AS-3731_28861_CA_MRP_20240206

JANUARY 2024
GROUNDWATER
MONITORING REPORT

for the
ONE STOP #15 146 Wiggins Road Candler, Buncombe County, North Carolina Incident #28861

PREPARED FOR: Samir Enterprises, LLC.
PO Box 1272 Old Fort, NC 28762 PREPARED BY: Singleton Environmental, Inc. PO Box 604 Fletcher, NC 28732 [phone]

February 6, 2024

Singleton Environmental, Inc.
Groundwater Monitoring Report One Stop #15 Candler, North Carolina

GROUNDWATER MONITORING REPORT
February 6, 2024 Incident Number: 28861
Site Name: One Stop #15
146 Wiggins Road Candler, NC 28715 Incident Number: 28861 Facility ID Number: 0-0021101
UST Responsible Party: Samir Enterprises, LLC. PO Box 1272 Old Fort, NC 28762
Consultant / Contractor: Singleton Environmental, Inc. PO Box 604 Fletcher, NC 28732 Telephone: [phone]
Date Release Discovered: June 6, 2012 Estimated Quantity of Release: Unknown/unquantified
Cause/Source of Release: Dispenser Islands

Latitude: 35.5432° North
Longitude: -82.7530° West
Signature and Seal of Certifying Professional Engineer: I, Christopher D. Singleton, a Professional Geologist, do certify that the information contained in this report is correct and accurate to the best of my knowledge.
Christopher D. Singleton, P.G. #1928

Groundwater Monitoring Report One Stop #15 Candler, North Carolina

Table of Contents
Introduction ................................................................................................................................. 1
Field Activities ............................................................................................................................. 1 Sampling Results ......................................................................................................................... 1 Monitoring Wells .................................................................................................................... 1 Water Supply Wells ................................................................................................................ 3
Groundwater Flow Direction ........................................................................................................ 3
Conclusions & Recommendations ................................................................................................ 3
Tables
Table 1. Groundwater Analytical Results Table 2. Groundwater Elevation Data Figures

Figure 1. Site Vicinity Map
Figure 2. Site Map Figure 3. Groundwater Analytical Results Figure 4. Groundwater Elevation Contour Map
Appendices Appendix A: Laboratory Analytical Report Appendix B: Field Notes
Groundwater Monitoring Report One Stop #15 Candler, North Carolina
1
Introduction
This report presents the results of the January 22, 2024, groundwater monitoring and sampling event conducted for the One Stop #15, located at 146 Wiggins Road in Candler, North Carolina.
Figure 1 is a USGS topographic map depicting the site location and vicinity with relevant topographic features. A total of eight monitoring wells on the subject property as depicted on Figure 2 and the site water supply well were sampled and are presented within this report.
Field Activities

On January 22, 2024, eight groundwater monitoring wells at the site were sampled which
included MW-1, MW-2, MW-4, MW-5, MW-6, MW-7, MW-8, and MW-9. Each well was sampled following a purge of approximately three (3) well volumes and allowing the well to equilibrate. A new, dedicated, disposable bailer with new cotton twine lanyard was used for sampling each well to prevent cross-contamination. The well head for MW-3 was full of
sediment and frozen debris and could not be sampled. The on-site water supply well (WSW-1) was also sampled following a 20-minute purge of the well at the spigot. Upon collection, each sample was transferred directly from the bailer or
spigot to the appropriate sample container provided by the laboratory with Hydrochloric Acid
(HCl) preservative. The samples were stored on ice and delivered to Pace Analytical in
Asheville, North Carolina. All samples were submitted for laboratory analysis of Volatile Organics (VOCs) by method 6200B. A copy of the laboratory deliverable package is included as Appendix A of this report. Field measurements were also collected in the field upon sample collection which included temperature (Co), conductivity (uS/cm), pH (SU), and turbidity
(NTU). A copy of the field measurement data is included as Appendix B. Sampling Results Monitoring Wells
The January 22, 2024, analytical results from the One Stop #15 are as follows:
• Laboratory analysis of the groundwater samples collected from monitoring wells MW-
5, MW-6, and MW-7 did not detect petroleum hydrocarbons at concentrations that exceed their respective North Carolina 2L Groundwater Quality Standards (NCAC 2L MCLS).
• Laboratory analysis of the groundwater sample collected from monitoring MW-1R detected the following analytes in excess of the NCAC 2L Standards:

• Benzene – 965 micrograms per liter (ug/l)
• 1,2,4-Trimethylbenzene – 1,250 ug/l
• Ethylbenzene – 1,260 ug/l
Groundwater Monitoring Report One Stop #15 Candler, North Carolina
2
• MTBE – 94.7 ug/l
• Naphthalene – 483 ug/l
• Styrene – 84.2 ug/l
• Toluene – 2,860 ug/l
• M&P Xylenes – 3,310 ug/l
• O Xylenes – 2,180 ug/l
• N-Propylbenzene – 141 ug/l

• Laboratory analysis of the groundwater sample collected from monitoring MW-2 detected the following analytes in excess of the NCAC 2L Standards:
• Benzene – 529 ug/l
• 1,2 Dichloroethane – 2.4 ug/l
• MTBE – 144 ug/l
• Naphthalene – 29.4 ug/l
• Laboratory analysis of the groundwater sample collected from monitoring MW-4 detected the following analytes in excess of the NCAC 2L Standards:

• Benzene – 186 ug/l
• 1,2,4 Trimethylbenzene – 396 ug/l
• 1,2 Dibromoethane – 4.2 ug/l
• 1,2 Dichloroethane – 25.9 ug/l
• Chlorobenzene – 65.3 ug/l
• MTBE – 483 ug/l
• Naphthalene – 110 ug/l
• M&P Xylenes – 1,240 ug/l
• O Xylenes – 550 ug/l

• Laboratory analysis of the groundwater sample collected from monitoring MW-8 detected the following analytes in excess of the NCAC 2L Standards:
• Benzene – 16 ug/l
• Naphthalene – 606 ug/l

• Laboratory analysis of the groundwater sample collected from monitoring MW-9 detected the following analytes in excess of the NCAC 2L Standards:
• Naphthalene – 13 ug/l
None of the concentrations detected exceeded the corresponding GCLs. However, benzene and toluene exceeded 10x the NCAC 2B Standards in MW-1R, benzene in MW-2, and toluene in MW-4.
Groundwater Monitoring Report One Stop #15 Candler, North Carolina
3
No free product was observed in any wells during the assessment. Groundwater analytical results are summarized in Table 1 and depicted on Figure 3. A copy of the laboratory analytical
report is included as Appendix A.
Water Supply Wells
On January 22, 2024, water supply well WSW-1 was also sampled. The water supply well sample was analyzed for EPA Method 6200B. The sample did not contain any compounds
above the Pace Analytical Laboratory detection limits. A copy of the laboratory analytical report
is included as Appendix A.
Groundwater Flow Direction
The established groundwater flow direction at the site is to the southeast. The closest surface water is Georges Branch, which is located in a buried culvert approximately 95 feet west of the property boundary. Groundwater elevations are summarized in Table 2 and Figure 4 depicts groundwater flow direction.
Conclusions and Recommendations

The results of this investigation indicated that VOCs exceeded their corresponding NCAC 2L Standards in MW-1R, MW-2, MW-4, MW-8, and MW-9. Benzene and toluene were also detected in excess of 10x the NCAC 2B Standards. Therefore, Singleton Environmental, Inc. recommends continued quarterly monitoring of the on-site monitoring wells and site water supply well.

Tables
Constituent of Concern
1,2,3-Trichloropr
opane
1,2,4-Trimethylb
enzene
1,2-Dibromoet
hane (EDB)
1,2-Dichloroet
hane
1,3,5-Trimethylb
enzene
Benzene Chlorobenzene Diisopropyl
ether Ethylbenzene Isopropylbenzene
(Cumene)
MTBE Naphthalene Styrene Toluene m&p-
Xylene n-Butylbenzene n-Propylbenzene o-Xylene
Collected ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L
8/21/2023 ND 1550 ND ND 489 937 ND 36.7 1290 35.2 79 437 149 6300 5230 ND 114 2910
1/22/2024 ND 1250 ND ND 340 965 ND 47.4 1260 40.6 94.7 483 84.2 2860 3310 ND 141 2180
12/04/2019 ND 17.5 ND 1.9 6.8 198 ND 22.0 ND ND 85.8 8.5 ND 1.1 35.9 ND ND 31.3
11/5/2020 ND 5.3 ND ND 2.9 65.5 ND 5.2 0.58 ND 13.5 2.4 ND ND 10.3 ND ND 10.3
ND 15.3 ND 1.3 7 190 ND 23.1 ND ND 51 9.6 ND 1.3 35.5 ND ND 36.5
12/10/2021 ND 2.8 0.57 1.6 7.9 15.8 ND 31.2 ND 1 87.2 ND ND ND 7.6 ND ND 14.5
7/8/2022 ND 22.9 ND 1.7 11 279 ND 33.8 2.5 ND 78.3 14.5 ND 1.7 51.1 ND ND 57.4
8/21/2023 ND 11.9 ND 1.9 8.7 142 ND 36.8 0.65 0.91 71.6 6.1 ND 0.56 27.2 ND ND 33.6
1/22/2024 ND 31.3 ND 2.4 14.5 529 ND 41.5 10.2 ND 144 29.4 ND ND 76.5 ND ND 86.3
12/04/2019 ND 238 ND ND 49.9 21.4 ND 2.5 70.6 7.7 76.7 53.1 ND 250 310 ND 27.8 158
11/5/2020 ND 3 ND ND ND ND ND 0.97 1.1 ND 74 ND ND 2.7 4.6 ND ND 2.3
ND 0.68 ND ND ND ND ND 0.62 ND ND 42.4 ND ND ND ND ND ND 0.57
12/10/2021 ND 1.5 ND ND ND ND ND 1.2 ND ND 59.5 ND ND ND ND ND ND ND
ND ND ND ND ND ND ND 0.79 ND ND 53.8 ND ND ND ND ND ND ND
8/21/2023 ND ND ND ND ND ND ND 0.63 ND ND 44.5 ND ND ND ND ND ND ND
1/22/2024 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
ND 90.2 138 9.7 507 99.4 ND 551 1220 ND ND 625
11/5/2020 ND 644 17.4 47.1 ND 426 ND 124 267 18.2 720 181 ND 1380 2160 ND ND 1100
9/9/2021 ND 449 9 43.3 ND 332 ND 112 225 15.8 602 156 ND 1090 1580 ND ND 826
ND 449 7.9 19.3 ND 201 ND 52 180 14.8 299 165 ND 653 1350 ND ND 663
7/8/2022 ND 495 10.9 29.2 131 256 ND 93 208 15.4 534 137 ND 850 1760 ND 29 837
ND 784 2050 ND 38.1 904
1/22/2024 ND 396 4.2 25.9 112 186 65.3 88.2 141 12.2 483 110 ND 350 1240 ND 23.6 550
0.005 400 0.02 0.4 400 1 50 70 600 70 20 6 70 600 500 70 70 500
N/A N/A N/A N/A N/A 510 N/A N/A N/A N/A N/A N/A N/A 110 N/A N/A N/A N/A
N/A 28500 50 400 25000 5000 50000 70000 84500 25000 20000 6000 70000 260000 85500 6900 30000 85500
10 X NCAC 2B Standards
Sample ID
MW-1R
MW-2
MW-3
MW-4
Analytical Method
Constituent of
Concern
1,2,3-
Trichloropr
opane
1,2,4-
Trimethylb
enzene
1,2-
Dibromoe
thane
(EDB)
1,2-
hane
1,3,5-
Trimethylb
enzene
Benzene Diisopropyl
ether Ethylbenzene
Isopropylbe
nzene
(Cumene)
MTBE Naphthalene Styrene Toluene m&p-
Xylene n-Butylbenzene n-Propylbenzene o-Xylene
Collected ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L
12/04/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
11/5/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/9/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/10/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
7/8/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
8/21/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1/22/2024 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/04/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
11/5/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/9/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
8/21/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1/22/2024 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/04/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
11/5/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/9/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/10/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
7/8/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
8/21/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1/22/2024 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/04/2019 ND ND ND ND 72.9 34.2 3.8 35.7 16.9 10.2 87.7 ND 13.2 59.2 ND 47.7 202
11/5/2020 ND 90.6 ND ND 72.5 25.4 3.6 21.6 19.1 9.1 65.8 ND 5.1 54.8 ND 40.2 181
9/9/2021 ND 92.9 ND ND ND 24.3 4.4 29.6 19.4 9.4 97.6 ND 12.3 86 ND ND 201
12/10/2021 ND 54.4 ND ND 75.3 23.9 4.2 33.6 23.3 10.1 109 ND 10 33.4 26.8 56.6 250
7/8/2022 ND ND ND ND 65.7 18.6 3.4 25.3 23 7.7 91.7 ND 9.4 19.4 ND 46 194
8/21/2023 ND ND ND ND 62.5 22.7 4.2 60.2 27.4 8.3 97.1 ND 19.2 18.5 ND 69.5 186
1/22/2024 ND 32.7 ND ND 42.5 16 3.8 9.6 21.2 7.3 60.6 ND 4.7 14.7 ND 39 123
400 0.02 0.4 400 1 70 600 70 20 6 70 600 500 70 70 500
28500 50 400 25000 5000 70000 84500 25000 20000 6000 70000 260000 85500 6900 30000 85500
10 X NCAC 2B Standards
MW-6
MW-7
MW-8
Sample ID
MW-5
Analytical Method
Constituent of
Concern
1,2,3-
Trichloropr
opane
1,2,4-
Trimethylb
enzene
1,2-
Dibromoe
thane
(EDB)
1,2-
hane
1,3,5-
Trimethylb
enzene
Benzene Diisopropyl
ether Ethylbenzene
Isopropylbe
nzene
(Cumene)
MTBE Naphthalene Styrene Toluene m&p-
Xylene n-Butylbenzene n-Propylbenzene o-Xylene
Collected ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L
12/04/2019 ND 67.6 ND ND 21.7 ND ND 11.5 2.5 ND 9.2 ND 2.9 79.3 2.8 4.6 24.4
11/5/2020 ND 3.3 ND ND 2.3 ND ND ND ND ND ND ND ND ND 2 ND 0.57
9/9/2021 ND 42.3 ND ND 15.8 ND ND 0.54 1.6 ND 2.3 ND ND 21.7 2.5 ND 5.4
ND 179 ND ND 60.2 ND ND 11.4 5.8 ND 16.3 ND 1.7 151 12.1 6.6 46.7
ND 192 ND ND 68.6 ND ND 6 7.5 ND 22.8 ND 1.6 155 ND 5.3 53.9
ND 300 ND ND 102 ND ND 28.3 11 ND 27.2 1.3 4.6 351 ND 13.3 113
1/22/2024 ND 193 ND ND 80.1 ND ND 16.4 5.4 ND 13 0.77 2.4 229 ND 8.3 80.2
12/04/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
11/5/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/9/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
8/21/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1/22/2024 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
0.005 400 0.02 0.4 400 1 70 600 70 20 6 70 600 500 70 70 500
N/A N/A N/A N/A N/A 510 N/A N/A N/A N/A N/A N/A 110 N/A N/A N/A N/A
28500 50 400 25000 5000 70000 84500 25000 20000 6000 70000 260000 85500 6900 30000 85500
ug/L = micrograms per liter
MW-9
WSW-1
10 X NCAC 2B Standards
Analytical Method
Sample ID
Table 1
Summary of Analytical Results - Water Samples
ONE STOP #15
MW Number Date (screened interval)Top of Casing to Free Product to GW Depth Groundwater Elevation (ft)
8/21/2023 ND 22.85 75.51
12/4/2019 21.90 (0.1 Ft)22.00 76.69
11/5/2020 21.52 (1.5 Ft)23.02 75.679/9/2021 20.53 (0.25 Ft)20.78 77.9112/10/2021 22.27 (0.17 Ft)22.44 76.25
12/4/2019 ND 23.18 75.26
11/5/2020 ND 22.54 75.909/9/2021 ND 22.40 76.041210/22 ND 23.35 75.09
7/8/2022 ND 22.97 75.47
8/21/2023 ND 24.06 74.38
12/4/2019 ND 25.10 74.74
11/5/2020 ND 22.74 77.10
9/9/2021 ND 23.77 76.07
12/10/2022 ND 25.00 74.84
7/8/2022 ND 23.96 75.88
8/21/2023 ND 25.80 74.04
12/4/2019 ND 21.07 78.93
11/5/2020 ND 19.31 80.69
9/9/2021 ND 20.61 79.39
12/10/2022 ND 21.29 78.71
7/8/2022 ND 20.92 79.088/21/2023 ND 21.69 78.31
12/4/2019 ND 25.30 73.32
11/5/2020 ND 22.93 75.699/9/2021 ND 24.21 74.4112/10/2022 ND 25.33 73.29
7/8/2022 ND 24.56 74.06
8/21/2023 ND 26.07 72.55
12/4/2019 ND 25.28 74.82
11/5/2020 ND 23.48 76.62
9/9/2021 ND 25.00 75.10
12/10/2022 ND 26.05 74.05
7/8/2022 ND 24.81 75.29
8/21/2023 ND 26.79 73.31
MW-6 100.1 (10' to 30')
Table 2
Groundwater Flow Mapping Elevation Details
One Stop #15 - Nov-2020
Candler, NC
UST Incident # 28861
146 Wiggins Road
MW-1R 98.36 (12' to 27')
MW-2 98.44 (15' to 30')
MW-3 99.84 (15' to 30')
MW-1 98.69 (15' to 30')
MW-4 100 (15' to 30')
MW-5 98.62 (20' to 30')
12/4/2019 ND 20.05 79.98
11/5/2020 ND 19.94 80.09
9/9/2021 ND 19.68 80.35
12/10/2022 ND 20.32 79.71
7/8/2022 ND 20.00 80.038/21/2023 ND 20.80 79.23
12/4/2019 ND 21.45 77.02
11/5/2020 ND 18.75 79.72
9/9/2021 ND 20.26 78.2112/10/2022 ND 20.82 77.657/8/2022 ND 20.56 77.91
8/21/2023 ND 21.22 77.25
12/4/2019 ND 21.26 75.9011/5/2020 ND 19.25 77.91
9/9/2021 ND 21.26 75.90
12/10/2022 ND 22.14 75.02
7/8/2022 ND 21.93 75.23
8/21/2023 ND 22.54 74.62
8/22/2023 ND 22.54 74.62
MW-7 100.03 (10' to 30')
MW-8 98.47 (10' to 30')
MW-9 97.16 (10' to 30')

