NCD991278953_200208_National Starch_2001 Site Monitoring Report

• R E P O R T Ji
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2001 Site Monitoring Report
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10029866
Nationa l Starc h & Chemica l Compan y
Salisbury, North Carolina
August 200 2
BBTBLASLAND, BOUC K & LEE , INC.engineers & scientists
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| 2001 Site Monitoring Report
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I Nationa l Starch & Chemica l Compan y
- Salisbury, North Carolina
. August 2002
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Table of Contents
Section 1. lntroduction..............................................................................................................1-1
1.1 Purpos e and Objectives................................................................................................... 1-1
1.2 Monitoring Progra m Overview......................................................................................... 1-2
1.2.1 Operable Units One and Two .............................................................................1-2
1.2.2 Operable Unit Three ...........................................................................................1-3
1.2.2.1 Groundwate r Monitoring...................................................................... 1-3
1.2.2.2 Surfac e Water Monitoring ...................................................................1-4
1.2.2.3 Sediment Monitoring ...........................................................................1-4
1.2.2.4 RCR A Sampling ..................................................................................1-4
1.3 Repor t Organization......................................................................................................... 1-4
Section 2. Field Procedures.....................................................................................................^-!
2.1 Water Level Measurement...............................................................................................2-1
2.1.1 Operable Units One andTwo.............................................................................2-12.1.2 Operable Unit Three ...........................................................................................2-1
2.2 Sample Collection............................................................................................................2-2
2.2.1 Operable Units One and Two .............................................................................2-2
2.2.2 Operable Unit Three ...........................................................................................2-2
2.2.3 RCR A Sampling..................................................................................................2-3
Sectio n 3. Result s .....................................................................................................................3-1
3.1 Groundwate r Elevations...................................................................................................3-1
3.1.1 Operable Units One and Two .............................................................................3-1
3.1.2 Operable Unit 3...................................................................................................3-1
3.2 Analytical Results.............................................................................................................3-1
3.2.1 Operable Units One and Two .............................................................................3-2
3.2.1.1 Plume Periphery Wells....................................................................r£3-2
3.2.1.2 Trenc h Are a Wells.........................................................................(T
3.2.2 Operable Unit Three .....................................................................................L
3.2.2.1 March 2002 ...................................................................................9
3.2.3 RCR A Sampling..................................................................................................3-5
3.2.3.1 July 2001 .......................................................................................^.«-5
3.2.3.2 February 2002.....................................................................................3-6
3.3 Pumping Data ..................................................................................................................3-7
Section 4. Data Validation.........................................................................................................^!
4.1 Laborator y Conformance.................................................................................................4-1
4.1.1 Operable Unit One..............................................................................................4-1
4.1.2 Operable Unit Three ...........................................................................................4-1
4.1.3 RCR A Sampling..................................................................................................4-2
4.2 Metho d Detectio n Limits and Dilutio n Factor s .................................................................4-2
4.2.1 Operable Unit One..............................................................................................4-2
4.2.1.1 Plume Periphery Wells........................................................................4-2
4.2.1.2 Trench Area Wells...............................................................................4-3
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4.2.2 Operable Unit Three ...........................................................................................4-3
4.2.3 RCR A Samples........................................................................................ ...........4-4
4.3 Blind Duplicat e Sample s ...................................................................................... ............4-5
4.3.1 Operable Unit One.................................................................................. ............4-5
4.3.2 Operable Unit Three ...........................................................................................4-5
4.3.3
Sectio n 5. Summar y ......................................................................................................... .........5-1
5.1 Groundwate r Quality and Trends........................................................................ ............. 5-1
5.2 Future Actions..................................................................................................................5-1
Tables
3-1 OU1/OU 2 Wate r Leve l Measurement s
3-2 OU 3 Wate r Level Measurement s
3-3 OU1 and OU3 Performanc e Standards
3-4 Compariso n of 2002 Analytica l Result s for Plum e Peripher y Wells to Performanc e Standard s
3-5 Historical Analytical Results - VOCs - Plume Periphery Extraction and Monitoring Wells
3-6 Historica l Analytica l Result s - SVOC s - Plum e Peripher y Extractio n and Monitoring Wells
3-7 Historica l Analytica l Result s - Metal s - Plume Peripher y Extractio n and Monitorin g Well s
3-8 Comparison of 2002 Analytical Result s for Trench Area Wells to Performanc e Standards
3-9 Historica l Analytica l Result s - VOC s - Trenc h Are a Extractio n and Monitorin g Wells
3-10 Historical Analytical Results - SVOC s - Trench Area Extractio n and Monitorin g Wells
3-1 1 Historica l Analytica l Result s - Metal s - Trenc h Area Extractio n and Monitorin g Wells
3-1 2 Comparison of 2002 Analytica l Result s for OU3 Wells to Performanc e Standards
3-1 3 Historical Analytical Results - VOCs - OU3 Extraction and Mbnitoring Wells
3-1 4 Historica l Analytica l Result s - SVOC s - OU3 Extractio n and Monitorin g Well s
3-15 Historical Analytical Results - Metals - OU3 Extractio n and Monitoring Well s
3-16 Compariso n of RCR A Analytica l Result s to Clas s GA Groundwate r Standard s - July 200 1
3-1 7 Compariso n of RCR A Analytical Results to Class GA Groundwate r Standards - February 2002
Figures
1-1 Site Location Map
1-2 Site Map
3-1 Groundwate r Elevation Contour Map for OU1/OU2 Saprolite Wells - Marc h 2002
3-2 Groundwate r Elevation Contour Map for OU1/OU2 Transition Zone Well s - March 2002
3-3 Groundwate r Elevation Contour Map for OU1/OU2 Bedrock Wells - March 2002
3-4 Groundwate r Elevation Contour Map for OU3 Saprolite and Transition Zone Wells - Marc h 2002
3-5 Groundwate r Elevation Contour Map for OU3 Bedrock Wells - March 2002
Appendi x
A Analytica l Form I's
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1. Introduction
Thi s Site Monitorin g Repor t present s the result s of th e annua l groundwate r monitorin g data for Operable Unit s
(OUs) 1, 2, and 3 at th e Nationa l Starc h & Chemica l Compan y (NSCC ) facilit y locate d on Ceda r Springs Roa d
in Salisbury , Nort h Carolin a (Figur e 1-1). OU 1 consist s of groundwate r locate d in the west-southwes t portio n
of th e facility , OU 2 consist s of soi l in the Trenc h Area , whic h is locate d west of the Productio n Area, and $U 3
consist s of groundwate r locate d i n th e eas t portio n o f th e facility . Groundwate r monitorin g is conducte d IB j .
accordanc e wit h the Record s of Decisio n (RODs ) issue d for OU1 , OU2, and OU3 by the United s^&s/** L
Environmenta l Protectio n Agenc y (USEPA ) in Septembe r 1988 , Septembe r 1990, and October 1993 ,
respectively .
1.1 Purpose and Objectives
The purpos e of the groundwate r monitorin g progra m is to provid e analytica l dat a to evaluat e the effectivenes s
and protectivenes s of the sit e remedia l actions . The objective s of the groundwate r monitorin g progra m for OU 1 .
and OU2 are as follows : j ^^n<> o-\/u
j^UtC^,monito r groundwate r for selecte d constituent s of concer n (COCs ) identifie d in the OU 1 ROD; i
evaluat e groundwate r qualit y relativ e to th e Performanc e Standard s identifie d in th e OU 1 ROD;
evaluat e groundwate r qualit y relativ e to histori c dat a to identif y concentratio n trends ;
collec t dat a to verif y curren t understandin g of sit e condition s as describe d in the conceptua l model; an d
provid e recommendation s base d on analytica l result s and histori c COC concentratio n trend s to improv e
the effectivenes s of th e monitorin g program .
The Plum e Peripher y Extractio n Syste m was shu t dow n in Januar y 2000. Th e Remedy Evaluation for
Unit One, submitte d in Novembe r 2000, conclude d tha t resumptio n of groundwate r pumpin g in any capacit y
woul d not furthe r the remedial objective s in the vicinit y of the Unname d Tributary . Th e focu s of the monitorin g
progra m ha s therefor e shifte d to monito r an d evaluat e wate r qualit y instea d of to monito r th e effectivenes s of the r ,
extractio n system . <=C "-Cl*L)|w
The objective s of the groundwater , surfac e water , and sedimen t monitorin g progra m for OU 3 are as follows :
• monito r groundwater , surfac e water , and sedimen t quality ;
• addres s vertica l delineatio n concern s per the OU3 ROD;
• collec t additiona l dat a to expan d the curren t site groundwater , surfac e water, and sedimen t qualit y
database ;
N)«> &
• evaluat e th e effectivenes s an d thoroughnes s of the existin g monitorin g syste m and evaluat e the nee d of
additiona l monitorin g well s to adequatel y monito r the extractio n syste m or if monitorin g points can be
eliminate d fro m the existin g monitorin g system ; an d
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• evaluat e if the present lis t of chemica l analyse s performe d on the groundwate r sample s is sufficient , or
shoul d be modified .
1.2 Monitoring Program Overvie w
Th e monitorin g program s fo r OU s 1 an d 2 an d OU 3 diffe r i n scope . The y wil l be describe d separatel y in th e
followin g sections.
1.2.1 Operabl e Units One and Two
Extractio n and monitorin g wells sample d as part of the monitorin g progra m for OU s I and 2 are show n in
Figur e 1 -2 an d includ e th e following :
• Plum e Peripher y Extractio n Wells : EX-01, EX-02, EX-03, and EX-04;
• Plum e Peripher y Monitorin g Wells : NS-29 , NS-30 , NS-31 , and NS-32 ;
• Trenc h Are a Extractio n Wells : EX-05, EX-06 , EX-07, EX-08, EX-09, and EX-10; and
• Trench Area Monitorin g Wells : NS-09, NS-10, NS-11, and NS-15.
Plum e Peripher y extractio n an d monitorin g well s wer e sample d quarterl y fo r 24 quarter s fro m firs t quarte r 1993
throug h fourt h quarte r 1998, wit h the exceptio n of extractio n wel l EX-02, whic h was not sample d durin g firs t
quarte r 1993. Trenc h Are a extractio n well s wer e sample d quarterl y fo r 11 quarter s fro m secon d quarte r 199 6
throug h fourt h quarte r 1998 , and Trenc h Area monitorin g well s were sample d quarterl y for 23 quarters fro m
second quarte r 1993 throug h fourt h quarte r 1998. Durin g the firs t quarter of 1999, NSCC requested tha t the
monitorin g frequenc y fo r th e Plum e Peripher y an d Trenc h Are a extractio n an d monitorin g well s b e reduce d
fro m quarterl y to annually . Th e reductio n in monitorin g frequenc y wa s approve d by the EPA . Annua l samplin g
commence d i n Decembe r 1999 fo r th e Plum e Peripher y monitorin g an d extractio n well s and Trench Are a
monitorin g wells . Samplin g o f th e Trenc h Are a extractio n well s wa s postpone d unti l February/Marc h 2000 ,
afte r the groundwate r pre-treatmen t plan t was in operation . The second annua l samplin g even t occurred in
December 2000. Annua l samplin g for OU1 and OU2 occurred in March 2002.
Groundwate r sample s collecte d fro m th e Plum e Peripher y an d Trenc h Are a extractio n an d monitorin g well s
have bee n analyze d for volatil e organi c compound s (VOCs), semivolatil e organi c compound s (SVOCs), an d
metals . Groundwate r COCs for OUs 1 and 2 includ e the followin g 14 VOCs, two SVOCs, and nin e metals:
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VOCs
Aceton e
Benzen e
Bromodichloromethan e
Chlorofor m
1,1-Dichloroethen e
1,2-Dichloroethan e
1,2-Dichloropropan e
Ethylbenzen e
Methylen e Chlorid e
Toluene
1 , 1 ,2-Trichloroethan e
Trichloroethen e
Viny l Chlorid e
Xylen e
SVOCs
4-Nitropheno l
Bis(2-chloroethyl)ethe r
Metal s
Arseni c
Bariu m
Berylliu m
Cadmiu m
Manganes e
Nicke l
Seleniu m
Zin c
1.2.2 Operable Unit Three
Monitorin g in OU3 consist s of groundwater , surfac e water , and sedimen t monitoring .
1.2.2.1 Groundwate r Monitorin g
Extractio n and monitorin g well s sample d as part of the monitorin g progra m for OU 3 includ e wells locate d
insid e an d outsid e th e groundwate r extractio n syste m zone of hydrauli c control :
• Well s Insid e Zone of Hydrauli c Control ;
- Monitorin g Wells : NS-13 , NS-14 , NS-39, NS-40, NS-41 , NS-42, NS-45 , NS-46, NS47, NS-48,
NS-50 , NS-52, NS-53, and NS-54;
Extractio n Wells : NS49 and NS-51 ;
Collectio n Trench: CT-1;
• Well s Outsid e Zon e of Hydrauli c Control ;
- Monitorin g Wells : NS-24, NS-35, NS-36, NS-37, NS-38 , NS-43, and NS-44.
Monitorin g well s in OU 3 wer e sample d tw o time s in 1998. Beginnin g in 1999 , monitorin g frequenc y fo r well s
in OU3 has followe d tha t propose d in the OU3 Performanc e Verificatio n Pla n (PVP). Th e PV P wa s submitte d
as an appendi x to th e OU 3 Fina l Desig n Repor t (BBL , 1998). Monitorin g well s locate d insid e the zone of
hydrauli c contro l ar e sample d annually . Monitorin g well s formerl y locate d outsid e th e zon e of hydrauli c
control , the extractio n wells , and the collectio n trenc h were sample d semi-annually . Semi-annua l sampling wa s
complete d in Januar y 2001 and occurre d for a perio d of tw o year s as outline d in the OU 3 PVP. Annua l
samplin g of all OU 3 monitorin g wells , extractio n wells , an d th e collectio n trenc h commence d in Januar y 2002 .
The OU3 annua l samplin g occurre d in Marc h 2002.
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2. Field Procedures
The annua l samplin g even t for OU1 , OU2 , and OU 3 wa s conducte d in Marc h 2002. Field samplin g procedure s
use d durin g each even t are discusse d below .
2.1 Wate r Level Measurement
Groundwate r leve l measurement s were mad e relativ e to the establishe d referenc e poin t on the wel l casing. Th e
dept h to wate r (DTW ) wa s measure d by introducin g an electroni c wate r leve l indicato r prob e int o each wel l an d
slowl y lowering the probe down the water column. The apparent DTW was recorded to the neares t 0.01 foo t at
the dept h indicate d by the pulsin g tone of the probe.
Prior to insertio n int o each well , the probe and prob e tap e wa s decontaminate d by a Liquino x an d ta p wate r
scru b followe d by a tap wate r rins e an d a distille d wate r rins e (USEP A 1996).
2.1.1 Operable Units One and Two
Wate r leve l measurement s wer e take n on Marc h 2, 2002 fro m tw o strea m gauge s (SG-1 an d SG-2) in the
Unname d Tributary , tw o surfac e water/sedimen t samplin g location s (UN-1 and UN-2), and the followin g
extractio n and monitorin g wells :
• Plum e Peripher y
Extractio n well s (4): EX-01 , EX-02, EX-03, and EX-04; and
Monitorin g well s (15): NS-05 , NS-06, NS-21 , NS-22 , NS-23, NS-26, NS-27, NS-28 , NS-29,
NS-30, NS-31 , NS-32 , P-01, P-02, and P-04.
• Trenc h Area
Extraction wells (6): EX-05, EX-06, EX-07, EX-08, EX-09, and EX-10; and
Monitorin g well s (13): NS-01 , NS-01A , NS-02, NS-03, NS-07 , NS-08, NS-09 , NS-10, NS-
11 , NS-12 , NS-15 , NS-16, and NS-17.
Table 3-1 present s th e OU1/OU 2 wate r leve l measurements . Th e stati c wate r level wa s not measure d in
monitorin g wel l NS-32 due to artesia n conditions , whic h have bee n presen t durin g all of the previou s samplin g
event s sinc e firs t quarte r 1993 . Artesia n condition s wer e also presen t i n monitorin g wel l NS-30 . Th e stati c
wate r leve l in monitorin g well s NS-01, NS-0 1 A, P-01, and NS-05 were unabl e to be measure d because the well s -,
were dry . The dry condition in NS-05 has been present since the fourt h quarte r 1998 sampling event. The stati c ~"
wate r leve l wa s no t measure d at SG-2 becaus e th e strea m gaug e wa s damaged . Extractio n wel l EX-08 coul d not'~
be accessed ; therefore , the stati c wate r leve l was not measured .
2.1.2 Operabl e Uni t Thre e
Wate r leve l measurement s wer e take n on Marc h 5, 2002 fro m the followin g strea m gauges , monitorin g wells ,
an d extractio n points :
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• Strea m gauges (3): NT-1, NT-2, and NT-3;
• Monitorin g wells (23): NS-13, NS-14, NS-24, NS-33, NS-34, NS-35, NS-36, NS-37, NS-38, NS-39 ,
NS-40, NS-41 , NS-42 , NS-43, NS-44, NS-45 , NS-46 , NS-47 , NS-48 , NS-50, NS-52 , NS-53, and NS -
54; and
• Extractio n points (3): NS-49, NS-51, and CT-1.
Table 3-2 presents th e OU 3 wate r leve l measurements . Th e stati c wate r leve l in monitorin g wel l NS-1 4 and
strea m gauge NT-1 were unabl e to be measure d because the well and gauge wer e dry.
2.2 Sample Collection
2.2.1 Operabl e Units One and Two
As indicate d in Section 1.2, groundwate r samples were collecte d fro m the followin g wells:
• Plume Periphery
Extractio n wells (4): EX-01, EX-02, EX-03, and EX-04; and
Monitorin g wells (4): NS-29, NS-30, NS-31, and NS-32.
• Trenc h Area
Extractio n well s (6): EX-05 , EX-06, EX-07, EX-08, EX-09, and EX-10; and
Monitorin g well s (4): NS-09, NS-10, NS-11 , and NS-15.
Groundwate r sample s wer e collecte d by fillin g sampl e jars directl y fro m th e dedicate d pump s locate d in eac h
well, with the exception of wells NS-09, NS-10, NS-11, NS-31, and NS-32, which do not contain dedicated
pumps . The extractio n wells were sampled by openin g the sample port and allowin g 3.0 gallons of water to
flo w fro m the samplin g port. Th e sample jars were the n fille d directl y from the port. Three wel l volume s wer e
purge d fro m the monitorin g well s whic h contained dedicate d pumps . Afte r purging , the sampl e bottles wer e
fille d directl y fro m the discharg e line . Monitorin g well s whic h di d no t contai n dedicate d pump s were purge d
and sample d usin g a bladde r pum p as describe d in the OU 3 PVP.
QA/QC samples include d collectio n of on e "blind duplicate " sampl e collected at EX-02 an d one matrix spik e
(MS) and one matri x spike duplicat e (MSD ) sample at EX-01.
2.2.2 Operable Unit Three
In accordanc e wit h the OU 3 PVP, annua l samplin g was complete d in March 2002. Th e Marc h 2002 samplin g
even t include d samplin g well s insid e an d outside the zone of hydrauli c control. Samples wer e collected fro m
the followin g well s an d surfac e water/sedimen t locations :
• Wells Insid e Zone of Hydrauli c Control
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- Monitorin g Wells : NS-13 , NS-14 , NS-39, NS-40, NS-41 , NS-42 , NS-45, NS-46 , NS-47, NS48,
NS-50, NS-52, NS-53, and NS-54;
Extractio n Wells : NS-4 9 an d NS-51 ; an d
Collectio n Trench: CT-1.
• Well s Outsid e Zone of Hydrauli c Contro l
Monitorin g Wells : NS-24 , NS-35, NS-36, NS-37, NS-38 , NS-43, and NS-44.
Groundwate r sample s wer e collecte d usin g a decontaminate d bladde r pum p at each monitorin g wel l in
accordanc e wit h the OU 3 PVP, wit h the exceptio n of NS-24 whic h contain s a dedicate d bladde r pump. Th e
well s wer e pumpe d at rate s betwee n 15 0 an d 30 0 milliliter s pe r minut e (ml/min). Groundwate r parameter s
(temperature , pH, specifi c conductivity , dissolve d oxygen , turbidity , and oxidation-reductio n potential) wer e
collecte d ever y fiv e minute s whil e the wel l wa s bein g pumped . Th e groundwate r sample wa s collected fro m the
pum p discharg e lin e afte r the groundwate r parameter s had stabilize d accordin g to th e criteri a prescribed in the
OU3 PVP.
QA/QC sample s for th e Marc h 2002 samplin g even t include d collectio n of two "blin d duplicate " groundwate r
sample s at NS-51 and NS-52 an d tw o matri x spik e (MS) and two matri x spik e duplicat e (MSD ) samples at NS -
49 and NS-54.
2.2.3 RCR A Sampling
Samplin g event s for RCR A occu r on a semi-annua l basi s in accordanc e wit h th e Post Closur e Pla n for RCR A
Jurisdictiona l Units . Th e Jul y 2001 and Februar y 2002 samplin g event s include d samplin g well s withi n and
outsid e the zone of hydrauli c control . Sample s were collecte d fro m the followin g wells :
• Monitorin g Wells : NS-33, NS-39, and NS-42 ; and
• Extractio n Wells: NS-49.
QA/QC sample s for the Jul y 2001 and Februar y 2002 samplin g event s include d collectio n of on e "blin d
duplicate " groundwate r sampl e collecte d at NS-42 and one matri x spike (MS) and matri x spik e duplicat e (MSD )
sampl e at NS-49 durin g eac h samplin g event .
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3. Results
This section outlines the results of the groundwater elevation measurements, laboratory analyses of groundwater
samples , and pumpin g data for 2001.
3.1 Groundwater Elevations
3.1.1 Operabl e Units One and Two
DTW and groundwate r elevation s for th e OU 1 an d 2 Marc h 2002 samplin g event ar e liste d in Table 3-1.
Figure s 3-1, 3-2, an d 3-3 sho w groundwate r contour s fo r th e saprolite , transitio n zone, an d bedroc k wells ,
respectively , fo r the Marc h 2002 samplin g event . Groundwate r elevation s are consisten t wit h recen t
measurements . Groundwate r flo w is fro m the Trenc h Are a towar d the Unname d Tributary . Groundwate r flo w is
presume d to follo w topographi c feature s suc h a s th e swal e tha t is eviden t in th e are a o f well s NS-21 , NS-26 , an d
EX-02 .
3.1.2 Operabl e Unit 3
DT W and groundwate r elevation s for the Marc h 2002 OU 3 samplin g event are liste d in Table s 3-2. Figur e 3-4
show s groundwate r contour s for the saprolit e an d transitio n zon e well s an d Figure 3-5 show s groundwate r
contour s for the bedroc k well s for the 2002 samplin g event . Groundwate r elevation s are consisten t wit h recen t
measurements . Groundwate r contour s in th e saprolite , transitio n zone , an d bedroc k indicat e tha t groundwate r
flow s int o th e Northeas t Tributary .
The observe d groundwate r elevation s provid e agreemen t wit h the conceptua l mode l of groundwate r flo w at the
site described by the following :
• groundwate r flo w occur s withi n groundwate r compartment s roughl y coinciden t wit h the watershe d
boundarie s of th e Unname d an d Northeas t Tributaries ;
• groundwate r is introduce d to the compartment s throug h recharg e fro m precipitation ;
• groundwate r flow s both horizontall y and verticall y withi n the groundwate r compartment , ultimatel y
dischargin g to surfac e wate r in the stream ; an d
• du e to difference s in primar y porosity , the saprolit e and transitio n zone s act as storag e reservoir s and
fracture s withi n the underlyin g bedroc k act as conduit s fo r groundwate r fro m the overlyin g regolith .
3.2 Analytica l Results
Thi s section summarize s the curren t analytica l result s for groundwate r sample s relativ e to the Performanc e
Standard s an d historica l data . Th e OU 1 an d OU 3 Performanc e Standard s ar e presente d in Tabl e 3-3 wit h th e
Nort h Carolin a Groundwate r Standards .
BLASLAND , BOUCK & LEE , INC.
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3.2.1 Operable Units One and Two
Groundwate r sample s collecte d fro m th e Plum e Peripher y well s wer e analyze d for VOCs, SVOCs , and metal s
liste d as site COCs . VOC s wer e analyze d by EP A metho d 8260, SVOC s wer e analyze d by EP A metho d 8270 ,
and metal s wer e analyze d by EP A metho d 6010.
3.2.1.1 Plume Peripher y Wells
Analytica l result s for the Plum e Peripher y well s are compare d to the Performanc e Standard s as shown in Tabl e
3-4. Thi s compariso n indicate s the following :
• Detecte d concentration s o f VOC s ar e les s tha n th e Performanc e Standards , wit h th e exceptio n of the
following :
voc
Wel l
Aceton e
1 ,2-Dichloroethan e
1 ,2-Dichloropropan e
Toluen e
Xylen e
Performanc e
Standard*
3,500
5
6
2,000
350
Groundwater Concentration
NS-2 9
220,00 0
-
-
3,300
650 -
NS-3 1
-
100
200
-
-
Al l concentration s in ug/1
"-" Concentratio n less tha n Performanc e Standar d
* Performanc e Standard s fro m OU1 ROD
Detecte d concentration s of SVOC s are les s tha n the Performanc e Standards , wit h the exceptio n of bis(2 -
chloroethyOethe r in EX-02 (740 ug/1), EX-03 (600 ug/1), NS-2 9 (9,900 ug/1), NS-30 (15 0 ug/1), and NS -
31 (81 ug/1). The concentratio n liste d fo r EX-02 is the averag e concentratio n of sampl e EX-02 and the
duplicat e sample . The Performanc e Standar d for bis(2-chloroethyl)ethe r is 5 ug/1.
Detecte d concentration s of metal s are less tha n the Performanc e Standards , wit h the exception of th e
following :
Metal
Well
Arseni c
Bariu m
Manganes e
Selenium
Performanc e
Standard*
1 0L 1,000
7,700
10
Groundwate r Concentration
EX-02
-
4,365**
15,050**
10.7***
NS-2 9
18.2
10,70 0
104,00 0
44
Al l concentration s in ug/1
"-" concentratio n less tha n Performanc e Standar d
* Performanc e Standard s fro m OU 1 RO D
** Averag e concentratio n of sampl e EX-02 an d duplicat e
*** Compoun d wa s no t detecte d in duplicat e sampl e fo r EX-0 2
Detection limit s and dilutio n factor s for the annua l samplin g event are discussed in Section 4.2.
8OD2
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Historica l analytica l result s for the 27 monitorin g event s are show n in Tables 3-5, 3-6, and 3-7 for VOCs ,
SVOCs, and metals , respectively . As show n in these tables, analytica l result s for the Marc h 2002 monitorin g
event are simila r to or lees than the historica l results .
3.2.1.2 Trench Area Wells
Analytica l result s fo r the Trench Are a well s are compare d to the Performanc e Standard s as show n in Table 3-8.
Thi s compariso n indicate s th e following :
• Detecte d concentration s of VOC s are less tha n the Performanc e Standards , wit h the exceptio n of the
following :
voc
Wel l
Acetone
1,2-Dichloroethan e
1,1-Dichloroethen e
1 ,2-Dichloropropan e
Ethylbenzen e
Toluen e
Viny l chlorid e
Xylen e
Performance
Standard*
3,500
5
7
6
3,500
2,000
2
350
Groundwater Concentration
EX-05
53,000 J
390,000
-
-
-
26,000
-
-
EX-07
-
270
-
-
-
-
-
-
EX-08
70,000
190,000
-
2,300 J
-
17,000
-
-
EX-09
30,000 J
91,000
-
7,000
-
39,000
-
-
EX- 10
44,000
14,000
-
11,00 0
1,400
3,000
14 0 J
5,900
NS-09
-
1,40 0
7.8
-
-
-
42 J
-
NS-10
-
13
-
-
-
-
-
-
NS-1 5
-
27
-
-
-
-
-
-
All concentration s in ug/1
"-" concentratio n less tha n Performanc e Standar d
* Performanc e Standard s fro m OU1 RO D
J - Estimate d concentratio n is less tha n the reportin g limit .
• Detecte d concentration s of SVOCs are less tha n the Performanc e Standards , wit h the exceptio n of bis(2 -
chloroethyl)ethe r in EX-08 (1,800 jig/1), EX-09 (2,900 fig/1), and EX-10 (4,800 ug/1). The Performanc e
Standar d fo r bis(2-chloroethyl)ethe r is 5 (xg/1 .
• Detecte d concentration s of metal s are less tha n the Performanc e Standards , wit h the exceptio n of the
following :
Metal
Wel l
Cadmiu m
Manganes e
Nicke l
Seleniu m
Performance
Standard *
10
7,700
350
10
Groundwater Concentration
EX-05
16.5 JE
52,600
1,640
47.6
EX-08
-
196,000
758
72.3
EX-09
-
108,000
407
42.5
EX - 10
-
101,00 0
-
33
NS-09
-
12,800-
-
NS-15
-
10,600
-
-
Al l concentration s in ug/1
"-" concentratio n less tha n Performanc e Standar d
* Performanc e Standard s fro m OU 1 ROD
J - Estimate d concentratio n is less tha n the reportin g limi t
E - Concentratio n exceede d the calibratio n range .
Detectio n limit s and dilutio n factor s for the annua l samplin g event are discusse d in Section 4.2.
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Analytica l result s fo r the 2 7 monitorin g event s conducte d in th e Trenc h Area monitorin g well s an d th e 14
monitorin g event s conducte d in the Trenc h Area extractio n well s are show n in Tables 3-9, 3-10, and 3-11 for
VOCs, SVOCs, and metals, respectively . As show n in these tables , analytica l results for the March 2002
monitorin g even t are simila r to or less tha n th e historica l results .
3.2.2 Operable Uni t Three
Groundwate r sample s collecte d fro m OU 3 well s wer e analyze d for VOCs, SVOCs, an d metal s liste d as site
COCs . VOC s wer e analyze d by EP A metho d 8260, SVOC s wer e analyze d by EP A metho d 8270 , an d metal s
wer e analyze d by EP A metho d 6010.
3.2.2.1 Marc h 2002
Groundwate r analytica l result s of the Marc h 2002 samplin g even t are compare d to the Performanc e Standard s as
show n in Table 3-12. This comparison indicate s the following :
• Detecte d concentration s of VOC s in groun d wate r are les s tha n the Performanc e Standards , wit h the
exceptio n of the following :
voc
Wel l
Acetone
Chlorofor m
1,2-Dichloroethan e
1 , 1 -Dichloroethen e
1 ,2-Dichloropropan e
Methylen e Chlorid e
Tetrachloroethen e
Trichloroethen e
Viny l chlorid e
Performance
Standard*
700
1
1
7
1
5
1
2.8
1
Groundwater Concentration . ,
NS-3 5-
-
6,700
-
-
-
-
-
-
Wel l
Aceton e
Chlorofor m
1,2-Dichloroethan e
1,1 -Dichloroethen e
1 ,2-Dichloropropan e
Methylen e Chlorid e
Tetrac h loroethen e
Trichloroethen e
Viny l chlorid e
700
1
1
7
1
5
1
2.8
1
NS-47
30,000 J
-
180,000
-
-
-
-
-
-
NS-3 6-
-
39,000
-
-
-
-
-
-
NS-48
-
-
3.2
-
-
-
-
-
-
NS-3 9-
-
46
-
1.7 J
13
1.3 J
-
9.7
NS-49
-
1.8
7,500
-
2.4
5.3
2.6
5.1
15
NS-4 0 NS-41 NS
-
73,000 3 6 1
-
-
-
1.7
2.9 :
NS-50 NS-51 N J
-
-
390 48,000** f
-
-
-
-
-2 6 j - :
5-4 2 NS-4 5 NS-4 6.
.
10 3.3 1 2
7.2.
.
1.2r.5 3.3 5.9
56 1.9J 9.5
5-5 2 NS-53 NS-5 4
6,500 J
175**
i.2 83** 69,000
.
.
.
1.2
5.9
5.4 - 9.5
Al l concentration s in ug/1
"-" concentratio n less tha n Performanc e Standar d
* Performanc e Standard s fro m OU3 ROD
** Averag e concentratio n of sampl e NS-51 an d duplicat e or NS-5 3 an d duplicat e
J - Estimate d concentratio n is belo w reportin g limi t
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• Detected concentration s of SVOCs in groun d wate r are less tha n the Performanc e Standards , wit h the
exceptio n of bis(2-cholorethyl)ethe r in NS-2 4 (40 jig/I), NS-3 9 (9.8 J ug/1), NS-40 (6.7 J ug/1), NS49
(12 ug/1), and NS-50 (24 u.g/1). Th e Performanc e Standar d for bis(2-chloroethyl)ethe r is 5 ug/1.
• Detecte d concentration s of metal s in groun d wate r are les s tha n the Performanc e Standards , wit h th e
exceptio n of the following :
voc
Wel l
Chromiu m
Manganes e
Performance
Standard*
50
50
Groundwater Concentration ;
NS-1 3
726
157
NS-24
-
3,200 J
NS-35-
11,10 0
NS-36-
2,600
NS-37
-
128 J
NS-38
-
34,700 J
NS-39
-
174 J
NS-40
-
7,360 J
NS-4 1
122
1,8301
. ' • ' • ' • • r - • . * . ' . .'
Wel l
Manganes e 50
NS-42
12,800 J
NS-45
4,570
NS-4 6
189
NS-47
1,81 0
NS-4 8
5,830
NS-49
5,870
NS-5 0
2,6801
NS-5 1
3,445**
NS-5 2
741**
Wel l
Manganes e 50
NS-5 3
411 J
NS-5 4
4,520
CT-1
163
Al l concentration s in ug/1
"-" concentratio n less tha n Performanc e Standar d
* Performance Standard s fro m OU3 ROD
** Averag e concentratio n of sampl e NS-5 1 an d duplicat e or NS-52 and duplicat e
J - Estimate d concentratio n is belo w reportin g limi t
Detectio n limit s an d dilutio n factor s fo r th e Marc h 200 2 samplin g even t ar e discusse d in Sectio n 4.2 .
Analytica l result s for the 7 monitorin g event s conducte d in th e OU 3 monitorin g an d extractio n well s are show n
in Table s 3-13, 3-14, and 3-15 for VOCs, SVOCs, and metals , respectively . As show n in thes e tables, analytica l
result s fo r the Marc h 2002 monitorin g even t are simila r to or less tha n the historica l results .
3.2.3 RCRA Sampling
In the Novembe r 2000 RCR A Post-Closur e Monitorin g Data Report , NSCC requeste d that in futur e monitorin g
events , delta-BH C no t be include d on th e lis t of compound s to be sampled . Delta-BH C had no t bee n detecte d
durin g the round s of RCRA Post-Closure groundwate r monitoring . The eliminatio n of the pesticide , delta-BHC,
was approve d by the Nort h Carolin a Departmen t of Environmen t and Natura l Resource s in a telephon e conversatio n
on Jul y 18 , 2001. Delta-BH C wa s eliminate d as a monitorin g paramete r fro m th e Februar y 200 2 samplin g event .
Delta-BH C wil l no t be include d on the lis t of compound s to be sample d in futur e RCR A monitorin g events
Groundwate r sample s collecte d fro m RCR A well s wer e analyze d fo r VOCs , SVOCs , an d metal s liste d as site COCs.
Samples collected durin g the Jul y 2001 samplin g even t were also analyze d for pesticides . VOC s were analyze d by
EPA metho d 8260, SVOCs were analyze d by EPA metho d 8270, and metal s wer e analyze d by EPA method 6010 .
3.2.3.1 Jul y 2001
Groundwate r analytica l result s o f th e Jul y 2001 samplin g even t ar e compare d to th e Clas s GA Groun d Wate r
Standard s (locate d in IS A NCA C 02L.0202(g)) as show n i n Tabl e 3-15. Thi s compariso n indicate s th e
following :
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• Det <
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• Det <
wit t
9 0 (
mar
Detectio n l i
3.2.3.2 Feb
Analytica l r
as show n in
• Del
exc <
scte d concentration s of VOC s in groun d wate r are les s tha n th e Clas s G A Groun d Wate r Standards ,L th e exceptio n o f th e following :
voc
Wel l
1 ,2-Dichloroethan e
1 ,2-Dichloropropan e
Chlorofor m
Methylen e Chlorid e
Trichloroethen e
Viny l Chlorid e
Class GA
Groundwate r
Standards
0.38
0.56
0.19
5
2.8
0.01 5
Groundwate r Concentration
NS-39 NS-42 NS-4 9
31 735* 7,900
2
0.7 J
10 10 *
11*
14 37.5 *
^*~ * °C4_o^
^ ,Vv<- v ^
All concentration s in pig/1
"-" concentratio n les s tha n Clas s GA Groun d Wate r Standar d
* Average concentratio n of sample NS-42 and duplicat e
2Cte d concentration s of SVOC s an d pesticide s in groun d wate r ar e les s tha n th e Clas s GA Groun d
er Standards ;
scte d concentration s o f metal s in groun d wate r ar e les s tha n th e Clas s G A Groun d Wate r Standards ,
i the exceptio n of manganes e in NS-39 (122 u,g/l), NS-42 (8,700 u,g/l), NS-49 (6,480 H-g/1), and NS -
,8,900 |ag/l). NS-90 is a duplicat e sampl e of NS-42. The Class GA Ground Wate r Standar d for
ganese is 50 ng/1 .
mil s an d dilutio n factor s fo r th e Jul y 2001 samplin g even t are discusse d in Section 4.2 .
iruar y 2002
esult s of the Februar y 2002 samplin g even t are compare d to the Clas s GA Groun d Water Standard s
Table 3-16. Thi s compariso n indicate s the following :
scted concentration s of VOCs are less tha n the Class GA Groun d Water Standards , wit h the
jptio n of th e following :
VOC
Wel l
1,2-Dichloroethan e
1 ,2-Dichloropropan e
Chlorofor m
Methylen e Chlorid e
Tetrachloroethen e
Trichloroethen e
Viny l Chlorid e
Class GA
Groundwater
Standards
0.3 8
0.5 6
0.19
5
0.7
2.8
0.015
Groundwater Concentration
NS-39 NS-4 2 NS-4 9
42 325* 5,700
1.74 - 2.4
0.5 - 1.9
13 10 *
1.5 - 3.0
9.5* 5.0
9.5 48 * 1 8
All concentration s in u,g/l
"-" concentratio n less tha n Clas s GA Groun d Wate r Standar d
* Averag e concentratio n of sampl e NS-4 2 an d duplicat e
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• Detecte d concentration s of SVOCs are less tha n the Clas s GA Groun d Wate r Standards .
• Detecte d concentration s of metal s are less tha n the Clas s GA Groun d Wate r Standards , wit h the
exceptio n of manganes e in NS-39 (211 ug/1), NS-42 (13,200 ug/1), NS-49 (6,270 ug/1), and DUP-9 0
(13,000 ug/1). Dup-9 0 is a duplicat e sampl e of NS-42. Th e Class GA Groun d Wate r Standar d for
manganes e is 50 ug/1 .
Detectio n limit s an d dilutio n factor s for the Februar y 2002 samplin g even t ar e discusse d in Sectio n 4.2.
3.3 Pumpin g Dat a
Evaluation s conducte d in 1998 indicate d tha t the Trenc h Area Extractio n Syste m ha s been successfu l an d tha t
the Plum e Peripher y Extractio n Syste m ha s no t been successful . In 2000, the Plum e Peripher y System was shu t
dow n to perfor m hydrauli c an d geochemica l analyse s to identif y opportunitie s to implemen t a more effectiv e
remedy . A repor t was submitte d in Novembe r 2000 whic h propose d additiona l investigatio n to identif y
potentia l bedroc k conduit s whic h ma y b e responsibl e fo r migratio n o f impacte d groundwate r fro m th e Trenc h
Are a to the Plum e Periphery .
The Trenc h Are a Extractio n Well s (EX-5 throug h EX-10 ) operat e o n hig h an d lo w leve l switches . Therefore ,
the groundwate r elevatio n control s the quantit y of wate r extracte d fro m eac h well . From Januar y 2, 2001
throug h Decembe r 31 , 2001, a tota l of 179,729 gallon s of wate r was extracte d fro m the Trench Area .
Approximatel y 0.34 gallon s pe r minut e (gpm ) o f groundwate r wa s pumpe d on averag e fro m eac h o f th e si x
extractio n wells .
Th e RO D fo r OU 3 call s fo r pump-and-trea t to addres s groundwate r impact s in OU3. In 1999 , a collectio n
trenc h was installe d in the low-lyin g area adjacen t to Are a 2 an d existin g well s wer e retrofitte d in the vicinit y of
the lagoons . Additionally , the existin g OU 1 syste m wa s upgrade d to improv e operation s and trea t the combine d
OU1 Trenc h Area and OU3 groundwate r streams . Sinc e Februar y 2000, the collectio n trenc h has been pumpin g
approximatel y 6 gpm and the tw o lagoo n area well s hav e been pumpin g at a combine d rate of approximatel y 21
gpm . From Januar y 2, 2001 throug h Decembe r 31, 2001, the collectio n trenc h pumpe d 307,956 gallon s of
groundwate r at a rate of approximatel y 0.59 gpm and the OU 3 extractio n well s (NS-49 and NS-51) pumpe d
11,142,416 gallons of water at a combined rate of 21.2 gpm. b>r
A tota l o f 11,610,10 1 gallon s of wate r wa s pumpe d fro m nin e extractio n point s on th e Sit e fro m Januar y 2, 200 1
through December 31, 2001.
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4. Data Validation
Dat a validatio n fo r the 200 1 an d 2002 groundwate r monitorin g sample s include d a review of genera l laborator y
conformance and an evaluatio n of method detection limits , dilutio n factors , and blind duplicate sample results.
4.1 Laboratory Conformance
The laborator y conformanc e summarie s fo r th e samplin g event s were reviewe d to identif y possibl e analytica l
difficultie s an d thei r potentia l effect s o n th e analytica l results .
4.1.1 Operabl e Unit One
Holdin g times , instrumen t calibration , surrogat e recoveries , and interna l standar d response s me t laborator y
criteri a for analyses performed on groundwate r samples from OU1 wit h the exceptio n of the following :
• SVOCs : (1) Sampl e NS-09 had the surrogat e recover y of phenol-d 5 belo w the lowe r QC limit. The
sampl e was reextracte d and reanalyze d wit h the sam e result . (2) Sample s EX-08, EX-09 , and EX-1 0
had a fina l extrac t volum e of 3.0 milliliter s (mis ) instea d of the metho d stated 1.0 mis due to the matrix .
The reportin g limit s wer e elevate d by a facto r of three for thes e sample s
• metals : (1) Manganes e recoverie s for the batc h MS/MSD , performe d on sampl e EX-01 , could not be
reliabl y calculate d becaus e of the hig h nativ e concentratio n of manganes e in the sampl e relative to the
amoun t adde d to th e MS/MSD . Manganes e concentration s wer e greater tha n fou r time s the
concentratio n of spik e added . (2 ) Th e seria l dilutio n o f sampl e EX-0 5 ha d a percen t differenc e fo r .
cadmiu m above QC limits . \ o70
4.1.2 Operable Unit Three
Holdin g times , instrumen t calibration , surrogat e recoveries , and interna l standar d response s me t laborator y
criteri a for analyse s performed on groundwate r sample s from OU3 wit h the exceptio n of the following :
• VOCs : (1) The MSD , performe d on sampl e NS-54 , had the recover y of benzen e belo w the lowe r QC
limits . (2) The relativ e percen t differenc e (RPD ) between the matri x spike s for chlorobenzene is abov e
QC limits .
• SVOCs : (1) Sampl e NS-1 3 was extracte d usin g 900 mis instea d of the metho d state d 1,00 0 mi s due to
the limite d sampl e volume . This elevate d the reportin g limi t by a facto r of 1.11 .
• metals : (1) Manganes e recoverie s for the MS/MSDs, performe d on sample s NS-49 and NS-
54 , coul d no t be reliabl y calculate d becaus e o f th e hig h nativ e concentratio n o f manganes e in
the sample relativ e to the amoun t added to the MS/MSDs . Manganes e concentration s wer e
greate r tha n fou r time s th e concentratio n of spik e added .
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4.1.3 RCR A Sampling
Holdin g times , instrumen t calibration , surrogat e recoveries , an d interna l standar d response s me t laborator y
criteria , fo r analyse s performe d on RCR A groundwate r samples in Jul y 2001 wit h the exception of the
following :
• VOCs : (1) The batc h MS for sampl e NS-49 had surrogat e recoverie s of 1,2-dichloroethane , 4-
bromofluorobenze , an d dibromofluoromethan e abov e the uppe r QC limits .
• SVOCs : (1) The batc h MS/MSD for sampl e NS-49 had recoverie s for analyte s 4-nitropheno l and
pentachloropheno l belo w QC limits . These recoverie s shoul d no t impac t the dat a because thes e
compound s wer e no t targe t analytes . Al l targe t analyte s wer e withi n laborator y Q C limits .
• Chlorinate d Pesticides : (1) Sample s NS-42 and NS-49 had the recoverie s for the surrogat e TCX belo w
the lowe r Q C limi t o n th e RTX-5 colum n analyses . Th e metho d blan k an d LC S ha d all surrogat e
recoverie s withi n QC limits .
• metals : (1) The batc h MS/MSD , performe d on sampl e NS-49 , ha d surrogat e recoverie s of mercur y
below laborator y QC limits . These recoverie s may be indicativ e of a bia s for mercury . (2) Manganes e
recoverie s fo r the MS/MSD , performe d on sampl e NS-49, coul d not be reliabl y calculate d because of
the hig h nativ e concentratio n of manganes e in the sampl e relativ e to the amoun t adde d to the MS/MSD.
Holdin g times , instrumen t calibration , surrogat e recoveries , an d interna l standar d response s me t laborator y
criteria , for analyse s performe d on RCR A groundwate r sample s in Februar y 2002 wit h the exception of the
following :
• SVOCs : (1) Sampl e DUP-90 was extracte d usin g 900 mis instea d of the metho d state d 1,000 mis due to
the limite d sampl e volume . Thi s elevate d the reportin g limi t by a facto r of 1.11.
• metals: (1) Manganese recoveries for the batc h MS/MSD, performe d on sample NS-49, could not be
reliabl y calculate d becaus e of th e hig h nativ e concentratio n of manganes e in th e sampl e relativ e to th e
amount added to the MS/MSD. Manganese concentration s were greater tha n fou r times the
concentratio n of spik e added .
4.2 Method Detection Limits and Dilution Factors
Metho d detectio n limit s and dilutio n factor s were reviewe d for all sample s collecte d in 2001 an d 2002.
4.2.1 Operabl e Uni t On e
4.2.1.1 Plume Peripher y Wells
Detectio n limit s fo r VOCs , SVOCs , an d metal s ar e less tha n th e Performanc e Standard s in sample s fo r th e
Plum e Peripher y well s wit h the exceptio n of:
_____________________________BLASLAND. BOUCK & LEE . INC._____________________________
M/K engineers & scientists 4-232222283.dix:
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I « Benzene , bromodichloromethane , chloroform , 1,1-dichloroethene , methylen e chloride , 1,1,2 -
trichloroethane , trichloroethene , and viny l chlorid e in DUP-031502, NS-29 , and NS-31 ;
• • 1,2-Dichloroethanean d 1,2-dichloropropan e in DUP-03150 2 and NS-29 ;
• 4-Nitropheno l in NS-29; and
| • Bis(2-chloroethyl)ethe r in EX-01 .
• The followin g sample s wer e analyze d at a dilution :
• VOCs: EX-02 (15X), DUP-031502 (15X), NS-29 (100 X and 5,OOOX), and NS-31(50X); and
I • SVOCs : EX-0 2 (15X), DUP-03150 2 (15X), EX-0 3 (10X), NS-2 9 (10 X and 200X), NS-30 (3X), and
NS-31(4X).
• 4.2.1.2 Trench Are a Wells
_ Detectio n limit s for VOCs, SVOCs , and metal s are less than the Performanc e Standard s in samples for the
• Trenc h Area well s wit h the exceptio n of:
_ • Benzene , bromodichloromethane , chloroform , 1,1-dichloroethene , methylen e chloride , 1,1,2 -
• trichloroethane , and trichloroethe n in EX-05, EX-07, EX-08, EX-09, and EX-10;
• 1,2-Dichloropropan e in EX-05 and EX-07;
• • Viny l chlorid e in EX-05 , EX-07 , and EX-08 ;
• • Xylen e in EX-05, EX-07, and EX-08;
• Bis(2-chloroethyl)ethe r in EX-05, EX-06, EX-07, NS-09, NS-10, NS-11, and NS-15; and
• • 4-Nitropheno l in EX-05 , EX-08 , EX-09 , and EX-10 .
• The followin g sample s were analyze d at a dilution :
• VOCs: EX-05 (3,OOO X and 15,OOOX), EX-07 (10X), EX-08(3,OOO X and 5,OOOX), EX-09 (2,OOO X -
• 3,OOOX), EX-1 0 (100 X and 1,OOOX), and NS-09 (60X); and
• SVOCs : EX-0 5 (60X), EX-0 8 (60X), EX-09 (60X), and EX-1 0 (20 X and 100X).
4.2.2 Operabl e Uni t ThreeI
| well s wit h the exceptio n of:
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Detectio n limit s fo r VOCs, SVOCs , and metal s ar e less tha n the Performanc e Standard s in sample s for OU 3
it h the exceptio n of :
• Aceton e in NS-35 , NS-36 , NS-40 , and NS-51 ;
_____________________________BLASLAND. BOUCK & LEE , INC._______________________
tate' engineers & scientists 4-332222283.doc
1111111111111111111
• Chlorofor m in NS-35, NS-36, NS-40, NS-42, NS-47, NS-50, NS-5 1 , and NS-54;
• 1 ,2-Dichloroethan e in NS-35 , NS-36 , and NS-40 ;
• Cis-l,2-Dichloroethen e and trans-l,2-Dichloroethen e in NS-35 , NS-36, NS-40, NS47, NS-5 1, and NS-
54;
• 1,1-Dichloroethen e in NS-35, NS-36, NS-40, NS-47, NS-50, NS-51, and NS-54;
• 1 ,2-Dichloropropane , Methylen e Chloride , Tetrachloroethane , and Trichloroethen e in NS-35,
NS-40, NS-42, NS-47, NS-50, NS-51, and NS-54;
• Viny l chlorid e in NS-35, NS-36, NS-40, NS-43, NS-44, NS-47 , NS-5 1, NS-53, NS-54, and CT-1
• Bis(2-chloroethy])ethe r in NS-13, NS-35 , NS-36 , NS-37, NS-38, NS-42, NS-43, NS-44, NS-45,
NS-47, NS-48, NS-49, NS-50, NS-51, NS-52, NS-53, NS-54, and CT-1;
NS-36,
»
NS-46 ,
• Bis(2-ethylhexyl)phthalat e in NS-13 , NS-24, NS-35, NS-36, NS-37, NS-38 , NS-39, NS-40 , NS-42, NS-
43, NS-44, NS-45, NS-46 , NS-47, NS-48, NS-49, NS-50, NS-51 , NS-52 , NS-53, NS-54 , and CT-1;
• Antimon y and Thalliu m in NS-13, NS-24 , NS-35, NS-36, NS-37, NS-38, NS-39, NS-40 , NS-41,
NS-43 , NS-44 , NS-45 , NS-46 , NS-47 , NS-48 , NS-49 , NS-50 , NS-51 , NS-52 , NS-53, NS-54 , and
The followin g sample s were analyze d at a dilution :
NS42,
CT-1 .
• VOCs : NS-35 (250X), NS-36 (1,500X), NS-40 (2.000X), NS-42 (6X), NS-47 (10,OOOX), NS49
(300X), NS-50 (15X), NS-51 (1,OOOX), DUP-030702 (2.000X), DUP-03130 2 (6X), NS-53 (5X) and
NS-54 (2,500X); and
• SVOCs: NS-13 (1.1 IX) and NS-45 (4X), and EX-09 (60X).
4.2.3 RCR A Samples
Detectio n limit s for VOCs, SVOCs, and metals are less than the Performance Standard s in Jul y 2001
fo r RCR A well s wit h th e exceptio n of:
• 1,2-Dichloropropane , bromodichloromethane , and tetrachloroethen e in NS-42 and NS-49 ;
• Chlorofor m in NS-33 , NS-42 , and NS-49;
• Methylen e chlorid e and trichloroethen e in NS-49; and
• Viny l chlorid e in NS-33 and NS-49.
Th e followin g sample s wer e analyze d at a dilution :
• VOCs: NS-42 (5X), NS-90 (5X), and NS-49 (50X).
BLASLAND , BOUC K & LEE , INC .
8/2/02 engineers & scientists32222283.iloc
sample s
4-4
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Detectio n limit s fo r VOCs, SVOCs, an d metal s ar e less tha n th e Performanc e Standard s in February 200 2
sample s fo r RCR A well s wit h th e exceptio n of :
• 1,2-Dichloropropane , Chloroform , Tetrachloroethen e in NS-33, NS-42, and NS-49;
• l,2-DichloroethaneinNS-33 ;
• Acetone , cis-l,2-dichloroethene , trans-l,2-dichloroethene , and ethylbenzen e in NS-49;
• Methylen e chlorid e in NS-4 2 and NS-49 .
4.3 Blin d Duplicate Samples
4.3.1 Operable Unit One
One blin d duplicat e sampl e wa s collecte d durin g the OU 1 samplin g even t fro m extractio n wel l EX-02. Th e
analytica l result s fo r the duplicat e sampl e are consisten t wit h those of sampl e EX-02 .
4.3.2 Operable Unit Three
Tw o blin d duplicat e groundwate r sample s wer e collecte d durin g the OU 3 samplin g event. On e duplicat e sampl e
was collecte d fro m extractio n wel l NS-51 and the othe r fro m monitorin g well NS-53 . Th e duplicat e sample of
NS-5 1 wa s analyze d at a greate r dilutio n tha n NS-51 . Th e analytica l result s fo r the duplicat e sampl e of NS-5 1
are consisten t wit h thos e of NS-51 for all analyte s wit h the exceptio n of 1,2-dichloroethane . 1,2-Dichloroethan e
was detecte d at the sam e order of magnitud e in NS-51 and the duplicat e sampl e at concentration s of 38,000 ug/1
and 58,000 u.g/1 , respectively . Th e analytica l result s for th e duplicat e sampl e of NS-53 are consisten t wit h the
correspondin g sample .
4.3.3 RCRA Sampling
One blind duplicate sample was collected durin g the Jul y 2001 and February 2002 RCRA samplin g events fro m
monitorin g well NS-42. Th e analytica l result s for the duplicat e samples are consisten t wit h the corresponding
samples .
BLASLAND, BOUCK & LEE, INC.
Kae engineers & scientists 4-532222283.doc
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5. Summary
5.1 Groundwater Quality and Trends
Groundwate r monitorin g analytica l result s fo r 200 1 an d 2002 do no t indicat e an y significan t change s in
concentratio n sinc e the extractio n syste m wa s shu t off . Concentration s in OU 1 well s remai n at or below level s
observed in 2000 for all constituents . Concentration s of all constituent s remaine d generall y consistent wit h
2000 level s in the OU 3 wells .
5.2 Future Actions
Annua l monitorin g of OU1/OU 2 and OU 3 monitorin g an d extractio n well s an d annua l monitorin g of surfac e
water and sedimen t in the Northeas t Tributar y wil l continu e in 2002. The annua l monitorin g of surface wate r
an d sediment s wil l occu r in Decembe r 2002 . Th e annua l monitorin g even t fo r OU1/OU 2 an d OU 3 is schedule d
to occur in Decembe r 2002. Samplin g method s for the 2002 samplin g event s wil l remai n the sam e as those use d
in 200 1 an d follo w thos e describe d in the PVP .
BLASLAND . BOUCK & LEE , INC .
8a(B engineers & scientists 5-1
32222283.doc
0 )
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Tabl e 3-1
OU1/OU 2 Wate r Leve l Measurement s
Nationa l Starc h an d Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
Wate r leve l measurement s collecte d fro m Top of Casin g (TOC)
* Wel l wa s dry
** Wel l is artesia n
*** Wel l coul d no t be accesse d
Measuremen t Types :
BE - Bedroc k Extractio n Wel l
BM - Bedroc k Monitorin g Wel l
TE - Transitio n Zon e Extractio n Wel l
TM - Transitio n Zon e Monitorin g Wel l
SM - Saprolit e Monitorin g Wel l
SG - Stream Gaug e (iro n pin s locate d in th e Unname d Tributary )
Measuremen t
Poin t
Measuremen t
Type Date TOC Elevatio n
(ft. MSL)
Depth to
Water (ft)
Water Leve l
Elevatio n (ft. MSL)
Plum e Peripher y Well s
EX-0 1
EX-0 2
EX-0 3
EX-0 4
NS-0 5
NS-06
NS-2 1
NS-2 2
NS-2 3
NS-2 6
NS-2 7
NS-2 8
NS-2 9
NS-3 0
NS-3 1
NS-32
P-01
P-0 2
P-04
UN-1
UN-2
SG-1
SG-2
BE
BE
BE
BE
SM
TM
TM
TM
TM
TM
TM
TM
BM
BM
TM
TM
TM
BM
BM
SG
SG
SG
SG
03/05/0 2
03/05/02
03/05/0 2
03/05/02
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/02
03/05/0 2
03/05/0 2
03/05/02
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/02
03/05/0 2
03/05/0 2
03/05/02
03/05/02
03/05/0 2
03/05/0 2
734.45
721.0 4
743.2 8
756.74
770.1 3
741.03
744.87
718.1 7
754.5 2
722.80
750.82
768.5 2
717.6 1
720.64
713.2 8
701.64
710.92
777.34
740.1 0
724.75
706.49
714.48
696.05
29.73
11.8 8
21.9 9
31.6 2
704.72
709.16
721.2 9
725.12
No t Measured *
14.72
7.31
15.4 5
27.1 5
7.22
24.5 1
31.1 2
12.52
726.31
737.56
702.72
727.37
715.58
726.31
737.40
705.09
No t Measured**
9.02 704.26
Not Measured**
Not Measured *
47.94
39.09
1.4 5
0.44
1.6 2
729.40
701.0 1
723.30
706.05
712.8 6
Damage d
Trench Area Well s
EX-0 5
EX-0 6
EX-0 7
EX-0 8
EX-0 9
EX - 10
NS-0 1
NS-01 A
NS-02
NS-03
NS-07
NS-08
NS-09
NS-1 0
NS-1 1
NS-1 2
NS-1 5
NS-1 6
NS-1 7
TE
TE
TE
TE
TE
TE
SM
SM
SM
SM
SM
SM
TM
SM
SM
TM
TM
TM
TM
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/02
03/05/02
03/05/02
03/05/02
03/05/02
03/05/02
03/05/02
03/05/02
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
781.2 6
788.28
789.2 3
789.19
782.29
775.9 2
793.26
787.07
787.01
774.26
764.07
780.39
780.61
788.88
777.81
777.34
795.2 9
765.33
783.1 3
38.9 1
42.90
43.82
742.35
745.38
745.41
No t Measured***
58.2 1
28.24
724.08
747.68
No t Measured *
Not Measured *
38.45 748.56
Not Measured *
23.87
35.75
37.14
41.7 1
26.74
22.64
52.05
25.9 1
40.29
740.20
744.64
743.47
747.17
751.07
754.7 0
743.24
739.42
742.84
or;-r
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Table 3-2
OU 3 Wate r Leve l Measurement s
Nationa l Starch and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
Measuremen t
Point
NS-1 3
NS-1 4
NS-2 4
NS-3 3
NS-34
NS-3 5
NS-3 6
NS-3 7
NS-38
NS-39
NS-40
NS-4 1
NS-4 2
NS-4 3
NS-4 4
NS-45
NS-4 6
NS-4 7
NS-4 8
NS-50
NS-5 2
NS-53
NS-54
NS-49
NS-5 1
CT-1
NT-1
NT-2
NT-4
Measuremen t
Type
TM
SM
TM
TM
TM
TM
TM
TM
TM
TM
TM
TM
TM
TM
TM
TM
BM
TM
BM
BM
BM
TM
BM
TE
TE
CT
SG
SG
SG
Date
03/05/02
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/02
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/02
03/05/02
03/05/02
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/0 2
03/05/02
03/05/0 2
TOC Elevatio n
(ft . MSL)
762.67
765.35
758.82
776.36
776.27
746.1 1
745.59
746.1 1
745.61
769.91
769.34
766.03
766.16
759.38
759.30
754.85
768.99
769.62
770.22
766.08
764.67
770.13
770.28
766.98
764.98
-
-
-
-
Depth to
Water (ft)
15.0 4
Wate r Leve l
Elevation (ft. MSL)
747.63
No t Measured *
26.76
17.5 0
18.6 9
4.6 9
3.7 5
32.1 1
31.6 0
30.31
29.42
25.1 1
27.29
15.2 4
15.0 3
9.99
23.72
25.23
26.23
31.9 5
22.99
24.25
- 22.7 4
38.1 6
67.55
10.7 1
732.06
758.8 6
757.5 8
741.4 2
741.8 4
714.0 0
714.0 1
739.60
739.92
740.92
738.87
744.14
744.27
744.86
745.2 7
744.3 9
743.99
734.1 3
741.6 8
745.88
747.5 4
728.8 2
697.43
-
No t Measured *
0.23
0.43
-
-
Wate r leve l measurement s collecte d fro m To p of Casin g (TOC)
* Well/Gaug e was dry
Measuremen t Types:
SM - Saprolit e Monitorin g Wel l
TM - Transition Zone Monitorin g Well
BM - Bedroc k Monitorin g Wel l
TE - Transitio n Zone Extractio n Wel l
CT - Collection Trench
SG - Stream Gaug e (iro n pin locate d in the Northeas t Tributary )
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Tabl e 3-3
OU 1 an d OU 3 Performanc e Standard s
Nationa l Starc h an d Chemica l Compan y
Ceda r Spring s Plan t Site
Salisbury , Nort h Carolin a
Constituen t
VOCs
Acetone
Benzen e
Bromodichloromethan e
Chlorofor m
1 , 1 -Dichloroethen e
1,2-Dichloroethan e
1 ,2-Dichloropropan e
cis- 1 ,2-Dichlorocthen e
trans - 1 ,2-Dichloroethen e
Ethylbenzen e
Methylen e chlorid e
Toluen e
Tetrachloroethen c
1,1,2-Trichloroethan e
Trichloroethen e
Viny l chlorid e
Xylene
SVOCs
Bis(2-chloroethyl)ethe r
Bis(2-ethylhexyl)phthalat e
4-Nitropheno l
Metals
Arseni c
Antimon y
Barium
Berylliu m
Cadmiu m
Chromiu m
Manganes e
Nicke l
Seleniu m
Thalliu m
Zin c
OU1 Performanc e
Standard 1
3,500
5
5
5
7
5
6
-
-
3,500
5
2,000
-
5
5
2
350
5
-
350
10-
1,000
17.5
10
50
7,700
350
10-
7,350
OU3 Performanc e
Standard 1
700
-
-
1
7
1
1
70
70
-
5-
1
5
2.8
1
-
5
5
-
-
6-
-
-
50
50
-
-
2
2,100
North Carolin a
Groundwate r
Standards3
700
1
0.6
0.1 9
7
0.3 8
0.5 6
70
70
29
5
1,00 0
0.7-
2.8
0.01 5 ,
530
-
-
-
50-
2,000
-
5
50
50
21
50-
2,10 0
MCL4
-
5
-
-
7
5
5
70
10 0
70
5
1,000
5
5
5
2
10,00 0
-
-
-
50
6
2,000
4
5
100
50
-
50
2
5,000
Metho d Detection
Limits5
1.0
0.6
0.6
0.6
1.0
0.8
0.7
0.8
1.0
0.7
1.0
0.7
1.0
0.7
1.0
0.9
1.0
2.0
2.0
4.0
1.7
1.4
4.5
0.1
0.5
0.9
1.2
2.4
2.3
3.8
8.6
Unit s in ug/1
1 -OU 1 ROD , page 10
2-OU3ROD , pag e 81
3 - Stat e Groundwate r Qualit y Standard s (NCA C 15-2L.0202 )
4 - Maximu m Concentratio n Limit s as specifie d in Saf e Drinkin g Wate r Ac t
5 - Metho d Detectio n Limit s for Undilute d Sample s provide d by Sever n Tren t Laboratories , Inc. (Baltimore , MD )
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Tabl e 3-4
Comparison of 2002 Analytica l Result s for Plum e Periphery Wells to Performanc e Standards
Nationa l Starc h an d Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
Well ID
Sampl e No .
Sample Date
Dilutio n Facto r
Associate d Metho d Blan kvocs
Aceton e
Benzen e
Bromodichloromethan e
Chlorofor m
1 ,2-Dichloroethan e
1,1-Dichloroethen e
1 ,2-Dichloropropan e
Ethylbenzen e
Methylen e chlorid e
Toluen e
1 , 1 ,2-Trichloroethan e
Trichloroethen e
Viny l chlorid e
Xylen e
Dilutio n Facto r
Associate d Metho d Blan ksvocs
bis(2-Chloroethyl ) ethe r
4-Nitropheno l
Dilutio n Factor
Associate d Metho d Blan k
METALS
Arseni c
Barium
Berylliu m
Cadmiu m
Chromiu m
Manganese
Nicke l
Seleniu m
Zin c
Performanc e
Standar d
3,500
5
5
5
5
7
6
3,500
5
2,000
5
5
2
350
5
350
10
1,000
17.5
10
50
7,700
350
10
7,350
EX-0 1
C2C 160 13800 6
03/15/0 2
1
EWJP81A A
10 U
.0 U
.OU
.O U
.O U
.0 U
.O U
.O U
2.0 U
.0 U
.O U
.0 U
2.0 U
3.0 U
1
EWJG81A A
10 U
50 U
1
C2C 18000-2 3 3
10 U
45.5 B
5.0 U
• 5.0 U
5.0 U169
40 U
5.0 U
20 U
EX-0 2
C2C16013800 1
03/15/02
1
EWJP81A A
10 U
1.4
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
33
2.0 U
310 E
1.0 U
1.0 U
2.0 U
130 E
1
EWJG81A A
550 E
50 U
1
C2C 1 8000-233
3.2 B
4^60
5.0 U
5.0 U
6.1
15,100 *
12.3 B
10.7 *
4.6 B
EX-02
C2C16013800 1
03/15/02
15
EWJP81A A
100 J
15 U
15 U
15 U
15 U
15 U
15 U
20
30 U
380
15 U
15 U
30 U
83
15
EWJG81A A
730
-'" 750 U
-
NA
NA
NA
NA
NA
NA
NA
NA
NA
DUP-03150 2
C2C 160 13800 6
03/15/0 2
15
EWJP81A A
96 J
15 U
15 U
15 U
15 U
15 U
15 U
24
SO U
480
15 U
15 U
30 U
97
1
EWJG81A A
560 E
SO U1
C2C 18000-233
3.8 B
4370
5.0 U
5.0 U
6.2
15,000 *
12.2 B
10 U*
5.9 B
DUP-031502
C2C16013800 6
03/15/02
-
EWJP8IAA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
15
EWJG81A A
750
750 U
-
NA
NA
NA
NA
NA
NA
NA
NA
NA
NOTES :
Units in ug/l
* Sampl e dilute d at a facto r of 2 for this compound .
U - Not detecte d at indicate d concentratio n
E - Estimate d concentratio n exceeds the calibratio n rang e
J (Organics ) - Estimate d concentratio n is less tha n the reportin g limi t
B (Inorganics ) - Estimate d concentratio n is less tha n the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greater tha n Performanc e Standar d
Page 1 of3
ii
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ii
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ii
i
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i
Tabl e 3-4
Compariso n of 2002 Analytica l Result s fo r Plum e Peripher y Well s to Performanc e Standard s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolina
Wel l ID
Sampl e No.
Sample Date
Dilutio n Facto r
Associate d Metho d Blan kvocs
Aceton e
Benzene
Bromodichloromethan e
Chlorofor m
1,2-Dichloroethan e
1,1-Dichloroethen e
1 ,2-Dichloropropan e
Ethylbenzen e
Methylen e chlorid e
Toluen e
1 , 1 ,2-Trichloroethan e
Trichloroethen e
Viny l chlorid e
Xylen e
Dilutio n Factor
Associate d Metho d Blan ksvocs
bis(2-Chloroethyl ) ether
4-Nitropheno l
Dilutio n Facto r
Associate d Metho d Blan k
METALS
Arseni c
Barium
Berylliu m
Cadmiu m
Chromiu m
Manganese
Nicke l
Seleniu m
Zin c
Performanc e
Standar d
3,500
5
5
5
5
7
6
3,500
5
2,000
5
5
2
350
5
350
10
1,00 0
17.5
10
50
7,700
350
10
7,350
EX-03
C2C16013800 4
03/15/0 2
1
EWJP81A A
39
0.6 1 J
1.0 U
1.0 U
0.9 6 J
1.0 U
1.0 U
7.3
2.0 U
7.5
1.0 U
1.0 U
2.0 U
12
1
EWJG81A A
480 E
50 U
1
C2C 18000-233
10 U
561
5.0 U
0.2 9 B
23.2
2,18 0
19.2 B
5.0 U
94.5
EX-03 DL
C2C16013800 4
03/15/02
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
10
EWJG81A A
600
500 U
.
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-04
C2C16013800 2
03/15/0 2
1
EWJP81A A
10 U
1.0 U
1.0 U
1.0 U
0.7 0 J
1.0 U
1.0 U
1.0 U
2.0 U
0.5 2 J
1.0 U
1.0 U
2.0 U
3.0 U
5
EWJG81A A
2.6 J
-''" 5 0 U
1
C2C 18000-233
10 U
61.2 B
5.0 U
5.0 U
5.0 U
2,240
40 U
5.0 U
20 U
NS-29
C2C20015100 7
03/19/02
100
EWRTQ1A A
250,000 E
100 U
400 U
100 U
100 U
100 U
100 U
140
200 U
3,300
100 U
100 U
200 U
650
10
EWPV51A A
8,10 0 E
500 U
1
C2C2 1000 - 158
18.2
10,700 *
5.0 U
5.0 U
26.9
104,000 **
45.3
44
4.8 B
NS-29 DL
C2C20015100 7
03/19/02
5000
EWWXW1A A
220,000
5,000 U
5,000 U
5,000 U
5,000 U
5,000 U
5,000 U
5,000 U
10,000 U
2,600 J
5,000 U
5,000 U
10,000 U
15,000 U
200
EWPV51A A
9,90010,00 0 U
--
NA
NA
NA
NA
NA
NA
NA
NA
NA
NOTES :
Units in ug/1
* Sampl e dilute d at a facto r of 2 for this compound .
** Sampl e dilute d at a facto r of 50 for this compound .
U - Not detected at indicate d concentration
E - Estimate d concentratio n exceeds the calibratio n rang e
J (Organics ) - Estimate d concentratio n is less tha n th e reportin g limi t
B (Inorganics ) - Estimate d concentratio n is less tha n the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n Performanc e Standar d
Page 2 of3
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Tabl e 3-4
Compariso n of 2002 Analytica l Result s for Plum e Peripher y Well s to Performanc e Standards
Nationa l Starch and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
Wel l ID
Sampl e No.
Sampl e Dat e
Dilutio n Facto r
Associate d Metho d Blan kvocs
Aceton e
Benzen e
Bromodichloromethan e
Chlorofor m
1 ,2-Dichloroethan e
1,1-Dichloroethen e
1 ,2-Dichloropropan e
Ethylbenzen e
Methylen e chlorid e
Toluen e
1,1,2-TrichIoroethan e
Trichloroethen e
Viny l chlorid e
Xylen e
Dilutio n Facto r
Associate d Metho d Blan ksvocs
bis(2-Chloroethyl ) ethe r
4-Nitropheno l
Dilutio n Facto r
Associate d Method Blan k
METALS
Arseni c
Bariu m
Berylliu m
Cadmiu m
Chromiu m
Manganes e
Nicke l
Seleniu m
Zin c
Performanc e
Standard
3,500
5
5
5
5
7
6
3,500
5
2,000
5
5
2
350
5
350
10
1,00 0
17.5
10
50
7,700
350
10
7,350
NS-30
C2C130 1 1900 1
03/1 1/02
1
EWC3V1A A
1.0 U
0.4 6 J
1.0 U
1.0 U
2.8
1.0 U
1.0 U
3.1
2.0 U
2.1
1.0 U
1.0 U
2.0 U
6.3
3
EWC441A A
150
150 U
1
C2C 140000- 174
10 U
405
5.0 U
5.0 U
5.0 U
1,07 0
1.8 B
5.0 U
20 U
NS-3 1
C2C20015100 6
03/19/02
50
EWWXW1A A
2,300
SO U
50 U
50 U
100
50 U
200
SO U
100 U
23 J
50 U
50 U
100 U
150 U
4
EWPV51A A
81
200 U
I
C2C2 1000 - 158
4.7 B
22.9 B
5.0 U
5.0 U
1.9 B
22.5
40 U
5.0 U
20 U
NS-32
C2 C 130 11 9002
03/1 1/02
1
EWC3V1A A
10 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
2.0 U
1.0 U
1.0 U
1.0 U
2.0 U
3.0 U
1
EWC441A A
10 U
••'" 5 0 U
1
C2C 140000- 174
10 U
107 B
5.0 U
5.0 U
5.0 U
119
40 U
5.0 U
20 U
NOTES:
Unit s in ug/1
U - Not detecte d at indicate d concentratio n
J (Organics ) - Estimate d concentratio n is less tha n the reporting limi t
B (Inorganics ) - Estimate d concentratio n is less tha n the reportin g limi t
Bold fon t indicate s detecte d concentratio n greater tha n Performanc e Standar d
Page 3 of 3
Table 3-5
Historica l Analytica l Result s - VOCs
Plum e Peripher y Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
ACETON E
Quarte r
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q96
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q9S
3Q98
4Q98
4Q99
4QO O
1Q02
EX-0 1
75
1 0 U
6 J
10 U
10 U
10 U
1 0 U
10 U
10 U
33 D
70
39
10 U
1 4
1 2
10 U
8 B J
4.5 J B
1 0 J
10 U
4 JB
3 J
10 U
10 U
10 U
2 U
10 U
EX-02
NS
29000 D
34000 DB
2700 0
26000
3100 0 B
4100 0
" 28000 ' E "
~"270d6"""
24000 D
29000 D
50000
1000 0
12000 ' E
3300 0 D
25000 D
30000 DB
780 0 D B
1200 0 D
7900 D
3200 DB3800
1400 0 D
3100 0 DB
33000
20 0 U10 U
EX-0 3
130 0 D
2200 D
610 0 DB
1200
2200
3700 B
140 0
3700
100 0
9200 D
2500 D
190 0
5800
2700 E "
8800 D
7200 D
14000 DB
1200 0 DB
15000 D
8000 D
10400 DB6900 D
5900 D
4600 DB
150 0 4
10 0 U39
EX-04
120 0 D
10 U
29 B
27
2 1
30 B
20
15
1 0 U
110 0 D
2000 D
820
9 J
1300 " E
67 5 D
460 D
81 0 D B
220 0 DB
240 0
460 D
85 0 DB7 J
9 •-.
10 ' U
49 4
2 U
1 0 U
NS-29
1200 0 D
10 U
1 0
1 0 U
1 0 U10 U
1 0 U
1 0 U
39
110 0 D
42000 D
80000
1200 0
6400" E
10000 0 D
50000 D
39000 DB
3700 0 DB
10000 0 DB
59000 D
93000 DB100000 DE
99000 D
220000 D
11000 0 4
200 0 U
220000
NS-30
2900
1 0 U
1 1
1 0 U
1 0 U
1 0 U
1 3
1 0 U
1 0 U
1 0 U
32
1 0 U
1 0 U
1 3
6 J
1 0 I f
6 B J
4 J B
6 B J
1 0 U
8 J B
9 1
160 0 D
310 0 D
3000 4
10 0 U
1 U
NS-3 1
4700 D
10 U
18
10 U
10 U
10 U
1 1
13 0 B
9200
1500 0 D
4800 D
1600 0
3500.hob o .E
"3300 0 D
41000 D
43000 DB
3000 0 DB
1900 0 B
3100 0 D
45000 DB
47000 DB
52000 D
1900 0 D
770 4
2900 U2300
NS-3 2
1 0 U
1 0 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 0 U
1 0 B J
3 J B
4 B J
1 0 U
1 3 B
4 J
1 0 U
14 0 B
10 U
2 U10 U
NOTES :
Unit s in ug/1
RO D Performanc e Standard : 3,50 0 ug/L
NS - Not Sampled " ~~
U - Not detected at indicate d concentration
D - Concentratio n fro m a secondar y dilutio n analysi s
E/4 - Estimate d concentratio n exceeds the calibratio n rang e
J (Organics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
B (Organics ) - Compoun d detecte d in associate d metho d blan k
Bold fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Italic fon t indicate s detection limi t greater tha n ROD Performanc e Standard
Shading indicates "E" qualified concentration for which a diluted run concentration is unavailable.
