022, November 1, 2022, and January 10, 2023, with thicknesses of 0.6
feet, 0.26 feet, 0.15 feet, and 0.03 feet, respectively. A total of approximately 0.53 gallons of FP was recovered via
product adsorbent socks. The socks were removed from the applicable monitoring wells and the FP thicknesses
were gauged during the January 10, 2023, monitoring well sampling event to determine the effectiveness of the
FP recovery efforts. Free product was only identified in monitoring well MW-2 at 0.03 feet during this sampling
event, which is a decrease in FP thickness in comparison to the August 2022 monitoring event.
Multiple petroleum compounds were detected in the groundwater samples collected from the monitoring wells
that exceeded the 15A NCAC 02L .0202 (21- Standards). However, no targeted constituents were detected at
concentrations exceeding their Gross Contaminant Levels (GCLs).
Free product recovery activities should continue until FP is not detected in the monitoring wells.
S&ME, Inc. 19751 Southern Pine Boulevard I Charlotte, NC 28273 1 p 704.523.4726 1 www.smeinc.com
Groundwater Monitoring and Free Product Recovery Report
Jefferson Pilot Communications — WBTV (Incident No. 7570)
I I 1 One Julian Price Place, Charlotte, North Carolina
S&ME Project No. 210963
If you have any questions concerning this report, please contact us at your convenience.
Sincerely,
S&ME, Inc.
Laura Beth Slagle
Staff Professional
Islagle@smeinc.com
Senior Reviewed by Wayne Watterson, P.E.
Lucas Barroso-Giachetti, P.E., CHMM
Senior Environmental Engineer
Ibarroso@smeinc.com
cc: Ms. Trudy Beverly, L.G., Hydrogeologist — NCDEQ, DWM, UST Section, Mooresville Regional Office
February 28, 2023 2
Groundwater Monitoring and Free Product Recovery Report
Jefferson Pilot Communications - WBTV (Incident No. 7570)
One Julian Price Place, Charlotte, North Carolina I
S&ME Project No. 210963
Table of Contents
1.0 Site Identification.............................................................................................................1
2.0 Facility Data.......................................................................................................................2
3.0 Liquid Level Measurements...........................................................................................2
4.0 AFVR Event........................................................................................................................2
5.0 Groundwater Sampling...................................................................................................2
5.1 Groundwater Levels and Flow.....................................................................................................3
5.2 Groundwater Sampling Results................................................................................................... 3
6.0 Free Product Recovery......................................................................................................3
7.0 Conclusions and Recommendations.............................................................................4
Appendices
Appendix I - Figures
Appendix II - Tables
Appendix III - Field Sampling Forms
Appendix IV - Laboratory Analytical Report and Chain -of -Custody Report
Appendix V - Waste Manifest
List of Figures
Figure 1 USGS Topographic Map.................................................................................................. Appendix I
Figure2 Site Map............................................................................................................................. Appendix I
Figure 3 Groundwater Quality Map (January 10, 2023)............................................................. Appendix I
February 28, 2023 iii
Groundwater Monitoring and Free Product Recovery Report
Jefferson Pilot Communications - WBTV (Incident No. 7570) r
One Julian Price Place, Charlotte, North Carolina 111
S&ME Project No. 210963 E
Table of Contents (Cont.)
List of Tables
Table 1 Current Liquid Level Data...............................................................................................Appendix II
Table 2 Summary of Historic Free Product and Liquid Levels ................................................ Appendix II
Table 3 Summary of Groundwater Sampling Results............................................................... Appendix II
Table 4 Free Product Recovery - Overall Summary..................................................................Appendix I1
Table 5 Free Product Recovery - Event Summaries..................................................................Appendix I1
Table6 AFVR Data.........................................................................................................................Appendix I1
February 28, 2023 iv
Groundwater Monitoring and Free Product Recovery Report
Jefferson Pilot Communications — WBTV (Incident No. 7570)
One Julian Price Place, Charlotte, North Carolina
S&ME Project No. 210963
1.0 Site Identification
Site Name: Jefferson Pilot Communications - WBTV
Site Location: One Julian Price Place, Charlotte, Mecklenburg County, North Carolina
UST Incident Number: 7570
Facility Number: 0-017251
Risk Classification/Ranking: Intermediate / 1160D
Reason for Classification: Free product (FP) present in multiple wells
Responsible for Release: Jefferson Pilot Communications Company
One Julian Price Place
Charlotte, North Carolina 28208
(704) 374-3639
Current Property Owner: Jefferson Pilot Communications/WBTV
One Julian Price Place
Charlotte, North Carolina 28208
Consultant: S&ME, Inc. (Contact: Lucas Barroso-Giachetti, P.E.)
2016 Ayrsley Town Boulevard, Suite 2-A
Charlotte, NC 28273
(704) 523-4723
Release Information:
Date Discovered: 1993
Latitude: 350 13' 39" N
Longitude: 800 52' 27" W
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release: Unknown
Size and contents of UST System: Two (2) 12,000-gallon gasoline USTs, one (1) 8,000-gallon gasoline UST,
one (1) 8,000-gallon diesel UST, and one (1) 2,000-gallon kerosene UST
Certification:
I, Lucas Barroso-Giachetti, a Professional Engineer for S&ME, Inc., do certify that the information contained in this
report is correct and accurate to the best of my knowledge. S&ME, Inc. is licensedJWp lt"" ology
(certification # C-145) and engineering (certification # F-0176) in North Carolin��'��( ...... „A,Aa'o,,
SEAL
c : 054857
Seal and Signature
2 '-..,,q �.�.Y,GIN,
February 28, 2023 �!l��1lR111lMa�'�`
Groundwater Monitoring and Free Product Recovery Report
Jefferson Pilot Communications - WBTV (Incident No. 7570) r
One Julian Price Place, Charlotte, North Carolina 111
S&ME Project No. 210963 E
2.0 Facility Data
The property currently serves as offices and studios for the Jefferson Pilot Communications Company (the "site").
The site is located at One Julian Price Place, Charlotte, Mecklenburg County, North Carolina (Figure 1, Appendix
Figure 2 depicts the site along with the monitoring well locations.
In a NORR dated March 14, 2022, issued by the North Carolina Department of Environmental Quality (NCDEQ) to
WBTV, WBTV is required to continue FP removal activities and sampling of the monitoring wells that do not
contain FP.
S&ME recently completed a six-month free product recovery effort at the site using product adsorbent socks
which ended in January 2023. Between August 30, 2022 and January 10, 2023, FP was observed only in
monitoring well MW-2 on August 30, 2022, October 7, 2022, November 1, 2022, and January 10, 2023.
3.0 Liquid Level Measurements
S&ME mobilized to the site on August 30, 2022, October 7, 2022, November 1, 2022 and January 10, 2023, to
collect FP thickness data. Free product was measured in monitoring well MW-2 on August 30, 2022, October 7,
2022, November 1, 2022, and January 10, 2023, at thicknesses of 0.6 feet, 0.26 feet, 0.15 feet, and 0.03 feet,
respectively. Current liquid levels are provided in Table 1, Appendix II, and a summary of historical free product
levels provided in Table 2. The Free Product and Water Level Gauging Forms are included in Appendix III.
4.0 AFVR Event
CCI Environmental Services, Inc. (CCI) conducted an 8-hour Aggressive Fluid Vapor Recovery (AFVR) event using
monitoring well MW-2 on August 16, 2022. Monitoring well MW-2 contained 0.36 feet of FP before the event.
No other wells contained FP at the time (Table 2 in Appendix II). A total of 227 gallons of fluid, including FP,
were removed. Field Forms are provided in Appendix III. Vapor emissions from the AFVR event were measured
every 15 to 30 minutes using an organic vapor analyzer. Based on vapor emissions recorded during the AFVR
event, approximately 31 pounds of vapor phase hydrocarbons were removed which corresponds to an equivalent
of 5 gallons of VOCs (Table 6 in Appendix II). The waste manifest is included in Appendix V. Liquid levels were
measured in nearby monitoring wells MW-3, MW-6, and MW-11 during the AFVR event. Free product was not
recorded in these monitoring wells.
5.0 Groundwater Sampling
S&ME mobilized to the site on January 10, 2023, to collect groundwater samples from monitoring wells MW-1,
MW-3, MW-4, MW-6, MW-7, MW-8, MW-9, MW-10, MW-11, MW-12, and EW-1. Free product was noted in
monitoring well MW-2 at a thickness of 0.03 feet and was not sampled. Monitoring well MW-5 was determined to
be dry.
Well gauging data was utilized to calculate well capacities with three well volumes purged prior to sampling in the
monitoring wells without FP. The monitoring wells were then purged using dedicated polyethylene disposable
February 28, 2023
Groundwater Monitoring and Free Product Recovery Report
Jefferson Pilot Communications - WBTV (Incident No. 7570) r
One Julian Price Place, Charlotte, North Carolina III
S&ME Project No. 210963
bailers. The groundwater samples were submitted to Waypoint Analytical (Waypoint), a North Carolina certified
laboratory, for analysis for volatile organic compounds (VOCs) by EPA Method 602 and semi -volatile organic
compounds (SVOCs) by EPA Method 625. The Groundwater Sampling Field Forms are included in Appendix III.
5.1 Groundwater Levels and Flow
On January 10, 2023, the depth to water within the sampled monitoring wells ranged from 29.67 feet below the
top of casing in monitoring well MW-7 to 53.15 feet below the top of casing in monitoring well MW-9. Current
liquid levels recorded during the January 10, 2023, sampling event are summarized in Table 1. As the top -of -
casings for the monitoring wells have not been measured, a calculation of the groundwater flow direction cannot
be performed at this time. Based upon topography at the site, groundwater flow is expected to be toward the
northeast and east.
5.2 Groundwater Sampling Results
Review of the laboratory analytical results indicated VOCs and SVOCs detected in the samples collected from
monitoring wells MW-1, MW-3, MW-4, MW-6, MW-7, MW-8, MW-9, MW-10, MW-12, and EW-1 at concentrations
greater than their respective 2L Standards. However, no targeted constituents were detected at concentrations
exceeding respective Gross Contaminant Levels (GCLs). No compounds were detected in the samples collected
from monitoring well MW-11 at concentrations exceeding their respective 2L Standards.
Two non -petroleum compounds, tetra chloroethene (PCE) and/or trichloroethene (TCE), were detected in
monitoring wells MW-7, MW-8, MW-10, and MW-12 at concentrations above their applicable 2L Standards.
A summary of the current and historical groundwater sampling results is included in Table 3 and Figure 3. The
laboratory analytical report and chain -of -custody record for the January 10, 2023, sampling event is provided in
the Appendix IV.
6.0 Free Product Recovery
Between August 30, 2022, and January 10, 2023, FP was observed in monitoring well MW-2 on August 30, 2022,
October 7, 2022, November 1, 2022, and January 10, 2023, at thicknesses of 0.6 feet, 0.26 feet, 0.15 feet, and 0.03
feet, respectively. Free product was only identified in MW-2 with 0.03 feet during the January 10, 2023,
monitoring well sampling event. A summary of historic FP and liquid levels are presented in the attached Table 2.
The free product recovery events conducted during this reporting period are summarized in the attached Table 4,
with details regarding each recovery event provided in the attached Table S. As can be seen in Table 4 and Table
5, a total of approximately 0.53 gallons of FP was recovered via product adsorbent socks during this reporting
period.
February 28, 2023
Groundwater Monitoring and Free Product Recovery Report
Jefferson Pilot Communications — WBTV (Incident No. 7570) r
One Julian Price Place, Charlotte, North Carolina 111
S&ME Project No. 210963 E
7.0 Conclusions and Recommendations
Based on the data provided herein, S&ME provides the following conclusions:
S&ME conducted FP removal activities using FP absorbent socks from August 30, 2022, and January
10, 2023. Free product thicknesses were measured to document the effectiveness of the absorbent
socks. A total of approximately 0.53 gallons of FP was recovered via product adsorbent socks during
this reporting period.
A review of the historical FP thickness data suggests that the volume of FP at the site has decreased.
The August 2022 AFVR event removed a total of 227 gallons of fluids, including FP, and approximately
5 gallons of vaporous hydrocarbons. Following the AFVR event, FP thickness measurements in
monitoring well MW-2 decreased from 0.6 feet to 0.03 feet suggesting the FP removal efforts were
effective in the area in the immediate vicinity of MW-2.
S&ME recommends continued FP recovery efforts and groundwater monitoring during 2023.
February 28, 2023
Appendices
Appendix I - Figures
BENZENE
1.82
NAPHTHALENE (VOC)
323
NAPHTHALENE (SVOC)
149
1-METHYLNAPHTHALENE
108
2-METHYLNAPHTHALENE
147
MW-3 Ng/L
BENZENE
16.1
NAPHTHALENE (VOC)
356
NAPHTHALENE (SVOC)
204
1-METHYLNAPHTHALENE
164
2-METHYLNAPHTHALE NE
205
MPLED
NOT SA7
•
0.03 FEET OF PRODUCT
Ak .
EW-1
kg/L
g BENZENE
1,570
DIISOPROPYL ETHER
5,970
o METHYL TERT-BUTYL
443
NAPHTHALENE (VOC)
355
a NAPHTHALENE (SVOC)
v
160
0 1-METHYLNAPHTHALENE
111
a 2-METHYLNAPHTHALENE
163
V-10 kg/L
"RACHLOROETHENE 6.96
CHLOROETHENE 16.1
z
6
o � t
MW-7 kg/L
NAPHTHALENE (VOC) 19.2
TETRACHLOROETHENE 1.45
'RACHLOROETHENE 1.94
CHLOROETHENE 3.48
MW-5
NOT SAMPLED - DRY
MW-9 ua/L
NAPHTHALENE (VOC) 88.4
NAPHTHALENE (SVOC) 37.2
1-METHYLNAPHTHALENE 52.1
2-METHYLNAPHTHALENE 60.9
i
MW-12 Pg/L
qp TETRACHLOROETHENE 0.765
` REFERENCE:
GIS BASE LAYERS WERE OBTAINED FROM THE ORTHOIMAGERY NCONEMAP.COM AND
d
MECKLENBURG COUNTY. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE Jr
LOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY
3 INFORMATION, UNLESS STATED OTHERWISE.
MW-11
ALL BELOW 2L
MW-4 Mg/L
BENZENE
2.05 J
NAPHTHALENE (VOC)
125
NAPHTHALENE (SVOC)
19.3
1-METHYLNAPHTHALENE
20.1
MW-1
kg/L
BENZENE
1,110
DIISOPROPYL ETHER
7,260
2-HEXANONE
47
METHYL TERT-BUTYL ETHER
793
NAPHTHALENE (VOC)
402
NAPHTHALENE (SVOC)
252
1-METHYLNAPHTHALENE
320
2-METHYLNAPHTHALENE
501
FREE PRODUCT MEASUREMENTS TAKEN 1/10/2023
CONCENTRATIONS EXCEEDING 2L STANDARDS ARE
PRESENTED IN MICROGRAMS PER LITER (Ng/L)
® MONITORING
MECKLENBURG COUNTY PARCELS
SCALE: FIGURE NO.
GROUNDWATER QUALITY MAP (JANUARY 10, 2023) 1 " = 75 '
DATE:
III E JEFFERSON PILOT COMMUNICATIONS 2-16-23 3
1 JULIAN PRICE PLACE PROJECT NUMBER
CHARLOTTE, MECKLENBURG COUNTY, NC 210963
Appendix II - Tables
Table 1
Current Liquid Level Data
Jefferson Pilot Communications Company (Incident No. 7570)
One Julian Price Place, Charlotte, Mecklenburg County, NC
S&ME Project No. 4335-14-135A / 210963
EW-1
Date
..
01/10/23
NP
43.85
0.00
0.00
Corrected
43.85
MW-1
01/10/23
NP
47.27
0.00
0.00
47.27
MW-2
01/10/23
45.66
45.69
0.03
0.36
45.66
MW-3
01/10/23
NP
42.80
0.00
0.00
42.80
MW-4
01/10/23
NP
41.24
0.00
0.00
41.24
MW-5
01/10/23
Dry
Dry
NA
NA
NA
MW-6
01/10/23
NP
35.60
0.00
0.00
35.60
MW-7
01/10/23
NP
29.67
0.00
0.00
29.67
MW-8
01/10/23
NP
33.45
0.00
0.00
33.45
MW-9
01/10/23
NP
53.15
0.00
0.00
53.15
MW-10
01/10/23
NP
52.27
0.00
0.00
52.27
MW-11
01/10/23
NP
46.60
0.00
0.00
46.60
MW-12
01/10/23
NP
39.61
0.00
1 0.00
39.61
Notes:
DTW: Depth to Water below top of casing
DTP: Depth to Product below top of casing
FPT: Apparent Free Product Thickness
ft: Feet
in: Inches
NP: Not Present
Corrected Depth to Water is calculated by: [ Depth to Water] + [free product thickness x 0.8581]
= 0
III Table 2
Summary of Historic Free Product and Liquid Levels
Jefferson Pilot Communications Company (Incident No. 7570)
One Julian Price Place, Charlotte, Mecklenburg County, NC
S&ME Project No. 4335-14-135A / 210963
Product Type: Gasoline
Well #
MW-1
Recovery
one
Date
DTP
I
DTW
I48.70
0.90
FPT
10.80
DTW
47.93
Comment
None
08/18/05
47.87
48.83
0.96
11.52
48.01
None
08/24/05
47.93
48.97
1.04
12.48
48.08
None
08/29/05
47.96
49.01
1.05
12.60
48.11
None
09/06/05
48.06
49.23
1.17
14.04
48.23
None
10/03/05
48.43
49.80
1.37
16.44
48.62
None
11/03/05
48.61
50.27
1.66
19.92
48.85
None
02/03/06
48.14
49.51
1.37
16.44
48.33
None
03/10/06
47.90
49.07
1.17
14.04
48.07
None
03/23/06
47.93
49.15
1.22
14.64
48.10
None
05/15/06
48.10
49.55
1.45
17.40
48.31
None
05/25/06
48.17
49.73
1.56
18.72
48.39
None
06/16/06
48.58
50.40
1.82
21.84
48.84
None
07/07/06
48.86
50.82
1.96
23.52
49.14
None
07/17/06
48.86
50.82
1.96
23.52
49.14
Bailing
08/18/06
49.29
51.53
2.24
26.88
49.61
Bailed approx 1 gallon of product/water
None
06/19/07
47.21
48.43
1.22
14.64
47.38
Bailing
07/15/11
47.14
48.52
1.38
16.56
47.34
Bailed approx 0.2 gallon of product/water
AFVR
11/29/11
47.37
1 48.61
1 1.24
14.88
1 47.55
Recovered 191 gallons of product total using MW-1, 2, 3 and EW-1
None
01/11/12
47.00
48.34
1.34
16.08
1 47.19
Product check following AFVR Event
AFVR
04/05/12
49.37
51.00
1.63
19.56
49.60
Recovered 36 gallons of product total using MW-1, 2, 3 and EW-1
None
05/09/12
46.64
46.84
0.20
2.40
46.67
Product check following AFVR Event
MMPE
08/20/12
47.94
48.28
0.34
4.08
47.99
Recovered 130.25 gallons of product total usinq MW-1, 2, 3 and EW-1
None
09/11/12
48.03
48.07
0.04
0.48
48.04
Product check following MMPE Event
MMPE
03/04/13
50.62
51.10
0.48
5.76
50.69
Product check before MMPE Event
MMPE
03/08/13
49.81
0.00
0.00
49.81
Product check following MMPE Event
None
03/14/13
50.65
50.91
0.26
3.12
50.69
MMPE
12/02/13
49.93
1 50.43
1 0.50
6.00
50.00
Product check before MMPE Event
MMPE
12/06/13
49.75
0.00
0.00
1 49.75
Product check following MMPE Event
None
01/06/14
46.85
46.89
0.04
0.48
46.86
MMPE
06/16/14
44.33
44.35
0.02
0.24
44.33
Product check before MMPE Event
MMPE
06/20/14
48.49
0.00
0.00
48.49
Product check following MMPE Event
None
07/08/14
44.37
44.38
0.01
0.12
44.37
MMPE
12/15/14
45.12
45.18
0.06
0.72
45.13
Product check before MMPE Event
MMPE
12/19/14
46.72
0.00
0.00
46.72
Product check following MMPE Event
None
01/05/15
47.92
0.00
0.00
47.92
MMPE
06/01/15
1 44.38
1 0.00
0.00
44.38
Product check before MMPE Event
MMPE
06/05/15
49.00
0.00
0.00
1 49.00
Product check following MMPE Event
None
07/01/15
44.83
44.85
0.02
0.24
44.83
Bailing
11/18/15
49.66
50.00
0.34
4.08
49.71
Boom
12/16/15
48.85
48.88
0.03
0.36
48.85
Boom
01/19/16
46.98
0.00
0.00
46.98
Boom
02/17/16
47.30
0.00
0.00
47.30
Boom
03/16/16
46.74
0.00
0.00
46.74
Boom
04/18/16
46.69
46.70
0.01
0.12
46.69
Boom
07/19/16
47.11
1 0.00
0.00
47.11
Boom
02/17/17
48.40
48.41
0.01
0.12
1 48.40
Boom
03/21/17
49.15
0.00
0.00
49.15
Boom
04/18/17
48.82
0.00
0.00
48.82
Boom
05/16/17
48.85
48.91
0.06
0.72
48.86
Boom
06/16/17
48.81
0.00
0.00
48.81
Boom
07/14/17
48.25
0.00
0.00
48.25
None
11/27/17
49.17
49.20
0.03
0.00
49.17
None
01/24/18
49.46
49.55
0.09
1.08
49.47
Boom
02/21/18
49.30
1 49.41
1 0.11
1.32
49.32
Boom
03/27/18
49.75
49.76
0.01
0.12
49.75
Boom
04/27/18
49.05
0.00
0.00
1 49.05
Boom
07/24/18
49.40
0.00
0.00
1 49.40
Boom
08/22/18
49.69
49.72
0.03
0.36
49.69
None
04/01/19
45.85
0.00
0.00
45.85
None
05/06/19
45.11
0.00
0.00
45.11
None
06/03/19
45.13
0.00
0.00
45.13
None
07/02/19
44.94
0.00
0.00
44.94
None
08/01/19
1 45.49
1 0.00
0.00
45.49
None
09/09/19
45.80
0.00
0.00
45.80
None
11/13/19
44.82
0.00
0.00
44.82
None
12/10/19
44.97
0.00
0.00
1 44.97
None
01/10/20
45.07
0.00
0.00
45.07
None
02/12/20
44.88
0.00
0.00
44.88
None
03/30/20
44.75
0.00
0.00
44.75
None
04/30/20
44.48
0.00
0.00
44.48
None
06/02/20
44.45
0.00
0.00
44.45
None
06/18/20
43.92
1 43.93
1 0.01
0.12
43.92
None
03/17/21
44.38
0.00
0.00
44.38
None
04/23/21
44.00
0.00
0.00
44.00
None
05/18/21
44.07
0.00
0.00
1 44.07
None
06/16/21
44.00
0.00
0.00
44.00
None
07/20/21
42.60
0.00
0.00
42.60
None
08/24/21
45.15
0.00
0.00
45.15
None
08/30/21
46.12
0.00
0.00
46.12
None
08/30/22
46.75
0.00
0.00
46.75
Product check following AFVR conducted on 08/16/2022.
None
10/07/22
47.09
0.00
0.00
47.09
None
11/01/22
47.15
1 0.00
0.00
47.15
None
01/10/23
47.27
1 0.00
0.00
47.27
Page 1 of 4
= r-
III Table 2
Summary of Historic Free Product and Liquid Levels
Jefferson Pilot Communications Company (Incident No. 7570)
One Julian Price Place, Charlotte, Mecklenburg County, INC
S&ME Project No. 4335-14-135A / 210963
Product Type: Gasoline
Well #
EW-1
Recovery
Skimmer
Date
08/24/05
DTP
DTW
45.19
0.00
FPT
0.00
DTW
45.19
Comment
Skimmer Off - Well Developed to check for the presence of free product
Skimmer
08/29/05
45.12
47.72
2.60
31.20
45.49
Skimmer Off
Skimmer
09/06/05
45.20
45.22
0.02
0.24
45.20
Skimmer Off
Skimmer
10/03/05
45.65
0.00
0.00
45.65
Skimmer Off
Skimmer
11/03/05
45.90
0.00
0.00
45.90
Skimmer Off
Skimmer
05/25/06
47.32
0.00
0.00
47.32
Skimmer Off
Skimmer
08/18/06
46.60
0.00
0.00
46.60
Skimmer Off
Skimmer
06/19/07
44.39
0.00
0.00
44.39
Skimmer Off
Bailing
1 07/15/11
50.08
1 52.16
1 2.08
24.96
1 50.38
Bailed approx 0.3 gallon of product/water
AFVR
11/29/11
50.41
50.98
0.57
6.84
50.49
Recovered 191 gallons of product total using MW-1, 2, 3 and EW-1
None
01/11/12
50.03
51.43
1.40
16.80
50.23
Product check following AFVR Event
AFVR
04/05/12
46.40
47.80
1.40
16.80
46.60
Recovered 36 gallons of product total using VW-1, 2, 3 and EW-1
None
05/09/12
49.48
50.77
1.29
15.48
49.66
Product check following AFVR Event
MMPE
08/20/12
50.75
52.49
1.74
20.88
51.00
Recovered 130.25 gallons of product total using MW-1, 2, 3 and EW-1
None
09/11/12
50.99
51.42
0.43
5.16
51.05
Product check following MMPE Event
MMPE
03/04/13
48.68
48.83
0.15
1.80
48.70
Product check before MMPE Event
MMPE
03/08/13
49.81
0.00
0.00
49.81
Product check following MMPE Event
None
03/14/13
45.67
1 45.70
1 0.03
0.36
1 45.67
MMPE
12/02/13
46.94
47.10
0.16
1.92
46.96
Product check before MMPE Event
MMPE
12/06/13
49.60
0.00
0.00
49.60
Product check following MMPE Event
None
01/06/14
49.84
50.09
0.25
3.00
49.88
MMPE
06/16/14
47.34
47.40
0.06
0.72
47.35
Product check before MMPE Event
MMPE
06/20/14
49.55
0.00
0.00
49.55
Product check following MMPE Event
None
07/08/14
47.41
47.44
0.03
0.36
47.41
MMPE
12/15/14
48.12
48.29
0.17
2.04
48.14
1 Product check before MMPE Event
MMPE
12/19/14
49.65
0.00
0.00
49.65
Product check following MMPE Event
None
01/05/15
48.25
1 48.33
0.08
1 0.96
48.26
MMPE
06/01/15
47.36
47.39
0.03
0.36
47.36
Product check before MMPE Event
MMPE
06/05/15
50.01
0.00
0.00
50.01
Product check following MMPE Event
None
07/01/15
47.82
47.91
0.09
1.08
47.83
Bailing
11/18/15
47.75
47.79
0.04
0.48
47.76
Boom
12/16/15
48.85
0.00
0.00
48.85
Boom
01/19/16
44.06
0.00
0.00
1 44.06
Boom
02/17/16
---
44.44
0.00
0.00
1 44.44
Boom
03/16/16
43.80
1 0.00
0.00
43.80
Boom
07/19/16
42.22
42.24
0.02
0.24
42.22
Boom
02/17/17
45.70
0.00
0.00
45.70
Boom
03/21/17
45.63
0.00
0.00
45.63
Boom
04/18/17
45.62
0.00
0.00
45.62
Boom
05/16/17
45.39
45.40
0.01
0.12
45.39
Boom
06/16/17
45.09
0.00
0.00
45.09
Boom
07/14/17
45.02
0.00
0.00
45.02
None
11/27/17
44.24
44.25
0.01
0.12
1 44.24
None
01/24/18
1 47.49
1 0.00
0.00
47.49
Boom
02/21/18
46.30
0.00
0.00
46.30
Boom
03/27/18
45.22
0.00
0.00
45.22
Boom
04/27/18
45.70
0.00
0.00
45.70
Boom
07/24/18
44.77
44.80
0.03
0.36
44.77
Boom
08/22/18
42.34
0.00
0.00
42.34
None
04/01/19
42.97
0.00
0.00
42.97
None
05/06/19
37.66
0.00
0.00
37.66
None
06/03/19
42.11
42.12
0.01
0.00
42.11
Installed sock
Boom
07/02/19
37.85
11.00
0.00
37.85
None
08/01/19
NO DATA
Sock was 5% saturated. Sock was removed
None
09/09/19
42.98
0.00
0.00
42.98
None
11/13/19
37.42
0.00
0.00
37.42
None
12/10/19
37.67
0.00
0.00
37.67
None
01/10/20
37.84
0.00
0.00
37.84
None
02/12/20
37.45
0.00
0.00
37.45
None
03/30/20
37.38
0.00
0.00
37.38
None
04/30/20
37.00
0.00
0.00
37.00
None
06/02/20
37.10
0.00
0.00
37.10
None
06/18/20
41.44
0.00
1 0.00
41.44
None
03/17/21
41.40
0.00
0.00
41.40
None
04/23/21
40.98
0.00
0.00
40.98
None
05/18/21
50.05
0.00
0.00
50.05
None
06/16/21
41.00
0.00
0.00
41.00
None
07/20/21
45.65
0.00
0.00
45.65
None
08/24/21
42.05
0.00
0.00
42.05
None
08/30/21
42.21
0.00
0.00
42.21
None
08/30/22
42.77
0.00
0.00
42.77
Product check following AFVR conducted on 08/16/2022.
None
10/07/22
38.95
0.00
0.00
38.95
None
11/01/22
38.98
0.00
0.00
38,98
None
01/10/23
43.85
0.00
0.00
43.85
Page 2 of 4
0
III Table 2
Summary of Historic Free Product and Liquid Levels
Jefferson Pilot Communications Company (Incident No. 7570)
One Julian Price Place, Charlotte, Mecklenburg County, INC
S&ME Project No. 4335-14-135A / 210963
Product Type: Gasoline
VW-2
cove
None
08/12/05
TP
43.13
T.
44.98
E
1.85
22.20
43.39
None
08/18/05
43.22
45.09
1.87
22.44
43.49
None
08/24/05
43.29
45.19
1.90
22.80
43.56
None
08/29/05
43.32
45.52
2.20
26.40
43.63
None
09/06/05
43.41
45.35
1.94
23.28
43.69
None
10/03/05
43.83
44.35
0.52
6.24
43.90
None
11/03/05
44.10
45.98
1.88
22.56
44.37
None
02/03/06
43.60
45.25
1.65
19.80
43.83
None
1 03/10/06
43.31
1 44.93
1 1.62
19.44
1 43.54
None
03/23/06
43.35
45.00
1.65
19.80
43.58
Skimmer
03/29/06
43.33
44.96
1.63
19.56
43.56
Skimmer moved from MW-9 to MW-2, Needs new belt to reach liquid surface
Skimmer
05/15/06
44.42
46.22
1.80
21.60
44.68
Skimmer
05/25/06
44.52
47.00
2.48
29.76
44.87
Skimmer
06/16/06
45.24
45.30
0.06
0.72
45.25
Skimmer
07/07/06
45.58
45.73
0.15
1.80
45.60
Skimmer
07/17/06
45.58
45.73
0.15
1.80
45.60
Skimmer
08/18/06
45.96
46.70
0.74
8.88
46.07
Base of Belt above liquid surface
Skimmer
06/19/07
43.64
44.60
0.96
11.52
43.78
Skimmer Off
Bailing
07/15/11
46.53
1 48.29
1 1.76
21.12
1 46.78
Bailed approx 0.2 gallon of product/water
AFVR
11/29/11
46.92
48.11
1.19
14.28
47.09
Recovered 191 gallons of product total using VW-1, 2, 3 and EW-1
None
01/11/12
45.65
46.31
0.66
7.92
45.74
Product check following AFVR Event
AFVR
04/05/12
45.05
45.82
0.77
9.24
45.16
Recovered 36 gallons of product total using VW-1, 2, 3 and EW-1
None
05/09/12
45.14
45.43
0.29
3.48
45.18
Product check following AFVR Event
MMPE
08/20/12
46.42
47.17
0.75
9.00
46.53
Recovered 130.25 gallons of product total using VW-1, 2, 3 and EW-1
None
09/11/12
46.51
46.89
0.38
4.56
46.56
Product check following MMPE Event
MMPE
03/04/13
46.08
47.10
1.02
12.24
46.22
Product check before MMPE Event
MMPE
03/08/13
46.41
0.00
0.00
46.41
Product check following MMPE Event
None
03/14/13
46.18
1 46.45
1 0.27
3.24
1 46.22
MMPE
12/02/13
45.28
46.48
1.20
14.40
45.45
Product check before MMPE Event
MMPE
12/06/13
47.05
0.00
0.00
47.05
Product check following MMPE Event
None
01/06/14
45.35
45.53
0.18
2.16
45.38
MMPE
06/16/14
42.76
42.89
0.13
1.56
42.78
Product check before MMPE Event
MMPE
06/20/14
47.79
0.00
0.00
47.79
Product check following MMPE Event
None
07/08/14
42.83
42.89
0.06
0.72
42.84
MMPE
12/15/14
43.52
43.98
0.46
5.52
43.59
Product check before MMPE Event
MMPE
12/19/14
46.17
0.00
0.00
46.17
Product check following MMPE Event
None
01/05/15
43.71
1 43.92
1 0.21
2.52
1 43.74
MMPE
06/01/15
42.81
42.96
0.15
1.80
42.83
Product check before MMPE Event
MMPE
06/05/15
46.41
0.00
0.00
46.41
Product check following MMPE Event
None
07/01/15
43.26
43.55
0.29
3A8
43.30
Bailing
11/18/15
45.20
45.65
0.45
5.40
45.26
Boom
12/16/15
49.90
49.91
0.01
0.12
49.90
Boom
01/19/16
44.08
0.00
0.00
44.08
Boom
02/17/16
44.40
0.00
0.00
44.40
Boom
04/18/16
42.09
0.00
0.00
42.09
Boom
07/19/16
42.62
1 42.65
1 0.03
0.36
1 42.62
Boom
02/17/17
NP
44.62
0.00
0.00
44.62
Boom
03/21/17
NP
44.31
0.00
0.00
44.31
Boom
04/18/17
NP
44.58
0.00
0.00
44.58
Boom
05/16/17
NP
44.18
0.00
0.00
44.18
Boom
06/16/17
NP
44.02
0.00
0.00
44.02
Boom
07/14/17
NP
43.73
0.00
0.00
43.73
None
11/27/17
44.25
44.30
0.05
0.00
44.26
None
01/24/18
45.01
45.17
0.16
1.92
45.03
Boom
02/21/18
45.25
0.00
1 0.00
45.25
Boom
03/27/18
48.95
0.00
0.00
48.95
Boom
04/27/18
44.50
0.00
0.00
44.50
Boom
07/24/18
48.95
0.00
0.00
48.95
Boom
08/22/18
45.28
45.34
0.06
0.72
45.29
None
04/01/19
40.60
0.00
0.00
40.60
None
05/06/19
40.80
0.00
0.00
40.80
None
06/03/19
41.11
0.00
0.00
41.11
None
07/02/19
40.62
1 0.00
0.00
1 40.62
None
08/01/19
41.08
0.00
0.00
41.08
None
09/09/19
41.20
41.24
0.04
0.48
41.21
Added new sock
Boom
11/13/19
40.10
0.00
0.00
40.10
Boom
12/10/19
40.88
40.90
0.02
0.24
40.88
Sock 10% saturated, left existing sock in well.
Boom
01/10/20
41.01
41.04
0.03
0.36
41.01
Sock replaced, 80%saturated.
Boom
02/12/20
40.72
40.76
0.04
0.48
40.73
Sock replaced, 60% saturated.
Boom
03/30/20
40.38
40.40
0.02
0.00
40.38
Sock replaced, 50% saturated.
Boom
04/30/20
39.95
39.97
0.02
0.24
39.95
Removed sock, 80% saturated.
None
06/02/20
40.10
40.12
1 0.02
0.24
1 40.10
None
06/18/20
39.75
0.00
0.00
39.75
Boom
03/17/21
40.75
40.77
0.02
0.24
40.75
Installed a new sock.
Boom
04/23/21
39.70
0.00
0.00
39.70
1 Removed sock, 100% saturated. Installed new sock.
Boom
05/18/21
39.75
0.00
0.00
39.75
Sock 25% saturated, left existing sock in well.
Boom
06/16/21
39.77
0.00
0.00
39.77
100% saturated, installed new sock.
Boom
07/20/21
43.58
0.00
0.00
43.58
Sock 25% saturated, left existing sock in well.
Boom
08/24/21
41.44
41.55
0.11
1.32
41.46
Sock removed for upcoming sampling event.
Boom
08/30/21
40.40
40.64
0.24
2.88
40.43
Added new sock.
Boom
08/30/22
42.10
42.70
0.60
7.20
42.19
Product check following AFVR conducted on 08/16/2022, Added new sock, 100% saturated.
Boom
10/07/22
42.84
43.10
0.26
2.86
42.87
Added new sock, 100% saturated.
Boom
11/01/22
42.85
43.00
0.15
1.80
1 42.87
Added new sock, 100% saturated,
Boom
01/10/23
45.66
45.69
0.03
0.36
1 45.66
1 Added new sock, 100% saturated.
Page 3 of 4
Q
Table 2
Summary of Historic Free Product and Liquid Levels
Jefferson Pilot Communications Company (Incident No. 7570)
One Julian Price Place, Charlotte, Mecklenburg County, INC
S&ME Project No. 4335-14-135A / 210963
Product Type: Gasoline
-ell
"'c'v'-
Date
DTP
FPT
DTW
Comment
MW-3
Skimmer
08/12/05
43.82
45.43
1.61
19.32
44.05
Skimmer started on 8/12/05
Skimmer
08/15/05
44.11
44.11
0.00
0.00
44.11
Skimmer
08/18/05
44.13
44.17
0.04
0.48
44.14
Skimmer
08/24/05
44.22
44.22
0.00
0.00
44.22
Skimmer
08/29/05
44.23
44.50
0.27
3.24
44.27
Skimmer
09/06/05
44.32
44.32
0.00
0.00
44.32
Skimmer
10/03/05
44.70
45.03
0.33
3.96
44.75
Skimmer
11/03/05
45.73
45.75
0.02
0.24
45.73
Skimmer
1 02/03/06
43.13
1 43.45
1 0.32
3.84
43.18
Skimmer
03/10/06
44.78
45.60
0.82
9.84
44.90
Skimmer
03/23/06
44.93
44.97
0.04
0.48
44.94
Skimmer
05/15/06
45.10
45.10
0.00
0.00
45.10
Skimmer
05/25/06
45.21
45.21
0.00
0.00
45.21
Skimmer
06/16/06
45.67
45.68
0.01
0.12
45.67
Skimmer
07/07/06
46.00
46.00
0.00
0.00
46.00
Skimmer
07/17/06
46.00
46.00
0.00
0.00
46.00
Skimmer
08/18/06
46.43
47.05
0.62
7.44
1 46.52
Base of Belt above liquid surface
Skimmer
06/19/07
44.00
45.45
1.45
17.40
44.21
1-gallon from MW-1 placed in drum
Bailing
07/15/11
46.86
1 48.98
1 2.12
25.44
47.16
Bailed approx 0.3gallon of product/water
AFVR
11/29/11
47.21
49.12
1.91
22.92
47.48
Recovered 191 gallons of product total using MW-1, 2, 3 and EW-1
None
01/11/12
45.97
47.08
1.11
13.32
46.13
Product check following AFVR Event
AFVR
04/05/12
45.35
46.65
1.30
15.60
45.53
Recovered 36 gallons of product total using MW-1, 2, 3 and EW-1
None
05/09/12
45.46
46.28
0.82
9.84
45.58
Product check following AFVR Event
MMPE
08/20/12
46.73
47.94
1.21
14.52
46.90
Recovered 130.25 gallons of product total using MW-1, 2, 3 and EW-1
None
09/11/12
46.88
47.32
0.44
5.28
46.94
Product check following MMPE Event
MMPE
03/04/13
46.53
47.00
0.47
5.64
46.60
Product check before MMPE Event
MMPE
03/08/13
48.55
0.00
0.00
48.55
Product check following MMPE Event
None
03/14/13
46.55
1 46.85
1 0.30
3.60
46.59
MMPE
12/02/13
45.86
46.20
0.34
4.08
45.91
Product check before MMPE Event
MMPE
12/06/13
48.47
0.00
0.00
48.47
Product check following MMPE Event
None
01/06/14
45.79
45.82
0.03
0.36
45.79
MMPE
06/16/14
43.27
43.28
0.01
0.12
43.27
Product check before MMPE Event
MMPE
06/20/14
46.31
0.00
0.00
46.31
Product check following MMPE Event
None
07/08/14
43.34
43.45
0.11
1.32
43.36
MMPE
12/15/14
44.02
44.51
0.49
5.88
44.09
1 Product check before MMPE Event
MMPE
12/19/14
48.28
0.00
0.00
48.28
Product check following MMPE Event
None
01/05/15
44.15
1 44.59
1 0.44
5.28
44.21
MMPE
06/01/15
43.30
43.51
0.21
2.52
43.33
Product check before MMPE Event
MMPE
06/05/15
47.49
0.00
0.00
47.49
Product check following MMPE Event
None
07/01/15
43.76
44.05
0.29
3A8
43.80
Boom
02/17/17
NP
44.84
0.00
0.00
44.84
Boom
03/21/17
NP
44.58
0.00
0.00
44.58
Boom
04/18/17
NP
44.29
0.00
0.00
44.29
Boom
05/16/17
NP
44.32
0.00
0.00
44.32
Boom
06/16/17
NP
44.05
0.00
0.00
44.05
Boom
07/14/17
NP
1 44.10
1 0.00
0.00
44.10
None
11/27/17
45.26
45.32
0.06
0.00
45.27
None
01/24/18
45.53
45.60
0.07
0.84
45.54
Boom
02/21/18
44.83
44.90
0.07
0.84
44.84
Boom
03/27/18
45.07
45.10
0.03
0.36
45.07
Boom
04/27/18
44.64
0.00
0.00
44.64
Boom
07/24/18
49.27
0.00
0.00
1 49.27
Boom
08/22/18
45.66
45.74
0.08
0.96
45.67
None
04/01/19
42.29
42.31
0.02
0.24
42.29
Installed new sock
Boom
05/06/19
41.53
1 41.68
1 0.15
1.80
41.55
Sock was 80% saturated. Installed new sock.
Boom
06/03/19
40.52
40.56
0.04
0.48
40.53
Sock was 100% saturated. Installed new sock.
Boom
07/02/19
41.32
41.44
0.12
1.44
41.34
Sock was 90% saturated. Installed new sock.
Boom
08/01/19
41.40
0.00
0.00
41.40
Sock was 50% saturated. Sock was removed
None
09/09/19
41.73
0.00
0.00
41.73
None
11/13/19
40.51
0.00
0.00
40.51
None
12/10/20
40.48
0.00
0.00
1 40.48
None
01/10/20
40.62
0.00
0.00
40.62
None
02/12/20
40.20
0.00
0.00
40.20
None
03/30/20
1 40.02
1 0.00
0.00
40.02
None
04/30/20
39.82
0.00
0.00
39.82
None
06/02/20
39.77
0.00
0.00
39.77
None
06/18/20
39.89
0.00
0.00
39.89
None
03/17/21
40.30
0.00
0.00
40.30
None
04/23/21
39.95
0.00
0.00
39.95
None
05/18/21
40.01
0.00
0.00
40.01
None
06/16/21
39.99
0.00
0.00
39.99
None
07/20/21
40.23
0.00
0.00
40.23
None
08/24/21
1 41.00
1 0.00
0.00
41.00
None
08/30/21
40.94
0.00
0.00
40.94
None
08/30/22
42.64
0.00
0.00
42,64
Product check following AFVR conducted on 08/16/2022.
None
10/07/22
43.01
0.00
0.00
43.01
None
11/01/22
43.05
0.00
0.00
43.05
None
01/10/23
42.80
0.00
1 0.00
1 42.80
Notes:
DTP : Depth to Product from Top of Casing (R) : Feet
DTW : Depth to Water from Top of Casing (n) : Inches
FPT: Free Product Thickness (gal) : GO-
- I No Free Product Indicated
Corrected Depth to Water is calculated by: [Depth to Water] - [Free Product Thickness x 0.8581]
Page 4 of 4
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_ Table 4
II Free Product Recovery - Overall Summary
Jefferson Pilot Communications (UST Incident # 7570)
One Julian Price Place, Charlotte, NC
S&ME Project No. 4335-14-135A / 210963
Date
08/30/22
DTP
(ft)
NM
DTW
(ft)
46.75
FP
(ft)
0.00
FP
Recovered
0.00
DTP
(ft)
42.10
DTW
(ft)
42.70
FP
(ft)
0.60
FP
Recovered
0.13
DTP
(ft)
0.00
DTW
(ft)
42.64
FP
(ft)
0.00
FP
Recovered
0.00
DTP
(ft)
NM
DTW
(ft)
46.50
FP
(ft)
0.00
FP
Recovered
0.00
DTP
(ft)
NM
DTW
(ft)
42.77
FP
(ft)
0.00
FP
Recovered
0.00
FP
Recovered
0.13
10/07/22
NM
47.09
0.00
0.00
42.84
43.10
0.26
0.13
NM
43.01
0.00
0.00
NM
46.84
0.00
0.00
NM
38.95
0.00
0.00
0.13
11/01/22
NM
47.15
0.00
0.00
42.85
43.00
0.15
0.13
NM
43.05
0.00
0.00
NM
46.88
0.00
0.00
NM
38.98
0.00
0.00
0.13
01/10/23
NM
47.27
0.00
0.00
45.66
45.69
0.03
0.13
0.00
42.80
0.00
0.00
NM
46.60
0.00
0.00
NM
43.85
0.00
0.00
0.13
Totals
0.00
0.53
0.00
0.00
0.00
0.53
Note,.