Figures
CANTON QUADRANGLE
NORTH CAROLINA
7.5 MINUTE SERIES (TOPOGRAPHIC)
Figure 1 Site Map
One Stop #15 – Candler, NC
Singleton Environmental, Inc
SB-1/MW-1 SB-3/MW-3
SB-2/MW-2
Current USTs
SB-4/MW-4
One Stop #15
WSW-1
SB-5/MW-5
SB-6/MW-6
SB-7/MW-7
SB-8/MW-8
SB-9/MW-9
Singleton Environmental, Inc
SB-1/MW-1 SB-3/MW-3
SB-2/MW-2
Current USTs
SB-4/MW-4 One Stop #15
WSW-1
SB-5/MW-5
SB-6/MW-6
SB-7/MW-7
SB-8/MW-8
SB-9/MW-9
78.98'
75.66'
74.38'
NM
78.14'
73.04'
73.24'
77.17'
74.53'
GW Flow

Groundwater samples collected on January 22, 2024.
4
Singleton Environmental, Inc
MW-1R
MW-3
MW-2
Previous USTs
MW-4
One Stop #15
WSW-1
MW-5
MW-6
MW-7
MW-8
MW-9
GW Exceeding 2L
GW Exceeding 10x2B

Appendix A

Field Notes

Appendix B

Laboratory Analytical Report

#=CL#
February 02, 2024
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92709767
92709767
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
One Stop 15 1/22/24
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on January 24, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc:Brian Bauer, Singleton Environmental
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 41
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 41
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92709767001 MW-5 SM 6200B 63 PASI-CSAS
92709767002 MW-2 SM 6200B 63 PASI-CSAS
92709767003 MW-9 SM 6200B 63 PASI-CSAS
92709767004 MW-6 SM 6200B 63 PASI-CSAS
92709767005 MW-7 SM 6200B 63 PASI-CSAS
92709767006 MW-4 SM 6200B 63 PASI-CSAS
92709767007 MW-8 SM 6200B 63 PASI-CSAS
92709767008 MW-1R SM 6200B 63 PASI-CSAS
92709767009 WSW-1 SM 6200B 63 PASI-CJJK
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-5 Lab ID:92709767001 Collected:01/22/24 11:00 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 01/30/24 14:54 71-43-20.50 1
Bromobenzene ND ug/L 01/30/24 14:54 108-86-10.50 1
Bromochloromethane ND ug/L 01/30/24 14:54 74-97-50.50 1
Bromodichloromethane ND ug/L 01/30/24 14:54 75-27-40.50 1
Bromoform ND ug/L 01/30/24 14:54 75-25-20.50 1
Bromomethane ND ug/L 01/30/24 14:54 74-83-95.0 1
n-Butylbenzene ND ug/L 01/30/24 14:54 104-51-80.50 1
sec-Butylbenzene ND ug/L 01/30/24 14:54 135-98-80.50 1
tert-Butylbenzene ND ug/L 01/30/24 14:54 98-06-60.50 1
Carbon tetrachloride ND ug/L 01/30/24 14:54 56-23-50.50 1
Chlorobenzene ND ug/L 01/30/24 14:54 108-90-70.50 1
Chloroethane ND ug/L 01/30/24 14:54 75-00-31.0 1
Chloroform ND ug/L 01/30/24 14:54 67-66-30.50 1
Chloromethane ND ug/L 01/30/24 14:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 01/30/24 14:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 01/30/24 14:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 01/30/24 14:54 96-12-81.0 1
Dibromochloromethane ND ug/L 01/30/24 14:54 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 01/30/24 14:54 106-93-40.50 1
Dibromomethane ND ug/L 01/30/24 14:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 01/30/24 14:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 01/30/24 14:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 01/30/24 14:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 01/30/24 14:54 75-71-80.50 1
1,1-Dichloroethane ND ug/L 01/30/24 14:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 01/30/24 14:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 01/30/24 14:54 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 01/30/24 14:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 01/30/24 14:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 01/30/24 14:54 78-87-50.50 1
1,3-Dichloropropane ND ug/L 01/30/24 14:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 01/30/24 14:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 01/30/24 14:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 01/30/24 14:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 01/30/24 14:54 10061-02-60.50 1
Diisopropyl ether ND ug/L 01/30/24 14:54 108-20-30.50 1
Ethylbenzene ND ug/L 01/30/24 14:54 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 01/30/24 14:54 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 01/30/24 14:54 98-82-80.50 1
Methylene Chloride ND ug/L 01/30/24 14:54 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 01/30/24 14:54 1634-04-40.50 1
Naphthalene ND ug/L 01/30/24 14:54 91-20-32.0 1
n-Propylbenzene ND ug/L 01/30/24 14:54 103-65-10.50 1
Styrene ND ug/L 01/30/24 14:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 01/30/24 14:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 01/30/24 14:54 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-5 Lab ID:92709767001 Collected:01/22/24 11:00 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 01/30/24 14:54 127-18-40.50 1
Toluene ND ug/L 01/30/24 14:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 01/30/24 14:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 01/30/24 14:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 01/30/24 14:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 01/30/24 14:54 79-00-50.50 1
Trichloroethene ND ug/L 01/30/24 14:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 01/30/24 14:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/30/24 14:54 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 01/30/24 14:54 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 01/30/24 14:54 108-67-80.50 1
Vinyl chloride ND ug/L 01/30/24 14:54 75-01-41.0 1
m&p-Xylene ND ug/L 01/30/24 14:54 179601-23-11.0 1
o-Xylene ND ug/L 01/30/24 14:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %01/30/24 14:54 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %01/30/24 14:54 460-00-470-130 1
Toluene-d8 (S)99 %01/30/24 14:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-2 Lab ID:92709767002 Collected:01/22/24 11:30 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 529 ug/L 01/29/24 18:38 71-43-22.0 4
Bromobenzene ND ug/L 01/29/24 18:38 108-86-12.0 4
Bromochloromethane ND ug/L 01/29/24 18:38 74-97-52.0 4
Bromodichloromethane ND ug/L 01/29/24 18:38 75-27-42.0 4
Bromoform ND ug/L 01/29/24 18:38 75-25-22.0 4
Bromomethane ND ug/L 01/29/24 18:38 74-83-920.0 4
n-Butylbenzene ND ug/L 01/29/24 18:38 104-51-82.0 4
sec-Butylbenzene ND ug/L 01/29/24 18:38 135-98-82.0 4
tert-Butylbenzene ND ug/L 01/29/24 18:38 98-06-62.0 4
Carbon tetrachloride ND ug/L 01/29/24 18:38 56-23-52.0 4
Chlorobenzene ND ug/L 01/29/24 18:38 108-90-72.0 4
Chloroethane ND ug/L 01/29/24 18:38 75-00-34.0 4
Chloroform ND ug/L 01/29/24 18:38 67-66-32.0 4
Chloromethane ND ug/L 01/29/24 18:38 74-87-34.0 4
2-Chlorotoluene ND ug/L 01/29/24 18:38 95-49-82.0 4
4-Chlorotoluene ND ug/L 01/29/24 18:38 106-43-42.0 4
1,2-Dibromo-3-chloropropane ND ug/L 01/29/24 18:38 96-12-84.0 4
Dibromochloromethane ND ug/L 01/29/24 18:38 124-48-12.0 4
1,2-Dibromoethane (EDB)ND ug/L 01/29/24 18:38 106-93-42.0 4
Dibromomethane ND ug/L 01/29/24 18:38 74-95-32.0 4
1,2-Dichlorobenzene ND ug/L 01/29/24 18:38 95-50-12.0 4
1,3-Dichlorobenzene ND ug/L 01/29/24 18:38 541-73-12.0 4
1,4-Dichlorobenzene ND ug/L 01/29/24 18:38 106-46-72.0 4
Dichlorodifluoromethane ND ug/L 01/29/24 18:38 75-71-82.0 4
1,1-Dichloroethane ND ug/L 01/29/24 18:38 75-34-32.0 4
1,2-Dichloroethane 2.4 ug/L 01/29/24 18:38 107-06-22.0 4
1,1-Dichloroethene ND ug/L 01/29/24 18:38 75-35-42.0 4
cis-1,2-Dichloroethene ND ug/L 01/29/24 18:38 156-59-22.0 4
trans-1,2-Dichloroethene ND ug/L 01/29/24 18:38 156-60-52.0 4
1,2-Dichloropropane ND ug/L 01/29/24 18:38 78-87-52.0 4
1,3-Dichloropropane ND ug/L 01/29/24 18:38 142-28-92.0 4
2,2-Dichloropropane ND ug/L 01/29/24 18:38 594-20-72.0 4
1,1-Dichloropropene ND ug/L 01/29/24 18:38 563-58-62.0 4
cis-1,3-Dichloropropene ND ug/L 01/29/24 18:38 10061-01-52.0 4
trans-1,3-Dichloropropene ND ug/L 01/29/24 18:38 10061-02-62.0 4
Diisopropyl ether 41.5 ug/L 01/29/24 18:38 108-20-32.0 4
Ethylbenzene 10.2 ug/L 01/29/24 18:38 100-41-42.0 4
Hexachloro-1,3-butadiene ND ug/L 01/29/24 18:38 87-68-38.0 4
Isopropylbenzene (Cumene)ND ug/L 01/29/24 18:38 98-82-82.0 4
Methylene Chloride ND ug/L 01/29/24 18:38 75-09-28.0 4
Methyl-tert-butyl ether 144 ug/L 01/29/24 18:38 1634-04-42.0 4
Naphthalene 29.4 ug/L 01/29/24 18:38 91-20-38.0 4
n-Propylbenzene ND ug/L 01/29/24 18:38 103-65-12.0 4
Styrene ND ug/L 01/29/24 18:38 100-42-52.0 4
1,1,1,2-Tetrachloroethane ND ug/L 01/29/24 18:38 630-20-62.0 4
1,1,2,2-Tetrachloroethane ND ug/L 01/29/24 18:38 79-34-52.0 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-2 Lab ID:92709767002 Collected:01/22/24 11:30 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 01/29/24 18:38 127-18-42.0 4
Toluene ND ug/L 01/29/24 18:38 108-88-32.0 4
1,2,3-Trichlorobenzene ND ug/L 01/29/24 18:38 87-61-68.0 4
1,2,4-Trichlorobenzene ND ug/L 01/29/24 18:38 120-82-18.0 4
1,1,1-Trichloroethane ND ug/L 01/29/24 18:38 71-55-62.0 4
1,1,2-Trichloroethane ND ug/L 01/29/24 18:38 79-00-52.0 4
Trichloroethene ND ug/L 01/29/24 18:38 79-01-62.0 4
Trichlorofluoromethane ND ug/L 01/29/24 18:38 75-69-44.0 4
1,2,3-Trichloropropane ND ug/L 01/29/24 18:38 96-18-42.0 4
1,2,4-Trimethylbenzene 31.3 ug/L 01/29/24 18:38 95-63-62.0 4
1,3,5-Trimethylbenzene 14.5 ug/L 01/29/24 18:38 108-67-82.0 4
Vinyl chloride ND ug/L 01/29/24 18:38 75-01-44.0 4
m&p-Xylene 76.5 ug/L 01/29/24 18:38 179601-23-14.0 4
o-Xylene 86.3 ug/L 01/29/24 18:38 95-47-62.0 4
Surrogates
1,2-Dichloroethane-d4 (S)108 %01/29/24 18:38 17060-07-070-130 4
4-Bromofluorobenzene (S)100 %01/29/24 18:38 460-00-470-130 4
Toluene-d8 (S)98 %01/29/24 18:38 2037-26-570-130 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-9 Lab ID:92709767003 Collected:01/22/24 12:15 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 01/29/24 15:54 71-43-20.50 1
Bromobenzene ND ug/L 01/29/24 15:54 108-86-10.50 1