»f
Pag e 1 o f 1 4
Table 3-5
Historica l Analytica l Result s - VOCs
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Ceda r Springs Plan t Site
Salisbury , Nort h Carolin a
BENZEN E
Quarter
1Q93
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q964Q961Q97
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-01
5 U
5 U
10 U
JO U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
EX-02
NS
5 U
1 J
3300 U
2500 U
1700 U
1200 U
660 U
1000 U
42 U
250 U
2500 U
500 U
50 U
1000 U
250 U250 U
250 U
250 U
250 U
50 U
250 U100 U
100 U
1 U
100 U
1.4
EX-03
5 U
5 U
10 U
170 U
250 U
120 U
50 U
93 U
33 U
45 U
17 U
50 U
500 U
25 U
250 U
250 U250 U
250 U
250 U
250 U
100 U
100 U
200 U
200 U
1 U
50 U
1 J
EX-04
2 J
5 U
1 J
10 U
10 U
5 U
5 U
5 U
5 U
5 U
17 U
62 U
5 U
25 U
2 J
0.6 J
10 U
2 J
10 U
10 U
10 U
10 U10 . U10 '•-. u
1 U
1
1 U
NS-29
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
12 U
250 U
3100 U
500 U
50 U
97 J
500 U
500 U
500 U
500 U
500 U
500 U500 U
2500 U
250 U
1 U
700 0 U
100 U
NS-30
120 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 V50 U
10 U
1 U
50 U
0.46 J
NS-3 1
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
.250 U
10 U
32 U
500 U
250 U
100 U
1000 U
1000 U
1000 U
1000 U
1000 U
1000 U
250 U
2500 U1000 U
100 U
1 U
1 U
50 U
NS-32
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
NOTES :
Unit s in ug/I
RO D Performanc e Standard : 5 ug/L
NS - Not Sampled
U - Not detected at indicate d concentratio n
J (Organics ) - Estimate d concentratio n is less tha n the reportin g limi t
Bold font indicates detected concentratio n greater than ROD Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Page 2 of 14
Table 3-5
Historica l Analytica l Result s - VOCs
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
BROMODICHLOROMETHAN E
Quarter
1Q93
2Q93
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q96
2Q96
3Q96
4Q96
1Q97
2Q97
3Q97
4Q9 7
1Q98
2Q98
3Q98
4Q98
4Q9 9
4QO O
1Q0 2
EX-0 1
5 U
5 U
10 U
JO U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U1 U
EX-02
NS
5 U
10 U
3300 U
2500 U
1700 U
1200 U
660 U
1000 U
42 U
250 U
2500 U
500 U
50 U
1000 U
250 U
250 U
250 U
250 U
250 U
50 U
250 U
100 U
100 U
1 U
100 U1 U
EX-03
5 U
5 U
10 U
170 U
250 U
120 U
50 U
93 U
33 U
45 U17 U
50 U
500 U
25 U
250 U
250 U
250 U
250 U
250 U
250 U
100 U
100 U
200 U
200 U
1 U
50 U1 U
EX-04
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
17 U
62 U
5 U
25 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 , U
10 ' U
1 U
1 U
1 U
NS-29
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
12 U
250 U
3100 U
500 U
50 U
500 U
500 U500 U
500 U
500 U
500 U
500 U
500 U
2500 U
250 U
1 U
700 0 U400 U
NS-30
120 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
50 U
10 U
1 U
50 U1 U
NS-31
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
250 U
10 U32 U
500 U
250 U
100 U
1000 U
1000 U1000 U
1000 U
1000 U
1000 U
250 U
2500 U
1000 U
100 U
1 U
1 U
50 U
NS-32
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
NOTES:
Unit s in ug/1
RO D Performance Standard : 5 ug/L
NS - Not Sampled
U - Not detected at indicate d concentratio n
Itali c fon t indicate s detectio n limit greater tha n ROD Performanc e Standar d
Pag e 3 o f 1 4
Tabl e 3-5
Historica l Analytica l Result s - VOC s
Plum e Peripher y Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
CHLOROFOR M
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-0 1
5 U
5 U
10 U
JO U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
EX-02
NS
5 U
10 U
3300 U
2500 U
1700 U
1200 U
660 U
1000 U
42 U
250 U
2500 U
500 U
50 U
1000 U
250 U
250 U
250 U
250 U
250 U
50 U
250 U
100 U
100 U
I U
100 U
1 U
EX-03
5 U
5 U
10 U
170 U
250 U
120 U
50 U
93 U
33 U
45 U
17 U
50 U
500 U
25 U
250 U
250 U
250 U
250 U
250 U
250 U
100 U
100 U
200 U
200 U
1 U
50 U
1 U
EX-04
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
17 U
62 U
5 U
25 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 ' U
1 U
1 U
1 U
NS-29
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
12 U
250 U
3100 U
500 U
50 U
500 U
500 U500 U
500 U
500 U
500 U
500 U
500 U
2500 U
250 U
1 U
1000 U100 U
NS-30
120 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
50 U
10 U
1 U
50 U1 U
NS-3 1
2 J
5 U
10 U
10 U
10 U
5 U
5 U
5 U
250 U
10 U
32 U
500 U
250 U
100 U
1000 U
1000 U
1000 U
1000 U
1000 U
1000 U
250 U
2500 U
1000 U
100 U
1 U
1 U
50 U
NS-32
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U\ U
1 U
1 U
NOTES :
Unit s in ug/1
RO D Performance Standard : 5 ug/L
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
J (Organics) - Estimate d concentratio n is less tha n the reporting limi t
Italic fon t indicate s detection limi t greater than RO D Performanc e Standar d
Pag e 4 o f 1 4
Table 3-5
Historica l Analytica l Result s - VOC s
Plum e Peripher y Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
1,2-DICHLOROETHAN E
Quarter
IQ93
2Q93
3Q93
4Q931Q94
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 82Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-0 1
20
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
3 J
5
5 U
4 J
10 U5 i
7 J
3.5 J10 U
10 U
10 U10 U
JO U
10 U
1 U
1 U1 U
EX-0 2
N S
460 D J
510 DJ
3300 U2500 U
1700 U
1200 U
550 J
1000 U
750
570
2500 U
120 0
590
610 J140 J
520
290
690
920
230410
600
100 0
880
100 U
1 U
EX-03
23
65
60
55 J
250 U
120 U
50 U
93 U
33 U
59
10 J
61
150 J
42
250 U
60 J
220 J
240 J
200 J
230 J
200
190
200 U200 U
9.1
50 U
0.96 J
EX-04
4 J
3 J
5 J
10 U
10 U
5 U
5
3 J
7
517 U
62 U
4 J
25 U
10 U
3 J
5 J
6 J
5 J
10 U
10 U10 U
5 •. 3
10 ' U
1 U
1 U
0.7 J
NS-2 9
110
22
3 J
3 J10 U
17
3 J
43
8
37
690
3100 U
860
300
500 U
1200
760
680
190 0
170 0
2300
4200
2400 J
3600
3500
1000 U
100 U
NS-3 0
79 J
8
56
10 U10 U
4 J
5 U
5 U
5 U
5 U5 U
5 U
5 U
5 U
10 U10 U
3 J
10 U10 U
10 U
10 U
5 J
42 J
58
84
50 U2.8
NS-3 1
100
71
49
20
9 J
5
4 J
4 J
250 U
41
120
500 U
250 U
100 U
1000 U
170 J
150 J
1000 U1000 U
1000 U
2602500 U
1000 U
100 U
62; :;iio.v E '
100
NS-32
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
NOTES:Unit s in ug/I
RO D Performanc e Standard : 5 ug/L
NS - Not SampledU - Not detected at indicate d concentratio n
D - Concentratio n fro m a secondar y dilutio n analysi s
E - Estimated concentration exceeds the calibratio n rangeJ (Organics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Italic fon t indicate s detectio n limi t greater tha n RO D Performanc e Standar d
Shadin g indicate s "E " qualifie d concentratio n fo r whic h a dilute d ru n concentratio n is unavailable .
Pag e 5 o f 1 4
Tabl e 3-5
Historica l Analytica l Result s - VOCs
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Ceda r Spring s Plan t Site
Salisbury , Nort h Carolin a
1,1-DICHLOROETHEN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q964Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 82Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-0 1
5 U
5 U
10 U
JO U
10 U
7 U
7 U
7 U
7 U
7 U
7 U
7 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U10 U
10 U
10 U
1 U
1 U
1 U
EX-02
NS
5 U
10 U
3300 U
2500 U
2300 U
1800 U
920 U
1400 U
59 U
350 U
3500 U500 U
50 U
1000 U250 U
250 U
250 U
250 U
250 U
50 U
250 U
100 U
100 U
1 U
100 U
1 U
EX-03
5 U
5 U
10 U
170 U
250 U
180 U
70 U
130 U
47 U
63 U
23 U
70 U
500 U
25 U
250 U250 U
250 U
250 U
250 U
250 U
100 U100 U
200 U
200 U
1 U
50 U
1 U
EX-04
5 U
5 U
10 U
10 U
10 U
1 U
7 U
7 U
7 U
7 U
23 U
88 U
5 U
25 U
10 U10 U
10 U
10 U
10 U
10 U
10 U10 U
10 , U
10 N U
1 U
1 U
1 U
NS-29
5 U
5 U
10 U
10 U
10 U
7 U
7 U
7 U
7 U
18 U
350 U
4400 U
500 U
50 U
500 U500 U
500 U
500 U
500 U
500 U
500 U500 U
2500 U
250 U
3.8
1000 U
100 U
NS-30
120 U
5 U
10 U
10 U
10 U
1 U
7 U
7 U
7 U
7 U
7 U
7 U
5 U
5 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
50 U
10 U
1 U
50 U
1 U
NS-3I
5 U
5 U
10 U
10 U
10 U
7 U
7 U
7 U
350 U
15 U
45 U
700 U
250 U
100 U
1000 U1000 U
1000 U
1000 U
1000 U
1000 U
250 U
2500 U
WOO U
100 U
1 U
1 U
50 U
NS-32
5 U
5 U
10 U
10 U
10 U
7 U
7 U
7 U
7 U
7 U
7 U
7 U
5 U
5 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
NOTES:
Unit s in ug/1
RO D Performanc e Standard : 7 ug/L
NS - Not SampledU - Not detected at indicate d concentratio n
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 6 o f 1 4
Tabl e 3-5
Historica l Analytica l Result s - VOCs
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
1,2-DICHLOROPROPAN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q95
2Q953Q95
4Q95
1Q96
2Q96
3Q96
4Q961Q97
2Q97
3Q97
4Q97
1Q98
2Q98
3Q9 8
4Q98
4Q99
4QO O
1Q02
EX-01
35
4 J
10 U
10 U
10 U
6 U
6 U
6 U
6 U
6 U
6 U
6 U
5 U
5 U
10 U
1 J7 J
3 J
2 J
10 U
10 U10 U10 U
10 U
1 U
1 U1 U
EX-02
NS
820 DJ
1000 D J
3300 U
2500 U
1600 J
1200 J
1200
670 J
1300
890
3000 U
830
650
640 J
100 J
400
190 J
460
730
130
170 J
360
490
810
100 U
1 U
EX-03
120
180
150
170 U
250 U
70 J
44 J
53 J
40 U
160
24
130
140 J
33
87 J
71 J150 J
240 J
230 J
310
200
235
100 J
200 U
30
50 U
1 U
EX-04
5 U
5 U
10 U
10 U
10 U
6 U
6 U
6 U
6 U
626
75 U
5 U
25 U
2 J
1 J7 J
17
7 J
2 J
3 J
10 U
10 -. U10 '•• u
1 U
1 U
1 U
NS-29
350 D
46.5
5 J
10 U
10 U
6 U
6 U
6 U
6 U
12 J
1000
2200 J
1600
710
1900
18001200
980
2500
270 0
2700
3700
2100 J
2700
3100
7000 U100 U
NS-30
190
23
97
10 U
10 U
6 U
6 U
6 U
6 U
6 U6 U
6 U
5 U
5 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
5 J
68
54
20
50 U1 U
NS-31
170
200
83
31
10 U
3 J
6 U
6 U
300 U
50
260
340 J
250 U
94 J
1000 U160 J1000 U
1000 U
1000 U
1000 U
170 J
2500 U
1000 U
100 U
160~ iso " "-. ..; E
266" '""""
NS-32
5 U
5 U
1 J
10 U
10 U
6 U
6 U
6 U
6 U
6 U
6 U
6 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
NOTES :
Unit s in ug/1
RO D Performanc e Standard : 6 ug/L
NS - Not Sampled
U - Not detected at indicated concentratio n
D - Concentratio n fro m a secondary dilutio n analysi s
E - Estimate d concentratio n exceeds the calibratio n rang e
J (Organics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greater tha n RO D Performanc e Standar d
Shading indicates "E" qualifie d concentratio n for which a dilute d run concentratio n is unavailable .
Pag e 7 o f 1 4
Table 3-5
Historica l Analytica l Result s - VOCs
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolin a
ETHYLBENZEN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-0 1
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U10 U
10 U
10 U
1 U
1 U
1 U
EX-02
NS
9
13
3300 U
2500 U
3300 U
2500 U
130 0 U
2000 U
85 U500 U
5000 U
500 U
12 J
100 0 U
32 J
250 U
250 U
250 U
25 0 U
50 U250 U
10 0 U
18 J
24
72 J D
33
EX-03
5 U
2 J
3 J
170 U
250 U
25 0 U
10 0 U
190 U
67 U
89 U33 U
100 U
500 U
25 U
250 U
250 U
250 U
250 U
250 U
250 U
100 U100 U
200 U
200 U
6.3
50 U7.3
EX-04
2 J
5 U
10 U
10 U10 U
3 J
10 U
10 U
10 U
10 U
33 U
120 U
5 U
25 U
2 J
2 J
3 J
4 J
10 U
2 J
2 J2 J
3 . J
3 ''-. J
2.4
2
1 U
NS-29
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
25 U
500 U
6200 U
500 U
50 U
500 U
500 U
500 U
50 0 U
500 U
50 0 U
500 U500 U
2500 U
74 J
68 4
100 0 U
140
NS-30
12 0 U
5 U
1 J
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
50 U
10 U
1.8
50 U
3.1
NS-3 1
2 J
2 J
1 J
10 U
10 U
10 U
10 U
10 U
50 0 U
21 U
65 U
100 0 U
250 U
100 U
100 0 U
100 0 U
100 0 U
100 0 U
100 0 U
100 0 U
250 U
2500 U
100 0 U
48 J
5.9
3
50 U
MS-3 2
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
NOTES :
Unit s in ug/1
RO D Performanc e Standard : 3,50 0 ug/L
NS - Not Sample d
U - Not detecte d at indicate d concentratio n
O - Concentratio n fro m a secondar y dilutio n analysi s
E/4 - Estimated concentration exceeds the calibratio n range
J (Organics ) - Estimate d concentratio n is less tha n the reportin g limi t
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 8 of 1 4
Tabl e 3-5
Historica l Analytica l Result s - VOC s
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
METHYLEN E CHLORID E
Quarter
1Q93
2Q93
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q95
2Q95
3Q95
4Q95
IQ96
2Q96
3Q96
4Q96
1Q97
2Q97
3Q97
4Q97
1Q98
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-01
2 B J
1 J
2 B J
NR
NR
5 U
9 B
5 U
5 U
3 B J
5 U
5 U
2 B J
1 B J
10 U
0.6 J
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
2 U
EX-02
NS
4 J
10 U
NR
NR
1700 U
2900 B
1200 B
1300 B
44 B
250 U
2500 U
IS O B J
13 J
620 J
74 J
250 U
250 U
250 U
40 J
50 U250 U
100 U
9 J
7.5 1
300 B D
2 U
EX-03
2 B J
2 J
10 U
NR
NR
720 U
110 B
150 B
37 B
41 B J
17 U
72 B
160 BJ
25 U
140 J
16 J
250 U
250 U
250 U
40 J
100 U
100 U
110 J
200 U
1 U
160 B D
2 U
EX-04
5 U
2 J
5 B J
NR
NR
5 U
7 B
6 B
3 B J
7 B
17 U
62 U
2 B J
5 B J
4 J
1 J
10 U
10 U
10 U
10 U
10 U
10 U
10 .. U10 '•• u
1 U
1 U
2 U
NS-2 9
3 B J
2 J
2 B J
NR
NR
5 U
8 B
7 B
3 B J
13 B
250 U
3100 U
150 BJ
50 U
2200
37 J
500 U
500 U
500 U
89 J
500 U500 U
1100 J
250 U
14 1
2000 B D200 U
NS-30
48 BJ
5 U
2 B J
NR
NR
5 U
8 B
5 U
5 U
10 B
5 U
5 U
2 B J
5 U
10 U
0.6 J
10 U
10 U
10 U
10 U
10 U10 U
12 J
10 U
1 U
38 JB D
2 U
NS-3 1
3 B J
5 U
2 B J
NR
NR
5 U
9 B
6 B
200 B J
16 B
32 U
480 BJ
71 B J
21 J
310 J
110 J
1600 B
1000 U
1000 U
160 J
250 U2500 U
1000 U
100 U
1 U
1 U
700 U
NS-32
2 B J
1 J
1 J
NR
NR
5 U
9 B
9 B
4 B J
11 B
5 U
5 U
2 B J
5 U
70 U
0.7 J
3 J
70 U
10 U
10 U
10 U10 U
10 U
10 U
1 U
1 U
2 U
NOTES :
Unit s in ug/1
RO D Performanc e Standard : 5 ug/L
NS - Not Sample d
NR - Not Reporte d
U - Not detected at indicate d concentratio n1 - Commo n laborator y contaminan t
D - Concentratio n fro m a secondar y dilutio n analysi s
J (Organics ) - Estimate d concentratio n is less tha n th e reportin g limi t
B (Organics ) - Compoun d detecte d in associate d metho d blan k
Bold fon t indicate s detected concentratio n greate r than RO D Performanc e Standar dItalic font indicates detection limit greater than ROD Performance Standard
Pag e 9 of 1 4
Table 3-5
Historica l Analytica l Result s - VOCs
Plum e Peripher y Extractio n and Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
TOLUEN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-0 1
13
5 U
10 U
10 U10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
5 U
5 U
10 U
1 J
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
EX-02
NSno
2500 U
3300 U
2500 U3300 U
2500 U
420 J
2000 U
280
280 J
5000 U
290 J
260
340 J
280
300
11 0 J
210 J
290
62
130 J
260
540
430
140 0 D
380
EX-03
5846
55
66 J
25 0 U
91 J
60 J
87 J
69
80 J
32 J
60 J
130 J
55
99 J
12 0 J
190 J
16 0 J
IS O J
20 0 J
16 5185
15 0 J
220
100 4
480 D
7.5
EX-04
5
2 J
3 J
3 J
10 U7 J
4 J
7 J
10 U
26
31 J
120 U
2 J
46
31 J
26
41
33
23
17
22
11
1 7 -.
19 '
10
0.7 J
0.5 2 J
NS-2 9
60
6.5
3 J
10 U
10 U
10 U
10 U
10 U
10 U
25 U
200 J
6200 U
370 J
150
850
440 J
40 0 J
260 J
910
110 0
950
140 0
100 0 J
180 0
140 0
5500 D
3300
NS-30
34 J
2 J
23
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
5 U
5 U
10 U
10 U
10 U
10 U
1 0 U
10 U
10 U
10 U
12 J
26
36
560 D
2.1
NS-3 1
34
34
15
6 J
10 U10 U
10 U
10 U
500 U
12 J
45 J
100 0 U
64 J
150
310 J
370 J
315 J
37 0 J
390 J
610 J
620
980 J
940 J
120 0
140
31
23 J
NS-32
5 U
5 U
10 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
5 U
5 U
10 U
0.8 J
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
NOTES:
Unit s in ug/1
RO D Performanc e Standard : 2,000 ug/L
NS - Not Sample d
U - Not detected at indicated concentratio n
D - Concentratio n fro m a secondar y dilutio n analysi s
E/4 - Estimated concentration exceeds the calibratio n range
J (Organics ) - Estimate d concentratio n is les s tha n the reportin g limi t
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 1 0 o f 1 4
Tabl e 3-5
Historica l Analytica l Result s - VOC s
Plum e Peripher y Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Springs Plan t Site
Salisbury , Nort h Carolin a
1,1,2-TRICHLOROET H AN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q97
2Q97
3Q97
4Q97
1Q982Q98
3Q98
4Q98
4Q99
4QO O
IQ02
EX-01
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
EX-02
NS
5 U
10 U
3300 U
2500 U
1700 U
1200 U
660 U
1000 U
42 U
250 U
2500 U
500 U
50 U
1000 U
250 U
250 U
250 U
250 U
250 U
50 U
250 U
100 U
100 U
1 U
100 U
1 U
EX-03
5 U
5 U
10 U
170 U
250 U
120 U
50 U
93 U
33 U
45 U
17 U
50 U
500 U
25 U
250 U
250 U
250 U
250 U
250 U
250 U
100 U
100 U
200 U
200 U
1 U
50 U
1 U
EX-04
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
17 U
62 U
5 U
25 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 , U
10 ' U
1 U
1 U
1 U
NS-29
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
12 U
250 U
3100 U
500 U
50 U
500 U
500 U
500 U
500 U
500 U
500 U
500 U
500 U
2500 U
250 U
1 U
1000 U
100 U
NS-30
12 0 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
50 U
2 J
1 U
50 U
1 U
NS-3 1
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
250 U
10 U
32 U
500 U
250 U
100 U
1000 U
1000 U
1000 U
1000 U
1000 U
1000 U
250 U
2500 U
1000 U
100 U
1 U
1 U
50 U
NS-32
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
NOTES :
Unit s in ug/1
RO D Performance Standard : 5 ug/L
NS - Not Sample d
U - Not detected at indicated concentration
J (Organics ) - Estimate d concentratio n is less tha n the reportin g limi t
Itali c fon t indicate s detectio n limi t greater tha n RO D Performanc e Standar d
Page 11 Of 14
Table 3-5
Historica l Analytica l Result s - VOC s
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
TRICHLOROETHEN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q95
2Q95
3Q9 5
4Q9 5
1Q96
2Q96
3Q96
4Q96
1Q97
2Q9 7
3Q97
4Q97
1Q9 8
2Q983Q98
4Q9 8
4Q9 9
4QO O
1Q02
EX-01
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
2 S
1 U
1 U
1 U
EX-0 2
NS
5 U
10 U
3300 U
2500 U
1700 U
1200 U
660 U
1000 U
42 U
250 U
2500 U
500 U
50 U
WOO U
250 U
250 U
250 U
250 U
250 U
50 U
250 U
100 U
4 J
1 U
100 U
1 U
EX-0 3
5 U
5 U
10 U
170 U
250 U
120 U
50 U
93 U
33 U
45 U
17 U
50 U
500 U
25 U
250 U
250 U
250 U
250 U
250 U
250 U
100 U
100 U
200 U
200 U
1 U
50 U
1 U
EX-0 4
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
17 U
62 U
5 U
25 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U10 U
10 , U
10 • U
\ U
1 U
1 U
NS-29
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
12 U
250 U
3100 U
500 U
50 U
500 U
500 U
500 U
500 U
500 U
500 U
500 U
500 U2500 U
150 J
1 U
WOO U
100 U
NS-30
120 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
50 U
10 U
1 U
50 U
1 U
NS-31
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
250 U
10 U
32 U
500 U
250 U
100 U
WOO U
1000 U
1000 U
WOO U
WOO U
WOO U
250 U2500 U
WOO U
100 U
\ U
1 U
50 U
NS-32
5 U
5 U
10 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
NOTES:
Unit s in ug/1
RO D Performanc e Standard : 5 ug/L
NS - No t Sample d
U - Not detected at indicate d concentratio n
J (Organics ) - Estimate d concentratio n is less tha n th e reportin g limi t
Itali c fon t indicate s detectio n limi t greater tha n RO D Performanc e Standar d
Page 1 2 O f 1 4
Tabl e 3-5
Historica l Analytica l Result s - VOC s
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
VINY L CHLORID E
Quarter
1Q9 3
2Q93
3Q9 3
4Q93
1Q9 4
2Q94
3Q9 4
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q9 8
4Q99
4QO O1Q02
EX-0 1
10 U
10 U
10 U
10 U
10 U
2 U
2 U
2 U
2 U
2 U
2 U
2 U
10 U
10 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U10 U
10 U
1 U
1 U
2 U
EX-02
NS
10 U
19
3300 U
2500 U
670 U
500 U
260 U
400 U
17 U
100 U
1000 U
1000 U
100 U
1000 U
250 U250 U
250 U
250 U
250 U
50 U
250 U
100 U
15
6.5
70 0 U2 U
EX-03
10 U
10 U
10 U
170 U
250 U
50 U
20 U
37 U
13 U
18 U
7 U
20 U
1000 U
50 U
250 U
250 U
250 U
250 U
250 U
250 U
100 U100 U
200 U
200 U
1.9
50 U
2 U
EX-04
28
10 U
10 U
10 U
10 U
2 U
2 U2 U
2 U
2 U
7 U
25 U
10 U
50 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U10 •, U10 ''• u
1 U
1 U
2 U
NS-29
10 U
10 U
10 U
10 U
10 U
2 U
2 U
2 U
2 U
5 U
100 U
1200 U
1000 U
100 U
500 U500 U
500 U
500 U
500 U
500 U
500 U
500 U
2500 U
250 U
5.8
700 0 U
200 U
NS-30
250 U
10 U
10 U
10 U
10 U
2 U
2 U
2 U
2 U
2 U
2 U
2 U
10 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
50 U
10 U
1 U
50 U
2 U
NS-3 1
10 U
10 U
2 S
10 U
10 U
2 U
2 U
2 U
100 U
4 U
13 U
200 U
500 U
200 U
1000 U1000 U
1000 U
1000 U
1000 U
1000 U
250 U
2500 U
1000 U
100 U
1.7
1 U
100 U
NS-32
10 U
10 U
10 U
10 U
10 U
2 U
2 U
2 U
2 U
2 U
2 U
2 U
10 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
2 U
NOTES:
Unit s in ug/1
RO D Performanc e Standard : 2 ug/L
NS - Not SampledU - No t detecte d at indicate d concentratio n
J (Organics ) - Estimate d concentratio n is less tha n the reportin g limi t
Bold fon t indicates detected concentration greater than ROD Performanc e StandardItalic fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 1 3 o f 1 4
Tabl e 3-5
Historica l Analytica l Results - VOCs
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
XYLEN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-0 1
2 J
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10
10 U
10 U
10 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
3 U
1 U
3 U
EX-02
NS
38
52
3300 U
2500 U
3300 U
2500 U
1300 U
2000 U
24 J
500 U
5000 U
500 U
34 J
1000 U
26 J
250 U
250 U
250 U
250 U
50 U
25 0 J
30 J
68 J
98
290 D
83
EX-03
10
7
10
170 U
250 U
250 U
100 U
190 U
67 U
89 U
33 U
100 U
500 U
6 3
250 U
250 U
250 U
250 U
250 U
250 U
17 J
33.5 J
200 U
200 U
18.9
75 D
12
EX-04
2 J
1 J
2 J
10 U
10 U
10 U
10 U
10 U
10 U
10 U
33 U
12 0 U
5 U
25 U
6 J
5 J
6 J
10
2 J
4 J
5 J
6 J
4 .. J
4 "' J
1.5
1
3 U
NS-2912
2 J
2 J
10 U
10 U
10 U
10 U
10 U
10 U
25 U
500 U
6200 U
500 U
20 J
110 J
56 J
500 U
500 U
11 0 J
160 J
130 J
220 J
2500 U
320
270 4
120 0 D
650
NS-30
120 U
5 U
4 J
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
50 U
5 J
7.3
42 D
6.3
NS-3I
6
7
4 J
10 U
10 U
10 U
10 U
10 U
500 U
21 U
65 U
1000 U
25 0 U
100 U
700 0 U
1000 U
1000 U
1000 U
1000 U
WOO U
89 J
2500 U
1000 U
200
23.2
9
150 U
NS-32
5 U
5 U
10 U
10 U
^ 10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
3 U
1 U
3 U
NOTES :
Unit s in ug/1
ROD Performanc e Standard : 350 ug/L
NS - Not Sample d
U - Not detected at indicate d concentratio nD - Concentratio n fro m a secondar y dilutio n analysi s
E/4 - Estimate d concentratio n exceed s the calibratio n rang e
J (Organics ) - Estimate d concentratio n i s les s tha n th e reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greater tha n RO D Performanc e Standar d
Pag e 1 4 o f 1 4
Table 3-6
Historica l Analytica l Result s - SVOCs
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Springs Plan t Site
Salisbury , Nort h Carolin a
BIS(2-CHLOROETHYL)ETHE R
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q97
2Q97
3Q97
4Q97
1Q982Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-01
38
4 Ju u
11 U
10 U11 U
6 U
5 U
5 U
3 J
14
11
9 J
7 J
10 U
17
31
21
24
17
46
14
23
34
20
2 U
10 U
EX-02
NS
380 D
540 D
440
510
770
680
570
540
650
570
570
400
500 / :;:E
430
320 D
490 D
250 D
310 D
43
180 D
140 D
310 D
850 D
1300."iTix f " :E
730
EX-03
82
100
10 U
74
150 D
120
56
110
130
180 D
120
140
130
93
170
130
180
180
210 D
260 D
350 D
195 D
230 D
10 U
310
110 0 D600
EX-04
12
5 J
11
53 U
22 J
17 J
13 J
21 J
14 J
55
64
41
10
71
48
49
68 D
74 D
68 D
47 D
94 D
28
26.5 \
58 D
51
1
2.6 J
NS-29
190
52
25
188 J
12
12
17
13
32
450
1100
590 D
250
1400 D
740
810
410
1400 D
1400 D
2400 D
3100 D
10 0 U
3600 D
3800
710 0 D9900
NS-30
44
32
10 U
10 J
41
29
17
21
17.5
16
12
10
5 J
7 J
7 J
4 J
10 J
7 J
8 J
10 U
9 J
2 J
23
37
57
1000 D150
NS-31
71
95
38
25
24
20
21
14
11
78
130
320
72
160
380200 D
540 D
390 D
21 U
19
1500 D
2700 D
2400 D
2200 D
160
2 U81
NS-32
10 U
10 U
10 U
11 U
11 U
10 U
5 U
5 U
5 U
5 U
6 U
370
10 U
10 U
10 U
10 U
10 U
10 U
650 D
560 D
10 U
10 U
10 U
10 U
10 U
52 U10 U
NOTES:
Unit s in ug/1
ROD Performanc e Standard: 5 ug/L
NS - Not Sampled
U - Not detected at indicate d concentratio n
D - Concentration from a secondary dilutio n analysis
E - Estimate d concentratio n exceeds the calibratio n rang e
J (Organics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
Bold fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detection limi t greater tha n ROD Performanc e Standar d
Shading indicate s "E" qualifie d concentratio n for whic h a diluted run concentratio n is unavailable .
Pag e 1 of 2
Table 3-6
Historica l Analytica l Result s - SVOC s
Plum e Peripher y Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Company
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
4-NITROPHENO L
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
IQ96
2Q96
3Q964Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-0 1
50 U
50 U
26 U
27 U
26 U
27 U
29 U
27 U
27 U
26 U
28 U
25 U
25 U
25 U
25 U
25 U
26 U
25 U
25 U
26 U
26 U
26 U
26 U
26 U
50 U
4 U
50 U
EX-02
NS
52 U
26 U
260 U
250 U
1100 U
530 U
1400 U
540 U
270 U
670 U
500 U
500 U
120 U
250 U25 U
25 U
26 U
26 U
26 U
26 U
26 U
26 U
26 U
50 U
4 U
50 U
EX-03
52 U
56 U
25 U
52 U
26 U
54 U
27 U
53 U
53 U52 U
11 0 U
53 U
50 U
50 U
25 0 U100 U
10 0 U
10 0 U
26 U
26 U
26 U
26 U
27 U
26 U
50 U
41 U
50 U
EX-04
50 U
54 U
25 U
130 U
100 U
100 U
110 U
260 U
260 U
140 U
140 U
54 U
25 U
12 0 U
50 U25 U
25 U
25 U
26 U
28 U
27 U
26 . U
26 • U
26 U
50 U
4 U
50 U
NS-29
52 U
54 U
26 U
26 U
25 U
26 U
27 U
26 U
29 U
27 U
690 U
1300 U
25 U
12 0 U
250 U250 U
260 U
250 U
250 U
260 U
130 U
260 U
260 U
280 U
50 U
410 U
500 U
NS-30
50 U
50 U
26 U
27 U
26 U
27 U
26 U
26 U
26 U
28 U
27 U
26 U
25 U
25 U
25 U25 U
26 U
25 U
26 U
26 U
26 U
26 U
27 U
27 U
50 U
51 U
150 U
NS-3 1
50 U
52 U
25 U
26 U
27 U
26 U
27 U
26 U
26 U
51 U
13 0 U
260 U
25 U
12 0 U
120 U50 U
50 U
50 U
52 U
26 U
26 U
26 0 U
26 U
270 U
50 U
4 U
200 U
NS-32
50 U
50 U
25 U
26 U
27 U
26 U
26 U
27 U
25 U
26 U
28 U
520 U
25 U
25 U
25 U25 U
26 U
25 U
26 U
26 U
26 U
26 U
26 U
26 U
50 U
10 U
50 U
NOTES:
Unit s in ug/1
ROD Performanc e Standard: 350 ug/L
NS - Not Sample d
U - Not detected at indicate d concentratio n
Italic fon t indicates detection limi t greater tha n ROD Performanc e Standard
Pag e 2 of 2
Tabl e 3-7
Historica l Analytica l Result s - Metal s
Plum e Peripher y Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
ARSENI C
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q944Q94
1Q95
2Q95
3Q95
4Q95
1Q96
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q98
2Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-0 1
2 U
2 U
2 U
2.4 U
2.9 U
2.6 U
2.1 U
3.3 B
0.8 U
2.7 U
.9 U
.5 U
.1 U
.1 U
.1 U
.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
1.3 U
5 U
5 U
1.5 U10 U
EX-02
NS
2 U
2 U
4.8 U
5.8 U
7.8 U
2.1 U
2.1 U
1.1 B
3.8 B
2.8 B
.5 U
.1 U
.1 U
.1 U
.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
1.3 U
5 U
5 U
2.9 B3.2 B
EX-03
2 U
2 U
2 U
4.8 U
5.8 U
2.6 U
2.1 U
2.1 U
0.8 U
2.7 U
1.9 U
.5 U
.1 U
.1 U
.1 U
.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
1.3 U
5 U
5 U
1.5 Uto u
EX-04
2 U
2 U
2 U
2.4 U
2.9 U
2.6 U
2.1 U
2.8 B
0.8 U
2.7 U
.9 U
.5 U
.1 U
.1 U
.1 U
.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
1.3 "'••-. U
5 U
5 U
3 B
10 U
NS-29
2 U
2 U
2 U
2.4 U
2.9 U
2.6 U
2.1 U
2.1 U
1.5 B
2.7 U
2.2 B
1.5 U
1.1 U
1.1 U
1.5 B
1.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
1.3 U
5 U
5 U
9.1 B
18.2
NS-30
2 U
2 U
2 U
2.4 U
2.9 U
2.9 B
2.1 U
2.1 B
0.8 U
2.7 U
.9 U
.5 U
.1 U
.1 U
.1 U
1.1 U
7 U
7 U
7 U
7 B
6 U
1.3 U
1.3 U
5 U
5 U
37.2 B
10 U
NS-3 1
2 U
2 U
2 U
2.9 B
2.9 U
3.7 B
2.1 U
2.1 U
1.3 B
2.9 B
1.9 U
1.5 U
1.1 U
1.1 U
1.1 U
1.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
2.6 U
5 U
5 U
3.8 B
4.7 B
NS-32
2 U
2 U
2 U
2.4 B
2.9 U
2.6 U
2.1 U
3.1 B
0.8 U
2.8 B
2.3 B
.5 U
.1 U
.1 U
.1 U
.1 U
7 U
7 U
7 U
6 . U
6 U
1.3 U
1.3 U
5 U
5 U
1.5 U
10 U
NOTES:
Unit s in ug/1
ROD Performance Standard : 10 ug/L
NS - Not Sampled
U - Not detected at indicate d concentratio n
B (Inorganics ) - Estimate d concentratio n is less than the reporting limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Pag e 1 of 9
Tabl e 3-7
Historica l Analytica l Result s - Metals
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolin a
BARIU M
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q95
2Q95
3Q95
4Q95
1Q96
2Q96
3Q96
4Q96
1Q97
2Q97
3Q97
4Q97
1Q98
2Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-01
68.2 B
25.3 B
27.2 B
22.8 B
17.1 B
23 B
18.3 B
25.3 B
17.7 B
26.5 B
61.4 B
54.5 B
104 B
93.6 B
37.9 B
126 B
154 B
163 B
173 B
181 B
213
137 J
89.7
138
5 U
40.9 B45.5 B
EX-02
NS
1250
1780
149 0
1680
1830
154 0
1070
1080
1860
1820
1930
1970
1780
1560
1370
1170
982
1110
1210
713
1130
864
1485
1600
85804360
EX-03
166 B
140 B
235
278
405
516
608
498
625
475
265
387
553
415
440
349
519
647
722
703
71 7
676
390
592
490
968561
EX-04
37.3 B
26.9 B
29.4 B
36.3 B
29.3 B
56.4 B
27 B
45.9 B
34.4 B
72.7 B
52.6 B
42.8 B
35.4 B
114 B
71.6 B
61.5 B
40.8 B
45.1 B
44.7 B
42 B
46 B
36 J
26.5 "'•-.
47.7
53
61.6 B61.2 B
NS-29
182 B
87.4 B
80.9 B
61.7 B
45.3 B
64.1 B
52.2 B
57.6 B
64 B
84.7 B
190 B
1420
867
324
2490
1150
1360
720
1800
211 0
1600
1370
636
1410
1800
853010700
NS-30
23.4 B
31.8 B
33 B
29.8 B
49.4 B
35.6 B
31.6 B
26.9 B
27.3 B
27.5 B
19.7 B
18.1 B
28 B
31.1 B
32.5 B
32.1 B
27.4 B
28 B
29.1 B
25.8 B
28.7 B
36 J
18.5
53.4
57.-.--- 232 •"•••-— E"
405
NS-31
193 B
36.3 B
19.5 B
15.6 B
2.4 U
17.4 B
8.2 B
1.7 B
19.6 B
12.6 B
207
1680
1630
3350
5180
6280
6780
6870
9280
4680
9850
9330
11400
18900
36
87.6 B22.9 B
NS-32
65.8 B
69 B
86 B
85.6 B
85.5 B
82.6 B
85.2 B
85.5 B
85 B
93.3 B
89.7
86.6 B
87.8 B
96.5 B
95.8 B
91.5 B
97.3 B
93 B
96.3 B
98.2 B
99.1 B
105 J
61.9
10 3
100
10 5 B107 B
NOTES :Unit s in ug/1
ROD Performance Standard : 1,000 ug/L
NS - Not Sampled
U - No t detecte d at indicate d concentratio n
E - Estimated concentration exceeds the calibration range
B (Inorganics ) - Estimate d concentratio n is les s tha n the reportin g limi t
J (Inorganics ) - Compoun d detecte d i n associate d metho d blan k
Bold fon t indicate s detecte d concentratio n greate r tha n ROD Performanc e Standar d
Shadin g indicate s "E " qualifie d concentratio n for whic h a dilute d run concentratio n is unavailable .
Pag e 2 of9
Tabl e 3-7
Historica l Analytica l Result s - Metal s
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Company
Cedar Springs Plan t Site
Salisbury , Nort h Carolin a
BERYLLIU M
Quarter
1Q9 3
2Q93
3Q93
4Q93
IQ94
2Q94
3Q94
4Q94
1Q95
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q98
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-01
1 U
1 U
1.5 B
0.4 U
0.4 U
0.2 U
0.3 U
0.3 U
0.3 U
0.2 U
0.32 B
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
1 U
1 U
1 U
1 U
1 U
1 U
0.1 U
5 U
EX-0 2
NS
1 U
1.7 B
0.4 U
0.4 U
0.32 B
0.3 U
0.3 U
0.3 U
0.23 B
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
U
U
U
U
U
U
0.2 B
5 U
EX-03
1 U
1 U
1.8 B
0.4 U
0.4 U
0.24 B
0.3 U
0.3 U
0.3 U
0.2 U
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
U
U
U
U
U
U
0.1 U
5 U
EX-04
1 U
1 U
1.5 B
0.4 U
0.4 U
0.23 B
0.3 U
0.3 U
0.3 U
0.28 B
0.3 U
0.3 U
0.45 B
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
U
U
U
\ UU
U
0.1 U
5 U
NS-29
1 U
1 U
1.4 B
0.4 U
0.4 U
0.23 B
0.3 U
0.3 U
0.3 U
0.2 U
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
1 U
I U
1.2 J
2.1 J
1 U
1 U
0.1 U
5 U
NS-30
1 U
1 U
1.4 B
0.4 U
0.4 U
0.2 U
0.3 U
0.3 U
0.3 U
0.2 U
0.3 U
0.3 U
0.3 B
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
1 U
1 U
1 U
1 U
1 U
1 U
0.1 U
5 U
NS-31
1 U
1 U
1.8 B
0.4 U
0.4 U
0.2 U
0.3 U
0.3 U
0.3 U
0.2 U
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
1 U
1 U
1 U
1 U
1 U
1 U
0.1 U
5 U
NS-3 2
1 U
1 U
1.6 B
0.4 U
0.4 U
0.2 U
0.3 U
0.3 U
0.3 U
0.28 B
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
UU
U
U
U
1 U
0.1 U
5 U
NOTES :
Unit s i n ug/1
ROD Performanc e Standard: 17.5 ug/L
NS - Not Sample d
U - Not detected at indicate d concentration
B (Inorganics ) - Estimate d concentratio n is less tha n the reportin g limi t
J (Inorganics ) - Compoun d detecte d in associate d metho d blan k
Pag e 3 of 9
Table 3-7
Historica l Analytica l Result s - Metal s
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Springs Plant Site
Salisbury , Nort h Carolin a
CADMIU M
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-01
5 U
5 U
5 U
2.3 U
2.1 U
.3 U
.6 U
.6 U
2.1 U
.4 U
.2 U
.9 U
4.8 U
5 U
5 U
4.8 U
0.5 U
3 U
3 U
4 U
4 U0.2 6 U
0.2 6 U
0.5 U
1 U
0.5 U5 U
EX-02
NS
5 U
5 U
2.3 U
2.1 U
1.7 B
1.6 U
1.6 U
2.1 U
1.4 U
1.2 U
1.9 U
4.8 U
5 U
5 U
4.8 U
0.74 B
3 U
3 U
4.5 B
4 U
0.2 6 U
0.2 6 U
0.5 U
1 U
0.5 U5 U
EX-03
5 U
5 U
5 U
2.3 U
2.1 U
1.3 U
1.6 U
1.6 U
2.1 U
1.4 U
1.2 U
1.9 U
4.8 U
5 U
5 U
4.8 U
0.5 U
3 U
10.4
4 U
4 U
0.26 U
0.26 U
0.5 U
1 U
0.5 U
0.29 B
EX-04
5 U
5 U
5 U
2.3 U
2.1 U
.3 U
.7 B
.7 B
2.1 U
.4 U
.2 U
.9 U
4.8 U
5 U
5 U
4.8 U
0.5 U
3 U
3 U
17.8
4 U
0.26 . U
0.26 U
0.5 U
1 U
0.5 U
5 U
NS-29
5 U
5 U
5 U
2.3 U
2.1 U
.3 U
.6 U
.6 U
2.1 U
.4 U
.2 U
.9 U
4.8 U
5 U
5 U
4.8 U
0.5 U
3 U
3 U
4.5 B
4 U
0.26 U
0.26 U
0.5 U
1 U
0.5 U
5 U
NS-30
5 U
5 U
5 U
2.3 U
2.1 U
.3 U
.6 U
.6 U
2.1 U
.4 U
.2 U
.9 U
4.8 U
5 U
5 U
4.8 U
0.5 U
3 U
3 U
4 U4 U0.2 6 U
0.2 6 U
0.5 U
1 U
0.5 U
5 U
NS-31
5 U
5 U
5 U
2.3 U
2.1 U
1.3 U
1.6 U
1.6 U
2.1 U
1.4 U
1.2 U
1.9 U
4.8 U
5 U
5 U
4.8 U
0.5 U
3 U
26.9
4 U
4 U
0.26 U
0.53 U
0.5 U
1 U
0.5 U
5 U
NS-32
5 U
5 U
5 U
2.3 U
2.1 U
.3 U
.6 U
.6 U
.1 U
.4 U
.2 U
.9 U
4.8 U
5 U
5 U
4.8 U
0.5 U
3 U
3 U
4 U
4 U
0.26 U
0.2 6 U
0.5 U
1 U
0.5 U
5 U
NOTES:
Unit s in ug/1
ROD Performanc e Standard: 10 ug/L
NS - Not Sample d
U - Not detected at indicate d concentratio n
B (Inorganics) - Estimated concentration is less than the reporting limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Page 4 of 9
Tabl e 3-7
Historica l Analytica l Result s - Metal s
Plum e Peripher y Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Springs Plan t Site
Salisbury , Nort h Carolin a
CHROMIU M
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
IQ96
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-01
12
10 U
10 U
2.7 U
2.3 U
2.9 U
2.4 U
3 B
4.3 U
2 U3.1 U
2.4 U
7.7 B
5 U
5 U4.9 U
5 U
5 U
5 U
4 U
4 U
4.8 J
4 U
7.6 J
2 U
11.9
5 U
EX-02
NS
12.8
13.7
2.7 U
3.1 B
2.9 U
2.4 U
3 B
4.3 U
2 U
5.1 B
2.9 B
4.9 U
5 U
31.1
17.1
5 U
5.6 B
5 U
4 U
4 U
4.2 J
4 J
14.6
2 U
12.7
6.1
EX-03
10 U
10 U
10 U
2.8 B
2.4 B
2.9 U
2.4 U
2.4 U
4.3 U
2 U3.4 B
2.4 U
7.8 B
5 U
5 U
62.6
5 U
5 U
5 U
4 U
4 U
8.25 J
4 U
8.2 J
2 U
16.7
23.2
EX-04
10 U
10 U
10 U
2.7 U
4.3 B
2.9 U
2.4 U
3.9 B
4.3 U
2 U3.1 U
2.4 U
7.4 B
5 U
5 U4.9 U
11.6
5 U
5 U
4 U
4 U
4.1 . J
4 X U
5.1 J
2 U
1.9 B
5 U
NS-29
11.1
14.5
10 U
2.7 U
3 B
2.9 U
2.4 U
2.4 U
4.3 U
2 U
3.1 U
2.4 U
6.9 B
5 U
5 U4.9 U
5.8 B
5 U
5 U
4.3 B
4 U
12.3
8.8 J
10.8
9.9
36.8
26.9
NS-30
10 U
10 U
10 U
2.7 U
2.7 B
2.9 U
2.6 B
2.4 U
4.3 U
2 U
3.1 U
2.4 U
9.8 B
5 U
5 U
4.9 U
5 U
5 U
5 U
4 U
4 U
4.1 J
4 U
4.8 J
2 U
1.9 B
5 U
NS-31
77.5
74
22.2
2.7 U
2.3 U
13.3
2.4 U
2.4 U
4.3 U
2 U
3.1 U
2.4 U
4.9 U
5 U
5 U
4.9 U
7.2 B
5 U
5 U
4 U
101
12.9
5.5 J
12.9
25
2 B
1.9 B
NS-32
10 U
10 U
10
2.7 U
2.3 U
2.9 U
3.1 B
2.4 B
4.3 U
2 U3.1 U
2.4 U
8.8 B
5 U
5 U
4.9 U
5 U
5 U
5 U
4 U
4 U
4 U
4 U
8.6 J
2 U
0.9 U
5 U
NOTES:
Unit s in ug/1
ROD Performanc e Standard: 50 ug/L
NS - Not Sampled
U - Not detected at indicate d concentratio n
B (Inorganics) - Estimated concentratio n is less than the reporting limi t
J (Inorganics ) - Compoun d detecte d in associate d metho d blan k
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Pag e 5 of 9
Tabl e 3-7
Historica l Analytica l Result s - Metal s
Plum e Peripher y Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
MANGANES E
Quarte r
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
IQ9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QOO1Q02
EX-0 1
222
206
11 2
24.3
25.1
78.8
50.3
42
9.9 B
53.4
11 7
98.6
14 2
13 2
53.1205
345
46 1
31 6
33 2
345
23 7
18 2
28 5
320
80.6169
EX-02
NS
718 0
1080 0
1080 0
14300
1710 0
1510 0
14000
1190 0
18800
1830 0
19000
17900
1610 0
16300
16800
1800 0
1160 0
1390 0
1690 0
1100 0
1210 0
1150 0
2060 0
2000 0
3810 0
1510 0
EX-03
3950
2760
338 0
1120 0
1100 0
3980
143 0
3640
201 0
481 0
3970
338 0
213 0
285 5
4270
3920
261 0
3960
3840
451 0
4695
467 5
3040
481 0
3300
3270
218 0
EX-04
4290
3270
481 0
5090
561 0
5280
5430
4970
4730
417 0
321 0
4750
358 0
388 0
316 5
334 0
514 0
4530
4330
3880
4520
413 0
305 5
5250
530 0
3980
2240
NS-29
475
192.5
20 1
17 7
15 3
265
28 7
25 9
23 9
268
61 1
381 0
4030
178 0
85605840
4820
371 0
1200 0
18400
22200
3210 0
13600
39300
360 0
11700 0
104000
NS-3 0
839
162 0
143 5
211 0
217 0
2270
193 0
2480
2360
2290
180 0
199 0
154 0
172 0
157 0
140 0
166 0
151 0
153 0
152 0
14 7
125 0
83 1
104 0
970
"~ 12~30': V :E'-'
107 0
NS-3 1
17.9
47.1
28.9
21.4
22.1
52
26.1
20.4
372
25.8
35.7
63.9
60.3
14 1
12 3510
111 0
993
110 0
187 0
2670
415 0
198 0
215 0
340
82.522.5
NS-3 2
80.6
78.2
10 8
99.8107
10 6
10 6
10 8
10 7
11 7
10 7
11 2
92.6
10 5
10 9
10 9
11 4
11 4
11 5
11 8
11 8
13 9
81.4
13 1
12 0
12 5119
NOTES:
Unit s in ug/1
ROD Performanc e Standard : 7,700 ug/L
NS - No t Sample d
E - Estimate d concentratio n exceed s the calibratio n rang e
B (Inorganics ) - Estimate d concentratio n is less than the reporting limi tBold fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Shadin g indicate s "E " qualifie d concentratio n fo r whic h a dilute d ru n concentratio n i s unavailable .
Pag e 6 of 9
Tabl e 3-7
Historica l Analytica l Result s - Metal s
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
NICKE L
Quarter
1Q9 32Q93
3Q93
4Q93
1Q9 4
2Q9 4
3Q9 4
4Q9 4
1Q9 5
2Q9 5
3Q95
4Q9 5
1Q9 6
2Q9 6
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q9 94QOO
1Q0 2
EX-0 1
20 U
20 U
20 U
11.8 B
10.4 U
6.2 U
6.9 U
6.9 U
10.3 U
5.5 U
7.2 U
8.8 U
15.3 U
15 U
15 U
15.3 U
20 U
20 U
20 U
16 U
16 U
14 U
14 U
14 U
5 U
30.4
40 U
EX-02
NS
75.5
20 U
13.8 B
10.4 U
6.2 U
6.9 U
6.9 U
10.3 U
5.5 U
7.2 U
8.8 U
15.3 U
15 U
43.815.3 U
20 U
20 U
20 U
16 U
16 U
14 U
14 U
14 U
8.8
22.7
12.3 U
EX-03
20 U
20 U
20 U
8.4 U
10.4 U
6.2 U
6.9 U
6.9 U
10.3 U
5.5 U
7.2 U
8.8 U
15.3 U
15 U
15 U81.6
20 U
20 U
20 U
16 U
16 U
14 U
14 U
14 U
5 U
12.5
19.2 B
EX-04
20 U
20 U
20 U
8.4 U
10.4 U
6.2 U
6.9 U
6.9 U
10.3 U
5.5 U
7.2 U
8.8 U
15.3 U
15 U
15 U15.3 U
20 U
20 U
20 U
16 U
16 U
14 , U
14 '•• U
14 U
5 U
4.7 B
40 U
NS-29
20 U
20 U
20 U
8.4 U
10.4 U
6.2 U
6.9 U
6.9 U
10.3 U
5.5 U
7.2 U
8.8 U
15.3 U
15 U
15 U15.3 U
20 U
20 U
20 U
16 U
16 U
14 U
14 U
14 U
51
46.9
45.3
NS-30
20 U
20 U
20 U
8.4 U
10.4 U
6.2 U
6.9 U
6.9 U
10.3 U
5.5 U
7.2 U
8.8 U
15.3 U
15 U
15 U15.3 U
20 U
20 U
20 U
16 U
16 U
14 U
14 U
14 U
5 U
1.8 B
1.8 B
NS-3 1
39.3 B
47.5
20 U
8.4 U
10.4 U
9.6 B
6.9 U
6.9 U
10.3 U
5.5 U
7.2 U
8.8 U
15.3 U
15 U
15 U15.3 U
20 U
20 U
20 U
16 U
51.6
23.2 J
14 U
14 U
17
1.7 B
40 U
NS-32
20 U
20 U
20 U
8.4 U
10.4 U
6.2 U
6.9 U
6.9 U
10.3 U
5.5 U
7.2 U
8.8 U
15.3 U
15 U
15 U15.3 U
20 U
20 U
20 U
16 U
16 U
14 U
14 U
14 U
5 U
1 U
40 U
NOTES:
Unit s in ug/1
ROD Performance Standard: 350 ug/L
NS - Not Sampled
U - No t detecte d at indicate d concentratio n
B (Inorganics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
J (Inorganics ) - Compoun d detecte d in associate d metho d blan k
Pag e 7 of 9
Table 3-7
Historica l Analytica l Result s - Metal s
Plum e Peripher y Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Ceda r Spring s Plan t Site
Salisbury , Nort h Carolin a
SELENIU M
Quarter
1Q9 3
2Q93
3Q93
4Q931Q94
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 82Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-0 1
2 U
2 U
2 U
2.3 U
1.7 U
2.6 U
3.1 U
3.1 U
0.9 U
2.7 B
1.7 U
1 U
1.6 U
0.8 U
0.8 U
0.8 U
6.9
5 U
5 U
5 U
5 U4.3 U
4.3 U
5 U
5 U
2.3 U
5 U
EX-02
NS
2 U
2 U
4.6 U
3.4 U
1.6 B
3.1 U
3.1 U
0.9 U
3 B
1.8 B
1 U
3.2 U
1.6 U
1.6 U
0.8 U
12.4
9.8
5 U
10.5
5.5
4.4 J
4.3 U
5.6
7.4
14.9
10.7
EX-03
4 U
2 U
2 U
4.6 U
3.4 U
2.6 U
3.1 U
3.1 U
0.9 U
2.7 U
1.7 U
1 U
1.6 U
0.8 U
1.6 U
0.8 U
5
5 U
6.3
5 U
5 U
4.3 U
4.3 U
5 U
5 U
2.3 U5 U
EX-04
4 U
2 U
2 U
2.3 U
1.7 U
2.6 U
3.1 U
3.1 U
0.9 U
2.7 U
1.7 U
1 U
1.6 U
0.8 U
0.8 U
0.8 U
5 U
5 U
5 U
5 U
5 U
4.3 U
4.3 \ U
5 U
5 U
2.3 U
5 U
NS-29
2 U
2 U
2 U
2.3 U
1.7 U
2.6 U
3.1 U
3.1 U
0.9 U
2.7 U
3 B
1 U
3.2 U
0.8 U
1.6 U
1.6 U
5 U
7.2
5 U
5 U
12.8
15.6
5.9
14.7
14
50.7
44
NS-30
2 U
2 U
2 U
2.3 U1.7 U
2.6 U
3.1 U
3.1 U
0.9 U
2.7 U
2 B
I U
1.6 U
0.8 U
1.6 U
0.8 U
5 U
5 U
5 U
5 U
5 U
4.3 U
4.3 U
5 U
5 U
2.8 B
5 U
NS-3 1
2 U
2 U
2 U
2.3 U1.7 U
2.6 U
3.1 U
3.1 U
0.9 U
2.7 U
2.7 B
1 U
1.6 U
0.8 U
0.8 U
0.8 U
5 U
5 U
5 U
5 U
5 U
4.3 U
8.6 U
5 U
5 U
2.3 U
5 U
NS-32
2 U
2 U
2 U
2.3 U
1.7 U
2.6 U
3.1 U
3.1 U
0.9 U
3.2 B
2 B
1 U
1.6 U
0.8 U
0.8 U
0.8 U
5 U
5 U
5 U
5 U
5 U
4.3 U
4.3 U
5 U
5 U
2.3 U
5 U
NOTES:
Unit s i n ug/1
ROD Performanc e Standard : 10 ug/L
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
B (Inorganics ) - Estimate d concentratio n is les s tha n the reportin g limi t
J (Inorganics ) - Compoun d detecte d in associate d metho d blan k
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Pag e 8 of 9
Tabl e 3-7
Historica l Analytica l Result s - Metal s
Plum e Peripher y Extractio n and Monitorin g Wells
Nationa l Starch and Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
ZINC
Quarter
1Q9 3
2093
3Q93
4Q931Q94
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q9S
3Q98
4Q98
4Q99
4QO O1Q02
EX-01
35.3
32.7
15.5 B
9.7 B
15.5 B
15.3 B
9.5 B
11.3 B
15.7 B
9.4 B
43.6
5.2 U
7.6 B
12.1 B
57.6
33.9
6.9 B
5 U
13.8 B
15.1 B
15 U
5 U
5 U
5 U
15
18.8 B
20 U
EX-02
NS
15.4 B
29.5
56.5
5.4 B
3.4 B
76.5
11.1 B
15.4 B
5.8 U
2.6 U
5.2 U
14.3 B
7.7 B
31.9
28.2
8.6 B
10.9 B
28.4
15 U
15 U
5 U
5 U
22.5
10 U
63.2
4.6 B
EX-03
11.2 B
16.9 B
7.6 B
2.5 B
9 B
0.9 U
3.8 U
8.8 B
48
16 B
2.6 U
5.2 U
9 B
16.2
14.7 B
34
12.1 B
5 U
8.6 B
15 U
15 U
5 U
5 U
5 U
10 U
72.894.5
EX-04
13 B
17.2 B
7 B
1.8 U
55.2
37.7
12.4 B
13 B
7.6 B
5.8 U
4 B
5.2 U
15.6 B
8.8 B
2 U
109
14.5 B
5 U
18.1 B
15 U
15 U
5 U
8.2 '••-, J
5 U
10 U
234
20 U
NS-29
10.3 B
17 B
11.1 B
2.6 B
5.2 B
2 B
11.8 B
6.5 B
4.5 B
5.8 U
2.6 U
5.2 U
2.4 U
6.6 B
3.1 B
19 B
10.3 B
5 U
21.8
15 U
15 U
5 U
5 U
5 U
18
24.44.8 B
NS-30
8.2 B
12.1 B
5 U
2.2 B
1.7 U
0.9 U
3.8 U
15.7 B
3.6 B
5.8 U
2.6 U
5.2 U
2.4 B
6.4 B
2 U
23.5
7.7 B
5 U
13.2 B
15 U
15 U
5 U
5 U
5 U
13
17.2 B20 U
NS-31
27.9
164 0
26.6
2.6 B
1.7 U
10.7 B
4 B
5 B
14.4 B
5.8 U
2.6 U
5.2 U
3.2 B
5.5 B
2.1 B
15.3 B
15.5 B
5 U
15.9 B
15 U
15.2 B
5 U
5 U
17.2 J
21
31.420 U
NS-32
6.4 B
57
25.2
1.8 U
3.3 B
3.4 B
7.9 B
10.2 B
11.3 B
6 B
2.6 U
5.2 U
9.4 B
6.9 B
4.4 B
19.9 B
23.7
5 U
31.8
15 U
15 U5 U
5 U
5 U
10 U
8.6 U
20 U
NOTES:
Unit s in ug/1
ROD Performanc e Standard : 7,350 ug/L
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
B (Inorganics) - Estimated concentration is less than the reporting limi t
J (Inorganics ) - Compoun d detecte d in associate d metho d blan k
Page 9 of9
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Tabl e 3-8
Compariso n of 2002 Analytica l Result s for Trenc h Area Well s to Performanc e Standard s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolina
Wel l ID
Sample No.
Sample Date
Dilutio n Facto r
Associated Method Blan k
VOCs
Aceton e
Benzene
Bromodichloromethan e
Chlorofor m
1 ,2-Dichloroethan e
1,1-Dichloroethen e
1 ,2-Dichloropropan e
Ethylbenzen e
Methylen e chlorid e
Toluen e
1 , 1 ,2-Trichloroethane
Trichloroethen e
Viny l chlorid e
Xylen e
Dilutio n Facto r
Associate d Metho d Blan k
SVOCs
bis(2-Chloroethyl ) ethe r
4-Nitropheno l
Dilutio n Factor
Associate d Metho d Blan k
Metals
Arsenic
Bariu m
Berylliu m
Cadmiu m
Chromiu m
Manganes e
Nicke l
Seleniu m
Zinc
Performanc e
Standar d
3,500
5
5
5
5
7
6
3,50 0
5
2,00 0
5
5
2
350
5
350
10
1,00 0
17.5
10
50
7,700
350
10
7,350
EX-0 5
C2C08 0 16600 1
03/06/02
3,000
EV8PW1A A
24,000 J
3,000 U
3,000 U
3,000 U
3,000 E
3,000 U
3,000 U
3,000 U
6,000 U
26,000
3,000 U
3,000 U
6,000 U
9,000 U
60
EV71V1A A
600 U
3,000 U
1
C2C 11 0000- 128
7.1 B
228
5.0 U
16.5 J E
15.2
52,600 *
1640
47.6
365
EX-0 5 DL
C2C08 0 166001
03/06/02
15,000
EWFRTIA A
53,000 J
15,00 0 U
15,000 U
15,00 0 U
390,000
15,00 0 U
15,000 U
15,000 U
30,000 U
24,000
15,000 U
15,000 U
30,000 U
45,000 U
-
-
NA
NA
-
-
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-06
C2C 130 11 9003
03/11/02
1
EWC3V1A A
10 U
U
U
U
U
U
U
U
2 U
U
U
U
2 U
.-• 3 U
1
EWC441A A
10 U
50 U
1
EWC441A A
10 U
24.6 B
5.0 U
5.0 U
13.6
256
2.2 B
5.0 U
17.5 B
EX-07
C2C080 16600 2
03/06/02
10
EV8VXIA A
80 J
10U
10 U
10 U
270
10 U
10 U
10 U
20 U
48
10 U
10 U
20 U
30 U
1
EV71V1A A
10 U
50 U
1
C2C 11 0000- 128
10 U
29.5 B
0.6 BJ
5.0 U
5.0 U
1,17 0
13.8 B
5.0 U
5.7 B
EX-08
C2C080 166003
03/06/02
3,000
EV8VX1A A
58,000
3,000 U
3,000 U
3,000 U
170,000 E
3,000 U
2,000 J
3,000 U
6,000 U
17,000
3,000 U
3,000 U
6,000 U
9,000 U
60
EV71V1A A
1,80 0
3,000 U
1
C2C 11 0000- 128
6.6 B
21.5 B
11.7 J
6.3 J
35.7
196,000 **
758
72.3
1,000
Units in ug/1
* Sampl e dilute d at a facto r of 10 for thi s compound .
** Sampl e dilute d at a facto r of 100 for thi s compound .
U - Not detected at indicate d concentratio n
E - Estimate d concentratio n exceed s the calibratio n range
J (Organics ) - Estimate d concentratio n is less than the reportin g limi t
J (Inorganics ) - Compoun d detected in associate d metho d blan k
B (Inorganics ) - Estimate d concentratio n is less tha n the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n Performanc e Standar d
Jw ^\
Page 1 of3
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Table 3-8
Compariso n of 2002 Analytica l Result s for Trenc h Area Well s to Performanc e Standard s
Nationa l Starc h an d Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
Well ID
Sample No.
Sample Date
Dilutio n Factor
Associated Metho d Blan k
VOCs
Aceton e
Benzen e
Bromodichloromethan e
Chlorofor m
1 ,2-Dichloroethan e
1 , 1 -Dichloroethcn e
1 ,2-Dichloropropan e
Ethylbenzen e
Methylen e chlorid e
Toluen e
1 ,1 ,2-Trichloroethan e
Trichloroethen e
Viny l chlorid e
Xylene
Dilutio n Factor
Associate d Metho d Blan k
SVOCs
bis(2-Chloroethyl ) ethe r
4-Nitropheno l
Dilutio n Factor
Associate d Metho d Blan k
Metals
Arsenic
Barium
Berylliu m
Cadmiu m
Chromiu m
Manganes e
Nicke l
Seleniu m
Zinc
Performanc e
Standard
3,500
5
5
5
5
7
6
3,500
5
2,000
5
5
2
350
5
350
10
1,00 0
17.5
10
50
7,700
350
10
' 7,350
EX-0 8 DL
C2C080 166003
03/06/02
5,000
EV8VX1A A
70,000
5,000 U
5,000 U
5,000 U
190,000
5,00 0 U
2,300 J
5,000 U
10,000 U
23,000
5,000 U
5,000 U
10,000 U
15,000 U
-
-
NA
NA
-
-
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-0 9
C2C080 166004
03/06/02
2,000
EV8VX1A A
30,000 J
2,000 U
2,000 U
2,000 U
87,000 E
2,000 U
6,400
2,000 U
4,000 U
30,000
2,000 U
2,000 U
4,000 U
2,200 J
60
EV71V1A A
2,900
3,000 U
1
C2C 11 0000- 128
3 B
12.7 B
11 J
2.0 BJ
21.7
108,000 **
407
42.5
983
EX-09 DL
C2C080 166004
03/06/02
3,000
EV8VX1A A
25,000 J
3,000 U
3,000 U
3,000 U
91,000
3,000 U
7,000
3,000 U
6,000 U
39,000
3,000 U
3,000 U
6,000 U•"9,00 0 u
-
-
NA
NA
-
-
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX- 10
C2C080 166005
03/06/02
100
EV8VX1A A
33,000 E
100 U
100 U
10 0 U
12,000 E
10 0 U
9,800 E
1,60 0
20 0 U
2,900
100 U
100 U
140 J
5,900
20
EV71V1A A
4,000 E
1,000 U1
C2C 11 0000- 128
3.1 B
14.3 B
12.1 J
1.1 B J
32.8
101,000 **
292
33
789
EX-10D L
C2C080 16600 5
03/06/02
1,000
EV8VX1A A
44,000
1 ,000 U
1,0001)
1,OOO U
14,000
1 ,000 U
11,000
1,400
2,000 U
3,000
l.OOO U
1 ,000 U
2,000 U
5,300
100
EV71V1A A
4,800
5,000 U
-
-
NA
NA
NA
NA
NA
NA
NA
NA
NA
Unit s in ug/1
** Sampl e dilute d at a facto r of 100 for this compound .
U - No t detecte d at indicate d concentratio n
E - Estimate d concentratio n exceeds the calibratio n range
J (Organics) - Estimate d concentratio n is less than the reporting limi t
J (Inorganics ) - Compoun d detecte d in associate d metho d blan k
B (Inorganics ) - Estimate d concentratio n is less than the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greater tha n Performanc e Standar d
Page 2 of3
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Tabl e 3-8
Comparison of 2002 Analytical Results for Trench Area Wells to Performance Standards
Nationa l Starc h an d Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
Wel l ID
Sample No.
Sampl e Dat e
Dilutio n Facto r
Associate d Metho d Blan k
VOCs
Aceton e
Benzen e
Bromodichloromethan e
Chlorofor m
1,2-Dichloroethan e
1 , 1 -Dichloroethen e
1 ,2-Dichloropropan e
Ethylbenzen e
Methylen c chloride
Toluene
1 ,1 ,2-Trichloroethan e
Trichloroethen c
Viny l chlorid e
Xylen e
Dilutio n Facto r
Associate d Metho d Blan k
SVOCs
bis(2-Chloroethyl ) ethe r
4-Nitropheno l
Dilutio n Facto r
Associate d Metho d Blan k
Metals
Arseni c
Bariu m
Berylliu m
Cadmiu m
Chromiu m
Manganes e
Nicke l
Seleniu m
Zin c
Performanc e
Standar d
3,500
5
5
5
5
7
6
3,500
5
2,000
5
5
2
350
5
350
10
1,000
17.5
10
50
7,700
350
10
7,350
NS-09
C2C20015100 1
03/18/0 2
1
EWRTQ1A A
10 U
1.0 U
1.0 U
0.64 J
1,400 E
7.8
0.53 J
8.2
3.8
180 E
1.9
4.7
47 E
25
1
EWPV51A A
10 U
50 U
1
C2C2 1000- 158
2.5 B
346
5.0 U
5.0 U
5.9
12,800 *
6.6 B
5.2
5.8 B
NS-09 DL
C2C20015100 1
03/18/02
60
EWWXW1A A
600 U
60 U
60 U
60 U
1,400
60 U
60 U
60 U
120 U
150
60 U
60 U
42 J
180 U
1
EW4FN1A A
10 U
50 U
-
-
NA
NA
NA
NA
NA
NA
NA
NA
NA
NS-10
C2C20015I00 3
03/18/02
1
EWRTQ1A A
10 U
.0 U
.0 U
.0 U
13
.0 U
.0 U
.0 U
2.0 U
.0 U
.0 U
.0 U
2.0 U
•••' 3.0 U
1
EWPV51A A
10 U
50 U
1
C2C2 1000- 158
10 U
98.5 B
5.0 U
5.0 U
2.1 B
1,86 0
15.1 B
5.0 U
9.3 B
NS-1 1
C2C20015100 2
03/18/02
1
EWWXW1A A
10 U
.O U
.O U
.O U
.O U
.O U
.O U
2.2
2.0 U
1.4
1.0 U
1.0 U
2.0 U
9.1
1
EWPV51A A
10 U
SO U
1
C2C2 1000- 158
2.7 B
73 B
5.0 U
5.0 U
1.4 B
117
40 U
5.0 U
20 U
NS-1 5
C2C20015100 5
03/18/02
1
EWWXW1AA
10 U
.0 U
.0 U
.0 U
27
.0 U
.0 U
.0 U
2.0 U
0.8 J
1.0 U
1.0 U
2.0 U
3.0 U
1
EWPV51A A
10 U
50 U
1
C2C2 1000- 158
10 U
305
5.0 U
5.0 U
4.5 B
10,600 *
2.0 B
5.0 U
20 U
NOTES :
Unit s in ug/1
* Sampl e dilute d at a facto r of 2 for this compound .
U - No t detected at indicate d concentratio n
E - Estimate d concentratio n exceeds the calibratio n range
J (Organics ) - Estimate d concentratio n is less tha n the reportin g limi t
B (Inorganics ) - Estimate d concentratio n is less tha n the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n Performanc e Standar d
Page 3 of3
Tabl e 3-9
Historica l Analytica l Result s - VOC s
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Ceda r Spring s Plan t Site
Salisbury , North Carolin a
ACETON E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
IQ98
2Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
2400 0 D
3200 J
28000
27000 B
33000 B
34000
36000
29000 B
17000 B
29000
45000 DB
86000 4
100000 D
24000 J
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
420
36
300 D
170 B
470 D B
500 D
540 D
120 B
430 B
120
73
11
2 U
10 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
710 0 D J
920 J
550 D J
4900 B
4000 B
2000 B
3600
3300 B
59 J B
47000 D
36000 D
5000 U
10 U80 J
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
230000 D
1100 0
72000
12000 0 D B
130000 DB
67000 B
220000 D
63000 DB
72000 D
130000 D
65000 D
100000
4000 U
58000
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
23000 D
810 0
37000
53000 DB
40000 B
23000 B
19000
24000 DB
14000
21000.