Liquid levels measured from well top of casing, after removing socks
ft : feet
gal : gallons
NM : None measured
ND : No Data
Table 5
I Free Product Recovery - Event Summaries
Jefferson Pilot Communications (UST Incident # 7570)
One Julian Price Place, Charlotte, NC
S&ME Project No. 4335-14-135A / 210963
Date
Casing Diameter
in
2
2
8/30/2022
2 2
4
Boring Diameter
in
8
8
8
8
10
Annulus Porosity
%
30%
30%
30%
30%
30%
Depth to Product
ft
46.75
42.10
42.64
46.50
42.77
Depth to Water
ft
46.75
42.70
42.64
46.50
42.77
Product Thickness
ft
0.00
0.60
0.00
0.00
0.00
in
0.00
7.20
0.00
0.00
0.00
Total Boring Volume
ft^3
0.00
0.21
0.00
0.00
0.00
Well Volume
ft^3
0.00
0.01
0.00
0.00
0.00
Annulus Volume
ft^3
0.00
0.06
0.00
0.00
0.00
Product Volume
ft^3
0.00
0.07
0.00
0.00
0.00
gal
0.00
0.54
0.00
0.00
0.00
oz
0.0
68.9
0.0
0.0
0.0
% Sock Capacity
%
0%
405%
0%
0%
0%
Sock Capacity
oz
17
17
17
17
17
gal
0.13
0.13
0.13
0.13
0.13
# of Socks
0
1
0
0
0
Sock % Full
0%
100%
0%
0%
0%
Old Sock Replaced (#)
0
0
0
0
0
New Sock Installed (#)
0
1
0
0
0
Sock Volume
gal
0.00
0.13
0.00
0.00
0.00
0.13
Bailed Volume
gal
0.00
0.00
0.00
0.00
0.00
0.00
Total Volume
gal
0.00
0.13
0.00
0.00
0.00
0.13
Notes:
Liquid levels measured after removing socks
�r
Table 5
Free Product Recovery - Event Summaries
= Jefferson Pilot Communications (UST Incident # 7570)
One Julian Price Place, Charlotte, NC
S&ME Project No. 4335-14-135A / 210963
..10/7/2022
Casing Diameter
in
2
2
2 2
4
Boring Diameter
in
8
8
8
8
10
Annulus Porosity
%
30%
30%
30%
30%
30%
Depth to Product
ft
47.09
42.84
43.01
46.84
38.95
Depth to Water
ft
47.09
43.10
43.01
46.84
38.95
Product Thickness
ft
0.00
0.26
0.00
0.00
0.00
in
0.00
3.12
0.00
0.00
0.00
Total Boring Volume
ft^3
0.00
0.09
0.00
0.00
0.00
Well Volume
ft^3
0.00
0.01
0.00
0.00
0.00
Annulus Volume
ft^3
0.00
0.03
0.00
0.00
0.00
Product Volume
ft^3
0.00
0.03
0.00
0.00
0.00
gal
0.00
0.23
0.00
0.00
0.00
oz
0.0
29.9
0.0
0.0
0.0
% Sock Capacity
%
0%
176%
0%
0%
0%
Sock Capacity
oz
17
17
17
17
17
gal
0.13
0.13
0.13
0.13
0.13
# of Socks
0
1
0
0
0
Sock % Full
0%
100%
0%
0%
0%
Old Sock Replaced (#)
0
0
0
0
0
New Sock Installed (#)
0
1
0
0
0
Sock Volume
gal
0.00
0.13
0.00
0.00
0.00
0.13
Bailed Volume
gal
0.00
0.00
0.00
0.00
0.00
0.00
Total Volume
gal
0.00
0.13
0.00
0.00
0.00
0.13
Notes:
Liquid levels measured after removing socks
Table 5
Free Product Recovery - Event Summaries
Jefferson Pilot Communications (UST Incident # 7570)
One Julian Price Place, Charlotte, NC
S&ME Project No. 4335-14-135A / 210963
Date
Casing Diameter
in
2
2
11/1/2022
2 2
4
Boring Diameter
in
8
8
8
8
10
Annulus Porosity
%
30%
30%
30%
30%
30%
Depth to Product
ft
47.15
42.85
43.05
46.88
38.98
Depth to Water
ft
47.15
43.00
43.05
46.88
38.98
Product Thickness
ft
0.00
0.15
0.00
0.00
0.00
in
0.00
1.80
0.00
0.00
0.00
Total Boring Volume
ft^3
0.00
0.05
0.00
0.00
0.00
Well Volume
ft^3
0.00
0.00
0.00
0.00
0.00
Annulus Volume
ft^3
0.00
0.01
0.00
0.00
0.00
Product Volume
ft^3
0.00
0.02
0.00
0.00
0.00
gal
0.00
0.13
0.00
0.00
0.00
oz
0.0
17.2
0.0
0.0
0.0
% Sock Capacity
%
0%
101 %
0%
0%
0%
Sock Capacity
oz
17
17
17
17
17
gal
0.13
0.13
0.13
0.13
0.13
# of Socks
0
1
0
0
0
Sock % Full
0%
100%
0%
0%
0%
Old Sock Replaced (#)
0
0
0
0
0
New Sock Installed (#)
0
1
0
0
0
Sock Volume
gal
0.00
0.13
0.00
0.00
0.00
0.13
Bailed Volume
gal
0.00
0.00
0.00
0.00
0.00
0.00
Total Volume
gal
0.00
0.13
0.00
0.00
0.00
0.13
Notes:
Liquid levels measured after removing socks
Table 5
Free Product Recovery - Event Summaries
Jefferson Pilot Communications (UST Incident # 7570)
One Julian Price Place, Charlotte, NC
S&ME Project No. 4335-14-135A / 210963
Date
Casing Diameter
in
2
2
1/10/2023
2 2
4
Boring Diameter
in
8
8
8
8
10
Annulus Porosity
%
30%
30%
30%
30%
30%
Depth to Product
ft
47.27
45.66
42.80
46.60
43.85
Depth to Water
ft
47.27
45.69
42.80
46.60
43.85
Product Thickness
ft
0.00
0.03
0.00
0.00
0.00
in
0.00
0.36
0.00
0.00
0.00
Total Boring Volume
ft^3
0.00
0.01
0.00
0.00
0.00
Well Volume
ft^3
0.00
0.00
0.00
0.00
0.00
Annulus Volume
ft^3
0.00
0.00
0.00
0.00
0.00
Product Volume
ft^3
0.00
0.00
0.00
0.00
0.00
gal
0.00
0.03
0.00
0.00
0.00
oz
0.0
3.4
0.0
0.0
0.0
% Sock Capacity
%
0%
20%
0%
0%
0%
Sock Capacity
oz
17
17
17
17
17
gal
0.13
0.13
0.13
0.13
0.13
# of Socks
0
1
0
0
0
Sock % Full
0%
100%
0%
0%
0%
Old Sock Replaced (#)
0
0
0
0
0
New Sock Installed (#)
0
1
0
0
0
Sock Volume
gal
0.00
0.13
0.00
0.00
0.00
0.13
Bailed Volume
gal
0.00
0.00
0.00
0.00
0.00
0.00
Total Volume
gal
0.00
0.13
0.00
0.00
0.00
0.13
Notes:
Liquid levels measured after removing socks
Table 6
AFVR Data
Jefferson Pilot Communications - WBTV
III Charlotte, Mecklenburg County, North Carolina
Incident No. 7570
S&ME Project No. 4335-14-135A
Aggressive Fluid Vapor Recovery Date: 8/16/2022
Site Name and County: Jefferson Pilot Communications
Average depth to product/groundwater (in feet): MW-2 = _42.64 /_43.0 ft-TOC;
Indicate avg. Hydraulic Conductivity (if known): Unknown
List the well I.D. and diameter used for AFVR: MW-2, 2" diameter
List blower specifications: Press Vac Vacuum Truck: _20_ in Hg max,
Type of free product: Gasoline
Total gallons of product/water recovered, as measured from the vacuum truck tank (in gallons):
Emissions VOC meter and calibration gas: PID, Isobutylene
272
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd)
Date
Time as
8/16/2022 08:00(in-Hg)
Vacuum
Velocity
Pipe ID
Temp
Temp
Rel Humid
Water
Qstd
ft/min)
(in
*F
*K
%/100
Vapor %
flow
8/16/2022
8:00
20
2,248
6
163
345.93
0.2200
0.0514
331
8/16/2022
8:15
20
1,870
6
165
347.04
0.1800
0.0435
276
8/16/2022
8:30
20
1,780
6
180
355.37
0.0900
0.0300
261
8/16/2022
1 8:45
20
1,695
6
177
353.71
1 0.0360
0.0109
254
8/16/2022
9:00
20
1,470
6
168
348.71
0.0420
0.0104
224
8/16/2022
9:30
20
1,430
6
188
359.82
0.0350
0.0136
210
8/16/2022
10:00
20
1,388
6
200
366.48
0.0330
0.0165
200
8/16/2022
10:30
20
1,266
6
200
366.48
0.0300
0.0150
182
8/16/2022
11:00
20
1,330
6
200
366.48
0.0240
0.0119
1 192
8/16/2022
11:30
20
1,310
6
200
366.48
1 0.0240
0.0119
189
8/16/2022
12:00
20
1,414
6
200
366.48
0.0300
0.0150
204
8/16/2022
12:30
20
1,380
6
200
366.48
0.0240
0.0119
200
8/16/2022
13:00
20
1,366
6
200
366.48
0.0330
0.0165
197
8/16/2022
13:30
20
1,447
6
200
366.48
0.0300
0.0150
209
8/16/2022
14:00
20
1,410
6
200
366.48
0.0240
0.0119
204
8/16/2022
14:30
20
1,500
6
200
366.48
1 0.0280
0.0140
216
8/16/2022
15:00
20
1,369
6
200
366.48
0.0200
0.0099
198
8/16/2022
15:30
20
1,430
6
200
366.48
0.0210
0.0104
207
8/16/2022
16:00
1 20
1 1,354
1 6
200
366.48
0.0220
0.0109
196
Total Time
8 Hrs.
I Hours:Minutesl
480
NOTES
Qstd = Flow at DSCFM
Vacuum = The level of vacuum being applied should be recorded from the vacuum truck tank (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the vacuum truck)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)
Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Water Vapor in % = Pounds of water per pound of dry air, derived from the Psychrometric chart (temp Vs relative humidity)
EQUATION
Qstd = (1-Water Vapor) * velocity * (PI * (diameter/24)A2) * (5280R/(Temp + 460))
Table 6
AFVR Data
Jefferson Pilot Communications - WBTV
ICharlotte, Mecklenburg County, North Carolina
r' Incident No. 7570
S&ME Project No. 4335-14-135A
EMISSION CALCULATIONS
Elapsed
Time
Flow
VOC
K
PPM
Cg:m
Cg
PMRg
PMR
min
DSCFM
m
#C -gas)
m /dsm^3
Ib/dsc
Ib/hr(lb)
0
331
20.80
15
276
18.50
4
83
795
0.0000496
0.8
0.2
30
1 261
22.40
4
74
707
0.0000441
0.7
0.3
45
254
17.60
4
90
856
0.0000535
0.8
0.6
60
224
14.40
4
70
673
0.0000420
0.6
0.6
90
210
12.20
4
58
550
0.0000344
0.4
0.7
120
200
11.80
4
49
466
0.0000291
0.3
0.7
150
182
10.20
4
1 47
451
0.0000282
0.3
0.8
180
192
9.60
4
41
390
0.0000243
0.3
0.8
210
189
12.40
4
38
367
0.0000229
0.3
0.9
240
204
13.60
4
50
474
0.0000296
0.4
1.4
270
200
11.70
4
54
520
0.0000325
0.4
1.7
300
197
16.40
4
47
447
0.0000279
0.3
1:6
330
209
15.70
4
66
627
0.0000391
0.5
2.7
360
204
18.20
4
63
600
0.0000375
0.5
2.7
390
216
16.70
4
73
696
0.0000434
0.6
3.7
420
198
17.40
4
67
638
0.0000398
0.5
3.3
450
207
1 19.20
4
70
1 665
1 0.0000415
1 0.5
3.9
480
196
12.50
4
77
734
0.0000458
0.5
4.3
Total emissions in pounds 31.0
Total emissions in gallons 5.0
NOTES
PPM measured = Actual measurements (ppm) taken with a OVA or TVA at the blower discharge piping
K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, Isobutylene = 4, or Hexane K = 6)
PPMg = PPMv, Volumetric concentration as gasoline emission, dry basis at STP
Cg:m = mg/dsm3, mass concentration of gasoline emission
Mg = 105 mg/mg-mole, molecular weight of gasoline (this value may vary depending on contaminant)
K3 = 24.07 dsm^3/1 E6 mg -mole, mass to volume conversion factor at STP
Cg = Ib/dcsf, mass concentration of gasoline emission, dry basis at STP
PMRg = Ib/hr, pollutant mass removal rate of gasoline emission
PMR = pollutant mass removal of gasoline emission overtime
EQUATIONS
PPMg = PPM measured * K
Cg:m = PPMg * (Mg / K3)
Cg = Cg:m ' 62.43E-09 lb-MA3/mg-ft"3
PMRg = Cg * Qstd * 60 min/hr
PMR = PMRg * ((T2 - T1) / 60)
Appendix III - Field Sampling Forms
Project Name: Jefferson Pilot Communications
Project Location: 1 Julian Price Place, Charlotte NC I
Project Number: 210963
Date:
August 30, 2022
Weather: Sunny
Air Temp. ff):
80
Water Level & Well Data
Name Signature Date
(1) Matthew Brundage
Notes: All measurements were collected from the Top of Casing (TOC)
Well ID
Time
Flush Mount
/Stick Up
Depth to
Free
Product
(ft-TOC)
Depth to
Water
(ft-TOC)
Total Well
Depth
(ft-TOC)
Screen
Length
(feet)
Top of
Screen
Depth
(ft-TOC)
Free Product
Below Top of
Well Screen?
(Yes/No)
Free
Product
Thickness
(feet)
EW 1
Flush Mount
NP
42.77
56.9
Unknown
Unknown
Unknown
0.00
MW_1
Flush Mount
NP
46.75
53.8
15.0
38.8
NP
0.00
MW-2
Flush Mount
42.10
42.70
50.0
Unknown
Unknown
Unknown
0.60
MW-3
Flush Mount
NP
42.64
50.0
Unknown
Unknown
Unknown
0.00
MW-11
Flush Mount
NP
46.50
76.0
Unknown
Unknown
Unknown
0.00
Revision: 9/1/17 12:50 PM
Project Name:
Project Location:
Project Number:
Weather:
& Well Data
Jefferson Pilot Communications
1 Julian Price Place, Charlotte NC
210963
Sunny
Date:
Air Temp. ff):
III
October 7, 2022
77
Well ID
Time
Flush Mount
/ Stick Up
Depth to
Free
Product
(ft-TOC)
Depth to
Water
(ft-TOC)
Total Well
Depth
(ft-TOC)
Screen
Length
(feet)
Top of
Screen
Depth
(ft-TOC)
Free Product
Below Top of
Well Screen?
(Yes/No)
Free
Product
Thickness
(feet)
EW-1
Flush Mount
NP
38.95
56.9
Unknown
Unknown
Unknown
0.00
MW_1
Flush Mount
NP
47.09
53.8
15.0
38.8
NP
0.00
MW-2
Flush Mount
42.84
43.10
50.0
Unknown
Unknown
Unknown
0.26
MW-3
Flush Mount
NP
43.01
50.0
Unknown
Unknown
Unknown
0.00
MW-11
Flush Mount
NP
46.84
76.0
Unknown
Unknown
Unknown
0.00
I(1) Matthew Brund
All measurements were collected from the Top of Casing (TOC)
10/7/202211
Revision: 9/1/17 12:50 PM
Project Name: Jefferson Pilot Communications
i
Project Location: 1 Julian Price Place, Charlotte NC
Project Number: 210963
Date:
November 1, 2022
Weather: Sunny
Air Temp. ff):
68
Water Level & Well Data
Name Signature Date
��
(1) Matthew Brundage 11/1/2022
Notes: All measurements were collected from the Top of Casing (TOC)
Replaced sock in MW-2 with a new one. Completely saturated.
Well ID
Time
Flush Mount
/Stick Up
Depth to
Free
Product
(ft-TOC)
Depth to
Water
(ft-TOC)
Total Well
Depth
(ft-TOC)
Screen
Length
(feet)
Top of
Screen
Depth
(ft-TOC)
Free Product
Below Top of
Well Screen?
(Yes/No)
Free
Product
Thickness
(feet)
EW 1
Flush Mount
NP
38.98
56.9
Unknown
Unknown
Unknown
0.00
MW_1
Flush Mount
NP
47.15
53.8
15.0
38.8
NP
0.00
MW-2
Flush Mount
42.85
43.00
50.0
Unknown
Unknown
Unknown
0.15
MW-3
Flush Mount
NP
43.05
50.0
Unknown
Unknown
Unknown
0.00
MW-11
Flush Mount
NP
46.88
76.0
Unknown
Unknown
Unknown
0.00
Revision: 9/1/17 12:50 PM
Aggressive Fluid Vapor Recovery Date: 8/16/2022
Site Name and County: Jefferson Pilot Communications
UST Incident Number: 7570
Average depth to product/groundwater (in feet): MW-2 = DTP- 42.64/DTW-43.0
Indicate avg. Hydraulic Conductivity (if known): unknown
List the well I.D. and diameter used for AFVR: MW- 2: 2" diameter
List blower specifications: Press Vac Vacuum Truck: 20 in Hg max
Blower outlet pipe diameter: 6" in
Type of free product: Gasoline
Total gallons of product/water recovered, as measured from the vacuum truck tank: _ 227 Gals.
Emissions VOC meter and calibration gas: Mini -Rae PID, Isobutylene
Date
Time as
Vacuum
Velocity
Temp
PID/OVA
Rel Humid
(inches of Hg)
fps
(°F)
(ppm)
(%/100)
8/17/2022
8:00
20
2,248
163
20.80
22.0000
8/17/2022
8:15
20
1,870
165
18.50
18.0000
8/17/2022
1 8:30
20
1,780
180
22.40
9.0000
8/17/2022
8:45
20
1,695
177
17.60
3.6000
8/17/2022
9:00
20
1,470
168
14.40
4.2000
8/17/2022
9:30
20
1,430
188
12.20
3.5000
8/17/2022
10:00
20
1,388
>200
11.80
3.3000
8/17/2022
10:30
20
1,266
>200
10.20
3.0000
8/17/2022
11:00
20
1,330
>200
9.60
2.4000
8/17/2022
11:30
20
1,310
>200
12.40
2.4000
8/17/2022
12:00
20
1,414
>200
13.60
3.0000
8/17/2022
12:30
20
1,380
>200
11.70
2.4000
8/17/2022
13:00
20
1,366
>200
16.40
3.3000
8/17/2022
13:30
20
1,447
>200
15.70
3.0000
8/17/2022
14:00
20
1,410
>200
18.20
2.4000
8/17/2022
14:30
20
1,500
>200
16.70
2.8000
8/17/2022
15:00
20
1,369
>200
17.40
2.0000
8/17/2022
15:30
20
1,430
>200
19.20
2.1000
8/17/2022
16:00
20
1,354
>200
12.50
2.2000
16:00
Shutdown
Total Time
8hrs.
Hours:Minutes
480
Staff: Matthew Brundage F�
Fri;
Project Name:
Project Location:
Project Number:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
s
January 10, 2023
Source Well:
EW-1
Purge Time (Min.):
20
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage / Clark Appling
Sample Time:
11:45
Weather:
Sunny
Air Temp:
45 ° F
Measuring Point:
Top of Casing
Depth to Water:
43.85
ft-TOC
Total Well Depth:
56.90
ft-TOC
Height of Water Column:
13.05
feet
Screen Length:
20
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
4
inch
Well Volume
8.5
gal
3 * Well Volume
25.6
gal
5 * Well Volume
42.6
gal
Purge Method: Submersible Pump Purge Start Time: 11:25 End Time: 11:45
Total Volume Purged: 30.0 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
(NTU)
Comments
10.0
11:25
6.3
18.7
711
20.0
11:35
6.4
19.6
717
Clear
30.0
11:45
6.5
19.7
714
Clear
Sample Method: I Bailer Sample Time: 11:45
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250mL A
None
(1) Matthew Brundage
1/10/2023
Form Revision Date: 9/13/17 8:00 AM
Project Name:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
January 10, 2023
Project Location:
Project Number:
Source Well:
MW-1
Purge Time (Min.):
10
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage / Clark Appling
Sample Time:
12:05
Weather:
Sunny
Air Temp:
Measuring Point:
Top of Casing
Depth to Water:
47.27
ft-TOC
Total Well Depth:
53.84
ft-TOC
Height of Water Column:
6.57
feet
Screen Length:
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
2
inch
Well Volume
1.1
gal
3 * Well Volume
3.2
gal
5 * Well Volume
5.4
gal
Purge Method: Bailer Purge Start Time: 11:55 End Time: 12:05
Total Volume Purged: 3.0 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
(NTU)
Comments
1.0
11:55
6.4
19.7
932
2.0
12:00
6.5
19.2
964
Turbid
3.0
12:05
6.6
19.3
923
Sample Method: I Bailer Sample Time: 12:05
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250ml- A
None
(1) Matthew Brundage
1/10/2023
Form Revision Date: 9/13/17 8:00 AM
Fri;
Project Name:
Project Location:
Project Number:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
s
January 10, 2023
Source Well:
MW-3
Purge Time (Min.):
10
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage / Clark Appling
Sample Time:
10:35
Weather:
Sunny
Air Temp:
45 ° F
Measuring Point:
Top of Casing
Depth to Water:
42.80
ft-TOC
Total Well Depth:
50.00
ft-TOC
Height of Water Column:
7.20
feet
Screen Length:
15
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
2
inch
Well Volume
1.2
gal
3 * Well Volume
3.5
gal
5 * Well Volume
5.9
gal
Purge Method: Peristaltic Pump Purge Start Time: 10:25 End Time: 10:35
Total Volume Purged: 3.5 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
(NTU)
Comments
1.0
10:25
6.5
17.9
536
2.0
10:30
6.5
18.4
625
Turbid
3.5
10:35
6.6
18.5
535
Turbid
Sample Method: Bailer Sample Time: 10:35
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250mL A
None
(1) Matthew Brundage
1/10/2023
Form Revision Date: 9/13/17 8:00 AM
Project Name:
Project Location:
Project Number:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
January 10, 2023
Source Well:
MW-4
Purge Time (Min.):
10
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage /Clark appling
Sample Time:
14:30
Weather:
Sunny
Air Temp:
45 ° F
Measuring Point:
Top of Casing
Depth to Water:
41.24
ft-TOC
Total Well Depth:
50.00
ft-TOC
Height of Water Column:
8.76
feet
Screen Length:
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
2
inch
Well Volume
1.4
gal
3 * Well Volume
4.3
gal
5 * Well Volume
7.1
gal
Purge Method: Peristaltic Pump Purge Start Time: 14:20 End Time: 14:30
Total Volume Purged: 4.5 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
(NTU)
Comments
1.5
14:20
6.2
17.5
209
Clear
3.0
14:25
6.2
17.9
222
4.5
14:30
6.2
17.5
232
Turbid
Sample Method: I Bailer Sample Time: 14:30
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250ml- A
None
I(1) Matthew Brundage
�•-,.�f�.:.�.��{ram_• ._-��- �-
1/10/2023
Form Revision Date: 9/13/17 8:00 AM
Project Name:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
January 10, 2023
Project Location:
Project Number:
Source Well:
MW-6
Purge Time (Min.):
25
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage / Clark Appling
Sample Time:
10:10
Weather:
Sunny
Air Temp:
Measuring Point:
Top of Casing
Depth to Water:
35.60
ft-TOC
Total Well Depth:
49.59
ft-TOC
Height of Water Column:
13.99
feet
Screen Length:
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
2
inch
Well Volume
2.3
gal
3 * Well Volume
6.8
gal
5 * Well Volume
11.4
gal
Purge Method: Bailer Purge Start Time: 09:45 End Time: 10:10
Total Volume Purged: 7.0 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
Comments
2.5
09:50
6.4
17.8
545
turbid
5.0
10:00
6.3
18.1
530
Turbid
7.0
10:10
6.3
18.3
515
Turbid
Sample Method: I Bailer Sample Time: 10:10
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250ml- A
None
(1) Matthew Brundage
1/10/2023
Form Revision Date: 9/13/17 8:00 AM
Project Name:
Project Location:
Project Number:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
January 10, 2023
Source Well:
MW-7
Purge Time (Min.):
15
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage / Clarck Appling
Sample Time:
13:30
Weather:
Sunny
Air Temp:
45 ° F
Measuring Point:
Top of Casing
Depth to Water:
29.67
ft-TOC
Total Well Depth:
49.00
ft-TOC
Height of Water Column:
19.33
feet
Screen Length:
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
2
inch
Well Volume
3.2
gal
3 * Well Volume
9.5
gal
5 * Well Volume
15.8
gal
Purge Method: Peristaltic Pump Purge Start Time: 13:15 End Time: 13:30
Total Volume Purged: 9.0 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
(NTU)
Comments
3.0
13:15
6.2
17.1
148
Clear
6.0
13:22
6.1
17
148
9.0
13:30
6.2
16.6
153
Turbid
Sample Method: I Bailer I Sample Time: 13:30
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250ml- A
None
I(1) Matthew Brundage
�•-,.�f�.:.�.��{ram_• ._-��- �-
1/10/2023
Form Revision Date: 9/13/17 8:00 AM
Project Name:
Project Location:
Project Number:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
January 10, 2023
Source Well:
MW-8
Purge Time (Min.):
10
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage / Clarck Appling
Sample Time:
14:10
Weather:
Sunny
Air Temp:
45 ° F
Measuring Point:
Top of Casing
Depth to Water:
33.45
ft-TOC
Total Well Depth:
44.00
ft-TOC
Height of Water Column:
10.55
feet
Screen Length:
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
2
inch
Well Volume
1.7
gal
3 * Well Volume
5.2
gal
5 * Well Volume
8.6
gal
Purge Method: Peristaltic Pump Purge Start Time: 14:00 End Time: 14:10
Total Volume Purged: 6.0 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
(NTU)
Comments
2.0
14:00
6.1
16.5
153
Clear
4.0
14:05
6.1
16.8
153
6.0
14:10
6.2
16.8
153
Turbid
Sample Method: I Bailer Sample Time: 14:10
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250ml- A
None
I(1) Matthew Brundage
�•-,.�f�.:.�.��{ram_• ._-��- �-
1/10/2023
Form Revision Date: 9/13/17 8:00 AM
Fri;
Project Name:
Project Location:
Project Number:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
s
January 10, 2023
Source Well:
MW-9
Purge Time (Min.):
10
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage / Clarck Appling
Sample Time:
12:35
Weather:
Sunny
Air Temp:
45 ° F
Measuring Point:
Top of Casing
Depth to Water:
53.15
ft-TOC
Total Well Depth:
60.76
ft-TOC
Height of Water Column:
7.61
feet
Screen Length:
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
2
inch
Well Volume
1.2
gal
3 * Well Volume
3.7
gal
5 * Well Volume
6.2
gal
Purge Method: Peristaltic Pump Purge Start Time: 12:25 End Time: 12:35
Total Volume Purged: 3.5 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
(NTU)
Comments
1.0
12:25
6.6
18.5
501
Clear
2.0
12:30
6.6
18.3
456
3.5
12:35
6.3
18.5
460
Turbid
Sample Method: I Bailer Sample Time: 12:35
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250mL A
None
(1) Matthew Brundage
1/10/2023
Form Revision Date: 9/13/17 8:00 AM
Fri;
Project Name:
Project Location:
Project Number:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
s
January 10, 2023
Source Well:
MW-10
Purge Time (Min.):
15
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage / Clarck Appling
Sample Time:
13:00
Weather:
Sunny
Air Temp:
45 ° F
Measuring Point:
Top of Casing
Depth to Water:
52.27
ft-TOC
Total Well Depth:
63.00
ft-TOC
Height of Water Column:
10.73
feet
Screen Length:
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
2
inch
Well Volume
1.8
gal
3 * Well Volume
5.3
gal
5 * Well Volume
8.8
gal
Purge Method: Peristaltic Pump Purge Start Time: 12:45 End Time: 13:00
Total Volume Purged: 6.0 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
(NTU)
Comments
2.0
12:45
6.6
19.5
172
4.0
12:52
6.3
19.5
163
Turbid
6.0
13:00
6.4
19.4
160
Turbid
Sample Method: I Bailer Sample Time: 13:00
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250mL A
None
(1) Matthew Brundage
1/10/2023
Form Revision Date: 9/13/17 8:00 AM
Project Name:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
January 10, 2023
Project Location:
Project Number:
Source Well:
MW-11
Purge Time (Min.):
15
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage / Clarck Appling
Sample Time:
11:10
Weather:
Sunny
Air Temp:
Measuring Point:
Top of Casing
Depth to Water:
46.60
ft-TOC
Total Well Depth:
75.96
ft-TOC
Height of Water Column:
29.36
feet
Screen Length:
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
2
inch
Well Volume
4.8
gal
3 * Well Volume
14.4
gal
5 * Well Volume
24.0
gal
Purge Method: Peristaltic Pump Purge Start Time: 10:55 End Time: 11:10
Total Volume Purged: 15.0 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
(NTU)
Comments
5.0
10:55
6.1
18
17
10.0
11:05
6.1
18.7
15
15.0
11:10
Sample Method: I Bailer I Sample Time: 11:10
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250ml- A
None
(1) Matthew Brundage
1/10/2023
Form Revision Date: 9/13/17 8:00 AM
Fri;
Project Name:
Project Location:
Project Number:
WBTV Jefferson Pilot Communications
One Julian Price Place, Charlotte, Noth Carolina
210963 TA-25
Purge Date:
s
January 10, 2023
Source Well:
MW-12
Purge Time (Min.):
10
Locked?:
Yes
Sample Date:
January 10, 2023
Sampled By:
Matthew Brundage / Clarck Appling
Sample Time:
14:50
Weather:
Sunny
Air Temp:
45 ° F
Measuring Point:
Top of Casing
Depth to Water:
39.61
ft-TOC
Total Well Depth:
50.60
ft-TOC
Height of Water Column:
10.99
feet
Screen Length:
20
ft-GRD
Stickup Height:
ft-GRD
Purging Information
Well Volume
Well Diameter
2
inch
Well Volume
1.8
gal
3 * Well Volume
5.4
gal
5 * Well Volume
9.0
gal
Purge Method: Peristaltic Pump Purge Start Time: 14:40 End Time: 14:50
Total Volume Purged: 6.0 gal Well Purged Dry?: No
Cumulative Volume
(Gal)
Time
pH
(s.u.)
Temp
(°C)
Cond
PS/Cm
Turbidity
(NTU)
Comments
2.0
14:40
6.1
18
115
4.0
14:45
6.2
19.4
113
6.0
14:50
Sample Method: Bailer Sample Time: 14:50
Method
Qty
Container
Pres.
Method
Qty
Container
Pres.
VOCs 6200
3
40mL VOAs
HCI
SVOCs 625
2
250mL A
None
(1) Matthew Brundage
•�-��f�� - 2/21/2023
Form Revision Date: 9/13/17 8:00 AM
Appendix IV - Laboratory Analytical Report and Chain -of -Custody
Report
Waypointo
ANALYTICAL
1 /19/2023
S&ME, Inc - Charlotte
Lucas-Barroso-Giachetti
2016 Ayrsley Town Blvd .2Suite 2-A
Suite 2-A
Charlotte, NC, 28273
Ref: Analytical Testing
Lab Report Number: 23-011-0018
Client Project Description: Jefferson Pilot Comm
Dear Lucas-Barroso-Giachetti:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/11/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 118
Waypointo
ANALYTICAL
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytica Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2023
North Carolina
State Program
402
12/31/2023
South Carolina
State Program
99012
07/31/2023
South Carolina
State Program
99012
12/31/2022
Page 1 of 1 00016/23-011-0018
Page 2 of 118
•
Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Sample Summary Table
Report Number: 23-011-0018
Client Project Description: Jefferson Pilot Comm
Lab No Client Sample ID Matrix Date Collected Date Received
97322
EW-1
Aqueous
01/10/2023
11:45
01/11/2023
13:20
97323
MW-1
Aqueous
01/10/2023
12:05
01/11/2023
13:20
97324
MW-3
Aqueous
01/10/2023
10:35
01/11/2023
13:20
97325
MW-4
Aqueous
01/10/2023
14:30
01/11/2023
13:20
97326
MW-6
Aqueous
01/10/2023
10:10
01/11/2023
13:20
97327
MW-7
Aqueous
01/10/2023
13:30
01/11/2023
13:20
97328
MW-8
Aqueous
01/10/2023
14:10
01/11/2023
13:20
97329
MW-9
Aqueous
01/10/2023
12:35
01/11/2023
13:20
97330
MW-10
Aqueous
01/10/2023
13:00
01/11/2023
13:20
97331
MW-11
Aqueous
01/10/2023
11:10
01/11/2023
13:20
97332
MW-12
Aqueous
01/10/2023
14:50
01/11/2023
13:20
Page 3 of 118
(D
Waypo�•
a
nt
449 5pringbrook
Rd, Charlotte, NC
28217
,
Main 704.529.6364
ANALYTICAL
www.waypointanalytiw I som
Summary of Detected Analytes
Project:
Jefferson Pilot Comm
Report Number:
23-011-0018
Client Sample ID
Lab Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
EW-1
V 97322
6200B
Acetone
22.0
pg/L
18.0
01/17/2023 09:48
1
6200E
Benzene
1570
pq/L
18.0
01/18/202310:30
6200E
n-Butylbenzene
5.60
pg/L
1.80
01/17/2023 09:48
6200E
sec -Butyl benzene
2.55
pq/L
2.00
01/17/2023 09:48
1
6200E
Di -Isopropyl Ether (DIPE)
5970
pg/L
50.0
01/18/2023 10:30
6200E
Ethylbenzene
350
pq/L
1.70
01/17/2023 09:48
6200E
2-Hexanone
13.6
pg/L
3.80
01/17/2023 09:48
6200E
Isopropylbenzene
15.3
pq/L
1.80
01/17/2023 09:48
6200E
4-Isopropyl toluene
3.63
pg/L
0.890
01/17/2023 09:48
1
6200E
Methyl tert-butyl ether (MTBE)
443
pq/L
1.40
01/17/2023 09:48
6200E
4-Methyl-2-Pentanone
7.78
pg/L
0.780
01/17/2023 09:48
1
6200E
Naphthalene
355
pq/L
4.70
01/17/2023 09:48
6200E
n-Propylbenzene
27.3
pg/L
1.90
01/17/2023 09:48
6200E
Toluene
30.2
pq/L
2.20
01/17/2023 09:48
6200E
1,2,4-Trimethylbenzene
186
pq/L
1.90
01/17/2023 09:48
6200E
1,3,5-Trimethylbenzene
28.4
pq/L
1.80
01/17/2023 09:48
6200E
o-Xylene
16.1
pg/L
2.10
01/17/2023 09:48
6200E
m,p-Xylene
391
pq/L
4.20
01/17/2023 09:48
6200E
Xylene (Total)
407
pg/L
2.10
01/17/2023 09:48
625.1
2,4-Dimethylphenol
11.9
pq/L
1.57
01/17/202316:46
1
625.1
1-Methylnaphthalene
111
pg/L
1.14
01/17/202316:46
625.1
2-Methylnaphthalene
163
pq/L
0.666
01/17/202316:46
625.1
Naphthalene
160
pg/L
0.728
01/17/202316:46
MW-1
V 97323
6200E
Acetone
85.8
pg/L
18.0
01/17/2023 10:13
1
6200E
Benzene
1110
pq/L
18.0
01/18/202310:56
6200E
n-Butylbenzene
6.43
pg/L
1.80
01/17/2023 10:13
6200E
sec -Butyl benzene
2.30
pq/L
2.00
01/17/2023 10:13
1
6200E
Di -Isopropyl Ether (DIPE)
7260
pg/L
50.0
01/18/2023 10:56
6200E
Ethylbenzene
97.3
pq/L
1.70
01/17/2023 10:13
6200E
2-Hexanone
47.0
pg/L
3.80
01/17/2023 10:13
6200E
Isopropylbenzene
8.93
pq/L
1.80
01/17/2023 10:13
6200E
4-Isopropyl toluene
3.99
pg/L
0.890
01/17/2023 10:13
1
6200E
Methyl Ethyl Ketone (MEK)
44.0
pq/L
7.10
01/17/2023 10:13
1
6200E
Methyl tert-butyl ether (MTBE)
793
pg/L
1.40
01/17/2023 10:13
6200E
Naphthalene
402
pq/L
4.70
01/17/2023 10:13
Page 4 of 118
Waypoint.:(D
ANALYTICAL
Project: Jefferson Pilot Comm
Report Number: 23-011-0018
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytica Isom
Summary of Detected
Client Sample ID
Method
Lab Sample ID
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
MW-1
V 97323
6200B
n-Propylbenzene
11.4
pg/L
1.90
01/17/202310:13
6200E
Toluene
59.8
pq/L
2.20
01/17/202310:13
6200E
1,2,4-Trimethylbenzene
170
pg/L
1.90
01/17/202310:13
6200E
1,3,5-Trimethylbenzene
68.5
pq/L
1.80
01/17/202310:13
6200E
o-Xylene
25.5
pg/L
2.10
01/17/202310:13
6200E
m,p-Xylene
301
pq/L
4.20
01/17/202310:13
6200E
Xylene (Total)
327
pg/L
2.10
01/17/2023 10:13
625.1
Fluorene
22.9
pg/L
0.807
01/17/202317:09
625.1
1-Methylnaphthalene
320
pg/L
4.56
01/19/202313:50
625.1
2-Methylnaphthalene
501
pq/L
2.66
01/19/202313:50
625.1
Naphthalene
252
pg/L
2.91
01/19/202313:50
625.1
Phenanthrene
54.1
pq/L
0.428
01/17/202317:09
625.1
Pyrene
1.80
pg/L
0.434
01/17/202317:09
1
MW-3
V 97324
6200E
Acetone
45.9
pg/L
18.0
01/19/2023 09:00
1
6200E
Benzene
16.1
pq/L
1.80
01/19/2023 09:00
6200E
n-Butylbenzene
6.55
pg/L
1.80
01/19/2023 09:00
6200E
sec -Butyl benzene
2.97
pq/L
2.00
01/19/2023 09:00
1
6200E
Di -Isopropyl Ether (DIPE)
7.17
pg/L
5.00
01/19/2023 09:00
6200E
Isopropylbenzene
7.41
pq/L
1.80
01/19/2023 09:00
6200E
4-Isopropyl toluene
6.12
pg/L
0.890
01/19/2023 09:00
6200E
Naphthalene
356
pq/L
4.70
01/19/2023 09:00
6200E
n-Propylbenzene
3.13
pg/L
1.90
01/19/2023 09:00
1
6200E
1,2,4-Trimethylbenzene
161
pq/L
1.90
01/19/2023 09:00
6200E
1,3,5-Trimethylbenzene
58.2
pg/L
1.80
01/19/2023 09:00
6200E
o-Xylene
27.4
pq/L
2.10
01/19/2023 09:00
6200E
m,p-Xylene
46.9
pg/L
4.20
01/19/2023 09:00
6200E
Xylene (Total)
74.3
pq/L
2.10
01/19/2023 09:00
625.1
1-Methylnaphthalene
164
pg/L
1.23
01/17/202316:01
625.1
2-Methylnaphthalene
205
pq/L
0.719
01/17/202316:01
625.1
Naphthalene
204
pg/L
0.786
01/17/202316:01
625.1
Phenanthrene
16.4
pq/L
0.462
01/17/202316:01
MW-4
V 97325
6200E
Benzene
2.05
pq/L
1.80
01/18/2023 09:15
1
6200E
n-Butylbenzene
2.13
pg/L
1.80
01/18/2023 09:15
1
6200E
Di -Isopropyl Ether (DIPE)
46.0
pq/L
5.00
01/18/2023 09:15
Page 5 of 118
Waypoint.:(D
ANALYTICAL
Project: Jefferson Pilot Comm
Report Number: 23-011-0018
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytica Isom
Summary of Detected
Client Sample ID
Method
Lab Sample ID
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
MW-4
V 97325
6200B
Isopropylbenzene
2.95
pg/L
1.80
01/18/2023 09:15
1
6200E
Methyl tert-butyl ether (MTBE)
3.60
pq/L
1.40
01/18/2023 09:15
1
6200E
Naphthalene
125
pg/L
4.70
01/18/2023 09:15
6200E
1,2,4-Trimethylbenzene
13.4
pq/L
1.90
01/18/2023 09:15
6200E
o-Xylene
2.18
pg/L
2.10
01/18/2023 09:15
1
6200E
Xylene (Total)
2.18
pq/L
2.10
01/18/2023 09:15
1
625.1
Acenaphthene
2.12
pg/L
0.321
01/17/202317:31
1
625.1
Fluorene
2.47
pg/L
0.859
01/17/202317:31
625.1
1-Methylnaphthalene
20.1
pg/L
1.21
01/17/202317:31
625.1
2-Methylnaphthalene
27.0
pq/L
0.709
01/17/202317:31
625.1
Naphthalene
19.3
pg/L
0.775
01/17/202317:31
625.1
Phenanthrene
4.75
pq/L
0.455
01/17/202317:31
MW-6
V 97326
6200E
Acetone
6.98
pq/L
1.80
01/18/2023 04:38
1
6200E
Benzene
1.82
pg/L
0.180
01/18/2023 04:38
6200E
n-Butylbenzene
2.71
pq/L
0.180
01/18/2023 04:38
6200E
sec -Butyl benzene
2.64
pg/L
0.200
01/18/2023 04:38
6200E
tert-Butyl benzene
1.37
pq/L
0.920
01/18/2023 04:38
1
6200E
Chloroform
3.66
pg/L
0.220
01/18/2023 04:38
6200E
Ethylbenzene
0.653
pq/L
0.170
01/18/2023 04:38
6200E
Isopropylbenzene
6.42
pg/L
0.180
01/18/2023 04:38
6200E
4-Isopropyl toluene
3.37
pq/L
0.089
01/18/2023 04:38
6200E
Methyl Ethyl Ketone (MEK)
1.64
pg/L
0.710
01/18/2023 04:38
1
6200E
Naphthalene
323
pq/L
4.70
01/19/2023 09:25
6200E
n-Propylbenzene
1.21
pg/L
0.190
01/18/2023 04:38
6200E
Toluene
0.223
pq/L
0.220
01/18/2023 04:38
1
6200E
1,2,4-Trimethylbenzene
85.5
pg/L
0.190
01/18/2023 04:38
6200E
1,3,5-Trimethylbenzene
34.9
pq/L
0.180
01/18/2023 04:38
6200E
o-Xylene
5.61
pg/L
0.210
01/18/2023 04:38
6200E
m,p-Xylene
38.0
pq/L
0.420
01/18/2023 04:38
6200E
Xylene (Total)
43.6
pg/L
0.210
01/18/2023 04:38
625.1
Acenaphthene
2.35
pq/L
0.333
01/18/202317:42
625.1
Dibenzofuran
4.31
pg/L
0.945
01/18/202317:42
1
625.1
Fluorene
26.9
pq/L
0.891
01/18/202317:42
625.1
1-Methylnaphthalene
108
pg/L
1.26
01/18/202317:42
625.1
2-Methylnaphthalene
147
pq/L
0.735
01/18/202317:42
Page 6 of 118
•
Waypoint.
(2) 449 Springbrook
Rd, Charlotte, NC
28217
Main 704.529.6364
ANALYTICAL
www.waypointana lyti ca I som
Summary of Detected Analytes
Project:
Jefferson Pilot Comm
Report Number: 23-011-0018
Client Sample ID Lab Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
MW-6
V 97326
625.1
Naphthalene
149
pq/L
0.804
01/18/202317:42
625.1
Phenanthrene
4.52
pq/L
0.472
01/18/202317:42
MW-7
V 97327
6200B
Chloroform
2.53
pq/L
0.220
01/18/2023 05:03
6200B
1,1-Dichloroethene
1.55
pq/L
0.150
01/18/2023 05:03
6200B
cis- 1,2-Dichloroethene
1.14
pq/L
0.200
01/18/2023 05:03
6200B
Naphthalene
19.2
pq/L
0.470
01/18/2023 05:03
6200B
Tetrachloroethene
1.45
pq/L
0.220
01/18/2023 05:03
6200B
Trichloroethene
2.03
uq/L
0.180
01/18/2023 05:03
6200B
1,2,4-Trimethyl benzene
0.437
pq/L
0.190
01/18/2023 05:03
1
6200B
1,3,5-Trimethyl benzene
0.289
pq/L
0.180
01/18/2023 05:03
1
MW-8
V 97328
6200B
Chloroform
0.971
pq/L
0.220
01/18/2023 05:28
6200B
1,1-Dichloroethene
1.33
pq/L
0.150
01/18/2023 05:28
6200B
cis- 1,2-Dichloroethene
2.06
uq/L
0.200
01/18/2023 05:28
6200B
Naphthalene
2.05
pq/L
0.470
01/18/2023 05:28
6200B
Tetrachloroethene
1.94
uq/L
0.220
01/18/2023 05:28
6200B
Trichloroethene
3.48
pq/L
0.180
01/18/2023 05:28
MW-9
V 97329
6200B
Acetone
5.82
pq/L
1.80
01/19/2023 08:09
1
6200B
Benzene
0.315
pq/L
0.180
01/19/2023 08:09
1
6200B
n-Butylbenzene
1.06
pq/L
0.180
01/19/2023 08:09
6200B
sec -Butyl benzene
0.981
pq/L
0.200
01/19/2023 08:09
6200B
tert-Butyl benzene
1.22
pq/L
0.920
01/19/2023 08:09
1
6200B
Di -Isopropyl Ether (DIPE)
1.01
uq/L
0.500
01/19/2023 08:09
6200B
Ethylbenzene
1.94
pq/L
0.170
01/19/2023 08:09
6200B
Isopropylbenzene
1.66
uq/L
0.180
01/19/2023 08:09
6200B
4-Isopropyl toluene
2.26
pq/L
0.089
01/19/2023 08:09
6200B
4-Methyl-2-Pentanone
2.66
uq/L
0.078
01/19/2023 08:09
6200B
Methylene Chloride
0.404
pq/L
0.330
01/19/2023 08:09
1
6200B
Naphthalene
88.4
uq/L
0.470
01/19/2023 08:09
6200B
n-Propylbenzene
2.87
pq/L
0.190
01/19/2023 08:09
6200B
Toluene
2.13
uq/L
0.220
01/19/2023 08:09
6200B
1,2,4-Trimethyl benzene
33.0
pq/L
0.190
01/19/2023 08:09
6200B
1,3,5-Trimethyl benzene
3.89
pq/L
0.180
01/19/2023 08:09
Page 7 of 118
Waypoint.(2)
ANALYTICAL
Sumi
Project: Jefferson Pilot Comm
Report Number: 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
of Detected
Client Sample ID
Method
Lab Sample ID
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
MW-9
V 97329
6200B
o-Xylene
5.51
pq/L
0.210
01/19/2023 08:09
6200B
m,p-Xylene
11.3
pq/L
0.420
01/19/2023 08:09
6200B
Xylene (Total)
16.8
pq/L
0.210
01/19/2023 08:09
625.1
Fluorene
5.35
pq/L
0.839
01/18/202318:27
625.1
1-Methylnaphthalene
52.1
pq/L
1.19
01/18/202318:27
625.1
2-Methylnaphthalene
60.9
pq/L
0.692
01/18/202318:27
625.1
Naphthalene
37.2
pq/L
0.757
01/18/202318:27
625.1
Phenanthrene
6.09
pq/L
0.445
01/18/202318:27
MW-10
V 97330
6200B
Chloroform
0.537
pq/L
0.220
01/18/2023 05:54
6200B
1,1-Dichloroethene
0.374
pq/L
0.150
01/18/2023 05:54 1
6200B
cis- 1,2-Dichloroethene
11.4
pq/L
0.200
01/18/2023 05:54
6200B
trans-1,2-Dichloroethene
0.633
pq/L
0.180
01/18/2023 05:54
6200B
Tetrachloroethene
6.96
pq/L
0.220
01/18/2023 05:54
6200B
Trichloroethene
16.1
pq/L
0.180
01/18/2023 05:54
MW-11
V 97331
6200B
Acetone
2.61
pq/L
1.80
01/18/2023 06:19 1
MW-12
V 97332
6200B
Chloroform
1.40
pq/L
0.220
01/18/2023 06:44
6200B
cis- 1,2-Dichloroethene
0.870
pq/L
0.200
01/18/2023 06:44
6200B
Tetrachloroethene
0.765
pq/L
0.220
01/18/2023 06:44
6200B
Trichloroethene
1.13
pq/L
0.180
01/18/2023 06:44
Page 8 of 118
Waypointo
ANALYTICAL
Client: S&ME, Inc - Charlotte
Project: Jefferson Pilot Comm
Lab Report Number: 23-011-0018
Date: 1 /19/2023
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
CASE NARRATIVE
625.1 - Base/Neutrals and Acids by GC/MS Method 625.1
Sample 97323 (MW-1)
Analyte: 2-Fluorophenol
QC Batch No: V29017/V28891
Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the
extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory
Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due
to the sample matrix.