Bromochloromethane ND ug/L 01/29/24 15:54 74-97-50.50 1
Bromodichloromethane ND ug/L 01/29/24 15:54 75-27-40.50 1
Bromoform ND ug/L 01/29/24 15:54 75-25-20.50 1
Bromomethane ND ug/L 01/29/24 15:54 74-83-95.0 1
n-Butylbenzene ND ug/L 01/29/24 15:54 104-51-80.50 1
sec-Butylbenzene ND ug/L 01/29/24 15:54 135-98-80.50 1
tert-Butylbenzene ND ug/L 01/29/24 15:54 98-06-60.50 1
Carbon tetrachloride ND ug/L 01/29/24 15:54 56-23-50.50 1
Chlorobenzene ND ug/L 01/29/24 15:54 108-90-70.50 1
Chloroethane ND ug/L 01/29/24 15:54 75-00-31.0 1
Chloroform ND ug/L 01/29/24 15:54 67-66-30.50 1
Chloromethane ND ug/L 01/29/24 15:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 01/29/24 15:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 01/29/24 15:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 01/29/24 15:54 96-12-81.0 1
Dibromochloromethane ND ug/L 01/29/24 15:54 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 01/29/24 15:54 106-93-40.50 1
Dibromomethane ND ug/L 01/29/24 15:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 01/29/24 15:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 01/29/24 15:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 01/29/24 15:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 01/29/24 15:54 75-71-80.50 1
1,1-Dichloroethane ND ug/L 01/29/24 15:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 01/29/24 15:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 01/29/24 15:54 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 01/29/24 15:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 01/29/24 15:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 01/29/24 15:54 78-87-50.50 1
1,3-Dichloropropane ND ug/L 01/29/24 15:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 01/29/24 15:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 01/29/24 15:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 01/29/24 15:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 01/29/24 15:54 10061-02-60.50 1
Diisopropyl ether ND ug/L 01/29/24 15:54 108-20-30.50 1
Ethylbenzene 16.4 ug/L 01/29/24 15:54 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 01/29/24 15:54 87-68-32.0 1
Isopropylbenzene (Cumene)5.4 ug/L 01/29/24 15:54 98-82-80.50 1
Methylene Chloride ND ug/L 01/29/24 15:54 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 01/29/24 15:54 1634-04-40.50 1
Naphthalene 13.0 ug/L 01/29/24 15:54 91-20-32.0 1
n-Propylbenzene 8.3 ug/L 01/29/24 15:54 103-65-10.50 1
Styrene 0.77 ug/L 01/29/24 15:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 01/29/24 15:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 01/29/24 15:54 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-9 Lab ID:92709767003 Collected:01/22/24 12:15 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 01/29/24 15:54 127-18-40.50 1
Toluene 2.4 ug/L 01/29/24 15:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 01/29/24 15:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 01/29/24 15:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 01/29/24 15:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 01/29/24 15:54 79-00-50.50 1
Trichloroethene ND ug/L 01/29/24 15:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 01/29/24 15:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/29/24 15:54 96-18-40.50 1
1,2,4-Trimethylbenzene 193 ug/L 01/29/24 15:54 95-63-60.50 1
1,3,5-Trimethylbenzene 80.1 ug/L 01/29/24 15:54 108-67-80.50 1
Vinyl chloride ND ug/L 01/29/24 15:54 75-01-41.0 1
m&p-Xylene 229 ug/L 01/29/24 15:54 179601-23-11.0 1
o-Xylene 80.2 ug/L 01/29/24 15:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)112 %01/29/24 15:54 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %01/29/24 15:54 460-00-470-130 1
Toluene-d8 (S)100 %01/29/24 15:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-6 Lab ID:92709767004 Collected:01/22/24 12:50 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 01/30/24 15:13 71-43-20.50 1
Bromobenzene ND ug/L 01/30/24 15:13 108-86-10.50 1
Bromochloromethane ND ug/L 01/30/24 15:13 74-97-50.50 1
Bromodichloromethane ND ug/L 01/30/24 15:13 75-27-40.50 1
Bromoform ND ug/L 01/30/24 15:13 75-25-20.50 1
Bromomethane ND ug/L 01/30/24 15:13 74-83-95.0 1
n-Butylbenzene ND ug/L 01/30/24 15:13 104-51-80.50 1
sec-Butylbenzene ND ug/L 01/30/24 15:13 135-98-80.50 1
tert-Butylbenzene ND ug/L 01/30/24 15:13 98-06-60.50 1
Carbon tetrachloride ND ug/L 01/30/24 15:13 56-23-50.50 1
Chlorobenzene ND ug/L 01/30/24 15:13 108-90-70.50 1
Chloroethane ND ug/L 01/30/24 15:13 75-00-31.0 1
Chloroform ND ug/L 01/30/24 15:13 67-66-30.50 1
Chloromethane ND ug/L 01/30/24 15:13 74-87-31.0 1
2-Chlorotoluene ND ug/L 01/30/24 15:13 95-49-80.50 1
4-Chlorotoluene ND ug/L 01/30/24 15:13 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 01/30/24 15:13 96-12-81.0 1
Dibromochloromethane ND ug/L 01/30/24 15:13 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 01/30/24 15:13 106-93-40.50 1
Dibromomethane ND ug/L 01/30/24 15:13 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 01/30/24 15:13 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 01/30/24 15:13 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 01/30/24 15:13 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 01/30/24 15:13 75-71-80.50 1
1,1-Dichloroethane ND ug/L 01/30/24 15:13 75-34-30.50 1
1,2-Dichloroethane ND ug/L 01/30/24 15:13 107-06-20.50 1
1,1-Dichloroethene ND ug/L 01/30/24 15:13 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 01/30/24 15:13 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 01/30/24 15:13 156-60-50.50 1
1,2-Dichloropropane ND ug/L 01/30/24 15:13 78-87-50.50 1
1,3-Dichloropropane ND ug/L 01/30/24 15:13 142-28-90.50 1
2,2-Dichloropropane ND ug/L 01/30/24 15:13 594-20-70.50 1
1,1-Dichloropropene ND ug/L 01/30/24 15:13 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 01/30/24 15:13 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 01/30/24 15:13 10061-02-60.50 1
Diisopropyl ether ND ug/L 01/30/24 15:13 108-20-30.50 1
Ethylbenzene ND ug/L 01/30/24 15:13 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 01/30/24 15:13 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 01/30/24 15:13 98-82-80.50 1
Methylene Chloride ND ug/L 01/30/24 15:13 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 01/30/24 15:13 1634-04-40.50 1
Naphthalene ND ug/L 01/30/24 15:13 91-20-32.0 1
n-Propylbenzene ND ug/L 01/30/24 15:13 103-65-10.50 1
Styrene ND ug/L 01/30/24 15:13 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 01/30/24 15:13 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 01/30/24 15:13 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-6 Lab ID:92709767004 Collected:01/22/24 12:50 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 01/30/24 15:13 127-18-40.50 1
Toluene ND ug/L 01/30/24 15:13 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 01/30/24 15:13 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 01/30/24 15:13 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 01/30/24 15:13 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 01/30/24 15:13 79-00-50.50 1
Trichloroethene ND ug/L 01/30/24 15:13 79-01-60.50 1
Trichlorofluoromethane ND ug/L 01/30/24 15:13 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/30/24 15:13 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 01/30/24 15:13 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 01/30/24 15:13 108-67-80.50 1
Vinyl chloride ND ug/L 01/30/24 15:13 75-01-41.0 1
m&p-Xylene ND ug/L 01/30/24 15:13 179601-23-11.0 1
o-Xylene ND ug/L 01/30/24 15:13 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %01/30/24 15:13 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %01/30/24 15:13 460-00-470-130 1
Toluene-d8 (S)99 %01/30/24 15:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-7 Lab ID:92709767005 Collected:01/22/24 13:30 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 01/30/24 15:31 71-43-20.50 1
Bromobenzene ND ug/L 01/30/24 15:31 108-86-10.50 1
Bromochloromethane ND ug/L 01/30/24 15:31 74-97-50.50 1
Bromodichloromethane ND ug/L 01/30/24 15:31 75-27-40.50 1
Bromoform ND ug/L 01/30/24 15:31 75-25-20.50 1
Bromomethane ND ug/L 01/30/24 15:31 74-83-95.0 1
n-Butylbenzene ND ug/L 01/30/24 15:31 104-51-80.50 1
sec-Butylbenzene ND ug/L 01/30/24 15:31 135-98-80.50 1
tert-Butylbenzene ND ug/L 01/30/24 15:31 98-06-60.50 1
Carbon tetrachloride ND ug/L 01/30/24 15:31 56-23-50.50 1
Chlorobenzene ND ug/L 01/30/24 15:31 108-90-70.50 1
Chloroethane ND ug/L 01/30/24 15:31 75-00-31.0 1
Chloroform ND ug/L 01/30/24 15:31 67-66-30.50 1
Chloromethane ND ug/L 01/30/24 15:31 74-87-31.0 1
2-Chlorotoluene ND ug/L 01/30/24 15:31 95-49-80.50 1
4-Chlorotoluene ND ug/L 01/30/24 15:31 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 01/30/24 15:31 96-12-81.0 1
Dibromochloromethane ND ug/L 01/30/24 15:31 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 01/30/24 15:31 106-93-40.50 1
Dibromomethane ND ug/L 01/30/24 15:31 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 01/30/24 15:31 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 01/30/24 15:31 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 01/30/24 15:31 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 01/30/24 15:31 75-71-80.50 1
1,1-Dichloroethane ND ug/L 01/30/24 15:31 75-34-30.50 1
1,2-Dichloroethane ND ug/L 01/30/24 15:31 107-06-20.50 1
1,1-Dichloroethene ND ug/L 01/30/24 15:31 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 01/30/24 15:31 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 01/30/24 15:31 156-60-50.50 1
1,2-Dichloropropane ND ug/L 01/30/24 15:31 78-87-50.50 1
1,3-Dichloropropane ND ug/L 01/30/24 15:31 142-28-90.50 1