13000
100000 U
10000 U
30000 J
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
43000 D
8200
75000
96000 B
92000 B
49000 B
210000 " ' E
82000 D B
93000 B
20000 0 D
77000 D
150000 4
93000 D44000
NS-09
NS
10 U
3000 D
720
130
65000 B
330000
390000
5400 D
87000 D
450 D
160 0
7 J
110
22 J
200
110 B
94 JB
830 B
180
79 JB
53 J
570
22 J
10 U
20 U
10 U
NS-1 0
NS
10 U
100
330 U
500 U
210 0 B
670 U
270
620 U
800
17 0 U
670 U
500 U
10 0 U
8 J
10 0 U
88 B J
78 J B
300 D B
10 0 U
10 U
6 J
10 U
2 J
12
42
10 U
NS-1 1
NS
10 U
15
130
410 0
44 B
29
54
21
10 U
10 U
17
10 U
10 U
7 J
10 U
6 B J
22 B
32 DB J
14
10 U
2 J
10 U
6 J
16
4 U
10 U
NS-1 5
NS
NR
10 U
67 U
50 U
25 U
530
18 B
25 U
10 U
120
27
20 U
5 J
8 J
10 U
15 B
10 U
40 B
7 J
9 JB
6 J
10 U
10 U
120 4
20 U10 U
NOTES :
Unit s in ug/1
RO D Performanc e Standard : 3,500 ug/L
NR - Not Reporte d
NS - Not Sample d
U - No t detected at indicate d concentratio nD - Concentratio n fro m a secondar y dilutio n analysi s
E/4 - Estimate d concentratio n exceed s th e calibratio n rang e
J (Organics ) - Estimate d concentratio n is less tha n th e reportin g limi t
B (Organics ) - Compoun d detecte d in associate d metho d blan k
Bold fon t indicate s detected concentratio n greater than ROD Performanc e Standar d
Italic fon t indicates detection limit greater than ROD Performanc e StandardShading indicates "E" qualifie d concentratio n for whic h a dilute d run concentratio n is unavailabl e
Pag e 1 o f 1 4
Tabl e 3-9
Historica l Analytica l Result s - VOCs
Trench Area Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolin a
BENZEN E
Quarter
1Q9 3
2Q9 3
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q961Q97
2Q9 7
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
49 J
5000 U
2000 U2000 U
2000 U
2000 U
2000 U
5000 U
5000 U
5000 U
2500 U
500 U
5000 U3000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
30 J
3300 U250 U
250 U
250 U
250 U
250 U
1000 U100 U
500 U
1000 U
500 U
5 U
10 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
34 J
5000 U5000 U5000 U
5000 U
5000 U
5000 U
2500 U
2500 U
1000 U
2500 U
1200 U
2000 U
3000 U
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
64 J
3300 U
2500 U
2500 U
2500 U
2500 U2500 U
1000 U
1000 U
2000 : U
1000 '•' U
5000 U
2000 U2000 U
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
40 J
/70 0 U5000 U5000 U
5000 U
5000 U
5000 U
500 U
500 U
5000 U
500 U
1000 U
5000 U
100 U
NS-09
NS
5 U
10 U
250 U
10 U3100 U
8300 U
10000 U
1 J
500 U
5 U
57 U
10 U
50 U
50 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
500 U
100 U
1 U
10 U
1 U
NS-1 0
NS
5 U
10 U
330 U
500 U
310 U
330 U
17 U
310 U
89 U
83 U
330 U
250 U
50 U
10 U
100 U100 U
100 U
100 U
100 U
10 U
20 U
10 U
10 U
1 U
1 U
1 U
NS-1 1
NS
5 U
10 U
25 U
500 U
5 V
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
2 U
1 U
NS-1 S
NSNR
10 U
67 U
50 U
12 U
25 U
5 U
12 U
5 U
5 U
8 U
10 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
10 U
1 U
NOTES :
Unit s in ug/l
RO D Performanc e Standard : 5 ug/L
NR - Not Reporte d
NS - Not Sampled
U - Not detected at indicate d concentratio n
J (Organics) - Estimated concentratio n is less than the reporting limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 2 o f 1 4
Tabl e 3-9
Historica l Analytica l Result s - VOCs
Trench Are a Extractio n and Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Cedar Springs Plan t Site
Salisbury , Nort h Carolin a
BROMODICHLOROMETHAN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q9 6
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
5000 U
2000 U
2000 U
2000 U
2000 U
2000 U
5000 U5000 U
5000 U
2500 U
500 U
5000 U
3000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U10 U
10 U
10 U
1 U
1 U
1 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
3300 U
250 U
250 U
250 U
250 U
250 U
1000 U
100 U
500 U
1000 U
500 U
5 U
10 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
5000 U
5000 U
5000 U5000 U
5000 U5000 U
2500 U
2500 U
1000 U
2500 U
1200 U
2000 U
3000 U
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
3300 U2500 U
2500 U2500 U
2500 U
2500 U
1000 U
1000 U
2000 . U
1000 '•: U
1000 U
5000 U
2000 U
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
1700 U
5000 U
5000 U5000 U
5000 U
5000 U
500 U
500 U
5000 U
500 U
1000 U
5000 U
100 U
NS-09
NS
5 U
70 U
250 U
10 U
3100 U
8300 U
10000 U
5 U
500 U
5 U
57 U
10 U
50 U
50 U100 U
100 U
100 U
100 U
100 U
100 U
100 U
500 U
100 U
1 U
70 U
1 U
NS-I O
NS
5 U
70 U
330 U
500 U
310 U
330 U
17 U
310 U
89 U
83 U
330 U250 U
50 U
10 U
100 U
100 U
100 U
100 U
100 U
10 U
20 U
10 U
10 U
1 U
1 U
1 U
NS-1 1
NS
5 U
70 U
25 U
500 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
2 U
1 U
NS-1 5
NS
NR
10 U
67 U
50 U
12 U
25 U
5 U
72 U
5 U
5 U
8 U
10 U
5 U
70 U
10 U
10 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
1 U10 U
1 U
NOTES:
Unit s in ug/1
RO D Performanc e Standard : 5 ug/L
N R - No t Reporte d
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
Itali c fon t indicate s detectio n limi t greate r than ROD Performanc e Standar d
Page 3 of 14
Table 3-9
Historica l Analytica l Result s - VOCs
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Springs Plan t Site
Salisbury , North Carolin a
CHLOROFOR M
Quarter
1Q93
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q9 5
3Q95
4Q95
1Q96
2Q96
3Q96
4Q96
1Q97
2Q97
3Q97
4Q97
1Q98
2Q98
3Q98
4Q98
4Q9 9
4QO OIQ02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
44 J
5000 U
2000 U2000 U
2000 U
2000 U
2000 U
5000 U
5000 U
5000 U
2500 U
500 U
5000 U3000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25 U
10 U10 U10 U
10 U
10 U
10 U
10 U
10 U10 U
10 U
1 U
1 U
1 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
3300 U
250 U250 U
250 U
250 U
250 U
1000 U
100 V500 U
WOO U
500 U
5 U10 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 U
5000 U
5000 U5000 U
5000 U
5000 U
5000 U
2500 U2500 U
1000 U
2500 U
1200 U
2000 U3000 U
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 U
3300 U2500 U
2500 U
2500 U
2500 U
2500 U
1000 U1000 U
2000 . U
1000 '-• U
5000 U
5000 U
2000 U
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
1700 U5000 U
5000 U
5000 U
5000 U
5000 U
500 U500 U
5000 U
500 U
1000 U
5000 U
100 U
MS-0 9
NS
5 U
10 U
250 U
10 U
3100 U
8300 U
10000 U
5 U
500 U
5 U
57 U
10 U
50 U
50 U
100 U100 U
100 U
100 U
100 U
100 U
100 U
500 U
100 U
1.8
10 U
0.64 J
NS-1 0
NS
5 U
1 J
330 U
500 U
310 U
330 U
17 U
310 U
89 U
83 U
330 U
250 U
50 U
10 U
100 U100 U
100 U
100 U
100 U
10 U20 U
10 U
10 U
1 U
1 U
1 U
NS-n
NS
5 U
10 U
25 U
500 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U10 U
10 U
10 U
2 J
10 U10 U
10 U
10 U
1 U
2 U
1 U
NS-15
NS
NR
10 U
67 U
50 U
12 U
25 U
5 U
12 U
5 U
5 U
8 U
10 U
5 U
10 U10 U
10 U
10 U
10 U
10 U
10 U10 U
10 U
10 U
1 U
10 U
1 U
NOTES :
Unit s in ug/1
RO D Performanc e Standard : 5 ug/L
NR - Not Reporte d
NS - Not Sampled
U - Not detected at indicate d concentratio n
J (Organics) - Estimated concentration is less than the reporting limit
Bold fon t indicate s detected concentratio n greater than ROD Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 4 of 1 4
Tabl e 3-9
Historica l Analytica l Result s - VOCs
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
1,2-DICHLOROETHAN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q961Q97
2Q97
3Q97
4Q97
1Q9 82Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
350000 D
5000 U
430000 D
510000 D
470000 D
340000 D
380000 D
340000 D
340000 D
230000 D
300000 D
400000
530000 D
390000
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
920
10 U
240 D
53
530 D
550 D
140
80
550
120
12
1 U
1 U
1 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
83000 D
3300 U
50000 D
34000 D
35000 D
36000 D
27000 D
19000100 U
14000 0 D
13000 0 D
JO O U
180 D
270
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
N SNS
NS
NS
330000 D
5000 U
350000 D390000 D
290000 D
310000 D
270000 D
220000 D220000 D
210000 D
180000 D
180000
19000 0 D
19000 0
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
71000 D
3300 U
190000 D
180000 D
130000 D
160000 D
130000 D
110000 D
85000 D
79000. D
71000 D
100000
160000 D
9100 0
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
28000 D
7700 U
35000
31000
30000
53000
59000
44000 D29000 D
39000
36000 D
25000
4000 0 D
1400 0
NS-0 9
NS
10000 D
14000 D
470 0
170
3100 U
8300 U
10000 U
30
500 U11
170 0
9 J
840
210 0 D
710 0 D
10000 D
4400 D
4900 D
5900 D
10000 D
25000
25000 D
17000 D
21000
550 D
140 0
NS-1 0
NS
16000 D
8000 D
2800
8800
9700
710 0
420
910 0
9800 D
7600 D
810 0
610 0
410 0 • E
220 0 D
4500 D
2000 D
870
180 0
160 0
920 D
190 0 D
120 0 D
460 D
330
13
13
NS-1 1
NS
5 U
100
25 U
500 U
8
5 U
5 U
5 U
5 U
65
9
5 U
11
34
400 D
3 J
170 D
260 D
24
4 J
15
15
1 U
2 U
1 U
MS-1 5
NS
NR
440 D
530
480
400
380
, 380 E
370
330 D
250 D
260
250
210 ""E '
67'
150
190
120
160 D
160
100
130
20
98
69
76 D
27
NOTES:
Unit s in ug/1
RO D Performanc e Standard : 5 ug/L
NR - Not ReportedNS - Not Sampled
U - Not detected at indicate d concentratio n
E - Estimated concentration exceeds the calibration range
D - Concentratio n from a secondary dilutio n analysis
J (Organics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
Bold fon t indicate s detected concentratio n greater than ROD Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r than RO D Performanc e Standar d
Shadin g indicate s "E" qualifie d concentratio n for whic h a dilute d run concentratio n is unavailabl e
Pag e 5 of 1 4
Tabl e 3-9
Historica l Analytica l Results - VOC s
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Springs Plan t Site
Salisbury , Nort h Carolin a
1,1-DICHLOROETHEN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 U
5000 U2000 U
2000 U
2000 U
2000 U
2000 U
5000 U
5000 U
5000 U
2500 U
500 U
5000 U
3000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U10 U
10 U
10 U
1 U
1 U
1 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 U
3300 U
250 U
250 U
250 U
250 U
250 U
1000 U100 U
500 U
1000 U
500 U
5 U
10 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 U
5000 U
5000 U
5000 U
5000 U
5000 U
5000 U
2500 U
2500 U
1000 U
2500 U
1200 U
2000 U
3000 U
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 U
3300 U
2500 U
2500 U
2500 U
2500 U
2500 U
1000 U
1000 U
2000 , U
1000 '''•• U
5000 U
5000 U2000 U
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
1700 U
5000 U
5000 U
5000 U
5000 U
5000 U
500 U
500 U
5000 U
500 U
1000 U
5000 U100 U
NS-09
NS
10
18
250 U
10 U
4400 U
12000 U
14000 U
6 J
700 U
9
80 U
9 J
50 U
50 U
15 J
100 U
100 U
25 J
100 U
100 U
100 U
500 U
100 U
30
18 D
7.8
NS-1 0
NS
5 U
2 J
330 U
500 U
440 U
470 U
23 U
440 U
130 U
120 U
470 U
250 U
50 U
10 U
100 U
100 U
100 U
100 U
100 U
10 U
20 U
10 U
10 U
1 U
1 U
1 U
NS-1 1
NS
5 U
10 U
25 U
500 U
1 U
7 U
7 U
7 U
7 U
7 U
7 U
5 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
2 U
1 U
NS-1 5
NS
NR
10 U
67 U
50 U
18 U
35 U
7 U
18 U
7 U
7 U
12 U
10 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
10 U
1 U
NOTES:
Unit s in ug/l
ROD Performanc e Standard : 7 ug/L
NR - Not Reporte d
NS - Not Sampled
U - No t detected at indicate d concentratio n
D - Concentration fro m a secondar y dilutio n analysi s
J (Organics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greater tha n RO D Performanc e Standar d
Pag e 6 o f 1 4
Table 3-9
Historica l Analytica l Result s - VOC s
Trench Area Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , North Carolin a
1,2-DICHLOROPROPAN E
Quarter
1Q9 3
2Q93
3Q93
4Q9 3
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q96
2Q96
3Q96
4Q961Q97
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
iq02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
350
5000 U
250 J2000 U
2000 U
2000 U
2000 U
5000 U
5000 U
5000 U
2500 U
500 U
5000 U
3000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
JO U
10 U
10 U
1 U
1 U
1 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
3300 U250 U250 U
250 U
250 U
250 U
1000 U
100 U
88 J
7000 U
500 U
5 U
10 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
530
5000 U
5000 U
5000 U
5000 U5000 U
100 0 J
120 0 J
28003100
3600
2700
150 0 JD
2300 J
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
9400 D
12000
11000
12000
9100
1100 0
12000
1200 0
1300014000,
15000
13000
16000 D
6400
EX- 10
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
82000 D
81000 D
78000
68000
56000
60000
75000
4100 0 0
44000 D
54000
42000 D
22000
31000 D
1100 0
NS-09
NS
5 U
10 U
250 U10 U
3800 U
10000 U
12000 U
6 U
600 U
6 U
68 U
10 U
50 U
50 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
500 U
100 U
2
10 U
0.53 J
NS-1 0
NS
2 J
1 J
330 U500 U380 U
400 U
20 U
380 U
110 U
100 U
400 U
250 U
50 U
10 U
100 U
100 U
100 U
100 U
100 U
10 U20 U
10 U
10 U
1 U1
1 U
NS-1 1
NS
5 U
70 U
25 U
500 U
6 U
6 U
6 U
6 U
6 U
6 U
6 U
5 U
5 U
70 U
10 U
10 U
10 U
10 U
10 U
10 U10 U
10 U
10 U
1 U
2 U
1 U
NS-1 5
NS
NR
2 J
67 U
50 U
15 U
30 U
6 U
75 U
6 U
6 U
70 U
10 U
5 U
70 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U10 U
10 U
1.5
10 U
1 U
NOTES :
Units in ug/1
RO D Performanc e Standard : 6 ug/L
NR - No t Reporte d
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
D - Concentration from a secondary dilutio n analysi s
J (Organics) - Estimate d concentratio n is less than the reporting limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 7 of 1 4
Tabl e 3-9
Historica l Analytica l Result s - VOCs
Trench Area Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Ceda r Spring s Plan t Site
Salisbury , Nort h Carolin a
ETHYLBENZEN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
190
5000 U
120 J
2000 U
2000 U
2000 U
2000 U
5000 U
5000 U
5000 U
2500 U
500 U
5000 U
3000 U
EX-06
NS
NS
NS
NSNS
NS
NS
NS
NS
NS
NS
NS
NS
25 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 J
10 U
10 U
1 U
1 U
1 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 U
3300 U
250 U
250 U
250 U
250 U
25 0 U
100 0 U
100 U
81 J
100 0 U
500 U
2 J D
10 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
140
5000 U
5000 U
5000 U
5000 U
5000 U
5000 U
2500 U
2500 U
370 J
380 J
120 0 U
2000 U
3000 U
EX-09
NS
NS
NS
N S
NS
NS
NS
NS
NS
NS
NS
NS
NS
130 0
590 J
480 J
410 J
2500 U
2500 U
500 J
490 J
660 J
560 -, J
630 " J
5000 U
5000 U
2000 U
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
2400
2400
2400 J
2200 J
180 0 J
190 0 J
2500 J
190 0
2000
210 0 J
2200
170 0
3400 JD
160 0
NS-09
NS
32
98
250 U
6 J
6200 U
17000 U
20000 U
4 J
100 0 U
5 J
11 0 U
10
50 U
50 U
8 J
100 U
100 U
100 U
10 0 U
100 U
100 U
500 U
100 U
1.8
5 J D
8.2
NS-1 0
NS
4 J
4 J
330 U
500 U
620 U
670 U
33 U
620 U
180 U
170 U
670 U
250 U
50 U
10 U
100 U
100 U
100 U
100 U
100 U
10 U
20 U
10 U
2 J
1 U
1 U
1 U
NS-1 1
NS
95
14 0
300
500 U
10 U
91
40
120
76
98
57
62
81
100
92
140
20
5 J
22
54
15
22
29
6.5
8 D
2.2
NS-1 5
NS
NR
10 U
67 U
50 U
25 U
50 U
10 U
25 U
10 U
10 U
17 U
10 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
10 U
1 U
NOTES:
Unit s in ug/1
RO D Performanc e Standard : 3,50 0 ug/L
NR - Not Reported
NS - Not Sample dU - Not detected at indicate d concentratio n
D - Concentratio n fro m a secondar y dilutio n analysi s
J (Organics ) - Estimate d concentratio n is les s tha n the reportin g limi t
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Page8ofl 4
Table 3-9
Historical Analytica l Results - VOCs
Trench Are a Extractio n and Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Cedar Spring s Plant Site
Salisbury , Nort h Carolin a
METHYLEN E CHLORID E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q9 5
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
56 J
190 0 B J
130 J
2000 U
2000 U
2000 U
340 J
5000 U5000 U
5000 U
2500 U
500 U
510 0 B D
6000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25 U
4 B J
2 J
10 U
10 U
10 U
10 U
10 U10 U
10 U
10 U
1 U
1 U
2 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NSNS
NS
NS
720 U
120 0 B J
16 J
250 U
250 U
250 U
44 J
1000 U100 U
170 J
1000 U
500 U
4 JB D
20 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
40 J
5000 U
300 J
5000 U
5000 U
5000 U
5000 U
2500 U
420 J
270 J
2500 U
1200 U
160 0 JBD
6000 U
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
48 J
490 BJ
170 J
2500 U
2500 U
2500 U
2500 U
1000 U
220 J
550 , J
7000 '• U
500 U
510 0 BD
4000 U
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
94 J
880 B J
370 J
5000 U
5000 U
5000 U
5000 U
200 J
130 J
980 J
500 U
1000 U
3800 JBD
200 U
NS-09
NS
5 U
9 BJ
NR
NR
3/00 U
1400 0 B
13000 B
4 B J
130 0 B
5 U57 U
10 U
50 U
50 U
1 J
700 U
100 U
100 U
100 U
100 U
100 U
500 U
100 U
8.8 1
14 D
3.8
NS-1 0
NS
3 J
6 BJ
NR
NR
170 BJ
930 B
17 U
350 B
230 B
83 U
330 U
73 BJ
10 BJ
2 J
7 J
700 U
100 U
100 U
100 U
10 U
20 U
10 U
10 U
1 U
1 U
2 U
NS-1 1
NS
1 J
4 B J
NR
NR
5 U
8 B
5 U
2 B J
7 B
5 U
5 U
2 B J
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 JB D
2 U
NS-1 5
NS
NR
3 B J
NR
NR
72 U
24 B J
11 B
72 U
5 B
5 U
7 BJ
3 B J
2 J
2 J
1 J
70 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
8.9 1
8 JBD
2 U
NOTES:
Unit s in ug/l
RO D Performanc e Standard : 5 ug/L
NR - Not Reported
NS - Not Sampled
U - Not detected at indicate d concentratio n
D - Concentration from a secondary dilutio n analysis
1 - Commo n laborator y contaminan t
J (Organics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
B (Organics) - Compoun d detected in associated metho d blan k
Bol d fon t indicates detected concentratio n greater than ROD Performanc e Standar d
Itali c fon t indicates detection limi t greater tha n ROD Performanc e Standard
Pag e 9 o f 1 4
Table 3-9
Historica l Analytica l Result s - VOCs
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Company
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
TOLUEN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q95
2Q95
3Q95
4Q95
1Q96
2Q96
3Q964Q96
1Q97
2Q973Q97
4Q97
1Q98
2Q98
3Q98
4Q98
4Q99
4QO O
1Q02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16000 D
1900020000
24000
23000
22000
21000
21000
14000
13000
14000
24000 4
51000 D
26000
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
74
6765
42
37
82
43
40
75
48
31
1 U
1 U
1 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
3200
2200 J
1700
1600
1200
110 0
1100
820 J
56 J
6800
6600
50 0 U
12 0 D48
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NSNS
NS
NS
NS
68000 D
28000
2SOO O
3000 0
2400 025000
26000
24000
20000
22000 0
20000
3400 0
2600 0 D
17000
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
38000 D
2900 0
28000
28000
20000
23000
22000
21000 D
1SOO O
18000
18000
31000
65000 D30000
EX-10
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
14000 D
15000
15000
16000
1200012000
14000
9000
7600
10000
9000
5000
9500 D
2900
NS-09
NS
400 D
110 0 D
330
100
6200 U
17000 U
20000 U
47
340 J
130
410
180
170
69
200
10 0 U
80 J
150
11 0
30 J
76 J
500 U
29 J
53 4
11 0 D150
NS-10
NS
2 J
17
330 U
500 U
620 U
670 U
33 U
620 U
180 U
170 U
670 U
250 U
50 U
4 J
9 J
100 U
100 U
100 U
100 U
10 U
5 J
5 J
10
1 U
1
1 U
NS-11
NS
61
59
120
500 U
7 J
13
6 J
23
11
15
6 J
6
11
12
19
28
5 J
7 J
29
9 J
6 J
10
28
3.3
6 D
1.4
NS-15
NS
NR
23
18 J
50 U
13 J
17 J
10
10 i
8 J
5 J
9 J
11
15
2 J
6 J
5 J
4 J
10
8 J
3 J
7 J
10 U
2 J
2.6
13 D
0.77 J
NOTES:
Unit s in ug/1
RO D Performanc e Standard : 2,00 0 ug/L
NR - Not Reported
NS - Not Sample d
U - Not detected at indicate d concentratio nD - Concentration from a secondary dilutio n analysisE/4 - Estimate d concentratio n exceed s th e calibratio n rang e
J (Organics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
Bold fon t indicate s detected concentratio n greater than ROD Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 1 0 o f 1 4
Tabl e 3-9
Historica l Analytica l Result s - VOC s
Trenc h Are a Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Ceda r Spring s Plan t Site
Salisbury , Nort h Carolin a
1,1,2-TRICHLOROETHAN E
Quarter
1Q93
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q95
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
66 J
5000 U
2000 U
2000 U
2000 U
2000 U
5000 U
5000 U
5000 U
2500 U
500 U
5000 U
3000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
1 U
1 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
3300 U
250 U
250 U
250 U
250 U
1000 U
100 U
500 U
1000 U
500 U
5 U
10 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 J
5000 U
5000 U
5000 U
5000 U
5000 U
2500 U
2500 U
1000 U
2500 U
1200 U
2000 U3000 U
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
N S
NS
NS
NS
720 U
3300 U
2500 U
2500 U
2500 U
2500 U
1000 U
1000 U
2000 U
1000 , U
5000 • U
5000 U
2000 U
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
1700 U
5000 U
5000 U
5000 U
5000 U
500 U
500 U5000 U
79 J
700 U
5000 U
100 U
NS-09
NS
3 J
6 J
250 U
10 U
3100 U
8300 U
10000 U
5 U
500 U
5 U
57 U
10 U
50 U
50 U
100 U
100 U
100 U
100 U
100 U
100 U
500 U
100 U
7.7
70 U
1.9
NS-10
NS
10
12
330 U
500 U
310 U
330 U
17 U
310 U
89 U
83 U
330 U
250 U
50 U
6 J
20 J
700 U
100 U
100 U
2 i
20 U
2 )
10 U
1 U
1 U
1 U
NS-11
NS
5 U
70 U
25 U
500 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
70 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
2 U
1 U
NS-15
NS
NR
10 U
67 U
50 U
12 U
25 U
5 U
72 U
5 U
5 U
5 U
10 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
10 U
\ U
NOTES :
Units in ug/1
ROD Performanc e Standard: 5 ug/L
NR - Not Reporte d
NS - Not Sample dU - Not detected at indicate d concentratio n
J (Organics) - Estimated concentratio n is less than the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greater tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 1 1 o f 1 4
Table 3-9
Historica l Analytica l Result s - VOCs
Trench Area Extractio n and Monitorin g Well s
Nationa l Starch and Chemical Company
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
TRICHLOROETHEN E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-O S
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
5000 U
2000 U
2000 U
2000 U
2000 U
2000 U
5000 U
5000 U
5000 U
2500 U
500 U
5000 U
3000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
2 J
1 U
1 U
1 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 U
3300 U
250 U250 U
250 U
250 U
250 U
1000 U
100 U
500 U
1000 U
500 U
5 U10 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
5000 U
5000 U5000 U
5000 U
5000 U
5000 U
2500 U2500 U1000 U
2500 U
1200 U
2000 U3000 U
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 U
3300 U
2500 U2500 U
2500 U
2500 U
2500 U
1000 U
1000 U
2000 : U
1000 U
5000 U
5000 U2000 U
EX-1 0
NS
NS
NS
N S
NS
NS
NS
NS
NS
NS
NS
NS
NS
720 U
1700 U
5000 U5000 U
5000 U
5000 U
5000 U
500 U
500 U
5000 U
500 U
1000 U
5000 U100 U
NS-09
NS
5 U
3 J
250 U
10 U
3100 U
8300 U
10000 U
5 U
500 U
5 U
57 U
10 U
50 U
50 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
500 U
17 J
5.3
7 JD
4.7
NS-1 0
NS
1 J
10 U
330 U
500 U
310 U
330 U
17 U
310 U
89 U
83 U
330 U
250 U
50 U
10 U
100 U100 U
100 U
100 U
100 U
10 U
20 U
10 U
JO U
1 U
1 U
1 U
NS-1 1
NS
5 U10 U
25 U
500 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
10 U10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
2 U
1 U
MS-1 5
NS
NR
10 U
67 U
50 U
12 U
25 U
5 U
12 U
5 U
5 U
8 U
10 U
5 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
10 U
1 U
NOTES :
Unit s in ug/1
RO D Performanc e Standard : 5 ug/L
NR - No t Reporte d
NS - Not Sampled
U - Not detected at indicate d concentratio n
D - Concentratio n fro m a secondar y dilutio n analysis
J (Organics ) - Estimate d concentratio n is less tha n the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Italic fon t indicates detection limi t greater than RO D Performanc e Standar d
Pag e 1 2 o f 1 4
Table 3-9
Historica l Analytica l Result s - VOC s
Trenc h Area Extractio n and Monitorin g Wells
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
VINY L CHLORID E
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
990
5000 U
2000 U
970 J
120 0 J
580 J
820 J
5000 U
5000 U
5000 U
500 J
500 U
5000 U6000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
50 U
JO U
4 J4 J
3 J
3 J
10 U
10 U
2 J
2 J
10 U
1 U
1 U
2 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
250 U
3300 U
250 U
53 J
25 0 U
250 U
250 U
1000 U
100 U
270 J
220 J
500 U
5 U
20 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
250 U
5000 U
5000 U5000 U
5000 U
5000 U
5000 U
2500 U
2500 U
1000 U
2500 U
2500 U
2000 U
6000 U
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
250 U
3300 U
2500 U
2500 U
2500 U
2500 U
2500 U
1000 U
1000 U
2000 , U1000 ''•• u
10000 U
5000 U
4000 U
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
220 J
/70 0 U
5000 U
5000 U5000 U
5000 U
5000 U
250 J
21 0 J
5000 U
200 J
1000 U
5000 U
140 J
NS-09
NS
10 U
480 DJ
75 J
48
/20 0 U
3300 U
4000 U
46
200 U
81
160
62
89 J
50 U
110
20 J
49 J
84 J
100 U
53 J
17 J
500 U
25 J
140 4
140 O
42 J
NS-1 0
NS
8 J
10 U
330 U
500 U
120 U
130 U
7 U
120 U
36 U
33 U
130 U
500 U
100 U
10 U
100 U
100 U
100 U
100 U
100 U
10 U
20 U
10 U
10 U
1.3
1 U
2 U
NS-1 1
NS
10 U
10 U
25 U
500 U
2 U
2 U
2 U
2 U
2 U
2 U
2 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
1 U
2 U
2 U
NS-1 5
NS
NR
18
67 U
50 U
5 U
10 U
2 U
6
4
4
5
20 U
10 U
10 U
10 U
3 J
2 J
2 J
10 U
10 U
10 U
10 U
10 U
1.2
10 U
2 U
NOTES :
Unit s in ug/I
RO D Performanc e Standard : 2 ug/L
NR - No t Reporte d
NS - Not Sampled
U - Not detected at indicate d concentratio n
D - Concentration from a secondary dilutio n analysis
E/4 - Estimate d concentratio n exceed s th e calibratio n rang e
J (Organics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
Bold fon t indicate s detecte d concentratio n greate r tha n ROD Performanc e Standar d
Italic fon t indicates detection limit greater than ROD Performance Standard
Page 1 3 O f 14
Table 3-9
Historica l Analytica l Result s - VOCs
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Salisbury , Nort h Carolin a
XYLENE
Quarter
1Q93
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q95
2Q95
3Q954Q95
1Q96
2Q96
3Q96
4Q96
1Q97
2Q97
3Q97
4Q97
1Q9 8
2Q983Q98
4Q98
4Q99
4QO O
1Q0 2
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
470
5000 U
250 J
2000 U
2000 U
390 J
340 J
5000 U
5000 U5000 U
2500 U1500 U
5000 U
9000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NSNS
NS
25 U
10 U
0.6 J
10 U
10 U
10 U
10 U
10 U
10 U2 J
10 U
3 U
1 U
3 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NSNS
NS
29 J
3300 U
18 J
250 U
250 U
250 U
250 U
7000 U
10 0 U150 J
16 0 J
/500 U
6 D
30 U
EX -08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NSNS
NS
550
5000 U
5000 U
5000 U5000 U
5000 U
5000 U
680 J
110 0 J1400
160 0 J
3700 U1800 D
900 0 U
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NSNS
NS
3000
2300 J
1800 J
1300 J
1000 J
1100 J
1800 J
1800
23002000
2200 ..
75000 • U5000 JD
2200 J
EX-1 0
NS
NS
NS
NS
NSNSNS
NS
NS
NS
NS
NS
NS
7700 D
7800
7300
6800
5800
6300
8300
6200
62006800
7900
5800
12000 D
5900
NS-0 9
NS
69
120 D J
250 U
13
6200 U
17000 U
20000 U
4 J
1000 U
15110 U
23
12 J
6 J
21 J
100 U
100 U
100 U
100 U
10 0 U
22 J
500 U
100 U
8
20 D
25
NS-10
NS
10
10
330 U
500 U
620 U
670 U
33 U
<J2 0 U
180 U
170 U670 U
250 U
50 U
10 U
100 U
100 U
100 U
100 U
100 U
2 J
4 J
10 U
5 J
3 U
1 U
3 U
NS-1 1
NS
150
220
560
500 U
100110
50
120
44
6622
21
46
50
140
180
35
4 3
42
110
6447
53
23.4
35 D
9.1
NS-15
NS
NR
1 J
67 U
50 U
25 U
50 U
10 U
25 U
10 U
10 U
17 U
10 U
5 U
10 U
1 J
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
3 U
10 U
3 U
NOTES :
Unit s in ug/1
RO D Performanc e Standard : 35 0 ug/L
N R - No t Reporte d
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
D - Concentratio n fro m a secondar y dilutio n analysi s
J (Organics) - Estimated concentration is less tha n the reporting limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 1 4 of 1 4
Tabl e 3-10
Historica l Analytica l Result s - SVOCs
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
BIS(2-CHLOROETHYL)ETHE R
Quarter
1Q9 3
2Q93
3Q93
4Q931Q94
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
2500 U
5000 U
170 J
530 U
110 V
500 U
55 J
53 U
110 U
110 U
120 J
200 U260 U600 U
EX-06
NS
NS
NS
NSNS
NS
NS
NS
NS
NS
NS
NS
NSyo o u
4 J
1610 U
10 U
10 U
10 U
10 U
11 U
10 U
10 U
10 U
51 U
10 U
EX-07
NS
NS
NS
NSNS
NS
NS
NS
NS
NS
NS
NS
NS
200 U
100 U100 U
100 U
100 U
110 U
18 J
14 J
// U
990 D
100 U
10 U
51 -U10 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
320 J
5000 U
2500 U
210
390
620
810
110 0
190 0
140 0
2900
200 U
51 U1800
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
1000 0
NR
6600
7200
3800 D
7500
7400 D
10000 D
710 0 D
6200 D18000 D
500 U
2600 U
2900
EX-10
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
3500 0 D
4700029000 D
29000 D
1400 0
30000 D
16000 D
68000 D
23000 D
15000 D
14000 D
1100 0" 5io" ."E D
4800
NS-09
NS
10 U
56 U
530 U
8 J
20 U6 U
11 U
53 U
27 U
28 U
50 U
10 U
50 U
50 U20 U
10 U
20 U
20 U
2 J
11 U
3 J
2 J
2 J
10 U
51 U10 U
NS-1 0
NS
11 U
10 U
50 U220 U
1100 U
110 U
22 U
520 U
250 U
310 U
260 U
500 U
200 U
200 U100 U
10 U
100 U
10 U
11 U
10 U
10 U
JO U
10 U
10 U
NAJO U
NS-1 1
NS
// U
10 U
10 U10 U
11 U
5 U
5 U
5 U
5 U
6 U
5 U
10 U
50 U
JO U10 U
10 U
10 U
10 U
11 U
10 U
U U
10 U
2 J
10 U
51 U10 U
NS-15
NS
11 U
10 U
42 U
10 U
22 U
21 U
10 U
U U
6 U
5 U
5 U
10 U
50 U
20 U10 U
10 U
10 U
10 U
10 U
11 U
10 U
10 U
11 U
10 U
52 U10 U
NOTES :
Unit s in ug/1
ROD Performanc e Standard: 5 ug/L
NR - Not Reporte d
NS - Not Sample d
U - Not detected at indicated concentration
E - Estimate d concentratio n exceed s the calibratio n rang e
D - Concentratio n fro m a secondar y dilutio n analysi s
J (Organics ) - Estimate d concentratio n is less tha n th e reportin g limi t
Bold fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Italic font indicates detection limit greater than ROD Performanc e Standard
Shading indicates "E" qualified concentration for which a diluted run concentration is'unavailable
Pag e 1 of 2
Table 3-10
Historica l Analytica l Result s - SVOC s
Trenc h Are a Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
4-NITROPHENO L
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q94
2Q94
3Q94
4Q94
1Q95
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q97
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QOO
1Q02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6200 U
12000 U6200 U
1300 U
260 U
1200 U
260 U
130 U
280 U
270 U
2800 U
1000 U
53 U
3000 U
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
250 U
25 U
25 U
25 U
25 U
26 U
26 U
26 U
28 U
26 U
26 U
50 U
10 U
50 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
500 U
250 U
250 U
260 U
25 0 U
280 U
26 0 U
26 0 U
26 U
260 U
26 0 U
50 U
10 U
50 U
EX-0 8
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6200 U
12000 U6200 U
25 U
250 U
1400 U
260 U
260 U
260 U
270 U
2600 U
1000 U
'" "410 "•"''"• E
"3000 "~~U"
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6200 U
12000 U2500 U
520 U
100 U
530 U
260 U
260 U
270 U
270 X U
2600 U
2500 U'";• 760 6 "'••' ED ;" JOO O """""" "U "
EX-10
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
2500 U
25000 U
7500 U
260 U
5300 U
WOO U
260 U270 U
260 U
26 0 U
7300 U
1000 U
8800 U1000 U
NS-09
NS
50 U
140 U
/300 U
25 U
50 U
28 U
56 U
260 U
140 U
140 U
250 U
25 U
12 0 U
120 U
3 J
25 U
50 U
50 U
26 U
27 U
26 U
26 U
26 U
50 U
10 U50 U
NS-10
NS
53 U
25 U
12 0 U
540 U
2600 U
530 U
110 U
2600 U
1200 U
1600 U
1300 U
1200 U
500 U
500 U
250 U
26 U
250 U
26 U
27 U
26 U
26 U
26 U
26 U
50 U
NA
50 U
NS-11
NS
56 U
26 U
26 U
26 U
27 U
27 U
26 U
26 U
27 U
28 U
25 U
25 U
12 0 U
25 U
25 U
26 U
25 U
26 U
26 U
26 U
27 U
26 U
26 U
50 U
10 U50 U
NS-1 5
NS
54 U
25 U
110 U
26 U
54 U
11 0 U
51 U
54 U
28 U
27 U
26 U
25 U
12 0 U
50 U
25 U
26 U
25 U
26 U
26 U
26 U
26 U
25 U
27 U
50 U
10 U
50 U
NOTES :
Unit s in ug/1
ROD Performanc e Standard : 350 ug/L
NA - Not Analyze d
NR - Not Reported
NS - Not Sample d
U - No t detecte d at indicate d concentratio n
E - Estimate d concentratio n exceed s th e calibratio n rang e
D - Concentratio n fro m a secondar y dilutio n analysi s
J (Organics ) - Estimate d concentratio n is less than the reportin g limi t
Italic fon t indicate s detection limi t greate r than ROD Performanc e Standar d
Shading indicate s "E" qualifie d concentratio n fo r whic h a dilute d run concentratio n is unavailabl e
Pag e 2 of 2
Table 3-1 1
Historica l Analytica l Result s - Metal s
Trenc h Are a Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
ARSENI C
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-O S
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11
2.2 U
4.4 U
7 U
10.6
7 U
6 U
6 U
1.3 U
4.5 J
9.2 1
7.7
3.6 B
7.1 B
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
N S
NS
NS
NS
NS
1.1 U
1.1 U
1.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
1.3 U
5 U
5 U
1.5 U10 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
1.1 U
1.1 U
1.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
2.3 J
5.3 7
5 U
1.5 U10 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
22 U
2.2 U2.2 U
7 U
7 U
7 U
9 B6 U
1.3 U
7.4
14.8
11
1.5 U
6.6 B
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
// U
2.2 U
4.4 U
9.8 B
7 U
7 U
8.5 B
6 U
1.3 U
5 '••-.
10.5
8.3
3 B
3 B
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
// U
2.2 U
2.2 U
7 U
7 U
7 U
9.5 B
6 U
1.3 U
4.1 J
9.2
5.8
1.5 B3.1 B
NS-09
NS
2 U
2.2 B
8.2 B
2.9 U
2.6 U
2.1 U
2.1 U
1.5 B
2.7 U
3.2 B
1.5 U
1.1 U
1.1 U
1.1 U1.1 U
7 U
7 U7.4 B
6 U
6 U
1.3 U
1.3 U
5 U
5 U
1.5 U2.5 B
NS-1 0
NS
2 U
2 U
2.4 U
2.9 U
2.6 U
2.1 U
2.9 B
1.7 B
2.7 U
2.2 B
.5 U
.1 U
.1 U
.1 U.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
1.3 U
5 U
5 U
1.6 B
10 U
NS-1 1
NS
2 U
2 U
2.4 U
2.9 U
2.6 U
2.1 U
2.1 U
2 B
2.7 U
2.4 B
1.5 U
1.1 U
1.1 U
1.1 U1.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
1.3 U
5 U
5 U
1.5 U
2.7 B
NS-I5
NS
2 U
2 U
4.8 U
5.8 U
5.2 U
2.1 U
3.7 B
0.8 U
2.7 U
1.9 U
1.5 U
1.1 U
1.1 U
1.1 U1.1 U
7 U
7 U
7 U
6 U
6 U
1.3 U
1.3 U
5 U
5 U
1.5 U10 U
NOTES:
Unit s in ug/1
ROD Performance Standard: 10 ug/L
NS - Not Sampled
U - No t detected at indicate d concentratio n
J (Inorganics) - Compound detected in associated method blankB (Inorganics ) - Estimate d concentratio n i s les s tha n th e reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Italic fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Page 1 of 9
Table 3-I I
Historica l Analytica l Result s - Metal s
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolin a
BARIU M
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
124 B
159 B
157 B
158 B
138 B
179 B
217
244
540 J
186
281
500
239
228
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
313
106 B
107 B
80.9 B
87.6 B
98.2 B
70.8 B
81.6 B
90.3 J
63.2
14 2
40
20 B
24.6 B
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
425
305
319
335
31 5
280
260
290
248
12 9
204
230
171 B
29.5 B
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25.6 B
28.6 B
29.1 B
21 B
22.9 B
26 B
25.5 B
21.3 B
80 U
15.9
22.1 J
21
17.5 B
21.5 B
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
12.9 B
17.9 B
17.1 B
10.9 B
11.8 B
15.7 B
15.5 B
11 B
80 . U
10.1 "'•
20 U
127 B12.7 B
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19.3 B
18.6 B
21.4 B
29.2 B
18 B
19.1 B
17.8 B
15.7 B
80 U
11.8
20 U
1614.2 B14.3 B
NS-09
NS
148 0
3160
102 0
412
264
227
428
573
2030
120 0
134 0
993
752
504
785
127 0
329
523
507
605
270
186
305
420309346
NS-1 0
NS
297
155 B
155 B
276
144 B
13 1 B
96.3 B
124 B
193 B
176 B
164 B
156 B
27 7
18 1 B
293
305
205
236
280
234
259
132
156
110
72.7 B98.5 B
NS-1 1
NS
115 B
190 B
85.9 B
143 B
134 B
127 B
151 B
169 B
140 B
237
98.8 B
156 B
13 6 B
144 B
301
12 4 B
19 9 B
576
178 B
178 B
180 J
11 3
270
12 0
80.373 B
NS-1 5
NS
448
445
444
416
418
461
370
364
428
387
452
432
533
29 6
405
398
342
506
467
365
469
12 5
368
420
364305
NOTES:
Unit s in ug/1
ROD Performance Standard: 1,000 ug/L
NS - Not Sampled
U - Not detected at indicate d concentratio nJ (Inorganics ) - Compoun d detecte d in associated metho d blan kB (Inorganics ) - Estimate d concentratio n i s les s tha n th e reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Pag e 2 of 9
Table 3-1 1
Historica l Analytica l Result s - Metal s
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Springs Plant Site
Salisbury , Nort h Carolin a
BERYLLIU M
Quarter
1Q9 3
2Q93
3Q93
4Q93
IQ94
2Q9 4
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
1 U
1 U
40 U
\ U
10 U
1 U
0.2 B5 U
EX-06
NS
NS
NS
NSNS
NS
NS
NS
NS
NS
NS
NS
NS
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
U
U
U
U
U
U
0.1 U5 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
0.3 U
0.3 U
0.3 U
2 U
2 U
2 U
1 U
1 U
1 U
1 U
10 U
1 U
0.1 U0.6 3 B J
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
34
22.7
20.6
18.5
15.4
14
13.414.1
40 U
7.7
16.8 J
14
7.2
11.7 J
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
26.1
27.5
25.6
22
17.1
19.8
18.4
18.9
46.8 J
9.7 \
22 J
12
16.711 J
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25.1
21.3
18.8
14.9
12.1
14.3
13.814.940 U
815.9 J
9.7
10.612.1 J
NS-09
NS
1 U
3.4 B
0.7 5 B
0.4 U
0.2 1 B
0.3 U
0.3 U
0.3 U
0.2 2 B
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U
0.4 B
2 U
2 U
2 U
1 U
1 U
1 U
1 U
1 U
1 U
O.I U5 U
NS-1 0
NS
1 U
1.8 B
0.4 U
0.4 U
0.2 U
0.3 U
0.3 U
0.3 U
0.2 U
0.3 U
0.3 U0.4 B
0.3 U
0.3 U0.3 U
2 U
2 U
2 U
U
U
U
U
U
U
0.1 U5 U
NS-1 1
NS
1 U
1.9 B
0.4 U
0.4 U
0.2 U
0.3 U
0.3 U
0.3 U
0.2 4 B
0.5 5 B
0.3 U
0.3 U
0.3 U
0.3 U
0.6 B
2 U
2 U
2 U
1 U
1 U
1 U
1 U
I.I J
1 U
0.1 U5 U
NS-1 5
NS
1 U
1.2 B
0.4 U
0.4 U
0.3 2 B
0.3 U
0.3 U
0.3 U
0.2 U0.3 U
0.3 U
0.3 U
0.3 U
0.3 U0.3 U
2 U
2 U
2 U
U
U
U
U
U
1 U
0.1 U5 U
NOTES:
Unit s in ug/1
ROD Performanc e Standard : 17.5 ug/L
NS - Not Sample d
U - No t detecte d at indicate d concentratio n
J (Inorganics ) - Compoun d detected in associated method blan k
B (Inorganics ) - Estimate d concentratio n is less tha n th e reponin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Pag e 3 of9
Tabl e 3-1 1
Historica l Analytica l Result s - Metal s
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury, Nort h Carolin a
CADMIU M
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O1Q02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
17.5
10.6
6.8
6.9
12.8
15.4
21
10.1
8.9
28.1
31.7
9.5
6.1
16.5 J E
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
5 U
4.8 U
4.8 U
0.5 U
3 U
18
4 U
4 U
0.2 6 U
0.2 6 U
0.5 U
1 U
0.5 U5 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
5 U
4.8 U
4.8 U
0.7 4 B
4.2 B
4.7 B
4 U
4 U
0.2 6 U
0.2 6 U
7.6 3
1 U
0.5 U5 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
44
18.7
15.5
13.4
3 U
7.4
4.1 B
12.7
7.5
3.9
11.5
7.1
2 B6.3 J
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
12.7
7.7
8.4
6.1
3 U
4.6
4 U
5.4
1-9
1.5 '•-.
3.6 1
1.7
2.6 B2 BJ
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
12.6
6.6
4.8 U
4.3 B
3 U
3 U
4.3 B
6.3
2.3
1.5
3.7 2
1.3
3.8 B1.1 B J
NS-09
NS
5 U
5 U
2.3 U
2.1 U
1.3 U
4.9 B
1.6 U
2.1 U
1.4 U
1.8 B
1.9 U
4.8 U
5 U
5 U
4.8 U
1.5 B
3 U
3 U
4 U
4 U
0.2 6 U
0.2 6 U
0.5 U
1 U
0.5 U5 U
NS-1 0
NS
5 U
5 U
2.3 U
2.1 U
1.3 U
1.6 U
1.6 U
2.1 U
1.4 U
1.2 U
1.9 U
4.8 U
5 U
5 U
4.8 U
0.5 U
3 U
3 U
18
4 U
0.2 6 U
0.2 6 U
0.5 U
1 U
0.5 U5 U
NS-1 1
NS
5 U
5 U
2.3 U
2.1 U
.3 U
.6 U
.6 U
2.1 U.4 U
.2 U
.9 U
4.8 U
5 U
5 U
4.8 U
0.5 U
3 U
3 U
4 U
4 U
0.2 6 U
0.2 6 U
0.5 U
1 U
0.5 U5 U
NS-1 5
NS
5 U
5 U
2.3 U
2.1 U
1.3 U
1.6 U
1.6 U
2.1 U
1.4 U
1.2 U
1.9 U
4.8 U
5 U
5 U
4.8 U
0.5 U
3 U
3 U
4 U
4 U
0.2 6 U
0.2 6 U
0.5 U
1 U
0.5 U5 U
NOTES:
Unit s i n ug/1
ROD Performance Standard: 10 ug/L
NS - Not Sample d
U - Not detected at indicate d concentratio n
E - Estimated concentratio n exceeds the calibratio n rangeB (Inorganics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
J (Inorganics ) - Compoun d detecte d in associate d metho d blan k
Bold fon t indicate s detecte d concentratio n greate r tha n ROD Performanc e Standar d
Pag e 4 of9
Table 3-11
Historica l Analytica l Result s - Metal s
Trench Area Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Springs Plant Site
Salisbury , Nort h Carolin a
CHROMIU M
Quarter
IQ93
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q96
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-OS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
18.1
25.1
26.2
5 U
5 U
5 U11
4 U
160 U
11.1
85.9 J
2 U
14.115.2
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
5 U
4.9 U
4.9 U
5 U
5 U
5 U
4 U
4 U
4 U
4 U
12.1
2 U
3.5 B
13.6
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
7.5 B
14.8
16.9
5 U
5 U
5.8 B
4 U
4 U
15.4
19.4
231
2 U
2.9 B
5 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
80.2
84.7
79.8
19.8
12.6
9.6 B
9.9 B
4 U
160 U
11.5
101
2 U
31.4
35.7
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
48
63.9
63.5
27.4
19.5
19.2
17.6
14.4
160 U
16.4 ''--.
85.S J
4.6
34
21.7
EX- 10
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
44.4
56.1
46.5
16.3
10.3
11.8
11.2
4 U
160 U
24
82.5 J
2 U
28.3
32.8
NS-09
NS
50.1
304
127
20.6
11.9
24.3
7.1 B
8.8 B
127
42
31.1
4.9 U
5 U
20.3
97.2
375
21.7
62.7
69.6
175
8.4 J
12.3
74.5
25
7.2 B
5.9
NS-10
NS
14.2
11.7
16.3
36.9
6.1 B
3.1 B
8.8 B
9.1 B
4 B
6.7 B
2.4 U
4.9 U
5 U
5 U
4.9 U
5 U
5 U
5 U
4 U
5.1 B
5.5 J
4 U
10
2 U
2.2 B
2.1 B
NS-11
NS
10 U
35.6
17.4
4.2 B
2.9 U
2.4 U
4.1 B
4.3 U
2 U
5.2 B
2.4 U
7 B
5 U
5 U
34.2
5 U
8.2 B
57.2
4 U
4 U
4 U
4 U
41.6
5
0.9 U
1.4 B
NS-15
NS
11.7
10.6
3.6 B
3.6 B
2.9 U
4.3 B
4.3 B
4.3 U
2 U
3.1 U
2.4 U
9.4 B
5 U
5 U
4.9 U
5 U
5 U
5 U
4 U
4 U
5.2 J
4 U
9.6 J
2 U
3.2 B
4.5 B
NOTES :
Unit s in ug/1
ROD Performanc e Standard: 50 ug/L
NS - Not SampledU - Not detected at indicate d concentratio n
J (Inorganics ) - Compoun d detected in associate d metho d blan k
B (Inorganics ) - Estimate d concentratio n is less tha n the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Pag e 5 of9
Table 3-1 1
Historica l Analytica l Result s - Metal s
Trenc h Are a Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Company
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
MANGANES E
Quarte r
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QOO1Q02
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
200000
170000
144000
138000
125000
11800 0
98900
161000
255000
84700
134000
62000
56300
52600
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
7680
325 0
362 0
2520
2850
3300
218 0
281 0
317 0
2230
310 0
850
402
256
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
73700
64200
60400
68000
43600
41300
40200
43400
26200
48000
8110 0
36000
931 0
117 0
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
51600 0
393000
332000
352000
232000
23100 0
203000
27100 0
31100 0
134000
21200 0
21000 0
10000 0
196000
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
98800
16000 0
170000
192000
11400 0
14300 0
11300 0
138000
178000
69400 ,
12200 0
11000 0
129000
108000
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19800 0
15900 0
13800 0
126000
91900
13200 0
10300 0
14300 0
184000
79100
13800 0
12000 0
11400 0
10100 0
NS-0 9
NS
5130 0
6050 0
2810 0
1530 0
1100 0
6760
14300
1880 0
51800
33600
34600
25700
20500
1380 0
18200
31600
10300
22400
19600
8280
1240 0
340 0
834 0
1200 0
1500 0
1280 0
NS-1 0
NS
1430 0
7760
354 0
7930
9650
9200
2760
14400
8960
9320
8880
5860
1005 0
229 0
4850
4260
215 0
2730
2760
183 0
2670
145 0
141 0
2400
44 1
186 0
NS-1 1
NS
63.1
11 8
55.6
71.5
47
67
83.2
12 4
62.6
248
37.8
32
48.2
44
84 1
67.2
889
366
13 6
13 2
13 3
42.7
33 5
19 0
90.9117
NS-1 5
NS
1520 0
1500 0
1510 0
17600
17800
18600
14900
14300
16800
1340 0
1620 0
14200
16400
8670
1380 0
1430 0
1180 0
16700
1550 0
1300 0
15600
398 0
1280 0
1400 0
1310 0
10600
NOTES:
Unit s in ug/1
ROD Performanc e Standard: 7,700 ug/L
NS - Not Sampled
Bold fon t indicates detected concentration greater than ROD Performanc e Standard
Pag e 6 of 9
Tabl e 3-1 1
Historica l Analytica l Results - Metal s
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starch and Chemica l Company
Ceda r Spring s Plan t Site
Salisbury , Nort h Carolin a
NICKE L
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
IQ98
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
678
601
654
732
587
622
566591
960 J
503
698
640
154 0
164 0
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19.7 B
15.3 U
15.3 U
20 U
20 U
20 U
16 U16 U
14 U
14 U
14 U
5 U
1.5 B2.2 B
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11 7
11 0
91.1
69.7
61.3
35.8 B
22.9 B
16 U14 U
213
690
53
1.9 B
13.8 B
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
199 0
144 0
135 0
127 0
114 0
112 0
989
102 0
133 0 J
567
110 0
800
575
758
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
645
798
906
843
653
706
657
680
940 . J
329
771
430
599
407
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
698
549
505
444
365
451
410
484
560 U
271
501
320
370
292
NS-09
NS
23.9 B
102
54
10.4 U
13.8 B
19.2 B
10.5 B
10.3 U
43.6
9.4 B
20.1 B
15.3 U
15 U
15 U
40.9
223
20 U
34.8 B
63.2
81.9
23.3 J
14 U
17.9 J
12
4 B
6.6 B
NS-1 0
NS
45.2
25.1 B
33.9 B
57.5
30.2 B
27.5 B
25.6 B
33.7 B
20.1 B
20.6 B
26.9 B
15.3 U
27.6 B
22.9 B
35.4 B
35.6 B
23.2 B
21 B
30.5 B
23.6 B
14 U
14 U
14 U
5.7
5.7 B
15.1 B
NS-1 1
NS
20 U
28.2 B
35.1 B
10.4 U
6.4 B
6.9 U
10.3 B
16.2 B
5.5 U
12 B
8.8 U
15.3 U
15 U
15 U
40.7
20 U
21.9 B
64.3
16.5 B
16 U14 U
14 U
42.9
22
1.6 B
40 U
NS-1 5
NS
20 U
20 U
10.3 B
10.4 U
6.2 U
6.9 U
7 B
10.3 U
5.5 U
7.2 U
8.8 U
15.3 U
15 U
15 U
15.3 U
20 U
20 U
20 U
16 U
16 U14 U
14 U
14 U
5 U
1 U2 B
NOTES:
Unit s in ug/1
ROD Performance Standard: 350 ug/L
NS - Not Sampled
U - Not detected at indicated concentratio n
J (Inorganics ) - Compound detected in associated method blan k
B (Inorganics ) - Estimate d concentration is less tha n the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Pag e 7 of 9
Table 3-1 1
Historica l Analytica l Result s - Metal s
Trenc h Are a Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Springs Plan t Site
Salisbury , Nort h Carolin a
SELENIU M
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q95
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q9 8
4Q98
4Q9 9
4QO O
1Q0 2
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
8 U
16 U
5.2 U
86.1
773
68.1
66.164.6
66.9
36.2
50.2
26
30.247.6
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NSNS
NSNS
0.8 U
0.8 U
1.3 U
5 U
5 U
5 U
5 U5 U4.3 U
4.3 U
5 U
5 U
2.3 U
5 U
EX-07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
1.6 U1.6 U
1.3 U
31.7
24.7
24.7
19.5
20.6
8.2
18.2
28
6.5
2.3 U
5 U
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NSNS
NS
NS
8 U
1.6 U5.2 U
171
59.9
58.9
118
104
78.7
47.3
61.6
67
49.1
72.3
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
8 U
1.6 U
5.2 U
88.3
19.7
23.5
61.1
61.6
43
26.4
39.4
38
47
42.5
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
8 U
4 U
2.6 U
67.9
25.8
32.8
63.7
58.2
46
27.3
39.9
34
42.2
33
NS-09
NS
10 U
4 U
6.9 U
1.7 U
2.6 U
3.1 U
3.1 U
0.9 U
2.7 U
2 B
1 U
1.6 U
0.8 U
0.8 U
0.8 U
21.9
6.8
18.8
12.6
5 U
4.3 U
4.3 U
5 U
5 U
2.8 B
5.2
NS-1 0
NS
2 U
2 U
2.3 U
1.7 U
2.6 U
3.1 U
3.1 U
0.9 U
2.7 U
1.7 U
1 U
1.6 U
0.8 U
0.8 U
0.8 U
5 U
5 U
6.8
5 U
5 U
4.3 U
4.3 U
5 U
5 U
2.3 U
5 U
NS-1 1
NS
2 U
2 U
2.3 U
1.7 U
2.6 U
3.1 U
3.1 U
0.9 U
2.7 U
3.6 B
1 U
1.6 U
0.8 U
0.8 U
0.8 U
5.2
5 U
5 U
5 U
5 U
4.3 U
4.3 U
5 U
5 U
2.3 U
5 U
NS-1 5
NS
2 U
2 U
4.6 U
3.4 U
5.2 U
3.1 U
3.1 U
0.9 U
2.7 U
1.7 U
1 U1.6 U
0.8 U
0.8 U0.8 U
6.6
5 U
9.1
11.4
9
4.8 J
4.3 U
5 U
5 U
3 B
5 U
NOTES:
Unit s in ug/1
ROD Performanc e Standard : 10 ug/L
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
J (Inorganics ) - Compound detected in associated method blan k
B (Inorganics ) - Estimate d concentratio n i s les s tha n th e reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greater than ROD Performanc e Standard
Pag e 8 of 9
Tabl e 3-1 1
Historica l Analytica l Result s - Metal s
Trenc h Are a Extractio n an d Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolin a
ZINC
Quarter
1Q9 3
2Q93
3Q93
4Q93
1Q9 4
2Q94
3Q94
4Q94
1Q9 5
2Q9 5
3Q95
4Q95
1Q9 6
2Q96
3Q96
4Q96
1Q9 7
2Q97
3Q97
4Q97
1Q9 8
2Q98
3Q98
4Q98
4Q99
4QO O
1Q0 2
EX-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
363234
220
221
219
188
135126
20 0 U
883
132 0
350
186
365
EX-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
10.2 B
3.7 B
2.4 U
25.1
25.4
24.7
15 U15 U
5 U
5 U
9.3 J
10 U
8.6 U
17.5 B
EX-07
NS
NS
NS
NS
NS
N S -
NS
NS
NS
NS
NS
NS
NS
43.2
34.3
20.1
35.3
11 3
11 9
15 U15 U6.7 J
27.5
306
12
8.6 U
5.7 B
EX-08
NS
NS
NS
NS
NS
NS
NS
NS
NSNSNS
NSNS
320 0
182 0
169 0
186 0
151 0
140 0
125 01320
154 0
686
132 0
120 0
5981000
EX-09
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
2880
2750
2850
2900
2060
2230
194 0
I960
2450
936
180 0
130 0
160 0
983
EX-1 0
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
328 0
232 02120
201 0
136 0
137 0
123 01540
195 0
924
163 0
100 0
115 0
789
NS-09
NS
49.2
156
75.6
11.4 B
8.7 B
217
35.6
31
14 1
46.6
13.8 B
10.8 B
37.8
16.3 B
84.2
11 1
10.9 B
47.9
10 7
153
47.1
26
97.5
25
8.6 U
5.8 B
NS-1 0
NS
47.4
54
43.2
85.2
20.1
54.1
33.1
44.9
24.8
16.6 B
24.5
28.6
24
25.4
41.1
50.6
37.2
54
4991.132.2
18.6 J
45.5
14
29.5
9.3 B
NS-1 1
NS
32.5
37.4
15 B
7.2 B
3.1 B
12.8 B
27.8
38.7
13.2 B
41.3
5.2 U
8.2 B
9.6 B
3.9 B
65
11.9 B
22.4
127
31.2
29.8
11.3 J
5.2 J
71.7
84
8.6 U
20 U
NS-1 5
NS
14.5 B
12.6 B
1.8 U
1.7 U
0.9 U
3.8 U
3.8 U
3.5 U
5.8 U
2.6 U
5.2 U
3.6 B
6.4 B
2.5 B
30.6
11.7 B
5 U
15.1 B
15 U15 U
5 U
5 U
5 U
10 U
8.6 U
20 U
NOTES:
Unit s in ug/1
ROD Performance Standard: 7,350 ug/L
NS - No t Sample d
U - No t detecte d at indicate d concentratio n
J (Inorganics ) - Compoun d detected in associated metho d blan kB (Inorganics ) - Estimate d concentratio n is les s tha n th e reponin g limi t
Pag e 9 of 9
Table 3-12
Compariso n of 2002 Analytica l Result s for OU3Well s to Performanc e Standard s
Nationa l Starch and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
Wel l ID
Sampl e No .
Sampl e Dat e
Dilutio n Facto r
Associate d Metho d Blan kvoc
Aceton e
Chlorofor m
1 ,2-Dichloroethan e
cis-1 ,2-Dichloroethen e
trans - 1 ,2-Dichloroethen e
1 , 1 -Dichloroethen e
1 ,2-Dichloropropane
Methylen e chlorid e
Tctrachloroethen e
1,1,2-Trichloroethan e
Trichloroethen c
Viny l chlorid e
Dilutio n Facto r
Associate d Metho d Blan ksvocs
bis(2-Chloroethyl ) ethe r
bis(2-Eihylhexyl ) phthalat e
Dilutio n Facto r
Associate d Metho d Blan k
METALS
Antimon y
Chromiu m
Manganes e
Thalliu mZinc
Performanc e
Standar d
700
1
1
70
70
7
1
5
1
5
2.81
5
5
6
50
50
2
2,10 0
NS-1 3
C2C09 0 13300 1
03/08/0 2
1
EV7G61A A
10 U
1.0 U
0.53 J
1.0 U
1.0 U
1.0 U
0.66 J
2.0 U
1.0 U
2.5
0.6 2 J
2.0 U
1.1 1
EV71V1A A
1 1 U
11 U
1
C2C 1 10000-22 5
10 U
72.6
157
10 U
7.6 B
NS-2 4
C2C16014001 3
03/14/02
I
EWK9G1A A
10 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
2.0 U
1.0 U
1.0 U
1.0 U
2.0 U
1
EWJG81A A
40
10 U1
C2C 18000-23 1
10 U
1.5 B
3200 J
10 U
10.1 B
NS-3 5
C2C080 109005
03/07/02
250
EV7L81A A
2,500 U
250 U
6,700
250 U
250 U
250 U
250 U
500 U
250 U
250 U
250 U
500 U
1
EV71V1A A
10 U
10 U
1
C2C 1 10000 - 129
10 U
4.5 B
11,10 0
20 U *
20 U
NS-3 6
C2C080 109004
03/07/0 2
1,50 0
EV7GRIA A
15,000 U
1,50 0 U
39,000
1,50 0 U
1,50 0 U
1,50 0 U
1,50 0 U
3,000 U
1,50 0 U
1,50 0 U
1,50 0 U
3,000 U
1
EV71V1A A
10 U
10 U
1
C2 C 11 0000 - 12 9
10 U
2.6 B
2,600
10 U
7.8 B
NS-37
C2C16014001 2
03/14/02
1
EWRDV1A A
10 U
.0 U
.O U
.0 U
.0 U
.O U
.O U
2.0 U
.O U
.O U
.O U2.0 U
1
EWJG81A A
10 U
10 U
1
C2C 18000-23 1
10 U30
128 0 J
1 0 U
5 B
NS-38
C2C16014001 1
03/14/02
1
EWRTQ1A A
31
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
2.0 U
1.0 U
1.0 U
1.0 U
^_ 3-6
1
EWJG81A A
10 U
10 U
1
C2C 18000-23 1
10 U
9.1
34,700 J**
SOU**
20 U
NS-3 9
C2C 160 140009
03/14/02
2.5
EWRDV1A A
25 U
2.5 U
46
2.5 U
2.5 U
2.5 U
1.7 J
13
U J
1.5 J
1.4 J
9.7
1
EWJG81A A
9.8 J
10 U
1
C2C 18000-23 1
10 U
7.2
174 J
10 U
20 U
NOTES:
* Sample dilute d at a facto r of 2 for this compound .
** Sampl e dilute d at a facto r of 5 for thi s compound .
U - No t detecte d at indicate d concentratio n
J (Organics ) - Estimate d concentratio n is less tha n the reportin g limi t
J (Inorganics) - Compoun d detected in associated metho d blank
B (Inorganics) - Estimated concentration is less than the reportin g limi tBold fon t indicate s detecte d concentratio n greate r tha n Performanc e Standar d
Pag e I of 4
Table 3-12
Compariso n of 2002 Analytica l Result s for OU3Well s to Performanc e Standard s
Nationa l Starc h an d Chemica l Compan y
Cedar Springs Plan t Site
Salisbury , Nort h Carolin a
Wel l ID
Sampl e No.
Sampl e Dat e
Dilutio n Factor
Associated Method Blankvoc
Acetone
Chlorofor m
1 ,2-Dichloroethan e
cis- 1 ,2-Dichloroethen e
trans-1 ,2-Dichloroethen e
1 , 1 -Dichloroethen e
1 ,2-Dichloropropan e
Methylen e chlorid e
Tetrachloroethene
1 ,1 ,2-Trichloroethan e
Trichloroethen e
Viny l chlorid e
Dilutio n Facto r
Associated Metho d Blanksvocs
bis(2-Chloroethyl) ether
bis(2-Ethylhexyl ) phthalat e
Dilutio n Facto r
Associated Method Blan k
METALS
Antimon y
Chromiu m
Manganes e
Thalliu m
Zinc
Performanc e
Standar d
700
I
1
70
70
7
1
5
1
5
2.8
1
5
5
6
50
50
2
2,100
NS-4 0
C2C 1 60 140008
03/14/02
2,000
EWRTQ1A A
20,000 U
2,000 U
73,000
2,000 U
2,000 U
2,000 U
2,000 U
4,000 U
2,000 U
2,000 U
2,000 U
4,000 U
1
EWJG81A A
6.7 J
10 U
1
C2C 18000-23 1
10 U
2.2 B
7,360 J
10 U
20 U
NS-4 1
C2C 160 14000 6
03/13/0 2
1
EWK9G1A A
10 U
1.0 U
36
1.2
1.0 U
1.0 U
1.0 U
1.2 J
1.7
0.55 J
2.3
2.9
-
-
NS
NS
C2C 18000-231
10 U
122
1,830 J
10 U
8.9 B
NS-42
C2C 160 140007
03/13/02
6
EWRDV1A A
60 U
6.0 U
110
18
6.0 U
3.3 J
6.0 U
12 U
6.0 U
6.0 U
7.5
36
1
EWJG81A A
10 U
10 U
1
C2C 18000-23 1
10 U
32.4
12,800 J
20 U
20.3
NS-43
C2C080 109003
03/06/02
1
EV7GR1A A
10 U
.0 U
.0 U
.0 U
.OU
.0 U
1.0 U
2.0 U
1.0 U
1.0 U
1.0 U
2.0 U
1
EV71V1A A
10 U
10 U
1
C2C 11 0000- 129
10 U
4.1 B
5.2 B
10 U
20 U
NS-4 4
C2C080 109002
03/06/02
1
EV7GR1A A
10 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
2.0 U
1.0 U
1.0 U
1.0 U
2.0 U
1
EV71V1A A
10 U
10 U
1
C2 C 11 0000 - 12 9
10 U
3 B
15 U
10 U
20 U
NS-4 5
C2C090 133002
03/08/02
1
EV7G61AA
10 U
1.0 U
3.3
6.4
1.0 U
7.2
1.0 U
1.1 J
1.0 U
1.0 U
3J
1.9 J
4
EV71V1A A
40 U
40 U
4
C2 C 11 0000-22 5
10 U
1.3 B
4,570
10 U
7.6 B
NS-46
C2C1301 16004
03/12/02
1
EWC3V1A A
3.7 J
1.0 U
12
0.33 J
l.O U
1.8
l.O U
2.0 U
1.2
1.0 U
5.9
9.5
1
EWC3V1A A
10 U
1.4 J
1
C2C 150000-1 31
10 U
5 U
189
10 U
20 U
NOTES:
Unit s in ug/1
U - No t detecte d a t indicate d concentratio n
J (Organics) - Estimated concentratio n is less than the reportin g limi t
J (Inorganics) - Compoun d detecte d in associated metho d blan k
B (Inorganics) - Estimate d concentratio n is less tha n the reportin g limi tBold font indicates detected concentration greater than Performanc e Standar d
Page 2 of4
Table 3-1 2
Compariso n of 200 2 Analytica l Result s for OU3Well s to Performanc e Standard s
Nationa l Starc h and Chemica l Compan y
Cedar Springs Plan t Site
Salisbury , Nort h Carolin a
Well ID
Sampl e No.
Sample Date
Dilutio n Facto r
Associated Method Blan kvoc
Aceton e
Chlorofor m
1,2-Dichloroethan e
cis - 1 ,2-Dichloroethen e
trans- 1 ,2-Dichloroethen e
1,1-Dichloroethen e
1 ,2-Dichloropropan e
Methylen e chlorid e
Tetrachloroethen e
1,1,2-Trichloroethan e
Trichloroethene
Viny l chlorid e
Dilutio n Factor
Associated Metho d Blan ksvocs
bis(2-Chloroethyl ) ethe r
bis(2-Ethylhexyl ) phthalat e
Dilutio n Facto r
Associate d Metho d Blan k
METALS
Antimon y
Chromiu m
Manganes e
Thalliu m
Zinc
Performanc e
Standar d
700
1
1
70
70
7
1
5
1
5
2.8
1
5
5
6
50
50
2
2,10 0
NS-47
C2C 13 0 11 6003
03/11/0 2
10,000
EWC3V1A A
30,000 J
10,000 U
180,000
10,000 U
10,000 U
10,000 U
10,000 U
20,00 0 U
10,000 U
10,000 U
10,000 U
20,00 0 U1
EWC3V1A A
10 U
10 U
1
C2C150000-131
10 U
5 U
1,81 0
10 U
9.9 B
NS-48
C2C130 1 1600 1
03/11/0 2
1
EWC3V1A A
10 U
1.0 U
3.2.o u
.0 U
.0 U.o u
2.0 U
.O U
.0 U
.0 U
2.0 U
1
EWC3V1A A
10 U
10 U
1
C2C150000-131
10 U
2 B
5,830
10 U
20 U
NS-49
C2C080 10900 6
03/07/0 2
1
EV7GR1A A
10 U
1.8
2,500 E
0.7 6 J
1.0 U
1.3
2.4
S3
2.6
3.7
5.1
15
1
EV71V1A A
12
10 U
1
C2 C 1 1 0000- 12 9
13 U
1.6 B
5,870
10 U
47.9
NS-49 DL
C2C080109006 D
03/07/02
300
EV7GR1A A
300 U
30 0 U
7,500
300 U
300 U
300 U
300 U
600 U
300 U
3,000 U
300 U
600 U
-
-
NA
NA
-
-
NA
NA
NA
NA
NA
NS-50
C2C 160 14000 3
03/13/02
15
EWRDV1A A
150 U
15 U
390
15 U
15 U
15 U
15 U
30 U
15 U
15 U
15 U
26 J
1
EWJG81A A
24
10 U
1
C2C 18000-23 1
10 U
2.4 B
2,680 J
10 U
20 U
NS-5 1
C2C0801 09007
03/07/02
1,00 0
EV7G6IA A
10,000 U
1,00 0 U
38,000
,00 0 U
,000 U
,00 0 U
,000 U
2,000 U
,000 U
,00 0 U
,000 U
2,000 U1
EV7IV1A A
10 U
10 U
1
C2 C 11 0000 - 129
10 U
1.6 B
3,460
1 0 U
41.8
DUP-03070 2
C2C080 109009
03/07/02
2,000
EV7G61A A
20,000 U
2,000 U
58,000
2,000 U
2,000 U
2,000 U
2,000 U
4,000 U
2,000 U
2,000 U
2,000 U
4,000 U
1
EV71V1A A
10 U
10 U
1
C2 C 11 0000 - 129
10 U
1.7 B
3,430
10 U
31
NOTES:
Unit s in ug/I
U - Not detecte d at indicate d concentratio n
E - Estimate d concentratio n exceed s th e calibratio n rang e
J (Organics) - Estimate d concentratio n is less than the reportin g limi t
J (Inorganics) - Compoun d detected in associated metho d blan k
B (Inorganics) - Estimate d concentratio n is less than the reportin g limi t
Bold font indicates detected concentration greater than Performanc e Standard
Pag e 3 of 4
Tabl e 3-1 2
Compariso n of 2002 Analytica l Result s for OU3Well s to Performanc e Standard s
Nationa l Starc h and Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
Wel l ID
Sampl e No.
Sampl e Date
Dilutio n Facto r
Associate d Metho d Blan kvoc
Aceton e
Chlorofor m
1 ,2-Dichloroethan e
cis- 1 ,2-Dichloroethen e
trans-1 ,2-Dichloroethene
1 , 1 -Dichloroethen e
1 ,2-Dichloropropan e
Methylen e chlorid e
Tetrachloroethen e
1 ,1 ,2-Trichloroethan e
Trichloroethen e
Viny l chlorid e
Dilutio n Facto r
Associate d Metho d Blan ksvocs
bis(2-Chloroethyl ) ethe r
bis(2-Ethylhexyl ) phthalat e
Dilutio n Facto r
Associate d Metho d Blan k
METALS
Antimony
Chromiu m
Manganese
Thalliu m
Zin c
Performanc e
Standar d
700
1
1
70
70
7
1
5
1
5
2.8
1
5
5
6
50
50
2
2,10 0
NS-5 2
C2C 160 140002
03/13/0 2
1
EWK9G1A A
10 U
1.0 U
5.2
0.44 J
1.0 U
1.0 U
1.0 U
2.0 U
0.8 J
1.0 U
0.72 J
3.4
1
EWJG81A A
10 U
10 U
1
C2C18000-23 1
1 0 U
I.I B
1,07 0 J
10 U
20 U
NS-5 3
C2C1 60 140001
03/03/02
1
EWJP81A A
10 U
99 E
47 E
1.0 U
.0 U
.O U
.0 U
2.5
.1
.0 U
0.52 J
2.0 U
1
EWJG81A A
10 U
10 U '•-,
1
C2 C 18000-23 1
1 0 U
1.1 B
411 J
10 U
31.9
NS-5 3 D L
C2C 160 14000 1
03/03/02
5
EWK9G1A A
SO U
170
82
5.0 U
5.0 U
5.0 U
5.0 U
4.4 J
5.0 U5.0 U
5.0 U
10 U
-
-
NA
NA
-
-
NA
NA
NA
NA
NA
DUP-03130 2
C2C 160 140005
03/13/02
1
EWK9G1A A
10 U
95 E
47 E
1.0 U
1.0 U
1.0 U
1.0 U
2.4
0.87 J1.0 U
0.46 J
2.0 U
1
EWJG81A A
10 U
10 U
1
C2C 1 8000-23 1
10 U
5.0 U
412 J
10 U
26.8
DUP-03130 2
C2C 160 140005
03/13/02
6
EWK9G1A A
60 U
180
83
6.0 U
6.0 U
6.0 U
6.0 U
4.9 J
6.0 U
6.0 U
6.0 U
12 U
-
-
NA
NA
-
-
NA
NA
NA
NA
NA
NS-5 4
C2C 1 301 16005
03/12/02
2,500
EWC3V1A A
6,500 J
2,500 U
69,000
2,500 U
2,500 U
2,500 U
2,500 U
5,000 U
2,500 U
2,500 U
2,500 U
5,000 U
1
EWC3V1A A
10 U
10 U
1
C2C150000-13 1
1 0 U
1.5 B
4,520
10 U
248
CT-1
C2C080 109-008
03/07/02
1
EV7GR1A A
10 U
1.0 U
2.0
0.67 J
1.0 U
0.51 J
I . O U
2.0 U
I.O U1.0 U0.3 9 J
2.0 U
1
EV71V1A A
10 U
10 U
1
C2 C 11 0000- 129
10 U
5 U
163
10 U
22.7
NOTES:
Units in ug/l
U - No t detected at indicate d concentratio n
E - Estimate d concentratio n exceed s th e calibratio n rang e
J (Organics) - Estimated concentratio n is less than the reportin g limi t
J (Inorganics ) - Compoun d detecte d in associate d metho d blan k
B (Inorganics) - Estimated concentratio n is less than the reportin g limi t
Bold font indicates detected concentration greater than Performance Standard
Pag e 4 of4
Table 3-1 3
Historica l Analytica l Result s - VOCs
OU3 Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury, North Carolina
ACETONE
Quarter
2Q98
3Q983Q99
1QO O
3QO O
IQ0 1
1Q0 2
NS-1 31000 U
NS100 U
NS
10 U
NS10 U
NS-1 4
10 U
NS100 U
NS
10 U
NS
NS
NS-2 4
NR
NS
100 U
10 U10 U
20 U
10 U
NS-35
2500 U
NS
10 0 U
10 U
10 U
20 U
2500 U
NS-36
500 U
23
25000 U10 U
8 J
5 U
75000 U
NS-37
10
NS
100 U
10 U
10 U
2 U10 U
NS-38
49
10 U
IS O
16010 U
11 0 D
31
NS-39
25 0 U
38
100 U
10 U
10 U
NS
25 U
NS-40
2000 U
50 U
100 U
NS
10000 U
NS
20000 U
NS-4 1
5000 U
NS
200 U
NS
10 U
NS
10 U
ISS-4 2
120 0 J
240010000 U
NS
120 0 E
NS
60 U
NS^I3
4 J
10 U
100 U
10 U
10 U
2 U
10 U
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O
1Q0 1
100 2
NS-44
10 U
NS
10 0 U
10 U
10 U
2 U
10 U
NS-45
140
NS100 U
NS
10 U
NS
10 U
NS-46
10 U
NS
100 U
NS
100 0 U
NS
3.7 J
NS-47
10000 U
NS
100 U
NS
10 U
NS
30000 J
NS-48ISO J
NS
100 U
NS
10 U
NS10 U
NS-49
2900
NS
10000 U10000 U
10 . U
5000 U
10 U
NS-50
2500
NS
100 U
NS
10 U
2 U
150 U
NS-5 1
10000 U
NS
10000 U
25000 U
20 U
NS10000 V
NS-52
2500 U
NS;ooo o u
NS
10 U
NS
10 U
NS-53
2200 J
NS
10 0 U
NS
10 U
NS
50 U
NS-54
500 U
NS
20000 U
NS
10 U
2 U
6500 J
CT-1
NS
NS
10 0 U
10 U
10 U
5 U
10 U
NOTES:
Unit s in ug/l
ROD Performanc e Standard: 700 ug/L
NS - Not Sampled
U - Not detected at indicate d concentratio nE - Estimate d concentratio n exceed s the calibratio n rang e
J (Organics ) - Estimate d concentratio n is les s tha n th e reportin g limi t
Bold fon t indicate s detected concentratio n greater than ROD Performanc e Standar d
Itali c fon t indicates detection limi t greater tha n RO D Performanc e Standard
Pag e 1 of 1 2
Table 3-1 3
Historica l Analytica l Result s - VOCs
OU 3 Extractio n an d Monitorin g Well s
Nationa l Starc h an d Chemica l Compan yCedar Spring s Plan t Site
Salisbury , Nort h Carolin a
CHLOROFOR M
Quarter
2Q983Q98
3Q99
1QO O
3QO O
1QO I
1Q0 2
NS-1 3
1000 U
NS
14
NS
5
NS
1 U
NS-1 4
10 U
NS5 U
NS
5 U
NS
NS
NS-2 4
5 U
NS
5 U1 U
5 U
1 U
1 U
NS-35
2500 U
100 U
5 U1 U
5 U
I U
250 U
NS-36
500 U
10 U5 U
2J
3 J
41500 U
NS-3710 U
NS
5 U
1 U
5 V
1 U
1 U
NS-38
10 U
10 U5 U1 U
5 U
5 U1 U
NS-39250 U
5 J
5 UNS
5 U
NS2.5 U
NS-40
2000 U
50 U
5 U
NS
5000 U
NS
2000 U
NS-4 1
5000 U
NS10 U
NS
5 U
NS
1 U
NS-42
2500 U
500 U500 U
NS
20
NS6 U
NS-43
10 U
10 U
5 U
1 U
5 U
1 U
1 U
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O
IQO t
IQ02
NS-44
10 U
NS
5 U
1 U
5 U
1 U
1 U
NS-»5
100 U
NS
5 U
NS
5 U
NS
1 U
NS-46
10 U
NS
5 U
NS500 U
NS
1 U
NS-47
10000 U
NS
5 U
NS
3 J
NS10000 U
NS-48
250 U
NS
5 U
NS
3 J
NS1 U
NS-49
2500 U
NS
500 U
1000 U
3 1
1000 U
1.8
NS-50
2500 U
NS
5 U
NS
4 J
315 U
l_ NS-51
10000 U
NS
500 U
25000 U10 U
NS1000 U
NS-52
2500 U
NS
500 U
NS
5 U
NS1 U
NS-S3
2500 U
NS
5 U
NS
55
NS
170
NS-54
500 U
NS
1000 U
NS
19
22
2500 U
CT-1
NSNS
5 U
1 U
5 U
1 U
1 U
NOTES :
Unit s in ug/l
ROD Performanc e Standard: 1 ug/L
NS - Not Sampled
U - Not detected at indicate d concentratio n
J (Organics ) - Estimate d concentratio n is less than the reportin g limi t
Bold fon t indicate s detected concentratio n greater than ROD Performanc e Standar d
Italic fon t indicates detectio n limi t greate r than ROD Performanc e Standar d
Pag e 2 o f 1 2
Tabl e 3-1 3
Historical Analytica l Result s - VOCs
OU 3 Extractio n and Monitorin g Well s
Nationa l Starch and Chemical Company
Ceda r Spring s Plan t Site
Salisbury , Nort h Carolin a
1,2-DICHLOROETHAN E
Quarter
2Q9 8
3Q9 83Q991QOO
3QO O
1Q0 1
1Q0 2
NS-1 3
1000 U
NS
76NS
I 0000 O
NS
0.5 3 J
NS-1 4
10 U
NS
5 VNS51 D
NS
NS
NS-2 4
NS
NS5 U
1 U5 U
211 U
NS-35
2500 U
100 V
40000
41000 417000 D
5000 D
6700
NS-36
500 U10 U
5200060000
63000 D
130000 D
39000
NS-37
10 U
NS5 U
1 U5 U\ U
1 U
NS-38
10 U
10 U
5 U
1 U
5 U
5 U
1 U
NS-39
250 U
10 U
270NS
19
NS
46
NS^t O
2000 U
50 U
92000
NS
84000 D
NS
73000
NS-4 1
5000 U
NS
84
NS
130
NS
36
NS^»2
2500 U
500 U
92000NS
320000 D
NS
110
NS-43
10 U
10 U
5 U
1 U
5 U
1 U
1 U
Quarter
2Q98
3Q983Q99
1QO O
3QO O
1Q0 1
1Q0 2
NS-44
10 U
NS
5 U
1 U
5 UI U1 U
NS-45
100 U
20 U
310 0
NS
190
NS3.3
NS-46
10 U
NS18
NS
3000 D
NS12
NS-47
10000 U
NS
310000NS
26000 0 D
NS
180000
NS-48
250 U
NS
67
NS
18
NS
3.2
NS-49
2500 U
N S15000
34000
32000 D
22000 D7500
NS-50
2500 U
NS
29000
NS
4500 D
160000 D
390
NS-5 1
10000 U
NS
290000
410000
9200 0 D
NS
38000
NS-52
2500 U
NS
8400
NS
410 0 D
NS
5.2
NS-53
2500 U
NS
13000
NS
2000 0
NS
82
NS-54
500 U
NS
31000
NS
7200 D
78000 D
69000
CT-1
NS
NS5 U
8.1
2 J
25
2
NOTES .