Analyte: Benzidine
QC Batch No: V29002/V28891
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Benzoic Acid
QC Batch No: V29002/V28891
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Volatile Organic Compounds - GUMS Method 6200B
Analyte: Carbon Tetrachloride
QC Batch No: V28980/V28947
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 1,2-Dibromo-3-chloropropane
QC Batch No: V28980/V28947
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 9 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97322
Matrix: Aqueous
Sample ID: EW-1
Sampled:
1/10/2023 11:45
Analytical Method: 6200E
Prep Batch(es):
V28947
01/16/23 14:00
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
22.03
N9/L
18.0
100
10
01/17/23 09:48
MSA
V28948
Benzene
1570
N9/L
18.0
50.0
100
01/18/23 10:30
MSA
V28980
Bromobenzene
<2.10
N9/L
2.10
5.00
10
01/17/23 09:48
MSA
V28948
Bromochloromethane
<4.20
N9/L
4.20
10.0
10
01/17/23 09:48
MSA
V28948
Bromodichloromethane
<1.60
N9/L
1.60
5.00
10
01/17/23 09:48
MSA
V28948
Bromoform
<15.0
N9/L
15.0
50.0
10
01/17/23 09:48
MSA
V28948
Bromomethane
<2.80
N9/L
2.80
10.0
10
01/17/23 09:48
MSA
V28948
n-Butylbenzene
5.60
N9/L
1.80
5.00
10
01/17/23 09:48
MSA
V28948
sec -Butyl benzene
2.553
N9/L
2.00
5.00
10
01/17/23 09:48
MSA
V28948
tert-Butyl benzene
<9.20
N9/L
9.20
20.0
10
01/17/23 09:48
MSA
V28948
Carbon Tetrachloride
<1.80
N9/L
1.80
5.00
10
01/17/23 09:48
MSA
V28948
Chlorobenzene
<1.90
N9/L
1.90
5.00
10
01/17/23 09:48
MSA
V28948
Chlorodibromomethane
<1.90
N9/L
1.90
5.00
10
01/17/23 09:48
MSA
V28948
Chloroethane
<4.30
N9/L
4.30
10.0
10
01/17/23 09:48
MSA
V28948
Chloroform
<2.20
N9/L
2.20
5.00
10
01/17/23 09:48
MSA
V28948
Chloromethane
<2.20
N9/L
2.20
5.00
10
01/17/23 09:48
MSA
V28948
2-Chlorotoluene
<2.00
N9/L
2.00
5.00
10
01/17/23 09:48
MSA
V28948
4-Chlorotoluene
<2.00
N9/L
2.00
5.00
10
01/17/23 09:48
MSA
V28948
Di -Isopropyl Ether (DIPE)
5970
N9/L
50.0
50.0
100
01/18/23 10:30
MSA
V28980
1,2-Dibromo-3-Chloropropane
<11.0
N9/L
11.0
20.0
10
01/17/23 09:48
MSA
V28948
1,2-Dibromoethane
<2.00
N9/L
2.00
5.00
10
01/17/23 09:48
MSA
V28948
Dibromomethane
<2.30
N9/L
2.30
5.00
10
01/17/23 09:48
MSA
V28948
1,2-Dichlorobenzene
<2.20
N9/L
2.20
5.00
10
01/17/23 09:48
MSA
V28948
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 10 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97322
Matrix: Aqueous
Sample ID: EW-1
Sampled:
1/10/2023 11:45
Analytical Method: 6200E
Prep Batch(es):
V28947
01/16/23 14:00
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<1.90
N9/L
1.90
5.00
10
01/17/23 09:48
MSA
V28948
1,4-Dichlorobenzene
<2.10
N9/L
2.10
5.00
10
01/17/23 09:48
MSA
V28948
Dichlorodifluoromethane
<12.0
N9/L
12.0
50.0
10
01/17/23 09:48
MSA
V28948
1,1-Dichloroethane
<2.40
N9/L
2.40
5.00
10
01/17/23 09:48
MSA
V28948
1,2-Dichloroethane
<1.50
N9/L
1.50
5.00
10
01/17/23 09:48
MSA
V28948
1,1-Dichloroethene
<1.50
N9/L
1.50
5.00
10
01/17/23 09:48
MSA
V28948
cis- 1,2-Dich loroethene
<2.00
N9/L
2.00
5.00
10
01/17/23 09:48
MSA
V28948
trans- 1, 2-Dichloroethene
<1.80
N9/L
1.80
5.00
10
01/17/23 09:48
MSA
V28948
1,2-Dichloropropane
<1.90
N9/L
1.90
5.00
10
01/17/23 09:48
MSA
V28948
1,3-Dichloropropane
<1.30
N9/L
1.30
5.00
10
01/17/23 09:48
MSA
V28948
2,2-Dichloropropane
<2.10
N9/L
2.10
20.0
10
01/17/23 09:48
MSA
V28948
1,1-Dichloropropene
<2.00
N9/L
2.00
5.00
10
01/17/23 09:48
MSA
V28948
cis-1,3-Dichloropropene
<2.10
N9/L
2.10
5.00
10
01/17/23 09:48
MSA
V28948
trans-1,3-Dichloropropene
<1.50
N9/L
1.50
5.00
10
01/17/23 09:48
MSA
V28948
Ethanol
<420
N9/L
420
2000
10
01/17/23 09:48
MSA
V28948
Ethylbenzene
350
N9/L
1.70
5.00
10
01/17/23 09:48
MSA
V28948
Hexachlorobutadiene
<3.50
N9/L
3.50
30.0
10
01/17/23 09:48
MSA
V28948
2-Hexanone
13.6
N9/L
3.80
10.0
10
01/17/23 09:48
MSA
V28948
Isopropyl benzene
15.3
N9/L
1.80
5.00
10
01/17/23 09:48
MSA
V28948
4-Isopropyl toluene
3.633
N9/L
0.890
5.00
10
01/17/23 09:48
MSA
V28948
Methyl Ethyl Ketone (MEK)
<7.10
N9/L
7.10
50.0
10
01/17/23 09:48
MSA
V28948
Methyl tert-butyl ether (MTBE)
443
N9/L
1.40
10.0
10
01/17/23 09:48
MSA
V28948
4-Methyl-2-Pentanone
7.783
N9/L
0.780
10.0
10
01/17/23 09:48
MSA
V28948
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 11 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97322
Matrix: Aqueous
Sample ID: EW-1
Sampled:
1/10/2023 11:45
Analytical Method: 6200E
Prep Batch(es):
V28947
01/16/23 14:00
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
<3.30
N9/L
3.30
20.0
10
01/17/23 09:48
MSA
V28948
Naphthalene
355
N9/L
4.70
10.0
10
01/17/23 09:48
MSA
V28948
n-Propylbenzene
27.3
N9/L
1.90
5.00
10
01/17/23 09:48
MSA
V28948
Styrene
<2.20
N9/L
2.20
5.00
10
01/17/23 09:48
MSA
V28948
1,1,1,2-Tetrachloroethane
<1.60
N9/L
1.60
5.00
10
01/17/23 09:48
MSA
V28948
1,1,2,2-Tetrachloroethane
<1.60
N9/L
1.60
5.00
10
01/17/23 09:48
MSA
V28948
Tetrachloroethene
<2.20
N9/L
2.20
5.00
10
01/17/23 09:48
MSA
V28948
Toluene
30.2
N9/L
2.20
5.00
10
01/17/23 09:48
MSA
V28948
1,2,3-Trichlorobenzene
<3.80
N9/L
3.80
5.00
10
01/17/23 09:48
MSA
V28948
1,2,4-Trichlorobenzene
<3.10
N9/L
3.10
5.00
10
01/17/23 09:48
MSA
V28948
1, 1, 1 -Trich loroetha ne
<1.60
N9/L
1.60
5.00
10
01/17/23 09:48
MSA
V28948
1,1,2-Trichloroethane
<0.960
N9/L
0.960
5.00
10
01/17/23 09:48
MSA
V28948
Trichloroethene
<1.80
N9/L
1.80
5.00
10
01/17/23 09:48
MSA
V28948
Trichlorofluoromethane
<1.80
N9/L
1.80
5.00
10
01/17/23 09:48
MSA
V28948
1,2,3-Trichloropropane
<2.70
N9/L
2.70
5.00
10
01/17/23 09:48
MSA
V28948
1,2,4-Trimethyl benzene
186
N9/L
1.90
5.00
10
01/17/23 09:48
MSA
V28948
1,3,5-Trimethyl benzene
28.4
N9/L
1.80
5.00
10
01/17/23 09:48
MSA
V28948
Vinyl Acetate
<10.0
N9/L
10.0
50.0
10
01/17/23 09:48
MSA
V28948
Vinyl Chloride
<1.70
N9/L
1.70
5.00
10
01/17/23 09:48
MSA
V28948
o-Xylene
16.1
N9/L
2.10
5.00
10
01/17/23 09:48
MSA
V28948
m,p-Xylene
391
N9/L
4.20
10.0
10
01/17/23 09:48
MSA
V28948
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 12 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97322 Matrix: Aqueous
Sample ID: EW-1 Sampled: 1/10/2023 11:4S
Analytical Method: 6200E Prep Batch(es): V28947 01/16/23 14:00 V28979 01/17/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
407
N9/L
2.10 5.00
10 01/17/23 09:48
V28948
Surrogate: 4-Bromofluorobenzene
103
Limits: 70-130%
10 01/17/23 09:48 MSA
V28948
Surrogate: Dibromofluoromethane
98.8
Limits: 70-130%
10 01/17/23 09:48 MSA
V28948
Surrogate: 1,2-Dichloroethane - d4
99.2
Limits: 70-130%
10 01/17/23 09:48 MSA
V28948
Surrogate: Toluene-d8
96.6
Limits: 70-130%
10 01/17/23 09:48 MSA
V28948
Surrogate:4-Bromofluorobenzene
99.4
Limits: 70-130%
100 01/18/23 10:30 MSA
V28980
Surrogate: Dibromofluoromethane
94.8
Limits: 70-130%
100 01/18/23 10:30 MSA
V28980
Surrogate: 1,2-Dichloroethane - d4
97.0
Limits: 70-130%
100 01/18/23 10:30 MSA
V28980
Surrogate: Toluene-d8
97.4
Limits: 70-130%
100 01/18/23 10:30 MSA
V28980
Analytical Method: 625.1
Prep Batch(es):
V28891 01/16/23
10:31
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL MQL
DF Date / Time By
Analytical
Analyzed
Batch
Acenaphthene
<0.302
ug/L
0.302 2.00
1 01/17/23 16:46 JMV
V29017
Acenaphthylene
<0.297
ug/L
0.297 2.00
1 01/17/23 16:46 JMV
V29017
Anthracene
<0.836
ug/L
0.836 2.00
1 01/17/23 16:46 JMV
V29017
Benzidine
<1.32
u9/L
1.32 10.0
1 01/17/23 16:46 JMV
V29017
Benzo(a)anthracene
<0.637
ug/L
0.637 2.00
1 01/17/23 16:46 JMV
V29017
Benzo(a)pyrene
<1.02
ug/L
1.02 2.00
1 01/17/23 16:46 JMV
V29017
Benzo(b)fluoranthene
<2.49
ug/L
2.49 5.00
1 01/17/23 16:46 JMV
V29017
Benzo(g,h,i)perylene
<1.01
u9/L
1.01 5.00
1 01/17/23 16:46 JMV
V29017
Benzo(k)fluoranthene
<1.99
ug/L
1.99 5.00
1 01/17/23 16:46 JMV
V29017
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 13 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97322
Matrix: Aqueous
Sample ID: EW-1
Sampled:
1/10/2023 11:45
Analytical Method: 625.1
Prep Batch(es):
V28891
01/16/23 10:31
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzoic Acid
<1.10
N9/L
1.10
10.0
1
01/17/23 16:46
JMV
V29017
Benzyl alcohol
<0.684
N9/L
0.684
5.00
1
01/17/23 16:46
JMV
V29017
Bis(2-Chloroethoxy)methane
<0.468
N9/L
0.468
5.00
1
01/17/23 16:46
JMV
V29017
Bis(2-Chloroethyl)ether
<1.04
N9/L
1.04
5.00
1
01/17/23 16:46
JMV
V29017
Bis(2-Chloroisopropyl)ether
<1.08
N9/L
1.08
5.00
1
01/17/23 16:46
JMV
V29017
Bis(2-ethylhexyl)phthalate
<24.0
N9/L
24.0
50.0
1
01/17/23 16:46
JMV
V29017
4-13romophenyl phenyl ether
<1.11
N9/L
1.11
5.00
1
01/17/23 16:46
JMV
V29017
Butyl benzyl phthalate
<1.83
N9/L
1.83
5.00
1
01/17/23 16:46
JMV
V29017
4-Chloro-3-methylphenol
<1.18
N9/L
1.18
5.00
1
01/17/23 16:46
JMV
V29017
2-Chloronaphthalene
<7.38
N9/L
7.38
20.0
1
01/17/23 16:46
JMV
V29017
2-Chlorophenol
<0.938
N9/L
0.938
10.0
1
01/17/23 16:46
JMV
V29017
4-Chlorophenyl phenyl ether
<1.71
N9/L
1.71
5.00
1
01/17/23 16:46
JMV
V29017
Chrysene
<0.405
N9/L
0.405
2.00
1
01/17/23 16:46
JMV
V29017
Dibenz(a,h)anthracene
<0.434
N9/L
0.434
2.00
1
01/17/23 16:46
JMV
V29017
Dibenzofuran
<0.856
N9/L
0.856
5.00
1
01/17/23 16:46
JMV
V29017
1,2-Dichlorobenzene
<2.00
N9/L
2.00
5.00
1
01/17/23 16:46
JMV
V29017
1,3-Dichlorobenzene
<2.00
N9/L
2.00
5.00
1
01/17/23 16:46
JMV
V29017
1,4-Dichlorobenzene
<2.05
N9/L
2.05
5.00
1
01/17/23 16:46
JMV
V29017
3,3'-Dichlorobenzidine
<1.89
N9/L
1.89
5.00
1
01/17/23 16:46
JMV
V29017
2,4-Dichlorophenol
<1.46
N9/L
1.46
10.0
1
01/17/23 16:46
JMV
V29017
Diethyl phthalate
<0.745
N9/L
0.745
5.00
1
01/17/23 16:46
JMV
V29017
Dimethyl phthalate
<0.939
N9/L
0.939
5.00
1
01/17/23 16:46
JMV
V29017
2,4-Dimethyl phenol
11.93
N9/L
1.57
20.0
1
01/17/23 16:46
JMV
V29017
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 14 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97322
Matrix: Aqueous
Sample ID: EW-1
Sampled:
1/10/2023 11:45
Analytical Method: 625.1
Prep Batch(es):
V28891
01/16/23 10:31
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Di-n-butyl phthalate
<2.06
N9/L
2.06
5.00
1
01/17/23 16:46
JMV
V29017
4,6-Dinitro-2-methylphenol
<2.07
N9/L
2.07
10.0
1
01/17/23 16:46
JMV
V29017
2,4-Dinitrophenol
<1.92
N9/L
1.92
10.0
1
01/17/23 16:46
JMV
V29017
2,4-Dinitrotoluene
<1.11
N9/L
1.11
5.00
1
01/17/23 16:46
JMV
V29017
2,6-Dinitrotoluene
<0.809
N9/L
0.809
5.00
1
01/17/23 16:46
JMV
V29017
Di-n-Octyl Phthalate
<1.65
N9/L
1.65
5.00
1
01/17/23 16:46
JMV
V29017
Fluoranthene
<0.250
N9/L
0.250
2.00
1
01/17/23 16:46
JMV
V29017
Fluorene
<0.807
N9/L
0.807
2.00
1
01/17/23 16:46
JMV
V29017
Hexachlorobenzene
<0.979
N9/L
0.979
5.00
1
01/17/23 16:46
JMV
V29017
Hexachlorobutadiene
<2.73
N9/L
2.73
5.00
1
01/17/23 16:46
JMV
V29017
Hexachlorocyclopentadiene
<2.05
N9/L
2.05
5.00
1
01/17/23 16:46
JMV
V29017
Hexachloroethane
<1.76
N9/L
1.76
5.00
1
01/17/23 16:46
JMV
V29017
Indeno(1,2,3-cd)pyrene
<0.477
N9/L
0.477
2.00
1
01/17/23 16:46
JMV
V29017
Isophorone
<0.444
N9/L
0.444
5.00
1
01/17/23 16:46
JMV
V29017
1-Methylnaphthalene
ill
N9/L
1.14
2.00
1
01/17/23 16:46
JMV
V29017
2-Methylnaphthalene
163
N9/L
0.666
2.00
1
01/17/23 16:46
JMV
V29017
Naphthalene
160
N9/L
0.728
2.00
1
01/17/23 16:46
JMV
V29017
Nitrobenzene
<0.905
N9/L
0.905
5.00
1
01/17/23 16:46
JMV
V29017
2-Nitrophenol
<0.493
N9/L
0.493
5.00
1
01/17/23 16:46
JMV
V29017
4-Nitrophenol
<1.23
N9/L
1.23
10.0
1
01/17/23 16:46
JMV
V29017
N-Nitrosodiphenylamine
<1.10
N9/L
1.10
5.00
1
01/17/23 16:46
JMV
V29017
N-Nitroso-di-n-propylamine
<0.641
N9/L
0.641
5.00
1
01/17/23 16:46
JMV
V29017
Pentachlorophenol
<1.43
N9/L
1.43
5.00
1
01/17/23 16:46
JMV
V29017
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 15 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97322 Matrix: Aqueous
Sample ID: EW-1 Sampled: 1/10/2023 11:45
Analytical Method: 625.1
Prep Method: 625.1 (Prep)
Test Results
Phenanthrene
<0.428
Phenol
<0.651
Pyrene
<0.434
1,2,4-Trichlorobenzene
<2.21
2,4,6-Trichlorophenol
<1.32
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d 14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
Prep Batch(es): V28891 01/16/23 10:31
Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Ng/L
0.428 2.00
Ng/L
0.651 5.00
Ng/L
0.434 2.00
Ng/L
2.21 5.00
Ng/L
1.32 5.00
32.9
Limits: 10-63%
57.2
Limits: 49-118%
40.1
Limits: 22-84%
79.8
Limits: 43-123%
77.6
Limits: 49-151%
57.4
Limits: 31-144%
1 01/17/23 16:46 JMV
V29017
1 01/17/23 16:46 JMV
V29017
1 01/17/23 16:46 JMV
V29017
1 01/17/23 16:46 JMV
V29017
1 01/17/23 16:46 JMV
V29017
1 01/17/23 16:46 JMV
625.1
1 01/17/23 16:46 JMV
V29017
1 01/17/23 16:46 JMV
V29017
1 01/17/23 16:46 JMV
V29017
1 01/17/23 16:46 JMV
V29017
1 01/17/23 16:46 JMV
V29017
DF Dilution Factor
MQL Method Quantitation Limit
Page 16 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97323
Matrix: Aqueous
Sample ID: MW-1
Sampled:
1/10/2023 12:05
Analytical Method: 6200E
Prep Batch(es):
V28947
01/16/23 14:00
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
85.83
N9/L
18.0
100
10
01/17/23 10:13
MSA
V28948
Benzene
1110
N9/L
18.0
50.0
100
01/18/23 10:56
MSA
V28980
Bromobenzene
<2.10
N9/L
2.10
5.00
10
01/17/23 10:13
MSA
V28948
Bromochloromethane
<4.20
N9/L
4.20
10.0
10
01/17/23 10:13
MSA
V28948
Bromodichloromethane
<1.60
N9/L
1.60
5.00
10
01/17/23 10:13
MSA
V28948
Bromoform
<15.0
N9/L
15.0
50.0
10
01/17/23 10:13
MSA
V28948
Bromomethane
<2.80
N9/L
2.80
10.0
10
01/17/23 10:13
MSA
V28948
n-Butylbenzene
6.43
N9/L
1.80
5.00
10
01/17/23 10:13
MSA
V28948
sec -Butyl benzene
2.303
N9/L
2.00
5.00
10
01/17/23 10:13
MSA
V28948
tert-Butyl benzene
<9.20
N9/L
9.20
20.0
10
01/17/23 10:13
MSA
V28948
Carbon Tetrachloride
<1.80
N9/L
1.80
5.00
10
01/17/23 10:13
MSA
V28948
Chlorobenzene
<1.90
N9/L
1.90
5.00
10
01/17/23 10:13
MSA
V28948
Chlorodibromomethane
<1.90
N9/L
1.90
5.00
10
01/17/23 10:13
MSA
V28948
Chloroethane
<4.30
N9/L
4.30
10.0
10
01/17/23 10:13
MSA
V28948
Chloroform
<2.20
N9/L
2.20
5.00
10
01/17/23 10:13
MSA
V28948
Chloromethane
<2.20
N9/L
2.20
5.00
10
01/17/23 10:13
MSA
V28948
2-Chlorotoluene
<2.00
N9/L
2.00
5.00
10
01/17/23 10:13
MSA
V28948
4-Chlorotoluene
<2.00
N9/L
2.00
5.00
10
01/17/23 10:13
MSA
V28948
Di -Isopropyl Ether (DIPE)
7260
N9/L
50.0
50.0
100
01/18/23 10:56
MSA
V28980
1,2-Dibromo-3-Chloropropane
<11.0
N9/L
11.0
20.0
10
01/17/23 10:13
MSA
V28948
1,2-Dibromoethane
<2.00
N9/L
2.00
5.00
10
01/17/23 10:13
MSA
V28948
Dibromomethane
<2.30
N9/L
2.30
5.00
10
01/17/23 10:13
MSA
V28948
1,2-Dichlorobenzene
<2.20
N9/L
2.20
5.00
10
01/17/23 10:13
MSA
V28948
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 17 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97323
Matrix: Aqueous
Sample ID: MW-1
Sampled:
1/10/2023 12:OS
Analytical Method: 6200E
Prep Batch(es):
V28947
01/16/23 14:00
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<1.90
N9/L
1.90
5.00
10
01/17/23 10:13
MSA
V28948
1,4-Dichlorobenzene
<2.10
N9/L
2.10
5.00
10
01/17/23 10:13
MSA
V28948
Dichlorodifluoromethane
<12.0
N9/L
12.0
50.0
10
01/17/23 10:13
MSA
V28948
1,1-Dichloroethane
<2.40
N9/L
2.40
5.00
10
01/17/23 10:13
MSA
V28948
1,2-Dichloroethane
<1.50
N9/L
1.50
5.00
10
01/17/23 10:13
MSA
V28948
1,1-Dichloroethene
<1.50
N9/L
1.50
5.00
10
01/17/23 10:13
MSA
V28948
cis- 1,2-Dich loroethene
<2.00
N9/L
2.00
5.00
10
01/17/23 10:13
MSA
V28948
trans- 1, 2-Dichloroethene
<1.80
N9/L
1.80
5.00
10
01/17/23 10:13
MSA
V28948
1,2-Dichloropropane
<1.90
N9/L
1.90
5.00
10
01/17/23 10:13
MSA
V28948
1,3-Dichloropropane
<1.30
N9/L
1.30
5.00
10
01/17/23 10:13
MSA
V28948
2,2-Dichloropropane
<2.10
N9/L
2.10
20.0
10
01/17/23 10:13
MSA
V28948
1,1-Dichloropropene
<2.00
N9/L
2.00
5.00
10
01/17/23 10:13
MSA
V28948
cis-1,3-Dichloropropene
<2.10
N9/L
2.10
5.00
10
01/17/23 10:13
MSA
V28948
trans-1,3-Dichloropropene
<1.50
N9/L
1.50
5.00
10
01/17/23 10:13
MSA
V28948
Ethanol
<420
N9/L
420
2000
10
01/17/23 10:13
MSA
V28948
Ethylbenzene
97.3
N9/L
1.70
5.00
10
01/17/23 10:13
MSA
V28948
Hexachlorobutadiene
<3.50
N9/L
3.50
30.0
10
01/17/23 10:13
MSA
V28948
2-Hexanone
47.0
N9/L
3.80
10.0
10
01/17/23 10:13
MSA
V28948
Isopropyl benzene
8.93
N9/L
1.80
5.00
10
01/17/23 10:13
MSA
V28948
4-Isopropyl toluene
3.993
N9/L
0.890
5.00
10
01/17/23 10:13
MSA
V28948
Methyl Ethyl Ketone (MEK)
44.03
N9/L
7.10
50.0
10
01/17/23 10:13
MSA
V28948
Methyl tert-butyl ether (MTBE)
793
N9/L
1.40
10.0
10
01/17/23 10:13
MSA
V28948
4-Methyl-2-Pentanone
<0.780
N9/L
0.780
10.0
10
01/17/23 10:13
MSA
V28948
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 18 of 118
a
Wayp��•
nt . 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01176
S&ME, Inc - Charlotte Project Jefferson Pilot Comm
Lucas- Barroso-Giachetti Report Date : 01/19/2023
2016 Ayrsley Town Blvd.2Suite 2-A Information : Received : 01/11/2023
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018 REPORT OFANAL YSIS
Lab No : 97323
Matrix: Aqueous
Sample ID: MW-1
Sampled:
1/10/2023 12:05
Analytical Method: 6200E
Prep Batch(es):
V28947
01/16/23 14:00
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
<3.30
N9/L
3.30
20.0
10
01/17/23 10:13
MSA
V28948
Naphthalene
402
N9/L
4.70
10.0
10
01/17/23 10:13
MSA
V28948
n-Propylbenzene
11.4
N9/L
1.90
5.00
10
01/17/23 10:13
MSA
V28948
Styrene
<2.20
N9/L
2.20
5.00
10
01/17/23 10:13
MSA
V28948
1,1,1,2-Tetrachloroethane
<1.60
N9/L
1.60
5.00
10
01/17/23 10:13
MSA
V28948
1,1,2,2-Tetrachloroethane
<1.60
N9/L
1.60
5.00
10
01/17/23 10:13
MSA
V28948
Tetrachloroethene
<2.20
N9/L
2.20
5.00
10
01/17/23 10:13
MSA
V28948
Toluene
59.8
N9/L
2.20
5.00
10
01/17/23 10:13
MSA
V28948
1,2,3-Trichlorobenzene
<3.80
N9/L
3.80
5.00
10
01/17/23 10:13
MSA
V28948
1,2,4-Trichlorobenzene
<3.10
N9/L
3.10
5.00
10
01/17/23 10:13
MSA
V28948
1, 1, 1 -Trich loroetha ne
<1.60
N9/L
1.60
5.00
10
01/17/23 10:13
MSA
V28948
1,1,2-Trichloroethane
<0.960
N9/L
0.960
5.00
10
01/17/23 10:13
MSA
V28948
Trichloroethene
<1.80
N9/L
1.80
5.00
10
01/17/23 10:13
MSA
V28948
Trichlorofluoromethane
<1.80
N9/L
1.80
5.00
10
01/17/23 10:13
MSA
V28948
1,2,3-Trichloropropane
<2.70
N9/L
2.70
5.00
10
01/17/23 10:13
MSA
V28948
1,2,4-Trimethyl benzene
170
N9/L
1.90
5.00
10
01/17/23 10:13
MSA
V28948
1,3,5-Trimethyl benzene
68.5
N9/L
1.80
5.00
10
01/17/23 10:13
MSA
V28948
Vinyl Acetate
<10.0
N9/L
10.0
50.0
10
01/17/23 10:13
MSA
V28948
Vinyl Chloride
<1.70
N9/L
1.70
5.00
10
01/17/23 10:13
MSA
V28948
o-Xylene
25.5
N9/L
2.10
5.00
10
01/17/23 10:13
MSA
V28948
m,p-Xylene
301
N9/L
4.20
10.0
10
01/17/23 10:13
MSA
V28948
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 19 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97323 Matrix: Aqueous
Sample ID: MW-1 Sampled: 1/10/2023 12:OS
Analytical Method: 6200E Prep Batch(es): V28947 01/16/23 14:00 V28979 01/17/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
327
N9/L
2.10 5.00
10 01/17/23 10:13
V28948
Surrogate:4-Bromofluorobenzene
105
Limits: 70-130%
10 01/17/23 10:13 MSA
V28948
Surrogate: Dibromofluoromethane
96.4
Limits: 70-130%
10 01/17/23 10:13 MSA
V28948
Surrogate: 1,2-Dichloroethane - d4
97.2
Limits: 70-130%
10 01/17/23 10:13 MSA
V28948
Surrogate: Toluene-d8
98.2
Limits: 70-130%
10 01/17/23 10:13 MSA
V28948
Surrogate:4-Bromofluorobenzene
103
Limits: 70-130%
100 01/18/23 10:56 MSA
V28980
Surrogate: Dibromofluoromethane
95.8
Limits: 70-130%
100 01/18/23 10:56 MSA
V28980
Surrogate: 1,2-Dichloroethane - d4
91.0
Limits: 70-130%
100 01/18/23 10:56 MSA
V28980
Surrogate: Toluene-d8
99.4
Limits: 70-130%
100 01/18/23 10:56 MSA
V28980
Analytical Method: 625.1
Prep Batch(es):
V28891 01/16/23
10:31
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL MQL
DF Date / Time By
Analytical
Analyzed
Batch
Acenaphthene
<0.302
ug/L
0.302 2.00
1 01/17/23 17:09 JMV
V29017
Acenaphthylene
<0.297
ug/L
0.297 2.00
1 01/17/23 17:09 JMV
V29017
Anthracene
<0.836
ug/L
0.836 2.00
1 01/17/23 17:09 JMV
V29017
Benzidine
<1.32
u9/L
1.32 10.0
1 01/17/23 17:09 JMV
V29017
Benzo(a)anthracene
<0.637
ug/L
0.637 2.00
1 01/17/23 17:09 JMV
V29017
Benzo(a)pyrene
<1.02
u9/L
1.02 2.00
1 01/17/23 17:09 JMV
V29017
Benzo(b)fluoranthene
<2.49
ug/L
2.49 5.00
1 01/17/23 17:09 JMV
V29017
Benzo(g,h,i)perylene
<1.01
u9/L
1.01 5.00
1 01/17/23 17:09 JMV
V29017
Benzo(k)fluoranthene
<1.99
ug/L
1.99 5.00
1 01/17/23 17:09 JMV
V29017
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 20 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97323
Matrix: Aqueous
Sample ID: MW-1
Sampled:
1/10/2023 12:05
Analytical Method: 625.1
Prep Batch(es):
V28891
01/16/23 10:31
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzoic Acid
<1.10
N9/L
1.10
10.0
1
01/17/23 17:09
JMV
V29017
Benzyl alcohol
<0.684
N9/L
0.684
5.00
1
01/17/23 17:09
JMV
V29017
Bis(2-Chloroethoxy)methane
<0.468
N9/L
0.468
5.00
1
01/17/23 17:09
JMV
V29017
Bis(2-Chloroethyl)ether
<1.04
N9/L
1.04
5.00
1
01/17/23 17:09
JMV
V29017
Bis(2-Chloroisopropyl)ether
<1.08
N9/L
1.08
5.00
1
01/17/23 17:09
JMV
V29017
Bis(2-ethylhexyl)phthalate
<24.0
N9/L
24.0
50.0
1
01/17/23 17:09
JMV
V29017
4-13romophenyl phenyl ether
<1.11
N9/L
1.11
5.00
1
01/17/23 17:09
JMV
V29017
Butyl benzyl phthalate
<1.83
N9/L
1.83
5.00
1
01/17/23 17:09
JMV
V29017
4-Chloro-3-methylphenol
<1.18
N9/L
1.18
5.00
1
01/17/23 17:09
JMV
V29017
2-Chloronaphthalene
<7.38
N9/L
7.38
20.0
1
01/17/23 17:09
JMV
V29017
2-Chlorophenol
<0.938
N9/L
0.938
10.0
1
01/17/23 17:09
JMV
V29017
4-Chlorophenyl phenyl ether
<1.71
N9/L
1.71
5.00
1
01/17/23 17:09
JMV
V29017
Chrysene
<0.405
N9/L
0.405
2.00
1
01/17/23 17:09
JMV
V29017
Dibenz(a,h)anthracene
<0.434
N9/L
0.434
2.00
1
01/17/23 17:09
JMV
V29017
Dibenzofuran
<0.856
N9/L
0.856
5.00
1
01/17/23 17:09
JMV
V29017
1,2-Dichlorobenzene
<2.00
N9/L
2.00
5.00
1
01/17/23 17:09
JMV
V29017
1,3-Dichlorobenzene
<2.00
N9/L
2.00
5.00
1
01/17/23 17:09
JMV
V29017
1,4-Dichlorobenzene
<2.05
N9/L
2.05
5.00
1
01/17/23 17:09
JMV
V29017
3,3'-Dichlorobenzidine
<1.89
N9/L
1.89
5.00
1
01/17/23 17:09
JMV
V29017
2,4-Dichlorophenol
<1.46
N9/L
1.46
10.0
1
01/17/23 17:09
JMV
V29017
Diethyl phthalate
<0.745
N9/L
0.745
5.00
1
01/17/23 17:09
JMV
V29017
Dimethyl phthalate
<0.939
N9/L
0.939
5.00
1
01/17/23 17:09
JMV
V29017
2,4-Dimethyl phenol
<1.57
N9/L
1.57
20.0
1
01/17/23 17:09
JMV
V29017
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 21 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97323
Matrix: Aqueous
Sample ID: MW-1
Sampled:
1/10/2023 12:05
Analytical Method: 625.1
Prep Batch(es):
V28891
01/16/23 10:31
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Di-n-butyl phthalate
<2.06
Ng/L
2.06
5.00
1
01/17/23 17:09
JMV
V29017
4,6-Dinitro-2-methylphenol
<2.07
Ng/L
2.07
10.0
1
01/17/23 17:09
JMV
V29017
2,4-Dinitrophenol
<1.92
Ng/L
1.92
10.0
1
01/17/23 17:09
JMV
V29017
2,4-Dinitrotoluene
<1.11
Ng/L
1.11
5.00
1
01/17/23 17:09
JMV
V29017
2,6-Dinitrotoluene
<0.809
Ng/L
0.809
5.00
1
01/17/23 17:09
JMV
V29017
Di-n-Octyl Phthalate
<1.65
Ng/L
1.65
5.00
1
01/17/23 17:09
JMV
V29017
Fluoranthene
<0.250
Ng/L
0.250
2.00
1
01/17/23 17:09
JMV
V29017
Fluorene
22.9
Ng/L
0.807
2.00
1
01/17/23 17:09
JMV
V29017
Hexachlorobenzene
<0.979
Ng/L
0.979
5.00
1
01/17/23 17:09
JMV
V29017
Hexachlorobutadiene
<2.73
Ng/L
2.73
5.00
1
01/17/23 17:09
JMV
V29017
Hexachlorocyclopentadiene
<2.05
Ng/L
2.05
5.00
1
01/17/23 17:09
JMV
V29017
Hexachloroethane
<1.76
Ng/L
1.76
5.00
1
01/17/23 17:09
JMV
V29017
Indeno(1,2,3-cd)pyrene
<0.477
Ng/L
0.477
2.00
1
01/17/23 17:09
JMV
V29017
Isophorone
<0.444
Ng/L
0.444
5.00
1
01/17/23 17:09
JMV
V29017
1-Methylnaphthalene
320
Ng/L
4.56
8.00
4
01/19/2313:50
JMV
V29017
2-Methylnaphthalene
501
Ng/L
2.66
8.00
4
01/19/2313:50
JMV
V29017
Naphthalene
252
Ng/L
2.91
8.00
4
01/19/2313:50
JMV
V29017
Nitrobenzene
<0.905
Ng/L
0.905
5.00
1
01/17/23 17:09
JMV
V29017
2-Nitrophenol
<0.493
Ng/L
0.493
5.00
1
01/17/23 17:09
JMV
V29017
4-Nitrophenol
<1.23
Ng/L
1.23
10.0
1
01/17/23 17:09
JMV
V29017
N-Nitrosodiphenylamine
<1.10
Ng/L
1.10
5.00
1
01/17/23 17:09
JMV
V29017
N-Nitroso-di-n-propylamine
<0.641
Ng/L
0.641
5.00
1
01/17/23 17:09
JMV
V29017
Pentachlorophenol
<1.43
Ng/L
1.43
5.00
1
01/17/23 17:09
JMV
V29017
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 22 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97323 Matrix: Aqueous
Sample ID: MW-1 Sampled: 1/10/2023 12:05
Analytical Method: 625.1
Prep Method: 625.1 (Prep)
Test Results
Phenanthrene
54.1
Phenol
<0.651
Pyrene
1.803
1,2,4-Trichlorobenzene
<2.21
2,4,6-Trichlorophenol
<1.32
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d 14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
Prep Batch(es): V28891 01/16/23 10:31
Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Ng/L
0.428 2.00
Ng/L
0.651 5.00
Ng/L
0.434 2.00
Ng/L
2.21 5.00
Ng/L
1.32 5.00
29.3
Limits: 10-63%
53.8
Limits: 49-118%
12.1 *
Limits: 22-84%
105
Limits: 43-123%
73.0
Limits: 49-151%
60.2
Limits: 31-144%
1 01/17/23 17:09 JMV
V29017
1 01/17/23 17:09 JMV
V29017
1 01/17/23 17:09 JMV
V29017
1 01/17/23 17:09 JMV
V29017
1 01/17/23 17:09 JMV
V29017
1 01/17/23 17:09 JMV
625.1
1 01/17/23 17:09 JMV
V29017
1 01/17/23 17:09 JMV
V29017
1 01/17/23 17:09 JMV
V29017
1 01/17/23 17:09 JMV
V29017
1 01/17/23 17:09 JMV
V29017
DF Dilution Factor
MQL Method Quantitation Limit
Page 23 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97324
Matrix: Aqueous
Sample ID: MW-3
Sampled:
1/10/2023 10:35
Analytical Method: 6200E
Prep Batch(es):
V29020
01/18/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
45.93
N9/L
18.0
100
10
01/19/23 09:00
MSA
V29021
Benzene
16.1
N9/L
1.80
5.00
10
01/19/23 09:00
MSA
V29021
Bromobenzene
<2.10
N9/L
2.10
5.00
10
01/19/23 09:00
MSA
V29021
Bromochloromethane
<4.20
N9/L
4.20
10.0
10
01/19/23 09:00
MSA
V29021
Bromodichloromethane
<1.60
N9/L
1.60
5.00
10
01/19/23 09:00
MSA
V29021
Bromoform
<15.0
N9/L
15.0
50.0
10
01/19/23 09:00
MSA
V29021
Bromomethane
<2.80
N9/L
2.80
10.0
10
01/19/23 09:00
MSA
V29021
n-Butylbenzene
6.55
N9/L
1.80
5.00
10
01/19/23 09:00
MSA
V29021
sec -Butyl benzene
2.973
N9/L
2.00
5.00
10
01/19/23 09:00
MSA
V29021
tert-Butyl benzene
<9.20
N9/L
9.20
20.0
10
01/19/23 09:00
MSA
V29021
Carbon Tetrachloride
<1.80
N9/L
1.80
5.00
10
01/19/23 09:00
MSA
V29021
Chlorobenzene
<1.90
N9/L
1.90
5.00
10
01/19/23 09:00
MSA
V29021
Chlorodibromomethane
<1.90
N9/L
1.90
5.00
10
01/19/23 09:00
MSA
V29021
Chloroethane
<4.30
N9/L
4.30
10.0
10
01/19/23 09:00
MSA
V29021
Chloroform
<2.20
N9/L
2.20
5.00
10
01/19/23 09:00
MSA
V29021
Chloromethane
<2.20
N9/L
2.20
5.00
10
01/19/23 09:00
MSA
V29021
2-Chlorotoluene
<2.00
N9/L
2.00
5.00
10
01/19/23 09:00
MSA
V29021
4-Chlorotoluene
<2.00
N9/L
2.00
5.00
10
01/19/23 09:00
MSA
V29021
Di -Isopropyl Ether (DIPE)
7.17
N9/L
5.00
5.00
10
01/19/23 09:00
MSA
V29021
1,2-Dibromo-3-Chloropropane
<11.0
N9/L
11.0
20.0
10
01/19/23 09:00
MSA
V29021
1,2-Dibromoethane
<2.00
N9/L
2.00
5.00
10
01/19/23 09:00
MSA
V29021
Dibromomethane
<2.30
N9/L
2.30
5.00
10
01/19/23 09:00
MSA
V29021
1,2-Dichlorobenzene
<2.20
N9/L
2.20
5.00
10
01/19/23 09:00
MSA
V29021
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 24 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97324
Matrix: Aqueous
Sample ID: MW-3
Sampled:
1/10/2023 10:35
Analytical Method: 6200E
Prep Batch(es):
V29020
01/18/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<1.90
N9/L
1.90
5.00
10
01/19/23 09:00
MSA
V29021
1,4-Dichlorobenzene
<2.10
N9/L
2.10
5.00
10
01/19/23 09:00
MSA
V29021
Dichlorodifluoromethane
<12.0
N9/L
12.0
50.0
10
01/19/23 09:00
MSA
V29021
1,1-Dichloroethane
<2.40
N9/L
2.40
5.00
10
01/19/23 09:00
MSA
V29021
1,2-Dichloroethane
<1.50
N9/L
1.50
5.00
10
01/19/23 09:00
MSA
V29021
1,1-Dichloroethene
<1.50
N9/L
1.50
5.00
10
01/19/23 09:00
MSA
V29021
cis- 1,2-Dich loroethene
<2.00
N9/L
2.00
5.00
10
01/19/23 09:00
MSA
V29021
trans- 1, 2-Dichloroethene
<1.80
N9/L
1.80
5.00
10
01/19/23 09:00
MSA
V29021
1,2-Dichloropropane
<1.90
N9/L
1.90
5.00
10
01/19/23 09:00
MSA
V29021
1,3-Dichloropropane
<1.30
N9/L
1.30
5.00
10
01/19/23 09:00
MSA
V29021
2,2-Dichloropropane
<2.10
N9/L
2.10
20.0
10
01/19/23 09:00
MSA
V29021
1,1-Dichloropropene
<2.00
N9/L
2.00
5.00
10
01/19/23 09:00
MSA
V29021
cis-1,3-Dichloropropene
<2.10
N9/L
2.10
5.00
10
01/19/23 09:00
MSA
V29021
trans-1,3-Dichloropropene
<1.50
N9/L
1.50
5.00
10
01/19/23 09:00
MSA
V29021
Ethanol
<420
N9/L
420
2000
10
01/19/23 09:00
MSA
V29021
Ethylbenzene
<1.70
N9/L
1.70
5.00
10
01/19/23 09:00
MSA
V29021
Hexachlorobutadiene
<3.50
N9/L
3.50
30.0
10
01/19/23 09:00
MSA
V29021
2-Hexanone
<3.80
N9/L
3.80
10.0
10
01/19/23 09:00
MSA
V29021
Isopropyl benzene
7.41
N9/L
1.80
5.00
10
01/19/23 09:00
MSA
V29021
4-Isopropyl toluene
6.12
N9/L
0.890
5.00
10
01/19/23 09:00
MSA
V29021
Methyl Ethyl Ketone (MEK)
<7.10
N9/L
7.10
50.0
10
01/19/23 09:00
MSA
V29021
Methyl tert-butyl ether (MTBE)
<1.40
N9/L
1.40
10.0
10
01/19/23 09:00
MSA
V29021
4-Methyl-2-Pentanone
<0.780
N9/L
0.780
10.0
10
01/19/23 09:00
MSA
V29021
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 25 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97324
Matrix: Aqueous
Sample ID: MW-3
Sampled:
1/10/2023 10:35
Analytical Method: 6200E
Prep Batch(es):
V29020
01/18/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
<3.30
Ng/L
3.30
20.0
10
01/19/23 09:00
MSA
V29021
Naphthalene
356
Ng/L
4.70
10.0
10
01/19/23 09:00
MSA
V29021
n-Propylbenzene
3.133
Ng/L
1.90
5.00
10
01/19/23 09:00
MSA
V29021
Styrene
<2.20
Ng/L
2.20
5.00
10
01/19/23 09:00
MSA
V29021
1,1,1,2-Tetrachloroethane
<1.60
Ng/L
1.60
5.00
10
01/19/23 09:00
MSA
V29021
1,1,2,2-Tetrachloroethane
<1.60
Ng/L
1.60
5.00
10
01/19/23 09:00
MSA
V29021
Tetrachloroethene
<2.20
Ng/L
2.20
5.00
10
01/19/23 09:00
MSA
V29021
Toluene
<2.20
Ng/L
2.20
5.00
10
01/19/23 09:00
MSA
V29021
1,2,3-Trichlorobenzene
<3.80
Ng/L
3.80
5.00
10
01/19/23 09:00
MSA
V29021
1,2,4-Trichlorobenzene
<3.10
Ng/L
3.10
5.00
10
01/19/23 09:00
MSA
V29021
1, 1, 1 -Trich loroetha ne
<1.60
Ng/L
1.60
5.00
10
01/19/23 09:00
MSA
V29021
1,1,2-Trichloroethane
<0.960
Ng/L
0.960
5.00
10
01/19/23 09:00
MSA
V29021
Trichloroethene
<1.80
Ng/L
1.80
5.00
10
01/19/23 09:00
MSA
V29021
Trichlorofluoromethane
<1.80
Ng/L
1.80
5.00
10
01/19/23 09:00
MSA
V29021
1,2,3-Trichloropropane
<2.70
Ng/L
2.70
5.00
10
01/19/23 09:00
MSA
V29021
1,2,4-Trimethyl benzene
161
Ng/L
1.90
5.00
10
01/19/23 09:00
MSA
V29021
1,3,5-Trimethyl benzene
58.2
Ng/L
1.80
5.00
10
01/19/23 09:00
MSA
V29021
Vinyl Acetate
<10.0
Ng/L
10.0
50.0
10
01/19/23 09:00
MSA
V29021
Vinyl Chloride
<1.70
Ng/L
1.70
5.00
10
01/19/23 09:00
MSA
V29021
o-Xylene
27.4
Ng/L
2.10
5.00
10
01/19/23 09:00
MSA
V29021
m,p-Xylene
46.9
Ng/L
4.20
10.0
10
01/19/23 09:00
MSA
V29021
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 26 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97324 Matrix: Aqueous
Sample ID: MW-3 Sampled: 1/10/2023 10:35
Analytical Method: 6200E Prep Batch(es): V29020 01/18/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
74.3
N9/L
2.10
5.00
10
01/19/23 09:00
V29021
Surrogate: 4-Bromofluorobenzene
104
Limits:
70-130%
10 01/19/23 09:00 MSA
V29021
Surrogate: Dibromofluoromethane
94.2
Limits:
70-130%
10 01/19/23 09:00 MSA
V29021
Surrogate: 1,2-Dichloroethane - d4
91.2
Limits:
70-130%
10 01/19/23 09:00 MSA
V29021
Surrogate: Toluene-d8
102
Limits:
70-130%
10 01/19/23 09:00 MSA
V29021
Analytical Method: 625.1
Prep Batch(es):
V28891
01/16/23
10:31
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.326
N9/L
0.326
2.16
1
01/17/23 16:01
JMV
V29017
Acenaphthylene
<0.320
N9/L
0.320
2.16
1
01/17/23 16:01
JMV
V29017
Anthracene
<0.902
N9/L
0.902
2.16
1
01/17/23 16:01
JMV
V29017
Benzidine
<1.43
N9/L
1.43
10.8
1
01/17/23 16:01
JMV
V29017
Benzo(a)anthracene
<0.687
N9/L
0.687
2.16
1
01/17/23 16:01
JMV
V29017
Benzo(a)pyrene
<1.10
N9/L
1.10
2.16
1
01/17/23 16:01
JMV
V29017
Benzo(b)fluoranthene
<2.69
N9/L
2.69
5.41
1
01/17/23 16:01
JMV
V29017
Benzo(g,h,i)perylene
<1.09
N9/L
1.09
5.41
1
01/17/23 16:01
JMV
V29017
Benzo(k)fluoranthene
<2.15
N9/L
2.15
5.41
1
01/17/23 16:01
JMV
V29017
Benzoic Acid
<1.19
N9/L
1.19
10.8
1
01/17/23 16:01
JMV
V29017
Benzyl alcohol
<0.740
N9/L
0.740
5.41
1
01/17/23 16:01
JMV
V29017
Bis(2-Chloroethoxy)methane
<0.506
N9/L
0.506
5.41
1
01/17/23 16:01
JMV
V29017
Bis(2-Chloroethyl)ether
<1.13
N9/L
1.13
5.41
1
01/17/23 16:01
JMV
V29017
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method
Quantitation
Limit
Page 27 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97324
Matrix: Aqueous
Sample ID: MW-3
Sampled:
1/10/2023 10:35
Analytical Method: 625.1
Prep Batch(es):
V28891
01/16/23 10:31
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Bis(2-Chloroisopropyl)ether
<1.17
Ng/L
1.17
5.41
1
01/17/23 16:01
JMV
V29017
Bis(2-ethylhexyl)phthalate
<26.0
Ng/L
26.0
54.1
1
01/17/23 16:01
JMV
V29017
4-13romophenyl phenyl ether
<1.20
Ng/L
1.20
5.41
1
01/17/23 16:01
JMV
V29017
Butyl benzyl phthalate
<1.98
Ng/L
1.98
5.41
1
01/17/23 16:01
JMV
V29017
4-Chloro-3-methylphenol
<1.28
Ng/L
1.28
5.41
1
01/17/23 16:01
JMV
V29017
2-Chloronaphthalene
<7.97
pg/L
7.97
21.6
1
01/17/23 16:01
JMV
V29017
2-Chlorophenol
<1.01
Ng/L
1.01
10.8
1
01/17/23 16:01
JMV
V29017
4-Chlorophenyl phenyl ether
<1.85
Ng/L
1.85
5.41
1
01/17/23 16:01
JMV
V29017
Chrysene
<0.437
Ng/L
0.437
2.16
1
01/17/23 16:01
JMV
V29017
Dibenz(a,h)anthracene
<0.468
Ng/L
0.468
2.16
1
01/17/23 16:01
JMV
V29017
Dibenzofuran
<0.926
Ng/L
0.926
5.41
1
01/17/23 16:01
JMV
V29017
1,2-Dichlorobenzene
<2.16
Ng/L
2.16
5.41
1
01/17/23 16:01
JMV
V29017
1,3-Dichlorobenzene
<2.16
Ng/L
2.16
5.41
1
01/17/23 16:01
JMV
V29017
1,4-Dichlorobenzene
<2.22
Ng/L
2.22
5.41
1
01/17/23 16:01
JMV
V29017
3,3'-Dichlorobenzidine
<2.04
Ng/L
2.04
5.41
1
01/17/23 16:01
JMV
V29017
2,4-Dichlorophenol
<1.58
Ng/L
1.58
10.8
1
01/17/23 16:01
JMV
V29017
Diethyl phthalate
<0.806
Ng/L
0.806
5.41
1
01/17/23 16:01
JMV
V29017
Dimethyl phthalate
<1.02
Ng/L
1.02
5.41
1
01/17/23 16:01
JMV
V29017
2,4-Dimethylphenol
<1.70
Ng/L
1.70
21.6
1
01/17/23 16:01
JMV
V29017
Di-n-butyl phthalate
<2.23
Ng/L
2.23
5.41
1
01/17/23 16:01
JMV
V29017
4,6- Din itro-2-methylphenol
<2.24
Ng/L
2.24
10.8
1
01/17/23 16:01
JMV
V29017
2,4-Dinitrophenol
<2.07
Ng/L
2.07
10.8
1
01/17/23 16:01
JMV
V29017
2,4-Dinitrotoluene
<1.20
Ng/L
1.20
5.41
1
01/17/23 16:01
JMV
V29017
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 28 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97324