2,2-Dichloropropane ND ug/L 01/30/24 15:31 594-20-70.50 1
1,1-Dichloropropene ND ug/L 01/30/24 15:31 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 01/30/24 15:31 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 01/30/24 15:31 10061-02-60.50 1
Diisopropyl ether ND ug/L 01/30/24 15:31 108-20-30.50 1
Ethylbenzene ND ug/L 01/30/24 15:31 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 01/30/24 15:31 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 01/30/24 15:31 98-82-80.50 1
Methylene Chloride ND ug/L 01/30/24 15:31 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 01/30/24 15:31 1634-04-40.50 1
Naphthalene ND ug/L 01/30/24 15:31 91-20-32.0 1
n-Propylbenzene ND ug/L 01/30/24 15:31 103-65-10.50 1
Styrene ND ug/L 01/30/24 15:31 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 01/30/24 15:31 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 01/30/24 15:31 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-7 Lab ID:92709767005 Collected:01/22/24 13:30 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 01/30/24 15:31 127-18-40.50 1
Toluene ND ug/L 01/30/24 15:31 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 01/30/24 15:31 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 01/30/24 15:31 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 01/30/24 15:31 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 01/30/24 15:31 79-00-50.50 1
Trichloroethene ND ug/L 01/30/24 15:31 79-01-60.50 1
Trichlorofluoromethane ND ug/L 01/30/24 15:31 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/30/24 15:31 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 01/30/24 15:31 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 01/30/24 15:31 108-67-80.50 1
Vinyl chloride ND ug/L 01/30/24 15:31 75-01-41.0 1
m&p-Xylene ND ug/L 01/30/24 15:31 179601-23-11.0 1
o-Xylene ND ug/L 01/30/24 15:31 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %01/30/24 15:31 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %01/30/24 15:31 460-00-470-130 1
Toluene-d8 (S)100 %01/30/24 15:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-4 Lab ID:92709767006 Collected:01/22/24 14:00 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 186 ug/L 01/29/24 18:20 71-43-22.0 4
Bromobenzene ND ug/L 01/29/24 18:20 108-86-12.0 4
Bromochloromethane ND ug/L 01/29/24 18:20 74-97-52.0 4
Bromodichloromethane ND ug/L 01/29/24 18:20 75-27-42.0 4
Bromoform ND ug/L 01/29/24 18:20 75-25-22.0 4
Bromomethane ND ug/L 01/29/24 18:20 74-83-920.0 4
n-Butylbenzene ND ug/L 01/29/24 18:20 104-51-82.0 4
sec-Butylbenzene ND ug/L 01/29/24 18:20 135-98-82.0 4
tert-Butylbenzene ND ug/L 01/29/24 18:20 98-06-62.0 4
Carbon tetrachloride ND ug/L 01/29/24 18:20 56-23-52.0 4
Chlorobenzene 65.3 ug/L 01/29/24 18:20 108-90-72.0 4
Chloroethane ND ug/L 01/29/24 18:20 75-00-34.0 4
Chloroform ND ug/L 01/29/24 18:20 67-66-32.0 4
Chloromethane ND ug/L 01/29/24 18:20 74-87-34.0 4
2-Chlorotoluene ND ug/L 01/29/24 18:20 95-49-82.0 4
4-Chlorotoluene ND ug/L 01/29/24 18:20 106-43-42.0 4
1,2-Dibromo-3-chloropropane ND ug/L 01/29/24 18:20 96-12-84.0 4
Dibromochloromethane ND ug/L 01/29/24 18:20 124-48-12.0 4
1,2-Dibromoethane (EDB)4.2 ug/L 01/29/24 18:20 106-93-42.0 4
Dibromomethane ND ug/L 01/29/24 18:20 74-95-32.0 4
1,2-Dichlorobenzene ND ug/L 01/29/24 18:20 95-50-12.0 4
1,3-Dichlorobenzene ND ug/L 01/29/24 18:20 541-73-12.0 4
1,4-Dichlorobenzene ND ug/L 01/29/24 18:20 106-46-72.0 4
Dichlorodifluoromethane ND ug/L 01/29/24 18:20 75-71-82.0 4
1,1-Dichloroethane ND ug/L 01/29/24 18:20 75-34-32.0 4
1,2-Dichloroethane 25.9 ug/L 01/29/24 18:20 107-06-22.0 4
1,1-Dichloroethene ND ug/L 01/29/24 18:20 75-35-42.0 4
cis-1,2-Dichloroethene ND ug/L 01/29/24 18:20 156-59-22.0 4
trans-1,2-Dichloroethene ND ug/L 01/29/24 18:20 156-60-52.0 4
1,2-Dichloropropane ND ug/L 01/29/24 18:20 78-87-52.0 4
1,3-Dichloropropane ND ug/L 01/29/24 18:20 142-28-92.0 4
2,2-Dichloropropane ND ug/L 01/29/24 18:20 594-20-72.0 4
1,1-Dichloropropene ND ug/L 01/29/24 18:20 563-58-62.0 4
cis-1,3-Dichloropropene ND ug/L 01/29/24 18:20 10061-01-52.0 4
trans-1,3-Dichloropropene ND ug/L 01/29/24 18:20 10061-02-62.0 4
Diisopropyl ether 88.2 ug/L 01/29/24 18:20 108-20-32.0 4
Ethylbenzene 141 ug/L 01/29/24 18:20 100-41-42.0 4
Hexachloro-1,3-butadiene ND ug/L 01/29/24 18:20 87-68-38.0 4
Isopropylbenzene (Cumene)12.2 ug/L 01/29/24 18:20 98-82-82.0 4
Methylene Chloride ND ug/L 01/29/24 18:20 75-09-28.0 4
Methyl-tert-butyl ether 483 ug/L 01/29/24 18:20 1634-04-42.0 4
Naphthalene 110 ug/L 01/29/24 18:20 91-20-38.0 4
n-Propylbenzene 23.6 ug/L 01/29/24 18:20 103-65-12.0 4
Styrene ND ug/L 01/29/24 18:20 100-42-52.0 4
1,1,1,2-Tetrachloroethane ND ug/L 01/29/24 18:20 630-20-62.0 4
1,1,2,2-Tetrachloroethane ND ug/L 01/29/24 18:20 79-34-52.0 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-4 Lab ID:92709767006 Collected:01/22/24 14:00 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 01/29/24 18:20 127-18-42.0 4
Toluene 350 ug/L 01/29/24 18:20 108-88-32.0 4
1,2,3-Trichlorobenzene ND ug/L 01/29/24 18:20 87-61-68.0 4
1,2,4-Trichlorobenzene ND ug/L 01/29/24 18:20 120-82-18.0 4
1,1,1-Trichloroethane ND ug/L 01/29/24 18:20 71-55-62.0 4
1,1,2-Trichloroethane ND ug/L 01/29/24 18:20 79-00-52.0 4
Trichloroethene ND ug/L 01/29/24 18:20 79-01-62.0 4
Trichlorofluoromethane ND ug/L 01/29/24 18:20 75-69-44.0 4
1,2,3-Trichloropropane ND ug/L 01/29/24 18:20 96-18-42.0 4
1,2,4-Trimethylbenzene 396 ug/L 01/29/24 18:20 95-63-62.0 4
1,3,5-Trimethylbenzene 112 ug/L 01/29/24 18:20 108-67-82.0 4
Vinyl chloride ND ug/L 01/29/24 18:20 75-01-44.0 4
m&p-Xylene 1240 ug/L 01/29/24 18:20 179601-23-14.0 4
o-Xylene 550 ug/L 01/29/24 18:20 95-47-62.0 4
Surrogates
1,2-Dichloroethane-d4 (S)109 %01/29/24 18:20 17060-07-070-130 4
4-Bromofluorobenzene (S)100 %01/29/24 18:20 460-00-470-130 4
Toluene-d8 (S)100 %01/29/24 18:20 2037-26-570-130 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-8 Lab ID:92709767007 Collected:01/22/24 14:30 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 16.0 ug/L 01/29/24 16:31 71-43-20.50 1
Bromobenzene ND ug/L 01/29/24 16:31 108-86-10.50 1
Bromochloromethane ND ug/L 01/29/24 16:31 74-97-50.50 1
Bromodichloromethane ND ug/L 01/29/24 16:31 75-27-40.50 1
Bromoform ND ug/L 01/29/24 16:31 75-25-20.50 1
Bromomethane ND ug/L 01/29/24 16:31 74-83-95.0 1
n-Butylbenzene ND ug/L 01/29/24 16:31 104-51-80.50 1
sec-Butylbenzene ND ug/L 01/29/24 16:31 135-98-80.50 1
tert-Butylbenzene ND ug/L 01/29/24 16:31 98-06-60.50 1
Carbon tetrachloride ND ug/L 01/29/24 16:31 56-23-50.50 1
Chlorobenzene ND ug/L 01/29/24 16:31 108-90-70.50 1
Chloroethane ND ug/L 01/29/24 16:31 75-00-31.0 1
Chloroform ND ug/L 01/29/24 16:31 67-66-30.50 1
Chloromethane ND ug/L 01/29/24 16:31 74-87-31.0 1
2-Chlorotoluene ND ug/L 01/29/24 16:31 95-49-80.50 1
4-Chlorotoluene ND ug/L 01/29/24 16:31 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 01/29/24 16:31 96-12-81.0 1
Dibromochloromethane ND ug/L 01/29/24 16:31 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 01/29/24 16:31 106-93-40.50 1
Dibromomethane ND ug/L 01/29/24 16:31 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 01/29/24 16:31 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 01/29/24 16:31 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 01/29/24 16:31 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 01/29/24 16:31 75-71-80.50 1
1,1-Dichloroethane ND ug/L 01/29/24 16:31 75-34-30.50 1
1,2-Dichloroethane ND ug/L 01/29/24 16:31 107-06-20.50 1
1,1-Dichloroethene ND ug/L 01/29/24 16:31 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 01/29/24 16:31 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 01/29/24 16:31 156-60-50.50 1
1,2-Dichloropropane ND ug/L 01/29/24 16:31 78-87-50.50 1
1,3-Dichloropropane ND ug/L 01/29/24 16:31 142-28-90.50 1
2,2-Dichloropropane ND ug/L 01/29/24 16:31 594-20-70.50 1
1,1-Dichloropropene ND ug/L 01/29/24 16:31 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 01/29/24 16:31 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 01/29/24 16:31 10061-02-60.50 1
Diisopropyl ether 3.8 ug/L 01/29/24 16:31 108-20-30.50 1
Ethylbenzene 9.6 ug/L 01/29/24 16:31 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 01/29/24 16:31 87-68-32.0 1
Isopropylbenzene (Cumene)21.2 ug/L 01/29/24 16:31 98-82-80.50 1
Methylene Chloride ND ug/L 01/29/24 16:31 75-09-22.0 1
Methyl-tert-butyl ether 7.3 ug/L 01/29/24 16:31 1634-04-40.50 1
Naphthalene 60.6 ug/L 01/29/24 16:31 91-20-32.0 1
n-Propylbenzene 39.0 ug/L 01/29/24 16:31 103-65-10.50 1
Styrene ND ug/L 01/29/24 16:31 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 01/29/24 16:31 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 01/29/24 16:31 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-8 Lab ID:92709767007 Collected:01/22/24 14:30 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 01/29/24 16:31 127-18-40.50 1
Toluene 4.7 ug/L 01/29/24 16:31 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 01/29/24 16:31 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 01/29/24 16:31 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 01/29/24 16:31 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 01/29/24 16:31 79-00-50.50 1
Trichloroethene ND ug/L 01/29/24 16:31 79-01-60.50 1
Trichlorofluoromethane ND ug/L 01/29/24 16:31 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/29/24 16:31 96-18-40.50 1
1,2,4-Trimethylbenzene 32.7 ug/L 01/29/24 16:31 95-63-60.50 1
1,3,5-Trimethylbenzene 42.5 ug/L 01/29/24 16:31 108-67-80.50 1
Vinyl chloride ND ug/L 01/29/24 16:31 75-01-41.0 1
m&p-Xylene 14.7 ug/L 01/29/24 16:31 179601-23-11.0 1