Unit s in ug/1
RO D Performanc e Standard : 1 ug/L
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
D - Concentratio n fro m a secondary dilutio n analysi s
E/4 - Estimated concentration exceeds the calibration range
J (Organics ) - Estimate d concentratio n is less than th e reportin g limi t
Bold fon t indicate s detected concentratio n greate r than RO D Performanc e Standar d
Itali c font indicates detection limi t greater than ROD Performanc e Standard
Pag e 3 o f 1 2
Table 3-13
Historica l Analytica l Result s - VOCs
OU 3 Extractio n an d Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolin a
1,1-DICHLOROETHEN E
Quarter2QJ98
3Q9 83Q99IQOO
3QO O
1Q0 1
1Q0 2
NS-1 3
1000 V
NS5 U
NS
3 J
NS
1 U
NS-14
10 U
NS
5 UNS
5 U
NSNS
NS-2 4
NS
NS
5 U
1 U
5 U
1 U1 U
NS-35
2500 U
100 U
5 U1.6
5 U
0.7 J
250 U
NS-36
50 0 U
10 U
5 U
5.4
7
NS/500 U
NS-37
10 U
NS
5 U
1 U
5 U
1 U
1 U
NS-38
10 U
10 U
5 U
1 U
5 U
5 U1 U
NS-3 9
250 U
10 U
5 UNS
NS
NS
2.5 U
NS-40
2000 U
50 U
5 U
NS
5000 U
NS
2000 U
NS-41
5000 U
NS10 U
NS
5 U
NS
1 U
NS-42
2500 (/
500 U
500 U
NS
NS
NS
3.3 J
NS-4 3
10 U
10 U5 U1 U
5 U
1 U
1 U
Quarter
2Q983Q98
3Q99
IQO O
3QO OIQ01
1O0 2
NS-44
10 U
NS
5 U
1 U
5 U1 UI U
NS-45
700 U
NS
24
NS
16
NS7.2
NS-46
10 U
NS5 U
NS
500 U
NS1.8
NS-47
10000 U
NS5 U
NS
3 J
NS/ooo o u
NS-48
250 U
NS5 U
NS
5 U
NS1 U
NS-49
2500 U
NS
500 U
1000 U
NS
1000 U
1.3
NS-50
2500 U
NS5 U
NS
4 J
4
15 U
NS-51
10000 U
NS
500 U
25000 U
10 U
NS1000 U
NS-52
2500 U
NS
500 U
NS
5 UNS1 U
NS-53
2500 U
NS
5 U
NS
5 U
NS
5 U
NS-54
500 U
NS1000 U
NS
3 J
102500 U
CT-1
NS
NS
5 U
1.2
5 U20.5 1 J
NOTES:Unit s in ug/l
RO D Performanc e Standard : 7 ug/L
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
J (Organics ) - Estimate d concentratio n is less tha n the reportin g limi t
Bol d fon t indicate s detected concentratio n greater tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r than RO D Performanc e Standar d
Page 4 of 12
Table 3-13
Historica l Analytica l Result s - VOCs
OU3 Extractio n and Monitorin g Well s
Nationa l Starch an d Chemica l Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolin a
CIS-1.2-DICHLOROETHEN E
Quarter
2Q98
3Q983Q99
IQO O
3QO O
1QO I
1Q02
NS-13
NS
NS5 UNS
5 U
NS
1 U
NS-14
NS
NS
5 U
NS
5 U
NS
NS
NS-24
NS
NS
5 U
1 U
5 U
1 U
1 U
NS-3 5
NS
NS
5 U
1.2
5 U2
750 U
NS-36
NS
NS
5 U
1.3
5 U
3
1500 U
NS-37
NS
NS
5 U
1 U
5 U
1 U
1 U
NS-38
NS
NS
5 U
1 U
5 U
5 U
1 U
NS-39
NS
NS
5 U
NS
NS
NS
2.5 U
NS-4 0
NS
NS
5 U
NS
5000 U
NS
2000 U
NS^l
NS
NS
10 U
NS
5 U
NS
1.2
NS-42
NS
NS
500 U
NS
NS
NS
18
NS-43
NS
NS
5 U
I U
5 U
1 U
1 U
Quarter
2Q983Q98
3Q99
IQO O
3QO O
1Q0 1
1002
NS-44
NSNS
5 U
1 U
5 U
1 U1 U
NS-45
NS
NS
16
NS11
NS
6.4
NS-46
NS
NS
5 U
NS
500 U
NS0.33 J
NS-47
NS
NS
5 U
NS
5 U
NS
10000 U
NS-48
NS
NS
5 U
NS
5 U
NS
1 U
NS-49
NS
NS
500 U
1000 U
NS
1000 U
0.76 J
NS-50
NS
NS
5 U
NS5 U
5
15 U
NS-S1
NS
NS
500 U
25000 U
10 U
NS
1000 U
NS-52
NS
NS
500 U
NS
5 J
NS
0.44 J
NS-53
NS
NS
5 U
NS
5 U
NS
5 U
NS-54
NS
NS
1000 U
NS
5 U
1 U2500 U
CT-1
NS
NS
5 U
1 U
5 U
10.67 J
NOTES:
Unit s in ug/l
ROD Performance Standard: 70 ug/L
NS - Not SampledU - No t detected at indicate d concentratio n
J (Orga n ics ) - Estimate d concentratio n is less tha n the reportin g limi t
Itali c fon t indicate s detectio n limi t greate r than RO D Performanc e Standar d
Pag e 5 o f 1 2
Table 3-13Historical Analytica l Result s - VOC s
OU 3 Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolin a
TRANS-1,2-DICHLOROETHEN E
Quarter
2Q98
3Q983Q99
1QO O
3QO O1Q01
1Q0 2
NS-13
NS
NS5 U
NS
5 UNS
1 U
NS-14
NS
NS5 U
NS
5 UNS
NS
NS-2 4
NS
N S5 U
1 U
5 U1 U
1 U
NS-35
NS
100 U
5 U
1 U
5 U1 U250 U
NS-36
NS
10 U
5 U
1 U
5 U0.9 J
1500 U
NS-37
NS
NS
5 U1 U
5 U
1 U
1 U
NS-38
NS
10 U5 U
1 U
5 U5 U
1 U
MS-3 9
NS
10 U5 U
NS
NSNS2.5 U
NS^O
NS
50 U5 U
NS
5000 UNS
2000 U
NS-41
NS
NS10 U
NS
5 UNS1 U
NS-42
NS
500 U500 U
NS
NSNS
6 U
NS^»3
NS
10 U5 U
1 U
5 U1 U1 U
Quarter
2Q98
3Q983Q99
IQO O
3QO O
1Q0 1
1Q0 2
NS^»4
NS
NS
5 U
1 U
5 U
1 U
1 U
NS-45
NS
NS
5 U
NS
5 UNS
1 U
NS-46
NS
NS
5 U
NS
500 U
NS
1 U
NS-47
NS
NS
5 U
NS
5 U
NS
10000 U
NS^J S
NS
NS
5 U
NS
5 U
NS1 U
NS^49
NS
NS
500 U
1000 U
NS;oo o u
1 U
NS-50
NS
NS
5 U
NS
5 U
1 U
15 U
NS-51
NS
NS
500 U
25000 U
10 U
NS
7000 U
NS-S2
NS
NS500 U
NS
5 U
NS
1 U
NS-53
NS
NS
5 U
NS
5 U
NS
5 U
NS-54
NS
NS
1000 U
NS
5 U
1 U
2500 U
CT-1
NS
NS
5 U
1 U
5 U
1 U
1 U
NOTES:
Unit s i n ug/l
RO D Performanc e Standard : 70 ug/L
NS - Not SampledU - No t detecte d at indicate d concentration
J (Organics ) - Estimated concentratio n is les s than the reportin g limi t
Itali c fon t indicate s detectio n limi t greate r than ROD Performanc e Standar d
Pag e 6 of 12
Table 3-13Historical Analytica l Result s - VOC s
OU3 Extractio n an d Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
1,2-DICHLOROPROPAN E
Quarter
2Q98
3Q983Q99
1QO O
3QO O
1QO I
1Q0 2
NS-13
1000 U
NS
14
NS
7NS
0.66 J
NS-1 4
10 U
NS
5 U
NS
5 U
NS
NS
NS-2 4
NSNS
5 U
1 U5 U
1 U
1 U
NS-35
2500 U
100 U
5 U
2.7
5 U
1 U250 U
NS-36
500 U
10 U
5 U
2.1
3 J
1 U7500 U
NS-37
10 U
NS
5 U
1 U
5 U
1 U
1 U
NS-38
10 U
10 U
i U
2.7
5 U
5 U1 U
NS-39
250 U
5 J5 U
NS
5 U
NS1.7 J
NWO
2000 U
50 U
5 U
NS
5000 U
NS2000 U
NS-4 1
5000 U
NS
10 U
NS
5 U
NS
1 U
NS-4 2
2500 U
500 U
500 UNS
5 U
NS6 U
NS-43
10 U
10 U
5 U
1 U
5 U
1 U
1 U
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O
IQ0 1
1O02
NS-44
10 U
NS
5 UI U
5 U
1 U1 U
NS-45
100 U
NS
5 U
NS
5 U
NS1 U
NS-4610 U
NS
5 U
NS
500 U
NS1 U
NS^»710000 U
NS
5 U
NS
3 J
NS10000 V
NS-48
250 U
NS
5 U
NS
5 U
NS
1 U
NS-49
2500 U
NS
500 U
1000 U
5 U1000 U
2.4
NS-50
2500 U
NS
5 U
NS
5 U
1 U
15 U
NS-51
10000 U
NS
500 U
25000 U
12 D
NS
7000 U
NS-52
2500 U
NS
500 U
NS
2 J
NS
1 U
NS-53
2500 U
NS
5 U
NS5 U
NS
5 U
NS-54
500 U
NS
7000 U
NS5 U
1 U
2500 U
CT-1
NS
NS
5 U
1 U5 U
1 U1 U
NOTES:
Unit s in ug/1
RO D Performanc e Standard : 1 ug/L
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
D - Concentratio n fro m a secondar y dilutio n analysi s
J (Orgarncs ) - Estimate d concentratio n is less tha n th e reportin g limi t
Bol d fon t indicate s detected concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greater tha n RO D Performanc e Standar d
Page7ofl 2
Table 3-13
Historica l Analytica l Result s - VOCsOU3 Extractio n and Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
METHYLEN E CHLORID E
Quarter
2Q98
3Q98
3Q99
IQO O
3QO O1Q01
1Q0 2
NS-13
1000 V
NS
7.6
NS
6
NS2 U
NS-14
10 U
NS
5 U
NS
6
NSNS
NS-24
NS
NS5 U1 U
5 U
1 U
2 U
NS-35
2500 U
100 U5 U
1 U
5 U
1 U500 U
NS-36
500 U
10 U5 U
2.3 4
4 J
6 B3000 U
NS-37
10 U
NS
5 U
1 U
5 U
0.2 J B
2 U
NS-38
10 U
10 U
5.93 4
5 U
5 U2 U
NS-39
250 U
6 J5 UNS
5 U
NS13
NS-40
2000 U
120
87
NS
5000 U
NS4000 U
NS-415000 U
NS10 UNS
5 U
NS
1.2 J
NS-42
2500 U
500 U500 U
NS
32
NS12 U
NS-4310 U
10 U5 U
1 U
5 U
0.2 J B2 U
Quarter2Q98
3Q98
3Q99
IQO O
3QO O
IQ0 1
1O0 2
NS-44
10 U
NS
5 U
1 U
5 U
1 U2 U
NS-45
700 U
NS
5 U
NS
5 U
NS
1.1 J
NS-46
10 UNS
5 U
NS
500 U
NS2 U
NS-47
10000 U
NS
5 U
NS
5 U
NS
20000 U
NS-48
250 U
NS
6.6
NS
5 U
NS
2 U
NS-492500 U
NS500 U
1000 U
21
7000 U
5.3
NS-50
2500 U
NS
52
NS
17
3700 JD
30 U
NS-5170000 U
NS
500 U
25000 U
38 D
NS
2000 U
NS-52
1300 J
NS
500 U
NS
18
NS
2 U
NS-532500 U
NS
14
NS
5
NS4.4 J
NS-54
500 U
NS
1000 U
NS
20
3700 JD
5000 U
CT-1
NS
NS
5 U
1 U
5 U
1 U
2 U
NOTES:
Unit s in ug/l
ROD Performanc e Standard : 5 ug/L
NS - Not Sampled
U - Not detecte d at indicate d concentratio n
D - Concentratio n fro m a secondary dilutio n analysis
E/4 - Estimate d concentratio n exceed s the calibratio n range
J (Organics ) - Estimate d concentratio n is less tha n the reportin g limi t
B (Organics ) - Compoun d detecte d in associate d metho d blan k
Bold font indicates detected concentration greater than ROD Performance Standard
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 8 of 1 2
Tabl e 3-13
Historica l Analytica l Result s - VOCs
OU 3 Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
TETRACHLORETHENE
Quarter
2Q9 83Q98
3Q99
1QO O
3QO O
IQ0 1
1Q0 2
NS-131000 U
NS
5 U
NS
4 J
NS1 U
NS-14
10 U
NS
5 U
NS
5 UNSNS
NS-24
NS
NS
5 U
1 U
5 U1 U1 U
NS-35
2500 U
100 U5 U
3.8
4 J0.9 J250 U
NS-36
500 U
10 U
5 U
3.54 J
7/500 U
NS-37
10 U
NS
5 U
1 U5 U1 U1 U
NS-38
10 U
10 U
5 U
1 U5 U
5 U
I U
NS-39
250 U
10 U
5 U
NS5 U
NS
U J
NS-40
2000 U
10 J
13
NS
5000 U
NS2000 U
NS-4 1
5000 U
NS
10 U
NS5 U
NS
1.7
NS-42
2500 U
500 U
500 U
NS
37NS6 U
NS-43
10 U
10 U
5 U
1 U
5 U
1 U
1 U
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O1QOI
1002
NS-44
10 U
NS
5 U
1 U
5 U1 U
1 U
NS-45
100 U
NS
5 UNS
5 UNS
1 U
NS-46
10 U
NS
5 VNS
500 UNS1.2
NS-47
10000 U
NS
9.6NS
8
NS
10000 U
NS-48
250 U
NS
5 UNS
5 U
NS
1 U
NS-49
2500 UNS
500 U
1000 U
61000 U
2.6
NS-SO2500 U
NS
6.3NS
5 U7
15 U
NS-S1
10000 U
NS
500 V
25000 U
7 JD
NS
1000 U
NS-522500 U
NS
500 U
NS
3 JNS
0.8 J
NS-532500 U
NS
5 U
NS
5 U
NS5 U
NS-S4
500 U
NS
7000 U
NS
7
162500 U
CT-1
NS
NS
5 U
1 U
5 UI U
1 U
NOTES:
Unit s in ug/1
ROD Performance Standard: 1 ug/L
NS - Not Sampled
U - No t detecte d at indicate d concentratio n
D - Concentratio n fro m a secondar y dilutio n analysi s
J (Organics ) - Estimate d concentratio n is less than the reportin g limi t
Bol d fon t indicate s detected concentratio n greate r tha n ROD Performanc e Standar d
Italic fon t indicates detection limi t greater than ROD Performanc e Standard
Pag e 9 o f 1 2
Tabl e 3-13
Historica l Analytica l Results - VOCs
OU3 Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Company
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
1,1,2-TRlCHLOROETHAN E
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O
1Q0 11Q02
NS-13
1000 U
NS
41
NS
28
NS
2.5
NS-1 4
10 U
NS
5 UNS
5 U
NS
NS
NS-24
NS
NS
5 U1 U
5 U1 U
1 U
NS-35
2500 U
100 U5 U2.8
5 U
1 U
250 U
NS-36500 U
10 U
2023
20
1 U
/5C O U
NS-37
10 U
NS
5 U1 U
5 U
1 U
1 U
NS-38
10 U10 U
5 U1 U5 U
5 U
1 U
NS-39
250 U
2 J5 U
NS
5 U
NS
1.5 J
NS-40
2000 U
7 J
8.5
NS5000 U
NS
2000 U
NS-41
5000 U
N S10 UNS
5 U
NS
0.55 J
NS-4 22500 U
83 J
500 U
NS
160
NS
6 U
NS-43
10 U
10 U
5 U
1 U
5 U
1 U
1 U
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O
1QO I
1Q02
NS-44
10 U
NS
5 U
1 U
5 U
1 U1 U
NS-45
100 U
NS
5 U
NS5 U
NS
1 U
NS-46
10 U
NS
5 U
NS
500 UNS1 U
NS-4 7
10000 U
NS
2500 U
NS
12
NS
10000 U
NS-48
250 U
NS
5 U
NS
5 UNS
1 U
NS^t9
2500 U
NS
500 U
1000 U
12
1000 U
3.7
NS-SO
2500 U
NS
6.1
NS
131 UIS U
NS-5 1
10000 U
NS
500 U
25000 U
42 D
NS1000 U
NS-52
2500 U
NS
500 U
NS
5 U
NS
1 U
NS-53
2500 U
NS
5 U
NS
5 UNS
5 U
NS-54
500 U
NS
7000 UNS
4 J
7
2500 U
CT-1
NS
NS
5 U
1 U
5 U1 U1 U
NOTES:
Units in ug/l
ROD Performanc e Standard : 5 ug/L
NS - Not SampledU - Not detecte d at indicate d concentratio n
D - Concentratio n fro m a secondar y dilutio n analysi s
J (Organics ) - Estimate d concentratio n is less than the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r than RO D Performanc e Standar d
Pag e 1 0 o f 1 2
Table 3-13
Historica l Analytica l Results - VOCs
OU 3 Extractio n and Monitorin g Well s
Nationa l Starch and Chemical Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolin a
TRICHLOROETHEN E
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O
1Q0 1
1Q0 2
NS-131000 U
NS
12NS
8
NS
0.6 2 J
NS-14
10 U
NS
5 U
NS
2 J
NS
NS
NS-24
NS
NS
} U1 U
5 U1 U
1 U
NS-35
2500 U
100 U
5 U5.2
6
3250 U
NS-36
500 U
10 U
6.78
12
217500 U
NS-37
10 U
NS
5 U
1 U5 U
1 U
1 U
NS-38
10 U
10 U
5 U
1 U
5 U
5 U
1 U
NS-39
250 U
10 U
5 U
NS
5 U
NS
1.4 J
NS-40
2000 U
7 J
9.2NS
5000 U
NS
2000 U
NS-4 1
5000 U
NS
10 U
NS
5 U
NS
2.3
NS-42
2500 U
500 U
500 U
NS
66
NS
7.5
NS-43
10 U
10 U5 U1 U
5 U
1 U
1 U
Quarter
2Q983Q98
3Q99
IQO O
3QO O
1QO I
1Q02
NS-44
10 U
NS
5 U
1 U
5 U1 U1 U
NS-45
100 U
NS
63
NS
5 J
NS
3.3
NS-46
10 U
NS
5 U
NS
500 U
NS
5.9
NS-47
10000 U
NS
13NS
9
NS10000 U
NS-48
250 U
NS
5 f
NS
5 U
NS
1 U
NS-49
2500 U
NS
500 U
1000 U
1
1000 U
5.1
NS-50
2500 UNS
5.6
NS
2 J
16/5 U
NS-51
10000 U
NS
500 U
25000 U
12 DNS;oo o u
NS-52
2500 U
NS
500 U
NS
4 JNS
0.72 J
NS-53
2500 U
NS
5 U
NS
5 U
NS
5 U
NS-54
500 U
NS
1000 U
NS
2 J
132500 U
CT-1
NS
NS
5 U
1 U
5 U
1
0.39 J
NOTES:
Unit s in ug/1
ROD Performanc e Standard : 2.8 ug/L
NS - Not SampledU - No t detecte d at indicate d concentratio n
D - Concentratio n fro m a secondar y dilutio n analysi s
J (Organics ) - Estimated concentratio n is less than the reportin g limi t
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Italic fon t indicates detection limi t greate r than ROD Performanc e Standard
Page 11 of 12
Table 3-13
Historica l Analytica l Result s - VOCs
OU 3 Extractio n and Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury, North Carolin a
VINYL CHLORID E
Quarter
2Q9 83Q98
3Q99
1QO O
3QO O
1Q0 1
1Q0 2
NS-I3
1000 U
NS
10 U
NS5 U
NS
2 U
NS-I4
10 U
NS10 U
NS
4 J
NS
NS
NS-24
NS
NS10 U1 U
5 U
1 U
2 U
NS-35
2500 U
60 J58
110 4
210 E
48 E
500 U
NS-36500 U
1299
130 4
280 E
350 E
3000 U
NS-3710 U
NS10 U
1 U
5 U
1 U
2 U
NS-38
10 U
9 J23
14
24
27 D3.6
NS-39
250 U
1210 U
NS
4 J
NS
9.7
1VS-4 0
2000 U
7956NS
5000 U
NS
4000 U
NS-4 1
5000 U
NS20 U
NS
5 U
NS
2.9
NS-42
2500 U
500 U1000 U
NS
200
NS36
IVS-4 3
10 U
10 U10 U
1 U
5 U
1 U
2 U
Quarter
2Q98
3Q98
3Q99
IQO O
3QO O
1Q0 1
1Q0 2
NS-44
10 UNS10 V
1 U
5 V
1 U
2 U
NS-45
100 U
NS10 U
NS
4 J
NS1.9 J
NS-46
10 U
NS
10 U
NS
500 U
NS
9.5
NS-47
10000 U
NS
580
NS
570 E
NS20000 U
NS-48
250 U
NS
10 V
NS
5 U
NS2 U
NS-492500 U
NS
1000 U
1000 U
46
1000 UIS
NS-50
2500 U
NS10 U
NS
260 E
73 E
26 J
NS-5 1
10000 U
NS
1000 U
NS
28 D
NS2000 U
NS-522500 U
NS
1000 U
25000 U
60
NS
3.4
NS-53
2500 U
NS
10 U
NS
8
NS
10 U
NS-54
78 J
NS
2000 U
NS
110
260 E
5000 U
CT-1
NS
NS
10 U
1 U5 U1 U2 U
NOTES :
Unit s in ug/lROD Performanc e Standard : 1 ug/L
NS - Not Sample dU - Not detected at indicate d concentratio n
D - Concentratio n fro m a secondar y dilutio n analysi sE/4 - Estimate d concentratio n exceed s th e calibratio n rang e
J (Organics ) - Estimate d concentratio n is less than the reportin g limi t
Bol d fon t indicate s detected concentratio n greate r than RO D Performanc e Standar d
Itali c fon t indicate s detection limi t greater than ROD Performanc e Standard
Pag e 1 2 o f 1 2
Table 3-14
Historica l Analytica l Result s - SVOCs
OU 3 Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
BIS(2-CHLOROETHYL)ETHE R
Quarter
2Q98
3Q983Q99
1QO O
3QO O
1Q0 1
190 2
NS-1 3
NS
NS
10 U
NS
1 J
NS
// U
NS-1 4
NS
NS
10 U
NS
10 U
NS
NS
NS-24
NS
NS
57
45
50
5340
NS-35
NS
NS
10 U10 U
10 U
10 U10 U
NS-36
NS
NS
10 U
II U
10 U
1 J
10 U
NS-37
NS
NS
10 U
10 U
10 U
10 U
10 U
NS-38
NS
NS
10 U
NS
4 J
7 J
10 U
NS-39
NS
NS
10 U
NS
4.2 J
NS
9.8 J
NS-40
NS
NS
11NS
17
NS
6.7 J
NS-4 1
NS
NS
10 U
NS
10 U
NS
NS
NS-42
NS
NS10 UNS
9.5 U
NS
10 U
NS-43
NS
NS10 U10 U
10 U
10 U10 U
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O1Q01
1Q0 2
NS-44
NS
NS
10 U10 U
10 U
10 U
10 U
NS-4S
NS
NS
10 U
NS10 U
NS
40 U
NS-46
NS
NS
10 U
NS10 UNS
10 U
N&47
NS
NS
10 U
NS
10 U
NS10 U
NS-48
NS
NS
10 U
NS10 U
NS10 U
NS-49
NS
NS
14
10 U
20
17
12
NS-50
NS
NS
12
NS
19
10 U
24
NS-5 1
NS
NS
10 U
10 U10 U
NS10 U
NS-52
NS
NS
10 U
NS10 U
NS10 U
NS-53
NS
NS
10 U
NS
2 J
NS10 U
NS-54
NS
NS
10 U
NS10 U10 V10 U
CT-1
10 U
10 U10 U
10 V
NOTES:
Unit s in ug/l
ROD Performanc e Standard: 5 ug/L
NS - Not SampledU - No t detecte d at indicate d concentratio n
J (Organics ) - Estimate d concentratio n is less than the reportin g limi t
Bold fon t indicate s detected concentratio n greater than ROD Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 1 o f 2
Table 3-14
Historica l Analytica l Results - SVOCs
OU3 Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Sit e
Salisbury , Nort h Carolin a
BIS(2-ETHYLHEXYL)PHTHALAT E
Quarter
2Q98
3Q98
3Q991QOO
3QO O
1Q0 1
1Q0 2
NS-1 3
NS
NS10 UNS10 U
NS
// U
NS-1 4
NSNS
10 U
NS10 U
NS
NS
NS-24
NS
NS
57
10 U
10 U10 U10 U
NS-35
NS
NS
10 U
10 U
3 J10 U10 U
NS-36
NSNS10 U11 U
2 }10 U10 U
NS-37
NS
NS
10 U
10 V
10 U1 J10 U
NS-38
NS
NS
10 U
10 U
10 U
10 U10 U
NS-3 9
NS
NS
10 U
NS
9.5 U
NS10 U
NS-40
NS
NS
10 U
NS
10 UNS10 U
NS-4 1
NS
NS
10 U
NS
10 U
NS
NS
NS-4 2
NS
NS
10 U
NS9.5 U
NS
10 U
NS-43
NS
NS
10 V10 U10 U
10 U10 U
Quarter
2Q98
3Q98
3Q99
IQO O
3QO O1QOI
1Q0 2
NS^4
NS
NS10 U
10 U
10 U10 U10 V
NS-45
NS
NS
10 U
NS
10 UNS40 U
NS-46
NS
NS
10 U
NS
10 UNS
1.4 J
NS-47
NS
NS
10 U
NS10 V
NS10 U
MS-48
NS
NS
10 U
NS10 U
NS10 U
NS-49
NS
NS
10 U
10 U
6.3 J10 U
10 U
NS-50
NS
NS
10 U
NS
4 J
10 U
10 U
NS-5 1
NS
NS
10 U
10 U
10 U
NS
10 U
NS-S 2
NS
NS
10 U
NS
10 U
NS10 U
NS-53
NS
NS
10 U
NS
10 U
NS10 U
NS-54
NS
NS
10 U
NS
10 U
4 JB10 U
CT-1
NS
NS
10 U
10 U10 U
10 U10 U
NOTES:
Unit s in ug/1
RO D Performanc e Standard : 5 ug/L
NS - Not SampledU - No t detecte d at indicate d concentratio n
J (Organics ) - Estimate d concentratio n is less than the reportin g limi t
B (Organics) - Compound detected in associated method blan k
Bol d fon t indicate s detected concentratio n greate r tha n RO D Performanc e Standar d
Itali c fon t indicate s detectio n limi t greate r tha n RO D Performanc e Standar d
Pag e 2 of 2
Table 3-15
Historica l Analytica l Result s - Metal s
OU3 Extraction and Monitorin g Well s
Nationa l Starc h an d Chemica l Compan y
Ceda r Spring s Plan t Sit e
Salisbury , Nort h Carolin a
ANTIMONY
Quarter
2Q983Q98
3Q99
1QO O
3QO O
1Q0 11Q02
NS-1 3
4.2 U
NS
5 U
NS
1.6 U
NS10 U
NS-14
NS
NS
5 UNS
1.6 U
NS
NS
NS-24
NSNS
5 U5 U
1.6 U
1 U
10 U
NS-35
4.2 U
4.2 U
5 U5 U
1.6 U
1 U
10 U
NS-36
NS
NS5 U5 U
1.6 U
1 U
10 U
NS-37
NS
NSS V5 U
1.6 U
NS
10 U
NS-38NS
5.8
5 U5 U
1.6 U
1.4 B
10 U
NS-39NS
NS
5 UNS
1.6 U
NS
10 U
NS-404.2 U
4.2 U
5 UNS
1.6 U
NS
10 U
NS-41
NS
NS
5 UNS
1.6 U
NS
10 U
NS-42
4.2 U
4.2 U
5 U
NS
1.6 U
NS
10 U
NS^»3
NS
4.2 U
5 U
5 U
1.6 U
NS10 U
Quarter
2Q98
3Q98
3(J99
IQO O
3QO O
IQ0 1
100 2
NS-44
NS
NS
5 U
5 U
1.6 U
NS10 U
NS-45
4.2 U
4.2 U
5 U
NS
1.6 U
NS10 U
NS-46
4.2 U
4.2 U
5 U
NS
1.6 U
NS10 U
NS-47
4.2 U
4.2 U
5 U
NS
1.6 U
NS
10 U
NS-48
4.2 U
4.2 U
5 U
NS
1.6 U
NS10 U
NS-49
4.2 U
4.2 U
5 U
5 U
1.6 U
I U
13 U
NS-50
4.2 U
4.2 U
5 U
NS1.6 U
2 B10 U
NS-51
4.2 U
4.2 U
5 U
5 U
1.6 U
NS10 U
NS-52
4.2 U
4.2 U
5 U
NS
1.6 U
NS
10 U
NS-53
4.2 U
4.2 U
5 U
NS
1.6 U
NS
10 U
NS-54
4.2 U
4.2 U
5 U
NS
1.6 U
1 U
10 U
CT-I
NS
NS
5 U
5 U
1.6 U
3.2 B
10 U
NOTES:
Unit s in ug/l
ROD Performanc e Standard: 6 ug/L
NS - Not Sampled
U - No t detected at indicate d concentratio n
B (Inorganics ) - Estimate d concentratio n is less tha n the reportin g limi t
Pag e 1 of 5
Tabl e 3-1 5
Historica l Analytica l Result s - Metal s
OU 3 Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
CHROMIU M
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O1Q011Q02
NS-1 3
9.8 J
NS2 UNS
50.5
NS72.6
NS-1 4
NSNS
4.4
NS
7.8 B
NS
NS
NS-2 4
NS
NS
2 U
2 U
0.7 U
0.9 U
1.5 B
NS-35
13
7.3 J
2 U
2 U
0.7 U
3.1 B
4.5 B
NS-36
NS
NS
2 U
2 U
0.7 U
1.2 B2.6 B
NS-3 7
NS
NS
240
38
7.4 B
5.7 B30
MS-38
NS
8 J
2 U
2.5
4.7 B
9.1 B
9.1
NS-39
NS
NS
2 U
NS
4.9 U
NS
7.2
NS-40
6.6 J
4 U
2 U
NS
0.96 BNS2.2 B
NS-4 1
NS
NS
25
NS
8.2 BNS122
NS-42
5.2 J
4 U
26 U
NS
4.9 U
NS32.4
NS-43
NS
10.4
14
13
2.4 B4.3 B4.1 B
Quarter
2Q98
3Q983Q99
1QO O
3QO O1Q01
100 2
NS^U
NSNS3.8
2.6
1.3 B2.9 B3 B
NS-45
10.8
4 U
2 U
NS
0.7 U
NS
1.3 B
NS-46
4 U
4 U
2 UNS
0.7 U
NS
5 U
NS-47
10.2
4 U
2 U
NS
0.7 U
NS5 U
NS-48
4 U
4 U
2 UNS
0.7 U
NS
2 B
NS-49
4 U
4.9 J
2 U
2 U
4.9 U
3.1 B1.6 B
NS-50
4 U
4 U
2 U
NS
1.4 B
1.3 B2.4 B
NS-5 1
4 U
4 U
2 U
2 U
0.89 B
NS1.6 B
NS-52
4.5 J
4 U
3.9
NS
0.7 U
NS1.1 B
NS-53
4 U
4 U
2 UNS
0.7 U
NS
1.1 B
NS-54
4 U
4 U
2 U
NS
0.7 U
3.1 B1.5 B
CT-1
NS
NS
2 U
2 U
0.7 U0.99 B
5 U
NOTES:
Unit s in ug/1
ROD Performanc e Standard: 50 ug/L
NS - Not SampledU - No t detecte d at indicate d concentratio n
B (Inorganics ) - Estimate d concentratio n is less than the reportin g limi t
J (Inorganics ) - Compoun d detecte d in associate d metho d blan k
Bol d fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Pag e 2 of 5
Table 3-15
Historica l Analytica l Result s - Metal s
OU 3 Extractio n and Monitorin g Well s
Nationa l Starc h and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , North Carolin a
MANGANES E
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O
1Q0 1
1Q0 2
NS-1 3
240
NS
2900
NS
2060
NS
157
NS-1 4
NS
NS
8.2
NS
80
NS
NS
NS-2 4
NS
NS
7600
4900
48804820 E .
3200 J
NS-35
780
928
360053006730
9730 . E
1110 0
NS-36
NS
NS
120 0
130 0
185 0
2290 E
2600
NS-37
NS
NS
490150
91.5
: 14 2 E
128 0 J
NS-38
NS
15000
27000
22000
2950036400 . E
34700 J
NS-39
NSNS
170
NS
97.6
NS
174 J
NS^J O
13500
1010 0
14000
NS
9600
NS
7360 J
NS-4 1
NS
NS
2300
NS
2420NS1830 J
NS-42
1800
411 0
8200
NS
14900
NS
12800 J
NS-43
NS
17.3
76
7528
13 B E
5.2 B
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O
1Q0 11Q02
NS-44
NSNS
8.5
5 U
11.9 B
,1.8 B E
15 U
NS-45
3790
3220
4500
NS
5240
NS
4570
NS^»6
80
117
190
NS
69.7
NS
189
NS^»7
1500
808
110 0
NS
1490
NS
1810
NS-48
68404100
4900
NS
7540
NS
5830
NS-49
9870
6440
7000
8600
8180
7270 E
5870
NS-50
10600
10700
6900
NS
4860
3620 E
2680 J
NS-51
5590
4040
12000
3500
3400
NS
3460
NS-52
584
561
360
NS
4280
NS
1070 J
NS-53
4760
3320
840
NS
960
NS
411 J
NS-54
1540
1160
4000
NS
3610
4320 E
4520
CT-1
NS
NS
2500
320
606
101 0 E
163
NOTES :
Unit s in ug/1
RO D Performanc e Standard : 50 ug/L
NS - Not Sample dU - No t detected at indicate d concentratio n
B (Inorganics ) - Estimate d concentratio n is less tha n the reportin g limi t
E - Estimate d concentratio n exceeds the calibratio n range
J (Inorganics ) - Compoun d detected in associated metho d blan k
Bold fon t indicate s detected concentratio n greate r tha n RO D Performanc e Standar dShading indicate s "E " qualifie d concentratio n fo r whic h a dilute d run concentratio n is unavailable .
Pag e 3 of 5
Table 3-15
Historica l Analytica l Result s - Metal s
OU 3 Extractio n and Monitorin g Well sNational Starch and Chemica l Compan y
Cedar Spring s Plan t Site
Salisbury , Nort h Carolin a
THALLIU M
Quarter
2Q98
3Q98
3Q99
1QO O
3QO O
1Q0 1
1Q0 2
NS-1 33.3 V
NS
2 U
NS1.3 UN W
NS
10 U
NS-14
NS
NS
2 U
NS
1.3 U NNSNS
NS-2 4
NS
NS
2 U
2 U
1.3 UN W
1.7 U
10 U
NS-35
5.7 J
3.3 U2 U
2 U
1.3 U1.7 U
20 U
NS-36
NS
N S
2 U
2 U
1.3 U W
1.7 U
10 U
NS-37
NS
NS
2 U
2 U
1.3 U NNS
10 U
NS-38
NS
20.2
2 U
2 U
1.3 UN W
1.7 U W50 U
NS-39
NS
NS
2 U
NS
1.3 U W
NS10 U
NS-40
6.8 J
10.7
2 U
NS
1.3 U
NS
10 U
NS-4 1
NS
NS
2 U
NS
1.3 U N
NS
10 U
NS-42
3.3 U
3.3 U2 U
NS
1.3 U W
NS
20 U
NS-43
NS
3.3 U2 U
2 U
1.3 U N
NS
10 U
Quarter
2Q98
3Q98
3Q99
IQO O
3QO O1Q01
1Q0 2
NS-44
NS
NS
2 U
2 U
1.3 U N
NS
10 U
NS-45
4.1 J
3.3 U
2 U
NS
1.3 UN W
NS
10 U
NS-46
3.7 J
3.3 U2 U
NS
1.3 U N
NS
10 U
NS-47
5.6 J3.3 U2 U
NS
1.3 UNS
10 U
NS-48
5.2 J3.3 U2 U
NS
1.3 UN W
NS
10 U
NS-49
6.3 J
6.1 J
2 U
2 U
1.3 U1.7 U W
10 U
NS-50
5.8 J
9.7 J
2 U
NS
1.3 U1.7 U W
10 U
NS-51
6.7 J
4.6 J
2 U
2 U
1.3 UN W
NS
10 U
NS-52
3.3 U
3.3 U2 U
NS
1.3 U W
NS
10 U
NS-53
3.8 J3.3 U
2 U
NS
1.3 UNS
10 U
NS-54
3.4 J3.3 V
2 U
NS
1.3 U1.7 U
10 U
CT-1
NS
NS
2 U
2 U
1.3 U
40.310 U
NOTES:
Unit s in ug/1
ROD Performanc e Standard: 2 ug/L
NS - Not Sampled
U - Not detected at indicate d concentratio n
N - Spike d sample recovery is not withi n contro l limit s
W - Post digestio n spike is out of contro l limit s
J (Inorganics ) - Compoun d detecte d in associated metho d blan k
Bol d fon t indicate s detected concentratio n greater than RO D Performanc e Standar d
Itali c fon t indicates detection limi t greater than ROD Performanc e Standard
Pag e 4 of 5
Table 3-1 5
Historica l Analytica l Result s - Metal s
OU3 Extractio n and Monitorin g Well s
Nationa l Starch and Chemica l Compan y
Cedar Springs Plan t Site
Salisbury , Nort h Carolin a
ZINC
Quarter
2Q98
3Q9 8
3Q99
IQO O
3QO O
IQ0 1
1Q0 2
NS-1 3
5 U
NS
16
NS
1.7 B
NS
7.6 B
NS-1 4
NS
NS16
NS
137
NS
NS
NS-24
NS
NS
88
10 U
1.6 U
31
10.1 B
NS-35
5.1 J
9.2 J
17
10 U
7.8 B
24.1
20 U
NS-36
NS
NS
17
10 U
1.6 U8.6 U
7.8 B
NS-37
NS
NS
66
10 U
21.624.1
5 B
NS-38
NS
7.5 J
14
10 U
31.9
21.2
20 U
NS-39
NS
NS
16
NS
1.6 U
NS
20 U
NS-40
5 U
5 U
16
NS
1.6 U
NS
20 U
NS-4 1
NS
NS
26
NS
3.9 B
NS
8.9 B
NS^»2
180
15.5 J
40
NS
4.4 B
NS
20.3
NS-43
NS
5 U
17
10 U
1.6 U
8.6 U
20 U
Quarter
2Q98
3Q98
3Q99
IQO O
3QO O
IQO I1Q02
NS-44
NSNS
12
10 U
1.6 U10.6 B20 U
NS-45
9.4 J
9.7 J
16
NS
1.6 U
NS7.6 B
NS-46
21.7
5 U
14
NS
1.9 B
NS20 U
N&47
35.8
5 U
17
NS
1.6 UNS9.9 B
NS-48
5 U
5 U
18
NS
1.6 U
NS20 U
NS-49
5 U
5 U
14
41
76.9
37.547.9
NS-50
14.2 J
5 U
16
NS
1.6 U
4620 U
NS-5 1
130
5 U
14
84
1390
NS41.8
NS-52
5 U
5 U
28
NS
6.2 B
NS20 U
NS-53
9.3 J
5 U
20
NS
1.6 UNS31.9
NS-S 4
587
474
3400
NS
129 0
154
248
CT-1
NS
NS
27
3815.7 B
1.7 U
22.7
NOTES:
Units in ug/l
ROD Performanc e Standard : 2,10 0 ug/L
NS - Not Sampled
U - Not detected at indicate d concentratio n
B (Inorganics ) - Estimated concentration is less than the reportin g limi t
J (Inorganics ) - Compound detected in associated method blankBold fon t indicate s detecte d concentratio n greate r tha n RO D Performanc e Standar d
Pag e 5 of 5
Tabl e 3-16
Compariso n of RCR A Analytica l Result s to Clas s GA Groundwate r Standard s
Jul y 200 1
Nationa l Starc h and Chemica l Compan y
Salisbury , Nort h Carolin a
Wel l ID
Laborator y ID
Sampl e Dat e
Dilutio n Facto r
VOC s
1,1,2-Trichloroethan e
1 ,2-Dichloroethan e
1 ,2-Dichloropropan e
2-Butanon e
Aceton e
Bromodichloromcthan c
Carbo n Disulfid e
Chlorocthan e
Chlorofor m
cis-1 ,2-Dichloroethen e
Dibromochloromethan e
Ethylbenzen e
Methylen e Chloride
Tetrachloroethen e
Toluen e
trans - 1 ,2-Dichloroethen e
Trichloroethen e
Viny l Chloride
Xylen e
SVOC s
Dilutio n Facto r
Bis(2-chloroethyl)ethe r
Di-n-bury l phthalat c
Bis(2-ethylhexyl)phthalat e
Di-n-octy l phthalat e
Pesticid e
Dilutio n Factor
delta-BH C
Metal s
Dilutio n Facto r
Antimon y
Arseni c
Bariu m
Berylliu m
Chromiu m
Cobal t
Coppe r
Lead
Manganes eNickel
Seleniu m
Thalliu m
Vanadiu m
Zin c
Mercur y
Clas s G A
Groundwate r
Standard s
NS
0.3 8
0.5 6
NS
700
NS
NS
NS
0.1 9
70
NS
29
5
0.7
1,00 0
70
2.8
0.01 5
530
NS
NS
700
14 0
NS
NS
50
2,000
NS
50
NS
1,00 0
15
50
100
50
NS
NS
2,10 0
1.1
NS-33
200987-2
07/26/0 1
1
0.4 U
0.3 U
0.3 U
0.9 U
1.0 U
0.3 U
0.3 U
0.3 U
0.3 U
0.3 U0.3 U
0.3 U
0.5 U
0.5 U
0.3 U
0.3 U
0.3 U
0.4 U
0.5 U
1
2.0 U
4.0 U
2.0 U
3.0 U
1
0.01 1 U
1
1.4 U
1.7 U
23.5 B
0.087 U
6.6 B
4.2 U
1.7 B
1.6 U
19.1
8.4 B
2.3 U
3.8 U
20.2 B
28.2 B
0.08 1 B
NS-3 9
200987-5
07/26/0 1
1
1.0
31
2
0.9 U
1.0 U
0.3 U
0.3 U
0.3 U
0.7 J
0.3 U
0.5 U
0.3 U
10
0.8 J
0.3 U
0.3 U
1.0
14
0.5 U
1
9.0 J
4.0 U
2.0 U
3.0 U
1
0.01 1 U
1
2.7 B
1.7 U
39.9 B
0.087 U
5.7 B
4.2 U
1.4 U
1.6 U
122
2.9 B
2.3 U
3.8 U
19.5 B
45.5
0.044 B
NS-42
200987-3
07/26/01
5
2.0 U
680
2.0 U
4 U
56
2.0 U
2.0 U
40
2.0 U
30
2.0 U
2.0 U
10
2.0 U
1 1
2.0 U
11
37
6.0
1
2.0 U
•••'4.0 U
2.0 U
3.0 U
1
0.01 1 U
1
2.3 B
1.7 U
94.2 B
0.087 U
3.0 B
22.6 B
3.1 B
1.6 U
8,700
19.7
2.3 U
4.6 B
3.4 U
17.2 U
0.06 1 B
NS-90
200987-6
07/26/0 1
5
2.0 U
790
2.0 U
4.0 U
32 B
2.0 U
2.0 U
38
2.0 U
29
2.0 U
2.0 U
10 B
2.0 U
13
2.0 U
11
38
7
1
2.0 U
4.0 U
2.0 U
3.0 U
1
0.01 1 U
1
1.4 U
1.7 U
96.4 B
0.087 U
5.0 B
23.2 B
3.4 B
1.6 U
8,900
22.7
2.3 U
6.2 B
3.4 U
101
0.052 B
NS-49
200987-4
07/26/01
50
20 U
7,900
15 U
45 U
130
15 U
15 J B
15 U
15 U
15 U
15 U
15 U
25 U
25 U
15 U
15 U
15 U
20 U
25 U
1
9.0 J
4.0 U
2.0 U
3.0 U
1
0.01 1 U
1
1.4 U
1.7 U
52.3 B
0.087 U
1.3 B
20.3 B
1.4 U
1.6 U
6,480
5.7 B
2.3 U
3.8 U
3.4 U
68.8
1.1
NOTES :
Unit s in ug/1
NS-9 0 is a duplicat e sampl e of NS-42 .
N S - N o standar d exist s fo r thi s constituen t
NA - The sampl e was no t analyze d for thi s constituen t
U - Not detecte d at indicate d concentratio n
J (Organics ) - Estimate d concentratio n is less tha n th e reportin g limi t
B (Organics ) - Compoun d detecte d in associate d metho d blan k
B (Inorganics ) - Estimate d concentratio n is less tha n the reportin g limi t
Table 3-17
Compariso n of RCR A Analytica l Result s to Class GA Groundwate r Standard s
Februar y 2002
Nationa l Starc h and Chemical Compan y
Salisbury , Nort h Carolin a
Wel l ID
Laborator y ID
Sample Date
Dilutio n Facto r
VOCs
AcetoneBromodichloromethan e2-Butanon eCarbon Disulfid eDibromochloromethan e
Chloroethan e
Chloroform
1,2-Dichloroethanecis- 1 ,2-Dichloroethen etrans- 1 ,2-Dichloroethen e
1,2-Dichloroethen e
1 ,2-Dichloropropan e
Ethylbenzen eMcthylene ChlorideTetrachloroetheneToluene1,1,2-Trichloroethen e
Trichloroethen e
Viny l Chlorid e
Xvlene
SVOCs
Dilutio n FactorBis(2-chloroethyl)etbe rBis(2-ethylhexyl)phthalat e
Di-n-buty l phmalat c
Di-n-octv l phthalat e
Metals
Dilution Factor
Antimon y
Arsenic
Barium
Berylliu m
Chromiu m
Cobalt
Copper
Lead
Manganes e
Nickel
Seleniu m
Thalliu mVanadiumZinc
Mercurv
Class GA
Groundwate r
Standards
700
NSNS
NSNSNS0.1 90.387070
NA
O.S 6
295
0.7
1,000
NS
2.8
0.015
530
NS
NS
700
140
NS
50
2,000
NS
50
NS
1.000
15
50
100
50
NSNS2,10 0
1.1
NS-33
C2B080259001
02/07/0 2
10 U1.0 U5.0 U
1.0 U1.0 U2.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 Ui.o u
1.0 U2.0 U
1.0 U
1.0 U
1.0 U
1.0 U
2.0 U
3.0 U
110 u10 U
10 U
10 U
1
4.1 U
2.02 U
22.3 B
0.73 B
3.8 B0.8 4 U2.5 U1.8 U
3.1 B
6.1 B
3.2 U
5.7 U
21.3 B
3.7 U
0.093 U
NS-39
C2B080259 004
02/07/021
10 U1.0 U5.0 U
1.0 U1.0 U
0.9 2 J
0.64 J
41 E
1.0 U
1.0 Ui.o u
1.7
1.0 U
13
I.Si.o u
1.8
1.4
9.5
3.0 U
1
13
10 U
10 U
10 U
1
5.1 B
2.2 U
44.1 B
0.7 2 B
4.4 B
0.84 U
2.5 U
1.8 U
211
2.4 U
3.2 U
5.7 U
20.5 B8.4 B
0.13 B
NS-39-R E 1C2B080259 004
02/07/02
2
20 U
2.0 U10 U
2.0 U
2.0 U
4.0 U
0.53
42
2.0 U
2.0 U
2.0 U
1.5 J
2.0 U11
1.0 J
2.0 U
1.6 J
1.1 J
7.2
6.0 U
NA
NA
NANA
NA
NANA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NANA
NA
NS-4 2C2B080259 002
02/07/02
10
100 U
10 U50 U
10 U
10 U
17 J
10 U
310
22
10 U
23
10 U
10 U
20 U
10 U
5.0 J
10 U
8.9 J
45
30 U
1
2.1 J
10 U
10 U
10 U
1
4.7 B
2.2 U
123 B
0.5 7 B
24.936.5 B47.81.8 U
13,200 •
34.1 B
3.6 B
5.7 U
13.2 B12.4 B0.098 B
DUP-9 0C2B080259 005
02/07/0 2
10
100 U
10 U
50 U
10 U
10 U
19 J
10 U
340
25
10 U
25
10 U
10 U20 U
10 U
5.2 J
10 U
10
51
11 J
1
1.9 J
11 U
II U
II U
1
4.1 U
2.2 U
107 B
0.5 8 B
4.8 B24.4 B
5.6 B
2.5 B
13,000 *
16.5 B
4.0 B
5.7 U
5.4 B5.5 B
0.093 U
NS-49
C2B080259 003
02/07/02250
2500 U
250 U1200 U
250 U
250 U
500 U
250 U
5,700250 U
250 U
250 U
250 U
250 U
500 U
250 U
250 U
250 U
250 U
500 U
750 U
1
1410 u
10 U
10 U
1
4.1 U
2.2 U47.4 B
0.7 3 B
1.5 B20 B2.5 U3.1
6,2704.8 B
3.2 U
5.7 U
1.8 B
44.6
0.093 U
NS-49-RE 1
C2B080259 003
02/07/02
1
10 U
1.0 U
5.0 U
I.O UI.O U
5.9
1.9
2,900 E
0.69 J
1.0 U
0.7 1 J
2^4
1.0 U
4.8
3.0
5.1
3.9
5.0
18
1.2 J
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NANA
NA
NOTES:
Unit s in ug/1
• Sampl e dilute d at a facto r of 2 for this compound .DUP-9 0 is a duplicat e sample of NS-42 .
NS - No standard exists for this constituen tNA - The sample was not analyze d for this constituen t
U - Not detected at indicated concentration
£ - Estimated concentration exceeds the calibration rangeJ (Organic:) - Estimate d concentratio n is less dun the reportin g limi t
B (Inorganics ) - Estimate d concentratio n is les s tha n the reportin g limi t
3.2u.
SOURCES:
ROWAN MILLS, CHINA GROVE,
NORTH CAROLINA7.5 MINUTE QUADRANGLE
CONTOUR INTERVAL = 10 FEET
2000'2000'
• N.C.
Approximate Scale: 1" = 2000'
QUADRANGL E LOCATION UTM GRID AND 1987 MAGNETIC NORTH
DECLINATIO N AT CENTE R OF SHEE T
08/02/01 CRA-54-TLF
05007001/05007B06.<xir
NATIONAL STARCH AND CHEMICAL COMPANY
CEDAR SPRINGS ROAD PLANT
SALISBURY, NORTH CAROLINA
2001 SITE MONITORING REPORT
SITE LOCATION MAP
BBI BLASLAND , BOUCK & LEE, INC.
engineers & scientists
FIGURE
1-1
\
LEGEND
• MONITORING WELL LOCATION
•$- EXTRACTIO N WEL L LOCATIO N
A SURFAC E WATER/SEDIMEN T SAMPLE LOCATION
SOURCES:
- MAP ENTITLE D 'SITE MAP' PREPARE D FOR NATIONAL STARC HAND CHEMICA L COMPAN Y BY INTERNATIONA L TECHNOLOG YCORPORATION. KNOXVILLE . TENN.. DATE D 5/18/93.
- MONITORIN G WEa SURVE Y BY SCHULENBERGE R SURVEYINGCOMPANY, SALISBURY, N.C.. DATED 1/21/97
- MONITORING WELL SURVEY BY TAYLOR WEISMAN & TAYLOR,RALEIG H N.C., DATE D 3/98
X: NSC01.0WCL OFT-REFP: PAGESET/PLT-DL8/02/02 CSA-54-IY. TIF05007001/05007B01.0WG
NATIONAL STARC H AND CHEMICAL COMPAN YCEDAR SPRIN G ROA D PLANT, SALISBURY, NORTH CAROLIN A2001 SIT E MONITORIN G REPOR T
SITE MAP
BBCBLAStANP. flOUC K ft LEE . INC.• nginmon B icluntlttt
FIGURE
1-2
v \xf//
LEGEND
• MONITORIN G WEL L LOCATIO N
•$• EXTRACTIO N WELL LOCATION
A SURFAC E WATER/SEDIMEN T SAMPL E LOCATION
!fr STREA M GAUG E LOCATIO N
(747.17) GROUNDWATER ELEVATION
GROUNDWATE R ELEVATIO N CONTOU R
~-——"" (DASHE D WHER E INFERRED)
SOURCES :
- MAP ENTITLE D "SITE MAP' PREPARE D FOR NATIONA L STARC HAND CHEMICAL COMPANY BY INTERNATIONAL TECHNOLOGYCORPORATION. KNOXVILLE , TENN., DATE D 5/18/93.
- MONITORIN G WELL SURVE Y BY SCHULENBERGE R SURVEYINGCOMPANY, SALISBURY , N.C.. DATED 1/21/97
- MONITORING WELL SURVEY BY TAYLOR WEISMAN k TAYLOR.RALEIG H NC.. DATED 3/98
X: NSCOV .L: OFF.REF
P: PACESET/PLT-Dl8/02/02 CRA-M-IY.TLF0500700I/05007W1.0WC
NATIONAL STARCH AND CHEMICAL COMPANY
CEDA R SPRING ROA D PLANT , SALISBURY. NORTH CAROLIN A2001 SITE MONITORIN G REPOR T
GROUNDWATER ELEVATION CONTOUR
MAP FOR OU1/OU2 SAPROLITE WELLS
MARCH 2002BBI:
BLASIAND. BOUCK & IEE. INC.engineer* &tcl»ntltti
FIGURE
3-1
\
X: NSCOV-U OFF-REFP: PACESEVPLT-DL.a/02/02 CRA-M-IY. HJ05O07001 /OW07W02.DW;
LEGEND
• MONITORIN G WEL L LOCATION
4- EXTRACTIO N WEL L LOCATIO N
A SURFAC E WATER/SEDIMEN T SAMPL E LOCATIO N
•!B STREA M GAUG E LOCATIO N
(747.68) GROUNDWATE R ELEVATIO N
GROUNDWATE R ELEVATIO N CONTOU R————" (DASHE D WHER E INFERRED)
SOURCES:
MAP ENTITLED "SITE MAP 1 PREPARE D FOR NATIONAL STARC HAND CHEMICAL COMPANY BY INTERNATIONAL TECHNOLOGYCORPORATION, KNOXVILLE , TENN., DATE D 5/18/93.
MONITORIN G WELL SURVE Y BY SCHULENBERGE R SURVEYINGCOMPANY. SALISBURY . N.C.. DATED 1/21/97
MONITORIN G WEL L SURVE Y BY TAYLO R WEISMA N k TAYLOR ,RALEIG H N.C., DATE D 3/98
NATIONA L STARC H AND CHEMICA L COMPAN Y
CEDA R SPRIN G ROA D PLANT . SALISBURY , NORT H CAROLIN A2001 SIT E MONITORIN G REPOR T
GROUNDWATER ELEVATION CONTOUR
MAP FOR OU1/OU2 TRANSITION
ZONE WELLS - MARCH 2002BBe
J
BIASLAMD, BOUCK > LEE . INC.
FIGURE
3-2
LEGEND
• MONITORIN G WELL LOCATIO N
4- EXTRACTIO N WEL L LOCATIO N
A SURFAC E WATER/SEDIMEN T SAMPL E LOCATIO N
•S- STREA M GAUG E LOCATIO N
(747.68) GROUNDWATE R ELEVATIO N
GROUNDWATE R ELEVATIO N CONTOU R
————' (DASHED WHER E INFERRED )
SOURCES:
- MAP ENTITLED 'SITE MAP' PREPARE D FOR NATIONAL STARC HAND CHEMICA L COMPAN Y BY INTERNATIONA L TECHNOLOG YCORPORATION. KNOXVILLE , TENN.. DATE D 5/18/93.
- MONITORIN G WEL L SURVE Y BY SCHULENBERGE R SURVEYINGCOMPANY. SALISBURY. N.C., DATE D 1/21/97
- MONITORIN G WEL L SURVE Y BY TAYLO R WEISMAN & TAYLOR,RALEIG H N.C., DATE D 3/98
X: NSC01U OFF-REFP-. PAGESCT/Pt.T-DL/02/02 CRA-34-IY.TL F05007001 /05007W3.0WC
NATIONA L STARC H AND CHEMICA L COMPAN YCEDAR SPRING ROA D PLANT. SALISBURY. NORTH CAROLIN A2001 SIT E MONITORIN G REPOR T
GROUNDWATER ELEVATION CONTOUR
MAP FOR OU1/OU2 BEDROCK WELLS
MARCH 2002BBC
61ASUWD. BOUCK 4 LEE. INC.• nplnven Aic(«n/fifi
FIGURE
3-3
\ f\ \\ V\ ( \ \\ \
LEGEND
• MONITORIN G WEL L LOCATIO N
4- EXTRACTIO N WELL LOCATION
A SURFAC E WATER/SEDIMEN T SAMPLE LOCATIO N
-!t STREA M GUAG E LOCATIO N
(714.00) GROUNDWATE R ELEVATIO N
GROUNDWATE R ELEVATIO N CONTOU R
^"^ (DASHED WHER E INFERRED)
SOURCES:
- MAP ENTITLE D "SITE MAP' PREPARED FOR NATIONAL STARC HAND CHEMICA L COMPAN Y BY INTERNATIONA L TECHNOLOGYCORPORATION, KNOXVILLE , TENN.. DATED 5/18/93.
- MONITORIN G WELL SURVEY BY SCHULENBERGE R SURVEYINGCOMPANY, SALISBURY. N.C., DATE D 1/21/97
- MONITORIN G WELL SURVE Y BY TAYLO R WEISMAN & TAYLOR ,RALEIGH N.C.. DATED 3/98
NATIONAL STARC H AND CHEMICA L COMPAN Y
CEDA R SPRING ROA D PLANT, SALISBURY. NORTH CAROLINA2001 SIT E MONITORIN G REPOR T
GROUNDWATER ELEVATION CONTOUR MAP
FOR OU3 SAPROLITE AND TRANSITION
ZONE WELLS - MARCH 2002
X:L QfF-REFP: P»CEStT/PlT-OL
8/02/02 CRA-54-IY.TU05007001 /05007WM.OWG
BBC
BLASLAND, BOUCK » LEE. INC.
»nQln»mn »icl»nllitt
FIGURE
3-4
LEGEND
• MONITORIN G WEL L LOCATIO N
4" EXTRACTIO N WEL L LOCATION
A SURFAC E WATER/SEDIMEN T SAMPLE LOCATION
* STREA M GUAG E LOCATIO N
(734.13) GROUNDWATE R ELEVATION
GROUNDWATE R ELEVATIO N CONTOUR
^"^ (DASHED WHER E INFERRED )
SOURCES:
- MAP ENTITLED "SITE MAP 1 PREPARED FOR NATIONAL STARC HAND CHEMICAL COMPANY BY INTERNATIONAL TECHNOLOGYCORPORATION, KNOXVILLE, TENN., DATE D 5/18/93.
- MONITORIN G WEL L SURVE Y BY SCHULENBERGE R SURVEYINGCOMPANY, SALISBURY, N.C.. DATE D 1/21/97
- MONITORING WELL SURVEY BY TAYLOR WEISMAN & TAYLOR,RALEIG H N.C., DATED 3/98
NATIONA L STARC H AND CHEMICA L COMPAN Y
CEDA R SPRING ROA D PLANT. SALISBURY, NORT H CAROLIN A2001 SITE MONITORIN G REPOR T
GROUNDWATER ELEVATION CONTOUR MAP
FOR OU3 BEDROCK WELLS - MARCH 2002
U OFT«REF
P; PAGESET/PLT-DL6/02/02 CRA-54-IY.TLF05007001 /05007W05.DWC
BBC
BIASLAND. BOUCK & LEE. IMC.
FIGURE
3-5
Appendix A
1111111111111111111
BLASLAND BOUCK & LKB
Client Sample ID: EX -01
GC/MS Volatiles
Lot-Sample #...: C2C160138-005 Work Order ft . . . EWHDWiaa
Date Sampled. . . : 03/15/02
Prep Date.... ..: 03/18/02
Prep Batch #...: 2077420
Dilution Factor: 1
Analyst ID. . . . . : 034635
PARAMETER
Aceton e
Benzen e
Bromodichloromethan e
Chlorofor m
1 , 2-Dichloro«than e
1, 1-Dichloroethen e
1 , 2 -Dichloropropan eEthylbenzene
Methyl ene chloride
Toluen e
1, 1,2-Trichloroethan e
Trichloroethene
Vinyl chloride
Xylene s (total)
SURROGATE
Toluene-d 8
l,2-Dichloroethane-d 4
4 -Bromo f luorobenzene
Dibromofluorome thane
Date Received . .
Analysis Date . .
Analysis Time. .initial Wgt/Vo lInstrument ID. .
Method. ... . -
RESULT
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
93
93
80
104
03/16/02
03/18/02
14:59
5 mL
Matrix. . • WJVTW D
MS RUD * - - - - . - -• 5>mT»oe
Final Wgt/Vol..: 5 mL
HP5
SH846 8260B
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0i . o ,-<;'
2.0
3.0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITSug/L
ug/L
ug/L
ug/L
ug/L
ug/Lug/L
ug/L
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
MDL
2.5
0.40
0.30
0.49
0.49
0.51
0.46
0.49
0.36
0.22
0.44
0.39
0.60
0.96
1 P.
111111111111111111
\
Lot -Sample «...: C2C160138-001
Date Sampled. ..: 03/15/02
Prep Date. .....: 03/18/02
Prep Batch #...: 207742 0
Dilution Factor; 1
Analyst ID.....: 034635
PARAMETER
Acetone
Benzene
Bromodichlorome thane
Chlorofor m
1 , 2 -Dichloroethan e
1, 1-Dichloroethene
1 , 2 -Dichloropropan e
Kthylbenzene
Methylen e chlorideToluene
1, 1, 2-Trichloroethane
Trichloroethen e
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene -d8
1 , 2 -Dichloroethane-d 4
4 -Bromo f luorobenzene
Dibromofluoromethane
NOTE(S) :
BLASLAND BOUCK & LEE
Client Sample ID: EX-02
GC/MS Volatiles
Work Order #. . .
Date Received. .
Analysis Date..
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
1.4
ND
ND
ND
ND
ND
33
ND
310 E
ND
ND
ND
130 E
PERCENT
RECOVERY
85
86
113
99
EWHC61AA
03/16/02
03/18/02
16:44
5 mL
HP5
Matrix
MS Run
• PJR'I*UP
*.......: 2077285
Final Hgt/Vo l . . : 5 mL
SW846 8260B
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1 . 0 ....
2.0
3.0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITSug/L
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
ug/Lug/L
ug/Lug/L
ug/L
ug/L
ug/L
MDL
2.5
0.40
0.30
0.49
0.49
0.51
0.46
0.49
0.36
0.22
0.44
0.39
0.60
0 . 96
E Estimate d result . Resut l concentratio n exceed s th e calibraiio n range .
I
STT. Pi 13
1111111111111111111
Lot-Sample #...: C2C160138-001
Date Sampled. . . : 03/15/02
Prep Date. .....: 03/18/02
Prep Batch #...: 2077420
Dilution Factor: 15
Analyst ID. . . . . : 034635
PARAMETER
Acetone
Benzen e
Bromodichlorome thane
Chlorofor m
1 , 2 -Dichloroethan e
1, 1-Dichloroethen e
1 , 2 -Dichloropropane
Ethyl-benzene
Methylen e chlorid e
Toluene
1,1,2 -Trichloroethane
Trichloroethen e
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene-d8
1 , 2-Dichloroethane-d4
4 -Bromof luorobenzene
Dibromof luoromethane
NOTB(S) :
I Esiimitc d rciutl . Resul t i s les s tlia n RL .
BLASLAND BOUCK J
Client Sampl e ID
GC/MS Volati!
work Order *. . .Date Received. .
Anal vw? f t Ttit~AAUA.l.jrEfXD JJai*G • •
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
100 J
ND
ND
ND
ND
ND
ND
20
ND
380
ND
ND
ND
83
PERCENT
RECOVERY
81
99
102
105
& LEE
: EX-02
Le s
EWHC62AA
03/16/02
03/18/02
21:58
5 mL
WD<^TlJr J
SW846 82601
REPORTING
LIMIT
150
15
15
15
15
15
15
15
30
15
15
15
30
45
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Matrix.........: WATE R
MS Run #.......: 2077285
Final Wgt/Vol.. : 5 mL
3
UNITS MDL
ug/L 38
ug/L 6.0
ug/L 4 . 6
ug/L 7 . 3
ug/L 7 . 3
ug/L 7 . 7
ug/L 6 . 9
ug/L 7.3
ug/L 5.4
ug/L 3.4
ug/L 6 . 5
ug/L 5 . 9
ug/L 9-0
ug/L 1 4
CTT. D -! H- eKi i •\ A.
1111111111111111111
Lot-Sample #...: C2C160138
Date Sampled. . . : 03/15/02
Prep Date. .....: 03/18/02
Prep Batch #...: 2077420
Dilution Factor: 15
Analyst ID.....: 034635
PARAMETER
Acetone
Benzen e
Bromodichloromethane
Chloroform
1 , 2 -Dichloro e than e
1, 1-Dichloroethene
1, 2-Dichloropropan e
Ethylbenzene
Methylen e chlorid e
Toluene
1,1 , 2 -Trichloroethan e
Trichloroethen e
Vinyl chlorid e
Xylenes (total)
SURROGATE
Toluene-d 8
1 , 2 -Dichloroethane-d4
4 -Bromof luorobenzeneDibromof luoromethan e
NOTB(S) :
1 Estimate d result . Resul t i s le u tha n RL .
BLASLAND BOUCK
Client Sample ID:
GC/HS Volat
-00 6 Work Order #...
Date Received. .
Ana 1 VR i a T^sk f * ^«Uia^JfOXE» UClUC • •
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT96 a
ND
ND
ND
ND
ND
ND
24
ND
480
ND
ND
ND
97
PERCENT
RECOVERY
94
97
103
104
& LEE
DOP-031502
iles
EWHD21AA
03/16/02
03/18/02
22:23
5 mL
HP 5
SW846 82601
REPORTING
LIMIT
150
15
15
15
15
15
15
15
30
15
15
15 .•;•:'
30
45
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Mat-T-i v - WJVTTZT J
MS Run #.......: 2077285
Final Wgt/Vo l . . : 5 mL
3
UNITS MDL
ug/L 3 8
ug/L 6 . 0
ug/L 4.6
ug/L 7 . 3
ug/L 7 . 3
ug/L 7.7
ug/L 6 . 9
ug/L 7 . 3
ug/L 5.4
ug/L 3 . 4
ug/L 6.5
ug/L 5 . 9
ug/L 9 . 0
ug/L 14
I-TTIT -nJ 1 Q
1111111111111111111
Lot-Sample*... C2C160138-004
Date Sampled . . . 03/15/0 2
Prep Date. ..... 03/18/02
Prep Batch #... 2077420Dilution Factor 1
Analyst ID. .... 034635
PARAMETER
Acetone
Benzene
Bromodichloromethan e
Chloroform
1, 2-Dich l oroethane
1, 1-Dichloroethene
1, 2-Dichloropropan e
Ethylbenzene
Methylene chloride
Toluene
1, 1,2-Trichloroethane
Trichloroethen e
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d44-Bromof luorobenzeneDibromofluoromethane
NOTB(S) :
J Estimate d result . Resul t i t tei s tha n RL .
BLASLAND BOUCK I
Client Sample ID
GC/MS Volati:
Work Order ft . . .
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
39
0.61 J
ND
ND
0.96 J
ND
ND
7.3
ND
7.5
ND
ND
ND
12
PERCENT
RECOVERY
97
97
107
109
i LEE
: EX-03
Les
TSWITHD 1 TV TVEiVinJJKlAA
03/16/02
03/18/02
21:34
5 mL
HP5
SW846 82601
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1 . 0 ..,;:
2.0
3.0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Mat-rlil^dl • i JLj
MS Rux
Final
3
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/Lug/L
ug/L
ug/Lug/L
1 C * WA.TRP
i #.......: 2077285
Wgt/Vol. . s 5 mL
MDL
2.5
0.40
0.3 0
0.4 9
0.49
0.5 1
0.46
0.49
0.36
0.22
0.44
0.39
0.60
0.96
17
1111111111111111111
Lot-Sample #... C2C160138-O I
Date Sampled. .. 03/15/02
Prep Date. ..... 03/18/02
Prep Batch «... 2077420
Dilution Factor 1
Analyst ID..... 034635
PARAMETER
Acetone
Benzen e
Bromodichloromethane
Chloroform
1 , 2-Dichloroethane
1, 1-Dichloroethen e
1 , 2-Dichloropropane
Ethylbenzene
Methylene chloride
Toluene
1,1 , 2-Trichloroethane
Trichloroethen e
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene -d8
1 , 2 -Dichloroethane-d4
4 - Bromo f luorobenzene
Dibromofluorome thane
NOTE(S) :
J Estimate d rewilt . Resul t i s les s tha n R U
BLASLAND BOUCK & LEE
Client Sample ID: EX- 04
GC/MS Volatiles
3 2 Wor k Order #... EWHDMA A
Date Received. .
Analysis Date. .
Analysis Time . .
Initial Wgt/Vbl
Instrument ID. .
Method. . ... . :
RESULT
ND
ND
ND
ND
0.70 J
ND
ND
ND
ND
0.52 J
ND
ND
ND
ND
PERCENT
RECOVERY
78
78
86
95
03/16/02
03/18/02
18:19
5 mL
Matrix • WATER
MS Run a.--.-.-; 2m79ai ;
Final Wgt/Vol . . : 5 mL
HP5
SW846 8260B
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0i.o _.,-.
2.0
3.0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
MDL
2.5
0.40
0.30
0.49
0.49
0.5 1
0.46
0.49
0.36
0.22
0.44
0.39
0.60
0.96
n-i *-)-£,VYIIT-rrh
IIIIIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Client Sample ID: NS-29
GC/MS Volatiles
Lot-Sampl e #...: C2C200151-007 Work Order #...: EWMN11AA
Date Sampled...: 03/19/02
Pre p Date......: 03/22/02
Prep Batch ft...: 2081189
Dilution Factor: 100
Analys t ID.....: 034635
Date Received..: 03/20/02
Analysi s Date..: 03/22/0 2
Analysis Time..: 17:42
Initial Wgt/Vol : 5 mL
Instrument ID..: HP5
Method.........: SW846 8260B
Matrix...
MS Ru n ft .
WATER
Final Wgt/Vol..: 5 mL
PARAMETER
Acetone
Benzen e
Bromodichlorom e thane
Chlorofor m
1 , 2 -Dichloroethane
1 , 1-Dichloroethen e
1 , 2 -Dichloropropane
Ethylbenzene
Methylen e chlorid e
Toluene
1,1,2 -Trichloroethan e
Trichloroethen e
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene -d8
1 , 2 -Dichloroethan e - d4
4 -Bromof luorobenzene
Dibromo f 1 uorome thane
HOTB(S) :
RESULT
250000 E
ND
ND
ND
ND
ND
ND
140
ND
3300
ND
ND
ND
650
PERCENT
RECOVERY
90
106
90
111
REPORTING
LIMIT
1000
100
100
100
100
100
100
100
200
100
100
100 /
20 0 '.-'"
300
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/Lug/L
MDL
250
40
30
49
49
51
46
49
36
22
44
39
60
96
E Estimate d result . Resul t concentratio n exceed s th e calibratio n range .
STL Pittsburgh 1 O79
1111111111111111111
BLASLAND BOUCK & T.l?B
Client Sample ID: MS -29
GC/MS Volatiles
Lot -Sample ft . ..: C2C200151-007
Date Sampled. ..: 03/19/02
Prep Date. .....: 03/25/02
Prep Batch #...-. 2084404
Dilution Factor: 5000
Analyst ID.....: 034635
PARAMETER
Acetone
Benzene
Bromodichlorotnethan e
Chlorofor m
1, 2-Dichloroethane
1, 1-Dichloroethen e
1, 2-Dichloropropane
Ethylbenzen e
Methylen e chloride
Toluene
1,1 , 2 -Trichloroethane
Trichloroethene
Viny l chlorid e
Xylenes (total )
SURROGATE
Toluene -d8
l,2-Dichloroethane-d 4
4-Bromof luorobenzene
Dibromof luorome thane
NOTB(S) :
] Esiimace d result . Resul t i s les s du n RL .
Work Order «...
Date Received. .
Analysis Date . .
Analysis Tine . .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
220000
ND
ND
ND
ND
ND
ND
ND
ND
2600 J
ND
ND
ND
ND
PERCENT
RECOVERY
95
90
82
92
EWMN12AA Matrix
03/20/02 MS Run
03/25/02
15:18
- W2XTTZD
5 mL Final Wgt/Vol . . : 5 mL
HP5
SW846 8260B
REPORTING
LIMIT UNITS
50000 ug/L
5000 ug/L
5000 ug/L
5000 ug/L
5000 ug/L
5000 ug/L
5000 ug/L
5000 ug/L
10000 ug/L
5000 ug/L
5000 ug/L
5000 ... ug/L
10000: ug/L
15000 ug/L
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
MDL
12000
2000
1500
2400
2400
2600
2300
2400
1800
1100
2200
2000
3000
4800
D i *- f <q>-,, i T-rrh 1089
1111111111111111111
Lot-Saaple #. ...- C2C13 011 9 -00 1
Date Sampled. ..: 03/11/02
Prep Date. ....... 03/14/02
Prep Batch #. . . : 2073113
Dilution Factor: 1
Analyst ID.....: 034635
PARAMETER
Acetone
Benzene
Bromodichloromethan e
Chloroform
1 , 2 -Dichloroethane
1, l-Dichloroethene
1 , 2 -Dichloropropane
Ethylbenzene
Methylene chloride
Toluene
1,1 , 2-Trichloroethane
Trichloroethen e
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene -d8
l,2-Dichloroethane-d4
4-Bromofluorobenzene
Dibromofluoromethane
NOTE (S) :
1 Estimate d rcailc . Resul t i s let s tha n RL .
BLASLAND BOOCK )
Client Sample ID
GC/MS VolatoJ
Work Order #. . .
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
0.46 J
ND
ND
2.8
ND
ND
3.1
ND
2.1
ND
ND
ND
6.3
PERCENT
RECOVERY-
89
93
95
100
i USE
: NS-30
Le s
EWAHN1AA
03/13/02
03/14/02
13:3 7
5 mL
TTD5Jdlr 3
SW846 82601
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0i.o ,-;
2.0
3.0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Matrix
MS Run
Final 1
3
UNITS
ug/L
ug/L
ug/L
ug/L
ug/Lug/L
ug/Lug/Lug/L
ug/Lug/Lug/L
ug/L
ug/L
.........: WATER
i.......: 2073057
»gt/Vol..: 5 mL
MDL
2.5
0.40
0.3 0
0.4 9
0.49
0.5 1
0.4 6
0.49
0.3 6
0.2 2
0.44
0.3 9
0.6 0
0.96
13
1111111111111111111
Lot-Sample #...: C2C200151-006
Date Sampled. ..: 03/19/02
Prep Date. .....: 03/25/0 2
Prep Batch #...: 2084404
Dilution Factor: 50
Analyst ID.....: 034635
PARAMETER
Acetone
Benzene
Bromodichl orome thane
Chloroform
1 , 2-Dichloroetnane
I f 1-Dichloroethen e
1, 2-Dichloropropane
Ethylbenzene
Methylene chloride
Toluene
1, 1,2-Trichloroethan e
Trichloroethene
vinyl chloride
Xylenes (total)
SURROGATE
Toluene -d8
1 , 2 -Dichloroethan e -d 4
4-Bromof luorobenzene
Dibromof luoromethane
KOTE(S) :
J Estimate d result . Resul t i s les s tha n RL .
BLASLAND BOUCK >
Client Sample ID
GC/MS Volati!
Work Order # . . . :
Date Received. . :
Analysis Date . . :
Analysis Time . . :
Initial Wgt/Vol:
Instrument ID . . :
Method. ........:
RESULT
2300
ND
ND
ND
100
ND
200
ND
ND
23 J
ND
ND
ND
ND
PERCENT
RECOVERY
97
97
82
97
& LEE
: NS-31
Les
EWMNM1AA
03/20/02
03/25/02
15:44
5 mL
HP 5
SW846 8260]
REPORTING
LIMIT
500
50
50
50
50
50
50
50
100
50
50
50 .,-;
100
150
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Matrix.
MS Run
Final t
B
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
•ug/L
• bTZVPlTD
#.......:
fgt/Vol. . : 5 mL
MDL
120
20
15
24
24
26
23
24
18
11
22
20
30
48
STL Pittsburcrh 1070
1111111111111111111
BLASLAND BOCOC & LEE
Client Sample ID: NS-32
GC/MS Volatiles
Lot-Sample*...: C2C130119-002
Date Sampled...: 03/11/02
Prep Date. .....: 03/14/02
Prep Batch #...: 2073113
Dilution Factor: 1
Analyst ID. . . . . : 034635
PARAMETER
Acetone
Benzen e
Bromodichloromethan e
Chloroform
1 , 2 -Dichloroethan e
1, l-Dichloroethene
1, 2-Dichloropropan e
Ethylbenzen e
Methylen e chloride
Toluen e
1, 1,2-Trichloroethane
Trichloroethene
Viny l chlorid e
Xylene s (total )
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d4
4-Bromof luorobenzene
Dibromofluorome thane
Work Order #...
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
104
92
82
104
EWAHX1AA
03/13/02
03/14/02
14:1 4
5 mL
MS Run #.......1 2073057
Final Wgt/Vol.,: 5 mL
HP5
SW846 82SOB
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1 . 0 .,,
2.0
3.0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS MDL
ug/L 2 . 5
ug/L 0.40
ug/L 0.30
ug/L 0.49
ug/L 0.49
ug/L 0.51
ug/L 0 . 46
ug/L 0.49
ug/L 0.36
ug/L 0.22
ug/L 0.44
ug/L 0.39
ug/L 0 . 60
ug/L 0.96
14
11
BLASLAND BOUCK & LEE
1
1
1
1
1
1
1
1
1
Client Sample ID: EX-01
GC/HS Semi volatiles
Lot -Sample #... C2C160138-005
Date Sampled.. . 03/15/02
Prep Date.. .... 03/18/02
Prep Batch #... 2077326
Dilution Factor 1
Analyst ED. .... 003200
PARAMETER
bis(2-Chloroethyl) -
ether
4 -Nitropheno l
' —
SURROGATE
Phenol -d 5
2 -Fluorobiphenyl
Ni t robenzene - d5
Terphenyl-dl 4
2-Fluorophenol
2,4 , 6-Tribromopheno l
Work Order # . . .
Date Received. .
Analysis Date. .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVERY
64
70
72
71
69
63
EWHDW1AE Matrix. ........: WATER
03/16/02 MS Run #.......: 2077154
03/19/02
09:20
100 0 mL Final Wtft/Vol..: 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L 1.8
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
II
I
I
I
I
I
I
STT . Pi t-t-shnr-ah 34
111111111111111
BLASLAND B00CK
Client Saropl e ID
& LEE
: EX- 02
GC/MS Semivolatiles
Lot -Sample #... C2C160138-001
Date Sampled. .. 03/15/02
Prep Date. ..... 03/18/02
Prep Batch ft... 2077326
Dilution Factor 1
Analyst ID..... 003200
PARAMETER
bis (2-Chloroethyl) -
ether
4-Nitropheno l
SURROGATE
Phenol -dS
2 - Fluorobipheny l
Nitrobenzene -d5
Terphenyl-dl 4
2 - Fluorophenol
2,4,6 -Tribromophenol
NOTE(S) :
Work Order #. . .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
550 E
ND
PERCENT
RECOVERY
50
53
110
36
86
70
BWHC61AC Matrix. ........: VJATE R
03/16/02 MS Run &.......: 2077154
03/19/02
18:03
1000 mL Final Wgt/Vol..: 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MDL10 ug/L 1.4
50 ug/L 1.8
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - ,122)
E Ettlnutc d result . Resul t concentratio n exceed s (h e calibratio n range .
C"TIT -/-rV,28
1111
BLASLAND BOUCK
Client Sample ID
& LEE
: EX-02
GC/MS Semivolatiles
T.nl--Sanm1«» «. - r">ri Kft l 78- nm MxWm-lr Ovd*>l- it...
riah*» flarnnlpd . . 0^/1^/05 Tlal-*» Beceiired. .
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Prep Date. ..... 03/18/02
Prep Batch #... 2077326
Dilution Factor 15
Analyst ID ..... 003200
PARAMETER
bis (2-Chloroethyl) -
ether
4-Nitropheno l
SURROGATE
Phenol -dS
2 - Fluorobiphenyl
Nitrobenzene-d5
Terphenyl-dl 4
2 -Fluorophenol
2,4,6 -Tribromophenol
Analysis Date..
Analysis Time . .
Initial Wgt/Vol
Instrument ID . .
Method.........
RESULT
730
ND
PERCENT
RECOVERY
68
65
68
38
65
65
EWHC62AC Matrix. ........: WATER
03/16/02 MS Run #.......: 2077154
03/22/02
17:44
100 0 mL Final Wgt/Vol..: 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MDL
150 ug/L 22
750 ug/L 27
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 -.122)
I1111111111111
BLASLAND BOUCK & LEE
Client Sample ID: DOP-031502
GC/MS Setnivolatiles
Lot -Sample ft. .. C2C160138
Date Sampled. . . 03/15/02
Prep Date. ..... 03/18/0 2
Prep Batch #... 2077326
Dilution Factor 1
Analyst ID..... 003200
PARAMETER
bis (2-Chloroethyl) -
ether
4-Nitrophenol
SURROGATE
Phenol -d5
2 - Fluorobiphen y 1
Nitrobenzene-d 5
Terphenyl -d!4
2 - Fluoropheno l2,4 , 6 -Tribromophenol
NOTB(S) :
-006 Work Order ft...
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method... ......
RESULT
560 B
ND
PERCENT
RECOVERY
46
57
110
38
85
72
EWHD21AC Matrix. .......... WATER
03/16/02 MS Run #.......: 2077154
03/19/02
19:04
1000 mL Final Wgt/Vol.. r 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L 1.8
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
E Estimate d result . Resul t concentratio n exceed s th e calibratio n range .
c-mr o-;35
111
•
™ Lot -Sample #... C2C160138-
Date Sampled ... 03/15/021Prep Date. ..... 03/18/02
Prep Batch #... 2077326
Dilution Factor 15
m m Analyst ID. .... 003200
•
PARAMETER
bis (2-Chloroetbyl) -
ether
• 4-Nitropheno l
SURROGATE
• Phenol -d5
• 2-Fluorobipheny l
Nitrobenzene -d5
|
Terphenyl-dl 4
2 - Fluorophenol
2,4 , 6-Tribromophenol
1
1
1
1
1
1
1
1
1
BLASLAND BOUCK & LEE
Client Sample ID: DOT - 031502
GC/HS Semivolatiles
f \ f\ Ct\lsWr\v]r f\^f^^f ft • TTMWnO 0 ^f* Vfcl^T*^ TT • UTV'PI^U
Date Received. . 03/16/02 MS Run #.......: 2077154
Analysis Date.. 03/22/02Analysis Time.. 18:44
Initial Wgt/Vol 100 0 mL Final Wgt/Vol..: 1 mL
Instrument ID. . 731
Method. ........ SW846 8270C
REPORTING
RESULT LIMIT UNITS MDL
750 150 ug/L 22
ND 750 ug/L 27
PERCENT RECOVERY
RECOVERY LIMITS
71 . (1 0 - 113)
69 (3 0 - 110)
70 (3 2 - 112)
41 (10 - 144)
65 (1 3 - 110)
70 (2 1 - 122)
-'
36
11
BLASIAND BOUCK & LEE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Client Sample ID:EX-03
GC/MS Semivolatiles
Lot-Sample # . . . C2C160138-004
Date Sampled. .. 03/15/02
Prep Date. ..... 03/18/02
Prep Batch #... 2077326
Dilution Factor 1
Analyst ID ..... 003200
PARAMETER
bis (2-Chloroethyl) -
ether
4 -Nitrophenol
SURROGATE
Pheno l -d5
2 - Fluorobiphenyl
Ni t robenz ene - d5
Terphenyl -d!4
2 -Fluorophenol
2,4 , 6 -Tribromophenol
NOTE(S) :
Work Order «...