Matrix: Aqueous
Sample ID: MW-3
Sampled:
1/10/2023 10:35
Analytical Method: 625.1
Prep Batch(es):
V28891
01/16/23 10:31
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2,6-Dinitrotoluene
<0.875
N9/L
0.875
5.41
1
01/17/23 16:01
JMV
V29017
Di-n-Octyl Phthalate
<1.79
N9/L
1.79
5.41
1
01/17/23 16:01
JMV
V29017
Fluoranthene
<0.270
N9/L
0.270
2.16
1
01/17/23 16:01
JMV
V29017
Fluorene
<0.871
N9/L
0.871
2.16
1
01/17/23 16:01
JMV
V29017
Hexachlorobenzene
<1.06
N9/L
1.06
5.41
1
01/17/23 16:01
JMV
V29017
Hexachlorobutadiene
<2.95
N9/L
2.95
5.41
1
01/17/23 16:01
JMV
V29017
Hexachlorocyclopentadiene
<2.22
N9/L
2.22
5.41
1
01/17/23 16:01
JMV
V29017
Hexachloroethane
<1.90
N9/L
1.90
5.41
1
01/17/23 16:01
JMV
V29017
Indeno(1,2,3-cd)pyrene
<0.515
N9/L
0.515
2.16
1
01/17/23 16:01
JMV
V29017
Isophorone
<0.480
N9/L
0.480
5.41
1
01/17/23 16:01
JMV
V29017
1-Methylnaphthalene
164
N9/L
1.23
2.16
1
01/17/23 16:01
JMV
V29017
2-Methylnaphthalene
205
N9/L
0.719
2.16
1
01/17/23 16:01
JMV
V29017
Naphthalene
204
N9/L
0.786
2.16
1
01/17/23 16:01
JMV
V29017
Nitrobenzene
<0.979
N9/L
0.979
5.41
1
01/17/23 16:01
JMV
V29017
2-Nitrophenol
<0.533
N9/L
0.533
5.41
1
01/17/23 16:01
JMV
V29017
4-Nitrophenol
<1.33
N9/L
1.33
10.8
1
01/17/23 16:01
JMV
V29017
N-Nitrosodiphenylamine
<1.19
N9/L
1.19
5.41
1
01/17/23 16:01
JMV
V29017
N-Nitroso-di-n-propylamine
<0.693
N9/L
0.693
5.41
1
01/17/23 16:01
JMV
V29017
Pentachlorophenol
<1.55
N9/L
1.55
5.41
1
01/17/23 16:01
JMV
V29017
Phenanthrene
16.4
N9/L
0.462
2.16
1
01/17/23 16:01
JMV
V29017
Phenol
<0.704
N9/L
0.704
5.41
1
01/17/23 16:01
JMV
V29017
Pyrene
<0.468
N9/L
0.468
2.16
1
01/17/23 16:01
JMV
V29017
1,2,4-Trichlorobenzene
<2.39
N9/L
2.39
5.41
1
01/17/23 16:01
JMV
V29017
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 29 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
Report Date : 01/19/2023
Received : 01/11/2023
Report Number : 23-011-0018
Lab No : 97324
Sample ID: MW-3
REPORT OFANAL YSIS
Matrix: Aqueous
Sampled: 1/10/2023 10:35
Analytical Method: 625.1
Prep Batch(es):
V28891 01/16/23 10:31
Prep Method: 625.1 (Prep)
Test
Results Units
MDL MQL DF
Date / Time By Analytical
Analyzed
Batch
2,4,6-Trichlorophenol
<1.43 N9/L
1.43 5.41 1
01/17/23 16:01 JMV
V29017
Surrogate: Phenol-d5
24.8
Limits: 10-63%
1 01/17/23 16:01 JMV
625.1
Surrogate:2-Fluorobiphenyl
66.9
Limits:49-118%
1 01/17/23 16:01 JMV
V29017
Surrogate:2-Fluorophenol
34.4
Limits:22-84%
1 01/17/23 16:01 JMV
V29017
Surrogate: Nitrobenzene-d5
59.0
Limits: 43-123%
1 01/17/23 16:01 JMV
V29017
Surrogate:4-Terphenyl-d14
74.5
Limits:49-151%
1 01/17/23 16:01 JMV
V29017
Surrogate: 2,4,6-Tribromophenol
64.6
Limits:31-144%
1 01/17/23 16:01 JMV
V29017
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 30 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97325
Matrix: Aqueous
Sample ID: MW-4
Sampled:
1/10/2023 14:30
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<18.0
N9/L
18.0
100
10
01/18/23 09:15
MSA
V28980
Benzene
2.053
N9/L
1.80
5.00
10
01/18/23 09:15
MSA
V28980
Bromobenzene
<2.10
N9/L
2.10
5.00
10
01/18/23 09:15
MSA
V28980
Bromochloromethane
<4.20
N9/L
4.20
10.0
10
01/18/23 09:15
MSA
V28980
Bromodichloromethane
<1.60
N9/L
1.60
5.00
10
01/18/23 09:15
MSA
V28980
Bromoform
<15.0
N9/L
15.0
50.0
10
01/18/23 09:15
MSA
V28980
Bromomethane
<2.80
N9/L
2.80
10.0
10
01/18/23 09:15
MSA
V28980
n-Butylbenzene
2.133
N9/L
1.80
5.00
10
01/18/23 09:15
MSA
V28980
sec -Butyl benzene
<2.00
N9/L
2.00
5.00
10
01/18/23 09:15
MSA
V28980
tert-Butyl benzene
<9.20
N9/L
9.20
20.0
10
01/18/23 09:15
MSA
V28980
Carbon Tetrachloride
<1.80
N9/L
1.80
5.00
10
01/18/23 09:15
MSA
V28980
Chlorobenzene
<1.90
N9/L
1.90
5.00
10
01/18/23 09:15
MSA
V28980
Chlorodibromomethane
<1.90
N9/L
1.90
5.00
10
01/18/23 09:15
MSA
V28980
Chloroethane
<4.30
N9/L
4.30
10.0
10
01/18/23 09:15
MSA
V28980
Chloroform
<2.20
N9/L
2.20
5.00
10
01/18/23 09:15
MSA
V28980
Chloromethane
<2.20
N9/L
2.20
5.00
10
01/18/23 09:15
MSA
V28980
2-Chlorotoluene
<2.00
N9/L
2.00
5.00
10
01/18/23 09:15
MSA
V28980
4-Chlorotoluene
<2.00
N9/L
2.00
5.00
10
01/18/23 09:15
MSA
V28980
Di -Isopropyl Ether (DIPE)
46.0
N9/L
5.00
5.00
10
01/18/23 09:15
MSA
V28980
1,2-Dibromo-3-Chloropropane
<11.0
N9/L
11.0
20.0
10
01/18/23 09:15
MSA
V28980
1,2-Dibromoethane
<2.00
N9/L
2.00
5.00
10
01/18/23 09:15
MSA
V28980
Dibromomethane
<2.30
N9/L
2.30
5.00
10
01/18/23 09:15
MSA
V28980
1,2-Dichlorobenzene
<2.20
N9/L
2.20
5.00
10
01/18/23 09:15
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 31 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97325
Matrix: Aqueous
Sample ID: MW-4
Sampled:
1/10/2023 14:30
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<1.90
N9/L
1.90
5.00
10
01/18/23 09:15
MSA
V28980
1,4-Dichlorobenzene
<2.10
N9/L
2.10
5.00
10
01/18/23 09:15
MSA
V28980
Dichlorodifluoromethane
<12.0
N9/L
12.0
50.0
10
01/18/23 09:15
MSA
V28980
1,1-Dichloroethane
<2.40
N9/L
2.40
5.00
10
01/18/23 09:15
MSA
V28980
1,2-Dichloroethane
<1.50
N9/L
1.50
5.00
10
01/18/23 09:15
MSA
V28980
1,1-Dichloroethene
<1.50
N9/L
1.50
5.00
10
01/18/23 09:15
MSA
V28980
cis- 1,2-Dich loroethene
<2.00
N9/L
2.00
5.00
10
01/18/23 09:15
MSA
V28980
trans- 1, 2-Dichloroethene
<1.80
N9/L
1.80
5.00
10
01/18/23 09:15
MSA
V28980
1,2-Dichloropropane
<1.90
N9/L
1.90
5.00
10
01/18/23 09:15
MSA
V28980
1,3-Dichloropropane
<1.30
N9/L
1.30
5.00
10
01/18/23 09:15
MSA
V28980
2,2-Dichloropropane
<2.10
N9/L
2.10
20.0
10
01/18/23 09:15
MSA
V28980
1,1-Dichloropropene
<2.00
N9/L
2.00
5.00
10
01/18/23 09:15
MSA
V28980
cis-1,3-Dichloropropene
<2.10
N9/L
2.10
5.00
10
01/18/23 09:15
MSA
V28980
trans-1,3-Dichloropropene
<1.50
N9/L
1.50
5.00
10
01/18/23 09:15
MSA
V28980
Ethanol
<420
N9/L
420
2000
10
01/18/23 09:15
MSA
V28980
Ethylbenzene
<1.70
N9/L
1.70
5.00
10
01/18/23 09:15
MSA
V28980
Hexachlorobutadiene
<3.50
N9/L
3.50
30.0
10
01/18/23 09:15
MSA
V28980
2-Hexanone
<3.80
N9/L
3.80
10.0
10
01/18/23 09:15
MSA
V28980
Isopropyl benzene
2.953
N9/L
1.80
5.00
10
01/18/23 09:15
MSA
V28980
4-Isopropyl toluene
<0.890
N9/L
0.890
5.00
10
01/18/23 09:15
MSA
V28980
Methyl Ethyl Ketone (MEK)
<7.10
N9/L
7.10
50.0
10
01/18/23 09:15
MSA
V28980
Methyl tert-butyl ether (MTBE)
3.603
N9/L
1.40
10.0
10
01/18/23 09:15
MSA
V28980
4-Methyl-2-Pentanone
<0.780
N9/L
0.780
10.0
10
01/18/23 09:15
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 32 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97325
Matrix: Aqueous
Sample ID: MW-4
Sampled:
1/10/2023 14:30
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
<3.30
N9/L
3.30
20.0
10
01/18/23 09:15
MSA
V28980
Naphthalene
125
N9/L
4.70
10.0
10
01/18/23 09:15
MSA
V28980
n-Propylbenzene
<1.90
N9/L
1.90
5.00
10
01/18/23 09:15
MSA
V28980
Styrene
<2.20
N9/L
2.20
5.00
10
01/18/23 09:15
MSA
V28980
1,1,1,2-Tetrachloroethane
<1.60
N9/L
1.60
5.00
10
01/18/23 09:15
MSA
V28980
1,1,2,2-Tetrachloroethane
<1.60
N9/L
1.60
5.00
10
01/18/23 09:15
MSA
V28980
Tetrachloroethene
<2.20
N9/L
2.20
5.00
10
01/18/23 09:15
MSA
V28980
Toluene
<2.20
N9/L
2.20
5.00
10
01/18/23 09:15
MSA
V28980
1,2,3-Trichlorobenzene
<3.80
N9/L
3.80
5.00
10
01/18/23 09:15
MSA
V28980
1,2,4-Trichlorobenzene
<3.10
N9/L
3.10
5.00
10
01/18/23 09:15
MSA
V28980
1, 1, 1 -Trich loroetha ne
<1.60
N9/L
1.60
5.00
10
01/18/23 09:15
MSA
V28980
1,1,2-Trichloroethane
<0.960
N9/L
0.960
5.00
10
01/18/23 09:15
MSA
V28980
Trichloroethene
<1.80
N9/L
1.80
5.00
10
01/18/23 09:15
MSA
V28980
Trichlorofluoromethane
<1.80
N9/L
1.80
5.00
10
01/18/23 09:15
MSA
V28980
1,2,3-Trichloropropane
<2.70
N9/L
2.70
5.00
10
01/18/23 09:15
MSA
V28980
1,2,4-Trimethyl benzene
13.4
N9/L
1.90
5.00
10
01/18/23 09:15
MSA
V28980
1,3,5-Trimethyl benzene
<1.80
N9/L
1.80
5.00
10
01/18/23 09:15
MSA
V28980
Vinyl Acetate
<10.0
N9/L
10.0
50.0
10
01/18/23 09:15
MSA
V28980
Vinyl Chloride
<1.70
N9/L
1.70
5.00
10
01/18/23 09:15
MSA
V28980
o-Xylene
2.183
N9/L
2.10
5.00
10
01/18/23 09:15
MSA
V28980
m,p-Xylene
<4.20
N9/L
4.20
10.0
10
01/18/23 09:15
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 33 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97325 Matrix: Aqueous
Sample ID: MW-4 Sampled: 1/10/2023 14:30
Analytical Method: 6200E Prep Batch(es): V28979 01/17/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
2.183
N9/L
2.10
5.00
10
01/18/23 09:15
V28980
Surrogate: 4-Bromofluorobenzene
103
Limits:
70-130%
10 01/18/23 09:15
MSA
V28980
Surrogate: Dibromofluoromethane
95.0
Limits:
70-130%
10 01/18/23 09:15
MSA
V28980
Surrogate: 1,2-Dichloroethane - d4
96.2
Limits:
70-130%
10 01/18/23 09:15
MSA
V28980
Surrogate: Toluene-d8
99.2
Limits:
70-130%
10 01/18/23 09:15
MSA
V28980
Analytical Method: 625.1
Prep Batch(es):
V28891
01/16/23
10:31
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
2.123
N9/L
0.321
2.13
1
01/17/23 17:31
JMV
V29017
Acenaphthylene
<0.316
N9/L
0.316
2.13
1
01/17/23 17:31
JMV
V29017
Anthracene
<0.890
N9/L
0.890
2.13
1
01/17/23 17:31
JMV
V29017
Benzidine
<1.40
N9/L
1.40
10.6
1
01/17/23 17:31
JMV
V29017
Benzo(a)anthracene
<0.678
N9/L
0.678
2.13
1
01/17/23 17:31
JMV
V29017
Benzo(a)pyrene
<1.09
N9/L
1.09
2.13
1
01/17/23 17:31
JMV
V29017
Benzo(b)fluoranthene
<2.65
N9/L
2.65
5.32
1
01/17/23 17:31
JMV
V29017
Benzo(g,h,i)perylene
<1.07
N9/L
1.07
5.32
1
01/17/23 17:31
JMV
V29017
Benzo(k)fluoranthene
<2.12
N9/L
2.12
5.32
1
01/17/23 17:31
JMV
V29017
Benzoic Acid
<1.17
N9/L
1.17
10.6
1
01/17/23 17:31
JMV
V29017
Benzyl alcohol
<0.727
N9/L
0.727
5.32
1
01/17/23 17:31
JMV
V29017
Bis(2-Chloroethoxy)methane
<0.497
N9/L
0.497
5.32
1
01/17/23 17:31
JMV
V29017
Bis(2-Chloroethyl)ether
<1.11
N9/L
1.11
5.32
1
01/17/23 17:31
JMV
V29017
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method
Quantitation
Limit
Page 34 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97325
Matrix: Aqueous
Sample ID: MW-4
Sampled:
1/10/2023 14:30
Analytical Method: 625.1
Prep Batch(es):
V28891
01/16/23 10:31
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Bis(2-Chloroisopropyl)ether
<1.15
N9/L
1.15
5.32
1
01/17/23 17:31
JMV
V29017
Bis(2-ethylhexyl)phthalate
<25.6
N9/L
25.6
53.2
1
01/17/23 17:31
JMV
V29017
4-13romophenyl phenyl ether
<1.18
N9/L
1.18
5.32
1
01/17/23 17:31
JMV
V29017
Butyl benzyl phthalate
<1.95
N9/L
1.95
5.32
1
01/17/23 17:31
JMV
V29017
4-Chloro-3-methylphenol
<1.26
N9/L
1.26
5.32
1
01/17/23 17:31
JMV
V29017
2-Chloronaphthalene
<7.86
N9/L
7.86
21.3
1
01/17/23 17:31
JMV
V29017
2-Chlorophenol
<0.994
N9/L
0.994
10.6
1
01/17/23 17:31
JMV
V29017
4-Chlorophenyl phenyl ether
<1.82
N9/L
1.82
5.32
1
01/17/23 17:31
JMV
V29017
Chrysene
<0.431
N9/L
0.431
2.13
1
01/17/23 17:31
JMV
V29017
Dibenz(a,h)anthracene
<0.462
N9/L
0.462
2.13
1
01/17/23 17:31
JMV
V29017
Dibenzofuran
<0.910
N9/L
0.910
5.32
1
01/17/23 17:31
JMV
V29017
1,2-Dichlorobenzene
<2.13
N9/L
2.13
5.32
1
01/17/23 17:31
JMV
V29017
1,3-Dichlorobenzene
<2.13
N9/L
2.13
5.32
1
01/17/23 17:31
JMV
V29017
1,4-Dichlorobenzene
<2.18
N9/L
2.18
5.32
1
01/17/23 17:31
JMV
V29017
3,3'-Dichlorobenzidine
<2.01
N9/L
2.01
5.32
1
01/17/23 17:31
JMV
V29017
2,4-Dichlorophenol
<1.55
N9/L
1.55
10.6
1
01/17/23 17:31
JMV
V29017
Diethyl phthalate
<0.792
N9/L
0.792
5.32
1
01/17/23 17:31
JMV
V29017
Dimethyl phthalate
<0.999
N9/L
0.999
5.32
1
01/17/23 17:31
JMV
V29017
2,4-Dimethylphenol
<1.67
N9/L
1.67
21.3
1
01/17/23 17:31
JMV
V29017
Di-n-butyl phthalate
<2.19
N9/L
2.19
5.32
1
01/17/23 17:31
JMV
V29017
4,6- Din itro-2-methylphenol
<2.19
N9/L
2.19
10.6
1
01/17/23 17:31
JMV
V29017
2,4-Dinitrophenol
<2.04
N9/L
2.04
10.6
1
01/17/23 17:31
JMV
V29017
2,4-Dinitrotoluene
<1.18
N9/L
1.18
5.32
1
01/17/23 17:31
JMV
V29017
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 35 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97325
Matrix: Aqueous
Sample ID: MW-4
Sampled:
1/10/2023 14:30
Analytical Method: 625.1
Prep Batch(es):
V28891
01/16/23 10:31
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2,6-Dinitrotoluene
<0.860
N9/L
0.860
5.32
1
01/17/23 17:31
JMV
V29017
Di-n-Octyl Phthalate
<1.76
N9/L
1.76
5.32
1
01/17/23 17:31
JMV
V29017
Fluoranthene
<0.266
N9/L
0.266
2.13
1
01/17/23 17:31
JMV
V29017
Fluorene
2.47
N9/L
0.859
2.13
1
01/17/23 17:31
JMV
V29017
Hexachlorobenzene
<1.04
N9/L
1.04
5.32
1
01/17/23 17:31
JMV
V29017
Hexachlorobutadiene
<2.90
N9/L
2.90
5.32
1
01/17/23 17:31
JMV
V29017
Hexachlorocyclopentadiene
<2.18
N9/L
2.18
5.32
1
01/17/23 17:31
JMV
V29017
Hexachloroethane
<1.87
N9/L
1.87
5.32
1
01/17/23 17:31
JMV
V29017
Indeno(1,2,3-cd)pyrene
<0.508
N9/L
0.508
2.13
1
01/17/23 17:31
JMV
V29017
Isophorone
<0.472
N9/L
0.472
5.32
1
01/17/23 17:31
JMV
V29017
1-Methylnaphthalene
20.1
N9/L
1.21
2.13
1
01/17/23 17:31
JMV
V29017
2-Methylnaphthalene
27.0
N9/L
0.709
2.13
1
01/17/23 17:31
JMV
V29017
Naphthalene
19.3
N9/L
0.775
2.13
1
01/17/23 17:31
JMV
V29017
Nitrobenzene
<0.962
N9/L
0.962
5.32
1
01/17/23 17:31
JMV
V29017
2-Nitrophenol
<0.524
N9/L
0.524
5.32
1
01/17/23 17:31
JMV
V29017
4-Nitrophenol
<1.30
N9/L
1.30
10.6
1
01/17/23 17:31
JMV
V29017
N-Nitrosodiphenylamine
<1.17
N9/L
1.17
5.32
1
01/17/23 17:31
JMV
V29017
N-Nitroso-di-n-propylamine
<0.682
N9/L
0.682
5.32
1
01/17/23 17:31
JMV
V29017
Pentachlorophenol
<1.52
N9/L
1.52
5.32
1
01/17/23 17:31
JMV
V29017
Phenanthrene
4.75
N9/L
0.455
2.13
1
01/17/23 17:31
JMV
V29017
Phenol
<0.692
N9/L
0.692
5.32
1
01/17/23 17:31
JMV
V29017
Pyrene
<0.462
N9/L
0.462
2.13
1
01/17/23 17:31
JMV
V29017
1,2,4-Trichlorobenzene
<2.35
N9/L
2.35
5.32
1
01/17/23 17:31
JMV
V29017
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 36 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
Report Date : 01/19/2023
Received : 01/11/2023
Report Number : 23-011-0018
Lab No : 97325
Sample ID: MW-4
REPORT OFANAL YSIS
Matrix: Aqueous
Sampled: 1/10/2023 14:30
Analytical Method: 625.1
Prep Batch(es):
V28891 01/16/23 10:31
Prep Method: 625.1 (Prep)
Test
Results Units
MDL MQL DF
Date / Time By Analytical
Analyzed
Batch
2,4,6-Trichlorophenol
<1.40 N9/L
1.40 5.32 1
01/17/23 17:31 JMV
V29017
Surrogate: Phenol-d5
18.4
Limits: 10-63%
1 01/17/23 17:31 JMV
625.1
Surrogate:2-Fluorobiphenyl
60.5
Limits:49-118%
1 01/17/23 17:31 JMV
V29017
Surrogate:2-Fluorophenol
25.6
Limits:22-84%
1 01/17/23 17:31 JMV
V29017
Surrogate: Nitrobenzene-d5
45.1
Limits: 43-123%
1 01/17/23 17:31 JMV
V29017
Surrogate:4-Terphenyl-d14
69.7
Limits:49-151%
1 01/17/23 17:31 JMV
V29017
Surrogate: 2,4,6-Tribromophenol
65.1
Limits:31-144%
1 01/17/23 17:31 JMV
V29017
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 37 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97326
Matrix: Aqueous
Sample ID: MW-6
Sampled:
1/10/2023 10:10
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
V29020
01/18/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
6.983
N9/L
1.80
10.0
1
01/18/23 04:38
MSA
V28980
Benzene
1.82
N9/L
0.180
0.500
1
01/18/23 04:38
MSA
V28980
Bromobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 04:38
MSA
V28980
Bromochloromethane
<0.420
N9/L
0.420
1.00
1
01/18/23 04:38
MSA
V28980
Bromodichloromethane
<0.160
N9/L
0.160
0.500
1
01/18/23 04:38
MSA
V28980
Bromoform
<1.50
N9/L
1.50
5.00
1
01/18/23 04:38
MSA
V28980
Bromomethane
<0.280
N9/L
0.280
1.00
1
01/18/23 04:38
MSA
V28980
n-Butylbenzene
2.71
N9/L
0.180
0.500
1
01/18/23 04:38
MSA
V28980
sec -Butyl benzene
2.64
N9/L
0.200
0.500
1
01/18/23 04:38
MSA
V28980
tert-Butyl benzene
1.373
N9/L
0.920
2.00
1
01/18/23 04:38
MSA
V28980
Carbon Tetrachloride
<0.180
N9/L
0.180
0.500
1
01/18/23 04:38
MSA
V28980
Chlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 04:38
MSA
V28980
Chlorodibromomethane
<0.190
N9/L
0.190
0.500
1
01/18/23 04:38
MSA
V28980
Chloroethane
<0.430
N9/L
0.430
1.00
1
01/18/23 04:38
MSA
V28980
Chloroform
3.66
N9/L
0.220
0.500
1
01/18/23 04:38
MSA
V28980
Chloromethane
<0.220
N9/L
0.220
0.500
1
01/18/23 04:38
MSA
V28980
2-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 04:38
MSA
V28980
4-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 04:38
MSA
V28980
Di -Isopropyl Ether (DIPE)
<0.500
N9/L
0.500
0.500
1
01/18/23 04:38
MSA
V28980
1,2-Dibromo-3-Chloropropane
<1.10
N9/L
1.10
2.00
1
01/18/23 04:38
MSA
V28980
1,2-Dibromoethane
<0.200
N9/L
0.200
0.500
1
01/18/23 04:38
MSA
V28980
Dibromomethane
<0.230
N9/L
0.230
0.500
1
01/18/23 04:38
MSA
V28980
1,2-Dichlorobenzene
<0.220
N9/L
0.220
0.500
1
01/18/23 04:38
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 38 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97326
Matrix: Aqueous
Sample ID: MW-6
Sampled:
1/10/2023 10:10
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
V29020
01/18/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 04:38
MSA
V28980
1,4-Dichlorobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 04:38
MSA
V28980
Dichlorodifluoromethane
<1.20
N9/L
1.20
5.00
1
01/18/23 04:38
MSA
V28980
1,1-Dichloroethane
<0.240
N9/L
0.240
0.500
1
01/18/23 04:38
MSA
V28980
1,2-Dichloroethane
<0.150
N9/L
0.150
0.500
1
01/18/23 04:38
MSA
V28980
1,1-Dichloroethene
<0.150
N9/L
0.150
0.500
1
01/18/23 04:38
MSA
V28980
cis- 1,2-Dichloroethene
<0.200
N9/L
0.200
0.500
1
01/18/23 04:38
MSA
V28980
trans-1,2-Dichloroethene
<0.180
N9/L
0.180
0.500
1
01/18/23 04:38
MSA
V28980
1,2-Dichloropropane
<0.190
N9/L
0.190
0.500
1
01/18/23 04:38
MSA
V28980
1,3-Dichloropropane
<0.130
N9/L
0.130
0.500
1
01/18/23 04:38
MSA
V28980
2,2-Dichloropropane
<0.210
N9/L
0.210
2.00
1
01/18/23 04:38
MSA
V28980
1,1-Dichloropropene
<0.200
N9/L
0.200
0.500
1
01/18/23 04:38
MSA
V28980
cis- 1,3-Dichloropropene
<0.210
N9/L
0.210
0.500
1
01/18/23 04:38
MSA
V28980
trans-1,3-Dichloropropene
<0.150
N9/L
0.150
0.500
1
01/18/23 04:38
MSA
V28980
Ethanol
<42.0
N9/L
42.0
200
1
01/18/23 04:38
MSA
V28980
Ethylbenzene
0.653
N9/L
0.170
0.500
1
01/18/23 04:38
MSA
V28980
Hexachlorobutadiene
<0.350
N9/L
0.350
3.00
1
01/18/23 04:38
MSA
V28980
2-Hexanone
<0.380
N9/L
0.380
1.00
1
01/18/23 04:38
MSA
V28980
Isopropyl benzene
6.42
N9/L
0.180
0.500
1
01/18/23 04:38
MSA
V28980
4-Isopropyl toluene
3.37
N9/L
0.089
0.500
1
01/18/23 04:38
MSA
V28980
Methyl Ethyl Ketone (MEK)
1.643
N9/L
0.710
5.00
1
01/18/23 04:38
MSA
V28980
Methyl tert-butyl ether (MTBE)
<0.140
N9/L
0.140
1.00
1
01/18/23 04:38
MSA
V28980
4-Methyl-2-Pentanone
<0.078
N9/L
0.078
1.00
1
01/18/23 04:38
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 39 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97326
Matrix: Aqueous
Sample ID: MW-6
Sampled:
1/10/2023 10:10
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
V29020
01/18/23 14:00
Prep Method: 6200
PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
<0.330
N9/L
0.330
2.00
1
01/18/23 04:38
MSA
V28980
Naphthalene
323
N9/L
4.70
10.0
10
01/19/23 09:25
MSA
V29021
n-Propylbenzene
1.21
N9/L
0.190
0.500
1
01/18/23 04:38
MSA
V28980
Styrene
<0.220
N9/L
0.220
0.500
1
01/18/23 04:38
MSA
V28980
1,1,1,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 04:38
MSA
V28980
1,1,2,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 04:38
MSA
V28980
Tetrachloroethene
<0.220
N9/L
0.220
0.500
1
01/18/23 04:38
MSA
V28980
Toluene
0.2233
N9/L
0.220
0.500
1
01/18/23 04:38
MSA
V28980
1,2,3-Trichlorobenzene
<0.380
N9/L
0.380
0.500
1
01/18/23 04:38
MSA
V28980
1,2,4-Trichlorobenzene
<0.310
N9/L
0.310
0.500
1
01/18/23 04:38
MSA
V28980
1,1,1-Trichloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 04:38
MSA
V28980
1,1,2-Trichloroethane
<0.096
N9/L
0.096
0.500
1
01/18/23 04:38
MSA
V28980
Trichloroethene
<0.180
N9/L
0.180
0.500
1
01/18/23 04:38
MSA
V28980
Trichlorofluoromethane
<0.180
N9/L
0.180
0.500
1
01/18/23 04:38
MSA
V28980
1,2,3-Trichloropropane
<0.270
N9/L
0.270
0.500
1
01/18/23 04:38
MSA
V28980
1,2,4-Trimethyl benzene
85.5
N9/L
0.190
0.500
1
01/18/23 04:38
MSA
V28980
1,3,5-Trimethyl benzene
34.9
N9/L
0.180
0.500
1
01/18/23 04:38
MSA
V28980
Vinyl Acetate
<1.00
N9/L
1.00
5.00
1
01/18/23 04:38
MSA
V28980
Vinyl Chloride
<0.170
N9/L
0.170
0.500
1
01/18/23 04:38
MSA
V28980
o-Xylene
5.61
N9/L
0.210
0.500
1
01/18/23 04:38
MSA
V28980
m,p-Xylene
38.0
N9/L
0.420
1.00
1
01/18/23 04:38
MSA
V28980
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 40 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97326 Matrix: Aqueous
Sample ID: MW-6 Sampled: 1/10/2023 10:10
Analytical Method: 6200E Prep Batch(es): V28979 01/17/23 14:00 V29020 01/18/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
43.6
Ng/L
0.210 0.500
1 01/18/23 04:38
V28980
Surrogate: 4-Bromofluorobenzene
100
Limits: 70-130%
1 01/18/23 04:38 MSA
V28980
Surrogate: Dibromofluoromethane
97.2
Limits: 70-130%
1 01/18/23 04:38 MSA
V28980
Surrogate: 1,2-Dichloroethane - d4
90.2
Limits: 70-130%
1 01/18/23 04:38 MSA
V28980
Surrogate: Toluene-d8
102
Limits: 70-130%
1 01/18/23 04:38 MSA
V28980
Surrogate: 4-Bromofluorobenzene
101
Limits: 70-130%
10 01/19/23 09:25 MSA
V29021
Surrogate: Dibromofluoromethane
103
Limits: 70-130%
10 01/19/23 09:25 MSA
V29021
Surrogate: 1,2-Dichloroethane - d4
103
Limits: 70-130%
10 01/19/23 09:25 MSA
V29021
Surrogate: Toluene-d8
96.4
Limits: 70-130%
10 01/19/23 09:25 MSA
V29021
Analytical Method: 625.1
Prep Batch(es):
V28943 01/17/23
08:54
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL MQL
DF Date / Time By
Analytical
Analyzed
Batch
Acenaphthene
2.35
ug/L
0.333 2.21
1 01/18/23 17:42 JMV
V29002
Acenaphthylene
<0.328
ug/L
0.328 2.21
1 01/18/23 17:42 JMV
V29002
Anthracene
<0.923
ug/L
0.923 2.21
1 01/18/23 17:42 JMV
V29002
Benzidine
<1.45
ug/L
1.45 11.0
1 01/18/23 17:42 JMV
V29002
Benzo(a)anthracene
<0.703
ug/L
0.703 2.21
1 01/18/23 17:42 JMV
V29002
Benzo(a)pyrene
<1.13
ug/L
1.13 2.21
1 01/18/23 17:42 JMV
V29002
Benzo(b)fluoranthene
<2.75
ug/L
2.75 5.52
1 01/18/23 17:42 JMV
V29002
Benzo(g,h,i)perylene
<1.12
ug/L
1.12 5.52
1 01/18/23 17:42 JMV
V29002
Benzo(k)fluoranthene
<2.20
ug/L
2.20 5.52
1 01/18/23 17:42 JMV
V29002
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 41 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97326
Matrix: Aqueous
Sample ID: MW-6
Sampled:
1/10/2023 10:10
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzoic Acid
<1.21
N9/L
1.21
11.0
1
01/18/23 17:42
JMV
V29002
Benzyl alcohol
<0.755
N9/L
0.755
5.52
1
01/18/23 17:42
JMV
V29002
Bis(2-Chloroethoxy)methane
<0.516
N9/L
0.516
5.52
1
01/18/23 17:42
JMV
V29002
Bis(2-Chloroethyl)ether
<1.15
N9/L
1.15
5.52
1
01/18/23 17:42
JMV
V29002
Bis(2-Chloroisopropyl)ether
<1.19
N9/L
1.19
5.52
1
01/18/23 17:42
JMV
V29002
Bis(2-ethylhexyl)phthalate
<26.5
N9/L
26.5
55.2
1
01/18/23 17:42
JMV
V29002
4-13romophenyl phenyl ether
<1.23
N9/L
1.23
5.52
1
01/18/23 17:42
JMV
V29002
Butyl benzyl phthalate
<2.02
N9/L
2.02
5.52
1
01/18/23 17:42
JMV
V29002
4-Chloro-3-methylphenol
<1.30
N9/L
1.30
5.52
1
01/18/23 17:42
JMV
V29002
2-Chloronaphthalene
<8.15
N9/L
8.15
22.1
1
01/18/23 17:42
JMV
V29002
2-Chlorophenol
<1.03
N9/L
1.03
11.0
1
01/18/23 17:42
JMV
V29002
4-Chlorophenyl phenyl ether
<1.89
N9/L
1.89
5.52
1
01/18/23 17:42
JMV
V29002
Chrysene
<0.447
N9/L
0.447
2.21
1
01/18/23 17:42
JMV
V29002
Dibenz(a,h)anthracene
<0.479
N9/L
0.479
2.21
1
01/18/23 17:42
JMV
V29002
Dibenzofuran
4.313
N9/L
0.945
5.52
1
01/18/23 17:42
JMV
V29002
1,2-Dichlorobenzene
<2.21
N9/L
2.21
5.52
1
01/18/23 17:42
JMV
V29002
1,3-Dichlorobenzene
<2.21
N9/L
2.21
5.52
1
01/18/23 17:42
JMV
V29002
1,4-Dichlorobenzene
<2.26
N9/L
2.26
5.52
1
01/18/23 17:42
JMV
V29002
3,3'-Dichlorobenzidine
<2.09
N9/L
2.09
5.52
1
01/18/23 17:42
JMV
V29002
2,4-Dichlorophenol
<1.61
N9/L
1.61
11.0
1
01/18/23 17:42
JMV
V29002
Diethyl phthalate
<0.822
N9/L
0.822
5.52
1
01/18/23 17:42
JMV
V29002
Dimethyl phthalate
<1.04
N9/L
1.04
5.52
1
01/18/23 17:42
JMV
V29002
2,4-Dimethylphenol
<1.73
N9/L
1.73
22.1
1
01/18/23 17:42
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 42 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97326
Matrix: Aqueous
Sample ID: MW-6
Sampled:
1/10/2023 10:10
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Di-n-butyl phthalate
<2.27
Ng/L
2.27
5.52
1
01/18/23 17:42
JMV
V29002
4,6-Dinitro-2-methylphenol
<2.28
Ng/L
2.28
11.0
1
01/18/23 17:42
JMV
V29002
2,4-Dinitrophenol
<2.11
Ng/L
2.11
11.0
1
01/18/23 17:42
JMV
V29002
2,4-Dinitrotoluene
<1.23
Ng/L
1.23
5.52
1
01/18/23 17:42
JMV
V29002
2,6-Dinitrotoluene
<0.893
Ng/L
0.893
5.52
1
01/18/23 17:42
JMV
V29002
Di-n-Octyl Phthalate
<1.82
Ng/L
1.82
5.52
1
01/18/23 17:42
JMV
V29002
Fluoranthene
<0.276
Ng/L
0.276
2.21
1
01/18/23 17:42
JMV
V29002
Fluorene
26.9
Ng/L
0.891
2.21
1
01/18/23 17:42
JMV
V29002
Hexachlorobenzene
<1.08
Ng/L
1.08
5.52
1
01/18/23 17:42
JMV
V29002
Hexachlorobutadiene
<3.01
Ng/L
3.01
5.52
1
01/18/23 17:42
JMV
V29002
Hexachlorocyclopentadiene
<2.26
Ng/L
2.26
5.52
1
01/18/23 17:42
JMV
V29002
Hexachloroethane
<1.94
Ng/L
1.94
5.52
1
01/18/23 17:42
JMV
V29002
Indeno(1,2,3-cd)pyrene
<0.527
Ng/L
0.527
2.21
1
01/18/23 17:42
JMV
V29002
Isophorone
<0.490
Ng/L
0.490
5.52
1
01/18/23 17:42
JMV
V29002
1-Methylnaphthalene
108
Ng/L
1.26
2.21
1
01/18/23 17:42
JMV
V29002
2-Methylnaphthalene
147
Ng/L
0.735
2.21
1
01/18/23 17:42
JMV
V29002
Naphthalene
149
Ng/L
0.804
2.21
1
01/18/23 17:42
JMV
V29002
Nitrobenzene
<0.999
Ng/L
0.999
5.52
1
01/18/23 17:42
JMV
V29002
2-Nitrophenol
<0.544
Ng/L
0.544
5.52
1
01/18/23 17:42
JMV
V29002
4-Nitrophenol
<1.35
Ng/L
1.35
11.0
1
01/18/23 17:42
JMV
V29002
N-Nitrosodiphenylamine
<1.21
Ng/L
1.21
5.52
1
01/18/23 17:42
JMV
V29002
N-Nitroso-di-n-propylamine
<0.707
Ng/L
0.707
5.52
1
01/18/23 17:42
JMV
V29002
Pentachlorophenol
<1.58
Ng/L
1.58
5.52
1
01/18/23 17:42
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 43 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97326 Matrix: Aqueous
Sample ID: MW-6 Sampled: 1/10/2023 10:10
Analytical Method: 625.1
Prep Method: 625.1 (Prep)
Test Results
Phenanthrene
4.52
Phenol
<0.718
Pyrene
<0.479
1,2,4-Trichlorobenzene
<2.44
2,4,6-Trichlorophenol
<1.46
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d 14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
Prep Batch(es): V28943 01/17/23 08:54
Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Ng/L
0.472 2.21
N9/L
0.718 5.52
N9/L
0.479 2.21
N9/L
2.44 5.52
N9/L
1.46 5.52
31.4
Limits: 10-63%
70.1
Limits: 49-118%
39.2
Limits: 22-84%
59.2
Limits: 43-123%
86.1
Limits: 49-151%
82.6
Limits: 31-144%
1 01/18/23 17:42 JMV V29002
1 01/18/23 17:42 JMV V29002
1 01/18/23 17:42 JMV V29002
1 01/18/23 17:42 JMV V29002
1 01/18/23 17:42 JMV V29002
1 01/18/23 17:42 JMV 625.1
1 01/18/23 17:42 JMV V29002
1 01/18/23 17:42 JMV V29002
1 01/18/23 17:42 JMV V29002
1 01/18/23 17:42 JMV V29002
1 01/18/23 17:42 JMV V29002
DF Dilution Factor
MQL Method Quantitation Limit
Page 44 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97327
Matrix: Aqueous
Sample ID: MW-7
Sampled:
1/10/2023 13:30
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
N9/L
1.80
10.0
1
01/18/23 05:03
MSA
V28980
Benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:03
MSA
V28980
Bromobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:03
MSA
V28980
Bromochloromethane
<0.420
N9/L
0.420
1.00
1
01/18/23 05:03
MSA
V28980
Bromodichloromethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:03
MSA
V28980
Bromoform
<1.50
N9/L
1.50
5.00
1
01/18/23 05:03
MSA
V28980
Bromomethane
<0.280
N9/L
0.280
1.00
1
01/18/23 05:03
MSA
V28980
n-Butylbenzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:03
MSA
V28980
sec -Butyl benzene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:03
MSA
V28980
tert-Butyl benzene
<0.920
N9/L
0.920
2.00
1
01/18/23 05:03
MSA
V28980
Carbon Tetrachloride
<0.180
N9/L
0.180
0.500
1
01/18/23 05:03
MSA
V28980
Chlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:03
MSA
V28980
Chlorodibromomethane
<0.190
N9/L
0.190
0.500
1
01/18/23 05:03
MSA
V28980
Chloroethane
<0.430
N9/L
0.430
1.00
1
01/18/23 05:03
MSA
V28980
Chloroform
2.53
N9/L
0.220
0.500
1
01/18/23 05:03
MSA
V28980
Chloromethane
<0.220
N9/L
0.220
0.500
1
01/18/23 05:03
MSA
V28980
2-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:03
MSA
V28980
4-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:03
MSA
V28980
Di -Isopropyl Ether (DIPE)
<0.500
N9/L
0.500
0.500
1
01/18/23 05:03
MSA
V28980
1,2-Dibromo-3-Chloropropane
<1.10
N9/L
1.10
2.00
1
01/18/23 05:03
MSA
V28980
1,2-Dibromoethane
<0.200
N9/L
0.200
0.500
1
01/18/23 05:03
MSA
V28980
Dibromomethane
<0.230
N9/L
0.230
0.500
1
01/18/23 05:03
MSA
V28980
1,2-Dichlorobenzene
<0.220
N9/L
0.220
0.500
1
01/18/23 05:03
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 45 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97327
Matrix: Aqueous
Sample ID: MW-7
Sampled:
1/10/2023 13:30
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:03
MSA
V28980
1,4-Dichlorobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:03
MSA
V28980
Dichlorodifluoromethane
<1.20
N9/L
1.20
5.00
1
01/18/23 05:03
MSA
V28980
1,1-Dichloroethane
<0.240
N9/L
0.240
0.500
1
01/18/23 05:03
MSA
V28980
1,2-Dichloroethane
<0.150
N9/L
0.150
0.500
1
01/18/23 05:03
MSA
V28980
1,1-Dichloroethene
1.55
N9/L
0.150
0.500
1
01/18/23 05:03
MSA
V28980
cis- 1,2-Dichloroethene
1.14
N9/L
0.200
0.500
1
01/18/23 05:03
MSA
V28980
trans-1,2-Dichloroethene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:03
MSA
V28980
1,2-Dichloropropane
<0.190
N9/L
0.190
0.500
1
01/18/23 05:03
MSA
V28980
1,3-Dichloropropane
<0.130
N9/L
0.130
0.500
1
01/18/23 05:03
MSA
V28980
2,2-Dichloropropane
<0.210
N9/L
0.210
2.00
1
01/18/23 05:03
MSA
V28980
1,1-Dichloropropene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:03
MSA
V28980
cis- 1,3-Dichloropropene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:03
MSA
V28980
trans-1,3-Dichloropropene
<0.150
N9/L
0.150
0.500
1
01/18/23 05:03
MSA
V28980
Ethanol
<42.0
N9/L
42.0
200
1
01/18/23 05:03
MSA
V28980
Ethylbenzene
<0.170
N9/L
0.170
0.500
1
01/18/23 05:03
MSA
V28980
Hexachlorobutadiene
<0.350
N9/L
0.350
3.00
1
01/18/23 05:03
MSA
V28980
2-Hexanone
<0.380
N9/L
0.380
1.00
1
01/18/23 05:03
MSA
V28980
Isopropyl benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:03
MSA
V28980
4-Isopropyl toluene
<0.089
N9/L
0.089
0.500
1
01/18/23 05:03
MSA
V28980
Methyl Ethyl Ketone (MEK)
<0.710
N9/L
0.710
5.00
1
01/18/23 05:03
MSA
V28980
Methyl tert-butyl ether (MTBE)
<0.140
N9/L
0.140
1.00
1
01/18/23 05:03
MSA
V28980
4-Methyl-2-Pentanone
<0.078
N9/L
0.078
1.00
1
01/18/23 05:03
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 46 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97327
Matrix: Aqueous
Sample ID: MW-7
Sampled:
1/10/2023 13:30
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200
PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
<0.330
N9/L
0.330
2.00
1
01/18/23 05:03
MSA
V28980
Naphthalene
19.2
N9/L
0.470
1.00
1
01/18/23 05:03
MSA
V28980
n-Propylbenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:03
MSA
V28980
Styrene
<0.220
N9/L
0.220
0.500
1
01/18/23 05:03
MSA
V28980
1,1,1,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:03
MSA
V28980
1,1,2,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:03
MSA
V28980
Tetrachloroethene
1.45
N9/L
0.220
0.500
1
01/18/23 05:03
MSA
V28980
Toluene
<0.220
N9/L
0.220
0.500
1
01/18/23 05:03
MSA
V28980
1,2,3-Trichlorobenzene
<0.380
N9/L
0.380
0.500
1
01/18/23 05:03
MSA
V28980
1,2,4-Trichlorobenzene
<0.310
N9/L
0.310
0.500
1
01/18/23 05:03
MSA
V28980
1,1,1-Trichloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:03
MSA
V28980
1,1,2-Trichloroethane
<0.096
N9/L
0.096
0.500
1
01/18/23 05:03
MSA
V28980
Trichloroethene
2.03
N9/L
0.180
0.500
1
01/18/23 05:03
MSA
V28980
Trichlorofluoromethane
<0.180
N9/L
0.180
0.500
1
01/18/23 05:03
MSA
V28980
1,2,3-Trichloropropane
<0.270
N9/L
0.270
0.500
1
01/18/23 05:03
MSA
V28980
1,2,4-Trimethyl benzene
0.4373
N9/L
0.190
0.500
1
01/18/23 05:03
MSA
V28980
1,3,5-Trimethyl benzene
0.2893
N9/L
0.180
0.500
1
01/18/23 05:03
MSA
V28980
Vinyl Acetate
<1.00
N9/L
1.00
5.00
1
01/18/23 05:03
MSA
V28980
Vinyl Chloride
<0.170
N9/L
0.170
0.500
1
01/18/23 05:03
MSA
V28980
o-Xylene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:03
MSA
V28980
m,p-Xylene
<0.420
N9/L
0.420
1.00
1
01/18/23 05:03
MSA
V28980
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 47 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97327 Matrix: Aqueous
Sample ID: MW-7 Sampled: 1/10/2023 13:30
Analytical Method: 6200E Prep Batch(es): V28979 01/17/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
01/18/23 05:03
V28980
Surrogate: 4-Bromofluorobenzene
102
Limits:
70-130%
1 01/18/23 05:03 MSA
V28980
Surrogate: Dibromofluoromethane
93.8
Limits:
70-130%
1 01/18/23 05:03 MSA
V28980
Surrogate: 1,2-Dichloroethane - d4
96.6
Limits:
70-130%
1 01/18/23 05:03 MSA
V28980
Surrogate: Toluene-d8
96.4
Limits:
70-130%
1 01/18/23 05:03 MSA
V28980
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23
08:54
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.308
Ng/L
0.308
2.04
1
01/18/23 19:12
JMV
V29002
Acenaphthylene
<0.302
Ng/L
0.302
2.04
1
01/18/23 19:12
JMV
V29002
Anthracene
<0.852
Ng/L
0.852
2.04
1
01/18/23 19:12
JMV
V29002
Benzidine
<1.35
Ng/L
1.35
10.2
1
01/18/23 19:12
JMV
V29002
Benzo(a)anthracene
<0.649
Ng/L
0.649
2.04
1
01/18/23 19:12
JMV
V29002
Benzo(a)pyrene
<1.04
Ng/L
1.04
2.04
1
01/18/23 19:12
JMV
V29002
Benzo(b)fluoranthene
<2.54
Ng/L
2.54
5.10
1
01/18/23 19:12
JMV
V29002
Benzo(g,h,i)perylene
<1.03
Ng/L
1.03
5.10
1
01/18/23 19:12
JMV
V29002
Benzo(k)fluoranthene
<2.03
Ng/L
2.03
5.10
1
01/18/23 19:12
JMV
V29002
Benzoic Acid
<1.12
Ng/L
1.12
10.2
1
01/18/23 19:12
JMV
V29002
Benzyl alcohol
<0.697
Ng/L
0.697
5.10
1
01/18/23 19:12
JMV
V29002
Bis(2-Chloroethoxy)methane
<0.477
Ng/L
0.477
5.10
1
01/18/23 19:12
JMV
V29002
Bis(2-Chloroethyl)ether
<1.06
Ng/L
1.06
5.10
1
01/18/23 19:12
JMV
V29002
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation
Limit
Page 48 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97327
Matrix: Aqueous
Sample ID: MW-7
Sampled:
1/10/2023 13:30
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Bis(2-Chloroisopropyl)ether
<1.10
N9/L
1.10
5.10
1
01/18/23 19:12
JMV
V29002
Bis(2-ethylhexyl)phthalate
<24.5
N9/L
24.5
51.0
1
01/18/23 19:12
JMV
V29002
4-13romophenyl phenyl ether
<1.13
N9/L
1.13
5.10
1
01/18/23 19:12
JMV
V29002
Butyl benzyl phthalate
<1.87