o-Xylene 123 ug/L 01/29/24 16:31 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)111 %01/29/24 16:31 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %01/29/24 16:31 460-00-470-130 1
Toluene-d8 (S)99 %01/29/24 16:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-1R Lab ID:92709767008 Collected:01/22/24 15:00 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 965 ug/L 01/29/24 19:15 71-43-212.5 25
Bromobenzene ND ug/L 01/29/24 19:15 108-86-112.5 25
Bromochloromethane ND ug/L 01/29/24 19:15 74-97-512.5 25
Bromodichloromethane ND ug/L 01/29/24 19:15 75-27-412.5 25
Bromoform ND ug/L 01/29/24 19:15 75-25-212.5 25
Bromomethane ND ug/L 01/29/24 19:15 74-83-912525
n-Butylbenzene ND ug/L 01/29/24 19:15 104-51-812.5 25
sec-Butylbenzene ND ug/L 01/29/24 19:15 135-98-812.5 25
tert-Butylbenzene ND ug/L 01/29/24 19:15 98-06-612.5 25
Carbon tetrachloride ND ug/L 01/29/24 19:15 56-23-512.5 25
Chlorobenzene ND ug/L 01/29/24 19:15 108-90-712.5 25
Chloroethane ND ug/L 01/29/24 19:15 75-00-325.0 25
Chloroform ND ug/L 01/29/24 19:15 67-66-312.5 25
Chloromethane ND ug/L 01/29/24 19:15 74-87-325.0 25
2-Chlorotoluene ND ug/L 01/29/24 19:15 95-49-812.5 25
4-Chlorotoluene ND ug/L 01/29/24 19:15 106-43-412.5 25
1,2-Dibromo-3-chloropropane ND ug/L 01/29/24 19:15 96-12-825.0 25
Dibromochloromethane ND ug/L 01/29/24 19:15 124-48-112.5 25
1,2-Dibromoethane (EDB)ND ug/L 01/29/24 19:15 106-93-412.5 25
Dibromomethane ND ug/L 01/29/24 19:15 74-95-312.5 25
1,2-Dichlorobenzene ND ug/L 01/29/24 19:15 95-50-112.5 25
1,3-Dichlorobenzene ND ug/L 01/29/24 19:15 541-73-112.5 25
1,4-Dichlorobenzene ND ug/L 01/29/24 19:15 106-46-712.5 25
Dichlorodifluoromethane ND ug/L 01/29/24 19:15 75-71-812.5 25
1,1-Dichloroethane ND ug/L 01/29/24 19:15 75-34-312.5 25
1,2-Dichloroethane ND ug/L 01/29/24 19:15 107-06-212.5 25
1,1-Dichloroethene ND ug/L 01/29/24 19:15 75-35-412.5 25
cis-1,2-Dichloroethene ND ug/L 01/29/24 19:15 156-59-212.5 25
trans-1,2-Dichloroethene ND ug/L 01/29/24 19:15 156-60-512.5 25
1,2-Dichloropropane ND ug/L 01/29/24 19:15 78-87-512.5 25
1,3-Dichloropropane ND ug/L 01/29/24 19:15 142-28-912.5 25
2,2-Dichloropropane ND ug/L 01/29/24 19:15 594-20-712.5 25
1,1-Dichloropropene ND ug/L 01/29/24 19:15 563-58-612.5 25
cis-1,3-Dichloropropene ND ug/L 01/29/24 19:15 10061-01-512.5 25
trans-1,3-Dichloropropene ND ug/L 01/29/24 19:15 10061-02-612.5 25
Diisopropyl ether 47.4 ug/L 01/29/24 19:15 108-20-312.5 25
Ethylbenzene 1260 ug/L 01/29/24 19:15 100-41-412.5 25
Hexachloro-1,3-butadiene ND ug/L 01/29/24 19:15 87-68-350.0 25
Isopropylbenzene (Cumene)40.6 ug/L 01/29/24 19:15 98-82-812.5 25
Methylene Chloride ND ug/L 01/29/24 19:15 75-09-250.0 25
Methyl-tert-butyl ether 94.7 ug/L 01/29/24 19:15 1634-04-412.5 25
Naphthalene 483 ug/L 01/29/24 19:15 91-20-350.0 25
n-Propylbenzene 141 ug/L 01/29/24 19:15 103-65-112.5 25
Styrene 84.2 ug/L 01/29/24 19:15 100-42-512.5 25
1,1,1,2-Tetrachloroethane ND ug/L 01/29/24 19:15 630-20-612.5 25
1,1,2,2-Tetrachloroethane ND ug/L 01/29/24 19:15 79-34-512.5 25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
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Page 18 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:MW-1R Lab ID:92709767008 Collected:01/22/24 15:00 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 01/29/24 19:15 127-18-412.5 25
Toluene 2860 ug/L 01/29/24 19:15 108-88-312.5 25
1,2,3-Trichlorobenzene ND ug/L 01/29/24 19:15 87-61-650.0 25
1,2,4-Trichlorobenzene ND ug/L 01/29/24 19:15 120-82-150.0 25
1,1,1-Trichloroethane ND ug/L 01/29/24 19:15 71-55-612.5 25
1,1,2-Trichloroethane ND ug/L 01/29/24 19:15 79-00-512.5 25
Trichloroethene ND ug/L 01/29/24 19:15 79-01-612.5 25
Trichlorofluoromethane ND ug/L 01/29/24 19:15 75-69-425.0 25
1,2,3-Trichloropropane ND ug/L 01/29/24 19:15 96-18-412.5 25
1,2,4-Trimethylbenzene 1250 ug/L 01/29/24 19:15 95-63-612.5 25
1,3,5-Trimethylbenzene 340 ug/L 01/29/24 19:15 108-67-812.5 25
Vinyl chloride ND ug/L 01/29/24 19:15 75-01-425.0 25
m&p-Xylene 3310 ug/L 01/29/24 19:15 179601-23-125.0 25
o-Xylene 2180 ug/L 01/29/24 19:15 95-47-612.5 25
Surrogates
1,2-Dichloroethane-d4 (S)107 %01/29/24 19:15 17060-07-070-130 25
4-Bromofluorobenzene (S)99 %01/29/24 19:15 460-00-470-130 25
Toluene-d8 (S)99 %01/29/24 19:15 2037-26-570-130 25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
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2225 Riverside Dr.
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[phone]
Page 19 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:WSW-1 Lab ID:92709767009 Collected:01/22/24 15:15 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 01/26/24 07:20 71-43-20.50 1
Bromobenzene ND ug/L 01/26/24 07:20 108-86-10.50 1
Bromochloromethane ND ug/L 01/26/24 07:20 74-97-50.50 1
Bromodichloromethane ND ug/L 01/26/24 07:20 75-27-40.50 1
Bromoform ND ug/L 01/26/24 07:20 75-25-20.50 1
Bromomethane ND ug/L 01/26/24 07:20 74-83-95.0 1
n-Butylbenzene ND ug/L 01/26/24 07:20 104-51-80.50 1
sec-Butylbenzene ND ug/L 01/26/24 07:20 135-98-80.50 1
tert-Butylbenzene ND ug/L 01/26/24 07:20 98-06-60.50 1
Carbon tetrachloride ND ug/L 01/26/24 07:20 56-23-50.50 1
Chlorobenzene ND ug/L 01/26/24 07:20 108-90-70.50 1
Chloroethane ND ug/L 01/26/24 07:20 75-00-31.0 1
Chloroform ND ug/L 01/26/24 07:20 67-66-30.50 1
Chloromethane ND ug/L 01/26/24 07:20 74-87-31.0 1
2-Chlorotoluene ND ug/L 01/26/24 07:20 95-49-80.50 1
4-Chlorotoluene ND ug/L 01/26/24 07:20 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 01/26/24 07:20 96-12-81.0 1
Dibromochloromethane ND ug/L 01/26/24 07:20 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 01/26/24 07:20 106-93-40.50 1
Dibromomethane ND ug/L 01/26/24 07:20 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 01/26/24 07:20 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 01/26/24 07:20 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 01/26/24 07:20 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 01/26/24 07:20 75-71-80.50 1
1,1-Dichloroethane ND ug/L 01/26/24 07:20 75-34-30.50 1
1,2-Dichloroethane ND ug/L 01/26/24 07:20 107-06-20.50 1
1,1-Dichloroethene ND ug/L 01/26/24 07:20 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 01/26/24 07:20 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 01/26/24 07:20 156-60-50.50 1
1,2-Dichloropropane ND ug/L 01/26/24 07:20 78-87-50.50 1
1,3-Dichloropropane ND ug/L 01/26/24 07:20 142-28-90.50 1
2,2-Dichloropropane ND ug/L 01/26/24 07:20 594-20-70.50 1
1,1-Dichloropropene ND ug/L 01/26/24 07:20 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 01/26/24 07:20 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 01/26/24 07:20 10061-02-60.50 1
Diisopropyl ether ND ug/L 01/26/24 07:20 108-20-30.50 1
Ethylbenzene ND ug/L 01/26/24 07:20 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 01/26/24 07:20 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 01/26/24 07:20 98-82-80.50 1
Methylene Chloride ND ug/L 01/26/24 07:20 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 01/26/24 07:20 1634-04-40.50 1
Naphthalene ND ug/L 01/26/24 07:20 91-20-32.0 1
n-Propylbenzene ND ug/L 01/26/24 07:20 103-65-10.50 1
Styrene ND ug/L 01/26/24 07:20 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 01/26/24 07:20 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 01/26/24 07:20 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Sample:WSW-1 Lab ID:92709767009 Collected:01/22/24 15:15 Received:01/24/24 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 01/26/24 07:20 127-18-40.50 1
Toluene ND ug/L 01/26/24 07:20 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 01/26/24 07:20 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 01/26/24 07:20 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 01/26/24 07:20 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 01/26/24 07:20 79-00-50.50 1
Trichloroethene ND ug/L 01/26/24 07:20 79-01-60.50 1
Trichlorofluoromethane ND ug/L 01/26/24 07:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/26/24 07:20 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 01/26/24 07:20 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 01/26/24 07:20 108-67-80.50 1
Vinyl chloride ND ug/L 01/26/24 07:20 75-01-41.0 1
m&p-Xylene ND ug/L 01/26/24 07:20 179601-23-11.0 1
o-Xylene ND ug/L 01/26/24 07:20 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %01/26/24 07:20 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %01/26/24 07:20 460-00-470-130 1
Toluene-d8 (S)100 %01/26/24 07:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
827894
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92709767001, 92709767004, 92709767005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4280502
Associated Lab Samples:92709767001, 92709767004, 92709767005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 01/30/24 11:16
1,1,1-Trichloroethane ug/L ND 0.50 01/30/24 11:16
1,1,2,2-Tetrachloroethane ug/L ND 0.50 01/30/24 11:16
1,1,2-Trichloroethane ug/L ND 0.50 01/30/24 11:16
1,1-Dichloroethane ug/L ND 0.50 01/30/24 11:16
1,1-Dichloroethene ug/L ND 0.50 01/30/24 11:16
1,1-Dichloropropene ug/L ND 0.50 01/30/24 11:16
1,2,3-Trichlorobenzene ug/L ND 2.0 01/30/24 11:16
1,2,3-Trichloropropane ug/L ND 0.50 01/30/24 11:16
1,2,4-Trichlorobenzene ug/L ND 2.0 01/30/24 11:16
1,2,4-Trimethylbenzene ug/L ND 0.50 01/30/24 11:16
1,2-Dibromo-3-chloropropane ug/L ND 1.0 01/30/24 11:16
1,2-Dibromoethane (EDB)ug/L ND 0.50 01/30/24 11:16
1,2-Dichlorobenzene ug/L ND 0.50 01/30/24 11:16
1,2-Dichloroethane ug/L ND 0.50 01/30/24 11:16
1,2-Dichloropropane ug/L ND 0.50 01/30/24 11:16
1,3,5-Trimethylbenzene ug/L ND 0.50 01/30/24 11:16
1,3-Dichlorobenzene ug/L ND 0.50 01/30/24 11:16