Date Received. .
Analysi s Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID . .
Method. ........
RESULT
480 K
ND
PERCENT
RECOVERY
47
58
65
35
76
64
EWHDR1AC Matrix. ........: WATER
03/16/02 MS Run #.......: 2077154
03/19/02
18:34
1000 mL Final Wgt/Vol..: 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L 1.8
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 1,22)
E Estimate d result . Resol t concemralio n exceed s (h e calibrallo n range .
CTT. D-;32
III BLASLAND BOUCK & LEB
Client Sample ID: EX-03
GC/MS Semivolatiles
.krv w •^vi*»i£r^.^_» TT • • • \f£*\*^*\s\*^*J\j VV^U** v*x^jb*fe >»^%»^— *. if • • *
nat**» <3amvVI «w3 f!7/1 5 /fl O Hai-<* P*»r*#*-i tr^H .1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Prep Date... ... 03/18/02
Prep Batch #... 2077326
Dilution Factor 10
Analyst ID..... 003200
PARAMETER
bis (2-Chloroethyl) -
ether
4 -Nitrophenol
SURROGATE
Phenol -d5
2 - Fluorobipheny l
Nitrobenzene -d5
Terphenyl -d!4
2 -Fluoropheno l
2,4 , 6-Tribromophenol
Analysis Date . .
Analysis Time..
Initial Wgt/Vol
Instrument ID . .
Method. ........
RESULT
600
ND
PERCENT
RECOVERY
58
65
63
36
57
59
03/16/02 MS Run #.......: 2077154
03/22/02
18:1 4
100 0 mL Final Wgt/Vol..: 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MDL
100 ug/L 14
500 ug/L 18
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
11
BLASLAND BOUCK & LEE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Client Sample ID: BX-04
GC/MS Semivolatiles
Lot - Sample #... C2C160138-002
Date Sampled ... 03/15/02
Prep Date.. .... 03/18/0 2
Prep Batch #... 2077326
Dilution Factor 1
Analyst ID.. ... 003200
PARAMETER
bis (2-Chloroethyl) -
ether
4-Nitrophenol
SURROGATE
Phenol -d5
2 -Fluorobiphenyl
Nitrobenzene-d 5
Terphenyl -d!4
2 - Fluoropheno l
2,4,6 -Tribromophenol
NOTE(S) :
J Estimate d result . Resul t i s les s (hai l RL .
Work Order f t ...
Dat e Received . .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
2.6 J
ND
PERCENT
RECOVERY
68
73
77
69
74
68
EWHDL1AC Matrix. ........: WATER
03/16/02 MS Run #.......: 2077154
03/19/02
10:52
100 0 mL Final Wgt/Vol..: 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L 1.8
RECOVERY
LIMITS
(10 - 113) •
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
n
11111111111
BLASLAND BOTJC K
Client Sample ID
& LKB
: EX-05
GC/M S Semivolatiles
Lot-Sample #. . . : C2C08 0166 -001
Date Sampled. . . : 03/06/02
Prep Date. .....: 03/11/02
Prep Batch #...: 2070291
Dilution Factor: 60
Analyst 3D.....: 001562
PARAMETER
bis (2-Chloroethyl) -
ether
4-Nitrophenol
SURROGAT E
Phenol -d5
2 - Fluorobiphenyl
Nitrobenzene -d5
Te rpheny 1 - dl 4
2 - Fluorophenol
2,4, 6 -Tribromophenol
NOTE(S) :
NC The recover y and/o r RPD were not calculated .
Work Order #. . .
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ...
RESULT
ND
ND
PERCENT
RECOVER Y
NC.DIL
NC,DIL
NC , DIL
NC,DIL
NC.DIL
NC,DIL
EV5FH1A C Matrix. ........ i WATE R
03/08/02 MS Run ft. ......: 2070152
03/12/02
15:34
1000 mL Final Wgt/Vol. . : 3 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
600 ug/L 86
3000 ug/L 110
RECOVER Y
LIMITS
(10 - 113)
(30 - 110}
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
OI L The concentratio n is estimate d or no t reporte d due to dilutio n or the presenc e of interferin g inalytcs.
1
1
1
1
1
1
1
1
III
IIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Client Sample ID: NS-1 1
GC/MS Volatiles
Lot-Sample #. . . : C2C200151-002
Date Sampled. . . .- 03/18/0 2
Prep Date.. ....: 03/25/0 2
Prep Batch #...: 2084404
Dilution Factor: 1
Analyst ID. ....: 034635
PARAMETERAcetone
Benzene
Bromodichloromethane
Chloroform
1 , 2 -Dichloroethan e
1 , 1-Dichloroethene
1 , 2 -Dichloropropane
Ethylbenzene
Methylen e chloride
Toluene
1,1 , 2-Trichloro e thane
Trichloroethen e
Viny l chloride
Xylenes (total)
SURROGATE
Toluene -d 8
1 , 2 - Dichloroethan e - d4
4 -Bromo f luorobenzene
Dibromof luoromethane
Work Order t t . . .
Date Received . .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID . .
Method. ........:
RESULT
ND
ND
ND
ND
ND
ND
ND
2.2
ND
1.4
ND
ND
ND
9.1
PERCENT
RECOVERY
95
88
75
88
EWMM71AA Matrix
03/20/02 MS Run
03/25/02
13:2 8
5 mL Final V
HP5
SW846 8260B
REPORTING
LIMIT UNITS
10 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
2 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ,- ug/L
2.0 ug/L
3.0 ug/L
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
• UZiTlTD
£
Igt/Vol . . : 5 mL
MDL
2.5
0.4 0
0.3 0
0.4 9
0.4 9
0.5 1
0.4 6
0.49
0.3 6
0.2 2
0.44
0.3 9
0.6 0
0 . 96
STL Pi.t-.t-.shi i rob 104 2
111111111111111111
BLASLAND BOUCK & LEE
Client Satqpl e ID: NS-15
GC/MS Volatiles
Lot-Sample #...: C2C200151-005
Date Sampled. ..: 03/18/02
Prep Date. .....: 03/25/02
Prep Batch #...: 2084404
Dilution Factor: 1
Analyst ID.....: 034635
PARAMETER
Acetone
Benzene
Bromodichloromethan e
Chloroform
1 , 2-Dichloroethane
1 , 1-Dichloroethen e
l , 2-Dichloropropane
Ethylbenzen e
Methylen e chlorid e
Toluene
1,1 , 2 -Trichloroe thane
Trichloroethene
Vinyl chlorid e
Xylenes (total)
SURROGATE
Toluene -d8
l,2-Dichloroethane-d 4
4 -Bromof luorobenzene
Dibromof luoromethane
NOTE(S):
J Estimate d result . Resul t a les s du n RL .
work Order #. . . :
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
ND
ND
27
ND
ND
ND
ND
0.77 J
ND
ND
ND
ND
PERCENT
RECOVERY
92
91
90
92
EWMNF1AA Matrix
03/20/02 MS Run
03/25/02
14:03
• U&TITD
#.......:
5 mL Final Wgt/Vol . . : 5 mL
HP5
SW846 8260B
REPORTING
LIMIT UNITS
10 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
2 . 0 ug/L
1.0 ug/L
1 . 0 ug/L
1 . 0 _.,-; ug/L
2.0 ug/L
3 . 0 ug/L
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
MDL
2.5
0.40
0.30
0.49
0.49
0.51
0.46
0.49
0.36
0.22
0.44
0.39
0.60
0 . 96
I
.QTT . p-i M-Q>-iiiT-rrV i 1063
111111111111111111
BLASLAND BOUCK
Client Sample ID
& USE
: NS-29
GC/MS Semivolatiles
Lo t- Sample #... C2C200151-007
Date Sampled... 03/19/02
Prep Date. ..... 03/21/0 2
Prep Batch #. . . 2080243
Dilution Factor 10
Analyst ID..... 001562
PARAMETER
bis (2-Chloroethyl) -
ether
4-Nitrophenol
SURROGATE
Phenol -d5
2 - Fluorobipheny l
Nitrobenzene -d5
Terphenyl-dl4
2 - Fluorophenol
2,4 , 6 -Tr ibromophenol
NOTK(S) :
Work Order # . . .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
8100 E
ND
PERCENT
RECOVERY
92
76
79
35
76
78
EWMN11AC Matrix. ........: WATER
03/20/02 MS Run ft. ......:
03/22/02
15:00
1000 niL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
100 ug/L 14
500 ug/L 18
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
E Eaiiiuio l result . Rcsu K concentratio n exceed ! Ih e calibraiio n range .
STL Pittsburgh 2060
111 BLASLAND BOUC K
•
Client Sample ID
& LEE
: NS-29 OL
GC/M S Semivolatiles
1
1
1
1
1
1
1
1
Lot-Sample ft...: C2C200151-007
Date Sampled. . . : 03/19/02
Prep Date. .....: 03/21/02
Prep Batch #...: 2080243
Dilution Factor: 200
Analyst ID.....: 001562
PARAMETE R
bis (2-Chloroethyl) -
ether
4-Nitrophenol
SURROGAT E
Phenol -d5
2 -Fluorobiphenyl
Nitrobenzene-d5
Terphenyl-dl4
2 -Pluorophenol
2,4,6 -Tribromophenol
NOTE(S) :
NC The recover y aiul/o r RPD were not calculated .
Work Order # . . .
Date Received. .Analysis Date . .
Analysis Time. .
Initial W^t/Vol
Instrument ID. .
Method.. .......:
RESULT
9900
ND
PERCENT
RECOVER Y
NC.DIL
NC,DIL
NC.DIL
NC,DIL
NC,DIL
NC,DIL
EWMN12A C Matrix. ........: WATE R
03/20/02 MS Run #.......:
03/25/02
12:4 6
100 0 roL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
2000 ug/L 290
10000 ug/L 360
RECOVER Y
LIMITS
(10 - 113}
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
OIL Tli c concentratio n is estimate d or no ( reporte d due 10 dilutio n or the presence of interferin g aiulytcs .
1
1
1
1
1
1
1
1
STL Pittsburgh 2069
11
BLASLAND BOUCK & LEE
1
1
1
1
1
1
1
1
1
Client Sample ID:NS-30
GC/MS Semivolatiles
Lot -Sample #... C2C130119-001
Date Sampled. . . 03/11/02
Prep Date. ..... 03/14/02
Prep Batch #... 2073127
Dilution Factor 1
Analyst ID. .... 001562
PARAMETER
bis (2-Chloroethyl) -
ether
4 -Nitrophenol
SURROGATE
Phenol -d5
2 - Fluorobiphenyl
Ni t robenzen e - d5
Terphenyl -dl 4
2 - Fluorophenol
2,4,6 -Tribromophenol
NOTE(S) :
Work Order #...
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. .
RESULT
140 E
ND
PERCENT
RECOVERY
70
81
81
63
68
92
EWAHN1AC Matrix......... i WATER
03/13/02 MS Run #.......: 2073022
03/15/02
21:45
100 0 mL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L 1.8
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
E Estimate d result . Resul t concentratio n exceed s th e calibratio n range .
II
I
I
II
I
I
CTT. Pi t-fcl-iiir-rrVi 24
IIIIIII
BLASLAND BODCK & LEE
Client Sample ID: NS-30
Lot-Sample #...
Date Sampled...
Prep Date......
Prep Batch ft...
Dilution Factor
Analyst ID.....
C2C130119-001
03/11/02
03/14/02
2073127
3
001562
V GC/MS Semivolatiles
Work Order f...
Date Received..
Analysis Date..
Analysis Time..
Initial Wgt/Vo l
Instrument ID..
Method.........
EWAHN2AC
03/13/02
03/18/02
11:3 6
1000 mL
721
SW846 8270C
MS Run #.......: 2073022
Final Wgt/Vol..: 1 mL
•
PARAMETER RESULT
bis(2-Chloroethyl)-
ether
4 - N i t ropheno1
150
ND
REPORTING
LIMIT UNITS
30
MDL
150
ug/L
ug/L
4.3
5.3
V
SURROGATE1Phenol -d S
2 - Fluorobiphenyl
Nitrobenzene-dS
ITerphenyl -d!4
2 - Fluorophenol
2,4,6 -Tribromopheno l
1
1
1
1
1
1
PERCENT RECOVERY
RECOVERY LIMITS
69 (10 - 113)
84 (30 - 110)
82 (32 - 112)
67 (10 - 144)
69 (13 - 110)
106 (21 - 122)
OTT. D-i h t- cV-inr-rrV-i 25
111 BLASLAND BOUCK
Client Sample ID
& LEE
: NS-31
GC/MS Semivolatiles
1
1
1
1
1
1
1
1
Lot - Sample #... C2C200151-006
Date Sampled. . . 03/19/02
Prep Date. ..... 03/21/02
Prep Batch #... 2080243
Dilution Factor 4
Analyst ID..... 001562
PARAMETER
bis (2-Chloroethyl) -
ether
4-Nitropheno l
SURROGATE
Phenol -d5
2 - Fluorobipheny l
Nitrobenzene -dS
Terphenyl-dl4
2 - Fluorophenol
2,4 , 6 -Tribromopheno l
Work Order # . . .
Date Received. .
Analysis Date. .
Analysis Time . .
Initial Wgt/Vo l
Instrument ID. .
Method. ........
RESULT
81
ND
PERCENT
RECOVERY
88
102
99
102
74
113
EWMNM1AC Matrix. ........: WATER
03/20/02 MS Run ft..... . . :
03/22/02
14:3 3
1000 mL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
40 ug/L 5.8
200 ug/L 7.1
RECOVERY
LIMITS
{10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
STL Pittsburgh 2053
1111111111111111111
BLASLAND BODCK
Client Sample XD
& LEE
: NS-32
GC/MS Semivolatilea
Lot-Sample t t ... C2C130H9-002
Date Sampled. . . 03/11/02
Prep Date. ..... 03/14/02
Prep Batch #... 2073127
Dilution Factor 1
Analyst ID . . . 001562
PARAMETER
bis (2-Chloroethyl ) -
ethe r
4-Nitropheno l
SURROGATE
Phenol -d5
2 - Fluorobipheny l
Nitrobenzene -d5
Terphenyl-dl 4
2 - Fluorophenol
2,4 , 6 -Tribromophenol
Work Order #. . .
Date Received. .
Analysis Date. .
Analysis Tine. .Initial Wgt/Vol
Instrument: ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVERY
67
80
77
85
64
95
EWAHX1AC Matrix.. .......: WATER
03/13/02 MS Run ft....... : 2073022
03/18/02
12:03
100 0 mL Final Wgt/Vol..s l mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L 1.8
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
26
IIIIIIIIIIIIIIIIIII
Lot-Sample tt . ..-. C2C160138-005
Date Sampled...: 03/15/0 2
BLASLMTO BOUCK & LEE
Client Sample JD: EX-01
TOTAL Metals
Date Received..: 03/16/02
Matrix.WATER
PARAMETER RESULT
REPORTING
LIMIT UNITS METHO D
PREPARATION- WOR K
ANALYSIS DATE ORDE R #
Prep Batch #...: 2077233
Arsenic N D
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
KOTE(S) ;
45.5 B
ND
ND
169
ND
ND
ND
10.0 ug/L SW84 6 6010B 03/18-03/22/02 EWHDW1A H
Dilution Factor: 1 Analysis Time..: 10:29 Analyst ID.... .: 400149
Instrument ID. .: TRACEICP MS Run « . . . . . . .: 2077088 MDL. ...........: 2.4
200 ug/L SW846 6010B 03/18-03/22/02 EWHDW1A L
Dilution Factor: 1 Analysis Time...- 10:29 Analyst I D . . . . .: 40014 9
Instrument ID..: TRACEIC P MS Run f t . . . . . . .: 2077088 MDL. ...........: 1.1
5.0 ug/L SW84 6 6010B 03/18-03/22/02 EWHDW1A P
Dilution Factor: 1 Analysis Time..: 10:29 Analyst I D . . . . .: 400149
Instrument ID. . : TRACEICP MS Run «.......: 2077088 MDL. ...........: 0.47
5.0 ug/L SW84 6 6010B 03/18-03/22/02 EWHDW1A T
Dilution Factor: 1 Analysis Time..: 10:29 Analyst I D . . . . .: 40014 9
Instrument ID. . : TRACEICP MS Run ».......: 2077088 MDL. . . . . - . . . . . .: 0.24
5.0 ug/L SW84 6 6010B 03/18-03/22/02 EWHDW1A W
Dilution Factor: 1 Analysis Time..: 10:29 Analyst I D . . . . .: 40014 9
Instrument ID..: TRACEIC P MS Run ».......: 2077088 M D L . . . . . . . . . . . .: 1.1
15.0 ug/L SW846 6010B 03/18-03/22/O2 EWHDK1A1
Dilution Factor: 1 Analysis Time..: 10:29 Analyst I D . . . . . .. 400149
Instrument ID..: TRACEICP MS Run 8. ......: 2077088 M D L . . . . . . . . . . . .: 0.45
40.0 ug/L SW846 6010B 03/18-03/22/O2 EWHDW1A.4
Dilution Factor-. 1 Analysis Time..: 10.-2 9 Analyst ID.....: 40014 9
Instrument ID. .: TRACEIC P MS Run tt.......: 207708 8 MDL . ............. 1.8
5.0 ug/L SW84 6 6010B 03/18-03/22/02 EWHDW1A 7
Dilution Factor: l Analysis Time..: 10:29 Analyst ID.....: 40014 9
Instrument ID..: TRACEICP MS Run #.......: 2077088 M D L . . . . . . . . . . . .: 2.7
20.0 ug/L SW84 6 6010B 03/18-03/22/02 EWHDW1C A
Dilution Factor: 1 Analysis Time..: 10:29 Analyst ID.....: 400149
Instrument ID..: TRACEICP MS Run # . . . . . . .: 2077088 MDL. ...........: 4.4
0 GMiniaK.il rtwill. Result is less (tan RL.
52
1111111111111111111
BLASLAND BOUCK & LEE
Client Sample ID: EX- 02
TOTAL Metals
Lot-Sample #...: C2C160138-001
Date Sampled. ..: 03/15/02 Date Received. .: 03/16/02
REPORTIN G
PARAMETE R RESULT LIMIT UNITS METHO D
Prep Batch #. . . : 2077233
Arsenic 3.2 B 10.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
Barium 4360 200 ug/L
Dilution Factor: l
Instrument ID..: TRACEIC P
Beryllium ND 5.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
Cadmiu m ND 5.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
Chromium 6.1 5.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEICP
Manganese 15100 30.0 ug/L
Dilution Factor: 2
Instrument ID . . : TRACEIC P
Nickel 12.3 B 40.O ug/L
Dilution Factor: 1
Instrument ID. . : TRACBIC P
Selenium 10.7 10.0 ug/L
Dilution Factor: 2
Instrument ID . . ; TRACEIC P
Zinc 4.6 B 20.0 ug/L
Dilution Factor: 1
Ir-struraent 1C..: TRACSIC P
NOTE(S) :
B Estimate d result . Rcsil i is less tha n RL .
SW846 6010B
Analysis Time . . :
M S Run tt .........
SW846 6010B
Analysis Time. . :
MS Run #.......:
SW846 6010B
Analysis Time. . :
MS Run tt .......:
SW846 6010B
Analysis Time. . :
M S Run tt .......:
SW846 6010B
Analysis Time. . :
MS Run tt .......:
SW846 6010B
Analysis Time. . :
M S Run # . . . . . . .:
SW846 6010B
Analysis Time. . :
MS Run « . . . . . . .:
SW846 6010B
Analysis Time . . :
M S Run » .......:
SW846 6010B
Analysis Time. . :
M S Run 8 .......:
Matrix. ......:
PREPARATION -
ANALYSIS DAT E
03/18-03/22/02
10:0 7 Analyst ID. ....
2077088 MDL . ...........
03/18-03/22/02
10:0 7 Analyst ID. ....
2077088 MDL . ...........
03/18-03/22/02
10:0 7 Analyst ID. ....
2077088 MDL . ...........
03/18-03/22/02
10:0 7 Analyst ID. ....
2077088 MDL . ...........
03/18-03/22/02
10:0 7 Analyst ID. ....
2077088 MDL . ...........
03/18-03/22/O2
16:1 8 Analyst ID. . . . .
2077088 MDL . .........
03/18-03/22/02
10:0 7 Analyst ID. . . . .
2077088 MDL . ...........
03/18-03/22/02
16:1 8 Analyst ID. . . . .
2077088 MDL . ...........
03/18-03/22/02
10:0 7 Analyst ID. . . . .
2C77C88 MDL . ..........
WATE R
WOR K
ORDE R #
EWHC61A D
: 400149
: 2.4
EWHC61A R
: 400149
: 1.1
EWHC61AF
: 400149
: 0.47
EWHC61A G
: 400149
: 0.2 4
EWHC61AH
: 400149
: 1.1
EWHC61AV J
: 400149
: 0.8 9
EWHC61AK
: 400149
: 1.8
EWHC61A L
: 400149
. : 5.5
EWHC61A M
. : 400149
.: 4.4
QTT . Di ft-cl-,iiT-rrVi 48
111
1 Lot-Sample #...-. C2C160138-
Date Sampled. . . : 03/15/02
• PARAMETE R RESULT
I Prep Batch #...: 2077233
Arsenic 3.8 B
Barium 4370
1
Beryllium N D
1
Cadmium N D
• Chromium 6.2
• Manganese 15000
Nickel 12.2 B
Selenium ND
1
Zinc 5.9 B
1
NOTE (S) :
• B Esimuuu l result . Rgail l is les s linn RL.
1
1
BLASLAND BOUCK & LEE
Client Sample ID: DUP-031502
TOTA L Metals
•006
Date Received. . : 03/16/02
REPORTING
LIMIT UNIT S METHO D
10 . 0 ug/L
Dilution Factor: 1
instrument ID..: TRACEIC P
200 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
5.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
5.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
5 . 0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEICP
30.0 ug/L
Dilution Factor: 2
Instrument ID..: TRACEICP
40 . 0 ug/L
Dilution Factor: 1
Instrument ID . . : TRACEIC P
10.0 ug/L
Dilution Factor: 2
Instrument ID..: TRACEICP
20 . 0 ug/L
Dilution Factor: 1
instrument ID...- THACEIC P
SW846 6010B
Analysis Time..:
MS Run (t .......:
SW846 6010B
Analysis Time. . :
MS Run #.......:
SW846 6010B
Analysis Time. . :
M S Run ».......:
SW846 6010B
Analysis Time. . :
MS Run #........:
SW846 6010B
Analysis Time. . :
M S Run #.......:
SW846 6010B
Analysis Time . . :
MS Run # . . . . . . .:
SW846 6010B
Analysis Time. . :
M S Ru n ft .......:
SW846 6010B
Analysis Time . . :
MS Run «.......:
SW846 6010B
Analysis Time . . :
MS Run ft .......:
Matrix. ......: WATE R
PREPARATION - WOR K
ANALYSIS DATE ORDE R #
03/18-03/22/02 EWHD21AD
11:01 Analyst ID. . . . . : 400149
2077088 MDL. ...........: 2.4
03/18-03/22/02 EHHD21AB
11:01 Analyst ID.....: 400149
2077088 MDL. ...........: 1.1
03/18-03/22/02 EWHD21AF
11:01 Analyst I D . . . . .: 400149
2077088 MDL. ...........: 0.47
03/18-03/22/02 EWHD21A G
11:01 Analyst I D . . . . .: 400149
2077088 MDL. . . . . . . . . . . .: 0.24
03/18-03/22/O2 EWHD21AH
11:01 Analyst I D . . . . .: 400149
2077088 MDL. . . . . . . . . . . .: 1.1
03/18-03/22/O2 EWHD21AJ
16:23 Analyst ID.....: 40014 9
2077088 MDL. ...........: 0.89
03/18-03/22/O2 EWHD21AK
11:01 Analyst ID. . . . . : 400149
2077088 MDL. ...........: 1.8
03/18-03/22/02 EWHD21AL ,
16:23 Analyst ID.....: 400149
2077088 MDL. ...........: S.S
03/18-03/22/02 EWHD21A M
11:01 Analyst ID. ....: 400149
2077088 MDL. ...........: 4.4
t-t-,~VM ,-v-^-53
III
I
II
I
I
I
BLASLAND BO0CK & LEE
Client Sample ID: EX-03
TOTAL Metals
II
IIIIII
Lot -Sample # .
Date Sampled.
PARAMETE R
Prep Batch # .
Arsenic
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
..: C2C160138-004
..: 03/15/02 Date Received. .:
REPORTIN G
RESULT LIMIT UNITS
..: 2077233
ND 10.0 ug/L
instrument ID..: TRACEIC P
561 200 ug/L
Instrument ID..: TRACEIC P
ND 5.0 ug/L
Instrument ID..: TRACEIC P
0.2 9 B 5.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
23.2 5.0 ug/L
Instrument ID..: TRACEIC P
218 0 15.0 ug/L
19.2 B 40.0 ug/L
ND 5.0 ug/L
Instrument ID. . : TRACEIC P
94.5 20.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACBIC P
03/16/02
METHO D
SW846 6010B
MS Run # . . . . . . .:
SW846 6 01 OB
MS Run *.......:
SW846 6010B
MS Run B .......:
SW846 6010B
MS Run ».......:
SW846 6010B
MS Run ».......:
SW846 6010B
MS Run fl .......:
SW846 6010B
M S Run % .......:
SW846 6010B
MS Run ».......:
SW846 6010B
MS Run *f .......:
Matrix. ......: WATE R
PREPARATION- WOR K
ANALYSIS DAT E ORDE R #
03/18-03/22/02 EWHDR1A D
10:2 3 Analyst I D . . . . .: 400149
2077088 MDL . ...........: 2.4
03/18-03/22/02 BWHDR1A E
10:2 3 Analyst ID. . . . . : 400149
2077088 MDL . ...........: 1.1
03/18-03/22/02 EWHDR1AF
10:2 3 Analyst I D . . . . .: 400149
2077088 MDL . ...........: 0.4 7
03/18-03/22/O2 EWHDR1AG
10:2 3 Analyst ID.....: 400149
2077088 MDL . ...........: 0.2 4
03/18-03/22/02 BWBDR1AH
10:2 3 Analyst ID. . . . . : 400149
2077088 MDL . ...........: 1.1
03/18-03/22/02 EWBDR1AJ
10:2 3 Analyst ID. . . . . : 400149
2077088 MDL . ...........: 0.4 5
03/18-03/22/02 EHHDR1AK
10:2 3 Analyst ID. . . . . : 400149
2077088 MDL . ...........: 1.8
03/18-03/22/02 EWHDR1A L
10:2 3 Analyst ID. ....: 400149
2077088 MDL . ...........: 2 . 7
03/18-03/22/02 BWHDRXA M
10:2 3 Analyst ID.....: 400149
2077088 MDL . ...........: 4.4
NOTE(S) :
B Eslimaici ) result . Resul t in k» lio n RL .
CTT 51
IIIIIIIIIIIIIIIIIII
Lot-Sample #...: C2C160138
Date Sampled...: 03/15/02
-00 2
BLASLAND BODCK & LEE
Client Sample ID: EX-04
TOTAL Metals
Date Received..: 03/16/02
PARAMETER RESULT
REPORTING
LIMIT UNITS METHO D
Matrix.......: WATE R
PREPARATION- WOR K
ANALYSIS DATE ORDE R ft
Prep Batch f t . .. : 2077233
Arsenic ND
Barium
Beryllium
Cadmium
Chromiu m
Manganese
Nickel
Selenium
Zinc
NOTE(S):
61.2 B
ND
ND
2240
ND
ND
ND
10.0 ug/L SW846 6010B 03/18-03/22/02 EWHDL1A D
Dilution Factor: 1 Analysis Time..: 10;12 Analyst I D . . . . .: 40014 9
Instrument ID. . : TRACEICP MS Run # . . . . . . .: 2077088 MDL . ...........: 2.4
200 ug/L SW846 6010B 03/18-03/22/02 EWHDL1A E
Dilution Factor: 1 Analysis Time..: 10:12 Analyst I D . . . . .: 400149
Instrument ID. . : TRACEICP MS Run t t . . . . . . .: 2077088 MDL - . . . . . . . . . . .: 1.1
5.0 ug/L SW846 6010B 03/18-03/22/02 EWHDL1A F
Dilution Factor: 1 Analysis Time..: 10:12 Analyst I D . . . . .: 40014 9
Instrument ID. . : TRACEICP MS Run #.......: 2077088 MDL . , . . . . . . . . . .: 0.47
5.0 ug/L SW846 6010B 03/18-03/22/02 EWHDL1A G
Dilution Factor-. 1 Analysis Time..: 10:12 Analyst I D . . . . .: 400149
Instrument ID..: TRACEIC P MS Run « . . . . . . .: 2077088 MDL . . . . . . . . . . . .: 0.24
5.0 ug/L SW84 6 6010B 03/18-03/22/02 EWHDL1A H
Dilution Factor: 1 Analysis Time..: 10:12 Analyst 10.....: 400149
Instrument ID..: TRACEICP MS Run #.......: 2077088 M D L . . . . . . . . . . . .: 1.1
15.0 ug/L SW846 6010B 03/18-03/22/02 EWHDL1A J
Dilution Factor: 1 Analysis Time..: 10:12 Analyst ID.....: 400H9
Instrument ID..: TRACEICP MS Run #.......: 2077088 M D L . . . . . . . . . . . .: 0.45
40.0 ug/L SW846 6010B 03/18-03/22/O2 EWHDL1AK
Dilution Factor: 1 Analysis Time..: 10:12 Analyst ID... . . ;. 40014 9
Instrument ID..: TRACEICP MS Run # . . . . . . .: 2077088 M D L . . . . . . . . . . . .: 1.8
5.0 ug/L SW84 6 6010B 03/18-03/22/02 EWHDL1A L
Dilution Factor.- 1 Analysis Time..: 10:12 Analyst I D . . . . .: 400149
Instrument ID. . : TRACEICP MS Run « . . . . . . .: 2077088 MDL . ...........: 2.7
20.0 ug/L SW84 6 6010B 03/18-03/22/O2 EWHDL1A M
Dilution Factor: 1 Analysis Time..: 10:12 Analyst I D . . . . .: 400149
Instrument ID..: TRACEIC P MS Run t.......: 2077083 M D L . . . . . . . . . . . .: 4.4
B felimaiu l result . Resul t is less lim n RL .
CTT . Di t-t-cV-Mi-rrrh 49
IIIIIIIIIIIIIIIIIII
Lot-Sample #.
Date Sampled.
PARAMETER
C2C200151-007
03/19/02
BLASLAND BOUCK & LEE
Client Sample ID: NS-29
TOTAL Metals
Date Received..: 03/20/0 2
RESULT
REPORTING
LIMIT UNITS METHOD
Matrix......... WATE R
PREPARATION- WORK
ANALYSIS DATE ORDER #
Prep Batch #.
Arsenic
Barium
Berylliu m
Cadmiu m
Chromium
Manganese
Hickel
Selenium
Zinc
NOTE (S ) .-
: 2080158
18.2 10.0 ug/L SW846 6010B 03/21-03/26/02 EWMNllAD
Dilution Factor : 1 Analysi s Time.. i 10:24 Analys t ID.. ...: 400149
Instrument ID..: TRACEICP MS Run «.......: 2080030 MDL............: 2.4
10700 400 ug/L SW846 6010B 03/21-03/26/02 EHMH11AB
Dilution Factor: 2 Analysis Time..: 15:55 Analyst ID.....: 400149
Instrument ID..: TRACEICP MS Run #.......: 2080030 M D L . . . . . . . . . . . .: 2.2
ND 5.0 ug/L SW846 6010B 03/21-03/26/02 EWMM11AF
Dilution Factor.- 1 Analysis Time..: 10:24 Analyst ID.....: 40014 9
Instrument ID..: TRACEICP MS Run S....... i 20S0030 M D L . . . . . . . . . . . .: 0.47
ND 5.0 ug/L SW846 6010B 03/21-03/26/02 EWMN11A G
Dilution Factor: 1 Analysis Time..: 10:24 Analyst ID.....: 40014 9
Instrument ID..: TRACEICP MS Run « . . . . . . .: 2080030 M D L . . . . . . . . . . . .: 0.24
26.9 5.0 ug/L SW846 6010B 03/21-03/26/02 EWHH11AH
Dilutio n Factor : 1 Analysi s Time..: 10:24 Analys t ID.....: 400149
Instrument ID. . : TRACEICP MS Run #.......: 2080030 MDL............: 1.1
104000 750 ug/L SH846 6010B 03/21-03/26/02 BWMH11AJ
Dilution Factor: 50 Analysis Time..: 16:01 Analyst ID.....: 400149
Instrument ID. . : TRACEICP MS Run #.......: 2080030 MDL. ...........: 22.3
45.3 40.0 ug/L SW846 6010B 03/21-03/26/02 BWNIOAK
Dilutio n Factor : 1 Analysi s Time..: 10:24 Analys t ID.....: 40014 9
Instrument ID..i TRACEICP MS Run tf.......: 2080030 MDL............: 1.8
44.0 5.0 ug/L SW846 6010B 03/21-03/26/02 BWMN13-A L
Dilutio n Factor : 1 Analysi s Time..: 10:24 Analys t ID.....: 40014 9
Instrument ID..: TRACEICP MS Run #.......: 2080030 MDL............ t 2.7
4.8 B 20.0 ug/L SW846 6010B 03/21-03/26/02 EHMNllAM
Dilution Factor: 1 Analysis Time..: 10:24 Analyst ID.....: 400149
Instrument ID..: TRACEIC P MS Run «.......: 2080030 M D L . . . . . . . . . . . .: 4.4
B Eaimale d result . Resul t is less tha n RL .
3009
1111111111111111111
BLASLAND BOUCK &
Client Sample ID:
TOTAL Metals
Lot-Sample #...: C2C130119-001
Date Sampled...: 03/11/02 Date Received..:
REPORTING
PARAMETE R RESULT LIMIT DNITS
Prep Batch #. . . : 2073174
Arsenic ND 10.0 ug/L
Barium 405 200 ug/L
Beryllium ND 5.0 ug/L
Instrument ID . . : TRACEIC P
Cadmium ND 5.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
Chromium ND 5.0 ug/L
Instrument ID..: TRACEIC P
Manganese 1070 15.0 ug/L
Instrument ID . . : TRACEIC P
Nickel 1.8 B 40.0 ug/L
Instrument ID..: TRACEIC P
Selenium ND 5.0 ug/L
Instrument ID . . •. TRACEIC P
Zinc ND 20.0 ug/L
Instrument ID..: TRACBIC P
NOTE(S) :
B Estimate d rtsuti . Resul t is les s Hu m RL .
LEE
NS-30
03/13/02
METHO D
SW84 6 6010B
MS Run » . . . . . . .:
SW846 6010B
MS Run t) .......:
SW846 6010B
MS Run « . . . . . . .:
SW846 6010B
MS Run tt .......:
SW846 6010B
M S Run *.......:
SW846 6010B
M S Run tt .......:
SW846 6010B
M S Run #.......
SW84 6 6010B
Analysis Time. .
M S Run tt .......
SW846 6010B
M S Run » .......
Matrix. ......: WATE R
PREPARATION- WOR K
ANALYSIS DAT E ORDE R #
03/14-03/17/02 EWAHN1A D
14:0 7 Analyst I D . . . . .: 400149
2073052 MDL . . . . . . . . . . . .: 2.4
03/14-03/17/02 EWAHN1AE
14:0 7 Analyst I D . . . . .: 400149
2073052 MDL . . . . . . . . . . . .: 1.1
03/14-03/17/02 EWAHN1A F
14:0 7 Analyst ID. ....: 400149
2073052 MDL . ...........: 0.47
03/14-03/17/02 EWAHN1A G
14 :07 Analyst ID. . . . . : 400149
2073052 MDL . ...........: 0.24
03/14-03/17/O2 EWAHN1A H
14:0 7 Analyst ID. . . . . : 400149
2073052 MDL . ...........: 1.1
03/14-03/17/O2 EWAHN1AJ
14:07 Analyst ID. . . . . : 400149
2073052 MDL . . . . . . . . . . . .: 0.45
03/14-03/17/02 EW7AHH1AK
: 14:07 Analyst I D . . . . .: 400149
: 2073052 MDL . . . . . . . . . . . .: 1.8
03/14-03/17/02 EWAHN1A L
: 14:07 Analyst I D . . . . .: 400149
: 2073052 MDL . ...........: 2.7
03/14-03/17/02 EWAHN1A M
: 14:07 Analyst I D . . . . .: 400149
: 2073052 MDL . ...........: 4.4
39
fIIIIIIIIIIIIIIII
Lot-Sample #.
Date Sampled.
PARAMETER
C2C200151-006
03/19/02
BLASLAND BO0CK & LEE
Client Sampl e ID.- NS-3 1
TOTAL Metal s
Date Received..: 03/20/02
RESULT
REPORTING
LIMIT UNITS METHOD
Matrix.......: WATE R
PREPARATION- WORK
ANALYSIS DATE ORDER ft
Prep Batc h #.
Arsenic
Barium
Berylliu m
Cadmiu m
Chromiu m
Manganese
Nickel
Selenium
Zinc
NOTE(S);
: 2080158
4.7 B 10.0 ug/L SW846 6010B 03/21-03/26/O2 EHMNKLAD
Dilution Factor: 1 Analysis Time..: 10:19 Analyst ID.....: 40014 9
Instrument ID..; TRACEIC P MS Run 8.......: 208003 0 M D L . . . . . . . . . . . .i 2.4
22.9 B 200 ug/L SW846 6010B 03/21-03/26/02 KWMHM1A K
Dilution Factor: 1 Analysis Time..: 10:19 Analyst ID.....: 40014 9
Instrument ID..: TRACEIC P MS Run # . . . . . .. : 2080030 M D L . . . . . . . . . . . .: 1.1
ND 5.0 ug/L SW84 6 6010B 03/21-03/26/02 EWMNM1A P
Dilution Factor: 1 Analysis Time..: 10:19 Analyst ID.....: 40014 9
Instrument ID..: TRACEIC P MS Run #.......: 2080030 M D L . . . . . . . . . . . .: 0.47
ND 5.0 ug/L SW84 6 6010B 03/21-03/26/02 EWMNM1A G
Dilution Factor: 1 Analysis Time..: 10:19 Analyst ID.....I 40014 9
Instrument ID..: TRACEICP MS Run «.......: 2080030 M D L . . . . . . . . . . . .: 0.24
1.9 B 5.0 ug/L SW846 6010B 03/21-03/26/02 EHMHMLA H
Dilution Factor: 1 Analysis Time..: 10:19 Analyst ID.....: 400149
Instrument ID. .: TRACEICP MS Run S- ......: 2080030 MDL . ......'.....: 1.1
22.5 15.0 ug/L SW846 6010B 03/21-03/26/O2 EWMNM1AJ
Dilution Factor-. 1 Analysis Time..: 10:19 Analyst ID.....: 400149
Instrument ID. . : TRACEICP MS Run #.......: 2080030 MDL . ...........: 0.45
ND 40.0 ug/L SW846 6010B 03/21-03/26/02 EWMNM1A K
Dilution Factor: 1 Analysis Time..: 10:19 Analyst ID.....: 400149
Instrument ID. . : TRACEIC P MS Run tt.......: 2080030 M D L . . . . . . . . . . . .: 1.8
ND 5.0 ug/L SW84 6 6010B 03/21-03/26/02 EWMNM1A L
Dilution Factor: 1 Analysis Time..: 10:19 Analyst ID.....: 400149
Instrument ID..: TRACEIC P MS Run #.......: 2080030 M D L . . . . . . . . . . . .: 2.7
ND 20.0 ug/L SW84 6 6010B 03/21-03/26/02 EWMNM1A M
Dilution Factor: 1 Analysis Time..: 10:19 Analyst ID.....: 400149
Instrument ID. . : TRACEIC P MS Run ».......: 2080030 M D L . . . . . . . . . . . .: 4.4
D Estimate d result . Resul t ii lest tha n RL .
3008
IIIIIIIIIIIIIIIIIII
Lot-Sampl e tt . .
Date Sampled..
C2C130119-002
03/11/02
BLASLAND BOCTC K &. LEE
Client Sample ID: NS-3 2
TOTAL Metal s
Date Received..: 03/13/0 2
Matrix.WATE R
PARAMETE R RESULT
Prep Batch #...: 2073174
Arsenic ND
Barium 107 B
Beryllium ND
Cadmiu m N D
Chromiu m N D
Manganese 119
Nickel N D
Selenium ND
Zinc N D
REPORTING
LIMIT UNITS
10.0 ug/L
Instrument ID..: TRACEIC P
200 ug/L
Instrument ID..: TRACEIC P
5 . 0 ug/L
Instrument ID. . : TRACEIC P
5 . 0 ug/L
Instrument ID..: TRACEIC P
5.0 ug/L
15 . 0 ug/L
Instrument ID . . : TRACEIC P
40.0 ug/L
Dilution Factor: 1
Instrument ID..-. TRACEIC P
5 . 0 ug/L
Instrument ID..: TRACEICP
20.0 ug/L
Instrument ID. . : TRACEIC P
METHOD
SW846 6010B
Analysis Time. . :
M S Run # . . . . . . .:
SW846 6010B
M S Run )» . . . . . . .:
SW846 6010B
M S Run # . . . . . . .:
SW84 6 6010B
MS Run tt .......:
SW846 6010B
M S Run tt .......:
SW846 6010B
M S Run « . . . . . . .:
SW846 6010B
Analysis Time. . :
M S Run 3 .......:
SW84 6 6010B
M S Run 8 .......:
SW84 6 6010B
MS Run tt .......:
PREPARATION - WOR K
ANALYSIS DATE ORDE R #
03/14-03/17/02 EWAHX1AD
14:2 9 Analyst ID.....: 400149
2073052 MDL . . . . . . . . . . . .: 2.4
03/14-03/17/02 EWAHX1AE
14:2 9 Analyst I D . . . . .: 400149
2073052 MDL . . . . . . . . . . . .: 1.1
03/14-03/17/02 EWAHX1A F
14:2 9 Analvst ID .....: 400149
2073052 MDL . . . . . . . . . . . .: 0.47
03/14-03/17/02 EWAHX1A G
14 :29 Analyst ID. . . . . : 400149
2073052 MDL . . . . . . . . . . . .: 0.24
03/14-03/17/02 EWAHX1A H
14:2 9 Analyst I D . . . . .: 400149
2073052 MDL . . . . . . . . . . . .: 1.1
03/14-03/17/O2 EWAHX1AJ
14:2 9 Analyst ID.....: 400149
2073052 MDL . . . . . . . . . . . .: 0.45
03/14-03/17/02 EWAHX1A K
14:2 9 Analyst I D . . . . .: 400149
2073052 MDL . . . . . . . . . . . .: 1.8
03/14-03/17/02 EWAHX1A L
14:2 9 Analyst I D . . . . .: 400149
2073052 MDL . ...........: 2.7
03/14-03/17/02 EWAHX1A M
14:2 9 Analyst I D . . . . .: 400149
207305^ MDL . ...........: 4.4
NOTE(S):
EviniDicJ result. Resul t « les s dun KL.
1111111111111111111
BLASLAND BOUCK & LEE
Client Sampl e ID: EX- 05
GC/MS volatiles
Lot-Sample #...: C2C080166-001 Work Order- «- . . EV5FH1AA Mahr-ix - _ . . _ _ _ _ _• WiTRD
Date Sampled. ..: 03/06/02
Prep Date. .....: 03/11/02
Prep Batch #...: 2070568
Dilution Factor: 3000
Analyst ID. . . . . : 034635
PARAMETER
Acetone
Benzene
Bromodichloromethan e
Chlorofor m
1,2 -Dichloroethane
l, 1-Dichloroethen e
1 , 2 -Dichloropropane
Ethylbenzene
Methylen e chlorid e
Toluene
1,1,2 - Tr i chloroethane
Trichloroethen e
Vinyl chloride
Xylenes (total)
SURROGATE
Toluen e -d a
1, 2-Dichloroethane-d4
4 - Bromo f luorobenzene
D ibr omo f 1 uor ome t hane
NOTE(S) :
J Estimate d result . Rcju H i t les s tha n RL .
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgft/Vo l
Instrument ID. .
Method. ........:
RESULT
24000 J
ND
ND
ND
350000 E
ND
ND
ND
ND
26000
ND
ND
ND
ND
PERCENT
RECOVERY
99
91
84
98
03/08/02
03/11/02
23:1 0
5 mL
MS Run a. - - - - - --
Final Wgt/Vol.. : 5 mL
HP5
SW846 8260B
REPORTING
LIMIT
30000
3000
3000
3000
3000
3000
3000
3000
6000
3000
3000
3000 .-'.'.'
6000
9000
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITSug/L
ug/L
ug/L
ug/L
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
MDL
7500
1200
910
150 0
1500
150 0
140 0
150 0
110 0
680
1300
120 0
180 0
2900
E Estimate d retull . Resul l concentratio n exceed s th e calibratio n range .
rrnr r\-t
1111111111111111111
BLASLAND BOUCK & LEE
Client Sample ID: EX-05
GC/MS Volatiles
Lot-Sample #...: C2C080166-001
Date Sampled...: 03/06/02
Prep Date. .....: 03/15/02
Prep Batch #...: 2074228
Dilution Factor: 15000
Analyst ID.....: 034635
PARAMETER
Acetone
Benzen e
Bromodichloromethan e
Chloroform
1 , 2 -Dichloroethane
1,1 -Dichloroethen e
1 , 2 -Dichloropropan e
Ethylbenzene
Methylen e chloride
Toluene
1,1,2 -Trichloroethan e
Trichloroethen e
Vinyl chloride
Xylenes (total )
SURROGATE
Toluene-d 8
1, 2-Dichloroethane-d4
4 -Bromo f luorobenzen eDibromof luoromethane
NOTB(S) :
I Estimate d result . Resul t a le a tha n RL .
Work Order #.. .
Date Received. .
Analysis Date. .
Analysis Time..
Initial Wgt/Vol
Instrument ID. .
Method.. .......:
RESULT
53000 J
ND
ND
ND
390000
ND
ND
ND
ND
24000
ND
ND
ND
ND
PERCENT
RECOVERY
105
110
85
115
EV5FH2AA Matrix
03/08/02 MS Run
03/15/02
11:4 3
........: WATERfi . . :
5 mL Final Wgt/Vol . . r 5 mL
HP5
SW846 8260B
REPORTING
LIMIT UNITS
150000 ug/L
15000 ug/L
15000 ug/L
15000 ug/L
15000 ug/L
15000 ug/L
15000 ug/L
15000 ug/L
30000 ug/L
15000 ug/L
15000 ug/L
15000,'.. ug/L
30000 ug/L
45000 ug/L
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
MDL
38000
6000
4600
7300
7300
7700
6900
7300
5400
3400
6500
5900
9000
14000
1111111111111111111
BLASLAND BOUCK & USE
Client Sample ID: EX- 06
GC/MS Volatiles
Lot -Sample #...: C2C130119-003
Date Sampled. ..: 03/11/02
Prep Date.. ....: 03/14/02
Prep Batch #...: 2073113
Dilution Factor: 1
Analyst ID.....: 010099
PARAMETER
Acetone
Benzen e
Bromodichloromethan e
Chloroform
l , 2 -Dichloroethan e
1 , 1-Dichloroethen e
1 , 2 -Dichloropropane
Ethylbenzen e
Methylene chloride
Toluene1,1 , 2-Trichloroethan e
Trichloroethen e
Viny l chlorid e
Xylenes (total)
SURROGATE
Toluen e -d8
1, 2-Dichloroethane-d4
4-Bromofluorobenzene
Dibromof luorome thane
Work Order #. . .
Date Received. .
Analysis Date. .
Analysis Time..
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
99
95
88
103
EWAH01AA
03/13/02
03/14/02
13:12
5 mL
HP5
Mafrr-i y - W&TKD
MS Run i. ......; 2073057
Final Wgt/Vol. . s 5 raL
SW846 8260B
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1 • 0 ..-'.
2.0
3.0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
{74 - 116)
(73 - 122)
UNITS MDL
ug/L 2 . 5
ug/L 0.40
ug/L 0.30
ug/L 0.49
ug/L 0.49
ug/L 0.51
ug/L 0.46
ug/L 0.49
ug/L 0.36
ug/L 0.22
ug/L 0.44
ug/L 0.39
ug/L 0.60
ug/L 0.96
15
11111111111111111
BLASLAND BODCK & LEE
Client Sample ID: EX-07
GC/MS Volatiles
Lot -Sample ft...: C2C080166-002
Date Sampled. . . : 03/06/02
Prep Date.. ....: 03/12/02
Prep Batch #. . . : 2071132
Dilution Factor: 10
Analyst ID. . . . . : 01009 9
PARAMETER
Acetone
Benzene
Bromodichloromethan e
Chloroform
1,2 -Dichloroe thane
1, 1-Dichloroethen e
1 , 2 -Dichloropropane
Ethylbenzene
Methylene chlorid e
Toluene
1,1 , 2 -Trichloroethane
Trichloroethen e
Vinyl chloride
Xylenes (total )
SURROGATE
Toluene-d 8
l,2-Dichloroethane-d44 -Bromo f luorobenzene
D ibromof luorome thane
NOTB(S) :
1 Estimate d result . Resul t i s les s (tu n RL .
Work Order f . . .
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. . . . :
RESULT
80 J
ND
ND
ND
270
ND
ND
ND
ND
48
ND
ND
ND
ND
PERCENT
RECOVERY
84
117
83
115
EV5FN1AA
03/08/02
03/12/02
13:0 6
5 mL
Matrix. ........: WATER
MS Run #.......:
Final Wgt/Vol. . : 5 mL
HP5
SW846 8260B
REPORTING
LIMIT
100
10
10
10
10
10
10
10
20
10
1010 ...-•;.
20
30
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS MDL
ug/L 25
ug/L 4 . 0
ug/L 3 . 0
ug/L 4 . 9
ug/L 4 . 9
ug/L 5 . 1
ug/L 4.6
ug/L 4 . 9
ug/L 3 . 6
ug/L 2.2
ug/L 4 . 4
ug/L 3.9
ug/L 6 . 0
ug/L 9.6
I
1111111111111111111
BLASLAND BOUCK & LBB
Client Sample ID: EX-08
GC/MS Volatiles
Lot-Sample*...: C2C080166-0
Prep Date. .....: 03/12/02
Prep Batch #....- 2071132
Dilution Factor: 3000
Analyst ID. ....: 010099
PARAMETER
Acetone
Benzene
Bromodichloromethan e
Chlorofor m
1 , 2 -Dichloroethane
l, l-Dichloroethen e
1 , 2 -Dichloropropane
Ethylbenzen eMethylene chlorid e
Toluene
1,1 , 2-Trichloroethane
Trichloroethene
Viny l chlorid e
Xylene s (total)
SURROGATE
Toluen e -d8
1 , 2 -Dichloroethane ~d4
4 -Bromo f luorobenzene
Dibromofluoromethan e
NOTB(S) :
33 Work Order #. . .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
58000
ND
ND
ND
17000O E
ND
2000 J
ND
ND
17000
ND
ND
ND
ND
PERCENT
RECOVERY
93
107
76
116
E V5 FP1 AA
03/08/02
03/12/02
09:57
5 mL
Matrix
MS Run * - - . . - - -•
Final Wgt/Vol.. : 5 mL
HP5
SW846 8260B
REPORTING
LIMIT
30000
3000
3000
3000
3000
3000
3000
3000
6000
3000
30003000 ,-•;:
6000
9000
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS
ug/L
ug/L
ug/L
ug/L
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
ug/Lug/Lug/L
ug/L
MDL
7500
1200
910
1500
1500
1500
1400
1500
1100
680
1300
1200
1800
2900
E Estimate d result . Resul t coiiccntralio n exceed s th e calibratio n ranee .
J Eaimaie d result . Resul t i t le u tha n RL .
1 Q
1111111111111111111
Lot-Sample # . . . : C2C080166-003
Date Sampled. ..: 03/06/02
Prep Date. .....: 03/12/0 2
Prep Batch #. . . : 2071132
Dilution Factor: 5000
Analyst ID.....: 034635
PARAMETER
Acetone
Benzene
Bromodichloromethane
Chlorofor m
1 , 2-Dichloroethane
1, 1-Dichloroethene
1, 2-Dichloropropane
Ethylbenzene
Methylen e chlorid e
Toluene
1,1 , 2-Trichloroethan e
Trichloroethen e
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene-d 8
l,2-Dichloroethane-d4
4 -Bromo f luorobenzene
Dibromofluorome thane
NOTB(S) :
J Estimate d result . Resul t i s let s tha n RL .
BLASLAND BODCK
Client Sample ID
GC/MS Volati:
Work Order #. . .
Date Received. .
IVnii l A/R ^ f t T^a^^•nUCL.LjrO.LE> L/O.L-C • •
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
70000
ND
ND
ND
190000
ND
2300 J
ND
ND
23000
ND
ND
ND
ND
PERCENT
RECOVERY
96
94
80
104
i LEB
: EX-08
Les
EV5FP2AA Matrix
03/08/02 MS Run
03/12/02
13:5 5
5 mL Final f
Ut>«;fltr J
SW846 8260B
REPORTING
LIMIT UNITS
50000 ug/L
5000 ug/L
5000 ug/L
5000 ug/L
5000 ug/L
5000 ug/L
5000 ug/L
5000 ug/L
10000 ug/L
5000 ug/L
5000 ug/L
5000 /'. ug/L
10000 ug/L
15000 ug/L
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
* u&Tm>#
fgt/Vol.. : 5 mL
MDL
12000
2000
150 0
2400
2400
2600
2300
2400
180 0
1100
2200
2000
3000
4800
1 Q
1111111111111111111
BLASLAND BOUCK i LEE
Client Sample ID: EX-09
GC/MS Volatiles
Lot-Sample #...: C2C080166-004
Date Sampled. . . : 03/06/02
Prep Date. .....: 03/12/02
Prep Batch tt. ..: 2071132
Dilution Factor: 2000
Analyst ID. ....: 010099
PARAMETER
Acetone
Benzen e
Bromodichlorome thane
Chlorofor m
1 , 2 -Dichloroethane
1, l-Dichloroethene
1 , 2 -Dichloropropane
Ethylbenzene
Methylene chloride
Vinyl chloride
Xylenes (total)
Toluene
1,1 , 2-Trichloroethane
Trichloroethen e
SURROGATE
Toluene-d8
i,2-Dichloroethane-d4
4 -Bron\o£luorobenzene
Dibromof. voromethane
NOTE(S) :
Work Order # . . . :
Date Received. . :
Analysis Date . . :
Analysis Time . . :
Initial Bgt/Vol:
Instrument ID. . :
Method. ........:
RESULT
30000
ND
ND
ND
87000 E
ND
640O
ND
ND
ND
2200 J
30000
ND
ND
PERCENT
RECOVERY
95
116
88
116
EVSFT1AA
03/08/02
03/12/02
11:5 5
5 mL
Matrix,
MS Run
* W&TT2D
#.
Final Wgt/Vol . . : 0 mL
HP5
SW846 8260B
REPORTING
LIMIT
20000
2000
2000
2000
2000
2000
2000
2000
4000
4000
6000
2000
2000
2000
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS
ug/L
ug/L
ug/L
ug/Lug/L
ug/L
ug/Lug/Lug/L
ug/L
ug/L
ug/L
ug/Lug/L
MDL
5000
790
610
970
970
1000
920
970
720
120 0
190 0
450
870
780
E Estimate d result . Resul t concentratio n exceed s th e calibratio n range .
J Estimate d result . Resul t i » le u Du n RL .
1111111111111111111
Lot -Sample #. . . : C2C080166-004
Date Sampled. . . : 03/06/02
Prep Date... ...: 03/12/0 2
Prep Batch #...: 2071132
Dilution Factor: 3000
Analyst ID. ....: 034635
PARAMETER
Acetone
Benzene
Bromodich l o r ome than e
Chlorofor m
1 , 2 -Dichloroethane
1, l-Dichloroethen e
1,2 -Dichloropropane
Ethylbenzene
Methylen e chlorid e
Toluene
1,1 , 2-Trichloroethan e
Trichloroethen e
Vinyl chloride
Xylene s (total )
SURROGATE
Toluene -d8
1 , 2-Dichloroethane-d4
4-Bromof luorobenzene
Dibromof luoromethane
MOTE(S):
J Estimate d result . Resul t i t les s du n RL .
BLASLAND BOtTCK I
Client Sample ID
GC/MS Volati]
Work Order #. . .
Date Received. .
Analysis Date. .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. . . ... •
RESULT
25000 J
ND
ND
ND
91000
ND
7000
ND
ND
39000
ND
ND
ND
ND
PERCENT
RECOVERY
97
94
82
99
. T.KB
• EX-09
Le s
EV5FT2AA
03/08/02
03/12/02
13:30
5 mL
HP5
SW846 8260!
REPORTING
LIMIT
30000
3000
3000
3000
3000
3000
3000
3000
6000
3000
3000
3000 ,;•:.'
6000
9000
RECOVERY
LIMITS
(76 - 110}
(61 - 128)
(74 - 116)
(73 - 122)
I1
1
Matrix
MS Run
Final
J
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
.........: WATER
#
Wgt/Vol. . : 5 mL
MDL
7500
1200
910
1500
1500
1500
1400
1500
1100
680
1300
1200
1800
2900 :
1111111111111111111
BLASLAND BOUCK & LEE
Client Sample ID: BX-10
GC/MS volatiles
Lot-Sample #...: C2C080166-005
Date Sampled. ..: 03/06/0 2
Prep Date. .....: 03/12/02
Prep Batch #...: 2071132
Dilution Factor: 100
Analyst ID. . . . . : 010099
PARAMETER
Acetone
Benzene
Bromodichloromethane
Chloroform
1 , 2 -Dichloroethane
1, 1-Dichloroethene
1 , 2 -Dichloropropane
Kthylbenzene
Methylene chloride
Toluene
1,1 , 2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene-d 8
1 , 2 -Dichloroethane -d4
4 -Bromo f luorobenzene
Dibromof luorome thane
NOTB(S) :
Work Order #. . .
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
33000 E
ND
ND
ND
12000 E
ND
9800 E
1600
ND
2900
ND
ND
140 J
5900
PERCENT
RECOVERY
93
96
94
100
EV5FW1AA
03/08/02
03/12/02
08:44
5 mL
Matrix.
MS Run
* WKTITD
#.......:
Final Wgt/Vol..: 5 raL
HP 5
SW846 8260B
REPORTING
LIMIT
100 0
100
100
100
100
100
100
100
200
100
100100 ..;•;:
200
300
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITSug/L
ug/L
ug/L
ug/L
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
MDL
250
40
30
49
49
51
46
49
36
22
44
39
60
96
E Estimate d result . Resul t concentratio n exceed * th e calibratio n range .
J Estimate d result . Resu h i s le a thi n RL .
1111111111111111111
Lot -Sample »...: C2C080166-005
Date Sampled. . . : 03/06/02
Prep Date. .....: 03/12/02
Prep Batch ft...: 2071132
Dilution Factor: 1000
Analyst ID.....: 010099
PARAMETER
Vinyl chloride
Xylenes (total)
1, 1-Dichloroethene
1 , 2 -Dichloropropane
Bthylbenzene
Methylene chloride
Toluene
1,1 , 2 -Trichloro e thane
Acetone
Benzene
Bromodichloromethane
Chlorofor m
1 , 2 -Dichloroethane
Trichloroethene
SURROGATE
Toluene -d8
1, 2 -Dichloroethane -d4
4 - Bromof luorobenzene
Dibromofluoromethane
BLASLAND BOUCK I
Client Sample ID:
GC/MS Volati]
Work Order #. . . :
Date Received. . :
Analysis Date . . :
Analysis Time . . :
Initial Wgt/Vol:
Instrument ID. . :
Method. ........:
RESULT
ND
5300
ND
1100 0
140 0
ND
3000
ND
44000
ND
ND
ND
14000
ND
PERCENT
RECOVERY
96
109
86
112
i LEE
: EX-10
Le s
EV5FW2AA
03/08/02
03/12/02
11:3 1
5 mL
HP 5
SW846 82601
REPORTING
LIMIT
2000
3000
100 0
100 0
100 0
2000
100 0
100 0
10000
100 0
100 0100 0 ."•;."
100 0
100 0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Matrix
MS Run
Final 1
3
UNITS
ug/L
ug/L
ug/Lug/L
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
* WATER«.
Jgt/Vol.. : 5 mL
MDL
600
960
510
460
490
360
220
440
2500
400
300
490
490
390
111 BLASLAND BOOCK & USE
Client Sample ID: NS-09
GC/MS Volatiles
1iiiiiiiiiiiiiii
Lot-Sample ft...: C2C200151-00 1
Date Sampled. ..: 03/18/02
Prep Date. .....: 03/22/0 2
Prep Batch #...: 2081189
Dilution Factor: 1
Analyst ID.....: 034635
PARAMETER
Acetone
Benzene
Bromodichloromethan e
Chloroform
1 , 2-Dichloroethane
1, l-Dichloroethene
1 , 2-Dichloropropane
Ethylbenzene
Methylene chloride
Toluene
1,1,2 -Trichloroe thane
Trichloroethene
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d 4
4 -Bromof luorobenzene
Dibrotnof l uorome thane
KOTE(S):
J Estimate d remit . Rciul t i i les s tha n RL .
Work Order #...-.
Date Received. . :
Analysis Date . . :
Analysis Time . . :
Initial Wgt/Vol:
Instrument ID. . :
Method. ........:
RESULT
ND
ND
ND
0.6 4 J
1400 B
7.8
0.53 J
8.2
3.8
180 B
1.9
4.7
47 E
25
PERCENT
RECOVERY
88
79
101
91
EWMM51AA Matrix
03/20/02 MS Run
03/22/02
14:0 7
• WA*n?o#.......-.
5 mL Final Wgt/Vol. . : 5 mL
HP5
SW846 8260B
REPORTING
LIMIT UNITS
10 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
2 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 , ug/L
2.0 ug/L
3 . 0 ug/L
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
MDL
2.5
0.40
0.30
0.49
0.49
0.51
0.46
0.49
0.36
0.22
0.44
0.39
0.60
0.96
E Estimate d rcjult . Resul t concetltralio n exceed s th e olibratio n range .
C"T»T 1017
IIIIIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Client Sample ID: NS-09
GC/MS Volatiles
Lot-Sample #...: C2C200151-00 1
Date Sampled...: 03/18/02
Prep Date. .....: 03/25/02
Prep Batch #...: 2084404
Dilution Factor: 60
Analyst ID.....: 03463 5
PARAMETER
Acetone
Benzen e
Bromodichloromethan e
Chloroform
1 , 2-Dichloroethane
1, l-Dichloroethene
1 , 2-Dichloropropane
Ethylbenzene
Methylen e chloride
Toluene
1,1,2 - Tri chloroethan e
Trichloroethen e
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene -d8
1, 2 -Di chloroethan e -d4
4 -Bromof luorobenzene
Dibromof luorome thane
NOTE(S):
Work Order # . . .
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
ND
ND
ND
140 0
ND
ND
ND
ND
150
ND
ND
42 J
ND
PERCENT
RECOVERY
97
84
76
90
EWMM52A A Matrix
03/20/02 MS Run
03/25/02
14:5 4
5 m L Final »
UpCnr3
SW846 8260B
REPORTING
LIMIT UNITS
600 ug/L
60 ug/L
6 0 ug/L
60 ug/L
6 0 ug/L
6 0 ug/L
60 ug/L
60 ug/L
120 ug/L
60 ug/L
60 ug/L
60 X'. ug/L
120 ug/L
180 ug/L
RECOVERY
LIMITS
(76 - 110)
(61 - 128 )
(74 - 116)
(73 - 122)
. U&TT7D......... nAlcR
#.
Igt/Vol . . : 5 mL
MDL
150
24
18
29
29
31
28
29
22
14
26
24
36
57
J Estimate d result . Resul t a less tha n RL .
CHPT . D-i
1111111111111111111
BLASLAND BOUCK & LEE
Client Sample ID: NS-10
GC/MS Volatiles
Lot-Sample t t ...: C2C200151-003
Date Sampled.. .: 03/18/02
Prep Date.. ....: 03/22/02
Prep Batch #...: 2081189
Dilution Factor: 1
Analyst ID....... 03463 5
PARAMETER
Aceton e
Benzen e
Bromodichloromethan e
Chlorofor m
1, 2-Dichloroethane
l, l-Dichloroethen e
1 , 2-Dichloropropan e
Ethylbenzen e
Methylen e chloride
Toluene
1,1, 2 -Tr ichloroe than e
Trichloroethen e
Vinyl chloride
Xylenes (total)
SURROGATE
Toluene -d8
l,2-Dichloroethane-d 4
4 -Bromo f luorobenzene
Dibromofluoromethane
Work Order #. . .
risi^rf a 17^r*^iV9f^L>Cil»C ACI-C.L VCU. • *
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
ND
ND
ND
13
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
85
110
86
112
EWMM91AA
03/20/02
03/22/02
16:22
5 mL
HP 5
Matrix. ........: WATER
MS Run #.......:
Final Wgt/Vo l . . : 5 mL
SW846 8260B
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0i . o .-•;.'
2.0 •
3.0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS MDL
ug/L 2 . 5
ug/L . 0.40
ug/L 0.30
ug/L 0.49
ug/L 0.49
ug/L 0.51
ug/L 0 . 46
ug/L 0.49
ug/L 0.36
ug/L 0.22
ug/L 0.44
ug/L 0.39
ug/L 0.60
ug/L 0 . 96
n-,'
1111111111111111111
Lot-Sanple #. . .: C2C130119-003
Date Sampled. . . : 03/11/02
Prep Date. ....... 03/14/02
Prep Batch #...: 2073127
Dilution Factor: 1
analyst ID. . . . . : 001562
PARAMETER
bis (2-Chloroethyl ) -
ether
4 -Nitrophenol
SURROGATE
Phenol -d5
2 - Fluorobiphenyl
Ni t robenz ene - dS
Te rphen y 1 - d 1 4
2 - Fluorophenol
2,4,6 -Tribromophenol
BIASLAND BOUCK £ LEE
Client Sample ED: EX- 06
GC/MS Semivolatiles
Work Order #... EWAH01AC Matrix. ........: WATER
Date Received.. 03/13/02 MS Run #.......: 2073022
Analysis Date.. 03/18/0 2
Analysis Time. . 12:30
Initial W^t/Vol 1000 mL Final wgt/Vol..: l mL
Instrument ID. . 721
Method. ........ SW84S 8270C
REPORTING
RESULT LIMIT UNITS MDL
ND 10 ug/L 1.4
ND 50 ug/L 1.8
PERCENT RECOVERY
RECOVERY LIMITS
64 (10 - 113)
83 (30 - 110)
75 (32 - 112)
83 (10 - 144)
63 (13 - 110)
101 (21 - 122)
27
1111111111111111111
Lot - Sample #... C2C080166-00 2
Date Sampled. .. 03/06/02
Prep Date. ..... 03/11/0 2
Prep Batch #. . . 2070291
Dilution Factor 1
Analyst ID..... 001562
PARAMETER
bis(2-Chloroethyl ) -
ethe r
4-Nitropheno l
SURROGATE
Pheno l -d 5
2 - Fluorobipheny l
Nitrobenzene-d 5
Terphenyl-dl 4
2 - Fluorophenol
2,4 , 6 -Tribromopheno l
BLASLAND BOUCK & LEE
Client Sample ID: EX- 07
GC/MS Semivolatiles
Work Order #. . . EV5FN1AC Matrix. ........: WATER
Date Received. . 03/08/02 MS Run #.......: 2070152
Analysis Date .. 03/13/0 2
Analysis Time.. 14:09
Initial Wgt/Vol 1000 mL Final Wgt/Vol. . : 1 mL
Instrument ID. . 721
Method. ........ SW846 8270C
REPORTING
RESULT LIMIT UNITS MDL
ND 10 ug/L 1.4
ND 50 ug/L 1.8
PERCENT RECOVERY
RECOVERY LIMITS
64 (10 - 113)
69 (3 0 - 110)
73 (3 2 - 112)
68 (10 - 144)
58 (1 3 - 110)
81 (21 - .122)
A a
11111111111
BLASLAND BODCK
Client Sample ID
& LBE
: EX- 08
GC/M S Semivolatiles
Lot-Sample #. . . : C2C080166-003
Date Sampled. ..: 03/06/02
Prep Date. .....: 03/11/02
Prep Batch #...: 2070291
Dilution Factor: 60
Analyst ID.....: 001562
PARAMETE R
bis (2-Chloroethyl) -
ether
4 - Ni t ropheno 1
SURROGATE
Phenol -d5
2 - Pluorobiphenyl
Nitrobenzene-d5Terphenyl -d!4
2 - Fluorophenol
2,4, 6-Tribromophenol
NOTE(S) :
NC Tli c recover y and/o r RPD were not calculated .
Work Order # . . .
Date Received. .
Analysis Date..
Analysis Time. .
Initial Wgt/Vol
Instrument ED. .
Method. ...,....:
RESULT
1800
ND
PERCENT
RECOVERY
NC,DIL
NC.DIL
NC,DIL
NC.DIL
NC.DIL
NC,DIL
EV5FP1AC Matrix .........: WATE R
03/08/02 MS Run •.......: 2070152
03/12/02
16:56
1000 mL Final Wgt/VoL.i 3 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
600 ug/L 86
3000 ug/L 110
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
OIL The concentratio n is estimated or not reporte d due 10 dilutio n or the presence of interferin g arulytes .
1
1
1
1
1
1
1
1
47
11 t
BLASLAND BODCK & LEE
1
1
1
1
1
1
1
1
1
\
Client Sample ID:EX-09
GC/M S Semlvolatiles
Lot-Saraple #. . . : C2C080166-004
Date Sampled. . . : 03/06/02
Prep Date.... ..: 03/11/02
Prep Batch #...: 2070291
Dilution Factor: 60
Analyst ID.....: 001562
PARAMETE R
bis (2-Chloroethyl) -
ether
4-Nitrophenol
SURROGATE
Phenol - d5
2 - Fluorobiphenyl
Nitrobenzene-d5
Terphenyl -d!4
2 - Fluorophenol
2,4 , 6 -Tribromophenol
NOTE(S) :
NC The recovery and/or RPD were not calculated.
Work Order # . . . :
Date Received. . :
Analysis Date. . :
Analysis Time. . :
Initial Wgt/Vol:
Instruraent ID. . :
Method. ........:
RESULT
2900
ND
PERCENT
RECOVERY
NC , OIL
NC,DIL
NC,DIL
NC,DIL
NC,DIL
NC,DIL
PVSPT1 AP Msit-T-n ir - WATT7D
03/08/02 MS Run f .......: 2070152
03/12/02
17:5 0
1000 mL Final Wgt/Vol. . : 3 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
600 ug/L 86
3000 ug/L 110
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - .122)
OI L The concentratio n Is estimate d or no t rcponcd du e to dilutio n or the presence of interferin g inalyte*.
1
1
1
1
1
1
1
1
11111111111
BLASLAND BOOC K
Client Sample ID
& LEE
: EX- 10
GC/M S Semivolatiles
Lot-Sample #...: C2C080166-005
Date Sampled. . . : 03/06/02
Prep Date. ....... 03/11/02
Prep Batch #. . . : 2070291
Dilution Factor: 20
Analyst ID. . . . . : 001562
PARAMETE R
bis (2-Chloroethyl) -
ether
4 -Nitrophenol
SURROGATE
Phenol -d5
2 - Fluor obiphenyl
Nitrobenzene-d5
Terphenyl-dl4
2 - Fluorophenol
2,4, 6 -Tribromophenol
NOTE(S) :
NC Th e recover y and/o r RP D wer e no t calculated .
Work Order #...
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method . . •
RESULT
4000 B
ND
PERCENT
RECOVER Y
NC,DIL
NC.DIL
NC,DIL
NC,DIL
NC , DIL
NC.DIL
EV5FW1AC Matrix. ........: WATE R
03/08/02 MS Run #.......: 2070152
03/12/02
18 :45
1000 mL Final Wgt/Vol.. : 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
200 ug/L 29
1000 ug/L 36
RECOVER Y
LIMITS
(10 - 113}
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - .122)
OIL Tic concentratio n is estimate d or not reporte d due to dilutio n or the pretence of interferin g analytes .
1
1
1
1
1
1
1
1
E Estimate d result. Resul t concentratio n exceed s the calibratio n range .
11111111111
BLASLAND BODC K
Client Sample ID
& LEE
: EX-10 $L-
GC/MS Semivolatiles
Lot-Sample #...: C2C080166-005
Date Sampled. ..: 03/06/02
Prep Date. .....: 03/11/02
Prep Batch tt...: 2070291
Dilution Factor: 100
Analyst 3D. . . . . : 001562
PARAMETE R
bis (2-Chloroethyl) -
ether
4-Nitrophenol
SURROGAT E
Phenol -d5
2 - Fluorobiphenyl
Nitrobenzene -d5
Terphenyl - d!4
2-Fluorophenol
2,4 , 6 -Tribromophenol
NOTE(S) :
NC The recovery aiid/or RPD were not calculated.
Work Order #. . .
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
4800
ND
PERCEN T
RECOVERY
NC , DIL
NC,DIL
NC.DIL
NC,DIL
NC,DIL
NC.DIL
EV5FW2AC Matrix. ........ r WATE R
03/08/02 MS Run #.......: 2070152
03/13/02
13:15
1000 niL Final Wgt/Vol.. -. 1 mi
721
SW846 8270C
REPORTIN G
LIMIT UNITS MDL
1000 ug/L 140
5000 ug/L 180
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
DIL The concentratio n is estimate d or not reporte d duv to dilutio n or Ihc presence or interferin g analytu.
1
1
1
1
1
1
1
1
OTT D-i t- f- c?V-M iT-^
I11 BLASLAND BODCK
Client Sample ID
& LEE
: NS-09
GC/MS Semivolatiles
1
1
1
1
1
1
1
1
1
1i
Lot-Sample #... C2C200151-001
Date Sanrpled . . . 03/18/02
Prep Date. . .... 03/21/02
Prep Batch #._. 2080243
Dilution Factor 1
Analyst ID. .... 00156 2
PARAMETER
bis (2-Chloroethyl ) -
ether
4-Nitropheno l
SURROGATE
Pheno l -d 5
2 - Fluorobipheny l
Ni t roben z en e - d5
Terphenyl-dl 4
2 - Fluorophenol
2,4 , 6 -Tribromopheno l
NOTE(S):
* Surrogat e recover y i s outsid e state d contro l limits .
Work Order #...
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vo l
Instrument ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVERY
4.3 *
80
85
65
18
84
EWMM51AC Matrix. ........: WATER
03/20/02 MS Run #.......:
03/22/02
12:17
1000 mL Final Wgt/Vol..: 1 tnL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L 1 . 8
RECOVERY
LIMITS
{10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
STL Pittsburgh 2020
I11 BLASLAND BOUCK
Client Sample ID
& LEE
: NS-09 RE
GC/MS Semivolatiles
1
1
1
1
1
1
1
1
ft fLot - Sample #... C2C200151-00 1
Date Sampled. . . 03/18/02
Prep Date.. .... 03/25/02
Prep Batch #. . . 2084333
Dilution Factor 1
Analyst ID..... 001562
PARAMETER
bis (2-Chloroethyl) -
ether
4 -Nitre-pheno l
SURROGATE
Phenol -d 5
2 - Fluorobiphenyl
Nitrobenzene- d5
Terphenyl-dl4
2 - Fluorophenol
2,4 , 6 -Tribromopheno l
NOTB(S) :
' Surrogat e rccuvcr y » outsid e state d contro l limits .
Work Order #.. .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wtft/Vo l
Instrument ID. .
Method. ........:
RESULT
ND
ND
PERCENT
RECOVERY
4.3 *
75
78
61
18
76
EWMM52AC Matrix. ........: WATER
03/20/02 MS Run ft.......:
03/27/02
20:42
100 0 mL Final W§rt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L 1.8
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
<13 - 110)
(21 - 122)
II
I
I
I
I
I
STL Pittsburgh 2026
I1
BLASLAND BOUCK £ LEE
1
1
1
1
1
1
1
1
1
Client Sample ID: NS-10
GC/MS Semivolatiles
Lot-Sample #...: C2C200151-003
Date Sampled. . . 03/18/02
Prep Date. ..... 03/21/02
Prep Batch #... 2080243
Dilution Factor l
Analyst ID..... 001562
PARAMETER
bis (2-Chloroethyl ) -
ether
4-Nitrophenol
SURROGATE
Pheno l -d 5
2 - Fluorobiphenyl
Ni t robenzene - d5
Terphenyl-dl 4
2 - Fluorophenol
2,4 , 6 -Tribromopheno l
Work Order # . . .
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vo l
Instrument ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVERY
80
78
67
64
63
81
T?tiJMMQl aP Mat- v*i -v - WZkTTPD
03/20/02 MS Run #.......:
03/22/02
13:12
100 0 mL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L 1.8
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
CTT . Pit-tsburcrh 2037
111111111111111111
Lot-Sample # . . . C2C200151-002
Date Sampled. .. 03/18/02
Prep Date. ..... 03/21/02
Prep Batch #... 2080243
Dilution Factor 1
Analyst ID..... 001562
PARAMETER
bi s ( 2 - Chloroethyl } -
ether
4-Nitropheno l
SURROGATE
Phenol -d5
2-Fluorobiphenyl
Nitrobenzene- d5
Te rpheny 1 - d.1 4
2 - Fluorophenol
2,4,6 - Tr ibromophenol
BLASLAND BOOCK
Client Sample ID
GC/MS Semivola
Work Order tt - . .Date Received. .
Analysis Date . .
Analysis Tim e . .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVERY
75
71
68
72
60
80
& LEE
: NS-11
tiles
EWMM71AC Matrix........-: WATER
03/20/02 MS Run #.......:
03/22/02
12:44
1000 mL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L 1.8
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(1.0 - 144)
(13 - 110)
(21 - 122)
S*
I
STL Pittsburgh 2032
11111111111
BLASLAND BOCTCK
Client Sample ID
& LEE
: NS-15
GC/MS Semivolatiles
Lot - Sample #... C2C200151-005
Date Sampled. . . 03/18/02
Prep Date. ..... 03/21/0 2
Prep Batch #... 2080243
Dilution Factor 1
Analyst ID. .... 001562
PARAMETER
bi s (2-Chloroethyl ) -
ether
4 -Nitrophenol
SURROGATE
Phenol -d5
2 -Fluorobipheny l
Nitrobenzene-d S
Terphenyl-dl 4
2 - Fluorophenol
2,4,6 - Tribromopheno l
Work Order #...
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVERY
76
74
78
77
66
81
EWMNF1AC Matrix.........: WATER
03/20/02 MS Run *.......:
03/25/02
11:5 2
100 0 mL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
50 ug/L \ . 8
RECOVERY
LIMITS
(10 - 113)
{30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
ST L Pittsburah 2047
II
II
III
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Lot-Sample #.
Date Sampled.
PARAMETER
BLASLAND BOTCK & LEE
Client Sample ID: EX-05
TOTAL Metals
..: C2C080166-001
..: 03/06/02 Date Received..: 03/08/02
RESULT
REPORTING
LIMIT UNITS METHOD
Matrix.......: WATER
PREPARATION- WORK
ANALYSIS DATE ORDE R ft
Batch #.