N9/L
1.87
5.10
1
01/18/23 19:12
JMV
V29002
4-Chloro-3-methylphenol
<1.20
N9/L
1.20
5.10
1
01/18/23 19:12
JMV
V29002
2-Chloronaphthalene
<7.53
N9/L
7.53
20.4
1
01/18/23 19:12
JMV
V29002
2-Chlorophenol
<0.956
N9/L
0.956
10.2
1
01/18/23 19:12
JMV
V29002
4-Chlorophenyl phenyl ether
<1.74
N9/L
1.74
5.10
1
01/18/23 19:12
JMV
V29002
Chrysene
<0.413
N9/L
0.413
2.04
1
01/18/23 19:12
JMV
V29002
Dibenz(a,h)anthracene
<0.442
N9/L
0.442
2.04
1
01/18/23 19:12
JMV
V29002
Dibenzofuran
<0.873
N9/L
0.873
5.10
1
01/18/23 19:12
JMV
V29002
1,2-Dichlorobenzene
<2.04
N9/L
2.04
5.10
1
01/18/23 19:12
JMV
V29002
1,3-Dichlorobenzene
<2.04
N9/L
2.04
5.10
1
01/18/23 19:12
JMV
V29002
1,4-Dichlorobenzene
<2.09
N9/L
2.09
5.10
1
01/18/23 19:12
JMV
V29002
3,3'-Dichlorobenzidine
<1.93
N9/L
1.93
5.10
1
01/18/23 19:12
JMV
V29002
2,4-Dichlorophenol
<1.49
N9/L
1.49
10.2
1
01/18/23 19:12
JMV
V29002
Diethyl phthalate
<0.759
N9/L
0.759
5.10
1
01/18/23 19:12
JMV
V29002
Dimethyl phthalate
<0.957
N9/L
0.957
5.10
1
01/18/23 19:12
JMV
V29002
2,4-Dimethylphenol
<1.60
N9/L
1.60
20.4
1
01/18/23 19:12
JMV
V29002
Di-n-butyl phthalate
<2.10
N9/L
2.10
5.10
1
01/18/23 19:12
JMV
V29002
4,6- Din itro-2-methylphenol
<2.11
N9/L
2.11
10.2
1
01/18/23 19:12
JMV
V29002
2,4-Dinitrophenol
<1.96
N9/L
1.96
10.2
1
01/18/23 19:12
JMV
V29002
2,4-Dinitrotoluene
<1.13
N9/L
1.13
5.10
1
01/18/23 19:12
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 49 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97327
Matrix: Aqueous
Sample ID: MW-7
Sampled:
1/10/2023 13:30
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2,6-Dinitrotoluene
<0.825
N9/L
0.825
5.10
1
01/18/23 19:12
JMV
V29002
Di-n-Octyl Phthalate
<1.68
N9/L
1.68
5.10
1
01/18/23 19:12
JMV
V29002
Fluoranthene
<0.255
N9/L
0.255
2.04
1
01/18/23 19:12
JMV
V29002
Fluorene
<0.823
N9/L
0.823
2.04
1
01/18/23 19:12
JMV
V29002
Hexachlorobenzene
<0.998
N9/L
0.998
5.10
1
01/18/23 19:12
JMV
V29002
Hexachlorobutadiene
<2.78
N9/L
2.78
5.10
1
01/18/23 19:12
JMV
V29002
Hexachlorocyclopentadiene
<2.09
N9/L
2.09
5.10
1
01/18/23 19:12
JMV
V29002
Hexachloroethane
<1.80
N9/L
1.80
5.10
1
01/18/23 19:12
JMV
V29002
Indeno(1,2,3-cd)pyrene
<0.486
N9/L
0.486
2.04
1
01/18/23 19:12
JMV
V29002
Isophorone
<0.452
N9/L
0.452
5.10
1
01/18/23 19:12
JMV
V29002
1-Methylnaphthalene
<1.16
N9/L
1.16
2.04
1
01/18/23 19:12
JMV
V29002
2-Methylnaphthalene
<0.679
N9/L
0.679
2.04
1
01/18/23 19:12
JMV
V29002
Naphthalene
<0.742
N9/L
0.742
2.04
1
01/18/23 19:12
JMV
V29002
Nitrobenzene
<0.923
N9/L
0.923
5.10
1
01/18/23 19:12
JMV
V29002
2-Nitrophenol
<0.502
N9/L
0.502
5.10
1
01/18/23 19:12
JMV
V29002
4-Nitrophenol
<1.25
N9/L
1.25
10.2
1
01/18/23 19:12
JMV
V29002
N-Nitrosodiphenylamine
<1.12
N9/L
1.12
5.10
1
01/18/23 19:12
JMV
V29002
N-Nitroso-di-n-propylamine
<0.653
N9/L
0.653
5.10
1
01/18/23 19:12
JMV
V29002
Pentachlorophenol
<1.46
N9/L
1.46
5.10
1
01/18/23 19:12
JMV
V29002
Phenanthrene
<0.436
N9/L
0.436
2.04
1
01/18/23 19:12
JMV
V29002
Phenol
<0.664
N9/L
0.664
5.10
1
01/18/23 19:12
JMV
V29002
Pyrene
<0.442
N9/L
0.442
2.04
1
01/18/23 19:12
JMV
V29002
1,2,4-Trichlorobenzene
<2.25
N9/L
2.25
5.10
1
01/18/23 19:12
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 50 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
Report Date : 01/19/2023
Received : 01/11/2023
Report Number : 23-011-0018
Lab No : 97327
Sample ID: MW-7
REPORT OFANAL YSIS
Matrix: Aqueous
Sampled: 1/10/2023 13:30
Analytical Method: 625.1
Prep Batch(es):
V28943 01/17/23 08:54
Prep Method: 625.1 (Prep)
Test
Results Units
MDL MQL DF
Date / Time By Analytical
Analyzed
Batch
2,4,6-Trichlorophenol
<1.35 N9/L
1.35 5.10 1
01/18/23 19:12 JMV
V29002
Surrogate: Phenol-d5
25.8
Limits: 10-63%
1 01/18/23 19:12 JMV
625.1
Surrogate:2-Fluorobiphenyl
66.7
Limits:49-118%
1 01/18/23 19:12 JMV
V29002
Surrogate:2-Fluorophenol
33.7
Limits:22-84%
1 01/18/23 19:12 JMV
V29002
Surrogate: Nitrobenzene-d5
57.8
Limits: 43-123%
1 01/18/23 19:12 JMV
V29002
Surrogate:4-Terphenyl-d14
74.9
Limits:49-151%
1 01/18/23 19:12 JMV
V29002
Surrogate: 2,4,6-Tribromophenol
69.6
Limits:31-144%
1 01/18/23 19:12 JMV
V29002
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 51 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97328
Matrix: Aqueous
Sample ID: MW-8
Sampled:
1/10/2023 14:10
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
N9/L
1.80
10.0
1
01/18/23 05:28
MSA
V28980
Benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:28
MSA
V28980
Bromobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:28
MSA
V28980
Bromochloromethane
<0.420
N9/L
0.420
1.00
1
01/18/23 05:28
MSA
V28980
Bromodichloromethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:28
MSA
V28980
Bromoform
<1.50
N9/L
1.50
5.00
1
01/18/23 05:28
MSA
V28980
Bromomethane
<0.280
N9/L
0.280
1.00
1
01/18/23 05:28
MSA
V28980
n-Butylbenzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:28
MSA
V28980
sec -Butyl benzene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:28
MSA
V28980
tert-Butyl benzene
<0.920
N9/L
0.920
2.00
1
01/18/23 05:28
MSA
V28980
Carbon Tetrachloride
<0.180
N9/L
0.180
0.500
1
01/18/23 05:28
MSA
V28980
Chlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:28
MSA
V28980
Chlorodibromomethane
<0.190
N9/L
0.190
0.500
1
01/18/23 05:28
MSA
V28980
Chloroethane
<0.430
N9/L
0.430
1.00
1
01/18/23 05:28
MSA
V28980
Chloroform
0.971
N9/L
0.220
0.500
1
01/18/23 05:28
MSA
V28980
Chloromethane
<0.220
N9/L
0.220
0.500
1
01/18/23 05:28
MSA
V28980
2-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:28
MSA
V28980
4-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:28
MSA
V28980
Di -Isopropyl Ether (DIPE)
<0.500
N9/L
0.500
0.500
1
01/18/23 05:28
MSA
V28980
1,2-Dibromo-3-Chloropropane
<1.10
N9/L
1.10
2.00
1
01/18/23 05:28
MSA
V28980
1,2-Dibromoethane
<0.200
N9/L
0.200
0.500
1
01/18/23 05:28
MSA
V28980
Dibromomethane
<0.230
N9/L
0.230
0.500
1
01/18/23 05:28
MSA
V28980
1,2-Dichlorobenzene
<0.220
N9/L
0.220
0.500
1
01/18/23 05:28
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 52 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97328
Matrix: Aqueous
Sample ID: MW-8
Sampled:
1/10/2023 14:10
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:28
MSA
V28980
1,4-Dichlorobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:28
MSA
V28980
Dichlorodifluoromethane
<1.20
N9/L
1.20
5.00
1
01/18/23 05:28
MSA
V28980
1,1-Dichloroethane
<0.240
N9/L
0.240
0.500
1
01/18/23 05:28
MSA
V28980
1,2-Dichloroethane
<0.150
N9/L
0.150
0.500
1
01/18/23 05:28
MSA
V28980
1,1-Dichloroethene
1.33
N9/L
0.150
0.500
1
01/18/23 05:28
MSA
V28980
cis- 1,2-Dichloroethene
2.06
N9/L
0.200
0.500
1
01/18/23 05:28
MSA
V28980
trans-1,2-Dichloroethene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:28
MSA
V28980
1,2-Dichloropropane
<0.190
N9/L
0.190
0.500
1
01/18/23 05:28
MSA
V28980
1,3-Dichloropropane
<0.130
N9/L
0.130
0.500
1
01/18/23 05:28
MSA
V28980
2,2-Dichloropropane
<0.210
N9/L
0.210
2.00
1
01/18/23 05:28
MSA
V28980
1,1-Dichloropropene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:28
MSA
V28980
cis- 1,3-Dichloropropene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:28
MSA
V28980
trans-1,3-Dichloropropene
<0.150
N9/L
0.150
0.500
1
01/18/23 05:28
MSA
V28980
Ethanol
<42.0
N9/L
42.0
200
1
01/18/23 05:28
MSA
V28980
Ethylbenzene
<0.170
N9/L
0.170
0.500
1
01/18/23 05:28
MSA
V28980
Hexachlorobutadiene
<0.350
N9/L
0.350
3.00
1
01/18/23 05:28
MSA
V28980
2-Hexanone
<0.380
N9/L
0.380
1.00
1
01/18/23 05:28
MSA
V28980
Isopropyl benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:28
MSA
V28980
4-Isopropyl toluene
<0.089
N9/L
0.089
0.500
1
01/18/23 05:28
MSA
V28980
Methyl Ethyl Ketone (MEK)
<0.710
N9/L
0.710
5.00
1
01/18/23 05:28
MSA
V28980
Methyl tert-butyl ether (MTBE)
<0.140
N9/L
0.140
1.00
1
01/18/23 05:28
MSA
V28980
4-Methyl-2-Pentanone
<0.078
N9/L
0.078
1.00
1
01/18/23 05:28
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 53 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97328
Matrix: Aqueous
Sample ID: MW-8
Sampled:
1/10/2023 14:10
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200
PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
<0.330
N9/L
0.330
2.00
1
01/18/23 05:28
MSA
V28980
Naphthalene
2.05
N9/L
0.470
1.00
1
01/18/23 05:28
MSA
V28980
n-Propylbenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:28
MSA
V28980
Styrene
<0.220
N9/L
0.220
0.500
1
01/18/23 05:28
MSA
V28980
1,1,1,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:28
MSA
V28980
1,1,2,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:28
MSA
V28980
Tetrachloroethene
1.94
N9/L
0.220
0.500
1
01/18/23 05:28
MSA
V28980
Toluene
<0.220
N9/L
0.220
0.500
1
01/18/23 05:28
MSA
V28980
1,2,3-Trichlorobenzene
<0.380
N9/L
0.380
0.500
1
01/18/23 05:28
MSA
V28980
1,2,4-Trichlorobenzene
<0.310
N9/L
0.310
0.500
1
01/18/23 05:28
MSA
V28980
1,1,1-Trichloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:28
MSA
V28980
1,1,2-Trichloroethane
<0.096
N9/L
0.096
0.500
1
01/18/23 05:28
MSA
V28980
Trichloroethene
3.48
N9/L
0.180
0.500
1
01/18/23 05:28
MSA
V28980
Trichlorofluoromethane
<0.180
N9/L
0.180
0.500
1
01/18/23 05:28
MSA
V28980
1,2,3-Trichloropropane
<0.270
N9/L
0.270
0.500
1
01/18/23 05:28
MSA
V28980
1,2,4-Trimethyl benzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:28
MSA
V28980
1,3,5-Trimethyl benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:28
MSA
V28980
Vinyl Acetate
<1.00
N9/L
1.00
5.00
1
01/18/23 05:28
MSA
V28980
Vinyl Chloride
<0.170
N9/L
0.170
0.500
1
01/18/23 05:28
MSA
V28980
o-Xylene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:28
MSA
V28980
m,p-Xylene
<0.420
N9/L
0.420
1.00
1
01/18/23 05:28
MSA
V28980
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 54 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97328 Matrix: Aqueous
Sample ID: MW-8 Sampled: 1/10/2023 14:10
Analytical Method: 6200E Prep Batch(es): V28979 01/17/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
01/18/23 05:28
V28980
Surrogate: 4-Bromofluorobenzene
103
Limits:
70-130%
1 01/18/23 05:28 MSA
V28980
Surrogate: Dibromofluoromethane
93.6
Limits:
70-130%
1 01/18/23 05:28 MSA
V28980
Surrogate: 1,2-Dichloroethane - d4
93.8
Limits:
70-130%
1 01/18/23 05:28 MSA
V28980
Surrogate: Toluene-d8
99.0
Limits:
70-130%
1 01/18/23 05:28 MSA
V28980
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23
08:54
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.306
Ng/L
0.306
2.03
1
01/18/23 20:20
JMV
V29002
Acenaphthylene
<0.301
Ng/L
0.301
2.03
1
01/18/23 20:20
JMV
V29002
Anthracene
<0.848
Ng/L
0.848
2.03
1
01/18/23 20:20
JMV
V29002
Benzidine
<1.35
Ng/L
1.35
10.2
1
01/18/23 20:20
JMV
V29002
Benzo(a)anthracene
<0.646
Ng/L
0.646
2.03
1
01/18/23 20:20
JMV
V29002
Benzo(a)pyrene
<1.04
Ng/L
1.04
2.03
1
01/18/23 20:20
JMV
V29002
Benzo(b)fluoranthene
<2.53
Ng/L
2.53
5.08
1
01/18/23 20:20
JMV
V29002
Benzo(g,h,i)perylene
<1.03
Ng/L
1.03
5.08
1
01/18/23 20:20
JMV
V29002
Benzo(k)fluoranthene
<2.02
Ng/L
2.02
5.08
1
01/18/23 20:20
JMV
V29002
Benzoic Acid
<1.12
Ng/L
1.12
10.2
1
01/18/23 20:20
JMV
V29002
Benzyl alcohol
<0.694
Ng/L
0.694
5.08
1
01/18/23 20:20
JMV
V29002
Bis(2-Chloroethoxy)methane
<0.475
Ng/L
0.475
5.08
1
01/18/23 20:20
JMV
V29002
Bis(2-Chloroethyl)ether
<1.06
Ng/L
1.06
5.08
1
01/18/23 20:20
JMV
V29002
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation
Limit
Page 55 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97328
Sample ID: MW-8
Matrix: Aqueous
Sampled: 1/10/2023 14:10
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Bis(2-Chloroisopropyl)ether
<1.10
N9/L
1.10
5.08
1
01/18/23 20:20
JMV
V29002
Bis(2-ethylhexyl)phthalate
<24.4
N9/L
24.4
50.8
1
01/18/23 20:20
JMV
V29002
4-13romophenyl phenyl ether
<1.13
N9/L
1.13
5.08
1
01/18/23 20:20
JMV
V29002
Butyl benzyl phthalate
<1.86
N9/L
1.86
5.08
1
01/18/23 20:20
JMV
V29002
4-Chloro-3-methylphenol
<1.20
N9/L
1.20
5.08
1
01/18/23 20:20
JMV
V29002
2-Chloronaphthalene
<7.49
N9/L
7.49
20.3
1
01/18/23 20:20
JMV
V29002
2-Chlorophenol
<0.956
N9/L
0.956
10.2
1
01/18/23 20:20
JMV
V29002
4-Chlorophenyl phenyl ether
<1.74
N9/L
1.74
5.08
1
01/18/23 20:20
JMV
V29002
Chrysene
<0.411
N9/L
0.411
2.03
1
01/18/23 20:20
JMV
V29002
Dibenz(a,h)anthracene
<0.440
N9/L
0.440
2.03
1
01/18/23 20:20
JMV
V29002
Dibenzofuran
<0.869
N9/L
0.869
5.08
1
01/18/23 20:20
JMV
V29002
1,2-Dichlorobenzene
<2.03
N9/L
2.03
5.08
1
01/18/23 20:20
JMV
V29002
1,3-Dichlorobenzene
<2.03
N9/L
2.03
5.08
1
01/18/23 20:20
JMV
V29002
1,4-Dichlorobenzene
<2.08
N9/L
2.08
5.08
1
01/18/23 20:20
JMV
V29002
3,3'-Dichlorobenzidine
<1.92
N9/L
1.92
5.08
1
01/18/23 20:20
JMV
V29002
2,4-Dichlorophenol
<1.49
N9/L
1.49
10.2
1
01/18/23 20:20
JMV
V29002
Diethyl phthalate
<0.756
N9/L
0.756
5.08
1
01/18/23 20:20
JMV
V29002
Dimethyl phthalate
<0.954
N9/L
0.954
5.08
1
01/18/23 20:20
JMV
V29002
2,4-Dimethylphenol
<1.59
N9/L
1.59
20.3
1
01/18/23 20:20
JMV
V29002
Di-n-butyl phthalate
<2.09
N9/L
2.09
5.08
1
01/18/23 20:20
JMV
V29002
4,6- Din itro-2-methylphenol
<2.11
N9/L
2.11
10.2
1
01/18/23 20:20
JMV
V29002
2,4-Dinitrophenol
<1.96
N9/L
1.96
10.2
1
01/18/23 20:20
JMV
V29002
2,4-Dinitrotoluene
<1.13
N9/L
1.13
5.08
1
01/18/23 20:20
JMV
V29002
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 56 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97328
Matrix: Aqueous
Sample ID: MW-8
Sampled:
1/10/2023 14:10
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2,6-Dinitrotoluene
<0.821
N9/L
0.821
5.08
1
01/18/23 20:20
JMV
V29002
Di-n-Octyl Phthalate
<1.68
N9/L
1.68
5.08
1
01/18/23 20:20
JMV
V29002
Fluoranthene
<0.253
N9/L
0.253
2.03
1
01/18/23 20:20
JMV
V29002
Fluorene
<0.819
N9/L
0.819
2.03
1
01/18/23 20:20
JMV
V29002
Hexachlorobenzene
<0.994
N9/L
0.994
5.08
1
01/18/23 20:20
JMV
V29002
Hexachlorobutadiene
<2.77
N9/L
2.77
5.08
1
01/18/23 20:20
JMV
V29002
Hexachlorocyclopentadiene
<2.08
N9/L
2.08
5.08
1
01/18/23 20:20
JMV
V29002
Hexachloroethane
<1.79
N9/L
1.79
5.08
1
01/18/23 20:20
JMV
V29002
Indeno(1,2,3-cd)pyrene
<0.484
N9/L
0.484
2.03
1
01/18/23 20:20
JMV
V29002
Isophorone
<0.451
N9/L
0.451
5.08
1
01/18/23 20:20
JMV
V29002
1-Methylnaphthalene
<1.16
N9/L
1.16
2.03
1
01/18/23 20:20
JMV
V29002
2-Methylnaphthalene
<0.675
N9/L
0.675
2.03
1
01/18/23 20:20
JMV
V29002
Naphthalene
<0.738
N9/L
0.738
2.03
1
01/18/23 20:20
JMV
V29002
Nitrobenzene
<0.919
N9/L
0.919
5.08
1
01/18/23 20:20
JMV
V29002
2-Nitrophenol
<0.500
N9/L
0.500
5.08
1
01/18/23 20:20
JMV
V29002
4-Nitrophenol
<1.25
N9/L
1.25
10.2
1
01/18/23 20:20
JMV
V29002
N-Nitrosodiphenylamine
<1.12
N9/L
1.12
5.08
1
01/18/23 20:20
JMV
V29002
N-Nitroso-di-n-propylamine
<0.651
N9/L
0.651
5.08
1
01/18/23 20:20
JMV
V29002
Pentachlorophenol
<1.45
N9/L
1.45
5.08
1
01/18/23 20:20
JMV
V29002
Phenanthrene
<0.434
N9/L
0.434
2.03
1
01/18/23 20:20
JMV
V29002
Phenol
<0.661
N9/L
0.661
5.08
1
01/18/23 20:20
JMV
V29002
Pyrene
<0.440
N9/L
0.440
2.03
1
01/18/23 20:20
JMV
V29002
1,2,4-Trichlorobenzene
<2.25
N9/L
2.25
5.08
1
01/18/23 20:20
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 57 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
Report Date : 01/19/2023
Received : 01/11/2023
Report Number : 23-011-0018
Lab No : 97328
Sample ID: MW-8
REPORT OFANAL YSIS
Matrix: Aqueous
Sampled: 1/10/2023 14:10
Analytical Method: 625.1
Prep Batch(es):
V28943 01/17/23 08:54
Prep Method: 625.1 (Prep)
Test
Results Units
MDL MQL DF
Date / Time By Analytical
Analyzed
Batch
2,4,6-Trichlorophenol
<1.34 N9/L
1.34 5.08 1
01/18/23 20:20 JMV
V29002
Surrogate: Phenol-d5
26.4
Limits: 10-63%
1 01/18/23 20:20 JMV
625.1
Surrogate: 2-Fluorobiphenyl
66.1
Limits: 49-118%
1 01/18/23 20:20 JMV
V29002
Surrogate: 2-Fluorophenol
35.0
Limits: 22-84%
1 01/18/23 20:20 JMV
V29002
Surrogate: Nitrobenzene-d5
55.5
Limits: 43-123%
1 01/18/23 20:20 JMV
V29002
Surrogate: 4-Terphenyl-d14
79.5
Limits: 49-151%
1 01/18/23 20:20 JMV
V29002
Surrogate: 2,4,6-Tribromophenol
76.6
Limits: 31-144%
1 01/18/23 20:20 JMV
V29002
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 58 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97329
Matrix: Aqueous
Sample ID: MW-9
Sampled:
1/10/2023 12:35
Analytical Method: 6200E
Prep Batch(es):
V29020
01/18/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
5.823
Ng/L
1.80
10.0
1
01/19/23 08:09
MSA
V29021
Benzene
0.3153
Ng/L
0.180
0.500
1
01/19/23 08:09
MSA
V29021
Bromobenzene
<0.210
Ng/L
0.210
0.500
1
01/19/23 08:09
MSA
V29021
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
01/19/23 08:09
MSA
V29021
Bromodichloromethane
<0.160
Ng/L
0.160
0.500
1
01/19/23 08:09
MSA
V29021
Bromoform
<1.50
Ng/L
1.50
5.00
1
01/19/23 08:09
MSA
V29021
Bromomethane
<0.280
Ng/L
0.280
1.00
1
01/19/23 08:09
MSA
V29021
n-Butylbenzene
1.06
Ng/L
0.180
0.500
1
01/19/23 08:09
MSA
V29021
sec -Butyl benzene
0.981
Ng/L
0.200
0.500
1
01/19/23 08:09
MSA
V29021
tert-Butyl benzene
1.223
Ng/L
0.920
2.00
1
01/19/23 08:09
MSA
V29021
Carbon Tetrachloride
<0.180
Ng/L
0.180
0.500
1
01/19/23 08:09
MSA
V29021
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
01/19/23 08:09
MSA
V29021
Chlorodibromomethane
<0.190
Ng/L
0.190
0.500
1
01/19/23 08:09
MSA
V29021
Chloroethane
<0.430
Ng/L
0.430
1.00
1
01/19/23 08:09
MSA
V29021
Chloroform
<0.220
Ng/L
0.220
0.500
1
01/19/23 08:09
MSA
V29021
Chloromethane
<0.220
Ng/L
0.220
0.500
1
01/19/23 08:09
MSA
V29021
2-Chlorotoluene
<0.200
Ng/L
0.200
0.500
1
01/19/23 08:09
MSA
V29021
4-Chlorotoluene
<0.200
Ng/L
0.200
0.500
1
01/19/23 08:09
MSA
V29021
Di -Isopropyl Ether (DIPE)
1.01
Ng/L
0.500
0.500
1
01/19/23 08:09
MSA
V29021
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
01/19/23 08:09
MSA
V29021
1,2-Dibromoethane
<0.200
Ng/L
0.200
0.500
1
01/19/23 08:09
MSA
V29021
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
01/19/23 08:09
MSA
V29021
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
01/19/23 08:09
MSA
V29021
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 59 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97329
Matrix: Aqueous
Sample ID: MW-9
Sampled:
1/10/2023 12:35
Analytical Method: 6200E
Prep Batch(es):
V29020
01/18/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<0.190
N9/L
0.190
0.500
1
01/19/23 08:09
MSA
V29021
1,4-Dichlorobenzene
<0.210
N9/L
0.210
0.500
1
01/19/23 08:09
MSA
V29021
Dichlorodifluoromethane
<1.20
N9/L
1.20
5.00
1
01/19/23 08:09
MSA
V29021
1,1-Dichloroethane
<0.240
N9/L
0.240
0.500
1
01/19/23 08:09
MSA
V29021
1,2-Dichloroethane
<0.150
N9/L
0.150
0.500
1
01/19/23 08:09
MSA
V29021
1,1-Dichloroethene
<0.150
N9/L
0.150
0.500
1
01/19/23 08:09
MSA
V29021
cis- 1,2-Dichloroethene
<0.200
N9/L
0.200
0.500
1
01/19/23 08:09
MSA
V29021
trans-1,2-Dichloroethene
<0.180
N9/L
0.180
0.500
1
01/19/23 08:09
MSA
V29021
1,2-Dichloropropane
<0.190
N9/L
0.190
0.500
1
01/19/23 08:09
MSA
V29021
1,3-Dichloropropane
<0.130
N9/L
0.130
0.500
1
01/19/23 08:09
MSA
V29021
2,2-Dichloropropane
<0.210
N9/L
0.210
2.00
1
01/19/23 08:09
MSA
V29021
1,1-Dichloropropene
<0.200
N9/L
0.200
0.500
1
01/19/23 08:09
MSA
V29021
cis- 1,3-Dichloropropene
<0.210
N9/L
0.210
0.500
1
01/19/23 08:09
MSA
V29021
trans-1,3-Dichloropropene
<0.150
N9/L
0.150
0.500
1
01/19/23 08:09
MSA
V29021
Ethanol
<42.0
N9/L
42.0
200
1
01/19/23 08:09
MSA
V29021
Ethylbenzene
1.94
N9/L
0.170
0.500
1
01/19/23 08:09
MSA
V29021
Hexachlorobutadiene
<0.350
N9/L
0.350
3.00
1
01/19/23 08:09
MSA
V29021
2-Hexanone
<0.380
N9/L
0.380
1.00
1
01/19/23 08:09
MSA
V29021
Isopropyl benzene
1.66
N9/L
0.180
0.500
1
01/19/23 08:09
MSA
V29021
4-Isopropyl toluene
2.26
N9/L
0.089
0.500
1
01/19/23 08:09
MSA
V29021
Methyl Ethyl Ketone (MEK)
<0.710
N9/L
0.710
5.00
1
01/19/23 08:09
MSA
V29021
Methyl tert-butyl ether (MTBE)
<0.140
N9/L
0.140
1.00
1
01/19/23 08:09
MSA
V29021
4-Methyl-2-Pentanone
2.66
N9/L
0.078
1.00
1
01/19/23 08:09
MSA
V29021
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 60 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97329
Matrix: Aqueous
Sample ID: MW-9
Sampled:
1/10/2023 12:35
Analytical Method: 6200E
Prep Batch(es):
V29020
01/18/23 14:00
Prep Method: 6200
PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
0.4043
N9/L
0.330
2.00
1
01/19/23 08:09
MSA
V29021
Naphthalene
88.4
N9/L
0.470
1.00
1
01/19/23 08:09
MSA
V29021
n-Propylbenzene
2.87
N9/L
0.190
0.500
1
01/19/23 08:09
MSA
V29021
Styrene
<0.220
N9/L
0.220
0.500
1
01/19/23 08:09
MSA
V29021
1,1,1,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/19/23 08:09
MSA
V29021
1,1,2,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/19/23 08:09
MSA
V29021
Tetrachloroethene
<0.220
N9/L
0.220
0.500
1
01/19/23 08:09
MSA
V29021
Toluene
2.13
N9/L
0.220
0.500
1
01/19/23 08:09
MSA
V29021
1,2,3-Trichlorobenzene
<0.380
N9/L
0.380
0.500
1
01/19/23 08:09
MSA
V29021
1,2,4-Trichlorobenzene
<0.310
N9/L
0.310
0.500
1
01/19/23 08:09
MSA
V29021
1,1,1-Trichloroethane
<0.160
N9/L
0.160
0.500
1
01/19/23 08:09
MSA
V29021
1,1,2-Trichloroethane
<0.096
N9/L
0.096
0.500
1
01/19/23 08:09
MSA
V29021
Trichloroethene
<0.180
N9/L
0.180
0.500
1
01/19/23 08:09
MSA
V29021
Trichlorofluoromethane
<0.180
N9/L
0.180
0.500
1
01/19/23 08:09
MSA
V29021
1,2,3-Trichloropropane
<0.270
N9/L
0.270
0.500
1
01/19/23 08:09
MSA
V29021
1,2,4-Trimethyl benzene
33.0
N9/L
0.190
0.500
1
01/19/23 08:09
MSA
V29021
1,3,5-Trimethyl benzene
3.89
N9/L
0.180
0.500
1
01/19/23 08:09
MSA
V29021
Vinyl Acetate
<1.00
N9/L
1.00
5.00
1
01/19/23 08:09
MSA
V29021
Vinyl Chloride
<0.170
N9/L
0.170
0.500
1
01/19/23 08:09
MSA
V29021
o-Xylene
5.51
N9/L
0.210
0.500
1
01/19/23 08:09
MSA
V29021
m,p-Xylene
11.3
N9/L
0.420
1.00
1
01/19/23 08:09
MSA
V29021
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 61 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97329 Matrix: Aqueous
Sample ID: MW-9 Sampled: 1/10/2023 12:35
Analytical Method: 6200E Prep Batch(es): V29020 01/18/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
16.8
Ng/L
0.210
0.500
1
01/19/23 08:09
V29021
Surrogate: 4-Bromofluorobenzene
102
Limits:
70-130%
1 01/19/23 08:09 MSA
V29021
Surrogate: Dibromofluoromethane
93.2
Limits:
70-130%
1 01/19/23 08:09 MSA
V29021
Surrogate: 1,2-Dichloroethane - d4
91.0
Limits:
70-130%
1 01/19/23 08:09 MSA
V29021
Surrogate: Toluene-d8
99.6
Limits:
70-130%
1 01/19/23 08:09 MSA
V29021
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23
08:54
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.314
Ng/L
0.314
2.08
1
01/18/23 18:27
JMV
V29002
Acenaphthylene
<0.308
Ng/L
0.308
2.08
1
01/18/23 18:27
JMV
V29002
Anthracene
<0.869
Ng/L
0.869
2.08
1
01/18/23 18:27
JMV
V29002
Benzidine
<1.37
Ng/L
1.37
10.4
1
01/18/23 18:27
JMV
V29002
Benzo(a)anthracene
<0.662
Ng/L
0.662
2.08
1
01/18/23 18:27
JMV
V29002
Benzo(a)pyrene
<1.06
Ng/L
1.06
2.08
1
01/18/23 18:27
JMV
V29002
Benzo(b)fluoranthene
<2.59
Ng/L
2.59
5.21
1
01/18/23 18:27
JMV
V29002
Benzo(g,h,i)perylene
<1.05
Ng/L
1.05
5.21
1
01/18/23 18:27
JMV
V29002
Benzo(k)fluoranthene
<2.07
Ng/L
2.07
5.21
1
01/18/23 18:27
JMV
V29002
Benzoic Acid
<1.14
Ng/L
1.14
10.4
1
01/18/23 18:27
JMV
V29002
Benzyl alcohol
<0.712
Ng/L
0.712
5.21
1
01/18/23 18:27
JMV
V29002
Bis(2-Chloroethoxy)methane
<0.487
Ng/L
0.487
5.21
1
01/18/23 18:27
JMV
V29002
Bis(2-Chloroethyl)ether
<1.08
Ng/L
1.08
5.21
1
01/18/23 18:27
JMV
V29002
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation
Limit
Page 62 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97329
Matrix: Aqueous
Sample ID: MW-9
Sampled:
1/10/2023 12:35
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Bis(2-Chloroisopropyl)ether
<1.13
N9/L
1.13
5.21
1
01/18/23 18:27
JMV
V29002
Bis(2-ethylhexyl)phthalate
<25.0
N9/L
25.0
52.1
1
01/18/23 18:27
JMV
V29002
4-13romophenyl phenyl ether
<1.16
N9/L
1.16
5.21
1
01/18/23 18:27
JMV
V29002
Butyl benzyl phthalate
<1.91
N9/L
1.91
5.21
1
01/18/23 18:27
JMV
V29002
4-Chloro-3-methylphenol
<1.23
N9/L
1.23
5.21
1
01/18/23 18:27
JMV
V29002
2-Chloronaphthalene
<7.68
N9/L
7.68
20.8
1
01/18/23 18:27
JMV
V29002
2-Chlorophenol
<0.975
N9/L
0.975
10.4
1
01/18/23 18:27
JMV
V29002
4-Chlorophenyl phenyl ether
<1.78
N9/L
1.78
5.21
1
01/18/23 18:27
JMV
V29002
Chrysene
<0.421
N9/L
0.421
2.08
1
01/18/23 18:27
JMV
V29002
Dibenz(a,h)anthracene
<0.451
N9/L
0.451
2.08
1
01/18/23 18:27
JMV
V29002
Dibenzofuran
<0.891
N9/L
0.891
5.21
1
01/18/23 18:27
JMV
V29002
1,2-Dichlorobenzene
<2.08
N9/L
2.08
5.21
1
01/18/23 18:27
JMV
V29002
1,3-Dichlorobenzene
<2.08
N9/L
2.08
5.21
1
01/18/23 18:27
JMV
V29002
1,4-Dichlorobenzene
<2.14
N9/L
2.14
5.21
1
01/18/23 18:27
JMV
V29002
3,3'-Dichlorobenzidine
<1.97
N9/L
1.97
5.21
1
01/18/23 18:27
JMV
V29002
2,4-Dichlorophenol
<1.52
N9/L
1.52
10.4
1
01/18/23 18:27
JMV
V29002
Diethyl phthalate
<0.776
N9/L
0.776
5.21
1
01/18/23 18:27
JMV
V29002
Dimethyl phthalate
<0.978
N9/L
0.978
5.21
1
01/18/23 18:27
JMV
V29002
2,4-Dimethylphenol
<1.63
N9/L
1.63
20.8
1
01/18/23 18:27
JMV
V29002
Di-n-butyl phthalate
<2.15
N9/L
2.15
5.21
1
01/18/23 18:27
JMV
V29002
4,6- Din itro-2-methylphenol
<2.15
N9/L
2.15
10.4
1
01/18/23 18:27
JMV
V29002
2,4-Dinitrophenol
<2.00
N9/L
2.00
10.4
1
01/18/23 18:27
JMV
V29002
2,4-Dinitrotoluene
<1.16
N9/L
1.16
5.21
1
01/18/23 18:27
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 63 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97329
Matrix: Aqueous
Sample ID: MW-9
Sampled:
1/10/2023 12:35
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2,6-Dinitrotoluene
<0.842
N9/L
0.842
5.21
1
01/18/23 18:27
JMV
V29002
Di-n-Octyl Phthalate
<1.72
N9/L
1.72
5.21
1
01/18/23 18:27
JMV
V29002
Fluoranthene
<0.260
N9/L
0.260
2.08
1
01/18/23 18:27
JMV
V29002
Fluorene
5.35
N9/L
0.839
2.08
1
01/18/23 18:27
JMV
V29002
Hexachlorobenzene
<1.02
N9/L
1.02
5.21
1
01/18/23 18:27
JMV
V29002
Hexachlorobutadiene
<2.84
N9/L
2.84
5.21
1
01/18/23 18:27
JMV
V29002
Hexachlorocyclopentadiene
<2.14
N9/L
2.14
5.21
1
01/18/23 18:27
JMV
V29002
Hexachloroethane
<1.83
N9/L
1.83
5.21
1
01/18/23 18:27
JMV
V29002
Indeno(1,2,3-cd)pyrene
<0.496
N9/L
0.496
2.08
1
01/18/23 18:27
JMV
V29002
Isophorone
<0.462
N9/L
0.462
5.21
1
01/18/23 18:27
JMV
V29002
1-Methylnaphthalene
52.1
N9/L
1.19
2.08
1
01/18/23 18:27
JMV
V29002
2-Methylnaphthalene
60.9
N9/L
0.692
2.08
1
01/18/23 18:27
JMV
V29002
Naphthalene
37.2
N9/L
0.757
2.08
1
01/18/23 18:27
JMV
V29002
Nitrobenzene
<0.943
N9/L
0.943
5.21
1
01/18/23 18:27
JMV
V29002
2-Nitrophenol
<0.513
N9/L
0.513
5.21
1
01/18/23 18:27
JMV
V29002
4-Nitrophenol
<1.28
N9/L
1.28
10.4
1
01/18/23 18:27
JMV
V29002
N-Nitrosodiphenylamine
<1.15
N9/L
1.15
5.21
1
01/18/23 18:27
JMV
V29002
N-Nitroso-di-n-propylamine
<0.667
N9/L
0.667
5.21
1
01/18/23 18:27
JMV
V29002
Pentachlorophenol
<1.49
N9/L
1.49
5.21
1
01/18/23 18:27
JMV
V29002
Phenanthrene
6.09
N9/L
0.445
2.08
1
01/18/23 18:27
JMV
V29002
Phenol
<0.678
N9/L
0.678
5.21
1
01/18/23 18:27
JMV
V29002
Pyrene
<0.451
N9/L
0.451
2.08
1
01/18/23 18:27
JMV
V29002
1,2,4-Trichlorobenzene
<2.30
N9/L
2.30
5.21
1
01/18/23 18:27
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 64 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
Report Date : 01/19/2023
Received : 01/11/2023
Report Number : 23-011-0018
Lab No : 97329
Sample ID: MW-9
REPORT OFANAL YSIS
Matrix: Aqueous
Sampled: 1/10/2023 12:35
Analytical Method: 625.1
Prep Batch(es):
V28943 01/17/23 08:54
Prep Method: 625.1 (Prep)
Test
Results Units
MDL MQL DF
Date / Time By Analytical
Analyzed
Batch
2,4,6-Trichlorophenol
<1.38 N9/L
1.38 5.21 1
01/18/23 18:27 JMV
V29002
Surrogate: Phenol-d5
28.8
Limits: 10-63%
1 01/18/23 18:27 JMV
625.1
Surrogate:2-Fluorobiphenyl
67.2
Limits:49-118%
1 01/18/23 18:27 JMV
V29002
Surrogate:2-Fluorophenol
39.0
Limits:22-84%
1 01/18/23 18:27 JMV
V29002
Surrogate: Nitrobenzene-d5
63.9
Limits: 43-123%
1 01/18/23 18:27 JMV
V29002
Surrogate:4-Terphenyl-d14
82.5
Limits:49-151%
1 01/18/23 18:27 JMV
V29002
Surrogate: 2,4,6-Tribromophenol
70.5
Limits:31-144%
1 01/18/23 18:27 JMV
V29002
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 65 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97330
Matrix: Aqueous
Sample ID: MW-10
Sampled:
1/10/2023 13:00
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
N9/L
1.80
10.0
1
01/18/23 05:54
MSA
V28980
Benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:54
MSA
V28980
Bromobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:54
MSA
V28980
Bromochloromethane
<0.420
N9/L
0.420
1.00
1
01/18/23 05:54
MSA
V28980
Bromodichloromethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:54
MSA
V28980
Bromoform
<1.50
N9/L
1.50
5.00
1
01/18/23 05:54
MSA
V28980
Bromomethane
<0.280
N9/L
0.280
1.00
1
01/18/23 05:54
MSA
V28980
n-Butylbenzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:54
MSA
V28980
sec -Butyl benzene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:54
MSA
V28980
tert-Butyl benzene
<0.920
N9/L
0.920
2.00
1
01/18/23 05:54
MSA
V28980
Carbon Tetrachloride
<0.180
N9/L
0.180
0.500
1
01/18/23 05:54
MSA
V28980
Chlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:54
MSA
V28980
Chlorodibromomethane
<0.190
N9/L
0.190
0.500
1
01/18/23 05:54
MSA
V28980
Chloroethane
<0.430
N9/L
0.430
1.00
1
01/18/23 05:54
MSA
V28980
Chloroform
0.537
N9/L
0.220
0.500
1
01/18/23 05:54
MSA
V28980
Chloromethane
<0.220
N9/L
0.220
0.500
1
01/18/23 05:54
MSA
V28980
2-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:54
MSA
V28980
4-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:54
MSA
V28980
Di -Isopropyl Ether (DIPE)
<0.500
N9/L
0.500
0.500
1
01/18/23 05:54
MSA
V28980
1,2-Dibromo-3-Chloropropane
<1.10
N9/L
1.10
2.00
1
01/18/23 05:54
MSA
V28980
1,2-Dibromoethane
<0.200
N9/L
0.200
0.500
1
01/18/23 05:54
MSA
V28980
Dibromomethane
<0.230
N9/L
0.230
0.500
1
01/18/23 05:54
MSA
V28980
1,2-Dichlorobenzene
<0.220
N9/L
0.220
0.500
1
01/18/23 05:54
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 66 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97330
Matrix: Aqueous
Sample ID: MW-10
Sampled:
1/10/2023 13:00
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:54
MSA
V28980
1,4-Dichlorobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:54
MSA
V28980
Dichlorodifluoromethane
<1.20
N9/L
1.20
5.00
1
01/18/23 05:54
MSA
V28980
1,1-Dichloroethane
<0.240
N9/L
0.240
0.500
1
01/18/23 05:54
MSA
V28980
1,2-Dichloroethane
<0.150
N9/L
0.150
0.500
1
01/18/23 05:54
MSA
V28980
1,1-Dichloroethene
0.3743
N9/L
0.150
0.500
1
01/18/23 05:54
MSA
V28980
cis- 1,2-Dichloroethene
11.4
N9/L
0.200
0.500
1
01/18/23 05:54
MSA
V28980
trans-1,2-Dichloroethene
0.633
N9/L
0.180
0.500
1
01/18/23 05:54
MSA
V28980
1,2-Dichloropropane
<0.190
N9/L
0.190
0.500
1
01/18/23 05:54
MSA
V28980
1,3-Dichloropropane
<0.130
N9/L
0.130
0.500
1
01/18/23 05:54
MSA
V28980
2,2-Dichloropropane
<0.210
N9/L
0.210
2.00
1
01/18/23 05:54
MSA
V28980
1,1-Dichloropropene
<0.200
N9/L
0.200
0.500
1
01/18/23 05:54
MSA
V28980
cis- 1,3-Dichloropropene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:54
MSA
V28980
trans-1,3-Dichloropropene
<0.150
N9/L
0.150
0.500
1
01/18/23 05:54
MSA
V28980
Ethanol
<42.0
N9/L
42.0
200
1
01/18/23 05:54
MSA
V28980
Ethylbenzene
<0.170
N9/L
0.170
0.500
1
01/18/23 05:54
MSA
V28980
Hexachlorobutadiene
<0.350
N9/L
0.350
3.00
1
01/18/23 05:54
MSA
V28980
2-Hexanone
<0.380
N9/L
0.380
1.00
1
01/18/23 05:54
MSA
V28980
Isopropyl benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:54
MSA
V28980
4-Isopropyl toluene
<0.089
N9/L
0.089
0.500
1
01/18/23 05:54
MSA
V28980
Methyl Ethyl Ketone (MEK)
<0.710
N9/L
0.710
5.00
1
01/18/23 05:54
MSA
V28980
Methyl tert-butyl ether (MTBE)
<0.140
N9/L
0.140
1.00
1
01/18/23 05:54
MSA
V28980
4-Methyl-2-Pentanone
<0.078
N9/L
0.078
1.00
1
01/18/23 05:54
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 67 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97330
Matrix: Aqueous
Sample ID: MW-10
Sampled:
1/10/2023 13:00
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200
PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
<0.330
N9/L
0.330
2.00
1
01/18/23 05:54
MSA
V28980
Naphthalene
<0.470
N9/L
0.470
1.00
1
01/18/23 05:54
MSA
V28980
n-Propylbenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:54
MSA
V28980
Styrene
<0.220
N9/L
0.220
0.500
1
01/18/23 05:54
MSA
V28980
1,1,1,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:54
MSA
V28980
1,1,2,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:54
MSA
V28980
Tetrachloroethene
6.96
N9/L
0.220
0.500
1
01/18/23 05:54
MSA
V28980
Toluene
<0.220
N9/L
0.220
0.500
1
01/18/23 05:54
MSA
V28980
1,2,3-Trichlorobenzene
<0.380
N9/L
0.380
0.500
1
01/18/23 05:54
MSA
V28980
1,2,4-Trichlorobenzene
<0.310
N9/L
0.310
0.500
1
01/18/23 05:54
MSA
V28980
1,1,1-Trichloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 05:54
MSA
V28980
1,1,2-Trichloroethane
<0.096
N9/L
0.096
0.500
1
01/18/23 05:54
MSA
V28980
Trichloroethene
16.1
N9/L
0.180
0.500
1
01/18/23 05:54
MSA
V28980
Trichlorofluoromethane
<0.180
N9/L
0.180
0.500
1
01/18/23 05:54
MSA
V28980
1,2,3-Trichloropropane
<0.270
N9/L
0.270
0.500
1
01/18/23 05:54
MSA
V28980
1,2,4-Trimethyl benzene
<0.190
N9/L
0.190
0.500
1
01/18/23 05:54
MSA
V28980
1,3,5-Trimethyl benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 05:54
MSA
V28980
Vinyl Acetate
<1.00
N9/L
1.00
5.00
1
01/18/23 05:54
MSA
V28980
Vinyl Chloride
<0.170
N9/L
0.170
0.500
1
01/18/23 05:54
MSA
V28980
o-Xylene
<0.210
N9/L
0.210
0.500
1
01/18/23 05:54
MSA
V28980
m,p-Xylene
<0.420
N9/L
0.420
1.00
1
01/18/23 05:54
MSA
V28980
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 68 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97330 Matrix: Aqueous
Sample ID: MW-10 Sampled: 1/10/2023 13:00
Analytical Method: 6200E Prep Batch(es): V28979 01/17/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
01/18/23 05:54
V28980
Surrogate: 4-Bromofluorobenzene
101
Limits:
70-130%
1 01/18/23 05:54 MSA
V28980
Surrogate: Dibromofluoromethane
95.2
Limits:
70-130%
1 01/18/23 05:54 MSA
V28980
Surrogate: 1,2-Dichloroethane - d4
89.8
Limits:
70-130%
1 01/18/23 05:54 MSA
V28980
Surrogate: Toluene-d8
99.0
Limits:
70-130%
1 01/18/23 05:54 MSA
V28980
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23
08:54
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MOL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.303