1,3-Dichloropropane ug/L ND 0.50 01/30/24 11:16
1,4-Dichlorobenzene ug/L ND 0.50 01/30/24 11:16
2,2-Dichloropropane ug/L ND 0.50 01/30/24 11:16
2-Chlorotoluene ug/L ND 0.50 01/30/24 11:16
4-Chlorotoluene ug/L ND 0.50 01/30/24 11:16
Benzene ug/L ND 0.50 01/30/24 11:16
Bromobenzene ug/L ND 0.50 01/30/24 11:16
Bromochloromethane ug/L ND 0.50 01/30/24 11:16
Bromodichloromethane ug/L ND 0.50 01/30/24 11:16
Bromoform ug/L ND 0.50 01/30/24 11:16
Bromomethane ug/L ND 5.0 01/30/24 11:16
Carbon tetrachloride ug/L ND 0.50 01/30/24 11:16
Chlorobenzene ug/L ND 0.50 01/30/24 11:16
Chloroethane ug/L ND 1.0 01/30/24 11:16
Chloroform ug/L ND 0.50 01/30/24 11:16
Chloromethane ug/L ND 1.0 01/30/24 11:16
cis-1,2-Dichloroethene ug/L ND 0.50 01/30/24 11:16
cis-1,3-Dichloropropene ug/L ND 0.50 01/30/24 11:16
Dibromochloromethane ug/L ND 0.50 01/30/24 11:16
Dibromomethane ug/L ND 0.50 01/30/24 11:16
Dichlorodifluoromethane ug/L ND 0.50 01/30/24 11:16
Diisopropyl ether ug/L ND 0.50 01/30/24 11:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4280502
Associated Lab Samples:92709767001, 92709767004, 92709767005
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 01/30/24 11:16
Hexachloro-1,3-butadiene ug/L ND 2.0 01/30/24 11:16
Isopropylbenzene (Cumene)ug/L ND 0.50 01/30/24 11:16
m&p-Xylene ug/L ND 1.0 01/30/24 11:16
Methyl-tert-butyl ether ug/L ND 0.50 01/30/24 11:16
Methylene Chloride ug/L ND 2.0 01/30/24 11:16
n-Butylbenzene ug/L ND 0.50 01/30/24 11:16
n-Propylbenzene ug/L ND 0.50 01/30/24 11:16
Naphthalene ug/L ND 2.0 01/30/24 11:16
o-Xylene ug/L ND 0.50 01/30/24 11:16
sec-Butylbenzene ug/L ND 0.50 01/30/24 11:16
Styrene ug/L ND 0.50 01/30/24 11:16
tert-Butylbenzene ug/L ND 0.50 01/30/24 11:16
Tetrachloroethene ug/L ND 0.50 01/30/24 11:16
Toluene ug/L ND 0.50 01/30/24 11:16
trans-1,2-Dichloroethene ug/L ND 0.50 01/30/24 11:16
trans-1,3-Dichloropropene ug/L ND 0.50 01/30/24 11:16
Trichloroethene ug/L ND 0.50 01/30/24 11:16
Trichlorofluoromethane ug/L ND 1.0 01/30/24 11:16
Vinyl chloride ug/L ND 1.0 01/30/24 11:16
1,2-Dichloroethane-d4 (S)%105 70-130 01/30/24 11:16
4-Bromofluorobenzene (S)%100 70-130 01/30/24 11:16
Toluene-d8 (S)%99 70-130 01/30/24 11:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4280503LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.820 109 60-140
1,1,1-Trichloroethane ug/L 23.520 117 60-140
1,1,2,2-Tetrachloroethane ug/L 21.520 107 60-140
1,1,2-Trichloroethane ug/L 22.220 111 60-140
1,1-Dichloroethane ug/L 22.020 110 60-140
1,1-Dichloroethene ug/L 25.320 126 60-140
1,1-Dichloropropene ug/L 24.220 121 60-140
1,2,3-Trichlorobenzene ug/L 21.320 107 60-140
1,2,3-Trichloropropane ug/L 20.720 103 60-140
1,2,4-Trichlorobenzene ug/L 21.220 106 60-140
1,2,4-Trimethylbenzene ug/L 23.020 115 60-140
1,2-Dibromo-3-chloropropane ug/L 19.820 99 60-140
1,2-Dibromoethane (EDB)ug/L 21.720 109 60-140
1,2-Dichlorobenzene ug/L 21.620 108 60-140
1,2-Dichloroethane ug/L 22.920 114 60-140
1,2-Dichloropropane ug/L 21.720 109 60-140
1,3,5-Trimethylbenzene ug/L 22.820 114 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4280503LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 21.820 109 60-140
1,3-Dichloropropane ug/L 21.420 107 60-140
1,4-Dichlorobenzene ug/L 21.120 106 60-140
2,2-Dichloropropane ug/L 23.720 119 60-140
2-Chlorotoluene ug/L 22.120 110 60-140
4-Chlorotoluene ug/L 22.520 112 60-140
Benzene ug/L 21.720 108 60-140
Bromobenzene ug/L 21.020 105 60-140
Bromochloromethane ug/L 22.320 112 60-140
Bromodichloromethane ug/L 21.920 109 60-140
Bromoform ug/L 20.620 103 60-140
Bromomethane ug/L 22.220 111 60-140
Carbon tetrachloride ug/L 22.920 114 60-140
Chlorobenzene ug/L 21.120 105 60-140
Chloroethane ug/L 25.620 128 60-140
Chloroform ug/L 22.020 110 60-140
Chloromethane ug/L 18.320 91 60-140
cis-1,2-Dichloroethene ug/L 22.620 113 60-140
cis-1,3-Dichloropropene ug/L 22.120 110 60-140
Dibromochloromethane ug/L 21.820 109 60-140
Dibromomethane ug/L 21.620 108 60-140
Dichlorodifluoromethane ug/L 21.120 106 60-140
Diisopropyl ether ug/L 21.420 107 60-140
Ethylbenzene ug/L 21.520 107 60-140
Hexachloro-1,3-butadiene ug/L 24.120 121 60-140
Isopropylbenzene (Cumene)ug/L 23.020 115 60-140
m&p-Xylene ug/L 44.240 111 60-140
Methyl-tert-butyl ether ug/L 20.820 104 60-140
Methylene Chloride ug/L 20.120 100 60-140
n-Butylbenzene ug/L 24.120 120 60-140
n-Propylbenzene ug/L 22.320 111 60-140
Naphthalene ug/L 20.220 101 60-140
o-Xylene ug/L 22.120 110 60-140
sec-Butylbenzene ug/L 22.720 113 60-140
Styrene ug/L 22.320 112 60-140
tert-Butylbenzene ug/L 17.920 89 60-140
Tetrachloroethene ug/L 21.420 107 60-140
Toluene ug/L 20.920 105 60-140
trans-1,2-Dichloroethene ug/L 22.620 113 60-140
trans-1,3-Dichloropropene ug/L 22.420 112 60-140
Trichloroethene ug/L 22.220 111 60-140
Trichlorofluoromethane ug/L 22.420 112 60-140
Vinyl chloride ug/L 18.520 93 60-140
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4280504MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92709742005
4280505
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 102 60-140114 1120ND20.4 22.8
1,1,1-Trichloroethane ug/L 20 106 60-140123 1520ND21.2 24.7
1,1,2,2-Tetrachloroethane ug/L 20 101 60-140109 820ND20.1 21.8
1,1,2-Trichloroethane ug/L 20 100 60-140116 1420ND20.1 23.1
1,1-Dichloroethane ug/L 20 97 60-140112 1520ND19.3 22.5
1,1-Dichloroethene ug/L 20 107 60-140120 1220ND21.3 24.0
1,1-Dichloropropene ug/L 20 110 60-140125 1220ND22.1 24.9
1,2,3-Trichlorobenzene ug/L 20 99 60-140114 1320ND19.9 22.7
1,2,3-Trichloropropane ug/L 20 93 60-140108 1520ND18.5 21.5
1,2,4-Trichlorobenzene ug/L 20 100 60-140113 1220ND20.0 22.6
1,2,4-Trimethylbenzene ug/L 20 103 60-140115 1120ND20.6 23.0
1,2-Dibromo-3-chloropropane ug/L 20 91 60-14099 820ND18.2 19.8
1,2-Dibromoethane (EDB)ug/L 20 98 60-140112 1320ND19.6 22.4
1,2-Dichlorobenzene ug/L 20 99 60-140113 1320ND19.8 22.5
1,2-Dichloroethane ug/L 20 100 60-140110 920ND20.0 21.9
1,2-Dichloropropane ug/L 20 102 60-140117 1420ND20.3 23.4
1,3,5-Trimethylbenzene ug/L 20 103 60-140115 1120ND20.6 23.0
1,3-Dichlorobenzene ug/L 20 102 60-140114 1120ND20.4 22.7
1,3-Dichloropropane ug/L 20 96 60-140109 1220ND19.3 21.8
1,4-Dichlorobenzene ug/L 20 100 60-140113 1220ND20.0 22.6
2,2-Dichloropropane ug/L 20 108 60-140121 1120ND21.7 24.2
2-Chlorotoluene ug/L 20 101 60-140110 920ND20.2 22.0
4-Chlorotoluene ug/L 20 98 60-140111 1220ND19.6 22.2
Benzene ug/L 20 103 60-140114 1020ND20.6 22.8
Bromobenzene ug/L 20 97 60-140110 1220ND19.4 22.0
Bromochloromethane ug/L 20 100 60-140118 1620ND20.0 23.5
Bromodichloromethane ug/L 20 103 60-140114 1020ND20.6 22.8
Bromoform ug/L 20 102 60-140115 1220ND20.5 23.0
Bromomethane ug/L 20 75 60-14089 1720ND15.1 17.9
Carbon tetrachloride ug/L 20 116 60-140132 1320ND23.2 26.5
Chlorobenzene ug/L 20 97 60-140110 1320ND19.3 22.0
Chloroethane ug/L 20 100 60-140114 1420ND19.9 22.9
Chloroform ug/L 20 98 60-140109 1020ND19.7 21.8
Chloromethane ug/L 20 85 60-14094 1020ND17.1 18.9
cis-1,2-Dichloroethene ug/L 20 99 60-140113 1420ND19.7 22.6
cis-1,3-Dichloropropene ug/L 20 105 60-140115 920ND20.9 23.0
Dibromochloromethane ug/L 20 104 60-140115 1020ND20.7 23.0
Dibromomethane ug/L 20 97 60-140108 1020ND19.5 21.6
Dichlorodifluoromethane ug/L 20 71 60-14080 1220ND14.2 16.0
Diisopropyl ether ug/L 20 92 60-140105 1220ND18.5 20.9
Ethylbenzene ug/L 20 98 60-140111 1220ND19.6 22.1
Hexachloro-1,3-butadiene ug/L 20 108 60-140121 1220ND21.5 24.2
Isopropylbenzene (Cumene)ug/L 20 107 60-140120 1120ND21.5 24.1
m&p-Xylene ug/L 40 100 60-140112 1240ND39.8 44.8
Methyl-tert-butyl ether ug/L 20 93 60-140104 1120ND18.7 20.8
Methylene Chloride ug/L 20 102 60-140116 1220ND20.5 23.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4280504MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92709742005
4280505
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 109 60-140122 1120ND21.9 24.4
n-Propylbenzene ug/L 20 101 60-140113 1120ND20.3 22.7
Naphthalene ug/L 20 97 60-140108 1120ND19.3 21.6
o-Xylene ug/L 20 101 60-140109 820ND20.2 21.8
sec-Butylbenzene ug/L 20 104 60-140118 1320ND20.8 23.7
Styrene ug/L 20 100 60-140112 1220ND19.9 22.4
tert-Butylbenzene ug/L 20 87 60-14097 1120ND17.4 19.4
Tetrachloroethene ug/L 20 99 60-140112 1220ND19.8 22.4
Toluene ug/L 20 99 60-140109 1020ND19.8 21.9
trans-1,2-Dichloroethene ug/L 20 102 60-140115 1320ND20.3 23.0
trans-1,3-Dichloropropene ug/L 20 106 60-140115 820ND21.1 22.9
Trichloroethene ug/L 20 107 60-140119 1120ND21.3 23.7
Trichlorofluoromethane ug/L 20 108 60-140120 1120ND21.5 24.0
Vinyl chloride ug/L 20 84 60-14094 1120ND16.9 18.9
1,2-Dichloroethane-d4 (S)%101 70-130100
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%102 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
827898
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92709767009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4280515
Associated Lab Samples:92709767009
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 01/26/24 03:42
1,1,1-Trichloroethane ug/L ND 0.50 01/26/24 03:42
1,1,2,2-Tetrachloroethane ug/L ND 0.50 01/26/24 03:42
1,1,2-Trichloroethane ug/L ND 0.50 01/26/24 03:42
1,1-Dichloroethane ug/L ND 0.50 01/26/24 03:42
1,1-Dichloroethene ug/L ND 0.50 01/26/24 03:42
1,1-Dichloropropene ug/L ND 0.50 01/26/24 03:42
1,2,3-Trichlorobenzene ug/L ND 2.0 01/26/24 03:42
1,2,3-Trichloropropane ug/L ND 0.50 01/26/24 03:42
1,2,4-Trichlorobenzene ug/L ND 2.0 01/26/24 03:42
1,2,4-Trimethylbenzene ug/L ND 0.50 01/26/24 03:42
1,2-Dibromo-3-chloropropane ug/L ND 1.0 01/26/24 03:42
1,2-Dibromoethane (EDB)ug/L ND 0.50 01/26/24 03:42
1,2-Dichlorobenzene ug/L ND 0.50 01/26/24 03:42
1,2-Dichloroethane ug/L ND 0.50 01/26/24 03:42
1,2-Dichloropropane ug/L ND 0.50 01/26/24 03:42