Arsenic
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
MOTE(S ) ;
: 2070128
7.1 B 10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time.. i
Instrument ID..: TRACEICP HS Run ft. ......:
228 200 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time.. :
Instrument ID..: TRACEIC P MS Run ».......:
ND 5.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time. . :
Instrument ID..: TRACEIC P MS Run 8.......:
16.5 J,B 5.0 ug/L SW846 6010B
Dilutio n Factor : 1 Analysi s Time . . :
Instrumen t ID..: TRACEICP MS Run 0.......:
15.2 5.0 ug/L SW846 6010B
Dilutio n Factor : 1 Analysi s Time.. :
Instrumen t ID . . > TRACEIC P M S Ru n t». ...... i
52600 150 ug/L SW846 6010B
Dilutio n Factor : 10 Analysi s Time..:
Instrumen t ID.. : TRACEIC P MS Run #.......-.
1640 40.0 ug/L SW846 6010B
Dilutio n Factor : 1 Analysi s Time...-
Instrumen t ID..i TRACEIC P M S Ru n f.......:
47.6 5.0 ug/L SW846 6010B
Dilution Factor : 1 Analysi s Time. . :
instrumen t ID . . : TRACEIC P M S Ru n *........
365 20.0 ug/L SW846 6010B
Dilutio n Factor : 1 Analysi s Time..:
Instrumen t ID..: TRACEIC P MS Run #.......:
03/11-03/12/02 EV5FH1AD
14:06 Analyst ID.....: 400149
2070022 MDL . ...........: 2.4
03/11-03/12/02 EV5FH1AK
14:06 Analyst ID. . ...i 400149
2070022 M D L . . . . . . . . . . . .: 1.1
03/11-03/12/02 EV5FH1AF
14:0 6 Analyst ID.....: 400149
2070022 MDL............: 0.47
03/11-03/12/02 EV5FH1AG
14:06 Analyst ID. ... .1 400149
2070022 M D L . . . . . . . . . . . .: 0.24
03/11-03/12/02 EV5FH1AH
14:06 Analyst I D . . . . .t 400149
2070022 MDL . ...........: 1.1
03/11-03/12/02 EV5FH1AJ
21:5 0 Analyst ID. ....: 400149
2070022 MDL............: 4.5
03/11-03/12/02 EV5FH1AK
14:06 Analyst ID. ....: 400149
2070022 MDL............: 1.8
03/11-03/12/02 HV5FH1AL
14:06 Analyst ID.....: 400149
2070022 M D L . . . . . . . . . . . .: 2.7
03/11-03/12/02 BV5FH1AM
14:06 Analyst ID ..... t 400149
2070022 M D L . . . . . . . . . . . .: 4.4
B Eaimate d mult. Retul t is tes s tha n RL .
I Metho d blan k contamination . Th e associate d metho d blan k contain s the targe t analyt e at a reportabl e level .
E Matri x interference .
CT>T. D-i
III
I Lot-Sample #...: C2C130119
Date Sampled...: 03/11/02
I
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-00 3
BLASLAND BOUCK & LEE
Client Sample ID: EX-06
TOTAL Metals
Date Received..: 03/13/0 2
Matrix.WATER
PARAMETER RESULT
REPORTING
LIMIT UNITS METHO D
PREPARATION - WOR K
ANALYSIS DATE ORDE R
Prep Batch # . . .: 2073174
Arsenic
Barium
Beryllium
Cadmiu m
Chromium
Manganese
Nickel
Selenium
Zinc
NOTE(S):
ND
24.6 B
ND
ND
13.6
256
2.2 B
ND
17.5 B
10,0 ug/L SW846 6010B 03/14-03/17/02 EWAH01AD
Dilution Factor: 1 Analysis Time..: 14:45 Analyst ID. . . . . : 40014 9
Instrument ID. . : TRACEICP MS Run » . . . . . . .: 2073052 MDL . . . . . . . . . . . .: 2.4
200 ug/L SW846 6010B 03/14-03/17/O2 EWAH01AE
Dilution Factor: 1 Analysis Time..: 14:45 Analyst ID... ..: 40014 9
Instrument ID. . : TRACBICP MS Run 8. ......: 2073052 MDL . ...........: 1.1
5.0 ug/L SW846 6010B 03/14-03/17/02 EWAH01AF
Dilution Factor: l Analysis Time..: 14:45 Analyst I D . . . . .: 40014 9
Instrument ID..: TRACEICP MS Run f t . . . . . . .: 2073052 MDL . . . . . . . . . . . .: 0.47
5.0 ug/L SW846 6010B 03/14-03/17/02 EWAH01AG
Dilution Factor: l Analysis Time..: 14:45 Analyst I D . . . . .: 40014 9
Instrument ID. . : TRACEICP MS Run fl. .,.....: 2073052 MDL . . . . . . . . . . . . .: 0.24
5.0 ug/L SW846 6010B 03/14-03/17/O2 EWAH01AH
Dilution Factor: 1 Analysis Time..: 14:45 Analyst ID.....: 400149
Instrument ID..: TRACEICP MS Run *.......: 2073052 MDL............: 1.1
15.0 ug/L SW846 6010B 03/14-03/17/O2 EWAH01AJ
Dilution Factor: 1 Analysis Time..: 14:45 Analyst ID... ..: 400149
Instrument ID. . : TRACEICP MS Run tt. ......: 2073052 MDL . . . . . . . . . . . .: 0.45
40.0 ug/L SW846 6010B 03/14-03/17/O2 EWAH01AK
Dilution Factor: 1 Analysis Time..: 14:45 Analyst ID... ..: 400149
Instrument ID..: TRACEICP MS Run 8. ......: 2073052 M D L . . . . . . . . . . . .: 1.8
5.0 ug/L SW84 6 6010B 03/14-03/17/02 EWAH01AL.
Dilution Factor: 1 Analysis Time..: 14:45 Analyse ID.....: 400149
Instrument ID. .: TRACEICP MS Run tt. ......: 2073052 M D L . . . . . . . . . . . .: 2.7
20.0 ug/L SW846 6010B 03/14-03/17/O2 EWAH01A M
Dilution Factor: 1 Analysis Time..: 14:45 Analyst ID.....: 40014 9
Instrument ID..: TRACEICP MS Run ».......: 2073052 M D L . . . . . . . . . . . .: 4.4
I) Esiinialct l rcsiili . Kcnil i o lew ilun RL.
41
1111111111111111111
BLASLAN D BOUC K & LEE
Client Sample ID: EX- 07
TOTAL Metals
Lot -Sample #...: C2C080166-002
Date Sampled. . .: 03/06/02 Date Received. .: 03/08/02
REPORTING
PARAMETE R RESULT LIMIT UNITS METHO D
Prep Batch #...: 2070128
Arsenic ND 10.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACBIC P
Barium 29.5 B 200 ug/L
Dilution Factor: 1
Instrument ID...- THACEIC P
Beryllium 0.63 B,J 5.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
Cadmiu m ND 5.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
Chromium ND 5.0 ug/L
Dilution Factor: 1
Instrument ID . . : TRACEIC P
Manganese 1170 15.0 ug/L
Dilution Factor: 1
Instrument ID . . : TRACEIC P
Nickel 13.8 B 40.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
Selenium ND 5.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
Zinc 5.7 B 20.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
NOTE(S) :
SW84 6 6010B
Analysis Time . . :
MS Run ft .......:
SW846 6010B
Analysis Time . ..:
MS Run #.......:
SW846 6010B
Analysis Time . . i
MS Run tt .......:
SW846 6010B
Analysis Time. . :
M S Run f t ....... i
SW846 6010B
Analysis Time. . i
M S Run #.......:
SW846 6010B
Analysis Time . . :
MS Run #.......:
SW846 6010B
Analysis Time. . :
MS Run #.......:
SW84 6 6010B
Analysis Time. . :
M S Run ».......:
SW846 6010B
Analysis Time..:
M S Run tt ....... i
Matrix. ......:
PREPARATION -
ANALYSIS DATE
03/11-03/12/02
14:28 Analyst ID. . . . .
2070022 MDL . ...........
03/11-03/12/02
14:28 Analyst ID. . . . .
2070022 MDL . ...........
03/11-03/12/02
14 :28 Analyst ID. . . . .
2070022 MDL . ...........
03/11-03/12/02
14:2 8 Analyst ID. . . . .
2070022 MDL . ...........
03/11-03/12/02
14,2 8 Analyst ID. . . . .
2070022 MDL . ...........
03/11-03/12/02
14:2 8 Analyst ID. . . . .
2070022 MDL . ...........
03/11-03/12/02
14:2 8 Analyst ID. . . . .
2070022 MDL . ...........
03/11-03/12/02
14:2 8 Analyst ID . . . . .
2070022 MDL . ...........
03/11-03/12/02
14:28 Analyst ID. . . . .
2070022 MDL.. ..........
WATE R
WOR K
ORDE R #
EV5FN1AD
: 400149
: 2.4
BV5FW1AE
: 400149
i 1.1
EV5FN1AF
: 400149
: 0.47
EV5FN1AG
: 400149
: 0.24
EV5FN1AH
: 400149
: 1.1
EV5EN1AJ
: 400149
: 0.4S
EV5FN1AK
: 400149
: 1.8
EV5FN1AL
: 400149
: 2.7
EV5FN1AM
: 400149
: 4.4
B Estimate d result . Resul t Is less tha n RL .
J Metho d blan k contamination . Th e associate d metho d blan k contai m th e targe t analyl e at a reportabt e level .
STL Pittsbura h
IIIIIIIIIIIIIIIII
Lot-Sample #.
Date Sampled.
PARAMETE R
BLASLAN D BOT7C K & LEE
Client Sample ID: EX-08
TOTA L Metals
.: C2C080166-003
.: 03/06/02 Date Received..: 03/08/02
RESULT
REPORTIN G
LIMIT UNITS METHO D
Matrix.......: WATE R
PREPARATION- WOR K
ANALYSIS DATE ORDE R ft
Prep Batch #...: 2070128
Arsenic 6.6 B
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
MOTE(S):
21.5 B
11.7 J
6.3 J
35.7
196000
758
72.3
1000
10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time. . :
Instrument ID. . : TRACEIC P MS Run tt. ......:
200 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time. . :
Instrument ID..: TRACEIC P MS Run tt.......:
5.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time.. :
Instrument ID. . : TRACEIC P MS Run It. ......:
5.0 ug/L SW846 601OB
Dilution Factor: 1 Analysis Time - .:
Instrument ID..: TRACEIC P MS Run f t . . . . . . .:
5.0 ug/L SW846 6010B
Dilution Factori 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run ft.......:
1500 ug/L SH846 6010B
Dilution Factor: 100 Analysis Time. . :
Instrument ID. - : TRACEIC P MS Run #........-
40.0 ug/L SW846 6010B
Dilution Factors 1 Analysis Time. . :
Instrument ID..: TRACEIC P MS Run #.......:
5.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Tiroe..i
Instrument ID..: TRACEICP MS Run #.......:
20.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run f.......:
03/11-03/12/02 BV5FP1AD
14:48 Analyst ID.....: 400149
2070022 MDIi. ...........: 2.4
03/11-03/12/02 EV5FP1AK
14:48 Analyst I D . . . . .: 400149
2070022 M D L . . . . . . . . . . . .: 1.1
03/11-03/12/02 EV5PP1AF
14i48 Analyst ID.....: 400149
2070022 M D L . . . . . . . . . . . .: 0.47
03/11-03/12/02 EV5FP1AG
14:46 Analyst ID. ....: 400149
2070022 M D L . . . . . . . . . . . .: 0.24
03/11-03/12/02 EV5FP3.AH
14:48 Analyst ID.....: 400149
2070022 M D L . . . . . . . . . . . .: 1.1
03/11-03/12/02 EV5FPXAJ
22:1 2 Analyst ID.....: 400149
2070022 M D L . . . . . . . . . . . .: 44.6
03/11-03/12/02 KV5FP1-AK
14:48 Analyst ID .....: 400149
2070022 HDL............: 1.8
03/11-03/12/02 EV5FP1AI.
14:48 Analyst ID.....: 400149
2070022 MDL . ...........: 2.7
03/11-03/12/02 BV5FPXA M
14:4 8 Analyst ID....... 40014 9
2070022 M D L . . . . . . . . . . . .i 4.4
B Estimate d result . Resul t i s les s tha n RL .
J Metho d blan k contamination . Th e associate d metho d blan k contain s th e targe t anaryt e a t a reportabt e level .
IIIIIIIIIIIIIIIII
Lot-Sample f.
Date Sampled.
PARAMETE R
BLASLAHD BOtJCK & USE
Client Sample ID: EX-09
TOTAL Metals
.: C2C080166-004
.-. 03/06/02 Date Received..: 03/08/02
RESULT
REPORTING
LIMIT UNITS METHO D
Matrix.......: WATE R
PREPARATION- WOR K
ANALYSIS DATE ORDE R ft
Prep Batch #.
Arsenic
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
ROTB(S);
: 2070128
3.0 B 10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time.. :
Instrument ID.. •. TRACEIC P M S Run 8.......:
12.7 B 200 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEICP MS Run H . . . . . .. i
11.0 J 5.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEICP MS Run ».......:
2.0 B.J 5.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..-,
instrument ID..: TRACEIC P MS Run #.......:
_.!-' '
21.7 5.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..!
Instrument ID..: TRACEIC P MS Run tt.......:
108000 1500 ug/L SW846 601OB
Dilution Factor: 100 Analysis Time..:
Instrument ID..: TRACEIC P MS Run f t . . . . . . .:
407 40.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACBIC P NS Run #.......:
42.5 5.0 ug/L SW846 601OB
Dilution Factor: 1 Analysis Time..:
Instrument ID... TRACEIC P MS Run #....... i
983 20.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run #.......:
03/11-03/12/02 EV5FT1AD
14:54 Analyst ID .....: 400149
2070022 MDL. ...........: 2.4
03/11-03/12/02 EVSFT1AE
14:54 Analyst ID.....: 400149
2070023 M D L . . . . . . . . . . . .: 1.1
03/11-03/12/02 BV5FT1AF
14:54 Analyst ID. ....: 400149
2070022 MDL . ...........: 0.47
03/11-03/12/02 BV5FT1AG
14:54 Analyst ID.....: 400149
2070022 M D L . . . . . . . . . . . .: 0.24
03/11-03/12/02 EV5PT1AH
14:54 Analyst ID .....: 400149
2070022 MDL............. 1.1
03/11-03/12/02 EV5FT1AJ
22:28 Analyst ID.....: 400149
2070022 MDL. ...........: 44.6
O3/11-03/12/02 BV5PT1AK
14:54 Analyst ID .....: 400149
2070022 MDL.. ..........: 1.8
03/11-03/12/02 EV5FT1AL
14:54 Analyst ID.....: 400149
2070022 M D L . . . . . . . . . . . .1 2.7
03/11-03/12/02 BV5FT1AM
14 154 Analyst ID.....: 400149
2070022 MDL. ...........: 4.4
B Estimate d result . Resul t is les s tha n RL .
J Metho d blan k contamination . Th e associate d metho d blan k contain s th e targe t analyt e at a reponabl e level .
fifl
IIIIIIIIIIIIIIIIIII
BLASLAHD BOUCK & LEE
Client Sample ID: EX-10
TOTAL Metals
Lot -Sample §. .
Date Sampled. .
PARAMETE R
Prep Batch #..
Arsenic
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
.: C2C080166-005
. : 03/06/02 Date Received. . :
REPORTIN G
RESULT LIMIT UNITS
. : 2070128
3.1 B 10.0 ug/L
Dilution Factor: 1
Instrument 10..: TRACEIC P
14.3 B 200 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
12.1 J 5.0 ug/L
Dilution Factor: 1
Instrument ID . . : TRACEIC P
1.1 B,J 5.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
32.8 5.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
101000 1500 ug/L
Dilution Factor: 100
Instrument ID . . : TRACEIC P
292 40.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
33.0 5.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
789 20.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
03/08/02
METHO D
SW846
Analysis
MS Ru n f t
SW846
Analysis
M S Ru n f l
SW846
Analysis
M S Ru n f t
SW846
Analysis
M S Ru n 1 *
SW846
Analysis
M S Ru n f t
SW846
Analysis
M S Ru n f t
SW846
Analysis
M S Ru n #
SW846
Analysis
MS Ru n 0
SW846
Analysis
M S Ru n 8
6010B
Time . . :
6010B
Time . . :
6010B
Time . . :
6010B
Time . . :
6010B
Time. . ;
6010B
Time . . :
6010B
Time . . :
6010B
Time . . :
6010B
Time . . :
.......:
14:59
2070022
14:59
2070022
14:59
2070022
14:59
2070022
14:59
2070022
22:34
2070022
14:59
2070022
14:59
2070022
14:59
2070022
Matrix. .......
PREPARATION-
ANALYSIS DATE
03/11-03/12/02
Analyst ID. . . . .
MDL . ...........
03/11-03/12/02
MD L ............
03/11-03/12/02
Analyst ID. . . . .
MDL . ...........
03/11-03/12/02
Analyst ID. . . . .
MDL . ...........
03/11-03/12/02
Analyst ID .....
MDL . ..........:
03/11-03/12/02
Analyst ID.
MDL . ...........
03/11-03/12/02
Analyst ID. . ... .
MDL . ...........
03/11-03/12/02
Analyst ID . - . . .
MD L ............
03/11-03/12/02
Analyst ID . . . . .
MD L ............
WATE R
WOR K
ORDE R f t
EV5FW1AD
: 400149
: 2.4
EV5FW1AB
: 400149
: 1.1
EV5FW1AF
: 400149
: 0.47
EV5FWLAG
: 400149
: 0.24
BV5FW1AH
t 400149
> 1.1
BV5PW1AJ
: 400149
: 44.6
BV5FW1AK
: 400149
: 1.8
BV5FW1AL
: 400149
: 2.7
EV5FW1AM
: 400149
: 4.4
NOTE(S)
B Estimate d resul t Resul t is les s ma n RL .
i Metho d blan k contamination . Th e associate d metho d blan k contain s th e targe t analyt e at a reportabl e level .
69
1II
• Lot-Sample #•- -: C2C200151-001
Date Sampled...: 03/18/02
BLASLAND BOUCK & LEE
Client Sample ID: NS-09
TOTAL Metals
Date Received..: 03/20/0 2
I
I
I
I
I
I
I
I
I
I
I
I
I
PARAMETER RESULT
REPORTING
LIMIT UNITS METHO D
Matrix....... r WATE R
PREPARATION- WOR K
ANALYSI S PATE ORDE R f t
Prep Batch #...: 2080158
Arsenic 2.5 B
Barium
Beryllium
Cadmiu m
Chromium
Manganese
Nickel
Selenium
Zinc
346
ND
ND
5.9
12800
6.6 B
5.2
5.8 B
10.0 ug/L SW846 6010B 03/21-03/26/02 EWMM51A D
Dilution Factor: 1 Analysis Time..: 09:24 Analyst ID.....: 400149
Instrument 10..: TRACEICP MS Run #..,....: 2060030 M D L . . . . . . . . . . . .: 2.4
200 ug/L SW846 6010B 03/21-03/26/O2 EWMMSIA B
Dilution Factor. 1 Analysis Time..: 09:2 4 Analyst ID.....: 400149
instrument ID..: TRACEICP MS Run & . , . . . . .: 2080030 M D L . . . . . . . . . . . .: 1.1
5.0 ug/L SW846 6010B 03/21-03/26/02 EWMM51A F
Dilution Factor: 1 Analysis Time..: 09:24 Analyst ID.....: 400149
Instrument ID..: TRACEIC P MS Run «.......: 2080030 MDL............: 0.47
5.0 ug/L SW84 6 6010B 03/21-03/26/02 EWMM51A G
Dilution Factor: ^ Analysis Time...- 09:24 Analyst ID.....: 400149
Instrument ID... TRACEIC P MS Run f t . . . . . . .: 2080030 MDL............: 0.24
5.0 ug/L SW846 6010B 03/21-03/26/02 BNMK51A H
Dilutio n Factor : 1 Analysi s Time..: 09>2 4 Analys t ID.....: 400149
Instrument ID..t TRACEICP MS Run it.......: 2080030 MDL............ i 1.1
30.0 ug/L SW846 6010B 03/21-03/26/02 BWMM51AJ
Dilutio n Factor : 2 Analysi s Time..: 15:17 Analys t ID.....: 400149
Instrument ID..: TRACEICP MS Run #.......: 2080030 MDL. ...........: 0.89
40.0 ug/L SW846 6010B 03/21-03/26/02 BHMM51AK
Dilution Factor: 1 Analysis Time..: 09:24 Analyst ID.....: 400149
Instrument ID..: TRACEIC P MS Run ».......: 2080030 M D L . . . . . . . . . . . .: 1.8
5.0 ug/L SW846 6010B 03/21-03/26/02 EWMM5OA L
Dilution Factor: 1 Analysis Time...- 09:24 Analyst ID.....I 400149
Instrument ID.. : TRACEIC P MS Run ft. ......: 2080030 M D L . . . . . . . . . . . .: 2.7
20.0 ug/L SW846 6010B 03/21-03/26/02 EWMM51A M
Dilution Factor: 1 Analysis Time..: 09i34 Analyst ID.....I 400149
Instrument ID..: TRACEICP MS Run «.......: 2080030 M D L . . . . . . . . . . . .: 4.4
NOTE(S) ;__________
B Estimate d result . Rciul t is les s tha n RL .
3003
tI
I
I
I
I
I
I
I
I
I
II
I
I
I
I
I
I
BLASLAMD BOUCK & LEE
Client Sample ID: NS-10
TOTAL Metals
Lot -Sample #.
Date Sampled.
PARAMETE R
Prep Batch ft.
Arsenic
Barium
Beryllium
Cadmiu m
Chromium
Manganese
Nickel
Selenium
Zinc
. . : C2C200151-003
..: 03/18/02 Date Received. .:
REPORTING
RESUL T LIMIT UNITS
..: 2080158
N D 10.0 ug/L
Instrument ID..: TRACEIC P
98.5 B 200 ug/L
instrument ID..: TRACEIC P
ND 5.0 ug/L
Dilution Factor: 1
Instrument ID . .' : TRACEIC P
ND 5.0 ug/L
Instrument ID. . i TRACEIC P
2.1 B 5.0 ug/L
Instrument ID..: TRACEIC P
1860 15.0 ug/L
Instrument ID . . : TRACEIC P
15.1 B 40.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEIC P
ND 5.0 ug/L
Instrument ID..: TRACEIC P
9.3 B 20.0 ug/L
Instrument ID..: TRACEIC P
03/20/02
METHO D
SW84 6 6010B
MS Run tt .......:
SW846 6010B
MS Run * .......:
SW84 6 6010B
Analysis Time. . :
MS Run t) ....... i
SW846 6010B
Analysis Time. . :
MS Run ft .......:
SW846 6010B
MS Run «.......:
SW846 6010B
Analysis Time. . :
MS Run *.......:
SW846 E010B
Analysis Time . . :
MS Run ft .......:
SW846 6010B
MS Run tt. ......:
SH846 6010B
Analysis Tine. . :
M S Run 8 .......:
Matrix. ......: WATE R
PREPARATION - WOR K
ANALYSIS DATE ORDE R #
03/21-03/26/02 EWMM91A D
10:02 Analyst ID.....: 400149
2080030 MDL. ........... t 2.4
03/21-03/26/02 EWMM91A E
10:02 Analyst ID.....: 400149
2080030 MDL.. ..........: 1.1
03/21-03/26/02 EWMM91A F
10:02 Analyst ID. .... i 400149
2080030 MDL. ...........: 0.47
03/21-03/26/02 EWMM91A G
10:02 Analyst ID. ...... 40014 9
2080030 MDL. ...........: 0.24
03/21-03/26/02 BWMM91A H
10i02 Analyst ID.....: 400149
2080030 MDL. ...........: 1.1
03/21-03/26/02 BWMM91A J
10:02 Analyst ID.....: 400149
2080030 MDL. ...........: 0.4S
03/21-03/26/02 EVJMM91AK
10:02 Analyst ID ....... 400149
2080030 MDL. ...........: 1.8
03/21-03/26/02 EWMM91A L
10:02 Analyst ID.....I 400149
2080030 MDL. ...........: 2.7
03/21-03/26/02 EWMM91A M
10:02 Analyst ID.....: 400149
2080030 MDL. ........... i 4.4
NOTE(S) :
B Estimate d resulc . Resul t I s less (tan RL .
30Q5
IIIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Client Sample ID: NS-11
TOTAL Metals
Lot-Sample #. . . : C2C200151
Date Sampled. . . : 03/18/02
PARAMETE R RESULT
Prep Batch g. . . : 2080158
Arsenic 2,7 B
Barium 73 . 0 B
Beryllium ND
Cadmium N D
Chromium 1.4 B
Manganese 117
Nickel ND
Selenium N D
Zinc ND
-002
Date Received. . :
REPORTING
LIMIT UNITS
10 . 0 ug/L
Instrument ID. . : TRACEIC P
200 ug/L
Instrument ID... TRACEIC P
5 . 0 ug/L
Dilution Factor: l
Instrument ID... TRACEIC P
5 . 0 ug/L
Dilution Factor: 1
Instrument ID . . : TRACEIC P
5 . 0 ug/L
Dilution Factor: 1
Instrument ID... TRACEIC P
15.0 ug/L
Dilution Factor i 1
Instrument ID..: TRACEIC P
40.0 ug/L
Dilution Factor: 1
Instrument ID . . i TRACEIC P
5 . 0 ug/L
Dilution Factor: I
Instrument ID . . : TRACEIC P
20.0 ug/L
Instrument ID. . : TRACEIC P
03/20/02
METHO D
SW846 6010B
M S Run ».......:
SW846 6010B
Analysis Time . . :
M S Run 8 .........
SW846 6010B
MS Run 8 .......:
SW84 6 6010B
M S Run It .......:
SH846 6010B
Analysis Time. . :
M S Run ».......:
SH846 6010B
MS Run #.......:
SW846 6010B
MS Run «.......:
SW846 6010B
MS Run S .......:
SW846 6010B
Analysis Time. . :
MS Run ft .......:
Matrix. ......:
PREPARATION-
ANALYSIS DATE
03/21-03/26/02
09:46 Analyst ID. . . . .
2080030 MDL. ...........
03/21-03/26/02
09:46 Analyst ID. ....
2080030 MDL. ...........
03/21-03/26/02
09:46 Analyst ID. . . . .
2080030 MDL. ...........
03/21-03/26/02
09i46 Analyst ID. . . . .
2080030 MDL . ...........
03/21-03/26/02
09:46 Analyst ID. . . . .
2080030 MDL. .......
03/21-03/26/02
09:46 Analyst ID.
2080030 MDL . ...........
03/21-03/26/02
09:46 Analyst ID.
2080030 MDL . ...........
03/21-03/26/02
09.4 6 Analyst ID. . .. .
2080030 MDL. ...........
03/21-03/26/02
09:46 Analyst ID. . .. .
2080030 MDL. ...........
WOR K
ORDE R #
BHMM71AD
: 400H9
: 2.4
BWMM7XA E
: 400149
: 1.1
EWMM71A F
: 400149
: 0.47
EWMM71A G
: 400149
: 0.24
BWW71AH
: 400149
: 1.1
EWMM71AJ
: 400149
: 0.45
EWMM71A K
: 400149i i.a
EWMM71A L
: 400149
: 2.7
EWMM71A M
,i 400149
, : 4.4
NOTE (5) ;
0 Estimate d result. Resul t is lea tlu n RL .
STL Pittsburgh 3004
IIIIIIIIIIIIIIIIIII
Lot-Sample ft...: C2C200151-005
Date Sampled.,.: 03/18/02
BLASLAND BOUCK & LEE
Client Sample ID: NS-15
TOTAL Metals
Date Received..: 03/20/02
Matrix.WATER
PARAMETER RESULT
REPORTING
LIMIT UNITS METHO D
PREPARATION - WOR K
ANALYSIS DATE ORDE R #
Prep Batch #...: 2080158
Arsenic
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
NOTB(S) ;
ND
305
ND
ND
4.5 B
10600
2.0 B
ND
ND
10.0 ug/L SW84 6 6010B 03/21-03/26/02 EWMNF1A D
Dilution Factor: 1 Analysis Time..: 10:13 Analyst I D . . . . .: 400149
Instrument ID..t TRACEICP MS Run f t . . . . . . .: 2080030 M D L . . . . . . . . . . . .: 2.4
200 ug/L SW846 6010B 03/21-03/26/02 EWMHF1AE
Dilution Factor: 1 Analysis Time..: 10:13 Analyst ID.....: 40014 9
Instrument ID..: TRACEICP MS Run & . . . . . . .: 2080030 MDL.. .......... i 1.1
5.0 ug/L SW846 6010B 03/21-03/26/02 EWMNF1A F
Dilution Factor: 1 Analysis Time..: 10-.13 Analyst ID.....: 40014 9
Instrument ID..: TRACEICP MS Run 8....... i 2080030 M D L . . . . . . . . . . . .: 0.47
5.0 ug/L SW846 6010B 03/21-03/26/02 EWMNF1A G
Dilution Factor: 1 Analysis Time..-. 10:13 Analyst ID.....: 400149
Instrument ID, . : TRACEIC P MS Run #.......: 2080030 M D L . . . . . . . . . . . .: 0.24
5.0 ug/L SW846 6010B 03/21-03/26/02 EWMNF1A H
Dilutio n Factor : 1 Analysi s Time..: 10:1 3 Analys t ID.....: 40014 9
Instrument ID. . : TRACEICP MS Run ft.......: 2080030 MDL............: 1.1
30.0 ug/L SW846 6010B 03/21-03/26/02 ENMNF1A7
Dilutio n Factor : 2 Analysi s Time..: ISiS O Analys t ID.....: 400149
Instrument ID..: TRACEIC P MS Run ft......... 2080030 MDL . ...........: 0.89
40.0 ug/L SW846 6010B O3/21-03/26/02 EHMNF1AK
Dilutio n Factor : 1 Analysi s Time..: 10:13 Analys t ID.....: 40014 9
Instrument ID..i TRACEICP MS Run «.......: 2080030 NDL. ...........: 1.8
5.0 ug/L SW84 S 6010B 03/21-03/26/02 EWMNF1A L
Dilution Factor: 1 Analysis Time. .: 10-.13 Analyst I D . . . . .S 400149
Instrument ID..: TRACEICP MS Run ».......: 2080030 MDL............: 2.7
20.0 ug/L SW84 6 6010B 03/21-03/26/02 EWMNF1A M
Dilution Factor: 1 Analysis Time..: 10:13 Analyst ID.....: 400149
Instrument ID..: TRACEICP MS Run ».......: 2080030 MDL. ...........: 4.4
B Estimate d result . Resul t is less tha n RL .
STT. Pi t-fshiir-rrh
I11111111111111111
Lot-Sample tt ...: C2C090133-001
Date Sampled. ..: 03/08/02
Prep Date. .....: 03/10/02
Prep Batch #...: 2069099
Dilution Factor: l
Analyst ID.....: 034635
PARAMETE R
Acetone
Chloroform
1 , 2 -DichJLoroethane
cis-1, 2-Dichloroethene
trans-1, 2-Dichloroethene
1, 1-Dichloroethene
1, 2-Dichloropropane
Methylene chloride
Tetrachloroethene
i , l , 2 -TrichloroethaneTrichloroethene
Vinyl chloride
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d4
4-Bromofluorobenzene
Dibromo f 1 uorome thane
NOTE (S) :
J Estimate d reaill. Resul t it less tha n RL .
BLASLAND BODCK I
Client Sample ID
GC/MS Volati:
Work Order #.. .
nji^t* u**f (^*i vo^JLsa l*t? A.d«G -L V tSU. • •
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method ........:
RESULT
ND
ND
0.53 J
ND
ND
ND
0.66 J
ND
ND
2.5
0.62 J
ND
PERCENT
RECOVERY
92
100
87
99
i LEE
: NS-13
Les
EV6601AA
03/09/02
03/10/02
18 : 12
5 mL
HP5
SW846 82601
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
2.0
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Mal~f -i -v * WATTED
MS Run ft .......:
Final Wgt/Vol . . .- 5 mL
3
UNITS MDL
ug/L 2 . 5
ug/L 0.49
ug/L 0.49
ug/L 0.29
ug/L 0.37
ug/L 0.51
ug/L 0.46
ug/L 0.36
ug/L 0.36
ug/L 0.44
ug/L 0.39
ug/L 0.60
ISTL Pittsburgh 13
I11111111111111111
BLASLAND BOUC K & LEE
Client Sanqple ID: NS-24
GC/MS Volatiles
Lot - Sample #...: C2C160140-013
Date Sampled. ..: 03/14/02
Prep Date.... ..: 03/19/02
Prep Batch #. . . : 2078361
Dilution Factor: 1
Analyst ID.....: 034635
PARAMETE R
Acetone
Chloroform
1 , 2 -Dichloroethane
cis-1, 2-Dichloroethene
trans-1 , 2-Dichloroethene
1, l-Dichloroethene
1, 2-Dichloropropane
Methylene chloride
Tetrachloroethene
l, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
SURROGAT EToluene -d8
l,2-Dichloroethane-d4
4 -Bromof luorobenzene
Dibromofluoromethane
Wor k Order f t ...
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
.. ND
ND
PERCENT
RECOVERY
76
94
87
102
EWHEC1AA
03/16/02
03/19/02
20:20
5 mL
HP5
Matrisr - WZVFP D
MS Run #.......:
Final Wgt/Vol . . : 5 mL
SW846 8260B
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
2.0
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS MD L
ug/L 2 . 5
ug/L 0.49
ug/L 0.49
ug/L 0.29
ug/L 0.37
ug/L 0.51
ug/L 0.46
ug/L 0.36
ug/L 0.36
ug/L 0.44
ug/L 0.39
ug/L 0.60
ISTL Pittsburgh 28
1111111111111111111
Lot-Sample ft...: C2C080109-005
Date Sampled. ..: 03/07/02
Prep Date. .....: 03/11/02
Prep Batch tt...: 2070158
Dilution Factor: 250
Analyst ID.....: 010099
PARAMETER
Aceton e
Chloroform
1 , 2-Dichloroethane
cis-1 , 2-Dichloroethene
trans-1 , 2-Dichloroethen e
1, 1-Dichloroethene
1 , 2-Dichloropropan e
Methylen e chlorid e
Tetrachloroethene
1,1 , 2 -Trichloroethan e
Trichloroethene
Viny l chloride
SURROGATE
Toluene -d8
l,2-Dichloroethane-d 4
4-Bromofluorobenzen e
Dibrotno f luoromethane
BLASLAND BOOCK I
Client Sample ID
GC/MS Volati;
work Order #...
Date Received. .
Analysis Date. .
Analysis Time . .
Initial Wgt/Vol
Instrument ID . .
Method. ........:
RESULT
ND
ND
6700
ND
ND
ND
ND
ND
ND
...N D
' ND
ND
PERCENT
RECOVERY
79
101
86
110
i LEE
: NS-35
Les
EV4X71AA
03/08/02
03/11/02
12:42
5 mil
HP5
SW846 8260]
REPORTING
LIMIT
2500
250
250
250
250
250
250
500
250
250
250
500
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Matrix
MS Run
Final V
3
UNITS
ug/L
ug/L
ug/l .
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
. wATis n
f t
fgt/Vol. .: 5 mL
MDL
620
120
120
72
93
130
120
90
90
110
98
150
STL Pittsburah 16
1111111111111111111
Lot-Sample #...: C2C080109-004
Dat e Sampled. . . : 03/07/0 2
Prep Date. .....: 03/09/02
Prep Batch #. . . : 2068179
Dilution Factor: 1500
Analyst ID. . . . . : 034635
PARAMETER
Acetone
Chloro f or m
1 , 2-Dichloroethane
cis - 1 , 2 -Dichloroethene
trans-1 , 2 -Dichloroethen e
1, l-Dichloroethene
l , 2-Dichloropropan e
Methylen e chlorid e
Tetrachloroethene
1 , 1 , 2 -Trichloroethan e
Trichloroethene
Vinyl chloride
SURROGATE
Toluene-d 8
1, 2-Dichloroethane-d4
4-Bromofluorobenzene
Dibrotno f luorome thane
BLASLAHD BOTJCK 1
Client Sample ID
GC/MS Volati:
Work Order «...
Date Received. .
ATI s i 1 TTCin 0 n^t*oMItd.Lyo.l-o UdtrC » •
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
ND
39000
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
97
94
82
102
i USE
: NS-36
Lea
EV4X41AA Matrix
03/08/02 MS Run
03/10/02
07:34
5 m L Final 1
HP 5
SW846 8260B
REPORTING
LIMIT UNITS
15000 ug/L
1500 ug/L
1500 ug/L
1500 ug/L
1500 ug/L
1500 ug/L
1500 ug/L
3000 ug/L
1500 ug/L
1500 ug/L
150 0 ug/L
3000 ug/L
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
• unmj
#.......: 2069003
«gt/Vol..: 5 mL
MDL
3800
730
730
430
560
770
690
540
540
650
590
900
STL Pittsburgh 15
I11111111111111
BLASLAND BOUC K & LEE
Client Sample ID: NS-37
GC/M S Volatiles
Lot-Sample*...: C2C160140-012
Date Sampled. ..: 03/14/02
Prep Date. .....: 03/21/02
Prep Batch #...: 2080515
Dilution Factor: 1
Analyst ID.....: 034635
PARAMETER
Acetone
Chloroform
1 , 2 -Dichloroethane
cis-1 , 2-Dichloroethene
trans-l, 2-Dichloroethene
1 , 1-Dichloroethene
1 , 2-Dichloropropane
Methyl ene chloride
. Tetrachloroethene
1,1,2- Tr ichloroethane
Tr ichl oroethene
Vinyl chloride
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d4
4-Bromofluorobenzene
D ibr omo f luororae thane
Work Order 8. . .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVER Y
84
90
93
94
EWHD91A A Matrix
03/16/02 MS Run
03/21/02
- WHTWP
#.......:
20:40
5 mL Final Wgt/Vol . - : 5 mL
HP 5
SW84 6 8260B
REPORTING
LIMIT UNITS
10 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
2 . 0 ug/L
1 . 0 ug/L
1 . 0 ug/L
1.0 ug/L
2 . 0 ug/L
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
MDL
2.5
0.49
0.49
0.29
0.37
0.51
0.46
0.36
0.36
0.44
0.39
0.60
STL Pittsburgh 27
111111111111111
BLASLAN D BOUC K & LE E
Client Sample ID: NS-38
GC/MS Volatiles
Lot -Sample ft. ..: C2C160140-011
Date Sampled. . . : 03/14/02
Prep Date.... ..: 03/22/02
Prep Batch #...: 2081189
Dilution Factor: 1
Analyst ID. . . . . : 03463S
PARAMETE R
Acetone
Chloroform
1,2-Dichloroethane
cis-l , 2 -Dichloroethene
trans -1,2 -Dichloroethene
1 , l-Dichloroethene
1 , 2-Dichloropropane
Methylene chloride
. Tetrachloroethene
1, 1,2-Trichloroethane
Trichloroethene
vinyl chloride
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d4
4 -Bromof luorobenzene
Dibromofluorome thane
Work Order #. . .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
31
ND
ND
ND
ND
ND
ND
ND
ND
ND
• N D
3.6
PERCENT
RECOVER Y
103
97
115
114
EWHD71AA
03/16/02
03/22/02
10:07
5 mL
HP5
Matrix. ........: WATE R
MS Run #
Final Wgt/Vol..: 5 mL
SW846 8260B
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
2.0
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS MD L
ug/L 2 . 5
ug/L 0.49
ug/L 0.49
ug/L 0.29
ug/L 0.37
ug/L 0.51
ug/L 0.46
ug/L 0.36
ug/L 0.36
ug/L 0 . 44
ug/L 0.39
ug/L 0.60
STL Pittsburgh 26
111 BLASLAND BOUCK
Client Sample XD
& LEE
: NS-39
CSC/M S Volatiles
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lot - Sample #...: C2C160140-009
Date Sampled. . . : 03/14/02
Prep Date. .....: 03/21/02
Prep Batch #....- 2080515
Dilution Factor : 2.5
Analyst ID.....: 034635
PARAMETER
Acetone
Chloroform
1 , 2-Dichloroethane
cis-1, 2-Dichloroethene
trans-l, 2-Dichloroethene
1, l-Dichloroethene1 , 2-Dichloropropane
Methylene chloride
Tetrachloroethene
1,1,2 -Trichloroe thane
Trichloroethene
Vinyl chloride
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d4
4-Bromof luorobenzene
Dibromo f luorome thane
NOTE(S) :
J Estimate d result . Resul t a lest tha n RL .
Wor k Order #. . .
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument XD. .
Method. ........:
RESUL T
ND
ND
46
ND
ND
ND
1.7 J
131.3 a
1.5 J1.4 or
9.7
PERCENT
RECOVERY
89
95
92
99
tprjirm 1 2XZ L Ma^T"iY • MRT'iPB
03/16/02 MS Run #.......:
03/21/02
23:47
5 tnL Final Wgt/Vol . . : 5 raL
HP5
SW846 8260B
REPORTING
LIMIT UNITS MDL
25 ug/L 6.2
2.5 ug/L 1.2
2.5 ug/L 1.2
2.5 ug/L 0.72
2.5 ug/L 0.93
2 . 5 ug/L 1 . 3
2 . 5 ug/L l . 2
5.0 ug/L 0.90
2 . 5 ug/L 0 . 90
2 . 5 ug/L 1 . 1
2 . 5 ug/L 0 . 98
5 . 0 ug/L 1 . 5
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - .122)
STL Pittsburgh 24
111111111111111111
• ST"
BLASLAND BOUCK & LEE
Client: Sample ID: NS-40
GC/MS Volatiles
Lot-Sample*...: C2C160140-008
Date Sampled...: 03/14/02
Prep Date. .....: 03/22/02
Prep Batch #. . . : 2081189
Dilution Factor : 200 0
Analyst ID.....: 034635
PARAMETER
Aceton e
Chloroform
1, 2-Dichloroethane
cis-1 , 2-Dichloroethene
trans-1 , 2-Dichloroethen e
1 , 1-Dichloroethene
1 , 2 -Dichloropropane
Methylen e chlorid e
Tetrachloroethen e
1 , 1,2-Trichloroethane
Trichloroethen e
Viny l chloride
SURROGATE
Toluene -d8l,2-Dichloroethane-d 4
4-Bromofluorobenzen e
Dibromofluoromethane
r . P i t - 1 - C5>-)1 1 r-rr h
Work Order #. . .
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. . . . :
RESULT
ND
ND
73000
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
87
93
82
98
EWHD11AA
03/16/02
03/22/02
13:1 4
5 mL
HP5
Matrix .........: WATER
MS Run #.......:
Final Wgt/Vol..: 5 mL
SW846 8260B
REPORTING
LIMIT
20000
2000
2000
2000
2000
2000
2000
4000
2000
2000
2000
4000
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
{73 - 122)
UNITS MDL
ug/L 5000
ug/L 970
ug/L 970
ug/L 570
ug/L 740
ug/L 1000
ug/L 920
ug/L 72 0
ug/L 720
ug/L 870
ug/L 780
ug/L 1200
23
11111111111111
BLASLAND BOUC K & LEE
Client Sample ID: NS-41
GC/MS Volatiles
Lot-Sample #...: C2C160140-006
Date Sampled. . . : 03/13/02
Prep Date.... ..: 03/19/02
Prep Batch #...: 2078361
Dilution Factor: 1
Analyst ID.....: 034635
PARAMETER
Acetone
Chloroform
1 , 2 -Dichloroethane
cis-1, 2 -Dichloroethene
trans-l, 2 -Dichloroethene
1, 1-Dichloroethene
1 , 2 -Dichloropropane
Methylene chloride
Tetrachloroethene
1 , 1 , 2 - Tr ichloroe thane
Trichloroethene
Vinyl chloride
SURROGAT E
Toluene -d8
1 , 2 -Di chloroethane - d4
4 -Bromof luorobenzene
Dibromof luor ome t hane
NOTE(S) :
J Estimate d result . Resul t \s less Uuii RL .
Work Order #.. .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
ND
36
1.2
ND
N D
ND1.2 a
1.7
0.55 J
2.3
2.9
PERCENT
RECOVER Y
91
86
92
96
EWHDT1A A
03/16/02
03/19/02
15:01
5 mL
HP5
Mat"r*i 3C • U^TUW
MS Run ft.. .....:
Final Wgt/Vol . . : 5 mL
SW846 8260B
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
2.0
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS MD L
ug/L 2 . 5
ug/L 0.49
ug/L 0 . 49
ug/L 0.29
ug/L 0.37
ug/L 0.51
ug/L 0.46
ug/L 0.36
ug/L 0 . 36
ug/L 0 . 44
ug/L 0 . 39
ug/L 0.60
STL Pittsburgh 21
BLASLAMD BOUCK & LEE
Client Sampl e ID: NS-42
GC/MS Volatiles
Lot - Sample #...-. C2C160140-007 Wor k Order f...: EWHDX1AA
Dat e Sampled...: 03/13/0 2
Prep Date...... : 03/22/02
Prep Batch #...: 2080515
Dilution Factor: 6
Analyst ID..... : 034635
IIII
II
I
I
I
I
I
II
I
I
I
I
I
I STL Pittsburgh
J Emulated result. Resul t is (es s Ihati RL.
Date Received..: 03/16/0 2
Analysis Date..: 03/22/02
Analysis Time..: 01:0 8
Initial Wgt/Vol : 5 mL
Instrument ID..: HP5
Method.........: SW846 8260B
Matrix...
MS Run #.
.: WATER
Final Wgt/Vol..: 5 mL
PARAMETER
Acetone
Chloroform
1 , 2-Dichloroethane
cis-1, 2-Dichloroethene
trans-1 , 2-Dichloroethene
1, l-Dichloroethene
1,2-Dichloropropane
Methyl ene chloride
Tetrachloroethene
1,1,2- Trichloroethane
Trichloroethene
Vinyl chloride
SURROGATE
Toluene -d8
l,2-Dichloroethane-d4
4 -Brotnof luorobenzeneDibromofluororaethane
NOTK(S) :
RESULT
ND
ND
110
18
N D
3.3 J
ND
ND
ND
ND
/ 7-5
36
PERCEN T
RECOVER Y
87
92
94
99
REPORTING
LIMIT
60
6.0
6.0
6.0
6.0
6.0
6.0
12
6.0
6.0
6.0
12
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS
ug/L
ug/L
ug/L
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
MD L
15
2.9
2.9
1.7
2.2
3.1
2.8
2.2
2.2
2.6
2.4
3.6
22
1111111111111111111
Lot-SainpleS...: C2C080109-003
Date Sampled. . . : 03/06/02
Prep Date. .....: 03/10/02
Prep Batch ft...: 2068179
Dilution Factor : 1
Analyst ID.....: 010099
PARAMETER
Acetone
Chlorofor m
1 , 2 -Dichloroethane
cis-1, 2-Dichloroethene
trans-1 , 2-Dichloroethene
1, 1-Dichloroeth.ene
l , 2 -Dichloropropane
Methylen e chloride
Tetrachloroethene
1,1 , 2 -Trichloroethan e
Trichloroethene
Viny l chlorid e
SURROGATE
Toluene -d8
l,2-Dichloroethane-d 4
4-Bromofluorobenzen e
Dibromof luoromethane
BLASLAND BOUCK 1
Client Sample ID
GC/MS Volati]
Wor k Order #. . . :
Date Received. . :
Analysis Date . . :
Analysis Time . . :
Initial Wgt/Vol:
Instrument ID. . :
Method. ........:
RESULT
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
91
103
89
105
i LEE
: NS-43
Les
EV4X31AA Matrix. ........: WATER
03/08/02 MS Run #.......: 2069003
03/10/02
03:55
5 mL Final Wgt/Vol..: 5 mL
HP5
SW846 8260B
REPORTING
LIMIT UNITS MDL
10 ug/L 2.5
1 . 0 ug/L 0.49
1.0 ug/L 0.49
1.0 ug/L 0.29
1.0 ug/L 0.37
1.0 ug/L 0.51
1.0 ug/L 0.46
2.0 ug/L 0.36
1.0 ug/L 0.36
1 . 0 ug/L 0 . 44
1.0 ug/L 0.39
2.0 ug/L 0.60
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
RTL Pittsburah 14
1111111111111111111
Lot-Sample #. ..t C2C080109-002
Date Sampled. ..: 03/06/02
Prep Date.... ..: 03/10/02
Prep Batch #...: 2068179
Dilution Factor: l
Analyst ID.....: 010099
PARAMETER
Aceton e
Chloroform
1 , 2-Dichloroethan e
cis-1 , 2-Dichloroethene
trans-x , 2-Dichloroethen e1, 1-Dichloroethen e
1 , 2 -Dichloropropane
.Methylen e chloride
Tetrachloroethen e1,1 , 2-Trichloroethan e
Trichloroethene
Viny l chlorid e
SURROGATE
Toluene-d8
1, 2-Dichloroethane-d4
4-Bromo f luorobenzen e
Dibromof luoromethane
BLASLAND BOUCK 1
Client Sample ID
GC/MS Volati:
Wor k Orde r #...
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Mot-Virvl
RESULT
ND
ND
ND
ND
ND
ND
ND
ND
ND
,ND
ND
ND
PERCENT
RECOVERY
95
101
83
107
i LEB
: NTS-44
Les
EV4X21AA Matrix. ........: WATER
03/08/02 MS Run #.......: 2069003
03/10/02
03:28
5 mL Final Wgt/Vol . . : 5 mL
HPS
SW846 8260B
REPORTING
LIMIT UNITS MDL
10 ug/L 2.5
1.0 ug/L 0.49
1.0 ug/L 0.49
1.0 ug/L 0.29
1.0 ug/L 0.37
1.0 ug/L 0.51
1.0 ug/L 0.46
2.0 ug/L 0.36
1.0 ug/L 0.36
1 . 0 ug/L 0 . 44
1.0 ug/L 0.39
2.0 ug/L 0.60
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Pif.t-.sburcrh 13
111111111111111111
Lot- Sample #...: C2C090133-002
Date Sampled. ..: 03/08/02
Prep Date.. ....: 03/10/02
Prep Batch #...: 2069099
Dilution Factor: l
Analyst ID.....: 034635
PARAMETER
Aceton e
Chloroform
1, 2-Dichloroethane
cis-1 , 2 -Dichloroethene
tran.s -1 , 2 -Dichloroethen e
l, l-Dichloroethene
1 , 2 -Dichloropropane
Methylene chloride
Tetrachloroethen e
1,1 , 2-Trichloroethane
Trichloroethene
Vinyl chloride
SURROGATE
Toluene -d8
1 , 2-Dichloroethane-d 4
4-Bromo f luorobenzene
Dibromofluoromethan e
NOTE(S) :
J Estimate d rcsuli . Rcuil l i t les s tha n RL .
BLASLAND BOOCK fi
Client Sample ID:
GC/MS Volatil
Work Order #. . .
Date Received. .
Analysis Date..
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
ND
3.3
6.4
ND
7.2
ND
1.1 J
ND
ND
3.3
1.9 J
PERCENT
RECOVERY
98
95
93
101
LEE
NS-45
es
EV6621AA Matrix. ........: WATER
03/09/02 MS Run #......,:
03/10/02
17:46
5 iti L Final Wgt/Vol . . : 5 mL
HP5
SW846 8260B
REPORTING
LIMIT UNITS MDL
10 ug/L 2 . 5
1.0 ug/L 0.49
1.0 ug/L 0.49
1.0 ug/L 0.29
1.0 ug/L 0.37
1.0 ug/L 0.51
1.0 ug/L 0.46
2.0 ug/L 0.36
1.0 ug/L 0.36
1.0 ug/L 0.44
1.0 Ug/L 0.39
2.0 ug/L 0.60
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
STL Pittsburgh 14
1111111111111111111
Lot - Sample #...: C2C130116-004
Date Sampled. ..: 03/12/02
Prep Date...... : 03/14/02
Prep Batch #...: 2073113
Dilution Factor: 1
Analyst ID.....: 010099
PARAMETE R
Vinyl chloride
Methyl ene chloride
Tetrachl oroethene
1, 1,2-Trichloroethane
Trichloroethene
Acetone
Chloroform
1 , 2 -Dichloroe thane
cis-1 , 2 -Dichloroethene
trans-1 , 2 -Dichloroethene
1 , 1 -Dichloroethene
l, 2-Dichloropropan.e
SURROGATE
Toluene -d8
l,2-Dichloroethane-d4
4 -Bromof luorobenzene
Dibromofluoromethane
KOTB(S) :
1 Estimate d result . Resul t is (ess tha n RL .
BLASLAND BOUCK t
Client Sample ID
GC/M S Volati]
Work Order #. . .
Analysis Date. .
Analysis Time. .Initial Wgt/vol
Instrument ID. .
Method. ........:
RESUL T
9.5
ND
1.2
ND
5.9
3.7 J
ND
12
0.33 J
. ND
1.8
ND
PERCENT
RECOVER Y
97
96
81
101
t LEE
: NS-46
Les
EWAG71A A Matrix.... .....: WATE R
03/13/02 MS Run #.......: 2073057
03/14/02
12:24
5 mL Final Hgt/Vol . . ; 5 mL
HP 5
SW84 6 8260B
REPORTING
LIMIT UNITS MDL
2 . 0 ug/L 0 . 60
2.0 ug/L 0.36
1.0 ug/L 0.36
1.0 ug/L 0.44
1.0 ug/L 0.39
10 ug/L 2 . 5
1.0 ug/L 0.49
1.0 ug/L 0.49
1.0 ug/L 0.29
1.0 ug/L 0.37
1.0 ug/L 0.51
1.0 ug/L 0.46
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Pi 1-t-«T~ni-rrrh 18
1111111111
11111111
BLASLAN D BOUC K & LEE
Client Sample ID: NS-47
GC/MS Volatiles
Lot-Sample #...: C2C130116-003 Work Order #... EWAG61A A Matru
Date Sampled...: 03/11/02
Prep Date. .....: 03/14/02
Prep Batch #...: 2073113
Dilution Factor: 10000
Analyst ID. . . . . : 010099
PARAMETE R
Vinyl chloride
Methylene chloride
Tetrachl oroethene
1, 1, 2-Trichloroethane
Trichloroethene
Acetone
Chloroform
l , 2 -Dichloroethane
cis-1 , 2 -Dichloroethene
trans-1 , 2 -Dichloroethene
1 , 1 -Dichloroethene
1 , 2 -Dichloropropane
SURROGATEToluene -d8
l,2-Dichloroethane-d4
4-Bromofluorobenzene
Dibromofluoromethane
NOTE(S) :
I Estimate d result . Resul t is less tha n RL .
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
N D
N D
ND
ND
ND
30000 J
ND
180000
ND
,-• N D
ND
ND
PERCENT
RECOVER Y
86
104
82
109
C . WATE R
03/13/02 MS Run *..--.-. s 2073O«?7sr~^/.*»ss/v« • a»* * LJ-U-
03/14/02
12:48
5 mL Final
HP5
SW846 8260B
REPORTIN G
LIMIT UNITS
20000 ug/L
20000 ug/L
10000 ug/L
10000 ug/L
10000 ug/L
100000 ug/L
10000 ug/L
10000 ug/L
10000 ug/L
10000 ug/L
10000 ug/L
10000 ug/L
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Wgt/Vol . . : 5 mL
MDL
6000
3600
3600
4400
3900
25000
4900
4900
2900
3700
5100
4600
17
111 BIASLAMD BO0CK & LEE
Client Sample ID: NS-48
GC/MS Volatiles
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lot-Sample #...: C2C130116-001
Date Sanqpled. . . : 03/11/02
Prep Date. .,...: 03/14/02
Prep Batch #...: 2073113
Dilution Factor: 1
Analyst ID.....: 010099
PARAMETE R
Vinyl chloride
Methylene chloride
Te t r achl o r oe thene
1,1,2 -Tr ichloroethane
Trichloroethene
Acetone
Chloroform
l, 2-DichJLoroethane
cis-l, 2-Dichloroethene
trans-1, 2-Dichloroethene
1, 1-Dichloroethene
l, 2-Dichloropropane
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d4
4-Bromof luorobenzene
Dibromof luoromethane
Work Order i . . . i
Date Received. . :
Analysis Date. . :
Analysis Time. . :
Initial Wgt/Vol:
Instrument ID. . :
Method. ........:
RESULT
ND
ND
ND
ND
ND
ND
ND
3.2
ND
,,N D
ND
ND
PERCENT
RECOVER Y
97
89
86
94
EWAG41AA
03/13/02
03/14/02
11:37
5 mL
HP5
Mat"T"IV • UATTTO
MS Run i.......: 2073057
Final Wgt/Vol . . : 5 ml.
SW846 8260B
REPORTING
LIMIT
2.0
2.0
1.0
1.0
1.0
10
1.0
1.0
1.0
1.0
1.0
1.0 .
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS MDL
ug/L 0.60
ug/L 0.36
ug/L 0.36
ug/L 0.44
ug/L 0.39
ug/L 2 . 5
ug/L 0.49
ug/L 0.49
ug/L 0.29
ug/L 0.37
ug/L 0.51
ug/L 0.46
Pi 15
111
111111111111111
BLASLAND BOUC K & LEE
Client Sample ID: NS-49
GC/M S Volatiles
Lot -Sample # ..: C2C080109-OOS W«ir> Orrlo-r & .- RV4X92A A Matn-iif- ...... • WATBT R
Date Sampled...: 03/07/02
Prep Date. .....: O3/09/02
Prep Batch #...: 2068179
Dilution. Factor: 1
Analyst ID.....: 010099
PARAMETE R
Acetone
Chloroform
1 , 2 -DiclLLoroethane
cis-1 , 2 -Dichloroethene
trans-1, 2 -Dichloroethene
1, 1 -Dichloroethene1, 2-Dichloropropane
Methylene chloride
Tetrachl oroethene
1,1,2- Trichloroethane
Trichloroethene
Vinyl chloride
SURROGATE
Toluene-d8
l, 2-Dichloroethane-d4
4-Bromof luorobenzene
Dibromofluoromethane
NOTE(S) :
Date Received. . :
Analysis Date. . :
Analysis Time . . :
Initial Wgt/Vol:
Instrument ID. . :
Method. ........:
RESULT
ND
1.8
2500 B
0.76 J
ND
1.3
2.4
5.3
2.6
3.7
5.1
15
PERCEN T
RECOVER Y
97
82
86
83
03/08/02 MS Run #.......: 2069003
03/09/02
23:24
5 mL Final Wgt/Vol . . : 5 mL
HP5
SW846 8260B
REPORTING
LIMIT UNITS MDL
10 ug/L 2 . 5
1.0 ug/L 0.49
1.0 ug/L 0.49
1.0 ug/L 0.29
1.0 ug/L 0.37
1 . 0 ug/L 0 . 51
1.0 ug/L 0.46
2.0 ug/L 0.36
1.0 ug/L 0,36
1.0 ug/L 0.44
1.0 ug/L 0.39
2.0 ug/L 0.60
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
E Estimate d result . Resul t concentratio n exceed s (h e calibratio n range .
1 Estimate d result . Resul t it less tha n RL .
Pi 19
111 BLASLAHD BOUCK & LEE
Client Sanple ID: NS-49
GC/MS Volatiles
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lot-Sairple ft...: C2C080109-006
Date Sampled. ..: 03/07/02
Prep Date. .....: 03/10/02
Prep Batch #...: 2068179
Dilution Factor: 300
Analyst ID.....: 010099
PARAMETER
Aceton e
Chloroform
1 , 2-Dichloroethane
cis-1 , 2-Dichloroethene
trans-1 , 2-Dichloroethene
1, 1-Dichloroethen e
1, 2-Dichloropropane
Methylen e chlorid e
tetrachloroethene
1,1 , 2 -Trichloroethane
Trichloroethen e
Vinyl chloride
/\
SURROGATE
Toluene-d 8
1 , 2-Dichloroethane-d4
4-Bromo f luorobenzene
Dibromo f luorom e thane
Work Order #. . . :
DatQ Received *
Analysis Date . . :
Analysis Time . . :
Initial Wgt/Vol:
Instrument ID . . :
Method. ........:
RESULT
ND
ND
7500
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
95
103
89
110
EV4X91AA
03/08/02
03/10/02
04:48
5 mL
HP5
Matrix
MS Run #.......: 2069003
Final Wgt/Vol . . : 5 mL
SW846 8260B
REPORTING
LIMIT
3000
300
300
300
300
300
300
600
300
300
300
600
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
MDL
750
150
150
86
110
150
140
110
110
130
120
180
STL Pittsburgh 17
111111111111111111
• orp
BLASLAND BOUC K & T.KB
Client Sample ID: NS-50
GC/M S Volatiles
Lot - Sample S ...: C2C160140-003
Date Sampled. . . : 03/13/02
Prep Date... ...: 03/22/02
Prep Batch #. . . : 2080515
Dilution Factor: 15
Analyst ID.....: 034635
PARAMETER
Acetone
Chloroform
1 , 2-Dichloroethan.e
cis-1 , 2-Dichloroethene
trans -1,2 -Dichloroethene
1 , 1 -Dichloroethene
1 , 2-Dichloropropane
Methylene chloride
Tetrachloroethene
l, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
SURROGATEToluene -d8
l , 2-Dichloroethane-d4
4 - Bromo f luorobenz ene
Dibromofluorome thane
HOTB(S) :
J Estimate d result. Result it less (ter n RL.
T n •* 4-4-—.*w.. _ _ i*
Work Order # . . .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESUL T
ND
ND
390
ND
ND
ND
ND
ND
ND
ND
ND
26 J
PERCENT
RECOVERY
86
92
87
97
EWHDM1A A Matrix .........: WATE R
03/16/02 MS Run 8. ......:
03/22/02
01:34
5 mL Final Wgt/Vol . . : 5 mL
HP 5
SW846 8260B
REPORTING
LIMIT UNITS MDL
150 ug/L 38
15 ug/L 7.3
15 ug/L 7.3
15 ug/L 4 . 3
15 ug/L 5.6
15 ug/L 7.7
15 ug/L 6.9
30 ug/L 5.4
15 ug/L 5 . 4
IS ug/L 6.5
15 ug/L 5.9
30 ug/L 9.0
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
17
1111111111111111111
Lot-Sample #...: C2C080109-007
Date Sampled. ..: 03/07/02
Prep Date. .....: 03/10/02
Prep Batch ft...: 2069099
Dilution Factor: 1000
Analyst ID.....: 034635
PARAMETE R
Acetone
Chloroform
1, 2 -Pichloroethane
cis-l, 2-Dichloroethene
trans-l, 2-Dichloroethene
1, l-Dictiloroethene
1, 2-Dichloropropane
Methylene chloride
tetrachloroethene
1,1, 2-Trichloroethane
Trichloroethene
Vinyl chloride
SURROGAT E
Toluene -de
1 , 2 -Dichloroethane-d4
4 - Bromof luorobenzene
Dibromof luorotnethane
BLASLAND BOUCK 1
Client Sample ID:
GC/MS Volati]
Wor k Order #...:
Date Received. . :
Analysis Date . . :
Analysis Time. . :
Initial Wgt/Vol:
Instrument ID. . :
Method. ........:
RESULT
ND
ND
38000
ND
ND
ND
ND
ND
ND
ND
' ND
ND
PERCEN T
RECOVER Y
95
102
81
109
t LEE
: NS-51
Les
EV40F1AA Matrix.
03/08/02 MS Run
03/10/02
20:24
5 mL Final 1
HP5
CLJQ A £ P "5 fi ntlCtiniOTiv o^DUO
REPORTING
LIMIT UNITS
10000 ug/L
1000 ug/L
1OO O ug/L
1000 ug/L
1000 ug/L
1000 ug/L
1000 ug/L
2000 ug/L
1000 ug/L
1000 ug/L
1000 ug/L
2000 . ug/L
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
• 1iJA'|*li'U
#
»gt/Vol..: 5 mL
MD L
2500
490
490
290
370
510
460
360
360
440
390
600
Pit-.t-.sh>urah 20
1111111111111111111
BIASLAHD BODC K & LEE
Client Sample ID: OOP- 03 0702
GC/MS Volatiles
Lot-Sample tf . . . : C2C080109-009
Date Sampled...: 03/07/02
Prep Date. .....: 03/11/02
Prep Batch. #. . . : 2070158
Dilution Factor: 2000
analyst ID.....: 010099
PARAMETE R
Acetone
Chloroform
1 , 2 -Dichloroe thane
cis - 1 , 2 - Dichloroethene
trans-1 , 2 -Dichloroethene
l, 1 -Dichloroethene
1, 2-Dichloropropane
Methylene chloride
Tetrachloroethene
1, 1, 2-Trichloroethane
Trichloroethene
Vinyl chloride
SURROGATE
Toluene -d8
1, 2-Dichloroetnane-d4
4-Bromofluorobenzene
Dibromof luoromethane
Work Order #. . .
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
ND
58000
ND
ND
ND
ND
ND
ND
, ND
ND
ND
PERCENT
RECOVER Y
94
104
82
112
EV40J1AA
03/08/02
03/11/02
13:05
5 mL
HP5
Matrix
MS Run
• ojn'i''L||jft
Final Wgt/Vol . . : 5 mL
SW84 6 8260B
REPORTING
LIMIT
20000
2000
2000
2000
2000
2000
2000
4000
2000
2000
2000
4000
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS
ug/L
ug/L
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/Lug/L
ug/L
MD L
5000
970
970
570
740
1000
920
720
720
870
?80
1200
r r,^ «. «-„!22
111111111111111111
~ C"TI
Lot -Sample 8...: C2C160140-002
Date Sampled. . . : 03/13/02
Prep Date.. ....: 03/19/02
Prep Batch #...: 2078361
Dilution Factor: 1
Analyst ID.....: 034635
PARAMETER
Acetone
Chloroform
1 , 2-Dichloroethane
cis-1, 2 -Dichloroethene
trans- 1 , 2 -Dichloroethene
1, 1-Dichloroethene
1 , 2 -Dichloropropane
Methylene chloride
Tetracfaloroethene1 , 1 , 2-Trichloroethane
Trichloroethene
Vinyl chloride
SURROGAT E
Toluene -d8
1 , 2-Dichloroethane-d4
4-Bromofluorobenzene
Dibromof luorome thane
NOTE(S) :
J Estimate d result . Resul t is less tha n RL.
r T ^ ™ ^ J _ _ I . i
BLASLAND BODCK &
Client Sample rD:
GC/M S Volatil
Work Order #. . .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
ND
5.2
0.44 J
ND
ND
ND
ND
0.80 J
ND
0.72 J
3.4
PERCENT
RECOVER Y
94
92
99
99
LEE
JUS-52
es
EWHDK1A A Matrix. ........: WATE R
03/16/02 MS Run #.......:
03/19/02
14 : 34
5 mL Final Wgt/Vol . . : 5 mL
HP5
SW846 8260B
REPORTING
LIMIT UNITS MDL
10 ug/L 2.5
1.0 ug/L 0.49
1.0 ug/L 0.49
1.0 ug/L 0.29
1.0 ug/L 0.37
1.0 ug/L 0.51
1 . 0 ug/L 0 . 46
2.0 ug/L 0.36
1 . 0 ug/L 0 . 36
1.0 ug/L 0.44
1.0 ug/L 0.39
2.0 ug/L 0.60
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
STL Pittsburgh 16
111 BLASLAND BOTJCK Sc LEE
Client Sample ID: DOT-031302
GC/MS Volatiles
1
1
1
1
1
1
1
1
1
1
1
Lot -Sample #...: C2C160140-005
Date Sampled. ..: 03/13/02
Prep Date. .....: 03/19/02
Prep Batch #. . . : 2078361
Dilution Factor: 1
Analyst ID.....: 034635
PARAMETER
Acetone
Chloroform
1 , 2 -Dichloroethane
cis-1 , 2-Dichloroethen e
tran s -1,2 - D i chloroethen e
1 , 1-Dichloroethene
1 , 2-Dichloropropan e
Methylene chloride
' Tetrachloroethene
1,1,2 - Trichloroethan e
Trichloroethene
Viny l chlorid e
SURROGATE
Toluene -d8
l, 2-Dichloroethane-d 4
4 -Bromo f luorobenzene
Dibroroo f luoromethan e
NOTE(S) :
Wor k Orde r # . . .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ..........
RESULT
ND
95 E
47 E
ND
ND
ND
ND
2.4
0.87 J
ND
0.46 J
ND
PERCENT
RECOVERY
94
102
92
107
EWHDQ1AA
03/16/02
03/19/02
21:13
5 mL
HP5
Matrix
MS Run # . .
Final Wgt/Vol . . : 5 mL
SW846 8260B
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
2.0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS
ug/L
ug/L
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
MDL
2.5
0.49
0.49
0.29
0.37
0.51
0.46
0.36
0.36
0.44
0.39
0.60
£ Estimate d result . Resul t concentratio n exceed s th e calibratio n range .
J Estimated result . Resul t i s les s tha n RL .
STL Pittsburgh 19
111 BLASLAND BOUC K & LE B
Client Sample ID: DUP-031302
GC/MS Volatiles
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lot-Sample #... : C2C160140-005
Date Sampled. . . : 03/13/02
Prep Date.... ..: 03/22/02
Prep Batch #...: 2081189
Dilution Factor: 6
Analyst ID.....: 034635
PARAMETE R
Acetone
Chloroform1, 2-Dicliloroetnajtie
cis-l, 2-Dichloroethene
trans- 1 , 2-Dichloroethene
1, l-Dichloroethene
l , 2 -Dichloropropane
Hethylene chloride
. Tetrachloroethene
1,1,2- Trichloroe thane
Trichloroethene
Vinyl chloride
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d4
4 -Bromof luorobenzene
Dibromofluorome thane
NOTE(S) :
J Estimated result. Resul t is less the n RL.
Work Order #. . .
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
180
83
ND
ND
ND
ND
4.9 J
ND
ND
ND
ND
PERCENT
RECOVER Y
89
96
87
104
EWHDQ2A A Matrix
03/16/02 MS Run
03/22/02
. WiTPB
#
11:01
5 mL Final Wgt/Vol..: 5 mL
HP 5
SW846 8260B
REPORTING
LIMIT UNITS
60 ug/L
6 . 0 ug/L
6 . 0 ug/L
6 . 0 ug/L
6 . 0 ug/L
6 . 0 ug/L
6 . 0 ug/L
12 ug/L
6 . 0 ug/L
6 . 0 ug/L
6 . 0 ug/L
12 ug/L
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
MDL
15
2.9
2.9
1.7
2.2
3.1
2.8
2.2
2.2
2.6
2.4
3.6
STL Pittsburgh 20
111 BLASLAN D BOUC K & LE E
Client Sample ID: NS-53
GC/MS Volatiles
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lot-Sample #...: C2C160140-OO X
Date S anqaled. ..: 03/13/02
Prep Date. .....: 03/18/02
Prep Batch #...: 2077420
Dilution Factor: l
Analyst ID. . . . . : 034635
PARAMETER
Acetone
Chloroform
1 , 2 -Dichloroethane
cis-l, 2 -Dichloroethene
trans -1,2 -Dichloroethene
l , l-Dichloroethene
1, 2-Dichloropropane
Methylene chloride
Tetrachloroethene
1,1,2- Trichloroe thane
Trichloroethene
Vinyl chloride
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d4
4 - Br omo f luorobenz ene
Dibrotnofluoromethane
NOTE(S) :
Work Order # . . .
Date Received. .
Analysis Date. .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ..........
RESULT
ND
99 E
47 B
ND
ND
ND
ND
2.5
1.1
ND
0.52 J
ND
PERCENT
RECOVER Y
97
95
95
110
EWHDH1AA
03/16/02
03/18/02
22:50
5 mL
HP5
Matrix • U&TR O
MS Run #.......: 2077285
Final Hgt/Vol . . : 5 mL
SW846 8260B
REPORTING
LIMIT
10
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
2.0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
UNITS MD L
ug/L 2 . 5
ug/L 0.49
ug/L 0.49
ug/L 0.29
ug/L 0.37
ug/L 0.51
ug/L 0.46ug/L 0.36
ug/L 0 . 36
ug/L 0 . 44
ug/L 0.39
ug/L 0.60
E Estimate d rutult . Rcnil l concentration exceed] the calibratio n range .
J Estimate d result . Resul t is less tha n R L
STL Pittsburgh 14
1111111111111111111
Lot- Sample #...: C2C160140-001
Date Sampled. ..: 03/13/02
Prep Date. . . . . . : 03/19/02
Prep Batch #...: 2078361
Dilution Factor: 5
Analyst ID.....: 034635
PARAMETE R
Acetone
Chloroform
1 , 2-Dichloroethane
cis-i, 2 -Dichloroethene
trans - 1 , 2 -Dichloroethene
1, l-Dichloroethene
1, 2-Dichloropropane
Methylene chloride
Tetrachloroethene
1,1, 2 -Trichloroethane
Trichloroethene
Vinyl chloride
SURROGATE
Toluene -d8
1, 2-Dichloroethane-d4
4 - Bromo f luor obenz ene
Dibromof luorome thane
NOTE(S) :
J Estiaiuctl result . Resul t is less du n Rl_.
BLASLAND BOtJCK
Client Sample ID
GC/MS Volati
Work Order #. . .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
170
82
ND
ND
ND
ND
4.4 J
ND
ND
' ND
ND
PERCENT
RECOVER Y
89
98
94
103
t LEE
: NS-53
les
EWHDH2A A Matrix. ........: WATE R
03/16/02 MS Run #.......:
03/19/02
17:13
5 mL Final Wgt/Vol..: 5 mL
HP5
SW846 8260B
REPORTING
LIMIT UNITS MDL
50 ug/L 12
5 . 0 ug/L 2 . 4
5 . 0 ug/L 2 . 4
5.0 ug/L 1.4
5 . 0 ug/L 1 . 9
5 . 0 ug/L 2 . 6
5 . 0 ug/L 2 . 3
10 ug/L 1 . 8
5 . 0 ug/L 1 . 8
5 . 0 ug/L 2 . 2
5 . 0 ug/L 2 . 0
10 ug/L 3 . 0
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
STL Pittsburgh 15
1111111111111111111
Lot -Sample f... : C2C130116-005
Date Sampled. . . : 03/12/02
Prep Date......: 03/14/02
Prep Batch #. . . : 2073113
Dilution Factor: 2500
Analyst ID.....: 010099
PARAMETER
Vinyl chlorideMethylene chloride
Tetrachloroethene
l , l , 2-Trichloroethane
Trichloroethene
AcetoneChloroform
1, 2-Dichloroethane
cis-1, 2-Dichloroethene
trans- 1 , 2-Dichloroethene
l , l-Dichloroethene
1, 2-Dichloropropane
SURROGATE
Toluene -d8
1 , 2 -Dichloroethane-d4
4 -Bromof luorobenzene
Dibromofluoromethane
NOTH(S) :
1 Estimate d result . Resul t Is less tha n RL .
BLASLAND BODCK I
Client Sample ID
GC/MS Volati]
Work Order #. . .
Date Received. .
ZVnal vni c Teat'1*jtno Lyoj-Q iyai.cz » •
Analysis Time. .
Initial Wgt/VolInstrument ID. .
Method. ........:
RESULT
ND
ND
ND
ND
ND
£500 J
ND
£9000
ND
ND
ND
ND
PERCENT
RECOVER Y
98
101
76
108
fc I£E
: NS-54
Lea
EWAG81AA
03/13/02
03/14/02
08:50
5 mL
HP5
SW84S 82601
REPORTING
LIMIT
5000
5000
2500
2500
2500
25000
2500
2500
2500
2500
2500
2500 ..-'•
RECOVER Y
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Matrix
MS Run
Final \
3
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/Lug/L
ug/L
ug/L
ug/L
ug/L
• UHTWD
ft.. .....: 2073057
*gt/Vol . . : 5 mL
MDL
1500
900
900
1100
980
620O
1200
1200
720
930
1300
1200
T3-!
1111111111111111111
Lot-Sample #. ..: C2C080109-008
Date Sampled. ..: 03/07/02
Prep Date. .....: 03/10/02
Prep Batch #....- 2068179
Dilutio n Factor : i
Analyst ID.....: 010099
PARAMETER
Aceton e
Chloroform
1 , 2-Dichloroethane
cis -1,2 -Dicbloroethene
trans-l , 2-Dichloroethene
1, 1-Dichloroethene
1 , 2-Dichloropropan e
.Methylen e chlorid e
Tetrachloroethen e
1,1,2 -Tr ichloroethane
Trichloroethene
Vinyl chloride
SURROGATE
Toluen e -d 8
1, 2-Dichloroethane-d4
4 -Bromof luorobenzene
Dibromofluoromethan e
NOTB(S) :
S Estimate d resul t Resul t i t les s tha n RL .
BLASLAND BODCK t
Client Sample ID
GC/MS Volati]
Work Order #...
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........:
RESULT
ND
ND
2.0
0.67 J
ND
0.51 J
ND
ND
ND
ND
0.39 J
ND
PERCENT
RECOVERY
93
103
85
106
i LEE
. CT-1
Le s
WVAOW1 2X& Mat-T-i v • WATIPB
03/08/02 MS Run ft.... .. .: 2069003
03/10/02
04:21
5 mL Final Wgt/Vol..: 50 mL
HP5
SW846 8260B
REPORTING
LIMIT UNITS MDL
10 ug/L 2 . 5
1.0 ug/L 0.49
1.0 ug/L 0.49
1.0 ug/L 0.29
1.0 ug/L 0.37
1.0 ug/L 0.51
1.0 ug/L 0.46
2.0 ug/L 0.36
1.0 ug/L 0.36
1.0 ug/L 0.44
1.0 ug/L 0.39
2.0 . ug/L 0.60
RECOVERY
LIMITS
(76 - 110)
(61 - 128)
(74 - 116)
(73 - 122)
Di *-t-
21
11111111111
BLASLAND BOUCK
Client Sample ID
t LEE
: NS-13
GC/M S Semivolatiles
Lot-Sample tt... C2C090133-001
Date Sampled. .. 03/08/02
Prep Date. ..... 03/11/02
Prep Batch #... 2070291
Dilution Factor 1.11
Analyst ID..... 001562
PARAMETE R
bis(2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGATE
Phenol -d5
2 - Fl uor obiphenyl
Nitrobenzene-clS
Terpheny 1 -dl4
2 - Fluorophenol
2,4, 6 -Tribromophenol
Work Order #.. .
Date Received. .
Analysis Date . .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVER Y
62
72
73
72
" 58
84
EV6601AC Matrix. ........: WATE R
03/09/02 MS Run #.-..... s 2070152
03/12/02
14:11
900 mL Final Wgt/Vol..: 1 mL
721
SW84 6 8270C
REPORTING
LIMIT UNITS MDL
11 ug/L 1.6
11 ug/L 1.0
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
III
I
I
II
STL Pittsburgh 24
111 BLASLAN D BOUC K & LEE
Client Sample ID : NS-24
GC/MS Semivolatiles
1
1
1
1
1
1
1
1
Lot-Sample #... C2C160140-013
Date Sampled. .. 03/14/02
Prep Date.. .... 03/18/02
Prep Batch #... 207732 6
Dilution Factor 1
Analyst ID..... 003200
PARAMETE R
bis(2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGAT E
Phenol -d5
. 2 -Fluorobiphenyl
Nitrobenzene-d5
Terphenyl-dl4
2-Fluorophenol
2,4,6- Tribromophenol
Work Order # . . .
Date Received. .
ATial v*3T R T^jit"^tuuatj~]foj.Q A/auc . .