Ng/L
0.303
2.01
1
01/18/23 18:50
JMV
V29002
Acenaphthylene
<0.298
Ng/L
0.298
2.01
1
01/18/23 18:50
JMV
V29002
Anthracene
<0.840
Ng/L
0.840
2.01
1
01/18/23 18:50
JMV
V29002
Benzidine
<1.33
Ng/L
1.33
10.1
1
01/18/23 18:50
JMV
V29002
Benzo(a)anthracene
<0.640
Ng/L
0.640
2.01
1
01/18/23 18:50
JMV
V29002
Benzo(a)pyrene
<1.03
Ng/L
1.03
2.01
1
01/18/23 18:50
JMV
V29002
Benzo(b)fluoranthene
<2.50
Ng/L
2.50
5.03
1
01/18/23 18:50
JMV
V29002
Benzo(g,h,i)perylene
<1.02
Ng/L
1.02
5.03
1
01/18/23 18:50
JMV
V29002
Benzo(k)fluoranthene
<2.00
Ng/L
2.00
5.03
1
01/18/23 18:50
JMV
V29002
Benzoic Acid
<1.11
Ng/L
1.11
10.1
1
01/18/23 18:50
JMV
V29002
Benzyl alcohol
<0.688
Ng/L
0.688
5.03
1
01/18/23 18:50
JMV
V29002
Bis(2-Chloroethoxy)methane
<0.470
Ng/L
0.470
5.03
1
01/18/23 18:50
JMV
V29002
Bis(2-Chloroethyl)ether
<1.05
Ng/L
1.05
5.03
1
01/18/23 18:50
JMV
V29002
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation
Limit
Page 69 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97330
Matrix: Aqueous
Sample ID: MW-10
Sampled:
1/10/2023 13:00
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Bis(2-Chloroisopropyl)ether
<1.09
N9/L
1.09
5.03
1
01/18/23 18:50
JMV
V29002
Bis(2-ethylhexyl)phthalate
<24.2
N9/L
24.2
50.3
1
01/18/23 18:50
JMV
V29002
4-13romophenyl phenyl ether
<1.12
N9/L
1.12
5.03
1
01/18/23 18:50
JMV
V29002
Butyl benzyl phthalate
<1.84
N9/L
1.84
5.03
1
01/18/23 18:50
JMV
V29002
4-Chloro-3-methylphenol
<1.19
N9/L
1.19
5.03
1
01/18/23 18:50
JMV
V29002
2-Chloronaphthalene
<7.42
N9/L
7.42
20.1
1
01/18/23 18:50
JMV
V29002
2-Chlorophenol
<0.947
N9/L
0.947
10.1
1
01/18/23 18:50
JMV
V29002
4-Chlorophenyl phenyl ether
<1.72
N9/L
1.72
5.03
1
01/18/23 18:50
JMV
V29002
Chrysene
<0.407
N9/L
0.407
2.01
1
01/18/23 18:50
JMV
V29002
Dibenz(a,h)anthracene
<0.436
N9/L
0.436
2.01
1
01/18/23 18:50
JMV
V29002
Dibenzofuran
<0.861
N9/L
0.861
5.03
1
01/18/23 18:50
JMV
V29002
1,2-Dichlorobenzene
<2.01
N9/L
2.01
5.03
1
01/18/23 18:50
JMV
V29002
1,3-Dichlorobenzene
<2.01
N9/L
2.01
5.03
1
01/18/23 18:50
JMV
V29002
1,4-Dichlorobenzene
<2.06
N9/L
2.06
5.03
1
01/18/23 18:50
JMV
V29002
3,3'-Dichlorobenzidine
<1.90
N9/L
1.90
5.03
1
01/18/23 18:50
JMV
V29002
2,4-Dichlorophenol
<1.47
N9/L
1.47
10.1
1
01/18/23 18:50
JMV
V29002
Diethyl phthalate
<0.749
N9/L
0.749
5.03
1
01/18/23 18:50
JMV
V29002
Dimethyl phthalate
<0.944
N9/L
0.944
5.03
1
01/18/23 18:50
JMV
V29002
2,4-Dimethylphenol
<1.58
N9/L
1.58
20.1
1
01/18/23 18:50
JMV
V29002
Di-n-butyl phthalate
<2.07
N9/L
2.07
5.03
1
01/18/23 18:50
JMV
V29002
4,6- Din itro-2-methylphenol
<2.09
N9/L
2.09
10.1
1
01/18/23 18:50
JMV
V29002
2,4-Dinitrophenol
<1.94
N9/L
1.94
10.1
1
01/18/23 18:50
JMV
V29002
2,4-Dinitrotoluene
<1.12
N9/L
1.12
5.03
1
01/18/23 18:50
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 70 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97330
Matrix: Aqueous
Sample ID: MW-10
Sampled:
1/10/2023 13:00
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2,6-Dinitrotoluene
<0.813
Ng/L
0.813
5.03
1
01/18/23 18:50
JMV
V29002
Di-n-Octyl Phthalate
<1.66
Ng/L
1.66
5.03
1
01/18/23 18:50
JMV
V29002
Fluoranthene
<0.251
Ng/L
0.251
2.01
1
01/18/23 18:50
JMV
V29002
Fluorene
<0.811
Ng/L
0.811
2.01
1
01/18/23 18:50
JMV
V29002
Hexachlorobenzene
<0.984
Ng/L
0.984
5.03
1
01/18/23 18:50
JMV
V29002
Hexachlorobutadiene
<2.75
Ng/L
2.75
5.03
1
01/18/23 18:50
JMV
V29002
Hexachlorocyclopentadiene
<2.06
Ng/L
2.06
5.03
1
01/18/23 18:50
JMV
V29002
Hexachloroethane
<1.77
Ng/L
1.77
5.03
1
01/18/23 18:50
JMV
V29002
Indeno(1,2,3-cd)pyrene
<0.479
Ng/L
0.479
2.01
1
01/18/23 18:50
JMV
V29002
Isophorone
<0.446
Ng/L
0.446
5.03
1
01/18/23 18:50
JMV
V29002
1-Methylnaphthalene
<1.15
Ng/L
1.15
2.01
1
01/18/23 18:50
JMV
V29002
2-Methylnaphthalene
<0.669
Ng/L
0.669
2.01
1
01/18/23 18:50
JMV
V29002
Naphthalene
<0.731
Ng/L
0.731
2.01
1
01/18/23 18:50
JMV
V29002
Nitrobenzene
<0.910
Ng/L
0.910
5.03
1
01/18/23 18:50
JMV
V29002
2-Nitrophenol
<0.495
Ng/L
0.495
5.03
1
01/18/23 18:50
JMV
V29002
4-Nitrophenol
<1.24
Ng/L
1.24
10.1
1
01/18/23 18:50
JMV
V29002
N-Nitrosodiphenylamine
<1.11
Ng/L
1.11
5.03
1
01/18/23 18:50
JMV
V29002
N-Nitroso-di-n-propylamine
<0.644
Ng/L
0.644
5.03
1
01/18/23 18:50
JMV
V29002
Pentachlorophenol
<1.44
Ng/L
1.44
5.03
1
01/18/23 18:50
JMV
V29002
Phenanthrene
<0.430
Ng/L
0.430
2.01
1
01/18/23 18:50
JMV
V29002
Phenol
<0.654
Ng/L
0.654
5.03
1
01/18/23 18:50
JMV
V29002
Pyrene
<0.436
Ng/L
0.436
2.01
1
01/18/23 18:50
JMV
V29002
1,2,4-Trichlorobenzene
<2.22
Ng/L
2.22
5.03
1
01/18/23 18:50
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 71 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
Report Date : 01/19/2023
Received : 01/11/2023
Report Number : 23-011-0018
Lab No : 97330
Sample ID: MW-10
REPORT OFANAL YSIS
Matrix: Aqueous
Sampled: 1/10/2023 13:00
Analytical Method: 625.1
Prep Batch(es):
V28943 01/17/23 08:54
Prep Method: 625.1 (Prep)
Test
Results Units
MDL MQL DF
Date / Time By Analytical
Analyzed
Batch
2,4,6-Trichlorophenol
<1.33 N9/L
1.33 5.03 1
01/18/23 18:50 JMV
V29002
Surrogate: Phenol-d5
25.6
Limits: 10-63%
1 01/18/23 18:50 JMV
625.1
Surrogate:2-Fluorobiphenyl
67.2
Limits:49-118%
1 01/18/23 18:50 JMV
V29002
Surrogate:2-Fluorophenol
34.2
Limits:22-84%
1 01/18/23 18:50 JMV
V29002
Surrogate: Nitrobenzene-d5
59.8
Limits: 43-123%
1 01/18/23 18:50 JMV
V29002
Surrogate:4-Terphenyl-d14
77.5
Limits:49-151%
1 01/18/23 18:50 JMV
V29002
Surrogate: 2,4,6-Tribromophenol
65.7
Limits:31-144%
1 01/18/23 18:50 JMV
V29002
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 72 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97331
Matrix: Aqueous
Sample ID: MW-11
Sampled:
1/10/2023 11:10
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
2.613
N9/L
1.80
10.0
1
01/18/23 06:19
MSA
V28980
Benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:19
MSA
V28980
Bromobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 06:19
MSA
V28980
Bromochloromethane
<0.420
N9/L
0.420
1.00
1
01/18/23 06:19
MSA
V28980
Bromodichloromethane
<0.160
N9/L
0.160
0.500
1
01/18/23 06:19
MSA
V28980
Bromoform
<1.50
N9/L
1.50
5.00
1
01/18/23 06:19
MSA
V28980
Bromomethane
<0.280
N9/L
0.280
1.00
1
01/18/23 06:19
MSA
V28980
n-Butylbenzene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:19
MSA
V28980
sec -Butyl benzene
<0.200
N9/L
0.200
0.500
1
01/18/23 06:19
MSA
V28980
tert-Butyl benzene
<0.920
N9/L
0.920
2.00
1
01/18/23 06:19
MSA
V28980
Carbon Tetrachloride
<0.180
N9/L
0.180
0.500
1
01/18/23 06:19
MSA
V28980
Chlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 06:19
MSA
V28980
Chlorodibromomethane
<0.190
N9/L
0.190
0.500
1
01/18/23 06:19
MSA
V28980
Chloroethane
<0.430
N9/L
0.430
1.00
1
01/18/23 06:19
MSA
V28980
Chloroform
<0.220
N9/L
0.220
0.500
1
01/18/23 06:19
MSA
V28980
Chloromethane
<0.220
N9/L
0.220
0.500
1
01/18/23 06:19
MSA
V28980
2-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 06:19
MSA
V28980
4-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 06:19
MSA
V28980
Di -Isopropyl Ether (DIPE)
<0.500
N9/L
0.500
0.500
1
01/18/23 06:19
MSA
V28980
1,2-Dibromo-3-Chloropropane
<1.10
N9/L
1.10
2.00
1
01/18/23 06:19
MSA
V28980
1,2-Dibromoethane
<0.200
N9/L
0.200
0.500
1
01/18/23 06:19
MSA
V28980
Dibromomethane
<0.230
N9/L
0.230
0.500
1
01/18/23 06:19
MSA
V28980
1,2-Dichlorobenzene
<0.220
N9/L
0.220
0.500
1
01/18/23 06:19
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 73 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97331
Matrix: Aqueous
Sample ID: MW-11
Sampled:
1/10/2023 11:10
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 06:19
MSA
V28980
1,4-Dichlorobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 06:19
MSA
V28980
Dichlorodifluoromethane
<1.20
N9/L
1.20
5.00
1
01/18/23 06:19
MSA
V28980
1,1-Dichloroethane
<0.240
N9/L
0.240
0.500
1
01/18/23 06:19
MSA
V28980
1,2-Dichloroethane
<0.150
N9/L
0.150
0.500
1
01/18/23 06:19
MSA
V28980
1,1-Dichloroethene
<0.150
N9/L
0.150
0.500
1
01/18/23 06:19
MSA
V28980
cis- 1,2-Dichloroethene
<0.200
N9/L
0.200
0.500
1
01/18/23 06:19
MSA
V28980
trans-1,2-Dichloroethene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:19
MSA
V28980
1,2-Dichloropropane
<0.190
N9/L
0.190
0.500
1
01/18/23 06:19
MSA
V28980
1,3-Dichloropropane
<0.130
N9/L
0.130
0.500
1
01/18/23 06:19
MSA
V28980
2,2-Dichloropropane
<0.210
N9/L
0.210
2.00
1
01/18/23 06:19
MSA
V28980
1,1-Dichloropropene
<0.200
N9/L
0.200
0.500
1
01/18/23 06:19
MSA
V28980
cis- 1,3-Dichloropropene
<0.210
N9/L
0.210
0.500
1
01/18/23 06:19
MSA
V28980
trans-1,3-Dichloropropene
<0.150
N9/L
0.150
0.500
1
01/18/23 06:19
MSA
V28980
Ethanol
<42.0
N9/L
42.0
200
1
01/18/23 06:19
MSA
V28980
Ethylbenzene
<0.170
N9/L
0.170
0.500
1
01/18/23 06:19
MSA
V28980
Hexachlorobutadiene
<0.350
N9/L
0.350
3.00
1
01/18/23 06:19
MSA
V28980
2-Hexanone
<0.380
N9/L
0.380
1.00
1
01/18/23 06:19
MSA
V28980
Isopropyl benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:19
MSA
V28980
4-Isopropyl toluene
<0.089
N9/L
0.089
0.500
1
01/18/23 06:19
MSA
V28980
Methyl Ethyl Ketone (MEK)
<0.710
N9/L
0.710
5.00
1
01/18/23 06:19
MSA
V28980
Methyl tert-butyl ether (MTBE)
<0.140
N9/L
0.140
1.00
1
01/18/23 06:19
MSA
V28980
4-Methyl-2-Pentanone
<0.078
N9/L
0.078
1.00
1
01/18/23 06:19
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 74 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97331
Matrix: Aqueous
Sample ID: MW-11
Sampled:
1/10/2023 11:10
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200
PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
<0.330
N9/L
0.330
2.00
1
01/18/23 06:19
MSA
V28980
Naphthalene
<0.470
N9/L
0.470
1.00
1
01/18/23 06:19
MSA
V28980
n-Propylbenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 06:19
MSA
V28980
Styrene
<0.220
N9/L
0.220
0.500
1
01/18/23 06:19
MSA
V28980
1,1,1,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 06:19
MSA
V28980
1,1,2,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 06:19
MSA
V28980
Tetrachloroethene
<0.220
N9/L
0.220
0.500
1
01/18/23 06:19
MSA
V28980
Toluene
<0.220
N9/L
0.220
0.500
1
01/18/23 06:19
MSA
V28980
1,2,3-Trichlorobenzene
<0.380
N9/L
0.380
0.500
1
01/18/23 06:19
MSA
V28980
1,2,4-Trichlorobenzene
<0.310
N9/L
0.310
0.500
1
01/18/23 06:19
MSA
V28980
1,1,1-Trichloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 06:19
MSA
V28980
1,1,2-Trichloroethane
<0.096
N9/L
0.096
0.500
1
01/18/23 06:19
MSA
V28980
Trichloroethene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:19
MSA
V28980
Trichlorofluoromethane
<0.180
N9/L
0.180
0.500
1
01/18/23 06:19
MSA
V28980
1,2,3-Trichloropropane
<0.270
N9/L
0.270
0.500
1
01/18/23 06:19
MSA
V28980
1,2,4-Trimethyl benzene
<0.190
N9/L
0.190
0.500
1
01/18/23 06:19
MSA
V28980
1,3,5-Trimethyl benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:19
MSA
V28980
Vinyl Acetate
<1.00
N9/L
1.00
5.00
1
01/18/23 06:19
MSA
V28980
Vinyl Chloride
<0.170
N9/L
0.170
0.500
1
01/18/23 06:19
MSA
V28980
o-Xylene
<0.210
N9/L
0.210
0.500
1
01/18/23 06:19
MSA
V28980
m,p-Xylene
<0.420
N9/L
0.420
1.00
1
01/18/23 06:19
MSA
V28980
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 75 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97331 Matrix: Aqueous
Sample ID: MW-11 Sampled: 1/10/2023 11:10
Analytical Method: 6200E Prep Batch(es): V28979 01/17/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
01/18/23 06:19
V28980
Surrogate: 4-Bromofluorobenzene
114
Limits:
70-130%
1 01/18/23 06:19
MSA
V28980
Surrogate: Dibromofluoromethane
89.2
Limits:
70-130%
1 01/18/23 06:19
MSA
V28980
Surrogate: 1,2-Dichloroethane - d4
91.4
Limits:
70-130%
1 01/18/23 06:19
MSA
V28980
Surrogate: Toluene-d8
101
Limits:
70-130%
1 01/18/23 06:19
MSA
V28980
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23
08:54
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.302
Ng/L
0.302
2.00
1
01/18/23 18:05
JMV
V29002
Acenaphthylene
<0.297
Ng/L
0.297
2.00
1
01/18/23 18:05
JMV
V29002
Anthracene
<0.836
Ng/L
0.836
2.00
1
01/18/23 18:05
JMV
V29002
Benzidine
<1.32
Ng/L
1.32
10.0
1
01/18/23 18:05
JMV
V29002
Benzo(a)anthracene
<0.637
Ng/L
0.637
2.00
1
01/18/23 18:05
JMV
V29002
Benzo(a)pyrene
<1.02
Ng/L
1.02
2.00
1
01/18/23 18:05
JMV
V29002
Benzo(b)fluoranthene
<2.49
Ng/L
2.49
5.00
1
01/18/23 18:05
JMV
V29002
Benzo(g,h,i)perylene
<1.01
Ng/L
1.01
5.00
1
01/18/23 18:05
JMV
V29002
Benzo(k)fluoranthene
<1.99
Ng/L
1.99
5.00
1
01/18/23 18:05
JMV
V29002
Benzoic Acid
<1.10
Ng/L
1.10
10.0
1
01/18/23 18:05
JMV
V29002
Benzyl alcohol
<0.684
Ng/L
0.684
5.00
1
01/18/23 18:05
JMV
V29002
Bis(2-Chloroethoxy)methane
<0.468
Ng/L
0.468
5.00
1
01/18/23 18:05
JMV
V29002
Bis(2-Chloroethyl)ether
<1.04
Ng/L
1.04
5.00
1
01/18/23 18:05
JMV
V29002
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation
Limit
Page 76 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97331
Matrix: Aqueous
Sample ID: MW-11
Sampled:
1/10/2023 11:10
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Bis(2-Chloroisopropyl)ether
<1.08
N9/L
1.08
5.00
1
01/18/23 18:05
JMV
V29002
Bis(2-ethylhexyl)phthalate
<24.0
N9/L
24.0
50.0
1
01/18/23 18:05
JMV
V29002
4-13romophenyl phenyl ether
<1.11
N9/L
1.11
5.00
1
01/18/23 18:05
JMV
V29002
Butyl benzyl phthalate
<1.83
N9/L
1.83
5.00
1
01/18/23 18:05
JMV
V29002
4-Chloro-3-methylphenol
<1.18
N9/L
1.18
5.00
1
01/18/23 18:05
JMV
V29002
2-Chloronaphthalene
<7.38
N9/L
7.38
20.0
1
01/18/23 18:05
JMV
V29002
2-Chlorophenol
<0.938
N9/L
0.938
10.0
1
01/18/23 18:05
JMV
V29002
4-Chlorophenyl phenyl ether
<1.71
N9/L
1.71
5.00
1
01/18/23 18:05
JMV
V29002
Chrysene
<0.405
N9/L
0.405
2.00
1
01/18/23 18:05
JMV
V29002
Dibenz(a,h)anthracene
<0.434
N9/L
0.434
2.00
1
01/18/23 18:05
JMV
V29002
Dibenzofuran
<0.856
N9/L
0.856
5.00
1
01/18/23 18:05
JMV
V29002
1,2-Dichlorobenzene
<2.00
N9/L
2.00
5.00
1
01/18/23 18:05
JMV
V29002
1,3-Dichlorobenzene
<2.00
N9/L
2.00
5.00
1
01/18/23 18:05
JMV
V29002
1,4-Dichlorobenzene
<2.05
N9/L
2.05
5.00
1
01/18/23 18:05
JMV
V29002
3,3'-Dichlorobenzidine
<1.89
N9/L
1.89
5.00
1
01/18/23 18:05
JMV
V29002
2,4-Dichlorophenol
<1.46
N9/L
1.46
10.0
1
01/18/23 18:05
JMV
V29002
Diethyl phthalate
<0.745
N9/L
0.745
5.00
1
01/18/23 18:05
JMV
V29002
Dimethyl phthalate
<0.939
N9/L
0.939
5.00
1
01/18/23 18:05
JMV
V29002
2,4-Dimethylphenol
<1.57
N9/L
1.57
20.0
1
01/18/23 18:05
JMV
V29002
Di-n-butyl phthalate
<2.06
N9/L
2.06
5.00
1
01/18/23 18:05
JMV
V29002
4,6- Din itro-2-methylphenol
<2.07
N9/L
2.07
10.0
1
01/18/23 18:05
JMV
V29002
2,4-Dinitrophenol
<1.92
N9/L
1.92
10.0
1
01/18/23 18:05
JMV
V29002
2,4-Dinitrotoluene
<1.11
N9/L
1.11
5.00
1
01/18/23 18:05
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 77 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97331
Matrix: Aqueous
Sample ID: MW-11
Sampled:
1/10/2023 11:10
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2,6-Dinitrotoluene
<0.809
Ng/L
0.809
5.00
1
01/18/23 18:05
JMV
V29002
Di-n-Octyl Phthalate
<1.65
Ng/L
1.65
5.00
1
01/18/23 18:05
JMV
V29002
Fluoranthene
<0.250
Ng/L
0.250
2.00
1
01/18/23 18:05
JMV
V29002
Fluorene
<0.807
Ng/L
0.807
2.00
1
01/18/23 18:05
JMV
V29002
Hexachlorobenzene
<0.979
Ng/L
0.979
5.00
1
01/18/23 18:05
JMV
V29002
Hexachlorobutadiene
<2.73
Ng/L
2.73
5.00
1
01/18/23 18:05
JMV
V29002
Hexachlorocyclopentadiene
<2.05
Ng/L
2.05
5.00
1
01/18/23 18:05
JMV
V29002
Hexachloroethane
<1.76
Ng/L
1.76
5.00
1
01/18/23 18:05
JMV
V29002
Indeno(1,2,3-cd)pyrene
<0.477
Ng/L
0.477
2.00
1
01/18/23 18:05
JMV
V29002
Isophorone
<0.444
Ng/L
0.444
5.00
1
01/18/23 18:05
JMV
V29002
1-Methylnaphthalene
<1.14
Ng/L
1.14
2.00
1
01/18/23 18:05
JMV
V29002
2-Methylnaphthalene
<0.666
Ng/L
0.666
2.00
1
01/18/23 18:05
JMV
V29002
Naphthalene
<0.728
Ng/L
0.728
2.00
1
01/18/23 18:05
JMV
V29002
Nitrobenzene
<0.905
Ng/L
0.905
5.00
1
01/18/23 18:05
JMV
V29002
2-Nitrophenol
<0.493
Ng/L
0.493
5.00
1
01/18/23 18:05
JMV
V29002
4-Nitrophenol
<1.23
Ng/L
1.23
10.0
1
01/18/23 18:05
JMV
V29002
N-Nitrosodiphenylamine
<1.10
Ng/L
1.10
5.00
1
01/18/23 18:05
JMV
V29002
N-Nitroso-di-n-propylamine
<0.641
Ng/L
0.641
5.00
1
01/18/23 18:05
JMV
V29002
Pentachlorophenol
<1.43
Ng/L
1.43
5.00
1
01/18/23 18:05
JMV
V29002
Phenanthrene
<0.428
Ng/L
0.428
2.00
1
01/18/23 18:05
JMV
V29002
Phenol
<0.651
Ng/L
0.651
5.00
1
01/18/23 18:05
JMV
V29002
Pyrene
<0.434
Ng/L
0.434
2.00
1
01/18/23 18:05
JMV
V29002
1,2,4-Trichlorobenzene
<2.21
Ng/L
2.21
5.00
1
01/18/23 18:05
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 78 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
Report Date : 01/19/2023
Received : 01/11/2023
Report Number : 23-011-0018
Lab No : 97331
Sample ID: MW-11
REPORT OFANAL YSIS
Matrix: Aqueous
Sampled: 1/10/2023 11:10
Analytical Method: 625.1
Prep Batch(es):
V28943 01/17/23 08:54
Prep Method: 625.1 (Prep)
Test
Results Units
MDL MQL DF
Date / Time By Analytical
Analyzed
Batch
2,4,6-Trichlorophenol
<1.32 N9/L
1.32 5.00 1
01/18/23 18:05 JMV
V29002
Surrogate: Phenol-d5
25.5
Limits: 10-63%
1 01/18/23 18:05 JMV
625.1
Surrogate:2-Fluorobiphenyl
70.8
Limits:49-118%
1 01/18/23 18:05 JMV
V29002
Surrogate:2-Fluorophenol
34.4
Limits:22-84%
1 01/18/23 18:05 JMV
V29002
Surrogate: Nitrobenzene-d5
55.8
Limits: 43-123%
1 01/18/23 18:05 JMV
V29002
Surrogate:4-Terphenyl-d14
79.0
Limits:49-151%
1 01/18/23 18:05 JMV
V29002
Surrogate: 2,4,6-Tribromophenol
74.8
Limits:31-144%
1 01/18/23 18:05 JMV
V29002
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 79 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97332
Matrix: Aqueous
Sample ID: MW-12
Sampled:
1/10/2023 14:50
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
N9/L
1.80
10.0
1
01/18/23 06:44
MSA
V28980
Benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:44
MSA
V28980
Bromobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 06:44
MSA
V28980
Bromochloromethane
<0.420
N9/L
0.420
1.00
1
01/18/23 06:44
MSA
V28980
Bromodichloromethane
<0.160
N9/L
0.160
0.500
1
01/18/23 06:44
MSA
V28980
Bromoform
<1.50
N9/L
1.50
5.00
1
01/18/23 06:44
MSA
V28980
Bromomethane
<0.280
N9/L
0.280
1.00
1
01/18/23 06:44
MSA
V28980
n-Butylbenzene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:44
MSA
V28980
sec -Butyl benzene
<0.200
N9/L
0.200
0.500
1
01/18/23 06:44
MSA
V28980
tert-Butyl benzene
<0.920
N9/L
0.920
2.00
1
01/18/23 06:44
MSA
V28980
Carbon Tetrachloride
<0.180
N9/L
0.180
0.500
1
01/18/23 06:44
MSA
V28980
Chlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 06:44
MSA
V28980
Chlorodibromomethane
<0.190
N9/L
0.190
0.500
1
01/18/23 06:44
MSA
V28980
Chloroethane
<0.430
N9/L
0.430
1.00
1
01/18/23 06:44
MSA
V28980
Chloroform
1.40
N9/L
0.220
0.500
1
01/18/23 06:44
MSA
V28980
Chloromethane
<0.220
N9/L
0.220
0.500
1
01/18/23 06:44
MSA
V28980
2-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 06:44
MSA
V28980
4-Chlorotoluene
<0.200
N9/L
0.200
0.500
1
01/18/23 06:44
MSA
V28980
Di -Isopropyl Ether (DIPE)
<0.500
N9/L
0.500
0.500
1
01/18/23 06:44
MSA
V28980
1,2-Dibromo-3-Chloropropane
<1.10
N9/L
1.10
2.00
1
01/18/23 06:44
MSA
V28980
1,2-Dibromoethane
<0.200
N9/L
0.200
0.500
1
01/18/23 06:44
MSA
V28980
Dibromomethane
<0.230
N9/L
0.230
0.500
1
01/18/23 06:44
MSA
V28980
1,2-Dichlorobenzene
<0.220
N9/L
0.220
0.500
1
01/18/23 06:44
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 80 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97332
Matrix: Aqueous
Sample ID: MW-12
Sampled:
1/10/2023 14:50
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200 PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dichlorobenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 06:44
MSA
V28980
1,4-Dichlorobenzene
<0.210
N9/L
0.210
0.500
1
01/18/23 06:44
MSA
V28980
Dichlorodifluoromethane
<1.20
N9/L
1.20
5.00
1
01/18/23 06:44
MSA
V28980
1,1-Dichloroethane
<0.240
N9/L
0.240
0.500
1
01/18/23 06:44
MSA
V28980
1,2-Dichloroethane
<0.150
N9/L
0.150
0.500
1
01/18/23 06:44
MSA
V28980
1,1-Dichloroethene
<0.150
N9/L
0.150
0.500
1
01/18/23 06:44
MSA
V28980
cis- 1,2-Dichloroethene
0.870
N9/L
0.200
0.500
1
01/18/23 06:44
MSA
V28980
trans-1,2-Dichloroethene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:44
MSA
V28980
1,2-Dichloropropane
<0.190
N9/L
0.190
0.500
1
01/18/23 06:44
MSA
V28980
1,3-Dichloropropane
<0.130
N9/L
0.130
0.500
1
01/18/23 06:44
MSA
V28980
2,2-Dichloropropane
<0.210
N9/L
0.210
2.00
1
01/18/23 06:44
MSA
V28980
1,1-Dichloropropene
<0.200
N9/L
0.200
0.500
1
01/18/23 06:44
MSA
V28980
cis- 1,3-Dichloropropene
<0.210
N9/L
0.210
0.500
1
01/18/23 06:44
MSA
V28980
trans-1,3-Dichloropropene
<0.150
N9/L
0.150
0.500
1
01/18/23 06:44
MSA
V28980
Ethanol
<42.0
N9/L
42.0
200
1
01/18/23 06:44
MSA
V28980
Ethylbenzene
<0.170
N9/L
0.170
0.500
1
01/18/23 06:44
MSA
V28980
Hexachlorobutadiene
<0.350
N9/L
0.350
3.00
1
01/18/23 06:44
MSA
V28980
2-Hexanone
<0.380
N9/L
0.380
1.00
1
01/18/23 06:44
MSA
V28980
Isopropyl benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:44
MSA
V28980
4-Isopropyl toluene
<0.089
N9/L
0.089
0.500
1
01/18/23 06:44
MSA
V28980
Methyl Ethyl Ketone (MEK)
<0.710
N9/L
0.710
5.00
1
01/18/23 06:44
MSA
V28980
Methyl tert-butyl ether (MTBE)
<0.140
N9/L
0.140
1.00
1
01/18/23 06:44
MSA
V28980
4-Methyl-2-Pentanone
<0.078
N9/L
0.078
1.00
1
01/18/23 06:44
MSA
V28980
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 81 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97332
Matrix: Aqueous
Sample ID: MW-12
Sampled:
1/10/2023 14:50
Analytical Method: 6200E
Prep Batch(es):
V28979
01/17/23 14:00
Prep Method: 6200
PT
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Methylene Chloride
<0.330
N9/L
0.330
2.00
1
01/18/23 06:44
MSA
V28980
Naphthalene
<0.470
N9/L
0.470
1.00
1
01/18/23 06:44
MSA
V28980
n-Propylbenzene
<0.190
N9/L
0.190
0.500
1
01/18/23 06:44
MSA
V28980
Styrene
<0.220
N9/L
0.220
0.500
1
01/18/23 06:44
MSA
V28980
1,1,1,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 06:44
MSA
V28980
1,1,2,2-Tetrachloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 06:44
MSA
V28980
Tetrachloroethene
0.765
N9/L
0.220
0.500
1
01/18/23 06:44
MSA
V28980
Toluene
<0.220
N9/L
0.220
0.500
1
01/18/23 06:44
MSA
V28980
1,2,3-Trichlorobenzene
<0.380
N9/L
0.380
0.500
1
01/18/23 06:44
MSA
V28980
1,2,4-Trichlorobenzene
<0.310
N9/L
0.310
0.500
1
01/18/23 06:44
MSA
V28980
1,1,1-Trichloroethane
<0.160
N9/L
0.160
0.500
1
01/18/23 06:44
MSA
V28980
1,1,2-Trichloroethane
<0.096
N9/L
0.096
0.500
1
01/18/23 06:44
MSA
V28980
Trichloroethene
1.13
N9/L
0.180
0.500
1
01/18/23 06:44
MSA
V28980
Trichlorofluoromethane
<0.180
N9/L
0.180
0.500
1
01/18/23 06:44
MSA
V28980
1,2,3-Trichloropropane
<0.270
N9/L
0.270
0.500
1
01/18/23 06:44
MSA
V28980
1,2,4-Trimethyl benzene
<0.190
N9/L
0.190
0.500
1
01/18/23 06:44
MSA
V28980
1,3,5-Trimethyl benzene
<0.180
N9/L
0.180
0.500
1
01/18/23 06:44
MSA
V28980
Vinyl Acetate
<1.00
N9/L
1.00
5.00
1
01/18/23 06:44
MSA
V28980
Vinyl Chloride
<0.170
N9/L
0.170
0.500
1
01/18/23 06:44
MSA
V28980
o-Xylene
<0.210
N9/L
0.210
0.500
1
01/18/23 06:44
MSA
V28980
m,p-Xylene
<0.420
N9/L
0.420
1.00
1
01/18/23 06:44
MSA
V28980
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 82 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97332 Matrix: Aqueous
Sample ID: MW-12 Sampled: 1/10/2023 14:50
Analytical Method: 6200E Prep Batch(es): V28979 01/17/23 14:00
Prep Method: 6200 PT
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
01/18/23 06:44
V28980
Surrogate: 4-Bromofluorobenzene
101
Limits:
70-130%
1 01/18/23 06:44 MSA
V28980
Surrogate: Dibromofluoromethane
93.6
Limits:
70-130%
1 01/18/23 06:44 MSA
V28980
Surrogate: 1,2-Dichloroethane - d4
94.6
Limits:
70-130%
1 01/18/23 06:44 MSA
V28980
Surrogate: Toluene-d8
96.4
Limits:
70-130%
1 01/18/23 06:44 MSA
V28980
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23
08:54
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.309
Ng/L
0.309
2.05
1
01/18/23 21:50
JMV
V29002
Acenaphthylene
<0.304
Ng/L
0.304
2.05
1
01/18/23 21:50
JMV
V29002
Anthracene
<0.856
Ng/L
0.856
2.05
1
01/18/23 21:50
JMV
V29002
Benzidine
<1.36
Ng/L
1.36
10.3
1
01/18/23 21:50
JMV
V29002
Benzo(a)anthracene
<0.652
Ng/L
0.652
2.05
1
01/18/23 21:50
JMV
V29002
Benzo(a)pyrene
<1.05
Ng/L
1.05
2.05
1
01/18/23 21:50
JMV
V29002
Benzo(b)fluoranthene
<2.55
Ng/L
2.55
5.13
1
01/18/23 21:50
JMV
V29002
Benzo(g,h,i)perylene
<1.04
Ng/L
1.04
5.13
1
01/18/23 21:50
JMV
V29002
Benzo(k)fluoranthene
<2.04
Ng/L
2.04
5.13
1
01/18/23 21:50
JMV
V29002
Benzoic Acid
<1.13
Ng/L
1.13
10.3
1
01/18/23 21:50
JMV
V29002
Benzyl alcohol
<0.701
Ng/L
0.701
5.13
1
01/18/23 21:50
JMV
V29002
Bis(2-Chloroethoxy)methane
<0.480
Ng/L
0.480
5.13
1
01/18/23 21:50
JMV
V29002
Bis(2-Chloroethyl)ether
<1.07
Ng/L
1.07
5.13
1
01/18/23 21:50
JMV
V29002
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation
Limit
Page 83 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97332
Matrix: Aqueous
Sample ID: MW-12
Sampled:
1/10/2023 14:50
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Bis(2-Chloroisopropyl)ether
<1.11
N9/L
1.11
5.13
1
01/18/23 21:50
JMV
V29002
Bis(2-ethylhexyl)phthalate
<24.7
N9/L
24.7
51.3
1
01/18/23 21:50
JMV
V29002
4-13romophenyl phenyl ether
<1.14
N9/L
1.14
5.13
1
01/18/23 21:50
JMV
V29002
Butyl benzyl phthalate
<1.88
N9/L
1.88
5.13
1
01/18/23 21:50
JMV
V29002
4-Chloro-3-methylphenol
<1.21
N9/L
1.21
5.13
1
01/18/23 21:50
JMV
V29002
2-Chloronaphthalene
<7.56
N9/L
7.56
20.5
1
01/18/23 21:50
JMV
V29002
2-Chlorophenol
<0.966
N9/L
0.966
10.3
1
01/18/23 21:50
JMV
V29002
4-Chlorophenyl phenyl ether
<1.75
N9/L
1.75
5.13
1
01/18/23 21:50
JMV
V29002
Chrysene
<0.415
N9/L
0.415
2.05
1
01/18/23 21:50
JMV
V29002
Dibenz(a,h)anthracene
<0.444
N9/L
0.444
2.05
1
01/18/23 21:50
JMV
V29002
Dibenzofuran
<0.878
N9/L
0.878
5.13
1
01/18/23 21:50
JMV
V29002
1,2-Dichlorobenzene
<2.05
N9/L
2.05
5.13
1
01/18/23 21:50
JMV
V29002
1,3-Dichlorobenzene
<2.05
N9/L
2.05
5.13
1
01/18/23 21:50
JMV
V29002
1,4-Dichlorobenzene
<2.10
N9/L
2.10
5.13
1
01/18/23 21:50
JMV
V29002
3,3'-Dichlorobenzidine
<1.94
N9/L
1.94
5.13
1
01/18/23 21:50
JMV
V29002
2,4-Dichlorophenol
<1.50
N9/L
1.50
10.3
1
01/18/23 21:50
JMV
V29002
Diethyl phthalate
<0.764
N9/L
0.764
5.13
1
01/18/23 21:50
JMV
V29002
Dimethyl phthalate
<0.963
N9/L
0.963
5.13
1
01/18/23 21:50
JMV
V29002
2,4-Dimethylphenol
<1.61
N9/L
1.61
20.5
1
01/18/23 21:50
JMV
V29002
Di-n-butyl phthalate
<2.11
N9/L
2.11
5.13
1
01/18/23 21:50
JMV
V29002
4,6- Din itro-2-methylphenol
<2.13
N9/L
2.13
10.3
1
01/18/23 21:50
JMV
V29002
2,4-Dinitrophenol
<1.98
N9/L
1.98
10.3
1
01/18/23 21:50
JMV
V29002
2,4-Dinitrotoluene
<1.14
N9/L
1.14
5.13
1
01/18/23 21:50
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 84 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Project
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Information
Suite 2-A
Charlotte , NC 28273
Report Number : 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Jefferson Pilot Comm
REPORT OFANAL YSIS
Report Date : 01/19/2023
Received : 01/11/2023
Lab No : 97332
Matrix: Aqueous
Sample ID: MW-12
Sampled:
1/10/2023 14:50
Analytical Method: 625.1
Prep Batch(es):
V28943
01/17/23 08:54
Prep Method: 625.1
(Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2,6-Dinitrotoluene
<0.830
Ng/L
0.830
5.13
1
01/18/23 21:50
JMV
V29002
Di-n-Octyl Phthalate
<1.69
Ng/L
1.69
5.13
1
01/18/23 21:50
JMV
V29002
Fluoranthene
<0.256
Ng/L
0.256
2.05
1
01/18/23 21:50
JMV
V29002
Fluorene
<0.827
Ng/L
0.827
2.05
1
01/18/23 21:50
JMV
V29002
Hexachlorobenzene
<1.00
Ng/L
1.00
5.13
1
01/18/23 21:50
JMV
V29002
Hexachlorobutadiene
<2.80
Ng/L
2.80
5.13
1
01/18/23 21:50
JMV
V29002
Hexachlorocyclopentadiene
<2.10
Ng/L
2.10
5.13
1
01/18/23 21:50
JMV
V29002
Hexachloroethane
<1.81
Ng/L
1.81
5.13
1
01/18/23 21:50
JMV
V29002
Indeno(1,2,3-cd)pyrene
<0.488
Ng/L
0.488
2.05
1
01/18/23 21:50
JMV
V29002
Isophorone
<0.455
Ng/L
0.455
5.13
1
01/18/23 21:50
JMV
V29002
1-Methylnaphthalene
<1.17
Ng/L
1.17
2.05
1
01/18/23 21:50
JMV
V29002
2-Methylnaphthalene
<0.682
Ng/L
0.682
2.05
1
01/18/23 21:50
JMV
V29002
Naphthalene
<0.746
Ng/L
0.746
2.05
1
01/18/23 21:50
JMV
V29002
Nitrobenzene
<0.928
Ng/L
0.928
5.13
1
01/18/23 21:50
JMV
V29002
2-Nitrophenol
<0.505
Ng/L
0.505
5.13
1
01/18/23 21:50
JMV
V29002
4-Nitrophenol
<1.27
Ng/L
1.27
10.3
1
01/18/23 21:50
JMV
V29002
N-Nitrosodiphenylamine
<1.13
Ng/L
1.13
5.13
1
01/18/23 21:50
JMV
V29002
N-Nitroso-di-n-propylamine
<0.657
Ng/L
0.657
5.13
1
01/18/23 21:50
JMV
V29002
Pentachlorophenol
<1.47
Ng/L
1.47
5.13
1
01/18/23 21:50
JMV
V29002
Phenanthrene
<0.438
Ng/L
0.438
2.05
1
01/18/23 21:50
JMV
V29002
Phenol
<0.667
Ng/L
0.667
5.13
1
01/18/23 21:50
JMV
V29002
Pyrene
<0.444
Ng/L
0.444
2.05
1
01/18/23 21:50
JMV
V29002
1,2,4-Trichlorobenzene
<2.27
Ng/L
2.27
5.13
1
01/18/23 21:50
JMV
V29002
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 85 of 118
Waypoint.0
ANALYTICAL
01176
S&ME, Inc - Charlotte
Lucas-Ba rroso-G i achetti
2016 Ayrsley Town Blvd.2Suite 2-A
Suite 2-A
Charlotte , NC 28273
449 Springbrook Rd, Charlotte, NC 28217
Main 704.52 9.63 64
www.waypointana lyti ca Isom
Project Jefferson Pilot Comm
Information :
Report Date : 01/19/2023
Received : 01/11/2023
Report Number : 23-011-0018
Lab No : 97332
Sample ID: MW-12
REPORT OFANAL YSIS
Matrix: Aqueous
Sampled: 1/10/2023 14:50
Analytical Method: 625.1
Prep Batch(es):
V28943 01/17/23 08:54
Prep Method: 625.1 (Prep)
Test
Results Units
MDL MQL DF
Date / Time By Analytical
Analyzed
Batch
2,4,6-Trichlorophenol
<1.35 N9/L
1.35 5.13 1
01/18/23 21:50 JMV
V29002
Surrogate: Phenol-d5
31.6
Limits: 10-63%
1 01/18/23 21:50 JMV
625.1
Surrogate: 2-Fluorobiphenyl
70.0
Limits: 49-118%
1 01/18/23 21:50 JMV
V29002
Surrogate: 2-Fluorophenol
45.1
Limits: 22-84%
1 01/18/23 21:50 JMV
V29002
Surrogate: Nitrobenzene-d5
63.0
Limits: 43-123%
1 01/18/23 21:50 JMV
V29002
Surrogate: 4-Terphenyl-d14
75.0
Limits: 49-151%
1 01/18/23 21:50 JMV
V29002
Surrogate: 2,4,6-Tribromophenol
71.1
Limits: 31-144%
1 01/18/23 21:50 JMV
V29002
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 86 of 118
Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
S&ME, Inc - Charlotte
Jefferson Pilot Comm
23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypoi ntana lytica l.com
Quality Control Data
QC Prep: V28947 QC Analytical Batch(es): V28948
QC Prep Batch Method: 6200 PT Analysis Method: 6200B
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V28947 Matrix: AQU
Associated Lab Samples: 97322, 97323
Blank MDL MQL Analyzed a/o % Rec
Parameter Units Result Recovery Limits
Acetone
pg/L
<1.80
1.80
10.0
01/17/23 02:39
Bromobenzene
pg/L
<0.210
0.210
0.500
01/17/23 02:39
Bromochloromethane
pg/L
<0.420
0.420
1.00
01/17/23 02:39
Bromodichloromethane
pg/L
<0.160
0.160
0.500
01/17/23 02:39
Bromoform
pg/L
<1.50
1.50
5.00
01/17/23 02:39
Bromomethane
pg/L
<0.280
0.280
1.00
01/17/23 02:39
n-Butylbenzene
pg/L
<0.180
0.180
0.500
01/17/23 02:39
sec -Butyl benzene
pg/L
<0.200
0.200
0.500
01/17/23 02:39
tert-Butyl benzene
pg/L
<0.920
0.920
2.00
01/17/23 02:39
Carbon Tetrachloride
pg/L
<0.180
0.180
0.500
01/17/23 02:39
Chlorobenzene
pg/L
<0.190
0.190
0.500
01/17/23 02:39
Chlorodibromomethane
pg/L
<0.190
0.190
0.500
01/17/23 02:39
Chloroethane
pg/L
<0.430
0.430
1.00
01/17/23 02:39
Chloroform
pg/L
<0.220
0.220
0.500
01/17/23 02:39
Chloromethane
pg/L
<0.220
0.220
0.500
01/17/23 02:39
2-Chlorotoluene
pg/L
<0.200
0.200
0.500
01/17/23 02:39
4-Chlorotoluene
pg/L
<0.200
0.200
0.500
01/17/23 02:39
1,2-Dibromo-3-Chloropropane
pg/L
< 1.10
1.10
2.00
01/17/23 02:39
1,2-Dibromoethane
pg/L
<0.200
0.200
0.500
01/17/23 02:39
Dibromomethane
pg/L
<0.230
0.230
0.500
01/17/23 02:39
1,2-Dichlorobenzene
pg/L
<0.220
0.220
0.500
01/17/23 02:39
1,3-Dichlorobenzene
pg/L
<0.190
0.190
0.500
01/17/23 02:39
1,4-Dichlorobenzene
pg/L
<0.210
0.210
0.500
01/17/23 02:39
Dichlorodifluoromethane
pg/L
<1.20
1.20
5.00
01/17/23 02:39
1,1-Dichloroethane
pg/L
<0.240
0.240
0.500
01/17/23 02:39
1,2-Dichloroethane
pg/L
<0.150
0.150
0.500
01/17/23 02:39
1,1-Dichloroethene
pg/L
<0.150
0.150
0.500
01/17/23 02:39
Date: 01/19/2023 05:38 PM Page 1 of 30
Page 87 of 118
Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
S&ME, Inc - Charlotte
Jefferson Pilot Comm
23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypoi ntana lytica l.com
Quality Control Data
QC Prep: V28947 QC Analytical Batch(es): V28948
QC Prep Batch Method: 6200 PT Analysis Method: 6200B
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V28947 Matrix: AQU
Associated Lab Samples: 97322, 97323
Blank MDL MQL Analyzed a/o % Rec
Parameter Units Result Recovery Limits
cis-1,2-Dichloroethene
pg/L
<0.200
0.200
0.500
01/17/23 02:39
trans-1,2-Dichloroethene
pg/L
<0.180
0.180
0.500
01/17/23 02:39
1,2-Dichloropropane
pg/L
<0.190
0.190
0.500
01/17/23 02:39
1,3-Dichloropropane
pg/L
<0.130
0.130
0.500
01/17/23 02:39
2,2-Dichloropropane
pg/L
<0.210
0.210
2.00
01/17/23 02:39
1,1-Dichloropropene
pg/L
<0.200
0.200
0.500
01/17/23 02:39
cis-1,3-Dichloropropene
pg/L
<0.210
0.210
0.500
01/17/23 02:39
trans-1,3-Dichloropropene
pg/L
<0.150
0.150
0.500
01/17/23 02:39
Ethanol
pg/L
<42.0
42.0
200
01/17/23 02:39
Ethylbenzene
pg/L
<0.170
0.170
0.500
01/17/23 02:39
Hexachlorobutadiene
pg/L
<0.350
0.350
3.00
01/17/23 02:39
2-Hexanone
pg/L
<0.380
0.380
1.00
01/17/23 02:39
Isopropyl benzene
pg/L
<0.180
0.180
0.500
01/17/23 02:39
4-Isopropyl toluene
pg/L
<0.089
0.089
0.500
01/17/23 02:39
Methyl Ethyl Ketone (MEK)
pg/L
<0.710
0.710
5.00
01/17/23 02:39
Methyl tert-butyl ether (MTBE)
pg/L
<0.140
0.140
1.00
01/17/23 02:39
4-Methyl-2-Pentanone
pg/L
<0.078
0.078
1.00
01/17/23 02:39
Methylene Chloride
pg/L
<0.330
0.330
2.00
01/17/23 02:39
Naphthalene
pg/L
<0.470
0.470
1.00
01/17/23 02:39
n-Propylbenzene
pg/L
<0.190
0.190
0.500
01/17/23 02:39
Styrene
pg/L
<0.220
0.220
0.500
01/17/23 02:39
1,1,1,2-Tetrachloroethane
pg/L
<0.160
0.160
0.500
01/17/23 02:39
1,1,2,2-Tetrachloroethane
pg/L
<0.160
0.160
0.500
01/17/23 02:39
Tetrachloroethene
pg/L
<0.220
0.220
0.500
01/17/23 02:39
Toluene
pg/L
<0.220
0.220
0.500
01/17/23 02:39
1,2,3-Trichlorobenzene
pg/L
<0.380
0.380
0.500
01/17/23 02:39
1,2,4-Trichlorobenzene
pg/L
<0.310
0.310
0.500
01/17/23 02:39
Date: 01/19/2023 05:38 PM Page 2 of 30
Page 88 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28947