1,3,5-Trimethylbenzene ug/L ND 0.50 01/26/24 03:42
1,3-Dichlorobenzene ug/L ND 0.50 01/26/24 03:42
1,3-Dichloropropane ug/L ND 0.50 01/26/24 03:42
1,4-Dichlorobenzene ug/L ND 0.50 01/26/24 03:42
2,2-Dichloropropane ug/L ND 0.50 01/26/24 03:42
2-Chlorotoluene ug/L ND 0.50 01/26/24 03:42
4-Chlorotoluene ug/L ND 0.50 01/26/24 03:42
Benzene ug/L ND 0.50 01/26/24 03:42
Bromobenzene ug/L ND 0.50 01/26/24 03:42
Bromochloromethane ug/L ND 0.50 01/26/24 03:42
Bromodichloromethane ug/L ND 0.50 01/26/24 03:42
Bromoform ug/L ND 0.50 01/26/24 03:42
Bromomethane ug/L ND 5.0 01/26/24 03:42
Carbon tetrachloride ug/L ND 0.50 01/26/24 03:42
Chlorobenzene ug/L ND 0.50 01/26/24 03:42
Chloroethane ug/L ND 1.0 01/26/24 03:42
Chloroform ug/L ND 0.50 01/26/24 03:42
Chloromethane ug/L ND 1.0 01/26/24 03:42
cis-1,2-Dichloroethene ug/L ND 0.50 01/26/24 03:42
cis-1,3-Dichloropropene ug/L ND 0.50 01/26/24 03:42
Dibromochloromethane ug/L ND 0.50 01/26/24 03:42
Dibromomethane ug/L ND 0.50 01/26/24 03:42
Dichlorodifluoromethane ug/L ND 0.50 01/26/24 03:42
Diisopropyl ether ug/L ND 0.50 01/26/24 03:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4280515
Associated Lab Samples:92709767009
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 01/26/24 03:42
Hexachloro-1,3-butadiene ug/L ND 2.0 01/26/24 03:42
Isopropylbenzene (Cumene)ug/L ND 0.50 01/26/24 03:42
m&p-Xylene ug/L ND 1.0 01/26/24 03:42
Methyl-tert-butyl ether ug/L ND 0.50 01/26/24 03:42
Methylene Chloride ug/L ND 2.0 01/26/24 03:42
n-Butylbenzene ug/L ND 0.50 01/26/24 03:42
n-Propylbenzene ug/L ND 0.50 01/26/24 03:42
Naphthalene ug/L ND 2.0 01/26/24 03:42
o-Xylene ug/L ND 0.50 01/26/24 03:42
sec-Butylbenzene ug/L ND 0.50 01/26/24 03:42
Styrene ug/L ND 0.50 01/26/24 03:42
tert-Butylbenzene ug/L ND 0.50 01/26/24 03:42
Tetrachloroethene ug/L ND 0.50 01/26/24 03:42
Toluene ug/L ND 0.50 01/26/24 03:42
trans-1,2-Dichloroethene ug/L ND 0.50 01/26/24 03:42
trans-1,3-Dichloropropene ug/L ND 0.50 01/26/24 03:42
Trichloroethene ug/L ND 0.50 01/26/24 03:42
Trichlorofluoromethane ug/L ND 1.0 01/26/24 03:42
Vinyl chloride ug/L ND 1.0 01/26/24 03:42
1,2-Dichloroethane-d4 (S)%97 70-130 01/26/24 03:42
4-Bromofluorobenzene (S)%100 70-130 01/26/24 03:42
Toluene-d8 (S)%99 70-130 01/26/24 03:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4280516LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.920 104 60-140
1,1,1-Trichloroethane ug/L 20.420 102 60-140
1,1,2,2-Tetrachloroethane ug/L 20.920 105 60-140
1,1,2-Trichloroethane ug/L 20.820 104 60-140
1,1-Dichloroethane ug/L 20.020 100 60-140
1,1-Dichloroethene ug/L 20.020 100 60-140
1,1-Dichloropropene ug/L 20.820 104 60-140
1,2,3-Trichlorobenzene ug/L 17.420 87 60-140
1,2,3-Trichloropropane ug/L 19.720 99 60-140
1,2,4-Trichlorobenzene ug/L 17.720 89 60-140
1,2,4-Trimethylbenzene ug/L 21.520 107 60-140
1,2-Dibromo-3-chloropropane ug/L 20.720 104 60-140
1,2-Dibromoethane (EDB)ug/L 21.320 106 60-140
1,2-Dichlorobenzene ug/L 20.320 102 60-140
1,2-Dichloroethane ug/L 19.920 100 60-140
1,2-Dichloropropane ug/L 21.520 107 60-140
1,3,5-Trimethylbenzene ug/L 21.720 108 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4280516LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 20.220 101 60-140
1,3-Dichloropropane ug/L 20.620 103 60-140
1,4-Dichlorobenzene ug/L 19.820 99 60-140
2,2-Dichloropropane ug/L 19.520 98 60-140
2-Chlorotoluene ug/L 20.820 104 60-140
4-Chlorotoluene ug/L 21.320 106 60-140
Benzene ug/L 20.220 101 60-140
Bromobenzene ug/L 20.020 100 60-140
Bromochloromethane ug/L 19.820 99 60-140
Bromodichloromethane ug/L 20.620 103 60-140
Bromoform ug/L 20.820 104 60-140
Bromomethane ug/L 18.520 92 60-140
Carbon tetrachloride ug/L 21.120 106 60-140
Chlorobenzene ug/L 20.020 100 60-140
Chloroethane ug/L 20.520 102 60-140
Chloroform ug/L 19.620 98 60-140
Chloromethane ug/L 21.720 108 60-140
cis-1,2-Dichloroethene ug/L 20.220 101 60-140
cis-1,3-Dichloropropene ug/L 21.420 107 60-140
Dibromochloromethane ug/L 20.520 102 60-140
Dibromomethane ug/L 20.020 100 60-140
Dichlorodifluoromethane ug/L 17.020 85 60-140
Diisopropyl ether ug/L 19.720 99 60-140
Ethylbenzene ug/L 20.320 102 60-140
Hexachloro-1,3-butadiene ug/L 19.420 97 60-140
Isopropylbenzene (Cumene)ug/L 21.320 106 60-140
m&p-Xylene ug/L 41.840 105 60-140
Methyl-tert-butyl ether ug/L 18.920 95 60-140
Methylene Chloride ug/L 20.620 103 60-140
n-Butylbenzene ug/L 20.920 105 60-140
n-Propylbenzene ug/L 20.720 103 60-140
Naphthalene ug/L 19.220 96 60-140
o-Xylene ug/L 20.720 103 60-140
sec-Butylbenzene ug/L 21.020 105 60-140
Styrene ug/L 21.320 106 60-140
tert-Butylbenzene ug/L 17.520 87 60-140
Tetrachloroethene ug/L 19.320 96 60-140
Toluene ug/L 20.220 101 60-140
trans-1,2-Dichloroethene ug/L 20.420 102 60-140
trans-1,3-Dichloropropene ug/L 21.720 109 60-140
Trichloroethene ug/L 20.220 101 60-140
Trichlorofluoromethane ug/L 18.520 93 60-140
Vinyl chloride ug/L 19.020 95 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4280517MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92709760001
4280518
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 102 60-140106 420ND20.4 21.2
1,1,1-Trichloroethane ug/L 20 106 60-140109 320ND21.2 21.8
1,1,2,2-Tetrachloroethane ug/L 20 105 60-140102 220ND20.9 20.4
1,1,2-Trichloroethane ug/L 20 102 60-140102 020ND20.4 20.3
1,1-Dichloroethane ug/L 20 106 60-140107 120ND21.1 21.3
1,1-Dichloroethene ug/L 20 112 60-140111 120ND22.5 22.3
1,1-Dichloropropene ug/L 20 112 60-140111 020ND22.3 22.2
1,2,3-Trichlorobenzene ug/L 20 85 60-14082 320ND17.0 16.5
1,2,3-Trichloropropane ug/L 20 104 60-140100 420ND20.8 20.1
1,2,4-Trichlorobenzene ug/L 20 87 60-14087 020ND17.4 17.4
1,2,4-Trimethylbenzene ug/L 20 105 60-140107 220ND21.1 21.5
1,2-Dibromo-3-chloropropane ug/L 20 99 60-14094 520ND19.7 18.8
1,2-Dibromoethane (EDB)ug/L 20 104 60-140106 220ND20.8 21.3
1,2-Dichlorobenzene ug/L 20 99 60-140102 220ND19.8 20.3
1,2-Dichloroethane ug/L 20 103 60-140103 120ND20.7 20.5
1,2-Dichloropropane ug/L 20 108 60-140109 120ND21.6 21.8
1,3,5-Trimethylbenzene ug/L 20 106 60-140110 320ND21.3 22.0
1,3-Dichlorobenzene ug/L 20 100 60-140103 320ND20.0 20.6
1,3-Dichloropropane ug/L 20 102 60-140104 220ND20.4 20.7
1,4-Dichlorobenzene ug/L 20 96 60-14099 320ND19.3 19.8
2,2-Dichloropropane ug/L 20 106 60-140112 520ND21.2 22.3
2-Chlorotoluene ug/L 20 104 60-140107 320ND20.8 21.4
4-Chlorotoluene ug/L 20 104 60-140107 320ND20.8 21.4
Benzene ug/L 20 104 60-140106 220ND21.0 21.4
Bromobenzene ug/L 20 97 60-140101 420ND19.5 20.3
Bromochloromethane ug/L 20 103 60-140100 220ND20.5 20.0
Bromodichloromethane ug/L 20 102 60-140103 220ND20.4 20.7
Bromoform ug/L 20 98 60-140100 220ND19.6 20.1
Bromomethane ug/L 20 65 60-14078 1720ND13.1 15.6
Carbon tetrachloride ug/L 20 110 60-140113 220ND22.0 22.5
Chlorobenzene ug/L 20 100 60-140102 220ND20.1 20.4
Chloroethane ug/L 20 127 60-140121 520ND25.5 24.2
Chloroform ug/L 20 101 60-140102 120ND20.1 20.3
Chloromethane ug/L 20 123 60-140124 120ND24.8 25.0
cis-1,2-Dichloroethene ug/L 20 105 60-140107 220ND21.0 21.3
cis-1,3-Dichloropropene ug/L 20 102 60-140104 220ND20.4 20.8
Dibromochloromethane ug/L 20 101 60-140104 320ND20.3 20.8
Dibromomethane ug/L 20 98 60-14099 220ND19.6 19.9
Dichlorodifluoromethane ug/L 20 129 60-140129 020ND25.7 25.8
Diisopropyl ether ug/L 20 101 60-140102 120ND20.3 20.6
Ethylbenzene ug/L 20 103 60-140106 320ND20.6 21.3
Hexachloro-1,3-butadiene ug/L 20 92 60-14093 120ND18.4 18.7
Isopropylbenzene (Cumene)ug/L 20 106 60-140109 320ND21.2 21.9
m&p-Xylene ug/L 40 105 60-140107 240ND42.1 42.9
Methyl-tert-butyl ether ug/L 20 94 60-14094 0200.88 19.7 19.7
Methylene Chloride ug/L 20 107 60-140106 120ND21.4 21.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4280517MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92709760001
4280518
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 102 60-140104 220ND20.5 20.9
n-Propylbenzene ug/L 20 104 60-140106 220ND20.8 21.2
Naphthalene ug/L 20 92 60-14091 220ND18.5 18.2
o-Xylene ug/L 20 104 60-140107 320ND20.8 21.3
sec-Butylbenzene ug/L 20 104 60-140108 320ND21.2 21.9
Styrene ug/L 20 106 60-140108 220ND21.1 21.6
tert-Butylbenzene ug/L 20 86 60-14089 320ND17.3 17.8
Tetrachloroethene ug/L 20 99 60-140102 320ND19.9 20.5
Toluene ug/L 20 102 60-140102 120ND20.3 20.5
trans-1,2-Dichloroethene ug/L 20 109 60-140109 020ND21.8 21.7
trans-1,3-Dichloropropene ug/L 20 103 60-140104 220ND20.5 20.8
Trichloroethene ug/L 20 102 60-140103 120ND20.5 20.7
Trichlorofluoromethane ug/L 20 111 60-140112 120ND22.2 22.4
Vinyl chloride ug/L 20 115 60-140117 120ND23.1 23.4
1,2-Dichloroethane-d4 (S)%99 70-130100
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
828518
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92709767002, 92709767003, 92709767006, 92709767007, 92709767008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4283088
Associated Lab Samples:92709767002, 92709767003, 92709767006, 92709767007, 92709767008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 01/29/24 12:34
1,1,1-Trichloroethane ug/L ND 0.50 01/29/24 12:34
1,1,2,2-Tetrachloroethane ug/L ND 0.50 01/29/24 12:34
1,1,2-Trichloroethane ug/L ND 0.50 01/29/24 12:34
1,1-Dichloroethane ug/L ND 0.50 01/29/24 12:34
1,1-Dichloroethene ug/L ND 0.50 01/29/24 12:34
1,1-Dichloropropene ug/L ND 0.50 01/29/24 12:34
1,2,3-Trichlorobenzene ug/L ND 2.0 01/29/24 12:34
1,2,3-Trichloropropane ug/L ND 0.50 01/29/24 12:34
1,2,4-Trichlorobenzene ug/L ND 2.0 01/29/24 12:34
1,2,4-Trimethylbenzene ug/L ND 0.50 01/29/24 12:34
1,2-Dibromo-3-chloropropane ug/L ND 1.0 01/29/24 12:34
1,2-Dibromoethane (EDB)ug/L ND 0.50 01/29/24 12:34
1,2-Dichlorobenzene ug/L ND 0.50 01/29/24 12:34