Analysis Time. .
Initial Wgt/VolInstrument ID..
Method. ........:
RESULT
40
ND
PERCENT
RECOVER Y
74
74
77
74
78
65
EWHEC1A C Matrix. ........: WATE R
03/16/02 MS Run #.......: 2077154
03/19/02
16:31
1000 inL Final Wgt/Vol..: 1 mL
731
SW84 6 8270C
REPORTING
LIMIT UNITS MD L
10 ug/L 1.4
10 ug/L 0 . 91
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 -.. 122)
IIII
IIIISTL Pittsburgh 65
III
I
II
III
I
IIII
I
II
I
I
BLASLAND BOUCK & LEE
Client Sample ID: NS-35
GC/MS Semivolatiles
Lot-Sample ft...: C2C080109-005
Date Sampled...
Prep Date......
Prep Batch. #.. .
Dilution Factor
Analyst ID.....
03/07/02
03/11/02
2070291
1
007062
Work Order f t ...
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........
EV4X71AC
03/08/02
03/12/02
14:09
1000 mL
722
SW846 8270C
Matrix
MS Run #.......:
Final Wgt/Vol . . :
2070152
- . : 1 mL
PARAMETE R RESULT
bis(2-Chloroethyl) -
ether
bis (2-Ethylhexyl)
phthalate
SURROGATE
ND
ND
PERCENT
RECOVERY
Phenol-d 5
2-Fluorobiphenyl
Nitrobenzene-d5
Terphenyl -d!4
2-Fluorophenol
2,4 , 6 -Tribromophenol
56
82
110
75
85
96
REPORTING
LIMIT UNITS
10
MDL
10
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 r 110)
(21 - 122)
ug/L
ug/L
1.4
0.91
46
I
I
I
I
I
I
I
I
I
I
I
II
I
I
I
I
I
I
BLASLAND BOUCK & LEE
Client Saiqple ID: NS-36
GC/M S Semivolatiles
Lot-Sample #. ..: C2C080109-004
Date Sampled...: 03/07/02
Prep Date......: 03/11/02
Prep Batch ft...: 2070291
Dilution Factor: 1
Analyst ID..... = 007062
PARAMETER_________
bis(2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGATE__________Phenol-d5
2-Fluorobiphenyl
Nitrobenzene-d5
Terpheny 1 - d!4
2-Fluorophenol
2,4,6 -Tribromophenol
Work Order #. ..
Date Received..
Analysis Date..
Analysis Time..
Initial Wgt/Vol
Instrument ID..
EV4X41AC
03/08/02
03/12/02
13:43
1000 mL
722
Matrix.........: WATER
MS Run #.......: 2070152
Final Wgt/Vol..: 1 raL
Method.........: SW846 8270C
RESULT
ND
ND
PERCENT
RECOVERY
ug/L
ug/L
1.4
0.91
88
95
112
70
88
95
REPORTING
LIMIT UNITS MDL
10
10
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 -.. 110)
(21 - 122)
STL Pittsburcrh 45
1111111111111111111
Lot-Sample*...: C2C160140-012
Date Sampled. ..: 03/14/02
Prep Date. .....: 03/18/02
Pre p Batch f . . . : 207732 6
Dilution Factor: 1
Analyst ID.....: 003200
PARAMETER
bi s (2-Ch.loroethyl ) -
ether
bis(2-Ethylhexyl)
phthalat e
SURROGATE
Pheno l - d5
. 2-Fluorobiphenyl
Nitrobenzene-d 5
Terpheny 1 - d!4
2 - F luor opheno 1
2,4 , 6-Tribromophenol
BLASLAND BOUCK & LEE
Client Sample ID: US-37
GC/MS Semivolatiles
Work Order ft . . . EWHD91AC Matrix, ........: WATER
Date Received.. 03/16/02 MS Run #.......: 2077154
An A 1 ves i <s Tla f*^ f i ^ / 2 ? / f) 2£UAC(*Ly £> JLO AJcLlwC • * vO/A^/WM
Analysis Time.. 16:44
Initial Wgt/Vol 1000 mL Final Wgt/Vol..: 1 mL
Instrument ID. . 731
Method. ........ SW846 8270C
REPORTING
RESULT LIMIT UNITS MDL
ND 10 ug/L 1.4
ND 10 ug/L 0.91
PERCENT RECOVERY
RECOVERY LIMITS
34 (1 0 - 113)
65 (30 - 110)
66 (3 2 - 112)
73 (10 - 144)
46 (13 - 110)
66 (21 -.122)
STL Pittsburgh 64
111 BLASIAND BOUC K & LEE
Client Sample ID:NS-38
GC/M S Semivolatiles
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lot-Sample*... C2C160140-011Date Sampled... 03/14/02
ftrep Date. ..... 03/18/02
Prep Batch #... 2077326
Dilution Factor 1
Analyst ID..... 003200
PARAMETER
bis(2-Cliloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGATE
Phenol - d5
2 -Fluorobiphenyl
Nitrobenzene-d5
Terphenyl -d!4
2 - Fluor ophenol
2,4,6- Tr ibromophenol
Work Order »...:
Date Received. .
Analysis Date..
Analysis Time. .
Initial Wgt/VolInstrument ID. . :
Method. ........:
RESULT
ND
ND
PERCENT
RECOVER Y
56
70
76
"78
62
75
EWHD71A C Matrix. ........: WATE R
03/16/02 MS Run #.......: 2077154
03/22/02
17:14
1000 mL Final Wgt/Vol..: 1 mL
731
SW84 6 8270C
REPORTING
LIMIT UNITS MD L
10 ug/L 1.4
10 ug/L 0.91
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 -,122)
STL Pittsburgh 63
111111111111111111
BLASLAHD BOUC K &
Client Sample ID:
LEE
MS-39
GC/MS Seroivolatiles
Lot-Sample ft ...: C2C160140-00 9
Date Sampled. ..: 03/14/02
Prep Date......: 03/18/02
Prep Batch #...: 2077326
Dilution Factor: 1
Analyst: ID.....: 00320 0
PARAMETE R
bis(2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGAT E
Phenol -d5
2 - Fluorobiphenyl
Ni t robenzene - d5
Terphenyl-dl4
2-Fluoroph.enol
2,4,6 -Tribromophenol
NOTB(S) :
J Estimate d result . Resul t is less tlian RU
Work Order f t . . . :
Date Received. . :
Analysis Date . . :
Analysis Time . . :
Initial Wgt/Vol:
Instrument ID . . :
Method. ........:
RESUL T
9.8 J
ND
PERCENT
RECOVER Y
67
73
79
65
69
67
EWHD31A C Matrix... ......: WATE R
03/16/02 MS Run #.......: 2077154
03/19/02
14:5 9
100 0 mL Final Wgt/Vol..: i mL
731
SW84 6 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
10 ug/L 0 . 91
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 -.122)
STL Pittsburgh 61
1111111111111111111
Lot -Sample #...: C2C160140-008
Date Sampled. ..: 03/14/02
Prep Date...... : 03/18/02
Prep Batch #...: 2077326
Dilution Factor: 1
Analyst ID.....: 003200
PARAMETER
bis(2-Chloroethyl) -
ether
bis(2-Ethylhexyl )
phthalat e
SURROGATE
Phenol -d5
2 -Fluorobiphenyl
Nitrobenzene-d S
Terphenyl - d!42 -Fluoropheno l
2,4 , 6 -Tribromophenol
HOTB(S) :
J Ealnmie d result . Resul t i s les s tha n RI _
BLASLAND BOUCK
Client Sample ID
GC/MS Semivola
Work Order # . . . :
Date Received. . :
Analysis Date . . :
Analysis Time . . :
Initial Wgt/Vol:
Instrument ID..:
Method. ........:
RESULT
6.7 J
ND
PERCENT
RECOVERY
64
69
46
59
46
70
& LEE
: MS-40
tiles
EWHD11AC Matrix .........: WATER
03/16/02 MS Run #.......: 2077154
03/19/02
14:2 8
100 0 mL Final Wgt/Vol..: 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
10 ug/L 0.91
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 -, 122)
STL Pittsburgh 60
111 BLASIAND BOUCK & LEE
Client Sample ID : NS-42
GC/M S Semivolatiles
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lot-Sample #... : C2C160140-007
Date Sampled. ..: 03/13/02
Prep Date...... : 03/18/02
Prep Batch #...: 2077326
Dilution Factor: 1
Analyst ID.....: 003200
PARAMETE R
bis (2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGATE
Phenol -d5
2 -Fluorobiphenyl
Nitrobenzene-d5
Terphenyl-dl4
2 - Fluorophenol
2,4,6- Tribroraophenol
Work Order # . . .Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method........ .:
RESULT
ND
ND
PERCEN T
RECOVER Y
67
77
81
64
77
73
TTWUHYI Hip Mat*T*-i v - WJXTWT J
03/16/02 MS Run ft.. .....: 2077154
03/19/02
13:5 7
100 0 mL Final Wgt/Vol..: 1 mL
731
SW846 8270C
REPORTIN G
LIMIT UNITS MDL
10 ug/L 1.4
10 ug/L 0.91
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 -..122)
STL Pittsburgh 59
1111111111111111111
Lot-Sample #...: C2C080109-003
Date Sampled...: 03/06/02
Prep Date. ....... 03/11/02
Prep Batch #...: 2070291
Dilution Factor: 1
Analyst ID.....: 007062
PARAMETER
bis(2-Chloroethyl ) -
ether
bis(2-Ethylhexyl )
phthalat e
SURROGATE
Phenol -d5
2 -Fluorobipheny l
Nitrobenzene-d 5
Terphenyl-dl 4
2 -Fluoropheno l
2,4,6 -Tribromophenol
BLASLAHD BOUCK & LEE
Client Sample ID: NS-43
GC/MS Semivolatiles
Work Order #. . . EV4X31A C Matrix . ........: WATE R
Date Received.. 03/08/02 MS Run #.......: 2070152
Analysis Date .. 03/12/0 2
Analysis Time.. 13:17
Initial Wgt/Vol 1000 mL Fina l Wgt/Vol..: 1 mL
Instrument ID. . 722
Method. ........ SW846 8270C
REPORTING
RESULT LIMIT UNITS MDL
ND 10 ug/L 1.4
ND 10 ug/L 0.91
PERCENT RECOVERY
RECOVERY LIMITS
91 (10 - 113)
82 (30 - 110)
109 (32 - 112)
81 (10 - 144)
89 (1 3 -.. 110)
88 (21 - 122)
ciTT.44
II
I
I
III
I
I
I
IIII
I
I
III
BLASLAND BOUC K & LEE
Client Sample ID: NS-44
GC/MS Semivolatilea
Lot-Sample #... : C2C080109-002 Work Order «...
Date Sampled...: 03/06/0 2 Date Received..
Prep Date......: 03/11/02 Analysis Date..
Prep Batch #...: 2070291 Analysis Time..
Dilution Factor: 1 Initial Wgt/Vol
Analyst ID.....: 00706 2 Instrumen t ID..
EV4X21AC Matrix.........:
03/08/02 MS Run #.......: 2070152
03/13/02
08:2 1
1000 mL Final Wgt/Vol..: 1 raL
722
Method.......-.: SW846 8270C
REPORTING
PARAMETE R RESUL T LIMIT UNITS MDL
bis(2-Chloroethyl) - ND 10 ug/L 1.4
ether
bis(2-Ethylhexyl) ND 10 ug/L 0.91
phthalate
PERCEN T RECOVER Y
SURROGATE_________________ RECOVERY______ LIMITS
Phenol-dS 86 (10 - 113)
2-Fluorobiphenyl 78 (30 - 110)
Nitrobenzene-dS ,- 10S (32 - 112)
Terphenyl-dl4 85 (10 - 144)
2-Fluorophenol 85 (13 - 110)
2,4 , 6-Tribromophenol 87 (21 - 122)
^4-4- „!_..————V,43
I
1
1
1
1
1
1
1
1
1
1
Lot- Sample #... C2C090133-002
Date Sairgpled. . . 03/08/02
Prep Date. . .... 03/11/02
Prep Batch #... 2070291
Dilution Factor 4
Analyst ID..... 001562
PARAMETER
bis(2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGATE
Phenol -d5
2 - Fluorobiphenyl
Nitrobenzene -d5
Terphenyl-dl4
2 - Fluorophenol
2,4,6- Tribrotnophenol
BLASLAK D BODC K &
Client Sample ID:
GC/M S Semivolat
Work Order # . . . :
Date Received. .
Analysis Date..
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method.. .......
RESULT
ND
ND
PERCENT
RECOVER Y
77
84
82
..74
' 65
92
LEE
NS-45
iles
EV6621AC Matrix. ........: WATE R
03/09/02 MS Run #.......: 2070152
03/13/02
12:20
1000 raL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTIN G
LIMIT UNITS MDL
40 ug/L 5.8
40 ug/L 3.6
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
STL Pittsburgh 25
1111111111111111111
BLASLAND BOOCK
Client Sample ID
& LEE
: NS-46
GC/M S Semivolatiles
I*>t -Sample #... C2C130116-004Date Sampled. .. 03/12/02
Prep Date. ..... 03/14/02
Prep Batch ft... 2073127
Dilution Factor l
Analyst ID.....: 001562
PARAMETER
bis (2-Chloroethyl) -
ether
bis (2-Etbylhexyl)
phthalate
SURROGAT E
Phenol -d5
2 - FluorobiphenylNitrobenzene-dS
Terphenyl -d!4
2- Pluorophenol
2,4,6- Tr ibromophenol
KOTE(S) :
J Etiimac d result. Resul t n less than RL .
Wor k Order #...
Date Received. .
Analysis Date. .
Analysis Time . .
Initial Hjgrt/VolInstrument in. .
Method. ........
RESOLT
ND
1.4 J
PERCENT
RECOVER Y
69
74
,70
75
60
94
T?M2in*71 JVC"* Maf-T-T-y • TJLTPO
03/13/02 MS Run #.......: 2073022
03/15/02
17:40
1000 mL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MD L
10 ug/L 1.4
10 ug/L 0.91
RECOVER Y
LIMITS
(10 - 113)
(30 - 110}
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
I1 BLASLAN D BOUC K & LEE
1 Client Sample ID : NS-47
GC/MS Semivolatiles
1
1
1
1
1
1
1
1
Lot-Sample #... C2C130116-003
Date Sampled. .. 03/11/02
Prep Date. ..... 03/14/02
Prep Batch #... 2073127
Dilution Factor 1
Analyst ID. .... 001562
PARAMETE R
bis (2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGATE
Phenol -dS
2 - Fluorobiphenyl
Nitrobenzene-d5
Terphenyl-dl4
2 - Fluorophenol
2,4 , 6-Tribromophenol
Work Order #. . .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVERY
70
82
.75
81
64
102
EWAG61AC Matrix. ........: WATE R
03/13/02 MS Run #.......: 2073022
03/15/02
17:13
100 0 mL Pinal Wgt/Vol..: l mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
10 ug/L 0.91
RECOVER Y
LIMITS
(10 - 113)
{30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
II
II
II
I
OTT. D-i t-t-oV-iin-rrVi 32
11 BLASLAND BOUCK £ LEE
1 Client Sample ID: NS-48
GC/MS Semivolatiles
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lot - Sample #... C2C130116-001
Date Sampled. .. 03/11/02
Prep Date. ..... 03/14/02
Prep Batch #... 2073127
Dilution. Factor 1
Analyst ID..... 001562
PARAMETER
bi s (2-Chloroethyl) -
ether
bis(2-Ethylhexyl )
phthalate
SURROGATE
Phenol - d5
2 - Fluorobiphenyl
Nitrobenzene-d 5
Terphenyl-dl 4
2 - F l uo r opheno l
2,4,6 -Tr ibromophenol
Work Order #...
Date Received. .
Analysis Date. .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVERY
78
83
.78
'83
70
105
tPWBOAl 2ir * Mat'T'i v - WZVTTM3
03/13/02 MS Run #.......: 2073022
03/15/02
16:18
1000 mL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
10 ug/L 0.91
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
II
I
II
I
I
I
I
I
IIII
I
I
I
I
BLASLAND BOUCK & LEE
Client Saiqple ED: NS-49
GC/MS Semivolatiles
Date Sampled...
Prep Date......
Prep Batch #...
Dilution Factor
Analyst ID.....
03/07/02
03/11/02
207C291
1
007062
Work Order f t ...
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID , .
Method. ........
EV4X91AE
03/08/02
03/12/02
14:3 5
1000 mL
722
SW846 8270C
Matrix. .......
MS Run # ......
Final Wgt/Vol.
.
•
• :
2070152
: 1 mL
PARAMETE R RESULT
bis(2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGAT E
12
ND
PERCENT
RECOVERY
Phenol-d5
2 - Fluorobipheny 1
Ni t robenz ene - d5
Terphenyl-dl4
2-Fluorophenol
2,4,6 -Tribromophenol
83
76
103
74
81
86
REPORTIN G
LIMIT UNITS
10
MD L
10
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 -..110)
(21 - 122)
ug/L
ug/L
1.4
0.91
STL Pittsburah 47
111 BIASLMJD BOUC K
Client Sample ID
& LEE
: HS-50
GC/MS Semivolatiles
1
1
1
1
1
1
1
1
1
1
1
1
Lot-Sample # . . . C2C160140-003
Date Sampled- .. 03/13/02
Prep Date. ..... 03/18/02
Prep Batch ft. .. 2077326
Dilution Factor 1
Analyst ID..... 003200
PARAMETE R
bis (2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGATE
Phenol -d5
2 -Fluorobipheny 1
Nitrobenzene -d5
Terphenyl-dl4
2 -Fluorophenol
2,4,6 -Tribromophenol
Work Order # . . .
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
24
ND
PERCEN T
RECOVER Y
73
77
84
60
79
74
EWHDM1A C Matrix. ........: WATE R
03/16/02 MS Run #.......: 2077154
03/19/02
12:55
1000 tti L Final Wgt/Vol..: 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
10 ug/L 0.91
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 -..122)
S1L Pittsburgh 56
IIIIIIIIII1IIIIIIII
BLASLAND BOUCK & LEE
Client Sample ID: NS-S1
GC/MS Semivolatiles
Lot-Sample »... C2C080109-007 Work Order #... EV40F1AC
Dat e Sampled...
Prep Date......
Prep Batch #. . .
Dilution Factor
Analyst ID.....
03/07/02
03/11/02
2070291
1
007062
Date Received..
Analysis Date..
Analysis Time..
Initial Wgt/Vol
Instrument ID..
03/08/02
03/13/02
09:16
1000 mL
722
Matrix...
M S Run #., : WATER
.: 2070152
Final Wgt/Vol...- 1 mL
Method........... SW84 6 8270C
PARAMETE R RESULT
bis(2-Chloroethyl)-
ether
bis(2-Ethylhexyl)
phthalate
SURROGATE
Phenol-dS
2 - Fluorobipheny 1
Ni trobenzene-dS
Terphenyl-dl4
2-Fluorophenol
2,4,6 -Tribromophenol
ND
ND
PERCENT
RECOVERY
REPORTING
LIMIT UNITS
10
MDL
10
ug/L
ug/L
1.4
0.91
82
70
99
76
76
81
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
Pi 48
II
I
I
I
I
I
I
I
I
I
BLASLAND BOUCK & LEE
Client Sample ID: DDP-030702
GC/MS Semivolatiles
Lot-Sample*...: C2C080109-009
Date Sampled...: 03/07/02
Prep Date......: 03/11/02
Prep Batch ft...: 2070291
Dilution Factor: 1
Analyst ID..... s 007062
PARAMETER_________
bis (2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGATE_____________Phenol-d52 - Fluorobipheny 1
Nitrobenzene-dS
Terph.enyL-dl4
2 - Fluorophenol
2,4,6 -Tribromophenol
Work Order #. ..
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........
EV40J1AC
03/08/02
03/12/02
16:4 5
100 0 mL
722
SW846 8270C
Matrix. ........:
MS Run #.......:
Final Wgt/Vol . . :
2070152
1 mL
RESULT
ND
ND
PERCENT
RECOVERY
81
73
98
71
74
83
REPORTING
LIMIT UNITS
10
MDL
10
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 -. 110)
(21 - 122)
ug/L
ug/L
1.4
0.9 1
.CTT . Pi 50
111 BLASLAND BOOCK &
Client Sample ID:
LEE
NS-52
GC/MS Semivolatiles
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lot-Sample #...: C2C160140-002
Date Sampled. ..: 03/13/02
Prep Date. ....... 03/18/02
Prep Batch #...: 2077326
Dilution Factor: 1
Analyst ID.....: 003200
PARAMETER
bis(2-Chloroethyl ) -
ethe r
bis(2-Ethylhexyl)
phthalat e
SURROGATE
Pheno l -d 5
2 -Fluorobiphenyl
Nitrobenzene-d S
Terpheny l -dl 4
2 -Fluoropheno l
2,4 , 6 -Tribromophenol
Work Order # . . .
Date Received. .
Analysis Date. .
Analysis Time..
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVERY
69
73
76
,.7 1
73
65
EWHDK1AC Matrix. ........: WATER
03/16/02 MS Run #.......: 2077154
03/19/02
12:2 4
100 0 mL Final Wgt/Vol..: 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
10 ug/L 0.91
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - .122)
STL Pittsburgh 55
I11 BLASLAND BOUC K & LEE
Client Sample ID: DUP - 031302
GC/M S Semivolatiles
1
1
1
1
1
1
1
1
Lot-Sample*... C2C160140
Date Sampled... 03/13/02
Prep Date. ..... 03/18/02
Prep Batch #... 2077326
Dilution Factor 1
Analyst ID..... 003200
PARAMETE R
bis(2-Chloroethyl) -ether
bi s ( 2 - E thy Ihexyl )
phthalate
SURROGAT E
Phenol -d5
2 - Fluorobipheny 1
Nitrobenzene-dS
Terphenyl-dl4
2 - Fluor ophenol
2,4 , 6 -Tribromophenol
-005 Work Order #...
Date Received. .
Analysis Date. .
Analysis Time. .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
ND
ND
PERCENT
RECOVER Y
61
75
80
...••• 7 1
72
69
• PWWn^l Sf** MJS^T""I V * WATTTl?
03/16/02 MS Run #.......: 2077154
03/19/02
17:02
100 0 mL Final Wgt/Vol..: 1 mL
731
SW846 8270C
REPORTING
LIMIT UNITS MD L
10 ug/L 1.4
10 ug/L 0.91
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - .122)
STL Pittsburgh 58
1111111111111111111
Lot -Sample #...: C2C160140-001
Date Saiqpled... : 03/13/02
Prep Date. .....: 03/18/02Prep Batch ft. ...- 207732 6
Dilution. Factor: 1
Analyst ID.....: 003200
PARAMETE R
bis(2-Chloroethyl) -
ether
bis (2-Ethylhexyl)
phthalate
SURROGATE
Phenol - d5
. 2 - Fluorobiphenyl
Nitrobenzene -d5
Terphenyl-dl4
2 - Fluorophenol
2,4, 6 -Tribromophenol
BLASLAND BOUC K & LKB
Client Sample ID: NS-53
GC/MS Semivolatiles
Work Order ft. . . EWHDH1A C Matrix. .......... WATE R
Date Received.. 03/16/02 MS Run f .......: 2077154
Analysis Date.. 03/19/02
Analysis Time.. 11:54Initial Wgt/Vol 1000 mL Final Wgt/Vol..: 1 mL
Instrument ID. . 731
Method. ........ SW84 6 8270C
REPORTING
RESULT LIMIT UNITS MDL
N D 10 ug/L 1.4
ND 10 ug/L 0.91
PERCEN T RECOVER Y
RECOVER Y LIMITS
73 (10 - 113)
78 (30 - 110)
83 (32 - 112)
78 (10 - 144)
79 (13 - 110)
69 (21 - 122)
STL Pittsburgh 54
11 BLASLAND BOUCK & LEE
1 Client Sample ID : NS-54
GC/M S Semivolatiles
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lot - Sample #... C2C130116-005
Date Sampled. .. 03/12/02
Prep Date. . .... 03/14/02
Prep Batch f... 2073127
Dilution Factor 1
Analyst ID..... 001562
PARAMETER
bis(2-Chloroethyl) -
ether
bis (2-Ethylhexyl)
phthalate
SURROGAT E
Phenol -d.5
2-Fluorobiphenyl
Nitrobenzene-d5
Terphenyl-dl4
2-Fluorophenol
2,4, 6 -Tribromophenol
Work Order # . . .
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID. .
Method. ........
RESULT
NO
ND
PERCENT
RECOVERY
74
83
72
'71
64
100
EWAQ81A E Matrix. ........: WATE R
03/13/02 MS Run #.......: 2073022
03/15/02
18:07
1000 mL Final Wgt/Vol..: 1 mL
721
SW846 8270C
REPORTING
LIMIT UNITS MD L
10 ug/L 1 . 4
10 ug/L 0.91
RECOVERY
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 - 110)
(21 - 122)
34
11
BLASLAND BOUC K & LEE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Client Sample ID : CT-1
GC/MS Semivolatiles
Lot-Sample #... C2C080109-008
Date Sampled. .. 03/07/02
Prep Date. ..... 03/11/02
Prep Batch #... 2070291
Dilution Factor 1
Analyst ID..... 007062
PARAMETE R
bis(2-Chloroethyl) -
ether
bis(2-Ethylhexyl)
phthalate
SURROGATE
. Phenol -d5
2 -Fluorobiphenyl
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorophenol
2,4,6 -Tribromophenol
Work Order ft ...
Date Received. .
Analysis Date . .
Analysis Time . .
Initial Wgt/Vol
Instrument ID . .
Method. ........
RESULT
ND
ND
PERCENT
RECOVER Y
83
80
106
77
82
90
EV40H1AC Matrix. ........: WATE R
03/08/02 MS Run #.......: 2070152
03/12/02
16:19
100 0 mL Final Wgt/Vol..: 1 mL
722
SW846 8270C
REPORTING
LIMIT UNITS MDL
10 ug/L 1.4
10 ug/L 0.91
RECOVER Y
LIMITS
(10 - 113)
(30 - 110)
(32 - 112)
(10 - 144)
(13 -.110)
(21 - 122)
49
I
I
I
I
I
I
I
I
I
I
I
II
I
I
I
I
I
I
Lot-Sample » . . -: C2C090133-001
Date Sampled...: 03/08/02
PARAMETE R R RST7T..T
Prep Batch tt. .
Chromium
Manganese
Antimony
Thallium
Zinc
: 2070225
72.6
157
ND
ND
7.6 B
NOTE(S) :______ _ ___
0 Hummed result . Kcttll t is less ll>;lt i HI..
BLASLAND BOUC K t LEE
Client Sample ID: NS-13
TOTAL Metals
Date Received..: 03/09/02
REPORTIN G
Matrix.WATE R
IJNTT.8 METHO D
PREPARATION- WOR K
ANALYSI S DAT E ORDE R S
5.0 ug/L SW846 6010B 03/11-03/13/02 EV6601AF
Dilution Factor: 1 Analysis Time..: 14:29 Analyse I D . . . . .; 400149
Instrument ID. .: TRACEIC P MS Run « . . . . . . .: 2070093 MDL,. ...........: 1.1
15.0 ug/L SW846 6010B 03/11-03/13/02 KV6601AD
Dilution Factor: 1 Analysis Time..-. 14:25 analyst I D . . . . .: 40014 9
Instrument ID. . : TRACEICP MS Run a . . . . . . .: 2070093 MDb. . . . . . . . . . . .: 0.45
10.0 ug/L SW84 6 6010B 03/11-03/13/02 EV6601AE
Dilution Factor: 1 Analysis Time...- 14:29 Analyst ID. ...... 400149
Instrument I D . .: TRACEIC P MS Run B . . . . . . .: 2070093 MDL . . . . . . . . . . . .: 3.8
10.0 ug/L SW846 6010B 03/11-03/13/02 EV6601AG
Dilution Factor: 1 Analysis Time..-. 14:29 Analyst I D . . . . .: 400149
Instrument ID. .: TRACEICP MS Run « . . . . . . .: 2070093 MDL . . . . . . . . . . . .: 5.5
20.0 ug/L SW84.6 6010B 03/11-03/13/02 EV6601AH
Dilution Factor: 1 Analysis Time..: 14:29 Analyst ID....... 400149
Instrument ID..: TRACEIC P MS Run » . . . . . . .: 2070093 MDL . . . . . . . . . . . .: 4.4
STL Pittsburgh 40
I
II
I
I
I
I
I
I
I
I
I
II
II
I
I
I
Lot-Sample fl .
Date Sampled.
PARAMETER
BLASLAND BOUCK & LEE
Client Sample ID: NS-24
TOTAL Metals
. .: C2C160140-013
..: 03/14/02 Dat e Received..: 03/16/0 2
Matrix.WATER
RESULT
REPORTING
LIMIT UNITS METHOD
PREPARATION- WORK
ANALYSIS DATE ORDER
Prep Batch. #
Chromium
Manganese
Antimony
Thallium
Zinc
. . .: 2077231
1.5 B 5.0
Instrument ID.
320O J 15.0
ND 10.0
ND 10.0
10.1 B 20.0
Instrument ID.
ug/L
r: 1
ug/L
r: 1
ug/L
it: 1
ug/L
. : TRACEICP
ug/L
. : TRACEICP
SW846 6010B
MS Run f t . . . . . . .:
SW846 6010B
M S Run ft .......:
SW846 6010B
M S Run ft .......:
SW846 6010B
KS Run 8 .......:
SW846 6010B
MS Run « . . . . . . .:
03/18-03/22/02 EWHECUA F
13:04 Analyst I D . . . . .: 400149
2077087 MDL. . . . . . . . . . . .: 1.1
03/18-03/22/02 EWHEC1AD
13:04 Analyst I D . . . . .: 400149
2077087 MDL. ...........: 0.45
03/18-03/22/02 EWHEC1AE
13:04 Analyst I D . . . . .: 400149
2077087 MDL. ...........: 3.8
03/18-03/22/02 EWHEC1A G
13:04 Analyst I D . . . . .: 400149
2077087 MDL . . . . . . . . . . . .: 5.5
03/18-03/22/02 EWHEC1AH
13:04 Analyst I D . . . . .: 400149
2077087 MDL. ...........: 4.4
NOTE(S) :
B (-Minute d result . Resul t is lus s tha n RL .
J MtllHH l hbllk coiit^iniinuiim . "D i iiuihut l lilan k conuiiii s llK uirya analyi u al a rcporiubl c level.
STL Pittsburgh 89
IIIIIII
I
I
I
i
ii
i
i
i
i
Lot-Sample #.
Date Sampled.
PARAMETER
BLASLAND BOUC K & LE E
Client Sample ID: NS-35
TOTA L Metals
.: C2C080109-005
,.: 03/07/02 Date Received..: 03/08/02
Matrix.......: WATE R
RESULT
REPORTING
LIMIT UNITS METHOD
PREPARATION-
ANALYSTS DA1
WORK
ORDER
Prep Batch tt...: 2070129
Chromiu m 4.5 B
Manganese
Antimony
Thallium
Zin c
NOTE(S):
11100
ND
ND
B Estimate d result . Resul t is less tha n RL .
5.0 ug/L SW846 6010B 03/11-03/12/02 EV4X71AF
Dilution Factor: 1 Analysis Time..: 15:55 Analyst I D . . . . .: 400149
Instrument ID..: TRACEIC P MS Run » . . . . . . .: 2070023 MDL . ...........: 1.1
30.0 ug/L SW846 6010B 03/11-03/12/02 EV4X71AD
Dilution Factor: 2 Analysis Time..: 22:4 5 Analyst ID.....: 40014 9
Instrument ID..: TRACEICP MS Run ».......: 2070023 M D L . . . . . . . . . . . .: 0.89
10.0 ug/L SW846 6010B 03/11-03/12/02 EV4X71AE
Dilution Factor: 1 Analysis Time..: 15:55 Analyst I D . . . . .: 400149
Instrument ID..: TRACEICP MS Run # . . . . . . .: 2070023 M D L . . . . . . . . . . . .: 3.8
20.0 ug/L SW846 6010B 03/11-03/13/02 EV4X71AG
Dilution Factor: 2 Analysis Time..: 15:23 Analyst ID.....: 400149
Instrument ID..: TRACEIC P MS Run t t . . . . . . .: 2070023 M D L . . . . . . . . . . . .: 10 .9
20.0 ug/L SW846 6010B 03/11-03/12/02 EV4X71AH
Dilution Factor: 1 Analysis Time..: 15:55 Analyst I D . . . . .: 400149
Instrument ID. . : TRACEICP MS Run # . . . . . . .: 2070023 MDL . . . . . . . . . . . .: 4.4
STT , Pittsburah 66
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BLASLAND BOUCK & LEE
Client Sample ID: NS-36
TOTAL Metals
Lot -Sample #...
Date Sampled. . .
PARAMETE R
Prep Batch # . . .
Chromium
: C2C080109
: 03/07/02
RESULT
: 2070129
2.6 B
-004
Date Received. . :
REPORTING
LIMIT UNITS
5 . 0 ug/L
Instrument ID. . : TRACEIC P
03/08/02
METHO D
SN846 6010B
MS Run ».......:
Matrix. ......:
PREPARATION-
ANALYSIS DATE
03/11-03/12/02
1S-.39 Analyst ID. . . . .
2070023 MDL . . . . . . . . . . ..
WATT?D
WOR K
ORDE R #
EV4X41AF
: 400149
: 1.1
Manganese
Antimon y
Thallium
Zinc
NOTE(S) :
2600
ND
ND
7.8 B
B Estimate d reaili. Rcsul i is less lhai i RL.
15.0 ug/L SW846 6010B 03/11-03/12/02 EV4X41AD
Dilution Factor: 1 Analysis Time..: 15:39 Analyst I D . . . . .: 400149
Instrument ID. . : TRACEICP MS Run « . . . . . . .: 2070023 MDL . ...........: 0.4S
10.0 ug/L SW84 6 6010B 03/11-03/12/02 EV4X41AE
Dilution Factor: 1 Analysis Time..: 15:39 Analyse ID.....: 400149
Instrument ID..: TRACEIC P MS Run » . . . . . . .: 2070023 M D L . . . . . . . . . . . .: 3.8
10.0 ug/L SW846 6010B 03/11-03/12/02 EV4X41AG
Dilution Factor: 1 Analysis Time..: 15:39 Analyst I D . . . . .: 400149
Instrument ID.. : TRACEIC P MS Run 8. ......: 2070023 MDL . . . . . . . . . . . .: 5.5
20.0 ug/L SW846 6010B 03/11-03/12/02 EV4X41AK
Dilution Factor: 1 Analysis Time..: 15:39 Analyst ID.....:-400149
Instrument ID. . : THACEICP MS Run » . . . . . . .: 2070023 MDL . ...........: 4.4
<5TT . Pi ff.65
1111111111111111111
BLASLAND BOUCK & LEE
Client Sample ID: NS-37
TOTAL Metals
Lot-Sample #...: C2C160140-012
Date Sampled...: 03/14/02 Date Received...- 03/16/02
REPORTIN G
PARAMETE R RESULT LIMIT UNITS METHO D
Prep Batch #...: 2077231
Chromium 30.0 5.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time. . ;
Instrument ID. . : TRACEIC P MS Run ft . . . . . . .:
Manganese 1280 J 15.0 ug/L SW84 6 6010B
Dilution Factor: 1 Analysis Time. . :
Instrument ID . . : TRACEICP MS Run tf .......:
Antimony ND 10.0 ug/L SW84 6 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID. . : TRACEIC P MS Run tt. ......:
Thallium ND 10.0 ug/L SW84 6 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID. . : TRACEIC P MS Run #.......:
Zinc 5.0 B 20.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID. . : TRACEIC P MS Run #.......-.
NOTE(S) :
J Metho d blan k com.uniiuliiin . Tlic axsociaic d mcditx l blan k ctmiuii K ih v uirgc t iiulyic ni a rcporiahl c level .
B Estimate d result. Resul t is Ins Ih.in RL .
Matrix. ......:
PREPARATION-
ANALYSIS DATE
03/18-03/22/02
12:5 8 Analyst ID. . . . .
2077087 MDL . ...........
03/18-03/22/02
12:5 8 Analyst ID. . . . .
2077087 MDL . . . . . . . . . . ..
03/18-03/22/02
12:5 8 Analyst ID. . . . .
2077087 MDL . . . . . . . . . . ..
03/18-03/22/02
12:5 8 Analyst ID. . . . .
2077087 MDL . . . . . . . . . . ..
03/18-03/22/02
12:5 8 Analyst ID.
2077087 MDL . . . . . . . . . . ..
WATE R
WOR K
ORDE R #
EWHD91AF
• 400149
• 1.1
EWHD91AD
: 400149
: 0.45
EWHD91A E
• 400149
• 3.8
EWHD91AG
• 400149
• 5.5
EWHD91AH
: 400149
• 4.4
STL Pittsburgh 88
IIIIIIIIIIII
Lot-Sampl e #.
Date Sampled.
PARAMETE R
BLASLAND BOUCK & LEE
Client Sample ID: NS-38
TOTA L Metals
.: C2C160140-011
..: 03/14/02 Date Received..: 03/16/02
RESULT
REPORTIN G
LIMIT UNITS METHO D
Matrix. ........ WATE R
PREPARATION- WOR K
ANALYSIS DATE ORDER
Prep Batch #.
Chromium
Manganese
Antimony
Thallium
Zinc
NOTE(S) :
. : 2077231
9.1
34700 J
ND
ND
ND
5.0 ug/L SW846 6010B
Dilution Factor: l Analysis Time..:
Instrument ID..: TRACEIC P MS Run 8. ......:
75.0 ug/L SW846 6010B
Dilution Factor: S Analysis Time..:
Instrument ID. . : TRACEIC P MS Run t t . . . . . . .:
10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time...-
Instrument ID..: TRACEIC P MS Run t t . . . . . . -:
50.0 ug/L SW84 6 6010B
Dilution Factor: 5 Analysis Time..:
Instrument ID. .: TRACEIC P MS Run » . . . . . . .:
20.0 ug/L SW84 6 "6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID. . •. TRACEIC P MS Run tt.......:
03/18-03/22/02 EWBD71AF
12:42 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 1.1
03/18-03/22/02 EWHD71A D
16:3 4 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 2.2
03/18-03/22/02 EWHD71A E
12:4 2 Analyst ID.....: 400149
2077087 MDL............: 3.8
03/18-03/22/02 EWHD71AG
15:34 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 27.3
03/18-03/22/02 EWHD71AH
12:4 2 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 4.4
J Metho d libm k conutniimiiion . Tlic iissuciaic d metho d hlnn k cnmuin s Hi e larjc t nnalyc c a t it rcponabli : level .
STL Pittsburgh 87
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Lot-Sample #.
Date Sampled.
PARAMETER
BLASLAND BOUCK & LEE
Client Sample ID: NS-39
TOTAL Metals
.: C2C160140-009
..: 03/14/02 Date Received..: 03/16/02
RESULT
REPORTING
LIMIT UNITS METHOD
Matrix.......: WATE R
PREPARATION- WOR K
ANALYSIS DAT E ORDE R f c
Prep Batch #...: 2077231
Chromium 7.2
Manganese
Antimony
Thallium
Zinc
HOTE(S) :
174 J
ND
ND
ND
5.0 ug/L SW846 601OB
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run # . . . . . . .:
15.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run # . . . . . . .:
10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run # . . . . . . .:
10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run #.......:
20.0 ug/L SW846 6010B
Dilution Factor.- 1 Analysis Time..:
Instrument ID..: TRACEICP MS Run « . . . . . . .:
03/18-03/22/02 EWHD31AF
12:31 Analyst I D . . . . .: 400149
2077087 MDL. . . . . . . . . . . .: 1.1
03/18-03/22/02 EWHD31AD
12:31 Analyst ID.....: 400149
2077087 MDL. ...........: 0.45
03/18-03/22/02 EWHD31A E
12:31 Analyst ID.....: 400149
2077087 MDL............; 3.8
03/18-03/22/02 EWHD31A G
12:31 Analyst ID.....: 400149
2077087 MDL. . . . . . . . . . . .: S.5
03/18-03/22/02 EWHD31A H
12:31 Analyst ID.....: 400149
2077087 MDL. ...........: 4.4
J Mcil»x ) blan k conumimuion . Th e nssnchtc d metho d blan k contain s the tar[cl analyl e ai a rcpuriabl u level .
STL Pittsburgh 85
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Lot-Sample #.
Date Sampled.
PARAMETER
BLASLAND BOUCK & LEE
Client Sampl e ID: NS-40
TOTAL Metals
.: C2C160140-008
. .-. 03/14/02 Dat e Received. .: 03/16/02
Matrix.WATER
RESULT
REPORTING
LIMIT UNITS METHOD
PREPARATION- WORK
ANALYSIS DATE ORDER
Pre p Batch #.
Chromiu m
Manganese
Antimon y
Thalliu m
Zin c
NOTE(S) :
: 2077231
2.2 B
7360 J
5.0 ug/L SW846 6010B
Dilution Factor; 1 Analysis Time..:
Instrument ID..: TRACEICP MS Run « . . . . . . .:
15.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run a .......:
10.0 ug/L SW84 6 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run # . . . . . . .:
ND
ND
10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..-.
Instrument ID.. : TRACEIC P MS Run # . . . . . . .:
20.0 ug/L SW84 6 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEICP MS Run # . . . . . . .:
03/18-03/22/02 EWHD11AF
12:26 Analyst I D . . . . .: 400149
2077087 MDL. ...........: 1.1
03/18-03/22/02 EWHD11AD
12:26 Analyst I D . . . . .: 400149
2077087 MDL. . . . . . . . . . . .: 0.45
03/18-03/22/02 EWHD11AE
12:26 Analyst I D . . . . .: 400149
2077087 MDL. ...........: 3.8
03/18-03/22/02 EWHD11AG
12:26 Analyst ID.....: 400149
2077087 MDL. . . . . . . . . . . .: 5.5
03/18-03/22/02 EWHD11AH
12:26 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 4.4
R Enimaici l result. Rtsut t is Ins tha n RL .
J MvitMx l blank cnnuuninntiim . "Die .-umciaic d incilxx ) blan k contain s th e targe t nnalyt c at a rcportabli : level.
STL Pittsburgh 84
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Lot-Sample #.
Date Sampled.
PARAMETE R
BLASLAND BODCK & LEE
Client Sample ID: NS-41
TOTAL Metals
. : C2C160140-006
. .: 03/13/02 Date Received..: 03/16/02
RESULT
REPORTING
LIMIT UNITS METHO D
Matrix.......: WATE R
PREPARATION- WOR K
ANALYSIS DATE ORDE R £
Prep Batch #.
Chromium
Manganese
Antimony
Thallium
Zinc
NOTE(S) :
.: 2077231
122
1830 J
ND
N D
8.9 B
5.0 ug/L
Dilution Factor: 1
Instrument ID..:
SW846 6010B
Analysis Time..:
M S Run #.......-.
15.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID. . : TRACEIC P MS Run f t . . . . . . .:
10.0 ug/L
Dilution Factor: 1
Instrument ID..:
10.0 ug/L
Dilution Factor: 1
Instrument ID..:
20.0 ug/L
Dilution Factor: 1
Instrument ID..:
SW846 6010B
Analysis Time..:
M S Run « . . . . . . .:
SW846 6010B
Analysis Time..:
M S Run # . . . . . . .:
SW846 6010B
Analysis Time..:
MS Run # . . . . . . .:
03/18-03/22/02 EWHDT1AE
12:1 5 Analys t ID . ...... 40014 9
2077087 MDL............: 1.1
03/18-03/22/02 EWHDT1AC
12:15 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 0.45
03/18-03/22/02 EWHDT1AD
12:15 Analyst ID.....: 400149
2077087 M D L . . . . . . . . . . . .: 3.8
03/18-03/22/02 EWHDT1A F
12:15 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 5.5
03/18-03/22/02 EWHDT1AG
12:15 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 4.4
J Metho d blank coinaniiiwiion. The: njsociiinl niciluid lil.ink contains Ihc targe t aualylc at a rcporciblc level.
R Etimutctl result. Resul t is IL-S S ilua RL.
STL Pittsburgh 82
1111111111111111111
BLASLAND BOUCK & LEE
Client Sample ID: NS-42
TOTA L Metals
Lot-Sample #...: C2C160140-007
Date Sampled...: 03/13/02 Date Received. .: 03/16/02
REPORTING
PARAMETE R RESULT LIMIT UNITS METHO D
Prep Batch #...: 2077231
Chromium 32.4 5.0 ug/L SW84 6 6010B
Dilution Factor: 1 Analysis Time. . :
Instrument ID. . : TRACEIC P MS Run ft .......:
Manganese 12800 J 30.0 ug/L SW84 6 6010B
Dilution Factor: 2 Analysis Time. . :
Instrument ID. . : TRACEIC P MS Run # . . . . . . .:
Antimony ND 10. 0 ug/L SW84 6 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID. . : TRACEIC P MS Run «.......:
Thallium ND 20.0 ug/L SW84 6 6010B
Dilution Factor: 2 Analysis Time . . :
Instrument ID. . : TRACEICP MS Run #.......:
Zinc 20.3 20.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID. . : TRACEICP MS Run 8 .......:
NOTE(S) :
> Muhtx l blan k cuiuamiruiimi . Th e aratciaiu l metho d blan k comaiii s ih c targe t analyi c ai a rcpomblc level .
Matrix. ......:
PREPARATION -
ANALYSIS DAT E
03/18-03/22/02
12:20 Analyst ID. . . . .
2077087 MDL. . . . . . . . . . ..
03/18-03/22/02
16:28 Analyst ID. . . . .
2077087 MDL. . . . . . . . . . ..
03/18-03/22/02
12 :20 Analyst ID. . . . .
2077087 MDL. . . . . . . . . . ..
03/18-03/22/02
16:28 Analyst ID . . . . .
2077087 MDL. . . . . . . . . . ..
03/18-03/22/02
12:20 Analyst ID. . . . .
2077087 MDL. . . . . . . . . . ..
WATER
WOR K
ORDE R f c
EWHDX1AF
• 400149
: 1.1
EWHDXLA D
• 400149
- 0.89
EWHDX1AE
: 400149
• 3.8
EWHDX1A G
• 400149
s 10.9
EWHDX1AH
• 400149
: 4 .4
ST L Pittsburgh 83
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Lot-Sampl e #.
Dat e Sampled.
PARAMETER
C2C080109
03/06/02
RESULT
-003
BLASLAND BOUCK & LEE
Client Sample ID: NS-43
TOTAL Metals
Date Received..: 03/08/02
REPORTING
LIMIT__ UNITS METHO D
Matrix. . . . . . . .. WATE R
PREPARATION- WOR K
ANALYSIS DATE ORDE R S
Prep Batch #.
Chromium
Manganese
Antimony
Thallium
Zinc
NOTE(S) :
: 2070129
4.1 B
5.2 B
ND
ND
ND
B [-slimme d result . Risiil i is less tha n RL .
5.0 ug/L SW846 6010B 03/11-03/12/02 EV4X31AF
Dilution Factor: 1 Analysis Time..: 15:3 4 Analyst I D . . . . .: 40014 9
Instrument ID. .: TRACEIC P MS Run f t . . . . . . .: 2070023 M D L . . . . . . . . . . . .: 1.1
15.0 ug/L SW846 6010B 03/11-03/12/02 EV4X31AD
Dilution Factor: 1 Analysis Time..: 15:34 Analyse ID. ...... 400149
Instrument ID..: TRACEIC P MS Run » . . . . . . .: 2070023 M D L . . . . . . . . . . . .: 0.45
10.0 ug/L SW84 6 6010B 03/11-03/12/02 EV4X31AE
Dilution Factor: 1 Analysis Time..: 15:3 4 Analyst I D . . . . .: 40014 9
Instrument ID..: TRACEICP MS Run ».......: 2070023 M D L . . . . . . . . . . . .: 3.8
10.0 ug/L SW846 6010B 03/11-03/12/02 EV4X31AG
Dilution Factor: 1 Analysis Time..: 15:34 Analyst ID.....: 400149
Instrument ID..: TRACEIC P MS Run *.......: 2070023 M D L . . . . . . . . . . . .: 5.5
20.0 ug/L SW846 6010B 03/11-03/12/02 EV4X31AH
Dilution Factor: 1 Analysis Time..: 15:34 Analyst ID.....: 400149
Instrument ID..: TRACEIC P MS Run » . . . . . . .: 2070023 M D L . . . . . . . . . . . .: 4.4
Pi t-f sYynrrrh 64
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Lot-Sample ft.
Date Sampled.
BLASLAND BODCK & LEE
Client Sample ID: NS-44
TOTAL Metals
C2C080109-002
03/06/02 Date Received..: 03/08/02
Matrix.......: WATER
PARAMETER
Pre p Batch
Chromium
RESULT
#...: 2070129
3.0 B
REPORTING
LIMIT UNITS
5 . 0 ug/L
METHOD
SW846 6010B
PREPARATION- WORK
ANALYSIS DATE ORDER «
03/11-03/12/02 EV4X21AF
Manganese
Antimony
Thallium
Zinc
NOTE(S):
ND
ND
ND
ND
B Estimated resvilt . Remit is Icsa than RL.
Dilution Factor: 1
Instrument ID. . : TRACEICP
15.0 ug/L
Dilution Factor: 1
Instrument ID. .: TRACEICP
10.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEICP
10.0 ug/L
Dilution Factor: 1
instrument ID. . : TRACEICP
20.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEICP
Analysis Time..: 15:28 Analyst ID.....: 40014 9
MS Run tt .......: 2070023 MDL. . . . . . . . . . . .: 1.1
SW846 6010B 03/11-03/12/02 EV4X21AD
Analysis Time..: 15:28 Analyse ID ....... 400149
MS Run # . . . . . . .: 2070023 MDL. . . . . . . . . . . .: 0.45
SW846 6010B 03/11-03/12/02 EV4X21AE
Analysis Time...- 15:28 Analyst ID....... 400149
MS Run #.......: 2070023 MDL. ...........: 3.8
SW846 6010B 03/11-03/12/02 EV4X21AG
Analysis Time..: 15:28 Analyst ID .....: 400149
MS Run ff .......: 2070023 MDL. ...........: 5.5
SW846 6010B 03/11-03/12/02 EV4X21AI
Analysis Time..: 15:28 Analyst ID.....: -400149
M S Run ».......: 2070023 MDL. ...........: 4.4
62
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Lot-Sampl e tt . ..: C2C090133-002
Dat e Sampled...: 03/08/0 2
BLASLAND BOUCK & LEE
Client Sample ID: NS-45
TOTAL Metals
Dat e Received..: 03/09/02
PARSMET'SP RESULT
REPORTING
LIMIT UNITS METHO D
Matrix.......: WATE R
PREPARATION- WOR K
ANALYSIS SATE ORDE R S
Prep Batch #...: 207022 5
Chromium 1. 3 B
Manganese
Antimony
Thallium
Zinc
NOTE(S):
4570
ND
ND
7.6 B
II fiMiiiuiict l result. Resul t is less ih:in Rl..
5.0 ug/L SW846 6010B 03/11-03/13/02 EV6621AF
Dilution Factor: 1 Analysis Time..: 14:51 Analyst I D . . . . .: 400149
Instrument ID. . : TRACEICP MS Run i f - . . . . . .: 2070093 MDL. . . . . . . . . . . .: 1.1
15.0 ug/L SW846 6010B 03/11-03/13/02 EV6621AD
Dilution Factor: 1 Analysis Time..: 1-1:51 Analyst I D . . . . .: 400H9
Instrument I D . .: TRACEIC? MS Run « . . . . . . .: 2070093 M D L . . . . . . . . . . . .: 0.45
10.0 ug/L SW84 6 6010B 03/11-03/13/02 EV6621AE
Dilution Factor: 1 Analysis Time..: 14 :S1 Analyse I D . . . . .: 400149
Instrument ID..: TRACEIC P MS Run t t . . . . . . .: 2070093 MDIj . . . . . . . . . . . .: 3.8
10.0 ug/L SW846 6010B 03/11-03/13/02 EV6621AG
Dilution Factor: 1 Analysis Time..: l-i:5l Analyst I D . . . . .: 400149
Instrument ID.. : TRACEIC P MS Run f t . . . . . . .: 2070093 M D L . . . . . . . . . . . .: 5.5
20.0 ug/L SW846 6010B 03/11-03/13/02 EV6621AH
Dilution Factor: 1 Analysis Time..: 14:51 Analyst I D . . . . .: 40014,9
Instrument ID.. : TRACEIC P MS Run # . . . . . . .: 2070093 M D L . . . . . . . . . . . .; 4.4
STL Pittsburgh 41
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Lot-Sample #.
Date Sampled.
PARAMETE R
BLASLAND BODCK & LEE
Client Sample ID: NS-46
TOTAL Metals
C2C130Z16-004
03/12/02 Date Received..: 03/13/02
RESULT
REPORTIN G
LIMIT UNITS METHO D
Matrix.......: WATE R
PREPARATION- WOR K
ANALYSIS DATE ORDE R #
Prep Batch ft.
Chromiu m
Manganese
Antimony
Thallium
Zinc
: 2074131
ND
189
ND
ND
ND
5.0 ug/L
Dilution Factor: 1
Instrumen t ID..: TRACEIC P
15.0 ug/L
Dilution Factor.- 1
Instrument ID..: TRACEIC P
10.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
10 . 0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
SW846 6010B 03/15-03/18/02 EWAG71A F
Analysis Time..: 13:17 Analyst ID.....: 400149
MS Run ».......: 2074035 M D L . . , . . . . . . . . .: 1.1
SW846 6010B 03/15-03/18/02 EWAG71AD
Analysis Time..: 13:17 Analyst ID.....: 400149
MS Run # . . . . . . .: 2074035 M D L . . . . . . . . . . . .: 0.45
SW84 6 6010B 03/15-03/18/02 EWAG71A E
Analysis Time..: 13:17 Analyst I D . . . . .: 400149
MS Run #.......: 2074035 M D L . . . . . . . . . . . .: 3.8
SW846 6010B 03/15-03/18/02 EWAG71A G
Analysis Time..: 13:17 Analyst ID....... 400149
MS Run «.......: 2074035 MDL. ...........: S.5
20.0 ug/L SW84 6 6010B 03/15-03/18/02 EWAG71A H
Dilution Factor: 1 Analysis Time..: 13:17 Analyst ID.....: 400149
Instrument ID. . : TRACEICP MS Run ».......: 2074035 MDL. ...........: 4.4
Con. D •! 1- f- c>-,,48
III
I
II
I
I
I
I
I
II
I
I
II
Lot-Sample #.
Date Sampled.
PARAMETER
.: C2C130116-003
.: 03/11/02
BLASLAND BOUCK & LEE
Client Sample ID: NS-47
TOTAL Metals
Date Received..: 03/13/02
RESULT
REPORTING
LIMIT UNITS METHOD
Matrix. ........ WATER
PREPARATION- WORK
ANALYSIS DATE ORDER #
Prep Batch #...: 2074131
Chromium N D
Manganese
Antimony
Thai1ium
Zinc
MOTE(S ) :
1810
ND
ND
9.9 B
5.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
15.O ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
10.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
SW846 6010B 03/15-03/18/02 EWAG61AF
Analysis Time..: 13:12 Analyst ID.....: 400149
MS Run f t . . . . ; . .: 207403S M D L . . . . . . . . . . . .: 1.1
SW846 6010B
Analysis Time..:
M S Run # . . . . . . .:
03/15-03/18/02 EWAG61A D
13:12 Analyst ID.....: 400149
2074035 MDL . ...........: 0.45
SW846 6010B 03/15-03/18/02 EWAG61AE
Analysis Time..: 13:12 Analyst ID.....: 400149
MS Run ».......: 2074035 M D L . . . . . . . . . . . .: 3.8
10.0 ug/L SW84 6 6010B 03/15-03/18/02 EWAG61A G
Dilution Factor: 1 Analysis Time..: 13:12 Analyst ID.....: 400149
Instrument ID..: TRACEICP MS Run #.......: 2074035 M D L . . . . . . . . . . . .: S.S
20.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEICP
SW846 6010B 03/15-03/18/02 EHAG61AH
Analysis Time...- 13:12 Analyst ID.....: 400149
MS Run #.......: 207403S MDL . . . . . . . . . . . .: 4.4
6 Estimate d result. Rcni h * lu» H>a n RL.
<"»mT r> n *- +- 1-11 47
II
I
I
I
II
I
I
I
I
II
I
I
I
I
II
ZjOt-Sample #.
Date Sampled.
PARAMETE R
BLASLAND BOUCK & LEE
Client Sample ID: NS-48
TOTAL Metals
C2C130116-001
03/11/02 Date Received..: 03/13/02
RESULT
REPORTING
LIMIT UNITS METHOD
Matrix.......: WATER
PREPARATION- WORK
ANALYSIS DATE ORDER #
Prep Batch #.
Chromiu m
Manganes e
Antimon y
Thalliu m
Zin c
NOTB(S) :
: 2074131
2.0 B
583O
ND
ND
ND
B Eaiinaic d rcsuh. Resul t is les s tha n RL .
5.0 ug/L SW846 6010B 03/15-03/18/02 EWAG41AF
Dilution Factor: 1 Analysis Time..: 13:01 Analyst ID.....: 40014 9
Instrument ID. .: TRACEIC P MS Run ».......: 2074035 MDL . ............. 1.1
15.0 ug/L
Dilution Factor: 1
Instrument ID. . .- TRACEIC P
10.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
10.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
20.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
SW846 6010B 03/15-03/18/02 EWAG41AD
Analysis Time..: 13:01 Analyst I D . . . . .: 400149
M S Run ».......: 2074035 M D L . . . . . . . . . . . .: 0.45
SW846 6010B 03/15-03/18/02 EWAG41A E
Analysis Time..: 13:01 Analyst I D . . . . .: 40014 9
MS Run ft. ........ 2074035 MDL . . . . . . . . . . . .: 3.8
SW846 6010B 03/15-03/18/02 EWAG41A G
Analysis Time..: 13:01 Analyst ID. ...... 400149
MS Run ft. ......: 2074035 M D L . . . . . . . . . . . .: 5.5
SW846 6010B 03/15-03/18/02 EWAG41A H
Analysis Time..: 13:01 Analyst ID....... 400149
MS Run #.......': 2074035 M D L . . . . . . . . . . . .: 4.4
III
I
I
II
I
I
II
II
I
I
I
III
BLASLAND BOUCK & LEE
Client Sample ID: NS-49
TOTAL Metals
Lot -Sample #.
Date Sampled.
PARAMETE R
Prep Batch #.
Chromium
..: C2C080109
..: 03/07/02
RESULT
..: 2070129
1.6 B
-006
Date Received. . :
REPORTIN G
LIMIT UNITS
5 . 0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEICP
03/08/02
METHOD
SH846 6010B
Analysis Time. . :
MS Run f t . . . . . . .:
Matrix. ......:
PREPARATION-
ANALYSIS CATS
03/11-03/12/02
16 :01 Analyst ID . . . . .
2070023 MDL. . . . . . . . . . ..
WATE R
WOR K
ORDE R S
EV4X91AP
: 400149
: 1.1
Manganese
Antimony
Thallium
Zinc
KOTE(S) :
5870
ND
47.9
B Eahnatc d rotili. Resul t is less Hu n RL .
15.0 ug/L SW846 6010B 03/11-03/12/02 EV4X91AH
Dilution Factor: 1 Analysis Time..: 16:01 Analyst I D . . . . .: 400149
Instrument ID..: TRACEIC P MS Run tt.......: 2070023 M D L . . . . . . . . . . . .: 0.45
10.0 ug/L SW846 6010B 03/11-03/12/02 EV4X91AL
Dilution Factor: 1 Analysis Time..: 16:01 Analyst ID....... 400149
Instrument ID. . : TRACEICP MS Run ».......: 2070023 MDL. ...........: 3.8
10.0 ug/L SW846 6010B 03/11-03/12/02 EV4X91AT
Dilution Factor: 1 Analysis Time..: 16:01 Analyst ID.....: 400149
Instrument ID..: TRACEICP MS Run ».......: 2070023 MDL. . . . . . . . . . , .: S.5
20.0 ug/L SW846 6010B 03/11-03/12/02 EV4X91AW
Dilution Factor: 1 Analysis Time..: 16:01 Analyst ID.....: 400149
Instrument ID. . : TRACEICP MS Run ».......: 2070023 MDL. ...........: 4.4
Pi t-.t 67
II
I
I
I
I
I
I
I
I
I
II
I
I
I
Lot-Sample #.
Dace Sampled.
C2C160140-003
03/13/02
BLASLAND BOUC K & LEE
Client Sample ID: NS-50
TOTA L Metals
Date Received..: 03/16/02
Matrix.......: WATE R
PARAMETE R
Prep Batch
Chromium
RESULT
#. . . : 2077231
2.4 B
REPORTING
LIMIT
5.0
UNITS
ug/L
Instrument ID.. -. TRACEICP
METHO D
SW846 6010B
MS Run « . . , . ' . . .:
PREPARATION -
ANALYSIS DATE
03/18-03/22/02
11:5 6 Analyst ID. . . . .
2077087 MDL . . . . . . . . . . ..
WOR K
ORDE R #
EWHDM1A F
: 400149
: 1.1
Manganese
Antimony
Thallium
Zinc
NOTE(S) :
2680 J 15.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
ND 10.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEICP
ND 10.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
ND 20.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEICP
SW846 6010B 03/18-03/22/02 EWHDH1A D
Analysis Time..: 11:56 Analyst ID....... 40014 9
MS Run H .......: 2077087 M D L . . . . . . . . . . . .: 0.45
SW846 6010B 03/18-03/22/02 EWHDM1A E
Analysis Time..: 11:56 Analyst I D . . . . .: 400149
MS Run #.......: 2077087 M D L . . . . . . . . . . . .: 3.8
SW846 6010B 03/18-03/22/02 EWHDM1A G
Analysis Time...- ll:SG Analyst ID.....: 40014 9
MS Run #.......: 2077087 M D L . . . . . . . . . . . .: 5.5
SW846, 6010B 03/18-03/22/02 EWHDM1A H
Analysis Time..: ll:5« Analyst ID.....: 4001*9
MS Run #.......: 2077087 M D L . . . . . . . . . . . .: 4.4'
B Estimate d rcsuli. Resul t is less Ilian RL.
J MvfUtK l blank contiimiiiatkm . Tlic ajsociatcd niciliut l blan k cuiuaii u the targe t aiialyt c at a repnnablc level.
STL Pittsburgh 79
IIIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Client Sampl e ID: NS-51
TOTAL Metals
Lot-Sample ft. .
Date Sampled. .
PARAMETE R
Prep Batch ft . .
Chromium
c*f}c*c\ o m rt Q
.: 03/07/02
RESULT
. : 2070129
1.6 B
007
Date Received. . :
REPORTING
LIMIT UNITS
5 . 0 ug/L
Instrument ID. . : TRACEIC P
03/08/02
METHO D
SW846 6010B
MS Run 8 . . . . . . .;
Matrix. ......:
PREPARATION-
ANALYSIS DATE
03/11-03/12/02
16:2 3 Analyst ID. . . . .
2070023 MDL. ...........
UiaTlT?D
WOR K
ORDE R f t
EV40F1AF
: 400149
: 1.1
Manganese
Antimon y
Thallium
Zinc
NOTE(S):
3460
ND
ND
41.8
B Hsiimalix i result . Rcnil i in less tha n RL .
15.0 ug/L SW846 6010B 03/11-03/12/02 EV40F1AD
Dilution Factor: l Analysis Time..-. 16:23 Analyse ID.....: 400149
Instrument ID. . : TRACEIC P MS Run 8.......: 2070023 M D L . . . . . . . . . . . .: 0.4S
10.0 ug/L SW846 6010B 03/11-03/12/02 EV40P1AE
Dilution Factor: l Analysis Time..: 1S:23 Analyst ID.....: 40014 9
Instrument ID. . : TRACEICP MS Run # . . . . . . .: 2070023 M D L . . . . . . . . . . . .: 3.8
10.0 ug/L SW846 6010B 03/11-03/12/02 EV40F1AG
Dilution Factor: 1 Analysis Time..: 16:23 Analyst ID....... 400149
Instrument ID..: TRACEIC P MS Run f t . . . . . . .: 2070023 MDL . ...........: 5.5
20.0 ug/L SW846 6010B O3/11-03/12/02 BV40F1AH
Dilution Factor: l Analysis Time..: 16:23 Analyst ID.....: 400149
Instrument ID. .: TRACEICP MS Run ».......: 2070023 M D L . . . . . . . . . . . .: 4.4
CITT. P-i 68
1111111111111111111
BLASLAND BOUCK & LEE
Client Sample ID: DUP-030702
TOTAL Metals
Lot-Sample*...: C2C080109-00 9 Matrix. ......:
Date Sampled. ..: 03/07/02 Date Received ..: 03/08/02
REPORTING PREPARATION -
PARAMETE R RESULT LIMIT UNITS METHO D ANALYSIS DATE
Prep Batch #...: 2070129
Chromium 1.7 B 5.0 ug/L SW846 6010B 03/11-03/12/02
Dilution Factor: 1 Analysis Time..: 16:34 Analyst ID.....
Instrument ID. . : TRACEICP MS Run # . . . . . . .: 2070023 MDL . . . . . . . . . . ..
Manganese 3430 15.0 ug/L SW846 6010B 03/11-03/12/02
Dilution Factor: 1 Analysis Time..: 16:34 Analyst I D . . . ..
Instrument ID. . : TRACEICP MS Run # . . . . . . .: 2070023 MDL . ...........
Antimony ND 10.0 ug/L SW84 6 6010B 03/11-03/12/02
Dilution Factor: 1 Analysis Time..: 16:34 Analyst ID.....
Instrument ID. . : TRACEIC P MS Run ft. ......: 2070023 MDL. . . . . . . . . . ..
•Thallium ND 10.0 ug/L SW846 6010B 03/11-03/12/02
Dilution Factor: 1 Analysis Time..: 16:34 Analyst ID.....
Instrument ID. . : TRACEIC P MS Run tt .......: 2070023 MDL . . . . . . . . . . ..
Zinc 31.0 20.0 ug/L SW846 6010B 03/11-03/12/02
Dilution Factor: 1 Analysis Time..: 16:34 Analyst ID.....
instrument ID. . : TRACEICP MS Run ft .......: 2070023 MDL . . . . . . . . . . ..
NOTE(S) :
B Estimate d result . Resul t is less (Ira n RL .
Utt*ri?D"Al tK
WOR K
ORDE R #
EV40J1AF
• 400149
: 1.1
EV40J1AD
: 400149
; 0.45
EV40J1AE
• 400149
• 3.8
EV40J1AG
• 400149
: S.5
EV40J1AH
• 400149
: 4.4
STL Pittsburah 70
I
I
I
I
I
I
II
I
II
III
II
I
I
I
Lot-Sample #.
Date Sampled.
PARAMETE R
BLASLAND BOUC K & LEE
Client Sample ID: NS-52
TOTAL Metals
..: C2C160140-002
..: 03/13/02 Date Received..: 03/16/02
RESULT
REPORTIN G
LIMIT UNITS METHO D
Matrix.......: WATE R
PREPARATION- WOR K
ANALYSIS DATE ORDER
Prep Batch #...: 2077231
Chromium l.l B 5.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run # . . . . . . .:
Manganese
Antimony
Thallium
Zinc
NOTE(S) :
1070 J
ND
ND
ND
15.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run # . . . . . . .:
10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run « . . . . . . .:
10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID . . : TRACEIC P MS Run f t . . . . . . .:
20.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run # . . . . . . .:
03/18-03/22/02 EWHDKXA F
11:50 Analyst ID.....: 400119
2077087 MDL. ...........: 1.1
03/18-03/22/02 EWHDK1AD
11:50 Analyst ID.....: 400149
2077087 M D L . . . . . . . . . . . .: 0.45
03/18-03/22/02 EWHDK1A E
11:50 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 3.8
03/18-03/22/02 EWHDK1A G
11:50 Analyst ID.....: 400149
2077087 M D L . . . . . . . . . . . .: 5.5
03/18-03/22/02 EWHDK1A H
11:50 Analyst ID.....: 400149
2077087 M D L . . . . . . . . . . . .: 4.4
B Estimate d result . Rcail i is le u tha n RL .
J Mahm l hlun k contamination . Th e associate d mvtlio d blan k contain s th e targe t aiialyi c at u importabl e level .
STL Pittsburgh 78
1111111111111111111
BLASLAND BOUCK & LEE
Client Sample ID: DUP-031302
TOTA L Metals
Lot-Sample #...: C2C160140-005
Date Sampled...: 03/13/02 Date Received..: 03/16/02
REPORTING
PARAMETE R RESULT LIMIT UNITS METHO D
Prep Batch #...: 2077231
Chromiu m N D 5.0 ug/L SW84 6 6010 B
Dilution Factor: 1 Analysis. Time..:
Instrument ID . . : TRACEIC P MS Run ft .......:
Manganese 412 J 15.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time. . :
Instrument ID . . : TRACEIC P MS Run #.......;
Antimony ND 10.0 ug/L SW84 6 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID. . : TRACEIC P MS Run # . . . . . . .:
Thallium ND 10.0 ug/L SW84 6 6010B
Dilution Factor: 1 Analysis Time. . :
Instrument ID. . : TRACEICP MS Run #.......:
Zinc 26.8 20.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID. . : TRACEIC P MS Run «.......:
NOTE(S) :
J Mmlio U blan k cumamjiwmm . Tin ; associate d matKi d blan k en main s ilic larga inalyi e at a rc|K>rcabl c level .
ITT. D-i H- oVYiiT-rrTi
Matrix. ......:
PREPARATION-
ANALYSIS DATE
03/18-03/22/02
12:0 9 Analyst ID. . . . .
2077087 MDL . ...........
03/18-03/22/02
12:09 Analyst ID. . . . .
2077087 MDL . ...........
03/18-03/22/02
12:09 Analyst ID.
2077087 MDL . . . . . . . . . . ..
03/18-03/22/02
12:0 9 Analyst ID. . . . .
2077087 MDL . . . . . . . . . . ..
03/18-03/22/02
12:0 9 Analyst ID. . . . .
2077087 MDL . . . . . . . . . . ..
WATE R
WOR K
ORDE R f t
EWHDQ1A F
- 400149
• 1.1
EWHDQ1AD
• 400149
: 0.45
EWHDQ1A E
: 400149
• 3.8
EWHDQ1AG
: 400149
• 5.5
EWBDQ1AH
• 400149
• 4.4
81
I
I
I
I
I
I
I
I
I
I
I
II
I
I
I
I
I
I
Lot-Sample #.
Date Sampled.
PARAMETER
BLASLAND BOUCK & LEE
Client Sample ID: NS-53
TOTAL Metals
.: C2C160140-001
,.: 03/13/0 2 Date Received..: 03/16/0 2
RESULT
REPORTING
LIMIT UNITS METHOD
Matrix.......: WATER
PREPARATION- WORK
ANALYSIS DATE ORDER
Prep Batch. #..
Chromium
Manganese
Antimony
Thai1ium
Zinc
NOTE(S):
. : 2077231
1.1 B
411 J
ND
ND
31.9
5.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..-.
Instrument ID..: TRACEICP MS Run « . . . . . . .:
15.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run « . . . . . . .:
10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run * . . . . . . .:
10.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID. .: TRACEIC P MS Run # . . . . . . . -.
20.0 ug/L SW846 6010B
Dilution Factor: 1 Analysis Time..:
Instrument ID..: TRACEIC P MS Run 8 .......:
03/18-03/22/02 EWHDH1AF
11:18 Analyst ID.....: 400149
2077087 M D L . . . . . . . . . . . .: 1.1
03/18-03/22/02 EWHDH1AD
11:18 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 0.45
03/18-03/22/02 EWHDH1AE
11:18 Analyst ID.....: 400149
2077087 MDL . ...........: 3.8
03/18-03/22/02 EWHDH1A G
11:18 Analyst I D . . . . .: 400149
2077087 M D L . . . . . . . . . . . .: 5.5
03/18-03/22/02 EWHDHlft H
11:18 Analyst ID.....: 400149
2077087 M D L . . . . . . . . . . . .: 4.4
B Esliiiinici l result. Rcui h is less ilin n RL.
1 McihiK l hbnk riiniainiiEimm . Tli u associate d nicilHu l blan k cpmaiii s (h e (argu analyi c ai a rcponabl u level .
STL Pittsburgh 77
1111111111111111111
BLASLAND BOUCK & LEE
Client Sample ID: NS-54
TOTAL Metals
Lot-Sample #...: C2C130116-005 Matrix. ......:
Date Sampled. . . : 03/12/02 Date Received. . : 03/13/02
REPORTING PREPARATION-
PARAMETE R RESULT LIMIT UNITS METHO D ANALYSIS DATE
Prep Batch #...-. 2074131
Chromium 1.5 B 5.0 ug/L SW846 6010B 03/15-03/18/02
Dilution Factor: 1 Analysis Time..: 13:22 Analyst ID.....
Instrument ID. . : TRACEICP MS Run # . . . . . . .: 2074035 MDL. ...........
Manganese 4520 15.0 ug/L SW846 6010B 03/15-O3/18/02
Dilution Factor: l Analysis Time..: 13:22 Analyst I D . . . ..
Instrument ID. . : TRACEIC P MS Run tt. ......: 2074035 MDL. ...........
Antimony ND 10.0 ug/L SW84 6 6010B 03/15-03/18/02
Dilution Factor: 1 Analysis Time..: 13:22 Analyst I D . . . ..
Instrument ID. . : TRACEICP MS Run « . . . . . . .: 2074035 MDL . . . . . . . . . . ..
Thallium ND 10.0 ug/L SW846 6010B 03/15-03/18/02
Dilution Factor: 1 Analysis Time . . t 13:22 Analyst I D . . . ..
Instrument ID. . : TRACEIC P MS Run # . . . . . . .: 2074035 MDL. ...........
Zinc 248 20.0 ug/L SW846 6010B 03/15-03/18/02
Dilution Factor: 1 Analysis Time..: 13:22 Analyst ID.....
Instrument ID. . : TRACEICP MS Run #.......: 2074035 MDL. ...........
NOTE(S) :
B Eiiim.ilc d rvsuti. Rcsii H is less than RL.
WfiTTTDH*A I jc*i\
WOR K
ORDE R #
EWAG81AP
• 400149
• 1 .1
EWAG81A H
• 400149
• 0.45
EWAG81A L
: 400149
•a ft. J . O
E WA G 81 AT
: 400149
: 5.5
KWAG81A H
• 400149
T 4.4
CTT. D-i H-49
IIIIIIIIIIIIIIIIIII
Lot-Sampl e t.
Date Sampled.
PARAMETEP
BLASLAND BOUCK & LEE
Client Sampl e ID: CT-1
TOTAL Metals
C2C080109-008
03/07/02 Dat e Received..: 03/08/02
Matrix.WATER
RESULT
REPORTING
LIMIT UNITS METHOD
PREPARATION- WORK
ANALYSIS DATE ORDER
Prep Batch #.
Chromiu m
Manganese
Antimony
Thallium
Zinc
: 2070129
ND
163
ND
ND
22.7
5.0 ug/L
Dilution Factor: 1
Instrument ID. . : TRACEICP
15.0 ug/L
Dilution Factor: i
Instrument ID..: TRACEIC P
SW84 6 6010B 03/11-03/12/02 EV40H1AF
Analysis Time..: 16:29 Analyst I D . . . . .: 400149
MS Run *.......: 2070023 M D L . . . . . . . . . . . .: 1.1
SW846 6010B 03/11-03/12/02 EV40H1AD
Analysis Time..: 16:29 Analyst ID.....: 40014 9
MS Run « . . . . . . .: 2070023 MDL. . . . . . . . . . . .: 0.45
10.0 ug/L SW846 6010B 03/11-03/12/02 EV40H1AE
Dilution Factor: 1 Analysis Time..: 16:29 Analyst ID.....: 400149
Instrument ID..: TRACEIC P MS Run # . . . . . . .: 2070023 MDL . . . . . . . . . . . .: 3.8
10 .0 ug/L
Dilution Factor: 1
Instrumen t ID..: TRACEIC P
20.0 ug/L
Dilution Factor: 1
Instrument ID..: TRACEIC P
SW846 6010B 03/11-03/12/02 EV40H1AG
Analysis Time..: 16:29 Analyst ID.....: 400149
MS Run tt. ......: 2070023 MDL. ...........: 5.5
SW846 6010B 03/11-03/12/02 EV40H1AH
Analysis Time..: 16:29 Analyst I D . . . . .: 400149
MS Run «.......: 2070023 MDL. ...........: 4.4
STL Pittsburah 69
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Date:OS/07/200 1
CUSTOMER : Blasland . Bouc k & Lee. Inc. PROJECT : BB L ATTN : Csth y Yewdal l
Custome r Sairpl e ID : E8 - 07260 1 Laborator y Sampl e ID : 200987-1
Dat e Sampled . .....: 07/26/200 1 Dat e Received . ......: 07/27/200 1Time Sampled . .....: 08:15 Tim e Received . ......: 10:15Sample Matrix . ....: Wate r
TES T METHO D
SW84 6 8260B
>
PARAMETER/TES T DESCRIPTIO N
Volatil e Organic s (5mL Purge/2 5 m L RLs)Viny l chlorid eChloroethaneCarbon disulfid eAcetoneHethylene chlorid etrans-1,2-Dichloroethen ecis-1,2-Dichloroethen e2-Butanon e (MEK)Chlorofor m1.2-Dichloroethan eTrichloroethene
1 , 2 -D i c h I oropropan eBromodichloromethaneToluene1,1,2-Trichloroethan eTetrachloroethene0 i bromoc h I orom e than eEthylbenzeneXylenes (total )
i
SAMPL E RESUL T
MD
ND
NO
ND 2NDNO
ND
ND
NDND
ND
N D
NDND
N D
ND
ND
ND
Q
U
U
U
U
U
U
U
U
UU
U
U
U
U
UUU
U
FLAG S MO L , :
0.40.30.310.50.3
0.30.90.30.30.30.30.30.30.40.50.30.30.5
. ..:- R L ' !'