QC Analytical Batch(es): V28948
QC Prep Batch Method:
6200 PT
Analysis Method:
6200B
Analysis Description:
Volatile Organic
Compounds - GC/MS
Lab Reagent Blank
LRB-V28947
Matrix: AQU
Associated Lab Samples:
97322, 97323
Blank
MDL
MQL
Analyzed
a/o % Rec
Parameter
Units
Result
Recovery Limits
1,1,1-Trichloroethane
pg/L
<0.160
0.160
0.500
01/17/23 02:39
1,1,2-Trichloroethane
pg/L
<0.096
0.096
0.500
01/17/23 02:39
Trichloroethene
pg/L
<0.180
0.180
0.500
01/17/23 02:39
Trichlorofluoromethane
pg/L
<0.180
0.180
0.500
01/17/23 02:39
1,2,3-Trichloropropane
pg/L
<0.270
0.270
0.500
01/17/23 02:39
1,2,4-Trimethyl benzene
pg/L
<0.190
0.190
0.500
01/17/23 02:39
1,3,5-Trimethyl benzene
pg/L
<0.180
0.180
0.500
01/17/23 02:39
Vinyl Acetate
pg/L
<1.00
1.00
5.00
01/17/23 02:39
Vinyl Chloride
pg/L
<0.170
0.170
0.500
01/17/23 02:39
o-Xylene
pg/L
<0.210
0.210
0.500
01/17/23 02:39
m,p-Xylene
pg/L
<0.420
0.420
1.00
01/17/23 02:39
4-Bromofluorobenzene (S)
01/17/23 02:39
102 70-130
Dibromofluoromethane (S)
01/17/23 02:39
100 70-130
1,2-Dichloroethane - d4 (S)
01/17/23 02:39
95.8 70-130
Toluene-d8 (S)
01/17/23 02:39
97.4 70-130
Laboratory Control Sample & LCSD
LCS-V28947
LCSD-V28947
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
Acetone
pg/L
40.0
30.7
31.5
76.7
78.7
40-160
2.5
20.0
Bromobenzene
pg/L
20.0
22.4
20.6
112
103
70-130
8.3
20.0
Bromochloromethane
pg/L
20.0
21.2
21.5
106
108
70-130
1.4
20.0
Bromodichloromethane
pg/L
20.0
21.8
21.3
109
107
70-130
2.3
20.0
Bromoform
pg/L
20.0
22.2
21.8
111
109
70-130
1.8
20.0
Bromomethane
pg/L
20.0
22.4
22.5
112
113
60-140
0.4
20.0
n-Butylbenzene
pg/L
20.0
20.5
20.8
103
104
70-130
1.4
20.0
Date: 01/19/2023 05:38 PM Page 3 of 30
Page 89 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28947
QC Analytical Batch(es): V28948
QC Prep Batch Method:
6200 PT
Analysis
Method:
6200B
Analysis
Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V28947
LCSD-V28947
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
sec -Butyl benzene
pg/L
20.0
21.6
20.4
108
102
70-130
5.7
20.0
tert-Butyl benzene
pg/L
20.0
21.4
21.3
107
107
70-130
0.4
20.0
Carbon Tetrachloride
pg/L
20.0
20.5
20.2
103
101
70-130
1.4
20.0
Chlorobenzene
pg/L
20.0
22.1
21.5
111
108
70-130
2.7
20.0
Chlorodibromomethane
pg/L
20.0
20.8
20.6
104
103
70-130
0.9
20.0
Chloroethane
pg/L
20.0
21.6
20.8
108
104
60-140
3.7
20.0
Chloroform
pg/L
20.0
21.4
21.3
107
107
70-130
0.4
20.0
Chloromethane
pg/L
20.0
22.4
21.3
112
107
60-140
5.0
20.0
2-Chlorotoluene
pg/L
20.0
21.8
20.4
109
102
70-130
6.6
20.0
4-Chlorotoluene
pg/L
20.0
21.6
20.5
108
103
70-130
5.2
20.0
1,2-Dibromo-3-Chloropropane pg/L
20.0
20.4
22.0
102
110
70-130
7.5
20.0
1,2-Dibromoethane
pg/L
20.0
22.0
22.0
110
110
70-130
0.0
20.0
Dibromomethane
pg/L
20.0
21.4
21.2
107
106
70-130
0.9
20.0
1,2-Dichlorobenzene
pg/L
20.0
21.7
20.9
109
105
70-130
3.7
20.0
1,3-Dichlorobenzene
pg/L
20.0
21.7
21.0
109
105
70-130
3.2
20.0
1,4-Dichlorobenzene
pg/L
20.0
21.4
21.1
107
106
70-130
1.4
20.0
Dichlorodifluoromethane
pg/L
20.0
23.8
23.2
119
116
60-140
2.5
20.0
1,1-Dichloroethane
pg/L
20.0
21.1
21.7
106
109
70-130
2.8
20.0
1,2-Dichloroethane
pg/L
20.0
21.9
21.1
110
106
70-130
3.7
20.0
1,1-Dichloroethene
pg/L
20.0
21.7
21.1
109
106
70-130
2.8
20.0
cis-1,2-Dichloroethene
pg/L
20.0
21.9
21.2
110
106
70-130
3.2
20.0
trans-1,2-Dichloroethene
pg/L
20.0
21.7
21.7
109
109
70-130
0.0
20.0
1,2-Dichloropropane
pg/L
20.0
22.1
21.7
111
109
70-130
1.8
20.0
1,3-Dichloropropane
pg/L
20.0
22.0
20.8
110
104
70-130
5.6
20.0
2,2-Dichloropropane
pg/L
20.0
19.0
19.7
95.0
98.5
70-130
3.6
20.0
1,1-Dichloropropene
pg/L
20.0
22.6
21.8
113
109
70-130
3.6
20.0
Date: 01/19/2023 05:38 PM Page 4 of 30
Page 90 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28947
QC Analytical Batch(es): V28948
QC Prep Batch Method:
6200 PT
Analysis
Method:
6200B
Analysis
Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V28947
LCSD-V28947
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
cis-1,3-Dichloropropene
pg/L
20.0
21.2
21.0
106
105
70-130
0.9
20.0
trans-1,3-Dichloropropene
pg/L
20.0
21.2
20.9
106
105
70-130
1.4
20.0
Ethanol
pg/L
500
464
433
92.8
86.6
60-140
6.9
20.0
Ethylbenzene
pg/L
20.0
21.7
21.3
109
107
70-130
1.8
20.0
Hexachlorobutadiene
pg/L
20.0
22.6
21.5
113
108
70-130
4.9
20.0
2-Hexanone
pg/L
20.0
20.5
20.8
103
104
60-140
1.4
20.0
Isopropyl benzene
pg/L
20.0
22.5
20.9
113
105
70-130
7.3
20.0
4-Isopropyl toluene
pg/L
20.0
22.5
21.2
113
106
70-130
5.9
20.0
Methyl Ethyl Ketone (MEK)
pg/L
20.0
19.2
22.3
96.0
112
60-140
14.9
20.0
Methyl tert-butyl ether (MTBE)
pg/L
20.0
20.3
21.7
102
109
70-130
6.6
20.0
4-Methyl-2-Pentanone
pg/L
20.0
20.9
20.4
105
102
60-140
2.4
20.0
Methylene Chloride
pg/L
20.0
20.9
21.0
105
105
70-130
0.4
20.0
Naphthalene
pg/L
20.0
23.4
23.8
117
119
70-130
1.6
20.0
n-Propylbenzene
pg/L
20.0
22.5
20.5
113
103
70-130
9.3
20.0
Styrene
pg/L
20.0
22.7
20.7
114
104
70-130
9.2
20.0
1,1,1,2-Tetrachloroethane
pg/L
20.0
22.1
21.9
111
110
70-130
0.9
20.0
1,1,2,2-Tetrachloroethane
pg/L
20.0
22.6
21.1
113
106
70-130
6.8
20.0
Tetrachloroethene
pg/L
20.0
21.8
22.2
109
111
70-130
1.8
20.0
Toluene
pg/L
20.0
21.3
21.2
107
106
70-130
0.4
20.0
1,2,3-Trichlorobenzene
pg/L
20.0
24.8
22.8
124
114
70-130
8.4
20.0
1,2,4-Trichlorobenzene
pg/L
20.0
22.9
23.5
115
118
70-130
2.5
20.0
1,1,1-Trichloroethane
pg/L
20.0
21.3
21.0
107
105
70-130
1.4
20.0
1,1,2-Trichloroethane
pg/L
20.0
21.2
19.8
106
99.0
70-130
6.8
20.0
Trichloroethene
pg/L
20.0
22.3
22.0
112
110
70-130
1.3
20.0
Trichlorofluoromethane
pg/L
20.0
20.8
19.9
104
99.5
60-140
4.4
20.0
1,2,3-Trichloropropane
pg/L
20.0
21.5
20.7
108
104
70-130
3.7
20.0
Date: 01/19/2023 05:38 PM Page 5 of 30
Page 91 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28947
QC Analytical Batch(es): V28948
QC Prep Batch Method:
6200 PT
Analysis Method:
6200B
Analysis Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V28947
LCSD-V28947
Spike
LCS LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result Result
%Rec
% Rec
Limits
RPD
Max
RPD
1,2,4-Trimethyl benzene
pg/L
20.0
21.9 21.4
110
107
70-130
2.3
20.0
1,3,5-Trimethyl benzene
pg/L
20.0
21.8 20.5
109
103
70-130
6.1
20.0
Vinyl Acetate
pg/L
20.0
19.1 18.7
95.5
93.5
60-140
2.1
20.0
Vinyl Chloride
pg/L
20.0
24.5 20.7
123
104
60-140
16.8
20.0
o-Xylene
pg/L
20.0
21.6 20.9
108
105
70-130
3.2
20.0
m,p-Xylene
pg/L
40.0
44.7 43.8
112
110
70-130
2.0
20.0
4-Bromofluorobenzene (S)
98.8
96.2
70-130
Dibromofluoromethane (S)
99.8
101
70-130
1,2-Dichloroethane - d4 (S)
100
95.8
70-130
Toluene-d8(S)
103
101
70-130
Date: 01/19/2023 05:38 PM Page 6 of 30
Page 92 of 118
Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
S&ME, Inc - Charlotte
Jefferson Pilot Comm
23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypoi ntana lytica l.com
Quality Control Data
QC Prep: V28979 QC Analytical Batch(es): V28980
QC Prep Batch Method: 6200 PT Analysis Method: 6200B
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V28979 Matrix: AQU
Associated Lab Samples: 97322, 97323, 97325, 97326, 97327, 97328, 97330, 97331, 97332
Blank MDL MQL Analyzed a/o % Rec
Parameter Units Result Recovery Limits
Acetone
pg/L
<1.80
1.80
10.0
01/18/23 03:48
Benzene
pg/L
<0.180
0.180
0.500
01/18/23 03:48
Bromobenzene
pg/L
<0.210
0.210
0.500
01/18/23 03:48
Bromochloromethane
pg/L
<0.420
0.420
1.00
01/18/23 03:48
Bromodichloromethane
pg/L
<0.160
0.160
0.500
01/18/23 03:48
Bromoform
pg/L
<1.50
1.50
5.00
01/18/23 03:48
Bromomethane
pg/L
<0.280
0.280
1.00
01/18/23 03:48
n-Butylbenzene
pg/L
<0.180
0.180
0.500
01/18/23 03:48
sec -Butyl benzene
pg/L
<0.200
0.200
0.500
01/18/23 03:48
tert-Butyl benzene
pg/L
<0.920
0.920
2.00
01/18/23 03:48
Carbon Tetrachloride
pg/L
<0.180
0.180
0.500
01/18/23 03:48
Chlorobenzene
pg/L
<0.190
0.190
0.500
01/18/23 03:48
Chlorodibromomethane
pg/L
<0.190
0.190
0.500
01/18/23 03:48
Chloroethane
pg/L
<0.430
0.430
1.00
01/18/23 03:48
Chloroform
pg/L
<0.220
0.220
0.500
01/18/23 03:48
Chloromethane
pg/L
<0.220
0.220
0.500
01/18/23 03:48
2-Chlorotoluene
pg/L
<0.200
0.200
0.500
01/18/23 03:48
4-Chlorotoluene
pg/L
<0.200
0.200
0.500
01/18/23 03:48
Di -Isopropyl Ether (DIPE)
pg/L
<0.500
0.500
0.500
01/18/23 03:48
1,2-Dibromo-3-Chloropropane
pg/L
< 1.10
1.10
2.00
01/18/23 03:48
1,2-Dibromoethane
pg/L
<0.200
0.200
0.500
01/18/23 03:48
Dibromomethane
pg/L
<0.230
0.230
0.500
01/18/23 03:48
1,2-Dichlorobenzene
pg/L
<0.220
0.220
0.500
01/18/23 03:48
1,3-Dichlorobenzene
pg/L
<0.190
0.190
0.500
01/18/23 03:48
1,4-Dichlorobenzene
pg/L
<0.210
0.210
0.500
01/18/23 03:48
Dichlorodifluoromethane
pg/L
<1.20
1.20
5.00
01/18/23 03:48
1,1-Dichloroethane
pg/L
<0.240
0.240
0.500
01/18/23 03:48
Date: 01/19/2023 05:38 PM Page 7 of 30
Page 93 of 118
Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
S&ME, Inc - Charlotte
Jefferson Pilot Comm
23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypoi ntana lytica l.com
Quality Control Data
QC Prep: V28979 QC Analytical Batch(es): V28980
QC Prep Batch Method: 6200 PT Analysis Method: 6200B
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V28979 Matrix: AQU
Associated Lab Samples: 97322, 97323, 97325, 97326, 97327, 97328, 97330, 97331, 97332
Blank MDL MQL Analyzed a/o % Rec
Parameter Units Result Recovery Limits
1,2-Dichloroethane
pg/L
<0.150
0.150
0.500
01/18/23 03:48
1,1-Dichloroethene
pg/L
<0.150
0.150
0.500
01/18/23 03:48
cis-1,2-Dichloroethene
pg/L
<0.200
0.200
0.500
01/18/23 03:48
trans-1,2-Dichloroethene
pg/L
<0.180
0.180
0.500
01/18/23 03:48
1,2-Dichloropropane
pg/L
<0.190
0.190
0.500
01/18/23 03:48
1,3-Dichloropropane
pg/L
<0.130
0.130
0.500
01/18/23 03:48
2,2-Dichloropropane
pg/L
<0.210
0.210
2.00
01/18/23 03:48
1,1-Dichloropropene
pg/L
<0.200
0.200
0.500
01/18/23 03:48
cis-1,3-Dichloropropene
pg/L
<0.210
0.210
0.500
01/18/23 03:48
trans-1,3-Dichloropropene
pg/L
<0.150
0.150
0.500
01/18/23 03:48
Ethanol
pg/L
<42.0
42.0
200
01/18/23 03:48
Ethylbenzene
pg/L
<0.170
0.170
0.500
01/18/23 03:48
Hexachlorobutadiene
pg/L
<0.350
0.350
3.00
01/18/23 03:48
2-Hexanone
pg/L
<0.380
0.380
1.00
01/18/23 03:48
Isopropyl benzene
pg/L
<0.180
0.180
0.500
01/18/23 03:48
4-Isopropyl toluene
pg/L
<0.089
0.089
0.500
01/18/23 03:48
Methyl Ethyl Ketone (MEK)
pg/L
<0.710
0.710
5.00
01/18/23 03:48
Methyl tert-butyl ether (MTBE)
pg/L
<0.140
0.140
1.00
01/18/23 03:48
4-Methyl-2-Pentanone
pg/L
<0.078
0.078
1.00
01/18/23 03:48
Methylene Chloride
pg/L
<0.330
0.330
2.00
01/18/23 03:48
Naphthalene
pg/L
<0.470
0.470
1.00
01/18/23 03:48
n-Propylbenzene
pg/L
<0.190
0.190
0.500
01/18/23 03:48
Styrene
pg/L
<0.220
0.220
0.500
01/18/23 03:48
1,1,1,2-Tetrachloroethane
pg/L
<0.160
0.160
0.500
01/18/23 03:48
1,1,2,2-Tetrachloroethane
pg/L
<0.160
0.160
0.500
01/18/23 03:48
Tetrachloroethene
pg/L
<0.220
0.220
0.500
01/18/23 03:48
Toluene
pg/L
<0.220
0.220
0.500
01/18/23 03:48
Date: 01/19/2023 05:38 PM Page 8 of 30
Page 94 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28979
QC Analytical Batch(es): V28980
QC Prep Batch Method:
6200 PT
Analysis Method:
6200B
Analysis Description:
Volatile Organic
Compounds - GC/MS
Lab Reagent Blank
LRB-V28979
Matrix: AQU
Associated Lab Samples:
97322, 97323, 97325,
97326,
97327, 97328, 97330, 97331, 97332
Blank
MDL
MQL
Analyzed
a/o % Rec
Parameter
Units
Result
Recovery Limits
1,2,3-Trichlorobenzene
pg/L
<0.380
0.380
0.500
01/18/23 03:48
1,2,4-Trichlorobenzene
pg/L
<0.310
0.310
0.500
01/18/23 03:48
1,1,1-Trichloroethane
pg/L
<0.160
0.160
0.500
01/18/23 03:48
1,1,2-Trichloroethane
pg/L
<0.096
0.096
0.500
01/18/23 03:48
Trichloroethene
pg/L
<0.180
0.180
0.500
01/18/23 03:48
Trichlorofluoromethane
pg/L
<0.180
0.180
0.500
01/18/23 03:48
1,2,3-Trichloropropane
pg/L
<0.270
0.270
0.500
01/18/23 03:48
1,2,4-Trimethyl benzene
pg/L
<0.190
0.190
0.500
01/18/23 03:48
1,3,5-Trimethyl benzene
pg/L
<0.180
0.180
0.500
01/18/23 03:48
Vinyl Acetate
pg/L
<1.00
1.00
5.00
01/18/23 03:48
Vinyl Chloride
pg/L
<0.170
0.170
0.500
01/18/23 03:48
o-Xylene
pg/L
<0.210
0.210
0.500
01/18/23 03:48
m,p-Xylene
pg/L
<0.420
0.420
1.00
01/18/23 03:48
4-Bromofluorobenzene (S)
01/18/23 03:48
102 70-130
Dibromofluoromethane (S)
01/18/23 03:48
94.8 70-130
1,2-Dichloroethane - d4 (S)
01/18/23 03:48
94.0 70-130
Toluene-d8 (S)
01/18/23 03:48
98.4 70-130
Laboratory Control Sample & LCSD
LCS-V28979
LCSD-V28979
Spike
LCS
LCSD
LCS
LCSD
a/o Rec
Parameter Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
Acetone
pg/L
40.0
34.5
28.3
86.2
70.7
40-160
19.7
20.0
Benzene
pg/L
20.0
20.4
20.6
102
103
70-130
0.9
20.0
Bromobenzene
pg/L
20.0
20.3
21.9
102
110
70-130
7.5
20.0
Bromochloromethane
pg/L
20.0
21.4
21.5
107
108
70-130
0.4
20.0
Bromodichloromethane
pg/L
20.0
20.2
19.9
101
99.5
70-130
1.4
20.0
Date: 01/19/2023 05:38 PM Page 9 of 30
Page 95 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28979
QC Analytical Batch(es): V28980
QC Prep Batch Method:
6200 PT
Analysis
Method:
6200B
Analysis
Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V28979
LCSD-V28979
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
Bromoform
pg/L
20.0
21.4
21.1
107
106
70-130
1.4
20.0
Bromomethane
pg/L
20.0
17.9
17.6
89.5
88.0
60-140
1.6
20.0
n-Butylbenzene
pg/L
20.0
20.7
21.1
104
106
70-130
1.9
20.0
sec -Butyl benzene
pg/L
20.0
20.7
21.0
104
105
70-130
1.4
20.0
tert-Butyl benzene
pg/L
20.0
21.1
21.6
106
108
70-130
2.3
20.0
Carbon Tetrachloride
pg/L
20.0
23.7
18.9
119
94.5
70-130
22.5*
20.0
Chlorobenzene
pg/L
20.0
21.6
20.9
108
105
70-130
3.2
20.0
Chlorodibromomethane
pg/L
20.0
20.0
18.3
100
91.5
70-130
8.8
20.0
Chloroethane
pg/L
20.0
23.4
21.4
117
107
60-140
8.9
20.0
Chloroform
pg/L
20.0
21.4
20.9
107
105
70-130
2.3
20.0
Chloromethane
pg/L
20.0
21.4
20.1
107
101
60-140
6.2
20.0
2-Chlorotoluene
pg/L
20.0
20.0
21.9
100
110
70-130
9.0
20.0
4-Chlorotoluene
pg/L
20.0
19.9
21.8
99.5
109
70-130
9.1
20.0
Di -Isopropyl Ether(DIPE)
pg/L
20.0
22.6
21.8
113
109
70-130
3.6
20.0
1,2-Dibromo-3-Chloropropane pg/L
20.0
22.9
18.7
115
93.5
70-130
20.1*
20.0
1,2-Dibromoethane
pg/L
20.0
20.9
20.8
105
104
70-130
0.4
20.0
Dibromomethane
pg/L
20.0
20.5
20.6
103
103
70-130
0.4
20.0
1,2-Dichlorobenzene
pg/L
20.0
21.3
21.4
107
107
70-130
0.4
20.0
1,3-Dichlorobenzene
pg/L
20.0
21.2
22.0
106
110
70-130
3.7
20.0
1,4-Dichlorobenzene
pg/L
20.0
21.0
21.4
105
107
70-130
1.8
20.0
Dichlorodifluoromethane
pg/L
20.0
21.9
18.8
110
94.0
60-140
15.2
20.0
1,1-Dichloroethane
pg/L
20.0
23.2
21.2
116
106
70-130
9.0
20.0
1,2-Dichloroethane
pg/L
20.0
21.0
20.4
105
102
70-130
2.8
20.0
1,1-Dichloroethene
pg/L
20.0
22.1
21.0
111
105
70-130
5.1
20.0
cis-1,2-Dichloroethene
pg/L
20.0
22.5
22.1
113
111
70-130
1.7
20.0
trans-1,2-Dichloroethene
pg/L
20.0
23.3
21.3
117
107
70-130
8.9
20.0
* QC Fail Date: 01/19/2023 05:38 PM Page 10 of 30
Page 96 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28979
QC Analytical Batch(es): V28980
QC Prep Batch Method:
6200 PT
Analysis
Method:
6200B
Analysis
Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V28979
LCSD-V28979
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
1,2-Dichloropropane
pg/L
20.0
20.9
21.2
105
106
70-130
1.4
20.0
1,3-Dichloropropane
pg/L
20.0
20.5
19.9
103
99.5
70-130
2.9
20.0
2,2-Dichloropropane
pg/L
20.0
19.0
18.6
95.0
93.0
70-130
2.1
20.0
1,1-Dichloropropene
pg/L
20.0
21.3
21.5
107
108
70-130
0.9
20.0
cis-1,3-Dichloropropene
pg/L
20.0
20.9
20.3
105
102
70-130
2.9
20.0
trans-1,3-Dichloropropene
pg/L
20.0
21.4
20.3
107
102
70-130
5.2
20.0
Ethanol
pg/L
500
610
537
122
107
60-140
12.7
20.0
Ethylbenzene
pg/L
20.0
20.8
20.2
104
101
70-130
2.9
20.0
Hexachlorobutadiene
pg/L
20.0
21.0
21.0
105
105
70-130
0.0
20.0
2-Hexanone
pg/L
20.0
20.8
18.1
104
90.5
60-140
13.8
20.0
Isopropyl benzene
pg/L
20.0
20.5
22.3
103
112
70-130
8.4
20.0
4-Isopropyl toluene
pg/L
20.0
21.1
21.3
106
107
70-130
0.9
20.0
Methyl Ethyl Ketone (MEK)
pg/L
20.0
18.4
17.9
92.0
89.5
60-140
2.7
20.0
Methyl tert-butyl ether (MTBE)
pg/L
20.0
23.2
20.8
116
104
70-130
10.9
20.0
4-Methyl-2-Pentanone
pg/L
20.0
21.2
18.0
106
90.0
60-140
16.3
20.0
Methylene Chloride
pg/L
20.0
23.4
21.3
117
107
70-130
9.3
20.0
Naphthalene
pg/L
20.0
23.6
22.5
118
113
70-130
4.7
20.0
n-Propylbenzene
pg/L
20.0
20.1
21.9
101
110
70-130
8.5
20.0
Styrene
pg/L
20.0
21.1
21.2
106
106
70-130
0.4
20.0
1,1,1,2-Tetrachloroethane
pg/L
20.0
21.3
21.6
107
108
70-130
1.3
20.0
1,1,2,2-Tetrachloroethane
pg/L
20.0
21.1
21.8
106
109
70-130
3.2
20.0
Tetrachloroethene
pg/L
20.0
21.3
19.2
107
96.0
70-130
10.3
20.0
Toluene
pg/L
20.0
20.9
19.7
105
98.5
70-130
5.9
20.0
1,2,3-Trichlorobenzene
pg/L
20.0
24.7
24.3
124
122
70-130
1.6
20.0
1,2,4-Trichlorobenzene
pg/L
20.0
22.8
22.7
114
114
70-130
0.4
20.0
1,1,1-Trichloroethane
pg/L
20.0
21.4
20.7
107
104
70-130
3.3
20.0
Date: 01/19/2023 05:38 PM Page 11 of 30
Page 97 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28979
QC Analytical Batch(es): V28980
QC Prep Batch Method:
6200 PT
Analysis
Method:
6200B
Analysis
Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V28979
LCSD-V28979
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
1,1,2-Trichloroethane
pg/L
20.0
20.6
20.2
103
101
70-130
1.9
20.0
Trichloroethene
pg/L
20.0
21.9
21.4
110
107
70-130
2.3
20.0
Trichlorofluoromethane
pg/L
20.0
21.9
20.6
110
103
60-140
6.1
20.0
1,2,3-Trichloropropane
pg/L
20.0
20.1
21.0
101
105
70-130
4.3
20.0
1,2,4-Trimethyl benzene
pg/L
20.0
21.0
21.9
105
110
70-130
4.1
20.0
1,3,5-Trimethyl benzene
pg/L
20.0
20.6
22.2
103
111
70-130
7.4
20.0
Vinyl Acetate
pg/L
20.0
15.4
18.7
77.0
93.5
60-140
19.3
20.0
Vinyl Chloride
pg/L
20.0
23.2
21.2
116
106
60-140
9.0
20.0
o-Xylene
pg/L
20.0
21.3
21.2
107
106
70-130
0.4
20.0
m,p-Xylene
pg/L
40.0
42.7
41.5
107
104
70-130
2.8
20.0
4-Bromofluorobenzene (S)
95.4
109
70-130
Dibromofluoromethane (S)
101
99.6
70-130
1,2-Dichloroethane - d4 (S)
100
101
70-130
Toluene-d8(S)
96.0
93.8
70-130
Date: 01/19/2023 05:38 PM Page 12 of 30
Page 98 of 118
Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
S&ME, Inc - Charlotte
Jefferson Pilot Comm
23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V29020 QC Analytical Batch(es): V29021
QC Prep Batch Method: 6200 PT Analysis Method: 6200B
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V29020
Associated Lab Samples: 97324, 97326, 97329
Parameter
Blank MDL
Units Result
Matrix: AQU
MQL Analyzed a/o % Rec
Recovery Limits
Acetone
pg/L
<1.80
1.80
10.0
01/19/23 03:58
Benzene
pg/L
<0.180
0.180
0.500
01/19/23 03:58
Bromobenzene
pg/L
<0.210
0.210
0.500
01/19/23 03:58
Bromochloromethane
pg/L
<0.420
0.420
1.00
01/19/23 03:58
Bromodichloromethane
pg/L
<0.160
0.160
0.500
01/19/23 03:58
Bromoform
pg/L
<1.50
1.50
5.00
01/19/23 03:58
Bromomethane
pg/L
<0.280
0.280
1.00
01/19/23 03:58
n-Butylbenzene
pg/L
<0.180
0.180
0.500
01/19/23 03:58
sec -Butyl benzene
pg/L
<0.200
0.200
0.500
01/19/23 03:58
tert-Butyl benzene
pg/L
<0.920
0.920
2.00
01/19/23 03:58
Carbon Tetrachloride
pg/L
<0.180
0.180
0.500
01/19/23 03:58
Chlorobenzene
pg/L
<0.190
0.190
0.500
01/19/23 03:58
Chlorodibromomethane
pg/L
<0.190
0.190
0.500
01/19/23 03:58
Chloroethane
pg/L
<0.430
0.430
1.00
01/19/23 03:58
Chloroform
pg/L
<0.220
0.220
0.500
01/19/23 03:58
Chloromethane
pg/L
<0.220
0.220
0.500
01/19/23 03:58
2-Chlorotoluene
pg/L
<0.200
0.200
0.500
01/19/23 03:58
4-Chlorotoluene
pg/L
<0.200
0.200
0.500
01/19/23 03:58
Di -Isopropyl Ether (DIPE)
pg/L
<0.500
0.500
0.500
01/19/23 03:58
1,2-Dibromo-3-Chloropropane
pg/L
<1.10
1.10
2.00
01/19/23 03:58
1,2-Dibromoethane
pg/L
<0.200
0.200
0.500
01/19/23 03:58
Dibromomethane
pg/L
<0.230
0.230
0.500
01/19/23 03:58
1,2-Dichlorobenzene
pg/L
<0.220
0.220
0.500
01/19/23 03:58
1,3-Dichlorobenzene
pg/L
<0.190
0.190
0.500
01/19/23 03:58
1,4-Dichlorobenzene
pg/L
<0.210
0.210
0.500
01/19/23 03:58
Dichlorodifluoromethane
pg/L
<1.20
1.20
5.00
01/19/23 03:58
1,1-Dichloroethane
pg/L
<0.240
0.240
0.500
01/19/23 03:58
Date: 01/19/2023 05:38 PM Page 13 of 30
Page 99 of 118
Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
S&ME, Inc - Charlotte
Jefferson Pilot Comm
23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V29020 QC Analytical Batch(es): V29021
QC Prep Batch Method: 6200 PT Analysis Method: 6200B
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V29020
Associated Lab Samples: 97324, 97326, 97329
Parameter
Blank MDL
Units Result
Matrix: AQU
MQL Analyzed a/o % Rec
Recovery Limits
1,2-Dichloroethane
pg/L
<0.150
0.150
0.500
01/19/23 03:58
1,1-Dichloroethene
pg/L
<0.150
0.150
0.500
01/19/23 03:58
cis-1,2-Dichloroethene
pg/L
<0.200
0.200
0.500
01/19/23 03:58
trans-1,2-Dichloroethene
pg/L
<0.180
0.180
0.500
01/19/23 03:58
1,2-Dichloropropane
pg/L
<0.190
0.190
0.500
01/19/23 03:58
1,3-Dichloropropane
pg/L
<0.130
0.130
0.500
01/19/23 03:58
2,2-Dichloropropane
pg/L
<0.210
0.210
2.00
01/19/23 03:58
1,1-Dichloropropene
pg/L
<0.200
0.200
0.500
01/19/23 03:58
cis-1,3-Dichloropropene
pg/L
<0.210
0.210
0.500
01/19/23 03:58
trans-1,3-Dichloropropene
pg/L
<0.150
0.150
0.500
01/19/23 03:58
Ethanol
pg/L
<42.0
42.0
200
01/19/23 03:58
Ethylbenzene
pg/L
<0.170
0.170
0.500
01/19/23 03:58
Hexachlorobutadiene
pg/L
<0.350
0.350
3.00
01/19/23 03:58
2-Hexanone
pg/L
<0.380
0.380
1.00
01/19/23 03:58
Isopropyl benzene
pg/L
<0.180
0.180
0.500
01/19/23 03:58
4-Isopropyl toluene
pg/L
<0.089
0.089
0.500
01/19/23 03:58
Methyl Ethyl Ketone (MEK)
pg/L
<0.710
0.710
5.00
01/19/23 03:58
Methyl tert-butyl ether (MTBE)
pg/L
<0.140
0.140
1.00
01/19/23 03:58
4-Methyl-2-Pentanone
pg/L
<0.078
0.078
1.00
01/19/23 03:58
Methylene Chloride
pg/L
<0.330
0.330
2.00
01/19/23 03:58
Naphthalene
pg/L
<0.470
0.470
1.00
01/19/23 03:58
n-Propylbenzene
pg/L
<0.190
0.190
0.500
01/19/23 03:58
Styrene
pg/L
<0.220
0.220
0.500
01/19/23 03:58
1,1,1,2-Tetrachloroethane
pg/L
<0.160
0.160
0.500
01/19/23 03:58
1,1,2,2-Tetrachloroethane
pg/L
<0.160
0.160
0.500
01/19/23 03:58
Tetrachloroethene
pg/L
<0.220
0.220
0.500
01/19/23 03:58
Toluene
pg/L
<0.220
0.220
0.500
01/19/23 03:58
Date: 01/19/2023 05:38 PM Page 14 of 30
Page 100 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V29020
QC Analytical Batch(es): V29021
QC Prep Batch Method:
6200 PT
Analysis Method:
6200B
Analysis Description:
Volatile Organic
Compounds - GC/MS
Lab Reagent Blank
LRB-V29020
Matrix: AQU
Associated Lab Samples:
97324, 97326, 97329
Blank
MDL
MQL
Analyzed
a/o % Rec
Parameter
Units
Result
Recovery Limits
1,2,3-Trichlorobenzene
pg/L
<0.380
0.380
0.500
01/19/23 03:58
1,2,4-Trichlorobenzene
pg/L
<0.310
0.310
0.500
01/19/23 03:58
1,1,1-Trichloroethane
pg/L
<0.160
0.160
0.500
01/19/23 03:58
1,1,2-Trichloroethane
pg/L
<0.096
0.096
0.500
01/19/23 03:58
Trichloroethene
pg/L
<0.180
0.180
0.500
01/19/23 03:58
Trichlorofluoromethane
pg/L
<0.180
0.180
0.500
01/19/23 03:58
1,2,3-Trichloropropane
pg/L
<0.270
0.270
0.500
01/19/23 03:58
1,2,4-Trimethyl benzene
pg/L
<0.190
0.190
0.500
01/19/23 03:58
1,3,5-Trimethyl benzene
pg/L
<0.180
0.180
0.500
01/19/23 03:58
Vinyl Acetate
pg/L
<1.00
1.00
5.00
01/19/23 03:58
Vinyl Chloride
pg/L
<0.170
0.170
0.500
01/19/23 03:58
o-Xylene
pg/L
<0.210
0.210
0.500
01/19/23 03:58
m,p-Xylene
pg/L
<0.420
0.420
1.00
01/19/23 03:58
4-Bromofluorobenzene (S)
01/19/23 03:58
123 70-130
Dibromofluoromethane (S)
01/19/23 03:58
93.0 70-130
1,2-Dichloroethane - d4 (S)
01/19/23 03:58
97.0 70-130
Toluene-d8 (S)
01/19/23 03:58
95.4 70-130
Laboratory Control Sample & LCSD
LCS-V29020
LCSD-V29020
Spike
LCS
LCSD
LCS
LCSD
a/o Rec
Parameter Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
Acetone
pg/L
40.0
25.0
24.2
62.5
60.5
40-160
3.2
20.0
Benzene
pg/L
20.0
19.8
19.3
99.0
96.5
70-130
2.5
20.0
Bromobenzene
pg/L
20.0
21.2
20.4
106
102
70-130
3.8
20.0
Bromochloromethane
pg/L
20.0
20.3
20.3
102
102
70-130
0.0
20.0
Bromodichloromethane
pg/L
20.0
19.8
19.6
99.0
98.0
70-130
1.0
20.0
Date: 01/19/2023 05:38 PM Page 15 of 30
Page 101 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V29020
QC Analytical Batch(es): V29021
QC Prep Batch Method:
6200 PT
Analysis
Method:
6200B
Analysis
Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V29020
LCSD-V29020
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
Bromoform
pg/L
20.0
19.7
18.1
98.5
90.5
70-130
8.4
20.0
Bromomethane
pg/L
20.0
17.4
17.8
87.0
89.0
60-140
2.2
20.0
n-Butylbenzene
pg/L
20.0
21.0
20.1
105
101
70-130
4.3
20.0
sec -Butyl benzene
pg/L
20.0
20.4
19.8
102
99.0
70-130
2.9
20.0
tert-Butyl benzene
pg/L
20.0
20.6
19.7
103
98.5
70-130
4.4
20.0
Carbon Tetrachloride
pg/L
20.0
19.2
18.8
96.0
94.0
70-130
2.1
20.0
Chlorobenzene
pg/L
20.0
21.6
20.3
108
102
70-130
6.2
20.0
Chlorodibromomethane
pg/L
20.0
18.2
18.3
91.0
91.5
70-130
0.5
20.0
Chloroethane
pg/L
20.0
20.9
20.8
105
104
60-140
0.4
20.0
Chloroform
pg/L
20.0
20.5
20.1
103
101
70-130
1.9
20.0
Chloromethane
pg/L
20.0
19.4
18.9
97.0
94.5
60-140
2.6
20.0
2-Chlorotoluene
pg/L
20.0
20.8
20.1
104
101
70-130
3.4
20.0
4-Chlorotoluene
pg/L
20.0
20.9
19.8
105
99.0
70-130
5.4
20.0
Di -Isopropyl Ether (DIPE)
pg/L
20.0
20.0
19.2
100
96.0
70-130
4.0
20.0
1,2-Dibromo-3-Chloropropane pg/L
20.0
17.1
18.6
85.5
93.0
70-130
8.4
20.0
1,2-Dibromoethane
pg/L
20.0
20.0
19.4
100
97.0
70-130
3.0
20.0
Dibromomethane
pg/L
20.0
18.9
19.7
94.5
98.5
70-130
4.1
20.0
1,2-Dichlorobenzene
pg/L
20.0
20.8
19.7
104
98.5
70-130
5.4
20.0
1,3-Dichlorobenzene
pg/L
20.0
21.0
19.5
105
97.5
70-130
7.4
20.0
1,4-Dichlorobenzene
pg/L
20.0
20.7
19.4
104
97.0
70-130
6.4
20.0
Dichlorodifluoromethane
pg/L
20.0
21.2
21.8
106
109
60-140
2.7
20.0
1,1-Dichloroethane
pg/L
20.0
20.7
19.8
104
99.0
70-130
4.4
20.0
1,2-Dichloroethane
pg/L
20.0
19.4
19.4
97.0
97.0
70-130
0.0
20.0
1,1-Dichloroethene
pg/L
20.0
20.3
19.5
102
97.5
70-130
4.0
20.0
cis-1,2-Dichloroethene
pg/L
20.0
20.9
19.5
105
97.5
70-130
6.9
20.0
trans-1,2-Dichloroethene
pg/L
20.0
21.3
20.8
107
104
70-130
2.3
20.0
Date: 01/19/2023 05:38 PM Page 16 of 30
Page 102 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V29020
QC Analytical Batch(es): V29021
QC Prep Batch Method:
6200 PT
Analysis
Method:
6200B
Analysis
Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V29020
LCSD-V29020
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
1,2-Dichloropropane
pg/L
20.0
20.6
20.1
103
101
70-130
2.4
20.0
1,3-Dichloropropane
pg/L
20.0
19.8
19.2
99.0
96.0
70-130
3.0
20.0
2,2-Dichloropropane
pg/L
20.0
17.8
17.9
89.0
89.5
70-130
0.5
20.0
1,1-Dichloropropene
pg/L
20.0
20.4
20.6
102
103
70-130
0.9
20.0
cis-1,3-Dichloropropene
pg/L
20.0
19.2
19.9
96.0
99.5
70-130
3.5
20.0
trans-1,3-Dichloropropene
pg/L
20.0
19.0
19.7
95.0
98.5
70-130
3.6
20.0
Ethanol
pg/L
500
387
388
77.4
77.6
60-140
0.2
20.0
Ethylbenzene
pg/L
20.0
21.1
19.3
106
96.5
70-130
8.9
20.0
Hexachlorobutadiene
pg/L
20.0
19.2
20.5
96.0
103
70-130
6.5
20.0
2-Hexanone
pg/L
20.0
15.7
14.9
78.5
74.5
60-140
5.2
20.0
Isopropyl benzene
pg/L
20.0
22.0
21.1
110
106
70-130
4.1
20.0
4-Isopropyl toluene
pg/L
20.0
20.6
20.0
103
100
70-130
2.9
20.0
Methyl Ethyl Ketone (MEK)
pg/L
20.0
14.0
15.7
70.0
78.5
60-140
11.4
20.0
Methyl tert-butyl ether (MTBE)
pg/L
20.0
18.9
18.6
94.5
93.0
70-130
1.6
20.0
4-Methyl-2-Pentanone
pg/L
20.0
15.7
15.6
78.5
78.0
60-140
0.6
20.0
Methylene Chloride
pg/L
20.0
20.3
20.1
102
101
70-130
0.9
20.0
Naphthalene
pg/L
20.0
20.7
19.8
104
99.0
70-130
4.4
20.0
n-Propylbenzene
pg/L
20.0
21.2
20.4
106
102
70-130
3.8
20.0
Styrene
pg/L
20.0
21.1
18.7
106
93.5
70-130
12.0
20.0
1,1,1,2-Tetrachloroethane
pg/L
20.0
22.2
21.3
111
107
70-130
4.1
20.0
1,1,2,2-Tetrachloroethane
pg/L
20.0
18.6
18.2
93.0
91.0
70-130
2.1
20.0
Tetrachloroethene
pg/L
20.0
22.4
21.3
112
107
70-130
5.0
20.0
Toluene
pg/L
20.0
19.6
20.4
98.0
102
70-130
4.0
20.0
1,2,3-Trichlorobenzene
pg/L
20.0
22.1
23.3
111
117
70-130
5.2
20.0
1,2,4-Trichlorobenzene
pg/L
20.0
21.6
21.4
108
107
70-130
0.9
20.0
1,1,1-Trichloroethane
pg/L
20.0
20.2
20.2
101
101
70-130
0.0
20.0
Date: 01/19/2023 05:38 PM Page 17 of 30
Page 103 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V29020
QC Analytical Batch(es): V29021
QC Prep Batch Method:
6200 PT
Analysis
Method:
6200B
Analysis
Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V29020
LCSD-V29020
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
1,1,2-Trichloroethane
pg/L
20.0
18.8
19.2
94.0
96.0
70-130
2.1
20.0
Trichloroethene
pg/L
20.0
20.9
20.2
105
101
70-130
3.4
20.0
Trichlorofluoromethane
pg/L
20.0
20.0
20.0
100
100
60-140
0.0
20.0
1,2,3-Trichloropropane
pg/L
20.0
18.0
17.5
90.0
87.5
70-130
2.8
20.0
1,2,4-Trimethyl benzene
pg/L
20.0
21.1
20.3
106
102
70-130
3.8
20.0
1,3,5-Trimethyl benzene
pg/L
20.0
21.3
20.2
107
101
70-130
5.3
20.0
Vinyl Acetate
pg/L
20.0
14.1
15.8
70.5
79.0
60-140
11.3
20.0
Vinyl Chloride
pg/L
20.0
21.1
20.7
106
104
60-140
1.9
20.0
o-Xylene
pg/L
20.0
21.0
19.3
105
96.5
70-130
8.4
20.0
m,p-Xylene
pg/L
40.0
43.5
40.1
109
100
70-130
8.1
20.0
4-Bromofluorobenzene (S)
103
98.6
70-130
Dibromofluoromethane (S)
96.2
98.0
70-130
1,2-Dichloroethane - d4 (S)
96.2
97.2
70-130
Toluene-d8(S)
104
101
70-130
Date: 01/19/2023 05:38 PM Page 18 of 30
Page 104 of 118
Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
S&ME, Inc - Charlotte
Jefferson Pilot Comm
23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V28891 QC Analytical Batch(es): V29017
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Lab Reagent Blank LRB-V28891
Associated Lab Samples: 97322, 97323, 97324, 97325
Parameter
Blank MDL
Units Result
Matrix: AQU
MQL Analyzed a/o % Rec
Recovery Limits
Acenaphthene
pg/L
<0.302
0.302
2.00
01/17/23 14:53
Acenaphthylene
pg/L
<0.297
0.297
2.00
01/17/23 14:53
Anthracene
pg/L
<0.836
0.836
2.00
01/17/23 14:53
Benzidine
pg/L
<1.32
1.32
10.0
01/17/23 14:53
Benzo(a)anthracene
pg/L
<0.637
0.637
2.00
01/17/23 14:53
Benzo(a)pyrene
pg/L
<1.02
1.02
2.00
01/17/23 14:53
Benzo(b)fluoranthene
pg/L
<2.49
2.49
5.00
01/17/23 14:53
Benzo(g,h,i)perylene
pg/L
<1.01
1.01
5.00
01/17/23 14:53
Benzo(k)fluoranthene
pg/L
<1.99
1.99
5.00
01/17/23 14:53
Benzoic Acid
pg/L
<1.10
1.10
10.0
01/17/23 14:53
Benzyl alcohol
pg/L
<0.684
0.684
5.00
01/17/23 14:53
Bis(2-Chloroethoxy)methane
pg/L
<0.468
0.468
5.00
01/17/23 14:53
Bis(2-Chloroethyl)ether
pg/L
<1.04
1.04
5.00
01/17/23 14:53
Bis(2-Chloroisopropyl)ether
pg/L
<1.08
1.08
5.00
01/17/23 14:53
Bis(2-ethylhexyl)phthalate
pg/L
<24.0
24.0
50.0
01/17/23 14:53
4-Bromophenyl phenyl ether
pg/L
<1.11
1.11
5.00
01/17/23 14:53
Butyl benzyl phthalate
pg/L
<1.83
1.83
5.00
01/17/23 14:53
4-Chloro-3-methyl phenol
pg/L
<1.18
1.18
5.00
01/17/23 14:53
2-Chloronaphthalene
pg/L
<7.38
7.38
20.0
01/17/23 14:53
2-Chlorophenol
pg/L
<0.938
0.938
10.0
01/17/23 14:53
4-Chlorophenyl phenyl ether
pg/L
<1.71
1.71
5.00
01/17/23 14:53
Chrysene
pg/L
<0.405
0.405
2.00
01/17/23 14:53
Dibenz(a,h)anthracene
pg/L
<0.434
0.434
2.00
01/17/23 14:53
Dibenzofuran
pg/L
<0.856
0.856
5.00
01/17/23 14:53
1,2-Dichlorobenzene
pg/L
<2.00
2.00
5.00
01/17/23 14:53
1,3-Dichlorobenzene
pg/L
<2.00
2.00
5.00
01/17/23 14:53
1,4-Dichlorobenzene
pg/L
<2.05
2.05
5.00
01/17/23 14:53
Date: 01/19/2023 05:38 PM Page 19 of 30
Page 105 of 118
Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
S&ME, Inc - Charlotte
Jefferson Pilot Comm
23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V28891 QC Analytical Batch(es): V29017
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Lab Reagent Blank LRB-V28891
Associated Lab Samples: 97322, 97323, 97324, 97325
Parameter
Blank MDL
Units Result
Matrix: AQU
MQL Analyzed a/o % Rec
Recovery Limits
3,3'-Dichlorobenzidine
pg/L
<1.89
1.89
5.00
01/17/23 14:53
2,4-Dichlorophenol
pg/L
<1.46
1.46
10.0
01/17/23 14:53
Diethyl phthalate
pg/L
<0.745
0.745
5.00
01/17/23 14:53
Dimethyl phthalate
pg/L
<0.939
0.939
5.00
01/17/23 14:53
2,4-Dimethylphenol
pg/L
<1.57
1.57
20.0
01/17/23 14:53
Di-n-butyl phthalate
pg/L
<2.06
2.06
5.00
01/17/23 14:53
4,6- Din itro-2-methylphenol
pg/L
<2.07
2.07
10.0
01/17/23 14:53
2,4-Dinitrophenol
pg/L
<1.92
1.92
10.0
01/17/23 14:53
2,4-Dinitrotoluene
pg/L
<1.11
1.11
5.00
01/17/23 14:53
2,6-Dinitrotoluene
pg/L
<0.809
0.809
5.00
01/17/23 14:53
Di-n-Octyl Phthalate
pg/L
<1.65
1.65
5.00
01/17/23 14:53
Fluoranthene
pg/L
<0.250
0.250
2.00
01/17/23 14:53
Fluorene
pg/L
<0.807
0.807
2.00
01/17/23 14:53
Hexachlorobenzene
pg/L
<0.979
0.979
5.00
01/17/23 14:53
Hexachlorobutadiene
pg/L
<2.73
2.73
5.00
01/17/23 14:53
Hexachlorocyclopentadiene
pg/L
<2.05
2.05
5.00
01/17/23 14:53
Hexachloroethane
pg/L
<1.76
1.76
5.00
01/17/23 14:53
Indeno(1,2,3-cd)pyrene
pg/L
<0.477
0.477
2.00
01/17/23 14:53
Isophorone
pg/L
<0.444
0.444
5.00
01/17/23 14:53
1-Methylnaphthalene
pg/L
<1.14
1.14
2.00
01/17/23 14:53
2-Methylnaphthalene
pg/L
<0.666
0.666
2.00
01/17/23 14:53
Naphthalene
pg/L
<0.728
0.728
2.00
01/17/23 14:53
Nitrobenzene
pg/L
<0.905
0.905
5.00
01/17/23 14:53
2-Nitrophenol
pg/L
<0.493
0.493
5.00
01/17/23 14:53
4-Nitrophenol
pg/L
<1.23
1.23
10.0
01/17/23 14:53
N-Nitrosodiphenylamine
pg/L
<1.10
1.10
5.00
01/17/23 14:53
N-Nitroso-di-n-propylamine
pg/L
<0.641
0.641
5.00
01/17/23 14:53
Date: 01/19/2023 05:38 PM Page 20 of 30
Page 106 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28891
QC Analytical Batch(es): V29017
QC Prep Batch Method:
625.1 (Prep)
Analysis Method:
625.1
Analysis Description:
625.1 - Base/Neutrals and Acids by GC/MS
Lab Reagent Blank
LRB-V28891
Matrix: AQU
Associated Lab Samples:
97322, 97323, 97324,
97325
Blank MDL
MQL
Analyzed
a/o
% Rec
Parameter
Units
Result
Recovery
Limits
Pentachlorophenol
pg/L
<1.43
1.43
5.00
01/17/23 14:53
Phenanthrene
pg/L
<0.428
0.428
2.00
01/17/23 14:53
Phenol
pg/L
<0.651
0.651
5.00
01/17/23 14:53
Pyrene
pg/L
<0.434
0.434
2.00
01/17/23 14:53
1,2,4-Trichlorobenzene
pg/L
<2.21
2.21
5.00
01/17/23 14:53
2,4,6-Trichlorophenol
pg/L
< 1.32
1.32
5.00
01/17/23 14:53
2-Fluorobiphenyl (S)
01/17/23 14:53
75.4
49-118
2-Fluorophenol(S)
01/17/23 14:53
38.1
22-84
Nitrobenzene-d5 (S)
01/17/23 14:53
63.2
43-123
4-Terphenyl-d14 (S)
01/17/23 14:53
90.0
49-151
2,4,6-Tribromophenol(S)
01/17/23 14:53
77.9
31-144
Phenol-d5 (S)
01/17/23 14:53
26.1
10-63
Laboratory Control Sample & LCSD
LCS-V28891
LCSD-V28891
Spike
LCS
LCSD
LCS LCSD
a/o Rec
Parameter
Units
Conc.