1,2-Dichloroethane ug/L ND 0.50 01/29/24 12:34
1,2-Dichloropropane ug/L ND 0.50 01/29/24 12:34
1,3,5-Trimethylbenzene ug/L ND 0.50 01/29/24 12:34
1,3-Dichlorobenzene ug/L ND 0.50 01/29/24 12:34
1,3-Dichloropropane ug/L ND 0.50 01/29/24 12:34
1,4-Dichlorobenzene ug/L ND 0.50 01/29/24 12:34
2,2-Dichloropropane ug/L ND 0.50 01/29/24 12:34
2-Chlorotoluene ug/L ND 0.50 01/29/24 12:34
4-Chlorotoluene ug/L ND 0.50 01/29/24 12:34
Benzene ug/L ND 0.50 01/29/24 12:34
Bromobenzene ug/L ND 0.50 01/29/24 12:34
Bromochloromethane ug/L ND 0.50 01/29/24 12:34
Bromodichloromethane ug/L ND 0.50 01/29/24 12:34
Bromoform ug/L ND 0.50 01/29/24 12:34
Bromomethane ug/L ND 5.0 01/29/24 12:34
Carbon tetrachloride ug/L ND 0.50 01/29/24 12:34
Chlorobenzene ug/L ND 0.50 01/29/24 12:34
Chloroethane ug/L ND 1.0 01/29/24 12:34
Chloroform ug/L ND 0.50 01/29/24 12:34
Chloromethane ug/L ND 1.0 01/29/24 12:34
cis-1,2-Dichloroethene ug/L ND 0.50 01/29/24 12:34
cis-1,3-Dichloropropene ug/L ND 0.50 01/29/24 12:34
Dibromochloromethane ug/L ND 0.50 01/29/24 12:34
Dibromomethane ug/L ND 0.50 01/29/24 12:34
Dichlorodifluoromethane ug/L ND 0.50 01/29/24 12:34
Diisopropyl ether ug/L ND 0.50 01/29/24 12:34
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4283088
Associated Lab Samples:92709767002, 92709767003, 92709767006, 92709767007, 92709767008
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 01/29/24 12:34
Hexachloro-1,3-butadiene ug/L ND 2.0 01/29/24 12:34
Isopropylbenzene (Cumene)ug/L ND 0.50 01/29/24 12:34
m&p-Xylene ug/L ND 1.0 01/29/24 12:34
Methyl-tert-butyl ether ug/L ND 0.50 01/29/24 12:34
Methylene Chloride ug/L ND 2.0 01/29/24 12:34
n-Butylbenzene ug/L ND 0.50 01/29/24 12:34
n-Propylbenzene ug/L ND 0.50 01/29/24 12:34
Naphthalene ug/L ND 2.0 01/29/24 12:34
o-Xylene ug/L ND 0.50 01/29/24 12:34
sec-Butylbenzene ug/L ND 0.50 01/29/24 12:34
Styrene ug/L ND 0.50 01/29/24 12:34
tert-Butylbenzene ug/L ND 0.50 01/29/24 12:34
Tetrachloroethene ug/L ND 0.50 01/29/24 12:34
Toluene ug/L ND 0.50 01/29/24 12:34
trans-1,2-Dichloroethene ug/L ND 0.50 01/29/24 12:34
trans-1,3-Dichloropropene ug/L ND 0.50 01/29/24 12:34
Trichloroethene ug/L ND 0.50 01/29/24 12:34
Trichlorofluoromethane ug/L ND 1.0 01/29/24 12:34
Vinyl chloride ug/L ND 1.0 01/29/24 12:34
1,2-Dichloroethane-d4 (S)%110 70-130 01/29/24 12:34
4-Bromofluorobenzene (S)%99 70-130 01/29/24 12:34
Toluene-d8 (S)%99 70-130 01/29/24 12:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4283089LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 22.020 110 60-140
1,1,1-Trichloroethane ug/L 23.020 115 60-140
1,1,2,2-Tetrachloroethane ug/L 21.120 105 60-140
1,1,2-Trichloroethane ug/L 21.420 107 60-140
1,1-Dichloroethane ug/L 21.720 108 60-140
1,1-Dichloroethene ug/L 25.020 125 60-140
1,1-Dichloropropene ug/L 23.820 119 60-140
1,2,3-Trichlorobenzene ug/L 22.420 112 60-140
1,2,3-Trichloropropane ug/L 20.820 104 60-140
1,2,4-Trichlorobenzene ug/L 21.720 109 60-140
1,2,4-Trimethylbenzene ug/L 23.220 116 60-140
1,2-Dibromo-3-chloropropane ug/L 20.120 101 60-140
1,2-Dibromoethane (EDB)ug/L 21.920 109 60-140
1,2-Dichlorobenzene ug/L 22.120 111 60-140
1,2-Dichloroethane ug/L 22.420 112 60-140
1,2-Dichloropropane ug/L 21.420 107 60-140
1,3,5-Trimethylbenzene ug/L 23.120 116 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4283089LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 22.120 110 60-140
1,3-Dichloropropane ug/L 21.320 107 60-140
1,4-Dichlorobenzene ug/L 21.520 107 60-140
2,2-Dichloropropane ug/L 23.320 116 60-140
2-Chlorotoluene ug/L 22.120 111 60-140
4-Chlorotoluene ug/L 22.920 115 60-140
Benzene ug/L 21.120 106 60-140
Bromobenzene ug/L 20.820 104 60-140
Bromochloromethane ug/L 21.720 108 60-140
Bromodichloromethane ug/L 21.220 106 60-140
Bromoform ug/L 20.820 104 60-140
Bromomethane ug/L 22.320 112 60-140
Carbon tetrachloride ug/L 21.820 109 60-140
Chlorobenzene ug/L 21.120 106 60-140
Chloroethane ug/L 26.120 130 60-140
Chloroform ug/L 21.520 107 60-140
Chloromethane ug/L 18.820 94 60-140
cis-1,2-Dichloroethene ug/L 22.120 110 60-140
cis-1,3-Dichloropropene ug/L 21.720 109 60-140
Dibromochloromethane ug/L 21.820 109 60-140
Dibromomethane ug/L 20.520 103 60-140
Dichlorodifluoromethane ug/L 23.020 115 60-140
Diisopropyl ether ug/L 21.020 105 60-140
Ethylbenzene ug/L 21.520 107 60-140
Hexachloro-1,3-butadiene ug/L 23.620 118 60-140
Isopropylbenzene (Cumene)ug/L 22.720 113 60-140
m&p-Xylene ug/L 44.240 111 60-140
Methyl-tert-butyl ether ug/L 20.220 101 60-140
Methylene Chloride ug/L 20.720 103 60-140
n-Butylbenzene ug/L 24.620 123 60-140
n-Propylbenzene ug/L 22.520 112 60-140
Naphthalene ug/L 20.220 101 60-140
o-Xylene ug/L 21.420 107 60-140
sec-Butylbenzene ug/L 22.820 114 60-140
Styrene ug/L 22.220 111 60-140
tert-Butylbenzene ug/L 18.020 90 60-140
Tetrachloroethene ug/L 21.420 107 60-140
Toluene ug/L 20.420 102 60-140
trans-1,2-Dichloroethene ug/L 22.520 113 60-140
trans-1,3-Dichloropropene ug/L 22.120 110 60-140
Trichloroethene ug/L 21.920 109 60-140
Trichlorofluoromethane ug/L 22.020 110 60-140
Vinyl chloride ug/L 18.920 94 60-140
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4283090MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92710139002
4283091
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 113 60-140114 120<0.091 22.5 22.8
1,1,1-Trichloroethane ug/L 20 126 60-140125 020<0.11 25.1 25.0
1,1,2,2-Tetrachloroethane ug/L 20 107 60-140111 420<0.074 21.4 22.3
1,1,2-Trichloroethane ug/L 20 110 60-140112 220<0.096 21.9 22.4
1,1-Dichloroethane ug/L 20 120 60-140119 120<0.056 24.0 23.9
1,1-Dichloroethene ug/L 20 139 60-140136 220<0.079 27.7 27.3
1,1-Dichloropropene ug/L 20 133 60-140131 220<0.066 26.6 26.2
1,2,3-Trichlorobenzene ug/L 20 81 60-140102 2320<0.12 16.1 20.3
1,2,3-Trichloropropane ug/L 20 104 60-140106 320<0.17 20.7 21.3
1,2,4-Trichlorobenzene ug/L 20 88 60-140102 1520<0.16 17.6 20.4
1,2,4-Trimethylbenzene ug/L 20 116 60-140118 220<0.031 23.3 23.6
1,2-Dibromo-3-chloropropane ug/L 20 96 60-140106 1020<0.18 19.1 21.1
1,2-Dibromoethane (EDB)ug/L 20 111 60-140115 420<0.15 22.1 23.0
1,2-Dichlorobenzene ug/L 20 106 60-140111 520<0.094 21.3 22.3
1,2-Dichloroethane ug/L 20 122 60-140122 020<0.11 24.4 24.4
1,2-Dichloropropane ug/L 20 113 60-140114 120<0.14 22.6 22.9
1,3,5-Trimethylbenzene ug/L 20 116 60-140116 020<0.071 23.2 23.2
1,3-Dichlorobenzene ug/L 20 110 60-140112 220<0.098 22.0 22.4
1,3-Dichloropropane ug/L 20 111 60-140113 220<0.085 22.2 22.6
1,4-Dichlorobenzene ug/L 20 106 60-140108 220<0.090 21.1 21.7
2,2-Dichloropropane ug/L 20 122 60-140121 020<0.12 24.3 24.3
2-Chlorotoluene ug/L 20 114 60-140114 020<0.13 22.7 22.8
4-Chlorotoluene ug/L 20 115 60-140117 220<0.096 22.9 23.3
Benzene ug/L 20 114 60-140114 020<0.079 22.9 22.8
Bromobenzene ug/L 20 108 60-140107 120<0.14 21.6 21.5
Bromochloromethane ug/L 20 118 60-140118 120<0.094 23.7 23.6
Bromodichloromethane ug/L 20 111 60-140113 120<0.17 22.3 22.6
Bromoform ug/L 20 99 60-140105 520<0.20 19.9 20.9
Bromomethane ug/L 20 103 60-140108 520<0.22 20.6 21.6
Carbon tetrachloride ug/L 20 120 60-140119 020<0.17 23.9 23.8
Chlorobenzene ug/L 20 109 60-140110 120<0.085 21.7 22.0
Chloroethane ug/L M12014460-140138 520<0.17 28.8 27.6
Chloroform ug/L 20 118 60-140120 120<0.069 23.6 24.0
Chloromethane ug/L 20 95 60-14095 020<0.18 19.0 19.0
cis-1,2-Dichloroethene ug/L 20 123 60-140120 220<0.11 24.7 24.1
cis-1,3-Dichloropropene ug/L 20 107 60-140110 320<0.090 21.5 22.0
Dibromochloromethane ug/L 20 109 60-140113 320<0.15 21.9 22.5
Dibromomethane ug/L 20 107 60-140109 120<0.19 21.5 21.7
Dichlorodifluoromethane ug/L 20 105 60-140103 220<0.12 21.0 20.6
Diisopropyl ether ug/L 20 114 60-140114 020<0.072 22.8 22.8
Ethylbenzene ug/L 20 112 60-140113 120<0.081 22.4 22.5
Hexachloro-1,3-butadiene ug/L 20 101 60-140105 420<0.35 20.2 21.0
Isopropylbenzene (Cumene)ug/L 20 116 60-140118 120<0.11 23.2 23.5
m&p-Xylene ug/L 40 114 60-140115 140<0.094 45.7 46.0
Methyl-tert-butyl ether ug/L 20 106 60-140109 320<0.053 21.2 21.8
Methylene Chloride ug/L 20 113 60-140118 420<1.9 22.7 23.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4283090MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92710139002
4283091
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 119 60-140121 120<0.066 23.8 24.2
n-Propylbenzene ug/L 20 115 60-140114 020<0.10 22.9 22.8
Naphthalene ug/L 20 86 60-140101 1620<0.10 17.1 20.2
o-Xylene ug/L 20 113 60-140113 020<0.14 22.5 22.5
sec-Butylbenzene ug/L 20 114 60-140115 120<0.085 22.8 23.0
Styrene ug/L 20 114 60-140115 120<0.14 22.7 23.0
tert-Butylbenzene ug/L 20 91 60-14092 020<0.086 18.3 18.3
Tetrachloroethene ug/L 20 111 60-140112 120<0.086 22.1 22.4
Toluene ug/L 20 109 60-140111 220<0.090 21.8 22.2
trans-1,2-Dichloroethene ug/L 20 125 60-140124 120<0.10 25.0 24.7
trans-1,3-Dichloropropene ug/L 20 111 60-140113 220<0.13 22.1 22.5
Trichloroethene ug/L 20 116 60-140114 120<0.17 23.1 22.9
Trichlorofluoromethane ug/L 20 124 60-140120 320<0.14 24.7 24.0
Vinyl chloride ug/L 20 99 60-14097 220<0.15 19.8 19.5
1,2-Dichloroethane-d4 (S)%111 70-130109
4-Bromofluorobenzene (S)%103 70-130104
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92709767
One Stop 15 1/22/24
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92709767001 827894MW-5 SM 6200B
92709767002 828518MW-2 SM 6200B
92709767003 828518MW-9 SM 6200B
92709767004 827894MW-6 SM 6200B
92709767005 827894MW-7 SM 6200B
92709767006 828518MW-4 SM 6200B
92709767007 828518MW-8 SM 6200B
92709767008 828518MW-1R SM 6200B
92709767009 827898WSW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2024 08:53 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 41
Page 39 of 41
Page 40 of 41
Page 41 of 41