1115111511111111111
DILUTIO N
1111
1
11
1111111111
11
UNIT S
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
BATC H
405 5405540554055
405 540554055405540554055405540554055
40554055
4055405540554055
DT DATE/TIM E
08/03/0 1 032 508/03/0 1 032 5
08/03/01 032508/03/0 1 032 508/03/0 1 032 508/03/01 032508/03/0 1 032 508/03/0 1 032 508/03/0 1 032 508/03/0 1 032 5
08/03/0 1 032 508/03/01 032 508/03/01 032508/03/0 1 032 508/03/0 1 032 508/03/0 1 032 508/03/0 1 032 508/03/0 1 032 508/03/01 0325
TEC H
cgi acgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgia
In Description = Dry Wgt.Pag e 2
L A B O R A T O R Y T E S T R E S U L T S
0to00
Jo b Number : 200987 Date:08/07/200 1
CUSTOMER : Bia s 1 and , Bouc k & Lee. Inc. PROJECT : BB L ATTN : Cath y Yeudal l
Custome r Sampl e ID : NS-3 3 Laborator y Sampl e ID : 200987-2Date Sampled......: 07/26/200 1 Dat e Received.. .....: 07/27/200 1
Tim e Sampled...... : 10:20 Tim e Received.. .....: 10:15Sample Matrix.....: Uate r
TES T METHO D
SU846 8260B
PARAMETER/TES T DESCRIPTIO N
Volatil e Organic s (5mL Purge/2 5 m L RLs)Viny l chlorid eChloroethaneCarbon disulfid eAcetoneMethylene chlorid etrans-1,2-Dichloroethen ecis-1,2-Dich l oroethen e
2-Butanon e (MEK)Chlorofor m1 .2-0 i chloroethan eTrichloroethene1,2-Dichtoropropan eBromodi ch torom e than eToluene1. 1,2-Trichloroethan e
Tetrachloroethen eD i bromoc h I orom e than eEthytbenzeneXytenes (total )
i
SAMPL E RESUL T
NONDND
ND
ND
ND
ND
ND
ND
ND
NOND
ND
NO
NO
NDND
ND
ND
Q
U
UU
U
U
U
U
U
UU
U
UUU
U
U
UUU
FLAG S . . MD L ,
0.40.30.310.5
0.30.30.90.30.30.30.30.30.30.40.50.30.30.5
RL
1
11511151
1111
DILUTIO N
1
111
1
11
1
1
1
UNIT S
ug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
BATC H
40554055405540554055405540554055405540554055405540554055405540554055
40554055
DT DATE/TIM E
08/03/01 0422
08/03/01 042208/03/0 1 042 2
08/03/01 042208/03/0 1 042 208/03/0 1 042 208/03/0 1 042 208/03/01 042208/03/0 1 042 208/03/0 1 042 208/03/0 1 042 2
08/03/0 1 042 206/03/0 1 042 208/03/01 042208/03/0 1 042208/03/01 042208/03/01 042208/03/0 1 042 2
08/03/01 0422
TEC H
cgi acgiacgiacgiacgiacgiacgiacgfacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgia
In Description = Dry Ugt.Page 3
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Date:08/07/200 1
~
D
Z >
CUSTOMER : Blasland . Bouc k & Lee, Inc. . .• . PROJECT : BB L . ATTN : Cath y Yewdal l
Custome r Sampl e ID : NS-4 2 Laborator y Sampl e ID : 200987-3Date Sampled......: 07/26/200 1 Dat e Received . ......: 07/27/200 1
Tim e Sampled......: 13:50 Tim e Received... ....: 10:1 5Sample Matrix.....: Wate r
TES T METHO D
SU846 82608
PARAMETER/TES T DESCRIPTIO N
Volatil e Organic * (5mL Purge/2 5 m l RLs)Viny l chlorid eChloroethaneCarbon disti l fid e
Aceton eMethylen e chlorid et ran s - 1 , 2 - D i c h I oroethen ecis-1,2-Dich l oroethen e2-Butanon e (NEK)Chlorofor m1,2-Dichloroethan eTrichloroethene1,2-Dichloropropan eBromod i c h I oromethan eToluene1 , 1 ,2-Trichloroethan eTet rac h I oroethen eD i bromoc h I oromethan eEthyl benzen eXylenes (total )
i
SAMPL E RESUL T
3740
ND '56
10
ND 30
ND
ND 68011
ND
ND 1 1
ND
ND
NDNO 6
Q
U
U
U
U
UU
U
UU
U
FLAG S
6ft
MO L .
2225222422222222222
: RL.
555255552555555555555
DILUTIO N
5555
555555555555555
UNIT S
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
BATC H
40554055405540554055405540554055405540554055405540554055
40554055
405 540554055
D T DATE/TIM E
08/03/01 142008/03/0 1 142008/03/0 1 142008/03/0 1 1420
08/03/0 1 142008/03/0 1 142008/03/0 1 142008/03/0 1 142008/03/0 1 142008/03/0 1 1420
08/03/01 142008/03/0 1 142008/03/01 142008/03/0 1 142008/03/0 1 142008/03/0 1 142008/03/0 1 142008/03/0 1 142008/03/0 1 1420
TEC H
cgi acgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgia
* In Description = Dry Ugt.Page 4
L A B O R A T O R Y T E S T R E S U L T SJob Number : 200987 Oate:OS/07/200 1
CUSTOMER : Blastand , Bouc k & Lee , Inc . PROJECT : BB L ATTN : CathyYeudal l
Custome r Sampl e 10 : NS-4 9 Laborator y Sampl e ID : 200987-4Date Sampled......: 07/26/200 1 Dat e Received.. .....: 07/27/200 1Time Sampled . .....: H.-1 5 Tim e Received . ......: 10:1 5Sample Matrix.....: Uate r
TES T METHO D
SU846 8260B
CCJo0GJo
PARAMETER/TES T DESCRIPTIO N
Volatil e Organic s (Sm L Purge/2 5 m l RLs )Viny l chlorid eCh I ore-ethan eCarbon disulfid eAcetoneMethyl en e chlorid etrans-1 , 2-Oichloroethen ec i s - 1 , 2-0 i c h I oroethen e2-Butanon e (MEK )Chlorofor m1 ,2-Dichloroethan eTrichloroethene1 , 2 - 0 i c h I oropropan eBromodichloromethaneToluene1,1,2-Trichloroethan eTetrachloroetheneD i bromoc h 1 orom e than eEthylbenzene
Xylene s (total )
i
SAMPL E RESUL T
NDND
ND
130
NDND
ND
ND
ND
7900
ND
ND
NDND
ND
NDNDND
ND
0
UU
U
J
U
UUU
U
U
U
U
U
UU
U
UU
FLAG S
&
•'. •'.'- HD L
20151550251515
45
15
15151515152025
1 51525
• . : .R L .•• . •
50505025050505025050
50505050
505050
505050
DILUTIO N
5050505050505050505050505050
5050505050
UNIT S
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/L
BATC H
40554055405540554055405540554055
40554055405540554055405540554055405540554055
DT DATE/TIK E
08/03/01 144 908/03/0 1 144 908/03/0 1 144 9
08/03/0 1 144 9
08/03/0 1 144 908/03/0 1 144 908/03/0 1 144 908/03/01 144 9
08/03/0 1 K4908/03/01 144 908/03/0 1 144 908/03/0 1 144 908/03/0 1 144 908/03/01 144 908/03/01 144 908/03/01 144 908/03/0 1 144 9
08/03/0 1 144 908/03/0 1 144 9
TEC H
cgi acgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgia
In Description = Dry Ugt.Page 5
L A B O R A T O R Y T E S T R E S U L T S
DD.J
Jo b Nunfcer : 200987 Date : 08/07/200 1
CUSTOMER : Blasland , Bouc k & Lee. Inc. PROJECT : BB L ATTN : Cath y Yewdal l
Custome r Sampl e ID : NS-3 9 Laborator y Sampl e ID : 200987-5Date Sampled......: 07/26/200 1 Dat e Received.. .....: 07/27/200 1
Tim e Sampled.... ..: 17:10 Tim e Received.. .....: 10:15Sample Matrix.....: Wate r
TES T METHO D
SW846 8260B
PARAMETER/TES T DESCRIPTIO N :
Volatil e Organic s (5mL Purge/2 5 m C RLs )Viny l chlorid eChloroethaneCarbon disulfid eAcetoneHethylene chlorid etrans- 1 ,2-Oichloroethen ecis-1.2-Dichloroethen e2-Butanon e (MEK)Chlorofor m1 , 2 - D i c h I oroethan eTrichloroethene1 , 2 - D i c h I oropropan eBromodich loromethan e
Toluen e1 , 1 ,2-Trichloroethan eTetrachloroethene
D i bromoc h loromethan eEthylbenzeneXylenes (total )
i
SAMPL E RESUL T
1 4
ND
ND
ND 10
ND
ND
ND 0.73112
ND
N D
10.8
N DND
ND
Q
U
U
U
UU
U
J
UU
J
U
U
U
FLAG S • .-i MOL . ••,'..•: •
0.40.30.31
0.50.30.3
0.90.30.30.30.30.30.30.40.5
0.30.30.5
Y :;' Y.R L . ;' :• .DILUTIO N
1
1
11
UNIT S
ug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
BATC H
4055
405 5405540554055405540554055
405 540554055405540554055405540554055
405 54055
DT DATE/TIM E
08/03/01 0547
08/03/01 054708/03/0 1 054 708/03/01 054708/03/0 1 054 708/03/0 1 054 708/03/01 054708/03/01 054708/03/0 1 054 708/03/0 1 054 708/03/0 1 054 708/03/0 1 054 7
08/03/01 054708/03/01 054708/03/0 1 054 7
08/03/0 1 054 708/03/01 054708/03/0 1 054 708/03/0 1 054 7
TEC H
cgi acgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgia
cgi acgiacgia
cgi acgiacgiacgia
* In Description = Dry Ugt.Pag e 6
L A B O R A T O R Y T E S T R E S U L T SJob Number : 200987 Date:08/07/200 1
i
CUSTOMER : Blasland , Bouc k 4 Lee , Inc . PROJECT : BB L ATTN : Cath y Yewdal l
I
A
•5
Custome r Sampl e ID : NS-9 0 Laborator y Sampl e ID : 200987-6Date Sampled......: 07/26/200 1 Dat e Received . ......: 07/27/200 1
Tim e Sampled . .....: 00:00 Tim e Received . ......: 10:1 5Sample Matrix.....: Wate r
TES T METHO D
SWB4 6 8260 B
PARAMETER/TES T DESCRIPTIO N
Volatil e Organic s (5m L Purge/2 5 m l RLs )Viny l chlorid eChloroethaneCarbon disulfid e
Aceton eMethylen e chlorid etrans-1 ,2-Dichloroethen ecis-1,2-0ichloroethen e2-Butanon e (HEX )Chlorofor m
1,2-Dichloroethan eTrichloroethene1 , 2 -D i c h 1 oropropan cBromod i c h I oromethan e
Toluen e1 , 1 ,2-Trichloroethan eTetrachloroethene
D i bromoc h I orome t han eEthylbenzeneXylenes (total )
i
SAMPL E RESULT .
3838
NO •3 210
ND 29
NO
ND 790
1 1ND
ND 1 3
NO
ND
N D
ND 7
Q
U
U
U
U
UU
U
U
U
U
FLAG S
0Q>
•'..'• MDL . j /
2225222422222222222
R L
55
5255552555555
5
5
5555
DILUTIO N
555
5
555555555555555
UNIT S
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
BATC H
40554055
405 540554055405540554055405540554055
405 54055405540554055405540554055
DT DATE/TIM E
08/03/01 151708/03/01 151 708/03/01 151 708/03/01 151 708/03/0 1 151 7
08/03/0 1 151 708/03/0 1 151 708/03/01 151 708/03/0 1 151 708/03/0 1 151 708/03/0 1 151 708/03/0 1 151 708/03/0 1 151 708/03/0 1 151 708/03/0 1 151 708/03/0 1 151 708/03/0 1 151 708/03/0 1 151 708/03/0 1 151 7
TEC H
cgi acgiacgiacgiacgfacgiicgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgia
* In Description = Dry Ugt.Page 7
L A B O R A T O R Y T E S T R E S U L T S
CCO
0
OLTQD
Jo b Number : 200987 Oate:08/07/200 1
CUSTOMER : Blasland , Bouc k & Lee. Inc. ; PROJECT : BB L .{:'•'••• :. ATTN : Cath y Yewdal l
Custome r Sampl e ID : TRI P BLAN K Laborator y Sampl e ID : 200987-7
Dat e Sampled......: 07/26/2001 Dat e Received . ......: 07/27/200 1Time Sampled . .....: 00:00 Tim e Received.. .....: 10:15Sample Matrix.....: Wate r
TES T METHO D
SW846 8260 B
l "
PARAMETER/TES T DESCRIPTIO N
Volatil e Organic s (5mL Purge/2 5 m L RLs)Viny l chlorid eChloroethaneCarbon disulfid eAcetoneMethylene chlorid etrans- 1 ,2-Dichloroethen ecis-1.2-0ichloroethen e2-Butanon e (HEK)Chlorofor m1,2-Dichloroethan eTrichloroethene1,2-Dichloropropan eBromodichloromethan eToluene1, 1 , 2 - Tr i chloroethan eTetrachloroetheneD i bronwc h I oromethan eEthyl benzen e
Xylene s (total )
!
SAMPL E RESUL T
N O
NDND ' 2NDND
ND
ND
ND
ND
NDNO
NO
ND
ND
ND
NDND
ND
0
U
U
U
J
UUU
U
U
U
UU
U
U
UU
U
U
U
FLAG S . .; MDL . '
0.4
0.30.310.50.30.30.90.30.30.30.30.30.30.40.50.3
0.30.5
RL
1
1
1
DILUTIO N
1
1
1
11
1
11
1
1
1
UNIT S
ug/L
ug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
BATC H
40554055
4055
4055405540554055405540554055
405 5
405 5405540554055405540554055
405 5
D T DATE/TIM E
08/03/0 1 035 308/03/01 035308/03/0 1 035 308/03/0 1 035 308/03/0 1 035 308/03/0 1 035 3
08/03/0 1 035 308/03/01 035308/03/01 0353
08/03/0 1 035 308/03/0 1 035 308/03/0 1 035 308/03/0 1 035 308/03/01 035308/03/01 035308/03/0 1 035 308/03/0 1 035 308/03/0 1 035 308/03/0 1 035 3
TEC H
cgi acgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgiacgia
* In Description = Dry Wgt.Page 8
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Date:08/20/200 1
CUSTOMER : Bia s 1 and , Bouc k & Lee , Inc . PROJECT : BB L ATTN : Cath y Yewdal l
Custome rDate Sam ;Tim e Sam fSample H «
TES T METHO D
SU846 8270 C
0I*
O
Sampl e ID : EB - 072601iled......: 07/26/2001
iled......: 08:1 5
PARAMETER/TES T DESCRIPTIO N
Semivolatil e Organic *Bis(2-chloroethyl)ethe rOi-n-buty l phthalat e
Bis(2-ethylhexyl)phthalat eDi-n-octy t phthalat e
i
La t
Da tTin
SAMPL E RESUL T
N D
ND
ND
NO
Q
U
U
U
U
FLAG S
x
wrator y Sampl e ID : 200987-1e Received.......: 07/27/200 1
n e Received..... ..: 10:1 5
. MD L
2
2
3
.••;: ' • • R L ;
10101010
DILUTIO N
1
1
11
UNIT S
ug/L
ug/Lug/Lug/L
BATC H
428942894289
4289
DT DATE/TIM E
08/13/0 1 215 108/13/0 1 215 108/13/0 1 215 1
08/13/0 1 215 1
TEC H
shr ashrashrashra
O —— : — : ————————————————— ..—-.. - - ..
G D
L A B O R A T O R Y T E S T R E S U L T S
Job Number: 200987 Date:08/20/2001
CUSTOMER : Blasland. Bouck & Lee. Inc. PROJECT : BBL : : ATTN : Cathy Yeudall
Customer
Date Sam)
T iine Sam)
Sample H:
TES T METHO D
SU846 B270C
SV
1
)
) '•>
Sample ID: NS-3 3
>led. .....: 07/26/2001
>led....,.: 10:20itrix.....: Wate r
PARAMETER/TES T DESCRIPTIO N
Semivolat ile Organics
Bis(2-chloroethyl )etherDi-n-butyl phthalateBis(2-ethylhexyl)phtha(ate
Oi-n-octyl phthalate
i
Lal
DaTif
SAMPL E RESUL T
N O
N O
ND
ND
0
Uu
Uu
FLAG S
;•-,
joratory Sample ID: 200987-2
te Received.......: 07/27/2001
ne Received... ....: 10:15
MO L
2
4
2
3
. R L
10
10
1010
'
DILUTION
1
1
1
1
UNITS
ug/Lug/Lug/Lug/L
BATC H
4289
4289
4289
4289
DT DATE/TIM E
08/13/01 2230
08/13/01 2230
08/13/01 2230
08/13/01 2230
TEC H
shra
shra
shra
shra
In Description = Dry Ugt.Page 3
L A B O R A T O R Y T E S T R E S U L T SJob Number : 200987 Date:08/20/200 1
CUSTOMER : Blasland , Bouc k & Lee , Inc. : PROJECT : BB L ATTN : CathyYewdal l
Custome rDate Sa mT im e Sam ]Sampl e M <
TES T METHO D
SW846 8270C
i
^
JU0ol-k;/i
Sampl e ID : NS-4 2sled......: 07/26/200 1alcd......: 13:5 0
PARAMETER/TES T DESCR1PTIO M
Sem i volatil e Organic sBis(2-chloroethyl)ethe rDi-n-buty l phthalat eBis(2-ethylhexyl)phthalat e
Di-n-octy l phthalat e
i
La tDa1Tin
SAMPL E RESUL T
N O
N O
NO
HO
Q
U
U
U
U
FLAG S
\
xjrator y Sampl e ID : 200987-3e Received.......: 07/27/200 1w Received.......: 10:1 5
MD L
2423
R L
10101010
DILUTIO N
111
1
UNIT S
ug/L
ug/Lug/Lug/L
BATC H
4289
428942894289
D T DATE/TIM E
08/13/0 1 230808/13/0 1 230 808/13/0 1 230 808/13/0 1 230 8
TEC H
shr ashrashrashra
In Description = Dry Ugt.Page 4
L A B O R A T O R Y T E S T R E S U L T S
Job Number: 200987 Date:08/20/2001
CUSTOMER : Blasland, Bouck & Lee, Inc. PROJECT : BBL . • ; '• ATTN : Cathy Yewdall
Customer
Date Sam g
Time Sam;
Sample M <
TES T METHO D
SU8A 6 8270 C
Sample ID: NS-4 9
?led. .....: 07/26/2001
jled. .....: U:15
PARAMETER/TES T DESCRIPTIO N
Semi volatile OrganicsBis(2-chloroethyl)etherDi-n-butyl phthalateBis(2-ethylhexyl)phthalate
Di-n-octyl phthalate
i
Lat
DatTin
SAMPL E RESUL T
9
ND
ND
ND
Q
J
U
U
U
FLAG S
\
xiratory Sample tt): 200987-4
e Received.......: 07/27/200 1
ie Received. ......: 10:15
MD L
2
4
2
3
: • R l :
10
1010
10
DILUTIO N
1
1
1
1
UNIT S
ug/L
ug/L
ug/Lug/L
BATC H
4289
4289
4289
4289
DT DATE/TIM E
08/13/01 2346
08/13/01 2346
08/13/01 2346
08/13/01 2346
TEC H
shrashra
shra
shra
In Description = Dry Wgt.Pag e 5
L A B O R A T O R Y T E S T R E S U L T S
Job Number: 200987 Oate:08/20/2001
.'USTOMER : Blasland. Bouck & Lee. Inc. PROJECT : BBL ATTN : Cathy Yewdall
Custome r
Dote Sam)
T hu e Sant fSample M;
TES T METHO D
SW84 6 8270C
5k
)
>
I
k
Sample ID: NS-39
)led......: 07/26/2001
>led......: 17:10itrix.....: Wate r
PARAMETER/TES T DESCRIPTIO N
Semivotatite Organics
Bis(2-chloroethyl)etherDi-n-butyl phthalateBis(2-ethylhexyl)phthalate
Oi-n-octyl phthalate
i
Lat
Oal
Tin
SAMPL E RESUL T
9
N ONO
N O
Q
J
U
U
U
FLAG S
wratory Sample ID: 200987-5
>e Received.......: 07/27/Z001
n e Received. ......: 10:15
: .. HD L -.
2
U
23
'•'; v . R L ;
10
1010
10
DILUTION
11
1
1
UM1T S
U9/L
U9/Lug/L
U9/L
BATC H
4289
4289
4289
4289
DT DATE/TIM E
08/K/01 QUO
08/14/01 0140
08/H/01 0140
08/U/01 0140
TEC H
shra
shra
shra
shra
In Description = Dry Ugt.Page 6
L A B O R A T O R Y T E S T R E S U L T S
Jo b Hunker: 20098 7 Oate:08/20/200 1
CUSTOMER : Blasland . Bouc k & Lee. Inc. PROJECT : BB L ATTN : Cath y Yewdal l
Custome rDate Sam)Tim e Sam]Sampl e M ;
TES T METHO D
SU846 8270C
Sampl e ID: NS-9 0>led......: 07/26/2001iled......: 00:00trix. .. . . : Wate r
PARAMETER/TES T DESCRIPTIO N
Semivolat i l e Organic sBis(2-chloroethyl)ethe rOi-n-buty l phthalat eBis(2-ethylhexyl)phthalat eDi-n-octy l phthalat e
i
La t
DaTi r
SAMPL E RESUL T
ND
MD
ND
N D
Q
U
UU
U
FLAG S
>
xarator y Sampl e ID: 200987-6e Received . ......: 07/27/200 1ne Received . ......: 10:15
MDL . i
24
2
3
R L
10
101010
DILUTIO N
1
1
1
1
UNIT S
ug/Lug/Lug/Lug/L
BATC H
42894289
42894289
D T DATE/TIM E
08/14/0 1 021808/14/0 1 021808/14/0 1 021808/14/0 1 0218
TEC H
shr ashrashrashra
* In Description = Dry Wgt.Page 7
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Date:08/13/200 1
CUSTOMER : Blasland , Bouc k & Lee, Inc. PROJECT : BB L ATTN : Cath y Yewdal l
Custome rDate Sam jTime Sam)Sampl e M i
TES T METHO D
SW846 8081 A
Dn\3:>D
Sampl e ID : EB - 072601)led......: 07/26/2001>led......: 08:15itrix.... .: Wate r
PARAMETER/TES T DESCRIPTIO N
Organochlorin e Pesticid e Analysi sdelta-BH C
i
La tDaTir
SAMPL E RESUL T
ND
0
U
FLAG S
\
wrator y Sampl e ID : 200987-1te Received . ......: 07/27/200 1ne Received.......: 10:15
"'. "; HOL
0.01 1
R L
0.048
DILUTIO N
1
UNIT S
ug/L
BATC H
419 8
OT DATE/TIM E
08/11/0 1 0200
TEC H
jan z
In Description = Dry Wgt.Pag e 2
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Date:OB/13/200 1
CUSTOMER : Blasland , Bouc k & Lee, Inc. PROJECT : BB L ATTM : Cath y Yewdal l
Custome r
Dat e Sam fTime Sam fSample H a
TES T METHO D
SU846 8081 A
Sampl e ID : NS-3 3tied......: 07/26/2001>led......: 10:2 0trix.. . . .: Wate r
PARAMETER/TES T DESCRIPTIO N
Organochlorin e Pesticid e Analysi sdelta-BH C
i
La t
Da lTin
SAMPL E RESUL T
ND
0
U
FLAG S
wrator y Sampl e ID : 200987-2e Received.......: 07/27/200 1
MD L .
0.01 1
R L
0.048
DILUTIO N
1
UNIT S
ug/L
BATC H
4198
DT DATE/TIM E
08/11/0 1 0229
TEC H
jan z
In Description = Dry Ugt.Page 3
05
0
0
1
3
L A B O R A T O R Y T E S T R E S U L T S
Job Number: 200987 Oate:08/13/2001
CUSTOMER : Blasland, Bouck & Lee, Inc. PROJECT : BBL ATTN : Cathy Yewdall
Customer
Date Samf
Time Sam f
Sample Me
TES T METHO D
SU8A 6 8081 A
Sample 10: NS-4 2>led. .....: 07/26/2001
>led. .....: 13:50
PARAMETER/TES T DESCRIPTIO N
Organochlorine Pesticide Analysis
delta-BHC
i
Lat
Oa t
Tin
SAMPL E RESULT .
N O
0
U
FLAG S
moratory Sample ID: 200987-3
>e Received. ......: 07/27/2001
ne Received. ......: 10:15
. • • ': HO L ;. ' • -•
0.011
RL ;
0.048
DILUTIO N
1
. UNIT S
ug/L
BATC H
4198
O T DATE/TIM E
08/11/01 0258
TEC H
jam
In Description = Dry Ugt.Pag e 4
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Date:08/13/200 1
CUSTOMER : 8 1 a s I and , Bouc k & Lee , Inc . PROJECT : BB L ATTN : Cath y Yeudal l
Custome rDate Sam f
Tim e Sam )Sampl e M j
TES T METHO D
SU84 6 808 1 A
Sampl e ID : NS-4 9>led......: 07/26/200 1>led . .....: 14:1 5itrix.....: Wate r
PARAMETER/TES T DESCRIPTIO N
Organochlorin e Pesticid e Analysi s
delta-BN C
i
La tDatTin
SAMPL E RESUL T
ND
Q
U
FLAG S
xirator y Sampl e ID : 200987-4e Received.......: 07/27/200 1ne Received.......: 10:1 5
• MD L
0.01 1
R L
0.048
DILUTIO N
1
UNIT S
ug/L
BATC H
419 8
DT DATE/TIM E
08/11/0 1 0328
TEC H
jam
i
* In Description = Dr y Ugt .Pag e 5
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Date : 08/13/200 1
CUSTOMER : Blesland , Bouc k & Lee, Inc. PROJECT : BB L : ATTN: Cath y Yewdal l
Custome rDate Sam p
Tim e Sam pSample H i
TES T METHO D
SUB4 6 808 1 A
Sampl e ID : NS-3 9>led......: 07/26/2001>led . .....: 17:10trix.....: Wate r
PARAMETER/TES T DESCRIPTIO N
Organochlorin e Pesticid e Analysi sdelta-BH C
i
La tOalTin
SAMPL E RESUL T
ND
0
U
FLAG S
>,
wrator y Sampl e ID : 200987-5e Received.......: 07/27/200 1
HDL ; . . ;
0.01 1
RL
0.048
DILUTIO N
1
UNIT S
ug/L
BATC H
419 8
DT DATE/TIM E
08/11/0 1 0457
TEC H
jan z
In Description = Dry Ugt.Page 6
L A B O R A T O R Y T E S T R E S U L T SJob Number : 200987 Date:08/13/200 1
CUSTOMER : Blusland , Bouc k & Lee. Inc. PROJECT : BB L :; • ATTN : Cath y Yewdal l
Custome rDate Sam pTime Sam p
Sampl e M a
TES T METHO D
SU84 6 8081 A
Sampl e ID : NS-9 0
iled......: 07/26/200 1>led . .....: 00:00trix.....: Wate r
PARAMETER/TES T DESCRIPTIO N
Organochtorin e Pesticid e Analysi s
delta-BH C
i
La tDatTin
SAMPL E RESUL T
ND
Q
U
FLAG S
watory Sampl e ID : 200987-6e Received.......: 07/27/200 1re Received.......: 10:15
.' HD L •... : .
0.01 1
. ••".. R L • :.
O.OA 8
DILUTIO N
1
UNIT S
ug/L
BATC H
4198
DT DATE/TIM E
08/11/0 1 0526
TEC H
jam
* In Description = Dry Ugt.Pag e 7
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Date:08/07/200 1
CUSTOMER : Bia s land , Bouc k & Lee , Inc . PROJECT : BB L ATTN : Cath y Yewdal l
Custome r Sampl e ID : EB-07260 1 Laborator y Sampl e ID : 200987-1Date Sampled......: 07/26/200 1 Dat e Received . ......: 07/27/200 1Time Sampled . .....: 08:1 5 Tim e Received . ......: 10:1 5
Sampl e Matrix . . . . . : Wate r
TES T METHO D
SW846 7470 A
SW84 6 60 1 OB
PARAMETER/TES T DESCRIPTIO N
Mercur y (Hg )
Metal s Analysi s OC R Trace )Antimon y (Sb )
Arseni c (As )Bariu m (Ba )
Bery l liu m (Be )Chromiu m (Cr )
Cobal t (Co )Coppe r (Cu)
Lea d (Pb)
Manganes e (Mn )Nicke l (Ni )
Seleniu m (Se )Thalliu m (Tl )
Vanadiu m (V)Zin c (Zn)
I
SAMPL E RESUL T
0.06 1
2.3
NO
ND
ND
ND
ND
NO 2.6
ND
ND
ND 3.9
ND
NO
Q
B
B
U
U
U
U
U
U
B
U
U
U
B
UU
FLAG S MDL
0.01 1
1.41.74.5
0.087
0.8 9
4.21.4
1.6
1.2
2.4
2.33.83.417.2
R L
0.2 0
6.010.0
2005.0
10.0
50.0
10.03.015.010.05.010.050.040.0
DILUTIO N
1
1
1
11
1
2
UNIT S
ug/L
ug/L
ug/Lug/Lug/L
ug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/L
BATC H
399 1
400440044004
4004
40044004
40044004
4004400440044004
4004
4034
OT DATE/TIM E
08/03/0 1 132 0
08/03/01 215 9
08/03/0 1 215 908/03/0 1 215 908/03/01 215 908/03/01 215 908/03/01 215 908/03/0 1 215 9
08/03/01 215 908/03/01 215 908/03/01 215 9
08/03/01 215 9
08/03/01 215 9
08/03/01 215 908/07/01 012 5
TEC H
bre e
Ifu l
Ifu lIfulIful
Ifu lIful
Ifu l
Ifu lIfulIfulIfulIfulIfulIful
In Description = Dry Ugt.Page 2
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Oate:08/07/200 1
CUSTOMER : 8 1 as 1 and , Bouc k & Lee , Inc . PROJECT : BB L ATTN : Cath y Yewdal l
Custome r San^l e ID : NS-3 3 Laborator y Sampl e ID : 200987-2Date Sampled......: 07/26/200 1 Dat e Received . ......: 07/27/200 1Time Sampled..... .: 10:2 0 Tim e Received . ......: 10:1 5
Sampl e Matrix . ....: Wate r
TES T METHO D
SW846 7470A
SW846 601 OB
•X*}^^)bD
PARAMETER/TES T DESCRIPTIO N
Mercur y (Hg )
Metal s Analysi s (IC P Trace }Antimon y (Sb )Arseni c (As )Bariu m (Ba )Bery l I iu m (Be )Chromiu m (Cr )
Cobal t (Co )Coppe r (Cu)Lea d (Pb )Manganes e (Mn )Nicke l (Ni )Seleniu m (Se )Thalliu m (Tl )Vanadiu m (V )Zin c (Zn )
i
SAMPL E RESUL T
0.08 1
ND
ND 23.5
ND
6.6
ND 1.7
ND 19.18.4
ND
ND
20.228.2
0
B
UU
B
U
B
U
BU
B
U
U
B
B
FLAG S MD L
0.01 1
1.41.7
4.5
0.087
0.8 9
4.21.41.61.2
2.42.33.8
3.417.2
R L
0.2 0
6.0
10.0200
5.010.050.0
10.03.015.010.05.010.0
50.040.0
DILUTIO N
1
11
1
1
1
1
111
1
11
1
2
UNIT S
ug/L
ug/Lug/Lug/L
ug/L
ug/Lug/L
ug/Lug/Lug/Lug/L
ug/L
ug/L
ug/Lug/L
BATC H
399 1
400440044004
4004
40044004400440044004400440044004
40044034
D T DATE/TIM E
OB/03/0 1 132 2
08/03/0 1 220 408/03/0 1 220 408/03/0 1 220 408/03/0 1 220 4
08/03/0 1 220 408/03/0 1 220 408/03/0 1 220 408/03/0 1 220 408/03/01 220408/03/0 1 220 4
08/03/0 1 220 408/03/0 1 220 4
08/03/0 1 220 408/07/0 1 013 1
TEC H
bre e
Ifu lIfulIfulIfulIfulIfulIfulIfulIfulIful
Ifu lIfulIfulIful
In Description = Dry Ugt .Page 3
L A B O R A T O R Y T E S T R E S „ iA S
Jo b Number : 200987 Oace:08/07/200 1
CUSTOMER : Blasland . Souc k & lee. Inc. PROJECT : BB L ATTN : Cath y Yeudal t
Custome r Sampl e ID : NS-4 2 Laborator y Sampl e ID : 200987-3Date Sampled......: 07/26/200 1 Dat e Received . ......: 07/27/200 1Time Sampled... ...: 13:50 Tim e Received . ......: 10:1 5
Sampl e Matrix.....: Wate r
TES T METHO D
SU846 7470A
SW846 601 OB
5PK
3••** —————————
PARAMETER/TES T DESCRIPTIO N
Mercur y (Hg)
Metal s Analysi s (IC P Trace )Antimon y (Sb)
Arseni c (As)Bariu m (Ba)Beryl ! iu m (Be)Chromiu m (Cr)Cobal t (Co)Coppe r (Cu)Lea d (Pb)Manganes e (Mn )Nicke l (Hi)Seleniu m (Se)Thalliu m (Tl )Vanadiu m (V )Zin c (Zn)
i
SAMPL E RESUL T
0.06 1
2.3
NO 94.2
N D 3.022.6
3.1
ND
8700
19.7ND
4.6
NO
ND
0
B
B
UB
U
B
B
B
U
U
B
U
U
FLAG S
'*\
HD L
0.01 1
1.4
1.7
4.50.087
0.894.21.4
1.61.22.4
2.33.83.417.2
R L
0.2 0
6.010.02005.0
10.050.010.0
3.015.010.0
5.0
10.050.0
40.0
DILUTIO N
1
1111
1
111111
1
1
2
UNIT S
ug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
BATC H
3991
4004
40044004
40044004
4004
40044004
4004
40044004400440044034
DT DATE/TIM E
08/03/01 1324
08/03/0 1 221008/03/0 1 221 008/03/0 1 221 008/03/0 1 221008/03/01 221008/03/0 1 22T O08/03/0 1 221008/03/0 1 221 008/03/0 1 221 008/03/0 1 221008/03/0 1 2210
08/03/0 1 221008/03/0 1 221008/07/0 1 0139
TECI f
bre e
Ifu lIfulIfulIfulIfulIfulIfulIfulIfulIfulIfulIfulIfulIful
In Description = Dry Wgt.Page 4
cfvc
s_cIT
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Date:08/07/200 1
CUSTOMER : BlasUnd , Bouc k & Lee, Inc. PROJECT : BB L ATTN : Cath y Yeudal l
Custome r Sampl e ID : NS-4 9 Laborator y Sampl e ID : 200987-4Date Sampled......: 07/26/200 1 Dat e Received . ......: 07/27/200 1Time Sampled......: 14:15 Tim e Received . ......: 10:15
Sampl e Matrix.. ...: Wate r
TES T METHO D
SW84 A 7470 A
SU846 60108
PARAMETER/TES T DESCRIPTIO N
Mercur y (Hg )
Metal s Analysi s (ICP Trace )Antimon y (Sb)Arseni c (As)
Bariu m (Ba)Berylliu m (Be)Chromiu m (Cr )Cobal t (Co )
Coppe r (Cu)Lea d (Pb)Manganes e (Mn)Nicke l (Ni )
Seleniu m (Se)Thalliu m (T OVanadium (V)Zin c (Zn)
i
SAMPL E RESUL T
1.1
ND
ND 52.3
ND
1.3
20.3
ND
ND 64805.7
NO
ND
ND
68.8
0
U
U
B
U
B
B
U
U
B
U
U
U
FLAG S
\
HOL
0.01 1
1.4
1.7 .
4.5
0.087
0.89
4.2
1.41.61.22.42.33.8
3.417.2
R L
0.20
6.010.02005.010.050.010.03.015.010.0
5.0
10.050.040.0
DILUTIO N
1
1
12
UNIT S
ug/L
ug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
BATC H
3991
400440044004400440044004
400440044004400440044004
40044034
DT DATE/TIM E
08/03/0 1 1326
08/03/0 1 221608/03/0 1 2216
08/03/0 1 2216
08/03/0 1 2216
08/03/0 1 2216
08/03/0 1 221608/03/0 1 221608/03/0 1 2216
08/03/01 221608/03/0 1 221608/03/0 1 221608/03/0 1 2216
08/03/0 1 221608/07/0 1 014 5
TEC H
bre e
Ifu lIfutIful
Ifu l
Ifu lIfulIfutIfulIfultfulIfulIful
Ifu lIful
——————
In Description = Dry Wgt.Page 5
L A B O R A T O R T T E S T R E S U L T SJob Number : 200987 Date:08/07/200 1
CUSTOMER : Bia s I and. Bouc k & Lee. Inc. PROJECT : BB L ATTN : Catti y Yewdal l
Custome r Sampl e 10 : NS-3 9 Laborator y Sampl e ID : 200987-5Date Sampled......: 07/26/200 1 Dat e Received . ......: 07/27/200 1Time Sampled......: 17:10 Tim e Received . ......: 10:15
TES T METHO D
SUB46 7470A
SU846 601 OB
PARAMETER/TES T DESCRIPTIO N
Mercur y (Hg)
Hetal s Analysi s (ICP Trace )Antimon y (Sb)Arseni c (As)Bariu m (Ba)
Berylliu m (Be)Chromiu m (Cr)Cobal t (Co)Coppe r (Cu)Lea d (Pb)Manganes e (Mn)
Nicke l (Ni)Seleniu m (Se)
Thalliu m (Tl)Vanadiu m (V )Zin c (Zn)
i
SAMPL E RESUL T
0.044
' 2.7
NO
39.9
ND
5.7ND
ND
ND
1222.9
ND
NO 19.545.5
0
B
B
U
B
U
B
U
U
U
B
U
U
B
FLAG S
\(
MO L
0.01 1
1.41.74.50.087
0.894.2
1.4
1.61.22.4
2.33.8
3.4
17.2
R L
0.2 0
6.010.02005.0
10.050.010.0
3.015.0
10.05.010.050.0
40.0
DILUTIO N
1
1
1
11
1
1
12
UNIT S
ug/L
ug/L
ug/L
ug/Lug/LU9/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
BATC H
399 1
400 44004
40044004400440044004400440044004
4004
4004
40044034
DT DATE/TIM E
08/03/0 1 1339
08/03/0 1 225608/03/0 1 2256
08/03/0 1 225 608/03/01 225608/03/0 1 225608/03/0 1 225608/03/0 1 225 608/03/01 225608/03/0 1 225 608/03/01 225608/03/01 225608/03/0 1 225 6
08/03/0 1 225608/07/01 022 5
TEC H
bre e
Ifu lIfulIfulIfutIfultfulIfulIfulIfulIfulIfultfultfulIfut
In Description =
ccc
s_ca
L A B O R A T O R Y T E S T R E S U L T S
Jo b Number : 200987 Oate:08/07/200 1
CUSTOMER : Blasland , Bouc k & Lee , Inc . PROJECT : BB L . AIIN : Cath y Yewdat t
Custome r Sampl e 10 : NS-9 0 Laborator y Sampl e 10 : 200987-6
Dat e Sampled......: 07/26/200 1 Dat e Received . ......: 07/27/200 1
Tim e Sampled......: 00:00 Tim e Received . ......: 10:1 5
Sampl e Matrix.....: Wate r
TES T METHO D
SW846 7470A
SW846 60108
PARAMETER/TES T DESCRIPTIO N
Mercur y (Hg )
Metal s Analysi s (IC P Trace )Antimon y (Sb )
Arseni c (As )Bariu m (Ba )Berylliu m (Be )Chromiu m (Cr )Cobal t (Co )Coppe r (Cu )
Lea d (Pb )Manganes e (Mn )Nicke l (Ni )Seleniu m (Se )
Thalliu m (Tl )
Vanadiu m (V)Zin c (Zn )
i
SAMPL E RESUL T
0.05 2
NO
NO
96.4
H O 5.023.23.4
HD
890022.7
ND 6.2
NO
101
Q
B
U
U
B
U
B
B
BU
U
B
U
FLAG S
•-,
MDL
0.01 1
1.41.7
4.5
0.0870.894.21.4
1.61.22.4
2.3
3.83.417.2
R L
0.2 0
6.010.02005.0
10.050.0
10.03.015.010.05.010.0
50.040.0
DILUTIO N
1
1
12
UNIT S
ug/L
ug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
BATC H
399 1
400440044004
4004
40044004
4004400440044004
4004
4004
40044034
OT DATE/TIM E
08/03/01 134 1
08/03/0 1 230 108/03/0 1 230 108/03/01 230 108/03/0 1 230 108/03/0 1 230 108/03/0 1 230 108/03/0 1 230 108/03/0 1 230 108/03/0 1 230 108/03/0 1 230 1
08/03/0 1 230 108/03/01 230 1
08/03/0 1 230 108/07/0 1 023 0
TEC H
bre e
Ifu l
Ifu lIfulIfulIfulIfultfulIfulIfulIful
Ifu l
Ifu lIfulIful
In Description = Dry Ugt .Page 7
I
I
I
I
III
I
I
I
II
III
I
I
I
BLASLAN D BOUC K & LE E
Lab Name:Severn Trent Laboratories, Inc. SDG Number:
Matrix: (soil/water) WATE R Lab Sample ID:C2B08025 9 001
Method: SW846 8260B
Volatile Organics, GC/MS (8260B)
Sampl e WT/Vol: 5 / mL
Work Order: ETV8A1AA
Dilutio n factor : 1
Clien t Sampl e Id: NS-3 3
CAS NO. COMPOUND
Date Received : 02/08/0 2
Cats Extracted:02/08/02
Dat e Analyzed : 02/08/02
QC Batch: 2039128
CONCENTRATION UNITS:
(ug/L or uq/kg) ug/L
67-64--1
75-27-4
78-93-3
75-15-0
124-48-1
75-00-3
67-66-3
107-06-2
75-3S-4
156-59-2
156-60-5
540-59-0
78-87-5
100-41-4
75-09-2
127-18-4
108-88-3
79-00-5
| 79-01-6
75-01-4
I 1330-20-7
Acetone
Bromodichloromethane
2-Butanone
Carbon disulfid e
Dibromochloromethan e
ChloroethaneChloroform
1, 2-Dichloroethane
1, 1-Dichloroethen e
cis-l, 2 -Dichloroethene
trans-1 , 2 -Dichloroethen e1,2 -Dichloroethen e (total )
1 , 2-Dichloropropane
Ethylbenzene
Methylen e chlorid e
Tetrachloroethene
Toluene
1,1,2 -Trichloroethane
Trichloroethene
viny l chlorid e
Xylene s (total)
10
1.0
5.0
1.0
1.0
2.0
1.0
1.0
1.0i.o-.-;
1.0
1.0U.o
11 . 0
12.0U.o
1.0U.o
1.0
(2.0
3.0
U lul
U|u |u |
U|u l
Ulululululululululululululul
FORM I
II
II
IIII
I
I
I
III
BLASLAND BOUCK & LEE
Lab Name-.Severn Trent Laboratories, Inc. SDG Number:
Matrix: (soil/water) WATE R Lab Sample ID:C2B08025 9 002
Method: SW84 6 8260B
Volatile Organics, GC/M S (B260B )
Sample WT/Vol : 5 / mL
Work Order: ETV8E1A A
Dilution factor: 10
Client Sample Id: NS-4 2
CAS NO. COMPOUN D
Date Received: 02/08/02
Date Extracted:02/11/02Date Analyzed: 02/11/02
QC Batch: 2042281
CONCENTRATIO N UNITS:
(ug/L or uq/kq) ug/L
67-64-1
75-27-4
78-93-3
75-15-0
124-48-1
75-00-3
67-66-3
107-06-2
75-35-4
156-59-2
156-60-5
540-59-0
78-87-5
100-41-4
75-09-2
127-18-4
108-88-3
79-00-5
79-01-6
75-01-4
1330-20-7
Aceton e
Bromodichloromethan e
2 -Butanon e
Carbon disulfid e
Dibromochloromethane
Ctxloroethan e
Chlorofor m
1 , 2 -Dichloroethane
1 , 1 -Dichloroethen e
cis -1 , 2 -Dichloroethene
trans - 1 , 2 -Dichloroethene
1 , 2 -Dichloroethene (tota l )
1 , 2-Dichloropropan e
Ethylbenzene
Methylen e chloride
Tetrachloroethene
Toluene
1,1 , 2-Trichloroethane
Trichloroethene
Vinyl chlorideXylenes (total )
lio o
11 0
IS O
11 0
11 0
117
110
131 0lio ..
122
11 0
123
110
110
120
|10
|5.0
110
|8.9
|45
13 0
u |a |u lolulJ 1ul1ul1ul1ulu|u lulJ 1ulJ 11ul
FOR M I
IIIIIIIIIIII
BLASLAND BOUCK 4 LEE
Lab Name:Severn Trent Laboratories , Inc. SD G Number:
Matrix : (soil/water) WATER La b Sample ID:C2B080259 003
Method: SW846 8260B
Volatile Organics, GC/MS (8260B)
Sample WT/Vol: 5 / mL
Work Order: ETV8G1AA
Dilutio n factor : 25 0
Clien t Sample Id: NS-49
CAS NO. COMPOUND
Dat e Received : 02/08/02
Date Extracted:02/11/02
Date Analyzed: 02/11/02
QC Batch: 2042281
CONCENTRATION UNITS :
(uq/L or ug/kq) ug/L
67-64-1
75-27-4
78-93-3
75-15-0
124-48-1
75-00-3
67-66-3
107-06-2
75-35-4
156-59-2
156-60-5
540-59-0
78-87-5
100-41-4
75-09-2
127-18-4
108-88-3
79-00-5
79-01-6
75-01-4
1330-20-7
Aceton e
B romodi chl orome t hane
2-Butanon e
Carbon disulfid e
Dibromochloromethan e
Chloroethane
Chlorofor m
1 , 2-Dichloroethane
1 , 1-Dichloroethen e
cis-1 , 2-Dichloroethen e
trans-l,2-Dichloroethene
1, 2-Dichloroethen e (total )
1 , 2 -Dichloropropan e
Ethylbenzene
Methylen e chlorid e
Tetrachloroethen e
Toluene
1,1,2 -Trichloroethane
Trichloroethen e
Vinyl chlorid e
Xylenes (total )
1250 0
125 0
1120 0
(25 0
125 0
150 0
|25 0
|5700
|25 0
(25 0 .:•"•'
|250
|25 0
125 0
(25 0Iso o
125 0
125 0
|25 0
|25 0Iso o
175 0
u l
U|
H I
U|
U|u |u l
1ulululululululu|u lulu|
Ul
Ul
FORM I
I
I
I
I
III
I
I
I
I
II
I
II
I
I
I
BLASLAND BOUC K & LEE
Lab Name:Severn Trent Laboratories, Inc. SDG Number:
Matrix: (soil/water) WATE R Lab Sample ID:C2B080259 003
Method: SW846 8260B
Volatile Organics, GC/M S (8260B )
Sample WT/Vol: 5 / mL
Work Order; ETVSG2A A
Dilution factor: 1
Client Sample Id: NS-49 -RE 1
CA S NO .COMPOUN D
Date Received: 02/08/02
Date Extracted:02/08/02
Date Analyzed: 02/08/02
QC Batch: 2039128
CONCENTRATION UNITS:
(ug/L or uq/kg) uq/L
6-7-64-1
75-27-4
78-93-3
75-15-0
124-48-1
75-00-3
67-66-3
107-06-2
75-35-4
156-59-2
156-60-5
540-59-0
78-87-5
100-41-4
75-09-2
127-18-4
108-88-3
79-00-5
79-01-6
75-01-4
1330-20-7
Acetone
Bromodichlorom e thane
2-Butanon e
Carbon disulfid e
Dibromochlorom e than e
Chloroe thane
Chloroform
1. 2-Dichloroethane
1, 1-Dichloroethene
cis - 1 , 2 -Dichloroethene
trans -1,2 -Dichloroethen e .
1 , 2 -Dichloroethene (total)
1 , 2 -Dichloropropane
Ethylbenzen e
Methylene chloride
Tetrachloroethene
Toluene
1,1,2 -Trichloroe thane
Trichloroetliene
Vinyl chloride
Xylenes (total)
li o
11 . 0Is.o
|1. 0li.o
15.9
11.9
|2900
|1.4 ,
|0.6 9
|1. 0
|0.7 1
12.4li.o
|4.8
13.0
IS.!
13.9
15.0
118
11.2
u luluuul
E
1
J u lJ
u
J
FOR M I
IIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Lab Name:Severn Trent Laboratories, Inc. SDG Number :
Lab Sample ID:C2B080259 004Matrix: (soil/water ) WATE R
Method: SW846 8260B
Volatil e Organics , GC/M S (8260B )
Sampl e WT/Vol: 5 / m L
Work Order: ETV8H1AA
Dilution factor: 1
Clien t Sample Id: NS-39
Date Received : 02/08/02
Dat e Extracted:02/08/0 2
Dat e Analyzed: 02/08/02
QC Batch: 2039128
CAS NO.COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/kq) ug/L
67-64-1
75-27-4
78-93-3
75-15-0
124-48--1
7S-00-3
67-66-3
107-06-2
75-35-4
156-59-2
156-60-5
540-59-0
78-87-5
100-41-4
75-09-2
127-18-4
108-88-3
79-00-5
79-01-6
75-01-4
1330-20-7
Acetone
Bromodichlorotnethane
2-Butanone
Carbon disulfide
Dibromochloromethane
Cliloroe thane
Chloroform
1 . 2 -Dichloroethane1 . 1-Dichloroethene
cis-1 , 2-Dichloroethene
trans-1, 2-Dichloroethene
1 , 2 -Dichloroethene ( total )
1 , 2-Dichloropropane
Ethylbenzene
Methylene chloride
Tetrachloroethene
Toluene
1,1,2 -Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes (total)
110
ll.Ois.o
l l .O
ll.O
|0.92
10.64
141
ll.lli.o,-:|i.o -
ll.O
11.7
ll.O
113
|1.5
ll.O
11.8
11-4
19.5
)3.0
u lo|,u |u lulJJ
B
u lulul
u l
u
u
FORM I
IIIIIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Lab Name:Sever n Tren t Laboratories , Inc. SD G Number :
Lab Sample ID:C2B080259 004Matrix: (soil/water) WATER
Method: SW846 8260B
Volatile Organics, GC/MS (8260B)
Sampl e WT/Vol: 5 / mL
Work Order: ETV8H2AA
Dilutio n factor : 2
Client Sample Id: NS-39 -RE 1
Date Received : 02/08/02
Dat e Extracted:02/11/0 2
Dat e Analyzed: 02/11/02
QC Batch: 2042281
CAS NO.COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/L
67-64-1
75-27-4
78-93-3
75-15-0
124-48-1
75-00-3
67-66-3
107-06-2
75-35-4
156-59-2
156-60-5
540-59-0
78-87-5
100-41-4
75-09-2
127-18-4
108-88-3
79-00-5
79-01-6
75-01-4
1330-20-7
Aceton e
Bromodichloromethan e
2-Butanone
Carbo n disulfid e
Dibromochloromethane
Chloroethane
Chloroform
1 , 2-Dichloroethane
1, l-Dichloroethen e
cis - 1 , 2 -Dichloroethen e
tran s - 1 , 2 -Dichloroethen e
1,2 -Dichloroethen e (total )
1 , 2-Dichloropropane
Ethylbenzene
Methylene chloride
Tetrachloroethene
Toluene
1,1,2 -Trichloroethane
Trichloroethene
Vinyl chloride
Xylene s (total )
|20
|2.0Ho
|2.0
12.0
|4.0
|0.53
142
|2.0 .-
|2.0--.
12.0
12.0
11.5
|2.0
111
ll.O
|2.0
11.6
ll.l
17.2
16.0
1!111IU11111U11UIUU11
u |u |u |u |u |u |11o|u |o |u |1u|
u
u|
FORM I
IIIIIIIIIIIIIIIII
BLASLAND BOUCK 4 LEE
La b Name:Sever n Tren t Laboratories , Inc .
Matrix : (soil/water ) WATER
Method : SW846 8260B
Volatile Organics, GC/MS (8260B)
Sample WT/Vol: 5 / mL
Work Order: ETV8J1AA
Dilution factor: 10
Clien t Sampl e Id : DUP-9 0
SD G Number:
Lab Sample ID-.C2B08025 9 005
Date Received: 02/08/02Date Extracted:02/11/02
Date Analyzed.- 02/11/02
QC Batch: 2042281
CAS NO.COMPOUN D
CONCENTRATIO N UNITS:
(ug/L or uq/kg) ug/L
67-64-1
75-27-4
78-93-3
75-15-0
124-48-1
75-00-3
67-66-3
107-06-2
75-35-4
156-59-2
156-60-5
540-59-0
78-87-5
100-41-4
75-09-2
127-18-4
108-88-3
79-00-5
79-01-6
75-01-4
1330-20-7
Aceton e
Bromodichloromethan e
2-Butanon e
Carbon disulfid e
Dibromochloromethane
Chloroethane
Chloroform
1, 2-Dichloroettiane
1, 1-Dichloroethen e
cis-1 , 2 -Dicnloroethene
trans-1 , 2 -Dichloroethene
1 , 2 -Dichloroethene (total )
1 , 2 -Dichloropropan e
Ethylbenzene
Methylen e chlorid e
Tetrachloroethene
Toluene
1,1,2 - Trichloroethan e
Trichloroethene
Vinyl chlorideXylenes (total )
|10 0
11 0
|50
1 1 0
110
119
110
|34 0Ho ,-::
125
1 1 0
125
110
|10
120
110
IS.2
110lio
|51
111
u |u |
UlululJ 1ul1ul1ul1ululululJ 1ul11J 1
FOR M I
IIIIIIIIIIIIIIIIIII
BIASLAND BOUCK & LEE
Lab Name:Sever n Trent Laboratories , Inc. SD G Number :
Matrix : (soil/water) WATER La b Sampl e ID:C2B080259 006
Method: SW846 8260B
Volatile Organics, GC/MS (8260B)
Sampl e WT/Vol: 5 / mL
Work Order: 2TV3KIAA
Dilutio n factor : 1
Clien t Sample Id: EB-02070 2
CAS NO.COMPOUND
Date Received : 02/08/02
Date Extracted.-02/03/0 2
Date Analyzed: 02/08/02
QC Batch: 2039128
CONCENTRATION UNITS :
(ug/L or uq/kg) uq/L
67-64-1
75-27-4
78-93-3
75-15-0
124-48-1
75-00-3
67-66-3
107-06-2
75-35-4
1S6-59-2
156-60-5
540-59-0
78-87-5
100-41-4
75-09-2
127-18-4
108-88-3
79-00-5
79-01-6
75-01-4
| 1330-20-7
Aceton e
Bromodichloromethan e
2-Butanon e
Carbon disulfid e
Dibromochloromethan e
Chloroethan e
Chlorofor m
1 , 2 -Dichloroethan e
1, l-Dichloroethen e
cis-1 ; 2-Dichloroethen e
trans-1 , 2-Dichloroethen e
1 , 2 -Dichloroethene (total )
1 , 2 -Dichloropropane
Ethylbenzen e
Methylene chloride
Tetrachloroethen e
Toluene
1,1,2 -Trichloroethane
Trichloroethen e
Vinyl chloride
Xylenes (total )
11 0
ll.O
15.0
ll.O
ll.O
12.0
ll.O
ll.O
ll.O ,
ll.O Vli.-o
ll.O
ll.O
ll.O
|2.0
ll.O
ll.O
ll.O
l l -O
12.0
13.0
u lulolul
U lulululululululu|u lululu|u lululul
FORM I
IIIIIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Lab Name:Sever n Trent Laboratories , Inc . SD G Number:
Matrix: (soil/water) WATER Lab Sample ID.-C2B080259 007
Method: SW846 8260B
Volatil e Organics , GC/MS (8260B)
Sampl e WT/Vol: 5 / mL
Work Order: ETV8L1AA
Dilutio n factor : 1
Client Sampl e Id: TB-020702
Date Received : 02/08/02
Date Extracted:02/08/02
Dat e Analyzed : 02/08/02
QC Batch: 2039128
CAS NO.COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/L _Q
67-64-1
75-27-4
78-93-3
75-15-0
124-48-1
75-00-3
67-66-3
107-06-2
75-35-4
156-59-2
156-60-5
540-59-0
78-87-5
100-41-4
75-09-2
127-18-4
108-88-3
79-00-5
79-01-6
75-01-4
1330-20-7
Aceton e
Bromodichlorom e thane
2-Butanone
Carbon disulfid e
Dibromochlorotnethan e
Chloroethan e
Chloroform
1 , 2 -Dichloroethan e
1 , 1 -Dichloroethen e
cis-1 , 2-Dichloroethen e
trans-1 , 2-Dichloroethen e
1, 2-Dichloroethen e (total )
1, 2-Dichloropropan e
Ethylbenzene
Methylene chloride
Tetrachloroethen e
Toluene
1,1,2 -Trichloroethane
Trichloroethen e
Viny l chlorid e
Xylenes (total )
11 0
11 . 0
15.0
|1. 0
11 . 0
12.0
11 . 0
11 . 0
|1.0U. .ti -ll . oli.oU. oli. o
12.0
|1.0
11 . 0
11 . 0
11 . 0
12.0
13.0
u lir lululululululululu|u lulululu|u lululul
u|
FORM I
IIIIIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Lab Name:Severn Trent Laboratories, Inc. SDG Number:
Matrix : (soil/water ) WATE R La b Sampl e ID:C2B080259 001
Method: SW846 8270C
Base/Neutral s and Acid s (8270C )
Sample WT/Vol: 1000 / mL
Work Order: ETV8A1AC
Dilution factor: 1
Moisture %:NA
Clien t Sample Id : NS-3 3
CAS NO. COMPOUND
Date Received : 02/08/02
Dat e Extracted:02/11/02
Date Analyzed: 02/12/02
QC Batch : 2042266
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/L
111-44-4 bis(2-Chloroethyl ) ethe r
| 117-81-7
I 84-74-2
I 117-84-0
bis(2-Ethylhexyl) phthalate |10
Di-n-butyl phthalate
Di-n-octyl phthalate
.110.
10
FOR M I
.21JZl
JZlu
2013
IIIIIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
.La b Name:Severn Trent Laboratories, Inc. SDG Number:
Matrix.- (soil/water ) WATER La b Sample ID:C2B080259 002
Method: SW846 8270C
Base/Neutral s and Acid s (8270C )
Sample WT/Vol: 1000 / mL
Work Order: ETV8E1AC
Dilutio n factor : l
Moistur e %:N A
Clien t Sample Id-. NS-4 2
CAS NO. COMPOUND
| 111-44-4
Dat e Received : 02/08/0 2
Dat e Extracted:02/11/02
Dat e Analyzed: 02/12/02
QC Batch: 2042266
CONCENTRATION UNITS:
(ug/L o r ug/kg ) ug/L
bis(2-Chloroethyl) ether
| 117-81-7 bis(2-Bthylhexyl ) phthalat e |1 0 .li
84-74-2 Di-n-buty l phthalat e
117-84-0 Pi-n-octyl phthalate
u
.H I
FOR M I
2O1 8
IIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Lab Name:Severn Trent Laboratories, Irx c . SD G Number:
Matrix : (soil/water) WATER La b Sample ID:C2B080259 003
Method: SW846 8270C
Base/Neutral s and Acid s (8270C )
Sample WT/Vol: 1000 / mL
work Order : ETV8G1A E
Dilutio n factor: 1
Moistur e %:NA
Client Sample Id: NS-49
CAS NO. COMPOUND
Date Received: 02/08/02
Date Extracted:02/11/02
Dat e Analyzed : 02/12/0 2
QC Batch: 2042266
CONCENTRATION UNITS:
(ug/L or ug/kq) ug/L
| 111-44-4
| 117-81-7
bis<2-Chloroethyl) ether |l4
bis(2-Ethylhexyl) phthalat e |10
j 84-74-2 Di-n-buty l phthalate .112 .I 117-84-0 Di-n-octy l phthalat e 10
JZ I
JZ IJZl
FOR M I
2O24
IIIIIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
Lab Name:Sever n Trent Laboratories, Inc . SDG Number :
Matrix: (soil/water) WATER Lab Sample ID:C2B080259 004
Method: SW846 827OC
Base/Neutrals and Acids (8270C)
Sampl e WT/Vol: 100 0 / mL Dat e Received : 02/08/02
Work Order: ETV8H1AC Dat e Extracted.-02/11/0 2
Dilution factor : 1 Dat e Analyzed: 02/12/02
Moistur e %:N A
QC Batch: 2042266
Clien t Sampl e Id: NS-3 9
CONCENTRATION UNITS:
CAS NO.________COMPOUND_____(uq/L or uq/kg) ug/L
I 111-44-4______bis(2-Chloroethyl) ether
I 117-81-7______bis(2-Ethylhexyl) phthalate 110_________|______U|
I 84-74-2_______Di-n-butyl phthalate_______|10_________j______UJ
I 117-84-0______Di-n-octyl phthalate_______JJLO________j______U|
FOR M I
2O29
IIIIIIIIIIIIIIIIIII
BLASLAND BOUCK & LEE
La b Name:Sever n Tren t Laboratories , Inc. SD G Number :
Matrix : (soil/water) WATER La b Sample ID:C2B080259 005
Method: SW846 8270C
Base/Neutrals and Acids (8270C)
Sample WT/Vol: 900 / mL
Work Order: ETV8J1AC
Dilutio n factor : 1.11
Moistur e %:NA
Client Sample Id: DUP-9 0
CAS NO. COMPOUND
| 111-44-4
I 117-81-7
I. 84^74-2
| 117-84-0
Dat e Received : 02/08/02
Dat e Extracted:02/11/0 2
Date Analyzed: 02/12/02
QC Batch: 2042266
CONCENTRATION UNITS:
(ug/L or ug/kq) ug/L
bis(2-Chloroethyl) ether |l.9
bis(2-Ethylhexyl ) phthalat e |11
Di-n-buty l phthalat e 11
Di-n-octyl phthalate 11
u
."I
FOR M I
2034
IIIIIIIIIIIIIIIIIII
B LAS LAND BOUCK & LEE
Lab Name:Sever n Trent Laboratories , Inc. SDG Number :
La b Sample ID:C2B08025 9 006Matrix: (soil/water) WATER
Method : SW846 8270C
Base/Neutrals and Acids (8270C)
Sample WT/Vol: 1000 / mL
Work Order: ETV8K1AC
Dilutio n factor : 1
Moisture %:NA
Client Sample Id: EB-02070 2
Dat e Received : 02/08/02
Dat e Extracted:02/11/02
Dat e Analyzed: 02/12/02
QC Batch: 2042266
CAS NO.COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/L
111-44-4 bis(2-Chloroethyl ) ethe r 10 JZl
117-81-7 bis(2-Ethylhexyl ) phthalat e |10 .21
I 84-74-2 Pi-n-butyl phthalate 10 J2I117-84-0 Di-n-octyl phthalate 10
FOR M I
2O39
III STL-Pittsburg h
Metal s Dat a Reportin g For m
Sample Result s
I Lab Sa mplcID : ETV8 K Client ID: EB-02070 2
Matrix : Wate r Units: ug/L Prep Date: 2/12/0 2 Prep Batch: 2043299
1 Weight
1
1
1
1
1
1
: NA
Elemen t
Antimon y
Arseni c
Bariu m
Berylliu m
Chromiu m
Cobal t
Coppe r
Lea d
Manganese
Nicke l
Seleniu m
Thallium
Vanadiu m
Zin c
Volume: 50 Percen t Moisture: NA
WL/Mass
206.84
189.04
493.41
313.04
267.72
228.62
324.7 5
220.35
257.61
231.6 0
220.35
190.86
292.40
206.2
MDL
4.1
2.2
0.14
0.40
1.1
0.84
2.5
1.8
0.47
2.4
3.2
5.7
1.5
3.7
Repor t
Limit
10.0
10.0
200
5.0
5.0
50.0
25.0
3.0
15.0
40.0
5.0
10.0
50.0
20.0
i Cone
4.6
2.2
0.14
0.97
1.1
0.8 4
2.5
1.8
3.2
2.4
3.2
5.7
1.5
3.7
o
B
Uu
B
U
Uuu
B
Uuu .uu
DF
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Instr
ICPST
ICPS T
ICPS T
ICPST
ICPS T
ICPS T
ICPS T
ICPST
ICPST
ICPST
ICPS T
ICPS T
ICPS T
ICPS T
Ana lDate
2/18/02
2/18/02
2/18/0 2
2/18/02
2/18/02
2/18/02
2/18/02
2/18/02
2/18/0 2
2/18/0 2
2/18/02
2/18/0 2
2/18/02
2/18/0 2
Ana lTime
17:40
17:40
17:4 O
17:40
17:40
17:40
17-.4O
17:40
17:40
17:40
17:40
17:40
17:40
17:40
Comments : Lot #: C2B08Q25 9 Sampl e #: 6
Versio n 4.97.1
1-1.; 1-4. ,-.Vvi1
U Resul t is les s lha n th e MD L
B Resul t is betwee n MD L an d RL
Form I Equivalent
3015
1
STL-Pittsburgh
• Metal s Dat a Reportin g For m
Sample Results
1 Lab Sampl e ID: ETV8 J Clien t ID: DUP-9 0
Matrix : Wate r Units: ug/L Prep Date: 2/12/0 2 Prep Batch: 2043299
• Weight : NA Volume : 50 Percen t Moisture : NA
1
1
1
1
1
1
Elemen t
Antimon y
Arseni c
Barium
Berylliu m
Chromiu m
Cobalt
Copper
Lead
Manganes e
Nicke l
Seleniu m
Thalliu m
Vanadiu m
Zinc
WL/
Mas s
206.84
189.04
493.41
313.04
267.72
228.62
324.75
220.35
257.61
231.60
220.35
190.8 6
292.40
206.2
MDL
4.1
2.2
0.14
0.40
1.1
0.84
2.S
1.8
0.94
2.4
3.2
5.7
1.5
3.7
Repor t
Limi t
10.0
10.0
200
5.0
5.0
50.0
25.0
3.0
30.0
40.0
5.0
10.0
50.0
20.0
Cone
4.1
2.2
107
0.58
4.8
24.4
5.6
2.5
13000
16.5
4.0
5.7
5.4
5.5
Q
U
U
B
B
B
B
B
B
B
B
U
B
B
DF
1
1
1
1
1
1
1
1
2
1
1
1
1
1
Inst r
ICPS T
ICPS T
ICPST
ICPS TICPS T
ICPS T
ICPST
ICPST
ICPST
ICPST
ICPST
ICPS T
ICPST
ICPST
AnalDate
2/18/0 2
2/18/0 2
2/18/02
2/18/02
2/18/02
2/18/02
2/18/02
2/18/02
2/19/02
2/18/02
2/18/02
2/18/0 2
2/18/02
2/18/0 2
Ana l
Tim e
17:33
17:3 3
17:33
17:33
17:33
17:33
17:33
17:33
18:16
17:33
17:33
17:33
17:33
17:33
Comments: Lot #: C2B0802S 9 Sampl e #: 5
Version 4.97.1 U Resul t is les s tha n th e MD L
B Resul t it betwee n MD L an d RL
Form I Equivalent
3O14
II
I STL-Pittsburg h
Metal s Dat a Reportin g For m
1 Lab Sampl e ID: ETV8 H Clien t ID: NS-3 9
Matrix : Wate r Units : ug/L Prep Date: 2/12/02 Prep Batch: 20432991. , ...
Weight: N A Volume : 50 Percen t Moisture: N A
1
1
1
1
1
1
Elemen t
Antimon y
Arsenic
Bariu m
Berylliu m
Chromiu m
Cobal t
Coppe r
Lead
Manganes e
Nicke l
Seleniu m
Thalliu m
Vanadiu m
Zin c
WL/
Mass
206.84
189.04
493.41
313.04
267.72
228.62
324.75
220.35
257.61
231.60
220.35
190.86
292.40
206.2
MDL
4.1
2.2
0.1 4
0.4 0
1.1
0.8 4
2.5
1.8
0.4 7
2.4
3.2
5.7
1.5
3.7
Report
Limit
10.0
10.0
200
5.0
5.0
50.0
25.0
3.0
15.0
40.0
5.0
10.0
50.0
20.0
Cone
5.1
2.2
44.1
0.7 2
4.4
0.8 4
2.5
1.8
211
2.4
3.2
5.7
20.5
8.4
o
B
U
B
B
B
U
U
U
U
Uu.---
B
B
DF
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Instr
ICPST
ICPS T
ICPST
ICPSTrcpsT
ICPS T
ICPS T
ICPS T
ICPST
ICPS T
ICPS T
ICPS T
ICPST
ICPST
Ana l
Date
2/18/02
2/18/0 2
2/18/02
2/18/0 2
2/18/02
2/18/0 2
2/18/0 2
2/18/0 2
2/18/02
2/18/0 2
2/18/02
2/18/02
2/18/02
2/18/0 2
Anal
Time
17:2 7
17:2 7
17:2 7
17:2 7
17:2 7
17:2 7
17:2 7
17:2 7
17:2 7
17:2 7
17:2 7
17:2 7
17:2 7
17:2 7
1
1
1
Comments : Lot #: C2B08025 9 Sampl e #: 4
Versio n 4.97.1 U Resul t is les s tha n th e MD L
B Resul t is betwee n MD L an d R L
Form 1 Equivalent
301 3
II
I STL-Pittsburg h
Metal s Data Reportin g For m
• Lab Sai nplelD: ETV8 G Clien t ID: NS-4 9
Matrix : Wate r Units : ug/L Prep Date: 2/12/0 2 Prep Batch: 2043299
1 Weigh t
1
1
1
1
1
1
: NA
Elemen t
Antimon y
Arseni c
Bariu m
Berylliu m
Chromiu m
Cobal t
Copper
Lead
Manganes e
Nicke l
Selenium
Thalliu m
Vanadiu m
Zinc
Volume : 50 Percen t Moisture: N A
WL/
Mass
206.8 4
189.0 4
493.41
313.04
267.72
228.62
324.75
220.35
257.61
231.60
220.3 5
190.86
292.40
206.2
MDL
4.1
2.2
0.14
0.40
1.1
0.84
2.5
1.8
0.47
2.4
3.2
5.7
1.5
3.7
Repor t
Limit
10.0
10.0
200
5.0
5.0
50.0
25.0
3.0
15.0
40.0
5.0
10.0
50.0
20.0
Cone
4.1
2.2
47.4
0.73
1.5
20.0
2.5
3.1
6270
4.8
3.2
5.7
1.8
44.6
0
Uu
B
B
B
B
U
B
U
U,;
B
L DF
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Instr
ICPS T
ICPS T
ICPST
ICPST
ICPS T
ICPS T
ICPS T
ICPST
ICPST
ICPST
ICPS T
ICPS T
ICPST
ICPS T
Anal
Date
2/18/0 2
2/18/0 2
2/18/02
2/18/02
2/18/02
2/18/02
2/18/0 2
2/18/02
2/18/02
2/18/02
2/18/0 2
2/18/0 2
2/18/02
2/18/02
Anal
Time
16:4 6
16:46
16:46
16:4 6
16:46
16:46
16:4 6
16:46
16:46
16:4 6
16:46
16:4 6
16:4 6
16:46
1
1
1
1
1
1
Comments : Lot #: C2B080259 Sampl e #: 3
Versio n 4.97.1 U Resul t is les s tha n th e MD L
B Resul t is betwee n MD L an d R L
Form I Equivalent
3012
1
1 STL-Pittsburgh
• Metal s Data Reportin g For m
Sample Result s
1 Lab Sai
Matrix:
1 Weigh t
1
1
1
1
1
1
1
nplelD: ETV8 E Clien t ID: NS-42
Wate r
NA
Elemen t
Antimon y
Arseni c
Barium
Berylliu m
Chromiu m
Cobalt
Copper
Lea d
Manganes e
Nicke l
Seleniu m
Thalliu m
Vanadiu m
Zinc
Units:ug/L Prei
Volume: 50 Perc
WL/
Mass
206.84
189.04
493.41
313.04
267.72
228.62
324.75
220.3 5
257.61
231.60
220.35
190.86
292.40
206.2
MDL
4.1
2.2
0.14
0.40
1.1
0.84
2.5
1.8
0.94
2.4
3.2
5.7
1.5
3.7
Report
Limi t
10.0
10.0
200
5.0
5.0
50.0
25.0
3.0
30.0
40.0
5.0
10.0
50.0
20.0
i Date :
ent Moistu
Cone
4.7
2.2
123
0.57
24.9
36.5
47.8
1.8
13200
34.1
3.6
5.7
13.2
12.4
2/12/0 2
re: NA
Prep Batch:
0
B
U
B
B
B
U
B
B
U
B
B
DF
1
1
1
1
1
1
1
1
2
1
1
:" 1
1
1
Inst r
ICPST
ICPS T
ICPST
ICPST
ICPST
ICPST
ICPSTrcpsr
ICPS T
ICPS T
ICPST
ICPS T
ICPST
ICPST
Anal
Date
2/18/02
2/18/02
2/18/02
2/18/02
2/18/02
2/18/02
2/18/02
2/18/02
2/19/02
2/18/02
2/18/02
2/18/0 2
2/18/02
2/18/02
2043299
Anal
Time
16:40
16:40
16:40
16:40
16:40
16:40
16:40
16:4 O
18:09
16:40
16:40
16:40
16:40
16:40
1
1
Comments : Lot #: C2BQ8025 9 Sampl e #: 2
Versio n 4.97.1 U Resul t is les s tha n th e MD L
B Resul t is betwee n MD L an d R L
Form 1 Equivalent
3011
1
• STL-Pittsburg h
• Metal s Data Reportin g For m
Sampl e Result s
• Lab Sai
Matrix:
1 Weigh t
1
1
1
1
1
1
1
nplelD: ETV8 A Client ID: NS-33
Water
: NA
Elemen t
Antimon y
Arseni c
Bariu m
Berylliu m
Chromiu m
Cobal t
Coppe r
Lead
Manganese
Nicke l
Selenium
Thalliu m
Vanadiu m
Zinc
Units:ug/L Prep Date:2/12/02
Volume: 50 Percent Moisture: NA
WL/
Mass
206.8 4
189.0 4
493.41
313.04
267.72
228.62
324.75
220.3 5
257.61
231.60
220.35
190.86
292.40
206.2
MD L
4.1
2.2
0.14
0.40
1.1
0.84
2.5
1.8
0.47
2.4
3.2
5.7
1.5
3.7
Report
Limit
10.0
10.0
200
5.0
5.0
50.0
25.0
3.0
15.0
40.0
5.0
10.0
50.0
20.0
Cone
4.1
2.2
22.3
0.73
3.8
0.84
2.5
1.8
3.1
6.1
3.2
5.7
21.3
3.7
Prep Batch:
9
uu
B
B
B
U
U
U
B
B
Uu...-
B
U
DF
1
I
1
1
1
1
1
1
1
1
1
I
1
1
Inst r
ICPS T
ICPS T
ICPS T
ICPS T
FCPS T
ICPS T
ICPS T
ICPS T
[CPST
ICPST
ICPS T
ICPS T
ICPST
ICPS T
Anal
Date
2/18/0 2
2/18/0 2
2/18/02
2/18/02
2/18/02
2/18/0 2
2/18/0 2
2/18/02
2/18/02
2/18/02
2718/02
2i '18/0 2
2/18/02
2/18/0 2
2043299
Anal
Time
16:33
16:33
16:33
16:33
16:33
16:33
16:33
16:33
16:33
16:33
16:33
16:33
16:33
16:33
1
1
1
Comments : Lo t fr. C2B0802S 9 Sampl e #: 1
Versio n 4.97.1 U Resul t is les s tha n ih c MD L
B Resul t is betwee n MD L and RL
Form I Equivalent
3010
II
I
I
I
I
I
III
I
I
I
STL-Pittsburg h
Metal s Dat a Reportin g For m
T "" "JP •
• Lab Sai
Matrix:
• Weigh t
1
1
mpl e ID :
Wate r
: NA
Elemen t
Mercury
ETV8K
Units :ug/L
Volume : 10 0
VfU
Mass
253.7
Client ID:EB-02070 2
Prep Date : 2/12/0 2 Pre p Batch: 2043172
Percent Moisture: NA
MDL
0.093
Report
Limit
0.20
Cone <
0.12 1
5 DF Inst r
3 1 CVA A
Anal Ana l
Date Tim e
2/12/02 18:41
Comments : Lot #: C2B0802S 9 Sampl e #: 6
Versio n 4.97.1 U Resul t is less tha n the MD L
B Resul t is betwee n MD L an d R L
Form I Equivalent
3O09
II
I
II
II
III
I
I
I
STL-Pittsburg h
Metal s Dat a Reportin g For m
Sampl e Result s
| Lab Sampl e ID:
Matrix :
1 Weigh t
1
•
Wate r
: NA
Elemen t
Mercur y
ETV8 J
Units :ug/L
Volume : 10 0
WL/
Mass
253.7
MDL
0.093
Client ID:
Prep Date :
DUP-9 0
2/12/0 2
Percen t Moisture:
Repor t
Limi t
0.2 0
Cone
0.093
Q
U
NA
DF In:
1 CV /
Prep Batch:
Ana l
;tr Date
^A 2/12/02
2043172
Ana l
Time
18:3 9
Comments : Lo t #: C2B08025 9 Sampl e #: 5
Versio n 4.97.1 U Resul t i s les s tha n th e MD L
B Resul t is betwee n MD L an d RL
Form I Equivalent
3008
II
I
I
I
I
IIIII
II
I
I
STL-Pittsburg h
Metal s Dat a Reportin g For m
Sampl e Result s
• Lab Sa
Matrix
1 Weigh t
1
•
rapl e ID:
Water
: NA
Elemen t
Mercury
ETV8 H
Units :ug/L
Volume : 10 0
WL/
Mass
253.7
MOL
0.093
Client ID:
Prep Date :
NS-39
2/12/02
Percent Moisture:
Repor t
Limit
0.2 0
Cone
0.13
0
B
NA
DF In:
1 CV>
Prep Batch:
Anal
tr Date
U. 2/12/0 2
2043172
Ana l
Tim e
18:38
Comments : Lot #: C2BQ8025 9 Sampl e #: 4
Versio n 4.97.1 U Resul t is les s tha n th e MD L
B Resul t is betwee n MD L an d RL
Form 1 Equivalent
3007
111Sample Result ^
• Lab Sampl e ID:
Matrix : Wate r
| Weight : NA
STL-Pittsburg h
Metal s Dat a Reportin g For m
ETV8 G Clien t ID : NS-49
Units : ug/L Pre p Date : 2/12/0 2 Pre p Batch: 2043172
Volume : 10 0 Percen t Moisture : N A
I Elemen t
Mercur y
wuMass
253.7
MDL
0.093
Repor t
Limi t
0.2 0
Cone
0.093
9
U
DF
1
Inst r
CVA A
Anal
Date
2/12/02
Ana l
Tim e
18:33
Comments : Lot#: C2B08025 9 Sampled : 3
Versio n 4.97.1 U Resul t i s les s tha n th e MD L
B Resul t is betwee n MD L an d R L
Form 1 Equivalent
3O06
III
I
I
I
I
I
IIII
I
III
STL-Pittsburg h
Metal s Dat a Reportin g For m
Samole Results
1 Lab Sai
Matrix
I Weigh t
1
n
mpl e ID :
Wate r
: NA
Elemen t
Mercury
ETV8 E
Units :ug/L
Volume : 10 0
WL/
Mass
253.7
MDL
0.093
Client ID:
Prep Date:
NS-42
2/12/02
Percent Moisture:
Repor t
Limi t
0.20
Cone
0.098
0
B
NA
DF In:
1 CW
Prep Batch:
Anal
itr Date
\A 2/12/02
2043172
Ana l
Time
18:3 2
Comments : Lo t #: C2B0802S9 Sampl e tf: 2
Version 4.97.1 U Resul t is les s tha n th e MD L
B Resul t is betwee n MD L an d RL
Form I Equivalent
30O5
IIII
III
I
I
IIIIIfI
STL-Pittsburg h
Metal s Dat a Reportin g For m
Lab Sampl e ID:
Matrix :
Weight :
Wate r
NA
ETV8 A
Units :
Volume :
ug/L
10 0
Client ID: NS-3 3
Prep Date : 2/12/0 2
Percen t Moisture : N A
Prep Batch: 2043172
Element
Mercur y
WL /
Mass
253.7
MDL
0.093
Repor t
Limi t
0.2 0
Cone
0.093
o
U
DF
1
Inst r
CVA A
Ana l
Date
2/12/02
Anal
L Time
18:3 0
Comments : Lo t #: C2B080259 Sampl e #: 1
1 Versio n 4.97.1
QTT . P-i
U Resul t is les s tha n th e MD L
B Resul t i s betwee n MD L an d R L
Form I Equivalent
3004