Result
Result
%Rec % Rec
Limits
RPD
Max
RPD
Acenaphthene
pg/L
50.0
33.5
37.0
67.0 74.0
47-145
9.9
20.0
Acenaphthylene
pg/L
50.0
34.7
38.0
69.4 76.0
33-145
9.0
20.0
Anthracene
pg/L
50.0
38.2
40.7
76.4 81.4
27-133
6.3
20.0
Benzidine
pg/L
50.0
28.5
28.4
57.0 56.8
15-150
0.3
20.0
Benzo(a)anthracene
pg/L
50.0
36.8
39.7
73.6 79.4
33-143
7.5
20.0
Benzo(a)pyrene
pg/L
50.0
33.3
35.4
66.6 70.8
17-163
6.1
20.0
Benzo(b)fluoranthene
pg/L
50.0
32.5
34.9
65.0 69.8
24-159
7.1
20.0
Benzo(g,h,i)perylene
pg/L
50.0
29.2
31.1
58.4 62.2
10-219
6.3
20.0
Benzo(k)fluoranthene
pg/L
50.0
31.0
33.1
62.0 66.2
11-162
6.5
20.0
Benzoic Acid
pg/L
50.0
14.9
14.9
29.8 29.8
10-125
0.0
20.0
Date: 01/19/2023 05:38 PM Page 21 of 30
Page 107 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28891
QC Analytical Batch(es): V29017
QC Prep Batch Method:
625.1 (Prep)
Analysis
Method:
625.1
Analysis
Description:
625.1
- Base/Neutrals and Acids by GC/MS
Laboratory Control Sample & LCSD
LCS-V28891
LCSD-V28891
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits RPD
Max
RPD
Benzyl alcohol
pg/L
50.0
32.0
34.8
64.0
69.6
16-107
8.3
20.0
Bis(2-Chloroethoxy)methane
pg/L
50.0
30.6
32.8
61.2
65.6
33-184
6.9
20.0
Bis(2-Chloroethyl)ether
pg/L
50.0
29.8
33.9
59.6
67.8
12-158
12.8
20.0
Bis(2-Chloroisopropyl)ether
pg/L
50.0
30.8
32.0
61.6
64.0
36-166
3.8
20.0
Bis(2-ethylhexyl)phthalate
pg/L
50.0
37.5
40.9
75.0
81.8
10-158
8.6
20.0
4-Bromophenyl phenyl ether
pg/L
50.0
39.2
41.9
78.4
83.8
53-127
6.6
20.0
Butyl benzyl phthalate
pg/L
50.0
36.4
40.9
72.8
81.8
10-152
11.6
20.0
4-Chloro-3-methylphenol
pg/L
50.0
31.9
33.4
63.8
66.8
22-147
4.5
20.0
2-Chloronaphthalene
pg/L
50.0
34.7
38.6
69.4
77.2
60-118
10.6
20.0
2-Chlorophenol
pg/L
50.0
29.7
32.0
59.4
64.0
23-134
7.4
20.0
4-Chlorophenyl phenyl ether
pg/L
50.0
37.7
41.2
75.4
82.4
25-158
8.8
20.0
Chrysene
pg/L
50.0
36.1
40.1
72.2
80.2
17-168
10.4
20.0
Dibenz(a,h)anthracene
pg/L
50.0
30.5
32.5
61.0
65.0
10-227
6.3
20.0
Dibenzofuran
pg/L
50.0
35.9
39.0
71.8
78.0
39-114
8.2
20.0
1,2-Dichlorobenzene
pg/L
50.0
30.3
30.8
60.6
61.6
32-129
1.6
20.0
1,3-Dichlorobenzene
pg/L
50.0
29.4
30.1
58.8
60.2
20-124
2.3
20.0
1,4-Dichlorobenzene
pg/L
50.0
29.0
29.3
58.0
58.6
20-124
1.0
20.0
3,3'-Dichlorobenzidine
pg/L
50.0
35.8
38.7
71.6
77.4
10-262
7.7
20.0
2,4-Dichlorophenol
pg/L
50.0
30.2
32.9
60.4
65.8
39-135
8.5
20.0
Diethyl phthalate
pg/L
50.0
37.7
40.7
75.4
81.4
10-114
7.6
20.0
Dimethyl phthalate
pg/L
50.0
38.2
40.5
76.4
81.0
10-112
5.8
20.0
2,4-Dimethyl phenol
pg/L
50.0
38.0
42.5
76.0
85.0
32-119
11.1
20.0
Di-n-butyl phthalate
pg/L
50.0
39.3
42.2
78.6
84.4
10-118
7.1
20.0
4,6- Din itro-2-methylphenol
pg/L
50.0
42.6
45.6
85.2
91.2
10-181
6.8
20.0
2,4-Dinitrophenol
pg/L
50.0
43.2
48.1
86.4
96.2
10-191
10.7
20.0
2,4-Dinitrotoluene
pg/L
50.0
39.3
41.3
78.6
82.6
39-139
4.9
20.0
Date: 01/19/2023 05:38 PM Page 22 of 30
Page 108 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28891
QC Analytical Batch(es): V29017
QC Prep Batch Method:
625.1 (Prep)
Analysis
Method:
625.1
Analysis
Description:
625.1
- Base/Neutrals and Acids by GC/MS
Laboratory Control Sample & LCSD
LCS-V28891
LCSD-V28891
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
2,6-Dinitrotoluene
pg/L
50.0
38.9
41.8
77.8
83.6
50-158
7.1
20.0
Di-n-Octyl Phthalate
pg/L
50.0
31.6
33.9
63.2
67.8
10-146
7.0
20.0
Fluoranthene
pg/L
50.0
35.4
37.3
70.8
74.6
26-137
5.2
20.0
Fluorene
pg/L
50.0
37.4
40.2
74.8
80.4
59-121
7.2
20.0
Hexachlorobenzene
pg/L
50.0
38.9
41.3
77.8
82.6
10-152
5.9
20.0
Hexachlorobutadiene
pg/L
50.0
27.6
29.6
55.2
59.2
24-116
6.9
20.0
Hexachlorocyclopentadiene
pg/L
50.0
24.7
28.4
49.4
56.8
32-117
13.9
20.0
Hexachloroethane
pg/L
50.0
28.0
28.0
56.0
56.0
40-113
0.0
20.0
Indeno(1,2,3-cd)pyrene
pg/L
50.0
29.9
31.3
59.8
62.6
10-171
4.5
20.0
Isophorone
pg/L
50.0
20.2
21.8
40.4
43.6
21-196
7.6
20.0
1-Methylnaphthalene
pg/L
50.0
28.4
31.5
56.8
63.0
40-135
10.3
20.0
2-Methylnaphthalene
pg/L
50.0
28.5
30.9
57.0
61.8
18-121
8.0
20.0
Naphthalene
pg/L
50.0
27.4
29.2
54.8
58.4
21-133
6.3
20.0
Nitrobenzene
pg/L
50.0
26.2
28.2
52.4
56.4
35-180
7.3
20.0
2-Nitrophenol
pg/L
50.0
28.3
30.6
56.6
61.2
29-182
7.8
20.0
4-Nitrophenol
pg/L
50.0
17.2
17.6
34.4
35.2
10-132
2.2
20.0
N-Nitrosodiphenylamine
pg/L
50.0
45.3
48.1
90.6
96.2
69-152
5.9
20.0
N-Nitroso-di-n-propylamine
pg/L
50.0
31.2
34.1
62.4
68.2
10-230
8.8
20.0
Pentachlorophenol
pg/L
50.0
45.9
47.8
91.8
95.6
14-176
4.0
20.0
Phenanthrene
pg/L
50.0
38.1
40.8
76.2
81.6
54-120
6.8
20.0
Phenol
pg/L
50.0
13.6
13.9
27.2
27.8
10-112
2.1
20.0
Pyrene
pg/L
50.0
37.3
40.7
74.6
81.4
52-115
8.7
20.0
1,2,4-Trichlorobenzene
pg/L
50.0
27.0
28.9
54.0
57.8
44-142
6.7
20.0
2,4,6-Trichlorophenol
pg/L
50.0
34.9
39.3
69.8
78.6
37-144
11.8
20.0
2-Fluorobiphenyl (S)
70.8
75.6
49-118
2-Fluorophenol(S)
34.2
34.1
22-84
Date: 01/19/2023 05:38 PM
Page 23 of 30
Page 109
of 118
Waypointo
ANALYTICAL
Client ID: S&ME, Inc - Charlotte
Project Description: Jefferson Pilot Comm
Report No: 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypoi ntana lytica l.com
Quality Control Data
QC Prep: V28891 QC Analytical Batch(es): V29017
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Laboratory Control Sample & LCSD LCS-V28891 LCSD-V28891
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD
Nitrobenzene-d5 (S)
4-Terphenyl-d14 (S)
2,4,6-Tribromophenol (S)
Phenol-d5 (S)
53.8
56.2
43-123
78.2
83.8
49-151
71.1
74.1
31-144
23.8
24.0
10-63
Date: 01/19/2023 05:38 PM
Page 110 of 118
Page 24 of 30
Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
S&ME, Inc - Charlotte
Jefferson Pilot Comm
23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V28943 QC Analytical Batch(es): V29002
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Lab Reagent Blank LRB-V28943 Matrix: AQU
Associated Lab Samples: 97326, 97327, 97328, 97329, 97330, 97331, 97332
Parameter
Blank MDL MQL
Units Result
Analyzed a/o % Rec
Recovery Limits
Acenaphthene
pg/L
<0.302
0.302
2.00
01/18/23 16:31
Acenaphthylene
pg/L
<0.297
0.297
2.00
01/18/23 16:31
Anthracene
pg/L
<0.836
0.836
2.00
01/18/23 16:31
Benzidine
pg/L
<1.32
1.32
10.0
01/18/23 16:31
Benzo(a)anthracene
pg/L
<0.637
0.637
2.00
01/18/23 16:31
Benzo(a)pyrene
pg/L
<1.02
1.02
2.00
01/18/23 16:31
Benzo(b)fluoranthene
pg/L
<2.49
2.49
5.00
01/18/23 16:31
Benzo(g,h,i)perylene
pg/L
<1.01
1.01
5.00
01/18/23 16:31
Benzo(k)fluoranthene
pg/L
<1.99
1.99
5.00
01/18/23 16:31
Benzoic Acid
pg/L
<1.10
1.10
10.0
01/18/23 16:31
Benzyl alcohol
pg/L
<0.684
0.684
5.00
01/18/23 16:31
Bis(2-Chloroethoxy)methane
pg/L
<0.468
0.468
5.00
01/18/23 16:31
Bis(2-Chloroethyl)ether
pg/L
< 1.04
1.04
5.00
01/18/23 16:31
Bis(2-Chloroisopropyl)ether
pg/L
<1.08
1.08
5.00
01/18/23 16:31
Bis(2-ethylhexyl)phthalate
pg/L
<24.0
24.0
50.0
01/18/23 16:31
4-Bromophenyl phenyl ether
pg/L
<1.11
1.11
5.00
01/18/23 16:31
Butyl benzyl phthalate
pg/L
<1.83
1.83
5.00
01/18/23 16:31
4-Chloro-3-methyl phenol
pg/L
<1.18
1.18
5.00
01/18/23 16:31
2-Chloronaphthalene
pg/L
<7.38
7.38
20.0
01/18/23 16:31
2-Chlorophenol
pg/L
<0.938
0.938
10.0
01/18/23 16:31
4-Chlorophenyl phenyl ether
pg/L
<1.71
1.71
5.00
01/18/23 16:31
Chrysene
pg/L
<0.405
0.405
2.00
01/18/23 16:31
Dibenz(a,h)anthracene
pg/L
<0.434
0.434
2.00
01/18/23 16:31
Dibenzofuran
pg/L
<0.856
0.856
5.00
01/18/23 16:31
1,2-Dichlorobenzene
pg/L
<2.00
2.00
5.00
01/18/23 16:31
1,3-Dichlorobenzene
pg/L
<2.00
2.00
5.00
01/18/23 16:31
1,4-Dichlorobenzene
pg/L
<2.05
2.05
5.00
01/18/23 16:31
Date: 01/19/2023 05:38 PM Page 25 of 30
Page 111 of 118
Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
S&ME, Inc - Charlotte
Jefferson Pilot Comm
23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V28943 QC Analytical Batch(es): V29002
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Lab Reagent Blank LRB-V28943 Matrix: AQU
Associated Lab Samples: 97326, 97327, 97328, 97329, 97330, 97331, 97332
Parameter
Blank MDL MQL
Units Result
Analyzed a/o % Rec
Recovery Limits
3,3'-Dichlorobenzidine
pg/L
<1.89
1.89
5.00
01/18/23 16:31
2,4-Dichlorophenol
pg/L
<1.46
1.46
10.0
01/18/23 16:31
Diethyl phthalate
pg/L
<0.745
0.745
5.00
01/18/23 16:31
Dimethyl phthalate
pg/L
<0.939
0.939
5.00
01/18/23 16:31
2,4-Dimethylphenol
pg/L
<1.57
1.57
20.0
01/18/23 16:31
Di-n-butyl phthalate
pg/L
<2.06
2.06
5.00
01/18/23 16:31
4,6- Din itro-2-methylphenol
pg/L
<2.07
2.07
10.0
01/18/23 16:31
2,4-Dinitrophenol
pg/L
<1.92
1.92
10.0
01/18/23 16:31
2,4-Dinitrotoluene
pg/L
<1.11
1.11
5.00
01/18/23 16:31
2,6-Dinitrotoluene
pg/L
<0.809
0.809
5.00
01/18/23 16:31
Di-n-Octyl Phthalate
pg/L
<1.65
1.65
5.00
01/18/23 16:31
Fluoranthene
pg/L
<0.250
0.250
2.00
01/18/23 16:31
Fluorene
pg/L
<0.807
0.807
2.00
01/18/23 16:31
Hexachlorobenzene
pg/L
<0.979
0.979
5.00
01/18/23 16:31
Hexachlorobutadiene
pg/L
<2.73
2.73
5.00
01/18/23 16:31
Hexachlorocyclopentadiene
pg/L
<2.05
2.05
5.00
01/18/23 16:31
Hexachloroethane
pg/L
<1.76
1.76
5.00
01/18/23 16:31
Indeno(1,2,3-cd)pyrene
pg/L
<0.477
0.477
2.00
01/18/23 16:31
Isophorone
pg/L
<0.444
0.444
5.00
01/18/23 16:31
1-Methylnaphthalene
pg/L
<1.14
1.14
2.00
01/18/23 16:31
2-Methylnaphthalene
pg/L
<0.666
0.666
2.00
01/18/23 16:31
Naphthalene
pg/L
<0.728
0.728
2.00
01/18/23 16:31
Nitrobenzene
pg/L
<0.905
0.905
5.00
01/18/23 16:31
2-Nitrophenol
pg/L
<0.493
0.493
5.00
01/18/23 16:31
4-Nitrophenol
pg/L
<1.23
1.23
10.0
01/18/23 16:31
N-Nitrosodiphenylamine
pg/L
<1.10
1.10
5.00
01/18/23 16:31
N-Nitroso-di-n-propylamine
pg/L
<0.641
0.641
5.00
01/18/23 16:31
Date: 01/19/2023 05:38 PM Page 26 of 30
Page 112 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28943
QC Analytical Batch(es): V29002
QC Prep Batch Method:
625.1 (Prep)
Analysis Method:
625.1
Analysis Description:
625.1 - Base/Neutrals and Acids by GC/MS
Lab Reagent Blank
LRB-V28943
Matrix: AQU
Associated Lab Samples:
97326, 97327, 97328,
97329,
97330, 97331, 97332
Blank
MDL
MQL
Analyzed
a/o
% Rec
Parameter
Units
Result
Recovery
Limits
Pentachlorophenol
pg/L
<1.43
1.43
5.00
01/18/23 16:31
Phenanthrene
pg/L
<0.428
0.428
2.00
01/18/23 16:31
Phenol
pg/L
<0.651
0.651
5.00
01/18/23 16:31
Pyrene
pg/L
<0.434
0.434
2.00
01/18/23 16:31
1,2,4-Trichlorobenzene
pg/L
<2.21
2.21
5.00
01/18/23 16:31
2,4,6-Trichlorophenol
pg/L
<1.32
1.32
5.00
01/18/23 16:31
2-Fluorobiphenyl (S)
01/18/23 16:31
66.4
49-118
2-Fluorophenol (S)
01/18/23 16:31
36.7
22-84
Nitrobenzene-d5 (S)
01/18/23 16:31
59.0
43-123
4-Terphenyl-d14 (S)
01/18/23 16:31
78.0
49-151
2,4,6-Tribromophenol (S)
01/18/23 16:31
72.0
31-144
Phenol-d5 (S)
01/18/23 16:31
26.1
10-63
Laboratory Control Sample & LCSD
Parameter Units
LCS-V28943
Spike
Conc.
LCSD-V28943
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
a/o Rec
Limits
RPD
Max
RPD
Acenaphthene
pg/L
50.0
36.5
35.7
73.0
71.4
47-145
2.2
20.0
Acenaphthylene
pg/L
50.0
35.6
35.4
71.2
70.8
33-145
0.5
20.0
Anthracene
pg/L
50.0
40.3
40.8
80.6
81.6
27-133
1.2
20.0
Benzidine
pg/L
50.0
27.9
19.4
55.8
38.8
15-150
35.9*
20.0
Benzo(a)anthracene
pg/L
50.0
39.4
40.7
78.8
81.4
33-143
3.2
20.0
Benzo(a)pyrene
pg/L
50.0
48.8
50.1
97.6
100
17-163
2.6
20.0
Benzo(b)fluoranthene
pg/L
50.0
44.9
46.6
89.8
93.2
24-159
3.7
20.0
Benzo(g,h,i)perylene
pg/L
50.0
41.8
43.0
83.6
86.0
10-219
2.8
20.0
Benzo(k)fluoranthene
pg/L
50.0
43.9
45.0
87.8
90.0
11-162
2.4
20.0
Benzoic Acid
pg/L
50.0
11.3
14.3
22.6
28.6
10-125
23.4*
20.0
* QC Fail Date: 01/19/2023 05:38 PM Page 27 of 30
Page 113 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28943
QC Analytical Batch(es): V29002
QC Prep Batch Method:
625.1 (Prep)
Analysis
Method:
625.1
Analysis
Description:
625.1
- Base/Neutrals and Acids by GC/MS
Laboratory Control Sample & LCSD
LCS-V28943
LCSD-V28943
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits RPD
Max
RPD
Benzyl alcohol
pg/L
50.0
29.5
27.6
59.0
55.2
16-107
6.6
20.0
Bis(2-Chloroethoxy)methane
pg/L
50.0
29.8
28.2
59.6
56.4
33-184
5.5
20.0
Bis(2-Chloroethyl)ether
pg/L
50.0
25.6
23.4
51.2
46.8
12-158
8.9
20.0
Bis(2-Chloroisopropyl)ether
pg/L
50.0
29.2
26.4
58.4
52.8
36-166
10.0
20.0
Bis(2-ethylhexyl)phthalate
pg/L
50.0
41.3
42.1
82.6
84.2
10-158
1.9
20.0
4-Bromophenyl phenyl ether
pg/L
50.0
39.7
39.5
79.4
79.0
53-127
0.5
20.0
Butyl benzyl phthalate
pg/L
50.0
41.1
42.6
82.2
85.2
10-152
3.5
20.0
4-Chloro-3-methylphenol
pg/L
50.0
32.4
31.8
64.8
63.6
22-147
1.8
20.0
2-Chloronaphthalene
pg/L
50.0
34.5
33.5
69.0
67.0
60-118
2.9
20.0
2-Chlorophenol
pg/L
50.0
26.3
24.2
52.6
48.4
23-134
8.3
20.0
4-Chlorophenyl phenyl ether
pg/L
50.0
38.7
38.3
77.4
76.6
25-158
1.0
20.0
Chrysene
pg/L
50.0
40.2
41.3
80.4
82.6
17-168
2.6
20.0
Dibenz(a,h)anthracene
pg/L
50.0
41.7
42.4
83.4
84.8
10-227
1.6
20.0
Dibenzofuran
pg/L
50.0
36.5
35.9
73.0
71.8
39-114
1.6
20.0
1,2-Dichlorobenzene
pg/L
50.0
25.4
23.3
50.8
46.6
32-129
8.6
20.0
1,3-Dichlorobenzene
pg/L
50.0
25.3
22.7
50.6
45.4
20-124
10.8
20.0
1,4-Dichlorobenzene
pg/L
50.0
24.2
22.5
48.4
45.0
20-124
7.2
20.0
3,3'-Dichlorobenzidine
pg/L
50.0
33.5
32.7
67.0
65.4
10-262
2.4
20.0
2,4-Dichlorophenol
pg/L
50.0
28.8
27.6
57.6
55.2
39-135
4.2
20.0
Diethyl phthalate
pg/L
50.0
40.5
41.1
81.0
82.2
10-114
1.4
20.0
Dimethyl phthalate
pg/L
50.0
39.4
39.3
78.8
78.6
10-112
0.2
20.0
2,4-Dimethylphenol
pg/L
50.0
32.0
30.3
64.0
60.6
32-119
5.4
20.0
Di-n-butyl phthalate
pg/L
50.0
43.6
44.4
87.2
88.8
10-118
1.8
20.0
4,6- Din itro-2-methylphenol
pg/L
50.0
40.6
39.5
81.2
79.0
10-181
2.7
20.0
2,4-Dinitrophenol
pg/L
50.0
43.1
44.0
86.2
88.0
10-191
2.0
20.0
2,4-Dinitrotoluene
pg/L
50.0
41.5
42.2
83.0
84.4
39-139
1.6
20.0
Date: 01/19/2023 05:38 PM Page 28 of 30
Page 114 of 118
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
S&ME, Inc - Charlotte
Project Description:
Jefferson Pilot Comm
Report No:
23-011-0018
QC Prep:
V28943
QC Analytical Batch(es): V29002
QC Prep Batch Method:
625.1 (Prep)
Analysis
Method:
625.1
Analysis
Description:
625.1
- Base/Neutrals and Acids by GC/MS
Laboratory Control Sample & LCSD
LCS-V28943
LCSD-V28943
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
2,6-Dinitrotoluene
pg/L
50.0
40.9
40.1
81.8
80.2
50-158
1.9
20.0
Di-n-Octyl Phthalate
pg/L
50.0
45.0
45.2
90.0
90.4
10-146
0.4
20.0
Fluoranthene
pg/L
50.0
40.7
41.4
81.4
82.8
26-137
1.7
20.0
Fluorene
pg/L
50.0
39.2
38.4
78.4
76.8
59-121
2.0
20.0
Hexachlorobenzene
pg/L
50.0
39.4
40.2
78.8
80.4
10-152
2.0
20.0
Hexachlorobutadiene
pg/L
50.0
24.9
23.7
49.8
47.4
24-116
4.9
20.0
Hexachlorocyclopentadiene
pg/L
50.0
20.8
20.1
41.6
40.2
32-117
3.4
20.0
Hexachloroethane
pg/L
50.0
24.1
21.5
48.2
43.0
40-113
11.4
20.0
Indeno(1,2,3-cd)pyrene
pg/L
50.0
41.7
42.8
83.4
85.6
10-171
2.6
20.0
Isophorone
pg/L
50.0
22.2
21.8
44.4
43.6
21-196
1.8
20.0
1-Methylnaphthalene
pg/L
50.0
29.7
28.4
59.4
56.8
40-135
4.4
20.0
2-Methylnaphthalene
pg/L
50.0
28.1
27.2
56.2
54.4
18-121
3.2
20.0
Naphthalene
pg/L
50.0
26.6
25.0
53.2
50.0
21-133
6.2
20.0
Nitrobenzene
pg/L
50.0
27.1
25.8
54.2
51.6
35-180
4.9
20.0
2-Nitrophenol
pg/L
50.0
26.6
24.7
53.2
49.4
29-182
7.4
20.0
4-Nitrophenol
pg/L
50.0
17.9
17.8
35.8
35.6
10-132
0.5
20.0
N-Nitrosodiphenylamine
pg/L
50.0
48.8
47.7
97.6
95.4
69-152
2.2
20.0
N-Nitroso-di-n-propylamine
pg/L
50.0
30.5
28.4
61.0
56.8
10-230
7.1
20.0
Pentachlorophenol
pg/L
50.0
46.8
47.3
93.6
94.6
14-176
1.0
20.0
Phenanthrene
pg/L
50.0
40.6
41.0
81.2
82.0
54-120
0.9
20.0
Phenol
pg/L
50.0
12.3
11.3
24.6
22.6
10-112
8.4
20.0
Pyrene
pg/L
50.0
40.4
41.5
80.8
83.0
52-115
2.6
20.0
1,2,4-Trichlorobenzene
pg/L
50.0
25.7
23.6
51.4
47.2
44-142
8.5
20.0
2,4,6-Trichlorophenol
pg/L
50.0
36.7
34.5
73.4
69.0
37-144
6.1
20.0
2-Fluorobiphenyl (S)
68.0
64.6
49-118
2-Fluorophenol(S)
34.1
29.0
22-84
Date: 01/19/2023 05:38 PM
Page 29 of 30
Page 115
of 118
Waypointo
ANALYTICAL
Client ID: S&ME, Inc - Charlotte
Project Description: Jefferson Pilot Comm
Report No: 23-011-0018
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypoi ntana lytica l.com
Quality Control Data
QC Prep: V28943 QC Analytical Batch(es): V29002
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Laboratory Control Sample & LCSD LCS-V28943 LCSD-V28943
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD
Nitrobenzene-d5 (S)
4-Terphenyl-d14 (S)
2,4,6-Tribromophenol (S)
Phenol-d5 (S)
52.2
47.8
43-123
82.0
82.8
49-151
76.9
76.4
31-144
23.6
21.4
10-63
Date: 01/19/2023 05:38 PM
Page 116 of 118
Page 30 of 30
WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01176
Customer Name: S&ME, Inc - Charlotte
Report Number: 23-011-0018
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IRT15 2.3C
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample Iabel(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
U Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
U Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
* No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
U N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: ngelo Norvell Date & Time: 01/11/2023 16:20:47
Page 117 of 118
G
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Page 118 of 118
Appendix V— Waste Manifest
NONHAZARDOUS
I Generator 10 Number
2 Page 1 of
3. Emergency Response Phone
4. Waste Tracking Number
1
WASTE MANIFEST
1
T04 273-1500
2 5$ 2 6
5 Generators Name and Mailing Address
Generators Site Address (if differeril Ehan mailing address)
jeftsort Pilot
1 Julian P'rlce Place
Charlotte NC 28208
Generators Phone
6 Transporter 1 Company Name
US EPA ID Number
Contaminant Control. INC.
N C R 0 0 0 1
7 5 0 4 2
7 Transporter 2 Company Name
U S. EPA ID Number
8 Desi Hated Faalily Name and Site Address
ct�l 5wironrmrftucwr
US EPA ID Number
708 Martin LutherKing JR Drive
Thomtsvllle NC 27360
Faala s P one
N C R 0 0 0 1
7 5 0 4 2
9 Waste Shipping Name and Descapeon
10 Cont! a ners
11 Total
Unit
Na
Type
Duantily
Wit
WtNol.
'Non -Hazardous Material N.O.S. (Petroleum Contact V%ter)
0
t-
0 0 1
'L
G
w
z
W
2
Q
3
4
13. Special Handling Instructions and Addaicnal InilDminon
14. GFNERATOR'S70FFEROR S CERTIFICATIONi I hereby dedam that the Opnlenls of this
consignment are fully and accurately described above by the proper shipping name, and are classified, packaged,
marked and labeledtplararded, and are in a31 respects in groper condition Ior transport aceoi to appficaUe International and ralie al govemmenlal regulations
Ge eaiors tferors nledliyped N e � /
Lahit�
Signature
Month Day Year
Y .1 ., �/e
.5"
j
f Vniamarional Shipmerds ❑ Import to U.S. ❑ Export from U,S Porto) entryleol.
Z
Transporter Si narare (for exports only)
Date leaving US-.
16. Transporter Acknowledgment of Receipt of Materals
ogle I PnrdedTyped ame
Signature
Month Da Year
y
!L 2
aTransporter
2 P mted7yned Name
turn
Month Day Yew
It
17 Discreparicy
17a Discrepancy Indication Space
0uantiry El Type
❑ Residue ❑ Partial Reteokon
❑ Fug Rejection
Manifest Reference Number
r
17b Alternate F=hty (or Generator)
U.S EPA 1D Number
J
U
ii
Faraldy's Phone
h17c
SgnaMe of Af male Factory (or Generator)
Month Day Year
Z
Q
N
ul
O
18 DemgWed Fx" Ovi—er or Operator Ceriralilon of rece;pl 01 ma!enats Covered by the mai Except as rotes in Item 17a
PmdsdTyped Nara
I
Signature
Month Day Year
169-BBC-0 6 10498 (Rev. 9109) DESIGNATED FACILITY TO GENERATOR
Beverly, Trudy
From: Laura Beth Slagle <Islagle@smeinc.com>
Sent: Wednesday, March 1, 2023 10:55 AM
To: Beverly, Trudy
Cc: Lucas Barroso-Giachetti
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Sounds good, thanks!
Laura Beth "LB" Slagle H
Environmental Staff Professional
S&ME
2016 Ayrsley Town Blvd., Suite 2-A, Charlotte, NC 28273
M:828.779.4973 H 0:704.523.4726
www.smeinc.com
From: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Sent: Wednesday, March 1, 2023 10:45 AM
To: Laura Beth Slagle <Islagle@smeinc.com>
Cc: Lucas Barroso-Giachetti <Ibarroso@smeinc.com>
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
This message originated outside of S&ME. Please report this as phishing if it implies it is from an S&ME employee.
I'll get the report reviewed within the next couple of weeks and get a response back to you.
Have a great day,
Trudy
, � �d� D.. Q -i-�
rH era
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everly(a) ncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httDs://deu.nc. eov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaeement-eis-mans
File Review Procedures:
htt 2s:Hdeg.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
httns://dea.nc. eov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.aov/nedea/Waste%2OMana2ement/DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policv.l)df
htips://files.nc. gov/ncdeq/Wastc%2OManagementlDWM/UST/Corrective°/`2OAction/UST%20file%20names%20for%2OLaserfiche. docx
From: Laura Beth Slagle <Islagle@smeinc.com>
Sent: Wednesday, March 1, 2023 10:38 AM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Cc: Lucas Barroso-Giachetti <Ibarroso@smeinc.com>
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Thanks Trudy,
I am still a little new with this project. Do we need to wait until we get the NORR to submit a new TA for the next period?
Thanks,
Laura Beth
Laura Beth "LB" Slagle H
Environmental Staff Professional
S&ME
2016 Ayrsley Town Blvd., Suite 2-A, Charlotte, NC 28273
M:828.779.4973 H 0:704.523.4726
www.smeinc.com
From: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Sent: Wednesday, March 1, 2023 6:31 AM
To: Lucas Barroso-Giachetti <Ibarroso@smeinc.com>
Cc: Laura Beth Slagle <Islagle@smeinc.com>
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
This message originated outside of S&ME. Please report this as phishing if it implies it is from an S&ME employee.
Received.
Trudy
D E Q
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
hops://deq.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-maps
File Review Procedures:
hit 2s:Hdeq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hitps://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.aov/nedeci/Waste%2OMana2ement/DWMIUST/WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
https:Hfiles.nc. gov/ncdeq/Waste%2OManagement/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Lucas Barroso-Giachetti <Ibarroso@smeinc.com>
Sent: Tuesday, February 28, 2023 6:07 PM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Cc: Laura Beth Slagle <Islagle@smeinc.com>
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Good afternoon Trudy,
Please find the attached Groundwater Monitoring and Free Product Recovery Report for the Jefferson Pilot site in
Charlotte for your review.
Please let us know if you have any questions.
Thank you!
Lucas
Lucas Barroso-Giachetti, PE, CHMM
Senior Environmental Engineer
Registered PE in NC, SC and FL
- S&ME
• 2016 Ayrsley Town Blvd., Suite 2-A
- Charlotte, NC 28273 map
III M: 786.877.4363 H 0: 704.523.4726
www.smeinc.com
Linkedln // Twitter // Facebook
This electronic message is subject to the terms of use set forth at www.smeinc.com/email. If you received this message in error, please advise the sender
by reply and delete this electronic message and any attachments. Please consider the environment before printing this email.
From: Laura Beth Slagle <lslagle@smeinc.com>
Sent: Wednesday, August 17, 2022 1:13 PM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Cc: Lucas Barroso-Giachetti <lbarroso@smeinc.com>
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
Thanks Trudy,
I appreciate your help and the extension.
Best,
Laura Beth
Laura Beth "LB" Slagle
Environmental Staff Professional
she/her
S&ME
2016 Ayrsley Town Blvd. Suite 2-A
Charlotte, NC 28273 map
M: 828.779.4973
www.smeinc.com
Linkedln I Twitter I Facebook
OUILT raw
VER SAT 1 LI T T
This electronic message is subject to the terms of use set forth at www.smeinc.com/email. If you received this message in error please advise the sender
by reply and delete this electronic message and any attachments. Please consider the environment before printing this email.
From: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Sent: Wednesday, August 17, 2022 1:09 PM
To: Laura Beth Slagle <Islagle@smeinc.com>
Cc: Lucas Barroso-Giachetti <lbarroso@smeinc.com>
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
This message originated outside of S&ME. Please report this as phishing if it implies it is from an S&ME employee.
Thank you, Laura Beth. Extension granted. The next report is due no later than February 28, 2023.
Have a great day,
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudv. B everlv(&,ncdenr. ilov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deg.nc.aov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httDs://dea.nc.xov/about/divisions/waste-management/waste-management-rules-data/waste-management-xis-mans
File Review Procedures:
hns://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
httDs://deo.nc. eov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
htti)s:Hfiles.nc.¢ov/ncdeci/Waste%2OManaizement/DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policv.ndf
https:Hfiles.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%2Ofile%20names%20for%2OLaserf che. docx
From: Laura Beth Slagle <Islagle@smeinc.com>
Sent: Wednesday, August 17, 2022 1:03 PM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Cc: Lucas Barroso-Giachetti <Ibarroso@smeinc.com>
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Trudy,
Per the NORR, work was to be completed by October 2022, but our typical monitoring schedule is 6 months. I asked in
an email to you in July 2022 (prior to the submittal of TA-25) if we would have to fit all our work in over a few months or
if we would we have the full 6 months to get the work completed and have the report over to you sometime in
January/February of 2023.
You responded that we could request an extension if the TA were approved as long as we had an appropriate reason.
The reasoning being: this project has switched project managers 3 times over the last year and no work has been
conducted at Jefferson Pilot since fall of last year when the original project manager (David Loftis) left S&ME. I believe in
order to submit a representative monitoring report we need the 6-month period to monitor the groundwater and free
product after the AFVR event (which is happening today).
Let me know if you have any questions.
Thanks,
Laura Beth
Laura Beth "LB" Slagle
Environmental Staff Professional
she/her
i-MLVA10
2016 Ayrsley Town Blvd. Suite 2-A
Charlotte, NC 28273 map
M: 828.779.4973
www.smeinc.com
Linkedln I Twitter I Facebook
BUILT FOR
WERSATIL1 TY
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by reply and delete this electronic message and any attachments. Please consider the environment before printing this email.
From: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Sent: Wednesday, August 17, 2022 12:25 PM
To: Laura Beth Slagle <Islagle@smeinc.com>
Cc: Lucas Barroso-Giachetti <Ibarroso@smeinc.com>
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
This message originated outside of S&ME. Please report this as phishing if it implies it is from an S&ME employee.
Hey Laura Beth,
Remind me of the issues prompting the extension request and the time frame.
Thank you,
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
WN � ft. UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: hops://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: hops://deg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
hops://deg.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-mana eg ment- ig s=maps
File Review Procedures:
hops: //deg.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
fts://deq.nc.gov/about/divisions/waste-manamement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
htti)s:Hfiles.nc.¢ov/ncdea/Waste%2OManaizement/DWMIUST/W hatsNew/Final-Electronic-Document-Submittal-Policv.adf
https:Hfiles.nc. gov/ncdeq/Waste%20ManagementlDWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Laura Beth Slagle <Islagle@smeinc.com>
Sent: Wednesday, August 17, 2022 11:43 AM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Cc: Lucas Barroso-Giachetti <Ibarroso@smeinc.com>
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Hi Trudy,
What do we need to do formally to request the extension we discussed on this project?
Thank you,
Laura Beth
Laura Beth "LB" Slagle
Environmental Staff Professional
she/her
S&ME
2016 Ayrsley Town Blvd. Suite 2-A
Charlotte, NC 28273 map
M: 828.779.4973
IIIIIIIIIIIIF www.smeinc.com
Linkedln I Twitter I Facebook
BUILT r9H
VCHSATIL1 TT
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by reply and delete this electronic message and any attachments. Please consider the environment before printing this email.
From: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Sent: Wednesday, July 27, 2022 10:08 AM
To: Laura Beth Slagle <Islagle@smeinc.com>
Cc: Lucas Barroso-Giachetti <Ibarroso@smeinc.com>; Michael Gurthie <michael.gurthie@wbtv.com>
Subject: RE: [External] Jefferson Pilot ePATA 7570, TA-25
This message originated outside of S&ME. Please report this as phishing if it implies it is from an S&ME employee.
Please see the attached Preapproval Task Authorization Form (7570-25) for Jefferson Pilot Communications-WBTV
located in Charlotte, Mecklenburg County, North Carolina. The form should be signed and emailed to the UST Section's
Trust Fund Branch at ncTrustFundEPATA@ncdenr.gov. The ncTrustFundEPATA@ncdenr.gov email can be accessed by
anyone working on ePATA approval process in Trust Fund. "Preapproval is not valid (i.e., claimable) until receipt is
'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature indicates
agreement with the tasks and amounts approved. Any objections or appeals must be submitted via Change Order prior
to work proceeding. Scope/cost negotiations do not supersede other regulatory deadlines. Also, any ePATA that has
been signed as 'Confirmed' by both the UST Section and RP is not to be modified without written consent by all
signatories. Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules,
statutes, and RRD Task Scopes of Work to be reimbursed in full." If you have any questions, please call me at (704) 235-
2182 or email mail me at Trudy.Beverly@ncdenr.gov or Thomas Chapman at (919) 707-8170 and
Thomas.Chapman@ncdenr.gov.
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
z!5:fD,EW North Carolina Department of Environmental Quality
NoR r" iINA UST Section, Mooresville Regional Office
at 4�+ar�
704.235.2182 (Office)
Trudy. B everlykncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://dea.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
htti)s:Hfiles.nc.¢ov/ncdeci/Waste%2OManaizement/D WM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policv.ndf
https:Hfiles.nc. gov/ncdeq/Waste%20Management/D WM/UST/Corrective%2OAction/UST°/n20file%20names%20for%2OLaserfiche. docx
From: Laura Beth Slagle <Islagle@smeinc.com>
Sent: Tuesday, July 26, 2022 5:29 PM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Cc: Lucas Barroso-Giachetti <Ibarroso@smeinc.com>; Michael Gurthie <michael.gurthie@wbtv.com>
Subject: [External] Jefferson Pilot ePATA 7570, TA-25
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Hey Trudy,
Attached is the ePATA for Jefferson Pilot, Incident #7570, TA-25. As mentioned in previous emails, we are proposing an
AFVR event per our recommendations in the last monitoring report submitted on 10/20/21.
Pending approval, we plan to request an extension for this scope as the NORR, dated 3/14/22, requests the
monitoring/recovery report is due no later than October 31, 2022.
Also of importance, Lucas Barroso-Giachetti is the new project manager for this site. Mike Gurthie is still the site contact
at WBTV. Both Cc'd.
Let us know if you have any questions.
Thanks,
Laura Beth
Laura Beth "LB" Slagle
Environmental Staff Professional
she/her
S&ME
2016 Ayrsley Town Blvd. Suite 2-A
Charlotte, NC 28273 map
M: 828.779.4973
www.smeinc.com
Linkedln I Twitter I Facebook
BUILT roll
VCR SAT 1LI TT
This electronic message is subject to the terms of use set forth at www.smeinc.com/email. If you received this message in error please advise the sender
by reply and delete this electronic message and any attachments. Please consider the environment before printing this email.